Sample records for ac magnetic susceptibilities

  1. Characterizing superconducting thin films using AC Magnetic Susceptibility

    NASA Astrophysics Data System (ADS)

    Mahoney, C. H.; Porzio, J.; Sullivan, M. C.

    2014-03-01

    We present our work on using ac magnetic susceptibility to determine the critical temperature of superconducting thin films. In ac magnetic susceptibility, the thin film is placed between two coils. One coil carries an ac signal, creating a varying external magnetic field. We measure the voltage induced in the pick-up coil on the opposite side of the sample and measure how the sample magnetization changes as the temperature changes. We will present our work to use ac susceptibility to determine critical temperature and superconducting volume fraction. Using our own analysis program, we are able to accurately locate the critical temperatures of the samples and determine the transition width. For the superconducting volume fraction, we etch samples in order to control the thicknesses of the sample and measure how much of the material grown on the surface is superconducting. Supported by NFS grant DMR-1305637.

  2. Spectroscopic AC Susceptibility Imaging (sASI) of Magnetic Nanoparticles

    PubMed Central

    Ficko, Bradley W.; Nadar, Priyanka M.; Diamond, Solomon G.

    2014-01-01

    This study demonstrates a method for alternating current (AC) susceptibility imaging (ASI) of magnetic nanoparticles (mNPs) using low cost instrumentation. The ASI method uses AC magnetic susceptibility measurement to create tomographic images using an array of drive coils, compensation coils and fluxgate magnetometers. Using a spectroscopic approach in conjunction with ASI, a series of tomographic images can be created for each frequency measurement and is termed sASI. The advantage of sASI is that mNPs can be simultaneously characterized and imaged in a biological medium. System calibration was performed by fitting the in-phase and out-of-phase susceptibility measurements of an mNP sample with a hydrodynamic diameter of 100 nm to a Brownian relaxation model (R2 = 0.96). Samples of mNPs with core diameters of 10 and 40 nm and a sample of 100 nm hydrodynamic diameter were prepared in 0.5 ml tubes. Three mNP samples were arranged in a randomized array and then scanned using sASI with six frequencies between 425 and 925 Hz. The sASI scans showed the location and quantity of the mNP samples (R2 = 0.97). Biological compatibility of the sASI method was demonstrated by scanning mNPs that were injected into a pork sausage. The mNP response in the biological medium was found to correlate with a calibration sample (R2 = 0.97, p <0.001). These results demonstrate the concept of ASI and advantages of sASI. PMID:25477704

  3. Superconductor disks and cylinders in an axial magnetic field: II. Nonlinear and linear ac susceptibilities

    NASA Astrophysics Data System (ADS)

    Brandt, Ernst Helmut

    1998-09-01

    The ac susceptibility χ=χ'-iχ'' of superconductor cylinders of finite length in a magnetic field applied along the cylinder axis is calculated using the method developed in the preceding paper, part I. This method does not require any approximation of the infinitely extended magnetic field outside the cylinder or disk but directly computes the current density J inside the superconductor. The material is characterized by a general current-voltage law E(J), e.g., E(J)=Ec[J/Jc(B)]n(B), where E is the electric field, B=μ0H the magnetic induction, Ec a prefactor, Jc the critical current density, and n>=1 the creep exponent. For n>1, the nonlinear ac susceptibility is calculated from the hysteresis loops of the magnetic moment of the cylinder, which is obtained by time integration of the equation for J(r,t). For n>>1 these results go over into the Bean critical state model. For n=1, and for any linear complex resistivity ρac(ω)=E/J, the linear ac susceptibility is calculated from an eigenvalue problem which depends on the aspect ratio b/a of the cylinder or disk. In the limits b/a<<1 and b/a>>1, the known results for thin disks in a perpendicular field and long cylinders in a parallel field are reproduced. For thin disks in a perpendicular field, at large frequencies χ(ω) crosses over to the behavior of slabs in parallel geometry since the magnetic field lines are expelled and have to flow around the disk. The results presented may be used to obtain the nonlinear or linear resistivity from contact-free magnetic measurements on superconductors of realistic shape.

  4. Magnetic relaxation phenomena in the chiral magnet Fe1 -xCoxSi : An ac susceptibility study

    NASA Astrophysics Data System (ADS)

    Bannenberg, L. J.; Lefering, A. J. E.; Kakurai, K.; Onose, Y.; Endoh, Y.; Tokura, Y.; Pappas, C.

    2016-10-01

    We present a systematic study of the ac susceptibility of the chiral magnet Fe1 -xCoxSi with x =0.30 covering four orders of magnitude in frequencies from 0.1 Hz to 1 kHz, with particular emphasis to the pronounced history dependence. Characteristic relaxation times ranging from a few milliseconds to tens of seconds are observed around the skyrmion lattice A phase, the helical-to-conical transition and in a region above TC. The distribution of relaxation frequencies around the A phase is broad, asymmetric, and originates from multiple coexisting relaxation processes. The pronounced dependence of the magnetic phase diagram on the magnetic history and cooling rates as well as the asymmetric frequency dependence and slow dynamics suggest more complicated physical phenomena in Fe0.7Co0.3Si than in other chiral magnets.

  5. Nonlinear AC susceptibility, surface and bulk shielding

    NASA Astrophysics Data System (ADS)

    van der Beek, C. J.; Indenbom, M. V.; D'Anna, G.; Benoit, W.

    1996-02-01

    We calculate the nonlinear AC response of a thin superconducting strip in perpendicular field, shielded by an edge current due to the geometrical barrier. A comparison with the results for infinite samples in parallel field, screened by a surface barrier, and with those for screening by a bulk current in the critical state, shows that the AC response due to a barrier has general features that are independent of geometry, and that are significantly different from those for screening by a bulk current in the critical state. By consequence, the nonlinear (global) AC susceptibility can be used to determine the origin of magnetic irreversibility. A comparison with experiments on a Bi 2Sr 2CaCu 2O 8+δ crystal shows that in this material, the low-frequency AC screening at high temperature is mainly due to the screening by an edge current, and that this is the unique source of the nonlinear magnetic response at temperatures above 40 K.

  6. Field-dependence of AC susceptibility in titanomagnetites

    USGS Publications Warehouse

    Jackson, M.; Moskowitz, B.; Rosenbaum, J.; Kissel, Catherie

    1998-01-01

    AC susceptibility measurements as a function of field amplitude Hac and of frequency show a strong field dependence for a set of synthetic titanomagnetites (Fe3-xTixO4) and for certain basalts from the SOH-1 Hawaiian drill hole and from Iceland. In-phase susceptibility is constant below fields of about 10-100 A/m, and then increases by as much as a factor of two as Hsc is increased to 2000 A/m. Both the initial field-independent susceptibilities and field-dependence of susceptibility are systematically related to composition: initial susceptibility is 3 SI for a single-crystal sphere of TMO (x = 0) and decreases with increasing titanium content; field-dependence is nearly zero for TM0 and increases systematically to a maximum near TM60 (x = 0.6). This field dependence can in some cases be mistaken for frequency dependence, and leaf to incorrect interpretations of magnetic grain size and composition when titanomagnetite is present.

  7. Effect of molecule-particle binding on the reduction in the mixed-frequency alternating current magnetic susceptibility of magnetic bio-reagents

    NASA Astrophysics Data System (ADS)

    Yang, C. C.; Yang, S. Y.; Chen, H. H.; Weng, W. L.; Horng, H. E.; Chieh, J. J.; Hong, C. Y.; Yang, H. C.

    2012-07-01

    By specifically bio-functionalizing magnetic nanoparticles, magnetic nanoparticles are able to label target bio-molecules. This property can be applied to quantitatively detect molecules invitro by measuring the related magnetic signals of nanoparticles bound with target molecules. One of the magnetic signals is the reduction in the mixed-frequency ac magnetic susceptibility of suspended magnetic nanoparticles due to the molecule-particle association. Many experimental results show empirically that the molecular-concentration dependent reduction in ac magnetic susceptibility follows the logistic function. In this study, it has been demonstrated that the logistic behavior is originated from the growth of particle sizes due to the molecule-particle association. The analytic relationship between the growth of particle sizes and the reduction in ac magnetic susceptibility is developed.

  8. AC magnetic-field response of the ferromagnetic superconductor UGe2 with different magnetized states

    NASA Astrophysics Data System (ADS)

    Tanaka, Hiroyuki; Yamaguchi, Akira; Kawasaki, Ikuto; Sumiyama, Akihiko; Motoyama, Gaku; Yamamura, Tomoo

    2018-01-01

    We have performed parallel measurements of dc-magnetization and ac-magnetic susceptibility for a ferromagnetic superconductor, UGe2, in the ferromagnetic-superconducting phase. dc-magnetization measurements revealed that adequate demagnetizing of the sample allows for the preparation of various magnetized states with different zero-field residual magnetization. We observed that these states exhibit varying ac superconducting response at large ac-field amplitudes. The amount of ac flux penetration is less in the demagnetized state involving many domain walls. This result seems to contradict the theory that considers the domain walls as weak links. Moreover, the ferromagnetic domain walls enforce the shielding capability of superconductivity. This observation sheds light on the role of the domain walls on superconductivity, which has been a controversial issue for several decades. Two possible scenarios are presented to explain the enhancement of the shielding capability by the domain walls.

  9. Nonlinear susceptibility and dynamic hysteresis loops of magnetic nanoparticles with biaxial anisotropy

    NASA Astrophysics Data System (ADS)

    Ouari, Bachir; Titov, Serguey V.; El Mrabti, Halim; Kalmykov, Yuri P.

    2013-02-01

    The nonlinear ac susceptibility and dynamic magnetic hysteresis (DMH) of a single domain ferromagnetic particle with biaxial anisotropy subjected to both external ac and dc fields of arbitrary strength and orientation are treated via Brown's continuous diffusions model [W. F. Brown, Jr., Phys. Rev. 130, 1677 (1963)] of magnetization orientations. The DMH loops and nonlinear ac susceptibility strongly depend on the dc and ac field strengths, the polar angle between the easy axis of the particle, the external field vectors, temperature, and damping. In contrast to uniaxial particles, the nonlinear ac stationary response and DMH strongly depend on the azimuthal direction of the ac field and the biaxiality parameter Δ.

  10. Third harmonic ac susceptibility of superconductors with finite thickness

    NASA Astrophysics Data System (ADS)

    Qin, M. J.; Ong, C. K.

    Third harmonic ac susceptibility of superconducting strips with finite thickness in perpendicularly applied magnetic field Ha = H0 sin(ω t) have been calculated. The flux creep effect is taken into account by using a power-law electric field E( j) = Ec( j/ jc) n. Results for different thicknesses and creep exponents n have been derived and compared to the results derived from the Bean critical state model.

  11. Dynamic magnetic hysteresis and nonlinear susceptibility of antiferromagnetic nanoparticles

    NASA Astrophysics Data System (ADS)

    Kalmykov, Yuri P.; Ouari, Bachir; Titov, Serguey V.

    2016-08-01

    The nonlinear ac stationary response of antiferromagnetic nanoparticles subjected to both external ac and dc fields of arbitrary strength and orientation is investigated using Brown's continuous diffusion model. The nonlinear complex susceptibility and dynamic magnetic hysteresis (DMH) loops of an individual antiferromagnetic nanoparticle are evaluated and compared with the linear regime for extensive ranges of the anisotropy, the ac and dc magnetic fields, damping, and the specific antiferromagnetic parameter. It is shown that the shape and area of the DMH loops of antiferromagnetic particles are substantially altered by applying a dc field that permits tuning of the specific magnetic power loss in the nanoparticles.

  12. Effect of Cr3+ substitution on AC susceptibility of Ba hexaferrite nanoparticles

    NASA Astrophysics Data System (ADS)

    Slimani, Y.; Baykal, A.; Manikandan, A.

    2018-07-01

    In this study, nano-sized particles of BaCrxFe12-xO19 (0.0 ≤ x ≤ 1.0) hexaferrite were fabricated through citrate auto gel combustion process and the impact of Cr-ion substitution on ac magnetic susceptibility properties of Ba-hexaferrite were explored. X-ray powder diffraction (XRD) measurements approved the purity of prepared samples and showed a reduction of the average crystallite size with increasing the content of Cr. Transmission electron microscopy (TEM) observation indicated the hexagonal morphology of all samples. AC susceptibility measurements displayed a frequency dependence of the magnetic responses. These measurements indicated that there are strong magnetic interactions (which is the highest for BaCr0.3Fe11.7O19 NP) between particles which cause a superspin glass-like (SSG) behavior at low temperatures. Estimating the values of loss power density revealed an increase of loss power density with increasing Cr-substitution element. The relative sensitivity of the prepared MNPs to the variation of applied frequency is very influenced by Cr-substitution and is highest in BaCr0.3Fe11.7O19 MNPs, suggesting that this sample can be considered as magnetic nanomaterial for hyperthermia and for many other applications.

  13. Influence of the interaction between the inter- and intragranular magnetic responses in the analysis of the ac susceptibility of a granular FeSe0.5Te0.5 superconductor

    NASA Astrophysics Data System (ADS)

    Mancusi, D.; Polichetti, M.; Cimberle, M. R.; Pace, S.

    2015-09-01

    The temperature-dependent fundamental ac susceptibility of a granular superconductor in the absence of dc fields has been analyzed by developing a phenomenological model for effective magnetic fields, taking into account the influence of the magnetic interaction between the intergranular and the intragranular magnetizations due to demagnetizing effects. For this purpose a policrystal Fe-based superconductor FeSe0.5Te0.5 sample has been studied. By the frequency dependence of the peaks of the temperature-dependent imaginary part of the fundamental complex susceptibility, the dependence on temperature of the characteristic times both for intergranular and intragranular relaxations of magnetic flux are derived, and the corresponding relaxation processes due to combinations of the flux creep, the flux flow and the thermally activated flux flow regimes are identified on the basis of the effective magnetic fields both at the sample surface and at the grains’ surfaces. Such characteristic times, through the Havriliak-Negami function, determine the temperature and the frequency dependences of the complex susceptibility. The comparison of the numerically obtained curves with the experimental ones confirms the relevance, for identifying the intergranular and intragranular contributions to the ac magnetic response and the corresponding flux dynamical regimes, of the interaction between the intergranular and intragranular magnetizations due to demagnetizing effects.

  14. Improvement of immunoassay detection system by using alternating current magnetic susceptibility

    NASA Astrophysics Data System (ADS)

    Kawabata, R.; Mizoguchi, T.; Kandori, A.

    2016-03-01

    A major goal with this research was to develop a low-cost and highly sensitive immunoassay detection system by using alternating current (AC) magnetic susceptibility. We fabricated an improved prototype of our previously developed immunoassay detection system and evaluated its performance. The prototype continuously moved sample containers by using a magnetically shielded brushless motor, which passes between two anisotropic magneto resistance (AMR) sensors. These sensors detected the magnetic signal in the direction where each sample container passed them. We used the differential signal obtained from each AMR sensor's output to improve the signal-to-noise ratio (SNR) of the magnetic signal measurement. Biotin-conjugated polymer beads with avidin-coated magnetic particles were prepared to examine the calibration curve, which represents the relation between AC magnetic susceptibility change and polymer-bead concentration. For the calibration curve measurement, we, respectively, measured the magnetic signal caused by the magnetic particles by using each AMR sensor installed near the upper or lower part in the lateral position of the passing sample containers. As a result, the SNR of the prototype was 4.5 times better than that of our previous system. Moreover, the data obtained from each AMR sensor installed near the upper part in the lateral position of the passing sample containers exhibited an accurate calibration curve that represented good correlation between AC magnetic susceptibility change and polymer-bead concentration. The conclusion drawn from these findings is that our improved immunoassay detection system will enable a low-cost and highly sensitive immunoassay.

  15. Improvement of immunoassay detection system by using alternating current magnetic susceptibility.

    PubMed

    Kawabata, R; Mizoguchi, T; Kandori, A

    2016-03-01

    A major goal with this research was to develop a low-cost and highly sensitive immunoassay detection system by using alternating current (AC) magnetic susceptibility. We fabricated an improved prototype of our previously developed immunoassay detection system and evaluated its performance. The prototype continuously moved sample containers by using a magnetically shielded brushless motor, which passes between two anisotropic magneto resistance (AMR) sensors. These sensors detected the magnetic signal in the direction where each sample container passed them. We used the differential signal obtained from each AMR sensor's output to improve the signal-to-noise ratio (SNR) of the magnetic signal measurement. Biotin-conjugated polymer beads with avidin-coated magnetic particles were prepared to examine the calibration curve, which represents the relation between AC magnetic susceptibility change and polymer-bead concentration. For the calibration curve measurement, we, respectively, measured the magnetic signal caused by the magnetic particles by using each AMR sensor installed near the upper or lower part in the lateral position of the passing sample containers. As a result, the SNR of the prototype was 4.5 times better than that of our previous system. Moreover, the data obtained from each AMR sensor installed near the upper part in the lateral position of the passing sample containers exhibited an accurate calibration curve that represented good correlation between AC magnetic susceptibility change and polymer-bead concentration. The conclusion drawn from these findings is that our improved immunoassay detection system will enable a low-cost and highly sensitive immunoassay.

  16. Vortex dynamics and irreversibility line in optimally doped SmFeAsO0.8F0.2 from ac susceptibility and magnetization measurements

    NASA Astrophysics Data System (ADS)

    Prando, G.; Carretta, P.; de Renzi, R.; Sanna, S.; Palenzona, A.; Putti, M.; Tropeano, M.

    2011-05-01

    Ac susceptibility and static magnetization measurements were performed in the optimally doped SmFeAsO0.8F0.2 superconductor. The field-temperature phase diagram of the superconducting state was drawn, and, in particular, the features of the flux lines were derived. The dependence of the intragrain depinning energy on the magnetic field intensity was derived in the thermally activated flux-creep framework, enlightening a typical 1/H dependence in the high-field regime. The intragrain critical current density was extrapolated in the zero-temperature and zero-magnetic-field limit, showing a remarkably high value Jc0(0)~2×107 A/cm2, which demonstrates that this material is rather interesting for potential future technological applications.

  17. 21 CFR 886.4440 - AC-powered magnet.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 21 Food and Drugs 8 2010-04-01 2010-04-01 false AC-powered magnet. 886.4440 Section 886.4440 Food... DEVICES OPHTHALMIC DEVICES Surgical Devices § 886.4440 AC-powered magnet. (a) Identification. An AC-powered magnet is an AC-powered device that generates a magnetic field intended to find and remove...

  18. Magnetic susceptibility of Inconel alloys 718, 625, and 600 at cryogenic temperatures

    NASA Technical Reports Server (NTRS)

    Goldberg, Ira B.; Mitchell, Michael R.; Murphy, Allan R.; Goldfarb, Ronald B.; Loughran, Robert J.

    1990-01-01

    After a hydrogen fuel bleed valve problem on the Discovery Space Shuttle was traced to the strong magnetization of Inconel 718 in the armature of the linear variable differential transformer near liquid hydrogen temperatures, the ac magnetic susceptibility of three samples of Inconel 718 of slightly different compositions, one sample of Inconel 625, and on sample of Inconel 600 were measured as a function of temperature. Inconel 718 alloys are found to exhibit a spin glass state below 16 K. Inconel 600 exhibits three different magnetic phases, the lowest-temperature state (below 6 K) being somewhat similar to that of Inconel 718. The magnetic states of the Inconel alloys and their magnetic susceptibilities appear to be strongly dependent on the exact composition of the alloy.

  19. Vortex flux dynamics and harmonic ac magnetic response of Ba(Fe 0.94Ni 0.06) 2As 2 bulk superconductor

    DOE PAGES

    Nikolo, Martin; Zapf, Vivien S.; Singleton, John; ...

    2016-07-22

    Vortex dynamics and nonlinear ac response are studied in a Ba(Fe 0.94Ni 0.06) 2As 2( T c= 18.5 K) bulk superconductor in magnetic fields up to 12 T via ac susceptibility measurements of the first ten harmonics. A comprehensive study of the ac magnetic susceptibility and its first ten harmonics finds shifts to higher temperatures with increasing ac measurement frequencies (10 to 10,000 Hz) for a wide range of ac (1, 5, and 10 Oe) and dc fields (0 to 12 T). The characteristic measurement time constant t1 is extracted from the exponential fit of the data and linked tomore » vortex relaxation. The Anderson-Kim Arrhenius law is applied to determine flux activation energy E a/k as a function dc magnetic field. The de-pinning, or irreversibility lines, were determined by a variety of methods and extensively mapped. The ac response shows surprisingly weak higher harmonic components, suggesting weak nonlinear behavior. Lastly, our data does not support the Fisher model; we do not see an abrupt vortex glass to vortex liquid transition and the resistivity does not drop to zero, although it appears to approach zero exponentially.« less

  20. Magnetic nanobeads present during enzymatic amplification and labeling for a simplified DNA detection protocol based on AC susceptometry

    NASA Astrophysics Data System (ADS)

    Bejhed, Rebecca S.; Strømme, Maria; Svedlindh, Peter; Ahlford, Annika; Strömberg, Mattias

    2015-12-01

    Magnetic biosensors are promising candidates for low-cost point-of-care biodiagnostic devices. For optimal efficiency it is crucial to minimize the time and complexity of the assay protocol including target recognition, amplification, labeling and read-out. In this work, possibilities for protocol simplifications for a DNA biodetection principle relying on hybridization of magnetic nanobeads to rolling circle amplification (RCA) products are investigated. The target DNA is recognized through a padlock ligation assay resulting in DNA circles serving as templates for the RCA process. It is found that beads can be present during amplification without noticeably interfering with the enzyme used for RCA (phi29 polymerase). As a result, the bead-coil hybridization can be performed immediately after amplification in a one-step manner at elevated temperature within a few minutes prior to read-out in an AC susceptometer setup, i.e. a combined protocol approach. Moreover, by recording the phase angle ξ = arctan(χ″/χ'), where χ and χ″ are the in-phase and out-of-phase components of the AC susceptibility, respectively, at one single frequency the total assay time for the optimized combined protocol would be no more than 1.5 hours, often a relevant time frame for diagnosis of cancer and infectious disease. Also, applying the phase angle method normalization of AC susceptibility data is not needed. These findings are useful for the development of point-of-care biodiagnostic devices relying on bead-coil binding and magnetic AC susceptometry.

  1. Mg shallow doping effects on the ac magnetic self-heating characteristics of γ-Fe2O3 superparamagnetic nanoparticles for highly efficient hyperthermia

    NASA Astrophysics Data System (ADS)

    Jang, Jung-tak; Bae, Seongtae

    2017-10-01

    The effects of Mg doping on the magnetic and AC self-heating temperature rising characteristics of γ-Fe2O3 superparamagnetic nanoparticles (SPNPs) were investigated for hyperthermia applications in biomedicine. The doping concentration of nonmagnetic Mg2+ cation was systematically controlled from 0 to 0.15 at. % in Mgx-γFe2O3 SPNPs during chemically and thermally modified one-pot thermal decomposition synthesis under bubbling O2/Ar gas mixture. It was empirically observed that the saturation magnetization (Ms) and the out-of-phase magnetic susceptibility ( χm″)of Mgx-γFe2O3 SPNPs were increased by increasing the Mg2+ cation doping concentration from 0.05 to 0.13 at. %. Correspondingly, the AC magnetically induced self-heating temperature (Tac,max) in solid state and the intrinsic loss power in water were increased up to 184 °C and 14.2 nH m2 kg-1 (Mgx-γFe2O3, x = 0.13), respectively, at the biologically and physiologically safe range of AC magnetic field (Happl × fappl = 1.2 × 109 A m-1 s-1). All the chemically and physically analyzed results confirmed that the dramatically improved AC magnetic induction heating characteristics and the magnetic properties of Mgx-γFe2O3 SPNPs (x = 0.13) are primarily due to the significantly enhanced magnetic susceptibility (particularly, χm″) and the improved AC/DC magnetic softness (lower AC/DC magnetic anisotropy) resulting from the systematically controlled nonmagnetic Mg2+ cation concentrations and distributions (occupation ratio) in the Fe vacancy sites of γ-Fe2O3 (approximately 12% vacancy), instead of typically well-known Fe3O4 (no vacancy) SPNPs. The cell viability and biocompatibility with U87 MG cell lines demonstrated that Mgx-γFe2O3 SPNPs (x = 0.13) has promising bio-feasibility for hyperthermia agent applications.

  2. A magnetic-piezoelectric smart material-structure sensing three axis DC and AC magnetic-fields

    NASA Astrophysics Data System (ADS)

    Hung, Chiao-Fang; Chen, Chin-Chung; Yeh, Po-Chen; Chen, Po-Wen; Chung, Tien-Kan

    2017-12-01

    In this paper, we demonstrate a smart material-structure can sense not only three-axis AC magnetic-fields but also three-axis DC magnetic-fields. Under x-axis and z-axis AC magnetic field ranging from 0.2 to 3.2 gauss, sensing sensitivity of the smart material-structure stimulated at resonant frequency is approximate 8.79 and 2.80 mV/gauss, respectively. In addition, under x-axis and z-axis DC magnetic fields ranging from 2 to 12 gauss, the sensitivity of the smart material-structure is 1.24-1.54 and 1.25-1.41 mV/gauss, respectively. In addition, under x-axis and z-axis DC magnetic fields ranging from 12 to 20 gauss, the sensitivity of the smart material-structure is 5.17-6.2 and 3.97-4.57 mV/gauss, respectively. These experimental results show that the smart material-structure successfully achieves three-axis DC and AC magnetic sensing as we designed. Furthermore, we also compare the results of the AC and DC magnetic-field sensing to investigate discrepancies. Finally, when applying composite magnetic-fields to the smart material-structure, the smart material-structure shows decent outputs as expected (consistent to the sensing principle). In the future, we believe the smart material-structure capable of sensing AC and DC magnetic fields will have more applications than conventional structures capable of sensing only DC or AC magnetic field. Thus, the smart material-structure will be an important design reference for future magnetic-field sensing technologies.

  3. Separation of magnetic susceptibility components from magnetization curves

    NASA Astrophysics Data System (ADS)

    Kosareva, L.; Nourgaliev, D.; Kuzina, D.; Spassov, S.; Fattakhov, A.

    2014-12-01

    Modern lake sediments are a unique source of information for climate changes, regionally and globally, because all environmental variations are recorded by these sediments with high resolution. The magnetic properties of Chernyshov Bay (Aral Sea) sediments we investigated from core number 4 (N45o57'04.2''; E59o17'14.3'') are taken at far water depth of 9.5 m. The length of the core is 4.16 m. Samples for measurements were taken to plastic sample boxes with internal dimensions 2x2x2 cm. Remanent magnetization curves were measured by coercivity spectrometer for the separate determination of the different contributions to the total bulk magnetic susceptibility. There was measured also magnetic susceptibility using MS2 susceptibility meter. Those operations were done for data comparison between 2 susceptibilities obtained from different equipment. Our goal is to decipher the magnetic susceptibility signal in lake sediments by decomposing the bulk susceptibility signal of a lake sediment sequence into ferromagnetic (χf), dia-/paramagnetic (χp) and superparamagnetic (χsp) components using data from remanent and indused magnetization curves Each of these component has a different origin: paramagnetic minerals are usually attributed to terrigenous sediment input, ferromagnetics are of biogenic origin, and superparamagnetic minerals may be of either biogenic or terrigenous origin. Comparison between susceptibility measurements of MS2-Bartington susceptometer and of the coercivity spectrometer has shown good correlation. The susceptibility values measured in two different equipment are fairly close and indicate thus the reliability the proposed method. In research also has shown water level changes in Aral Sea based on magnetic susceptibility. The work is performed according to the Russian Government Program of Competitive Growth of Kazan Federal University also by RFBR research projects No. 14-05-31376 - а, 14-05-00785- а.

  4. Complex magnetic susceptibility setup for spectroscopy in the extremely low-frequency range.

    PubMed

    Kuipers, B W M; Bakelaar, I A; Klokkenburg, M; Erné, B H

    2008-01-01

    A sensitive balanced differential transformer was built to measure complex initial parallel magnetic susceptibility spectra in the 0.01-1000 Hz range. The alternating magnetic field can be chosen sufficiently weak that the magnetic structure of the samples is only slightly perturbed and the low frequencies make it possible to study the rotational dynamics of large magnetic colloidal particles or aggregates dispersed in a liquid. The distinguishing features of the setup are the novel multilayered cylindrical coils with a large sample volume and a large number of secondary turns (55 000) to measure induced voltages with a good signal-to-noise ratio, the use of a dual channel function generator to provide an ac current to the primary coils and an amplitude- and phase-adjusted compensation voltage to the dual phase differential lock-in amplifier, and the measurement of several vector quantities at each frequency. We present the electrical impedance characteristics of the coils, and we demonstrate the performance of the setup by measurement on magnetic colloidal dispersions covering a wide range of characteristic relaxation frequencies and magnetic susceptibilities, from chi approximately -10(-5) for pure water to chi>1 for concentrated ferrofluids.

  5. Active magnetic force microscopy of Sr-ferrite magnet by stimulating magnetization under an AC magnetic field: Direct observation of reversible and irreversible magnetization processes

    NASA Astrophysics Data System (ADS)

    Cao, Yongze; Kumar, Pawan; Zhao, Yue; Yoshimura, Satoru; Saito, Hitoshi

    2018-05-01

    Understanding the dynamic magnetization process of magnetic materials is crucial to improving their fundamental properties and technological applications. Here, we propose active magnetic force microscopy for observing reversible and irreversible magnetization processes by stimulating magnetization with an AC magnetic field based on alternating magnetic force microscopy with a sensitive superparamagnetic tip. This approach simultaneously measures sample's DC and AC magnetic fields. We used this microscopy approach to an anisotropic Sr-ferrite (SrF) sintered magnet. This is a single domain type magnet where magnetization mainly changes via magnetic rotation. The proposed method can directly observe the reversible and irreversible magnetization processes of SrF and clearly reveal magnetic domain evolution of SrF (without stimulating magnetization—stimulating reversible magnetization—stimulating irreversible magnetization switching) by slowly increasing the amplitude of the external AC magnetic field. This microscopy approach can evaluate magnetic inhomogeneity and explain the local magnetic process within the permanent magnet.

  6. AC magnetic field measurement using a small flip coil system for rapid cycling AC magnets at the China Spallation Neutron Source (CSNS)

    NASA Astrophysics Data System (ADS)

    Zhou, Jianxin; Kang, Wen; Li, Shuai; Liu, Yudong; Liu, Yiqin; Xu, Shouyan; Guo, Xiaoling; Wu, Xi; Deng, Changdong; Li, Li; Wu, Yuwen; Wang, Sheng

    2018-02-01

    The China Spallation Neutron Source (CSNS) has two major accelerator systems, a linear accelerator and a rapid cycling synchrotron (RCS). The RCS accelerator is used to accumulate and accelerate protons from the energy of 80 MeV to the design energy of 1.6 GeV at the repetition rate of 25 Hz, and extract the high energy beam to the target. The main magnets of the RCS accelerator are excited by AC current with DC bias. The magnetic field quality is very important for the RCS accelerator operation, since it should guarantee and focus a circulating beam. In order to characterize the AC magnets, a small flip coil measurement system has been developed and one of each type of AC magnets has been studied. The measurement system and selected measurement results are presented in this paper.

  7. Effects of head field and AC field on magnetization reversal for microwave assisted magnetic recording

    NASA Astrophysics Data System (ADS)

    Kase, Aina; Akagi, Fumiko; Yoshida, Kazuetsu

    2018-05-01

    Microwave assisted magnetic recording (MAMR) is a promising recording method for achieving high recording densities in hard disk drives. In MAMR, the AC field from a spin-torque oscillator (STO) assists the head field with magnetization reversal in a medium. Therefore, the relationship between the head field and the AC field is very important. In this study, the effects of the head field and the AC field on magnetization reversal were analyzed using a micromagnetic simulator that takes the magnetic interactions between a single-pole type (SPT) write-head, an exchange coupled composite (ECC) medium, and the STO into account. As a result, the magnetization reversal was assisted not just by the y-component of the AC field (Hstoy) but also by the y-component of the head field (Hhy) in the medium. The Hhy over 100 kA/m with a frequency of about 15.5 GHz induced the magnetic resonance. The large Hhy was produced by the field from the STO to the SPT head.

  8. Magnetic characteristics and AC losses of DC type-II superconductors under oscillating magnetic fields

    NASA Astrophysics Data System (ADS)

    Robert, B. C.; Ruiz, H. S.

    2018-07-01

    Remarkable features on the magnetic moment of type-II superconducting (SC) wires of cylindrical shape, subjected to direct current conditions (DC) and transverse oscillating (AC) magnetic fields, are reported. We show how for relatively low amplitudes of the applied magnetic field, B a , the superconducting wire rapidly develops a saturation state, | {M}p| , characterizing the limits of magnetization loops that exhibit a Boolean-like behaviour. Regardless of the premagnetization state of the SC wire, we show how after two cycles of magnetic relaxation, boolean-like ±M p states can be measured during the entire period of time from which the external magnetic field B 0 ranges from 0 to ±B a , with the signs rule defined by the sign of the slope ΔB 0y (t). In addition, for the practical implementation of SC DC wires sharing the right of way with AC lines, we report that for relatively low values of magnetic field, {B}a≤slant {B}P/2, being B P the analytical value for the full penetration field in absence of transport current, I tr, the use of semi-analytical approaches for the calculation of AC losses leads to a significant underestimation of the actual contribution of the induction losses. This phenomena is particularly relevant at dimensionless fields {b}a< 1-{i}a2/3, being b a = B a /B P and, i a = I a /I c the amplitude of an AC or DC transport current, due to the local motion of flux front profiles being dominated by the occurrence of transport current. On the other hand, we have found that regardless of the nature of the transport current, either be DC or AC, when a transverse oscillating magnetic field greater than the classical limit b a = (1 - i a ) is applied to the SC wire, the difference between the obtained AC losses in both situations results to be negligible indistinctly of the approach used, semi-analytical or numerical. Thus, the actual limits from which the estimation of the AC losses can be used as an asset for the deployment of DC SC wires

  9. Specific heat and magnetic susceptibility of CeNiSn doped with Rh.

    PubMed

    Slebarski, A; Maple, M B; Fijałkowski, M; Goraus, J

    2010-04-28

    CeNiSn is known as a semimetallic system with a small pseudogap at the Fermi energy. We investigate the effect of Rh doping on the Kondo insulator CeNiSn by means of measurements of ac magnetic susceptibility and specific heat. We show that the formation of the Kondo insulator narrow gap in CeNi(1 - x)Rh(x)Sn is associated with disorder-induced f-electron localization. For doped CeNiSn with x ≤ 0.06, the electrical resistivity data follow an activation and variable range hopping behaviour at low T, consistent with weak disorder and localization, while C/T is large, which is not a common feature of Kondo insulators. For x > 0.06, the system is metallic and exhibits non-Fermi liquid behaviour with magnetic susceptibility χ ∼ T( - n) with n ∼ 0.4 and electrical resistivity ρ ∼ T.

  10. Magnetic susceptibility characterisation of superparamagnetic microspheres

    NASA Astrophysics Data System (ADS)

    Grob, David Tim; Wise, Naomi; Oduwole, Olayinka; Sheard, Steve

    2018-04-01

    The separation of magnetic materials in microsystems using magnetophoresis has increased in popularity. The wide variety and availability of magnetic beads has fuelled this drive. It is important to know the magnetic characteristics of the microspheres in order to accurately use them in separation processes integrated on a lab-on-a-chip device. To investigate the magnetic susceptibility of magnetic microspheres, the magnetic responsiveness of three types of Dynabeads microspheres were tested using two different approaches. The magnetophoretic mobility of individual microspheres is studied using a particle tracking system and the magnetization of each type of Dynabeads microsphere is measured using SQUID relaxometry. The magnetic beads' susceptibility is obtained at four different applied magnetic fields in the range of 38-70 mT for both the mobility and SQUID measurements. The susceptibility values in both approaches show a consistent magnetic field dependence.

  11. High-frequency, transient magnetic susceptibility of ferroelectrics

    NASA Astrophysics Data System (ADS)

    Grimes, Craig A.

    1996-10-01

    A significant high-frequency magnetic susceptibility was measured both in weakly polarized and nonpolarized samples of barium titanate, lead zirconate titanate, and carnauba wax. Magnetic susceptibility measurements were made from 10 to 500 MHz using a thin film permeameter at room temperature; initial susceptibilities ranged from 0.1 to 2.5. These values are larger than expected for paramagnets and smaller than expected for ferromagnets. It was found that the magnetic susceptibility decreases rapidly with exposure to the exciting field. The origin of the magnetic susceptibility is thought to originate with the applied time varying electric field associated with the susceptibility measurements. An electric field acts to rotate an electric dipole, creating a magnetic quadrupole if the two moments are balanced, and a net magnetic dipole moment if imbalanced. It is thought that local electrostatic fields created at ferroelectric domain discontinuities associated with grain boundaries create an imbalance in the anion rotation that results in a net, measurable, magnetic moment. The origin of the magnetic aftereffect may be due to the local heating of the material through the moving charges associated with the magnetic moment.

  12. MR Measurement of Alloy Magnetic Susceptibility: Towards Developing Tissue-Susceptibility Matched Metals

    PubMed Central

    Astary, Garrett W.; Peprah, Marcus K.; Fisher, Charles R.; Stewart, Rachel L.; Carney, Paul R.; Sarntinoranont, Malisa; Meisel, Mark W.; Manuel, Michele V.; Mareci, Thomas H.

    2013-01-01

    Magnetic resonance imaging (MRI) can be used to relate structure to function mapped with high-temporal resolution electrophysiological recordings using metal electrodes. Additionally, MRI may be used to guide the placement of electrodes or conductive cannula in the brain. However, the magnetic susceptibility mismatch between implanted metals and surrounding brain tissue can severely distort MR images and spectra, particularly in high magnetic fields. In this study, we present a modified MR method of characterizing the magnetic susceptibility of materials that can be used to develop biocompatible, metal alloys that match the susceptibility of host tissue in order to eliminate MR distortions proximal to the implant. This method was applied at 4.7 T and 11.1 T to measure the susceptibility of a model solid-solution alloy of Cu and Sn, which is inexpensive but not biocompatible. MR-derived relative susceptibility values of four different compositions of Cu-Sn alloy deviated by less than 3.1% from SQUID magnetometry absolute susceptibility measurements performed up to 7 T. These results demonstrate that the magnetic susceptibility varies linearly with atomic percentage in these solid-solution alloys, but are not simply the weighted average of Cu and Sn magnetic susceptibilities. Therefore susceptibility measurements are necessary when developing susceptibility-matched, solid-solution alloys for the elimination of susceptibility artifacts in MR. This MR method does not require any specialized equipment and is free of geometrical constraints, such as sample shape requirements associated with SQUID magnetometry, so the method can be used at all stages of fabrication to guide the development of a susceptibility matched, biocompatible device. PMID:23727587

  13. Alternating current magnetic susceptibility and heat dissipation by Mn1-xZnxFe2O4 nanoparticles for hyperthermia treatment

    NASA Astrophysics Data System (ADS)

    Kondo, T.; Mori, K.; Hachisu, M.; Yamazaki, T.; Okamoto, D.; Watanabe, M.; Gonda, K.; Tada, H.; Hamada, Y.; Takano, M.; Ohuchi, N.; Ichiyanagi, Y.

    2015-05-01

    Mn-Zn ferrite, Mn1-xZnxFe2O4 nanoparticles encapsulated in amorphous SiO2 were prepared using our original wet chemical method. X-ray diffraction patterns confirmed that the diameters of these particles were within 7-30 nm. Magnetization measurements for various sample compositions revealed that the saturation magnetization (Ms) of 7 nm particles was maximum for the x = 0.2 sample. AC magnetic susceptibility measurements were performed for Mn0.8Zn0.2Fe2O4 (x = 0.2) samples with 13-30 nm particles. The peak of the imaginary part of the magnetic susceptibility χ″ shifted to higher temperatures as the particle size increased. An AC field was found to cause the increase in temperature, with the 18 nm particles exhibiting the highest temperature increase, as expected. In addition, in vitro experiments were carried out to study the hyperthermia effects of Mn1-xZnxFe2O4 (x = 0.2, 18 nm) particles on human cancer cells.

  14. Frequency-Dependent Magnetic Susceptibility of Magnetite and Cobalt Ferrite Nanoparticles Embedded in PAA Hydrogel

    PubMed Central

    van Berkum, Susanne; Dee, Joris T.; Philipse, Albert P.; Erné, Ben H.

    2013-01-01

    Chemically responsive hydrogels with embedded magnetic nanoparticles are of interest for biosensors that magnetically detect chemical changes. A crucial point is the irreversible linkage of nanoparticles to the hydrogel network, preventing loss of nanoparticles upon repeated swelling and shrinking of the gel. Here, acrylic acid monomers are adsorbed onto ferrite nanoparticles, which subsequently participate in polymerization during synthesis of poly(acrylic acid)-based hydrogels (PAA). To demonstrate the fixation of the nanoparticles to the polymer, our original approach is to measure low-field AC magnetic susceptibility spectra in the 0.1 Hz to 1 MHz range. In the hydrogel, the magnetization dynamics of small iron oxide nanoparticles are comparable to those of the particles dispersed in a liquid, due to fast Néel relaxation inside the particles; this renders the ferrogel useful for chemical sensing at frequencies of several kHz. However, ferrogels holding thermally blocked iron oxide or cobalt ferrite nanoparticles show significant decrease of the magnetic susceptibility resulting from a frozen magnetic structure. This confirms that the nanoparticles are unable to rotate thermally inside the hydrogel, in agreement with their irreversible fixation to the polymer network. PMID:23673482

  15. Magnetic susceptibility of petroleum fluids

    NASA Astrophysics Data System (ADS)

    Ivakhnenko, O. P.; Potter, D. K.

    2003-04-01

    Technological progress in petroleum exploration, production and processing requires a profound knowledge of the magnetic properties of the petroleum fluids. However, as far as we know there are not widely available constants of magnetic susceptibility for the majority of petroleum fluids. We have therefore measured the mass magnetic susceptibility (χ_m) of several petroleum fluids (such as crude oils, refined oil fractions, and formation waters) from local and worldwide sites. The magnetic features of natural reservoir petroleum fluids, together with fluids connected with the petroleum industry (such as drilling fluids etc.), fall into the following categories: diamagnetic solutions, paramagnetic suspensions and ferromagnetic "ferrofluid" suspensions. In the current investigations we have concentrated on the natural reservoir fluids, which are generally diamagnetic. There were distinct differences between the χ_m of the crude oils and the formation waters, with the oils having generally a more negative value of χ_m. The magnetic susceptibility of the oils appears to be related to their main physical and chemical properties, such as density, composition of group hydrocarbons, sulphur content and concentration of organometallic compounds. Low acidity and low sulphur oils have more negative values of χ_m. Light fractions of crude oil consisting mainly of paraffinic and naphtenic hydrocarbons are the most diamagnetic. The content of the less diamagnetic aromatics increases in the kerosene and gas oil fractions, and results in an increase in the magnetic susceptibility. Also, the magnetic susceptibility of the heavy oil fraction has a significantly higher χ_m than the light fractions, which appears to be connected with a higher concentration of paramagnetic components in the heavy fraction. The χ_m of the oil from various oil provinces were compared and found to be different. It seems that values of χ_m reflect specific features of the geological conditions for

  16. Accuracy of magnetic resonance based susceptibility measurements

    NASA Astrophysics Data System (ADS)

    Erdevig, Hannah E.; Russek, Stephen E.; Carnicka, Slavka; Stupic, Karl F.; Keenan, Kathryn E.

    2017-05-01

    Magnetic Resonance Imaging (MRI) is increasingly used to map the magnetic susceptibility of tissue to identify cerebral microbleeds associated with traumatic brain injury and pathological iron deposits associated with neurodegenerative diseases such as Parkinson's and Alzheimer's disease. Accurate measurements of susceptibility are important for determining oxygen and iron content in blood vessels and brain tissue for use in noninvasive clinical diagnosis and treatment assessments. Induced magnetic fields with amplitude on the order of 100 nT, can be detected using MRI phase images. The induced field distributions can then be inverted to obtain quantitative susceptibility maps. The focus of this research was to determine the accuracy of MRI-based susceptibility measurements using simple phantom geometries and to compare the susceptibility measurements with magnetometry measurements where SI-traceable standards are available. The susceptibilities of paramagnetic salt solutions in cylindrical containers were measured as a function of orientation relative to the static MRI field. The observed induced fields as a function of orientation of the cylinder were in good agreement with simple models. The MRI susceptibility measurements were compared with SQUID magnetometry using NIST-traceable standards. MRI can accurately measure relative magnetic susceptibilities while SQUID magnetometry measures absolute magnetic susceptibility. Given the accuracy of moment measurements of tissue mimicking samples, and the need to look at small differences in tissue properties, the use of existing NIST standard reference materials to calibrate MRI reference structures is problematic and better reference materials are required.

  17. Comparison of optomagnetic and AC susceptibility readouts in a magnetic nanoparticle agglutination assay for detection of C-reactive protein.

    PubMed

    Fock, Jeppe; Parmvi, Mattias; Strömberg, Mattias; Svedlindh, Peter; Donolato, Marco; Hansen, Mikkel Fougt

    2017-02-15

    There is an increasing need to develop biosensor methods that are highly sensitive and that can be combined with low-cost consumables. The use of magnetic nanoparticles (MNPs) is attractive because their detection is compatible with low-cost disposables and because application of a magnetic field can be used to accelerate assay kinetics. We present the first study and comparison of the performance of magnetic susceptibility measurements and a newly proposed optomagnetic method. For the comparison we use the C-reactive protein (CRP) induced agglutination of identical samples of 100nm MNPs conjugated with CRP antibodies. Both methods detect agglutination as a shift to lower frequencies in measurements of the dynamics in response to an applied oscillating magnetic field. The magnetic susceptibility method probes the magnetic response whereas the optomagnetic technique probes the modulation of laser light transmitted through the sample. The two techniques provided highly correlated results upon agglutination when they measure the decrease of the signal from the individual MNPs (turn-off detection strategy), whereas the techniques provided different results, strongly depending on the read-out frequency, when detecting the signal due to MNP agglomerates (turn-on detection strategy). These observations are considered to be caused by differences in the volume-dependence of the magnetic and optical signals from agglomerates. The highest signal from agglomerates was found in the optomagnetic signal at low frequencies. Copyright © 2016 Elsevier B.V. All rights reserved.

  18. Finite-size effects on the dynamic susceptibility of CoPhOMe single-chain molecular magnets in presence of a static magnetic field

    NASA Astrophysics Data System (ADS)

    Pini, M. G.; Rettori, A.; Bogani, L.; Lascialfari, A.; Mariani, M.; Caneschi, A.; Sessoli, R.

    2011-09-01

    The static and dynamic properties of the single-chain molecular magnet Co(hfac)2NITPhOMe (CoPhOMe) (hfac = hexafluoroacetylacetonate, NITPhOMe = 4'-methoxy-phenyl-4,4,5,5-tetramethylimidazoline-1-oxyl-3-oxide) are investigated in the framework of the Ising model with Glauber dynamics, in order to take into account both the effect of an applied magnetic field and a finite size of the chains. For static fields of moderate intensity and short chain lengths, the approximation of a monoexponential decay of the magnetization fluctuations is found to be valid at low temperatures; for strong fields and long chains, a multiexponential decay should rather be assumed. The effect of an oscillating magnetic field, with intensity much smaller than that of the static one, is included in the theory in order to obtain the dynamic susceptibility χ(ω). We find that, for an open chain with N spins, χ(ω) can be written as a weighted sum of N frequency contributions, with a sum rule relating the frequency weights to the static susceptibility of the chain. Very good agreement is found between the theoretical dynamic susceptibility and the ac susceptibility measured in moderate static fields (Hdc≤2 kOe), where the approximation of a single dominating frequency for each segment length turns out to be valid. For static fields in this range, data for the relaxation time, τ versus Hdc, of the magnetization of CoPhOMe at low temperature are also qualitatively reproduced by theory, provided that finite-size effects are included.

  19. In vitro cytotoxicity of Selol-loaded magnetic nanocapsules against neoplastic cell lines under AC magnetic field activation

    NASA Astrophysics Data System (ADS)

    Falqueiro, A. M.; Siqueira-Moura, M. P.; Jardim, D. R.; Primo, F. L.; Morais, P. C.; Mosiniewicz-Szablewska, E.; Suchocki, P.; Tedesco, A. C.

    2012-04-01

    The goals of this study are to evaluate invitro compatibility of magnetic nanomaterials and their therapeutic potential against cancer cells. Highly stable ionic magnetic fluid sample (maghemite, γ-Fe2O3) and Selol were incorporated into polymeric nanocapsules by nanoprecipitation method. The cytotoxic effect of Selol-loaded magnetic nanocapsules was assessed on murine melanoma (B16-F10) and oral squamous cell carcinoma (OSCC) cell lines following AC magnetic field application. The influence of different nanocapsules on cell viability was investigated by colorimetric MTT 3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyl tetrazolium bromide assay. In the absence of AC magnetic field Selol-loaded magnetic nanocapsules, containing 100 µg/mL Selol plus 5 × 1012 particle/mL, showed antitumoral activity of about 50% on B16-F10 melanoma cells while OSCC carcinoma cells demonstrated drug resistance at all concentrations of Selol and magnetic fluid (range of 100-500 µg/mL Selol and 5 × 1012-2.5 × 1013 particle/mL). On the other hand, under AC applied fields (1 MHz and 40 Oe amplitude) B16-F10 cell viability was reduced down to 40.5% (±3.33) at the highest concentration of nanoencapsulated Selol. The major effect, however, was observed on OSCC cells since the cell viability drops down to about 33.3% (±0.38) under application of AC magnetic field. These findings clearly indicate that the Selol-loaded magnetic nanocapsules present different toxic effects on neoplastic cell lines. Further, the cytotoxic effect was maximized under AC magnetic field application on OSCC, which emphasizes the effectiveness of the magnetohyperthermia approach.

  20. Absolute method of measuring magnetic susceptibility

    USGS Publications Warehouse

    Thorpe, A.; Senftle, F.E.

    1959-01-01

    An absolute method of standardization and measurement of the magnetic susceptibility of small samples is presented which can be applied to most techniques based on the Faraday method. The fact that the susceptibility is a function of the area under the curve of sample displacement versus distance of the magnet from the sample, offers a simple method of measuring the susceptibility without recourse to a standard sample. Typical results on a few substances are compared with reported values, and an error of less than 2% can be achieved. ?? 1959 The American Institute of Physics.

  1. Magnetic Susceptibility and Morphology of Natural Magnetic Mineral Deposit in Vicinity of Human’s Living

    NASA Astrophysics Data System (ADS)

    Zulaikah, S.; Azzahro, R.; Pranita, S. B.; Mu'alimah, E. S.; Munfarikha, N.; Dewiningsih; Fitria, W. L.; Niarta, H. A.

    2017-05-01

    Magnetic susceptibility and morphology of magnetic minerals have been explored to some samples from the different environment near the vicinity of human’s living, such as hot spring, apple plantation, paddy plantation, and reservoir. Magnetic susceptibility ranged from - 0.0009 × 10-6 m3/kg (Peat in central Borneo) to 98.27 × 10-6 m3/kg (Polluted Soil in Jalan Sukarno Hatta Malang). The grain size of magnetic mineral not more than that of 300 μm. Data analysis informs us that each environment where the magnetic minerals were deposited, influenced the two physical properties both of magnetic susceptibility and morphology of magnetic minerals. Regarding the environment process, magnetic susceptibility depends upon the grain size beside the kinds of magnetic minerals. So, it can be concluded that in every environment, the magnetic minerals have specific properties including magnetic susceptibility and the morphology of magnetic minerals.

  2. SQUIDs De-fluxing Using a Decaying AC Magnetic Field

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Matlashov, Andrei Nikolaevich; Semenov, Vasili Kirilovich; Anderson, Bill

    Flux trapping is the Achilles’ heel of all superconductor electronics. The most direct way to avoid flux trapping is a prevention of superconductor circuits from exposure to magnetic fields. Unfortunately this is not feasible if the circuits must be exposed to a strong DC magnetic field even for a short period of time. For example, such unavoidable exposures take place in superparamagnetic relaxation measurements (SPMR) and ultra-low field magnetic resonance imaging (ULF MRI) using unshielded thin-film SQUID-based gradiometers. Unshielded SQUIDs stop working after being exposed to DC magnetic fields of only a few Gauss in strength. In this paper wemore » present experimental results with de-fluxing of planar thin-film LTS SQUID-based gradiometers using a strong decaying AC magnetic field. We used four commercial G136 gradiometers for SPMR measurements with up to a 10 mT magnetizing field. Strong 12.9 kHz decaying magnetic field pulses reliably return SQUIDs to normal operation 50 ms after zeroing the DC magnetizing field. This new AC de-fluxing method was also successfully tested with seven other different types of LTS SQUID sensors and has been shown to dissipate extremely low energy.« less

  3. 21 CFR 886.4440 - AC-powered magnet.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... metallic foreign bodies from eye tissue. (b) Classification. Class II. ... 21 Food and Drugs 8 2014-04-01 2014-04-01 false AC-powered magnet. 886.4440 Section 886.4440 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL...

  4. 21 CFR 886.4440 - AC-powered magnet.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... metallic foreign bodies from eye tissue. (b) Classification. Class II. ... 21 Food and Drugs 8 2012-04-01 2012-04-01 false AC-powered magnet. 886.4440 Section 886.4440 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL...

  5. 21 CFR 886.4440 - AC-powered magnet.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... metallic foreign bodies from eye tissue. (b) Classification. Class II. ... 21 Food and Drugs 8 2011-04-01 2011-04-01 false AC-powered magnet. 886.4440 Section 886.4440 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL...

  6. 21 CFR 886.4440 - AC-powered magnet.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... metallic foreign bodies from eye tissue. (b) Classification. Class II. ... 21 Food and Drugs 8 2013-04-01 2013-04-01 false AC-powered magnet. 886.4440 Section 886.4440 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL...

  7. Computed inverse MRI for magnetic susceptibility map reconstruction

    PubMed Central

    Chen, Zikuan; Calhoun, Vince

    2015-01-01

    Objective This paper reports on a computed inverse magnetic resonance imaging (CIMRI) model for reconstructing the magnetic susceptibility source from MRI data using a two-step computational approach. Methods The forward T2*-weighted MRI (T2*MRI) process is decomposed into two steps: 1) from magnetic susceptibility source to fieldmap establishment via magnetization in a main field, and 2) from fieldmap to MR image formation by intravoxel dephasing average. The proposed CIMRI model includes two inverse steps to reverse the T2*MRI procedure: fieldmap calculation from MR phase image and susceptibility source calculation from the fieldmap. The inverse step from fieldmap to susceptibility map is a 3D ill-posed deconvolution problem, which can be solved by three kinds of approaches: Tikhonov-regularized matrix inverse, inverse filtering with a truncated filter, and total variation (TV) iteration. By numerical simulation, we validate the CIMRI model by comparing the reconstructed susceptibility maps for a predefined susceptibility source. Results Numerical simulations of CIMRI show that the split Bregman TV iteration solver can reconstruct the susceptibility map from a MR phase image with high fidelity (spatial correlation≈0.99). The split Bregman TV iteration solver includes noise reduction, edge preservation, and image energy conservation. For applications to brain susceptibility reconstruction, it is important to calibrate the TV iteration program by selecting suitable values of the regularization parameter. Conclusions The proposed CIMRI model can reconstruct the magnetic susceptibility source of T2*MRI by two computational steps: calculating the fieldmap from the phase image and reconstructing the susceptibility map from the fieldmap. The crux of CIMRI lies in an ill-posed 3D deconvolution problem, which can be effectively solved by the split Bregman TV iteration algorithm. PMID:22446372

  8. Magnetic susceptibility of tektites and some other glasses

    USGS Publications Warehouse

    Senftle, F.E.; Thorpe, A.

    1959-01-01

    The magnetic susceptibility at several magnetic field strengths of about thirty tektites from various localities have been measured. The susceptibility ranges from 2 ?? 10-6 to about 7.9 ?? 10-6 e.m.u./g. Tektites from a given locality have similar susceptibilities. The intensity of magnetization of all the tektites measured is zero or very small. For comparison, the same measurements have been made on about thirty obsidians. The magnetic susceptibilities cover approximately the same range, but the intensity of magnetization of the impurity was found to be much higher. By heating the obsidians to 1450??C the intensity of magnetization was reduced to zero. From the above data, it is shown that the tektites must have been heated well above 1400??C, and that essentially all the iron is in solution. On the other hand, the evidence shows that obsidians have not been heated much above this temperature, and that there is a significant amount of undissolved iron in the glass, probably as magnetite. Further, if tektites are extraterrestrial, they probably entered the earth's atmosphere as a glass. ?? 1959.

  9. Testing of a First Order AC Magnetic Susceptometer

    NASA Astrophysics Data System (ADS)

    Fukuda, Ryan; Sunny, Smitha; Ho, Pei-Chun

    2011-11-01

    A first-order AC magnetic susceptometer has been constructed and tested to find the magnetic response of strongly correlated electron materials. The instrument works by using a primary coil to apply a small AC magnetic field of .104 Oe to a sample with a cylindrical coil space of length .635 cm and diameter .355 cm. A lock-in amplifier is used to monitor the induced voltage from a set of secondary coils. By coupling a temperature-controlled system with this instrument, the change in the magnetic signal with respect to temperature is measured. Monitoring the signal changes may indicate the temperature that causes the material to transition to either a ferromagnetic, anti-ferromagnetic, or superconducting state. A 122.47 mg Gd polycrystal was used to test our susceptometer. The data qualitatively agrees with the previous results of magnetization vs. temperature of Gd single crystals by Nigh et al. [1]: there is a steep increase in the pick-up signal at 300 K where Gd becomes ferromagnetic and a peak at 210 K [1]. This susceptometer will be used for our future investigation of magnetic properties of rare earth compounds and nanoparticles in the temperature range of 10 K to 300 K. [4pt] [1] H. E. Nigh, S. Legvold, and F. H. Spedding, Physical Review 132, 1092 (1963)

  10. The magnetic susceptibility of soils in Krakow, southern Poland

    NASA Astrophysics Data System (ADS)

    Wojas, Anna

    2017-06-01

    Studies into the magnetic susceptibility have been used to assess the soils contamination in the Krakow area. The results of topsoil (over a 2 × 2 km grid), subsoil (37 shallow holes) and soil samples (112) measurements were presented as maps of soil magnetic susceptibility (both volume and mass) illustrating the distribution of parameters in topsoil horizon (0-10 cm) and differential magnetic susceptibility maps between topsoil horizon and subsoil (40-60 cm). All evidence leads to the finding that the highest values of magnetic susceptibility of soil are found exclusively in industrial areas. Taking into consideration the type of land use, the high median value (89.8 × 10-8 m3kg-1) was obtained for samples of cultivated soils and is likely to be connected with occurrence of fertile soil (chernozem). Moreover, enrichment of soils with Pb and Zn accompanies magnetic susceptibility anomalies in the vicinity of the high roads and in the steelworks area, respectively.

  11. Effect of dc field on ac-loss peak in a commercial Bi:2223/Ag tape

    NASA Astrophysics Data System (ADS)

    Öztürk, Ali; Düzgün, İbrahim; Çelebi, Selahattin

    2017-12-01

    Measurements of the ac susceptibility in a commercial Bi:2223/Ag tape for some different ac magnetic field amplitudes, Hac, in the presence of bias magnetic field Hdc directed along Hac are reported. It is found that the peak values of the imaginary component of ac susceptibility χ″max versus Hac trace a valley for the orientation where applied field Ha perpendicular to wide face of the tape total. We note that the observation of the valley depends on various parameters such as field dependence parameter n in the critical current density, in the simple power law expression jc = α(T)/Bn, choice of the bias field Hdc together with selected ac field amplitudes Hac, and dimension and geometry of sample studied. Our calculations based on critical state model with jc = α(1 - T/Tcm)p/Bn using the fitting parameters of n = 0.25, p = 2.2, Tcm = 108 K gives quite good results to compare the experimental and calculated curves.

  12. The DC and AC insulating properties of magnetic fluids based on transformer oil

    NASA Astrophysics Data System (ADS)

    Tomo, L.; Marton, K.; Herchl, F.; Kopanský, P.; Potoová, I.; Koneracká, M.; Timko, M.

    2006-01-01

    The AC-dielectric breakdown was investigated in magnetic fluids based on transformer oil TECHNOL US 4000 for two orientations of external magnetic field (B E and B E) and in B = 0. The found results were compared with those obtained formerly for the DC-dielectric breakdown. The observations of the time development of the AC-dielectric breakdown showed the presence of partial discharges long before the complete breakdown occurrence, while for DC-dielectric breakdown a complete breakdown of the gap next to the onset of a measurable ionization was characteristic. The comparison of the AC-dielectric breakdown strengths of pure transformer oil and transformer-oil-based magnetic fluid showed better dielectric properties of magnetic fluid in external magnetic field and comparable, but not worse, in B = 0. Regarding to the better heat transfer, provided by magnetic fluids, they could be used in power transformers as insulating fluids.

  13. Magnetic susceptibility of ultrahigh pressure eclogite: The role of retrogression

    NASA Astrophysics Data System (ADS)

    Xu, Haijun; Jin, Zhenmin; Mason, Roger; Ou, Xingong

    2009-09-01

    Retrograde metamorphism played the dominant role in changing the low-field rock magnetic properties and density of 198 specimens of variably retrograded eclogites from the main borehole of the Chinese Continental Scientific Drilling Project (CCSD) and from surface outcrops in the Donghai area in the southern part of the Sulu UHP belt, China. Bulk magnetic susceptibility ( κ) of unretrogressed UHP eclogite is controlled by whole-rock chemical composition and ranges from 397 to 2312 μSI with principal magnetic susceptibility carrying minerals paramagnetic garnet, omphacite, rutile and phengite. Partially retrograded eclogites show large variations in magnetic susceptibility between 804 and 24,277 μSI, with high mean magnetic susceptibility values of 4372 ± 4149 μSI caused by appreciable amounts of Fe-Ti oxide minerals such as magnetite, ilmenite and/or titanohematite produced by retrograde metamorphic reactions. Completely retrograded eclogites have lower susceptibilities of 1094 ± 600 μSI and amphibolite facies mineral assemblages lacking high magnetic susceptibility minerals. Jelínek's corrected anisotropy ( Pj) of eclogites ranges from 1.001 to 1.540, and shows a positive correlation with low-field magnetic susceptibility ( κ). Arithmetic mean bulk density ( ρ) shows a steady decrease from 3.54 ± 0.11 g/cm 3 (fresh eclogite) to 2.98 ± 0.06 g/cm 3 (completely retrograded eclogite). Retrograde metamorphic changes in mineral composition during exhumation appear to be the major factor causing variations in low field magnetic susceptibility and anisotropy. Retrograde processes must be taken into account when interpreting magnetic surveys and geophysical well logs in UHP metamorphic terranes, and petrophysical properties such as density and low-field magnetic susceptibility could provide a means for semi-quantifying the degree of retrogression of eclogite during exhumation.

  14. Magnetic susceptibility, nanorheology, and magnetoviscosity of magnetic nanoparticles in viscoelastic environments

    NASA Astrophysics Data System (ADS)

    Ilg, Patrick; Evangelopoulos, Apostolos E. A. S.

    2018-03-01

    While magnetic nanoparticles suspended in Newtonian solvents (ferrofluids) have been intensively studied in recent years, the effects of viscoelasticity of the surrounding medium on the nanoparticle dynamics are much less understood. Here we investigate a mesoscopic model for the orientational dynamics of isolated magnetic nanoparticles subject to external fields, viscous and viscoelastic friction, as well as the corresponding random torques. We solve the model analytically in the overdamped limit for weak viscoelasticity. By comparison to Brownian dynamics simulations we establish the limits of validity of the analytical solution. We find that viscoelasticity not only slows down the magnetization relaxation, shifts the peak of the imaginary magnetic susceptibility χ″ to lower frequencies, and increases the magnetoviscosity but also leads to nonexponential relaxation and a broadening of χ″. The model we study also allows us to test a recent proposal for using magnetic susceptibility measurements as a nanorheological tool using a variant of the Germant-DiMarzio-Bishop relation. We find for the present model and certain parameter ranges that the relation of the magnetic susceptibility to the shear modulus is satisfied to a good approximation.

  15. A Miniature Magnetic-Force-Based Three-Axis AC Magnetic Sensor with Piezoelectric/Vibrational Energy-Harvesting Functions.

    PubMed

    Hung, Chiao-Fang; Yeh, Po-Chen; Chung, Tien-Kan

    2017-02-08

    In this paper, we demonstrate a miniature magnetic-force-based, three-axis, AC magnetic sensor with piezoelectric/vibrational energy-harvesting functions. For magnetic sensing, the sensor employs a magnetic-mechanical-piezoelectric configuration (which uses magnetic force and torque, a compact, single, mechanical mechanism, and the piezoelectric effect) to convert x -axis and y -axis in-plane and z -axis magnetic fields into piezoelectric voltage outputs. Under the x -axis magnetic field (sine-wave, 100 Hz, 0.2-3.2 gauss) and the z -axis magnetic field (sine-wave, 142 Hz, 0.2-3.2 gauss), the voltage output with the sensitivity of the sensor are 1.13-26.15 mV with 8.79 mV/gauss and 1.31-8.92 mV with 2.63 mV/gauss, respectively. In addition, through this configuration, the sensor can harness ambient vibrational energy, i.e., possessing piezoelectric/vibrational energy-harvesting functions. Under x -axis vibration (sine-wave, 100 Hz, 3.5 g) and z -axis vibration (sine-wave, 142 Hz, 3.8 g), the root-mean-square voltage output with power output of the sensor is 439 mV with 0.333 μW and 138 mV with 0.051 μW, respectively. These results show that the sensor, using this configuration, successfully achieves three-axis magnetic field sensing and three-axis vibration energy-harvesting. Due to these features, the three-axis AC magnetic sensor could be an important design reference in order to develop future three-axis AC magnetic sensors, which possess energy-harvesting functions, for practical industrial applications, such as intelligent vehicle/traffic monitoring, processes monitoring, security systems, and so on.

  16. Computed inverse resonance imaging for magnetic susceptibility map reconstruction.

    PubMed

    Chen, Zikuan; Calhoun, Vince

    2012-01-01

    This article reports a computed inverse magnetic resonance imaging (CIMRI) model for reconstructing the magnetic susceptibility source from MRI data using a 2-step computational approach. The forward T2*-weighted MRI (T2*MRI) process is broken down into 2 steps: (1) from magnetic susceptibility source to field map establishment via magnetization in the main field and (2) from field map to MR image formation by intravoxel dephasing average. The proposed CIMRI model includes 2 inverse steps to reverse the T2*MRI procedure: field map calculation from MR-phase image and susceptibility source calculation from the field map. The inverse step from field map to susceptibility map is a 3-dimensional ill-posed deconvolution problem, which can be solved with 3 kinds of approaches: the Tikhonov-regularized matrix inverse, inverse filtering with a truncated filter, and total variation (TV) iteration. By numerical simulation, we validate the CIMRI model by comparing the reconstructed susceptibility maps for a predefined susceptibility source. Numerical simulations of CIMRI show that the split Bregman TV iteration solver can reconstruct the susceptibility map from an MR-phase image with high fidelity (spatial correlation ≈ 0.99). The split Bregman TV iteration solver includes noise reduction, edge preservation, and image energy conservation. For applications to brain susceptibility reconstruction, it is important to calibrate the TV iteration program by selecting suitable values of the regularization parameter. The proposed CIMRI model can reconstruct the magnetic susceptibility source of T2*MRI by 2 computational steps: calculating the field map from the phase image and reconstructing the susceptibility map from the field map. The crux of CIMRI lies in an ill-posed 3-dimensional deconvolution problem, which can be effectively solved by the split Bregman TV iteration algorithm.

  17. Magnetic susceptibilities of minerals

    USGS Publications Warehouse

    Rosenblum, Sam; Brownfield, I.K.

    2000-01-01

    Magnetic separation of minerals is a topic that is seldom reported in the literature for two reasons. First, separation data generally are byproducts of other projects; and second, this study requires a large amount of patience and is unusually tedious. Indeed, we suspect that most minerals probably are never investigated for this property. These data are timesaving for mineralogists who concentrate mono-mineralic fractions for chemical analysis, age dating, and for other purposes. The data can certainly be used in the ore-beneficiation industries. In some instances, magnetic-susceptibility data may help in mineral identification, where other information is insufficient. In past studies of magnetic separation of minerals, (Gaudin and Spedden, 1943; Tille and Kirkpatrick, 1956; Rosenblum, 1958; Rubinstein and others, 1958; Flinter, 1959; Hess, 1959; Baker, 1962; Meric and Peyre, 1963; Rojas and others, 1965; and Duchesne, 1966), the emphasis has been on the ferromagnetic and paramagnetic ranges of extraction. For readers interested in the history of magnetic separation of minerals, Krumbein and Pettijohn (1938, p. 344-346) indicated nine references back to 1848. The primary purpose of this paper is to report the magnetic-susceptibility data on as many minerals as possible, similar to tables of hardness, specific gravity, refractive indices, and other basic physical properties of minerals. A secondary purpose is to demonstrate that the total and best extraction ranges are influenced by the chemistry of the minerals. The following notes are offered to help avoid problems in separating a desired mineral concentrate from mixtures of mineral grains.

  18. Magnetic Susceptibility Measurements for in Situ Characterization of Lunar Soil

    NASA Technical Reports Server (NTRS)

    Oder, R. R.

    1992-01-01

    Magnetic separation is a viable method for concentration of components of lunar soils and rocks for use as feedstocks for manufacture of metals, oxygen, and for recovery of volatiles such as He-3. Work with lunar materials indicates that immature soils are the best candidates for magnetic beneficiation. The magnetic susceptibility at which selected soil components such as anorthite, ilmenite, or metallic iron are separated is not affected by soil maturity, but the recovery of the concentrated components is. Increasing soil maturity lowers recovery. Mature soils contain significant amounts of glass-encased metallic iron. Magnetic susceptibility, which is sensitive to metallic iron content, can be used to measure soil maturity. The relationship between the ratio of magnetic susceptibility and iron oxide and the conventional maturity parameter, I(sub s)/FeO, ferromagnetic resonant intensity divided by iron oxide content is given. The magnetic susceptibilities were determined using apparatus designed for magnetic separation of the lunar soils.

  19. Sensor-less pseudo-sinusoidal drive for a permanent-magnet brushless ac motor

    NASA Astrophysics Data System (ADS)

    Liu, Li-Hsiang; Chern, Tzuen-Lih; Pan, Ping-Lung; Huang, Tsung-Mou; Tsay, Der-Min; Kuang, Jao-Hwa

    2012-04-01

    The precise rotor-position information is required for a permanent-magnet brushless ac motor (BLACM) drive. In the conventional sinusoidal drive method, either an encoder or a resolver is usually employed. For position sensor-less vector control schemes, the rotor flux estimation and torque components are obtained by complicated coordinate transformations. These computational intensive methods are susceptible to current distortions and parameter variations. To simplify the method complexity, this work presents a sensor-less pseudo-sinusoidal drive scheme with speed control for a three-phase BLACM. Based on the sinusoidal drive scheme, a floating period of each phase current is inserted for back electromotive force detection. The zero-crossing point is determined directly by the proposed scheme, and the rotor magnetic position and rotor speed can be estimated simultaneously. Several experiments for various active angle periods are undertaken. Furthermore, a current feedback control is included to minimize and compensate the torque fluctuation. The experimental results show that the proposed method has a competitive performance compared with the conventional drive manners for BLACM. The proposed scheme is straightforward, bringing the benefits of sensor-less drive and negating the need for coordinate transformations in the operating process.

  20. A Miniature Magnetic-Force-Based Three-Axis AC Magnetic Sensor with Piezoelectric/Vibrational Energy-Harvesting Functions

    PubMed Central

    Hung, Chiao-Fang; Yeh, Po-Chen; Chung, Tien-Kan

    2017-01-01

    In this paper, we demonstrate a miniature magnetic-force-based, three-axis, AC magnetic sensor with piezoelectric/vibrational energy-harvesting functions. For magnetic sensing, the sensor employs a magnetic–mechanical–piezoelectric configuration (which uses magnetic force and torque, a compact, single, mechanical mechanism, and the piezoelectric effect) to convert x-axis and y-axis in-plane and z-axis magnetic fields into piezoelectric voltage outputs. Under the x-axis magnetic field (sine-wave, 100 Hz, 0.2–3.2 gauss) and the z-axis magnetic field (sine-wave, 142 Hz, 0.2–3.2 gauss), the voltage output with the sensitivity of the sensor are 1.13–26.15 mV with 8.79 mV/gauss and 1.31–8.92 mV with 2.63 mV/gauss, respectively. In addition, through this configuration, the sensor can harness ambient vibrational energy, i.e., possessing piezoelectric/vibrational energy-harvesting functions. Under x-axis vibration (sine-wave, 100 Hz, 3.5 g) and z-axis vibration (sine-wave, 142 Hz, 3.8 g), the root-mean-square voltage output with power output of the sensor is 439 mV with 0.333 μW and 138 mV with 0.051 μW, respectively. These results show that the sensor, using this configuration, successfully achieves three-axis magnetic field sensing and three-axis vibration energy-harvesting. Due to these features, the three-axis AC magnetic sensor could be an important design reference in order to develop future three-axis AC magnetic sensors, which possess energy-harvesting functions, for practical industrial applications, such as intelligent vehicle/traffic monitoring, processes monitoring, security systems, and so on. PMID:28208693

  1. Activation of Bt Protoxin Cry1Ac in Resistant and Susceptible Cotton Bollworm.

    PubMed

    Wei, Jizhen; Liang, Gemei; Wang, Bingjie; Zhong, Feng; Chen, Lin; Khaing, Myint Myint; Zhang, Jie; Guo, Yuyuan; Wu, Kongming; Tabashnik, Bruce E

    2016-01-01

    Crystalline (Cry) proteins from Bacillus thuringiensis (Bt) are used extensively for insect control in sprays and transgenic plants, but their efficacy is reduced by evolution of resistance in pests. Here we evaluated reduced activation of Cry1Ac protoxin as a potential mechanism of resistance in the invasive pest Helicoverpa armigera. Based on the concentration killing 50% of larvae (LC50) for a laboratory-selected resistant strain (LF120) divided by the LC50 for its susceptible parent strain (LF), the resistance ratio was 1600 for Cry1Ac protoxin and 1200 for trypsin-activated Cry1Ac toxin. The high level of resistance to activated toxin as well as to protoxin indicates reduced activation of protoxin is not a major mechanism of resistance to Cry1Ac in LF120. For both insect strains, treatment with either the trypsin inhibitor N-a-tosyl-L-lysine chloromethyl ketone (TLCK) or the chymotrypsin inhibitor N-a-tosyl-L-phenylalanine chloromethyl ketone (TPCK) did not significantly affect the LC50 of Cry1Ac protoxin. Enzyme activity was higher for LF than LF120 for trypsin-like proteases, but did not differ between strains for chymotrypsin-like proteases. The results here are consistent with previous reports indicating that reduced activation of protoxin is generally not a major mechanism of resistance to Bt proteins.

  2. Activation of Bt Protoxin Cry1Ac in Resistant and Susceptible Cotton Bollworm

    PubMed Central

    Liang, Gemei; Wang, Bingjie; Zhong, Feng; Chen, Lin; Khaing, Myint Myint; Zhang, Jie; Guo, Yuyuan; Wu, Kongming; Tabashnik, Bruce E.

    2016-01-01

    Crystalline (Cry) proteins from Bacillus thuringiensis (Bt) are used extensively for insect control in sprays and transgenic plants, but their efficacy is reduced by evolution of resistance in pests. Here we evaluated reduced activation of Cry1Ac protoxin as a potential mechanism of resistance in the invasive pest Helicoverpa armigera. Based on the concentration killing 50% of larvae (LC50) for a laboratory-selected resistant strain (LF120) divided by the LC50 for its susceptible parent strain (LF), the resistance ratio was 1600 for Cry1Ac protoxin and 1200 for trypsin-activated Cry1Ac toxin. The high level of resistance to activated toxin as well as to protoxin indicates reduced activation of protoxin is not a major mechanism of resistance to Cry1Ac in LF120. For both insect strains, treatment with either the trypsin inhibitor N-a-tosyl-L-lysine chloromethyl ketone (TLCK) or the chymotrypsin inhibitor N-a-tosyl-L-phenylalanine chloromethyl ketone (TPCK) did not significantly affect the LC50 of Cry1Ac protoxin. Enzyme activity was higher for LF than LF120 for trypsin-like proteases, but did not differ between strains for chymotrypsin-like proteases. The results here are consistent with previous reports indicating that reduced activation of protoxin is generally not a major mechanism of resistance to Bt proteins. PMID:27257885

  3. Effect of centrifugation on dynamic susceptibility of magnetic fluids

    NASA Astrophysics Data System (ADS)

    Pshenichnikov, Alexander; Lebedev, Alexander; Lakhtina, Ekaterina; Kuznetsov, Andrey

    2017-06-01

    The dispersive composition, dynamic susceptibility and spectrum of times of magnetization relaxation for six samples of magnetic fluid obtained by centrifuging two base colloidal solutions of the magnetite in kerosene was investigated experimentally. The base solutions differed by the concentration of the magnetic phase and the width of the particle size distribution. The procedure of cluster analysis allowing one to estimate the characteristic sizes of aggregates with uncompensated magnetic moments was described. The results of the magnetogranulometric and cluster analyses were discussed. It was shown that centrifugation has a strong effect on the physical properties of the separated fractions, which is related to the spatial redistribution of particles and multi-particle aggregates. The presence of aggregates in magnetic fluids is interpreted as the main reason of low-frequency (0.1-10 kHz) dispersion of the dynamic susceptibility. The obtained results count in favor of using centrifugation as an effective means of changing the dynamic susceptibility over wide limits and obtaining fluids with the specified type of susceptibility dispersion.

  4. Slow magnetic relaxation in a cobalt magnetic chain.

    PubMed

    Yang, Chen-I; Chuang, Po-Hsiang; Lu, Kuang-Lieh

    2011-04-21

    A homospin ladder-like chain, [Co(Hdhq)(OAc)](n) (1; H(2)dhq = 2,3-dihydroxyquinoxaline), shows a single-chain-magnet-like (SCM-like) behavior with the characteristics of frequency dependence of the out-of-phase component in alternating current (ac) magnetic susceptibilities and hysteresis loops. © The Royal Society of Chemistry 2011

  5. Alternating current magnetic susceptibility and heat dissipation by Mn{sub 1−x}Zn{sub x}Fe{sub 2}O{sub 4} nanoparticles for hyperthermia treatment

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Kondo, T.; Mori, K.; Hachisu, M.

    2015-05-07

    Mn-Zn ferrite, Mn{sub 1−x}Zn{sub x}Fe{sub 2}O{sub 4} nanoparticles encapsulated in amorphous SiO{sub 2} were prepared using our original wet chemical method. X-ray diffraction patterns confirmed that the diameters of these particles were within 7–30 nm. Magnetization measurements for various sample compositions revealed that the saturation magnetization (M{sub s}) of 7 nm particles was maximum for the x = 0.2 sample. AC magnetic susceptibility measurements were performed for Mn{sub 0.8}Zn{sub 0.2}Fe{sub 2}O{sub 4} (x = 0.2) samples with 13–30 nm particles. The peak of the imaginary part of the magnetic susceptibility χ″ shifted to higher temperatures as the particle size increased. An AC field was found to causemore » the increase in temperature, with the 18 nm particles exhibiting the highest temperature increase, as expected. In addition, in vitro experiments were carried out to study the hyperthermia effects of Mn{sub 1−x}Zn{sub x}Fe{sub 2}O{sub 4} (x = 0.2, 18 nm) particles on human cancer cells.« less

  6. ac response of thin superconductors in the flux-creep regime

    NASA Astrophysics Data System (ADS)

    Gurevich, A.; Brandt, E. H.

    1997-05-01

    We calculate both analytically and numerically the ac susceptibility χ(ω) and the nonlinear electromagnetic response of thin superconductor strips and disks of constant thickness in a perpendicular time-dependent magnetic field Ba(t)=B0cos ωt, taking account of the strong nonlinearity of the voltage-current characteristics below the irreversibility line. We consider integral equations of nonlinear nonlocal flux diffusion for a wide class of thermally activated creep models. It is shown that thin superconductors, despite being fully in the critical state, exhibit a universal Meissner-like electromagnetic response in the dissipative flux-creep regime. The expression for the linear ac susceptibility during flux creep appears to be similar to the susceptibility of Ohmic conductors, but with the relaxation time constant replaced by the time t elapsed after flux creep has started. This result is independent of any material parameter or temperature or dc field. For ωt>>:1, we obtain χ(ω)~-1+pln (qiωt)/(iωt), where p and q are constants. Above a critical ac amplitude B0=Bl, the local response of the electric field becomes nonlinear, and there are two distinctive nonlinear regimes at B0>Bl, where Bl~s(d/a)1/2Bp, Bp is a characteristic field of full flux penetration, s(T,B)=\\|dln j/dln t\\| is the dimensionless flux-creep rate and d and a are the sample thickness and width, respectively. For Blac field Ba(t) does not cause a periodic inversion of the critical state. As a result, the magnetic moment exhibits a Meissner-like nondissipative response, in stark contrast to the Bean model. For B0>Bh(ω) the ac field causes hysteresis dissipation due to a periodic remagnetization of the critical state that gives rise to the hysteretic magnetic response of the Bean model at B0>>:Bh. Here Bh(ω) weakly depends on ω and is of order (d/a)1/2Bp for a very wide frequency range, well

  7. Susceptibility of superconductor disks and rings with and without flux creep

    NASA Astrophysics Data System (ADS)

    Brandt, Ernst Helmut

    1997-06-01

    First some consequences of the Bean assumption of constant critical current Jc in type-II superconductors are listed and the Bean ac susceptibility of narrow rings is derived. Then flux creep is described by a nonlinear current-voltage law E~Jn, from which the saturated magnetic moment at constant ramp rate H-|Apa(t) is derived for rings with general hole radius a1 and general creep exponent n. Next the exact formulation for rings in a perpendicular applied field Ha(t) is presented in the form of an equation of motion for the current density in thick rings and disks or the sheet current in thin rings and disks. This method is used to compute general magnetization curves m(Ha) and ac susceptibilities χ of rings with and without creep, accounting also for nonconstant Jc(B). Typical current and field (B) profiles are depicted. The initial slope of m(Ha) (the ideal diamagnetic moment) and the field of full penetration are expressed as functions of the inner and outer ring radii a1 and a. A scaling law is derived which states that for arbitrary creep exponent n the complex nonlinear ac susceptibility χ(H0,ω) depends only on the combination Hn-10/ω of the ac amplitude H0 and the ac frequency ω/2π. This scaling law thus connects the known dependencies χ=χ(ω) in the ohmic limit (n=1) and χ=χ(H0) in the Bean limit (n-->∞).

  8. Spatial distribution of topsoil magnetic susceptibility in Sawahlunto City, West Sumatera

    NASA Astrophysics Data System (ADS)

    Afdal; Wahyuni, E. S.

    2018-03-01

    A research to determine the spatial distribution of top soil magnetic suceptibility at Sawahlunto City, West Sumatra has been conducted. The top soil samples were taken at four locations ie the downtown area, the steam power plant area, the agricultural area, and coal mine area. At each location, the soil samples were taken at 10 points at a depth of 20 cm. Magnetic susceptibility were measured using Bartington MS2B Magnetic Susceptibility Meter. The topsoil samples from Sawahlunto city have relatively low average value of the magnetic susceptibility that is 67.0×10-8 m3/kg. The magnetic susceptibility of topsoil samples from downtown area have the average and the highest value of magnetic susceptibility (100.6×10-8 and 259.9×10-8 m3/kg), and followed by sample from the steam power plant area (98.4×10-8 and 258.0×10-8 m3/kg), the agricultural area (56.2×10-8 and 83.7×10-8 m3/kg), and coal mine area (12.9×10-8 and 26.8×10-8 m3/kg). Soil samples from the steam power plant area have the widest range of magnetic susceptibility value range from 0.3 × 10-8 to 258.0 × 10-8 m3/kg.

