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Sample records for based hot plate

  1. Automation of a guarded hot plate thermal conductivity instrument

    SciTech Connect

    Holland, L.L.

    1980-06-01

    The Thermo-Physics Corporation's GP-1800 guarded hot plate thermal conductivity instrument has been automated using a Digital Equipment Corporation PDP 11/35 minicomputer with an Industrial Control Subsystem Remote. Automation included constructing a hardware link between the instrument and the minicomputer system and designing, writing, and documenting software to perform equipment control, data acquisition, data reduction, and report generation. The software was designed and written so that non-programmers can run the thermal conductivity experiment.

  2. Parallel-Plate Acoustic Absorbers For Hot Environments

    NASA Technical Reports Server (NTRS)

    Doychak, Joseph; Parrot, Tony L.

    1995-01-01

    Stacking patterns and materials chosen to suppress noise. Acoustic liners incorporating parallel-plate absorbing elements proposed for use in suppressing broadband aerodynamic noise originating in flows of hot gases in ducts. One potential application lies in suppressing noise generated in exhaust-jet mixer/ejectors in propulsion system of proposed High-Speed Civil Transport. In addition, such absorbers useful in any situation in which high temperature limits use of such conventional resonant acoustic-liner materials as perforated face sheets bonded to honey-comb-core panels.

  3. The Influence of Non-Nociceptive Factors on Hot Plate Latency in Rats

    PubMed Central

    Gunn, Amanda; Bobeck, Erin N.; Weber, Ceri; Morgan, Michael M.

    2010-01-01

    The hot plate is a widely used test to assess nociception. The effect of non-nociceptive factors (weight, sex, activity, habituation, and repeated testing) on hot plate latency was examined. Comparison of body weight and hot plate latency revealed a small but significant inverse correlation (light rats had longer latencies). Habituating rats to the test room for 1 hr prior to testing did not decrease hot plate latency except for female rats tested on Days 2 - 4. Hot plate latency decreased with repeated daily testing, but this was not caused by a decrease in locomotor activity or learning to respond. Activity on the hot plate was consistent across all four trials, and prior exposure to a room temperature plate caused a similar decrease in latency as rats tested repeatedly on the hot plate. Despite this decrease in baseline hot plate latency, there was no difference in morphine antinociceptive potency. The present study shows that weight, habituation to the test room, and repeated testing can alter baseline hot plate latency, but these effects are small and have relatively little impact on morphine antinociception. PMID:20797920

  4. Low-Cost Magnetic Stirrer from Recycled Computer Parts with Optional Hot Plate

    ERIC Educational Resources Information Center

    Guidote, Armando M., Jr.; Pacot, Giselle Mae M.; Cabacungan, Paul M.

    2015-01-01

    Magnetic stirrers and hot plates are key components of science laboratories. However, these are not readily available in many developing countries due to their high cost. This article describes the design of a low-cost magnetic stirrer with hot plate from recycled materials. Some of the materials used are neodymium magnets and CPU fans from…

  5. Experimental comparison and validation of hot-ball method with guarded hot plate method on polyurethane foams

    NASA Astrophysics Data System (ADS)

    Hudec, Ján; Glorieux, Christ; Dieška, Peter; Kubičár, Ľudovít

    2016-07-01

    The Hot-ball method is an innovative transient method for measuring thermophysical properties. The principle is based on heating of a small ball, incorporated in measured medium, by constant heating power and simultaneous measuring of the ball's temperature response since the heating was initiated. The shape of the temperature response depends on thermophysical properties of the medium, where the sensor is placed. This method is patented by Institute of Physics, SAS, where the method and sensors based on this method are being developed. At the beginning of the development of sensors for this method we were oriented on monitoring applications, where relative precision is much more important than accuracy. Meanwhile, the quality of sensors was improved good enough to be used for a new application - absolute measuring of thermophysical parameters of low thermally conductive materials. This paper describes experimental verification and validation of measurement by hot-ball method. Thanks to cooperation with Laboratory of Soft Matter and Biophysics of Catholic University of Leuven in Belgium, established Guarded Hot Plate method was used as a reference. Details about measuring setups, description of the experiments and results of the comparison are presented.

  6. Effects of the microstructure of twin roll cast and hot rolled plates on the surface quality of presensitized plates

    NASA Astrophysics Data System (ADS)

    Zhu, Yuan-Zhi; Zhang, Ya-Feng; Zhao, Chao-Qi; Zhou, Feng

    2014-09-01

    The effect of the microstructure of plates fabricated both in the traditional process, involving casting, hot rolling and cold rolling (HR), and in the novel twin roll casting + cold rolling (TRC) process on the surface quality of presensitized (PS) plates was analyzed by optical microscopy (OM), scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy (EDXS). The formation of pores on the surface of the electrolyzed HR plate could be attributed to the presence of approximately 1-μm-sized large Al-Fe precipitates in the HR plate compared to the smaller precipitates in the TRC plate. Moreover, residual graphite lubricants used during the TRC process were entrapped on the surface of the TRC plate during the subsequent rolling process. The entrapped pollutants tended to further deteriorate the formation of pores on the surface of the TRC plate, and no residual carbon was detected on the surface of the HR plate. Furthermore, the surface quality of the TRC plate can be improved by surface cleaning before the cold rolling process, which could dramatically lower the residual graphite on the surface.