  9. Real-time and quantitative isotropic spatial resolution susceptibility imaging for magnetic nanoparticles

    NASA Astrophysics Data System (ADS)

    Pi, Shiqiang; Liu, Wenzhong; Jiang, Tao

    2018-03-01

    The magnetic transparency of biological tissue allows the magnetic nanoparticle (MNP) to be a promising functional sensor and contrast agent. The complex susceptibility of MNPs, strongly influenced by particle concentration, excitation magnetic field and their surrounding microenvironment, provides significant implications for biomedical applications. Therefore, magnetic susceptibility imaging of high spatial resolution will give more detailed information during the process of MNP-aided diagnosis and therapy. In this study, we present a novel spatial magnetic susceptibility extraction method for MNPs under a gradient magnetic field, a low-frequency drive magnetic field, and a weak strength high-frequency magnetic field. Based on this novel method, a magnetic particle susceptibility imaging (MPSI) of millimeter-level spatial resolution (<3 mm) was achieved using our homemade imaging system. Corroborated by the experimental results, the MPSI shows real-time (1 s per frame acquisition) and quantitative abilities, and isotropic high resolution.

  10. Calorimetric method of ac loss measurement in a rotating magnetic field.

    PubMed

    Ghoshal, P K; Coombs, T A; Campbell, A M

    2010-07-01

    A method is described for calorimetric ac-loss measurements of high-T(c) superconductors (HTS) at 80 K. It is based on a technique used at 4.2 K for conventional superconducting wires that allows an easy loss measurement in parallel or perpendicular external field orientation. This paper focuses on ac loss measurement setup and calibration in a rotating magnetic field. This experimental setup is to demonstrate measuring loss using a temperature rise method under the influence of a rotating magnetic field. The slight temperature increase of the sample in an ac-field is used as a measure of losses. The aim is to simulate the loss in rotating machines using HTS. This is a unique technique to measure total ac loss in HTS at power frequencies. The sample is mounted on to a cold finger extended from a liquid nitrogen heat exchanger (HEX). The thermal insulation between the HEX and sample is provided by a material of low thermal conductivity, and low eddy current heating sample holder in vacuum vessel. A temperature sensor and noninductive heater have been incorporated in the sample holder allowing a rapid sample change. The main part of the data is obtained in the calorimetric measurement is used for calibration. The focus is on the accuracy and calibrations required to predict the actual ac losses in HTS. This setup has the advantage of being able to measure the total ac loss under the influence of a continuous moving field as experienced by any rotating machines.

  11. Hidden transition in multiferroic and magnetodielectric CuCrO2 evidenced by ac-susceptibility

    NASA Astrophysics Data System (ADS)

    Shukla, Kaushak K.; Pal, Arkadeb; Singh, Abhishek; Singh, Rahul; Saha, J.; Sinha, A. K.; Ghosh, A. K.; Patnaik, S.; Awasthi, A. M.; Chatterjee, Sandip

    2017-04-01

    Ferroelectric polarization, magnetic-field dependence of the dielectric constant and ac and dc magnetizations of frustrated CuCrO2 have been measured. A new spin freezing transition below 32 K is observed which is thermally driven. The nature of the spin freezing is to be a single-ion process. Dilution by the replacements of Cr ions by magnetic Mn ions showed suppression of the spin freezing transition suggesting it to be fundamentally a single-ion freezing process. The observed freezing, which is seemingly associated to geometrical spin frustration, represents a novel form of magnetic glassy behavior.

  12. Gastrointestinal transit and disintegration of enteric coated magnetic tablets assessed by ac biosusceptometry.

    PubMed

    Corá, Luciana A; Romeiro, Fernando G; Américo, Madileine F; Oliveira, Ricardo Brandt; Baffa, Oswaldo; Stelzer, Murilo; Miranda, José Ricardo de Arruda

    2006-01-01

    The oral administration is a common route in the drug therapy and the solid pharmaceutical forms are widely used. Although much about the performance of these formulations can be learned from in vitro studies using conventional methods, evaluation in vivo is essential in product development. The knowledge of the gastrointestinal transit and how the physiological variables can interfere with the disintegration and drug absorption is a prerequisite for development of dosage forms. The aim of this work was to employing the ac biosusceptometry (ACB) to monitoring magnetic tablets in the human gastrointestinal tract and to obtain the magnetic images of the disintegration process in the colonic region. The ac biosusceptometry showed accuracy in the quantification of the gastric residence time, the intestinal transit time and the disintegration time (DT) of the magnetic formulations in the human gastrointestinal tract. Moreover, ac biosusceptometry is a non-invasive technique, radiation-free and harmless to the volunteers, as well as an important research tool in the pharmaceutical, pharmacological and physiological investigations.

  13. Non-contact measurement of diamagnetic susceptibility change by a magnetic levitation technique

    NASA Astrophysics Data System (ADS)

    Takahashi, K.; Mogi, I.; Awaji, S.; Watanabe, K.

    2011-03-01

    A new method for measuring the temperature dependence of the diamagnetic susceptibility is described. It is based on the Faraday method and employs a magnetic levitation technique. The susceptibility of a magnetically levitating diamagnetic sample is determined from the product of the magnetic flux density and the field gradient at the levitating position observed using a micro CCD camera. The susceptibility of a sample during containerless melting and solidification can be measured to a precision of better than ±0.05%. The temperature dependence of the susceptibility of paraffin wax was measured by the magnetic levitation technique with an accuracy of ±0.25%. This method enables sensitive and contactless measurements of the diamagnetic susceptibility across the melting point with in situ observations.

  14. Quartz helix magnetic susceptibility balance using the Curie-Cheneveau principle

    USGS Publications Warehouse

    Senftle, F.E.; Lee, M.D.; Monkewicz, A.A.; Mayo, J.W.; Pankey, T.

    1958-01-01

    A quartz spring balance is described which can be used to measure the magnetic susceptibility of submilligram amounts of sample. The magnetic field is supplied by a moving permanent magnet, and the susceptibility is determined by the deflection of the spring observed in a measuring microscope. The apparatus is calibrated by a comparison standard (platinum) and results are shown for platinum, nickel aluminate, lead, manganese, and sucrose. A precision of better than 2% can be obtained on submilligram amounts of paramagnetic substances having a magnetic susceptibility of from 1 to 50??10-6 emu/g. On weakly paramagnetic or diamagnetic substances comparable precision can be obtained on less than 10 mg amounts of sample. ?? 1958 The American Institute of Physics.

  15. The effect of surface grain reversal on the AC losses of sintered Nd-Fe-B permanent magnets

    NASA Astrophysics Data System (ADS)

    Moore, Martina; Roth, Stefan; Gebert, Annett; Schultz, Ludwig; Gutfleisch, Oliver

    2015-02-01

    Sintered Nd-Fe-B magnets are exposed to AC magnetic fields in many applications, e.g. in permanent magnet electric motors. We have measured the AC losses of sintered Nd-Fe-B magnets in a closed circuit arrangement using AC fields with root mean square-values up to 80 mT (peak amplitude 113 mT) over the frequency range 50 to 1000 Hz. Two magnet grades with different dysprosium content were investigated. Around the remanence point the low grade material (1.7 wt% Dy) showed significant hysteresis losses; whereas the losses in the high grade material (8.9 wt% Dy) were dominated by classical eddy currents. Kerr microscopy images revealed that the hysteresis losses measured for the low grade magnet can be mainly ascribed to grains at the sample surface with multiple domains. This was further confirmed when the high grade material was subsequently exposed to DC and AC magnetic fields. Here a larger number of surface grains with multiple domains are also present once the step in the demagnetization curve attributed to the surface grain reversal is reached and a rise in the measured hysteresis losses is evident. If in the low grade material the operating point is slightly offset from the remanence point, such that zero field is not bypassed, its AC losses can also be fairly well described with classical eddy current theory.

  16. High susceptibility and low resistance allele frequency of Chrysodeixis includens (Lepidoptera: Noctuidae) field populations to Cry1Ac in Brazil.

    PubMed

    Yano, Silvia Ac; Specht, Alexandre; Moscardi, Flávio; Carvalho, Renato A; Dourado, Patrick M; Martinelli, Samuel; Head, Graham P; Sosa-Gómez, Daniel R

    2016-08-01

    The soybean looper (SBL), Chrysodeixis includens (Walker), is one of the most important soybean pests in Brazil. MON 87701 × MON 89788 soybean expressing Cry1Ac has been recently deployed in Brazil, providing high levels of control against the primary lepidopteran pests. To support insect resistance management (IRM) programmes, the baseline susceptibility of SBL to Cry1Ac was assessed, and the resistance allele frequency was estimated on the basis of an F2 screen. The toxicity (LC50 ) of Cry1Ac ranged from 0.39 to 2.01 µg mL(-1) diet among all SBL field populations collected from crop seasons 2008/09 to 2012/13, which indicated approximately fivefold variation. Cry1Ac diagnostic concentrations of 5.6 and 18 µg mL(-1) diet were established for monitoring purposes, and no shift in mortality was observed. A total of 626 F2 family lines derived from SBL collected from locations across Brazil during crop season 2014/15 were screened for the presence of Cry1Ac resistance alleles. None of the 626 families survived on MON 87701 × MON 89788 soybean leaf tissue (joint frequency 0.0004). SBL showed high susceptibility and low resistance allele frequency to Cry1Ac across the main soybean-producing regions in Brazil. These findings meet important criteria for effective IRM strategy. © 2015 Society of Chemical Industry. © 2015 Society of Chemical Industry.

  17. Development of a nano-tesla magnetic field shielded chamber and highly precise AC-susceptibility measurement coil at μK temperatures

    NASA Astrophysics Data System (ADS)

    Kumar, Anil; Prakash, Om; Ramakrishanan, S.

    2014-04-01

    A special sample measurement chamber has been developed to perform experiments at ultralow temperatures and ultralow magnetic field. A high permeability material known as cryoperm 10 and Pb is used to shield the measurement space consisting of the signal detecting set-up and the sample. The detecting setup consists of a very sensitive susceptibility coil wound on OFHC Cu bobbin.

  18. Single molecule magnet behavior of a pentanuclear Mn-based metallacrown complex: solid state and solution magnetic studies.

    PubMed

    Zaleski, Curtis M; Tricard, Simon; Depperman, Ezra C; Wernsdorfer, Wolfgang; Mallah, Talal; Kirk, Martin L; Pecoraro, Vincent L

    2011-11-21

    The magnetic behavior of the pentanuclear complex of formula Mn(II)(O(2)CCH(3))(2)[12-MC(Mn(III)(N)shi)-4](DMF)(6), 1, was investigated using magnetization and magnetic susceptibility measurements both in the solid state and in solution. Complex 1 has a nearly planar structure, made of a central Mn(II) ion surrounded by four peripheral Mn(III) ions. Solid state variable-field dc magnetic susceptibility experiments demonstrate that 1 possesses a low value for the total spin in the ground state; fitting appropriate expressions to the data results in antiferromangetic coupling both between the peripheral Mn(III) ions (J = -6.3 cm(-1)) and between the central Mn(II) ion and the Mn(III) ones (J' = -4.2 cm(-1)). In order to obtain a reasonable fit, a relatively large single ion magnetic anisotropy (D) value of 1 cm(-1) was necessary for the central Mn(II) ion. The single crystal magnetization measurements using a microsquid array display a very slight opening of the hysteresis loop but only at a very low temperature (0.04 K), which is in line with the ac susceptibility data where a slow relaxation of the magnetization occurs just around 2 K. In frozen solution, complex 1 displays a frequency dependent ac magnetic susceptibility signal with an energy barrier to magnetization reorientation (E) and relaxation time at an infinite temperature (τ(o)) of 14.7 cm(-1) and 1.4 × 10(-7) s, respectively, demonstrating the single molecule magnetic behavior in solution.

  19. Electroporation of cells using EM induction of ac fields by a magnetic stimulator

    NASA Astrophysics Data System (ADS)

    Chen, C.; Evans, J. A.; Robinson, M. P.; Smye, S. W.; O'Toole, P.

    2010-02-01

    This paper describes a method of effectively electroporating mammalian cell membranes with pulsed alternating-current (ac) electric fields at field strengths of 30-160 kV m-1. Although many in vivo electroporation protocols entail applying square wave or monotonically decreasing pulses via needles or electrode plates, relatively few have explored the use of pulsed ac fields. Following our previous study, which established the effectiveness of ac fields for electroporating cell membranes, a primary/secondary coil system was constructed to produce sufficiently strong electric fields by electromagnetic induction. The primary coil was formed from the applicator of an established transcranial magnetic stimulation (TMS) system, while the secondary coil was a purpose-built device of a design which could eventually be implanted into tissue. The effects of field strength, pulse interval and cumulative exposure time were investigated using microscopy and flow cytometry. Results from experiments on concentrated cell suspensions showed an optimized electroporation efficiency of around 50%, demonstrating that electroporation can be practicably achieved by inducing such pulsed ac fields. This finding confirms the possibility of a wide range of in vivo applications based on magnetically coupled ac electroporation.

  20. Heterogeneous anisotropic magnetic susceptibility of the myelin-water layers causes local magnetic field perturbations in axons.

    PubMed

    Puwal, Steffan; Roth, Bradley J; Basser, Peter J

    2017-04-01

    One goal of MRI is to determine the myelin water fraction in neural tissue. One approach is to measure the reduction in T 2 * arising from microscopic perturbations in the magnetic field caused by heterogeneities in the magnetic susceptibility of myelin. In this paper, analytic expressions for the induced magnetic field distribution are derived within and around an axon, assuming that the myelin susceptibility is anisotropic. Previous models considered the susceptibility to be piecewise continuous, whereas this model considers a sinusoidally varying susceptibility. Many conclusions are common in both models. When the magnetic field is applied perpendicular to the axon, the magnetic field in the intraaxonal space is uniformly perturbed, the magnetic field in the myelin sheath oscillates between the lipid and water layers, and the magnetic field in the extracellular space just outside the myelin sheath is heterogeneous. These field heterogeneities cause the spins to dephase, shortening T 2 *. When the magnetic field is applied along the axon, the field is homogeneous within water-filled regions, including between lipid layers. Therefore the spins do not dephase and the magnetic susceptibility has no effect on T 2 *. Generally, the response of an axon is given as the superposition of these two contributions. The sinusoidal model uses a different set of approximations compared with the piecewise model, so their common predictions indicate that the models are not too sensitive to the details of the myelin-water distribution. Other predictions, such as the sensitivity to water diffusion between myelin and water layers, may highlight differences between the two approaches. Copyright © 2016 John Wiley & Sons, Ltd. Copyright © 2016 John Wiley & Sons, Ltd.

  1. Definition of a magnetic susceptibility of conglomerates with magnetite particles. Particularities of defining single particle susceptibility

    NASA Astrophysics Data System (ADS)

    Sandulyak, A. A.; Sandulyak, A. V.; Ershova, V.; Pamme, N.; Ngmasom, B.; Iles, A.

    2017-11-01

    Data of a magnetic susceptibility of ferro-and the ferrimagnetic particles of many technogenic, natural, special media are especially demanded for the solution of various tasks connected with purposeful magnetic impact on these particles. One of productive approaches to definition of a magnetic susceptibility χ of these particles consists in receiving experimental data of a susceptibility of disperse samples 〈 χ 〉 with a disperse phase of these particles. The paper expounds and analyses the results of experiments on defining (by Faraday method in a magnetic field with intensity H = 90-730 kA/m) the magnetic susceptibility 〈 χ 〉 of disperse samples (conglomerates) with a given volume ratio γ of magnetite particles (γ = 0.0065-0.25). The corresponding families of concentration and field dependences are provided alongside with discussing the applicability of linear and exponential functions to describe these dependences. We consider the possibility of defining single particles susceptibility χ (with simultaneous obtaining field dependence of this susceptibility) by the commonly used relation χ = 〈 χ 〉 /γ both at relatively small (preferable for accuracy reasons) values γ - to γ = 0.02…0.025, as well as at increased values γ - up to γ = 0.25. The data χ are provided depending on H and correlating with known data at H < 90 kA/m; they are obtained at small values γ when with almost double distance between the neighbouring particles (in comparison with their proper dimensions) the mutual adverse (to determine valid data χ)magnetic impact of particles is practically excluded. The article also gives the data χ received at increased values γ with almost halved distance between the surfaces of the neighbouring particles. It is specified that in the studied (post-extreme) area of H both variants of obtained field dependencesχare functionally identical within the accuracy of a constant, and close to an exponential dependence χ ∼ 1/H0.75. With

  2. Demagnetization Treatment of Remanent Composite Microspheres Studied by Alternating Current Susceptibility Measurements

    PubMed Central

    van Berkum, Susanne; Erné, Ben H.

    2013-01-01

    The magnetic remanence of silica microspheres with a low concentration of embedded cobalt ferrite nanoparticles is studied after demagnetization and remagnetization treatments. When the microspheres are dispersed in a liquid, alternating current (AC) magnetic susceptibility spectra reveal a constant characteristic frequency, corresponding to the rotational diffusion of the microparticles; this depends only on particle size and liquid viscosity, making the particles suitable as a rheological probe and indicating that interactions between the microspheres are weak. On the macroscopic scale, a sample with the dry microparticles is magnetically remanent after treatment in a saturating field, and after a demagnetization treatment, the remanence goes down to zero. The AC susceptibility of a liquid dispersion, however, characterizes the remanence on the scale of the individual microparticles, which does not become zero after demagnetization. The reason is that an individual microparticle contains only a relatively small number of magnetic units, so that even if they can be reoriented magnetically at random, the average vector sum of the nanoparticle dipoles is not negligible on the scale of the microparticle. In contrast, on the macroscopic scale, the demagnetization procedure randomizes the orientations of a macroscopic number of magnetic units, resulting in a remanent magnetization that is negligible compared to the saturation magnetization of the entire sample. PMID:24009021

  3. Numerical and theoretical evaluations of AC losses for single and infinite numbers of superconductor strips with direct and alternating transport currents in external AC magnetic field

    NASA Astrophysics Data System (ADS)

    Kajikawa, K.; Funaki, K.; Shikimachi, K.; Hirano, N.; Nagaya, S.

    2010-11-01

    AC losses in a superconductor strip are numerically evaluated by means of a finite element method formulated with a current vector potential. The expressions of AC losses in an infinite slab that corresponds to a simple model of infinitely stacked strips are also derived theoretically. It is assumed that the voltage-current characteristics of the superconductors are represented by Bean's critical state model. The typical operation pattern of a Superconducting Magnetic Energy Storage (SMES) coil with direct and alternating transport currents in an external AC magnetic field is taken into account as the electromagnetic environment for both the single strip and the infinite slab. By using the obtained results of AC losses, the influences of the transport currents on the total losses are discussed quantitatively.

  4. 3D and 4D magnetic susceptibility tomography based on complex MR images

    DOEpatents

    Chen, Zikuan; Calhoun, Vince D

    2014-11-11

    Magnetic susceptibility is the physical property for T2*-weighted magnetic resonance imaging (T2*MRI). The invention relates to methods for reconstructing an internal distribution (3D map) of magnetic susceptibility values, .chi. (x,y,z), of an object, from 3D T2*MRI phase images, by using Computed Inverse Magnetic Resonance Imaging (CIMRI) tomography. The CIMRI technique solves the inverse problem of the 3D convolution by executing a 3D Total Variation (TV) regularized iterative convolution scheme, using a split Bregman iteration algorithm. The reconstruction of .chi. (x,y,z) can be designed for low-pass, band-pass, and high-pass features by using a convolution kernel that is modified from the standard dipole kernel. Multiple reconstructions can be implemented in parallel, and averaging the reconstructions can suppress noise. 4D dynamic magnetic susceptibility tomography can be implemented by reconstructing a 3D susceptibility volume from a 3D phase volume by performing 3D CIMRI magnetic susceptibility tomography at each snapshot time.

  5. Combined 677CC/1298AC genotypes of methylenetetrahydrofolate reductase (MTHFR ) reduce susceptibility to precursor B lymphoblastic leukemia in a Chinese population.

    PubMed

    Lv, Ling; Wu, Cuie; Sun, Henjuan; Zhu, Saijuan; Yang, Yongchen; Chen, Xi; Fu, Hua; Bao, Liming

    2010-06-01

    The methylenetetrahydrofolate reductase (MTHFR) encodes a major enzyme in folate metabolism. It has been suggested that two MTHFR polymorphisms, 677C>T and 1298A>C, influence risk of acute lymphoblastic leukemia (ALL). Most studies on relation of MTHFR polymorphisms to ALL susceptibility have been in pediatric populations because ALL is relatively rare in adults. Here, we report a case-control study of 127 Chinese patients with adult precursor B lymphoblastic leukemia (B-ALL) to examine correlation between the MTHFR polymorphisms and B-ALL susceptibility in adults. Our data show that although the prevalence of genotype 1298CC was significantly higher in the female patients than in the controls (P = 0.04), the differences in distributions of combined genotypes of 1298CC with either 677CC or 677CT between the cases and the controls were statistically insignificant. Haplotype analysis revealed no significant difference between the cases and the controls. The prevalence for joint MTHFR genotypes 677CC/1298AC was significantly lower in the female B-ALL cases than in the controls [odds ratio (OR) = 0.06, 95% CI = 0.00-0.53, P = 0.0033] and no differences among the men [OR = 0.71, 95% CI = 0.20-2.53, P = 0.55], suggesting that protective effects of combined MTHFR 677CC/1298AC genotypes on susceptibility of adult B-ALL are gender bias toward women with 677CC/1298AC women being at a 17-fold reduced odds to develop B-ALL.

  6. Magnetic susceptibility and dielectric properties of peat in Central Kalimantan, Indonesia

    NASA Astrophysics Data System (ADS)

    Budi, Pranitha Septiana; Zulaikah, Siti; Hidayat, Arif; Azzahro, Rosyida

    2017-07-01

    Peatlands dominate almost all regions of Borneo, yet its utilization has not been developed optimally. Any information in this field could be obtained using soil magnetization methods by determining the magnetic succeptibility in terms of magnetic susceptibility value that could describe the source and type of magnetic minerals which could describe the source and type of magnetic minerals. Moreover, the dielectric properties of peat soil were also investigated to determine the level of water content by using the dielectric constant value. Samples was taken at six different locations along Pulang pisau to Berengbengkel. Magnetic susceptibility mass value at these locations ranged between -0.0009 - 0.712 (×10-6 m3/kg). Based on the average magnetic susceptibility value, samples that were taken from T1, T3 and T5 belonged to the type of paramagnetic mineral, while samples which were taken from T2, T4 and T6 belonged to the group of diamagnetic mineral. The low value of magnetic susceptibility of peat was probably derived from the pedogenic process. The average value of peat soil in six locations has a large dielectric constant value that is 28.2 which indicated that there was considerable moisture content due to the hydrophilic nature of peatland which means that the ability of peat in water binding is considerably high.

  7. Current distribution and ac susceptibility response of a thin superconducting disc in an axial field: a theoretical approach

    NASA Astrophysics Data System (ADS)

    Aruna, S. A.; Zhang, P.; Lin, F. Y.; Ding, S. Y.; Yao, X. X.

    2000-04-01

    Within the framework of the thermally activated process of the flux line or flux line bundles, and by time integration of the 1D equation of motion of the circulating current density icons/Journals/Common/vecJ" ALT="vecJ" ALIGN="TOP"/> (icons/Journals/Common/rho" ALT="rho" ALIGN="TOP"/> ,t ), which is suitable for thin superconducting films (R >>d ,icons/Journals/Common/le" ALT="le" ALIGN="TOP"/> icons/Journals/Common/lambda" ALT="lambda" ALIGN="TOP"/> ), we present numerical calculations of the current profiles, magnetization hysteresis loops and ac susceptibility icons/Journals/Common/chi" ALT="chi" ALIGN="TOP"/> n = icons/Journals/Common/chi" ALT="chi" ALIGN="TOP"/> ´n +iicons/Journals/Common/chi" ALT="chi" ALIGN="TOP"/> ´´n for n = 1, 3 and 5 of a thin disc immersed in an axial time-dependent external magnetic field Ba (t ) = Bdc +Bac cos(2icons/Journals/Common/pi" ALT="pi" ALIGN="TOP"/> icons/Journals/Common/nu" ALT="nu" ALIGN="TOP"/> t ). Our calculated results are compared with those of the critical state model (CSM) and found to prove the approximate validity of the CSM below the irreversibility field. The differences between our computed results and those of the CSM are also discussed.

  8. Magnetic susceptibility of DHCP NpPd3

    NASA Astrophysics Data System (ADS)

    Walker, H. C.; McEwen, K. A.; Boulet, P.; Colineau, E.; Wastin, F.

    2005-04-01

    We have measured the magnetic susceptibility and magnetisation of the double-hexagonal close-packed (DHCP) phase of NpPd3 from T=2-300 K in magnetic fields up to 7 T. Our results clearly indicate the presence of two phase transitions in this compound, at 10 and 30 K. At higher temperatures, the susceptibility exhibits Curie-Weiss behaviour, with an effective moment of 2.8 μB/Np atom. This result implies that the Np ions are trivalent, with a 5f4 electronic configuration. Below the 30 K transition, the magnetisation of NpPd3 displays hysteresis in fields below 0.1 T with a residual ferromagnetic moment of the order of 0.06 μB/Np atom.

  9. Enhancement of MS2D Bartington point measurement of soil magnetic susceptibility

    NASA Astrophysics Data System (ADS)

    Fabijańczyk, Piotr; Zawadzki, Jarosław

    2015-04-01

    Field magnetometry is fast method used to assess the potential soil pollution. The most popular device used to measure the soil magnetic susceptibility on the soil surface is a MS2D Bartington. Single reading using MS2D device of soil magnetic susceptibility is low time-consuming but often characterized by considerable errors related to the instrument or environmental and lithogenic factors. Typically, in order to calculate the reliable average value of soil magnetic susceptibility, a series of MS2D readings is performed in the sample point. As it was analyzed previously, such methodology makes it possible to significantly reduce the nugget effect of the variograms of soil magnetic susceptibility that is related to the micro-scale variance and measurement errors. The goal of this study was to optimize the process of taking a series of MS2D readings, whose average value constitutes a single measurement, in order to take into account micro-scale variations of soil magnetic susceptibility in proper determination of this parameter. This was done using statistical and geostatistical analyses. The analyses were performed using field MS2D measurements that were carried out in the study area located in the direct vicinity of the Katowice agglomeration. At 150 sample points 10 MS2D readings of soil magnetic susceptibility were taken. Using this data set, series of experimental variograms were calculated and modeled. Firstly, using single random MS2D reading for each sample point, and next using the data set increased by adding one more MS2D reading, until their number reached 10. The parameters of variogram: nugget effect, sill and range of correlation were used to determine the most suitable number of MS2D readings at sample point. The distributions of soil magnetic susceptibility at sample point were also analyzed in order to determine adequate number of readings enabling to calculate reliable average soil magnetic susceptibility. The research leading to these results has

  10. Magnetic susceptibility properties of pesticide contaminated volcanic soil

    NASA Astrophysics Data System (ADS)

    Agustine, Eleonora; Fitriani, Dini; Safiuddin, La Ode; Tamuntuan, Gerald; Bijaksana, Satria

    2013-09-01

    Pesticides, unfortunately, are still widely used in many countries as way to eradicate agricultural pests. As they are being used continuously over a long period of time, they accumulate as residues in soils posing serious threats to the environment. In this study, we study the changes in magnetite-rich volcanic soils that were deliberately contaminated by pesticide. Such changes, in any, would be useful in the detection of pesticide residue in contaminated soils. Two different types of magnetically strong volcanic soil from the area near Lembang, West Java, Indonesia were used in this study where they were contaminated with varying concentrations of pesticide. The samples were then measured for magnetic susceptibility at two different frequencies. The measurements were then repeated after a period of three months. We found a reduction of magnetic susceptibility as well as a reduction in SP (superparamagnetic) grains proportion in contaminated soil. These might be caused by pesticide-induced magnetic dissolution as supported by SEM analyses. However the impact of pesticide concentration as well as exposure time on magnetic dissolution is still inconclusive.

  11. Magnetic susceptibilities measured on rocks of the upper Cook Inlet, Alaska

    USGS Publications Warehouse

    Alstatt, A.A.; Saltus, R.W.; Bruhn, R.L.; Haeussler, Peter J.

    2002-01-01

    We have measured magnetic susceptibility in the field on most of the geologic rock formations exposed in the upper Cook Inlet near Anchorage and Kenai, Alaska. Measured susceptibilities range from less than our detection limit of 0.01 x 10-3 (SI) to greater than 100 x 10-3 (SI). As expected, mafic igneous rocks have the highest susceptibilities and some sedimentary rocks the lowest. Rocks of the Tertiary Sterling Formation yielded some moderate to high susceptibility values. Although we do not have detailed information on the magnetic mineralogy of the rocks measured here, the higher susceptibilities are sufficient to explain the magnitudes of some short-wavelength aeromagnetic anomalies observed on recent surveys of the upper Cook Inlet.

  12. Magnetic susceptibility variations in Loess sequences and their relationship to astronomical forcing

    NASA Technical Reports Server (NTRS)

    Verosub, Kenneth L.; Singer, Michael J.

    1992-01-01

    The long, well-exposed and often continuous sequences of loess found throughout the world are generally thought to provide an excellent opportunity for studying long-term, large-scale environmental change during the last few million years. In recent years, the most fruitful loess studies have been those involving the deposits of the loess in China. One of the most intriguing results of that work has been the discovery of an apparent correlation between variations in the magnetic susceptibility of the loess sequence and the oxygen isotope record of the deep sea. This correlation implies that magnetic susceptibility variations are being driven by astronomical parameters. However, the basic data have been interpreted in various ways by different authors, most of whom assumed that the magnetic minerals in the loess have not been affected by post-depositional processes. Using a chemical extraction procedure that allows us to separate the contribution of secondary pedogenic magnetic minerals from primary inherited magnetic minerals, we have found that the magnetic susceptibility of the Chinese paleosols is largely due to a pedogenic component which is present to a lesser degree in the loess. We have also found that the smaller inherited component of the magnetic susceptibility is about the same in the paleosols and the loess. These results demonstrate the need for additional study of the processes that create magnetic susceptibility variations in order to interpret properly the role of astronomical forcing in producing these variations.

  13. Magnetic susceptibility and magnetic resonance measurements of the moisture content and hydration condition of a magnetic mixture material

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Tsukada, K., E-mail: tsukada@cc.okayama-u.ac.jp; Kusaka, T.; Saari, M. M.

    2014-05-07

    We developed a magnetic measurement method to measure the moisture content and hydration condition of mortar as a magnetic mixture material. Mortar is a mixture of Portland cement, sand, and water, and these materials exhibit different magnetic properties. The magnetization–magnetic field curves of these components and of mortars with different moisture contents were measured, using a specially developed high-temperature-superconductor superconducting quantum interference device. Using the differences in magnetic characteristics, the moisture content of mortar was measured at the ferromagnetic saturation region over 250 mT. A correlation between magnetic susceptibility and moisture content was successfully established. After Portland cement and water aremore » mixed, hydration begins. At the early stage of the hydration/gel, magnetization strength increased over time. To investigate the magnetization change, we measured the distribution between bound and free water in the mortar in the early stage by magnetic resonance imaging (MRI). The MRI results suggest that the amount of free water in mortar correlates with the change in magnetic susceptibility.« less

  14. Multifractal model of magnetic susceptibility distributions in some igneous rocks

    USGS Publications Warehouse

    Gettings, Mark E.

    2012-01-01

    Measurements of in-situ magnetic susceptibility were compiled from mainly Precambrian crystalline basement rocks beneath the Colorado Plateau and ranges in Arizona, Colorado, and New Mexico. The susceptibility meter used measures about 30 cm3 of rock and measures variations in the modal distribution of magnetic minerals that form a minor component volumetrically in these coarsely crystalline granitic to granodioritic rocks. Recent measurements include 50–150 measurements on each outcrop, and show that the distribution of magnetic susceptibilities is highly variable, multimodal and strongly non-Gaussian. Although the distribution of magnetic susceptibility is well known to be multifractal, the small number of data points at an outcrop precludes calculation of the multifractal spectrum by conventional methods. Instead, a brute force approach was adopted using multiplicative cascade models to fit the outcrop scale variability of magnetic minerals. Model segment proportion and length parameters resulted in 26 676 models to span parameter space. Distributions at each outcrop were normalized to unity magnetic susceptibility and added to compare all data for a rock body accounting for variations in petrology and alteration. Once the best-fitting model was found, the equation relating the segment proportion and length parameters was solved numerically to yield the multifractal spectrum estimate. For the best fits, the relative density (the proportion divided by the segment length) of one segment tends to be dominant and the other two densities are smaller and nearly equal. No other consistent relationships between the best fit parameters were identified. The multifractal spectrum estimates appear to distinguish between metamorphic gneiss sites and sites on plutons, even if the plutons have been metamorphosed. In particular, rocks that have undergone multiple tectonic events tend to have a larger range of scaling exponents.

  15. Microstructure, hyperfine interaction and magnetic transition of Fe-25%Ni-5%Si-x%Co alloys

    NASA Astrophysics Data System (ADS)

    Gungunes, H.

    2016-12-01

    Morphological and magnetic properties in Fe-25%Ni-5%Si-x%Co (x = 0, 10, 15) alloys are investigated. Scanning electron microscopy (SEM), Mössbauer spectroscopy and AC magnetic susceptibility measurements are used to determine the physical properties of alloys. The martensite morphology changed depending on the Co content. The Mössbauer study shows that the volume fraction and hyperfine field of martensite increases while isomer shift values decrease with increasing Co content. On the other hand; AC susceptibility results showed that; Co is an effective element which can be used to control both the magnetic transition and martensitic transformation temperatures.

  16. Magnetic Susceptibility and Heavy Metals in Guano from South Sulawesi Caves

    NASA Astrophysics Data System (ADS)

    Rifai, H.; Putra, R.; Fadila, M. R.; Erni, E.; Wurster, C. M.

    2018-04-01

    Measurement of some magnetic properties have been performed on vertical profile from South Sulawesi caves (Mampu and Bubau) by using low cost, rapid, sensitive and non destructive magnetic method. The aim is to attempt to use magnetic characters as a fingerprint for anthropogenic pollution in the caves. Guano samples were collected every 5 cm at a certain section of Mampu and Bubau cave, South Sulawesi, starting from surface through 300 cm in depth of mampu Cave and 30 cm of Bubau Cave. The magnetic parameters such as magnetic susceptibility and percentage frequency dependence susceptibility were measured using the Bartington MS2-MS2B instruments and supported by X-Ray Fluoroscence (XRF) to know their element composition. The results show that the samples had variations in magnetic susceptibility from 3.5 to 242.6 x 10‑8 m3/kg for Mampu Cave and from 8.6 to 106.5 x 10‑8 m3/kg for Bubau Cave and also magnetic domain. Then, the XRF results show that the caves contain several heavy metals. Magnetic and heavy metal analyses showing that the magnetic minerals in caves are lithogenic (Fe-bearing minerals) in origin and anthropogenic (Zn content) in the caves.

  17. Anisotropy of the magnetic susceptibility of gallium

    USGS Publications Warehouse

    Pankey, T.

    1960-01-01

    The bulk magnetic susceptibilities of single gallium crystals and polycrystalline gallium spheres were measured at 25??C. The following anisotropic diamagnetic susceptibilities were found: a axis (-0.119??0. 001)??10-6 emu/g, b axis (-0.416??0.002)??10 -6 emu/g, and c axis (-0.229??0.001) emu/g. The susceptibility of the polycrystalline spheres, assumed to be the average value for the bulk susceptibility of gallium, was (-0.257??0.003)??10-6 emu/g at 25??C, and (-0.299??0.003)??10-6 emu/g at -196??C. The susceptibility of liquid gallium was (0.0031??0.001) ??10-6 emu/g at 30??C and 100??C. Rotational diagrams of the susceptibilities in the three orthogonal planes of the unit cell were not sinusoidal. The anisotropy in the single crystals was presumably caused by the partial overlap of Brillouin zone boundaries by the Fermi-energy surface. The large change in susceptibility associated with the change in state was attributed to the absence of effective mass influence in the liquid state. ?? 1960 The American Institute of Physics.

  18. Accuracy of MRI-based Magnetic Susceptibility Measurements

    NASA Astrophysics Data System (ADS)

    Russek, Stephen; Erdevig, Hannah; Keenan, Kathryn; Stupic, Karl

    Magnetic Resonance Imaging (MRI) is increasingly used to map tissue susceptibility to identify microbleeds associated with brain injury and pathologic iron deposits associated with neurologic diseases such as Parkinson's and Alzheimer's disease. Field distortions with a resolution of a few parts per billion can be measured using MRI phase maps. The field distortion map can be inverted to obtain a quantitative susceptibility map. To determine the accuracy of MRI-based susceptibility measurements, a set of phantoms with paramagnetic salts and nano-iron gels were fabricated. The shapes and orientations of features were varied. Measured susceptibility of 1.0 mM GdCl3 solution in water as a function of temperature agreed well with the theoretical predictions, assuming Gd+3 is spin 7/2. The MRI susceptibility measurements were compared with SQUID magnetometry. The paramagnetic susceptibility sits on top of the much larger diamagnetic susceptibility of water (-9.04 x 10-6), which leads to errors in the SQUID measurements. To extract out the paramagnetic contribution using standard magnetometry, measurements must be made down to low temperature (2K). MRI-based susceptometry is shown to be as or more accurate than standard magnetometry and susceptometry techniques.

  19. Van Vleck and the magnetic susceptibilities of gaseous molecules

    NASA Astrophysics Data System (ADS)

    Meyer, Horst

    2011-03-01

    In his 1927 Physical Review article and in his 1932 book, ~The Theory of Electric and Magnetic Susceptibilities,~Van Vleck used the new quantum theory to derive the magnetic susceptibilities of O2 and NO in their gaseous form ~and compared them with experiments. ~He was therefore very interested in low temperature susceptibility experiments on O2 at Oxford University in 1954 where individual O2 molecules were trapped in small, almost spherical cages in organic clathrates. Correspondence between him and this speaker, then at Oxford, led to further measurements of O2 and also of NO in such clathrates, to theory and to subsequent publications and correspondence. Later communication with Van Vleck on the magnetism in rare earth iron garnets, a subject of long-term interest to him, will be described ~in connection with experiments carried out at Duke University. Some fond personal ~recollections of this speaker of his interaction with Van Vleck - both while at Harvard, during visits and through correspondence which extended into the seventies - will be presented.

  20. Quantitative susceptibility mapping (QSM): Decoding MRI data for a tissue magnetic biomarker

    PubMed Central

    Wang, Yi; Liu, Tian

    2015-01-01

    In MRI, the main magnetic field polarizes the electron cloud of a molecule, generating a chemical shift for observer protons within the molecule and a magnetic susceptibility inhomogeneity field for observer protons outside the molecule. The number of water protons surrounding a molecule for detecting its magnetic susceptibility is vastly greater than the number of protons within the molecule for detecting its chemical shift. However, the study of tissue magnetic susceptibility has been hindered by poor molecular specificities of hitherto used methods based on MRI signal phase and T2* contrast, which depend convolutedly on surrounding susceptibility sources. Deconvolution of the MRI signal phase can determine tissue susceptibility but is challenged by the lack of MRI signal in the background and by the zeroes in the dipole kernel. Recently, physically meaningful regularizations, including the Bayesian approach, have been developed to enable accurate quantitative susceptibility mapping (QSM) for studying iron distribution, metabolic oxygen consumption, blood degradation, calcification, demyelination, and other pathophysiological susceptibility changes, as well as contrast agent biodistribution in MRI. This paper attempts to summarize the basic physical concepts and essential algorithmic steps in QSM, to describe clinical and technical issues under active development, and to provide references, codes, and testing data for readers interested in QSM. Magn Reson Med 73:82–101, 2015. © 2014 The Authors. Magnetic Resonance in Medicine Published by Wiley Periodicals, Inc. on behalf of International Society of Medicine in Resonance. This is an open access article under the terms of the Creative commons Attribution License, which permits use, distribution, and reproduction in any medium, provided the original work is properly cited. PMID:25044035

  1. Encouragement of Enzyme Reaction Utilizing Heat Generation from Ferromagnetic Particles Subjected to an AC Magnetic Field.

    PubMed

    Suzuki, Masashi; Aki, Atsushi; Mizuki, Toru; Maekawa, Toru; Usami, Ron; Morimoto, Hisao

    2015-01-01

    We propose a method of activating an enzyme utilizing heat generation from ferromagnetic particles under an ac magnetic field. We immobilize α-amylase on the surface of ferromagnetic particles and analyze its activity. We find that when α-amylase/ferromagnetic particle hybrids, that is, ferromagnetic particles, on which α-amylase molecules are immobilized, are subjected to an ac magnetic field, the particles generate heat and as a result, α-amylase on the particles is heated up and activated. We next prepare a solution, in which α-amylase/ferromagnetic particle hybrids and free, nonimmobilized chitinase are dispersed, and analyze their activities. We find that when the solution is subjected to an ac magnetic field, the activity of α-amylase immobilized on the particles increases, whereas that of free chitinase hardly changes; in other words, only α-amylase immobilized on the particles is selectively activated due to heat generation from the particles.

  2. High-temperature-superconducting magnetic susceptibility bolometer

    NASA Technical Reports Server (NTRS)

    Brasunas, J.; Lakew, B.; Lee, C.

    1992-01-01

    An infrared detector called the magnetic susceptibility bolometer is introduced which is based on the tmperature dependence of the diamagnetic screening of a high-Tc superconductor film near Tc. Results are reported for the response of a prototype model to modulated blackbody radiation. Possible improvements are discussed as is the potential sensitivity of an improved device.

  3. Magnetic domain structure imaging near sample surface with alternating magnetic force microscopy by using AC magnetic field modulated superparamagnetic tip.

    PubMed

    Cao, Yongze; Nakayama, Shota; Kumar, Pawan; Zhao, Yue; Kinoshita, Yukinori; Yoshimura, Satoru; Saito, Hitoshi

    2018-05-03

    For magnetic domain imaging with a very high spatial resolution by magnetic force microscopy the tip-sample distance should be as small as possible. However, magnetic imaging near sample surface is very difficult with conventional MFM because the interactive forces between tip and sample includes van der Waals and electrostatic forces along with magnetic force. In this study, we proposed an alternating magnetic force microscopy (A-MFM) which extract only magnetic force near sample surface without any topographic and electrical crosstalk. In the present method, the magnetization of a FeCo-GdOx superparamagnetic tip is modulated by an external AC magnetic field in order to measure the magnetic domain structure without any perturbation from the other forces near the sample surface. Moreover, it is demonstrated that the proposed method can also measure the strength and identify the polarities of the second derivative of the perpendicular stray field from a thin-film permanent magnet with DC demagnetized state and remanent state. © 2018 IOP Publishing Ltd.

  4. AC transport in p-Ge/GeSi quantum well in high magnetic fields

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Drichko, I. L.; Malysh, V. A.; Smirnov, I. Yu.

    2014-08-20

    The contactless surface acoustic wave technique is implemented to probe the high-frequency conductivity of a high-mobility p-Ge/GeSi quantum well structure in the regime of integer quantum Hall effect (IQHE) at temperatures 0.3–5.8 K and magnetic fields up to 18 T. It is shown that, in the IQHE regime at the minima of conductivity, holes are localized and ac conductivity is of hopping nature and can be described within the “two-site” model. The analysis of the temperature and magnetic-field-orientation dependence of the ac conductivity at odd filing factors enables us to determine the effective hole g-factor, |g{sub zz}|≈4.5. It is shownmore » that the in-plane component of the magnetic field leads to a decrease in the g-factor as well as increase in the cyclotron mass, which is explained by orbital effects in the complex valence band of germanium.« less

  5. Hard permanent magnet development trends and their application to A.C. machines

    NASA Technical Reports Server (NTRS)

    Mildrum, H. F.

    1981-01-01

    The physical and magnetic properties of Mn-Al-C, Fe-Cr-Co, and RE-TM (rare earth-transition metal intermetallics) in polymer and soft metal bonded or sintered form are considered for ac circuit machine usage. The manufacturing processes for the magnetic materials are reviewed, and the mechanical and electrical properties of the magnetic materials are compared, with consideration given to the reference Alnico magnet. The Mn-Al-C magnets have the same magnetic properties and costs as Alnico units, operate well at low temperatures, but have poor high temperature performance. Fe-Cr-Co magnets also have comparable cost to Alnico magnets, and operate at high or low temperature, but are brittle, expensive, and contain Co. RE-Co magnets possess a high energy density, operate well in a wide temperature range, and are expensive. Recommendation for exploring the rare-earth alternatives are offered.

  6. Prediction of Stroke Subtype and Recanalization Using Susceptibility Vessel Sign on Susceptibility-Weighted Magnetic Resonance Imaging.

    PubMed

    Kang, Dong-Wan; Jeong, Han-Gil; Kim, Do Yeon; Yang, Wookjin; Lee, Seung-Hoon

    2017-06-01

    The susceptibility vessel sign (SVS) is a hypointense signal visualized because of the susceptibility effect of thrombi, sensitively detected on susceptibility-weighted magnetic resonance imaging. The relationship of SVS parameters with the stroke subtype and recanalization status after endovascular treatment remains uncertain. The data from 89 patients with acute stroke caused by anterior circulation infarcts who underwent susceptibility-weighted magnetic resonance imaging before endovascular treatment were examined. Independent reviewers, blinded to the stroke subtype and recanalization status, measured the SVS diameter, length, and estimated volume. The intra- and interrater agreements of the SVS parameters were assessed. The SVS was identified in 78% of the patients. SVS was more commonly associated with cardioembolism than with noncardioembolism ( P =0.01). The SVS diameter ( P <0.01) and length ( P =0.01) were larger in the cardioembolism group. The SVS diameter was larger in the recanalization group (thrombolysis in cerebral infarction ≥2b) than in the nonrecanalization group ( P =0.04). Multivariable analysis revealed that the SVS diameter was an independent predictor of cardioembolism (adjusted odds ratio, 1.97; 95% confidence interval, 1.34-2.90; P <0.01). There was no significant association between the SVS volume and the recanalization status (adjusted odds ratio, 1.003; 95% confidence interval, 0.999-1.006; P =0.12). The optimal cutoff value of the SVS diameter for the cardioembolism was 5.5 mm (sensitivity, 45.6%; specificity, 93.8%). Increased SVS diameter on susceptibility-weighted magnetic resonance imaging may predict cardioembolism. No clear association was found between SVS volume and endovascular recanalization. © 2017 The Authors.

  7. Measured losses in superconductor magnets for 60-Hertz ac operation.

    NASA Technical Reports Server (NTRS)

    Hamlet, I. L.; Kilgore, R. A.

    1971-01-01

    Results of an experimental study of electrical losses in superconductor magnets. Preliminary 60-Hz ac loss data are presented for coils constructed of Nb3Sn ribbon, Nb-Ti cable, and multifilament Nb-Ti. Losses have been measured for different size coils up to approximately 20 cm in diameter. Of the conductor types tested, Nb3Sn ribbon has the lowest losses for ac operation. In Nb3Sn-ribbon coils of different sizes, the loss per unit length of conductor is shown to decrease with a decrease in the rate of change of current and to increase, in general, with increase in coil size. An important aspect of the study is the high degree of repeatability of the data.

  8. Encouragement of Enzyme Reaction Utilizing Heat Generation from Ferromagnetic Particles Subjected to an AC Magnetic Field

    PubMed Central

    Suzuki, Masashi; Aki, Atsushi; Mizuki, Toru; Maekawa, Toru; Usami, Ron; Morimoto, Hisao

    2015-01-01

    We propose a method of activating an enzyme utilizing heat generation from ferromagnetic particles under an ac magnetic field. We immobilize α-amylase on the surface of ferromagnetic particles and analyze its activity. We find that when α-amylase/ferromagnetic particle hybrids, that is, ferromagnetic particles, on which α-amylase molecules are immobilized, are subjected to an ac magnetic field, the particles generate heat and as a result, α-amylase on the particles is heated up and activated. We next prepare a solution, in which α-amylase/ferromagnetic particle hybrids and free, nonimmobilized chitinase are dispersed, and analyze their activities. We find that when the solution is subjected to an ac magnetic field, the activity of α-amylase immobilized on the particles increases, whereas that of free chitinase hardly changes; in other words, only α-amylase immobilized on the particles is selectively activated due to heat generation from the particles. PMID:25993268

  9. Magnetic fluid hyperthermia (MFH): Cancer treatment with AC magnetic field induced excitation of biocompatible superparamagnetic nanoparticles

    NASA Astrophysics Data System (ADS)

    Jordan, Andreas; Scholz, Regina; Wust, Peter; Fähling, Horst; Felix, Roland

    1999-07-01

    The story of hyperthermia with small particles in AC magnetic fields started in the late 1950s, but most of the studies were unfortunately conducted with inadequate animal systems, inexact thermometry and poor AC magnetic field parameters, so that any clinical implication was far behind the horizon. More than three decades later, it was found, that colloidal dispersions of superparamagnetic (subdomain) iron oxide nanoparticles exhibit an extraordinary specific absorption rate (SAR [ W/ g]), which is much higher at clinically tolerable H 0 f combinations in comparison to hysteresis heating of larger multidomain particles. This was the renaissance of a cancer treatment method, which has gained more and more attention in the last few years. Due to the increasing number of randomized clinical trials preferentially in Europe with conventional E-field hyperthermia systems, the general medical and physical experience in hyperthermia application is also rapidly growing. Taking this increasing clinical experience carefully into account together with the huge amount of new biological data on heat response of cells and tissues, the approach of magnetic fluid hyperthermia (MFH) is nowadays more promising than ever before. The present contribution reviews the current state of the art and some of the future perspectives supported by advanced methods of the so-called nanotechnology.

  10. Ising-like chain magnetism, Arrhenius magnetic relaxation, and case against 3D magnetic ordering in β-manganese phthalocyanine (C₃₂H₁₆MnN₈).

    PubMed

    Wang, Zhengjun; Seehra, Mohindar S

    2016-04-06

    Previous magnetic studies in the organic semiconductor β-manganese phthalocyanine (β-MnPc) have reported it to be a canted ferromagnet below T(C)  ≈  8.6 K. However, the recent result of the lack of a λ-type anomaly in the specific heat versus temperature data near the quoted T(C) has questioned the presence of long-range 3-dimensional (3D) magnetic ordering in this system. In this paper, detailed measurements and analysis of the temperature (2 K-300 K) and magnetic field (up to 90 kOe) dependence of the dc and ac magnetic susceptibilities in a powder sample of β-MnPc leads us to conclude that 3D long-range magnetic ordering is absent in this material. This is supported by the Arrott plots and the lack of a peak in the ac susceptibilities, χ' and χ″, near the quoted T(C). Instead, the system can be best described as an Ising-like chain magnet with Arrhenius relaxation of the magnetization governed by an intra-layer ferromagnetic exchange constant J/k(B)  =  2.6 K and the single ion anisotropy energy parameter |D|/k(B)  =  8.3 K. The absence of 3D long range order is consistent with the measured |D|/  >  J.

  11. Effects of AC/DC magnetic fields, frequency, and nanoparticle aspect ratio on cellular transfection of gene vectors

    NASA Astrophysics Data System (ADS)

    Ford, Kris; Mair, Lamar; Fisher, Mike; Rowshon Alam, Md.; Juliano, Rudolph; Superfine, Richard

    2008-10-01

    In order to make non-viral gene delivery a useful tool in the study and treatment of genetic disorders, it is imperative that these methodologies be further refined to yield optimal results. Transfection of magnetic nanoparticles and nanorods are used as non-viral gene vectors to transfect HeLa EGFP-654 cells that stably express a mutated enhanced green fluorescent protein (EGFP) gene. We deliver antisense oligonucleotides to these cells designed to correct the aberrant splicing caused by the mutation in the EGFP gene. We also transfect human bronchial endothelial cells and immortalized WI-38 lung cells with pEGFP-N1 vectors. To achieve this we bind the genes to magnetic nanoparticles and nanorods and introduce magnetic fields to effect transfection. We wish to examine the effects of magnetic fields on the transfection of these particles and the benefits of using alternating (AC) magnetic fields in improving transfection rates over direct (DC) magnetic fields. We specifically look at the frequency dependence of the AC field and particle aspect ratio as it pertains to influencing transfection rate. We posit that the increase in angular momentum brought about by the AC field and the high aspect ratio of the nanorod particles, is vital to generating the force needed to move the particle through the cell membrane.

  12. Magnetic field tunable ac electrical transport of LaFeO3-wax nanocomposites

    NASA Astrophysics Data System (ADS)

    Roy, Supratim; Mandal, S. K.; Debnath, Rajesh; Nath, Debajyoti; Dey, P.

    2018-04-01

    Single phase perovskite LaFeO3 nanoparticles have been prepared through chemical pyrophoric reaction process. It is further grinded with paraffin wax of quantity 0.5 wt% of total composition to obtain an organic composite 99.5%LaFeO3-0.5%Wax. Studies of ac electrical properties viz. complex impedance, dielectric response, loss coefficient have been done in presence of external dc magnetic field, which reveals a good magnetoimpedance (˜221%) and a negative magnetodielectric (˜ 64%). The value of impedance, its real and imaginary part is observed to increase with dc field. The composite exhibits high dielectric constant (˜4760). The ac conductivity is found to decrease with applied field and increase with ac frequency.

  13. Distinguishing magnetic blocking and surface spin-glass freezing in nickel ferrite nanoparticles

    NASA Astrophysics Data System (ADS)

    Nadeem, K.; Krenn, H.; Traussing, T.; Letofsky-Papst, I.

    2011-01-01

    Nickel ferrite nanoparticles dispersed in SiO2 matrix have been synthesized by sol-gel method. Structural analysis has been performed by using x-ray diffraction and transmission electron microscopy. Magnetic properties have been investigated by using superconducting quantum interference device magnetometry. In addition to the average blocking temperature peak at TB=120 K measured by a zero field cooled temperature scan of the dc susceptibility, an additional hump near 15 K is observed. Temperature dependent out-of-phase ac susceptibility shows the same features: one broad peak at high temperature and a second narrow peak at low temperature. The high temperature peak corresponds to magnetic blocking of individual nanoparticles, while the low temperature peak is attributed to surface spin-glass freezing which becomes dominant for decreasing particle diameter. To prove the dynamics of the spin (dis)order in both regimes of freezing and blocking, the frequency dependent ac susceptibility is investigated under a biasing dc field. The frequency shift in the "frozen" low-temperature ac susceptibility peak is fitted to a dynamic scaling law with a critical exponent zv=7.5, which indicates a spin-glass phase. Exchange bias is turned on at low temperature which signifies the existence of a strong core-shell interaction. Aging and memory effects are further unique fingerprints of a spin-glass freezing on the surface of isolated magnetic nanoparticles.

  14. Initial susceptibility and viscosity properties of low concentration ɛ-Fe3 N based magnetic fluid

    NASA Astrophysics Data System (ADS)

    Huang, Wei; Wu, Jianmin; Guo, Wei; Li, Rong; Cui, Liya

    2007-03-01

    In this paper, the initial susceptibility of ɛ-Fe3N magnetic fluid at volume concentrations in the range Φ = 0.0 ˜ 0.0446 are measured. Compared with the experimental initial susceptibility, the Langevin, Weiss and Onsager susceptibility were calculated using the data obtained from the low concentration ɛ-Fe3N magnetic fluid samples. The viscosity of the ɛ-Fe3N magnetic fluid at the same concentrations is measured. The result shows that, the initial susceptibility of the low concentration ɛ-Fe3N magnetic fluid is proportional to the concentration. A linear relationship between relative viscosity and the volume fraction is observed when the concentration Φ < 0.02.

  15. Bound Magnon Dominance of the Magnetic Susceptibility of the One-Dimensional Heisenberg Spin One-Half Ferromagnet Cyclohexylammonium Trichlorocuprate

    NASA Astrophysics Data System (ADS)

    Haines, Donald Noble

    1987-09-01

    This study is an experimental investigation of the differential magnetic susceptibility of the spin one -half, one-dimensional, Ising-Heisenberg ferromagnet (S = 1over 2,1d,HIF). Recent theoretical work predicts the existence of magnon bound states in this model system, and that these bound spin wave states dominate its thermodynamic properties. Further, the theories indicate that classical linearized spin wave theory fails completely in such systems, and may also be intrinsically incorrect in certain higher dimensional systems. The purpose of this research is to confirm the existence of bound magnons in the S = 1over 2,1d,HIF for the nearly Heisenberg case, and demonstrate the dominance of the bound states over the spin wave states in determining thermodynamic behavior. A preliminary numerical study was performed to determine the ranges of magnetic field and temperature at which bound magnons might be expected to make a significant contribution to the magnetic susceptibility and specific heat of the S = 1over 2,1d,HIF. It was found that bound magnons dominate at low and high fields, and spin waves dominate at intermediate fields. For anisotropies less than 2% bound magnons dominate the low temperature regime for all fields. To test the theoretical predictions cyclohexylammonium trichlorocuprate(II) (CHAC) was chosen as a model S = 1over 2,1d,HIF compound for experimental study. The differential susceptibility of a powder sample of CHAC was measured as a function of temperature in fields of 0, 1, 2, and 3T. The temperature range for these studies was 4.2K to 40K. Susceptibility measurements were performed using an ac mutual inductance bridge which employs a SQUID (Superconducting Quantum Interference Device) as a null detector. The design, calibration, and operation of this instrument are described. Data from the experiments compare favorably with the theoretical predictions, confirming the existence of bound magnons in the nearly Heisenberg S = 1over 2,1d

  16. The low magnetic field properties of superconducting bulk yttrium barium copper oxide - Sintered versus partially melted material

    NASA Technical Reports Server (NTRS)

    Hein, R. A.; Hojaji, H.; Barkatt, A.; Shafii, H.; Michael, K. A.; Thorpe, A. N.; Ware, M. F.; Alterescu, S.

    1989-01-01

    A comparison of the low magnetic field properties of sintered (990 C) and partially melted samples (1050 C) has been performed. Changes in the microstructure produced by recrystallization from the melt result in a significant increase in flux pinning at 77 K. Low-frequency (10-100 Hz), low-ac magnetic-field (0.01-9.0 Oe) ac susceptibility data show that gross changes in the loss component accompany the observed changes in microstructure. The effects of applied dc magnetic fields (10-220 Oe) on the ac responses of these microstructures have also been probed.

  17. Crystal structure and partial Ising-like magnetic ordering of orthorhombic D y 2 Ti O 5

    DOE PAGES

    Shamblin, Jacob; Calder, Stuart; Dun, Zhiling; ...

    2016-07-12

    The structure and magnetic properties of orthorhombic Dy 2TiO 5 have been investigated using x-ray diffraction, neutron diffraction, and alternating current (ac)/direct current (dc) magnetic susceptibility measurements. In this paper, we report a continuous structural distortion below 100 K characterized by negative thermal expansion in the [0 1 0] direction. Neutron diffraction and magnetic susceptibility measurements revealed that two-dimensional (2D) magnetic ordering begins at 3.1 K, which is followed by a three-dimensional magnetic transition at 1.7 K. The magnetic structure has been solved through a representational analysis approach and can be indexed with the propagation vector k = [0 1/2more » 0]. The spin structure corresponds to a coplanar model of interwoven 2D “sheets” extending in the [0 1 0] direction. The local crystal field is different for each Dy 3+ ion (Dy1 and Dy2), one of which possesses strong uniaxial symmetry indicative of Ising-like magnetic ordering. In conclusion, consequently, two succeeding transitions under magnetic field are observed in the ac susceptibility, which are associated with flipping each Dy 3+ spin independently.« less

  18. Magnetic susceptibility and exchange coupling in the mineral ardennite

    USGS Publications Warehouse

    Thorpe, A.N.; Senftle, F.E.; Donnay, G.

    1969-01-01

    Ardennite, a rare silicate mineral, contains about 19 wt.% manganese. Some of the manganese atoms are in positions which are close enough to allow negative exchange and hence a reduction of the total magnetic susceptibility. It is shown that the susceptibility can be accounted for approximately by the treatment of Earnshaw and Lewis (1958) for S = 5 2 and a Hamiltonian H = -2g??Hb-2JS1??S2. ?? 1969.

  19. Complex magnetic behaviour and evidence of a superspin glass state in the binary intermetallic compound Er5Pd2

    NASA Astrophysics Data System (ADS)

    Sharma, Mohit K.; Yadav, Kavita; Mukherjee, K.

    2018-05-01

    The binary intermetallic compound Er5Pd2 has been investigated using dc and ac magnetic susceptibilities, magnetic memory effect, isothermal magnetization, non-linear dc susceptibility, heat capacity and magnetocaloric effect studies. Interestingly, even though the compound does not show geometrical frustration it undergoes glassy magnetic phase transition below 17.2 K. Investigation of dc magnetization and heat capacity data divulged absence of long-ranged magnetic ordering. Through the magnetic memory effect, time dependent magnetization and ac susceptibility studies it was revealed that the compound undergoes glass-like freezing below 17.2 K. Analysis of frequency dependence of this transition temperature through scaling and Arrhenius law; along with the Mydosh parameter indicate, that the dynamics in Er5Pd2 are due to the presence of strongly interacting superspins rather than individual spins. This phase transition was further investigated by non-linear dc susceptibility and was characterized by static critical exponents γ and δ. Our results indicate that this compound shows the signature of superspin glass at low temperature. Additionally, both conventional and inverse magnetocaloric effect was observed with a large value of magnetic entropy change and relative cooling power. Our results suggest that Er5Pd2 can be classified as a superspin glass system with large magnetocaloric effect.

  20. Anisotropy of susceptibility in rocks which are magnetically nonlinear even in low fields

    NASA Astrophysics Data System (ADS)

    Hrouda, František; Chadima, Martin; Ježek, Josef

    2018-06-01

    Theory of the low-field anisotropy of magnetic susceptibility (AMS) assumes a linear relationship between magnetization and magnetizing field, resulting in field-independent susceptibility. This is valid for diamagnetic and paramagnetic minerals by definition and also for pure magnetite, while in titanomagnetite, pyrrhotite and hematite the susceptibility may be clearly field-dependent even in low fields used in common AMS meter. Consequently, the use of the linear AMS theory is fully legitimate in the former minerals, but in principle incorrect in the latter ones. Automated measurement of susceptibility in 320 directions in variable low-fields ranging from 5 to 700 A m-1 was applied to more than 100 specimens of various pyrrhotite-bearing and titanomagnetite-bearing rocks. Data analysis showed that the anisotropic susceptibility remains well represented by an ellipsoid in the entire low-field span even though the ellipsoid increases its volume and eccentricity. The principal directions do not change their orientations with low-field in most specimens. Expressions for susceptibility as a function of field were found in the form of diagonal tensor whose elements are polynomials of low order. In a large proportion of samples, the susceptibility expressions can be further simplified to have one common skeleton polynomial.

  1. Quantitative interpretation of the magnetic susceptibility frequency dependence

    NASA Astrophysics Data System (ADS)

    Ustra, Andrea; Mendonça, Carlos A.; Leite, Aruã; Jovane, Luigi; Trindade, Ricardo I. F.

    2018-05-01

    Low-field mass-specific magnetic susceptibility (MS) measurements using multifrequency alternating fields are commonly used to evaluate concentration of ferrimagnetic particles in the transition of superparamagnetic (SP) to stable single domain (SSD). In classical palaeomagnetic analyses, this measurement serves as a preliminary assessment of rock samples providing rapid, non-destructive, economical and easy information of magnetic properties. The SP-SSD transition is relevant in environmental studies because it has been associated with several geological and biogeochemical processes affecting magnetic mineralogy. MS is a complex function of mineral-type and grain-size distribution, as well as measuring parameters such as external field magnitude and frequency. In this work, we propose a new technique to obtain quantitative information on grain-size variations of magnetic particles in the SP-SSD transition by inverting frequency-dependent susceptibility. We introduce a descriptive parameter named as `limiting frequency effect' that provides an accurate estimation of MS loss with frequency. Numerical simulations show the methodology capability in providing data fitting and model parameters in many practical situations. Real-data applications with magnetite nanoparticles and core samples from sediments of Poggio le Guaine section of Umbria-Marche Basin (Italy) provide additional information not clearly recognized when interpreting cruder MS data. Caution is needed when interpreting frequency dependence in terms of single relaxation processes, which are not universally applicable and depend upon the nature of magnetic mineral in the material. Nevertheless, the proposed technique is a promising tool for SP-SSD content analyses.

  2. [Correlativity study of the distribution of soil magnetic susceptibility and the heavy metal contents in Xi'an City].

    PubMed

    Chen, Xiu-Duan; Lu, Xin-Wei; Yang, Guang

    2013-03-01

    The magnetic susceptibility and the concentrations of Co, Cr, Cu, Pb, Sn, Sr and Ba in topsoil samples from Xi'an City were measured to study their spatial distribution and their correlation in this study. The results show that the concentrations of all measured heavy metals are higher than their background values in Cinnamon topsoil, which is the main soil type of Xi'an City. The heavy metals concentrations and the magnetic susceptibility of the studied samples display moderate variance. Co, Cr, Cu, Pb, Sn, Sr and Ba are significantly positively correlated with low-frequency magnetic susceptibility, while are significantly negatively correlated with frequency susceptibility. The spatial distribution of low-frequency magnetic susceptibility is identical with the concentrations of Pb and Cu. However, the spatial variation of frequency magnetic susceptibility is different from the concentrations of Co, Cr and Ba. The pollution assessment results show that the heavy metal pollution in topsoil of Xi'an City is moderate. The spatial contribution of the pollution load index was significantly correlated with the magnetic susceptibility of topsoil in Xi'an City. Therefore, soil magnetic susceptibility can be used as an effective monitoring means for heavy metal pollution in urban soil.

  3. A torque balance measurement of anisotropy of the magnetic susceptibility in white matter.

    PubMed

    van Gelderen, Peter; Mandelkow, Hendrik; de Zwart, Jacco A; Duyn, Jeff H

    2015-11-01

    Recent MRI studies have suggested that the magnetic susceptibility of white matter (WM) in the human brain is anisotropic, providing a new contrast mechanism for the visualization of fiber bundles and allowing the extraction of cellular compartment-specific information. This study provides an independent confirmation and quantification of this anisotropy. Anisotropic magnetic susceptibility results in a torque exerted on WM when placed in a uniform magnetic field, tending to align the WM fibers with the field. To quantify the effect, excised spinal cord samples were placed in a torque balance inside the magnet of a 7 T MRI system and the magnetic torque was measured as function of orientation. All tissue samples (n = 5) showed orienting effects, confirming the presence of anisotropic susceptibility. Analysis of the magnetic torque resulted in reproducible values for the WM volume anisotropy that ranged from 13.6 to 19.2 ppb. The independently determined anisotropy values confirm estimates inferred from MRI experiments and validate the use of anisotropy to extract novel information about brain fiber structure and myelination. © 2014 Wiley Periodicals, Inc.

  4. 3D linear inversion of magnetic susceptibility data acquired by frequency domain EMI

    NASA Astrophysics Data System (ADS)

    Thiesson, J.; Tabbagh, A.; Simon, F.-X.; Dabas, M.

    2017-01-01

    Low induction number EMI instruments are able to simultaneously measure a soil's apparent magnetic susceptibility and electrical conductivity. This family of dual measurement instruments is highly useful for the analysis of soils and archeological sites. However, the electromagnetic properties of soils are found to vary over considerably different ranges: whereas their electrical conductivity varies from ≤ 0.1 to ≥ 100 mS/m, their relative magnetic permeability remains within a very small range, between 1.0001 and 1.01 SI. Consequently, although apparent conductivity measurements need to be inverted using non-linear processes, the variations of the apparent magnetic susceptibility can be approximated through the use of linear processes, as in the case of the magnetic prospection technique. Our proposed 3D inversion algorithm starts from apparent susceptibility data sets, acquired using different instruments over a given area. A reference vertical profile is defined by considering the mode of the vertical distributions of both the electrical resistivity and of the magnetic susceptibility. At each point of the mapped area, the reference vertical profile response is subtracted to obtain the apparent susceptibility variation dataset. A 2D horizontal Fourier transform is applied to these variation datasets and to the dipole (impulse) response of each instrument, a (vertical) 1D inversion is performed at each point in the spectral domain, and finally the resulting dataset is inverse transformed to restore the apparent 3D susceptibility variations. It has been shown that when applied to synthetic results, this method is able to correct the apparent deformations of a buried object resulting from the geometry of the instrument, and to restore reliable quantitative susceptibility contrasts. It also allows the thin layer solution, similar to that used in magnetic prospection, to be implemented. When applied to field data it initially delivers a level of contrast

  5. In situ identification, pairing, and classification of meteorites from Antarctica through magnetic susceptibility measurements

    NASA Astrophysics Data System (ADS)

    Folco, Luigi; Rochette, Pierre; Gattacceca, JéRôMe; Perchiazzi, Natale

    2006-03-01

    We report on the effectiveness of using magnetic measurements in the search for meteorites on the Antarctic ice sheet, which is thus far the Earth's most productive terrain. Magnetic susceptibility measurements carried out with a pocket meter (SM30) during the 2003/04 PNRA meteorite collection expedition to northern Victoria Land (Antarctica) proved to be a rapid, sensitive, non-destructive means for the in situ identification, pairing, and classification of meteorites. In blue ice fields characterized by the presence of moraines and glacial drifts (e.g., Miller Butte, Roberts Butte, and Frontier Mountain), magnetic susceptibility measurements allowed discrimination of meteorites from abundant terrestrial stones that look like meteorites thanks to the relatively high magnetic susceptibility of the former with respect to terrestrial rocks. Comparative measurements helped identify 16 paired fragments found at Johannessen Nunataks, thereby reducing unnecessary duplication of laboratory analyses and statistical bias. Following classifications schemes developed by us in this and previous works, magnetic susceptibility measurements also helped classify stony meteorites directly in the field, thereby providing a means for selecting samples with higher research priority. A magnetic gradiometer capable of detecting perturbations in the Earth's magnetic field induced by the presence of meteorites was an efficient tool for locating meteorites buried in snow along the downwind margin of the Frontier Mountain blue ice field. Based on these results, we believe that magnetic sensors should constitute an additional payload for robotic search for meteorites on the Antarctic ice sheet and, by extension, on the surface of Mars where meteorite accumulations are predicted by theoretical works. Lastly, magnetic susceptibility data was successfully used to crosscheck the later petrographic classification of the 123 recovered meteorites, allowing the detection of misclassified or peculiar

  6. Static magnetic susceptibility of radiopaque NiTiPt and NiTiEr

    NASA Astrophysics Data System (ADS)

    Chovan, Drahomír; Gandhi, Abbasi; Butler, James; Tofail, Syed A. M.

    2018-04-01

    Magnetic properties of metallic alloys used in biomedical industry are important for the magnetic resonance imaging (MRI). If the alloys were to be used for long term implants or as guiding devices, safety of the patient as well as the medical staff has to be ensured. Strong response to the external magnetic field can cause mechanical damage to the patients body. In this paper we present magnetic susceptibility of nickel rich, ternary NiTiPt and NiTiEr to static magnetic field. We show that the magnetic susceptibility of these radiopaque alloys has values in low paramagnetic region comparable to the binary nickel-titanium. Furthermore, we studied the effect of the thermal and mechanical treatments on magnetic properties. Despite deviation from linear M (H) treated samples spanning small region around H = 0 , the linearity of the M (H) and χ =d M /d H values suggest that these ternary alloys are safe to use under MRI conditions.

  7. Rock magnetic and anisotropy of magnetic susceptibility(AMS) of earthquake affected soft sediments: Examples from Shillong and Latur (Deccan Trap), India.

    NASA Astrophysics Data System (ADS)

    Lakshmi, B. V., ,, Dr.; Gawali, Mr. Praveen B.; Deenadayalan, K., ,, Dr.; Ramesh, D. S., ,, Prof.

    2017-04-01

    Rock magnetic and anisotropy of magnetic susceptibility (AMS) of earthquake affected soft sediments: Examples from Shillong and Latur (Deccan Trap), India. B.V.Lakshmi, Praveen B.Gawali, K.Deenadayalan and D.S.Ramesh Indian Institute of Geomagnetism, plot 5, sector 18, Near Kalamboli Highway, New Panvel(W), Navi Mumbai 410218 Combined rock magnetism and anisotropy of magnetic susceptibility (AMS) studies on earthquake induced soft and non-soft sediments from Shillong and Latur, India have thrown up interesting results. The morphology of hysteresis loops, the pattern of isothermal remanent magnetization (IRM) acquisition, and temperature dependence of susceptibility indicate that titano-magnetite/magnetite is the main magnetic carrier in these sediments. We also analyzed the anisotropy of magnetic susceptibility (AMS) of liquefaction features within the seismically active Dauki fault, Shillong Plateau. We discovered that host sediments (non-liquefied), are characterized by an oblate AMS ellipsoid and liquefied sediment are characterized by a triaxial AMS ellipsoid, well grouped maximum susceptibility axis K1 (NNW-SSE trend). Field evidence and AMS analysis indicate that most of these features were emplaced by injection inferred to be due to seismically triggered fluidization. Anisotropy of magnetic susceptibility (AMS) of deformed and undeformed unconsolidated clay samples of Deccan Trap terrain from the 2000-year-old paleoearthquake site of Ther village, Maharashtra, India, was also studied. Such deposits are rare in the compact basaltic terrain because of which the results acquired are very important. The undeformed clay samples exhibit typical sedimentary fabric with an oblate AMS ellipsoid, whereas the deformed samples are tightly grouped in the inferred compression direction, probably effected by an earthquake, exhibiting prolate as well as oblate AMS ellipsoids. Rock magnetic and AMS methodology can help understand the behavior of different sediments to the

  8. Scaling ansatz for the ac magnetic response in two-dimensional spin ice

    NASA Astrophysics Data System (ADS)

    Otsuka, Hiromi; Takatsu, Hiroshi; Goto, Kazuki; Kadowaki, Hiroaki

    2014-10-01

    A theory for frequency-dependent magnetic susceptibility χ (ω ) is developed for thermally activated magnetic monopoles in a two-dimensional (2D) spin ice. By modeling the system in the vicinity of the ground-state manifold as a 2D Coulomb gas with an entropic interaction, and then as a 2D sine-Gordon model, we have shown that the susceptibility has a scaling form χ (ω ) /χ (0 ) =F (ω /ω1) , where the characteristic frequency ω1 is related to a charge correlation length between diffusively moving monopoles, and to the principal-breather excitation. The dynamical scaling is universal and applicable not only for kagome ice, but also for superfluid and superconducting films and generic 2D ices possibly including the artificial spin ice.

  9. Detection of superparamagnetic particles in soils developed on basalts using frequency- and amplitude-dependent magnetic susceptibility

    NASA Astrophysics Data System (ADS)

    Grison, H.; Petrovsky, E.; Kapicka, A.

    2016-12-01

    In rock, soil and environmental studies dealing with magnetic methods, the frequency-dependent magnetic susceptibility (κFD%) is parameter generally accepted as a tool for identification of ultrafine superparamagnetic (SP) particles. This parameter became an indicator of pedogenic magnetic fraction (increased pedogenesis). Despite the number of studies using this parameter, knowledge about threshold values of κFD% is not clear enough and this parameter may be misinterpreted. Moreover, in strongly magnetic soils, magnetic signal of the SP (mostly pedogenic) minerals may be masked by dominant lithological signal, carried by coarse-grain mineral fraction; therefore, influence of pedogenesis is hard to detect. The aim of this contribution is to compare results in determination of ultrafine SP magnetic particles in soils determined using different instruments: (a) Bartington MS2B dual-frequency meter, and (b) more sensitive AGICO Kappameter MFK1-FA. The values of the κFD % obtained by the Bartington MS2B varied from 0.9 to 5.8% (mass-specific magnetic susceptibility from 119 to 1533 × 10-8 m3/kg) while the AGICO MFK1-FA varied from 3.7 to 8.2% (mass-specific magnetic susceptibility from 295 to 1843 × 10-8 m3/kg). Although both instruments suggest significant portion of SP magnetic particles, the results can't be interpreted using the generally accepted threshold values based on Bartington data. However, our results suggest that relation between the mass-specific magnetic susceptibility and κFD% along whole soil profile may serve as suitable tool in discriminating between lithogenic and pedogenic control of magnetic fraction in the soil profile. Moreover, we propose new concept of identification of SP particles, based on field-dependent magnetic susceptibility. Its behaviour shows distinct features with significant change at amplitudes of about 100 A/m. Below this value, susceptibility decreases with increasing amplitude, reflecting saturation of magnetization due

  10. Slow magnetic relaxation at zero field in the tetrahedral complex [Co(SPh)4]2-.

    PubMed

    Zadrozny, Joseph M; Long, Jeffrey R

    2011-12-28

    The Ph(4)P(+) salt of the tetrahedral complex [Co(SPh)(4)](2-), possessing an S = (3)/(2) ground state with an axial zero-field splitting of D = -70 cm(-1), displays single-molecule magnet behavior in the absence of an applied magnetic field. At very low temperatures, ac magnetic susceptibility data show the magnetic relaxation time, τ, to be temperature-independent, while above 2.5 K thermally activated Arrhenius behavior is apparent with U(eff) = 21(1) cm(-1) and τ(0) = 1.0(3) × 10(-7) s. Under an applied field of 1 kOe, τ more closely approximates Arrhenius behavior over the entire temperature range. Upon dilution of the complex within a matrix of the isomorphous compound (Ph(4)P)(2)[Zn(SPh)(4)], ac susceptibility data reveal the molecular nature of the slow magnetic relaxation and indicate that the quantum tunneling pathway observed at low temperatures is likely mediated by intermolecular dipolar interactions. © 2011 American Chemical Society

  11. Magnetic Nanoparticle Thermometer: An Investigation of Minimum Error Transmission Path and AC Bias Error

    PubMed Central

    Du, Zhongzhou; Su, Rijian; Liu, Wenzhong; Huang, Zhixing

    2015-01-01

    The signal transmission module of a magnetic nanoparticle thermometer (MNPT) was established in this study to analyze the error sources introduced during the signal flow in the hardware system. The underlying error sources that significantly affected the precision of the MNPT were determined through mathematical modeling and simulation. A transfer module path with the minimum error in the hardware system was then proposed through the analysis of the variations of the system error caused by the significant error sources when the signal flew through the signal transmission module. In addition, a system parameter, named the signal-to-AC bias ratio (i.e., the ratio between the signal and AC bias), was identified as a direct determinant of the precision of the measured temperature. The temperature error was below 0.1 K when the signal-to-AC bias ratio was higher than 80 dB, and other system errors were not considered. The temperature error was below 0.1 K in the experiments with a commercial magnetic fluid (Sample SOR-10, Ocean Nanotechnology, Springdale, AR, USA) when the hardware system of the MNPT was designed with the aforementioned method. PMID:25875188

  12. Static electric and magnetic multipole susceptibilities for Dirac one-electron atoms in the ground state

    NASA Astrophysics Data System (ADS)

    Szmytkowski, Radosław; Łukasik, Grzegorz

    2016-09-01

    We present tabulated data for several families of static electric and magnetic multipole susceptibilities for hydrogenic atoms with nuclear charge numbers from the range 1 ⩽ Z ⩽ 137. Atomic nuclei are assumed to be point-like and spinless. The susceptibilities considered include the multipole electric polarizabilities α E L → E L and magnetizabilities (magnetic susceptibilities) χ M L → M L with 1 ⩽ L ⩽ 4 (i.e., the dipole, quadrupole, octupole and hexadecapole ones), the electric-to-magnetic cross-susceptibilities α E L → M(L - 1) with 2 ⩽ L ⩽ 5 and α E L → M(L + 1) with 1 ⩽ L ⩽ 4, the magnetic-to-electric cross-susceptibilities χ M L → E(L - 1) with 2 ⩽ L ⩽ 5 and χ M L → E(L + 1) with 1 ⩽ L ⩽ 4 (it holds that χ M L → E(L ∓ 1) =α E(L ∓ 1) → M L), and the electric-to-toroidal-magnetic cross-susceptibilities α E L → T L with 1 ⩽ L ⩽ 4. Numerical values are computed from general exact analytical formulas, derived by us elsewhere within the framework of the Dirac relativistic quantum mechanics, and involving generalized hypergeometric functions 3F2 of the unit argument.

  13. Rapid magnetic microfluidic mixer utilizing AC electromagnetic field.

    PubMed

    Wen, Chih-Yung; Yeh, Cheng-Peng; Tsai, Chien-Hsiung; Fu, Lung-Ming

    2009-12-01

    This paper presents a novel simple micromixer based on stable water suspensions of magnetic nanoparticles (i.e. ferrofluids). The micromixer chip is built using standard microfabrication and simple soft lithography, and the design can be incorporated as a subsystem into any chemical microreactor or a miniaturized biological sensor. An electromagnet driven by an AC power source is used to induce transient interactive flows between a ferrofluid and Rhodamine B. The alternative magnetic field causes the ferrofluid to expand significantly and uniformly toward Rhodamine B, associated with a great number of extremely fine fingering structures on the interface in the upstream and downstream regions of the microchannel. These pronounced fingering patterns, which have not been observed by other active mixing methods utilizing only magnetic force, increase the mixing interfacial length dramatically. Along with the dominant diffusion effects occurring around the circumferential regions of the fine finger structures, the mixing efficiency increases significantly. The miscible fingering instabilities are observed and applied in the microfluidics for the first time. This work is carried with a view to developing functionalized ferrofluids that can be used as sensitive pathogen detectors and the present experimental results demonstrate that the proposed micromixer has excellent mixing capabilities. The mixing efficiency can be as high as 95% within 2.0 s and a distance of 3.0 mm from the inlet of the mixing channel, when the applied peak magnetic field is higher than 29.2 Oe and frequency ranges from 45 to 300 Hz.

  14. AC loss in YBCO coated conductors at high dB/dt measured using a spinning magnet calorimeter (stator testbed environment)

    NASA Astrophysics Data System (ADS)

    Murphy, J. P.; Gheorghiu, N. N.; Bullard, T.; Haugan, T.; Sumption, M. D.; Majoros, M.; Collings, E. W.

    2017-09-01

    A new facility for the measurement of AC loss in superconductors at high dB/dt has been developed. The test device has a spinning rotor consisting of permanent magnets arranged in a Halbach array; the sample, positioned outside of this, is exposed to a time varying AC field with a peak radial field of 0.566 T. At a rotor speed of 3600 RPM the frequency of the AC field is 240 Hz, the radial dB/dt is 543 T/s and the tangential dB/dt is 249 T/s. Loss is measured using nitrogen boiloff from a double wall calorimeter feeding a gas flow meter. The system is calibrated using power from a known resistor. YBCO tape losses were measured in the new device and compared to the results from a solenoidal magnet AC loss system measurement of the same samples (in this latter case measurements were limited to a field of amplitude 0.1 T and a dB/dt of 100 T/s). Solenoidal magnet system AC loss measurements taken on a YBCO sample agreed with the Brandt loss expression associated with a 0-0.1 T Ic of 128 A. Subsequently, losses for two more YBCO tapes nominally identical to the first were individually measured in this spinning magnet calorimeter (SMC) machine with a Bmax of 0.566 T and dB/dt of up to 272 T/s. The losses, compared to a simplified version of the Brandt expression, were consistent with the average Ic expected for the tape in the 0-0.5 T range at 77 K. The eddy current contribution was consistent with a 77 K residual resistance ratio, RR, of 4.0. The SMC results for these samples agreed to within 5%. Good agreement was also obtained between the results of the SMC AC loss measurement and the solenoidal magnet AC loss measurement on the same samples.

  15. Tensor of effective susceptibility in random magnetic composites: Application to two-dimensional and three-dimensional cases

    NASA Astrophysics Data System (ADS)

    Posnansky, Oleg P.

    2018-05-01

    The measuring of dynamic magnetic susceptibility by nuclear magnetic resonance is used for revealing information about the internal structure of various magnetoactive composites. The response of such material on the applied external static and time-varying magnetic fields encodes intrinsic dynamic correlations and depends on links between macroscopic effective susceptibility and structure on the microscopic scale. In the current work we carried out computational analysis of the frequency dependent dynamic magnetic susceptibility and demonstrated its dependence on the microscopic architectural elements while also considering Euclidean dimensionality. The proposed numerical method is efficient in the simulation of nuclear magnetic resonance experiments in two- and three-dimensional random magnetic media by choosing and modeling the influence of the concentration of components and internal hierarchical characteristics of physical parameters.

  16. Definitive determination of the transverse Hamiltonian parameters in the single molecule magnet Mn_12-Ac

    NASA Astrophysics Data System (ADS)

    Edwards, Rachel S.; Hill, Stephen; North, J. Micah; Dalal, Naresh; Jones, Shaela; Maccagnano, Sara

    2003-03-01

    We present high frequency high field electron paramagnetic resonance (EPR) measurements on the single molecule magnet Mn_12-Ac. Using a split coil magnet and highly sensitive resonant cavity techniques we are able to perform an angle dependent study of the single crystal EPR with the field applied in the hard plane, and hence unambiguously determine the transverse Hamiltonian parameters to fourth order. A variation in the line-shape of the resonances with angle supports the recent proposal of a ligand disorder in this material causing local quadratic anisotropy, and is used to determine the magnitude of the second order transverse term. This could have important implications for describing magnetic quantum tunneling in Mn_12-Ac. S. Hill, J.A.A.J. Perenboom, N.S. Dalal, T. Hathaway, T. Stalcup and J.S. Brooks, Phys. Rev. Lett. 80, 2453 (1998). A. Cornia, R. Sessoli, L. Sorace, D. Gatteschi, A.L. Barra and C. Daiguebonne, cond-mat/0112112.

  17. Theory of the magnetic susceptibility including zero-point spin fluctuations of itinerant nearly ferromagnetic compounds

    NASA Astrophysics Data System (ADS)

    Konno, Rikio; Hatayama, Nobukuni; Takahashi, Yoshinori

    2018-05-01

    We have investigated the temperature dependence of the magnetic susceptibility of itinerant nearly ferromagnetic compounds based on the spin fluctuation theory. It is based on the conservation of the local spin amplitude that consists of both the thermal and the zero-point components. The linear dependence of the zero-point spin fluctuation amplitude on the inverse of magnetic susceptibility is usually assumed. The purpose of our present study is to include its higher order terms and to see their effects on the magnetic susceptibility. For the thermal amplitude, it shows T2-linear temperature dependence at low temperatures.

  18. Magnetic susceptibility and relation to initial 87Sr/86Sr for granitoids of the central Sierra Nevada, California

    USGS Publications Warehouse

    Bateman, P.C.; Dodge, F.C.W.; Kistler, R.W.

    1991-01-01

    Measurement of the magnetic susceptibility of more than 6000 samples of granitic rock from the Mariposa 1?? by 2?? quadrangle, which crosses the central part of the Sierra Nevada batholith between 37?? and 38??N latitude, shows that magnetic susceptibility values are above 10-2 SI units in the east and central parts of the batholith and drop abruptly to less than 10-3 SI units in the western foothills. In a narrow transitional zone, intermediate values (10-3 to 10-2) prevail. Magnetic susceptibility appears to decrease slightly westward within the zones of both high and low values. Magnetic susceptibility in plutonic rocks is chiefly a function of the abundance of magnetite, which depends, in turn, on the total iron content of the rocks and their oxidation ratio. Correlations of magnetic susceptibility with initial 87Sr/86Sr suggest that oxidation ratios have been inherited from the source regions for the magmas from which the rocks crystallized. Reduction of Fe3+ to Fe2+ by organic carbon or other reducing substances may also have affected magnetic susceptibility. -from Authors

  19. Eddy currents in the measurement of magnetic susceptibility of rocks

    NASA Astrophysics Data System (ADS)

    Ježek, Josef; Hrouda, František

    2018-01-01

    The in-phase and out-of-phase susceptibility of rocks is determined by the magnetic permeability of minerals, their viscous relaxation, and by eddy currents in electrically conductive minerals induced by the applied field. The last effect has been modelled by analytical solution of Maxwell equations for a conductive sphere immersed in a homogeneous, non-conductive medium with given permeability, in presence of an alternating field. The solution is a complex function of parameters describing the sphere (its size, conductivity and permeability), surrounding medium (permeability) and applied field (frequency). Without numerical evaluations, it is difficult to distinguish in-phase and out-of-phase (OPS) susceptibility. In this paper, approximate equations are derived for both susceptibility components, which depend only on the permeability contrast between the sphere and the surrounding medium, and the skin ratio, defined as the ratio between sphere radius and skin depth of the induced currents. These equations are used to obtain a systematic assessment of the role of electrical conductivity in determining the susceptibility of rock samples. The contribution of eddy currents to the susceptibility of diluted (<5%) magnetite particle dispersions is negligible at 1 kHz, but not at higher frequencies. Common rock-forming paramagnetic and diamagnetic minerals with weak electrical conductivity and magnetic permeability are characterized by negligible OPS at 1 kHz. Theoretically, measurable OPS and high phase angles can be produced by paramagnetic conductive minerals in certain combinations with a diamagnetic matrix. This can be excluded from practical point of view for paramagnetic minerals with susceptibilities >0.003 and conductivities not exceeding 5000 S/m.

  20. Linear ac Response of Thin Superconductors during Flux Creep

    NASA Astrophysics Data System (ADS)

    Brandt, Ernst Helmut; Gurevich, Alexander

    1996-03-01

    The linear magnetic susceptibility χ\\(ω\\) of superconducting strips and disks in a transverse magnetic field is calculated in the flux-creep regime. It is shown that χ\\(ω\\) = χ'-iχ'' for ω>>1/t is universal, independent of temperature, dc field, and material parameters, depending only on the sample shape, ac frequency ω/2π, and time t elapsed after creep has started. Qualitatively, χ\\(ω\\) can be obtained from the χ\\(ω\\) of metallic conductors by replacing the Ohmic relaxation time by t. At ωt>>1, which may apply down to rather low frequencies, the dissipative flux-creep state exhibits a nearly Meissner-like response with χ' = -1+0.40/ωt and χ'' = 0.25ln\\(29ωt\\)/ωt for disks.

  1. Magnetic susceptibility as an indicator of heavy metal contamination in compost.

    PubMed

    Paradelo, Remigio; Moldes, Ana Belén; Barral, María Teresa

    2009-02-01

    One of the main restrictions to the agronomic use of compost is the excess of heavy metals, which are often present due to inadequate separation of biodegradable fractions from non-degradable or inert materials. Magnetic susceptibility (MS) measurements are a simple technique that has been reported as a useful tool for assessing anthropogenic pollution, especially heavy metal pollution on soil and sediment samples. The close relationship of MS with heavy metal contamination has been proved by combined analyses of chemical and magnetic data. In this study, the MS and total heavy metal concentrations of eight composts from different origins were determined; all composts were passed under a magnet to remove the magnetic material, and total heavy metals were determined again. In our work, high correlations were found between magnetic susceptibility and total Cd, Zn, Pb, Cr and Ni, thus confirming the applicability of MS measurement as a proxy for heavy metal contamination in compost quality assessments. The application of a magnet over the composts reduced the MS as well as the heavy metal content, the reduction of Fe and MS being the most significantly correlated. Thus, the inclusion of an additional magnetic separation step in the post-process compost finishing could be envisaged.

  2. SU-F-I-24: Feasibility of Magnetic Susceptibility to Relative Electron Density Conversion Method for Radiation Therapy

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Ito, K; Kadoya, N; Chiba, M

    2016-06-15

    Purpose: The aim of this study is to develop radiation treatment planning using magnetic susceptibility obtained from quantitative susceptibility mapping (QSM) via MR imaging. This study demonstrates the feasibility of a method for generating a substitute for a CT image from an MRI. Methods: The head of a healthy volunteer was scanned using a CT scanner and a 3.0 T MRI scanner. The CT imaging was performed with a slice thickness of 2.5 mm at 80 and 120 kV (dual-energy scan). These CT images were converted to relative electron density (rED) using the CT-rED conversion table generated by a previousmore » dual-energy CT scan. The CT-rED conversion table was generated using the conversion of the energy-subtracted CT number to rED via a single linear relationship. One T2 star-weighted 3D gradient echo-based sequence with four different echo times images was acquired using the MRI scanner. These T2 star-weighted images were used to estimate the phase data. To estimate the local field map, a Laplacian unwrapping of the phase and background field removal algorithm were implemented to process phase data. To generate a magnetic susceptibility map from the local field map, we used morphology enabled dipole inversion method. The rED map was resampled to the same resolution as magnetic susceptibility, and the magnetic susceptibility-rED conversion table was obtained via voxel-by-voxel mapping between the magnetic susceptibility and rED maps. Results: A correlation between magnetic susceptibility and rED is not observed through our method. Conclusion: Our results show that the correlation between magnetic susceptibility and rED is not observed. As the next step, we assume that the voxel of the magnetic susceptibility map comprises two materials, such as water (0 ppm) and bone (-2.2 ppm) or water and marrow (0.81ppm). The elements of each voxel were estimated from the ratio of the two materials.« less

  3. Magnetic and transport properties of Pr2Pt3Si5

    NASA Astrophysics Data System (ADS)

    Anand, V. K.; Anupam; Hossain, Z.; Ramakrishnan, S.; Thamizhavel, A.; Adroja, D. T.

    2012-08-01

    We have investigated the magnetic and transport properties of a polycrystalline Pr2Pt3Si5 sample through the dc and ac magnetic susceptibilities, electrical resistivity, and specific heat measurements. The Rietveld refinement of the powder X-ray diffraction data reveals that Pr2Pt3Si5 crystallizes in the U2Co3Si5-type orthorhombic structure (space group Ibam). Both the dc and ac magnetic susceptibility data measured at low fields exhibit sharp anomaly near 15 K. In contrast, the specific heat data exhibit only a broad anomaly implying no long range magnetic order down to 2 K. The broad Schottky-type anomaly in low temperature specific heat data is interpreted in terms of crystal electric field (CEF) effect, and a CEF-split singlet ground state is inferred. The absence of the long range order is attributed to the presence of nonmagnetic singlet ground state of the Pr3+ ion. The electrical resistivity data exhibit metallic behavior and are well described by the Bloch-Grüniesen-Mott relation.

  4. Magnetic properties of M0.3Fe2.7O4 (M = Fe, Zn and Mn) ferrites nanoparticles

    NASA Astrophysics Data System (ADS)

    Modaresi, Nahid; Afzalzadeh, Reza; Aslibeiki, Bagher; Kameli, Parviz

    2018-06-01

    In the present article a comparative study on the structural and magnetic properties of nano-sized M0.3Fe0.7Fe2O4 (M = Fe, Zn and Mn) ferrites have been reported. The X-ray diffraction (XRD) patterns show that the crystallite size depends on the cation distribution. The Rietveld refinement of XRD patterns using MAUD software determines the distribution of cations and unit cell dimensions. The magnetic measurements show that the maximum and minimum value of saturation magnetization is obtained for Zn and Mn doped samples, respectively. The peak temperature of AC magnetic susceptibility of Zn and Fe doped samples below 300 K shows the superparamagnetic behavior in these samples at room temperature. the AC susceptibility results confirm the presence of strong interactions between the nanoparticles which leads to a superspin glass state in the samples at low temperatures.

  5. Thermally Assisted Macroscopic Quantum Resonance on a Single-Crystal of Mn12-ac

    NASA Astrophysics Data System (ADS)

    Lionti, F.; Thomas, L.; Ballou, R.; Wernsdorfer, W.; Barbara, B.; Sulpice, A.; Sessoli, R.; Gatteschi, D.

    1997-03-01

    Magnetization measurements have been performed on a single mono-crystal of the molecule Mn12-acetate (L. Thomas, F. Lionti, R. Ballou, R. Sessoli, D. Gatteschi and B. Barbara, Nature, 383, 145 (1996).). Steps were observed in the hysteresis loop for values of the applied field at which level crossings of the collective spin states of each manganese clusters take place. The influence of quartic terms is taken into account. At these fields, the magnetization relaxes at short time scales, being otherwise essentially blocked. This novel behavior is interpreted in terms of resonant quantum tunneling of the magnetization from thermally activated energy levels. Hysteresis loop measurements performed for different field orientations and ac-susceptibility experiments, confirm general trends of this picture.

  6. Multifractal magnetic susceptibility distribution models of hydrothermally altered rocks in the Needle Creek Igneous Center of the Absaroka Mountains, Wyoming

    USGS Publications Warehouse

    Gettings, M.E.

    2005-01-01

    Magnetic susceptibility was measured for 700 samples of drill core from thirteen drill holes in the porphyry copper-molybdenum deposit of the Stinkingwater mining district in the Absaroka Mountains, Wyoming. The magnetic susceptibility measurements, chemical analyses, and alteration class provided a database for study of magnetic susceptibility in these altered rocks. The distribution of the magnetic susceptibilities for all samples is multi-modal, with overlapping peaked distributions for samples in the propylitic and phyllic alteration class, a tail of higher susceptibilities for potassic alteration, and an approximately uniform distribution over a narrow range at the highest susceptibilities for unaltered rocks. Samples from all alteration and mineralization classes show susceptibilities across a wide range of values. Samples with secondary (supergene) alteration due to oxidation or enrichment show lower susceptibilities than primary (hypogene) alteration rock. Observed magnetic susceptibility variations and the monolithological character of the host rock suggest that the variations are due to varying degrees of alteration of blocks of rock between fractures that conducted hydrothermal fluids. Alteration of rock from the fractures inward progressively reduces the bulk magnetic susceptibility of the rock. The model introduced in this paper consists of a simulation of the fracture pattern and a simulation of the alteration of the rock between fractures. A multifractal model generated from multiplicative cascades with unequal ratios produces distributions statistically similar to the observed distributions. The reduction in susceptibility in the altered rocks was modelled as a diffusion process operating on the fracture distribution support. The average magnetic susceptibility was then computed for each block. For the purpose of comparing the model results with observation, the simulated magnetic susceptibilities were then averaged over the same interval as the

  7. Mapping Magnetic Susceptibility Anisotropies of White Matter in vivo in the Human Brain at 7 Tesla

    PubMed Central

    Li, Xu; Vikram, Deepti S; Lim, Issel Anne L; Jones, Craig K; Farrell, Jonathan A.D.; van Zijl, Peter C. M.

    2012-01-01

    High-resolution magnetic resonance phase- or frequency- shift images acquired at high field show contrast related to magnetic susceptibility differences between tissues. Such contrast varies with the orientation of the organ in the field, but the development of quantitative susceptibility mapping (QSM) has made it possible to reproducibly image the intrinsic tissue susceptibility contrast. However, recent studies indicate that magnetic susceptibility is anisotropic in brain white matter and, as such, needs to be described by a symmetric second-rank tensor (χ¯¯). To fully determine the elements of this tensor, it would be necessary to acquire frequency data at six or more orientations. Assuming cylindrical symmetry of the susceptibility tensor in myelinated white matter fibers, we propose a simplified method to reconstruct the susceptibility tensor in terms of a mean magnetic susceptibility, MMS = (χ∥ + 2χ⊥)/3 and a magnetic susceptibility anisotropy, MSA = χ∥ − χ⊥, where χ∥ and χ⊥ are susceptibility parallel and perpendicular to the white matter fiber direction, respectively. Computer simulations show that with a practical head rotation angle of around 20°–30°, four head orientations suffice to reproducibly reconstruct the tensor with good accuracy. We tested this approach on whole brain 1×1×1 mm3 frequency data acquired from five healthy subjects at 7 T. The frequency information from phase images collected at four head orientations was combined with the fiber direction information extracted from diffusion tensor imaging (DTI) to map the white matter susceptibility tensor. The MMS and MSA were quantified for regions in several large white matter fiber structures, including the corona radiata, posterior thalamic radiation and corpus callosum. MMS ranged from −0.037 to −0.053 ppm (referenced to CSF being about zero). MSA values could be quantified without the need for a reference and ranged between 0.004 and 0.029 ppm, in line with

  8. Calculation of susceptibility through multiple orientation sampling (COSMOS): a method for conditioning the inverse problem from measured magnetic field map to susceptibility source image in MRI.

    PubMed

    Liu, Tian; Spincemaille, Pascal; de Rochefort, Ludovic; Kressler, Bryan; Wang, Yi

    2009-01-01

    Magnetic susceptibility differs among tissues based on their contents of iron, calcium, contrast agent, and other molecular compositions. Susceptibility modifies the magnetic field detected in the MR signal phase. The determination of an arbitrary susceptibility distribution from the induced field shifts is a challenging, ill-posed inverse problem. A method called "calculation of susceptibility through multiple orientation sampling" (COSMOS) is proposed to stabilize this inverse problem. The field created by the susceptibility distribution is sampled at multiple orientations with respect to the polarization field, B(0), and the susceptibility map is reconstructed by weighted linear least squares to account for field noise and the signal void region. Numerical simulations and phantom and in vitro imaging validations demonstrated that COSMOS is a stable and precise approach to quantify a susceptibility distribution using MRI.

  9. Magnetic Properties and Phase Composition of Metamaterials Based on an Opal Matrix with 3 d-Transition Metal Particles

    NASA Astrophysics Data System (ADS)

    Rinkevich, A. B.; Korolev, A. V.; Samoilovich, M. I.; Perov, D. V.; Nemytova, O. V.

    2018-02-01

    The magnetic properties of metamaterials based on an opal matrix with transition-metal (iron, nickel, cobalt) particles have been studied. Magnetization curves and magnetic hysteresis loops have been measured and the dependences of real and imaginary parts of magnetization have been determined using the dynamic ac susceptibility measuring procedure. Structural studies of metamaterials have been performed. The saturation magnetization and coercive force of the studied metamaterials have been found to depend weakly on the temperature. The temperature dependence of magnetic susceptibility at a temperature above 30 K can be described adequately by Curie-Weiss law and, at lower temperature, deviates from the law.

  10. Effect of Dimension and Shape of Magnet on the Performance AC Generator with Translation Motion

    NASA Astrophysics Data System (ADS)

    Indriani, A.; Dimas, S.; Hendra

    2018-02-01

    The development of power plants using the renewable energy sources is very rapid. Renewable energy sources used solar energy, wind energy, ocean wave energy and other energy. All of these renewable energy sources require a processing device or a change of motion system to become electrical energy. One processing device is a generator which have work principle of converting motion (mechanical) energy into electrical energy with rotary shaft, blade and other motion components. Generator consists of several types of rotation motion and linear motion (translational). The generator have components such as rotor, stator and anchor. In the rotor and stator having magnet and winding coil as an electric generating part of the electric motion force. Working principle of AC generator with linear motion (translation) also apply the principle of Faraday that is using magnetic induction which change iron magnet to produce magnetic flux. Magnetic flux is captured by the stator to be converted into electrical energy. Linear motion generators consist of linear induction machine, wound synchronous machine field, and permanent magnet synchronous [1]. Performance of synchronous generator of translation motion is influenced by magnet type, magnetic shape, coil winding, magnetic and coil spacing and others. In this paper focus on the neodymium magnet with varying shapes, number of coil windings and gap of magnetic distances. This generator work by using pneumatic mechanism (PLTGL) for power plants system. Result testing of performance AC generator translation motion obtained that maximum voltage, current and power are 63 Volt for diameter winding coil 0.15 mm, number of winding coil 13000 and distance of magnet 20 mm. For effect shape of magnet, maximum voltage happen on rectangle magnet 30x20x5 mm with 4.64 Volt. Voltage and power on effect of diameter winding coil is 14.63 V and 17.82 W at the diameter winding coil 0.7 and number of winding coil is 1260 with the distance of magnet 25

  11. Effect of grain alignment on magnetic properties of Hg(Re)-1223 superconductors

    NASA Astrophysics Data System (ADS)

    Sakamoto, N.; Noguchi, S.; Akune, T.; Matsumoto, Y.

    2002-08-01

    Alignment of HgBa 2Ca 2Cu 3Re 0.2O y (Hg(Re)-1223) powders was made in epoxy resin under a high magnetic field of 10 T to be confirmed by X-ray analysis. DC magnetizations and AC susceptibilities of the grain aligned specimen were measured by SQUID and PPMS magnetometers at temperatures of 5-110 K and under the field of 0-14 T for both field directions of B parallel and perpendicular to ab-plane. The magnetization width for B parallel to the c-axis ΔMc showed high values at low field, decreased rather rapidly with the magnetic field compared to that for B parallel to the ab-plane ΔMab and became lower than ΔMab above a crossing field Bcr. Peak-heights of the imaginary parts of the AC susceptibilities χ″ were largest at B∥ c-axis. Non-aligned samples always showed intermediate characteristics between B∥ c-axis and B∥ ab-plane. Irreversibility fields of all samples were also evaluated. Correlations of the pinning mechanism with the crystal axis orientations are discussed.

  12. Frequency Dependent Susceptibility Analysis of Magnetic Carriers: Application to Fe-Oxides on Mars surface

    NASA Astrophysics Data System (ADS)

    Adachi, T.; Kletetschka, G.; Mikula, V.

    2007-12-01

    On Mars, Fe-oxides mineral phases (inferred/detected) are mainly magnetite, pyrrhotite, and hematite. Kletetschka et al., 2005 suggested that the grain size dependent potential may contribute to the Mars surface magnetic anomaly. Grain size of Fe-oxides may play a role for the magnetic signature and anomaly on Mars. According to Kletetschka et al., 2005, the larger the grain size, the larger the magnetization (in this case hematite's TRM). Weather they are magnetite, pyrrhotite or hematite, nano-phase or superparamagnetic grains may contribute to the absence of remanent magnetization on the surface of Mars. In this contribution we tackle how to resolve grain size variations by frequency dependent susceptibility measured on terrestrial hematite samples such as hemo-ilmenite from Allard Lake, Canada, Mars analogue concretions from Utah and Czech Republic, and hematite aggregates from Hawaii. The magnetic characteristics of hematite-goethite mineralogies of Utah and Czech concretions suggested (Adachi et al., 2007) that they contain super paramagnetic (SP) to single domain (SD) magnetic states. Coercivity spectra analysis from acquisition of isothermal remanent magnetization (IRM) data showed the distinct behaviors of hematite, goethite, and mixed composition of both. The estimated magnetic states are analyzed with the frequency-dependent susceptibility instrument (500-250,000 Hertz). The frequency- and size-dependent susceptibility for hematite, goethite, and magnetite are calibrated using the known size powdered (commercial) samples.

  13. Multiple magnetic transitions in EuNiSi3

    NASA Astrophysics Data System (ADS)

    Patil, Sujata M.; Paulose, P. L.

    2018-04-01

    EuNiSi3 undergoes multiple magnetic transitions below 50K. We have studied this system using low field ac susceptibility and 151Eu Mössbauer spectroscopy to understand the nature of multiple magnetic transitions. The estimated hyperfine field (hf) at Eu site at 5K is 45 Tesla which is unusually large compared to the normal observed hf of 33T in most of the Eu intermetallics.

  14. Particle Size Distribution of Heavy Metals and Magnetic Susceptibility in an Industrial Site.

    PubMed

    Ayoubi, Shamsollah; Soltani, Zeynab; Khademi, Hossein

    2018-05-01

    This study was conducted to explore the relationships between magnetic susceptibility and some soil heavy metals concentrations in various particle sizes in an industrial site, central Iran. Soils were partitioned into five fractions (< 28, 28-75, 75-150, 150-300, and 300-2000 µm). Heavy metals concentrations including Zn, Pb, Fe, Cu, Ni and Mn and magnetic susceptibility were determined in bulk soil samples and all fractions in 60 soil samples collected from the depth of 0-5 cm. The studied heavy metals except for Pb and Fe displayed a substantial enrichment in the < 28 µm. These two elements seemed to be independent of the selected size fractions. Magnetic minerals are specially linked with medium size fractions including 28-75, 75-150 and 150-300 µm. The highest correlations were found for < 28 µm and heavy metals followed by 150-300 µm fraction which are susceptible to wind erosion risk in an arid environment.

  15. Impact of Long-Term Irrigation with Treated Sewage on Soil Magnetic Susceptibility and Organic Matter Content in North China.

    PubMed

    Yang, P G; Yang, M; Mao, R Z; Byrne, J M

    2015-07-01

    This study assessed the effect on magnetic susceptibility and organic matter content of arable soil by irrigation with either treated sewage or groundwater. Results indicated that organic matter and magnetic susceptibility values in the soil irrigated with sewage were increased by 7.1 % and 13.5 %, respectively, compared to agricultural soil that irrigated with groundwater. Both the sewage and groundwater irrigated soils contained a significant fraction of ultrafine superpara magnetic grains, as indicated by high frequency dependent susceptibility (χfd > 6 %). The enhancement of soil magnetic properties was determined to be caused by anthropogenic sewage irrigation and agrochemical use by investigation of vertical soil profiles. Magnetic susceptibility parameters were shown to be significantly correlated with organic matter content (y = 0.0057x + 1.3439, R(2) = 0.09, p < 0.05). This work indicates that measurements of magnetic susceptibility may offer a rapid first step for identifying the potential pollution in arable soils.

  16. Magnetic susceptibility well-logging unit with single power supply thermoregulation system

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Seeley, R. L.

    1985-11-05

    The magnetic susceptibility well-logging unit with single power supply thermoregulation system provides power from a single surface power supply over a well-logging cable to an integrated circuit voltage regulator system downhole. This voltage regulator system supplies regulated voltages to a temperature control system and also to a Maxwell bridge sensing unit which includes the solenoid of a magnetic susceptibility probe. The temperature control system is provided with power from the voltage regulator system and operates to permit one of several predetermined temperatures to be chosen, and then operates to maintain the solenoid of a magnetic susceptibility probe at this chosenmore » temperature. The temperature control system responds to a temperature sensor mounted upon the probe solenoid to cause resistance heaters concentrically spaced from the probe solenoid to maintain the chosen temperature. A second temperature sensor on the probe solenoid provides a temperature signal to a temperature transmitting unit, which initially converts the sensed temperature to a representative voltage. This voltage is then converted to a representative current signal which is transmitted by current telemetry over the well logging cable to a surface electronic unit which then reconverts the current signal to a voltage signal.« less

  17. Quantum renormalizations in anisotropic multisublattice magnets and the modification of magnetic susceptibility under irradiation

    NASA Astrophysics Data System (ADS)

    Val'kov, V. V.; Shustin, M. S.

    2015-11-01

    The dispersion equation of a strongly anisotropic one-dimensional magnet catena-[FeII(ClO4)2{FeIII(bpca)2}]ClO4 containing alternating high-spin (HS) ( S = 2) and low-spin (LS) ( S = 1/2) iron ions is obtained by the diagram technique for Hubbard operators. The analysis of this equation yields six branches in the excitation spectrum of this magnet. It is important that the crystal field for ions with spin S = 2 is described by the Hamiltonian of single-ion easy-plane anisotropy, whose orientation is changed by 90° when passing from one HS iron ion to another. The U( N) transformation technique in the atomic representation is applied to diagonalize a single-ion Hamiltonian with a large number of levels. It is shown that the modulation of the orientation of easy magnetization planes leads to a model of a ferrimagnet with easy-axis anisotropy and to the formation of energy spectrum with a large gap. For HS iron ions, a decrease in the mean value of the spin projection due to quantum fluctuations is calculated. The analysis of the specific features of the spectrum of elementary excitations allows one to establish a correspondence to a generalized Ising model for which the magnetic susceptibility is calculated in a wide range of temperatures by the transfer-matrix method. The introduction of a statistical ensemble that takes into account the presence of chains of different lengths and the presence of iron ions with different spins allows one to describe the experimentally observed modification of the magnetic susceptibility of the magnet under optical irradiation.

  18. Association Between IL-10 Gene Promoter Polymorphisms (-592 A/C, -819 T/C, -1082 A/G) and Susceptibility to HBV Infection in an Iranian Population

    PubMed Central

    Moudi, Bita; Heidari, Zahra; Mahmoudzadeh-Sagheb, Hamidreza; Hashemi, Mohammad; Metanat, Malihe; Khosravi, Soheila; Farrokh, Parisa

    2016-01-01

    Background IL-10 can play a vital role in immune response against HBV. Three biallelic SNPs from the transcription start site control the transcription of the IL-10 gene. An association between susceptibility to HBV and IL-10 polymorphisms has been suggested in patients with HBV infection. Objectives The present study was designed to study the association between polymorphisms in interleukin-10 (-1082 A/G, -819 T/C and -592 A/C) promoter gene and chronic hepatitis B virus (HBV) infection. Patients and Methods 221 chronically infected patients and 200 healthy control subjects were enrolled in the study. Three biallelic (-1082 A/G, -819 T/C and -592 A/C) polymorphisms in the IL-10 promoter gene were determined by PCR-RFLP method. Results Persistent HBV infection was associated with IL-10-1082 AG (P = 0.001) and GG (P = 0.004) genotypes and G (P = 0.000) allele. IL-10-819 T/C and -592 A/C genotype and allele frequencies did not show any correlation with the risk of chronic hepatitis B infection. Conclusions These results suggest that polymorphisms in interleukin-10 gene promoter influence clinical outcome of HBV infection and susceptibility to HBV infection. PMID:27148384

  19. Association Between IL-10 Gene Promoter Polymorphisms (-592 A/C, -819 T/C, -1082 A/G) and Susceptibility to HBV Infection in an Iranian Population.

    PubMed

    Moudi, Bita; Heidari, Zahra; Mahmoudzadeh-Sagheb, Hamidreza; Hashemi, Mohammad; Metanat, Malihe; Khosravi, Soheila; Farrokh, Parisa

    2016-02-01

    IL-10 can play a vital role in immune response against HBV. Three biallelic SNPs from the transcription start site control the transcription of the IL-10 gene. An association between susceptibility to HBV and IL-10 polymorphisms has been suggested in patients with HBV infection. The present study was designed to study the association between polymorphisms in interleukin-10 (-1082 A/G, -819 T/C and -592 A/C) promoter gene and chronic hepatitis B virus (HBV) infection. 221 chronically infected patients and 200 healthy control subjects were enrolled in the study. Three biallelic (-1082 A/G, -819 T/C and -592 A/C) polymorphisms in the IL-10 promoter gene were determined by PCR-RFLP method. Persistent HBV infection was associated with IL-10-1082 AG (P = 0.001) and GG (P = 0.004) genotypes and G (P = 0.000) allele. IL-10-819 T/C and -592 A/C genotype and allele frequencies did not show any correlation with the risk of chronic hepatitis B infection. These results suggest that polymorphisms in interleukin-10 gene promoter influence clinical outcome of HBV infection and susceptibility to HBV infection.

  20. Magnetic properties of a new obsidian source, west Antelope Creek, Grant County, New Mexico

    NASA Astrophysics Data System (ADS)

    Sternberg, R. S.; Samuels, R.; Feinberg, J. M.; Shackley, M. S.

    2013-12-01

    This work is part of a Keck Geology Consortium project on characterizing obsidian sources in New Mexico using magnetic and geochemical properties. We collected over 3,000 samples, many of which were georeferenced, from 10 obsidian sources at three locales - Mule creek, Mt. Taylor, and Valles Caldera. One of the Mule Creek sources, herein called the west Antelope Creek (wAC) source, was previously unknown. The 143 samples collected at this source covered about 1 km2, but were not individually georeferenced. We plan to characterize the magnetic and chemical properties of this source to see if it is distinguishable from other nearby sources and useful for provenancing archaeological obsidians. Initial measurements on 34 specimens from 20 samples show NRM values range from 1-80 Am2/kg, and low-field susceptibilities range from 1.2-96 x 10-8 mass specific SI units. When there were two specimens from the same sample, results were in good agreement. The measurements define a rather broad field in NRM-susceptibility space compared to other Southwestern sources examined to date, and a considerably larger field than from the nearby Antelope Creek (AC) source. The previously measured NRM and susceptibility values from AC are all in the high end on both dimensions of the wAC field, so that these fields overlap but in many cases could be distinguished.

  1. Advanced AC permanent magnet axial flux disc motor for electric passenger vehicle

    NASA Technical Reports Server (NTRS)

    Kliman, G. B.

    1982-01-01

    An ac permanent magnet axial flux disc motor was developed to operate with a thyristor load commutated inverter as part of an electric vehicle drive system. The motor was required to deliver 29.8 kW (40 hp) peak and 10.4 kW (14 hp) average with a maximum speed of 11,000 rpm. It was also required to run at leading power factor to commutate the inverter. Three motors were built.

  2. Variable Temperature Equipment for a Commercial Magnetic Susceptibility Balance

    ERIC Educational Resources Information Center

    Lotz, Albert

    2008-01-01

    Variable temperature equipment for the magnetic susceptibility balance MSB-MK1 of Sherwood Scientific, Ltd., is described. The sample temperature is controlled with streaming air heated by water in a heat exchanger. Whereas the balance as sold commercially can be used only for room temperature measurements, the setup we designed extends the…

  3. Negative electric susceptibility and magnetism from translational invariance and rotational invariance

    NASA Astrophysics Data System (ADS)

    Koo, Je Huan

    2015-02-01

    In this work we investigate magnetic effects in terms of the translational and rotational invariances of magnetisation. Whilst Landau-type diamagnetism originates from translational invariance, a new diamagnetism could result from rotational invariance. Translational invariance results in only conventional Landau-type diamagnetism, whereas rotational invariance can induce a paramagnetic susceptibility for localised electrons and also a new kind of diamagnetism that is specific to conducting electrons. In solids, the moving electron shows a paramagnetic susceptibility but the surrounding screening of electrons may produce a new diamagnetic response by Lenz's law, resulting in a total susceptibility that tends to zero. For electricity, similar behaviours are obtained. We also derive the DC-type negative electric susceptibility via two methods in analogy with Landau diamagnetism.

  4. Influence of martensitic transformation on the magnetic transition in Ni-Mn-Ga

    NASA Astrophysics Data System (ADS)

    Kokorin, V. V.; Konoplyuk, S. M.; Dalinger, A.; Maier, H. J.

    2017-06-01

    The magnetic transition with a temperature hysteresis of about 7 K was observed in the martensitic phase of Ni51.9Mn27Ga211. The measurements of AC magnetic susceptibility in constant magnetic fields up to 570 kA/m have proved its magnetic origin. The transport and caloric measurements were used to gain better understanding of the nature of this phenomenon. The variation of the martensite lattice parameters with temperature is suggested to account for the hysteresis of the magnetic transition.

  5. Magnetic susceptibility, artifact volume in MRI, and tensile properties of swaged Zr-Ag composites for biomedical applications.

    PubMed

    Imai, Haruki; Tanaka, Yoji; Nomura, Naoyuki; Doi, Hisashi; Tsutsumi, Yusuke; Ono, Takashi; Hanawa, Takao

    2017-02-01

    Zr-Ag composites were fabricated to decrease the magnetic susceptibility by compensating for the magnetic susceptibility of their components. The Zr-Ag composites with a different Zr-Ag ratio were swaged, and their magnetic susceptibility, artifact volume, and mechanical properties were evaluated by magnetic balance, three-dimensional (3-D) artifact rendering, and a tensile test, respectively. These properties were correlated with the volume fraction of Ag using the linear rule of mixture. We successfully obtained the swaged Zr-Ag composites up to the reduction ratio of 96% for Zr-4, 16, 36, 64Ag and 86% for Zr-81Ag. However, the volume fraction of Ag after swaging tended to be lower than that before swaging, especially for Ag-rich Zr-Ag composites. The magnetic susceptibility of the composites linearly decreased with the increasing volume fraction of Ag. No artifact could be estimated with the Ag volume fraction in the range from 93.7% to 95.4% in three conditions. Young's modulus, ultimate tensile strength (UTS), and 0.2% yield strength of Zr-Ag composites showed slightly lower values compared to the estimated values using a linear rule of mixture. The decrease in magnetic susceptibility of Zr and Ag by alloying or combining would contribute to the decrease of the Ag fraction, leading to the improvement of mechanical properties. Copyright © 2016 Elsevier Ltd. All rights reserved.

  6. Enteric coated magnetic HPMC capsules evaluated in human gastrointestinal tract by AC biosusceptometry.

    PubMed

    Corá, Luciana A; Romeiro, Fernando G; Paixão, Fabiano C; Américo, Madileine F; Oliveira, Ricardo B; Baffa, Oswaldo; Miranda, José Ricardo A

    2006-08-01

    To employ the AC Biosusceptometry (ACB) technique to evaluate in vitro and in vivo characteristics of enteric coated magnetic hydroxypropyl methylcellulose (HPMC) capsules and to image the disintegration process. HPMC capsules filled with ferrite (MnFe2O4) and coated with Eudragit were evaluated using USP XXII method and administered to fasted volunteers. Single and multisensor ACB systems were used to characterize the gastrointestinal (GI) motility and to determine gastric residence time (GRT), small intestinal transit time (SITT) and orocaecal transit time (OCTT). Mean disintegration time (t50) was quantified from 50% increase of pixels in the imaging area. In vitro and in vivo performance of the magnetic HPMC capsules as well as the disintegration process were monitored using ACB systems. The mean disintegration time (t50) calculated for in vitro was 25+/-5 min and for in vivo was 13+/-5 min. In vivo also were determined mean values for GRT (55+/-19 min), SITT (185+/-82 min) and OCTT (240+/-88 min). AC Biosusceptometry is a non-invasive technique originally proposed to monitoring pharmaceutical dosage forms orally administered and to image the disintegration process.

  7. Study of the Dependence on Magnetic Field and Bias Voltage of an AC-Biased TES Microcalorimeter

    NASA Technical Reports Server (NTRS)

    Bandler, Simon

    2011-01-01

    At SRON we are studying the performance of a Goddard Space Flight Center single pixel TES microcalorimeter operated in the AC bias configuration. For x-ray photons at 6keV the AC biased pixel shows a best energy resolution of 3.7eV, which is about a factor of 2 worse than the energy resolution observed in identical DC-biased pixels. To better understand the reasons of this discrepancy, we investigated the detector performance as a function of temperature, bias working point and applied magnetic field. A strong periodic dependence of the detector noise on the TES AC bias voltage is measured. We discuss the results in the framework of the recent weak-link behaviour observed inTES microcalorimeters.

  8. Magnetic Properties and Phase Diagram of Ni50Mn_{50-x}Ga_{x/2}In_{x/2} Magnetic Shape Memory Alloys

    NASA Astrophysics Data System (ADS)

    Xu, Xiao; Yoshida, Yasuki; Omori, Toshihiro; Kanomata, Takeshi; Kainuma, Ryosuke

    2016-12-01

    Ni50Mn50- x Ga x/2In x/2 magnetic shape memory alloys were systematically prepared, and the magnetic properties as well as the phase diagram, including atomic ordering, martensitic and magnetic transitions, were investigated. The B2- L21 order-disorder transformation showed a parabolic-like curve against the Ga+In composition. The martensitic transformation temperature was found to decrease with increasing Ga+In composition and to slightly bend downwards below the Curie temperature of the parent phase. Spontaneous magnetization was investigated for both parent and martensite alloys. The magnetism of martensite phase was found to show glassy magnetic behaviors by thermomagnetization and AC susceptibility measurements.

  9. Anisotropic magnetic susceptibility of erbium and ytterbium in zircon, ZrSiO4

    USGS Publications Warehouse

    Thorpe, A.N.; Briggs, Charles; Tsang, T.; Senftle, F.; Alexander, Corrine

    1977-01-01

    Magnetic susceptibility measurements have been made for both Er- and Yb-doped (1̃03ppm) zircon single crystals with the magnetic field perpendicular and parallel to the [001] axis. Large susceptibility anisotropies were found in both cases. Our observed anisotropies of ZrSiO4: Yb indicate small populations (1̃9%) of Yb ions at the axial (tetragonal) sites, as the susceptibility of ZrSiO4: Yb would be nearly isotropic if the Yb ions only occupied the orthorhombic sites. For Er3+ in orthorhombic sites of zircon, our data indicate that the first excited state is paramagnetic with gx = 9 and gy 5̃ at 20 cm-1 above the ground state (gx 0̃, gy 1̃5). The first excited state is quite similar to the ground states observed for Er3+ in many host lattices. ?? 1977.

  10. Identification of Heavy Metal Pollution Derived From Traffic in Roadside Soil Using Magnetic Susceptibility.

    PubMed

    Yang, Pingguo; Ge, Jing; Yang, Miao

    2017-06-01

    The study integrates surface and vertical distribution of magnetic susceptibility and heavy metal contents (Pb, Cu, Zn and Fe) to characterize the signature of vehicle pollutants in roadside soils at Linfen city, China. Sites with reforestation and without vegetation cover were investigated. The results showed that magnetic susceptibility and heavy metal contents were higher at the roadside without trees than in the reforest belt. The variations of magnetic susceptibility and heavy metal contents decreased both with distance and with depth. The maximum value was observed at 5-10 m away from the roadside edge. The vertical distribution in soil revealed accumulation of pollutants in 0-5 cm topsoils. The average contents were higher than the background values and in the order Fe (107.21 g kg -1 ), Zn (99.72 mg kg -1 ), Pb (90.99 mg kg -1 ), Cu (36.14 mg kg -1 ). Coarse multi domain grains were identified as the dominating magnetic particles. Multivariate statistical and SEM/EDX analyses suggested that the heavy metals derived from traffic sources. Trees act as efficient receptors and green barrier, which can reduce vehicle derived pollution.

  11. Strain analysis in quartzites with negative magnetic susceptibility using AMS and EBSD data

    NASA Astrophysics Data System (ADS)

    Rajendraprasad Renjith, A.; Mamtani, Manish A.

    2016-04-01

    This study is being done with the objective of trying to understand whether the anisotropy of magnetic susceptibility (AMS) data can provide information about strain in quartzites with negative magnetic susceptibility. For this, nine quartzite samples have been collected from Rengali Province (located in the eastern part of India) with bulk magnetic susceptibility between -13.6 x 10-6 SI units and -3.06 x 10-6 SI units. Since these rocks did not show any visible foliation or lineation, AMS analysis was performed using KLY-4S Kappabridge and the orientation of three principal axes of the AMS ellipsoid (K1>K2>K3) were determined. Thin sections were prepared parallel to the K1K3 plane of the AMS ellipsoid (plane parallel to lineation and perpendicular to foliation), which is equivalent to the XZ plane of the strain ellipsoid. SEM based electron backscatter diffraction (EBSD) analysis, shape preferred orientation (SPO) analysis and strain analysis were carried out in these sections. Recently, Renjith et al. (2016) used the same samples to establish that the AMS in quartzites gives information about the SPO and not the CPO. To further evaluate the robustness of AMS in strain analysis, the authors have integrated the degree of magnetic anisotropy (Pj - a measure of the eccentricity of AMS ellipsoid; Tarling and Hrouda, 1993) with the intensity of SPO (κ ; Piazolo and Passchier, 2002), and the strain (E - calculated using AMOCADO; Gerik and Kruhl, 2009) from the same samples from Rengali. EBSD data were used as the basis for the above calculations. Whilst the orientation of long axis of quartz grains from EBSD statistical data was used to calculate κ , the grain boundary map generated from EBSD analysis was used as the basis to determine strain (E). It is found that the sample with minimum Pj also has a minimum κ and E, and vice-versa. Hence it is concluded that one-to-one correlation exists between the degree of magnetic anisotropy, strain and intensity of SPO in

  12. Experimental investigation of the critical magnetic fields of transition metal superconductors

    NASA Technical Reports Server (NTRS)

    Mcevoy, J. P.

    1973-01-01

    The isothermal magnetic transitions of a type 2 superconductor have been studied by AC susceptibility techniques as a function of the amplitude and frequency of the exciting field. The field variation of the complex susceptibility was used to determine the critical fields. The research was planned to clarify the determination (both experimentally and theoretically) of the maximum field at which the superconductive phase spontaneously nucleates in the bulk and on the surface of the metal.

  13. Impacts of geology and land use on magnetic susceptibility and selected heavy metals in surface soils of Mashhad plain, northeastern Iran

    NASA Astrophysics Data System (ADS)

    Karimi, Alireza; Haghnia, Gholam Hosain; Ayoubi, Shamsollah; Safari, Tayebeh

    2017-03-01

    Magnetic susceptibility is a fast, inexpensive and reliable technique for estimating and monitoring the anthropogenic contamination of soil with heavy metals. However, it is essential to determine the factors affecting magnetic susceptibility before applying this technique to environmental studies. The objectives of this study were to investigate i) the effect of parent materials and land use on the magnetic susceptibility and concentrations of Fe, Ni, Pb and Zn, and ii) capability of magnetic susceptibility as an indicator of anthropogenic heavy metals contamination of soil in Mashhad plain, northeastern Iran. One hundred seventy-eight composite surface soil samples (0-10 cm) were taken. The aqua-regia extractable concentrations of Fe, Ni, Zn and Pb were determined by atomic absorption spectroscopy. Magnetic susceptibility at low and high frequency (χlf and χhf) were measured and frequency dependent susceptibility (χfd) was calculated. The average concentrations of Fe, Ni, Pb and Zn were 22,812, 61.4, 74.1 and 31.6 mg kg- 1, respectively. The highest contents of Pb (69.1 mg kg- 1) and Zn (149 mg kg- 1) were observed in urban area. The highest concentration of Ni was 41,538 mg kg- 1 observed in the soils developed from ultramafic rocks. Magnetic susceptibility varied from 20.3 on marly sediments to 311.8 × 10- 8 m3 kg- 1 on ultramafic rocks. A positive strong correlation (Pvalue < 0.01, r = 0.88) was obtained between Ni and χlf. There were no significant relationships between Zn and Pb with χlf, therefore it seems that magnetic susceptibility has not been affected significantly by anthropogenic activities which enhanced Pb and Zn concentrations in urban soils. The results indicated that magnetic susceptibility was mainly controlled by Ni containing minerals with lithogenic origin. Therefore, in the soils studied, magnetic susceptibility could not be employed as indicator of anthropogenic contamination of soil with heavy metals.

  14. Integrated geophysical characterisation of Sunyani municipal solid waste disposal site using magnetic gradiometry, magnetic susceptibility survey and electrical resistivity tomography

    NASA Astrophysics Data System (ADS)

    Appiah, Isaac; Wemegah, David Dotse; Asare, Van-Dycke Sarpong; Danuor, Sylvester K.; Forson, Eric Dominic

    2018-06-01

    Non-invasive geophysical investigation using magnetic gradiometry, magnetic susceptibility survey and electrical resistivity tomography (ERT) was carried out on the Sunyani Municipal Assembly (SMA) solid waste disposal (SWD) site. The study was aimed at delineating the physical boundaries and the area extent of the waste deposit, mapping the distribution of the waste at the site, detecting and delineating zones of leachate contamination and its preferential migration pathways beneath the waste deposit and its surroundings. The results of both magnetic susceptibility and gradiometric methods displayed in anomaly maps clearly delineated the physical boundaries of the waste deposit with an approximate area extent of 82,650 m2 that are characterised by high magnetic susceptibilities between 426 × 10-5 SI and 9890 × 10-5 SI. They also revealed high magnetic anomalies erratically distributed within the waste deposit attributable to its heterogeneous and uncontrolled nature. The high magnetic anomalies outside the designated waste boundaries were also attributed to indiscriminate deposition of the waste. Similarly, the ERT sections delineated and characterised zones of leachate contamination beneath the waste body and its close surroundings as well as pathways for leachate migration with low resistivity signatures up to 43.9 Ωm. In spite of the successes reported herein using the ERT, this research also revealed that the ERT is less effective in estimating the thickness of the waste deposit in unlined SWD sites due to leachate infiltration into the ground beneath it that masks the resistivities of the top level ground and makes it indistinguishable from the waste body.

  15. Magnetic Properties of nickel hydroxides layers 30A apart obtained by intercalation with dodecyl sulfate ion

    NASA Astrophysics Data System (ADS)

    Shmavonyan, Gagik; Zadoyan, Ovsanna

    2013-03-01

    Magnetic systems with reduced dimensionality make good test beds for checks on theoretical models. Here, changes in the nature of magnetic ordering in quasi-2d system of layered Ni hydroxides (LH-Ni-) with variations in the interlayer spacing c are investigated. Magnetic properties of LH-Ni-DS with c ~ 30 A° synthesized by intercalating dodecyl sulfate ion, (C12H25OSO3)- between the layers are compared with those of LH-Ni-Ac (c ~ 8.5 A°) containing the acetate (Ac) ligand. Measurements included those of magnetization M vs. T and H, ac susceptibilities (f = 0.1 Hz - 1000 Hz) and EMR (Electron Magnetic Resonance) spectra at 9.28 GHz. Results show that just like LH-Ni-Ac, LH-Ni-DS also orders ferromagnetically but with Tc ~ 23 Kabout 45 % largerthanT c 16 Kreportedfor LH-Ni-Ac.. In EMR studies, linewidth is strongly temperature-dependent, decreasing with decreasing T from 300 K, reaching a minimum near 45 K and then increasing sharply for T < 45 K, the latter due to short range magnetic ordering. These results differ with the model of Drillon et al in which interlayer dipolar interaction between clusters of correlated spins in the layers yields TC nearly independent of c. Roles of magnetic anisotropy and exchange constants in determining TC in the LH-Ni systems is discussed.

  16. Generating an AC amplitude magnetic flux density value up to 150 μT at a frequency up to 100 kHz

    NASA Astrophysics Data System (ADS)

    Ulvr, Michal; Polonský, Jakub

    2017-05-01

    AC magnetic field analyzers with a triaxial coil probe are widely used by health and safety professionals, in manufacturing, and in service industries. For traceable calibration of these analyzers, it is important to be able to generate a stable, homogeneous reference AC magnetic flux density (MFD). In this paper, the generating of AC amplitude MFD value of 150 μT by single-layer Helmholtz type solenoid, described in previous work, was expanded up to a frequency of 100 kHz using the effect of serial resonance. A programmable capacitor array has been developed with a range of adjustable values from 50 pF to 51225 pF. In addition, the multi-layer search coil with a nominal area turns value of 1.3m2, used for adjusting AC MFD in the solenoid, has been modified by a transimpedance amplifier for use in a wider frequency range than up to 3 kHz. The possibility of using the programmable capacitor array up to 150 kHz has also been tested. An AC amplitude MFD value of 150 μT can be generated with expanded uncertainty better than 0.6% up to 100 kHz.

  17. Magnetic Susceptibility as a Proxy for Investigating Microbial Mediated Iron Reduction

    EPA Science Inventory

    We investigated magnetic susceptibility (MS) variations in hydrocarbon contaminated sediments. Our objective was to determine if MS can be used as an intrinsic bioremediation indicator due to the activity of iron-reducing bacteria. A contaminated and an uncontaminated core were r...

  18. Investigations of the effect of nonmagnetic Ca substitution for magnetic Dy on spin-freezing in Dy₂Ti₂O₇.

    PubMed

    Anand, V K; Tennant, D A; Lake, B

    2015-11-04

    Physical properties of partially Ca substituted hole-doped Dy2Ti2O7 have been investigated by ac magnetic susceptibility χ(ac)(T), dc magnetic susceptibility χ(T), isothermal magnetization M(H) and heat capacity C(p)(T) measurements on Dy1.8Ca0.2Ti2O7. The spin-ice system Dy2Ti2O7 exhibits a spin-glass type freezing behavior near 16 K. Our frequency dependent χ(ac)(T) data of Dy1.8Ca0.2Ti2O7 show that the spin-freezing behavior is significantly influenced by Ca substitution. The effect of partial nonmagnetic Ca(2+) substitution for magnetic Dy(3+) is similar to the previous study on nonmagnetic isovalent Y(3+) substituted Dy(2-x)Y(x) Ti2O7 (for low levels of dilution), however the suppression of spin-freezing behavior is substantially stronger for Ca than Y. The Cole-Cole plot analysis reveals semicircular character and a single relaxation mode in Dy1.8Ca0.2Ti2O7 as for Dy2Ti2O7. No noticeable change in the insulating behavior of Dy2Ti2O7 results from the holes produced by 10% Ca(2+) substitution for Dy(3+) ions.

  19. Correlations between soil magnetic susceptibility and the content of particular elements as a reflection of pollution level, land use and parent rocks

    NASA Astrophysics Data System (ADS)

    Rachwał, Marzena; Magiera, Tadeusz; Bens, Oliver; Kardel, Kati

    2015-04-01

    Magnetic susceptibility is a worldwide used measure of (ferri)magnetic minerals occurring in soils, sediments and dusts. In soils, these minerals are of various origin: air-derived particulate pollutions, parent rocks or pedogenesis. Human activity causes different changes in the content of magnetic minerals as well as their spatial and vertical distribution in soil profiles. Magnetic minerals are characterized by an affinity for other elements occurring in the soil, so positive correlations between magnetic susceptibility and particular elements like macrocomponents or heavy metals often occurs. The archival soil samples collected from different soil horizons in the territory of the Free State of Saxony (Germany) were subjected to the magnetic susceptibility measurements using Bartington MS2B. Additionally, samples were chemically analyzed by the S Helmholtz Centre Potsdam, GFZ German Research Centre for Geosciences in Potsdam. Values of magnetic susceptibility varied from 9.3 to 1382 ×10-8 m3/kg in organic soil horizon and from 0.1 to 2105 ×10-8 m3/kg in dipper layers. Calculated correlation coefficients between magnetic susceptibility and some elements indicate significant relationships characteristic for different factors influenced soil properties (pollution level, land use and parent rocks). The northern part of Saxony is divided by the Elbe into two parts: east part with loose sedimentary rocks and the west one with more solid loess bedrock enriched by spectrum of elements from the Ore Mountains. Correlations between magnetic susceptibility and Ca, Fe, Mn, and Zn were stated in the eastern, while soil magnetic susceptibility of the western part revealed a correlation with Fe, P, Cd, Cu, Pb, Zn, Mo, U, V, and W. Taking into account influences of industry and urbanization, soil magnetic susceptibility is enhanced in the areas with higher population density comparing with rural sites. In the area of Hoyerswerda and Weisswasser with low magnetic natural

  20. Dedicated phantom to study susceptibility artifacts caused by depth electrode in magnetic resonance imaging

    NASA Astrophysics Data System (ADS)

    Garcia, J.; Hidalgo, S. S.; Solis, S. E.; Vazquez, D.; Nuñez, J.; Rodriguez, A. O.

    2012-10-01

    The susceptibility artifacts can degrade of magnetic resonance image quality. Electrodes are an important source of artifacts when performing brain imaging. A dedicated phantom was built using a depth electrode to study the susceptibility effects under different pulse sequences. T2-weighted images were acquired with both gradient-and spin-echo sequences. The spin-echo sequences can significantly attenuate the susceptibility artifacts allowing a straightforward visualization of the regions surrounding the electrode.

  1. Investigation of ac-magnetic field stimulated nanoelectroporation of magneto-electric nano-drug-carrier inside CNS cells.

    PubMed

    Kaushik, Ajeet; Nikkhah-Moshaie, Roozbeh; Sinha, Raju; Bhardwaj, Vinay; Atluri, Venkata; Jayant, Rahul Dev; Yndart, Adriana; Kateb, Babak; Pala, Nezih; Nair, Madhavan

    2017-04-04

    In this research, we demonstrate cell uptake of magneto-electric nanoparticles (MENPs) through nanoelectroporation (NEP) using alternating current (ac)-magnetic field stimulation. Uptake of MENPs was confirmed using focused-ion-beam assisted transmission electron microscopy (FIB-TEM) and validated by a numerical simulation model. The NEP was performed in microglial (MG) brain cells, which are highly sensitive for neuro-viral infection and were selected as target for nano-neuro-therapeutics. When the ac-magnetic field optimized (60 Oe at 1 kHz), MENPs were taken up by MG cells without affecting cell health (viability > 92%). FIB-TEM analysis of porated MG cells confirmed the non-agglomerated distribution of MENPs inside the cell and no loss of their elemental and crystalline characteristics. The presented NEP method can be adopted as a part of future nanotherapeutics and nanoneurosurgery strategies where a high uptake of a nanomedicine is required for effective and timely treatment of brain diseases.

  2. Investigation of ac-magnetic field stimulated nanoelectroporation of magneto-electric nano-drug-carrier inside CNS cells

    PubMed Central

    Kaushik, Ajeet; Nikkhah-Moshaie, Roozbeh; Sinha, Raju; Bhardwaj, Vinay; Atluri, Venkata; Jayant, Rahul Dev; Yndart, Adriana; Kateb, Babak; Pala, Nezih; Nair, Madhavan

    2017-01-01

    In this research, we demonstrate cell uptake of magneto-electric nanoparticles (MENPs) through nanoelectroporation (NEP) using alternating current (ac)-magnetic field stimulation. Uptake of MENPs was confirmed using focused-ion-beam assisted transmission electron microscopy (FIB-TEM) and validated by a numerical simulation model. The NEP was performed in microglial (MG) brain cells, which are highly sensitive for neuro-viral infection and were selected as target for nano-neuro-therapeutics. When the ac-magnetic field optimized (60 Oe at 1 kHz), MENPs were taken up by MG cells without affecting cell health (viability > 92%). FIB-TEM analysis of porated MG cells confirmed the non-agglomerated distribution of MENPs inside the cell and no loss of their elemental and crystalline characteristics. The presented NEP method can be adopted as a part of future nanotherapeutics and nanoneurosurgery strategies where a high uptake of a nanomedicine is required for effective and timely treatment of brain diseases. PMID:28374799

  3. High Susceptibility to Cry1Ac and Low Resistance Allele Frequency Reduce the Risk of Resistance of Helicoverpa armigers to Bt Soybean in Brazil.

    PubMed

    Dourado, Patrick M; Bacalhau, Fabiana B; Amado, Douglas; Carvalho, Renato A; Martinelli, Samuel; Head, Graham P; Omoto, Celso

    2016-01-01

    The Old World bollworm, Helicoverpa armigera (Hübner), was recently introduced into Brazil, where it has caused extensive damage to cotton and soybean crops. MON 87701 × MON 89788 soybean, which expresses the Bt protein Cry1Ac, was recently deployed in Brazil, providing high levels of control against H. armigera. To assess the risk of resistance to the Cry1Ac protein expressed by MON 87701 × MON 89788 soybean in Brazil, we conducted studies to evaluate the baseline susceptibility of H. armigera to Cry1Ac, in planta efficacy including the assessment of the high-dose criterion, and the initial resistance allele frequency based on an F2 screen. The mean Cry1Ac lethal concentration (LC50) ranged from 0.11 to 1.82 μg·mL-1 of diet among all H. armigera field populations collected from crop seasons 2013/14 to 2014/15, which indicated about 16.5-fold variation. MON 87701 × MON 89788 soybean exhibited a high level of efficacy against H. armigera and most likely met the high dose criterion against this target species in leaf tissue dilution bioassays up to 50 times. A total of 212 F2 family lines of H. armigera were established from field collections sampled from seven locations across Brazil and were screened for the presence of MON 87701 × MON 89788 soybean resistance alleles. None of the 212 families survived on MON 87701 × MON 89788 soybean leaf tissue (estimated allele frequency = 0.0011). The responses of H. armigera to Cry1Ac protein, high susceptibility to MON 87701 × MON 89788 soybean, and low frequency of resistance alleles across the main soybean-producing regions support the assumptions of a high-dose/refuge strategy. However, maintenance of reasonable compliance with the refuge recommendation will be essential to delay the evolution of resistance in H. armigera to MON 87701 × MON 89788 soybean in Brazil.

  4. Magnetic and magnetocaloric properties of spin-glass material DyNi 0.67Si 1.34

    DOE PAGES

    Chen, X.; Mudryk, Y.; Pathak, A. K.; ...

    2017-04-18

    Structural, magnetic, and magnetocaloric properties of DyNi 0.67Si 1.34 were investigated using X-ray powder diffraction, magnetic susceptibility, and magnetization measurements. X-ray powder diffraction pattern shows that DyNi 0.67Si 1.34 crystallizes in the AlB 2-type hexagonal structure (space group: P6/ mmm, No. 191, a = b = 3.9873(9) Å, and c = 3.9733(1) Å). The compound is a spin-glass with the freezing temperature TG = 6.2 K. The ac magnetic susceptibility measurements confirm magnetic frustration in DyNi 0.67Si 1.34. Furthermore, the maximum value of the magnetic entropy change determined from M(H) data is –16.1 J/kg K at 10.5 K for amore » field change of 70 kOe.« less

  5. Mapping soil magnetic susceptibility and mineralogy in Ukraine

    NASA Astrophysics Data System (ADS)

    Menshov, Oleksandr; Pereira, Paulo; Kruglov, Oleksandr; Sukhorada, Anatoliy

    2017-04-01

    Soil suatainable planning is fundamental for agricultural areas. Soil mapping and modeling are increasingly used in agricultural areas in the entire world (Brevik et al., 2016). They are beneficial to land managers, to reduce soil degradation, increase soil productivity and their restoration. Magnetic susceptibility (MS) methods are low cost and accurate for the developing maps of agricultural areas.. The objective of this work is to identify the minerals responsible for MS increase in soils from the two study areas in Poltava and Kharkiv region. The thermomagnetic analyses were conducted using the KLY-4 with an oven apparatus. The hysteresis parameters were measured with the Rotating Magnetometer at the Geophysical Centre Dourbes, Belgium. The results showed that all of samples from Kharkiv area and the majortity of the samples collected in Poltava area represent the pseudo single domain (PSD) zone particles in Day plot. According to Hanesch et al. (2006), the transformation of goethite, ferrihydrite or hematite to a stronger ferrimagnetic phase like magnetite or maghemite is common in strongly magnetic soils with high values of organic carbon content. In our case of thermomagnetic study, the first peak on the heating curve near 260 ˚C indicates the presence of ferrihydrite which gradually transforms into maghemite (Jordanova et al., 2013). A further decrease in the MS identified on the heating curve may be related to the transformation of the maghemite to hematite. A second MS peak on the heating curve near 530 ˚C and the ultimate loss of magnetic susceptibility near 580 ˚C were caused by the reduction of hematite to magnetite. The shape of the thermomagnetic curves suggests the presence of single domain (SD) particles at room temperature and their transformation to a superparamagnetic (SP) state under heating. Magnetic mineralogical analyses suggest the presence of highly magnetic minerals like magnetite and maghemite as well as slightly magnetic goethite

  6. Low signal-to-noise FDEM in-phase data: Practical potential for magnetic susceptibility modelling

    NASA Astrophysics Data System (ADS)

    Delefortrie, Samuël; Hanssens, Daan; De Smedt, Philippe

    2018-05-01

    In this paper, we consider the use of land-based frequency-domain electromagnetics (FDEM) for magnetic susceptibility modelling. FDEM data comprises both out-of-phase and in-phase components, which can be related to the electrical conductivity and magnetic susceptibility of the subsurface. Though applying the FDEM method to obtain information on the subsurface conductivity is well established in various domains (e.g. through the low induction number approximation of subsurface apparent conductivity), the potential for susceptibility mapping is often overlooked. Especially given a subsurface with a low magnetite and maghemite content (e.g. most sedimentary environments), it is generally assumed that susceptibility is negligible. Nonetheless, the heterogeneity of the near surface and the impact of anthropogenic disturbances on the soil can cause sufficient variation in susceptibility for it to be detectable in a repeatable way. Unfortunately, it can be challenging to study the potential for susceptibility mapping due to systematic errors, an often poor low signal-to-noise ratio, and the intricacy of correlating in-phase responses with subsurface susceptibility and conductivity. Alongside use of an accurate forward model - accounting for out-of-phase/in-phase coupling - any attempt at relating the in-phase response with subsurface susceptibility requires overcoming instrument-specific limitations that burden the real-world application of FDEM susceptibility mapping. Firstly, the often erratic and drift-sensitive nature of in-phase responses calls for relative data levelling. In addition, a correction for absolute levelling offsets may be equally necessary: ancillary (subsurface) susceptibility data can be used to assess the importance of absolute in-phase calibration though hereby accurate in-situ data is required. To allow assessing the (importance of) in-phase calibration alongside the potential of FDEM data for susceptibility modelling, we consider an experimental

  7. Evaluation, development, and characterization of superconducting materials for space application

    NASA Technical Reports Server (NTRS)

    Thorpe, A. N.

    1989-01-01

    Results are reported of low magnetic field studies of dc magnetic susceptibility and ac magnetic susceptibility of bulk samples and powders. These data are analyzed and compared with the microstructures and compositions of the samples as determined by scanning electron microscopic micrographs, X-ray and chemical analysis. Particular emphasis is given to the interpretation of the ac magnetic susceptibility data which were obtained as function of the magnitude and frequency of the ac measuring field, and low values of an applied dc magnetic field. Two general conclusions are given and briefly discussed.

  8. The cellular magnetic response and biocompatibility of biogenic zinc- and cobalt-doped magnetite nanoparticles

    NASA Astrophysics Data System (ADS)

    Moise, Sandhya; Céspedes, Eva; Soukup, Dalibor; Byrne, James M.; El Haj, Alicia J.; Telling, Neil D.

    2017-01-01

    The magnetic moment and anisotropy of magnetite nanoparticles can be optimised by doping with transition metal cations, enabling their properties to be tuned for different biomedical applications. In this study, we assessed the suitability of bacterially synthesized zinc- and cobalt-doped magnetite nanoparticles for biomedical applications. To do this we measured cellular viability and activity in primary human bone marrow-derived mesenchymal stem cells and human osteosarcoma-derived cells. Using AC susceptibility we studied doping induced changes in the magnetic response of the nanoparticles both as stable aqueous suspensions and when associated with cells. Our findings show that the magnetic response of the particles was altered after cellular interaction with a reduction in their mobility. In particular, the strongest AC susceptibility signal measured in vitro was from cells containing high-moment zinc-doped particles, whilst no signal was observed in cells containing the high-anisotropy cobalt-doped particles. For both particle types we found that the moderate dopant levels required for optimum magnetic properties did not alter their cytotoxicity or affect osteogenic differentiation of the stem cells. Thus, despite the known cytotoxicity of cobalt and zinc ions, these results suggest that iron oxide nanoparticles can be doped to sufficiently tailor their magnetic properties without compromising cellular biocompatibility.

  9. The cellular magnetic response and biocompatibility of biogenic zinc- and cobalt-doped magnetite nanoparticles

    PubMed Central

    Moise, Sandhya; Céspedes, Eva; Soukup, Dalibor; Byrne, James M.; El Haj, Alicia J.; Telling, Neil D.

    2017-01-01

    The magnetic moment and anisotropy of magnetite nanoparticles can be optimised by doping with transition metal cations, enabling their properties to be tuned for different biomedical applications. In this study, we assessed the suitability of bacterially synthesized zinc- and cobalt-doped magnetite nanoparticles for biomedical applications. To do this we measured cellular viability and activity in primary human bone marrow-derived mesenchymal stem cells and human osteosarcoma-derived cells. Using AC susceptibility we studied doping induced changes in the magnetic response of the nanoparticles both as stable aqueous suspensions and when associated with cells. Our findings show that the magnetic response of the particles was altered after cellular interaction with a reduction in their mobility. In particular, the strongest AC susceptibility signal measured in vitro was from cells containing high-moment zinc-doped particles, whilst no signal was observed in cells containing the high-anisotropy cobalt-doped particles. For both particle types we found that the moderate dopant levels required for optimum magnetic properties did not alter their cytotoxicity or affect osteogenic differentiation of the stem cells. Thus, despite the known cytotoxicity of cobalt and zinc ions, these results suggest that iron oxide nanoparticles can be doped to sufficiently tailor their magnetic properties without compromising cellular biocompatibility. PMID:28045082

  10. The application of Halbach cylinders to brushless ac servo motors

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Atallah, K.; Howe, D.

    1998-07-01

    Halbach cylinders are applied to brushless ac servo motors. It is shown that a sinusoidal back-emf waveform and a low cogging torque can be achieved without recourse to conventional design features such as distributed windings and/or stator/rotor skew. A technique for imparting a multipole Halbach magnetization distribution on an isotropic permanent magnet cylinder is described, and it is shown that the torque capability of a Halbach ac servo motor can be up to 33% higher than conventional brushless permanent magnet ac motors.

  11. A comparative quantitative analysis of magnetic susceptibility artifacts in echo planar and PROPELLER diffusion-weighted images

    NASA Astrophysics Data System (ADS)

    Cho, Jae-Hwan; Lee, Hae-Kag; Yang, Han-Joon; Lee, Gui-Won; Park, Yong-Soon; Chung, Woon-Kwan

    2013-01-01

    In this study, the authors investigated whether periodically-rotated overlapping parallel lines with enhanced reconstruction (PROPELLER) diffusion-weighted imaging (DWI) can remove magnetic susceptibility artifacts and compared apparent diffusion coefficient (ADC) values for PROPELLER DWI and the common echo planar (EP) DWI. Twenty patients that underwent brain MRI with a metal dental implant were selected. A 3.0T MR scanner was then used to obtain EP DWI, PROPELLER DWI, and corresponding apparent diffusion coefficient (ADC) maps for a b-value of 0 and 1,000 s/mm2. The frequencies of magnetic susceptibility artifacts in four parts of the brain (bilateral temporal lobes, pons, and orbit) were selected. In the ADC maps, we measured the ADC values of both sides of the temporal lobe and the pons. According to the study results, the frequency of magnetic susceptibility artifacts in PROPELLER DW images was lower than it was in EP DW images. In ADC maps, the ADC values of the bilateral temporal lobes and the pons were all higher in PROPELLER ADC maps than in EP ADC maps. Our findings show that when a high-field MRI machine is used, magnetic susceptibility artifacts can distort anatomical structures and produce high-intensity signals. Furthermore, our findings suggest that in many cases, PROPELLER DWI would be helpful in terms of achieving a correct diagnosis.

  12. Structural and magnetic characterization of La{sub 0.8}Sr{sub 0.2}MnO{sub 3} nanoparticles prepared via a facile microwave-assisted method

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Moradi, J., E-mail: j_moradi@yahoo.com; Ghazi, M.E.; Ehsani, M.H., E-mail: mhe_ehsani@yahoo.com

    2014-07-01

    Nanoparticles of La{sub 0.8}Sr{sub 0.2}MnO{sub 3} (LSMO) with different particle sizes are synthesized by a very fast, inexpensive, reproducible, and environmentally friendly method: the microwave irradiation of the corresponding mixture of nitrates. The structural and magnetic properties of the samples are investigated by the X-Ray diffraction (XRD), Fourier transform infra-red (FT-IR) spectroscopy, field-emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), and magnetic (DC magnetization and AC susceptibility) measurements. The XRD study coupled with the Rietveld refinement show that all samples crystallize in a rhombohedral structure with the space group of R−3C. The FT-IR spectroscopy and FE-SEM images indicate formationmore » of the perovskite structure of LSMO. The DC magnetization measurements confirm the decrease in the particle size effects on the magnetic properties, e.g. reduction in the ferromagnetic (FM) moment and increase in the surface spin disorder. Magnetic dynamics of the samples studied by AC magnetic susceptibility shows that the magnetic behavior of the nanometer-sized samples is well-described by the Vogel-Fulcher and critical slowing down laws. Strong interaction between magnetic nanoparticles of LSMO was detected by fitting the experimental data with the mentioned models. - Graphical abstract: Temperature dependence of the magnetization M(T) was measured in the zero-field-cooling (ZFC) and field-cooling (FC) modes at the applied magnetic field of 100 Oe for the La{sub 0.8}Sr{sub 0.2}MnO{sub 3} with different size prepared via a facile microwave-assisted method. - Highlights: • Nanoparticles of La{sub 0.8}Sr{sub 0.2}MnO{sub 3} were synthesized by the microwave irradiation process. • The structural studies show that all samples crystallize in a rhombohedral structure with space group of R−3C. • The DC magnetic studies confirm tuning of the magnetic properties due to the particle size effects.

  13. Magnetic susceptibility of YBa2(Cu/1-x/Fe/x/)3O(y) prepared by various heat treatments

    NASA Astrophysics Data System (ADS)

    Shibata, Tomohiko; Katsuyama, Shigeru; Yoshimura, Kazuyoshi; Kosuge, Koji

    1991-02-01

    The magnetic susceptibility of YBa2(Cu/1-x/Fe/x/)3O(y) specimens was measured following a standard heat treatment and a special heat treament stabilizing the orthorhombic phase to higher Fe concentrations. The values of the effective magnetic moment per Fe in the Cu1 site, estimated from the magnetic susceptibility and Mossbauer effect measurements, were 4.4 and 2.2 muB for the standard and specially treated specimens, respectively. The smaller effective magnetic moment in the case of specially treated specimens is attributed to the antiferromagnetic coupling between Fe spins at high temperatures.

  14. Investigating the anisotropy of magnetic susceptibility and other rock magnetic properties of the Beaver River Diabase in northeastern Minnesota

    NASA Astrophysics Data System (ADS)

    Hariri, Samer H.

    The Beaver River Diabase (BRD) is a series of mafic dikes and sills within the Beaver Bay Complex (BBC) of northern Minnesota, which formed during the development of the ~1.1 Ga Midcontinent Rift (MCR). The BRD is one of the youngest and most extensive intrusive phases of the BBC. The BRD dikes and sills were emplaced into the medial levels of the 6-10 kilometer-thick North Shore Volcanic Group and occur over an arcuate area extending 120 by 20 kilometers. The BRD is composed of fine- to medium-grained ophitic olivine gabbro and does not display obvious foliation or lineation features and rarely displays modal layering. Without obvious magmatic internal structures, it is difficult to determine emplacement properties such as flow direction using standard geologic mapping or petrographic techniques. For this reason, we measured the anisotropy of magnetic susceptibility (AMS), in conjunction with other rock magnetic properties, to better understand the BRD's emplacement and deformation history in the context of the MCR. AMS measures the directional dependence of low-field magnetic susceptibility, and is used to infer a shape-preferred orientation of magnetic minerals within a rock, which can be related to specific emplacement mechanisms (e.g. directional flow or settling). Preliminary analysis of AMS at 20 sites within the southern half of the BRD (with 4-7 samples per site) shows maximum susceptibility values between 4.48 x 10-6 and 2.22 x 10-4 m 3/kg (1165 and 65400 μSI). Most specimens display nearly isotropic AMS ellipsoids (Pj < 1.15) with minor degrees of prolateness and oblateness. However, about 20% of specimens have higher anisotropies (Pj between 1.15 and 1.67) and higher degrees of oblateness and prolateness. Variations in AMS properties may reflect differences in concentration and composition of magnetic minerals, as well as emplacement mechanisms. Measurements of susceptibility as a function of temperature yield Curie points between 470 and 570

  15. Magnetic susceptibility and AMS of the Bushveld alkaline granites, South Africa

    NASA Astrophysics Data System (ADS)

    Ferré, Eric C.; Wilson, Jeff; Gleizes, Gérard

    1999-06-01

    The Bushveld Complex in South Africa includes one of the world's largest anorogenic alkaline granite intrusions (66,000 km 2). The granite forms a composite laccolith, of 350 × 250 km in area and about 2 km in thickness, which was emplaced at about 5 km depth into sediments overlying the Kaapvaal craton, at 2054 Ma. The Bushveld granite and its roof-rocks have long been mined for Sn, W and F. The Bushveld granites have high magnetic susceptibilities ( Km from 1000 to 4000 μSI), and a quantitative model is presented, suggesting that susceptibility fabrics are primarily carried by ferromagnetic minerals. The measured AMS foliations coincide with observed subhorizontal mineral lineations and compositional layering. Magnetic lineation trends vary considerably within the horizontal plane. The existence of a weak planar fabric and, an almost absent linear component may reflect (a) laccolithic emplacement by roof uplift, causing flattening magmatic fabrics, or (b) emplacement of largely crystal-free magma crystallizing in-situ and developing horizontal compositional layering from thermal chemical diffusion fronts and gravity-driven mechanisms. Weak magnétic fabrics, like those identified in the Bushveld granites require specific sampling schemes and procedures, in addition to rigorous constraint of magnetic mineralogy and crystallization sequence.

  16. Attenuation of Mouse Melanoma by A/C Magnetic Field after Delivery of Bi-Magnetic Nanoparticles by Neural Progenitor Cells

    PubMed Central

    Rachakatla, Raja Shekar; Balivada, Sivasai; Seo, Gwi-Moon; Myers, Carl B; Wang, Hongwang; Samarakoon, Thilani N.; Dani, Raj; Pyle, Marla; Kroh, Franklin O.; Walker, Brandon; Leaym, Xiaoxuan; Koper, Olga B.; Chikan, Viktor; Bossmann, Stefan H.; Tamura, Masaaki; Troyer, Deryl L.

    2010-01-01

    Localized magnetic hyperthermia as a treatment modality for cancer has generated renewed interest, particularly if it can be targeted to the tumor site. We examined whether tumor-tropic neural progenitor cells (NPCs) could be utilized as cell delivery vehicles for achieving preferential accumulation of core/shell iron/iron oxide magnetic nanoparticles (MNPs) within a mouse model of melanoma. We developed aminosiloxane-porphyrin functionalized MNPs, evaluated cell viability and loading efficiency, and transplanted neural progenitor cells loaded with this cargo into mice with melanoma. NPCs were efficiently loaded with core/shell Fe/Fe3O4 MNPs with minimal cytotoxicity; the MNPs accumulated as aggregates in the cytosol. The NPCs loaded with MNPs could travel to subcutaneous melanomas, and after A/C (alternating current) magnetic field (AMF) exposure, the targeted delivery of MNPs by the cells resulted in a measurable regression of the tumors. The tumor attenuation was significant (p<0.05) a short time (24 hours) after the last of three AMF exposures. PMID:21058696

  17. Statistical assessment to magnetic susceptibility and heavy metal data for characterizing the coastal sediment of East coast of Tamilnadu, India.

    PubMed

    Harikrishnan, N; Chandrasekaran, A; Ravisankar, R; Alagarsamy, R

    2018-05-01

    A rapid urbanization and industrialization enhances the significant heavy metal pollution in the sediments of coastal area and introduced a serious threat to the human health. In the present study, concentration of heavy metals such as Al, Ti, Fe, V, Cr, Mn, Co, Zn, La, Pb, Mg, Ca, Ni, Cd and Ba are determined in sediments along Periyakalapet to Parangaipettai coastal area, Tamilnadu using energy dispersive X-ray fluorescence spectrometer (EDXRF).These metals have more affinity to establish metallic bond with ferrous material leading to enhancement of sediment magnetic susceptibility. Hence, a magnetic susceptibility (χLF, χHF, χFD) measurement was carried for sediments by using MS2B dual frequency susceptibility meter. Multivariate statistical analysis (Pearson correlation, factor and cluster analysis) was carried out between heavy metals and magnetic susceptibility to assess the anthropogenic impact in the sediments. The study revealed that a magnetic susceptibility measurement is an inexpensive, fast, non-destructive and suitable method to identify the heavy metal pollution sources. Copyright © 2018 Elsevier Ltd. All rights reserved.

  18. Calibration of low-temperature ac susceptometers with a copper cylinder standard

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Chen, D.-X.; Skumryev, V.

    2010-02-15

    A high-quality low-temperature ac susceptometer is calibrated by comparing the measured ac susceptibility of a copper cylinder with its eddy-current ac susceptibility accurately calculated. Different from conventional calibration techniques that compare the measured results with the known property of a standard sample at certain fixed temperature T, field amplitude H{sub m}, and frequency f, to get a magnitude correction factor, here, the electromagnetic properties of the copper cylinder are unknown and are determined during the calibration of the ac susceptometer in the entire T, H{sub m}, and f range. It is shown that the maximum magnitude error and the maximummore » phase error of the susceptometer are less than 0.7% and 0.3 deg., respectively, in the region T=5-300 K and f=111-1111 Hz at H{sub m}=800 A/m, after a magnitude correction by a constant factor as done in a conventional calibration. However, the magnitude and phase errors can reach 2% and 4.3 deg. at 10 000 and 11 Hz, respectively. Since the errors are reproducible, a large portion of them may be further corrected after a calibration, the procedure for which is given. Conceptual discussions concerning the error sources, comparison with other calibration methods, and applications of ac susceptibility techniques are presented.« less

  19. Optimization of spin-torque switching using AC and DC pulses

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Dunn, Tom; Kamenev, Alex; Fine Theoretical Physics Institute, University of Minnesota, Minneapolis, Minnesota 55455

    2014-06-21

    We explore spin-torque induced magnetic reversal in magnetic tunnel junctions using combined AC and DC spin-current pulses. We calculate the optimal pulse times and current strengths for both AC and DC pulses as well as the optimal AC signal frequency, needed to minimize the Joule heat lost during the switching process. The results of this optimization are compared against numeric simulations. Finally, we show how this optimization leads to different dynamic regimes, where switching is optimized by either a purely AC or DC spin-current, or a combination AC/DC spin-current, depending on the anisotropy energies and the spin-current polarization.

  20. Effects of magnetic and nonmagnetic impurities on the spin susceptibility of a noncentrosymmetrical superconductor: Application to CePt3Si

    NASA Astrophysics Data System (ADS)

    Yavari, H.; Mokhtari, M.; Tamaddonpour, M.

    2013-10-01

    The combined effect of nonmagnetic and magnetic impurities on the spin susceptibility of a noncentrosymmetrical superconductor by considering a Cooper pairing model with a two-component order parameter composed of spin-singlet and spin-triplet pairing components is investigated. For clean superconductor CePt3Si, the low-temperature dependence (T →0) of spin susceptibility is linear which suggests that the gap function has line nodes, consistent with our gap model. We will show that in the presence of magnetic impurities the susceptibility does not vanish even in the absence of spin orbit coupling and in the region where the energy gap still is finite, and in the low concentration of magnetic impurities the spin susceptibility at zero temperature is proportional to impurity concentration.

  1. Aging dynamics in the polymer glass of poly(2-chlorostyrene): Dielectric susceptibility and volume

    NASA Astrophysics Data System (ADS)

    Fukao, Koji; Tahara, Daisuke

    2009-11-01

    Aging dynamics was investigated in the glassy states of poly(2-chlorostyrene) by measuring the complex electrical capacitance during aging below the glass transition temperature. The variations with time and temperature of the ac dielectric susceptibility and volume could be determined by simply measuring the variation in the complex electrical capacitance. Isothermal aging at a given temperature for several hours after an intermittent stop in constant-rate cooling is stored in the deviations of both the real and imaginary parts of the complex ac dielectric susceptibility and volume. During cooling after isothermal aging, the deviation of the ac dielectric susceptibility from the reference value decreases and almost vanishes at room temperature. By contrast, the deviation in volume induced during isothermal aging remains almost constant during cooling. The simultaneous measurement of ac dielectric susceptibility and volume clearly revealed that the ac dielectric susceptibility exhibits a full rejuvenation effect, whereas the volume does not show any rejuvenation effects. We discuss a plausible model that can reproduce the present experimental results.

  2. On the magnetism of the C14 Nb0.975Fe2.025 Laves phase compound: Determination of the H-T phase diagram

    NASA Astrophysics Data System (ADS)

    Bałanda, Maria; Dubiel, Stanisław M.

    2018-05-01

    A C14 Nb0.975Fe2.025 Laves phase compound was investigated aimed at determining the H-T magnetic phase diagram. Magnetization, M, and AC magnetic susceptibility measurement were performed. Concerning the former field-cooled and zero-field-cooled M-curves were recorded in the temperature range of 2-200 K and in applied magnetic field, H, up to 1000 Oe, isothermal M(H) curves at 2 K, 5 K, 50 K, 80 K and 110 K as well as hysteresis loops at several temperatures over the field range of ±10 kOe were measured. Regarding the AC susceptibility, χ, both real and imaginary components were registered as a function of increasing temperature in the interval of 2 K-150 K at the frequencies of the oscillating field, f, from 3 Hz up to 999 Hz. An influence of the external DC magnetic field on the temperature dependence of χ was investigated, too. The measurements clearly demonstrated that the magnetism of the studied sample is weak, itinerant and has a reentrant character. Based on the obtained results a magnetic phase diagram has been constructed in the H-T coordinates.

  3. Relationships Between Magnetic Susceptibility and Sedimentary Facies Along AL Qahmah, Southern Red Sea Coast

    NASA Astrophysics Data System (ADS)

    Nabhan, A. I.; Yang, W.