  7. Evaluation of the surface strength of glass plates shaped by hot slumping process

    NASA Astrophysics Data System (ADS)

    Proserpio, Laura; Basso, Stefano; Borsa, Francesco; Citterio, Oberto; Civitani, Marta; Ghigo, Mauro; Pareschi, Giovanni; Salmaso, Bianca; Sironi, Giorgia; Spiga, Daniele; Tagliaferri, Gianpiero; D'Este, Alberto; Dall'Igna, Roberto; Silvestri, Mirko; Parodi, Giancarlo; Martelli, Francesco; Bavdaz, Marcos; Wille, Eric

    2014-08-01

    Hot slumping technology is under development by several research groups in the world for the realization of grazing-incidence segmented mirrors for x-ray astronomy, based on thin glass plates shaped over a mold at temperatures above the transformation point. The performed thermal cycle and related operations might have effects on the strength of the glass, with consequences for the structural design of the elemental optical modules and, consequently, on the entire x-ray optic for large astronomical missions such as IXO and ATHENA. The mechanical strength of glass plates after they underwent the slumping process was tested through destructive double-ring tests in the context of a study performed by the Astronomical Observatory of Brera with the collaboration of Stazione Sperimentale del Vetro and BCV Progetti. The entire study was done on more than 200 D263 Schott borosilicate glass specimens of dimensions 100 mm×100 mm and a thickness 0.4 mm, either flat or bent at a radius of curvature of 1000 mm through the pressure-assisted hot slumping process developed by INAF-OAB. The collected experimental data have been compared with nonlinear finite element model analyses and treated with the Weibull statistic to assess the current IXO glass x-ray telescope design, in terms of survival probability, when subjected to static and acoustic loads characteristic of the launch phase. The paper describes the activities performed and presents the obtained results.

  8. A New Guarded Hot Plate Designed for Thermal-Conductivity Measurements at High Temperature

    NASA Astrophysics Data System (ADS)

    Scoarnec, V.; Hameury, J.; Hay, B.

    2015-03-01

    The Laboratoire National de Métrologie et d'Essais has developed a new guarded hot-plate apparatus operating from to in the thermal-conductivity range from to . This facility has been specifically designed for measuring medium thermal-conductivity materials at high temperature on square specimens (100 mm side), which are easier to machine than circular ones. The hot plate and cold plates are similar with a metering section independent from the guard ring. The specimens are laterally isolated by an air gap of 4 mm width and can be instrumented by temperature sensors in order to reduce effects of thermal contact resistances between the specimens and the heating plates. Measurements have been performed on certified reference materials and on "calibrated" materials. Relative deviations between thermal conductivities measured and reference values are less than 5 % in the operating range.

  9. Hot-air flat-plate solar collector-design package

    NASA Technical Reports Server (NTRS)

    1979-01-01

    Report contains design data, performance specifications, and drawings for hot-air flat-plate solar-energy collector. Evaluation consists of tests on thermal performance time constance, and incidence angle modifier test. Results are presented in table and graph form and are analyzed in detail.

  10. Evaluation of the surface strength of glass plates shaped by hot slumping process

    NASA Astrophysics Data System (ADS)

    Proserpio, L.; Crimi, G.; Ghigo, M.; Pareschi, G.; Salmaso, B.; D'Este, A.; Dall'Igna, R.; Silvestri, M.; Parodi, G.; Martelli, F.

    2013-09-01

    The Hot Slumping Technology is under development by several research groups in the world for the realization of X-ray segmented mirrors, based on thin glass plates: during the process of slumping, a glass foil is shaped over a mould at temperatures above its transformation point. The performed thermal cycle and related operations might have effects on the strength characteristics of the glass, with consequences on the structural design of the elemental optical module and consecutively on the whole X-ray telescope. No reference technical literature exists for this particular aspect since the strength of glass depends on several parameters connected to any of the manufacturing and glass history stages, such as the distribution of surface flaws or the residual internal stresses. It is therefore extremely important to test the mechanical strength of the glass plates after they underwent the slumping process. The Astronomical Observatory of Brera (INAFOAB, Merate - Italy) started a deep analysis of this aspect, with the collaboration of Stazione Sperimentale del Vetro (SSV, Murano - Italy) and BCV Progetti (Milano - Italy). The entire study has been realized on borosilicate glass D263 by Schott, largely considered for the realization of next-generation IXO-like X-ray telescope. More than 200 slumped plates of dimension 100 mm x 100 mm and thickness 0.4 mm, both flat and curved, have been produced and tested; the collected experimental data have been compared to non-linear FEM analyses and treated with Weibull statistics, giving the strength data necessary to assess the current IXO glass X-ray telescope design, in terms of survival probability, when subject to static and acoustic load characteristic of the launch phase. The paper describes the activities performed and presents the obtained results.

  11. Design and construction of a guarded hot plate apparatus operating down to liquid nitrogen temperature

    NASA Astrophysics Data System (ADS)

    Li, Manfeng; Zhang, Hua; Ju, Yonglin

    2012-07-01

    A double-sided guarded hot plate apparatus (GHP) is specifically designed, fabricated, and constructed for the measurement of thermal conductivities of insulation specimens operated down to liquid nitrogen temperature (-196 °C), at different controlled pressures from 0.005 Pa to 0.105 MPa. The specimens placed in this apparatus are 300 mm in diameter at various thicknesses ranging from 4 mm to 40 mm. The apparatus is different from traditional GHP in terms of structure, supporting and heating method. The details of the design and construction of the hot plate, the cold plates, the suspensions, the clampings, and the vacuum chamber of the system are presented. The measurement methods of the temperatures, the input power, the meter area, and the thickness of the specimens are given. The apparatus is calibrated with teflon plates as sample and the maximum deviation from the published data is about 6% for thermal conductivity. The uncertainties for the measurement are also discussed in this paper.

  12. Design and construction of a guarded hot plate apparatus operating down to liquid nitrogen temperature.

    PubMed

    Li, Manfeng; Zhang, Hua; Ju, Yonglin

    2012-07-01

    A double-sided guarded hot plate apparatus (GHP) is specifically designed, fabricated, and constructed for the measurement of thermal conductivities of insulation specimens operated down to liquid nitrogen temperature (-196 °C), at different controlled pressures from 0.005 Pa to 0.105 MPa. The specimens placed in this apparatus are 300 mm in diameter at various thicknesses ranging from 4 mm to 40 mm. The apparatus is different from traditional GHP in terms of structure, supporting and heating method. The details of the design and construction of the hot plate, the cold plates, the suspensions, the clampings, and the vacuum chamber of the system are presented. The measurement methods of the temperatures, the input power, the meter area, and the thickness of the specimens are given. The apparatus is calibrated with teflon plates as sample and the maximum deviation from the published data is about 6% for thermal conductivity. The uncertainties for the measurement are also discussed in this paper. PMID:22852723

  13. Evaluation of an advanced process control solution to detect wafer positioning issues within the hot and cold plate modules of a lithography track

    NASA Astrophysics Data System (ADS)

    Guillaume, Olivier; Bouchardy, Marc; Armellin, Louis-Pierre

    2006-03-01

    To run the various steps of the process, multiple robot arm transfers within the Hot and Cold Plate modules which directly influence the critical dimension of the production wafers were performed on the lithography track. Wafer positioning inside these modules was found to be one of the key parameters to obtain the best critical dimensional uniformity across the wafer. With the currently realized track monitoring and conventional Statistical Process Control (SPC), potential process drifts or errors within these modules can only be detected from wafers measured during the post process control of product parameters. To catch all potential non-conformal production wafers directly at the tool, minimize equipment downtime and identify the root cause of maintenance issues, the real-time control of tool and process parameters is required. This paper presents the results of the evaluation of an Advanced Process Control (APC) solution used to detect in real-time mode any wafer positioning issues within the Hot and Cold Plate modules of a lithography track based on the monitoring of the plate temperature profile during wafer processing. After an explanation of the methodology used to collect the data from the tool, an initial phase of analysis of the temperature profile of the different Hot Plate modules was carried out. The monitoring of the temperature range was identified as the key parameter for the detection of wafer positioning issues where the temperature profile depends on the number of resistive heating elements, temperature settings and process conditions of the Hot Plate. The wafer tilt was simulated to compare the temperature profile to standard process conditions and in turn determine the detection capability. For the Cold Plate module, it was necessary to know the time between the end of the hot step and the start of the following cold step in order to detect a real tilt issue.

  14. Hot Isostatic Press Manufacturing Process Development for Fabrication of RERTR Monolithic Fuel Plates

    SciTech Connect

    Crapps, Justin M.; Clarke, Kester D.; Katz, Joel D.; Alexander, David J.; Aikin, Beverly; Vargas, Victor D.; Montalvo, Joel D.; Dombrowski, David E.; Mihaila, Bogdan

    2012-06-06

    We use experimentation and finite element modeling to study a Hot Isostatic Press (HIP) manufacturing process for U-10Mo Monolithic Fuel Plates. Finite element simulations are used to identify the material properties affecting the process and improve the process geometry. Accounting for the high temperature material properties and plasticity is important to obtain qualitative agreement between model and experimental results. The model allows us to improve the process geometry and provide guidance on selection of material and finish conditions for the process strongbacks. We conclude that the HIP can must be fully filled to provide uniform normal stress across the bonding interface.

  15. Effect of nanostructure on rapid boiling of water on a hot copper plate: a molecular dynamics study

    NASA Astrophysics Data System (ADS)

    Fu, Ting; Mao, Yijin; Tang, Yong; Zhang, Yuwen; Yuan, Wei

    2016-08-01

    Molecular dynamic simulations are performed to study the effects of nanostructure on rapid boiling of water that is suddenly heated by a hot copper plate. The results show that the nanostructure has significant effects on energy transfer from solid copper plate to liquid water and phase change process from liquid water to vapor. The liquid water on the solid surface rapidly boil after contacting with an extremely hot copper plate and consequently a cluster of liquid water moves upward during phase change. The temperature of the water film when it separates from solid surface and its final temperature when the system is at equilibrium strongly depend on the size of the nanostructure. These temperatures increase with increasing size of nanostructure. Furthermore, a non-vaporized molecular layer is formed on the surface of the copper plate even continuous heat flux is passing into water domain through the plate.