    2016-12-01

    Facies and magnetic parameters of an arid siliciclastic coast were investigated in Al Qahmah, Saudi Arabia. The purpose of the survey was to map and understand the distribution of magnetic minerals in the different sedimentary facies in a 20-km2 area. Four NW-SE profiles parallel to shoreline and thirty-nine roughly perpendicular NE-SW profiles were measured. Petrographic study of sediment composition and texture of 152 samples was conducted. The coast sediments contain six lithofacies: beach, washover fan, tidal channel, eolian dune, sabkha, and wadi. The high concentration of heavy minerals in beach and dune facies causes high magnetic of susceptibility. Mineral composition of the total fraction in these facies confirms the presence of magnetite and ilmenite. The high values of susceptibility in beach and dune facies are attributed to strong winnowing and wave processes that control the pattern of transport, sorting of magnetic minerals in the beach facies. These minerals are picked up and moved by wind at low tide to form extensive low dune fields near the beach. The results showed that magnetic measurements are a sensitive and fast method, which can be used for studying the distribution of magnetic minerals in the sedimentary facies and help interpret various controlling processes.

  4. Soil magnetic susceptibility mapping as a pollution and provenance tool: an example from southern New Zealand

    NASA Astrophysics Data System (ADS)

    Martin, A. P.; Ohneiser, C.; Turnbull, R. E.; Strong, D. T.; Demler, S.

    2018-02-01

    The presence or absence, degree and variation of heavy metal contamination in New Zealand soils is a matter of ongoing debate as it affects soil quality, agriculture and human health. In many instances, however, the soil heavy metal concentration data do not exist to answer these questions and the debate is ongoing. To address this, magnetic susceptibility (a common proxy for heavy metal contamination) values were measured in topsoil (0-30 cm) and subsoil (50-70 cm) at grid sites spaced at 8 km intervals across ca. 20 000 km2 of southern New Zealand. Samples were measured for both mass- and volume-specific magnetic susceptibility, with results being strongly, positively correlated. Three different methods of determining anomalies were applied to the data including the topsoil-subsoil difference method, Tukey boxplot method and geoaccumulation index method, with each method filtering out progressively more anomalies. Additional soil magnetic (hysteresis, isothermal remanence and thermomagnetic) measurements were made on a select subset of samples from anomalous sites. Magnetite is the dominant remanence carrying mineral, and magnetic susceptibility is governed by that minerals concentration in soils, rather than mineral type. All except two anomalous sites have a dominant geogenic source (cf. anthropogenic). By proxy, heavy metal contamination in southern New Zealand soils is minimal, making them relatively pristine. The provenance of the magnetic minerals in the anomalous sites can be traced back to likely sources in outcrops of igneous rocks within the same catchment, terrane or rock type: a distance of <100 km but frequently <1 km. Soil provenance is a key step when mapping element or isotopic distribution, vectoring to mineralization or studying soil for agricultural suitability, water quality or environmental regulation. Measuring soil magnetic susceptibility is a useful, quick and inexpensive tool that usefully supplements soil geochemical data.

  5. On the room temperature multiferroic BiFeO3: magnetic, dielectric and thermal properties

    NASA Astrophysics Data System (ADS)

    Lu, J.; Günther, A.; Schrettle, F.; Mayr, F.; Krohns, S.; Lunkenheimer, P.; Pimenov, A.; Travkin, V. D.; Mukhin, A. A.; Loidl, A.

    2010-06-01

    Magnetic dc susceptibility between 1.5 and 800 K, ac susceptibility and magnetization, thermodynamic properties, temperature dependence of radio and audio-wave dielectric constants and conductivity, contact-free dielectric constants at mm-wavelengths, as well as ferroelectric polarization are reported for single crystalline BiFeO3. A well developed anomaly in the magnetic susceptibility signals the onset of antiferromagnetic order close to 635 K. Beside this anomaly no further indications of phase or glass transitions are indicated in the magnetic dc and ac susceptibilities down to the lowest temperatures. The heat capacity has been measured from 2 K up to room temperature and significant contributions from magnon excitations have been detected. From the low-temperature heat capacity an anisotropy gap of the magnon modes of the order of 6 meV has been determined. The dielectric constants measured in standard two-point configuration are dominated by Maxwell-Wagner like effects for temperatures T > 300 K and frequencies below 1 MHz. At lower temperatures the temperature dependence of the dielectric constant and loss reveals no anomalies outside the experimental errors, indicating neither phase transitions nor strong spin phonon coupling. The temperature dependence of the dielectric constant was measured contact free at microwave frequencies. At room temperature the dielectric constant has an intrinsic value of 53. The loss is substantial and strongly frequency dependent indicating the predominance of hopping conductivity. Finally, in small thin samples we were able to measure the ferroelectric polarization between 10 and 200 K. The saturation polarization is of the order of 40 μC/cm2, comparable to reports in literature.

  6. The metallofullerene field-induced single-ion magnet HoSc2 N@C80.

    PubMed

    Dreiser, Jan; Westerström, Rasmus; Zhang, Yang; Popov, Alexey A; Dunsch, Lothar; Krämer, Karl; Liu, Shi-Xia; Decurtins, Silvio; Greber, Thomas

    2014-10-13

    The low-temperature magnetic properties of the endohedral metallofullerene HoSc2 N@C80 have been studied by superconducting quantum interference device (SQUID) magnetometry. Alternating current (ac) susceptibility measurements reveal that this molecule exhibits slow relaxation of magnetization in a small applied field with timescales in the order of milliseconds. The equilibrium magnetic properties of HoSc2 N@C80 indicate strong magnetic anisotropy. The large differences in magnetization relaxation times between the present compound and the previously investigated DySc2 N@C80 are discussed. © 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  7. Design of PCB search coils for AC magnetic flux density measurement

    NASA Astrophysics Data System (ADS)

    Ulvr, Michal

    2018-04-01

    This paper presents single-layer, double-layer and ten-layer planar square search coils designed for AC magnetic flux density amplitude measurement up to 1 T in the low frequency range in a 10 mm air gap. The printed-circuit-board (PCB) method was used for producing the search coils. Special attention is given to a full characterization of the PCB search coils including a comparison between the detailed analytical design method and the finite integration technique method (FIT) on the one hand, and experimental results on the other. The results show very good agreement in the resistance, inductance and search coil constant values (the area turns) and also in the frequency dependence of the search coil constant.

  8. Irreversibility Line Measurement and Vortex Dynamics in High Magnetic Fields in Ni- and Co-Doped Iron Pnictide Bulk Superconductors

    DOE PAGES

    Nikolo, Martin; Singleton, John; Zapf, Vivien S.; ...

    2016-07-20

    The de-pinning or irreversibility lines were determined by ac susceptibility, magnetization, radio-frequency proximity detector oscillator (PDO), and resistivity methods in Ba(Fe 0.92Co 0.08) 2As 2 ( T c = 23.2 K), Ba(Fe 0.95Ni 0.05) 2As 2 ( T c = 20.4 K), and Ba(Fe 0.94Ni 0.06) 2As 2 ( T c = 18.5 K) bulk superconductors in ac, dc, and pulsed magnetic fields up to 65 T. A new method of extracting the irreversibility fields from the radio-frequency proximity detector oscillator induction technique is described. Wide temperature broadening of the irreversibility lines, for any given combination of ac and dcmore » fields, is dependent on the time frame of measurement. Increasing the magnetic field sweep rate (dH/dt) shifts the irreversibility lines to higher temperatures up to about dH/d t = 40,000 Oe/s; for higher dH/dt, there is little impact on the irreversibility line. There is an excellent data match between the irreversibility fields obtained from magnetization hysteresis loops, PDO, and ac susceptibility measurements, but not from resistivity measurements in these materials. Lower critical field vs. temperature phase diagrams are measured. Their very low values near 0 T indicate that these materials are in mixed state in nonzero magnetic fields, and yet the strength of the vortex pinning enables very high irreversibility fields, as high as 51 T at 1.5 K for the Ba(Fe 0.92Co 0.08) 2As 2 polycrystalline sample, showing a promise for liquid helium temperature applications.« less

  9. Global Lithospheric Apparent Susceptibility Distribution Converted from Geomagnetic Models by CHAMP and Swarm Satellite Magnetic Measurements

    NASA Astrophysics Data System (ADS)

    Du, Jinsong; Chen, Chao; Xiong, Xiong; Li, Yongdong; Liang, Qing

    2016-04-01

    Recently, because of continually accumulated magnetic measurements by CHAMP satellite and Swarm constellation of three satellites and well developed methodologies and techniques of data processing and geomagnetic field modeling etc., global lithospheric magnetic anomaly field models become more and more reliable. This makes the quantitative interpretation of lithospheric magnetic anomaly field possible for having an insight into large-scale magnetic structures in the crust and uppermost mantle. Many different approaches have been utilized to understand the magnetized sources, such as forward, inversion, statistics, correlation analysis, Euler deconvolution, signal transformations etc. Among all quantitative interpretation methods, the directly converting a magnetic anomaly map into a magnetic susceptibility anomaly map proposed by Arkani-Hamed & Strangway (1985) is, we think, the most fast quantitative interpretation tool for global studies. We just call this method AS85 hereinafter for short. Although Gubbins et al. (2011) provided a formula to directly calculate the apparent magnetic vector distribution, the AS85 method introduced constraints of magnetized direction and thus corresponding results are expected to be more robust especially in world-wide continents. Therefore, in this study, we first improved the AS85 method further considering non-axial dipolar inducing field using formulae by Nolte & Siebert (1987), initial model or priori information for starting coefficients in the apparent susceptibility conversion, hidden longest-wavelength components of lithospheric magnetic field and field contaminations from global oceanic remanent magnetization. Then, we used the vertically integrated susceptibility model by Hemant & Maus (2005) and vertically integrated remanent magnetization model by Masterton et al. (2013) to test the validity of our improved method. Subsequently, we applied the conversion method to geomagnetic field models by CHAMP and Swarm satellite

  10. Magnetism and atomic short-range order in Ni-Rh alloys

    NASA Astrophysics Data System (ADS)

    Carnegie, D. W., Jr.; Claus, H.

    1984-07-01

    Low-field ac susceptibility measurements of Ni-Rh samples of various concentrations are presented. Giant effects of the metallurgical state on the magnetic ordering temperature are associated with changes in the degree of atomic short-range order. By careful control of this degree of short-range order, it is possible to demonstrate the existence of a spin-glass state in Ni-Rh alloys.

  11. Low temperature magnetic susceptibility behavior of the Neuschwanstein EL6 meteorite and mineral daubreelite (FeCr2S4)

    NASA Astrophysics Data System (ADS)

    Kohout, T.; Kletetschka, G.; Lehtinen, M.; Pesonen, L. J.; Wasilewski, P. J.

    2006-12-01

    Neuschwanstein meteorite (enstatite chondrite EL-6) fall occurred on April 6, 2002 close to Neuschwanstein castle in Bavaria, Germany. Total three meteorite bodies were found on the fall site. Two fragments coming from a 1750g body found on July 14, 2002 were obtained to the Division of Geophysics, University of Helsinki. The low temperature magnetic properties were investigated using KLY-3 and KLY-4 kappabridges equipped with low temperature control unit. During the low-temperature susceptibility measurements an unknown kink feature was observed at ~150 K on all measured samples. The closest known magnetic transition is the curie temperature Tc ~170 K of synthetic FeCr2S4 mentioned in Müller et al., 2006. FeCr2S4 is naturally present in enstatite chondrites and iron meteorites in the form of mineral daubreelite and was reported to be present in the Neuschwanstein meteorite in Zipfel and Dreibus, 2003. The extensive study of magnetic susceptibility of Neuschwanstein meteorite and daubreelite extract form Coahuila iron meteorite (hexahedrite, II A) was conducted in order to investigate the low temperature magnetic susceptibility of those materials and its field and frequency dependence. The results indicate Tc of natural daubreelite extract from Coahuila meteorite to be ~160 K what is slightly lower than the Tc of synthetic FeCr2S4 reported in Müller et al., 2006. The magnetic susceptibility of natural daubreelite from Coahuila meteorite and of ~150 K feature in Neuschwanstein meteorite show no field dependence of magnetic susceptibility. Due to the similarity in the low temperature magnetic susceptibility behaviour of Neuschwanstein meteorite and daubreelite extract from Coahuila meteorite we link the Neuschwanstein ~150 K feature to the Tc of daubreelite present in this meteorite. The 10 K difference of the Tc of daubreelite in Neuschwanstein and Coahuila meteorites can be attributed to the presence of impurities or structural deformations in the daubreelite

  12. Determination of the Impregnant Concentrations on ASC Type Charcoal. A Magnetic Susceptibility Study

    DTIC Science & Technology

    1987-10-01

    commercial magnetic susceptometers were used on site at the Geological Division of CANMET , whose help is greatly appreciated. One of the susceptometers was a...CHARCOAL. A MAGNETIC SUSCEPTIBILITY STUDY (U) by S.H.C. Liang, B.H. Harrison and J.G. Pagotto Chemical Protection Section Protective Sciences Division ...analysis (11, 16-18), and surveys of literature reports (19-23). Some recent advances in instrumentation, such as the vibrating sample magnetometer (24

  13. Impact of grass cover on the magnetic susceptibility measurements for assessing metal contamination in urban topsoil.

    PubMed

    Golden, Nessa; Zhang, Chaosheng; Potito, Aaron P; Gibson, Paul J; Bargary, Norma; Morrison, Liam

    2017-05-01

    In recent decades, magnetic susceptibility monitoring has developed as a useful technique in environmental pollution studies, particularly metal contamination of soil. This study provides the first ever examination of the effects of grass cover on magnetic susceptibility (MS) measurements of underlying urban soils. Magnetic measurements were taken in situ to determine the effects on κ (volume magnetic susceptibility) when the grass layer was present (κ grass ) and after the grass layer was trimmed down to the root (κ no grass ). Height of grass was recorded in situ at each grid point. Soil samples (n=185) were collected and measurements of mass specific magnetic susceptibility (χ) were performed in the laboratory and frequency dependence (χ fd %) calculated. Metal concentrations (Pb, Cu, Zn and Fe) in the soil samples were determined and a gradiometry survey carried out in situ on a section of the study area. Significant correlations were found between each of the MS measurements and the metal content of the soil at the p<0.01 level. Spatial distribution maps were created using Inverse Distance Weighting (IDW) and Local Indicators of Spatial Association (LISA) to identify common patterns. κ grass (ranged from 1.67 to 301.00×10 -5 SI) and κ no grass (ranged from 2.08 to 530.67×10 -5 SI) measured in situ are highly correlated [r=0.966, n=194, p<0.01]. The volume susceptibility datasets in the presence and absence of grass coverage share a similar spatial distribution pattern. This study re-evaluates in situ κ monitoring techniques and the results suggest that the removal of grass coverage prior to obtaining in situ κ measurements of urban soil is unnecessary. This layer does not impede the MS sensor from accurately measuring elevated κ in soils, and therefore κ measurements recorded with grass coverage present can be reliably used to identify areas of urban soil metal contamination. Copyright © 2017 Elsevier Inc. All rights reserved.

  14. Understanding the magnetism in noncentrosymmetric CeIrGe3: Muon spin relaxation and neutron scattering studies

    NASA Astrophysics Data System (ADS)

    Anand, V. K.; Hillier, A. D.; Adroja, D. T.; Khalyavin, D. D.; Manuel, P.; Andre, G.; Rols, S.; Koza, M. M.

    2018-05-01

    The magnetic properties of a pressure induced noncentrosymmetric heavy-fermion superconductor CeIrGe3 have been investigated by muon spin relaxation (μ SR ), powder neutron diffraction (ND), and inelastic neutron scattering (INS) techniques at ambient pressure. For completeness we have also measured the ac magnetic susceptibility χac(T ) , dc magnetic susceptibility χ (T ) , dc isothermal magnetization M (H ) , and heat capacity Cp(T ,H ) down to 2 K. CeIrGe3 is known to exhibit pressure induced superconductivity (Tc≈1.5 K) at a pressure of 20 GPa and antiferromagnetic ordering at 8.7 K, 4.7 K, and 0.7 K at ambient pressure. Our χac(T ) and χ (T ) data show an additional anomaly near 6.2 K which is also captured in Cp(T ) data. From χac(T ) , χ (T ) , and Cp(T ) measurements we infer three antiferromagnetic transitions above 2 K at TN 1=8.5 K, TN 2=6.0 K, and TN 3=4.6 K. Our μ SR study also confirms the presence of three transitions through the observation of one frequency for TN 2magnetic ordering at T =7 K with the propagation vector k = (0,0,0.688(3)), and a commensurate magnetic structure at T =1.5 K with the propagation vector locked to the value k = (0, 0, 2/3) and magnetic moments oriented along the c axis. The commensurate structure couples a macroscopic ferromagnetic component, resulting in a strong dependence of the lock-in transition temperature on external magnetic field. The INS data show two well defined crystal electric field (CEF) excitations arising from the CEF-split Kramers doublet ground state of Ce3 +. The CEF energy levels scheme and wave functions have been determined. The ND and INS results together suggest that the anisotropic magnetic exchange are playing an important role in the magnetism of CeIrGe3.

  15. 150 000 Years of Loess Deposition in Interior Alaska as Told by Magnetic Susceptibility

    NASA Astrophysics Data System (ADS)

    Jensen, B. J. L.; Evans, M. E.; Froese, D. G.; Kravchinsky, V. A.

    2015-12-01

    The Halfway House loess deposit in interior Alaska contains a well-studied and complex paleomagnetic and paleoenvironmental record. Unfortunately, a lack of chronologic control has made it difficult to interpret the results of these studies. Detailed reexamination of stratigraphy, paleomagnetics and tephrostratigraphy reveals a relatively complete marine isotope stage (MIS) 6 to Holocene record constrained by the Old Crow (124 ± 10 ka), VT (106 ± 10 ka), Sheep Creek-Klondike (ca. 80 ka), Dominion Creek (77 ± 8 ka) and Dawson (ca. 30.2 cal ka BP) tephras. Two well-developed paleosols are shown to have formed during Marine Isotope Stages (MIS) 5e and 5a, while MIS 5c and 5b are either poorly represented or absent. A magnetic excursion is identified as the post-Blake excursion (94.1 ± 7.8 ka) and provides independent age control while adding to an increasing body of evidence that Alaskan loess is a detailed recorder of variations of the Earth's magnetic field over time. High-resolution magnetic susceptibility profiles placed into this new chronostratigraphic framework help refine loess deposition models for the interior of Alaska, while providing a means to correlate to previous magnetic studies at this site. The profiles support the hypothesis that wind-intensity is the main variable controlling fluctuations in susceptibility, with the highest susceptibility during peak glacial times and the lowest values in paleosols representing interglacials. However, the correlation of the susceptibility record to global marine d18O records is complicated by highly variable accumulation rates. We find the lowest rates of accumulation during peak warm and cold stages, while abrupt increases are associated with periods of transition between marine isotope stages, represented by intermediate susceptibility values. Previous accumulation models for Alaska have emphasized the role of surface roughness as an important variable controlling loess accumulation. However our results

  16. Magnetic Studies on Eu3MO7 (M = Nb, Ta, Ir) with Fluorite-related Structure by 151Eu Mössbauer Spectroscopy and Magnetic Susceptibility Measurements

    NASA Astrophysics Data System (ADS)

    Hinatsu, Yukio; Doi, Yoshihiro; Wakeshima, Makoto

    2018-06-01

    Magnetic properties of europium-containing compounds Eu3MO7 (M = Nb, Ta, Ir) with fluorite-related structure have been investigated. Magnetic susceptibility measurements show that all these compounds are paramagnetic and have no magnetic ordering down to 1.8 K. At very low temperatures (T<50 K), the susceptibilities of each compound attain constant values, which is characteristic of the ground state for Eu3+ ions. The results of 151Eu Mössbauer spectroscopic measurements show that the asymmetric parameter for Eu(2) in seven-coordination is much larger than that for Eu(1) in cubic environment, which in accordance with the crystallographic result.

  17. Experimentally determined transport and magnetization ac losses of small cable models constructed from YBCO coated conductors

    NASA Astrophysics Data System (ADS)

    Šouc, J.; Vojenčiak, M.; Gömöry, F.

    2010-04-01

    Several short cable models were constructed from YBCO coated conductor (YBCO CC) to study their basic dc and ac electrical properties. They were prepared using superconducting tapes helically wound on fiberglass former of different diameter (5, 8 and 10 mm) with different twist pitch (from 1.7 up to 2.4 cm). The number of parallel-connected tapes ranged from 1 up to 6. The standard length of the models was 11 cm. In one case a 35 cm long model has been manufactured in order to perform a bending test. We observed that the critical currents of the models were proportional to the number of tapes used for their construction. Transport and magnetization ac loss were measured at 36 and 72 Hz.

  18. Study of the Dependency on Magnetic Field and Bias Voltage of an AC-Biased TES Microcalorimeter

    NASA Technical Reports Server (NTRS)

    Gottardi, L.; Bruijn, M.; denHartog, R.; Hoevers, H.; deKorte, P.; vanderKuur, J.; Linderman, M.; Adams, J.; Bailey, C.; Bandler, S.; hide

    2012-01-01

    At SRON we are studying the performance of a Goddard Space Flight Center single pixel TES microcalorimeter operated in an AC bias configuration. For x-ray photons at 6 keV the pixel shows an x-ray energy resolution Delta E(sub FWHM) = 3.7 eV, which is about a factor 2 worse than the energy resolution observed in an identical DC-biased pixel. In order to better understand the reasons for this discrepancy we characterized the detector as a function of temperature, bias working point and applied perpendicular magnetic field. A strong periodic dependency of the detector noise on the TES AC bias voltage is measured. We discuss the results in the framework of the recently observed weak-link behaviour of a TES microcalorimeter.

  19. Magnetic susceptibilities of actinide 3d-metal intermetallic compounds

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Muniz, R.B.; d'Albuquerque e Castro, J.; Troper, A.

    1988-04-15

    We have numerically calculated the magnetic susceptibilities which appear in the Hartree--Fock instability criterion for actinide 3d transition-metal intermetallic compounds. This calculation is based on a previous tight-binding description of these actinide-based compounds (A. Troper and A. A. Gomes, Phys. Rev. B 34, 6487 (1986)). The parameters of the calculation, which starts from simple tight-binding d and f bands are (i) occupation numbers, (ii) ratio of d-f hybridization to d bandwidth, and (iii) electron-electron Coulomb-type interactions.

  20. Time-domain Response of a Metal Detector to a Target Buried in Soil with Frequency-dependent Magnetic Susceptibility

    DTIC Science & Technology

    2016-07-06

    The work reported in this paper is a part of on-going studies to clarify how and to what extent soil electromagnetic properties affect the...metallic sphere buried in a non-conducting soil half-space with frequency-dependent complex magnetic susceptibility. The sphere is chosen as a simple...prototype for the small metal parts in low-metal landmines, while soil with dispersive magnetic susceptibility is a good model for some soils that are

  1. A fast and remote magnetonanothermometry for a liquid environment

    NASA Astrophysics Data System (ADS)

    He, Le; Liu, Wenzhong; Xie, Qingguo; Pi, Shiqiang; Morais, P. C.

    2016-02-01

    This study reports on a new approach for remote nanothermometry with short response time (milliseconds) aiming to operate in liquid media using AC susceptibility components of a suspended magnetic nanoparticle subjected to the Brownian relaxation mechanism. A simple, low cost, and accurate system was designed to measure AC susceptibility using an AC magnetic field at small amplitude (6 Oe) and frequency range (5 kHz) superimposed on a weak DC magnetic field (up to 30 Oe). A model based on the AC susceptibility of magnetic nanoparticles (30 nm average diameter) was constructed to describe the temperature measurement sensitivity of the dominated Brownian relaxation time. A new approach for remote nanothermometry was achieved with measured AC susceptibility by the designed system and the proposed model. Our experimental results show that our magnetonanothermometer allows temperature errors lower than 0.3 K with standard deviations lower than 0.1 K in the temperature range from 310 to 320 K.

  2. Dynamic model tracking design for low inertia, high speed permanent magnet ac motors.

    PubMed

    Stewart, P; Kadirkamanathan, V

    2004-01-01

    Permanent magnet ac (PMAC) motors have existed in various configurations for many years. The advent of rare-earth magnets and their associated highly elevated levels of magnetic flux makes the permanent magnet motor attractive for many high performance applications from computer disk drives to all electric racing cars. The use of batteries as a prime storage element carries a cost penalty in terms of the unladen weight of the vehicle. Minimizing this cost function requires the minimum electric motor size and weight to be specified, while still retaining acceptable levels of output torque. This tradeoff can be achieved by applying a technique known as flux weakening which will be investigated in this paper. The technique allows the speed range of a PMAC motor to be greatly increased, giving a constant power range of more than 4:1. A dynamic model reference controller is presented which has advantages in ease of implementation, and is particularly suited to dynamic low inertia applications such as clutchless gear changing in high performance electric vehicles. The benefits of this approach are to maximize the torque speed envelope of the motor, particularly advantageous when considering low inertia operation. The controller is examined experimentally, confirming the predicted performance.

  3. An experimental study on the magnetic and exchange bias properties of selected Mn rich Ni-Mn-Ga based Heusler alloys

    NASA Astrophysics Data System (ADS)

    Albagami, Abdullah Mohamed

    In this Thesis project, an experimental study on the magnetic and exchange bias properties of a series of polycrystalline Ni1.7-xMn1.7+x Ga0.6 alloys have been investigated by x-ray diffraction, dc magnetization, and ac susceptibility measurements. X-ray diffraction measurement showed that all prepared samples have a tetragonal L10 martensitic structure at room temperature. Scanning electron microscopy measurements show that the compounds are single phase. With increasing Mn concentration x, the lattice parameters marginally increases. The temperature dependence of magnetization data show two distinct transitions in the alloys. At lower temperatures, a peak in the data is observed while the ferromagnetic to paramagnetic transition occurs at higher temperatures. With increasing Mn concentration, the temperature of both transitions increases. Thermomagnetic irreversibility is observed in the magnetization data of all alloys. The ac susceptibility measurements on the materials show the existence of frequency dependence, which suggest that the thermomagnetic irreversibility in the magnetization data is due to the spin glass like ground state in the alloys. The spin glass like ground state with competing magnetic interactions result in the observation of double-shifted hysteresis loop and exchange bias effects in the alloys. The magnitude of the exchange bias field is strongly dependent on the cooling field.

  4. Influences of Cry1Ac broccoli on larval survival and oviposition of diamondback moth.

    PubMed

    Yi, Dengxia; Cui, Shusong; Yang, Limei; Fang, Zhiyuan; Liu, Yumei; Zhuang, Mu; Zhang, Yangyong

    2015-01-01

    Larval survival and oviposition behavior of three genotypes of diamondback moth, Plutella xylostella L. (Lepidoptera: Plutellidae), (homozygous Cry1Ac-susceptibile, Cry1Ac-resistant, and their F1 hybrids), on transgenic Bacillus thuringiensis (Bt) broccoli expressing different levels of Cry1Ac protein were evaluated in laboratory. These Bt broccoli lines were designated as relative low, medium, and high, respectively, according to the Cry1Ac content. Untransformed brocccoli plants were used as control. Larval survival of diamondback moth on non-Bt leaves was not significantly different among the three genotypes. The Cry1Ac-resistant larvae could survive on the low level of Bt broccoli plants, while Cry1Ac-susceptible and F1 larvae could not survive on them. The three genotypes of P. xylostella larvae could not survive on medium and high levels of Bt broccoli. In oviposition choice tests, there was no significant difference in the number of eggs laid by the three P. xylostella genotypes among different Bt broccoli plants. The development of Cry1Ac-susceptible and Cry1Ac-resistant P. xylostella on intact Bt plants was also tested in greenhouse. All susceptible P. xylostella larvae died on all Bt plants, while resistant larvae could survive on broccoli, which expresses low Cry1Ac protein under greenhouse conditions. The results of the greenhouse trials were similar to that of laboratory tests. This study indicated that high dose of Bt toxins in broccoli cultivars or germplasm lines is required for effective resistance management. © The Author 2015. Published by Oxford University Press on behalf of the Entomological Society of America.

  5. Magnetic susceptibility and spin-lattice interactions in U1-xPuxO2 single crystals

    NASA Astrophysics Data System (ADS)

    Kolberg, D.; Wastin, F.; Rebizant, J.; Boulet, P.; Lander, G. H.; Schoenes, J.

    2002-12-01

    Single crystals of mixed uranium-plutonium dioxides have been grown by means of a chemical vapor transport reaction and characterized by x-ray diffraction on bulk and powdered single crystals. Magnetization and susceptibility data were taken using a commercial superconducting quantum interference device. Characteristic ordering temperatures have been determined as well as paramagnetic Curie temperatures and effective magnetic moments. Departures of the reciprocal susceptibility as a function of temperature from linearity have been treated in detail based on a model of vibronic interactions introduced to explain the gross features of susceptibility measurements on thorium-diluted UO2 [Sasaki and Obata, J. Phys. Soc. Jpn. 28, 1157 (1970)]. The influence of spin-lattice interactions causes a certain shape of the observed 1/χ vs T curves from which we are able to suggest different mechanisms for the interactions as a function of the constituent’s concentrations. From our susceptibility measurements characteristic parameters have been calculated using a model of tetragonal vibrational modes of the oxygen cage surrounding each uranium ion. These include specific coupling parameters G, mode characteristic temperatures Tω, and molecular-field constants λ.

  6. Susceptibility Tensor Imaging (STI) of the Brain

    PubMed Central

    Li, Wei; Liu, Chunlei; Duong, Timothy Q.; van Zijl, Peter C.M.; Li, Xu

    2016-01-01

    Susceptibility tensor imaging (STI) is a recently developed MRI technique that allows quantitative determination of orientation-independent magnetic susceptibility parameters from the dependence of gradient echo signal phase on the orientation of biological tissues with respect to the main magnetic field. By modeling the magnetic susceptibility of each voxel as a symmetric rank-2 tensor, individual magnetic susceptibility tensor elements as well as the mean magnetic susceptibility (MMS) and magnetic susceptibility anisotropy (MSA) can be determined for brain tissues that would still show orientation dependence after conventional scalar-based quantitative susceptibility mapping (QSM) to remove such dependence. Similar to diffusion tensor imaging (DTI), STI allows mapping of brain white matter fiber orientations and reconstruction of 3D white matter pathways using the principal eigenvectors of the susceptibility tensor. In contrast to diffusion anisotropy, the main determinant factor of susceptibility anisotropy in brain white matter is myelin. Another unique feature of susceptibility anisotropy of white matter is its sensitivity to gadolinium-based contrast agents. Mechanistically, MRI-observed susceptibility anisotropy is mainly attributed to the highly ordered lipid molecules in myelin sheath. STI provides a consistent interpretation of the dependence of phase and susceptibility on orientation at multiple scales. This article reviews the key experimental findings and physical theories that led to the development of STI, its practical implementations, and its applications for brain research. PMID:27120169

  7. Detection of the pedogenic magnetic fraction in volcanic soils developed on basalts using frequency-dependent magnetic susceptibility: comparison of two instruments

    NASA Astrophysics Data System (ADS)

    Grison, Hana; Petrovsky, Eduard; Kapicka, Ales; Hanzlikova, Hana

    2017-05-01

    In studies of the magnetic properties of soils, the frequency-dependent magnetic susceptibility percentage (χFD%) is often used for the identification of ultrafine magnetically superparamagnetic/stable single-domain (SP/SSD) particles. This parameter is commonly used as an indicator for increased pedogenesis. In strongly magnetic soils, the SP/SSD magnetic signal (mostly bio-pedogenic) may be masked by lithological signals; making pedogenesis hard to detect. In this study, we compare results for the detection of ultrafine SP/SSD magnetic particles in andic soils using two instruments: a Bartington MS2B dual-frequency meter and an AGICO Kappabridge MFK1-FA. In particular, the study focuses on the effect of pedogenesis by investigating the relationship between specific soil magnetic and chemical properties (soil organic carbon and pHH2O). The values of χFD% obtained with the MS2B varied from 2.4 to 5.9 per cent, and mass-specific magnetic susceptibility (χLF) from 283 to 1688 × 10-8 m3 kg-1, while values of χFD% and χLF obtained with the MFK1-FA varied from 2.7 to 8.2 per cent and from 299 to 1859 × 10-8 m3 kg-1, respectively. Our results suggest that the detection of the SP/SSD magnetic fraction can be accomplished by comparing relative trends of χFD% along the soil profile. Moreover, the discrimination between bio-pedogenic and lithogenic magnetic contributions in the SP/SSD fraction is possible by comparing the χFD% and χLF data determined in the fine earth (<2 mm) and the coarse fraction (4-10 mm) samples down the soil profile.

  8. Superconductor-Mediated Modification of Gravity? AC Motor Experiments with Bulk YBCO Disks in Rotating Magnetic Fields

    NASA Technical Reports Server (NTRS)

    Noever, David A.; Koczor, Ronald J.; Roberson, Rick

    1998-01-01

    We have previously reported results using a high precision gravimeter to probe local gravity changes in the neighborhood of large bulk-processed high-temperature superconductors. Podkietnov, et al (Podkietnov, E. and Nieminen, R. (1992) A Possibility of Gravitational Force Shielding by Bulk YBa2 Cu3 O7-x Superconductor, Physica C, C203:441-444.) have indicated that rotating AC fields play an essential role in their observed distortion of combined gravity and barometric pressure readings. We report experiments on large (15 cm diameter) bulk YBCO ceramic superconductors placed in the core of a three-phase, AC motor stator. The applied rotating field produces up to a 12,000 revolutions per minute magnetic field. The field intensity decays rapidly from the maximum at the outer diameter of the superconducting disk (less than 60 Gauss) to the center (less than 10 Gauss). This configuration was applied with and without a permanent DC magnetic field levitating the superconducting disk, with corresponding gravity readings indicating an apparent increase in observed gravity of less than 1 x 10(exp -6)/sq cm, measured above the superconductor. No effect of the rotating magnetic field or thermal environment on the gravimeter readings or on rotating the superconducting disk was noted within the high precision of the observation. Implications for propulsion initiatives and power storage flywheel technologies for high temperature superconductors will be discussed for various spacecraft and satellite applications.

  9. Self-induced pinning of vortices in the presence of ac driving force in magnetic superconductors

    NASA Astrophysics Data System (ADS)

    Bulaevskii, Lev N.; Lin, Shi-Zeng

    2012-12-01

    We derive the response of the magnetic superconductors in the vortex state to the ac Lorentz force, FL(t)=Facsin(ωt), taking into account the interaction of vortices with the magnetic moments described by the relaxation dynamics (polaronic effect). At low amplitudes of the driving force Fac the dissipation in the system is suppressed due to the enhancement of the effective viscosity at low frequencies and due to formation of the magnetic pinning at high frequencies ω. In the adiabatic limit with low frequencies ω and high amplitude of the driving force Fac, the vortex and magnetic polarization form a vortex polaron when FL(t) is small. When FL increases, the vortex polaron accelerates and at a threshold driving force, the vortex polaron dissociates and the motion of vortex and the relaxation of magnetization are decoupled. When FL decreases, the vortex is retrapped by the background of remnant magnetization and they again form vortex polaron. This process repeats when FL(t) increases in the opposite direction. Remarkably, after dissociation, decoupled vortices move in the periodic potential induced by magnetization which remains for some periods of time due to retardation after the decoupling. At this stage vortices oscillate with high frequencies determined by the Lorentz force at the moment of dissociation. We derive also the creep rate of vortices and show that magnetic moments suppress creep rate.

  10. Transport and magnetic properties of disordered Li xV yO 2 ( x=0.8 and y=0.8)

    NASA Astrophysics Data System (ADS)

    Du, Fei; Li, Ang; Liu, Daliang; Zhan, Shiying; Hu, Fang; Wang, Chunzhong; Chen, Yan; Feng, Shouhua; Chen, Gang

    2009-07-01

    The magnetic and electron transport properties of rhombohedral Li xV yO 2 ( x=0.8 and y=0.8) are studied. The dc susceptibility of Li xV yO 2 can be well fitted to the modified Curie-Weiss law, which verified the paramagnetic ground state. The magnetic hysteresis and ac susceptibility also confirm this paramagnetism. The Li xV yO 2 exhibits semiconducting behavior, which is explained by thermal activated process at high temperature and variable-range hopping mechanism at low temperature. Anderson localization plays an important role in both the electron transport behavior and the magnetic behavior due to the site disorder between the Li + ion and V 4+ ion.

  11. Helical patterns of magnetization and magnetic charge density in iron whiskers

    NASA Astrophysics Data System (ADS)

    Templeton, Terry L.; Hanham, Scott D.; Arrott, Anthony S.

    2018-05-01

    Studies with the (1 1 1) axis along the long axis of an iron whisker, 40 years ago, showed two phenomena that have remained unexplained: 1) In low fields, there are six peaks in the ac susceptibility, separated by 0.2 mT; 2) Bitter patterns showed striped domain patterns. Multipole columns of magnetic charge density distort to form helical patterns of the magnetization, accounting for the peaks in the susceptibility from the propagation of edge solitons along the intersections of the six sides of a (1 1 1) whisker. The stripes follow the helices. We report micromagnetic simulations in cylinders with various geometries for the cross-sections from rectangular, to hexagonal, to circular, with wide ranges of sizes and lengths, and different anisotropies, including (0 0 1) whiskers and the hypothetical case of no anisotropy. The helical patterns have been there in previous studies, but overlooked. The surface swirls and body helices are connected, but have their own individual behaviors. The magnetization patterns are more easily understood when viewed observing the scalar divergences of the magnetization as isosurfaces of magnetic charge density. The plus and minus charge densities form columns that interact with unlike charges attracting, but not annihilating as they are paid for by a decrease in exchange energy. Just as they start to form the helix, the columns are multipoles. If one could stretch the columns, the self-energy of the charges in a column would be diminished while making the attractive interactions of the unlike charges larger. The columns elongate by becoming helical. The visualization of 3-D magnetic charge distributions aids in the understanding of magnetization in soft magnetic materials.

  12. Measuring Nematic Susceptibilities from the Elastoresistivity Tensor

    NASA Astrophysics Data System (ADS)

    Hristov, A. T.; Shapiro, M. C.; Hlobil, Patrick; Maharaj, Akash; Chu, Jiun-Haw; Fisher, Ian

    The elastoresistivity tensor mijkl relates changes in resistivity to the strain on a material. As a fourth-rank tensor, it contains considerably more information about the material than the simpler (second-rank) resistivity tensor; in particular, certain elastoresistivity coefficients can be related to thermodynamic susceptibilities and serve as a direct probe of symmetry breaking at a phase transition. The aim of this talk is twofold. First, we enumerate how symmetry both constrains the structure of the elastoresistivity tensor into an easy-to-understand form and connects tensor elements to thermodynamic susceptibilities. In the process, we generalize previous studies of elastoresistivity to include the effects of magnetic field. Second, we describe an approach to measuring quantities in the elastoresistivity tensor with a novel transverse measurement, which is immune to relative strain offsets. These techniques are then applied to BaFe2As2 in a proof of principle measurement. This work is supported by the Department of Energy, Office of Science, Basic Energy Sciences, Materials Sciences and Engineering Division, under Contract DE-AC02-76SF00515.

  13. Study of the Dependency on Magnetic Field and Bias Voltage of an AC-Biased TES Microcalorimeter.

    PubMed

    Gottardi, L; Adams, J; Bailey, C; Bandler, S; Bruijn, M; Chervenak, J; Eckart, M; Finkbeiner, F; den Hartog, R; Hoevers, H; Kelley, R; Kilbourne, C; de Korte, P; van der Kuur, J; Lindeman, M; Porter, F; Sadlier, J; Smith, S

    At SRON we are studying the performance of a Goddard Space Flight Center single pixel TES microcalorimeter operated in an AC bias configuration. For x-ray photons at 6 keV the pixel shows an x-ray energy resolution Δ E FWHM =3.7 eV, which is about a factor 2 worse than the energy resolution observed in an identical DC-biased pixel. In order to better understand the reasons for this discrepancy we characterised the detector as a function of temperature, bias working point and applied perpendicular magnetic field. A strong periodic dependency of the detector noise on the TES AC bias voltage is measured. We discuss the results in the framework of the recently observed weak-link behaviour of a TES microcalorimeter.

  14. Diagnostics of the Fermilab Tevatron using an AC dipole

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Miyamoto, Ryoichi

    2008-08-01

    The Fermilab Tevatron is currently the world's highest energy colliding beam facility. Its counter-rotating proton and antiproton beams collide at 2 TeV center-of-mass. Delivery of such intense beam fluxes to experiments has required improved knowledge of the Tevatron's beam optical lattice. An oscillating dipole magnet, referred to as an AC dipole, is one of such a tool to non-destructively assess the optical properties of the synchrotron. We discusses development of an AC dipole system for the Tevatron, a fast-oscillating (f ~ 20 kHz) dipole magnet which can be adiabatically turned on and off to establish sustained coherent oscillations of themore » beam particles without affecting the transverse emittance. By utilizing an existing magnet and a higher power audio amplifier, the cost of the Tevatron AC dipole system became relatively inexpensive. We discuss corrections which must be applied to the driven oscillation measurements to obtain the proper interpretation of beam optical parameters from AC dipole studies. After successful operations of the Tevatron AC dipole system, AC dipole systems, similar to that in the Tevatron, will be build for the CERN LHC. We present several measurements of linear optical parameters (beta function and phase advance) for the Tevatron, as well as studies of non-linear perturbations from sextupole and octupole elements.« less

  15. High susceptibility prevalence for F4+ and F18+Escherichia coli in Flemish pigs.

    PubMed

    Nguyen, Ut V; Coddens, Annelies; Melkebeek, Vesna; Devriendt, Bert; Goetstouwers, Tiphanie; Poucke, Mario Van; Peelman, Luc; Cox, Eric

    2017-04-01

    F4 and/or F18 enterotoxigenic Escherichia coli (F4 + /F18 + ETEC) are responsible for diarrhea while F18 + verotoxigenic E. coli (F18 + VTEC) cause edema disease in pigs. Both infections can result in severe economic losses, which are mainly the result of the medication, growth retardation and mortality. The susceptibility of piglets to these pathogens is determined by the presence of F4 and F18 receptors (F4R and F18R). Understanding the composition of the susceptibility phenotypes of pigs is useful for animal health and breeding management. This study aimed to determine the prevalence of the F4 ETEC susceptibility phenotypes and F18 + E. coli susceptibility among Flemish pig breeds by using the in vitro villous adhesion assay. In this study, seven F4 ETEC susceptibility phenotypes were found, namely A (F4 ab R + , ac R + , ad R + ; 59.16%), B (F4 ab R + , ac R + , ad R - ; 6.28%), C (F4 ab R + , ac R - , ad R + ; 2.62%), D (F4 ab R - , ac R - , ad R + ; 6.28%), E (F4 ab R - , ac R - , ad R - ; 24.08%), F (F4 ab R + , ac R - , ad R - ; 1.05%) and G (F4 ab R - , ac R + , ad R - ; 0.52%). F4ab and F4ac E. coli showed a stronger degree of adhesion to the intestinal villi (53.40% and 52.88% strong adhesion, respectively), compared to F4ad E. coli (43.46% strong adhesion). Furthermore, the correlation between F4ac and F4ab adhesion was higher (r=0.78) than between F4ac and F4ad adhesion (r=0.41) and between F4ab and F4ad adhesion (r=0.57). For F18 + E. coli susceptibility, seven out of 82 pigs were F18R negative (8.54%), but only two of these seven pigs (2.44%) were also negative for F4R. As such, the chance to identify a pig that is positive for a F4 ETEC variant or F18 + E. coli is 97.56%. Therefore, significant economic losses will arise due to F4 + and/or F18 + E. coli infections in the Flemish pig population due to the high susceptibility prevalence. Copyright © 2016 Elsevier B.V. All rights reserved.

  16. A MEMS sensor for AC electric current

    NASA Astrophysics Data System (ADS)

    Leland, Eli Sidney

    This manuscript describes the development of a new MEMS sensor for the measurement of AC electric current. The sensor is comprised of a MEMS piezoelectric cantilever with a microscale permanent magnet mounted to the cantilever's free end. When placed near a wire carrying AC current, the magnet couples to the oscillating magnetic field surrounding the wire, causing the cantilever to deflect, and piezoelectric coupling produces a sinusoidal voltage proportional to the current in the wire. The sensor is itself passive, requiring no power supply to operate. It also operates on proximity and need only be placed near a current carrier in order to function. The sensor does not need to encircle the current carrier and it therefore can measure current in two-wire zip-cords without necessitating the separation of the two conductors. Applications for tins sensor include measuring residential and commercial electricity use and monitoring electric power distribution networks. An analytical model describing the behavior of the current sensor was developed. This model was also adapted to describe the power output of an energy scavenger coupled to a wire carrying AC current. A mesoscale sensor exhibited a sensitivity of 75 mV/A when measuring AC electric current in a zip-cord. A mesoscale energy scavenger produced 345 muW when coupled to a zip-cord carrying 13 A. MEMS current sensors were fabricated from aluminum nitride piezoelectric cantilevers and composite permanent magnets. The cantilevers were fabricated using a four-mask process. Microscale permanent magnets were dispenser-printed using NdFeB magnetic powder with an epoxy binder. The MEMS AC current sensor was interfaced with amplification circuitry and packaged inside an almninum enclosure. The sensor was also integrated with a mesoscale energy scavenger and power conditioning circuitry to create a fully self-powered current sensor. Unamplified sensitivity of the sensor was 0.1-1.1 mV/A when measuring currents in single

  17. Magnetic helicity balance at Taylor relaxed states sustained by AC helicity injection

    NASA Astrophysics Data System (ADS)

    Hirota, Makoto; Morrison, Philip J.; Horton, Wendell; Hattori, Yuji

    2017-10-01

    Magnitudes of Taylor relaxed states that are sustained by AC magnetic helicity injection (also known as oscillating field current drive, OFCD) are investigated numerically in a cylindrical geometry. Compared with the amplitude of the oscillating magnetic field at the skin layer (which is normalized to 1), the strength of the axial guide field Bz 0 is shown to be an important parameter. The relaxation process seems to be active only when Bz 0 < 1 . Moreover, in the case of weak guide field Bz 0 < 0.2 , a helically-symmetric relaxed state is self-generated instead of the axisymmetric reversed-field pinch. As a theoretical model, the helicity balance is considered in a similar way to R. G. O'Neill et al., where the helicity injection rate is directly equated with the dissipation rate at the Taylor states. Then, the bifurcation to the helical Taylor state is predicted theoretically and the estimated magnitudes of the relaxed states reasonably agree with numerical results as far as Bz 0 < 1 . This work was supported by JSPS KAKENHI Grant Number 16K05627.

  18. Magnetic Susceptibility and Quantum Oscillations in a Buckled Honeycomb Lattice

    NASA Astrophysics Data System (ADS)

    Tabert, Calvin; Carbotte, Jules; Nicol, Elisabeth

    2015-03-01

    We calculate the magnetic response of a low-buckled honeycomb lattice with intrinsic spin-orbit coupling which is described by the Kane-Mele Hamiltonian (a model which would describe the low-energy physics of a material like silicene). Included in the Hamiltonian, is a sublattice potential difference term which may be induced by a perpendicular electric field; this field can tune the system from a topological insulator (TI), through a valley-spin polarized metal, to a trivial band insulator (BI). In an external magnetic field, a distinct signature of the phase transition is seen in the derivative of the magnetization with respect to chemical potential; this gives the quantization of the Hall plateaus through the Streda relation. The results are compared with the zero-frequency conductivity obtained from the Kubo formula. The magnetic susceptibility also displays signatures of the different topological phases. We also explore the de-Haas van-Alphen effect. At the transition point between the TI and BI, magnetic oscillations exist for any value of chemical potential. Away from the critical point, the chemical potential must be larger than the minimum gap. For large chemical potential (or small but finite sublattice potential difference), there is a strong beating pattern.

  19. Stratigraphic correlations in mid- to late-Proterozoic carbonates of the Democratic Republic of Congo using magnetic susceptibility

    NASA Astrophysics Data System (ADS)

    Delpomdor, Franck R. A.; Devleeschouwer, Xavier; Spassov, Simo; Préat, Alain R.

    2017-04-01

    In this paper, we have tested the application of magnetic susceptibility measurements in Cu-Ag-Zn-Pb-(Fe)-mineralized carbonates of the BIe subgroup (Democratic Republic of Congo) as an efficient tool for regional and global high-resolution stratigraphic correlations in the Neoproterozoic marine carbonates. To achieve this goal, we integrate the low-field magnetic susceptibility (XLF) data with facies analyses, geochemistry and isotope stratigraphy. The microfacies analyses of two cores, Tshinyama#S70 and Kafuku#15, drilled in the early Neoproterozoic carbonates of the Mbuji-Mayi Supergroup reveal a deep carbonate ramp setting associated with a microbial/stromatolitic mid-ramp environment. High-resolution stratigraphic correlations using magnetic susceptibility and C-isotope curves established for both cores, 190 km apart, suggest a sedimentary hiatus at the base of the Tshinyama#S70 succession. C-O and Sr isotopes and Sr/Ca and Fe abundances show that a diagenetic meteoric overprint affected the series of the Tshinyama#S70 core and a thermal effect related to mineralizing fluids affected the Kafuku#15 core carbonates.

  20. Low-field anomalous magnetic phase in the kagome-lattice shandite C o3S n2S2

    NASA Astrophysics Data System (ADS)

    Kassem, Mohamed A.; Tabata, Yoshikazu; Waki, Takeshi; Nakamura, Hiroyuki

    2017-07-01

    The magnetization process of single crystals of the metallic kagome ferromagnet C o3S n2S2 was carefully measured via magnetization and ac susceptibility. Field-dependent anomalous transitions observed in low fields indicate the presence of an unconventional magnetic phase just below the Curie temperature, TC. The magnetic phase diagrams in low magnetic fields along different crystallographic directions were determined for the first time. The magnetic relaxation measurements at various frequencies covering five orders of magnitude from 0.01 to 1000 Hz indicate markedly slow spin dynamics only in the anomalous phase with characteristic relaxation times longer than 10 s.

  1. Single phase bi-directional AC-DC converter with reduced passive components size and common mode electro-magnetic interference

    DOEpatents

    Mi, Chris; Li, Siqi

    2017-01-31

    A bidirectional AC-DC converter is presented with reduced passive component size and common mode electro-magnetic interference. The converter includes an improved input stage formed by two coupled differential inductors, two coupled common and differential inductors, one differential capacitor and two common mode capacitors. With this input structure, the volume, weight and cost of the input stage can be reduced greatly. Additionally, the input current ripple and common mode electro-magnetic interference can be greatly attenuated, so lower switching frequency can be adopted to achieve higher efficiency.

  2. Implications of Late Pliocene-Pleistocene Humidity Fluctuations in the Qaidam Paleolake (NE Tibetan Plateau) Deduced from Magnetic Susceptibility Measurements

    NASA Astrophysics Data System (ADS)

    Herb, C.; Appel, E.; Koutsodendris, A.; Zhang, W.; Pross, J.; Fang, X.

    2014-12-01

    The Qaidam Basin (NE Tibetan Plateau) contains a near-continuous, up to 12 km thick sequence of Cenozoic strata that offers a unique opportunity for studying long-term climate change. We investigate the 940-m-long drill core SG-1 from the western Qaidam Basin, which is characterized by a long-term transition from a semi-deep freshwater lake to nearly complete exsiccation of the water body, detected by several studies including geochemical and lithological observations. Based on magnetostratigraphy and optically stimulated luminescence dating, and refined by orbital tuning, the SG-1 core spans the interval from 2.69 to 0.1 Ma. Moisture availability in the western Qaidam Basin deduced from the pollen ratio Artemisia/Chenopodiaceae (A/C), suggests desert to steppe vegetation along core SG-1 as a long-term feature. Magnetic susceptibility (χ) is well suited for the high-resolution investigation of paleohumidity. The meaning of χ as a paleohydrology proxy is shown by comparing χ to other magnetic proxies for checking its relation to magnetic grain sizes and magnetic mineralogy as well as to pollen results. χ variations are analyzed to obtain regional information on the factors leading to the drying process of the Qaidam paleolake as well as potential driving factors for humidity fluctuations (e.g., insolation). An important topic that needs further investigation is the influence of monsoon in the Qaidam Basin. While the southern part of the Tibetan Plateau is directly affected by monsoon precipitation through the topographic barrier, its influence in the past is questionable in the hyper-arid Qaidam Basin. We check a potential coupling to the monsoon system in the western Qaidam Basin by comparing our χ record to reconstructions of the Asian monsoon system from other archives as well as searching evidence from orbital cyclicities found in the χ time series.

  3. Determination of Magnetic Parameters of Maghemite (γ-Fe2O3) Core-Shell Nanoparticles from Nonlinear Magnetic Susceptibility Measurements

    NASA Astrophysics Data System (ADS)

    Syvorotka, Ihor I.; Pavlyk, Lyubomyr P.; Ubizskii, Sergii B.; Buryy, Oleg A.; Savytskyy, Hrygoriy V.; Mitina, Nataliya Y.; Zaichenko, Oleksandr S.

    2017-04-01

    Method of determining of magnetic moment and size from measurements of dependence of the nonlinear magnetic susceptibility upon magnetic field is proposed, substantiated and tested for superparamagnetic nanoparticles (SPNP) of the "magnetic core-polymer shell" type which are widely used in biomedical technologies. The model of the induction response of the SPNP ensemble on the combined action of the magnetic harmonic excitation field and permanent bias field is built, and the analysis of possible ways to determine the magnetic moment and size of the nanoparticles as well as the parameters of the distribution of these variables is performed. Experimental verification of the proposed method was implemented on samples of SPNP with maghemite core in dry form as well as in colloidal systems. The results have been compared with the data obtained by other methods. Advantages of the proposed method are analyzed and discussed, particularly in terms of its suitability for routine express testing of SPNP for biomedical technology.

  4. Quantitative Susceptibility Mapping: Contrast Mechanisms and Clinical Applications

    PubMed Central

    Liu, Chunlei; Wei, Hongjiang; Gong, Nan-Jie; Cronin, Matthew; Dibb, Russel; Decker, Kyle

    2016-01-01

    Quantitative susceptibility mapping (QSM) is a recently developed MRI technique for quantifying the spatial distribution of magnetic susceptibility within biological tissues. It first uses the frequency shift in the MRI signal to map the magnetic field profile within the tissue. The resulting field map is then used to determine the spatial distribution of the underlying magnetic susceptibility by solving an inverse problem. The solution is achieved by deconvolving the field map with a dipole field, under the assumption that the magnetic field is a result of the superposition of the dipole fields generated by all voxels and that each voxel has its unique magnetic susceptibility. QSM provides improved contrast to noise ratio for certain tissues and structures compared to its magnitude counterpart. More importantly, magnetic susceptibility is a direct reflection of the molecular composition and cellular architecture of the tissue. Consequently, by quantifying magnetic susceptibility, QSM is becoming a quantitative imaging approach for characterizing normal and pathological tissue properties. This article reviews the mechanism generating susceptibility contrast within tissues and some associated applications. PMID:26844301

  5. Spin-glass polyamorphism induced by a magnetic field in LaMnO3 single crystal

    NASA Astrophysics Data System (ADS)

    Eremenko, V. V.; Sirenko, V. A.; Baran, A.; Čižmár, E.; Feher, A.

    2018-05-01

    We present experimental evidence of field-driven transition in spin-glass state, similar to pressure-induced transition between amorphous phases in structural and metallic glasses, attributed to the polyamorphism phenomena. Cusp in temperature dependences of ac magnetic susceptibility of weakly disordered LaMnO3 single crystal is registered below the temperature of magnetic ordering. Frequency dependence of the cusp temperature proves its spin-glass origin. The transition induced by a magnetic field in spin-glass state, is manifested by peculiarity in dependence of cusp temperature on applied magnetic field. Field dependent maximum of heat capacity is observed in the same magnetic field and temperature range.

  6. Fragile magnetic order in the honeycomb lattice Iridate Na2IrO3 revealed by magnetic impurity doping

    NASA Astrophysics Data System (ADS)

    Mehlawat, Kavita; Sharma, G.; Singh, Yogesh

    2015-10-01

    We report the structure, magnetic, and thermal property measurements on single-crystalline and polycrystalline samples of the Ru-substituted honeycomb lattice iridate Na2Ir1 -xRuxO3 (x =0 ,0.05 ,0.1 ,0.15 ,0.2 ,0.3 ,0.5 ) . The evolution of magnetism in Na2Ir1 -xRuxO3 has been studied using dc and ac magnetic susceptibilities and heat-capacity measurements. The parent compound Na2IrO3 is a spin-orbit-driven Mott insulator with magnetic order of reduced moments below TN=15 K . In the Ru-substituted samples the antiferromagnetic long-range state is replaced by a spin-glass-like state even for the smallest substitution suggesting that the magnetic order in Na2IrO3 is extremely fragile. We argue that these behaviors indicate the importance of nearest-neighbor magnetic exchange in the parent Na2IrO3 . Additionally, all samples show insulating electrical transport.

  7. Investigating the anisotropy of magnetic susceptibility and other rock magnetic properties of the Beaver River Diabase in northeastern Minnesota

    NASA Astrophysics Data System (ADS)

    Hariri, S. H.; Brownlee, S. J.; Feinberg, J. M.; Jackson, M. J.; Miller, J. D.

    2013-12-01

    The Beaver River Diabase (BRD) is a series of mafic dikes and sills within the Beaver Bay Complex (BBC) of northern Minnesota, which formed during the development of the ~1.1 Ga Midcontinent Rift (MCR). The BRD is one of the youngest and most extensive intrusive phases of the BBC. The BRD dikes and sills were emplaced into the medial levels of the 6-10 kilometer-thick North Shore Volcanic Group and occur over an arcuate area extending 120 by 20 kilometers. The BRD is composed of fine- to medium-grained ophitic olivine gabbro and does not display obvious foliation or lineation features and rarely displays modal layering. Without obvious magmatic internal structures, it is difficult to determine emplacement properties such as flow direction using standard geologic mapping or petrographic techniques. For this reason, we measured the anisotropy of magnetic susceptibility (AMS), in conjunction with other rock magnetic properties, to better understand the BRD's emplacement and deformation history in the context of the MCR. AMS measures the directional dependence of low-field magnetic susceptibility, and is used to infer a shape-preferred orientation of magnetic minerals within a rock, which can be related to specific emplacement mechanisms (e.g. directional flow or settling). Preliminary analysis of AMS at 20 sites within the southern half of the BRD (with 4-7 samples per site) shows maximum susceptibility values between 4.48 x 10-6 and 2.22 x 10-4 m3/kg (1165 and 65400 μSI). Most specimens display nearly isotropic AMS ellipsoids (Pj < 1.15) with minor degrees of prolateness and oblateness. However, about 20% of specimens have higher anisotropies (Pj between 1.15 and 1.67) and higher degrees of oblateness and prolateness. Variations in AMS properties may reflect differences in concentration and composition, as well as emplacement mechanisms. Measurements of susceptibility as a function of temperature yield Curie points between 470 and 570 °C, indicating a presence of

  8. Asteroid impact vs. Deccan eruptions: The origin of low magnetic susceptibility beds below the Cretaceous-Paleogene boundary revisited

    NASA Astrophysics Data System (ADS)

    Abrajevitch, Alexandra; Font, Eric; Florindo, Fabio; Roberts, Andrew P.

    2015-11-01

    The respective roles of an asteroid impact and Deccan Traps eruptions in biotic changes at the Cretaceous-Paleogene (K-Pg) boundary are still debated. In many shallow marine sediments from around the world, the K-Pg boundary is marked by a distinct clay layer that is often underlain by a several decimeter-thick low susceptibility zone. A previous study of the Gubbio section, Italy (Lowrie et al., 1990), attributed low magnetization intensity in this interval to post-depositional dissolution of ferrimagnetic minerals. Dissolution was thought to be a consequence of downward infiltration of reducing waters that resulted from rapid accumulation of organic matter produced by mass extinctions after the K-Pg event. We compare the magnetic properties of sediments from the Gubbio section with those of the Bidart section in southern France. The two sections are similar in their carbonate lithology and the presence of a boundary clay and low susceptibility zone. When compared to background Cretaceous sediments, the low susceptibility zone in both sections is marked by an absence of biogenic magnetite, a decrease in total ferrimagnetic mineral content, and a preferential loss of magnetite with respect to hematite - features that are consistent with reductive dissolution. However, unlike the Gubbio section, where the low susceptibility zone starts immediately below the boundary clay, the low susceptibility zone and the clay layer at Bidart are separated by a ∼4-cm carbonate interval that contains abundant biogenic magnetite. Such separation casts doubt on a causal link between the impact and sediment bleaching. More likely, the low susceptibility layer marks a different environmental event that preceded the impact. An episode of increased atmospheric and oceanic acidity associated with Deccan Traps volcanism that occurred well before the K-Pg impact is argued here to account for the distinct magnetic properties of the low susceptibility intervals.

  9. Polarized Neutron Diffraction as a Tool for Mapping Molecular Magnetic Anisotropy: Local Susceptibility Tensors in Co(II) Complexes.

    PubMed

    Ridier, Karl; Gillon, Béatrice; Gukasov, Arsen; Chaboussant, Grégory; Cousson, Alain; Luneau, Dominique; Borta, Ana; Jacquot, Jean-François; Checa, Ruben; Chiba, Yukako; Sakiyama, Hiroshi; Mikuriya, Masahiro

    2016-01-11

    Polarized neutron diffraction (PND) experiments were carried out at low temperature to characterize with high precision the local magnetic anisotropy in two paramagnetic high-spin cobalt(II) complexes, namely [Co(II) (dmf)6 ](BPh4 )2 (1) and [Co(II) 2 (sym-hmp)2 ](BPh4 )2 (2), in which dmf=N,N-dimethylformamide; sym-hmp=2,6-bis[(2-hydroxyethyl)methylaminomethyl]-4-methylphenolate, and BPh4 (-) =tetraphenylborate. This allowed a unique and direct determination of the local magnetic susceptibility tensor on each individual Co(II) site. In compound 1, this approach reveals the correlation between the single-ion easy magnetization direction and a trigonal elongation axis of the Co(II) coordination octahedron. In exchange-coupled dimer 2, the determination of the individual Co(II) magnetic susceptibility tensors provides a clear outlook of how the local magnetic properties on both Co(II) sites deviate from the single-ion behavior because of antiferromagnetic exchange coupling. © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  10. The ground state magnetic moment and susceptibility of a two electron Gaussian quantum dot

    NASA Astrophysics Data System (ADS)

    Boda, Aalu; Chatterjee, Ashok

    2018-04-01

    The problem of two interacting electrons moving in a two-dimensional semiconductor quantum dot with Gaussian confinement under the influence of an external magnetic field is studied by using a method of numerical diagonalization of the Hamiltonian matrix with in the effective-mass approximation. The energy spectrum is calculated as a function of the magnetic field. We find the ground state magnetic moment and the magnetic susceptibility show zero temperature diamagnetic peaks due to exchange induced singlet-triplet oscillations. The position and the number of these peaks depend on the size of the quantum dot and also strength of the electro-electron interaction. The theory is applied to a GaAs quantum dot.

  11. Fabric analysis of quartzites with negative magnetic susceptibility - Does AMS provide information of SPO or CPO of quartz?

    NASA Astrophysics Data System (ADS)

    Renjith, A. R.; Mamtani, Manish A.; Urai, Janos L.

    2016-01-01

    We ask the question whether petrofabric data from anisotropy of magnetic susceptibility (AMS) analysis of deformed quartzites gives information about shape preferred orientation (SPO) or crystallographic preferred orientation (CPO) of quartz. Since quartz is diamagnetic and has a negative magnetic susceptibility, 11 samples of nearly pure quartzites with a negative magnetic susceptibility were chosen for this study. After performing AMS analysis, electron backscatter diffraction (EBSD) analysis was done in thin sections prepared parallel to the K1K3 plane of the AMS ellipsoid. Results show that in all the samples quartz SPO is sub-parallel to the orientation of the magnetic foliation. However, in most samples no clear correspondance is observed between quartz CPO and K1 (magnetic lineation) direction. This is contrary to the parallelism observed between K1 direction and orientation of quartz c-axis in the case of undeformed single quartz crystal. Pole figures of quartz indicate that quartz c-axis tends to be parallel to K1 direction only in the case where intracrystalline deformation of quartz is accommodated by prism slip. It is therefore established that AMS investigation of quartz from deformed rocks gives information of SPO. Thus, it is concluded that petrofabric information of quartzite obtained from AMS is a manifestation of its shape anisotropy and not crystallographic preferred orientation.

  12. Nutrition affects insect susceptibility to Bt toxins

    NASA Astrophysics Data System (ADS)

    Deans, Carrie A.; Behmer, Spencer T.; Tessnow, Ashley E.; Tamez-Guerra, Patricia; Pusztai-Carey, Marianne; Sword, Gregory A.

    2017-01-01

    Pesticide resistance represents a major challenge to global food production. The spread of resistance alleles is the primary explanation for observations of reduced pesticide efficacy over time, but the potential for gene-by-environment interactions (plasticity) to mediate susceptibility has largely been overlooked. Here we show that nutrition is an environmental factor that affects susceptibility to Bt toxins. Protein and carbohydrates are two key macronutrients for insect herbivores, and the polyphagous pest Helicoverpa zea self-selects and performs best on diets that are protein-biased relative to carbohydrates. Despite this, most Bt bioassays employ carbohydrate-biased rearing diets. This study explored the effect of diet protein-carbohydrate content on H. zea susceptibility to Cry1Ac, a common Bt endotoxin. We detected a 100-fold increase in LC50 for larvae on optimal versus carbohydrate-biased diets, and significant diet-mediated variation in survival and performance when challenged with Cry1Ac. Our results suggest that Bt resistance bioassays that use ecologically- and physiologically-mismatched diets over-estimate susceptibility and under-estimate resistance.

  13. Synthesis of Micelles Guided Magnetite (Fe3O4) Hollow Spheres and their application for AC Magnetic Field Responsive Drug Release

    PubMed Central

    Mandal Goswami, Madhuri

    2016-01-01

    This paper reports on synthesis of hollow spheres of magnetite, guided by micelles and their application in drug release by the stimulus responsive technique. Here oleyelamine micelles are used as the core substance for the formation of magnetite nano hollow spheres (NHS). Diameter and shell thickness of NHS have been changed by changing concentration of the micelles. Mechanism of NHS formation has been established by investigating the aliquot collected at different time during the synthesis of NHS. It has been observed that oleyelamine as micelles play an important role to generate hollow-sphere particles of different diameter and thickness just by varying its amount. Structural analysis was done by XRD measurement and morphological measurements, SEM and TEM were performed to confirm the shape and size of the NHS. FTIR measurement support the formation of magnetite phase too. Frequency dependent AC magnetic measurements and AC magnetic field stimulated drug release event by these particles provide a direction of the promising application of these NHS for better cancer treatment in near future. Being hollow & porous in structure and magnetic in nature, such materials will also be useful in other applications such as in removal of toxic materials, magnetic separation etc. PMID:27796329

  14. Magnetic susceptibility as an indicator to paleo-environmental pollution in an urban lagoon near Istanbul city

    NASA Astrophysics Data System (ADS)

    Alpar, Bedri; Unlu, Selma; Altinok, Yildiz; Ongen, Sinan

    2014-05-01

    For assessing anthropogenic pollution, magnetic susceptibility profiles and accompanying data were measured along three short cores recovered at the southern part of an urban lagoon; Kucukcekmece, Istanbul, Turkey. This marine inlet, connected to the Sea of Marmara by a very narrow channel, was used as a drinking water reservoir 40-50 years ago before it was contaminated by municipal, agricultural and industrial activities, mainly carried by three streams feeding the lagoon. The magnetic signals decrease gradually from the lake bottom towards the core base showing some characteristic anomalies. These signatures were tested as an environmental magnetic parameter against the lithological diversity (silici-clastic, total organic matter and carbonate), metal enrichments with larger variations (Pb, Mn, Zn, Ni, Co, Cr, U and Al) and probable hydrocarbon contamination. Mineral assemblage was determined by a computer driven X-ray diffractometer. The heavy metal concentrations and total petroleum hydrocarbons (TPH) were measured by ICP-MS and UVF spectrometry, respectively. Magnetic susceptibility shows slightly higher values in interlayers containing higher silici-clastic material and organic content which may suggest first-order changes in the relative supplies of terrigenous and biogenic materials. On the basis of cluster analyses, enhanced magnetic signals could be correlated with the elevated concentrations of Co, Zn, U, Pb and TPH along the cores. The Pb concentrations at the upper parts of the cores were higher than the "Severe Effect Level" and could pose a potential risk for living organisms. Greater amounts of organic carbon tend to accumulate in muddy sediments. In fact, there are a few studies reporting some relationship between enhanced magnetic signals and organic contamination mainly due to petroleum aromatic hydrocarbons. In conclusion, the magnetic susceptibility changes in sedimentary depositional environments could be used as a rapid and cost

  15. High magnetic susceptibility granodiorite as a source of surface magnetic anomalies in the King George Island, Antarctica

    NASA Astrophysics Data System (ADS)

    Kon, S.; Nakamura, N.; Funaki, M.; Sakanaka, S.

    2012-12-01

    station) in the western side of King George Island. The plutonic rocks of diorite and granodiorite show high values of bulk magnetic susceptibility of c.a. 0.01-0.4 SI, appearing to be the source of positive magnetic anomaly. We also revealed the preferred petrofabric lineation directions at the sites using anisotropy of magnetic susceptibility (AMS). The AMS showed the plutonic rocks represent the vertical intrusion from the deep seated magma. Our optical microscope observation verified the maximum AMS orientation is parallel to the preferred alignment of framework-forming plagioclase, suggesting the alignment of euhedral magnetite grains along the long-axes of plagioclases. Our ship-borne and foot-borne surveys of geomagnetic filed anomaly agree well with the distribution of the plutonic rocks, revealing the possible origin of surface magnetic anomaly. These suggests that the plutons in this area may be included ACG, and this magnetic surveys is proposed to infer the availability to find out the presence of granitoid.

  16. Susceptibility-Weighted Imaging and Quantitative Susceptibility Mapping in the Brain

    PubMed Central

    Liu, Chunlei; Li, Wei; Tong, Karen A.; Yeom, Kristen W.; Kuzminski, Samuel

    2015-01-01

    Susceptibility-weighted imaging (SWI) is a magnetic resonance imaging (MRI) technique that enhances image contrast by using the susceptibility differences between tissues. It is created by combining both magnitude and phase in the gradient echo data. SWI is sensitive to both paramagnetic and diamagnetic substances which generate different phase shift in MRI data. SWI images can be displayed as a minimum intensity projection that provides high resolution delineation of the cerebral venous architecture, a feature that is not available in other MRI techniques. As such, SWI has been widely applied to diagnose various venous abnormalities. SWI is especially sensitive to deoxygenated blood and intracranial mineral deposition and, for that reason, has been applied to image various pathologies including intracranial hemorrhage, traumatic brain injury, stroke, neoplasm, and multiple sclerosis. SWI, however, does not provide quantitative measures of magnetic susceptibility. This limitation is currently being addressed with the development of quantitative susceptibility mapping (QSM) and susceptibility tensor imaging (STI). While QSM treats susceptibility as isotropic, STI treats susceptibility as generally anisotropic characterized by a tensor quantity. This article reviews the basic principles of SWI, its clinical and research applications, the mechanisms governing brain susceptibility properties, and its practical implementation, with a focus on brain imaging. PMID:25270052

  17. A family of rare-earth-based single chain magnets: playing with anisotropy.

    PubMed

    Bernot, Kevin; Bogani, Lapo; Caneschi, Andrea; Gatteschi, Dante; Sessoli, Roberta

    2006-06-21

    The first family of rare-earth-based single chain magnets is presented. Compounds of general formula [M(hfac)3(NITPhOPh)], where M = Eu, Gd, Tb, Dy, Ho, Er, or Yb, and PhOPh is the nitronyl-nitroxide radical (2,4'-benzoxo-4,4,5,5-tetramethylimidazoline-1-oxyl-3-oxide), have been structurally characterized and found to be isostructural. The characterization of both static and dynamic magnetic properties of the whole family is reported. Dy, Tb, and Ho compounds display slow relaxation of the magnetization, and ac susceptibility shows a thermally activated regime with energy barriers of 69, 45, and 34 K for Dy, Tb, and Ho compounds, respectively, while only a frequency-dependent susceptibility is observed for Er below 2.0 K. In Gd and Yb derivatives, antiferromagnetic interactions dominate. The pre-exponential factors differ by about 4 orders of magnitude. Finite size effects, due to naturally occurring defects, affect the static and dynamic properties of the compounds differently.

  18. Magnetic Viruses: Utilizing Self-Assembly for Biomedical Applications

    NASA Astrophysics Data System (ADS)

    Hoffmann, Axel

    2006-03-01

    Magnetic nanoparticles coated with biochemical surfactants have emerged recently as an important component for enabling many biological and medical applications. We implemented a biotemplating approach to create such magnetic nanoparticles by utilizing native protein capsid shells derived in high yield from the T7 bacteriophage virus. The magnetic nanoparticles are grown via bio-mineralization reactions inside of hollowed-out capsids that retain their original chemical recognition properties. The resultant ``magnetic viruses'' are uniform in geometry, physical properties, and biochemical functionality. This makes these viruses ideally suited for many biomedical applications among which we investigated specifically a novel sensing scheme for target recognition based on Brownian relaxation. For this scheme we use the ac-susceptibility of the functionalized magnetic nanoparticles suspended in liquid. Upon binding the target of interest to the particles, their Brownian relaxation time is modified, which is readily detected by a change of the frequency dependence of the magnetic susceptibility. This scheme has several advantages; (i) it requires only one binding event for sensing; (ii) there is a useful signal both in the absence and presence of the target; (iii) the signal contains information about the size of the target besides the biochemical affinity; and (iv) since the binding modifies the magnetic susceptibility of the magnetic particles there is no need for removing unbound labels. C. Liu, S.-H. Chung, Q. Jin, A. Sutton, F. Yan, B. K. Kay, S. D. Bader, L. Makowski, and L. Chen, J. Magn. Magn. Mater, in press. S.H. Chung, A. Hoffmann, S. D. Bader, C. Liu, B. Kay, L. Makowski, and L. Chen, Appl. Phys. Lett. 85, 2971 (2004) ; S. H. Chung, A. Hoffmann, K. Guslienko, S. D. Bader, C. Liu, B. Kay, L. Makowski, and L. Chen, J. Appl. Phys. 97, 10R101 (2005).

  19. Evidence for single-chain magnet behavior in a Mn(III)-Ni(II) chain designed with high spin magnetic units: a route to high temperature metastable magnets.

    PubMed

    Clérac, Rodolphe; Miyasaka, Hitoshi; Yamashita, Masahiro; Coulon, Claude

    2002-10-30

    We herein present the synthesis, crystal structure, and magnetic properties of a new heterometallic chain of MnIII and NiII ions, [Mn2(saltmen)2Ni(pao)2(py)2](ClO4)2 (1) (saltmen2- = N,N'-(1,1,2,2-tetramethylethylene) bis(salicylideneiminate) and pao- = pyridine-2-aldoximate). The crystal structure of 1 was investigated by X-ray crystallographic analysis: compound 1 crystallized in monoclinic, space group C2/c (No. 15) with a = 21.140(3) A, b = 15.975(1) A, c = 18.6212(4) A, beta = 98.0586(4) degrees , V = 6226.5(7) A3, and Z = 4. This compound consists of two fragments, the out-of-plane dimer [Mn2(saltmen)2]2+ as a coordination acceptor building block and the neutral mononuclear unit [Ni(pao)2(py)2] as a coordination donor building block, forming an alternating chain having the repeating unit [-Mn-(O)2-Mn-ON-Ni-NO-]n. In the crystal structure, each chain is well separated with a minimum intermetallic distance between Mn and Ni ions of 10.39 A and with the absence of interchain pi overlaps between organic ligands. These features ensure a good magnetic isolation of the chains. The dc and ac magnetic measurements were performed on both the polycrystalline sample and the aligned single crystals of 1. Above 30 K, the magnetic susceptibility of this one-dimensional compound was successfully described in a mean field approximation as an assembly of trimers (Mn...Ni...Mn) with a NiII...MnIII antiferromagnetic interaction (J = -21 K) connected through a ferromagnetic MnIII...MnIII interaction (J'). However, the mean field theory fails to describe the magnetic behavior below 30 K emphasizing the one-dimensional magnetic character of the title compound. Between 5 and 15 K, the susceptibility in the chain direction was fitted to a one-dimensional Ising model leading to the same value of J'. Hysteresis loops are observed below 3.5 K, indicating a magnet-type behavior. In the same range of temperature, combined ac and dc measurements show a slow relaxation of the magnetization

  20. RECONSTRUCTING PALEO-SMT POSITIONS ON THE CASCADIA MARGIN USING MAGNETIC SUSCEPTIBILITY

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Johnson, Joel; Phillips, Stephen

    2014-09-30

    Magnetic susceptibility (κ) is a mixed signal in marine sediments, representing primary depositional and secondary diagenetic processes. Production of hydrogen sulfide via anaerobic oxidation of methane (AOM) at the sulfate-methane transition (SMT) and organoclastic sulfate reduction above the SMT can result in the dissolution of iron oxides, altering κ in sediments in methane gas and gas hydrate bearing regions. We investigated records of κ on the Cascadia margin (ODP Sites 1249 and 1252; IODP Site 1325) using a Zr/Rb heavy mineral proxy from XRF core scanning to identify intervals of primary detrital magnetic susceptibility and intervals and predict intervals affectedmore » by magnetite dissolutions. We also measured total sulfur content, grain size distributions, total organic carbon (TOC) content, and magnetic mineral assemblage. The upper 100 m of Site 1252 contains a short interval of κ driven by primary magnetite, with multiple intervals (> 90 m total) of decreased κ correlated with elevated sulfur content, consistent with dissolution of magnetite and re-precipitation of pyrite. In the upper 90 m of Site 1249, κ is almost entirely altered by diagenetic processes, with much of the low κ explained by a high degree of pyritization, and some intervals affected by the precipitation of magnetic iron sulfides. At Site 1325, κ between 0-20 and 51-73 mbsf represents primary mineralogy, and in the interval 24-51 mbsf, κ may be reduced due to pyritization. This integrated approach allows for a prediction of primary κ and the amount of κ loss at each site when compared to actual κ measurements. In the case of magnetite dissolution and full pyritization, these drawdowns in κ are supported by sulfur measurements, and the exposure times of magnetite to hydrogen sulfide can be modeled. The presence of methane and methane hydrates at these sites, as well as large variations in TOC content, suggest that the past migration rates of the SMT and variation in

  1. A case of time-dependent anisotropy of low-field susceptibility (AMS)

    NASA Astrophysics Data System (ADS)

    Borradaile, Graham J.; Geneviciene, Ieva

    2007-07-01

    A suite of non-tectonized, Meso-Proterozoic siliceous crystal tuffs and volcanic breccia with a visible stratification has a modal bulk susceptibility ( k) ˜ 160 μSI [mean; S.D. = 141 μSI; 44 μSI]. Normally, such susceptibilities suffice to make reliable measurements of anisotropy of low field susceptibility (AMS) using AC induction-coil instruments. However, for this suite, time-dependent susceptibility - variations during measurement are large in comparison to susceptibility - differences along different axes through a specimen. Thus, in many specimens, AMS axes determined by routine induction coil measurement in a (Sapphire Instruments SI2B; 19,200 Hz, 60 A/m) measurement procedures are not reproducible. The apparent variation of specimen susceptibility during a single, four minute AMS measurement can > 2 μSI whereas in the same interval the noise-level of our instrument is < 0.2 μSI. Thus, the time-dependence of the specimen-susceptibility is an intrinsic phenomenon due to the characteristics (grain size, domain structure) of the magnetite which dominates susceptibility during measurement and handling. Two procedures improved the reproducibility and stability of AMS axial orientations in some specimens. First, for some specimens, one or two cycles of LTD or AF demagnetization (≤ 15 mT) stabilized AMS axes. (Previous workers have observed that LTD and AF demagnetization may change slightly the AMS of polydomainal magnetite). Of course, exposure to alternating fields is preferably avoided before any AMS study. Second, for some specimens AMS measurement were improved by shielding the induction coil instrument in a large magnetically shielded space (ambient field < 5 nT). Further improvements were achieved by permitting the specimens to relax in side a magnetic shield for 24 h before measurement. The occurrence of time-dependent bulk susceptibility, especially noticeable in its AMS axial orientations is certainly a rare phenomenon and the procedures we used

  2. Magnetic susceptibility of the South African Agouron scientific drillcores quantifies iron and sulfur alteration relevant to geochemical oxygenation proxies

    NASA Astrophysics Data System (ADS)

    Raub, T. D.; Nayak, P. M.; Tikoo, S. M.; Johnson, J. E.; Peek, S.; Fischer, W. W.; Kirschvink, J. L.

    2010-12-01

    Various geochemical characteristics of sedimentary iron- and sulfur-bearing minerals motivate early- to late-oxygenation hypotheses from South African and Australian scientific drillcores. Most intervals of these drillcores appear to be remagnetized (in some cases multiple times); and ~2.0 Ga magnetic sulfide crystallization is particularly pervasive in carbonaceous siltstones of the ca. 2.7-2.2 Ga Griqualand margin of Kaapvaal craton. Robust interpretation of trace element abundances suggesting “whiffs” to “pervasive” levels of late Archean oxygen depends upon systematics of presumed depositional iron speciation; so multiple iron- and sulfur-mineral-altering events affecting existing drillcore records call straightforward interpretations into question. We report ca. 10,000 magnetic susceptibility measurements and associated detailed rock-magnetic results from all lithologies of Archean basinal and slope facies in drillcores GKP and GKF and relatively younger and shallower facies in Paleoproterozoic drillcores GEC and GTF. Specific carbonaceous siltstone and carbonate intervals are less-altered as revealed by coherent and relatively low magnetic susceptibilities: geochemical and biomarker interpretations based upon data from these intervals should be preferred to those from others. Magnetic susceptibility tracks subtle facies variation in drillcore GTF diamictite and suggests highly-structured Paleoproterozoic glacioeustatic sequence architecture consistent with assignment of Makganyene glaciation and its associated geochemical signature to a ca. 2.2 Ga “Snowball Earth” ice age.

  3. Design and development of novel MRI compatible zirconium- ruthenium alloys with ultralow magnetic susceptibility.

    PubMed

    Li, H F; Zhou, F Y; Li, L; Zheng, Y F

    2016-04-19

    In the present study, novel MRI compatible zirconium-ruthenium alloys with ultralow magnetic susceptibility were developed for biomedical and therapeutic devices under MRI diagnostics environments. The results demonstrated that alloying with ruthenium into pure zirconium would significantly increase the strength and hardness properties. The corrosion resistance of zirconium-ruthenium alloys increased significantly. High cell viability could be found and healthy cell morphology observed when culturing MG 63 osteoblast-like cells and L-929 fibroblast cells with zirconium-ruthenium alloys, whereas the hemolysis rates of zirconium-ruthenium alloys are <1%, much lower than 5%, the safe value for biomaterials according to ISO 10993-4 standard. Compared with conventional biomedical 316L stainless steel, Co-Cr alloys and Ti-based alloys, the magnetic susceptibilities of the zirconium-ruthenium alloys (1.25 × 10(-6) cm(3)·g(-1)-1.29 × 10(-6) cm(3)·g(-1) for zirconium-ruthenium alloys) are ultralow, about one-third that of Ti-based alloys (Ti-6Al-4V, ~3.5 × 10(-6) cm(3)·g(-1), CP Ti and Ti-6Al-7Nb, ~3.0 × 10(-6) cm(3)·g(-1)), and one-sixth that of Co-Cr alloys (Co-Cr-Mo, ~7.7 × 10(-6) cm(3)·g(-1)). Among the Zr-Ru alloy series, Zr-1Ru demonstrates enhanced mechanical properties, excellent corrosion resistance and cell viability with lowest magnetic susceptibility, and thus is the optimal Zr-Ru alloy system as therapeutic devices under MRI diagnostics environments.

  4. Design and development of novel MRI compatible zirconium- ruthenium alloys with ultralow magnetic susceptibility

    PubMed Central

    Li, H.F.; Zhou, F.Y.; Li, L.; Zheng, Y.F.