  16. Experimental study of the effect of spray inclination on ultrafast cooling of a hot steel plate

    NASA Astrophysics Data System (ADS)

    Ravikumar, Satya V.; Jha, Jay M.; Mohapatra, Soumya S.; Sinha, Apurva; Pal, Surjya K.; Chakraborty, Sudipto

    2013-10-01

    The ultrafast cooling that occurs during high mass flux air-atomized spray impingement on a hot 6 mm thick stainless steel plate has been studied experimentally in terms of the nozzle inclination between 0° and 60°. The average mass flux of water used in the study accounts to 510 kg/m2 s. The coolants used in the study are pure water and surfactant water of 600 ppm concentration. The initial temperature of the plate has been maintained at 900 °C, which is the temperature of a hot strip on run-out table in steel industry. The transient surface heat flux and temperature histories have been estimated by an inverse heat solver using measured temperature input data. Heat transfer results demonstrates that optimum cooling efficiency (~2.76 MW/m2, 194 °C/s) for pure water has been achieved at 30° nozzle orientation. The inclined nozzle has not been found beneficial when surfactant water is used as the coolant.

  17. Ultra fast cooling of hot steel plate by air atomized spray with salt solution

    NASA Astrophysics Data System (ADS)

    Mohapatra, Soumya S.; Ravikumar, Satya V.; Jha, Jay M.; Singh, Akhilendra K.; Bhattacharya, Chandrima; Pal, Surjya K.; Chakraborty, Sudipto

    2014-05-01

    In the present study, the applicability of air atomized spray with the salt added water has been studied for ultra fast cooling (UFC) of a 6 mm thick AISI-304 hot steel plate. The investigation includes the effect of salt (NaCl and MgSO4) concentration and spray mass flux on the cooling rate. The initial temperature of the steel plate before the commencement of cooling is kept at 900 °C or above, which is usually observed as the "finish rolling temperature" in the hot strip mill of a steel plant. The heat transfer analysis shows that air atomized spray with the MgSO4 salt produces 1.5 times higher cooling rate than atomized spray with the pure water, whereas air atomized spray with NaCl produces only 1.2 times higher cooling rate. In transition boiling regime, the salt deposition occurs which causes enhancement in heat transfer rate by conduction. Moreover, surface tension is the governing parameter behind the vapour film instability and this length scale increases with increase in surface tension of coolant. Overall, the achieved cooling rates produced by both types of salt added air atomized spray are found to be in the UFC regime.

  18. Metamaterial perfect absorber based hot electron photodetection.

    PubMed

    Li, Wei; Valentine, Jason

    2014-06-11

    While the nonradiative decay of surface plasmons was once thought to be only a parasitic process that limits the performance of plasmonic devices, it has recently been shown that it can be harnessed in the form of hot electrons for use in photocatalysis, photovoltaics, and photodetectors. Unfortunately, the quantum efficiency of hot electron devices remains low due to poor electron injection and in some cases low optical absorption. Here, we demonstrate how metamaterial perfect absorbers can be used to achieve near-unity optical absorption using ultrathin plasmonic nanostructures with thicknesses of 15 nm, smaller than the hot electron diffusion length. By integrating the metamaterial with a silicon substrate, we experimentally demonstrate a broadband and omnidirectional hot electron photodetector with a photoresponsivity that is among the highest yet reported. We also show how the spectral bandwidth and polarization-sensitivity can be manipulated through engineering the geometry of the metamaterial unit cell. These perfect absorber photodetectors could open a pathway for enhancing hot electron based photovoltaic, sensing, and photocatalysis systems. PMID:24837991

  19. A graphene-based hot electron transistor.

    PubMed

    Vaziri, Sam; Lupina, Grzegorz; Henkel, Christoph; Smith, Anderson D; Ostling, Mikael; Dabrowski, Jarek; Lippert, Gunther; Mehr, Wolfgang; Lemme, Max C

    2013-04-10

    We experimentally demonstrate DC functionality of graphene-based hot electron transistors, which we call graphene base transistors (GBT). The fabrication scheme is potentially compatible with silicon technology and can be carried out at the wafer scale with standard silicon technology. The state of the GBTs can be switched by a potential applied to the transistor base, which is made of graphene. Transfer characteristics of the GBTs show ON/OFF current ratios exceeding 10(4). PMID:23488893

  20. Direct Evaluation of the Figure of Merit of Thermoelectric Devices by Guarded Hot Plate Method

    NASA Astrophysics Data System (ADS)

    Kwon, Su Yong; Kim, Yong-Gyoo; Lee, Sanghyun; Kim, Jong Chul

    2013-03-01

    An apparatus for the evaluation of the figure of merit (ZT) of thermoelectric devices has been developed and ZT values have been estimated for a thermoelectric device. The most challenging problem in ZT value evaluation in this apparatus was measuring the thermal conductivity of the devices precisely. We have solved the problem by introducing a primary thermal conductivity measurement technique, a guarded hot plate method, which makes it possible to obtain directly and simultaneously four physical parameters related to the ZT, namely the thermal conductivity, electrical conductivity, Seebeck coefficient, and absolute temperature. The ZT evaluation was performed by a single scan of the temperature difference between the top and bottom surfaces of the device. We also addressed the thermoelectric properties and the power generation efficiency of a commercial thermoelectric device. The evaluation uncertainty of the ZT value was assessed to secure reliability of the apparatus and was found to be 3.59%.

  1. Is the Juan Fernandez Ridge (nazca Plate) a Deep-Mantle Hot SPOT Trail?

    NASA Astrophysics Data System (ADS)

    Lara, L. E.; Selles, D.; Díaz, A.; Piña-Gauthier, M.

    2011-12-01

    The Juan Fernández Ridge on the oceanic Nazca plate is thought to be a classic hot spot trail because of the apparent westward rejuvenation of the eruptive ages. Geochronological data is still scarce to prove this is the case, and other hypothesis should be taken into account. There are a few constrains, like the ca. 9 Ma Ar-Ar age of the O'Higgins seamount (115 km from the Chile-Perú trench), published K-Ar ages of ca. 3-4 Ma in Robinson Crusoe island (580 km from the trench) and ca. 1 Ma in Alejandro Selkirk (180 km further west). New reconnaissance K-Ar ages in Robinson Crusoe yield ca. 1-3 Ma, which partially overlap with the age of Alejandro Selkirk, breaking the expected age progression given that the Nazca plate moves eastwards at ca. 6-8 cm/yr. New geological mapping also shows a sharp unconformity between the older, strongly altered sequences and more recent, post-erosional volcanic piles, where only the vent facies have disappeared. A fixed deep-mantle plume origin for Pacific hot spots has been widely debated and concurrent phenomena arose as a possible explanation for non-linear age progressions and/or long-lived volcanic activity. In fact, intraplate regional tectonics, plume displacement, and mantle heterogeneities could be the main factor of the ridge architecture or the mask for a first-order linear trend. An ongoing mapping and dating effort is aimed to understand the evolution of the Juan Fernández Ridge, testing the main hypothesis. Fondecyt grant 110966 is acknowledged for financial support.

  2. Analgesic properties of Epilobium angustifolium, evaluated by the hot plate test and the writhing test.

    PubMed

    Tita, B; Abdel-Haq, H; Vitalone, A; Mazzanti, G; Saso, L

    2001-01-01

    The analgesic properties of Epilobium angustifolium (Ea), a plant containing flavonoids with anti-inflammatory activity, have not been sufficiently studied so far. Thus, we decided to evaluate, by the classical hot plate test and the writhing test, the analgesic effect of a dry extract of Ea obtained by evaporating a commercially available mother tincture. In the former assay, the effect of Ea (380 mg/kg) was slightly lower than that of morphine (10 mg/kg s.c.). In the writhing test, which is more sensitive for non-steroidal analgesics, the effect of Ea was already significant (P < 0.05) at 95 mg/kg while at doses > or = 190 mg/kg, its activity was similar to that of lysine acetylsalicylate (300 mg/kg). The LD50 of this dry extract of Ea was 1.4+/-0.1 g/kg. Further studies are necessary for the identification of the active principles and the elucidation of their mechanism of action. PMID:11482754

  3. Computer simulations of laser hot spots and implosion symmetry kiniform phase plate experiments on Nova

    SciTech Connect

    Peterson, R. R.; Lindman, E. L.; Delamater, N. D.; Magelssen, G. R.

    2000-05-01

    LASNEX computer code simulations have been performed for radiation symmetry experiments on the Nova laser with vacuum and gas-filled hohlraum targets [R. L. Kauffman et al., Phys. Plasmas 5, 1927 (1998)]. In previous experiments with unsmoothed laser beams, the symmetry was substantially shifted by deflection of the laser beams. In these experiments, laser beams have been smoothed with Kiniform Phase Plates in an attempt to remove deflection of the beams. The experiments have shown that this smoothing significantly improves the agreement with LASNEX calculations of implosion symmetry. The images of laser produced hot spots on the inside of the hohlraum case have been found to differ from LASNEX calculations, suggesting that some beam deflection or self-focusing may still be present or that emission from interpenetrating plasmas is an important component of the images. The measured neutron yields are in good agreement with simulations for vacuum hohlraums but are far different for gas-filled hohlraums. (c) 2000 American Institute of Physics.

  4. Laser-Based Characterization of Nuclear Fuel Plates

    SciTech Connect

    James A. Smith; David L. Cottle; Barry H. Rabin

    2013-07-01

    Ensuring the integrity of fuel-clad and clad-clad bonding in nuclear fuels is important for safe reactor operation and assessment of fuel performance, yet the measurement of bond strengths in actual fuels has proved challenging. The laser shockwave technique (LST) originally developed to characterize structural adhesion in composites is being employed to characterize interface strength in a new type of plate fuel being developed at Idaho National Laboratory (INL). LST is a non-contact method that uses lasers for the generation and detection of large-amplitude acoustic waves and is well suited for application to both fresh and irradiated nuclear-fuel plates. This paper will report on initial characterization results obtained from fresh fuel plates manufactured by different processes, including hot isostatic pressing, friction stir welding, and hot rolling.

  5. Laser-based characterization of nuclear fuel plates

    SciTech Connect

    Smith, James A.; Cottle, Dave L.; Rabin, Barry H.