    2016-01-01

    In the present study, novel MRI compatible zirconium-ruthenium alloys with ultralow magnetic susceptibility were developed for biomedical and therapeutic devices under MRI diagnostics environments. The results demonstrated that alloying with ruthenium into pure zirconium would significantly increase the strength and hardness properties. The corrosion resistance of zirconium-ruthenium alloys increased significantly. High cell viability could be found and healthy cell morphology observed when culturing MG 63 osteoblast-like cells and L-929 fibroblast cells with zirconium-ruthenium alloys, whereas the hemolysis rates of zirconium-ruthenium alloys are <1%, much lower than 5%, the safe value for biomaterials according to ISO 10993-4 standard. Compared with conventional biomedical 316L stainless steel, Co–Cr alloys and Ti-based alloys, the magnetic susceptibilities of the zirconium-ruthenium alloys (1.25 × 10−6 cm3·g−1–1.29 × 10−6 cm3·g−1 for zirconium-ruthenium alloys) are ultralow, about one-third that of Ti-based alloys (Ti–6Al–4V, ~3.5 × 10−6 cm3·g−1, CP Ti and Ti–6Al–7Nb, ~3.0 × 10−6 cm3·g−1), and one-sixth that of Co–Cr alloys (Co–Cr–Mo, ~7.7 × 10−6 cm3·g−1). Among the Zr–Ru alloy series, Zr–1Ru demonstrates enhanced mechanical properties, excellent corrosion resistance and cell viability with lowest magnetic susceptibility, and thus is the optimal Zr–Ru alloy system as therapeutic devices under MRI diagnostics environments. PMID:27090955

  5. Power dissipation in HTS coated conductor coils under the simultaneous action of AC and DC currents and fields

    NASA Astrophysics Data System (ADS)

    Shen, Boyang; Li, Chao; Geng, Jianzhao; Zhang, Xiuchang; Gawith, James; Ma, Jun; Liu, Yingzhen; Grilli, Francesco; Coombs, T. A.

    2018-07-01

    This paper presents a comprehensive alternating current (AC) loss study of a circular high temperature superconductor (HTS) coated conductor coil. The AC losses from a circular double pancake coil were measured using the electrical method. A 2D axisymmetric H -formulation model using the FEM package in COMSOL Multiphysics has been established to match the circular geometry of the coil used in the experiment. Three scenarios have been analysed: Scenario 1 with AC transport current and DC magnetic field (experiment and simulation); Scenario 2 with DC transport current and AC magnetic field (simulation); and Scenario 3 with AC transport current and AC magnetic field (simulation and experimental data support). The angular dependence analysis on the coil under a magnetic field with different orientation angle θ has been carried out for all three scenarios. For Scenario 3, the effect of the relative phase difference Δφ between the AC current and the AC field on the total AC loss of the coil has been investigated. In summary, a current/field/angle/phase dependent AC loss ( I , B , θ, Δφ) study of a circular HTS coil has been carried out. The obtained results provide useful indications for the future design and research of HTS AC systems.

  6. Reversible susceptibility studies of magnetization switching in FeCoB synthetic antiferromagnets

    NASA Astrophysics Data System (ADS)

    Radu, Cosmin; Cimpoesu, Dorin; Girt, Erol; Ju, Ganping; Stancu, Alexandru; Spinu, Leonard

    2007-05-01

    In this paper we present a study of switching characteristics of a series of synthetic antiferromagnet (SAF) structures using reversible susceptibility experiments. Three series of SAF samples were considered in our study with (t1, t2), the thickness of the FeCoB layers of (80nm, 80nm), (50nm, 50nm), and (80nm, 20nm) and with the interlayer of Ru ranging from 0to2nm. A vector vibrating sample magnetometer was used to measure the hysteresis loops along the different directions in the plane of the samples. The reversible susceptibility experiments were performed using a resonant method based on a tunnel diode oscillator. We showed that the switching peaks in the susceptibility versus field plots obtained for different orientations of the applied dc field can be used to construct the switching diagram of the SAF structure. The critical curve constitutes the fingerprint of the switching behavior and provides information about micromagnetic and structural properties of SAF which is an essential component of modern magnetic random access memories.

  7. Phase diagram of the chiral magnet Cr1 /3NbS2 in a magnetic field

    NASA Astrophysics Data System (ADS)

    Tsuruta, K.; Mito, M.; Deguchi, H.; Kishine, J.; Kousaka, Y.; Akimitsu, J.; Inoue, K.

    2016-03-01

    We construct the phase diagram of the chiral magnet Cr1 /3NbS2 in a dc magnetic field (Hdc) using ac magnetic susceptibility measurements. At Hdc=0 , the ac response at the transition from the helical magnetic (HM) state to the paramagnetic (PM) state consists of a giant third-order harmonic component (M3 ω) and a first-order harmonic component (M1 ω). By applying Hdc perpendicular to the c axis, the HM state is transformed to the chiral soliton lattice (CSL) state, which is a superlattice tuned by Hdc. The above giant M3 ω is markedly suppressed at small Hdc. The CSL state is found to consist of CSL-1, with dominant helical texture and a poor ferromagnetic array, and CSL-2, with a large ferromagnetic array. The transition between CSL-1 and the PM state causes a linear magnetic response, the dominant component of which is the in-phase M1 ω. With increasing temperature, CSL-2 is transformed into the forced ferromagnetic (FFM) state, and ultimately the PM state is reached. The transition between CSL-2 and the FFM state consists of a large M3 ω and large out-of-phase M1 ω as well as in-phase M1 ω. The transition between the FMM and PM states also yields a linear magnetic response, like the CSL-1-PM-state transition. Five typical magnetic dynamics in the transitions among the HM state, CSL-1, CSL-2, FFM state, and PM state were identified according to the equivalent dynamical motion equation of a nonlinear spring model.

  8. AC Application of HTS Conductors in Highly Dynamic Electric Motors

    NASA Astrophysics Data System (ADS)

    Oswald, B.; Best, K.-J.; Setzer, M.; Duffner, E.; Soell, M.; Gawalek, W.; Kovalev, L. K.

    2006-06-01

    Based on recent investigations we design highly dynamic electric motors up to 400 kW and linear motors up to 120 kN linear force using HTS bulk material and HTS tapes. The introduction of HTS tapes into AC applications in electric motors needs fundamental studies on double pancake coils under transversal magnetic fields. First theoretical and experimental results on AC field distributions in double-pancake-coils and corresponding AC losses will be presented. Based on these results the simulation of the motor performance confirms extremely high power density and efficiency of both types of electric motors. Improved characteristics of rare earth permanent magnets used in our motors at low temperatures give an additional technological benefit.

  9. Separation of pedogenic and lithogenic components of magnetic susceptibility in the Chinese loess/palaeosol sequence as determined by the CBD procedure and a mixing analysis

    NASA Astrophysics Data System (ADS)

    Vidic, Nataša. J.; TenPas, Jeff D.; Verosub, Kenneth L.; Singer, Michael J.

    2000-08-01

    Magnetic susceptibility variations in the Chinese loess/palaeosol sequences have been used extensively for palaeoclimatic interpretations. The magnetic signal of these sequences must be divided into lithogenic and pedogenic components because the palaeoclimatic record is primarily reflected in the pedogenic component. In this paper we compare two methods for separating the pedogenic and lithogenic components of the magnetic susceptibility signal: the citrate-bicarbonate-dithionite (CBD) extraction procedure, and a mixing analysis. Both methods yield good estimates of the pedogenic component, especially for the palaeosols. The CBD procedure underestimates the lithogenic component and overestimates the pedogenic component. The magnitude of this effect is moderately high in loess layers but almost negligible in palaeosols. The mixing model overestimates the lithogenic component and underestimates the pedogenic component. Both methods can be adjusted to yield better estimates of both components. The lithogenic susceptibility, as determined by either method, suggests that palaeoclimatic interpretations based only on total susceptibility will be in error and that a single estimate of the average lithogenic susceptibility is not an accurate basis for adjusting the total susceptibility. A long-term decline in lithogenic susceptibility with depth in the section suggests more intense or prolonged periods of weathering associated with the formation of the older palaeosols. The CBD procedure provides the most comprehensive information on the magnitude of the components and magnetic mineralogy of loess and palaeosols. However, the mixing analysis provides a sensitive, rapid, and easily applied alternative to the CBD procedure. A combination of the two approaches provides the most powerful and perhaps the most accurate way of separating the magnetic susceptibility components.

  10. Soil erosion at agricultural land in Moravia loess region estimated by using magnetic properties

    NASA Astrophysics Data System (ADS)

    Kapicka, Ales; Dlouha, Sarka; Petrovsky, Eduard; Jaksik, Ondrej; Grison, Hana; Kodesova, Radka

    2014-05-01

    A detailed field study on a small test site of agricultural land situated in loess region in Southern Moravia (Czech Republic) and subsequent laboratory analyses have been carried out in order to test the applicability of magnetic methods for the estimation of soil erosion. Chernozem, the original dominant soil unit in the wider area, is nowadays progressively transformed into different soil units along with intensive soil erosion. As a result, an extremely diversified soil cover structure has resulted from the erosion. The site was characterized by a flat upper part while the middle part, formed by a substantive side valley, is steeper (up to 15°). We carried out field measurements of magnetic susceptibility on a regular grid, resulting in 101 data points. The bulk soil material for laboratory investigation was gathered from all the grid points. We found a strong correlation between the volume magnetic susceptibility (field measurement) and mass specific magnetic susceptibility measured in the laboratory (R2 = 0.80). Values of the magnetic susceptibility are spatially distributed depending on the terrain. Higher values were measured in the flat upper part (where the original top horizon remained). The lowest values of magnetic susceptibility were obtained on the steep valley sides. Here the original topsoil was eroded and mixed by tillage with the soil substrate (loess). The soil profile that was unaffected by erosion was investigated in detail. The vertical distribution of magnetic susceptibility along this "virgin" profile was measured in laboratory on the samples from layers along the whole profile with 2-cm spacing. The undisturbed profile shows several soil horizons. Horizons Ac and A show a slight increase in magnetic susceptibility up to a depth of about 70 cm. Horizon A/Ck is characterized by a decrease in susceptibility, and the underlying C horizon (h > 103 cm) has a very low value of magnetic susceptibility. The differences between the values of

  11. Detection of magnetic nanoparticles with a large scale AC superconducting susceptometer

    NASA Astrophysics Data System (ADS)

    Hincapie Ladino, E. A.; Zufelato, N.; Bakuzis, A. F.; Oliveira Carneiro, A. A.; Covas, D. T.; Baffa, O.

    2017-08-01

    Magnetic nanoparticles (MNPs) are being used in several applications in medicine such as hyperthermia, magnetic particle imaging, in vitro and in vivo bioassay, and still there are many other possibilities for use of these particles to come as research progress in this field. One crucial step of its use is the detection of these particles when present in a certain tissue. For in vitro bioassay, the sample can be harvested and placed inside the detector in optimal conditions to favor sensitivity. However, for in vivo human measurements the system must be noninvasive and conform to the anatomic restrictions requiring sensitive detectors and dedicated setups. In this study, we detect nanoparticles with an AC biosusceptometer having an excitation homogeneous magnetic field with 145 μT, provided by a set of rectangular large Rubens coils driven at 10 Hz. The magnetization induced in the sample was detected by a second-order axial gradiometer (20 mm in diameter and 40 mm of baseline) coupled to an RF Superconducting Quantum Interference Device (SQUID) model 330X (BTi). The MNPs used were manganese ferrite-based surface-coated with citric acid ({{M}}{{n}}{{F}}{{{e}}}2{{{O}}}4-{{C}}{{i}}{{t}}{{r}}{{a}}{{t}}{{e}}), dissolved in water at various concentrations. The colloid is stable at physiological conditions. X-ray diffraction confirmed the spinel structure and using Scherrer’s relation revealed a particle size of 17.3 nm. The magnetization curve showed a typical superparamagnetic behavior with a specific saturation magnetization of 51.2 emu g-1. The stock solution of nanoparticles had a concentration of 23.17 mg ml-1, corresponding to 1.7 × 1015 NPs ml-1. Measurements were made in a volume of 30 ml with 20 × 103-100 × 103 dilutions of the stock solution of nanoparticles and performed at distances of 1.1, 1.5 and 2.5 cm from the top of the sample vial to the closest coil of the gradiometer. The limits of detection were 8.1 × 109 NP ml-1, 9.5 × 109 NP ml-1 and 11

  12. Kohn anomalies in momentum dependence of magnetic susceptibility of some three-dimensional systems

    NASA Astrophysics Data System (ADS)

    Stepanenko, A. A.; Volkova, D. O.; Igoshev, P. A.; Katanin, A. A.

    2017-11-01

    We study a question of the presence of Kohn points, yielding at low temperatures nonanalytic momentum dependence of magnetic susceptibility near its maximum, in electronic spectra of some threedimensional systems. In particular, we consider a one-band model on face-centered cubic lattice with hopping between the nearest and next-nearest neighbors, which models some aspects of the dispersion of ZrZn2, and the two-band model on body-centered cubic lattice, modeling the dispersion of chromium. For the former model, it is shown that Kohn points yielding maxima of susceptibility exist in a certain (sufficiently wide) region of electronic concentrations; the dependence of the wave vectors, corresponding to the maxima, on the chemical potential is investigated. For the two-band model, we show the existence of the lines of Kohn points, yielding maximum susceptibility, whose position agrees with the results of band structure calculations and experimental data on the wave vector of antiferromagnetism of chromium.

  13. Magnetic susceptibilities of liquid Cr-Au, Mn-Au and Fe-Au alloys

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Ohno, S.; Shimakura, H.; Tahara, S.

    The magnetic susceptibility of liquid Cr-Au, Mn-Au, Fe-Au and Cu-Au alloys was investigated as a function of temperature and composition. Liquid Cr{sub 1-c}Au{sub c} with 0.5 ≤ c and Mn{sub 1-c}Au{sub c} with 0.3≤c obeyed the Curie-Weiss law with regard to their dependence of χ on temperature. The magnetic susceptibilities of liquid Fe-Au alloys also exhibited Curie-Weiss behavior with a reasonable value for the effective number of Bohr magneton. On the Au-rich side, the composition dependence of χ for liquid TM-Au (TM=Cr, Mn, Fe) alloys increased rapidly with increasing TM content, respectively. Additionally, the composition dependences of χ for liquidmore » Cr-Au, Mn-Au, and Fe-Au alloys had maxima at compositions of 50 at% Cr, 70 at% Mn, and 85 at% Fe, respectively. We compared the composition dependences of χ{sub 3d} due to 3d electrons for liquid binary TM-M (M=Au, Al, Si, Sb), and investigated the relationship between χ{sub 3d} and E{sub F} in liquid binary TM-M alloys at a composition of 50 at% TM.« less

  14. Magnetic Susceptibility Effects and Lorentz Damping in Diamagnetic Fluids

    NASA Technical Reports Server (NTRS)

    Ramachandran, Narayanan; Leslie, Fred W.

    2000-01-01

    A great number of crystals (semi-conductor and protein) grown in space are plagued by convective motions which contribute to structural flaws. The character of these instabilities is not well understood but is associated with density variations in the presence of residual gravity and g-jitter. Both static and dynamic (rotating or travelling wave) magnetic fields can be used to reduce the effects of convection in materials processing. In semi-conductor melts, due to their relatively high electrical conductivity, the induced Lorentz force can be effectively used to curtail convective effects. In melts/solutions with reduced electrical conductivity, such as aqueous solutions used in solution crystal growth, protein crystal growth and/or model fluid experiments for simulating melt growth, however, the variation of the magnetic susceptibility with temperature and/or concentration can be utilized to better damp fluid convection than the Lorentz force method. This paper presents a comprehensive, comparative numerical study of the relative damping effects using static magnetic fields and gradients in a simple geometry subjected to a thermal gradient. The governing equations are formulated in general terms and then simplified for the numerical calculations. Operational regimes, based on the best damping technique for different melts/solutions are identified based on fluid properties. Comparisons are provided between the numerical results and available results from experiments in surveyed literature.

  15. Time as An Important Soil-Forming Factor Influencing Modern and Ancient Magnetic Susceptibility Enhancement Along the Delaware River Valley, USA

    NASA Astrophysics Data System (ADS)

    Stinchcomb, G. E.; Peppe, D. J.; Driese, S. G.

    2011-12-01

    Magnetic susceptibility is an increasingly popular low-cost method for rapidly assessing paleoclimate and paleoenvironmental impact on buried soils. The goal of this study is to determine the primary influence(s) on soil magnetic susceptibility along floodplain, terrace and upland soils in the middle Delaware River Valley, USA, using environmental magnetic, pedologic, and stratigraphic techniques. Two-hundred thirty samples were collected from age-constrained sandy, quartz-rich, floodplain, terrace, and upland soils (Entisols, Inceptisols). A Kruskal-Wallis (K-W) and post-hoc Tukey-Kramer (T-K) (α=0.05) multiple comparisons analysis on 176 mass-specific low-field susceptibility (Xlf) assays show that A and B horizons are magnetically enhanced compared to C and E horizons (p<0.0001). Results of descriptive soil micromorphology show that A and B horizons contain anywhere from 10-50% more amorphous organic matter and clay films along pores than do C and E horizons. Enhanced Xlf values also correlate positively (R^2=0.63) with the soil molecular weathering ratio of Alumina/Bases, suggesting that increased weathering likely results in the formation of pedogenic magnetic minerals and enhanced magnetic susceptibility signal. Additional K-W and T-K testing show that Xlf results, when grouped by floodplain-terrace designation (i.e., chronofunction) are significantly different (p<0.0001). The older T3 terrace and upland Xlf values (0.34±0.14 10^-6 m^3 kg^-1) are greater than the younger T2 terrace (0.18±0.06 10^-6 m^3 kg^-1) values, which are greater than modern floodplain (0.09±0.01 10^-6 m^3 kg^-1) Xlf values. These data suggest that longer intervals of soil formation enhance the Χlf value. This hypothesis is further supported when 159 Xlf values are plotted vs. age for the entire Holocene. A locally-weighted regression smoothing curve (LOESS) shows two distinct intervals of magnetic enhancement during previously established dry intervals, the early and late

  16. Symmetric Anderson impurity model: Magnetic susceptibility, specific heat and Wilson ratio

    NASA Astrophysics Data System (ADS)

    Zalom, Peter; Pokorný, Vladislav; Janiš, Václav

    2018-05-01

    We extend the spin-polarized effective-interaction approximation of the parquet renormalization scheme from Refs. [1,2] applied on the symmetric Anderson model by adding the low-temperature asymptotics of the total energy and the specific heat. We calculate numerically the Wilson ratio and determine analytically its asymptotic value in the strong-coupling limit. We demonstrate in this way that the exponentially small Kondo scale from the strong-coupling regime emerges in qualitatively the same way in the spectral function, magnetic susceptibility and the specific heat.

  17. EFFECT OF ANNEALING TEMPERATURE ON THE STRUCTURE AND AC MAGNETIC PROPERTIES OF Fe73Cu1Nb3.5-xVxSi13.5B9 (x = 1.0, 1.5, 2.0) NANOCRYSTALLINE SOFT MAGNETIC ALLOYS

    NASA Astrophysics Data System (ADS)

    Lu, Wei; Huang, Ping; Wang, Yuxin; Yan, Biao

    2013-07-01

    In this paper, Nb element was partially replaced by V element in Finemet-type Fe73Cu1Nb3.5-xVxSi13.5B9 (x = 1, 1.5, 2) alloys and the effect of annealing temperatures on the microstructure and AC magnetic properties of the samples are studied. The annealing temperatures affect the grain sizes of the bcc α-Fe phase greatly. When the annealing temperature is between 540-560°C, the samples have better AC magnetic properties than the samples annealed at other temperatures. The optimized annealing temperature of the studied samples is around 560°C. The coercivity and iron loss of the V2 sample is a little bit higher than that of V1 and V1.5 alloys while the amplitude permeability of V2 alloy is larger than that of V1 and V1.5, which indicate that the content of V element has strong influence on the magnetic properties of nanocrystalline soft magnetic alloys.

  18. Exploiting the Temperature Dependence of Magnetic Susceptibility to Control Convection in Fundamental Studies of Solidification Phenomena

    NASA Technical Reports Server (NTRS)

    Seybert, C. D.; Evans, J. W.; Leslie, Fred; Jones, W. K., Jr.

    2000-01-01

    It is well known that convection is a dominant mass transport mechanism when materials are solidified on Earth's surface. This convection is caused by gradients in density (and therefore gravitational force) that are brought about by gradients in temperature, composition or both. Diffusion of solute is therefore dwarfed by convection and the study of fundamental parameters, such as dendrite tip shape and growth velocity in the absence of convection is nearly impossible. Significant experimental work has therefore been carried out in orbiting laboratories with the intent of minimizing convection by minimizing gravity. One of the best known experiments of this kind is the Isothermal Dendritic Growth Experiment (IDGE), supported by NASA. Naturally such experiments are costly and one objective of the present investigation is to develop an experimental method whereby convection can be- halted, in solidification and other experiments, on the surface. A second objective is to use the method to minimize convection resulting from the residual accelerations suffered by experiments in microgravity. The method to be used to minimize convection relies on the dependence of the magnetic susceptibility of a fluid on temperature or composition (whichever is driving convection). All materials experience a force when placed in a magnetic field gradient. The direction and magnitude of that force depend on the magnetic susceptibility of the material. Consequently the force will vary if the susceptibility varies with temperature or composition. With a magnetic field gradient in the right direction (typically upward) and of the right magnitude, this variation in the magnetic force can be made to exactly cancel the variation in the gravitational force. Expressed another way, normal buoyancy is exactly countered by a "magnetic buoyancy". To demonstrate the principle, a solution of MnC12 in water has been used. First the variation of the susceptibility of this paramagnetic solution with

  19. Susceptibility and remanence studies in the quasi-1D mixed ferromagnet CoTAC : Mn

    NASA Astrophysics Data System (ADS)

    Cheikhrouhou, A.; Dupas, C.; Renard, J. P.; Veillet, P.

    1985-03-01

    The ac susceptibility and dc magnetization of CoTAC : Mn ((CH 3) 3NHCo 1- xMn xCl 3ṡ2H 2O) have been studied in the temperature range 1.3-4.2 K on two monocrystalline samples with x = 2.9 and 9.3%. In CoTAC : Mn (9.3%), the variation with the measuring frequency ν of the temperature of the susceptibility maximum Tg(ν) is well described over five decades of frequency by an Arrhenius law Tg-1(ν) = a - b log ν characteristic of superparamagnetic clusters. In CoTAC : Mn (2.9%) Tg(ν) does not differ significantly from that of pure CoTAC. Both compounds exhibit strong remanence effects below Tg. The variations with time, temperature and applied magnetic field of the IRM and TRM are similar to those observed in spin glasses. These experiments confirm the onset of spin-glass-like behaviour or superparamagnetism in quasi-1D insulators with random intrachain exchange at very low impurity concentration. Comparison with the previously studied mixed compound CHAC : Mn evidences the influence of the exchange anisotropy on the static properties of these systems.

  20. Microwave ac Zeeman force for ultracold atoms

    NASA Astrophysics Data System (ADS)

    Fancher, C. T.; Pyle, A. J.; Rotunno, A. P.; Aubin, S.

    2018-04-01

    We measure the ac Zeeman force on an ultracold gas of 87Rb due to a microwave magnetic field targeted to the 6.8 GHz hyperfine splitting of these atoms. An atom chip produces a microwave near field with a strong amplitude gradient, and we observe a force over three times the strength of gravity. Our measurements are consistent with a simple two-level theory for the ac Zeeman effect and demonstrate its resonant, bipolar, and spin-dependent nature. We observe that the dressed-atom eigenstates gradually mix over time and have mapped out this behavior as a function of magnetic field and detuning. We demonstrate the practical spin selectivity of the force by pushing or pulling a specific spin state while leaving other spin states unmoved.

  1. MR susceptibility imaging

    NASA Astrophysics Data System (ADS)

    Duyn, Jeff

    2013-04-01

    This work reviews recent developments in the use of magnetic susceptibility contrast for human MRI, with a focus on the study of brain anatomy. The increase in susceptibility contrast with modern high field scanners has led to novel applications and insights into the sources and mechanism contributing to this contrast in brain tissues. Dedicated experiments have demonstrated that in most of healthy brain, iron and myelin dominate tissue susceptibility variations, although their relative contribution varies substantially. Local variations in these compounds can affect both amplitude and frequency of the MRI signal. In white matter, the myelin sheath introduces an anisotropic susceptibility that has distinct effects on the water compartments inside the axons, between the myelin sheath, and the axonal space, and renders their signals dependent on the angle between the axon and the magnetic field. This offers opportunities to derive tissue properties specific to these cellular compartments.

  2. Ex-vivo quantitative susceptibility mapping of human brain hemispheres

    PubMed Central

    Kotrotsou, Aikaterini; Tamhane, Ashish A.; Dawe, Robert J.; Kapasi, Alifiya; Leurgans, Sue E.; Schneider, Julie A.; Bennett, David A.; Arfanakis, Konstantinos

    2017-01-01

    Ex-vivo brain quantitative susceptibility mapping (QSM) allows investigation of brain characteristics at essentially the same point in time as histopathologic examination, and therefore has the potential to become an important tool for determining the role of QSM as a diagnostic and monitoring tool of age-related neuropathologies. In order to be able to translate the ex-vivo QSM findings to in-vivo, it is crucial to understand the effects of death and chemical fixation on brain magnetic susceptibility measurements collected ex-vivo. Thus, the objective of this work was twofold: a) to assess the behavior of magnetic susceptibility in both gray and white matter of human brain hemispheres as a function of time postmortem, and b) to establish the relationship between in-vivo and ex-vivo gray matter susceptibility measurements on the same hemispheres. Five brain hemispheres from community-dwelling older adults were imaged ex-vivo with QSM on a weekly basis for six weeks postmortem, and the longitudinal behavior of ex-vivo magnetic susceptibility in both gray and white matter was assessed. The relationship between in-vivo and ex-vivo gray matter susceptibility measurements was investigated using QSM data from eleven older adults imaged both antemortem and postmortem. No systematic change in ex-vivo magnetic susceptibility of gray or white matter was observed over time postmortem. Additionally, it was demonstrated that, gray matter magnetic susceptibility measured ex-vivo may be well modeled as a linear function of susceptibility measured in-vivo. In conclusion, magnetic susceptibility in gray and white matter measured ex-vivo with QSM does not systematically change in the first six weeks after death. This information is important for future cross-sectional ex-vivo QSM studies of hemispheres imaged at different postmortem intervals. Furthermore, the linear relationship between in-vivo and ex-vivo gray matter magnetic susceptibility suggests that ex-vivo QSM captures

  3. Coupled dielectric permittivity and magnetic susceptibility in the insulating antiferromagnet Ba2FeSbSe5

    NASA Astrophysics Data System (ADS)

    Maier, S.; Moussa, C.; Berthebaud, D.; Gascoin, F.; Maignan, A.

    2018-05-01

    We report on coupled changes in the dielectric permittivity and the magnetic susceptibility in the insulating antiferromagnet Ba2FeSbSe5. The real part of the dielectric permittivity (ɛ') and the thermal conductivity (κ) shows pronounced anomalies at the Néel temperature (TN). Our findings show that there is a weak coupling between electric dipoles and magnetic spins, which is mediated by spin-lattice coupling possibly through exchange striction effects.

  4. The metallic sphere in a uniform ac magnetic field: A simple and precise experiment for exploring eddy currents and non-destructive testing

    NASA Astrophysics Data System (ADS)

    Honke, Michael L.; Bidinosti, Christopher P.

    2018-06-01

    We describe a very simple experiment that utilizes standard laboratory equipment to measure the electromagnetic response of a metallic sphere exposed to a uniform ac magnetic field. Measurements were made for a variety of non-magnetic and magnetic metals, and in all cases the results fit very well with theory over the four orders of frequency (25 Hz to 102 kHz) explored here. Precise values of magnetic permeability and electrical conductivity can be extracted from fits to the data given the sphere radius only. The same apparatus is also used to explore the effects of geometry on eddy current generation as well as to demonstrate non-destructive testing through measurements on coins of different composition.

  5. In Situ Magnetic Susceptibility Variations at Two Contaminated Sites: Brandywine, MD and Bemidji, MN

    NASA Astrophysics Data System (ADS)

    Donaldson, Y. Y.; Kessouri, P.; Ntarlagiannis, D.; Johnson, T. C.; Day-Lewis, F. D.; Johnson, C. D.; Bekins, B. A.; Slater, L. D.

    2017-12-01

    Geophysical methods are widely used monitoring tools for investigating subsurface processes. Compared to more traditional methods, they are low cost and minimally invasive. Magnetic susceptibility (MS) is a geophysical technique particularly sensitive to the presence of ferri/ ferro-magnetic particles such as iron oxides (e.g., magnetite, hematite and goethite). These oxides can be formed through microbially mediated redox reactions, inducing changes in the soil properties that can be observed by MS measurements. Monitoring MS changes over time provides indications of iron mineral transformations in the ground. These transformations are of particular interest for the characterization of contaminated sites. We acquired borehole MS measurements from two contaminated sites: Brandywine, MD and Bemidji, MN. Active remediation was applied at Brandywine, whereas natural attenuation has been geophysically monitored at Bemidji since 2011 using MS log measurements. High MS values were observed at both sites within the contaminated area only. We hypothesize that this is due to iron reducing bacteria reducing Fe-(III) to Fe-(II) and utilizing contaminants and/or amendments injected as a carbon source. At Bemidji, elevated MS readings were observed in the smear zone and correlate to the presence of magnetite. Furthermore, time-lapse MS observations at Bemidji indicate a decay in signal amplitude over time suggesting further redox transformation into less magnetic particles. For both field examples presented here, we observe variations in magnetic susceptibility within the contaminated areas that can be linked with redox reactions and mineral transformations occurring during the degradation of organic contaminants.

  6. Carbonate-Bridged Lanthanoid Triangles: Single-Molecule Magnet Behavior, Inelastic Neutron Scattering, and Ab Initio Studies.

    PubMed

    Giansiracusa, Marcus J; Vonci, Michele; Van den Heuvel, Willem; Gable, Robert W; Moubaraki, Boujemaa; Murray, Keith S; Yu, Dehong; Mole, Richard A; Soncini, Alessandro; Boskovic, Colette

    2016-06-06

    Optimization of literature synthetic procedures has afforded, in moderate yield, homogeneous and crystalline samples of the five analogues Na11[{RE(OH2)}3CO3(PW9O34)2] (1-RE; RE = Y, Tb, Dy, Ho, and Er). Phase-transfer methods have allowed isolation of the mixed salts (Et4N)9Na2[{RE(OH2)}3CO3(PW9O34)2] (2-RE; RE = Y and Er). The isostructural polyanions in these compounds are comprised of a triangular arrangement of trivalent rare-earth ions bridged by a μ3-carbonate ligand and sandwiched between two trilacunary Keggin {PW9O34} polyoxometalate ligands. Alternating-current (ac) magnetic susceptibility studies of 1-Dy, 1-Er, and 2-Er reveal the onset of frequency dependence for the out-of-phase susceptibility in the presence of an applied magnetic field at the lowest measured temperatures. Inelastic neutron scattering (INS) spectra of 1-Ho and 1-Er exhibit transitions between the lowest-lying crystal-field (CF) split states of the respective J = 8 and (15)/2 ground-state spin-orbit multiplets of the Ho(III) and Er(III) ions. Complementary ab initio calculations performed for these two analogues allow excellent reproduction of the experimental magnetic susceptibility and low-temperature magnetization data and are in reasonable agreement with the experimental INS data. The ab initio calculations reveal that the slight difference in coordination environments of the three Ln(III) ions in each complex gives rise to differences in the CF splitting that are not insignificant. This theoretical result is consistent with the observation of multiple relaxation processes by ac magnetic susceptibility and the broadness of the measured INS peaks. The ab initio calculations also indicate substantial mixing of the MJ contributions to the CF split energy levels of each Ln(III) ion. Calculations indicate that the CF ground states of the Ho(III) centers in 1-Ho are predominantly comprised of contributions from small MJ, while those of the Er(III) centers in 1-Er are predominantly

  7. LOW-TEMPERATURE MAGNETIC PROPERTIES OF SOME URANIUM OXIDES

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Leask, M.J.M.; Roberts, L.E.J.; Walter, A.J.

    1963-10-01

    The magnetic susceptibilities of UO/sub 2/, UO/sub 2.1/, U/sub 4/O/sub 9/ , U/s ub 3/O/sub 7/, and U/sub 3/O/sub 8/ at temperatures between 1.5 and 44 deg K were determined using an a-c inductance method. The susceptibility Of U/sub 3/ O/sub 8/ rises to a sharp maximum at 4.2 deg K, with smaller effects at 8 and at 25.3 deg K. The susceptibility of UO/sub 2/ reaches a maximum at 29 deg K and remains constant between 25 and 2 deg K. A maximum in the susceptibility- temperature plot for U/sub 4/O/sub 9/ at 6.4 deg K occurs also-in themore » plots for UO/sub 2.1/ an d U/sub 3/O/sub 7/ and appears to be primarily due to the inclusion of interstitial oxygen ions in the UO/sub 2/ lattice, independent of the precise nature of subsequent ordering effects. (auth)« less

  8. Magnetic relaxation behavior of lanthanide substituted Dawson-type tungstoarsenates

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Liu Lizhen; Li Fengyan; Xu Lin, E-mail: linxu@nenu.edu.c

    2010-02-15

    Two new polyoxometalate compounds [(CH{sub 3}){sub 4}N]{sub 8}[Ln(H{sub 2}O){sub 8}]{sub 2}[(alpha{sub 2}-As{sub 2}W{sub 17}O{sub 61})Ln(H{sub 2}O){sub 2}]{sub 2}.nH{sub 2}O (Ln=Er (1), Dy (2)) have been prepared by the trivacant Dawson-type anion [alpha-As{sub 2}W{sub 15}O{sub 56}]{sup 12-} and trivalent rare earth ion and characterized by single-crystal X-ray diffraction, IR spectra, thermogravimetric and electrochemical analyses. The centrosymmetric polyoxoanion, {l_brace}[(alpha{sub 2}-As{sub 2}W{sub 17}O{sub 61})Ln(H{sub 2}O){sub 2}]{sub 2}{r_brace}{sup 14-}, bounded to each other via Ln{sup 3+} connecting to terminal W-O oxygen atoms. Furthermore, the polyoxoanions are linked by [Ln(H{sub 2}O){sub 8}]{sup 3+} to form an extensive 3D supramolecular network structure depending on hydrogen bond.more » The magnetic properties of the two compounds have been studied by measuring their magnetic susceptibilities in the temperature range 2.0-300.0 K, indicating the depopulation of the stark components at low temperature and/or very weak antiferromagnetic interactions between magnetic centers. Low-temperature ac magnetic susceptibility measurements reveal a slow magnetic relaxation behavior for 2. - Graphical abstract: Two polyoxometalate compounds [(CH{sub 3}){sub 4}N]{sub 8}[Ln(H{sub 2}O){sub 8}]{sub 2}[(alpha{sub 2}-As{sub 2}W{sub 17}O{sub 61})Ln(H{sub 2}O){sub 2}]{sub 2}.nH{sub 2}O (Ln=Er (1), Dy (2)) have been prepared. The dynamic magnetic measurements for 2 display a slow relaxation of magnetization, showing a frequency-dependent susceptibility.« less

  9. [Heavy Metals Accmultio in the Caofeidian Reclamation Soils: Indicated by Soil Magnetic Susceptibility].

    PubMed

    Xue, Yong; Zhou, Qian; Li, Yuan; Zhang, Hai-bo; Hu, Xue-feng; Luo, Yong-ming

    2016-04-15

    The environmental magnetism method has been widely applied to identify soil heavy metal pollution, which is characterized by simplicity, efficiency, non-destructivity and sensitivity. The present study used magnetic susceptibility to assess the accumulation of heavy metals in soils of the Caofeidian industrial zone which is a typical reclamation area in northern China. The study area was divided into three sub-zones based on the function, including industrial zone, living zone, natural tidal flat and wetland. A total of 35 topsoil samples (0-10 cm) and 3 soil profiles were collected from the three sub-zones. Magnetic susceptibility (X(lf)), iron oxide (Fe2O3) contents and heavy metals contents (Cr, Ni, Cu, Zn, As, Pb, Mn and V) of the samples were analyzed. The results showed that X(lf) values and heavy metals contents exhibited higher spatial variability in the top soil of the industrial zone, indicating the severe impacts of industrial activities. In the soil profiles of the industrial and living zones, all heavy metals were enriched to different degrees in the upper layer (0-20 cm). However, there was no significant change of heavy metal contents in the soil profiles of tidal flat which was far from the industrial area. The X(lf) value was significantly (P < 0.01) positively correlated with the contents of Fe2O3, Ni, Cu, As and V in the industrial top soil. This indicated that X(lf) could be used as an indicator for heavy metal accumulation in the industrial zone. However, the X(lf) value was not suitable to be an indicator to show the heavy metal accumulation in the soils of living zone and natural tidal flat. This might be associated with the different sources of magnetic materials among the different sub-zones and the special characteristics of the soils in the tidal flat and wetland.

  10. Anisotropy of magnetic susceptibility (AMS) in the Siilinjärvi carbonatite complex, eastern Finland

    NASA Astrophysics Data System (ADS)

    Almqvist, Bjarne; Karell, Fredrik; Högdahl, Karin; Malehmir, Alireza; Heino, Pasi; Salo, Aleksi

    2017-04-01

    We present a set of AMS measurements on samples from the Siilinjärvi alkaline-carbonatite complex in eastern Finland. The complex has a tabular shape (ca. 16 km long, 1.5 km wide) that strikes north-south and is constrained within a steeply dipping N-S oriented deformation zone. It consists of a mixture of lithologies, including carbonatite, fenite and glimmerite (mica-rich rocks), which is hosted within a Precambrian granite and gneiss. After emplacement of the carbonatite, the complex was subsequently intruded by diabase dykes. Deformation has occurred in several episodes after dyke intrusions, and strain is heterogeneously distributed among the different lithologies. Strain localizes mainly within glimmerite and carbonatite, and at the contacts between dykes and glimmerite/carbonatite where shear zones develop locally. Structures provide indications for both simple (strike-slip) and pure shear components in the deformation history of the complex, although the former may dominate. Thirty-six localities were sampled, providing 272 specimens for AMS measurements, within the southern and eastern parts of the Siilinjärvi open-pit mine (within the complex), mainly from diabase dykes, glimmerite and carbonatites; a smaller number of samples were collected from fenite. Sampling was carried out in order to investigate magnetic fabrics in relation to the emplacement of the dykes and their structural relationship to the glimmerite/carbonatite. Structural measurements were made to accompany the magnetic fabric study. The magnetic fabric shows a magnetic foliation plane that is oriented north-south, with sub-horizontal k3-axes oriented nearly east-west. Magnetic lineation (k1) clusters sub-vertically, but does show a tendency to spread along the north-south magnetic foliation great circle. The dataset can be further divided into two sub-sets based on the bulk susceptibility (km) and degree of anisotropy (P). The bulk of the data set ( 70 %), belonging to samples of diabase

  11. Slow spin relaxation induced by magnetic field in [NdCo(bpdo)(H2O)4(CN)6]⋅3H2O.

    PubMed

    Vrábel, P; Orendáč, M; Orendáčová, A; Čižmár, E; Tarasenko, R; Zvyagin, S; Wosnitza, J; Prokleška, J; Sechovský, V; Pavlík, V; Gao, S

    2013-05-08

    We report on a comprehensive investigation of the magnetic properties of [NdCo(bpdo)(H2O)4(CN)6]⋅3H2O (bpdo=4, 4'-bipyridine-N,N'-dioxide) by use of electron paramagnetic resonance, magnetization, specific heat and susceptibility measurements. The studied material was identified as a magnet with an effective spin S = 1/2 and a weak exchange interaction J/kB = 25 mK. The ac susceptibility studies conducted at audio frequencies and at temperatures from 1.8 to 9 K revealed that the application of a static magnetic field induces a slow spin relaxation. It is suggested that the relaxation in the magnetic field appears due to an Orbach-like process between the two lowest doublet energy states of the magnetic Nd(3+) ion. The appearance of the slow relaxation in a magnetic field cannot be associated with a resonant phonon trapping. The obtained results suggest that the relaxation is influenced by nuclear spin driven quantum tunnelling which is suppressed by external magnetic field.

  12. Magnetic excitation and local magnetic susceptibility of the excitonic insulator Ta2NiSe5 investigated by 77Se NMR

    NASA Astrophysics Data System (ADS)

    Li, Shang; Kawai, Shunsuke; Kobayashi, Yoshiaki; Itoh, Masayuki

    2018-04-01

    77Se NMR measurements were made on polycrystalline and single-crystalline samples to elucidate local magnetic susceptibility and magnetic excitation of Ta2NiSe5 , which is proposed to undergo an exciton condensation accompanied by a structural transition at Tc=328 K . We determine the 77Se Knight shift tensors for the three Se sites and analyze their anisotropy based on the site symmetry. The temperature dependence of the Knight shift is discussed on the basis of spin and orbital susceptibilities calculated for two-chain and two-dimensional three-band models. The large fraction of the Se 4 p orbital polarization due to the mixing between Ni 3 d and Se 4 p orbitals is estimated from the analysis of the transferred hyperfine coupling constant. Also the nuclear spin-lattice relaxation rate 1 /T1 is found not to show a coherent peak just below Tc and to obey the thermally activated temperature dependence with a spin gap energy of 1770 ±40 K . This behavior of 1 /T1 monitors the exciton condensation as proposed by the theoretical study of 1 /T1 based on the three-chain Hubbard model for the excitonic insulator.

  13. Use of Magnetic Parameters to Asses Soil Erosion Rates on Agricultural Site

    NASA Astrophysics Data System (ADS)

    Petrovsky, E.; Kapicka, A.; Dlouha, S.; Jaksik, O.; Grison, H.; Kodesova, R.

    2014-12-01

    A detailed field study on a small test site of agricultural land situated in loess region in Southern Moravia (Czech Republic) and laboratory analyses were carried out in order to test the applicability of magnetic methods in assessing soil erosion. Haplic Chernozem, the original dominant soil unit in the area, is nowadays progressively transformed into different soil units along with intense soil erosion. As a result, an extremely diversified soil cover structure has developed due to the erosion. The site was characterized by a flat upper part while the middle part, formed by a substantive side valley, is steeper. We carried out field measurements of magnetic susceptibility on a regular grid, resulting in 101 data points. The bulk soil material for laboratory investigation was gathered from all the grid points. Values of the magnetic susceptibility are spatially distributed depending on the terrain. Higher values were measured in the flat upper part (where the original top horizon remained). The lowest values of were obtained on the steep valley sides. Here the original topsoil was eroded and mixed by tillage with the soil substrate (loess). A soil profile unaffected by erosion was investigated in detail. The vertical distribution of magnetic susceptibility along this "virgin" profile was measured in laboratory on the samples collected with 2-cm spacing. The undisturbed profile shows several soil horizons. Horizons Ac and A show a slight increase in magnetic susceptibility up to a depth of about 70 cm. Horizon A/Ck is characterized by a decrease in susceptibility, and the underlying C horizon (h > 103 cm) has a very low value of magnetic susceptibility. The differences between the values of susceptibility in the undisturbed soil profile and the magnetic signal after uniform mixing the soil material as a result of tillage and erosion are fundamental for the estimation of soil loss in the studied test field. Using the uneroded profile from the studied locality as a

  14. Lithology and chronology of ice-sheet fluctuations (magnetic susceptibility of cores from the western Ross Sea)

    NASA Technical Reports Server (NTRS)

    Jennings, Anne E.

    1993-01-01

    The goals of the marine geology part of WAIS include reconstructing the chronology and areal extent of ice-sheet fluctuations and understanding the climatic and oceanographic influences on ice-sheet history. As an initial step toward attaining these goals, down-core volume magnetic susceptibility (MS) logs of piston cores from three N-S transects in the western Ross Sea are compared. The core transects are within separate petrographic provinces based on analyses of till composition. The provinces are thought to reflect the previous locations of ice streams on the shelf during the last glaciation. Magnetic susceptibility is a function of magnetic mineral composition, sediment texture, and sediment density. It is applied in the western Ross Sea for two purposes: (1) to determine whether MS data differentiates the three transects (i.e., flow lines), and thus can be used to make paleodrainage reconstructions of the late Wisconsinan ice sheet; and (2) to determine whether the MS data can aid in distinguishing basal till diamictons from diamictons of glacial-marine origin and thus, aid paleoenvironmental interpretations. A comparison of the combined data of cores in each transect is presented.

  15. Phase diagram and magnetic relaxation phenomena in Cu2OSeO3

    NASA Astrophysics Data System (ADS)

    Qian, F.; Wilhelm, H.; Aqeel, A.; Palstra, T. T. M.; Lefering, A. J. E.; Brück, E. H.; Pappas, C.

    2016-08-01

    We present an investigation of the magnetic-field-temperature phase diagram of Cu2OSeO3 based on dc magnetization and ac susceptibility measurements covering a broad frequency range of four orders of magnitude, from very low frequencies reaching 0.1 Hz up to 1 kHz. The experiments were performed in the vicinity of Tc=58.2 K and around the skyrmion lattice A phase. At the borders between the different phases the characteristic relaxation times reach several milliseconds and the relaxation is nonexponential. Consequently the borders between the different phases depend on the specific criteria and frequency used and an unambiguous determination is not possible.

  16. Magnetothermal Convection of Water with the Presence or Absence of a Magnetic Force Acting on the Susceptibility Gradient

    PubMed Central

    Maki, Syou

    2016-01-01

    Heat transfer of magnetothermal convection with the presence or absence of the magnetic force acting on the susceptibility gradient (fsc) was examined by three-dimensional numerical computations. Thermal convection of water enclosed in a shallow cylindrical vessel (diameter over vessel height = 6.0) with the Rayleigh-Benard model was adopted as the model, under the conditions of Prandtl number 6.0 and Ra number 7000, respectively. The momentum equations of convection were nondimensionalized, which involved the term of fsc and the term of magnetic force acting on the magnetic field gradient (fb). All the computations resulted in axisymmetric steady rolls. The values of the averaged Nu, the averaged velocity components U, V, and W, and the isothermal distributions and flow patterns were almost completely the same, regardless of the presence or absence of the term of fsc. As a result, we found that the effect of fsc was extremely small, although much previous research emphasized the effect with paramagnetic solutions under an unsteady state. The magnitude of fsc depends not only on magnetic conditions (magnitudes of magnetic susceptibility and magnetic flux density), but also on the thermal properties of the solution (thermal conductivity, thermal diffusivity, and viscosity). Therefore the effect of fb becomes dominant on the magnetothermal convection. Active control over the density gradient with temperature will be required to advance heat transfer with the effect of fsc. PMID:27606823

  17. Magnetothermal Convection of Water with the Presence or Absence of a Magnetic Force Acting on the Susceptibility Gradient.

    PubMed

    Maki, Syou

    2016-01-01

    Heat transfer of magnetothermal convection with the presence or absence of the magnetic force acting on the susceptibility gradient (fsc) was examined by three-dimensional numerical computations. Thermal convection of water enclosed in a shallow cylindrical vessel (diameter over vessel height = 6.0) with the Rayleigh-Benard model was adopted as the model, under the conditions of Prandtl number 6.0 and Ra number 7000, respectively. The momentum equations of convection were nondimensionalized, which involved the term of fsc and the term of magnetic force acting on the magnetic field gradient (fb). All the computations resulted in axisymmetric steady rolls. The values of the averaged Nu, the averaged velocity components U, V, and W, and the isothermal distributions and flow patterns were almost completely the same, regardless of the presence or absence of the term of fsc. As a result, we found that the effect of fsc was extremely small, although much previous research emphasized the effect with paramagnetic solutions under an unsteady state. The magnitude of fsc depends not only on magnetic conditions (magnitudes of magnetic susceptibility and magnetic flux density), but also on the thermal properties of the solution (thermal conductivity, thermal diffusivity, and viscosity). Therefore the effect of fb becomes dominant on the magnetothermal convection. Active control over the density gradient with temperature will be required to advance heat transfer with the effect of fsc.

  18. Characteristics of Loess Magnetic Susceptibility and Its Influencing Factors analysis in Hebei Country

    NASA Astrophysics Data System (ADS)

    Yuan, Jie; Cao, Guangchao; Chongyi, E.; Yuan, Youjing; Wu, Chengyong; Yu, Ming; Yang, Rongrong

    2017-11-01

    Taking the loess profile of Hebei countryside area as the research object, the magnetic susceptibility, particle size, SOC and chroma were measured respectively. The following conclusions are drawn from the analysis of the above indicators: Xhf value is between 20.56×10-8 m3 kg-1 and 107.81×10-8 m3 kg-1, Xfd value is between 0.31% and 8.74%. The content of silt (4 ∼ 63μm) is the largest in the particle size composition, followed by the clay content (<4μm), the sand content (>63μm) is the least. The SOC content of the whole profile was less, with an average of 8.69 g / kg. Among the chroma values, a* is between 6.65 and 10.3, L* is between 43.34 and 63.79, and b* is between 15.66 and 22.58. The correlation analysis showed that the correlation between grain size and Xhf was not significant (P>0.05), but has a significant correlation with Xfd (P<0.01) SOC has a significant correlation with magnetic susceptibility (P<0.01) There was a significant positive correlation between Xhf and chromaticity (P<0.01), but there was no correlation between Xfd (P>0.05).

  19. Magnetic Susceptibility Measurements as a Proxy for Hydrocarbon Biodegradation

    NASA Astrophysics Data System (ADS)

    Mewafy, F.; Atekwana, E. A.; Slater, L. D.; Werkema, D.; Revil, A.; Ntarlagiannis, D.; Skold, M.

    2011-12-01

    Magnetic susceptibility (MS) measurements have been commonly used in paleoclimate studies, as a proxy for environmental pollution such as heavy metal contamination, and for delineating zones of oil seeps related to hydrocarbon exploration. Few studies have assessed the use of MS measurements for mapping zones of oil pollution. In this study, we investigated the variation in magnetic susceptibility across a hydrocarbon contaminated site undergoing biodegradation. Our objective was to investigate if MS measurements could be used as a proxy indicator of intrinsic bioremediation linked to the activity of iron reducing bacteria. An improved understanding of the mechanisms generating geophysical signatures associated with microbial enzymatic activity could permit the development of geophysical imaging technologies for long-term, minimally invasive and sustainable monitoring of natural biodegradation at oil spill sites. We used a Bartington MS probe to measure MS data along fifteen boreholes within contaminated (both free phase and dissolved phase hydrocarbon plumes) and clean areas. Our results show the following: (1) an enhanced zone of MS straddling the water table at the contaminated locations, not observed at the clean locations; (2) MS values within the free product plume are higher compared to values within the dissolved product plume; (3) the MS values within the vadoze zone above the free product plume are higher compared to values within the dissolved product plume; 4) the zone of high MS is thicker within the free product plume compared to the dissolved product plume. We suggest that the zone of enhanced MS results from the precipitation of magnetite related to the oxidation of the hydrocarbons coupled to iron reduction. Our data documents a strong correlation between MS and hydrocarbon concentration. We conclude that recognition of these zones of enhanced magnetite formation allows for the application of MS measurements as a: (1) low cost, rapid monitoring

  20. Beam ion susceptibility to loss in NSTX-U plasmas

    NASA Astrophysics Data System (ADS)

    Darrow, Douglass; Fredrickson, Eric; Podesta, Mario; Liu, Deyong; White, Roscoe

    2016-10-01

    NSTX-U has operated with three additional neutral beam sources whose tangency radii of 1.1, 1.2, and 1.3 m are significantly larger than the 0.5, 0.6, and 0.7 m tangency radii of the neutral beams previously used in NSTX. These latter beams have also be retained for NSTX-U. Here, we present an estimate of the susceptibility of the beam ions from all the various sources to loss under a range of NSTX-U plasma conditions. This estimation is based upon TRANSP calculations of beam ion deposition in phase space, and the location of the FLR-corrected loss boundary in that phase space. Since losses are often observed at the injection energy, a simple measure of loss susceptibility is the change in canonical toroidal momentum required to move beam ions from their deposition point to the loss boundary, as a function of magnetic moment. To augment this simple estimate, we intend to report some associated transport coefficients of beam ions due to AE activity. Work supported by U.S. DOE DE-AC0209CH11466, DE-FG02-06ER54867, and DE-FG03-02ER54681.

  1. Magnetic properties in polycrystalline and single crystal Ca-doped LaCoO3

    NASA Astrophysics Data System (ADS)

    Zeng, R.; Debnath, J. C.; Chen, D. P.; Shamba, P.; Wang, J. L.; Kennedy, S. J.; Campbell, S. J.; Silver, T.; Dou, S. X.

    2011-04-01

    Polycrystalline (PC) and single crystalline (SC) Ca-doped LaCoO3 (LCCO) samples with the perovskite structure were synthesized by conventional solid-state reaction and the floating-zone growth method. We present the results of a comprehensive investigation of the magnetic properties of the LCCO system. Systematic measurements have been conducted on dc magnetization, ac susceptibility, exchange-bias, and the magnetocaloric effect. These findings suggest that complex structural phases, ferromagnetic (FM), and spin-glass/cluster-spin-glass (CSG), and their transitions exist in PC samples, while there is a much simpler magnetic phase in SC samples. It was also of interest to discover that the CSG induced a magnetic field memory effect and an exchange-bias-like effect, and that a large inverse irreversible magnetocaloric effect exists in this system.

  2. Magnetocaloric effect and slow magnetic relaxation in CsGd(MoO4)2 induced by crystal-field anisotropy

    NASA Astrophysics Data System (ADS)

    Tkáč, V.; Tarasenko, R.; Orendáčová, A.; Orendáč, M.; Sechovský, V.; Feher, A.

    2018-05-01

    The experimental and theoretical study of magnetocaloric effect and magnetic relaxation of the powder sample of CsGd(MoO4)2 were performed. The large conventional magnetocaloric effect was found around 2 K with - ΔSmax ≈ 26.5 J/(kg K) for B = 7 T. AC susceptibility measurement revealed multiple-time scale magnetic relaxation effects on different time scales. Slowest relaxation effect was attributed to the direct process with a bottleneck effect and two faster relaxation processes are effectively temperature independent, probably as a result of averaging in the powder sample.

  3. Magnetic ordering of nickel hydroxide layers 30 Å apart obtained by intercalating dodecyl sulfate

    NASA Astrophysics Data System (ADS)

    Seehra, M. S.; Singh, V.

    2013-09-01

    The nature of magnetic ordering in quasi-2D layered hydroxide of Ni (LH-Ni-DS) with hexagonal structure and synthesized by intercalating dodecyl sulfate (DS) ligand, (C12H25OSO3)-, between the layers using a hydrothermal technique is investigated. The observation of (00l) peaks up to l = 8 in x-ray diffraction on the sample yields an interlayer spacing c ≃ 30.5 Å and a crystallite size ≃ 16 nm. Assignment of the lines observed in the FTIR spectra to the various groups of the DS ligand confirms the intercalation. From the analysis of detailed investigations of the temperature dependence of the magnetization M at different magnetic fields, ac susceptibilities at frequencies from 0.1 to 1 kHz, and electron magnetic resonance spectra at 9.28 GHz, it is concluded that LH-Ni-DS orders ferromagnetically at TC ≃ 23 K. This TC is about 45% higher than TC ≃ 16 K reported for LH-Ni-Ac with c ≃ 8.6 Å obtained by intercalating an acetate ligand between the layers. The roles of the interlayer dipolar interaction, magnetic anisotropy and exchange interactions in determining TC in LH-Ni-L systems for several ligands L yielding different c-axes are discussed.

  4. Simultaneous MR quantification of hepatic fat content, fatty acid composition, transverse relaxation time and magnetic susceptibility for the diagnosis of non-alcoholic steatohepatitis.

    PubMed

    Leporq, B; Lambert, S A; Ronot, M; Vilgrain, V; Van Beers, B E

    2017-10-01

    Non-alcoholic steatohepatitis (NASH) is characterized at histology by steatosis, hepatocyte ballooning and inflammatory infiltrates, with or without fibrosis. Although diamagnetic material in fibrosis and inflammation can be detected with quantitative susceptibility imaging, fatty acid composition changes in NASH relative to simple steatosis have also been reported. Therefore, our aim was to develop a single magnetic resonance (MR) acquisition and post-processing scheme for the diagnosis of steatohepatitis by the simultaneous quantification of hepatic fat content, fatty acid composition, T 2 * transverse relaxation time and magnetic susceptibility in patients with non-alcoholic fatty liver disease. MR acquisition was performed at 3.0 T using a three-dimensional, multi-echo, spoiled gradient echo sequence. Phase images were unwrapped to compute the B 0 field inhomogeneity (ΔB 0 ) map. The ΔB 0 -demodulated real part images were used for fat-water separation, T 2 * and fatty acid composition quantification. The external and internal fields were separated with the projection onto dipole field method. Susceptibility maps were obtained after dipole inversion from the internal field map with single-orientation Bayesian regularization including spatial priors. Method validation was performed in 32 patients with biopsy-proven, non-alcoholic fatty liver disease from which 12 had simple steatosis and 20 NASH. Liver fat fraction and T 2 * did not change significantly between patients with simple steatosis and NASH. In contrast, the saturated fatty acid fraction increased in patients with NASH relative to patients with simple steatosis (48 ± 2% versus 44 ± 4%; p < 0.05) and the magnetic susceptibility decreased (-0.30 ± 0.27 ppm versus 0.10 ± 0.14 ppm; p < 0.001). The area under the receiver operating characteristic curve for magnetic susceptibility as NASH marker was 0.91 (95% CI: 0.79-1.0). Simultaneous MR quantification of fat content, fatty acid

  5. Pressure measurements with a precision of 0.001 ppm in magnetic fields at low temperatures

    NASA Astrophysics Data System (ADS)

    Miura, Y.; Matsushima, N.; Ando, T.; Kuno, S.; Inoue, S.; Ito, K.; Mamiya, T.

    1993-11-01

    Pressure measurements made by an ac bridge technique with a precision of 0.001 ppm in magnetic fields at low temperatures using a Straty-Adams type gauge are described. In order to improve the sensitivity and the long-term stability of the bridge system, coaxial cables without dielectric insulator were developed, with a small cable capacitance temperature coefficient of the impedance. This pressure measurement system has a sensitivity of dP/P˜5×10-10 and a long-term stability of dP/P˜2.4×10-9 over 18 h. This is especially useful for measurements such as electric and magnetic susceptibility measurements in magnetic fields at low temperatures requiring a high precision.

  6. Preliminary AMS Study in Cretaceous Igneous Rocks of Valle Chico Complex, Uruguay: Statistical Determination of Magnetic Susceptibility

    NASA Astrophysics Data System (ADS)

    Barcelona, H.; Mena, M.; Sanchez-Bettucci, L.

    2009-05-01

    The Valle Chico Complex, at southeast Uruguay, is related Paraná-Etendeka Province. The study involved basaltic lavas, quarz-syenites, and rhyolitic and trachytic dikes. Samples were taken from 18 sites and the AMS of 250 specimens was analyzed. The AMS is modeled by a second order tensor K and it graphical representation is a symmetric ellipsoid. The axes relations determine parameters which describe different properties like shape, lineation, and foliation, degree of anisotropy and bulk magnetic susceptibility. Under this perspective, one lava, dike, or igneous body can be considered a mosaic of magnetic susceptibility domains (MSD). The DSM is an area with specific degree of homogeneity in the distribution of parameters values and cinematic conditions. An average tensor would weigh only one MSD, but if the site is a mosaic, subsets of specimens with similar parameters can be created. Hypothesis tests can be used to establish parameter similarities. It would be suitable considered as a MSD the subsets with statistically significant differences in at least one of its means parameters, and therefore, be treated independently. Once defined the MSDs the tensor analysis continues. The basalt-andesitic lavas present MSD with an NNW magnetic foliation, dipping 10. The K1 are sub-horizontal, oriented E-W and reprsent the magmatic flow direction. The quartz-syenites show a variable magnetic fabric or prolate ellipsoids mayor axes dispose parallel to the flow direction (10 to the SSE). Deformed syenites show N300/11 magnetic foliation, consistent with the trend of fractures. The K1 is subvertical. The MSD defined in rhyolitic dikes have magnetic foliations consistent with the structural trend. The trachytic dikes show an important indetermination in the magnetic response. However, a 62/N90 magnetic lineation was defined. The MSDs obtained are consistent with the geological structures and contribute to the knowledge of the tectonic, magmatic and kinematic events.

  7. Structure and magnetic properties of an unprecedented syn-anti μ-nitrito-1κO:2κO' bridged Mn(III)-salen complex and its isoelectronic and isostructural formate analogue.

    PubMed

    Kar, Paramita; Biswas, Rituparna; Drew, Michael G B; Ida, Yumi; Ishida, Takayuki; Ghosh, Ashutosh

    2011-04-07

    The preparation, crystal structures and magnetic properties of two new isoelectronic and isomorphous formate- and nitrite-bridged 1D chains of Mn(III)-salen complexes, [Mn(salen)(HCOO)](n) (1) and [Mn(salen)(NO(2))](n) (2), where salen is the dianion of N,N'-bis(salicylidene)-1,2-diaminoethane, are presented. The structures show that the salen ligand coordinates to the four equatorial sites of the metal ion and the formate or nitrite ions coordinate to the axial positions to bridge the Mn(III)-salen units through a syn-antiμ-1κO:2κO' coordination mode. Such a bridging mode is unprecedented in Mn(III) for formate and in any transition metal ion for nitrite. Variable-temperature magnetic susceptibility measurements of complexes 1 and 2 indicate the presence of ferromagnetic exchange interactions with J values of 0.0607 cm(-1) (for 1) and 0.0883 cm(-1) (for 2). The ac measurements indicate negligible frequency dependence for 1 whereas compound 2 exhibits a decrease of χ(ac)' and a concomitant increase of χ(ac)'' on elevating frequency around 2 K. This finding is an indication of slow magnetization reversal characteristic of single-chain magnets or spin-glasses. The μ-nitrito-1κO:2κO' bridge seems to be a potentially superior magnetic coupler to the formate bridge for the construction of single-molecule/-chain magnets as its coupling constant is greater and the χ(ac)' and χ(ac)'' show frequency dependence. © The Royal Society of Chemistry 2011

  8. A novel Ni(4) complex exhibiting microsecond quantum tunneling of the magnetization.

    PubMed

    Aromí, Guillem; Bouwman, Elisabeth; Burzurí, Enrique; Carbonera, Chiara; Krzystek, J; Luis, Fernando; Schlegel, Christoph; van Slageren, Joris; Tanase, Stefania; Teat, Simon J

    2008-01-01

    A highly asymmetric Ni(II) cluster [Ni(4)(OH)(OMe)(3)(Hphpz)(4)(MeOH)(3)](MeOH) (1) (H(2)phpz=3-methyl-5-(2-hydroxyphenyl)pyrazole) has been prepared and its structure determined by means of single-crystal X-ray diffraction by using synchrotron radiation. Variable-temperature bulk-magnetization measurements show that the complex exhibits intramolecular-ferromagnetic interactions leading to a spin ground state S=4 with close-lying excited states. Magnetization and high-frequency EPR measurements suggest the presence of sizable Ising-type magnetic anisotropy, with zero-field splitting parameters D=-0.263 cm(-1) and E=0.04 cm(-1) for the spin ground state, and an isotropic g value of 2.25. The presence of both axial and transverse anisotropy was confirmed through low-temperature specific heat determinations down to 300 mK, but no slow relaxation of the magnetization was observed by AC measurements down to 1.8 K. Interestingly, AC susceptibility measurements down to temperatures as low as 23 mK showed no indication of slow relaxation of the magnetization in 1. Thus, despite the presence of an anisotropy barrier (U approximately 4.21 cm(-1) for the purely axial limit), the magnetization relaxation remains extremely fast down to the lowest temperatures. The estimated quantum tunneling rate, Gamma>0.667 MHz, makes this complex a prime candidate for observation of coherent tunneling of the magnetization.

  9. The effect of boron doping on crystal structure, magnetic properties and magnetocaloric effect of DyCo 2

    DOE PAGES

    Wang, C. L.; Liu, J.; Mudryk, Y.; ...

    2015-12-19

    In this study, the magnetic properties and magnetic entropy changes of DyCo 2B x (x=0, 0.05, 0.1, and 0.2) alloys were investigated. The Curie temperature (TC) increases with increasing B concentration. The frequency dependence of ac magnetic susceptibility of DyCo 2 caused by the narrow domain wall pinning effect is depressed by B doping, but the coercivity and the magnetic viscosity are prominently increased in the B doped alloys. The magnetic transition nature of DyCo 2B x changes from the first-order to the second-order with increasing x, which leads to the decrease of the maximum magnetic entropy change. However, themore » relative cooling power (RCP) of DyCo 2 and the B doped alloys remains nearly constant.« less

  10. Anisotropy of magnetic susceptibility versus lattice- and shape-preferred orientation in the Lac Tio hemo-ilmenite ore body (Grenville province, Quebec)

    NASA Astrophysics Data System (ADS)

    Bolle, Olivier; Charlier, Bernard; Bascou, Jérôme; Diot, Hervé; McEnroe, Suzanne A.

    2014-08-01

    The Lac Tio hemo-ilmenite ore body crops out in the outer portion of the 1.06 Ga Lac Allard anorthosite, a member of the Havre-Saint-Pierre anorthosite suite from the Grenville province of North America. It is made up of ilmenitite (commonly with more than 95% hemo-ilmenite) associated with noritic lithologies and anorthosite. The present study compares the magnetic fabric of the ore body, as deduced from anisotropy of magnetic susceptibility (AMS) measurements, with the crystallographic and shape fabrics, obtained from lattice-preferred orientation (LPO) and shape-preferred orientation (SPO) measurements made using electron backscattered diffraction (EBSD) and 3D image analysis, respectively. Room-temperature hysteresis measurements, thermomagnetic curves and values of the bulk magnetic susceptibility reveal a magnetic mineralogy dominated by a mixed contribution of hemo-ilmenite and magnetite. The hemo-ilmenite grains display a LPO characterized by a strong preferred orientation of the basal (0001) plane of ilmenite along which hematite was exsolved. This LPO and the magnetic fabric fit well (angle between the crystallographic c-axis and the axis of minimum susceptibility ≤ ca. 15° for most samples), and the latter is thus strongly influenced by the hemo-ilmenite magneto-crystalline anisotropy. A magnetite SPO, concordant with the hemo-ilmenite LPO, may also influence and even dominate the magnetic fabric. The rock shape fabric is coaxial with the magnetic fabric that can thus be used to perform detailed structural mapping. Interpretation of the magnetic fabric and field structural data suggests that the Lac Tio ore body would be a sag point at the margin of the Lac Allard anorthosite, deformed by ballooning during the final stage of diapiric emplacement of the anorthosite body.

  11. A Lorentz model for weak magnetic field bioeffects: part I--thermal noise is an essential component of AC/DC effects on bound ion trajectory.

    PubMed

    Muehsam, David J; Pilla, Arthur A

    2009-09-01

    We have previously employed the Lorentz-Langevin model to describe the effects of weak exogenous magnetic fields via the classical Lorentz force on a charged ion bound in a harmonic oscillator potential, in the presence of thermal noise forces. Previous analyses predicted that microT-range fields give rise to a rotation of the oscillator orientation at the Larmor frequency and bioeffects were based upon the assumption that the classical trajectory of the bound charge itself could modulate a biochemical process. Here, it is shown that the thermal component of the motion follows the Larmor trajectory. The results show that the Larmor frequency is independent of the thermal noise strength, and the motion retains the form of a coherent oscillator throughout the binding lifetime, rather than devolving into a random walk. Thermal equilibration results in a continual increase in the vibrational amplitude of the rotating oscillator towards the steady-state amplitude, but does not affect the Larmor orbit. Thus, thermal noise contributes to, rather than inhibits, the effect of the magnetic field upon reactivity. Expressions are derived for the ensemble average of position and the velocity of the thermal component of the oscillator motion. The projection of position and velocity onto a Cartesian axis measures the nonuniformity of the Larmor trajectory and is illustrated for AC and combined AC/DC magnetic fields, suggesting a means of interpreting resonance phenomena. It is noted that the specific location and height of resonances are dependent upon binding lifetime and initial AC phase.

  12. Track of fluid paleocirculation in dolomite host rock at regional scale by the Anisotropy of Magnetic Susceptibility (AMS): An example from Aptian carbonates of La Florida, Northern Spain

    NASA Astrophysics Data System (ADS)

    Essalhi, Mourad; Sizaret, Stanislas; Barbanson, Luc; Chen, Yan; Branquet, Yannick; Panis, Dominique; Camps, Pierre; Rochette, Pierre; Canals, Angels

    2009-01-01

    The present study aims to apply the AMS method (Anisotropy of Magnetic Susceptibility) at a regional scale to track the fluid circulation direction that has produced an iron metasomatism within pre-existing dolomite host rock. The Urgonian formations hosting the Zn-Pb mineralizations in La Florida (Cantabria, northern Spain) have been taken as target for this purpose. Sampling was carried out, in addition to ferroan dolomite host rock enclosing the Zn-Pb mineralizations, in dolomite host rock and limestone to make the comparison possible between magnetic signals from mineralized rocks, where fluid circulation occurred, and their surrounding formations. AMS study was coupled with petrofabric analysis carried out by texture goniometry, Scanning Electron Microscopy (SEM) observations and also Shape Preferred Orientation (SPO) statistics. SEM observations of ferroan dolomite host rock illustrate both bright and dark grey ribbons corresponding respectively to Fe enriched and pure dolomites. SPO statistics applied on four images from ferroan dolomite host rock give a well-defined orientation of ribbons related to the intermediate axis of magnetic susceptibility K2. For AMS data, two magnetic fabrics are observed. The first one is observed in ferroan dolomite host rock and characterized by a prolate ellipsoid of magnetic susceptibility with a vertical magnetic lineation. The magnetic susceptibility carrier is Fe-rich dolomite. These features are probably acquired during metasomatic fluid circulations. In Fe-rich dolomite host rock, ‹ c› axes are vertical. As a rule, (0001) planes (i.e. planes perpendicular to ‹ c› axes) are isotropic with respect to crystallographic properties. So, the magnetic anisotropy measured in this plane should reflect crystallographic modification due to fluid circulation. This is confirmed by the texture observed using the SEM. Consequently, AMS results show a dominant NE-SW elongation interpreted as the global circulation direction and a

  13. Superconducting-magnetic heterostructures: a method of decreasing AC losses and improving critical current density in multifilamentary conductors

    NASA Astrophysics Data System (ADS)

    Glowacki, B. A.; Majoros, M.

    2009-06-01

    Magnetic materials can help to improve the performance of practical superconductors on the macroscale/microscale as magnetic diverters and also on the nanoscale as effective pinning centres. It has been established by numerical modelling that magnetic shielding of the filaments reduces AC losses in self-field conditions due to decoupling of the filaments and, at the same time, it increases the critical current of the composite. This effect is especially beneficial for coated conductors, in which the anisotropic properties of the superconductor are amplified by the conductor architecture. However, ferromagnetic coatings are often chemically incompatible with YBa2Cu3O7 and (Pb,Bi)2Sr2Ca2Cu3O9 conductors, and buffer layers have to be used. In contrast, in MgB2 conductors an iron matrix may remain in direct contact with the superconducting core. The application of superconducting-magnetic heterostructures requires consideration of the thermal and electromagnetic stability of the superconducting materials used. On one hand, magnetic materials reduce the critical current gradient across the individual filaments but, on the other hand, they often reduce the thermal conductivity between the superconducting core and the cryogen, which may cause destruction of the conductor in the event of thermal instability. A possible nanoscale method of improving the critical current density of superconducting conductors is the introduction of sub-micron magnetic pinning centres. However, the volumetric density and chemical compatibility of magnetic inclusions has to be controlled to avoid suppression of the superconducting properties.

  14. Boosted Hyperthermia Therapy by Combined AC Magnetic and Photothermal Exposures in Ag/Fe3O4 Nanoflowers.

    PubMed

    Das, R; Rinaldi-Montes, N; Alonso, J; Amghouz, Z; Garaio, E; García, J A; Gorria, P; Blanco, J A; Phan, M H; Srikanth, H

    2016-09-28

    Over the past two decades, magnetic hyperthermia and photothermal therapy are becoming very promising supplementary techniques to well-established cancer treatments such as radiotherapy and chemotherapy. These techniques have dramatically improved their ability to perform controlled treatments, relying on the procedure of delivering nanoscale objects into targeted tumor tissues, which can release therapeutic killing doses of heat either upon AC magnetic field exposure or laser irradiation. Although an intense research effort has been made in recent years to study, separately, magnetic hyperthermia using iron oxide nanoparticles and photothermal therapy based on gold or silver plasmonic nanostructures, the full potential of combining both techniques has not yet been systematically explored. Here we present a proof-of-principle experiment showing that designing multifunctional silver/magnetite (Ag/Fe3O4) nanoflowers acting as dual hyperthermia agents is an efficient route for enhancing their heating ability or specific absorption rate (SAR). Interestingly, the SAR of the nanoflowers is increased by at least 1 order of magnitude under the application of both an external magnetic field of 200 Oe and simultaneous laser irradiation. Furthermore, our results show that the synergistic exploitation of the magnetic and photothermal properties of the nanoflowers reduces the magnetic field and laser intensities that would be required in the case that both external stimuli were applied separately. This constitutes a key step toward optimizing the hyperthermia therapy through a combined multifunctional magnetic and photothermal treatment and improving our understanding of the therapeutic process to specific applications that will entail coordinated efforts in physics, engineering, biology, and medicine.

  15. A neutral molecular-based layered magnet [Fe(C2O4)(CH3OH)]n exhibiting magnetic ordering at TN approximately 23 K.

    PubMed

    Zhang, Bin; Zhang, Yan; Zhang, Jinbiao; Li, Junchao; Zhu, Daoben

    2008-10-07

    Solvothermal synthesis of FeCl(2).4H2O and H2C2O(4).2H2O in methanol at 120 degrees C yielded yellow plate-like crystals of [Fe(C2O4)(CH3OH)]n. Each iron atom is in a distorted octahedral environment, being bonded to four oxygen atoms from two bisbidentate oxalate anions, one O atom of a chelating oxalate anion and one O atom from a methanol molecule as an oxalate group bridging ligand in a five-coordination mode. The neutral layer of [Fe(C2O4)(CH3OH)]n with a [4,4] net along the ac plane. There is no interaction between layers. A long range magnetic ordering with spin canting at TN approximately 23 K was observed and confirmed by AC susceptibility measurements.

  16. A kinetic model to explain the grain size and organic matter content dependence of magnetic susceptibility in transitional marine environments: A case study in Ria de Muros (NW Iberia)

    NASA Astrophysics Data System (ADS)

    Mohamed, Kais J.; Andrade, Alba; Rey, Daniel; Rubio, Belén.; Bernabeu, Ana María.

    2017-06-01

    Magnetic minerals in marine sediments are sensitive indicators of processes such as provenance changes, climatic controls, pollution, and postdepositional geochemical changes. Magnetic susceptibility is the bulk property of the sediments most commonly used to understand the magnetic characteristics of sediments. Before conclusions can be drawn from changes in this parameter, it is important to understand what factors and to what extent control changes in magnetic susceptibility. The magnetic susceptibility of surficial sediments in the Galician Rias Baixas, in NW Spain, has been shown to covary with sediment texture and organic matter content. Downcore, the magnetic properties of these sediments experience drastic changes as a result of strong dissolution caused by early diagenesis. In this paper, we further explore the relationship between these factors and formalize the observed covariations as the result of a simple second-order kinetic model dependent on the content of organic matter in surficial sediments in the Ria de Muros. The reanalysis of previously reported data from the Rias de Vigo and Pontevedra confirmed the validity of this model and suggested further controls such as wave climate and water depth in the rates at which magnetic susceptibility changes are controlled by organic matter content.

  17. Comments on 'Anisotropic magnetic susceptibility in the continental lower crust and its implication for the shape of magnetic anomalies' by G. Florio et al.

    NASA Astrophysics Data System (ADS)

    Rochette, P.

    1994-12-01

    In their letter Lorio et al. (1993) recently explored the likelihood that the deflection with respect to present day magnetic North of dipolar lower crustal magnetic anomalies are caused by an induced magnetization deflected by strong anisotropy of magnetic susceptibility (AMS) rather than the usual explanation of an ancient natural remanent magnetization of a rotated body. Such an alternative would solve the theoretical problems raised by the stability of Natural Remanent Magnetization (NRM) at high temperature in the usually coarse grained magnetite bearing source rocks necessary to create large magnetic anomalies (Shive, 1989). They present a case study of two deep anomalies in southern Italy where the deflection is 30 to 40 deg. From a model of an anisotropic cubic source and an AMS dataset from representative deep crustal rocks from various part of the world, they conclude that no significant deflection of anomaly axis can be due to the average anisotropy ratio P(prime) = 1.5 observed in the dataset.

  18. Resistivity and magnetic susceptibility studies of Tl[sub m]Ca[sub n[minus]1]Ba[sub 2]Cu[sub n]O[sub y] before and after doping with LiF

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    El-Hamalawy, A.A.; El-Zaidia, M.M.; Ammar, A.A.

    1993-04-01

    Measurements of the superconducting resistance as a function of temperature were performed using the conventional four-probe method. The transition to complete superconductivity was recorded for samples of (Tl[sub 2]Ca[sub 2]Ba[sub 2]Cu[sub 3]O[sub 10])[sub 100[minus]x]LiF[sub x] (2223) mixed with different LiF ratios x = 0, 2, 4, 5, 6, 8, 10, and 12wt.%. It was found that the transition temperature T[sub c] was increased up to 5 wt.% of LiF. Further addition of LiF decreases T[sub c]. Therefore, 5 wt.% LiF is the optimum concentration giving a transition temperature of 130 K. Measurements of the superconducting resistance of all the samplesmore » except the (1111) compound show that the addition of 5 wt.% LiF increases T[sub c] and decreases the metastable phases. The real part of the a.c. magnetic susceptibility [chi][sub a.c.] is studied using a zero-field cooled mechanism. The temperature dependence of [chi][sub a.c.] for the prepared TlBaCaCuO having stoichiometric composition of (1111), (2223), (2234), and (3245) and that after doping with 5 wt.% LiF showed a broad feature. The transition to the complete diamagnetic state takes place in a broad transition region containing many transition steps, indicating the presence of metastable phases. The addition of LiF decreases the fluctuation in the transition region and its effect in reducing the number of multiphases. 29 refs., 10 refs.« less

  19. Dimensionality of superconductivity in the layered organic material EtMe3P [Pd(dmit)2] 2 under pressure

    NASA Astrophysics Data System (ADS)

    Yamamoto, R.; Yanagita, Y.; Namaizawa, T.; Komuro, S.; Furukawa, T.; Itou, T.; Kato, R.

    2018-06-01

    We measured the ac magnetic susceptibility for the layered organic superconductor EtMe3P [Pd(dmit)2] 2 under pressure with a dc magnetic field applied perpendicular to the ac field. We investigated the dc field dependence of the ac susceptibility in detail and concluded that the superconductivity in EtMe3P [Pd(dmit)2] 2 is an anisotropic three-dimensional superconductivity even at low temperatures, which contrasts with the large majority of other correlated electron layered superconductors such as high-Tc cuprate and κ -(ET) 2X systems.

  20. Relationships between magnetic susceptibility and heavy metals in urban topsoils in the arid region of Isfahan, central Iran

    NASA Astrophysics Data System (ADS)

    Karimi, Rezvan; Ayoubi, Shamsollah; Jalalian, Ahmad; Sheikh-Hosseini, Ahmad Reza; Afyuni, Majid

    2011-05-01

    Recently methods dealing with magnetometry have been proposed as a proper proxy for assessing the heavy metal pollution of soils. A total of 113 topsoil samples were collected from public parks and green strips along the rim of roads with high-density traffic within the city of Isfahan, central Iran. The magnetic susceptibility (χ) of the collected soil samples was measured at both low and high frequency (χlf and χhf) using the Bartington MS2 dual frequency sensor. As, Cd, Cr, Ba, Cu, Mn, Pb, Zn, Sr and V concentrations were measured in the all collected soil samples. Significant correlations were found between Zn and Cu (0.85) and between Zn and Pb (0.84). The χfd value of urban topsoil varied from 0.45% to 7.7%. Low mean value of χfd indicated that the magnetic properties of the samples are predominately contributed by multi-domain grains, rather than by super-paramagnetic particles. Lead, Cu, Zn, and Ba showed positive significant correlations with magnetic susceptibility, but As, Sr, Cd, Mn, Cr and V, had no significant correlation with the magnetic susceptibility. There was a significant correlation between pollution load index (PLI) and χlf. PLI was computed to evaluate the soil environmental quality of selected heavy metals. Moreover, the results of multiple regression analysis between χlf and heavy metal concentrations indicated the LnPb, V and LnCu could explain approximately 54% of the total variability of χlf in the study area. These results indicate the potential of the magnetometric methods to evaluate the heavy metal pollution of soils.

  1. Temperature-dependency of Magnetic Susceptibility U Advantages and Limits For Magneto-mineralogical Studies

    NASA Astrophysics Data System (ADS)

    Kontny, A.

    Low-field magnetic susceptibility measurements in the temperature range U192 to 700 C (k(T)) are a widely applied method used for the identification of magnetic phases and characteristic magnetic phase transitions. One of the advantages of this method is the precise determination of titanomagnetite composition independently from grain size. However, the interpretations of k(T)-curves often are discussed controversially because other effects like grain size or the occurrence of more than one magnetic phase complicate the courses. Case studies from the titanomagnetite and titanohe- matite solid solution series including pure magnetite and hematite will be presented and variations in chemical composition, alteration and grain size will be discussed in relation to their geological significance. (1) In subaerially extruded basaltic lava differences in the low-temperature legs of the k(T) curves indicate variations in the degree of high-temperature (deuteric) oxidation of titanomagnetite. This alteration to magnetite-rich titanomagnetite is accompanied by a grain size reduction, which can be correlated with the development of a susceptibility peak at about U160 C. Fur- ther oxidation transforms the titanomagnetite into titanohematite which again results in a characteristic k(T) behavior at low temperatures with a decrease in k with in- creasing temperature (2) Hydrothermal alteration from magnetite to hematite creates a hematite phase that cannot be seen in k(T)-curves. However, hematite that is grown in sediments, can be identified by its Tc. Therefore it is assumed that crystallinity of magnetic phases seems to play a significant role to explain a different behaviour. (3) Submarine basalts rapidly quenched from high temperatures often show wide anti- clines in the k(T)-curves which can be correlated with a range of chemical composition and grain sizes, including small amounts of pure magnetite. This feature is commonly attributed to low-temperature alteration of single

  2. Magnetic susceptibility and heat-capacity studies of NiS2-xSex single crystals: A study of transitions at nonzero temperature

    NASA Astrophysics Data System (ADS)

    Yao, X.; Kuo, Y.-K.; Powell, D. K.; Brill, J. W.; Honig, J. M.

    1997-09-01

    Heat-capacity and magnetic-susceptibility studies have been carried out on NiS2-xSex single crystals for 0.38<=x<=0.58 and 0<=x<=0.71, respectively. These and earlier physical measurements document the gradual evolution, with rising x, of the alloys from good insulators to poor metals at low temperatures. The transitions between various magnetically ordered or disordered phases are marked by anomalies in these physical measurements. The trend of magnetic susceptibility with temperature indicates that alloys near the crossover to the highly correlated metallic state exhibit increasing charge-carrier localization with rising temperature; this is ascribed to the dominance of entropic contributions to the free energy. It is stressed that these variations in properties are achieved by isoelectronic substitutions in the anion sublattice that leave the cation sublattice undisturbed.

  3. Evidence for short-range magnetic order in the nematic phase of FeSe from anisotropic in-plane magnetostriction and susceptibility measurements

    NASA Astrophysics Data System (ADS)

    He, Mingquan; Wang, Liran; Hardy, Frédéric; Xu, Liping; Wolf, Thomas; Adelmann, Peter; Meingast, Christoph

    2018-03-01

    The nature of the nematic state in FeSe remains one of the major unsolved mysteries in Fe-based superconductors. Both spin and orbital physics have been invoked to explain the origin of this phase. Here we present experimental evidence for frustrated, short-range magnetic order, as suggested by several recent theoretical works, in the nematic state of FeSe. We use a combination of magnetostriction, susceptibility, and resistivity measurements to probe the in-plane anisotropies of the nematic state and its associated fluctuations. Despite the absence of long-range magnetic order in FeSe, we observe a sizable in-plane magnetic susceptibility anisotropy, which is responsible for the field-induced in-plane distortion inferred from magnetostriction measurements. Further we demonstrate that all three anisotropies in FeSe are very similar to those of BaFe2As2 , which strongly suggests that the nematic phase in FeSe is also of magnetic origin.