    2014-02-18

    Ensuring the integrity of fuel-clad and clad-clad bonding in nuclear fuels is important for safe reactor operation and assessment of fuel performance, yet the measurement of bond strengths in actual fuels has proved challenging. The laser shockwave technique (LST) originally developed to characterize structural adhesion in composites is being employed to characterize interface strength in a new type of plate fuel being developed at Idaho National Laboratory (INL). LST is a non-contact method that uses lasers for the generation and detection of large-amplitude acoustic waves and is well suited for application to both fresh and irradiated nuclear-fuel plates. This paper will report on initial characterization results obtained from fresh fuel plates manufactured by different processes, including hot isostatic pressing, friction stir welding, and hot rolling.

  6. The Study of Analgesic Effects of Leonurus cardiaca L. in Mice by Formalin, Tail Flick and Hot Plate Tests

    PubMed Central

    Rezaee-Asl, Masoume; Sabour, Mandana; Ostadhadi, Sattar; Bakhtiarian, Azam

    2014-01-01

    Leonurus cardiaca, commonly known as motherwort, is a member of the Lamiaceae family. It has a number of interesting biological activities, for example, sedative and hypotensive, antioxidant, anti-inflammatory, and antimicrobial activities. The aim of the present study was to investigate the effect of alcoholic extract of aerial part of Leonurus cardiaca on nociceptive response using formalin, tail flick, and hot plate tests in mice. The acute treatment of mice with an ethanolic extract at doses of 500 and 250 mg/kg by intraperitoneal administration produced a significant antinociceptive in the first and second phases of formalin test, respectively. The hot plate and tail flick tests showed an increase in the antinociceptive effect at dose 500 mg/kg. These results suggest that Leonurus cardiaca possesses central and peripheral antinociceptive actions. PMID:27433501

  7. Evaluation of protective ensemble thermal characteristics through sweating hot plate, sweating thermal manikin, and human tests.

    PubMed

    Kim, Jung-Hyun; Powell, Jeffery B; Roberge, Raymond J; Shepherd, Angie; Coca, Aitor

    2014-01-01

    The purpose of this study was to evaluate the predictive capability of fabric Total Heat Loss (THL) values on thermal stress that Personal Protective Equipment (PPE) ensemble wearers may encounter while performing work. A series of three tests, consisting of the Sweating Hot Plate (SHP) test on two sample fabrics and the Sweating Thermal Manikin (STM) and human performance tests on two single-layer encapsulating ensembles (fabric/ensemble A = low THL and B = high THL), was conducted to compare THL values between SHP and STM methods along with human thermophysiological responses to wearing the ensembles. In human testing, ten male subjects performed a treadmill exercise at 4.8 km and 3% incline for 60 min in two environmental conditions (mild = 22°C, 50% relative humidity (RH) and hot/humid = 35°C, 65% RH). The thermal and evaporative resistances were significantly higher on a fabric level as measured in the SHP test than on the ensemble level as measured in the STM test. Consequently the THL values were also significantly different for both fabric types (SHP vs. STM: 191.3 vs. 81.5 W/m(2) in fabric/ensemble A, and 909.3 vs. 149.9 W/m(2) in fabric/ensemble B (p < 0.001). Body temperature and heart rate response between ensembles A and B were consistently different in both environmental conditions (p < 0.001), which is attributed to significantly higher sweat evaporation in ensemble B than in A (p < 0.05), despite a greater sweat production in ensemble A (p < 0.001) in both environmental conditions. Further, elevation of microclimate temperature (p < 0.001) and humidity (p < 0.01) was significantly greater in ensemble A than in B. It was concluded that: (1) SHP test determined THL values are significantly different from the actual THL potential of the PPE ensemble tested on STM, (2) physiological benefits from wearing a more breathable PPE ensemble may not be feasible with incremental THL values (SHP test) less than approximately 150-200 W·m(2), and (3) the

  8. Evaluation of the antinociceptive activities of enaminone compounds on the formalin and hot plate tests in mice

    PubMed Central

    Masocha, Willias; Kombian, Samuel B.; Edafiogho, Ivan O.

    2016-01-01

    Recently, we found that methyl 4-(4′-bromophenyl)aminocyclohex-3-en-6-methyl-2-oxo-1-oate (E139), an anticonvulsant enaminone, has antinociceptive activity in the hot plate test. In this study we evaluated the antinociceptive activity of five anilino enaminones E139, ethyl 4-(4′-chlorophenyl)amino-6-methyl-2-oxocyclohex-3-en-1-oate (E121), ethyl 4-(4′-bromophenyl)amino-6-methyl-2-oxocyclohex-3-en-1-oate (E122), methyl 4-(4′-chlorophenyl)amino-6-methyl-2-oxocyclohex-3-en-1-oate (E138) and ethyl 4-(4′-fluorophenyl)amino-6-methyl-2-oxocyclohex-3-en-1-oate (BRG 19) using the formalin and hot plate tests. E139 has been reported to exert its effects via enhancement of extracellular GABA levels, thus tiagabine, a GABA transporter inhibitor, was evaluated as a control together with indomethacin. Tiagabine had antinociceptive activity in both phase 1 (neurogenic pain) and phase 2 (inflammatory pain) of the formalin test, whereas indomethacin had activity only in phase 2. E139 and E138 had antinociceptive activity in both phases of the formalin test, whereas E121 had activity only in phase 1 and BRG 19 had activity only in phase 2. E122 had no significant activity in either phase. In the hot plate test only E139 had antinociceptive activity. Administration of either bicuculline, a GABAA receptor antagonist, or CGP 35348, a GABAB receptor antagonist, blocked the antinociceptive activity of E139. In conclusion our results indicate that E139 has antinociceptive activity in the formalin and hot plate tests that are dependent on GABA receptors. PMID:26916642

  9. Evaluation of the antinociceptive activities of enaminone compounds on the formalin and hot plate tests in mice

    NASA Astrophysics Data System (ADS)

    Masocha, Willias; Kombian, Samuel B.; Edafiogho, Ivan O.

    2016-02-01

    Recently, we found that methyl 4-(4‧-bromophenyl)aminocyclohex-3-en-6-methyl-2-oxo-1-oate (E139), an anticonvulsant enaminone, has antinociceptive activity in the hot plate test. In this study we evaluated the antinociceptive activity of five anilino enaminones E139, ethyl 4-(4‧-chlorophenyl)amino-6-methyl-2-oxocyclohex-3-en-1-oate (E121), ethyl 4-(4‧-bromophenyl)amino-6-methyl-2-oxocyclohex-3-en-1-oate (E122), methyl 4-(4‧-chlorophenyl)amino-6-methyl-2-oxocyclohex-3-en-1-oate (E138) and ethyl 4-(4‧-fluorophenyl)amino-6-methyl-2-oxocyclohex-3-en-1-oate (BRG 19) using the formalin and hot plate tests. E139 has been reported to exert its effects via enhancement of extracellular GABA levels, thus tiagabine, a GABA transporter inhibitor, was evaluated as a control together with indomethacin. Tiagabine had antinociceptive activity in both phase 1 (neurogenic pain) and phase 2 (inflammatory pain) of the formalin test, whereas indomethacin had activity only in phase 2. E139 and E138 had antinociceptive activity in both phases of the formalin test, whereas E121 had activity only in phase 1 and BRG 19 had activity only in phase 2. E122 had no significant activity in either phase. In the hot plate test only E139 had antinociceptive activity. Administration of either bicuculline, a GABAA receptor antagonist, or CGP 35348, a GABAB receptor antagonist, blocked the antinociceptive activity of E139. In conclusion our results indicate that E139 has antinociceptive activity in the formalin and hot plate tests that are dependent on GABA receptors.

  10. 21 CFR 872.6200 - Base plate shellac.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Base plate shellac. 872.6200 Section 872.6200 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES DENTAL DEVICES Miscellaneous Devices § 872.6200 Base plate shellac. (a) Identification. Base...

  11. The transference of heat from a hot plate to an air stream

    NASA Technical Reports Server (NTRS)

    Elias, Franz

    1931-01-01

    The object of the present study was to define experimentally the field of temperature and velocity in a heated flat plate when exposed to an air stream whose direction is parallel to it, then calculate therefrom the heat transference and the friction past the flat plate, and lastly, compare the test data with the mathematical theory. To ensure comparable results, we were to actually obtain or else approximate: a) two-dimensional flow; b) constant plate temperature in the direction of the stream. To approximate the flow in two dimensions, we chose a relatively wide plate and measured the velocity and temperature in the median plane.

  12. Structural Behavior of Monolithic Fuel Plates During Hot Isostatic Pressing and Annealing

    SciTech Connect

    Pavel G. Medvedev; Hakan Ozaltun

    2010-03-01

    This paper presents results of the stress analysis in the monolithic fuel plates during thermal transients performed using COMSOL finite element analysis software. Large difference in the thermal expansion between the U-Mo foil and Al cladding is the main load origin during heating and cooling of the fuel plates. In addition, the mechanical behavior of the plate is affected by the difference in yield points between the foil and the cladding. This is manifested by the plastic deformation and permanent strains in the cladding, and elastic deformation of the foil. The results show existence of the critical temperature points at which the stresses change from compressive to tensile. The paper highlights principal differences in mechanical behavior between monolithic and dispersion fuel plates, underlines the need for mechanical property data, especially for the U-Mo alloys, and discusses the methodology for mechanical analysis of the monolithic plates.

  13. PC-based car license plate reader

    NASA Astrophysics Data System (ADS)

    Hwang, Chung-Mu; Shu, Shyh-Yeong; Chen, Wen-Yu; Chen, Yie-Wern; Wen, Kuang-Pu

    1992-11-01

    A car license plate reader (CLPR) using fuzzy inference and neural network algorithm has been developed in Industrial Technology Research Institute (ITRI) and installed in highway toll stations to identify stolen cars. It takes an average of 0.7 seconds to recognize a car license plate by using a PC with 80486-50 CPU. The recognition rate of the system is about 97%. The techniques of CLPR include vehicle sensing, image grab control, optic pre- processing, lighting, and optic character recognition (OCR). The CLPR can be used in vehicle flow statistics, the checking of stolen vehicles, automatic charging systems in parking lots or garage management, and so on.