  4. Pressure effect on magnetic susceptibility of LaCoO3

    NASA Astrophysics Data System (ADS)

    Panfilov, A. S.; Grechnev, G. E.; Zhuravleva, I. P.; Lyogenkaya, A. A.; Pashchenko, V. A.; Savenko, B. N.; Novoselov, D.; Prabhakaran, D.; Troyanchuk, I. O.

    2018-04-01

    The effect of pressure on magnetic properties of LaCoO3 is studied experimentally and theoretically. The pressure dependence of magnetic susceptibility χ of LaCoO3 is obtained by precise measurements of χ as a function of the hydrostatic pressure P up to 2 kbar in the temperature range from 78 K to 300 K. A pronounced magnitude of the pressure effect is found to be negative in sign and strongly temperature dependent. The obtained experimental data are analysed by using a two-level model and DFT+U calculations of the electronic structure of LaCoO3. In particular, the fixed spin moment method was employed to obtain a volume dependence of the total energy difference Δ between the low spin and the intermediate spin states of LaCoO3. Analysis of the obtained experimental χ(P) dependence within the two-level model, as well as our DFT+U calculations, have revealed the anomalous large decrease in the energy difference Δ with increasing of the unit cell volume. This effect, taking into account a thermal expansion, can be responsible for the temperatures dependence of Δ, predicting its vanishing near room temperature.

  5. Layered copper hydroxide n-alkylsulfonate salts: synthesis, characterization, and magnetic behaviors in relation to the basal spacing.

    PubMed

    Park, Seong-Hun; Lee, Cheol Eui

    2005-01-27

    A series of hybrid inorganic-organic copper(II) hydroxy n-alkylsulfonate with a triangular lattice, Cu(2)(OH)(3)(C(n)H(2)(n)(+1)SO(3)) (n = 6, 8, 10), are prepared by anion exchange, starting from copper hydroxy nitrate Cu(2)(OH)(3)NO(3). These compounds show a layered structure as determined by X-ray diffraction, with interlayer distances of 14.3-34.8 A in alternation with interdigitated bilayer packing. Magnetic properties have been investigated by means of dc and ac measurements. All the compounds show similar metamagnet behaviors, with a Neel temperature of about 11 K. A subtle difference in the ac magnetic susceptibility among the compounds is understood by the existence of hydrogen bonding between the sulfonate headgroup and the hydroxide anion. A detailed molecular structure of the alkyl chains incorporated to the inorganic copper hydroxide layer is also discussed from the FTIR data.

  6. Magnetic characteristics of M2FeV3O11 (M = Mg, Zn, Pb, Co, Ni) compounds

    NASA Astrophysics Data System (ADS)

    Groń, T.; Blonska-Tabero, A.; Filipek, E.; Stokłosa, Z.; Duda, H.; Sawicki, B.

    2018-02-01

    The unusual physical characteristics of the multicomponent oxide systems renewed the interest as the potential cathode materials in high-energy cells. Since the earlier magnetic characteristics were not entirely conclusive, we report the results of dc magnetic measurements including higher harmonics of ac magnetic susceptibility of the M2FeV3O11 (M = Mg, Zn, Pb, Co, Ni) compounds. Ferrimagnetic long-range and antiferromagnetic short-range interactions for all compounds under study at low temperatures as well as superparamagnetic-like behavior with the blocking temperature of 29 K and the freezing parameter of 0.013 were observed. These effects are discussed within the framework of superexchange and double exchange magnetic interactions as well as the mixed valence band of iron ions.

  7. Effect of magnetic dipolar interactions on temperature dependent magnetic hyperthermia in ferrofluids

    NASA Astrophysics Data System (ADS)

    Palihawadana-Arachchige, Maheshika; Nemala, Humeshkar; Naik, Vaman M.; Naik, Ratna

    2017-01-01

    Magnetic hyperthermia (MHT), where localized heating is generated when magnetic nanoparticles (MNPs) are subjected to a radiofrequency magnetic field, has a great potential as a non-invasive cancer therapy treatment. The efficiency of heat generation depends on the magnetic properties of MNPs, such as saturation magnetization (Ms) and magnetic anisotropy (K), as well as the particle size distribution and magnetic dipolar interactions. We have investigated MHT in two Fe3O4 ferrofluids prepared by co-precipitation (CP) and hydrothermal (HT) synthesis methods showing similar physical particle size distribution (14 ± 4 nm) and saturation magnetization (70 ± 2 emu/g of Fe3O4) but very different specific absorption rates (SAR) of ˜110 W/g and ˜40 W/g at room temperature (measured with an ac magnetic field amplitude of 240 Oe and a frequency of 375 kHz). This observed reduction in SAR has been explained by taking into account the dipolar interactions and the distribution of the magnetic core size of MNPs in ferrofluids. The HT ferrofluid shows a higher effective dipolar interaction and a wider distribution of the magnetic core size of MNPs compared to those of the CP ferrofluid. We have fitted the temperature dependent SAR data using the linear response theory, incorporating an effective dipolar interaction, to determine the magnetic anisotropy constant of MNPs prepared by CP (22 ± 2 kJ/m3) and HT (26 ± 2 kJ/m3) synthesis methods. These values are in good agreement with the magnetic anisotropy constant determined using frequency and temperature dependent magnetic susceptibility data obtained on powder samples.

  8. Magnetic resonance characteristics and susceptibility weighted imaging of the brain in gadolinium encephalopathy.

    PubMed

    Samardzic, Dejan; Thamburaj, Krishnamoorthy

    2015-01-01

    To report the brain imaging features on magnetic resonance imaging (MRI) in inadvertent intrathecal gadolinium administration. A 67-year-old female with gadolinium encephalopathy from inadvertent high dose intrathecal gadolinium administration during an epidural steroid injection was studied with multisequence 3T MRI. T1-weighted imaging shows pseudo-T2 appearance with diffusion of gadolinium into the brain parenchyma, olivary bodies, and membranous labyrinth. Nulling of cerebrospinal fluid (CSF) signal is absent on fluid attenuation recovery (FLAIR). Susceptibility-weighted imaging (SWI) demonstrates features similar to subarachnoid hemorrhage. CT may demonstrate a pseudo-cerebral edema pattern given the high attenuation characteristics of gadolinium. Intrathecal gadolinium demonstrates characteristic imaging features on MRI of the brain and may mimic subarachnoid hemorrhage on susceptibility-weighted imaging. Identifying high dose gadolinium within the CSF spaces on MRI is essential to avoid diagnostic and therapeutic errors. Copyright © 2013 by the American Society of Neuroimaging.

  9. A new approach for AC loss reduction in HTS transformer using auxiliary windings, case study: 25 kA HTS current injection transformer

    NASA Astrophysics Data System (ADS)

    Heydari, Hossein; Faghihi, Faramarz; Aligholizadeh, Reza

    2008-01-01

    AC loss is one of the important parameters in HTS (high temperature superconducting) AC devices. Among the HTS AC power devices, the transformer is an essential part in the electrical power system. The AC losses in an HTS tape depend on the magnetic field. One of the techniques usually adopted to mitigate the unwanted magnetic field is using a system of coils that produce a magnetic field opposite to the incident one, reducing the total magnetic field. In this paper adding two auxiliary windings to the HTS transformer to produce this opposite magnetic field is proposed. The proper use of these auxiliary windings could reduce the leakage flux and, therefore, the AC loss. A mathematical model is used to describe the behaviour of a transformer operating with auxiliary windings, based on the theory of electromagnetic coupled circuits. The influence of the auxiliary windings on the leakage field is studied by the finite element method (FEM) and the AC loss of an HTS transformer was calculated. Also, the simulation results show that employing auxiliary windings will improve the HTS transformer efficiency.

  10. Noncontact technique for measuring the electrical resistivity and magnetic susceptibility of electrostatically levitated materials

    NASA Astrophysics Data System (ADS)

    Rustan, G. E.; Spyrison, N. S.; Kreyssig, A.; Prozorov, R.; Goldman, A. I.

    2012-10-01

    We describe the development of a new method for measuring the electrical resistivity and magnetic susceptibility of high temperature liquids and solids. The technique combines a tunnel diode oscillator with an electrostatic levitation furnace to perform noncontact measurements on spherical samples 2-3 mm in diameter. The tank circuit of the oscillator is inductively coupled to the sample, and measurements of the oscillator frequency as a function of sample temperature can be translated into changes in the sample's electrical resistivity and magnetic susceptibility. Particular emphasis is given on the need to improve the positional stability of the levitated samples, as well as the need to stabilize the temperature of the measurement coil. To demonstrate the validity of the technique, measurements have been performed on solid spheres of pure zirconium and low-carbon steel. In the case of zirconium, while absolute values of the resistivity were not determined, the temperature dependence of the resistivity was measured over the range of 640-1770 K and found to be in good agreement with literature data. In the case of low-carbon steel, the ferromagnetic-paramagnetic transition was clearly observable and, when combined with thermal data, appears to occur simultaneously with the solid-solid structural transition.

  11. Suppression/Reversal of Natural Convection by Exploiting the Temperature/Composition Dependence of Magnetic Susceptibility

    NASA Technical Reports Server (NTRS)

    Seybert, C. D.; Evans, J. W.; Leslie, F.; Jones, W. K., Jr.

    2000-01-01

    Natural convection, driven by temperature-or concentration gradients or both, is an inherent phenomenon during solidification of materials on Earth. This convection has practical consequences (e.g effecting macrosegregation) but also renders difficult the scientific examination of diffusive/conductive phenomena during solidification. It is possible to halt, or even reverse, natural convection by exploiting the variation (with temperature, for example) of the susceptibility of a material. If the material is placed in a vertical magnetic field gradient, a buoyancy force of magnetic origin arises and, at a critical field gradient, can balance the normal buoyancy forces to halt convection. At higher field gradients the convection can be reversed. The effect has been demonstrated in experiments at Marshall Space Flight Center where flow was measured by PIV in MnCl2 solution in a superconducting magnet. In auxiliary experiments the field in the magnet and the properties of the solution were measured. Computations of the natural convection, its halting and reversal, using the commercial software FLUENT were in good agreement with the measurements.

  12. Evolution of fabric in Chitradurga granite (south India) - A study based on microstructure, anisotropy of magnetic susceptibility (AMS) and vorticity analysis

    NASA Astrophysics Data System (ADS)

    Mondal, Tridib Kumar

    2018-01-01

    In this paper, the fabric in massive granite ( 2.6 Ga) from the Chitradurga region (Western Dharwar Craton, south India) is analyzed using microstructure, anisotropy of magnetic susceptibility (AMS) study and kinematic vorticity analysis. The microstructural investigation on the granite shows a progressive textural overprint from magmatic, through high-T to low-T solid-state deformation textures. The mean magnetic foliation in the rocks of the region is dominantly NW-SE striking which have developed during regional D1/D2 deformation on account of NE-SW shortening. The plunge of the magnetic lineation varies from NW to vertical to SE, and interpreted to be a consequence of regional D3 deformation on account of NW-SE to E-W shortening. The vorticity analysis from magnetic fabric in the region reveals that the NW-SE oriented fabric formed under pure shear condition during D1/D2 regional deformation. However, some parts of the region particularly close to the adjacent Chitradurga Shear Zone show that the magnetic fabrics are oblique to the foliation as well as shear zone orientation and inferred to be controlled by simple shearing during D3 regional deformation. The shape preferred orientation (SPO) analysis from oriented thin sections suggest that the shape of the recrystallized quartz grains define the magnetic fabric in Chitradurga granite and the degree of the SPO reduces away from the Chitradurga Shear Zone. It is interpreted that the change in magnetic fabrics in some parts of the granite in the region are dominantly controlled by the late stage sinistral shearing which occurred during the development of Chitradurga Shear Zone. Anisotropy of magnetic susceptibility (AMS) data of granite from the Chitradurga region (West Dharwar Craton, southern India). Km = Mean susceptibility; Pj = corrected degree of magnetic anisotropy; T = shape parameter. K1 and K3 are the maximum and minimum principal axes of the AMS ellipsoid, respectively. dec = Declination; inc

  13. Resistance to Bacillus thuringiensis Mediated by an ABC Transporter Mutation Increases Susceptibility to Toxins from Other Bacteria in an Invasive Insect

    PubMed Central

    Zhang, Dandan; Gong, Lingling; He, Fei; Soberón, Mario; Bravo, Alejandra; Tabashnik, Bruce E.; Wu, Kongming

    2016-01-01

    Evolution of pest resistance reduces the efficacy of insecticidal proteins from the gram-positive bacterium Bacillus thuringiensis (Bt) used widely in sprays and transgenic crops. Recent efforts to delay pest adaptation to Bt crops focus primarily on combinations of two or more Bt toxins that kill the same pest, but this approach is often compromised because resistance to one Bt toxin causes cross-resistance to others. Thus, integration of Bt toxins with alternative controls that do not exhibit such cross-resistance is urgently needed. The ideal scenario of negative cross-resistance, where selection for resistance to a Bt toxin increases susceptibility to alternative controls, has been elusive. Here we discovered that selection of the global crop pest, Helicoverpa armigera, for >1000-fold resistance to Bt toxin Cry1Ac increased susceptibility to abamectin and spineotram, insecticides derived from the soil bacteria Streptomyces avermitilis and Saccharopolyspora spinosa, respectively. Resistance to Cry1Ac did not affect susceptibility to the cyclodiene, organophospate, or pyrethroid insecticides tested. Whereas previous work demonstrated that the resistance to Cry1Ac in the strain analyzed here is conferred by a mutation disrupting an ATP-binding cassette protein named ABCC2, the new results show that increased susceptibility to abamectin is genetically linked with the same mutation. Moreover, RNAi silencing of HaABCC2 not only decreased susceptibility to Cry1Ac, it also increased susceptibility to abamectin. The mutation disrupting ABCC2 reduced removal of abamectin in live larvae and in transfected Hi5 cells. The results imply that negative cross-resistance occurs because the wild type ABCC2 protein plays a key role in conferring susceptibility to Cry1Ac and in decreasing susceptibility to abamectin. The negative cross-resistance between a Bt toxin and other bacterial insecticides reported here may facilitate more sustainable pest control. PMID:26872031

  14. Measurement of Meteorite Density, Porosity and Magnetic Susceptibility: Fast, Non- destructive, Non-contaminating and Very Informative

    NASA Astrophysics Data System (ADS)

    Macke, R. J.; Britt, D. T.; Consolmagno, G. J.

    2009-05-01

    The development of the "glass bead" method [1] for measuring bulk density, coupled with other fast, non- destructive and non-contaminating methods for measuring grain density and magnetic susceptibility, has enabled broad surveys of large meteorite collections. We have employed these methods extensively on meteorites in numerous collections, including those at the Vatican, the American Museum of Natural History (New York), the National Museum of Natural History (Washington, DC), Texas Christian University, University of New Mexico, and Arizona State University. We present here a summary of some of the findings to date. Using the glass bead method, the meteorite is placed into a container which is then filled entirely with small (sub- millimeter) glass beads. The beads behave collectively as an Archimedean fluid, flowing around the sample to fill the empty space in the container. Through mass measurement, the volume displaced by the sample can be determined. Grain density is determined via helium ideal-gas pycnometry. Magnetic susceptibility is determined using a commercially available hand-held device [2]. Among notable findings to date, grain density and magnetic susceptibility together can distinguish H, L and LL ordinary chondrite falls into clearly distinct groupings [3]. On the other hand, enstatite chondrites of EH and EL subgroups are indistinguishable in these properties, indicating that EH and EL do not differ significantly in iron content [4]. Carbonaceous chondrites can have porosities that are significantly higher than ordinary chondrites and (especially for aqueously altered meteorites) lower density, though these also vary according to subgroups [5]. References: [1] Consolmagno and Britt, 1998. M&PS 33, 1231-1240. [2] Gattacceca et al., 2004. GJI 158, 42-49. [3] Consolmagno et al., 2006. M&PS 41, 331-342. [4] Macke et al., 2009. LPSC 40, 1598. [5] Consolmagno et al., 2008. MetSoc 71, 5038.

  15. The midgut cadherin-like gene is not associated with resistance to Bacillus thuringiensis toxin Cry1Ac in Plutella xylostella (L.).

    PubMed

    Guo, Zhaojiang; Kang, Shi; Zhu, Xun; Wu, Qingjun; Wang, Shaoli; Xie, Wen; Zhang, Youjun

    2015-03-01

    The Gram-positive bacterium Bacillus thuringiensis (Bt) produces Cry toxins that have been used to control important agricultural pests. Evolution of resistance in target pests threatens the effectiveness of these toxins when used either in sprayed biopesticides or in Bt transgenic crops. Although alterations of the midgut cadherin-like receptor can lead to Bt Cry toxin resistance in many insects, whether the cadherin gene is involved in Cry1Ac resistance of Plutella xylostella (L.) remains unclear. Here, we present experimental evidence that resistance to Cry1Ac or Bt var. kurstaki (Btk) in P. xylostella is not due to alterations of the cadherin gene. The bona fide P. xylostella cadherin cDNA sequence was cloned and analyzed, and comparisons of the cadherin cDNA sequence among susceptible and resistant P. xylostella strains confirmed that Cry1Ac resistance was independent of mutations in this gene. In addition, real-time quantitative PCR (qPCR) indicated that cadherin transcript levels did not significantly differ among susceptible and resistant P. xylostella strains. RNA interference (RNAi)-mediated suppression of cadherin gene expression did not affect larval susceptibility to Cry1Ac toxin. Furthermore, genetic linkage assays using four cadherin gDNA allelic biomarkers confirmed that the cadherin gene is not linked to resistance against Cry1Ac in P. xylostella. Taken together, our findings demonstrate that Cry1Ac resistance of P. xylostella is independent of the cadherin gene. Copyright © 2015 Elsevier Inc. All rights reserved.

  16. Synthesis and magnetic hyperthermia studies on high susceptible Fe1-xMgxFe2O4 superparamagnetic nanospheres

    NASA Astrophysics Data System (ADS)

    Manohar, A.; Krishnamoorthi, C.

    2017-12-01

    Majority studies on magnetic hyperthermia properties were carried out by modifying the saturation mass magnetization (Ms) of the samples. Here efforts were made to enhance the specific heat generation rate (SHGR) of single domain superparamagnetic (SP) material by modifying its magnetic susceptibility. Well crystallined, inverse spinel structured and close to monosize Fe1-xMgxFe2O4 (x = 0, 0.1, 0.2, 0.3, 0.4, & 0.5) compounds with nanosphere geometry (diameter 10 nm) were synthesized by solvothermal reflux method at ≈ 300 °C . In the literature it is reported that magnesium ferrites synthesized at high temperatures yield mixed (normal & inverse) spinel structures. The inverse spinel structure was confirmed by X-ray powder diffraction (XRPD), lattice vibrations and magnetic characteristics of the compounds. The Ms of the compounds decrease with increase of substituent Mg2+ concentration. Under high excitation energy the inter-valance charge transfer whereas under low excitation energy the intra-valance charge transfer process were predominant. The as-synthesized nanospheres were encapsulated by hydrophobic oleic acid and were exchanged by hydrophilic poly(acrylic acid) by chemical exchange process. Estimated magnetic hyperthermia power or SHGR of the x = 0, 0.3 & 0.5 were 11, 11.4 & 22.4 W per gram of respective compounds, respectively, under 63.4 kA m-1 field amplitude and 126 kHz frequency. The SHGR enhances with Mg2+ concentration though its Ms reduces and is attributed to reduced spin-orbital coupling in the compounds with enhanced Mg2+ concentration. This may pave a new way to develop magnetic hyperthermia material by modifying magnetic susceptibility of the compounds against to the reported Ms modification approach. The obtained high SHGR of the biocompatible compounds could be used in magnetic hyperthermia applications in biomedical field.

  17. Magnetic dynamic properties of electron-doped La(0.23)Ca(0.77)MnO3 nanoparticles.

    PubMed

    Dolgin, B; Puzniak, R; Mogilyansky, D; Wisniewski, A; Markovich, V; Jung, G

    2013-02-20

    Magnetic properties of basically antiferromagnetic La(0.23)Ca(0.77)MnO(3) particles with average sizes of 12 and 60 nm have been investigated in a wide range of magnetic fields and temperature. Particular attention has been paid to magnetization dynamics through measurements of the temperature dependence of ac-susceptibility at various frequencies, the temperature and field dependence of thermoremanent and isothermoremanent magnetization originating from nanoparticles shells, and the time decay of the remanent magnetization. Experimental results and their analysis reveal the major role in magnetic behaviour of investigated antiferromagnetic nanoparticles played by the glassy component, associated mainly with the formation of the collective state formed by ferromagnetic clusters in frustrated coordination at the surfaces of interacting antiferromagnetic nanoparticles. Magnetic behaviour of nanoparticles has been ascribed to a core-shell scenario. Magnetic transitions have been found to play an important role in determining the dynamic properties of the phase separated state of coexisting different magnetic phases.

  18. EPR and Magnetic Susceptibility Studies of Manganese Ions in Bi2O3·CdO Glass Matrix

    NASA Astrophysics Data System (ADS)

    Ardelean, I.; Todor, Ioana; Ciceo-Lucacel, Raluca; Maniu, Dana

    Glasses of the xMnO·(100-x)[Bi2O3·CdO] system with 0magnetic susceptibility measurements. The EPR investigations indicated the compositional domains favorable to isolated manganese ions or to those magnetically clustered. The magnetic measurements evidenced the presence of both Mn2+ and Mn3+ ions, with their relative content depending on the MnO concentration. The prevalence of the dipolar and respectively the superexchange interactions between the manganese ions can be correlated with the relative content of the Mn2+ and Mn3+ species.

  19. AC Loss Minimization in High Temperature Superconductors - U.K.

    DTIC Science & Technology

    2003-11-07

    high currents in high magnetic fields. The DC properties are very attractive, but to reduce the AC losses it is necessary to use a narrow conductor... NiFe in the whole magnetic field region (goHext=0.01 T - 6 T) roughly by a factor of 2, reflecting the sample Jc(B) dependencies. Also the magnetic ...ratio of the tape, there is no visible effect in a parallel magnetic field. Hysteresis losses in metallic substrates - CeO2:Pd/ NiFe and CeO2:Pd/NiCrW

  20. Lack of fitness costs and inheritance of resistance to Bacillus thuringiensis Cry1Ac toxin in a near-isogenic strain of Plutella xylostella (Lepidoptera: Plutellidae).

    PubMed

    Zhu, Xun; Yang, Yanjv; Wu, Qingjun; Wang, Shaoli; Xie, Wen; Guo, Zhaojiang; Kang, Shi; Xia, Jixing; Zhang, Youjun

    2016-02-01

    Resistance to Bacillus thuringiensis (Bt) formulations in insects may be associated with fitness costs. A lack of costs enables resistance alleles to persist, which may contribute to the rapid development and spread of resistance in populations. To assess the fitness costs associated with Bt Cry1Ac resistance in Plutella xylostella, life tables were constructed for a near-isogenic resistant strain (NIL-R) and a susceptible strain in this study. No fitness costs associated with Cry1Ac resistance in NIL-R were detected, based on the duration of egg and larval stages, the survival of eggs and larvae, adult longevity, fecundity, net reproductive rate, gross reproduction rate, finite rate of increase and mean generation time. Based on log dose-probit lines, resistance in NIL-R is incompletely recessive and results from a single, autosomal, recessive locus; the degree of dominance was estimated to be -0.74 and -0.71 for F1 (resistant ♀ × susceptible ♂) and F1 ' (susceptible ♀ × resistant ♂) progeny respectively. Assessment of near-isogenic Cry1Ac-resistant and Cry1Ac-susceptible strains of P. xylostella indicated that resistance is not accompanied with fitness costs, and that resistance is incompletely recessive. These findings should be useful in managing the development of Bt Cry1Ac resistance. © 2015 Society of Chemical Industry.

  1. Introducing AC inductive reactance with a power tool

    NASA Astrophysics Data System (ADS)

    Bryant, Wesley; Baker, Blane

    2016-09-01

    The concept of reactance in AC electrical circuits is often non-intuitive and difficult for students to grasp. In order to address this lack of conceptual understanding, classroom exercises compare the predicted resistance of a power tool, based on electrical specifications, to measured resistance. Once students discover that measured resistance is smaller than expected, they are asked to explain these observations using previously studied principles of magnetic induction. Exercises also introduce the notion of inductive reactance and impedance in AC circuits and, ultimately, determine self-inductance of the motor windings within the power tool.

  2. Magnetic Nature of the CrIII-LnIII Interactions in [CrIII2LnIII3] Clusters with Slow Magnetic Relaxation.

    PubMed

    Zhao, Xiao-Qing; Xiang, Shuo; Wang, Jin; Bao, Dong-Xu; Li, Yun-Chun

    2018-02-01

    Two 3 d -4 f hetero-metal pentanuclear complexes with the formula {[Cr III 2 Ln III 3 L 10 (OH) 6 (H 2 O) 2 ]Et 3 NH} [Ln=Tb ( 1 ), Dy ( 2 ); HL=pivalic acid, Et 3 N=triethylamine] have been produced. The metal core of each cluster is made up of a trigonal bipyramid with three Ln III ions (plane) and two Cr III ions (above and below) held together by six μ 3 -OH bridges. Also reported with this series is the diamagnetic Cr III -Y III analogue ( 3 ). Fortunately, we successfully prepared Al III -Ln III analogues with the formula {[Al III 2 Ln III 3 L 10 (OH) 6 (H 2 O) 2 ]Et 3 NH⋅H 2 O} [Ln=Tb ( 4 ), Dy ( 5 )], containing diamagnetic Al III ions, which can be used to evaluate the Cr III -Ln III magnetic nature through a diamagnetic substitution method. Subsequently, static (dc) magnetic susceptibility studies reveal dominant ferromagnetic interactions between Cr III and Ln III ions. Dynamic (ac) magnetic susceptibility studies show frequency-dependent out-of-phase ( χ '') signals for [Cr III 2 Tb III 3 ] ( 1 ), [Cr III 2 Dy III 3 ] ( 2 ), and [Al III 2 Dy III 3 ] ( 5 ), which are derived from the single-ion behavior of Ln III ions and/or the Cr III -Ln III ferromagnetic interactions.

  3. Association between the -794 (CATT)5-8  MIF gene polymorphism and susceptibility to acute coronary syndrome in a western Mexican population.

    PubMed

    Valdés-Alvarado, Emmanuel; Muñoz-Valle, José Francisco; Valle, Yeminia; Sandoval-Pinto, Elena; García-González, Ilian Janet; Valdez-Haro, Angélica; De la Cruz-Mosso, Ulises; Flores-Salinas, Héctor Enrique; Padilla-Gutiérrez, Jorgé Ramón

    2014-01-01

    The macrophage migration inhibitory factor (MIF) is related to the progression of atherosclerosis, which, in turn, is a key factor in the development of acute coronary syndrome (ACS). MIF has a CATT short tandem repeat (STR) at position -794 that might be involved in its expression rate. The aim of this study was to investigate the association between the -794 (CATT)5-8  MIF gene polymorphism and susceptibility to ACS in a western Mexican population. This research included 200 ACS patients classified according to the criteria of the American College of Cardiology (ACC) and 200 healthy subjects (HS). The -794 (CATT)5-8  MIF gene polymorphism was analyzed using a conventional polymerase chain reaction (PCR) technique. The 6 allele was the most frequent in both groups (ACS: 54% and HS: 57%). The most common genotypes in ACS patients and HS were 6/7 and 6/6, respectively, and a significant association was found between the 6/7 genotype and susceptibility to ACS (68% versus 47% in ACS and HS, resp., P = 0.03). We conclude that the 6/7 genotype of the MIF -794 (CATT)5-8 polymorphism is associated with susceptibility to ACS in a western Mexican population.

  4. Tracking paleo-SMT positions using a magnetic susceptibility proxy approach from sediments on the Arctic Vestnesa Ridge, offshore western Svalbard

    NASA Astrophysics Data System (ADS)

    Johnson, Joel; Phillips, Stephen; Panieri, Giuliana; Sauer, Simone; Knies, Jochen; Mienert, Jurgen

    2014-05-01

    Methane in marine sediments, often existing ephemerally as gas hydrate, constitutes one of the largest reservoirs of natural gas on Earth and fluxes of methane in marine sediments are an important component in the global carbon cycle. Tracking changes in past methane flux, however, remains difficult and there are few available proxies that persist through geologic time. CAGE - Centre for Arctic Gas Hydrate, Environment, and Climate initiates a ten year interdisciplinary research and education program aimed at achieving a quantitative understanding of feedbacks between methane in sub-seabed reservoirs, the seabed and the ocean. In our recent work on the Indian continental margin we document that drawdowns in magnetic susceptibility, constrained by magnetic properties, and integrated with core sedimentology, XRF elemental data, authigenic mineralogy, and pore water geochemistry, can be used to track the paleo-positions of the SMT (sulfate-methane transition). Relative positions of the SMT in marine sediments are controlled by the balance of methane and sulfate fluxes. The products of the anaerobic oxidation of methane at the SMT, hydrogen sulfide and bicarbonate, allow for the dissolution of detrital magnetite, and the precipitation of authigenic carbonates and iron sulfides. We recently obtained 21 gravity cores in and between active and inactive pockmarks along the crest of the Vestnesa Ridge, an Arctic gas and gas hydrate bearing contourite sediment drift located offshore western Svalbard. Magnetic susceptibility records from reference cores outside of pockmarks show the stratigraphy across the ridge is quite uniform, whereas magnetic susceptibility records within the pockmarks, with and without observed water column gas flares, are significantly depleted. Integration of multiple data sets from these records and comparison with reconstructions of paleo-methane emissions at the seafloor from benthic foraminifera will allow us to interpret these drawdowns in

  5. Synthesis, characterisation and computational studies on a novel one-dimensional arrangement of Schiff-base Mn3 single-molecule magnet.

    PubMed

    Lin, Po-Heng; Gorelsky, Serge; Savard, Didier; Burchell, Tara J; Wernsdorfer, Wolfgang; Clérac, Rodolphe; Murugesu, Muralee

    2010-09-07

    The syntheses, structures and magnetic properties are reported for three new manganese complexes containing the Schiff-base ((2-hydroxy-3-methoxyphenyl)methylene)isonicotinohydrazine (H(2)hmi) ligand. Complex [Mn(II)(H(2)hmi)(2)(MeOH)(2)Cl(2)] (1) was obtained from the reaction of H(2)hmi with MnCl(2) in a MeOH-MeCN mixture. Addition of triethylamine to the previous reaction mixture followed by diethyl ether diffusion yielded a dinuclear manganese [Mn(III)(2)(hmi)(2)(OMe)(2)](infinity).2MeCN.2OEt(2) (2) compound. Upon increasing the MnCl(2)/H(2)hmi ratio, the mixed valence complex [Mn(III)(2)Mn(II)(hmi)(2)(OMe)(2)Cl(2)](infinity).MeOH (3) was obtained. Dc and ac magnetic measurements were carried out on all three samples. The ac susceptibility and field dependence of the magnetisation measurements confirmed that complex 3 exhibits a single-molecule magnet behaviour with an effective energy barrier of 8.1 K and an Arrhenius pre-exponential factor of 3 x 10(-9) s.

  6. Characterization of AC current sensor based on giant magnetoresistance and coil for power meter design

    NASA Astrophysics Data System (ADS)

    Dhani, H. S.; Aminudin, A.; Waslaluddin

    2018-05-01

    Electric current is the basic variable of measurement in instrumentation system. One of the current measurements had been developed was based on magnetic sensor. Giant Magnetoresistance (GMR) produces an output voltage when it detects the magnetic field from electric current flow. The purpose of this study was to characterize the response of GMR when variation number of coil was given. The characterization was the GMR voltage response to the AC current values from 0.01 A to 5.00 A. The linearity of the relation was reaching saturation point when the magnetic field measured higher than 10.5 Oe at room temperature. As the number of coil increased, the earlier saturation occurred. To see the sensitivity of the sensor response, the data graph was cut off at 1.56 A AC. From this research, we got single coil was ideal to measure electric current higher than 1.56 A AC, as the relation of GMR voltage to the current tended to maintain its linearity. For measurement of 1.56 A AC and less, coil number addition would increase the sensitivity of sensor response. This research hopefully will be benefit for further development using an electric current measurement based on GMR magnetic sensor for power meter design.

  7. Downhole logs of natural gamma radiation and magnetic susceptibility and their use in interpreting lithostratigraphy in AND-1B, Antarctica

    NASA Astrophysics Data System (ADS)

    Williams, T.; Morin, R. H.; Jarrard, R. D.; Jackolski, C. L.; Henrys, S. A.; Niessen, F.; Magens, D.; Kuhn, G.; Monien, D.; Powell, R. D.

    2010-12-01

    The ANDRILL McMurdo Ice Shelf (MIS) project drilled 1285 metres of sediment representing the last 14 million years of glacial history. Downhole geophysical logs were acquired to a depth of 1018 metres, and are complementary to data acquired from the core itself. We describe here the natural gamma radiation (NGR) and magnetic susceptibility logs, and their application to understanding lithological and paleoenvironmental change at ANDRILL McMurdo Ice Shelf Hole AND-1B. Natural gamma radiation logs cover the whole interval from the sea floor to 1018 metres, and magnetic susceptibility and other logs covered the open-hole intervals between 692-1018 and 237-342 metres. NGR logs were stacked and corrected for signal attenuation through the drill pipe, and magnetic susceptibility logs were corrected for drift. In the upper part of AND-1B, clear alternations between low and high NGR values distinguish between diatomite (lacking minerals containing naturally radioactive K, U, and Th) and diamict (containing K-bearing clays, K-feldspar, and heavy minerals). In the lower open-hole logged section, NGR and magnetic susceptibility can also distinguish claystones (rich in K-bearing clay minerals, relatively low in magnetite) and diamicts (relatively high in magnetite), while sandstones generally have high resistivity log values at AND-1B. On the basis of these three downhole logs, three sets of facies can be predicted correctly for 74% of the 692-1018m interval. The logs were then used to predict facies for the 7% of this interval that was unrecovered by coring. Similarly, the NGR log provides the best information on the lithology of the poorly recovered top 25m of AND-1B. Given the understanding of the physical property characteristics of different facies, it is also possible to identify subtle changes in lithology from the physical properties, and help refine parts of the lithostratigraphy (for example, the varying terrigenous content of diatomites).

  8. Magnetic energy flow imaging of magnetic recording head with enhanced resolution and sensitivity by A-MFM using high magnetic moment superparamagnetic tip

    NASA Astrophysics Data System (ADS)

    Kumar, Pawan; Cao, Yongze; Suzuki, Yudai; Yoshimura, Satoru; Saito, Hitoshi

    2018-06-01

    In this report, the magnetic energy flow of AC magnetic field is imaged from a perpendicular magnetic recording head by alternating magnetic force microscopy (A-MFM) with high magnetic moment Co0.43(GdOx)0.57 superparamagnetic (SP) tip. The present magnetic energy flow imaging phenomenon is able to detect the flow direction of AC magnetic field energy from the recording head. A simple model for the flow direction of the AC magnetic energy is given and revealed that when the AC magnetic field energy from the surface of main pole increases, the energy from the side cross section decreases due to the periodical change of magnetization direction at the main pole area. The A-MFM magnetic energy imaging performance by 100 nm Co0.43(GdOx)0.57 SP tip is compared with the magnetic field imaging with the 25 nm Co0.80Zr0.05Nb0.15 soft magnetic (SM) tip. The spatial resolution measured by Fourier analysis for Co0.43(GdOx)0.57 SP tip is enhanced dramatically to ˜10 nm with low thermal noise, as compared to ˜13 nm by Co0.80Zr0.05Nb0.15 SM tip as well as the previously reported MFM tip. Moreover, the sensitivity and resolution are investigated for a range of head current to confirm the suitability of the magnetic energy flow imaging by Co0.43(GdOx)0.57 SP tip to low as well as high magnetic field source. Further, the A-MFM measurements are performed with the 100 nm Au coated conducting tip to investigate the possibility of electrostatic contribution in magnetic energy imaging by Co0.43(GdOx)0.57 SP tip and revealed that the present A-MFM measurement is free from any electrostatic artifacts. The present magnetic energy flow imaging phenomena with the high magnetic moment Co0.43(GdOx)0.57 SP tip provides an avenue for the analysis of the magnetic field energy component from the head field profile.

  9. Pressure effect on spin-glass behavior in Ce0.9Er0.1Al2

    NASA Astrophysics Data System (ADS)

    Wakiya, Kazuhei; Hu, Guanghui; Fuseya, Ryohei; Ohashi, Masashi; Uehara, Masatomo; Umehara, Izuru

    2018-05-01

    The dc magnetization and ac susceptibility of the Laves phase compound Ce0.9Er0.1Al2 have been measured at ambient and high pressures up to 1.1 GPa. The ac susceptibility shows a peak at around Tf 2.5 K, and Tf shifts to higher temperatures with an increase in the measuring frequency. Below Tf, the zero-field-cooled (ZFC) and field-cooled (FC) dc magnetizations separate from each other. Furthermore, long-time magnetic relaxation behavior is observed. These results indicate that a spin-glass state is formed below Tf. We found that the Tf determined by dc magnetization measurement decreases with an increase in pressure.

  10. Study of flow fractionation characteristics of magnetic chromatography utilizing high-temperature superconducting bulk magnet.

    PubMed

    Fukui, Satoshi; Shoji, Yoshihiro; Ogawa, Jun; Oka, Tetsuo; Yamaguchi, Mitsugi; Sato, Takao; Ooizumi, Manabu; Imaizumi, Hiroshi; Ohara, Takeshi

    2009-02-01

    We present numerical simulation of separating magnetic particles with different magnetic susceptibilities by magnetic chromatography using a high-temperature superconducting bulk magnet. The transient transport is numerically simulated for two kinds of particles having different magnetic susceptibilities. The time evolutions were calculated for the particle concentration in the narrow channel of the spiral arrangement placed in the magnetic field. The field is produced by the highly magnetized high-temperature superconducting bulk magnet. The numerical results show the flow velocity difference of the particle transport corresponding to the difference in the magnetic susceptibility, as well as the possible separation of paramagnetic particles of 20 nm diameter.

  11. On the nature of magnetic state in the spinel Co₂SnO₄.

    PubMed

    Thota, S; Narang, V; Nayak, S; Sambasivam, S; Choi, B C; Sarkar, T; Andersson, M S; Mathieu, R; Seehra, M S

    2015-04-29

    In the spinel Co2SnO4, coexistence of ferrimagnetic ordering below T(N) ≃ 41 K followed by a spin glass state below T(SG) ≃ 39 K was proposed recently based on the temperature dependence of magnetization M(T) data. Here new measurements of the temperature dependence of the specific heat C(P)(T), ac-susceptibilities χ'(T) and χ″(T) measured at frequencies between 0.51 and 1.2 kHz, and the hysteresis loop parameters (coercivity H(C)(T) and remanence M(R)(T)) in two differently prepared samples of Co2SnO4 are reported. The presence of the Co(2+) and Sn(4+) states is confirmed by x-ray photoelectron spectroscopy (XPS) yielding the structure: Co2SnO4 = [Co(2+)][Co(2+)Sn(4+)]O4. The data of C(P) versus T shows only an inflection near 39 K characteristic of spin-glass ordering. The analysis of the frequency dependence of ac-magnetic susceptibility data near 39 K using the Vogel-Fulcher law and the power-law of the critical slowing-down suggests the presence of spin clusters in the system which is close to a spin-glass state. With a decrease in temperature below 39 K, the temperature dependence of the coercivity H(C) and remanence M(R) for the zero-field cooled samples show both H(C) and M(R) reaching their peak magnitudes near 25 K, then decreasing with decreasing T and becoming negligible below 15 K. The plot of C(P)/T versus T also yields a weak inflection near 15 K. This temperature dependence of H(C) and remanence M(R) is likely associated with the different magnitudes of the magnetic moments of Co(2+) ions on the 'A' and 'B' sites and their different temperature dependence.

  12. Linearity of the Faraday-rotation-type ac magnetic-field sensor with a ferrimagnetic or ferromagnetic rotator film

    NASA Astrophysics Data System (ADS)

    Mori, Hiroshi; Asahara, Yousuke

    1996-03-01

    We analyze the linearity and modulation depth of ac magnetic-field sensors or current sensors, using a ferrimagnetic or ferromagnetic film as the Faraday rotator and employing the detection of only the zeroth-order optical diffraction component from the rotator. It is theoretically shown that for this class of sensor the condition of a constant modulation depth and that of a constant ratio error give an identical series of curves for the relationship between Faraday rotation angle greater than or equals V and polarizer/analyzer relative angle Phi . We give some numerical examples to demonstrate the usefulness of the result with reference to a rare-earth iron garnet film as the rotator.

  13. Low-temperature magnetic properties of greigite (Fe3S4)

    NASA Astrophysics Data System (ADS)

    Chang, Liao; Roberts, Andrew P.; Rowan, Christopher J.; Tang, Yan; Pruner, Petr; Chen, Qianwang; Horng, Chorng-Shern

    2009-01-01

    We provide comprehensive low-temperature magnetic results for greigite (Fe3S4) across the spectrum from superparamagnetic (SP) to multidomain (MD) behavior. It is well known that greigite has no low-temperature magnetic transitions, but we also document that it has strong domain-state dependence of magnetic properties at low temperatures. Blocking of SP grains and increasing thermal stability with decreasing temperature is apparent in many magnetic measurements. Thermally stable single-domain greigite undergoes little change in magnetic properties below room temperature. For pseudo-single-domain (PSD)/MD greigite, hysteresis properties and first-order reversal curve diagrams exhibit minor changes at low temperatures, while remanence continuously demagnetizes because of progressive domain wall unpinning. The low-temperature demagnetization is grain size dependent for PSD/MD greigite, with coarser grains undergoing larger remanence loss. AC susceptibility measurements indicate consistent blocking temperatures (TB) for all synthetic and natural greigite samples, which are probably associated with surficial oxidation. Low-temperature magnetic analysis provides much more information about magnetic mineralogy and domain state than room temperature measurements and enables discrimination of individual components within mixed magnetic mineral assemblages. Low-temperature rock magnetometry is therefore a useful tool for studying magnetic mineralogy and granulometry of greigite-bearing sediments.

  14. Encapsulation of methotrexate loaded magnetic microcapsules for magnetic drug targeting and controlled drug release

    NASA Astrophysics Data System (ADS)

    Chakkarapani, Prabu; Subbiah, Latha; Palanisamy, Selvamani; Bibiana, Arputha; Ahrentorp, Fredrik; Jonasson, Christian; Johansson, Christer

    2015-04-01

    We report on the development and evaluation of methotrexate magnetic microcapsules (MMC) for targeted rheumatoid arthritis therapy. Methotrexate was loaded into CaCO3-PSS (poly (sodium 4-styrenesulfonate)) doped microparticles that were coated successively with poly (allylamine hydrochloride) and poly (sodium 4-styrenesulfonate) by layer-by-layer technique. Ferrofluid was incorporated between the polyelectrolyte layers. CaCO3-PSS core was etched by incubation with EDTA yielding spherical MMC. The MMC were evaluated for various physicochemical, pharmaceutical parameters and magnetic properties. Surface morphology, crystallinity, particle size, zeta potential, encapsulation efficiency, loading capacity, drug release pattern, release kinetics and AC susceptibility studies revealed spherical particles of ~3 μm size were obtained with a net zeta potential of +24.5 mV, 56% encapsulation and 18.6% drug loading capacity, 96% of cumulative drug release obeyed Hixson-Crowell model release kinetics. Drug excipient interaction, surface area, thermal and storage stability studies for the prepared MMC was also evaluated. The developed MMC offer a promising mode of targeted and sustained release drug delivery for rheumatoid arthritis therapy.

  15. The 3'UTR 1188A/C polymorphism of IL-12p40 is not associated with susceptibility for developing plaque psoriasis in Mestizo population from western Mexico.

    PubMed

    Sandoval-Talamantes, Ana Karen; Brito-Luna, Myrian Johanna; Fafutis-Morris, Mary; Villanueva-Quintero, Delfina Guadalupe; Graciano-Machuca, Omar; Ramírez-Dueñas, María Guadalupe; Alvarado-Navarro, Anabell

    2015-02-01

    Psoriasis is a chronic autoimmune inflammatory disease that affects the skin and the joints. Psoriasis is characterized by the keratinocyte proliferation, which is induced by cytokines Th1 and Th17. Patients with plaque psoriasis present a chronic inflammatory response with high levels of interleukin (IL)-12 and IL-23. Various single-nucleotide polymorphisms (SNP) have been identified in the IL12B gene, such as SNP 3' UTR 1188 A/C (SNP rs3212227), which has been associated with susceptibility to developing plaque psoriasis and with the production of IL-12 and IL-23 in individuals of different ethnic groups. In this study, we determined whether there is an association of SNP rs3212227 with the susceptibility of developing plaque psoriasis and with serum levels of IL-12 and IL-23 in Mestizo population in western Mexico. We included 112 patients with psoriasis and 112 clinical healthy individuals in the study. The frequencies of genotypes A/A, A/C, and C/C in patients with plaque psoriasis were 41, 53, and 6%, respectively, while in the control group, these were 37, 53, and 10%, respectively, without finding statistically significant differences between both groups (p>0.05). Although IL-12 and IL-23 serum levels were higher in patients than in controls, we found no significant differences. The group of patients with genotype CC presented the highest levels of IL-23 (p<0.05). These data suggest that the SNP rs3212227 phenotype is not associated with the risk of developing plaque psoriasis or with IL-12 and IL-23 levels in Mestizo population in western Mexico. Copyright © 2014 European Federation of Immunological Societies. Published by Elsevier B.V. All rights reserved.

  16. Magnetic Susceptibility as a B0 Field Strength Independent MRI Biomarker of Liver Iron Overload

    PubMed Central

    Hernando, Diego; Cook, Rachel J.; Diamond, Carol; Reeder, Scott B.

    2013-01-01

    Purpose MR-based quantification of liver magnetic susceptibility may enable field strength-independent measurement of liver iron concentration (LIC). However, susceptibility quantification is challenging, due to non-local effects of susceptibility on the B0 field. The purpose of this work is to demonstrate feasibility of susceptibility-based LIC quantification using a fat-referenced approach. Methods Phantoms consisting of vials with increasing iron concentrations immersed between oil/water layers, and twenty-seven subjects (9 controls/18 subjects with liver iron overload) were scanned. Ferriscan (1.5T) provided R2-based reference LIC. Multi-echo 3D-SPGR (1.5T/3T) enabled fat-water, B0- and R2*-mapping. Phantom iron concentration (mg Fe/l) was estimated from B0 differences (ΔB0) between vials and neighboring oil. Liver susceptibility and LIC (mg Fe/g dry tissue) was estimated from ΔB0 between the lateral right lobe of the liver and adjacent subcutaneous adipose tissue (SAT). Results Estimated phantom iron concentrations had good correlation with true iron concentrations (1.5T:slope=0.86, intercept=0.72, r2=0.98; 3T:slope=0.85, intercept=1.73, r2=0.98). In liver, ΔB0 correlated strongly with R2* (1.5T:r2=0.86; 3T:r2=0.93) and B0-LIC had good agreement with Ferriscan-LIC (slopes/intercepts nearly 1.0/0.0, 1.5T:r2=0.67, slope=0.93±0.13, p≈0.50, intercept=1.93±0.78, p≈0.02; 3T:r2=0.84, slope=1.01±0.09, p≈0.90, intercept=0.23±0.52, p≈0.68). Discussion Fat-referenced, susceptibility-based LIC estimation is feasible at both field strengths. This approach may enable improved susceptibility mapping in the abdomen. PMID:23801540

  17. Proteomics-based identification of midgut proteins correlated with Cry1Ac resistance in Plutella xylostella (L.).

    PubMed

    Xia, Jixing; Guo, Zhaojiang; Yang, Zezhong; Zhu, Xun; Kang, Shi; Yang, Xin; Yang, Fengshan; Wu, Qingjun; Wang, Shaoli; Xie, Wen; Xu, Weijun; Zhang, Youjun

    2016-09-01

    The diamondback moth, Plutella xylostella (L.), is a worldwide pest of cruciferous crops and can rapidly develop resistance to many chemical insecticides. Although insecticidal crystal proteins (i.e., Cry and Cyt toxins) derived from Bacillus thuringiensis (Bt) have been useful alternatives to chemical insecticides for the control of P. xylostella, resistance to Bt in field populations of P. xylostella has already been reported. A better understanding of the resistance mechanisms to Bt should be valuable in delaying resistance development. In this study, the mechanisms underlying P. xylostella resistance to Bt Cry1Ac toxin were investigated using two-dimensional differential in-gel electrophoresis (2D-DIGE) and ligand blotting for the first time. Comparative analyses of the constitutive expression of midgut proteins in Cry1Ac-susceptible and -resistant P. xylostella larvae revealed 31 differentially expressed proteins, 21 of which were identified by mass spectrometry. Of these identified proteins, the following fell into diverse eukaryotic orthologous group (KOG) subcategories may be involved in Cry1Ac resistance in P. xylostella: ATP-binding cassette (ABC) transporter subfamily G member 4 (ABCG4), trypsin, heat shock protein 70 (HSP70), vacuolar H(+)-ATPase, actin, glycosylphosphatidylinositol anchor attachment 1 protein (GAA1) and solute carrier family 30 member 1 (SLC30A1). Additionally, ligand blotting identified the following midgut proteins as Cry1Ac-binding proteins in Cry1Ac-susceptible P. xylostella larvae: ABC transporter subfamily C member 1 (ABCC1), solute carrier family 36 member 1 (SLC36A1), NADH dehydrogenase iron-sulfur protein 3 (NDUFS3), prohibitin and Rap1 GTPase-activating protein 1. Collectively, these proteomic results increase our understanding of the molecular resistance mechanisms to Bt Cry1Ac toxin in P. xylostella and also demonstrate that resistance to Bt Cry1Ac toxin is complex and multifaceted. Copyright © 2016 Elsevier B.V. All

  18. Numerical study on AC loss reduction of stacked HTS tapes by optimal design of flux diverter

    NASA Astrophysics Data System (ADS)

    Liu, Guole; Zhang, Guomin; Jing, Liwei; Yu, Hui

    2017-12-01

    High temperature superconducting (HTS) coils are key parts of many AC applications, such as generators, superconducting magnetic energy storage and transformers. AC loss reduction in HTS coils is essential for the commercialization of these HTS devices. Magnetic material is generally used as the flux diverter in an effort to reduce the AC loss in HTS coils. To achieve the greatest reduction in the AC loss of the coils, the flux diverter should be made of a material with low loss and high saturated magnetic density, and the optimization of the geometric size and location of the flux diverter is required. In this paper, we chose Ni-alloy as the flux diverter, which can be processed into a specific shape and size. The influence of the shape and location of the flux diverter on the AC loss characteristics of stacked (RE)BCO tapes is investigated by use of a finite element method. Taking both the AC loss of the (RE)BCO coils and the ferromagnetic loss of the flux diverter into account, the optimal geometry of the flux diverter is obtained. It is found that when the applied current is at half the value of the critical current, the total loss of the HTS stack with the optimal flux diverter is only 18% of the original loss of the HTS stack without the flux diverter. Besides, the effect of the flux diverter on the critical current of the (RE)BCO stack is investigated.

  19. Finite-size effects on the static properties of a single-chain magnet

    NASA Astrophysics Data System (ADS)

    Bogani, L.; Sessoli, R.; Pini, M. G.; Rettori, A.; Novak, M. A.; Rosa, P.; Massi, M.; Fedi, M. E.; Giuntini, L.; Caneschi, A.; Gatteschi, D.

    2005-08-01

    We study the role of defects in the “single-chain magnet” CoPhOMe by inserting a controlled number of diamagnetic impurities. The samples are analyzed with unprecedented accuracy with the particle induced x-ray emission technique, and with ac and dc magnetic measurements. In an external applied field the system shows an unexpected behavior, giving rise to a double peak in the susceptibility. The static thermodynamic properties of the randomly diluted Ising chain with alternating g values are then exactly obtained via a transfer matrix approach. These results are compared to the experimental behavior of CoPhOMe, showing qualitative agreement.

  20. Feasibility study of determining axial stress in ferromagnetic bars using reciprocal amplitude of initial differential susceptibility obtained from static magnetization by permanent magnets

    NASA Astrophysics Data System (ADS)

    Deng, Dongge; Wu, Xinjun

    2018-03-01

    An electromagnetic method for determining axial stress in ferromagnetic bars is proposed. In this method, the tested bar is under the static magnetization provided by permanent magnets. The tested bar do not have to be magnetized up to the technical saturation because reciprocal amplitude of initial differential susceptibility (RAIDS) is adopted as the feature parameter. RAIDS is calculated from the radial magnetic flux density Br Lo = 0.5 at the Lift-off Lo = 0.5 mm, radial magnetic flux density Br Lo = 1 at the Lift-off Lo = 1 mm and axial magnetic flux density Bz Lo = 1 at the Lift-off Lo = 1 mm from the surface of the tested bar. Firstly, the theoretical derivation of RAIDS is carried out according to Gauss' law for magnetism, Ampere's Law and the Rayleigh relation in Rayleigh region. Secondly, the experimental system is set up for a 2-meter length and 20 mm diameter steel bar. Thirdly, an experiment is carried out on the steel bar to analyze the relationship between the obtained RAIDS and the axial stress. Experimental results show that the obtained RAIDS decreases almost linearly with the increment of the axial stress inside the steel bar in the initial elastic region. The proposed method has the potential to determine tensile axial stress in the slender cylindrical ferromagnetic bar.

  1. Fabrication of highly dense isotropic Nd-Fe-B nylon bonded magnets via extrusion-based additive manufacturing [Fabrication of highly dense isotropic Nd-Fe-B bonded magnets via extrusion-based additive manufacturing

    DOE PAGES

    Li, Ling; Jones, Kodey E.; Sales, Brian C.; ...

    2018-04-03

    Magnetically isotropic bonded magnets with a high loading fraction of 70 vol.% Nd-Fe-B are fabricated via an extrusion-based additive manufacturing, or 3D printing system that enables rapid production of large parts. The density of the printed magnet is ~5.2 g/cm 3. The room temperature magnetic properties are: intrinsic coercivity Hci = 8.9 kOe (708.2 kA/m), remanence Br = 5.8 kG (0.58 T), and energy product (BH)max = 7.3 MGOe (58.1 kJ/m 3). The as-printed magnets are then coated with two types of polymers, both of which improve the thermal stability as revealed by flux aging loss measurements. Tensile tests performedmore » at 25 °C and 100 °C show that the ultimate tensile stress (UTS) increases with increasing loading fraction of the magnet powder, and decreases with increasing temperature. AC magnetic susceptibility and resistivity measurements show that the 3D printed Nd-Fe-B bonded magnets exhibit extremely low eddy current loss and high resistivity. Lastly, we demonstrate the performance of the 3D printed magnets in a DC motor configuration via back electromotive force measurements.« less

  2. Fabrication of highly dense isotropic Nd-Fe-B nylon bonded magnets via extrusion-based additive manufacturing [Fabrication of highly dense isotropic Nd-Fe-B bonded magnets via extrusion-based additive manufacturing

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Li, Ling; Jones, Kodey E.; Sales, Brian C.

    Magnetically isotropic bonded magnets with a high loading fraction of 70 vol.% Nd-Fe-B are fabricated via an extrusion-based additive manufacturing, or 3D printing system that enables rapid production of large parts. The density of the printed magnet is ~5.2 g/cm 3. The room temperature magnetic properties are: intrinsic coercivity Hci = 8.9 kOe (708.2 kA/m), remanence Br = 5.8 kG (0.58 T), and energy product (BH)max = 7.3 MGOe (58.1 kJ/m 3). The as-printed magnets are then coated with two types of polymers, both of which improve the thermal stability as revealed by flux aging loss measurements. Tensile tests performedmore » at 25 °C and 100 °C show that the ultimate tensile stress (UTS) increases with increasing loading fraction of the magnet powder, and decreases with increasing temperature. AC magnetic susceptibility and resistivity measurements show that the 3D printed Nd-Fe-B bonded magnets exhibit extremely low eddy current loss and high resistivity. Lastly, we demonstrate the performance of the 3D printed magnets in a DC motor configuration via back electromotive force measurements.« less

  3. Energy dissipation of composite multifilamentary superconductors for high-current ramp-field magnet applications

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Gung, C.Y.

    1993-01-01

    Energy dissipation, which is also called AC loss, of a composite multifilamentary superconducting wire is one of the most fundamental concerns in building a stable superconducting magnet. Characterization and reduction of AC losses are especially important in designing a superconducting magnet for generating transient magnetic fields. The goal of this thesis is to improve the understanding of AC-loss properties of superconducting wires developed for high-current ramp-field magnet applications. The major tasks include: (1) building an advanced AC-loss measurement system, (2) measuring AC losses of superconducting wires under simulated pulse magnet operations, (3) developing an analytical model for explaining the newmore » AC-loss properties found in the experiment, and (4) developing a computational methodology for comparing AC losses of a superconducting wire with those of a cable for a superconducting pulse magnet. A new experimental system using an isothermal calorimetric method was designed and constructed to measure the absolute AC losses in a composite superconductor. This unique experimental setup is capable of measuring AC losses of a brittle Nb{sub 3}Sn wire carrying high AC current in-phase with a large-amplitude pulse magnetic field. Improvements of the accuracy and the efficiency of this method are discussed. Three different types of composite wire have been measured: a Nb{sub 3}Sn modified jelly-roll (MJR) internal-tin wire used in a prototype ohmic heating coil, a Nb{sub 3}Sn internal-tin wire developed for a fusion reactor ohmic heating coil, and a NbTi wire developed for the magnets in a particle accelerator. The cross sectional constructions of these wires represent typical commercial wires manufactured for pulse magnet applications.« less

  4. Quantitative Susceptibility Mapping of Human Brain Reflects Spatial Variation in Tissue Composition

    PubMed Central

    Li, Wei; Wu, Bing; Liu, Chunlei

    2011-01-01

    Image phase from gradient echo MRI provides a unique contrast that reflects brain tissue composition variations, such as iron and myelin distribution. Phase imaging is emerging as a powerful tool for the investigation of functional brain anatomy and disease diagnosis. However, the quantitative value of phase is compromised by its nonlocal and orientation dependent properties. There is an increasing need for reliable quantification of magnetic susceptibility, the intrinsic property of tissue. In this study, we developed a novel and accurate susceptibility mapping method that is also phase-wrap insensitive. The proposed susceptibility mapping method utilized two complementary equations: (1) the Fourier relationship of phase and magnetic susceptibility; and (2) the first-order partial derivative of the first equation in the spatial frequency domain. In numerical simulation, this method reconstructed the susceptibility map almost free of streaking artifact. Further, the iterative implementation of this method allowed for high quality reconstruction of susceptibility maps of human brain in vivo. The reconstructed susceptibility map provided excellent contrast of iron-rich deep nuclei and white matter bundles from surrounding tissues. Further, it also revealed anisotropic magnetic susceptibility in brain white matter. Hence, the proposed susceptibility mapping method may provide a powerful tool for the study of brain physiology and pathophysiology. Further elucidation of anisotropic magnetic susceptibility in vivo may allow us to gain more insight into the white matter microarchitectures. PMID:21224002

  5. Note: A sample holder design for sensitive magnetic measurements at high temperatures in a magnetic properties measurement system

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Arauzo, A.; Guerrero, E.; Urtizberea, A.

    2012-06-15

    A sample holder design for high temperature measurements in a commercial MPMS SQUID magnetometer from Quantum Design is presented. It fulfills the requirements for the simultaneous use of the oven and reciprocating sample option (RSO) options, thus allowing sensitive magnetic measurements up to 800 K. Alternating current susceptibility can also be measured, since the holder does not induce any phase shift relative to the ac driven field. It is easily fabricated by twisting Constantan Copyright-Sign wires into a braid nesting the sample inside. This design ensures that the sample be placed tightly into a tough holder with its orientation fixed,more » and prevents any sample displacement during the fast movements of the RSO transport, up to high temperatures.« less

  6. Magnetic Nature of the CrIII–LnIII Interactions in [CrIII 2LnIII 3] Clusters with Slow Magnetic Relaxation

    PubMed Central

    Xiang, Shuo; Wang, Jin; Bao, Dong‐Xu; Li, Yun‐Chun

    2018-01-01

    Abstract Two 3d‐4f hetero‐metal pentanuclear complexes with the formula {[CrIII 2LnIII 3L10(OH)6(H2O)2]Et3NH} [Ln=Tb (1), Dy (2); HL=pivalic acid, Et3N=triethylamine] have been produced. The metal core of each cluster is made up of a trigonal bipyramid with three LnIII ions (plane) and two CrIII ions (above and below) held together by six μ 3‐OH bridges. Also reported with this series is the diamagnetic CrIII–YIII analogue (3). Fortunately, we successfully prepared AlIII–LnIII analogues with the formula {[AlIII 2LnIII 3L10(OH)6(H2O)2]Et3NH⋅H2O} [Ln=Tb (4), Dy (5)], containing diamagnetic AlIII ions, which can be used to evaluate the CrIII–LnIII magnetic nature through a diamagnetic substitution method. Subsequently, static (dc) magnetic susceptibility studies reveal dominant ferromagnetic interactions between CrIII and LnIII ions. Dynamic (ac) magnetic susceptibility studies show frequency‐dependent out‐of‐phase (χ′′) signals for [CrIII 2TbIII 3] (1), [CrIII 2DyIII 3] (2), and [AlIII 2DyIII 3] (5), which are derived from the single‐ion behavior of LnIII ions and/or the CrIII–LnIII ferromagnetic interactions. PMID:29435404

  7. Property and microstructural nonuniformity in the yttrium-barium-copper-oxide superconductor determined from electrical, magnetic, and ultrasonic measurements. Ph.D. Thesis - Case Western Reserve Univ.

    NASA Technical Reports Server (NTRS)

    Roth, Don J.

    1991-01-01

    The purpose of this dissertation was the following: (1) to characterize the effect of pore fraction on a comprehensive set of electrical and magnetic properties for the yttrium-barium-copper-oxide (YBCO) high temperature ceramic superconductor; and (2) to determine the viability of using a room-temperature, nondestructive characterization method to aid in the prediction of superconducting (cryogenic) properties. The latter involved correlating ultrasonic velocity measurements at room temperature with property-affecting pore fraction and oxygen content variations. The use of ultrasonic velocity for estimating pore fraction in YBCO is presented, and other polycrystalline materials are reviewed, modeled, and statistically analyzed. This provides the basis for using ultrasonic velocity to interrogate microstructure. The effect of pore fraction (0.10-0.25) on superconductor properties of YBCO samples was characterized. Spatial (within-sample) variations in microstructure and superconductor properties were investigated, and the effect of oxygen content on elastic behavior was examined. Experimental methods used included a.c. susceptibility, electrical, and ultrasonic velocity measurements. Superconductor properties measured included transition temperature, magnetic transition width, transport and magnetic critical current density, magnetic shielding, a.c. loss, and sharpness of the voltage-current characteristics. An ultrasonic velocity image constructed from measurements at 1mm increments across a YBCO sample revealed microstructural variations that correlated with variations in magnetic shielding and a.c. loss behavior. Destructive examination using quantitative image analysis revealed pore fraction to be the varying microstructural feature.

  8. Magnetic Susceptibility and Spin Exchange Interactions of the Hexagonal Perovskite-Type Oxides Sr 4/3(Mn 2/3Ni 1/3)O 3

    NASA Astrophysics Data System (ADS)

    El Abed, A.; Gaudin, E.; Darriet, J.; Whangbo, M.-H.

    2002-02-01

    Magnetic susceptibility measurements were carried out for two hexagonal perovskite-type oxides Sr1+x(Mn1-xNix)O3 with slightly different compositions (i.e., x={1}/{3} and 0.324). A significant difference in the susceptibilities of the two phases demonstrates the need to control phase compositions accurately. Sr4/3(Mn2/3Ni1/3)O3 consists of two spin sublattices, i.e., the Mn4+ and the Ni2+ ion sublattices. Spin dimer analysis was carried out to examine the relative strengths in the spin exchange interactions of the Mn4+ ion sublattice. The temperature dependence of the magnetic susceptibility of Sr4/3(Mn2/3Ni1/3)O3 was found consistent with a picture in which the Mn4+ ion sublattice has weakly interacting antiferromagnetically coupled (Mn4+)2 dimers, the Ni2+ ion sublattice acts as a paramagnetic system, and the two sublattices are nearly independent.

  9. Efficient enhancement of magnetic anisotropy by optimizing the ligand-field in a typically tetranuclear dysprosium cluster.

    PubMed

    Liu, Jiang; Chen, Yan-Cong; Jiang, Zhong-Xia; Liu, Jun-Liang; Jia, Jian-Hua; Wang, Long-Fei; Li, Quan-Wen; Tong, Ming-Liang

    2015-05-07

    The perturbation to the ligand field around the lanthanide ion may significantly contribute to the magnetic dynamics of single molecule magnets. This can be demonstrated by two typical Dy4 cluster-based single molecular magnets (SMMs), [Dy4X2(μ3-OH)2(μ-OH)2(2,2-bpt)4(H2O)4]X2·2H2O·4EtOH (X = Cl and Br for and , respectively), which were constructed by using 3,5-bis(pyridin-2-yl)-1,2,4-triazole (2,2-bptH) as the polynuclear-chelating ligand. Alternating-current (ac) magnetic susceptibility measurements show that the energy barriers in complexes and were immensely enhanced by comparing with our previous work due to the optimization of the ligand field around Dy(III) ions. Remarkably, their high thermal active barriers at 190 K () and 197 K () under a zero applied external dc magnetic field are also among the highest within the reported tetranuclear lanthanide-based SMMs.

  10. Magnetocaloric effect of polycrystalline Sm0.5Ca0.5MnO3 compound: Investigation of low temperature magnetic state

    NASA Astrophysics Data System (ADS)

    Das, Kalipada; Banu, Nasrin; Das, I.; Dev, B. N.

    2018-06-01

    An attempt has been made to probe low temperature magnetic state of the polycrystalline Sm0.5Ca0.5MnO3 compound via magnetization and magnetocaloric studies. In the context of the earlier debatable reports on the above mentioned compound between the existence of glassy magnetic state and small ferromagnetic domains from the 'ac' susceptibility measurements, our experimental observation from magnetocaloric effect study clearly indicates the existence of ferromagnetic droplets along with certain amount of superparamagnetic component at low temperature (< 40 K) which begins at T ∼ 100 K. In addition to that, the zero field cooled magnetization (even at H = 0.01 T) data do not exhibit the spin freezing nature at the low temperature which is almost a generic tendency of glassy magnetic state. Our study also highlights the competence of magnetocaloric effect as a tool to distinguish between different magnetic states of a compound.

  11. Structural and AC loss study for pure and doped MgB{sub 2} superconductor

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Hansdah, J. S.; Sarun, P. M., E-mail: sarun.res@gmail.com

    2015-06-24

    Superconducting polycrystalline bulk MgB{sub 2} samples doped with n-C, n-Y{sub 2}O{sub 3} and n-Ho{sub 2}O{sub 3} were prepared by powder-in-sealed (PIST) method. XRD measurement shows the influence of dopants on phase and lattice parameters of samples. The ac susceptibility measurement reveals ac loss and activation energy of the samples. Nano-C doped sample shows less ac loss in all frequency (208 Hz – 999 Hz) among the doped samples; whereas n-Ho{sub 2}O{sub 3} doped sample shows highest ac loss. The activation energy is high for rare earth (n-Y{sub 2}O{sub 3} and n-Ho{sub 2}O{sub 3}) doped samples as compare to n-C doped samples whichmore » reveals the enhancement in flux-pinning properties of these materials.« less

  12. Efficacy of Genetically Modified Bt Toxins Alone and in Combinations Against Pink Bollworm Resistant to Cry1Ac and Cry2Ab

    PubMed Central

    Tabashnik, Bruce E.; Fabrick, Jeffrey A.; Unnithan, Gopalan C.; Yelich, Alex J.; Masson, Luke; Zhang, Jie; Bravo, Alejandra; Soberón, Mario

    2013-01-01

    Evolution of resistance in pests threatens the long-term efficacy of insecticidal proteins from Bacillus thuringiensis (Bt) used in sprays and transgenic crops. Previous work showed that genetically modified Bt toxins Cry1AbMod and Cry1AcMod effectively countered resistance to native Bt toxins Cry1Ab and Cry1Ac in some pests, including pink bollworm (Pectinophora gossypiella). Here we report that Cry1AbMod and Cry1AcMod were also effective against a laboratory-selected strain of pink bollworm resistant to Cry2Ab as well as to Cry1Ab and Cry1Ac. Resistance ratios based on the concentration of toxin killing 50% of larvae for the resistant strain relative to a susceptible strain were 210 for Cry2Ab, 270 for Cry1Ab, and 310 for Cry1Ac, but only 1.6 for Cry1AbMod and 2.1 for Cry1AcMod. To evaluate the interactions among toxins, we tested combinations of Cry1AbMod, Cry1Ac, and Cry2Ab. For both the resistant and susceptible strains, the net results across all concentrations tested showed slight but significant synergism between Cry1AbMod and Cry2Ab, whereas the other combinations of toxins did not show consistent synergism or antagonism. The results suggest that the modified toxins might be useful for controlling populations of pink bollworm resistant to Cry1Ac, Cry2Ab, or both. PMID:24244692

  13. Magnetic susceptibility mapping of fly ash in soil samples near a coal-burning power plant in Pointe Coupee Parish, Louisiana.

    NASA Astrophysics Data System (ADS)

    Elhelou, O.; Richter, C.

    2015-12-01

    Atmospheric deposition of pollutants is a major health and environmental concern. In a 2010 study, the CATF attributed over 13,000 deaths each year to fly ash and other fine particles emitted by U.S. coal-burning power plants. The magnetic properties of fly ash allows for mapping an area suspect of PM pollution faster and more efficiently than by conducting chemical analysis as the former alternative. The objective of this study is to detect the presence of magnetic particles related to the migration of fly ash from a nearby coal power plant over parts of Pointe Coupee Parish, LA. This is based on the idea that the fly ash that is released into the atmosphere during the coal burning process contains heavy metals and magnetic particles in the form of ferrospheres, which can be used to trace back to the source. Maps of the top and sub soil were generated to differentiate the magnetic susceptibility values of the heavy metals potentially attributed to the migration and settling of fly ash onto the surface from any pre-existing or naturally occurring heavy metals in the sub soil. A 60 km2 area in Pointe Coupee Parish was investigated in approximately 0.5 km2 subsets. The area in Pointe Coupee Parish, LA was selected because land use is predominantly rural with the Big Cajun II power plant as the main contributor for air borne contaminants. Samples of fly ash obtained directly from the source below one of the power plant's precipitators were also analyzed to verify the field and laboratory analysis. Contour maps representing the spatial distribution of fly ash over Pointe Coupee, LA, along with histograms of magnetic susceptibility values, and chemical analysis all indicate a correlation between the proximity to the power plant and the predominant wind direction. Acquisition curves of the isothermal remnant magnetization demonstrate the presence of predominantly low coercivity minerals (magnetite) with a small amount of a high-coercivity phase. The microstructure of the

  14. Synthesis, structure, luminescence, and magnetic properties of a single-ion magnet "mer"-[tris(N-[(imidazol-4-yl)-methylidene]-DL-phenylalaninato)terbium(III) and related "fac"-DL-alaninato derivative.

    PubMed

    Yamauchi, Suguru; Fujinami, Takeshi; Matsumoto, Naohide; Mochida, Naotaka; Ishida, Takayuki; Sunatsuki, Yukinari; Watanabe, Masayuki; Tsuchimoto, Masanobu; Coletti, Cecilia; Re, Nazzareno

    2014-06-16

    Two Tb(III) complexes with the same N6O3 donor atoms but different coordination geometries, "fac"-[Tb(III)(HL(DL-ala))3]·7H2O (1) and "mer"-[Tb(III)(HL(DL-phe))3]·7H2O (2), were synthesized, where H2L(DL-ala) and H2L(DL-phe) are N-[(imidazol-4-yl)methylidene]-DL-alanine and -DL-phenylalanine, respectively. Each Tb(III) ion is coordinated by three electronically mononegative NNO tridentate ligands to form a coordination geometry of a tricapped trigonal prism. Compound 1 consists of enantiomers "fac"-[Tb(III)(HL(D-ala))3] and "fac"-[Tb(III)(HL(L-ala))3], while 2 consists of "mer"-[Tb(III)(HL(D-phe))2(HL(L-phe))] and "mer"-[Tb(III)(HL(D-phe))(HL(L-phe))2]. Magnetic data were analyzed by a spin Hamiltonian including the crystal field effect on the Tb(III) ion (4f(8), J = 6, S = 3, L = 3, gJ = 3/2, (7)F6). The Stark splitting of the ground state (7)F6 was evaluated from magnetic analysis, and the energy diagram pattern indicated easy-plane and easy-axis (Ising type) magnetic anisotropies for 1 and 2, respectively. Highly efficient luminescences with Φ = 0.50 and 0.61 for 1 and 2, respectively, were observed, and the luminescence fine structure due to the (5)D4 → (7)F6 transition is in good accordance with the energy diagram determined from magnetic analysis. The energy diagram of 1 shows an approximate single-well potential curve, whereas that of 2 shows a double- or quadruple-well potential within the (7)F6 multiplets. Complex 2 displayed an onset of the out-of-phase signal in alternating current (ac) susceptibility at a direct current bias field of 1000 Oe on cooling down to 1.9 K. A slight frequency dependence was recorded around 2 K. On the other hand, 1 did not show any meaningful out-of-phase ac susceptibility. Pulsed-field magnetizations of 1 and 2 were measured below 1.6 K, and only 2 exhibited magnetic hysteresis. This finding agrees well with the energy diagram pattern from crystal field calculation on 1 and 2. DFT calculation allowed us to estimate the

  15. Interleukin-10 promoter 1082/-819/-592 polymorphisms are associated with asthma susceptibility in Asians and atopic asthma: a meta-analysis.

    PubMed

    Zheng, Xue-yan; Guan, Wei-jie; Mao, Chen; Chen, Hui-fang; Ding, Hong; Zheng, Jin-ping; Hu, Ting-ting; Luo, Min-hong; Huang, Yan-hui; Chen, Qing

    2014-02-01

    Although interleukin-10 (IL-10) is a potent inhibitor of allergic diseases, the association between promoter -1082/-819/-592 polymorphisms and asthma susceptibility remains inconclusive. We sought to determine if IL-10 promoter -1082/-819/-592 polymorphisms contribute to asthma susceptibility and are associated with phenotypes of atopic asthma. Systematic computerized searches were performed. Pooled odds ratios (ORs) and 95 % confidence intervals (CIs) were estimated by using random-effect and fixed-effect models, based on between-study heterogeneity. Subgroup analyses were performed according to age, ethnicity, and atopy. Publication bias was detected by funnel plot using Egger's test. A total of 4,716 asthmatic patients and 5,093 controls were included. The asthma susceptibility correlated significantly with IL-10 promoter gene -1082 polymorphism [OR (95 % CI) 1.26 (1.02, 1.55) for AA vs. AG + GG] and -592 polymorphism [OR (95 % CI) 1.12 (1.07, 1.34) for AC + AA vs. CC] (both P < 0.05), but not with -819 polymorphism (P > 0.05). Subgroup analyzes suggested that the AA versus AG + GG genotype of -1082A/G polymorphism and AC + AA versus CC genotype of -592A/C polymorphism contributed significantly to increased asthma susceptibility in adults [OR (95 % CI) 1.39 (1.03, 1.87) for -1082A/G and 1.53 (1.25, 1.87) for -592A/C polymorphism]. The Asian population [OR (95 % CI) 1.35 (1.1, 1.7) for -1082A/G and 1.4 (1.12, 1.64) for -592A/C polymorphism] and subjects with atopic asthma [OR (95 % CI) 1.49 (1.18, 1.88) for -1082A/G and 1.23 (1.01, 1.48) for -592A/C polymorphism] also had an increased susceptibility of asthma. No publication bias was detected. IL-10 promoter -1028A/G, -592A/C polymorphisms and their haplotypes, but not -819T/C polymorphism, correlate with asthma susceptibility.

  16. A Method for Whole Brain Ex Vivo Magnetic Resonance Imaging with Minimal Susceptibility Artifacts

    PubMed Central

    Shatil, Anwar S.; Matsuda, Kant M.; Figley, Chase R.

    2016-01-01

    Magnetic resonance imaging (MRI) is a non-destructive technique that is capable of localizing pathologies and assessing other anatomical features (e.g., tissue volume, microstructure, and white matter connectivity) in postmortem, ex vivo human brains. However, when brains are removed from the skull and cerebrospinal fluid (i.e., their normal in vivo magnetic environment), air bubbles and air–tissue interfaces typically cause magnetic susceptibility artifacts that severely degrade the quality of ex vivo MRI data. In this report, we describe a relatively simple and cost-effective experimental setup for acquiring artifact-free ex vivo brain images using a clinical MRI system with standard hardware. In particular, we outline the necessary steps, from collecting an ex vivo human brain to the MRI scanner setup, and have also described changing the formalin (as might be necessary in longitudinal postmortem studies). Finally, we share some representative ex vivo MRI images that have been acquired using the proposed setup in order to demonstrate the efficacy of this approach. We hope that this protocol will provide both clinicians and researchers with a straight-forward and cost-effective solution for acquiring ex vivo MRI data from whole postmortem human brains. PMID:27965620

  17. Superconductivity of Cu/CuOx interface formed by shock-wave pressure

    NASA Astrophysics Data System (ADS)

    Shakhray, D. V.; Avdonin, V. V.; Palnichenko, A. V.

    2016-11-01

    A mixture of powdered Cu and CuO has been subjected to shock-wave pressure of 350 kbar with following quenching of the vacuum-encapsulated product to 77 K. The ac magnetic susceptibility measurements of the samples have revealed metastable superconductivity with Tc ≈ 19 K, characterized by glassy dynamics of the shielding currents below Tc . Comparison of the ac susceptibility and the DC magnetization measurements infers that the superconductivity arises within the granular interfacial layer formed between metallic Cu and its oxides due to the shock-wave treatment.

  18. A magnetic nanobead-based bioassay provides sensitive detection of single- and biplex bacterial DNA using a portable AC susceptometer

    PubMed Central

    Strömberg, Mattias; Zardán Gómez de la Torre, Teresa; Nilsson, Mats; Svedlindh, Peter; Strømme, Maria

    2014-01-01

    Bioassays relying on magnetic read-out using probe-tagged magnetic nanobeads are potential platforms for low-cost biodiagnostic devices for pathogen detection. For optimal assay performance it is crucial to apply an easy, efficient and robust bead-probe conjugation protocol. In this paper, sensitive (1.5 pM) singleplex detection of bacterial DNA sequences is demonstrated in a portable AC susceptometer by a magnetic nanobead-based bioassay principle; the volume-amplified magnetic nanobead detection assay (VAM-NDA). Two bead sizes, 100 and 250 nm, are investigated along with a highly efficient, rapid, robust, and stable conjugation chemistry relying on the avidin–biotin interaction for bead-probe attachment. Avidin-biotin conjugation gives easy control of the number of detection probes per bead; thus allowing for systematic investigation of the impact of varying the detection probe surface coverage upon bead immobilization in rolling circle amplified DNA-coils. The existence of an optimal surface coverage is discussed. Biplex VAM-NDA detection is for the first time demonstrated in the susceptometer: Semi-quantitative results are obtained and it is concluded that the concentration of DNA-coils in the incubation volume is of crucial importance for target quantification. The present findings bring the development of commercial biodiagnostic devices relying on the VAM–NDA further towards implementation in point-of-care and outpatient settings. PMID:24174315

  19. Evidence for a low-temperature magnetic ground state in double-perovskite iridates with I r5 +(5 d4) ions

    NASA Astrophysics Data System (ADS)

    Terzic, J.; Zheng, H.; Ye, Feng; Zhao, H. D.; Schlottmann, P.; De Long, L. E.; Yuan, S. J.; Cao, G.

    2017-08-01

    We report an unusual magnetic ground state in single-crystal, double-perovskite B a2YIr O6 and Sr-doped B a2YIr O6 with I r5 +(5 d4) ions. Long-range magnetic order below 1.7 K is confirmed by dc magnetization, ac magnetic susceptibility, and heat-capacity measurements. The observed magnetic order is extraordinarily delicate and cannot be explained in terms of either a low-spin S =1 state, or a singlet Jeff=0 state imposed by the spin-orbit interactions (SOI). Alternatively, the magnetic ground state appears consistent with a SOI that competes with comparable Hund's rule coupling and inherently large electron hopping, which cannot stabilize the singlet Jeff=0 ground state. However, this picture is controversial, and conflicting magnetic behavior for these materials is reported in both experimental and theoretical studies, which highlights the intricate interplay of interactions that determine the ground state of materials with strong SOI.

  20. Detail study on ac-dc magnetic and dye absorption properties of Fe3O4 hollow spheres for biological and industrial application.

    PubMed

    Sarkar, Debasish; Mandal, Kalyan; Mandal, Madhuri

    2014-03-01

    Here solvo-thermal technique has been used to synthesize hollow-nanospheres of magnetite. We have shown that PVP plays an important role to control the particle size and also helps the particles to take the shape of hollow spheres. Structural analysis was done by XRD measurement and morphological measurements like SEM and TEM were performed to confirm the hollow type spherical particles formation and their shape and sizes were also investigated. The detail ac-dc magnetic measurements give an idea about the application of these nano spheres for hyperthermia therapy and spontaneous dye adsorption properties (Gibbs free energy deltaG0 = -0.526 kJ/mol for Eosin and -1.832 kJ/mol for MB) of these particles indicate its use in dye manufacturing company. Being hollow in structure and magnetic in nature such materials will also be useful in other application fields like in drug delivery, arsenic and heavy metal removal by adsorption technique, magnetic separation etc.

  1. Low-temperature magnetic study of naturally and experimentally shocked pyrrhotite

    NASA Astrophysics Data System (ADS)

    Mang, C.; Kontny, A. M.; Hecht, L.

    2011-12-01

    The most intriguing observation from the suevite unit of the 35 Ma old Chesapeake Bay impact structure (CBIS), Virginia, USA, is the occurrence of "shocked pyrrhotite", which might provide clues for a better understanding of the acquisition of shock-induced remagnetization during an impact event. A large range of differently strong deformed and melted components are mixed in the suevite and maximum shock pressures up to 35 GPa are reported (Wittmann et al. 2009). Pyrrhotite occurs as grains and grain clusters within the suevite matrix and rarely in melt fragments, and abundant lattice defects in pyrrhotite prove a shock-induced deformation. The shocked mineral is characterized by a significant loss of iron and the stoichiometric formula lies between Fe0.808S and Fe0.811S. This composition falls significantly below the Fe/S ratio of regular pyrrhotite (Fe>0.875) and is similar to the one of smythite (Fe9S11). The Curie temperature (TC) is above that of the ferrimagnetic 4C modification (320°C) and lies between 350 and 365°C. However, a transition at 30 K (Rochette et al. 1990), visible in low temperature remanence curves, confirms the presence of ferrimagnetic monoclinic 4C pyrrhotite.The present work aims at the question if all these different features observed in the natural pyrrhotite from the CBIS suevite are impact-related. Therefore we experimentally shocked a pyrrhotite ore from the Cerro de Pasco mine, Peru at 3, 5, 8, 20 and 30 GPa using a high pressure gun and high explosive devices. The obtained samples have been investigated by low-temperature AC susceptibility and remanence measurements (LT). In addition, we determined TC using AC susceptibility as function of temperature. LT experiments of the pyrrhotite ore unfortunately do not only show magnetic transition temperatures related to pure pyrrhotite but additionally of accessory magnetic mineral phases like magnetite (Fe3O4) and pyrophanite (MnTiO3). The contribution of those phases makes especially

  2. Magnetic susceptibility of spider webs as a proxy of airborne metal pollution.

    PubMed

    Rachwał, Marzena; Rybak, Justyna; Rogula-Kozłowska, Wioletta

    2018-03-01

    The purpose of this pilot study was to test spider webs as a fast tool for magnetic biomonitoring of air pollution. The study involved the investigation of webs made by four types of spiders: Pholcus phalangioides (Pholcidae), Eratigena atrica and Agelena labirynthica (Agelenidae) and Linyphia triangularis (Linyphiidae). These webs were obtained from outdoor and indoor study sites. Compared to the clean reference webs, an increase was observed in the values of magnetic susceptibility in the webs sampled from both indoor and outdoor sites, which indicates contamination by anthropogenically produced pollution particles that contain ferrimagnetic iron minerals. This pilot study has demonstrated that spider webs are able to capture particulate matter in a manner that is equivalent to flora-based bioindicators applied to date (such as mosses, lichens, leaves). They also have additional advantages; for example, they can be generated in isolated clean habitats, and exposure can be monitored in indoor and outdoor locations, at any height and for any period of time. Moreover, webs are ubiquitous in an anthropogenic, heavily polluted environment, and they can be exposed throughout the year. As spider webs accumulate pollutants to which humans are exposed, they become a reliable source of information about the quality of the environment. Therefore, spider webs are recommended for magnetic biomonitoring of airborne pollution and for the assessment of the environment because they are non-destructive, low-cost, sensitive and efficient. Copyright © 2017 Elsevier Ltd. All rights reserved.

  3. Chilo suppressalis and Sesamia inferens display different susceptibility responses to Cry1A insecticidal proteins.

    PubMed

    Li, Bo; Xu, Yangyang; Han, Cao; Han, Lanzhi; Hou, Maolin; Peng, Yufa

    2015-10-01

    Chilo suppressalis and Sesamia inferens are important lepidopteran rice pests that occur concurrently in rice-growing areas of China. The development of transgenic rice expressing Cry1A insecticidal proteins has provided a useful strategy for controlling these pests. This study evaluated the baseline susceptibilities of C. suppressalis and S. inferens to Cry1A, as well as their responses to selection with Cry1A. Wide geographic variation in susceptibility was observed across all field populations. Within a given population, the LC50 of both Cry1Ab and Cry1Ac against S. inferens was drastically higher than that of C. suppressalis. Large LC50 differences (74.6-fold) were detected between the two species for Cry1Ab in the Poyang population, while small differences (3.6-fold) were detected for Cry1Ac in the Changsha population. The Cry1Ac LC50 of C. suppressalis and S. inferens increased 8.4- and 4.4-fold after 21 and eight selection generations respectively. Additionally, the estimated realised heritabilities (h(2) ) of Cry1Ac tolerance were 0.11 in C. suppressalis and 0.292 in S. inferens. S. inferens exhibited a significantly lower susceptibility and more rapidly evolved resistance to Cry1A compared with C. suppressalis. Therefore, S. inferens is more likely to evolve increased resistance, which threatens the sustainability of rice expressing Cry1A protein. © 2014 Society of Chemical Industry.

  4. Zn induced in-gap electronic states in La214 probed by uniform magnetic susceptibility: relevance to the suppression of superconducting T c

    NASA Astrophysics Data System (ADS)

    Islam, R. S.; Naqib, S. H.

    2018-02-01

    Substitution of isovalent non-magnetic defects, such as Zn, in the CuO2 plane strongly modifies the magnetic properties of strongly electron correlated hole doped cuprate superconductors. The reason for enhanced uniform magnetic susceptibility, χ, in Zn substituted cuprates is debatable. Generally the defect induced magnetic behavior has been analyzed mainly in terms of two somewhat contrasting scenarios. The first one is due to independent localized moments appearing in the vicinity of Zn arising because of the strong electronic/magnetic correlations present in the host compound and the second one is due to transfer of quasiparticle (QP) spectral weight and creation of weakly localized low-energy electronic states associated with each Zn atom in place of an in-plane Cu. If the second scenario is correct, one should expect a direct correspondence between Zn induced suppression of the superconducting transition temperature, T c, and the extent of the enhanced magnetic susceptibility at low temperature. In this case, the low-T enhancement of χ would be due to weakly localized QP states at low energy and these electronic states will be precluded from taking part in Cooper pairing. We explore this second possibility by analyzing the χ(T) data for La2-x Sr x Cu1-y Zn y O4 with different hole contents, p (=x), and Zn concentrations (y) in this paper. The results of our analysis support this scenario.

  5. Superconducting shielded core reactor with reduced AC losses

    DOEpatents

    Cha, Yung S.; Hull, John R.

    2006-04-04

    A superconducting shielded core reactor (SSCR) operates as a passive device for limiting excessive AC current in a circuit operating at a high power level under a fault condition such as shorting. The SSCR includes a ferromagnetic core which may be either closed or open (with an air gap) and extends into and through a superconducting tube or superconducting rings arranged in a stacked array. First and second series connected copper coils each disposed about a portion of the iron core are connected to the circuit to be protected and are respectively wound inside and outside of the superconducting tube or rings. A large impedance is inserted into the circuit by the core when the shielding capability of the superconducting arrangement is exceeded by the applied magnetic field generated by the two coils under a fault condition to limit the AC current in the circuit. The proposed SSCR also affords reduced AC loss compared to conventional SSCRs under continuous normal operation.

  6. Magnetic susceptibility in the normal phase of Bi2Sr2CaCu2O8+δ single crystals

    NASA Astrophysics Data System (ADS)

    Lopes, Lutiene F.; Peña, J. Paola; Schaf, Jacob; Tumelero, Milton A.; Vieira, Valdemar N.; Pureur, Paulo

    2018-05-01

    We report on measurements of the c-axis component of the magnetic susceptibility in the normal phase of several single crystal samples of the Bi2Sr2CaCu2O8+δ cuprate superconductor. These crystal were submitted to appropriate heat treatments so that the density of hole carriers could be varied in an extended region of the superconducting dome. In general, the measured susceptibility shows significant temperature dependence, which was attributed to the pseudogap phenomenon. The results were interpreted with basis on a phenomenological model that allows the determination of the pseudogap characteristic temperature T* as a function of the carrier density.

  7. An interleaved sequence for simultaneous magnetic resonance angiography (MRA), susceptibility weighted imaging (SWI) and quantitative susceptibility mapping (QSM).

    PubMed

    Chen, Yongsheng; Liu, Saifeng; Buch, Sagar; Hu, Jiani; Kang, Yan; Haacke, E Mark

    2018-04-01

    To image the entire vasculature of the brain with complete suppression of signal from background tissue using a single 3D excitation interleaved rephased/dephased multi-echo gradient echo sequence. This ensures no loss of signal from fast flow and provides co-registered susceptibility weighted images (SWI) and quantitative susceptibility maps (QSM) from the same scan. The suppression of background tissue was accomplished by subtracting the flow-dephased images from the flow-rephased images with the same echo time of 12.5ms to generate a magnetic resonance angiogram and venogram (MRAV). Further, a 2.5ms flow-compensated echo was added in the rephased portion to provide sufficient signal for major arteries with fast flow. The QSM data from the rephased 12.5ms echo was used to suppress veins on the MRAV to generate an artery-only MRA. The proposed approach was tested on five healthy volunteers at 3T. This three-echo interleaved GRE sequence provided complete background suppression of stationary tissues, while the short echo data gave high signal in the internal carotid and middle cerebral arteries (MCA). The contrast-to-noise ratio (CNR) of the arteries was significantly improved in the M3 territory of the MCA compared to the non-linear subtraction MRA and TOF-MRA. Veins were suppressed successfully utilizing the QSM data. The background tissue can be properly suppressed using the proposed interleaved MRAV sequence. One can obtain whole brain MRAV, MRA, SWI, true-SWI (or tSWI) and QSM data simultaneously from a single scan. Published by Elsevier Inc.

  8. Magnetism and 155Gd Mössbauer spectroscopy of GdAuMg

    NASA Astrophysics Data System (ADS)

    Łątka, Kazimierz; Kmieć, Roman; Pacyna, Andrzej W.; Fickenscher, Thomas; Hoffmann, Rolf-Dieter; Pöttgen, Rainer

    2004-03-01

    GdAuMg was synthesized by reaction of the elements in a sealed tantalum ampule in a high-frequency furnace. The structure was investigated by X-ray diffraction on both powders and single crystals: ZrNiAl type, P 6¯2m , a=756.3(1), c=412.71(7) pm, wR2=0.0285 for 308 F2 values, 14 variables. Geometrical motifs of the GdAuMg structure are gold centered tricapped trigonal prisms [Au1Mg 3Gd 6] and [Au2Mg 6Gd 3]. Together the gold and magnesium atoms form a three-dimensional [AuMg] network in which the gadolinium atoms fill distorted hexagonal channels. Bulk magnetic properties have been investigated by means of AC and DC magnetic susceptibility measurements and 155Gd Mössbauer spectroscopy was used to monitor the local electronic and magnetic structure. Two magnetic phase transitions were found. One transition, at T1= TN=81.1(1) K, is from a paramagnetic to an antiferromagnetic state of collinear character and the other at T2=19.0(1) from the antiferromagnetic to a kind of canted magnetic ordering characterized by a very narrow hysteresis loop.

  9. Three dimensional lithospheric magnetization structures beneath Australia derived by inverse modeling of CHAMP satellite magnetic field model

    NASA Astrophysics Data System (ADS)

    Du, Jinsong; Chen, Chao; Lesur, Vincent; Li, Yaoguo; Lane, Richard; Liang, Qing; Wang, Haoran

    2014-05-01

    We present an inversion algorithm for magnetic anomaly data in spherical coordinates to image the three dimensional (3-D) susceptibility distributions in the lithosphere. The method assumes that remanent magnetization is absent and that the magnetic anomalies are solely the result of lateral variations in magnetic susceptibility. To take into account the curvature of the Earth, the 3-D model is comprised of a set of spherical prisms (referred to as tesseroids), each of which has a constant isotropic susceptibility. The inversion method is formulated with a specifically designed model objective function and radial weighting function in spherical coordinates. A Tikhonov regularization technique is used to obtain an optimal solution with data misfit consistent with the estimated error level. Results for regional synthetic models with different magnetized inclinations and declinations are presented to demonstrate the capability of the method to recover large scale lithospheric magnetic structures. We have applied the algoithm to study the lithospheric susceptibility structures in the Australia region using magnetic anomaly data from the GRIMM_L120v0.0 model, which is based on ten years of CHAMP satellite data. As a self-constrained inversion, the maximum depths variation of magnetization layer is estimated first and then incorporated to the three dimensional (3-D) inversion. Results showed that the susceptibility anomalies concentrate in the depth range from 25 km to 45 km, i.e., focused in the lower crust. In addition, the results showed that the susceptibilities in continental lithosphere are higher than those in oceanic lithosphere. The inverted 3-D susceptibility distribution in the region of Australia reveals significant features related to tectonics, surface heat-flux, crustal thickness and Curie isotherm depths. In general, the higher susceptibility anomalies correlate with Precambrian rocks, and the lower susceptibility anomalies correlate with younger orogenic

  10. Anatomy of the chiral magnetic effect in and out of equilibrium

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Kharzeev, Dmitri; Stephanov, Mikhail; Yee, Ho-Ung

    Here, we identify a new contribution to the chiral magnetic conductivity at finite frequencies—the magnetization current. This allows us to quantitatively reproduce the known field-theoretic time-dependent (AC) chiral magnetic response in terms of kinetic theory. We also evaluate the corresponding AC chiral magnetic conductivity in two-flavor QCD plasma at weak coupling. The magnetization current results from the spin response of chiral quasiparticles to magnetic field, and is thus proportional to the quasiparticle’s g -factor. Furthemrore, in condensed matter systems, where the chiral quasiparticles are emergent and the g -factor can significantly differ from 2, this opens up the possibility ofmore » tuning the AC chiral magnetic response.« less

  11. Anatomy of the chiral magnetic effect in and out of equilibrium

    DOE PAGES

    Kharzeev, Dmitri; Stephanov, Mikhail; Yee, Ho-Ung

    2017-03-28

    Here, we identify a new contribution to the chiral magnetic conductivity at finite frequencies—the magnetization current. This allows us to quantitatively reproduce the known field-theoretic time-dependent (AC) chiral magnetic response in terms of kinetic theory. We also evaluate the corresponding AC chiral magnetic conductivity in two-flavor QCD plasma at weak coupling. The magnetization current results from the spin response of chiral quasiparticles to magnetic field, and is thus proportional to the quasiparticle’s g -factor. Furthemrore, in condensed matter systems, where the chiral quasiparticles are emergent and the g -factor can significantly differ from 2, this opens up the possibility ofmore » tuning the AC chiral magnetic response.« less

  12. Geophysical monitoring of simulated graves with resistivity, magnetic susceptibility, conductivity and GPR in Colombia, South America.

    PubMed

    Molina, Carlos Martin; Pringle, Jamie K; Saumett, Miguel; Evans, Gethin T

    2016-04-01

    In most Latin American countries there are significant numbers of both missing people and forced disappearances, ∼71,000 Colombia alone. Successful detection of buried human remains by forensic search teams can be difficult in varying terrain and climates. Three clandestine burials were simulated at two different depths commonly encountered in Latin America. In order to gain critical knowledge of optimum geophysical detection techniques, burials were monitored using: ground penetrating radar, magnetic susceptibility, bulk ground conductivity and electrical resistivity up to twenty-two months post-burial. Radar survey results showed good detection of modern 1/2 clothed pig cadavers throughout the survey period on 2D profiles, with the 250MHz antennae judged optimal. Both skeletonised and decapitated and burnt human remains were poorly imaged on 2D profiles with loss in signal continuity observed throughout the survey period. Horizontal radar time slices showed good anomalies observed over targets, but these decreased in amplitude over the post-burial time. These were judged due to detecting disturbed grave soil rather than just the buried targets. Magnetic susceptibility and electrical resistivity were successful at target detection in contrast to bulk ground conductivity surveys which were unsuccessful. Deeper burials were all harder to image than shallower ones. Forensic geophysical surveys should be undertaken at suspected burial sites. Copyright © 2016 Elsevier Ireland Ltd. All rights reserved.

  13. Effect of alignment of easy axes on dynamic magnetization of immobilized magnetic nanoparticles

    NASA Astrophysics Data System (ADS)

    Yoshida, Takashi; Matsugi, Yuki; Tsujimura, Naotaka; Sasayama, Teruyoshi; Enpuku, Keiji; Viereck, Thilo; Schilling, Meinhard; Ludwig, Frank

    2017-04-01

    In some biomedical applications of magnetic nanoparticles (MNPs), the particles are physically immobilized. In this study, we explore the effect of the alignment of the magnetic easy axes on the dynamic magnetization of immobilized MNPs under an AC excitation field. We prepared three immobilized MNP samples: (1) a sample in which easy axes are randomly oriented, (2) a parallel-aligned sample in which easy axes are parallel to the AC field, and (3) an orthogonally aligned sample in which easy axes are perpendicular to the AC field. First, we show that the parallel-aligned sample has the largest hysteresis in the magnetization curve and the largest harmonic magnetization spectra, followed by the randomly oriented and orthogonally aligned samples. For example, 1.6-fold increase was observed in the area of the hysteresis loop of the parallel-aligned sample compared to that of the randomly oriented sample. To quantitatively discuss the experimental results, we perform a numerical simulation based on a Fokker-Planck equation, in which probability distributions for the directions of the easy axes are taken into account in simulating the prepared MNP samples. We obtained quantitative agreement between experiment and simulation. These results indicate that the dynamic magnetization of immobilized MNPs is significantly affected by the alignment of the easy axes.

  14. Observation of unusual critical region behavior in the magnetic susceptibility of EuSe

    NASA Astrophysics Data System (ADS)

    Bykovetz, N.; Klein, J.; Lin, C. L.

    2018-05-01

    The Europium Chalcogenides (EuCh: EuO, EuS, EuSe, and EuTe) have been regarded as model examples of simple, cubic, Heisenberg exchange coupled magnetic systems, with a ferromagnetic nearest-neighbor exchange constant J1 and an antiferromagnetic next-nearest-neighbor constant J2. Unlike the other EuCh, EuSe exhibits a range of complex magnetic behaviors, the latter being attributed to EuSe being near the point where J2=-J1, where its magnetism appears to consist of nearly de-coupled 2D ferromagnetic sheets. Analysis of precision SQUID measurements of the magnetic susceptibility χ in EuSe showed that in the region from ˜Tc to ˜2Tc, a fit of the data to the critical equation χ = χ2Tc(T/Tc-1)-γ gives γ=2.0, an exponent not predicted by any current theory. Additionally, this fit predicts that Tc should be ˜0K. We tentatively interpret this by saying that in the paramagnetic region the system "thinks" EuSe should not order above T=0. Tc=0K is predicted by the Mermin-Wagner theorem (MW) for Heisenberg-coupled 2D magnetic systems, and we can show that when J2=-J1, MW can also be applied to the J1, J2 exchange model of the EuCh to give a rigorous Tc=0 prediction. Under 10 kbar applied pressure EuSe exhibits a different γ and fitted Tc. An additional, and rather strange, critical-region effect was discovered. The EuSe sample was found to exhibit a relaxation effect in a small range of temperatures, just above and just below the actual Tc of 4.7K, with time constants of up to 5 minutes. We cannot yet fully explain this observed macroscopic effect.

  15. AC losses and stability on large cable-in-conduit superconductors

    NASA Astrophysics Data System (ADS)

    Bruzzone, Pierluigi

    1998-12-01

    The cable-in-conduit superconductors are preferred for applications where the AC losses and stability are a major concern, e.g., fusion magnets and SMES. A review of coupling currents loss results for both NbTi and Nb 3Sn cable-in-conduit conductors (CICC) is presented and the AC loss relevant features are listed, with special emphasis for the role of the interstrand resistance and strand coating. The transient stability approach for CICCs is discussed and the analytical models are quoted as well as the relevant experimental database. The likely spectrum of transient disturbance in CICC is reviewed and the need to account for interstrand current sharing in the design is outlined. Eventually a practical criterion for the interstrand resistance is proposed to link the stability and AC loss design.

  16. Frequency-dependent tACS modulation of BOLD signal during rhythmic visual stimulation.

    PubMed

    Chai, Yuhui; Sheng, Jingwei; Bandettini, Peter A; Gao, Jia-Hong

    2018-05-01

    Transcranial alternating current stimulation (tACS) has emerged as a promising tool for modulating cortical oscillations. In previous electroencephalogram (EEG) studies, tACS has been found to modulate brain oscillatory activity in a frequency-specific manner. However, the spatial distribution and hemodynamic response for this modulation remains poorly understood. Functional magnetic resonance imaging (fMRI) has the advantage of measuring neuronal activity in regions not only below the tACS electrodes but also across the whole brain with high spatial resolution. Here, we measured fMRI signal while applying tACS to modulate rhythmic visual activity. During fMRI acquisition, tACS at different frequencies (4, 8, 16, and 32 Hz) was applied along with visual flicker stimulation at 8 and 16 Hz. We analyzed the blood-oxygen-level-dependent (BOLD) signal difference between tACS-ON vs tACS-OFF, and different frequency combinations (e.g., 4 Hz tACS, 8 Hz flicker vs 8 Hz tACS, 8 Hz flicker). We observed significant tACS modulation effects on BOLD responses when the tACS frequency matched the visual flicker frequency or the second harmonic frequency. The main effects were predominantly seen in regions that were activated by the visual task and targeted by the tACS current distribution. These findings bridge different scientific domains of tACS research and demonstrate that fMRI could localize the tACS effect on stimulus-induced brain rhythms, which could lead to a new approach for understanding the high-level cognitive process shaped by the ongoing oscillatory signal. © 2018 Wiley Periodicals, Inc.

  17. Intrinsic resonances and AC-dipole simulations of 3He in the AGS Booster

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Hock, Kiel; Meot, Francois; Huang, Haixin

    Polarized 3He collisions are part of future RHIC physics programs and of the eRHIC project. The anomalous magnetic moment of 3He (G=-4.184) is roughly three times greater than that of protons (G=1.793), a polarized species that is already used at the Collider-Accelerator complex at BNL. Because of the higher anomolous magnetic moment and possibly injecting into the AGS at rigidities beyond 7 T • m, 3He may have to cross depolarizing intrinsic resonances while accelerating in the Booster. To overcome these strong intrinsic resonances we look to an AC-dipole, which will need to be installed in the Booster. An AC-dipolemore » is a magnet that induces large betatron oscillations which forces the entire bunch to experience a stronger resonance and induce a spin flip of all particles. An artificial intrinsic resonance is created, with close proximity to the original intrinsic resonance, which requires simulations to gauge what magnet strength is required. Simulations have been performed using zgoubi regarding the resonances 0 + v y, 12 - v y, and 6 + v y and show that the AC-dipole is effective at overcoming these resonances. Benefits of avoiding the 0 + v y and crossing the 12 - v y and 6 + v y in the Booster presents the advantage of allowing injection above the 0 + v y in the AGS and minimizes the orbit distortions from the snakes.« less

  18. AC Initiation System.

    DTIC Science & Technology

    An ac initiation system is described which uses three ac transmission signals interlocked for safety by frequency, phase, and power discrimination...The ac initiation system is pre-armed by the application of two ac signals have the proper phases, and activates a load when an ac power signal of the proper frequency and power level is applied. (Author)

  19. Molecular engineering of lanthanide ion chelating phospholipids generating assemblies with a switched magnetic susceptibility.

    PubMed

    Isabettini, Stéphane; Massabni, Sarah; Hodzic, Arnel; Durovic, Dzana; Kohlbrecher, Joachim; Ishikawa, Takashi; Fischer, Peter; Windhab, Erich J; Walde, Peter; Kuster, Simon

    2017-08-09

    Lanthanide ion (Ln 3+ ) chelating amphiphiles are powerful molecules for tailoring the magnetic response of polymolecular assemblies. Mixtures of 1,2-dimyristoyl-sn-glycero-3-phosphocholine (DMPC) and 1,2-dimyristoyl-sn-glycero-3-phospho-ethanolamine-diethylene triaminepentaacetate (DMPE-DTPA) complexed to Ln 3+ deliver highly magnetically responsive bicelles. Their magnetic properties are readily tuned by changing the bicellar size or the magnetic susceptibility Δχ of the bilayer lipids. The former technique is intrinsically bound to the region of the phase diagram guarantying the formation of bicelles. Methods aiming towards manipulating the Δχ of the bilayer are comparatively more robust, flexible and lacking. Herein, we synthesized a new Ln 3+ chelating phospholipid using glutamic acid as a backbone: DMPE-Glu-DTPA. The chelate polyhedron was specifically engineered to alter the Δχ, whilst remaining geometrically similar to DMPE-DTPA. Planar asymmetric assemblies hundreds of nanometers in size were achieved presenting unprecedented magnetic alignments. The DMPE-Glu-DTPA/Ln 3+ complex switched the Δχ, achieving perpendicular alignment of assemblies containing Dy 3+ and parallel alignment of those containing Tm 3+ . Moreover, samples with chelated Yb 3+ were more alignable than the Tm 3+ chelating counterparts. Such a possibility has never been demonstrated for planar Ln 3+ chelating polymolecular assemblies. The physico-chemical properties of these novel assemblies were further studied by monitoring the alignment behavior at different temperatures and by including 16 mol% of cholesterol (Chol-OH) in the phospholipid bilayer. The DMPE-Glu-DTPA/Ln 3+ complex and the resulting assemblies are promising candidates for applications in numerous fields including pharmaceutical technologies, structural characterization of membrane biomolecules by NMR spectroscopy, as contrasting agents for magnetic resonance imaging, and for the development of smart optical gels.

  20. Magnetic susceptibility for use in delineating hydric soils

    USGS Publications Warehouse

    Grimley, D.A.; Vepraskas, M.J.

    2000-01-01

    Field indicators are used to identify hydric soil boundaries and to delineate wetlands. The most common field indicators may not be seen in some soils with thick, dark, mollic epipedons, and do not form in Fe-poor soils. This study evaluated magnetic susceptibility (MS) meter as a field tool to determine hydric soil boundaries. Five Mollisoldominated sites formed in glacial deposits in Illinois were evaluated along with one Ultisol-dominated site formed in Coastal Plain sediments of North Carolina. Measurements of volumetric MS were made along transects at each site that extended from wetland into upland areas. One created wetland was evaluated. Field indicators were used to identify the hydric soils. Results showed that volumetric MS values were significantly (P 0.15) differences in MS were found for Coastal Plain hydric and nonhydric soils where MS values were low (<10 ?? 10-5 SI). Critical MS values that separated hydric and nonhydric soils varied between 20 ?? 10-5 and 30 ?? 10-5 SI for the loessal soils evaluated in Illinois. Such critical values will have to be determined on site using field indicators until specific values can be defined for hydric soils within a given parent material. With a critical MS value in hand, a wetland delineator can make MS measurements along transects perpendicular to the envisioned hydric soil boundary to quickly and quantitatively identify it.

  1. Superconducting and magnetic properties of RBa/sub 2/Cu/sub 3/O/sub 7-//sub x/ compounds

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Shaheen, S.A.; Jisrawi, N.; Lee, Y.H.

    Superconducting properties of RBa/sub 2/Cu/sub 3/O/sub 7-//sub x/ compounds (R = Y, La, Nd, Sm, Eu, Gd, Dy, Ho, Er, Tm, and Yb) have been studied by dc electrical resistivity and ac magnetic susceptibility techniques. Except for R = La, which is superconducting below 50 K, RBa/sub 2/Cu/sub 3/O/sub 7-//sub x/ compounds exhibit sharp resistive and inductive transitions in the 90-K range. The nearly constant value of T/sub c/ for magnetic R ions indicates a very weak interaction between R ions, as anticipated from the known crystal structure of these materials. The effects of annealing in oxygen and argon, andmore » air quenching, on the superconducting properties are also discussed.« less

  2. Determination of atomic site susceptibility tensors from neutron diffraction data on polycrystalline samples.

    PubMed

    Gukasov, A; Brown, P J

    2010-12-22

    Polarized neutron diffraction can provide information about the atomic site susceptibility tensor χ(ij) characterizing the magnetic response of individual atoms to an external magnetic field (Gukasov and Brown 2002 J. Phys.: Condens. Mater. 14 8831). The six independent atomic susceptibility parameters (ASPs) can be determined from polarized neutron flipping ratio measurements on single crystals and visualized as magnetic ellipsoids which are analogous to the thermal ellipsoids obtained from atomic displacement parameters (ADPs). We demonstrate now that the information about local magnetic susceptibility at different magnetic sites in a crystal can also be obtained from polarized and unpolarized neutron diffraction measurements on magnetized powder samples. The validity of the method is illustrated by the results of such measurements on a polycrystalline sample of Tb(2)Sn(2)O(7).

  3. A Magnetic Paradox

    ERIC Educational Resources Information Center

    Arndt, Ebe

    2006-01-01

    Two recent articles in this journal described how an air core solenoid connected to an ac power source may restore the magnetization of a bar magnet with an alternating magnetic field (see Figs. 1 and 2). Although we are quite accustomed to using a constant magnetic field in an air core solenoid to remagnetize a ferromagnet, it is puzzling that we…

  4. 87Sr/86Sr dating and preliminary interpretation of magnetic susceptibility logs of giant piston cores from the Rio Grande Rise in the South Atlantic

    NASA Astrophysics Data System (ADS)

    Lacasse, Christian Michel; Santos, Roberto Ventura; Dantas, Elton Luiz; Vigneron, Quentin; de Sousa, Isabela Moreno Cordeiro; Harlamov, Vadim; Lisniowski, Maria Aline; Pessanha, Ivo Bruno Machado; Frazão, Eugênio Pires; Cavalcanti, José Adilson Dias

    2017-12-01

    Giant piston cores recovered from shallow depths (<1200 mbsl) on the northern flank of the Rio Grande Rise, bathed today in intermediate waters (AAIW, UCDW), have uncovered new stratigraphic and paleoceanographic aspects of the Plio-Pleistocene in the South Atlantic. Based on strontium isotope analysis of well-preserved foraminifera-rich sediment a stratigraphy was developed from lowess curve fitting of the data and an optimized matching with an internationally recognized timescale of 87Sr/86Sr seawater variation through geological times. Depth-to-age conversion of the magnetic susceptibility logs was implemented based on the identification of correlative peaks between cores and the developed 87Sr/86Sr age model. The influence of Northern Hemisphere glaciation is reflected in these new stratigraphic logs by a gradual increase from ∼2.7 Ma in the lower signal of magnetic susceptibility (below background level), to values approaching the arithmetic means, likely reflecting an overall increase in terrigenous input. The Rio Grande Rise cores have very low Plio-Pleistocene sedimentation rates (∼0.4-0.8 cm/ka), similar to gravity cores from the oligotrophic subtropical South Atlantic (below ∼2000 mbsl), and for which an inverse correlation between carbonate content and magnetic susceptibility was established. The coring depths on the Rio Grande Rise encompass strong gradients in oxygen concentration and other seawater parameters that define today's AAIW/UCDW transition. Depth-dependent variation in sedimentation rates since the onset of Northern Hemisphere glaciation coincides with the incursion of intermediate waters (UCDW, AAIW) in response to the overall reduction of NADW export to the Southern Ocean. Background levels of magnetic susceptibility in the cores suggest that this variation is mainly attributed to terrigenous input. The source region of this material has yet to be traced by considering in particular the mineral composition and paramagnetic properties

  5. Rational Design of a Lanthanide-Based Complex Featuring Different Single-Molecule Magnets.

    PubMed

    Pointillart, F; Guizouarn, T; Lefeuvre, B; Golhen, S; Cador, O; Ouahab, L

    2015-11-16

    The rational synthesis of the 2-{1-methylpyridine-N-oxide-4,5-[4,5-bis(propylthio)tetrathiafulvalenyl]-1H-benzimidazol-2-yl}pyridine ligand (L) is described. It led to the tetranuclear complex [Dy4(tta)12(L)2] (Dy-Dy2-Dy) after coordination reaction with the precursor Dy(tta)3⋅2 H2O (tta(-) = 2-thenoyltrifluoroacetonate). The X-ray structure of Dy-Dy2-Dy can be described as two terminal mononuclear units bridged by a central antiferromagnetically coupled dinuclear complex. The terminal N2O6 and central O8 environments are described as distorted square antiprisms. The ac magnetism measurements revealed a strong out-of-phase signal of the magnetic susceptibility with two distinct sets of data. The high- and low-frequency components were attributed to the two terminal mononuclear single-molecule magnets (SMMs) and the central dinuclear SMM, respectively. A magnetic hysteresis loop was detected at very low temperature. From both structural and magnetic points of view, the tetranuclear SMM Dy-Dy2-Dy is a self-assembly of two known mononuclear SMMs bridged by a known dinuclear SMM. © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  6. Slow magnetic relaxation in a dimeric Mn2Ca2 complex enabled by the large Mn(iii) rhombicity.

    PubMed

    Arauzo, Ana; Bartolomé, Elena; Benniston, Andrew C; Melnic, Silvia; Shova, Sergiu; Luzón, Javier; Alonso, Pablo J; Barra, Anne-Laure; Bartolomé, Juan

    2017-01-17

    In this paper we present the characterization of a complex with the formula [Mn 2 Ca 2 (hmp) 6 (H 2 O) 4 (CH 3 CN) 2 ](ClO 4 ) 4 (1), where hmp-H = 2-(hydroxymethyl)pyridine. Compound 1 crystallizes in the monoclinic space group C2/c with the cation lying on an inversion centre. Static magnetic susceptibility, magnetization and heat capacity measurements reflect a unique Mn(iii) valence state, and single-ion ligand field parameters with remarkable large rhombic distortion (D/k B = -6.4 K, E/k B = -2.1 K), in good agreement with the high-field electron paramagnetic resonance experiments. At low temperature Mn 2 Ca 2 cluster behaves as a system of ferromagnetically coupled (J/k B = 1.1 K) Mn dimers with a S T = 4 and m T = ±4 ground state doublet. Frequency dependent ac susceptibility measurements reveal the slow magnetic relaxation characteristic of a single molecule magnet (SMM) below T = 4 K. At zero magnetic field, an Orbach-type spin relaxation process (τ ∼ 10 -5 s) with an activation energy E a = 5.6 K is observed, enabled by the large E/D rhombicity of the Mn(iii) ions. Upon the application of a magnetic field, a second, very slow process (τ ∼ 0.2 s) is observed, attributed to a direct relaxation mechanism with enhanced relaxation time owing to the phonon bottleneck effect.

  7. Quantitative Susceptibility Mapping after Sports-Related Concussion.

    PubMed

    Koch, K M; Meier, T B; Karr, R; Nencka, A S; Muftuler, L T; McCrea, M

    2018-06-07

    Quantitative susceptibility mapping using MR imaging can assess changes in brain tissue structure and composition. This report presents preliminary results demonstrating changes in tissue magnetic susceptibility after sports-related concussion. Longitudinal quantitative susceptibility mapping metrics were produced from imaging data acquired from cohorts of concussed and control football athletes. One hundred thirty-six quantitative susceptibility mapping datasets were analyzed across 3 separate visits (24 hours after injury, 8 days postinjury, and 6 months postinjury). Longitudinal quantitative susceptibility mapping group analyses were performed on stability-thresholded brain tissue compartments and selected subregions. Clinical concussion metrics were also measured longitudinally in both cohorts and compared with the measured quantitative susceptibility mapping. Statistically significant increases in white matter susceptibility were identified in the concussed athlete group during the acute (24 hour) and subacute (day 8) period. These effects were most prominent at the 8-day visit but recovered and showed no significant difference from controls at the 6-month visit. The subcortical gray matter showed no statistically significant group differences. Observed susceptibility changes after concussion appeared to outlast self-reported clinical recovery metrics at a group level. At an individual subject level, susceptibility increases within the white matter showed statistically significant correlations with return-to-play durations. The results of this preliminary investigation suggest that sports-related concussion can induce physiologic changes to brain tissue that can be detected using MR imaging-based magnetic susceptibility estimates. In group analyses, the observed tissue changes appear to persist beyond those detected on clinical outcome assessments and were associated with return-to-play duration after sports-related concussion. © 2018 by American Journal of

  8. Evidence for a dynamical ground state in the frustrated pyrohafnate Tb2Hf2O7

    NASA Astrophysics Data System (ADS)

    Anand, V. K.; Opherden, L.; Xu, J.; Adroja, D. T.; Hillier, A. D.; Biswas, P. K.; Herrmannsdörfer, T.; Uhlarz, M.; Hornung, J.; Wosnitza, J.; Canévet, E.; Lake, B.

    2018-03-01

    We report the physical properties of Tb2Hf2O7 based on ac magnetic susceptibility χac(T ) , dc magnetic susceptibility χ (T ) , isothermal magnetization M (H ) , and heat capacity Cp(T ) measurements combined with muon spin relaxation (μ SR ) and neutron powder diffraction measurements. No evidence for long-range magnetic order is found down to 0.1 K. However, χac(T ) data present a frequency-dependent broad peak (near 0.9 K at 16 Hz) indicating slow spin dynamics. The slow spin dynamics is further evidenced from the μ SR data (characterized by a stretched exponential behavior) which show persistent spin fluctuations down to 0.3 K. The neutron powder diffraction data collected at 0.1 K show a broad peak of magnetic origin (diffuse scattering) but no magnetic Bragg peaks. The analysis of the diffuse scattering data reveals a dominant antiferromagnetic interaction in agreement with the negative Weiss temperature. The absence of long-range magnetic order and the presence of slow spin dynamics and persistent spin fluctuations together reflect a dynamical ground state in Tb2Hf2O7 .

  9. Temperature behavior of the antiferromagnetic susceptibility of nanoferrihydrite from the measurements of the magnetization curves in fields of up to 250 kOe

    NASA Astrophysics Data System (ADS)

    Balaev, D. A.; Popkov, S. I.; Krasikov, A. A.; Balaev, A. D.; Dubrovskiy, A. A.; Stolyar, S. V.; Yaroslavtsev, R. N.; Ladygina, V. P.; Iskhakov, R. S.

    2017-10-01

    The cross-breeding problem of the temperature dependence of the antiferromagnetic susceptibility of ferrihydrite nanoparticles is considered. Iron ions Fe3+ in ferrihydrite are ordered antiferromagnetically; however, the existence of defects on the surface and in the bulk of nanoparticles induces a noncompensated magnetic moment that leads to a typical superparamagnetic behavior of ensemble of the nanoparticles with a characteristic blocking temperature. In an unblocked state, magnetization curves of such objects are described as a superposition of the Langevin function and the linear-in-field contribution of the antiferromagnetic "core" of the nanoparticles. According to many studies of the magnetization curves performed on ferrihydrite (and related ferritin) nanoparticles in fields to 60 kOe, dependence χAF( T) decreases as temperature increases, which was related before to the superantiferromagnetism effect. As the magnetic field range increases to 250 kOe, the values of χAF obtained from an analysis of the magnetization curves become lower in magnitude; however, the character of the temperature evolution of χAF is changed: now, dependence χAF( T) is an increasing function. The latter is typical for a system of AF particles with random orientation of the crystallographic axes. To correctly determine the antiferromagnetic susceptibility of AF nanoparticles (at least, ferrihydrite) and to search for effects related to the superantiferromagnetism effect, it is necessary to use in experiments the range of magnetic field significantly higher than that the standard value 60 kOe used in most experiments. The study of the temperature evolution of the magnetization curves shows that the observed crossover is due to the existence of small magnetic moments in the samples.

  10. Nonstationary behavior of a high-spin molecule in a bifrequency alternating current magnetic field

    NASA Astrophysics Data System (ADS)

    Tokman, I. D.; Vugalter, G. A.

    2002-07-01

    An interaction of a high-spin molecule with a bifrequency ac magnetic field, occurring at times much shorter than the molecule relaxation times, has been considered. The molecule is subjected to a dc magnetic field perpendicular to the easy anisotropy axis of the molecule. The bifrequency ac field is a superposition of two ac fields, one of which is perpendicular to the easy anisotropy axis and causes resonant transitions between the lower states of the fundamental and first excited doublets. The other ac field is parallel to the easy anisotropy axis and has a frequency much smaller than the frequency of the first ac field. It has been shown that, first, the molecule can absorb or emit energy, depending on the frequency of the low-frequency ac field, second, the bifrequency ac magnetic field induces tunneling of the molecule magnetization with the Rabi frequency. The conditions of observation of the effects predicted are discussed.

  11. Magnetic susceptibility as a proxy for investigating microbially mediated iron reduction

    USGS Publications Warehouse

    Mewafy, F.M.; Atekwana, E.A.; Werkema, D.D.; Slater, L.D.; Ntarlagiannis, D.; Revil, A.; Skold, M.; Delin, G.N.

    2011-01-01

    We investigated magnetic susceptibility (MS) variations in hydrocarbon contaminated sediments. Our objective was to determine if MS can be used as an intrinsic bioremediation indicator due to the activity of iron-reducing bacteria. A contaminated and an uncontaminated core were retrieved from a site contaminated with crude oil near Bemidji, Minnesota and subsampled for MS measurements. The contaminated core revealed enriched MS zones within the hydrocarbon smear zone, which is related to iron-reduction coupled to oxidation of hydrocarbon compounds and the vadose zone, which is coincident with a zone of methane depletion suggesting aerobic or anaerobic oxidation of methane is coupled to iron-reduction. The latter has significant implications for methane cycling. We conclude that MS can serve as a proxy for intrinsic bioremediation due to the activity of iron-reducing bacteria iron-reducing bacteria and for the application of geophysics to iron cycling studies. ?? 2011 by the American Geophysical Union.

  12. Magnetic characterisation of folded aeolian sandstones: Interpretation of magnetic fabrics in diamagnetic rocks

    NASA Astrophysics Data System (ADS)

    Callot, J.-P.; Robion, P.; Sassi, W.; Guiton, M. L. E.; Faure, J.-L.; Daniel, J.-M.; Mengus, J.-M.; Schmitz, J.

    2010-12-01

    This study provides an original example of exploitation of Anisotropy of Magnetic Susceptibility (AMS) for rocks with weak magnetic susceptibility. Within the upper Weber Sandstone at Split Mountain, Utah, 430 cores from 31 sites were collected for magnetic characterization. The magnetic susceptibility ranges from -10 to 10 μSI, indicating a mostly diamagnetic matrix, with degree of anisotropy up to 1.6. Specific treatment of magnetic susceptibility allows using diamagnetic data. The fabrics are fairly clustered and triaxial. Sedimentary magnetic fabrics show a foliation plane parallel to the lamina of the sand dunes, without defined lineation. Apart from sedimentary fabrics (< 30%), most of the sites display intermediate to tectonic fabrics related to variable degree of strain (> 70%). Magnetic fabric patterns averaged for sites distributed on the anticline are well defined in sub-groups related to the major structural domains of the anticline. The fracture network at Split Mountain is composed of a dominant N120 set and a secondary N035 set. A scenario of strain record is proposed based on the correlation of (1) fracture sets orientation, (2) diagenetic cementation, (3) paleostresses and (4) distribution of magnetic susceptibility anisotropy. Following the Sevier orogeny and N120 fracture set emplacement, the N035 fracture network and AMS signal were recorded during the Laramide Layer Parallel Shortening phase, with local deviation along pre-existing structures, and recorded a partitioning of the strain during early folding, with a maximum horizontal stress axis perpendicular to the fold bounding faults within the fold.

  13. Magnetic hyperthermia in water based ferrofluids: Effects of initial susceptibility and size polydispersity on heating efficiency

    NASA Astrophysics Data System (ADS)

    Lahiri, B. B.; Ranoo, Surojit; Muthukumaran, T.; Philip, John

    2018-04-01

    The effects of initial susceptibility and size polydispersity on magnetic hyperthermia efficiency in two water based ferrofluids containing phosphate and TMAOH coated superparamagnetic Fe3O4 nanoparticles were studied. Experiments were performed at a fixed frequency of 126 kHz on four different concentrations of both samples and under different external field amplitudes. It was observed that for field amplitudes beyond 45.0 kAm-1, the maximum temperature rise was in the vicinity of 42°C (hyperthermia limit) which indicated the suitability of the water based ferrofluids for hyperthermia applications. The maximum temperature rise and specific absorption rate were found to vary linearly with square of the applied field amplitudes, in accordance with theoretical predictions. It was further observed that for a fixed sample concentration, specific absorption rate was higher for the phosphate coated samples which was attributed to the higher initial static susceptibility and lower size polydispersity of phosphate coated Fe3O4.

  14. Biosensing utilizing magnetic markers and superconducting quantum interference devices

    NASA Astrophysics Data System (ADS)

    Enpuku, Keiji; Tsujita, Yuya; Nakamura, Kota; Sasayama, Teruyoshi; Yoshida, Takashi

    2017-05-01

    Magnetic biosensing techniques that are based on the use of bio-functionalized magnetic nanoparticles (magnetic markers) and superconducting quantum interference devices (SQUIDs) are expected to have various advantages when compared with conventional biosensing methods. In this paper, we review the recent progress made in magnetic biosensing techniques. First, we describe the most important parameters of magnetic markers that are intended for use in biosensing, i.e., the magnetic signal and the relaxation time that are determined by the Brownian and/or Néel relaxation mechanisms. We note that these parameters are significantly dependent on the marker size, and as a result, commercial markers exhibit a wide variety of values for these key parameters. Next, we describe three measurement methods that have been developed based on the magnetic properties of these markers, i.e., AC susceptibility, relaxation and remanence-based measurement methods. The weak (picotesla-range) signals emitted by the markers can be measured precisely with a SQUID system using these methods. Finally, we give examples of biosensing for in vitro and in vivo medical diagnosis applications. For in vitro diagnosis, high-sensitivity detection of various biological targets has been demonstrated without use of any washing process to separate the bound and free markers. For in vivo applications, detection of the quantities and the three-dimensional positions of the markers that have been injected into the test subject are demonstrated. These results confirm the effectiveness of magnetic biosensing techniques.

  15. MAPK Signaling Pathway Alters Expression of Midgut ALP and ABCC Genes and Causes Resistance to Bacillus thuringiensis Cry1Ac Toxin in Diamondback Moth

    PubMed Central

    Wu, Qingjun; Wang, Shaoli; Xie, Wen; Zhu, Xun; Baxter, Simon W.; Zhou, Xuguo; Jurat-Fuentes, Juan Luis; Zhang, Youjun

    2015-01-01

    Insecticidal crystal toxins derived from the soil bacterium Bacillus thuringiensis (Bt) are widely used as biopesticide sprays or expressed in transgenic crops to control insect pests. However, large-scale use of Bt has led to field-evolved resistance in several lepidopteran pests. Resistance to Bt Cry1Ac toxin in the diamondback moth, Plutella xylostella (L.), was previously mapped to a multigenic resistance locus (BtR-1). Here, we assembled the 3.15 Mb BtR-1 locus and found high-level resistance to Cry1Ac and Bt biopesticide in four independent P. xylostella strains were all associated with differential expression of a midgut membrane-bound alkaline phosphatase (ALP) outside this locus and a suite of ATP-binding cassette transporter subfamily C (ABCC) genes inside this locus. The interplay between these resistance genes is controlled by a previously uncharacterized trans-regulatory mechanism via the mitogen-activated protein kinase (MAPK) signaling pathway. Molecular, biochemical, and functional analyses have established ALP as a functional Cry1Ac receptor. Phenotypic association experiments revealed that the recessive Cry1Ac resistance was tightly linked to down-regulation of ALP, ABCC2 and ABCC3, whereas it was not linked to up-regulation of ABCC1. Silencing of ABCC2 and ABCC3 in susceptible larvae reduced their susceptibility to Cry1Ac but did not affect the expression of ALP, whereas suppression of MAP4K4, a constitutively transcriptionally-activated MAPK upstream gene within the BtR-1 locus, led to a transient recovery of gene expression thereby restoring the susceptibility in resistant larvae. These results highlight a crucial role for ALP and ABCC genes in field-evolved resistance to Cry1Ac and reveal a novel trans-regulatory signaling mechanism responsible for modulating the expression of these pivotal genes in P. xylostella. PMID:25875245

  16. Ferrian Ilmenites: Investigating the Magnetic Phase Diagram

    NASA Astrophysics Data System (ADS)

    Lagroix, F.

    2007-12-01

    The main objective of this study is to investigate the magnetic phase changes within the hematite-ilmenite solid solution, yFeTiO3·(1-y)·Fe2O3. Two sets of synthetic ferrian ilmenites of y-values equal to 0.7, 0.8, 0.9, and 1.0 were available for this study. As currently drawn, the magnetic phase diagram, proposed by Ishikawa et al. [1985, J. Phys. Soc. Jpn. v.54, 312-325], predicts for increasing y values (0.5magnetic odering from paramagnetism to (1) ferrimagnetism, or (2) to superparamagnetism then ferrimagnetism, or (3) to superparamagnetism then antiferromagnetism. Moreover, for y values ranging between 0.65 and 1.0 a transition into a spin glass state is expected at 100K or below. Ilmenite, y=1.0, is antiferromagnetic. Various low tempreature experiments including temperature dependance of remanence and induced magnetizations and AC susceptibility were conducted in order to characterize the magnetic behaviour and changes of magnetic states. In general, the data confirms the predicted phase changes for the different compositions investigated. The y=1.0 sample, pure ilmenite, is antiferromagnetic below 57K, the measured Néel temperature. The y=0.9 sample magnetically orders at about 100K in a superparamagnetic state. Hysteresis loops remain effectively closed down to 60K below which an antiferromagnetic order prior to reaching the spin glass state is ambiguous. The y=0.8 sample magnetically orders at about 270K in an initially superparamagnetic states before entering a ferrimagnetic state below about 250K. Lastly, as previously demonstrated in Lagroix et al. [2004, JGR-B, v.109, doi:10.1029/2004JB003076], the y=0.7 samples order ferrimagnetically at 380K. However, like the y=0.7 samples which also demonstrated an antiferromagnetic state at temperature above the Curie temperature, hysteresis loops for y=0.9 and y=0.8 only achieve perfect linearity at 190K and 340K respectively. All samples (except y=1.0) show a frequency dependent amplitude non

  17. Quantitative susceptibility map analysis in preterm neonates with germinal matrix-intraventricular hemorrhage.

    PubMed

    Tortora, Domenico; Severino, Mariasavina; Sedlacik, Jan; Toselli, Benedetta; Malova, Mariya; Parodi, Alessandro; Morana, Giovanni; Fato, Marco Massimo; Ramenghi, Luca Antonio; Rossi, Andrea

    2018-05-10

    Germinal matrix-intraventricular hemorrhage (GMH-IVH) is a common form of intracranial hemorrhage occurring in preterm neonates that may affect normal brain development. Although the primary lesion is easily identified on MRI by the presence of blood products, its exact extent may not be recognizable with conventional sequences. Quantitative susceptibility mapping (QSM) quantify the spatial distribution of magnetic susceptibility within biological tissues, including blood degradation products. To evaluate magnetic susceptibility of normal-appearing white (WM) and gray matter regions in preterm neonates with and without GMH-IVH. Retrospective case-control. A total of 127 preterm neonates studied at term equivalent age: 20 had mild GMH-IVH (average gestational age 28.7 ± 2.1 weeks), 15 had severe GMH-IVH (average gestational age 29.3 ± 1.8 weeks), and 92 had normal brain MRI (average gestational age 29.8 ± 1.8 weeks). QSM at 1.5 Tesla. QSM analysis was performed for each brain hemisphere with a region of interest-based approach including five WM regions (centrum semiovale, frontal, parietal, temporal, and cerebellum), and a subcortical gray matter region (basal ganglia/thalami). Changes in magnetic susceptibility were explored using a one-way analysis of covariance, according to GMH-IVH severity (P < 0.05). In preterm neonates with normal brain MRI, all white and subcortical gray matter regions had negative magnetic susceptibility values (diamagnetic). Neonates with severe GMH-IVH showed higher positive magnetic susceptibility values (i.e. paramagnetic) in the centrum semiovale (0.0019 versus -0.0014 ppm; P < 0.001), temporal WM (0.0011 versus -0.0012 ppm; P = 0.037), and parietal WM (0.0005 versus -0.0001 ppm; P = 0.002) compared with controls. No differences in magnetic susceptibility were observed between neonates with mild GMH-IVH and controls (P = 0.236). Paramagnetic susceptibility changes occur in several normal

  18. Polymorphisms of methylenetetrahydrofolate reductase (MTHFR) and susceptibility to pediatric acute lymphoblastic leukemia in a German study population.

    PubMed

    Schnakenberg, Eckart; Mehles, Andrea; Cario, Gunnar; Rehe, Klaus; Seidemann, Kathrin; Schlegelberger, Brigitte; Elsner, Holger A; Welte, Karl H; Schrappe, Martin; Stanulla, Martin

    2005-05-27

    Methylenetetrahydrofolate reductase (MTHFR) has a major impact on the regulation of the folic acid pathway due to conversion of 5,10-methylenetetrahydrofolate (methylene-THF) to 5-methyl-THF. Two common polymorphisms (677C>T and 1298A>C) in the gene coding for MTHFR have been shown to reduce MTHFR enzyme activity and were associated with the susceptibility to different disorders, including vascular disease, neural tube defects and lymphoid malignancies. Studies on the role of these polymorphisms in the susceptibility to acute lymphoblastic leukemia (ALL) led to discrepant results. We retrospectively evaluated the association of the MTHFR 677C>T and 1298A>C polymorphisms with pediatric ALL by genotyping a study sample of 443 ALL patients consecutively enrolled onto the German multicenter trial ALL-BFM 2000 and 379 healthy controls. We calculated odds ratios of MTHFR genotypes based on the MTHFR 677C>T and 1298A>C polymorphisms to examine if one or both of these polymorphisms are associated with pediatric ALL. No significant associations between specific MTHFR variants or combinations of variants and risk of ALL were observed neither in the total patient group nor in analyses stratified by gender, age at diagnosis, DNA index, immunophenotype, or TEL/AML1 rearrangement. Our findings suggest that the MTHFR 677C>T and 1298A>C gene variants do not have a major influence on the susceptibility to pediatric ALL in the German population.

  19. Polymorphisms of methylenetetrahydrofolate reductase (MTHFR) and susceptibility to pediatric acute lymphoblastic leukemia in a German study population

    PubMed Central

    Schnakenberg, Eckart; Mehles, Andrea; Cario, Gunnar; Rehe, Klaus; Seidemann, Kathrin; Schlegelberger, Brigitte; Elsner, Holger A; Welte, Karl H; Schrappe, Martin; Stanulla, Martin

    2005-01-01

    Background Methylenetetrahydrofolate reductase (MTHFR) has a major impact on the regulation of the folic acid pathway due to conversion of 5,10-methylenetetrahydrofolate (methylene-THF) to 5-methyl-THF. Two common polymorphisms (677C>T and 1298A>C) in the gene coding for MTHFR have been shown to reduce MTHFR enzyme activity and were associated with the susceptibility to different disorders, including vascular disease, neural tube defects and lymphoid malignancies. Studies on the role of these polymorphisms in the susceptibility to acute lymphoblastic leukemia (ALL) led to discrepant results. Methods We retrospectively evaluated the association of the MTHFR 677C>T and 1298A>C polymorphisms with pediatric ALL by genotyping a study sample of 443 ALL patients consecutively enrolled onto the German multicenter trial ALL-BFM 2000 and 379 healthy controls. We calculated odds ratios of MTHFR genotypes based on the MTHFR 677C>T and 1298A>C polymorphisms to examine if one or both of these polymorphisms are associated with pediatric ALL. Results No significant associations between specific MTHFR variants or combinations of variants and risk of ALL were observed neither in the total patient group nor in analyses stratified by gender, age at diagnosis, DNA index, immunophenotype, or TEL/AML1 rearrangement. Conclusion Our findings suggest that the MTHFR 677C>T and 1298A>C gene variants do not have a major influence on the susceptibility to pediatric ALL in the German population. PMID:15921520

  20. AC Electric Field Communication for Human-Area Networking

    NASA Astrophysics Data System (ADS)

    Kado, Yuichi; Shinagawa, Mitsuru

    We have proposed a human-area networking technology that uses the surface of the human body as a data transmission path and uses an AC electric field signal below the resonant frequency of the human body. This technology aims to achieve a “touch and connect” intuitive form of communication by using the electric field signal that propagates along the surface of the human body, while suppressing both the electric field radiating from the human body and mutual interference. To suppress the radiation field, the frequency of the AC signal that excites the transmitter electrode must be lowered, and the sensitivity of the receiver must be raised while reducing transmission power to its minimally required level. We describe how we are developing AC electric field communication technologies to promote the further evolution of a human-area network in support of ubiquitous services, focusing on three main characteristics, enabling-transceiver technique, application-scenario modeling, and communications quality evaluation. Special attention is paid to the relationship between electro-magnetic compatibility evaluation and regulations for extremely low-power radio stations based on Japan's Radio Law.

  1. A catechol oxidase AcPPO from cherimoya (Annona cherimola Mill.) is localized to the Golgi apparatus.

    PubMed

    Olmedo, Patricio; Moreno, Adrián A; Sanhueza, Dayan; Balic, Iván; Silva-Sanzana, Christian; Zepeda, Baltasar; Verdonk, Julian C; Arriagada, César; Meneses, Claudio; Campos-Vargas, Reinaldo

    2018-01-01

    Cherimoya (Annona cherimola) is an exotic fruit with attractive organoleptic characteristics. However, it is highly perishable and susceptible to postharvest browning. In fresh fruit, browning is primarily caused by the polyphenol oxidase (PPO) enzyme catalyzing the oxidation of o-diphenols to quinones, which polymerize to form brown melanin pigment. There is no consensus in the literature regarding a specific role of PPO, and its subcellular localization in different plant species is mainly described within plastids. The present work determined the subcellular localization of a PPO protein from cherimoya (AcPPO). The obtained results revealed that the AcPPO- green fluorescent protein co-localized with a Golgi apparatus marker, and AcPPO activity was present in Golgi apparatus-enriched fractions. Likewise, transient expression assays revealed that AcPPO remained active in Golgi apparatus-enriched fractions obtained from tobacco leaves. These results suggest a putative function of AcPPO in the Golgi apparatus of cherimoya, providing new perspectives on PPO functionality in the secretory pathway, its effects on cherimoya physiology, and the evolution of this enzyme. Copyright © 2017. Published by Elsevier B.V.

  2. Nonlinear dynamics of a magnetically driven Duffing-type spring-magnet oscillator in the static magnetic field of a coil

    NASA Astrophysics Data System (ADS)

    Donoso, Guillermo; Ladera, Celso L.

    2012-11-01

    We study the nonlinear oscillations of a forced and weakly dissipative spring-magnet system moving in the magnetic fields of two fixed coaxial, hollow induction coils. As the first coil is excited with a dc current, both a linear and a cubic magnet-position dependent force appear on the magnet-spring system. The second coil, located below the first, excited with an ac current, provides the oscillating magnetic driving force on the system. From the magnet-coil interactions, we obtain, analytically, the nonlinear motion equation of the system, found to be a forced and damped cubic Duffing oscillator moving in a quartic potential. The relative strengths of the coefficients of the motion equation can be easily set by varying the coils’ dc and ac currents. We demonstrate, theoretically and experimentally, the nonlinear behaviour of this oscillator, including its oscillation modes and nonlinear resonances, the fold-over effect, the hysteresis and amplitude jumps, and its chaotic behaviour. It is an oscillating system suitable for teaching an advanced experiment in nonlinear dynamics both at senior undergraduate and graduate levels.

  3. Field-Driven Quantum Criticality in the Spinel Magnet ZnCr2 Se4

    NASA Astrophysics Data System (ADS)

    Gu, C. C.; Zhao, Z. Y.; Chen, X. L.; Lee, M.; Choi, E. S.; Han, Y. Y.; Ling, L. S.; Pi, L.; Zhang, Y. H.; Chen, G.; Yang, Z. R.; Zhou, H. D.; Sun, X. F.

    2018-04-01

    We report detailed dc and ac magnetic susceptibilities, specific heat, and thermal conductivity measurements on the frustrated magnet ZnCr2 Se4 . At low temperatures, with an increasing magnetic field, this spinel material goes through a series of spin state transitions from the helix spin state to the spiral spin state and then to the fully polarized state. Our results indicate a direct quantum phase transition from the spiral spin state to the fully polarized state. As the system approaches the quantum criticality, we find strong quantum fluctuations of the spins with behaviors such as an unconventional T2 -dependent specific heat and temperature-independent mean free path for the thermal transport. We complete the full phase diagram of ZnCr2 Se4 under the external magnetic field and propose the possibility of frustrated quantum criticality with extended densities of critical modes to account for the unusual low-energy excitations in the vicinity of the criticality. Our results reveal that ZnCr2 Se4 is a rare example of a 3D magnet exhibiting a field-driven quantum criticality with unconventional properties.

  4. Comparative Genomics of Two ST 195 Carbapenem-Resistant Acinetobacter baumannii with Different Susceptibility to Polymyxin Revealed Underlying Resistance Mechanism.

    PubMed

    Lean, Soo-Sum; Yeo, Chew Chieng; Suhaili, Zarizal; Thong, Kwai-Lin

    2015-01-01

    Acinetobacter baumannii is a Gram-negative nosocomial pathogen of importance due to its uncanny ability to acquire resistance to most antimicrobials. These include carbapenems, which are the drugs of choice for treating A. baumannii infections, and polymyxins, the drugs of last resort. Whole genome sequencing was performed on two clinical carbapenem-resistant A. baumannii AC29 and AC30 strains which had an indistinguishable ApaI pulsotype but different susceptibilities to polymyxin. Both genomes consisted of an approximately 3.8 Mbp circular chromosome each and several plasmids. AC29 (susceptible to polymyxin) and AC30 (resistant to polymyxin) belonged to the ST195 lineage and are phylogenetically clustered under the International Clone II (IC-II) group. An AbaR4-type resistance island (RI) interrupted the comM gene in the chromosomes of both strains and contained the bla OXA-23 carbapenemase gene and determinants for tetracycline and streptomycin resistance. AC29 harbored another copy of bla OXA-23 in a large (~74 kb) conjugative plasmid, pAC29b, but this gene was absent in a similar plasmid (pAC30c) found in AC30. A 7 kb Tn1548::armA RI which encodes determinants for aminoglycoside and macrolide resistance, is chromosomally-located in AC29 but found in a 16 kb plasmid in AC30, pAC30b. Analysis of known determinants for polymyxin resistance in AC30 showed mutations in the pmrA gene encoding the response regulator of the two-component pmrAB signal transduction system as well as in the lpxD, lpxC, and lpsB genes that encode enzymes involved in the biosynthesis of lipopolysaccharide (LPS). Experimental evidence indicated that impairment of LPS along with overexpression of pmrAB may have contributed to the development of polymyxin resistance in AC30. Cloning of a novel variant of the bla AmpC gene from AC29 and AC30, and its subsequent expression in E. coli also indicated its likely function as an extended-spectrum cephalosporinase.

  5. Imaging ac losses in superconducting films via scanning Hall probe microscopy

    NASA Astrophysics Data System (ADS)

    Dinner, Rafael B.; Moler, Kathryn A.; Feldmann, D. Matthew; Beasley, M. R.

    2007-04-01

    Various local probes have been applied to understanding current flow through superconducting films, which are often surprisingly inhomogeneous. Here, we show that magnetic imaging allows quantitative reconstruction of both current density J and electric field E resolved in time and space in a film carrying subcritical ac current. Current reconstruction entails inversion of the Biot-Savart law, while electric fields are reconstructed using Faraday’s law. We describe the corresponding numerical procedures, largely adapting existing work to the case of a strip carrying ac current, but including other methods of obtaining the complete electric field from the inductive portion determined by Faraday’s law. We also delineate the physical requirements behind the mathematical transformations. We then apply the procedures to images of a strip of YBa2Cu3O7-δ carrying an ac current at 400Hz . Our scanning Hall probe microscope produces a time series of magnetic images of the strip with 1μm spatial resolution and 25μs time resolution. Combining the reconstructed J and E , we obtain a complete characterization including local critical current density, E-J curves, and power losses. This analysis has a range of applications from fundamental studies of vortex dynamics to practical coated conductor development.

  6. Demonstrating and Measuring Relative Molar Magnetic Susceptibility Using a Neodymium Magnet

    ERIC Educational Resources Information Center

    Malerich, Charles; Ruff, Patricia K.; Bird, Aubrey

    2004-01-01

    An easy-to-see method for demonstrating and measuring the magnetic force between paramagnetic substance and a rare earth magnet is presented. The readily available trapezoid-shaped neodymium magnet and a low cost, easy-to-set-up, portable apparatus are used in the experiments.

  7. New perspectives to the enterotoxigenic E. coli F4 porcine infection model: Susceptibility genotypes in relation to performance, diarrhoea and bacterial shedding.

    PubMed

    Roubos-van den Hil, Petra J; Litjens, Ralph; Oudshoorn, Anna-Katharina; Resink, Jan Willem; Smits, Coen H M

    2017-04-01

    Enterotoxigenic E. coli (ETEC), causing post-weaning diarrhoea, is a major problem in weaned piglets. Individual animal responses to ETEC infection show high variability in animal experiments. Two studies were designed to optimize the ETEC F4ac infection model in piglets by combining the genotype susceptibility with performance, diarrhoea incidence and bacterial shedding. The studies were performed with respectively 120 and 80 male piglets that were tested for susceptibility or resistance towards ETEC O149:F4ac by a DNA marker based test. Three different genotypes were observed; resistant (RR), susceptible heterozygote (RS) and susceptible homozygote (SS). Piglets, were orally infected with an inoculum suspension (containing 1.5E8 CFU/ml ETEC F4ac) at day 0, 1 and 2 of the study. Performance, diarrhoea incidence and bacterial shedding were followed for 21days. In the first week after challenge a difference in average daily gain was observed between resistant and susceptible piglets in both studies. For the complete study period no significant differences were observed. Diarrhoea incidence was significantly higher in susceptible pigs compared to the resistant pigs in the first week after challenge. Bacterial shedding was much higher in the susceptible pigs and ETEC excretion lasted longer. ETEC was hardly detected in the faecal material of the resistant pigs. In conclusion, susceptible pigs showed higher diarrhoea incidence and higher numbers of faecal ETEC shedding in the first week after challenge compared to resistant pigs. The DNA marker based test can be used to select pigs that are susceptible for ETEC for inclusion in ETEC infection model, resulting in less animals needed to perform infection studies. Copyright © 2016 Elsevier B.V. All rights reserved.

  8. 3D chiral and 2D achiral cobalt(ii) compounds constructed from a 4-(benzimidazole-1-yl)benzoic ligand exhibiting field-induced single-ion-magnet-type slow magnetic relaxation.

    PubMed

    Wang, Yu-Ling; Chen, Lin; Liu, Cai-Ming; Du, Zi-Yi; Chen, Li-Li; Liu, Qing-Yan

    2016-05-04

    Organizing magnetically isolated 3d transition metal ions, which behave as single-ion magnet (SIM) units, in a coordination network is a promising approach to design novel single-molecule magnets (SMMs). Herein 3D chiral and 2D achiral cobalt(ii) coordination compounds based on single metal nodes with a 4-(benzimidazole-1-yl)benzoic acid (Hbmzbc) ligand, namely, [Co(bmzbc)2(1,2-etdio)]n () (1,2-etdio = 1,2-ethanediol) and [Co(bmzbc)2(Hbmzbc)]n (), have been synthesized and structurally characterized. The 3D chiral structure with 2-fold interpenetrating qtz topological nets consisting of totally achiral components was obtained via spontaneous resolution, while the achiral structure is a 2D (4,4) net. In both structures, individual cobalt(ii) ions are spatially well separated by the long organic ligands in the well-defined networks. Magnetic measurements on and showed field-induced slow magnetic relaxation resulting from single-ion anisotropy of the individual Co(ii) ions. Analysis of the dynamic ac susceptibilities with the Arrhenius law afforded an anisotropy energy barrier of 16.8(3) and 31.3(2) K under a 2 kOe static magnetic field for and , respectively. The distinct coordination environments of the Co(ii) ions in and lead to the different anisotropic energy barriers.

  9. Improving the method of low-temperature anisotropy of magnetic susceptibility (LT-AMS) measurements in air

    NASA Astrophysics Data System (ADS)

    Issachar, R.; Levi, T.; Lyakhovsky, V.; Marco, S.; Weinberger, R.

    2016-07-01

    This study examines the limitations of the method of low-temperature anisotropy of magnetic susceptibility (LT-AMS) measurements in air and presents technical improvements that significantly reduce the instrumental drift and measurement errors. We analyzed the temperature profile of porous chalk core after cooling in liquid nitrogen and found that the average temperature of the sample during the LT-AMS measurement in air is higher than 77K and close to 92K. This analysis indicates that the susceptibility of the paramagnetic minerals are amplified by a factor ˜3.2 relative to that of room temperature AMS (RT-AMS). In addition, it was found that liquid nitrogen was absorbed in the samples during immersing and contributed diamagnetic component of ˜-9 × 10-6 SI to the total mean susceptibility. We showed that silicone sheet placed around and at the bottom of the measuring coil is an effective thermal protection, preventing instrument drift by the cold sample. In this way, the measuring errors of LT-AMS reduced to the level of RT-AMS, allowing accurate comparison with standard AMS measurements. We examined the applicability of the LT-AMS measurements on chalk samples that consist <5% (weight) of paramagnetic minerals and showed that it helps to efficiently enhance the paramagnetic fabric. The present study offers a practical approach, which can be applied to various types of rocks to better delineate the paramagnetic phase using conventional equipment.

  10. Fabrication of cobalt-nickel binary nanowires in a highly ordered alumina template via AC electrodeposition

    PubMed Central

    2013-01-01

    Cobalt-nickel (Co-Ni) binary alloy nanowires of different compositions were co-deposited in the nanopores of highly ordered anodic aluminum oxide (AAO) templates from a single sulfate bath using alternating current (AC) electrodeposition. AC electrodeposition was accomplished without modifying or removing the barrier layer. Field emission scanning electron microscope was used to study the morphology of templates and alloy nanowires. Energy-dispersive X-ray analysis confirmed the deposition of Co-Ni alloy nanowires in the AAO templates. Average diameter of the alloy nanowires was approximately 40 nm which is equal to the diameter of nanopore. X-ray diffraction analysis showed that the alloy nanowires consisted of both hexagonal close-packed and face-centered cubic phases. Magnetic measurements showed that the easy x-axis of magnetization is parallel to the nanowires with coercivity of approximately 706 Oe. AC electrodeposition is very simple, fast, and is useful for the homogenous deposition of various secondary nanostuctured materials into the nanopores of AAO. PMID:23941234

  11. Controllable synthesis, crystal structure and magnetic properties of Monomer-Dimer Cocrystallized MnIII Salen-type composite material

    NASA Astrophysics Data System (ADS)

    Wu, Qiong; Wu, Wei; Wu, Yongmei; Li, Weili; Qiao, Yongfeng; Wang, Ying; Wang, Baoling

    2018-04-01

    By the reaction of manganese-Schiff-base complexes with penta-anionic Anderson heteropolyanion, a new supramolecular architecture [Mn2(Salen)2(H2O)2][Mn(Salen)(H2O)2]2Na[IMo6O24]·8H2O (1) (salen = N,N‧-ethylene-bis (salicylideneiminate) has been isolated. Compound 1 was characterized by the single-crystal X-ray diffraction, elemental, IR and thermal gravimetric analyses. Structural analysis reveals that the unit cell simultaneously contains MnIII-Salen dimer and monomer cation fragments, for which the Anderson-type polyanions serve as counter anions. In the packing arrangement, all the MnIII dimers are well separated by polyoxometalate units and form tertiary structure together with MnIII monomers. Interestingly, different from the previous work, in the exact same reaction conditions, we are able to template MnIII-Salen complexes into different configurations by varying the charge state of polyanions. Besides, the magnetic properties of 1 were also examined by using both dc and ac magnetic field of the superconducting quantum interference devices. Most importantly, our fitting of the experimental data to a Heisenberg-type spin model shows that there exists a ferromagnetic exchange interaction ∼5 K between the spins (S = 2) on MnIII in the dimer, while antiferromagnetic ones exist among monomers and dimer (∼2 K). This meta-magnetic state could induce a slight spin frustration at low temperature, which would in turn affect the magnetic behavior. In addition, our ac field measurement of the susceptibilities suggests a typical signature for a single-molecule magnet.

  12. Magnetic transit-time flowmeter

    DOEpatents

    Forster, George A.

    1976-07-06

    The flow rate of a conducting fluid in a stream is determined by disposing two permanent-magnet flowmeters in the stream, one downstream of the other. Flow of the conducting fluid causes the generation of both d-c and a-c electrical signals, the a-c comprising flow noise. Measurement of the time delay between similarities in the a-c signals by cross-correlation methods provides a measure of the rate of flow of the fluid.

  13. Impact of an iron mine and a nickel smelter at the Norwegian/Russian border close to the Barents Sea on surface soil magnetic susceptibility and content of potentially toxic elements.

    PubMed

    Magiera, Tadeusz; Zawadzki, Jarosław; Szuszkiewicz, Marcin; Fabijańczyk, Piotr; Steinnes, Eiliv; Fabian, Karl; Miszczak, Ewa

    2018-03-01

    An important problem in soil magnetometry is unraveling the soil contamination signal in areas with multiple emitters. Here, geophysical and geochemical measurements were performed at four sites on a north - south transect along the Pasvik River in the Barents Region (northern Norway). These sites are influenced by depositions from the Bjørnevatn iron mine and a Ni-Cu smelter in Nikel, Russia. To relate the degree and type of pollution from these sources to the corresponding magnetic signal, the topsoil concentrations of 12 Potentially Toxic Elements (PTEs) (As, Cd, Co, Cr, Cu, Fe, Mo, Ni, Pb, Se, Ti, Zn), were determined, magnetic hysteresis parameters and thermomagnetic properties were measured. In situ magnetic low-field susceptibility decreases from north to south with increasing distance from the iron mine. Relatively large magnetic multidomain grains of magnetite and/or titanomagnetite are responsible for the strong magnetic signal from the topsoil close to Bjørnevatn. These particles are related to increased enrichment factors of As, Mo and Cu, yielding high positive correlation coefficients with susceptibility values. At a site furthest away from the iron mine and located 7 km from the Ni-Cu smelter magnetic susceptibility values are much lower but significant positive correlations on the level of p < .1 with 8 PTEs (Ni, Cu, Co, Se, As, Zn, Cd, Cr) have been observed. The magnetic signal in this area is due to fine-grained primary sulphides and secondary fine-grained magnetite and/or maghemite. Copyright © 2017 Elsevier Ltd. All rights reserved.

  14. Serotonergic genes and depressive disorder in acute coronary syndrome: The Korean depression in ACS (K-DEPACS) study.

    PubMed

    Kim, Jae-Min; Stewart, Robert; Kang, Hee-Ju; Bae, Kyung-Yeol; Kim, Sung-Wan; Shin, Il-Seon; Hong, Young Joon; Ahn, Youngkeun; Jeong, Myung Ho; Park, Sung-Woo; Kim, Young-Hoon; Yoon, Jin-Sang

    2015-06-01

    Genes coding for the serotonergic pathway have been associated with depressive disorders. However, these associations have rarely been tested in acute coronary syndrome (ACS) patients vulnerable to depression. This study aimed to investigate whether polymorphisms of serotonin transporter (5-HTT) and serotonin 2a receptor (5-HTR2a) genes are associated with occurrence of depressive disorder in ACS. 969 patients with recently developed ACS were recruited at baseline, and 711 were followed 1 year thereafter. Depressive disorder was diagnosed according to DSM-IV criteria, and analysed as an outcome at baseline (prevalence), and follow up (incidence and persistence). Genotypes were ascertained for 5-HTTLPR, STin2 VNTR, 5-HTR2a 102T/C, and 5-HTR2a 1438A/G. Logistic regression models were used to investigate associations. The 5-HTTLPR s/s genotype was independently associated with depressive disorder prevalence and persistence following ACS, but no significant associations were found with the other polymorphisms. ACS patients with the 5-HTTLPR s allele are thus potentially susceptible to depressive disorder in the early phase after ACS, and with its persistence over the subsequent year. Copyright © 2015 Elsevier B.V. and ECNP. All rights reserved.

  15. Increased Iron Deposition on Brain Quantitative Susceptibility Mapping Correlates with Decreased Cognitive Function in Alzheimer's Disease.

    PubMed

    Du, Lei; Zhao, Zifang; Cui, Ailing; Zhu, Yijiang; Zhang, Lu; Liu, Jing; Shi, Sumin; Fu, Chao; Han, Xiaowei; Gao, Wenwen; Song, Tianbin; Xie, Lizhi; Wang, Lei; Sun, Shilong; Guo, Runcai; Ma, Guolin

    2018-05-15

    The excessive accumulation of iron in deep gray structures is an important pathological characteristic in patients with Alzheimer's disease (AD). Quantitative susceptibility mapping (QSM) is more specific than other imaging-based iron measurement modalities and allows noninvasive assessment of tissue magnetic susceptibility, which has been shown to correlate well with brain iron levels. This study aimed to investigate the correlations between the magnetic susceptibility values of deep gray matter nuclei and the cognitive functions assessed by mini-mental state examination (MMSE) and Montreal cognitive assessment (MoCA) in patients with mild and moderate AD. Thirty subjects with mild and moderate AD and 30 age- and sex-matched healthy controls were scanned with a 3.0 T magnetic resonance imaging (MRI) scanner. The magnetic susceptibilities of the regions of interest (ROIs), including caudate nucleus (Cd), putamen (Pt), globus pallidus (Gp), thalamus (Th), red nucleus (Rn), substantia nigra (Sn), and dentate nucleus (Dn), were quantified by QSM. We found that the susceptibility values of the bilateral Cd and Pt were significantly higher in AD patients than the controls ( P < 0.05). In contrast, bilateral Rn had significantly lower susceptibility values in AD than the controls. Regardless of gender and age, the increase of magnetic susceptibility in the left Cd was significantly correlated with the decrease of MMSE scores and MoCA scores ( P < 0.05). Our study indicated that magnetic susceptibility value of left Cd could be potentially used as a biomarker of disease severity in mild and moderate AD.

  16. Vortical susceptibility of finite-density QCD matter

    DOE PAGES

    Aristova, A.; Frenklakh, D.; Gorsky, A.; ...

    2016-10-07

    Here, the susceptibility of finite-density QCD matter to vorticity is introduced, as an analog of magnetic susceptibility. It describes the spin polarization of quarks and antiquarks in finite-density QCD matter induced by rotation. We estimate this quantity in the chirally broken phase using the mixed gauge-gravity anomaly at finite baryon density. It is proposed that the vortical susceptibility of QCD matter is responsible for the polarization of Λ and Λ¯ hyperons observed recently in heavy ion collisions at RHIC by the STAR collaboration.

  17. Proton Nuclear Magnetic Resonance Spectroscopy as a Technique for Gentamicin Drug Susceptibility Studies with Escherichia coli ATCC 25922

    PubMed Central

    García-Álvarez, Lara; Busto, Jesús H.; Avenoza, Alberto; Sáenz, Yolanda; Peregrina, Jesús Manuel

    2015-01-01

    Antimicrobial drug susceptibility tests involving multiple time-consuming steps are still used as reference methods. Today, there is a need for the development of new automated instruments that can provide faster results and reduce operating time, reagent costs, and labor requirements. Nuclear magnetic resonance (NMR) spectroscopy meets those requirements. The metabolism and antimicrobial susceptibility of Escherichia coli ATCC 25922 in the presence of gentamicin have been analyzed using NMR and compared with a reference method. Direct incubation of the bacteria (with and without gentamicin) into the NMR tube has also been performed, and differences in the NMR spectra were obtained. The MIC, determined by the reference method found in this study, would correspond with the termination of the bacterial metabolism observed with NMR. Experiments carried out directly into the NMR tube enabled the development of antimicrobial drug susceptibility tests to assess the effectiveness of the antibiotic. NMR is an objective and reproducible method for showing the effects of a drug on the subject bacterium and can emerge as an excellent tool for studying bacterial activity in the presence of different antibiotic concentrations. PMID:25972417

  18. Proton Nuclear Magnetic Resonance Spectroscopy as a Technique for Gentamicin Drug Susceptibility Studies with Escherichia coli ATCC 25922.

    PubMed

    García-Álvarez, Lara; Busto, Jesús H; Avenoza, Alberto; Sáenz, Yolanda; Peregrina, Jesús Manuel; Oteo, José A

    2015-08-01

    Antimicrobial drug susceptibility tests involving multiple time-consuming steps are still used as reference methods. Today, there is a need for the development of new automated instruments that can provide faster results and reduce operating time, reagent costs, and labor requirements. Nuclear magnetic resonance (NMR) spectroscopy meets those requirements. The metabolism and antimicrobial susceptibility of Escherichia coli ATCC 25922 in the presence of gentamicin have been analyzed using NMR and compared with a reference method. Direct incubation of the bacteria (with and without gentamicin) into the NMR tube has also been performed, and differences in the NMR spectra were obtained. The MIC, determined by the reference method found in this study, would correspond with the termination of the bacterial metabolism observed with NMR. Experiments carried out directly into the NMR tube enabled the development of antimicrobial drug susceptibility tests to assess the effectiveness of the antibiotic. NMR is an objective and reproducible method for showing the effects of a drug on the subject bacterium and can emerge as an excellent tool for studying bacterial activity in the presence of different antibiotic concentrations. Copyright © 2015, American Society for Microbiology. All Rights Reserved.

  19. Simultaneous Quantitative MRI Mapping of T1, T2* and Magnetic Susceptibility with Multi-Echo MP2RAGE

    PubMed Central

    Kober, Tobias; Möller, Harald E.; Schäfer, Andreas

    2017-01-01

    The knowledge of relaxation times is essential for understanding the biophysical mechanisms underlying contrast in magnetic resonance imaging. Quantitative experiments, while offering major advantages in terms of reproducibility, may benefit from simultaneous acquisitions. In this work, we demonstrate the possibility of simultaneously recording relaxation-time and susceptibility maps with a prototype Multi-Echo (ME) Magnetization-Prepared 2 RApid Gradient Echoes (MP2RAGE) sequence. T1 maps can be obtained using the MP2RAGE sequence, which is relatively insensitive to inhomogeneities of the radio-frequency transmit field, B1+. As an extension, multiple gradient echoes can be acquired in each of the MP2RAGE readout blocks, which permits the calculation of T2* and susceptibility maps. We used computer simulations to explore the effects of the parameters on the precision and accuracy of the mapping. In vivo parameter maps up to 0.6 mm nominal resolution were acquired at 7 T in 19 healthy volunteers. Voxel-by-voxel correlations and the test-retest reproducibility were used to assess the reliability of the results. When using optimized paramenters, T1 maps obtained with ME-MP2RAGE and standard MP2RAGE showed excellent agreement for the whole range of values found in brain tissues. Simultaneously obtained T2* and susceptibility maps were of comparable quality as Fast Low-Angle SHot (FLASH) results. The acquisition times were more favorable for the ME-MP2RAGE (≈ 19 min) sequence as opposed to the sum of MP2RAGE (≈ 12 min) and FLASH (≈ 10 min) acquisitions. Without relevant sacrifice in accuracy, precision or flexibility, the multi-echo version may yield advantages in terms of reduced acquisition time and intrinsic co-registration, provided that an appropriate optimization of the acquisition parameters is performed. PMID:28081157

  20. Magnetic properties of 1 : 4 complexes of CoCl2 and pyridines carrying carbenes (S(0) = 4/2, 6/2, and 8/2) in diluted frozen solution; influence of carbene multiplicity on heterospin single-molecule magnets.

    PubMed

    Karasawa, Satoru; Nakano, Kimihiro; Tanokashira, Jun-ichi; Yamamoto, Noriko; Yoshizaki, Takahito; Koga, Noboru

    2012-11-28

    The microcrystalline sample of a parent complex, [CoCl(2)(py)(4)], showed a single-molecule magnet (SMM) behavior with an effective activation barrier, U(eff)/k(B), of 16 K for reversal of the magnetism in the presence of a dc field of 3 kOe. Pyridine ligands having 2-4 diazo moieties, DYpy; Y = 2, 3l, 3b, and 4, were prepared and confirmed to be quintet, septet, septet, and nonet in the ground state, respectively, after irradiation. The 1 : 4 complexes, CoCl(2)(DYpy)(4); Y = 2, 3l, 3b, and 4 in frozen solutions after irradiation showed the magnetic behaviors of SMMs with total spin multiplicity, S(total) = 17/2, 25/2, 25/2, and 33/2, respectively. Hysteresis loops depending on the temperature were observed and the values of coercive force, H(c), at 1.9 K were 12, 8.4, 11, and 8.1 kOe for CoCl(2)(CYpy)(4); Y = 2, 3l, 3b, and 4, respectively. In dynamic magnetic susceptibility experiments, ac magnetic susceptibility data obeyed the Arrhenius law to give U(eff)/k(B) values of 94, 92, 93, and 87 K for CoCl(2)(CYpy)(4); Y = 2, 3l, 3b, and 4, respectively, while the relaxation times for CoCl(2)(CYpy)(4); Y = 2 and 3l, obtained by dc magnetization decay in the range of 3.5-1.9 K slightly deviated downward from Arrhenius plots on cooling. The dynamic magnetic behaviors for CoCl(2)(CYpy)(4) including [CoCl(2)(py)(4)] and CoCl(2)(C1py)(4) suggested that the generated carbenes interacted with the cobalt ion to increase the relaxation time, τ(q), due to the spin quantum tunneling magnetization, which became larger with increasing S(total) of the complex.

  1. Starch determination, amylose content and susceptibility to in vitro amylolysis in flours from the roots of 25 cassava varieties.

    PubMed

    Mejía-Agüero, Luisa Elena; Galeno, Florangel; Hernández-Hernández, Oswaldo; Matehus, Juan; Tovar, Juscelino

    2012-02-01

    Cassava cultivars are classified following different criteria, such as cyanogenic glucoside content or starch content. Here, flours from the roots of 25 cassava varieties cultivated simultaneously in a single plantation, were characterized in terms of starch content (SC), amylose content (AC), α-amylolysis index (AI) and gel formation ability. Resistant starch content (RS) was measured in 10 of the samples. Cassava flours exhibited high SC, low AC and low AI values, with differences among varieties. Cluster analysis based on these parameters divided the cultivars in four groups differing mainly in SC and AC. AI and AC were inversely correlated (r = -0.59, P < 0.05) in 18 of the cultivars, suggesting AC as an important factor governing the susceptibility to enzymatic hydrolysis of starch in raw cassava. Differences in susceptibility to amylolysis, assessed by RS, were also recorded in the sample subset analyzed. Most flours yielded pastes or gels upon heating and cooling. Gels differed in their subjective grade of firmness, but none exhibited syneresis, confirming the low retrogradation proclivity of cassava starch. Some differences were found among cassava samples, which may be ascribed to inter-cultivar variation. This information may have application in further agronomic studies or for developing industrial uses for this crop. Copyright © 2011 Society of Chemical Industry.

  2. Balancing structural distortions via competing 4f and itinerant interactions: A case of polymorphism in magnetocaloric HoCo 2

    DOE PAGES

    Mudryk, Y.; Paudyal, D.; Pathak, A. K.; ...

    2016-04-13

    The nature of multiple magnetostructural transformations in HoCo 2 has been studied by employing magnetic and specific heat measurements, temperature and magnetic field dependent X-ray powder diffraction, and first-principles calculations. Unexpected increase of magnetization observed below the spin-reorientation temperature (T SR) suggests that the low-temperature transition involves a reduction of Co moment. First principles calculations confirm that the paramagnetic cubic to ferrimagnetic tetragonal transformation at T C is assisted by itinerant electron metamagnetism, and that the reduction of Co moment in HoCo 2 occurs in parallel with the ferrimagnetic tetragonal to the nearly ferromagnetic orthorhombic transformation at T SRvia themore » rearrangement of both 3d states of Co and 5d states of Ho. The ac magnetic susceptibility measurements show significant magnetic frustration below T C. Furthermore, in contrast to earlier reports neither ac nor dc magnetic susceptibilities show anomalies in the paramagnetic region obeying the Curie–Weiss law.« less

  3. Effects of humidity on the magnetic and woody characteristics of powder-type magnetic wood

    NASA Astrophysics Data System (ADS)

    Oka, H.; Tokuta, H.; Namizaki, Y.; Sekino, N.

    2004-05-01

    Among three types of proposed magnetic wood, powder-type magnetic wood can be made of recycled magnetic materials from IT devices, consumer electronics and waste wood. Because of its wood powder content, powder-type magnetic wood shows special characteristics different from those of typical magnetic materials. We focused on the relationship between humidity and magnetic characteristics of powder-type magnetic wood. The magnetic powder ratio, wood powder density and magnetic binder density were all examined as parameters for AC permeability.

  4. Fragile singlet ground-state magnetism in the pyrochlore osmates R 2 Os 2 O 7 ( R = Y and Ho)

    DOE PAGES

    Zhao, Z. Y.; Calder, S.; Aczel, A. A.; ...

    2016-04-25

    The singlet ground state magnetism in pyrochlore osmates Y 2Os 2O 7 and Ho 2Os 2O 7 is studied by DC and AC susceptibility, specific heat, and neutron powder diffraction measurements. Despite the expected non-magnetic singlet in the strong spin-orbit coupling (SOC) limit for Os 4+ (5d 4), Y 2Os 2O 7 exhibits a spin-glass (SG) ground state below 4 K with weak magnetism, suggesting possible proximity to a quantum phase transition between the non-magnetic state in the strong SOC limit and the magnetic state in the strong superexchange limit. Ho 2Os 2O 7 has the same structural distortion asmore » occurs in Y 2Os 2O 7. However, the Os sublattice in Ho 2Os 2O 7 shows long- range magnetic ordering below 36 K. We find that the sharp difference of the magnetic ground state between Y 2Os 2O 7 and Ho 2Os 2O 7 signals the singlet ground state magnetism in R 2 Os 2 O 7 is fragile and can be disturbed by the weak 4f—5d interactions.« less

  5. Fragile singlet ground-state magnetism in the pyrochlore osmates R 2 Os 2 O 7 ( R = Y and Ho)

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Zhao, Z. Y.; Calder, S.; Aczel, A. A.

    The singlet ground state magnetism in pyrochlore osmates Y 2Os 2O 7 and Ho 2Os 2O 7 is studied by DC and AC susceptibility, specific heat, and neutron powder diffraction measurements. Despite the expected non-magnetic singlet in the strong spin-orbit coupling (SOC) limit for Os 4+ (5d 4), Y 2Os 2O 7 exhibits a spin-glass (SG) ground state below 4 K with weak magnetism, suggesting possible proximity to a quantum phase transition between the non-magnetic state in the strong SOC limit and the magnetic state in the strong superexchange limit. Ho 2Os 2O 7 has the same structural distortion asmore » occurs in Y 2Os 2O 7. However, the Os sublattice in Ho 2Os 2O 7 shows long- range magnetic ordering below 36 K. We find that the sharp difference of the magnetic ground state between Y 2Os 2O 7 and Ho 2Os 2O 7 signals the singlet ground state magnetism in R 2 Os 2 O 7 is fragile and can be disturbed by the weak 4f—5d interactions.« less

  6. A magnetic nanobead-based bioassay provides sensitive detection of single- and biplex bacterial DNA using a portable AC susceptometer.

    PubMed

    Strömberg, Mattias; Zardán Gómez de la Torre, Teresa; Nilsson, Mats; Svedlindh, Peter; Strømme, Maria

    2014-01-01

    Bioassays relying on magnetic read-out using probe-tagged magnetic nanobeads are potential platforms for low-cost biodiagnostic devices for pathogen detection. For optimal assay performance it is crucial to apply an easy, efficient and robust bead-probe conjugation protocol. In this paper, sensitive (1.5 pM) singleplex detection of bacterial DNA sequences is demonstrated in a portable AC susceptometer by a magnetic nanobead-based bioassay principle; the volume-amplified magnetic nanobead detection assay (VAM-NDA). Two bead sizes, 100 and 250 nm, are investigated along with a highly efficient, rapid, robust, and stable conjugation chemistry relying on the avidin-biotin interaction for bead-probe attachment. Avidin-biotin conjugation gives easy control of the number of detection probes per bead; thus allowing for systematic investigation of the impact of varying the detection probe surface coverage upon bead immobilization in rolling circle amplified DNA-coils. The existence of an optimal surface coverage is discussed. Biplex VAM-NDA detection is for the first time demonstrated in the susceptometer: Semi-quantitative results are obtained and it is concluded that the concentration of DNA-coils in the incubation volume is of crucial importance for target quantification. The present findings bring the development of commercial biodiagnostic devices relying on the VAM-NDA further towards implementation in point-of-care and outpatient settings. © 2013 The Authors. Biotechnology Journal published by Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim. This is an open access article under the terms of the Creative Commons Attribution-License, which permits use and distribution in any medium, provided the original work is properly cited.

  7. AC loss, interstrand resistance and mechanical properties of prototype EU DEMO TF conductors up to 30 000 load cycles

    NASA Astrophysics Data System (ADS)

    Yagotintsev, K.; Nijhuis, A.

    2018-07-01

    Two prototype Nb3Sn cable-in-conduit conductors conductors were designed and manufactured for the toroidal field (TF) magnet system of the envisaged European DEMO fusion reactor. The AC loss, contact resistance and mechanical properties of two sample conductors were tested in the Twente Cryogenic Cable Press under cyclic load up to 30 000 cycles. Though both conductors were designed to operate at 82 kA in a background magnetic field of 13.6 T, they reflect different approaches with respect to the magnet winding pack assembly. The first approach is based on react and wind technology while the second is the more common wind and react technology. Each conductor was tested first for AC loss in virgin condition without handling. The impact of Lorentz load during magnet operation was simulated using the cable press. In the press each conductor specimen was subjected to transverse cyclic load up to 30 000 cycles in liquid helium bath at 4.2 K. Here a summary of results for AC loss, contact resistance, conductor deformation, mechanical heat production and conductor stiffness evolution during cycling of the load is presented. Both conductors showed similar mechanical behaviour but quite different AC loss. In comparison with previously tested ITER TF conductors, both DEMO TF conductors possess very low contact resistance resulting in high coupling loss. At the same time, load cycling has limited impact on properties of DEMO TF conductors in comparison with ITER TF conductors.

  8. Determination of crystal-field energy levels and temperature dependence of magnetic susceptibility for Dy3+ in [Dy2Pd] heterometallic complex.

    PubMed

    Karbowiak, Mirosław; Rudowicz, Czesław; Ishida, Takayuki

    2013-11-18

    This study is the first in a series of experimental and theoretical investigations of the crystal-field (CF) energy levels obtained from optical electronic spectra for selected heterometallic 4f-3d compounds intensively studied for the development of novel single-molecule magnets (SMMs). An intriguing question is why the [{Dy(III)(hfac)3}2Cu(II)(dpk)2] (abbreviated as [Dy2Cu]; Hhfac = 1,1,1,5,5,5-hexafluoropentane-2,4-dione, Hdpk = di-2-pyridyl ketoxime) has antiferromagnetic coupling, whereas [Gd2Cu] and heavy [Ln2Cu] systems usually show ferromagnetic coupling. As the first step to explain this peculiarity, the recently synthesized complex, [Dy2Pd], is investigated. This complex is isostructural with [Dy2Cu] yet contains the diamagnetic Pd ion instead of the magnetic Cu(II) ion. Experimental energy levels of Dy(3+) ions in the powder [Dy2Pd] sample were determined from the 4.2 K absorption spectra. CF analysis was performed yielding the fitted free ion and CF parameters. The number of freely varied parameters was restricted using the superposition model. The fittings yield very satisfactory agreement between the experimental and the calculated energy levels (rms = 12.0 cm(-1)). The energies and exact composition of the state vector for the ground multiplet (6)H(15/2) of Dy(3+) are determined. These results are used for the simulation of the temperature dependence of the magnetic susceptibility, which enables the theoretical interpretation of the experimentally measured magnetic susceptibility in the range 1.8-300 K for the [Dy2Pd] complex. This study provides background for the subsequent investigation of the magnetic exchange interactions in the pertinent heterometallic complexes.

  9. Measuring iron in the brain using quantitative susceptibility mapping and X-ray fluorescence imaging

    PubMed Central

    Zheng, Weili; Nichol, Helen; Liu, Saifeng; Cheng, Yu-Chung N.; Haacke, E. Mark

    2013-01-01

    Measuring iron content in the brain has important implications for a number of neurodegenerative diseases. Quantitative susceptibility mapping (QSM), derived from magnetic resonance images, has been used to measure total iron content in vivo and in post mortem brain. In this paper, we show how magnetic susceptibility from QSM correlates with total iron content measured by X-ray fluorescence (XRF) imaging and by inductively coupled plasma mass spectrometry (ICPMS). The relationship between susceptibility and ferritin iron was estimated at 1.10 ± 0.08 ppb susceptibility per μg iron/g wet tissue, similar to that of iron in fixed (frozen/thawed) cadaveric brain and previously published data from unfixed brains. We conclude that magnetic susceptibility can provide a direct and reliable quantitative measurement of iron content and that it can be used clinically at least in regions with high iron content. PMID:23591072

  10. Simulation of the AC corona phenomenon with experimental validation

    NASA Astrophysics Data System (ADS)

    Villa, Andrea; Barbieri, Luca; Marco, Gondola; Malgesini, Roberto; Leon-Garzon, Andres R.

    2017-11-01

    The corona effect, and in particular the Trichel phenomenon, is an important aspect of plasma physics with many technical applications, such as pollution reduction, surface and medical treatments. This phenomenon is also associated with components used in the power industry where it is, in many cases, the source of electro-magnetic disturbance, noise and production of undesired chemically active species. Despite the power industry to date using mainly alternating current (AC) transmission, most of the studies related to the corona effect have been carried out with direct current (DC) sources. Therefore, there is technical interest in validating numerical codes capable of simulating the AC phenomenon. In this work we describe a set of partial differential equations that are comprehensive enough to reproduce the distinctive features of the corona in an AC regime. The model embeds some selectable chemical databases, comprising tens of chemical species and hundreds of reactions, the thermal dynamics of neutral species and photoionization. A large set of parameters—deduced from experiments and numerical estimations—are compared, to assess the effectiveness of the proposed approach.

  11. Investigation of the transition of multicycle AC operation in ISTTOK under edge electrode biasing

    NASA Astrophysics Data System (ADS)

    Malaquias, A.; Henriques, R. B.; Silva, C.; Figueiredo, H.; Nedzelskiy, I. S.; Fernandes, H.; Sharma, R.; Plyusnin, V. V.

    2017-11-01

    In this paper we present recent results obtained on plasma edge electrode biasing during AC discharges. The goal is to obtain experimental evidence on a number of plasma parameters that can play a role during the AC transition on the repeatability and reproducibility of AC operation. The control of the plasma density in the quiescent phase is made just before the AC transition by means of positive edge biasing leading to a transitory improved of density (30%-40%). Gas puff experiments show that the increase of background gas pressure during discharge led to a better success of the AC transition. The experimental results indicate that the increase of density during the AC transition induced by edge biasing is followed by an electron temperature drop. The drop in electron temperature leads in most cases the formation of runaway electrons. It has been observed that the runaway population during discharge flattop depends on the interplay between gas content and plasma density and temperature. The results also confirm that the correct balance of external magnetic fields is crucial during the AC transition phase where drift electron currents are formed. The results from the heavy ion beam diagnostic show that the formation of plasma current during consecutive AC transitions is asymmetric. Numerical simulations indicate that for some particular conditions this result could be reproduced from assuming the presence of two counter-currents during AC transition.

  12. Quantitative susceptibility mapping (QSM) as a means to measure brain iron? A post mortem validation study

    PubMed Central

    Langkammer, Christian; Schweser, Ferdinand; Krebs, Nikolaus; Deistung, Andreas; Goessler, Walter; Scheurer, Eva; Sommer, Karsten; Reishofer, Gernot; Yen, Kathrin; Fazekas, Franz; Ropele, Stefan; Reichenbach, Jürgen R.

    2012-01-01

    Quantitative susceptibility mapping (QSM) is a novel technique which allows determining the bulk magnetic susceptibility distribution of tissue in vivo from gradient echo magnetic resonance phase images. It is commonly assumed that paramagnetic iron is the predominant source of susceptibility variations in gray matter as many studies have reported a reasonable correlation of magnetic susceptibility with brain iron concentrations in vivo. Instead of performing direct comparisons, however, all these studies used the putative iron concentrations reported in the hallmark study by Hallgren and Sourander (1958) for their analysis. Consequently, the extent to which QSM can serve to reliably assess brain iron levels is not yet fully clear. To provide such information we investigated the relation between bulk tissue magnetic susceptibility and brain iron concentration in unfixed (in situ) post mortem brains of 13 subjects using MRI and inductively coupled plasma mass spectrometry. A strong linear correlation between chemically determined iron concentration and bulk magnetic susceptibility was found in gray matter structures (r = 0.84, p < 0.001), whereas the correlation coefficient was much lower in white matter (r = 0.27, p < 0.001). The slope of the overall linear correlation was consistent with theoretical considerations of the magnetism of ferritin supporting that most of the iron in the brain is bound to ferritin proteins. In conclusion, iron is the dominant source of magnetic susceptibility in deep gray matter and can be assessed with QSM. In white matter regions the estimation of iron concentrations by QSM is less accurate and more complex because the counteracting contribution from diamagnetic myelinated neuronal fibers confounds the interpretation. PMID:22634862

  13. Low-temperature spin dynamics of a valence bond glass in Ba2YMoO6

    NASA Astrophysics Data System (ADS)

    de Vries, M. A.; Piatek, J. O.; Misek, M.; Lord, J. S.; Rønnow, H. M.; Bos, J.-W. G.

    2013-04-01

    We carried out ac magnetic susceptibility measurements and muon spin relaxation spectroscopy on the cubic double perovskite Ba2YMoO6, down to 50 mK. Below ∼1 K the muon relaxation is typical of a magnetic insulator with a spin-liquid type ground state, i.e. without broken symmetries or frozen moments. However, the ac susceptibility revealed a dilute-spin-glass-like transition below ∼1 K. Antiferromagnetically coupled Mo5+ 4d1 electrons in triply degenerate t2g orbitals are in this material arranged in a geometrically frustrated fcc lattice. Bulk magnetic susceptibility data has previously been interpreted in terms of a freezing to a heterogeneous state with non-magnetic sites where 4d1 electrons have paired in spin-singlets dimers, and residual unpaired Mo5+ 4d1 electron spins. Based on the magnetic heat capacity data it has been suggested that this heterogeneity is the result of kinetic constraints intrinsic to the physics of the pure system (possibly due to topological overprotection) leading to a self-induced glass of valence bonds between neighbouring 4d1 electrons. The muon spin relaxation (μSR) unambiguously points to a heterogeneous state with a static arrangement of unpaired electrons in a background of (valence bond) dimers between the majority of Mo5+ 4d electrons. The ac susceptibility data indicate that the residual magnetic moments freeze into a dilute-spin-glass-like state. This is in apparent contradiction with the muon-spin decoupling at 50 mK in fields up to 200 mT, which indicates that, remarkably, the time scale of the field fluctuations from the residual moments is ∼5 ns. Comparable behaviour has been observed in other geometrically frustrated magnets with spin-liquid-like behaviour and the implications of our observations on Ba2YMoO6 are discussed in this context.

  14. Magnetic susceptibility data for some exposed bedrock in the western conterminous United States

    USGS Publications Warehouse

    Gettings, Mark E.; Bultman, Mark W.

    2014-01-01

    In-place rock magnetic susceptibility measurements for 746 sites in the western conterminous United States are reported in a database. Of these 746 sites, 408 sites are in the Silverton Caldera area of the San Juan Mountains of southwestern Colorado. Of the 408 sites in the Silverton Caldera area, 106 sites are underground. The remaining 338 sites outside the Silverton Caldera area were on outcropping rock, are distributed from southern Arizona to northwestern Wyoming, and include data from California, Nevada, Utah, Colorado, and New Mexico. Rock-density measurements are included for some sites. These data have been collected by various U.S. Geological Survey studies from 1991 through 2012 and are intended to help improve geophysical modeling of the Earth’s crust in the Western United States. A map-based graphical user interface is included to facilitate use of the data.

  15. AC-130 Employment

    DTIC Science & Technology

    2006-01-01

    1 AC -130 Employment Subject Area Aviation EWS 2006 Author Captain Robert Hornick, USMC Report Documentation Page Form ApprovedOMB No. 0704...00-2006 4. TITLE AND SUBTITLE AC -130 Employment 5a. CONTRACT NUMBER 5b. GRANT NUMBER 5c. PROGRAM ELEMENT NUMBER 6. AUTHOR(S) 5d. PROJECT NUMBER... AC -130 gunship is an aircraft that can provide all of these needs. Regrettably, there are too few AC -130’s in the inventory to cover all the needs

  16. Construction and characterisation of near-isogenic Plutella xylostella (Lepidoptera: Plutellidae) strains resistant to Cry1Ac toxin.

    PubMed

    Zhu, Xun; Lei, Yanyuan; Yang, Yanjv; Baxter, Simon W; Li, Jianhong; Wu, Qingjun; Wang, Shaoli; Xie, Wen; Guo, Zhaojiang; Fu, Wei; Zhang, Youjun

    2015-02-01

    Resistance to insecticidal Bacillus thuringiensis (Bt) toxins has arisen in multiple populations of the worldwide Brassica pest Plutella xylostella (L.). To help elucidate the mechanism of resistance to Bt Cry1Ac toxin in a population from Florida, two pairs of near-isogenic lines (NILs) were developed. NILs were generated using either backcross or recombinant inbred line methodologies and evaluated for near-isogenicity with inter-simple-sequence-repeat (ISSR) markers. Backcross line BC6F4 maintained a similar level of Cry1Ac resistance to parental strain DBM1Ac-R (>5000-fold) yet showed 98.24% genetic similarity to the susceptible parental strain DBM1Ac-S. Single-pair backcrosses between DBM1Ac-S and BC6F4 revealed that Cry1Ac resistance was controlled by one recessive autosomal locus. BC6F4 exhibited high levels of cross-resistance to Cry1Ab and Cry1Ah but not to Cry1Ca or Cry1Ie. Near-isogenic strains were constructed to provide a reliable biological system to investigate the mechanism of Cry1Ac resistance in P. xylostella. These data suggest that resistance to Cry1Ac, Cry1Ab and Cry1Ah is probably caused by the alteration of a common receptor not recognised by Cry1Ca or Cry1Ie. Understanding Bt toxin cross-resistance provides valuable information to consider when developing pest control strategies to delay resistance evolution. © 2014 Society of Chemical Industry. © 2014 Society of Chemical Industry.

  17. Frustrated magnetism in doped quasi-triangular lattice materials, Cu2(1-x)Zn2x(OH)3NO3/(C7H15COO)

    NASA Astrophysics Data System (ADS)

    Wu, Jian; Werner, Fletcher; Gangopadhyay, Anup K.; Solin, S. A.

    2010-03-01

    We have performed DC and AC magnetic susceptibility measurements on the spin S=1/2 quasi-triangular lattice materials Cu2(1-x)Zn2x(OH)3NO3/(C7H15COO). The X-ray diffraction experiments reveal that this class of materials has a crystal structure in P21/m space group, in which Cu^2+ and Zn^2+ ions are arranged on a slightly distorted triangular lattice [1]. Cu2(1-)Zn2x(OH)3NO3 with a short inorganic intercalation NO3 group, have a long-range antiferromagnetic order at low temperature. The Neel temperature TN decreases from 11K to 5.6K while the Curie-Weiss temperature increases from -5.1K to +2.8K as the Zn concentration increases from 0 to 65%. After a longer alkanecarboxylate C7H15COO group was introduced into the interlayer space, a spin-glass like behavior in magnetic properties was observed [2]. The value |θcw /TN| is approximately 20, indicating the materials are in a medium level frustrated state. The onset of a ferromagnetic correlation was found in both DC and AC susceptibility data. The interplay of geometrical frustration and the coexistence of ferromagnetic and antiferromagnetic couplings has driven the materials into a glassy ground state. [1] G. Linder, et al., Journal of Solid State Chemistry (1995) [2] M. A. Girtu et al, Phys Rev B 61,4117(2000).

  18. Bacterially synthesized ferrite nanoparticles for magnetic hyperthermia applications.

    PubMed

    Céspedes, Eva; Byrne, James M; Farrow, Neil; Moise, Sandhya; Coker, Victoria S; Bencsik, Martin; Lloyd, Jonathan R; Telling, Neil D

    2014-11-07

    Magnetic hyperthermia uses AC stimulation of magnetic nanoparticles to generate heat for cancer cell destruction. Whilst nanoparticles produced inside magnetotactic bacteria have shown amongst the highest reported heating to date, these particles are magnetically blocked so that strong heating occurs only for mobile particles, unless magnetic field parameters are far outside clinical limits. Here, nanoparticles extracellularly produced by the bacteria Geobacter sulfurreducens are investigated that contain Co or Zn dopants to tune the magnetic anisotropy, saturation magnetization and nanoparticle sizes, enabling heating within clinical field constraints. The heating mechanisms specific to either Co or Zn doping are determined from frequency dependent specific absorption rate (SAR) measurements and innovative AC susceptometry simulations that use a realistic model concerning clusters of polydisperse nanoparticles in suspension. Whilst both particle types undergo magnetization relaxation and show heating effects in water under low AC frequency and field, only Zn doped particles maintain relaxation combined with hysteresis losses even when immobilized. This magnetic heating process could prove important in the biological environment where nanoparticle mobility may not be possible. Obtained SARs are discussed regarding clinical conditions which, together with their enhanced MRI contrast, indicate that biogenic Zn doped particles are promising for combined diagnostics and cancer therapy.

  19. Binding Site Concentration Explains the Differential Susceptibility of Chilo suppressalis and Sesamia inferens to Cry1A-Producing Rice

    PubMed Central

    Han, Chao; Liu, Zewen; Chen, Fajun; Hou, Maolin; Peng, Yufa

    2014-01-01

    Chilo suppressalis and Sesamia inferens are two important lepidopteran rice pests that occur concurrently during outbreaks in paddy fields in the main rice-growing areas of China. Previous and current field tests demonstrate that the transgenic rice line Huahui 1 (HH1) producing a Cry1Ab-Cry1Ac hybrid toxin from the bacterium Bacillus thuringiensis reduces egg and larval densities of C. suppressalis but not of S. inferens. This differential susceptibility to HH1 rice correlates with the reduced susceptibility to Cry1Ab and Cry1Ac toxins in S. inferens larvae compared to C. suppressalis larvae. The goal of this study was to identify the mechanism responsible for this differential susceptibility. In saturation binding assays, both Cry1Ab and Cry1Ac toxins bound with high affinity and in a saturable manner to midgut brush border membrane vesicles (BBMV) from C. suppressalis and S. inferens larvae. While binding affinities were similar, a dramatically lower concentration of Cry1A toxin binding sites was detected for S. inferens BBMV than for C. suppressalis BBMV. In contrast, no significant differences between species were detected for Cry1Ca toxin binding to BBMV. Ligand blotting detected BBMV proteins binding Cry1Ac or Cry1Ca toxins, some of them unique to C. suppressalis or S. inferens. These data support that reduced Cry1A binding site concentration is associated with a lower susceptibility to Cry1A toxins and HH1 rice in S. inferens larvae than in C. suppressalis larvae. Moreover, our data support Cry1Ca as a candidate for pyramiding efforts with Cry1A-producing rice to extend the activity range and durability of this technology against rice stem borers. PMID:24928872

  20. Binding site concentration explains the differential susceptibility of Chilo suppressalis and Sesamia inferens to Cry1A-producing rice.

    PubMed

    Han, Lanzhi; Han, Chao; Liu, Zewen; Chen, Fajun; Jurat-Fuentes, Juan Luis; Hou, Maolin; Peng, Yufa

    2014-08-01

    Chilo suppressalis and Sesamia inferens are two important lepidopteran rice pests that occur concurrently during outbreaks in paddy fields in the main rice-growing areas of China. Previous and current field tests demonstrate that the transgenic rice line Huahui 1 (HH1) producing a Cry1Ab-Cry1Ac hybrid toxin from the bacterium Bacillus thuringiensis reduces egg and larval densities of C. suppressalis but not of S. inferens. This differential susceptibility to HH1 rice correlates with the reduced susceptibility to Cry1Ab and Cry1Ac toxins in S. inferens larvae compared to C. suppressalis larvae. The goal of this study was to identify the mechanism responsible for this differential susceptibility. In saturation binding assays, both Cry1Ab and Cry1Ac toxins bound with high affinity and in a saturable manner to midgut brush border membrane vesicles (BBMV) from C. suppressalis and S. inferens larvae. While binding affinities were similar, a dramatically lower concentration of Cry1A toxin binding sites was detected for S. inferens BBMV than for C. suppressalis BBMV. In contrast, no significant differences between species were detected for Cry1Ca toxin binding to BBMV. Ligand blotting detected BBMV proteins binding Cry1Ac or Cry1Ca toxins, some of them unique to C. suppressalis or S. inferens. These data support that reduced Cry1A binding site concentration is associated with a lower susceptibility to Cry1A toxins and HH1 rice in S. inferens larvae than in C. suppressalis larvae. Moreover, our data support Cry1Ca as a candidate for pyramiding efforts with Cry1A-producing rice to extend the activity range and durability of this technology against rice stem borers. Copyright © 2014, American Society for Microbiology. All Rights Reserved.

  1. Magnetic fabric and flow direction in the Ediacaran Imider dyke swarms (Eastern Anti-Atlas, Morocco), inferred from the Anisotropy of Magnetic Susceptibility (AMS)

    NASA Astrophysics Data System (ADS)

    Otmane, Khadija; Errami, Ezzoura; Olivier, Philippe; Berger, Julien; Triantafyllou, Antoine; Ennih, Nasser

    2018-03-01

    Located in the Imiter Inlier (Eastern Saghro, Anti-Atlas, Morocco), Ediacaran volcanic dykes have been studied for their petrofabric using Anisotropy of Magnetic Susceptibility (AMS) technique. Four dykes, namely TF, TD, FF and FE show andesitic compositions and are considered to belong to the same dyke swarm. They are oriented respectively N25E, N40E, N50E, and N10E and have been emplaced during a first tectonic event. The dyke FW, oriented N90E displays a composition of alkali basalt and its emplacement is attributed to a subsequent tectonic event. These rocks are propylitized under greenschist facies conditions forming a secondary paragenesis constituted by calcite, chlorite, epidote and sericite. The dykes TF, TD, FF and FE are sub-volcanic calc-alkaline, typical of post-collisional basalts/andesites, belonging to plate margin andesites. The FW dyke shows a within-plate basalt signature; alkaline affinity reflecting a different petrogenetic process. The thermomagnetic analyses show a dominantly ferromagnetic behaviour in the TF dyke core carried by single domain Ti-poor magnetite, maghemite and pyrrhotite. The dominantly paramagnetic susceptibilities in TF dyke rims and TD, FE, FF and FW dykes are controlled by ilmenite, amphibole, pyroxene and chlorite. The magnetic fabrics of the Imider dykes, determined by our AMS study, allows us to reconstitute the tectonic conditions which prevailed during the emplacement of these two generations of volcanic dykes. The first tectonic event was characterized by a roughly NE-SW compression and the second tectonic event is characterized by an E-W shortening followed by a relaxation recording the end of the Pan-African orogeny in the eastern Anti-Atlas.

  2. Phase processing for quantitative susceptibility mapping of regions with large susceptibility and lack of signal.

    PubMed

    Fortier, Véronique; Levesque, Ives R

    2018-06-01

    Phase processing impacts the accuracy of quantitative susceptibility mapping (QSM). Techniques for phase unwrapping and background removal have been proposed and demonstrated mostly in brain. In this work, phase processing was evaluated in the context of large susceptibility variations (Δχ) and negligible signal, in particular for susceptibility estimation using the iterative phase replacement (IPR) algorithm. Continuous Laplacian, region-growing, and quality-guided unwrapping were evaluated. For background removal, Laplacian boundary value (LBV), projection onto dipole fields (PDF), sophisticated harmonic artifact reduction for phase data (SHARP), variable-kernel sophisticated harmonic artifact reduction for phase data (V-SHARP), regularization enabled sophisticated harmonic artifact reduction for phase data (RESHARP), and 3D quadratic polynomial field removal were studied. Each algorithm was quantitatively evaluated in simulation and qualitatively in vivo. Additionally, IPR-QSM maps were produced to evaluate the impact of phase processing on the susceptibility in the context of large Δχ with negligible signal. Quality-guided unwrapping was the most accurate technique, whereas continuous Laplacian performed poorly in this context. All background removal algorithms tested resulted in important phase inaccuracies, suggesting that techniques used for brain do not translate well to situations where large Δχ and no or low signal are expected. LBV produced the smallest errors, followed closely by PDF. Results suggest that quality-guided unwrapping should be preferred, with PDF or LBV for background removal, for QSM in regions with large Δχ and negligible signal. This reduces the susceptibility inaccuracy introduced by phase processing. Accurate background removal remains an open question. Magn Reson Med 79:3103-3113, 2017. © 2017 International Society for Magnetic Resonance in Medicine. © 2017 International Society for Magnetic Resonance in Medicine.

  3. Exploiting the Temperature/Concentration Dependence of Magnetic Susceptibility to Control Convection in Fundamental Studies of Solidification Phenomena

    NASA Technical Reports Server (NTRS)

    Evans, J. W.; Xu, Dong; Jones, W. Kinzy, Jr.; Szofran, Frank R.

    1999-01-01

    The objective of this new research project is to demonstrate by experiment, supplemented by mathematical modeling and physical property measurement, that the effects of buoyancy driven convection can be largely eliminated in ground-based experiments, and further reduced in flight, by applying a new technique. That technique exploits the dependence of magnetic susceptibility on composition or temperature. It is emphasized at the outset that the phenomenon to be exploited is fundamentally and practically different from the magnetic damping of convection in conducting liquids that has been the subject of much prior research. The concept suggesting this research is that all materials, even non-conductors, when placed in a magnetic field gradient, experience a force. Of particular interest here are paramagnetic and diamagnetic materials, classes which embrace the "model alloys", such as succinonitrile-acetone, that have been used by others investigating the fundamentals of solidification. Such alloys will exhibit a dependence of susceptibility on composition. The consequence is that, with a properly oriented field (gradient) a force will arise that can be made to be equal to, but opposite, the buoyancy force arising from concentration (or temperature) gradients. In this way convection can be stilled. The role of convection in determining the microstructure, and thereby properties, of materials is well known. Elimination of that convection has both scientific and technological consequences. Our knowledge of diffusive phenomena in solidification, phenomena normally hidden by the dominance of convection, is enhanced if we can study solidification of quiescent liquids. Furthermore, the microstructure, microchemistry and properties of materials (thereby practical value) are affected by the convection occurring during their solidification. Hitherto the method of choice for elimination of convection has been experimentation in microgravity. However, even in low Earth orbit

  4. Finite-size behaviour of generalized susceptibilities in the whole phase plane of the Potts model

    NASA Astrophysics Data System (ADS)

    Pan, Xue; Zhang, Yanhua; Chen, Lizhu; Xu, Mingmei; Wu, Yuanfang

    2018-01-01

    We study the sign distribution of generalized magnetic susceptibilities in the temperature-external magnetic field plane using the three-dimensional three-state Potts model. We find that the sign of odd-order susceptibility is opposite in the symmetric (disorder) and broken (order) phases, but that of the even-order one remains positive when it is far away from the phase boundary. When the critical point is approached from the crossover side, negative fourth-order magnetic susceptibility is observable. It is also demonstrated that non-monotonic behavior occurs in the temperature dependence of the generalized susceptibilities of the energy. The finite-size scaling behavior of the specific heat in this model is mainly controlled by the critical exponent of the magnetic susceptibility in the three-dimensional Ising universality class. Supported by Fund Project of National Natural Science Foundation of China (11647093, 11405088, 11521064), Fund Project of Sichuan Provincial Department of Education (16ZB0339), Fund Project of Chengdu Technological University (2016RC004) and the Major State Basic Research Development Program of China (2014CB845402)

  5. Thermodynamic properties of a hard/soft-magnetic bilayer model

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Taaev, T. A., E-mail: taaev89@mail.ru; Khizriev, K. Sh.; Murtazaev, A. K.

    2016-05-15

    A model for describing the thermodynamic properties of a hard/soft-magnetic bilayer is proposed and thoroughly studied using the Monte Carlo method. Temperature dependences of the heat capacity, total magnetization, magnetizations of the hard- and soft-magnetic layers, total magnetic susceptibility, and susceptibilities of the hard- and soft-magnetic layers have been calculated by this method in the framework of the proposed model. The obtained temperature dependences of the heat capacity and magnetic susceptibility display double maxima that result from the two phase transitions that take place in the system. The influence of system dimensions on the thermodynamic properties of the model hasmore » been considered.« less

  6. FAST TRACK COMMUNICATION Determination of atomic site susceptibility tensors from neutron diffraction data on polycrystalline samples

    NASA Astrophysics Data System (ADS)

    Gukasov, A.; Brown, P. J.

    2010-12-01

    Polarized neutron diffraction can provide information about the atomic site susceptibility tensor χij characterizing the magnetic response of individual atoms to an external magnetic field (Gukasov and Brown 2002 J. Phys.: Condens. Mater. 14 8831). The six independent atomic susceptibility parameters (ASPs) can be determined from polarized neutron flipping ratio measurements on single crystals and visualized as magnetic ellipsoids which are analogous to the thermal ellipsoids obtained from atomic displacement parameters (ADPs). We demonstrate now that the information about local magnetic susceptibility at different magnetic sites in a crystal can also be obtained from polarized and unpolarized neutron diffraction measurements on magnetized powder samples. The validity of the method is illustrated by the results of such measurements on a polycrystalline sample of Tb2Sn2O7.

  7. Quantitative susceptibility mapping: Report from the 2016 reconstruction challenge.

    PubMed

    Langkammer, Christian; Schweser, Ferdinand; Shmueli, Karin; Kames, Christian; Li, Xu; Guo, Li; Milovic, Carlos; Kim, Jinsuh; Wei, Hongjiang; Bredies, Kristian; Buch, Sagar; Guo, Yihao; Liu, Zhe; Meineke, Jakob; Rauscher, Alexander; Marques, José P; Bilgic, Berkin

    2018-03-01

    The aim of the 2016 quantitative susceptibility mapping (QSM) reconstruction challenge was to test the ability of various QSM algorithms to recover the underlying susceptibility from phase data faithfully. Gradient-echo images of a healthy volunteer acquired at 3T in a single orientation with 1.06 mm isotropic resolution. A reference susceptibility map was provided, which was computed using the susceptibility tensor imaging algorithm on data acquired at 12 head orientations. Susceptibility maps calculated from the single orientation data were compared against the reference susceptibility map. Deviations were quantified using the following metrics: root mean squared error (RMSE), structure similarity index (SSIM), high-frequency error norm (HFEN), and the error in selected white and gray matter regions. Twenty-seven submissions were evaluated. Most of the best scoring approaches estimated the spatial frequency content in the ill-conditioned domain of the dipole kernel using compressed sensing strategies. The top 10 maps in each category had similar error metrics but substantially different visual appearance. Because QSM algorithms were optimized to minimize error metrics, the resulting susceptibility maps suffered from over-smoothing and conspicuity loss in fine features such as vessels. As such, the challenge highlighted the need for better numerical image quality criteria. Magn Reson Med 79:1661-1673, 2018. © 2017 International Society for Magnetic Resonance in Medicine. © 2017 International Society for Magnetic Resonance in Medicine.

  8. Critical magnetic fields of superconducting aluminum-substituted Ba{sub 8}Si{sub 42}Al{sub 4} clathrate

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Li, Yang, E-mail: yang.li@upr.edu; Garcia, Jose; Lu, Kejie

    2015-06-07

    In recent years, efforts have been made to explore the superconductivity of clathrates containing crystalline frameworks of group-IV elements. The superconducting silicon clathrate is unusual in that the structure is dominated by strong sp{sup 3} covalent bonds between silicon atoms, rather than the metallic bonding that is more typical of traditional superconductors. This paper reports on critical magnetic fields of superconducting Al-substituted silicon clathrates, which were investigated by transport, ac susceptibility, and dc magnetization measurements in magnetic fields up to 90 kOe. For the sample Ba{sub 8}Si{sub 42}Al{sub 4}, the critical magnetic fields were measured to be H{sub C1} = 40.2 Oe andmore » H{sub C2} = 66.4 kOe. The London penetration depth of 4360 Å and the coherence length 70 Å were obtained, whereas the estimated Ginzburg–Landau parameter of κ = 62 revealed that Ba{sub 8}Si{sub 42}Al{sub 4} is a strong type-II superconductor.« less

  9. Investigation on the IL-18 -607A/C and -137C/G on the susceptibility of ischemic stroke.

    PubMed

    Shi, Jin-He; Niu, Li-Dan; Chen, Xi-Yan; Hou, Jing-Yu; Yang, Ping; Li, Guang-Peng

    2015-01-01

    We conducted a case-control study with 322 cases and 322 controls to assess the role of the two common SNPs in the promoter of IL-18 gene. Polymerase chain reaction restriction fragment length of polymorphism (PCR-RFLP) was taken to genotype -607A/C and -137C/G in the promoter of the IL-18 gene. By comparing cases and control subjects, we found that IS cases were more likely to have higher BMI, higher proportion of hypertension, and have higher proportion of smokers and drinkers. We found that IL-18 -607CC genotype (OR=1.70, 95% CI=1.03-2.81) and C allele (OR=1.26, 95% CI=1.01-1.58) were significantly more frequent in IS patients when compared with AA genotype. We did not find significant association between IL-18 -607A/C gene polymorphism and BMI, hypertension, smoking and drinking on the risk of IS. Our study suggests that polymorphisms in IL-18 -607A/C can influence the development of IS, and this gene polymorphism is associated with risk of IS in a Chinese population.

  10. a Comparison of Anisotropy of Magnetic Susceptibility and Anisotropy of Anhysteretic Remanence Data from the Early Jurassic Basal Karoo Igneous Series, South Africa

    NASA Astrophysics Data System (ADS)

    Geissman, J. W.; Ferre, E. C.; Mason, S. N.; Maes, S. M.; Lehman, A.; Marsh, J.

    2011-12-01

    Although anisotropy of magnetic susceptibility (AMS) data from plutonic rocks has often been used as a proxy for magma flow, many studies indicate that the relationship between the principal axes of the anisotropy of magnetic susceptibility (AMS) and independently inferred flow patterns is not simple. Data from dikes show that complications may arise from the contribution of single domain (SD) magnetite grains, imbricated symmetric fabrics along dike margins and post-solidification thermal stresses. Limited studies have focused on subhorizontal tabular intrusions and their magnetic fabrics. The Karoo Large Igneous Province in South Africa hosts a well-exposed, laterally extensive set of undeformed, stacked gabbroic sills emplaced parallel to bedding in the Karoo Basin. The sills range in thickness from about 1 m up to 1000 m and have a relatively constant petrologic composition of gabbros and gabbro-norites. Theses sills are distributed throughout the entire Karoo Basin and were emplaced at several stratigraphic heights / depths in the Karoo stratigraphic column. Oriented core samples were collected from 30 different sills and yielded 1598 specimens for AMS and AARM fabric data as well as paleomagnetic measurements. The low-field magnetic susceptibility Km ranges widely from about 100 to 20,000 x 10-6 [SI Vol] and the degree of anisotropy P' ranges from 1.01 to 1.10, with a broad correlation between Km and P'. Thermomagnetic experiments reveal that the main magnetic carrier is titanomagnetite with variable ulvöspinel content; hysteresis data show a pseudo-single domain grain dominance. The AMS and AARM fabric data, collected for all sites, yield normal fabric relations and are consistent with the nearly horizontal attitude of the sills in most of the sills, with subvertical K3 AMS and AARM axes. Generally, AARM parameters are greater than AMS values, although the dispersion of AARM data is more variable among sites. In five of 30 sills, K3 and K1 AMS axes are

  11. Magnetic field dependent measurement techniques of surface tension of magnetic fluid at an air interface

    NASA Astrophysics Data System (ADS)

    Nair, Nishant; Virpura, Hiral; Patel, Rajesh

    2015-06-01

    We describe here two measurement techniques to determine surface tension of magnetic fluid. (i) magneti c field dependent capillary rise method and (ii) Taylor wavelength method in which the distance between the consecutive stable spikes was measured and then surface tension was calculated. The surface tension measurements from both the methods are compared. It is observed that surface tension of magnetic fluid increases with increase in magnetic field due to field dependent structure formation in magnetic fluid at an air interface. We have also measured magnetic susceptibility and surface tension for different volume fractions. The measurement of magnetic susceptibility is carried out using Quincke's experimental techniques.

  12. Effects of white matter microstructure on phase and susceptibility maps.

    PubMed

    Wharton, Samuel; Bowtell, Richard

    2015-03-01

    To investigate the effects on quantitative susceptibility mapping (QSM) and susceptibility tensor imaging (STI) of the frequency variation produced by the microstructure of white matter (WM). The frequency offsets in a WM tissue sample that are not explained by the effect of bulk isotropic or anisotropic magnetic susceptibility, but rather result from the local microstructure, were characterized for the first time. QSM and STI were then applied to simulated frequency maps that were calculated using a digitized whole-brain, WM model formed from anatomical and diffusion tensor imaging data acquired from a volunteer. In this model, the magnitudes of the frequency contributions due to anisotropy and microstructure were derived from the results of the tissue experiments. The simulations suggest that the frequency contribution of microstructure is much larger than that due to bulk effects of anisotropic magnetic susceptibility. In QSM, the microstructure contribution introduced artificial WM heterogeneity. For the STI processing, the microstructure contribution caused the susceptibility anisotropy to be significantly overestimated. Microstructure-related phase offsets in WM yield artifacts in the calculated susceptibility maps. If susceptibility mapping is to become a robust MRI technique, further research should be carried out to reduce the confounding effects of microstructure-related frequency contributions. © 2014 Wiley Periodicals, Inc.

  13. Analysis of Magnetic Anisotropy and the Role of Magnetic Dilution in Triggering Single-Molecule Magnet (SMM) Behavior in a Family of CoII YIII Dinuclear Complexes with Easy-Plane Anisotropy.

    PubMed

    Palacios, María A; Nehrkorn, Joscha; Suturina, Elizaveta A; Ruiz, Eliseo; Gómez-Coca, Silvia; Holldack, Karsten; Schnegg, Alexander; Krzystek, Jurek; Moreno, José M; Colacio, Enrique

    2017-08-25

    Three new closely related Co II Y III complexes of general formula [Co(μ-L)(μ-X)Y(NO 3 ) 2 ] (X - =NO 3 - 1, benzoate 2, or 9-anthracenecarboxylato 3) have been prepared with the compartmental ligand N,N',N''-trimethyl-N,N''-bis(2-hydroxy-3-methoxy-5-methylbenzyl)diethylenetriamine (H 2 L). In these complexes, Co II and Y III are triply bridged by two phenoxide groups belonging to the di-deprotonated ligand (L 2- ) and one ancillary anion X - . The change of the ancillary bridging group connecting Co II and Y III ions induces small differences in the trigonally distorted CoN 3 O 3 coordination sphere with a concomitant tuning of the magnetic anisotropy and intermolecular interactions. Direct current magnetic, high-frequency and -field EPR (HFEPR), frequency domain Fourier transform THz electron paramagnetic resonance (FD-FT THz-EPR) measurements, and ab initio theoretical calculations demonstrate that Co II ions in compounds 1-3 have large and positive D values (≈50 cm -1 ), which decrease with increasing the distortion of the pseudo-octahedral Co II coordination sphere. Dynamic ac magnetic susceptibility measurements indicate that compound 1 exhibits field-induced single-molecule magnet (SMM) behavior, whereas compounds 2 and 3 only display this behavior when they are magnetically diluted with diamagnetic Zn II (Zn/Co=10:1). In view of this, it is always advisable to use magnetically diluted complexes, in which intermolecular interactions and quantum tunneling of magnetism (QTM) would be at least partly suppressed, so that "hidden single-ion magnet (SIM)" behavior could emerge. Field- and temperature-dependence of the relaxation times indicate the prevalence of the Raman process in all these complexes above approximately 3 K. © 2017 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

  14. Synthesis, structure and magnetic properties of nanostructured La1-xAxFe0.5Mn0.5O3 (A = Ca, Sr and Pb; x = 0 & 0.25) perovskites

    NASA Astrophysics Data System (ADS)

    Hossain, Aslam; Ghosh, Debamalya; Dutta, Uma; Walke, Pravin S.; Mordvinova, Natalia E.; Lebedev, Oleg I.; Sinha, Bhavesh; Pal, Kamalesh; Gayen, Arup; Kundu, Asish K.; Seikh, Md. Motin

    2017-12-01

    The effect of hole doping on magnetic properties of LaFe0.5Mn0.5O3 have been investigated. All the ceramics samples La1-xAxFe0.5Mn0.5O3 (A = Ca, Sr and Pb; x = 0 & 0.25) were synthesized at 500 °C by sol-gel method and the particles size were found to be in nanodimension. The samples were characterized by X-ray and electron diffraction, HRTEM and both dc and ac-magnetization measurements. The X-ray and electron diffraction patterns were indexed by cubic Pm-3m space group. The particle size of the LaFe0.5Mn0.5O3 is ∼100 nm, whereas the Pb-doped sample is ∼50 nm and for Ca or Sr doped samples the size is ∼10-30 nm. Both dc and ac-susceptibility measurements suggest that the effect of hole doping and A-site cationic radius in LaFe0.5Mn0.5O3 have no significant role on magnetic properties. However, the particle size plays an important role on magnetic property due to the development of surface ferromagnetic cluster at nanoscale. The competing interactions lead to magnetic phase separation where local ferromagnetic clusters coexist within the antiferromagentic matrix in all the samples.

  15. AC current rectification in Nb films with or without symmetrical Nb/Ni periodic pinning arrays in perpendicular magnetic field

    NASA Astrophysics Data System (ADS)

    Pryadun, Vladimir

    2005-03-01

    Rectification of AC current has been observed in plain superconducting Nb films and in Nb/Ni films with symmetric periodic pinning centers. The rectified DC voltage appears for various sample geometries (cross or strip) both along and transverse to the alternating current direction, is nearly anti-symmetric with perpendicular magnetic field and strongly dependent on temperature below Tc. Analyses of the data at different temperatures, drive frequencies from 100kHz to 150MHz and at the different sample sides [1] shows that not far below Tc the rectification phenomena can be understood in terms of generation of electric fields due to local excess of critical current. Further below Tc anisotropic pinning effects could also contribute to the rectification. [1] F.G.Aliev, et al., Cond. Mat.405656. Supported by Comunidad Autonoma de Madrid -CAM/07N/0050/2002

  16. AC Loss Analysis of MgB2-Based Fully Superconducting Machines

    NASA Astrophysics Data System (ADS)

    Feddersen, M.; Haran, K. S.; Berg, F.

    2017-12-01

    Superconducting electric machines have shown potential for significant increase in power density, making them attractive for size and weight sensitive applications such as offshore wind generation, marine propulsion, and hybrid-electric aircraft propulsion. Superconductors exhibit no loss under dc conditions, though ac current and field produce considerable losses due to hysteresis, eddy currents, and coupling mechanisms. For this reason, many present machines are designed to be partially superconducting, meaning that the dc field components are superconducting while the ac armature coils are conventional conductors. Fully superconducting designs can provide increases in power density with significantly higher armature current; however, a good estimate of ac losses is required to determine the feasibility under the machines intended operating conditions. This paper aims to characterize the expected losses in a fully superconducting machine targeted towards aircraft, based on an actively-shielded, partially superconducting machine from prior work. Various factors are examined such as magnet strength, operating frequency, and machine load to produce a model for the loss in the superconducting components of the machine. This model is then used to optimize the design of the machine for minimal ac loss while maximizing power density. Important observations from the study are discussed.

  17. Effects of tissue susceptibility on brain temperature mapping.

    PubMed

    Maudsley, Andrew A; Goryawala, Mohammed Z; Sheriff, Sulaiman

    2017-02-01

    A method for mapping of temperature over a large volume of the brain using volumetric proton MR spectroscopic imaging has been implemented and applied to 150 normal subjects. Magnetic susceptibility-induced frequency shifts in gray- and white-matter regions were measured and included as a correction in the temperature mapping calculation. Additional sources of magnetic susceptibility variations of the individual metabolite resonance frequencies were also observed that reflect the cellular-level organization of the brain metabolites, with the most notable differences being attributed to changes of the N-Acetylaspartate resonance frequency that reflect the intra-axonal distribution and orientation of the white-matter tracts with respect to the applied magnetic field. These metabolite-specific susceptibility effects are also shown to change with age. Results indicate no change of apparent brain temperature with age from 18 to 84 years old, with a trend for increased brain temperature throughout the cerebrum in females relative for males on the order of 0.1°C; slightly increased temperatures in the left hemisphere relative to the right; and a lower temperature of 0.3°C in the cerebellum relative to that of cerebral white-matter. This study presents a novel acquisition method for noninvasive measurement of brain temperature that is of potential value for diagnostic purposes and treatment monitoring, while also demonstrating limitations of the measurement due to the confounding effects of tissue susceptibility variations. Copyright © 2016 Elsevier Inc. All rights reserved.

  18. Quantitative Susceptibility Mapping in Parkinson's Disease.

    PubMed

    Langkammer, Christian; Pirpamer, Lukas; Seiler, Stephan; Deistung, Andreas; Schweser, Ferdinand; Franthal, Sebastian; Homayoon, Nina; Katschnig-Winter, Petra; Koegl-Wallner, Mariella; Pendl, Tamara; Stoegerer, Eva Maria; Wenzel, Karoline; Fazekas, Franz; Ropele, Stefan; Reichenbach, Jürgen Rainer; Schmidt, Reinhold; Schwingenschuh, Petra

    2016-01-01

    Quantitative susceptibility mapping (QSM) and R2* relaxation rate mapping have demonstrated increased iron deposition in the substantia nigra of patients with idiopathic Parkinson's disease (PD). However, the findings in other subcortical deep gray matter nuclei are converse and the sensitivity of QSM and R2* for morphological changes and their relation to clinical measures of disease severity has so far been investigated only sparsely. The local ethics committee approved this study and all subjects gave written informed consent. 66 patients with idiopathic Parkinson's disease and 58 control subjects underwent quantitative MRI at 3T. Susceptibility and R2* maps were reconstructed from a spoiled multi-echo 3D gradient echo sequence. Mean susceptibilities and R2* rates were measured in subcortical deep gray matter nuclei and compared between patients with PD and controls as well as related to clinical variables. Compared to control subjects, patients with PD had increased R2* values in the substantia nigra. QSM also showed higher susceptibilities in patients with PD in substantia nigra, in the nucleus ruber, thalamus, and globus pallidus. Magnetic susceptibility of several of these structures was correlated with the levodopa-equivalent daily dose (LEDD) and clinical markers of motor and non-motor disease severity (total MDS-UPDRS, MDS-UPDRS-I and II). Disease severity as assessed by the Hoehn & Yahr scale was correlated with magnetic susceptibility in the substantia nigra. The established finding of higher R2* rates in the substantia nigra was extended by QSM showing superior sensitivity for PD-related tissue changes in nigrostriatal dopaminergic pathways. QSM additionally reflected the levodopa-dosage and disease severity. These results suggest a more widespread pathologic involvement and QSM as a novel means for its investigation, more sensitive than current MRI techniques.

  19. Spectroscopy of Magnetic Excitations in Magnetic Superconductors Using Vortex Motion

    NASA Astrophysics Data System (ADS)

    Bulaevskii, L. N.; Hruška, M.; Maley, M. P.

    2005-11-01

    In magnetic superconductors a moving vortex lattice is accompanied by an ac magnetic field which leads to the generation of spin waves. At resonance conditions the dynamics of vortices in magnetic superconductors changes drastically, resulting in strong peaks in the dc I-V characteristics at voltages at which the washboard frequency of the vortex lattice matches the spin wave frequency ωs(g), where g are the reciprocal vortex lattice vectors. We show that if the washboard frequency lies above the magnetic gap, measurement of the I-V characteristics provides a new method to obtain information on the spectrum of magnetic excitations in borocarbides and cuprate layered magnetic superconductors.

  20. Superconducting magnetic energy storage for asynchronous electrical systems

    DOEpatents

    Boenig, Heinrich J.

    1986-01-01

    A superconducting magnetic energy storage coil connected in parallel between converters of two or more ac power systems provides load leveling and stability improvement to any or all of the ac systems. Control is provided to direct the charging and independently the discharging of the superconducting coil to at least a selected one of the ac power systems.

  1. Magnetic suspension and balance system study

    NASA Technical Reports Server (NTRS)

    Boom, R. W.; Eyssa, Y. M.; Mcintosh, G. E.; Abdelsalam, M. K.

    1984-01-01

    A compact design for a superconducting magnetic suspension and balance system is developed for a 8 ft. x 8 ft. transonic wind tunnel. The main features of the design are: a compact superconducting solenoid in the suspended airplane model; permanent magnet wings; one common liquid helium dewar for all superconducting coils; efficient new race track coils for roll torques; use of established 11 kA cryostable AC conductor; acceptable AC losses during 10 Hz control even with all steel structure; and a 560 liter/hour helium liquefier. Considerable design simplicity, reduced magnet weights, and reduced heat leak results from using one common dewar which eliminates most heavy steel structure between coils and the suspended model. Operational availability is thought to approach 100% for such magnet systems. The weight and cost of the magnet system is approximately one-third that of previous less compact designs.

  2. Pinning Susceptibility at the Jamming Transition

    NASA Astrophysics Data System (ADS)

    Graves, Amy; Padgett, Elliot; Goodrich, Carl; Liu, Andrea

    2013-03-01

    Jamming in the presence of fixed or pinned obstacles, representing quenched disorder, is a situation of both practical and theoretical interest. We study the jamming of soft, bidisperse discs in which a subset of discs are pinned while the remaining particles equilibrate around them at a given volume fraction. The obstacles provide a supporting structure for the jammed configuration which not only lowers the jamming threshold, ϕJ, but affects the coordination number and other parameters of interest as the critical point is approached. In the limit of low obstacle density, one can calculate a pinning susceptibility χP, analogous to the magnetic susceptibility, with obstacle density playing the role of the magnetic field. The pinning susceptibility is thus expected to diverge in the thermodynamic limit as χP ~| ϕ -ϕJ | -γP . Finite-size scaling calculations allow us to confirm this and calculate the critical exponent, γP. Acknowledgement is made to the Donors of the Petrolium Research Fund administered by the American Chemical Society, Swarthmore College's Eugene M. Lang Faculty Fellowship, NSF grant DMR-1062638 and DOE grant DE-FG02-05ER46199.

  3. ESR1 single nucleotide polymorphisms predict breast cancer susceptibility in the central European Caucasian population.

    PubMed

    Lipphardt, Mark F; Deryal, Mustafa; Ong, Mei Fang; Schmidt, Werner; Mahlknecht, Ulrich

    2013-01-01

    Estrogen and progesterone hormones are key regulators of a wide variety of biological processes. In addition to their influence on reproduction, cell differentiation and apoptosis, they affect inflammatory response, cell metabolism and most importantly, they regulate physiological breast tissue proliferation and differentiation as well as the development and progression of breast cancer. In order to assess whether genetic variants in the steroid hormone receptor gene ESR1 (estrogen receptor alpha) had an effect on sporadic breast cancer susceptibility, we assessed 7 ESR1 single nucleotide polymorphisms (SNPs) for associations with breast cancer susceptibility and clinical parameters in 221 breast cancer patients and 221 controls, respectively. We identified ESR1 intron SNP +2464 C/T (rs3020314) and ESR1 intron SNP -4576 A/C (rs1514348) to correlate with breast cancer susceptibility and progesterone receptor expression status. Patients genotyped CT for ESR1 intron SNP +2464 (rs3020314) (p ≤ 0.045) or genotyped AC for ESR1 intron SNP -4576 (rs1514348) (p ≤ 0.000026) were identified to carry a significant risk as to the development of breast cancer in the Central European Caucasian population (both together: p ≤ 0.000488). Our study could confirm previous associations and revealed new associations of SNP rs1514348 with susceptibility to breast cancer and clinical outcome, which might be used as new additional SNP markers.

  4. Sensitivity Enhancement in Magnetic Sensors Based on Ferroelectric-Bimorphs and Multiferroic Composites.

    PubMed

    Sreenivasulu, Gollapudi; Qu, Peng; Petrov, Vladimir; Qu, Hongwei; Srinivasan, Gopalan

    2016-02-20

    Multiferroic composites with ferromagnetic and ferroelectric phases have been studied in recent years for use as sensors of AC and DC magnetic fields. Their operation is based on magneto-electric (ME) coupling between the electric and magnetic subsystems and is mediated by mechanical strain. Such sensors for AC magnetic fields require a bias magnetic field to achieve pT-sensitivity. Novel magnetic sensors with a permanent magnet proof mass, either on a ferroelectric bimorph or a ferromagnetic-ferroelectric composite, are discussed. In both types, the interaction between the applied AC magnetic field and remnant magnetization of the magnet results in a mechanical strain and a voltage response in the ferroelectric. Our studies have been performed on sensors with a Nd-Fe-B permanent magnet proof mass on (i) a bimorph of oppositely-poled lead zirconate titanate (PZT) platelets and (ii) a layered multiferroic composite of PZT-Metglas-Ni. The sensors have been characterized in terms of sensitivity and equivalent magnetic noise N. Noise N in both type of sensors is on the order of 200 pT/√Hz at 1 Hz, a factor of 10 improvement compared to multiferroic sensors without a proof mass. When the AC magnetic field is applied at the bending resonance for the bimorph, the measured N ≈ 700 pT/√Hz. We discuss models based on magneto-electro-mechanical coupling at low frequency and bending resonance in the sensors and theoretical estimates of ME voltage coefficients are in very good agreement with the data.

  5. Sensitivity Enhancement in Magnetic Sensors Based on Ferroelectric-Bimorphs and Multiferroic Composites

    PubMed Central

    Sreenivasulu, Gollapudi; Qu, Peng; Petrov, Vladimir; Qu, Hongwei; Srinivasan, Gopalan

    2016-01-01

    Multiferroic composites with ferromagnetic and ferroelectric phases have been studied in recent years for use as sensors of AC and DC magnetic fields. Their operation is based on magneto-electric (ME) coupling between the electric and magnetic subsystems and is mediated by mechanical strain. Such sensors for AC magnetic fields require a bias magnetic field to achieve pT-sensitivity. Novel magnetic sensors with a permanent magnet proof mass, either on a ferroelectric bimorph or a ferromagnetic-ferroelectric composite, are discussed. In both types, the interaction between the applied AC magnetic field and remnant magnetization of the magnet results in a mechanical strain and a voltage response in the ferroelectric. Our studies have been performed on sensors with a Nd-Fe-B permanent magnet proof mass on (i) a bimorph of oppositely-poled lead zirconate titanate (PZT) platelets and (ii) a layered multiferroic composite of PZT-Metglas-Ni. The sensors have been characterized in terms of sensitivity and equivalent magnetic noise N. Noise N in both type of sensors is on the order of 200 pT/√Hz at 1 Hz, a factor of 10 improvement compared to multiferroic sensors without a proof mass. When the AC magnetic field is applied at the bending resonance for the bimorph, the measured N ≈ 700 pT/√Hz. We discuss models based on magneto-electro-mechanical coupling at low frequency and bending resonance in the sensors and theoretical estimates of ME voltage coefficients are in very good agreement with the data. PMID:26907290

  6. Progressive Transformation between Two Magnetic Ground States for One Crystal Structure of a Chiral Molecular Magnet.

    PubMed

    Li, Li; Nishihara, Sadafumi; Inoue, Katsuya; Kurmoo, Mohamedally

    2016-03-21

    We report the exceptional observation of two different magnetic ground states (MGS), spin glass (SG, T(B) = 7 K) and ferrimagnet (FI, T(C) = 18 K), for one crystal structure of [{Mn(II)(D/L-NH2ala)}3{Mn(III)(CN)6}]·3H2O obtained from [Mn(CN)6](3-) and D/L-aminoalanine, in contrast to one MGS for [{Mn(II)(L-NH2ala)}3{Cr(III)(CN)6}]·3H2O. They consist of three Mn(NH2ala) helical chains bridged by M(III)(CN)6 to give the framework with disordered water molecules in channels and between the M(III)(CN)6. Both MGS are characterized by a negative Weiss constant, bifurcation in ZFC-FC magnetizations, blocking of the moments, both components of the ac susceptibilities, and hysteresis. They differ in the critical temperatures, absolute magnetization for 5 Oe FC (lack of spontaneous magnetization for the SG), and the shapes of the hysteresis and coercive fields. While isotropic pressure increases both T(crit) and the magnetizations linearly and reversibly in each case, dehydration progressively transforms the FI into the SG as followed by concerted in situ magnetic measurements and single-crystal diffraction. The relative strengths of the two moderate Mn(III)-CN-Mn(II) antiferromagnetic (J1 and J2), the weak Mn(II)-OCO-Mn(II) (J3), and Dzyaloshinkii-Moriya antisymmetric (DM) interactions generate the two sets of characters. Examination of the bond lengths and angles for several crystals and their corresponding magnetic properties reveals a correlation between the distortion of Mn(III)(CN)6 and the MGS. SG is favored by higher magnetic anisotropy by less distorted Mn(III)(CN)6 in good accordance with the Mn-Cr system. This conclusion is also born out of the magnetization measurements on orientated single crystals with fields parallel and perpendicular to the unique c axis of the hexagonal space group.

  7. A series of tetraazalene radical-bridged M2 (M = CrIII, MnII, FeII, CoII) complexes with strong magnetic exchange coupling.

    PubMed

    DeGayner, Jordan A; Jeon, Ie-Rang; Harris, T David

    2015-11-13

    The ability of tetraazalene radical bridging ligands to mediate exceptionally strong magnetic exchange coupling across a range of transition metal complexes is demonstrated. The redox-active bridging ligand N , N ', N '', N '''-tetra(2-methylphenyl)-2,5-diamino-1,4-diiminobenzoquinone ( NMePh LH 2 ) was metalated to give the series of dinuclear complexes [(TPyA) 2 M 2 ( NMePh L 2- )] 2+ (TPyA = tris(2-pyridylmethyl)amine, M = Mn II , Fe II , Co II ). Variable-temperature dc magnetic susceptibility data for these complexes reveal the presence of weak superexchange interactions between metal centers, and fits to the data provide coupling constants of J = -1.64(1) and -2.16(2) cm -1 for M = Mn II and Fe II , respectively. One-electron reduction of the complexes affords the reduced analogues [(TPyA) 2 M 2 ( NMePh L 3- ˙)] + . Following a slightly different synthetic procedure, the related complex [(TPyA) 2 CrIII2( NMePh L 3- ˙)] 3+ was obtained. X-ray diffraction, cyclic voltammetry, and Mössbauer spectroscopy indicate the presence of radical NMePh L 3- ˙ bridging ligands in these complexes. Variable-temperature dc magnetic susceptibility data of the radical-bridged species reveal the presence of strong magnetic interactions between metal centers and ligand radicals, with simulations to data providing exchange constants of J = -626(7), -157(7), -307(9), and -396(16) cm -1 for M = Cr III , Mn II , Fe II , and Co II , respectively. Moreover, the strength of magnetic exchange in the radical-bridged complexes increases linearly with decreasing M-L bond distance in the oxidized analogues. Finally, ac magnetic susceptibility measurements reveal that [(TPyA) 2 Fe 2 ( NMePh L 3- ˙)] + behaves as a single-molecule magnet with a relaxation barrier of U eff = 52(1) cm -1 . These results highlight the ability of redox-active tetraazalene bridging ligands to enable dramatic enhancement of magnetic exchange coupling upon redox chemistry and provide a rare opportunity to examine

  8. Modeling of screening currents in coated conductor magnets containing up to 40000 turns

    NASA Astrophysics Data System (ADS)

    Pardo, E.

    2016-08-01

    Screening currents caused by varying magnetic fields degrade the homogeneity and stability of the magnetic fields created by REBCO coated conductor coils. They are responsible for the AC loss; which is also important for other power applications containing windings, such as transformers, motors and generators. Since real magnets contain coils exceeding 10000 turns, accurate modeling tools for this number of turns or above are necessary for magnet design. This article presents a fast numerical method to model coils with no loss of accuracy. We model a 10400-turn coil for its real number of turns and coils of up to 40000 turns with continuous approximation, which introduces negligible errors. The screening currents, the screening current induced field (SCIF) and the AC loss is analyzed in detail. The SCIF is at a maximum at the remnant state with a considerably large value. The instantaneous AC loss for an anisotropic magnetic-field dependent J c is qualitatively different than for a constant J c , although the loss per cycle is similar. Saturation of the magnetization currents at the end pancakes causes the maximum AC loss at the first ramp to increase with J c . The presented modeling tool can accurately calculate the SCIF and AC loss in practical computing times for coils with any number of turns used in real windings, enabling parameter optimization.

  9. Flux-flow critical-state susceptibility of superconductors

    NASA Astrophysics Data System (ADS)

    Chen, D.-X.; Pardo, E.; Sanchez, A.

    2005-06-01

    The field-amplitude Hm and circular frequency ω dependent ac susceptibility, χ =χ'-jχ″, of a hard superconducting cylinder with flux-flow type current-voltage characteristic is calculated. A remarkable feature of the resultant χ(Hm,ω ) is that both the maximum χ″, χm″, and dlgHm(χm″)/dlgω increase with increasing ω. This behavior is observed in actual Bi-2223/Ag tapes and YBa2Cu3O7-δ-coated conductors. Our result provides a useful tool to study the intergranular critical state in high-temperature superconductors.

  10. Phase transition temperatures and magnetic entropy change in Ni-Mn-In-B based Heusler alloys

    NASA Astrophysics Data System (ADS)

    Pathak, Arjun; Gautam, Bhoj; Dubenko, Igor; Ali, Naushad

    2008-03-01

    One of the aspects of great attention of Heusler alloys is the large value of magnetic entropy change (δSM) and their possible application as a working material in magnetocaloric effect based magnetic refrigerators. It was reported earlier that Ni50Mn34.8In15.2 has first order martensitic transition temperature TM 212K, Curie temperature of austenitic phase TC 328K and δSM value associated with TM and TC are respectively 13 and -7 J/kg K [1]. In the present study, we are reporting the effect of partial substitution of In by B in Ni50Mn34.8In15.2 by AC susceptibility, thermal expansion, and magnetization measurements. We observed that substitution of boron sharply increase TM, and significantly enhance the δSM peak value higher than 30 J/kg K at TM 296K; however the δSM value remains almost same at TC. Therefore, the Ni-Mn-In-B based Heusler alloys will be potential material for the study of room temperature magnetic refrigerator materials. Reference: [1] A. K. Pathak, M. Khan, I. Dubenko, S. Stadler, and N. Ali, Appl. Phys. Lett. 90, 262504 (2007).

  11. Study of magnetization switching in coupled magnetic nanostructured systems

    NASA Astrophysics Data System (ADS)

    Radu, Cosmin

    A study of magnetization dynamics experiments in nanostructured materials using the rf susceptibility tunnel diode oscillator (TDO) method is presented along with a extensive theoretical analysis. An original, computer controlled experimental setup that measures the change in susceptibility with the variation in external magnetic field and sample temperature was constructed. The TDO-based experiment design and construction is explained in detail, showing all the elements of originality. This experimental technique has proven reliable for characterizing samples with uncoupled magnetic structure and various magnetic anisotropies like: CrO2, FeCo/IrMn and Co/SiO2 thin films. The TDO was subsequently used to explore the magnetization switching in coupled magnetic systems, like synthetic antiferromagnet (SAF) structures. Magnetoresistive random access memory (MRAM) is an important example of devices where the use of SAF structure is essential. To support the understanding of the SAF magnetic behavior, its configuration and application are reviewed and more details are provided in an appendix. Current problems in increasing the scalability and decreasing the error rate of MRAM devices are closely connected to the switching properties of the SAF structures. Several theoretical studies that were devoted to the understanding of the concepts of SAF critical curve are reviewed. As one can notice, there was no experimental determination of SAF critical curve, due to the difficulties in characterizing a magnetic coupled structure. Depending of the coupling strength between the two ferromagnetic layers, on the SAF critical curve one distinguishes several new features, inexistent in the case of uncoupled systems. Knowing the configuration of the SAF critical curve is of great importance in order to control its switching characteristics. For the first time a method of experimentally recording the critical curve for SAF is proposed in this work. In order to overcome technological

  12. Effect of added dietary threonine on growth performance, health, immunity and gastrointestinal function of weaning pigs with differing genetic susceptibility to Escherichia coli infection and challenged with E. coli K88ac.

    PubMed

    Trevisi, P; Corrent, E; Mazzoni, M; Messori, S; Priori, D; Gherpelli, Y; Simongiovanni, A; Bosi, P

    2015-06-01

    Threonine (Thr) is important for mucin and immunoglobulin production. We studied the effect of added dietary Thr on growth performance, health, immunity and gastrointestinal function of weaning pigs with differing genetic susceptibility to E. coli K88ac (ETEC) infection and challenged with ETEC. Forty-eight 24-day-old weaned pigs were divided into two groups by their ETEC susceptibility using mucin 4 (MUC4) gene as a marker (2 MUC4(-/-) , not-susceptible, and 2 MUC4(+/+) , susceptible, pigs per litter). Within genotype, pigs were fed two different diets: 8.5 (LThr) or 9.0 (HThr) g Thr/kg. Pigs were orally challenged on day 7 after weaning and slaughtered on day 12 or 13 after weaning. Before ETEC challenge, HThr pigs ate more (p < 0.05). The diet did not affect post-challenge growth, but HThr tended to increase post-challenge feed efficiency (p = 0.087) and overall growth (p = 0.087) and feed efficiency (p = 0.055). Before challenge, HThr pigs excreted less E. coli (p < 0.05), while after challenge, diet did not affect the number of days with diarrhoea and ETEC excretion. MUC4(+/+) pigs responded to the challenge with more diarrhoea, ETEC excretion and anti-K88 IgA in blood and jejunal secretion (p < 0.001). HThr pigs had a higher increase of anti-K88 IgA values in jejunal secretion (p = 0.089) and in blood (p = 0.089, in MUC4(+/+) pigs only). Thr did not affect total IgA and IgM values, morphometry of jejunum, goblet cells count in colon, total mucin from jejunum and colon, but varied jejunal goblet cells counts (p < 0.05). In the first two post-weaning weeks, 8.5 g Thr/kg diet may be not sufficient to optimize initial feed intake, overall feed efficiency and intestinal IgA secretion and to control the gut microbiota in the first post-weaning week, irrespective of the pig genetic susceptibility to ETEC infection. Journal of Animal Physiology and Animal Nutrition © 2014 Blackwell Verlag GmbH.

  13. KLY5 Kappabridge: High sensitivity susceptibility and anisotropy meter precisely decomposing in-phase and out-of-phase components

    NASA Astrophysics Data System (ADS)

    Pokorny, Petr; Pokorny, Jiri; Chadima, Martin; Hrouda, Frantisek; Studynka, Jan; Vejlupek, Josef

    2016-04-01

    The KLY5 Kappabridge is equipped, in addition to standard measurement of in-phase magnetic susceptibility and its anisotropy, for precise and calibrated measurement of out-of-phase susceptibility and its anisotropy. The phase angle is measured in "absolute" terms, i.e. without any residual phase error. The measured value of the out-of-phase susceptibility is independent on both the magnitude of the complex susceptibility and intensity of the driving magnetic field. The precise decomposition of the complex susceptibility into the in-phase and out-of-phase components is verified through presumably zero out-of-phase susceptibility of pure gadolinium oxide. The outstanding sensitivity in measurement of weak samples is achieved by newly developed drift compensation routine in addition to the latest models of electronic devices. In rocks, soils, and environmental materials, in which it is usually due to viscous relaxation, the out-of-phase susceptibility is able to substitute the more laborious frequency-dependent susceptibility routinely used in magnetic granulometry. Another new feature is measurement of the anisotropy of out-of-phase magnetic susceptibility (opAMS), which is also performed simultaneously and automatically with standard (in-phase) AMS measurement. The opAMS enables the direct determination of the magnetic sub-fabrics of the minerals that show non-zero out-of-phase susceptibility either due to viscous relaxation (ultrafine grains of magnetite or maghemite), or due to weak-field hysteresis (titanomagnetite, hematite, pyrrhotite), or due to eddy currents (in conductive minerals). Using the 3D rotator, the instrument performs the measurement of both the AMS and opAMS by only one insertion of the specimen into the specimen holder. In addition, fully automated measurement of the field variation of the AMS and opAMS is possible. The instrument is able to measure, in conjunction with the CS-4 Furnace and CS-L Cryostat, the temperature variation of

  14. Three dimensional inversion of magnetic survey data collected over kimberlite pipes in presence of remanent magnetization

    NASA Astrophysics Data System (ADS)

    Zhao, Pengzhi

    Magnetic method is a common geophysical technique used to explore kimberlites. The analysis and interpretation of measured magnetic data provides the information of magnetic and geometric properties of potential kimberlite pipes. A crucial parameter of kimberlite magnetic interpretation is the remanent magnetization that dominates the classification of kimberlite. However, the measured magnetic data is the total field affected by the remanent magnetization and the susceptibility. The presence of remanent magnetization can pose severe challenges to the quantitative interpretation of magnetic data by skewing or laterally shifting magnetic anomalies relative to the subsurface source (Haney and Li, 2002). Therefore, identification of remanence effects and determination of remanent magnetization are important in magnetic data interpretation. This project presents a new method to determine the magnetic and geometric properties of kimberlite pipes in the presence of strong remanent magnetization. This method consists of two steps. The first step is to estimate the total magnetization and geometric properties of magnetic anomaly. The second step is to separate the remanent magnetization from the total magnetization. In the first step, a joint parametric inversion of total-field magnetic data and its analytic signal (derived from the survey data by Fourier transform method) is used. The algorithm of the joint inversion is based on the Gauss-Newton method and it is more stable and more accurate than the separate inversion method. It has been tested with synthetic data and applied to interpret the field data from the Lac de Gras, North-West Territories of Canada. The results of the synthetic examples and the field data applications show that joint inversion can recovers the total magnetization and geometric properties of magnetic anomaly with a good data fit and stable convergence. In the second step, the remanent magnetization is separated from the total magnetization by

  15. Effects of White Matter Microstructure on Phase and Susceptibility Maps

    PubMed Central

    Wharton, Samuel; Bowtell, Richard

    2015-01-01

    Purpose To investigate the effects on quantitative susceptibility mapping (QSM) and susceptibility tensor imaging (STI) of the frequency variation produced by the microstructure of white matter (WM). Methods The frequency offsets in a WM tissue sample that are not explained by the effect of bulk isotropic or anisotropic magnetic susceptibility, but rather result from the local microstructure, were characterized for the first time. QSM and STI were then applied to simulated frequency maps that were calculated using a digitized whole-brain, WM model formed from anatomical and diffusion tensor imaging data acquired from a volunteer. In this model, the magnitudes of the frequency contributions due to anisotropy and microstructure were derived from the results of the tissue experiments. Results The simulations suggest that the frequency contribution of microstructure is much larger than that due to bulk effects of anisotropic magnetic susceptibility. In QSM, the microstructure contribution introduced artificial WM heterogeneity. For the STI processing, the microstructure contribution caused the susceptibility anisotropy to be significantly overestimated. Conclusion Microstructure-related phase offsets in WM yield artifacts in the calculated susceptibility maps. If susceptibility mapping is to become a robust MRI technique, further research should be carried out to reduce the confounding effects of microstructure-related frequency contributions. Magn Reson Med 73:1258–1269, 2015. © 2014 Wiley Periodicals, Inc. PMID:24619643

  16. Magnetic and mineralogical properties of salt rocks from the Zechstein of the Northern German Basin

    NASA Astrophysics Data System (ADS)

    Heinrich, Frances C.; Schmidt, Volkmar; Schramm, Michael; Mertineit, Michael

    2017-03-01

    Magnetic properties of rocks are often studied to characterize composition and fabric of rocks. For salt rocks, the basic relationships between their magnetic properties and composition, which are necessary to interpret rock magnetic data, are not yet established. Therefore, we studied different types of natural salt rock and pure salt minerals. We measured their magnetic properties (magnetic susceptibility, isothermal remanent magnetization acquisition curves, first-order reversal curve diagrams and temperature-dependent magnetic susceptibility) and used analytical methods such as microscopy, X-ray diffraction and inductively coupled plasma atomic emission spectroscopy to understand the relationship between magnetic properties and mineralogy. Salt rocks mainly consist of the diamagnetic minerals halite, carnallite, sylvine and anhydrite with negative magnetic susceptibilities. The magnetic susceptibilities of pure synthetic NaCl and KCl single crystals, show values of -14.5 × 10-6 and -13.5 × 10-6 SI, respectively. In contrast, in natural salt rocks higher magnetic susceptibility values were measured. The magnetic susceptibility of the samples investigated in this study shows a general increase from light rock salt (maximum -10 × 10-6 SI) over carnallitite (maximum 134 × 10-6 SI) to red sylvinite (maximum 270 × 10-6 SI). Whole rock analyses suggest that increased magnetic susceptibility can be attributed to paramagnetic and ferromagnetic minerals that are contained within the insoluble residue. The magnetic susceptibility is mainly controlled by magnetite and phyllosilicates. Its measurement can therefore be used to detect subtle changes in the content of these minerals.

  17. Research and simulation of the decoupling transformation in AC motor vector control

    NASA Astrophysics Data System (ADS)

    He, Jiaojiao; Zhao, Zhongjie; Liu, Ken; Zhang, Yongping; Yao, Tuozhong

    2018-04-01

    Permanent magnet synchronous motor (PMSM) is a nonlinear, strong coupling, multivariable complex object, and transformation decoupling can solve the coupling problem of permanent magnet synchronous motor. This paper gives a permanent magnet synchronous motor (PMSM) mathematical model, introduces the permanent magnet synchronous motor vector control coordinate transformation in the process of modal matrix inductance matrix transform through the matrix related knowledge of different coordinates of diagonalization, which makes the coupling between the independent, realize the control of motor current and excitation the torque current coupling separation, and derived the coordinate transformation matrix, the thought to solve the coupling problem of AC motor. Finally, in the Matlab/Simulink environment, through the establishment and combination between the PMSM ontology, coordinate conversion module, built the simulation model of permanent magnet synchronous motor vector control, introduces the model of each part, and analyzed the simulation results.

  18. Spatial variability of soil magnetic susceptibility in an agricultural field located in Eastern Ukraine

    NASA Astrophysics Data System (ADS)

    Menshov, Oleksandr; Pereira, Paulo; Kruglov, Oleksandr

    2015-04-01

    Magnetic susceptibility (MS) have been used to characterize soil properties. It gives an indirect information about heavy metals content and degree of human impacts on soil contamination derived from atmospheric pollution (Girault et al., 2011). This method is inexpensive in relation to chemical analysis and very useful to track soil pollution, since several toxic components deposited on soil surface are rich in particulates produced by oxidation processes (Boyko et al., 2004; Morton-Bernea et al., 2009). Thus, identify the spatial distribution of MS is of major importance, since can give an indirect information of high metals content (Dankoub et al., 2012). This allows also to distinguish the pedogenic and technogenic origin magnetic signal. For example Ukraine chernozems contain fine-grained oxidized magnetite and maghemite of pedogenic origin formed by weathering of the parent material (Jeleńska et al., 2004). However, to a correct understanding of variables distribution, the identification of the most accurate interpolation method is fundamental for a better interpretation of map information (Pereira et al., 2013). The objective of this work is to study the spatial variability of soil MS in an agricultural fields located in the Tcherkascy Tishki area (50.11°N, 36.43 °E, 162 m a.s.l), Ukraine. Soil MS was measured in 77 sampling points in a north facing slope. To estimate the best interpolation method, several interpolation methods were tested, as inverse distance to a weight (IDW) with the power of 1,2,3,4 and 5, Local Polynomial (LP) with the power of 1 and 2, Global Polynomial (GP), radial basis functions - spline with tension (SPT), completely regularized spline (CRS), multiquatratic (MTQ), inverse multiquatratic (IMTQ), and thin plate spline (TPS) - and some geostatistical methods as, ordinary kriging (OK), Simple Kriging (SK) and Universal Kriging (UK), used in previous works (Pereira et al., 2014). On average, the soil MS of the studied plot had 686

  19. Noncontact technique for measuring the electrical resistivity and magnetic susceptibility of electrostatically levitated melts

    NASA Astrophysics Data System (ADS)

    Rustan, G. E.; Spyrison, N. S.; Kreyssig, A.; Prozorov, R.; Goldman, A. I.

    2012-02-01

    Over the last two decades the popularity of levitation methods for studying equilibrium and supercooled melts has increased steadily. Measurements of density, viscosity, surface tension, and atomic structure have become well established. In contrast, measurements of electrical resistivity and magnetic susceptibility of levitated melts have been very limited. To fill this void, we have combined the tunnel diode oscillator (TDO) technique with electrostatic levitation (ESL) to perform inductively coupled measurements on levitated melts. A description of the basic operating principles of the TDO and ESL will be given, as well as a description of the implementation and performance characteristics of this technique. Preliminary measurements of electrical resistivity in the solid and liquid state will be presented for samples of Zr, Si, and Ge, as well as the measurements of ferromagnetic transitions in Fe and Co based alloys.

  20. ac Modeling and impedance spectrum tests of the superconducting magnetic field coils for the Wendelstein 7-X fusion experiment.

    PubMed

    Ehmler, Hartmut; Köppen, Matthias

    2007-10-01

    The impedance spectrum test was employed for detection of short circuits within Wendelstein 7-X (W7-X) superconducting magnetic field coils. This test is based on measuring the complex impedance over several decades of frequency. The results are compared to predictions of appropriate electrical equivalent circuits of coils in different production states or during cold test. When the equivalent circuit is not too complicated the impedance can be represented by an analytic function. A more detailed analysis is performed with a network simulation code. The overall agreement of measured and calculated or simulated spectra is good. Two types of short circuits which appeared are presented and analyzed. The detection limit of the method is discussed. It is concluded that combined high-voltage ac and low-voltage impedance spectrum tests are ideal means to rule out short circuits in the W7-X coils.