  14. Corrections for Thermal Expansion in Thermal Conductivity Measurement of Insulations Using the High-Temperature Guarded Hot-Plate Method

    NASA Astrophysics Data System (ADS)

    Wu, Jiyu; Morrell, Roger

    2012-02-01

    The anticipation of recently published European product standards for industrial thermal insulation has driven improvements in high-temperature thermal conductivity measurements in an attempt to obtain overall measurement uncertainties better than 5 % ( k = 2). The two measurement issues that are focused on in this article are the effect of thermal expansion on in situ thickness measurement and on determining the metering area at high temperatures. When implementing in situ thickness measurements, it is vital to correct the thermal expansion of components in a high-temperature guarded hot plate (HTGHP). For example, in the NPL HTGHP this could cause 3.2 % measurement error for a 50 mm thick specimen at 800 °C. The thermal expansion data for nickel 201 measured by NPL are presented, and the effect of this on the metering area of NPL's heater plate (nickel 201) is discussed.

  15. Application of MMC model on simulation of shearing process of thick hot-rolled high strength steel plate

    SciTech Connect

    Dong, Liang; Li, Shuhui; Yang, Bing; Gao, Yongsheng

    2013-12-16

    Shear operation is widely used as the first step in sheet metal forming to cut the sheet or plate into the required size. The shear of thick hot-rolled High Strength Steel (HSS) requires large shearing force and the sheared edge quality is relatively poor because of the large thickness and high strength compared with the traditional low carbon steel. Bad sheared edge quality will easily lead to edge cracking during the post-forming process. This study investigates the shearing process of thick hot-rolled HSS plate metal, which is generally exploited as the beam of heavy trucks. The Modified Mohr-Coulomb fracture criterion (MMC) is employed in numerical simulation to calculate the initiation and propagation of cracks during the process evolution. Tensile specimens are designed to obtain various stress states in tension. Equivalent fracture strains are measured with Digital Image Correlation (DIC) equipment to constitute the fracture locus. Simulation of the tension test is carried out to check the fracture model. Then the MMC model is applied to the simulation of the shearing process, and the simulation results show that the MMC model predicts the ductile fracture successfully.

  16. Application of MMC model on simulation of shearing process of thick hot-rolled high strength steel plate

    NASA Astrophysics Data System (ADS)

    Dong, Liang; Li, Shuhui; Yang, Bing; Gao, Yongsheng

    2013-12-01

    Shear operation is widely used as the first step in sheet metal forming to cut the sheet or plate into the required size. The shear of thick hot-rolled High Strength Steel (HSS) requires large shearing force and the sheared edge quality is relatively poor because of the large thickness and high strength compared with the traditional low carbon steel. Bad sheared edge quality will easily lead to edge cracking during the post-forming process. This study investigates the shearing process of thick hot-rolled HSS plate metal, which is generally exploited as the beam of heavy trucks. The Modified Mohr-Coulomb fracture criterion (MMC) is employed in numerical simulation to calculate the initiation and propagation of cracks during the process evolution. Tensile specimens are designed to obtain various stress states in tension. Equivalent fracture strains are measured with Digital Image Correlation (DIC) equipment to constitute the fracture locus. Simulation of the tension test is carried out to check the fracture model. Then the MMC model is applied to the simulation of the shearing process, and the simulation results show that the MMC model predicts the ductile fracture successfully.

  17. Plasmonically enhanced hot electron based photovoltaic device.

    PubMed

    Atar, Fatih B; Battal, Enes; Aygun, Levent E; Daglar, Bihter; Bayindir, Mehmet; Okyay, Ali K

    2013-03-25

    Hot electron photovoltaics is emerging as a candidate for low cost and ultra thin solar cells. Plasmonic means can be utilized to significantly boost device efficiency. We separately form the tunneling metal-insulator-metal (MIM) junction for electron collection and the plasmon exciting MIM structure on top of each other, which provides high flexibility in plasmonic design and tunneling MIM design separately. We demonstrate close to one order of magnitude enhancement in the short circuit current at the resonance wavelengths. PMID:23546103

  18. Bioinspired plate-based fog collectors.

    PubMed

    Heng, Xin; Luo, Cheng

    2014-09-24

    In a recent work, we explored the feeding mechanism of a shorebird to transport liquid drops by repeatedly opening and closing its beak. In this work, we apply the corresponding results to develop a new artificial fog collector. The collector includes two nonparallel plates. It has three advantages in comparison with existing artificial collectors: (i) easy fabrication, (ii) simple design to scale up, and (iii) active transport of condensed water drops. Two collectors have been built. A small one with dimensions of 4.2 × 2.1 × 0.05 cm(3) (length × width × thickness) was first built and tested to examine (i) the time evolution of condensed drop sizes and (ii) the collection processes and efficiencies on the glass, SiO2, and SU-8 plates. Under similar experimental conditions, the amount of water collected per unit area on the small collector is about 9.0, 4.7, and 3.7 times, respectively, as much as the ones reported for beetles, grasses, and metal wires, and the total amount of water collected is around 33, 18, and 15 times. On the basis of the understanding gained from the tests on the small collector, a large collector with dimensions of 26 × 10 × 0.2 cm(3) was further built and tested, which was capable of collecting 15.8 mL of water during a period of 36 min. The amount of water collected, when it is scaled from 36 to 120 min, is about 878, 479, or 405 times more than what was collected by individual beetles, grasses, or metal wires. PMID:25192549

  19. High-pressure, high-temperature equations of state using nanofabricated controlled-geometry Ni/SiO2/Ni double hot-plate samples

    NASA Astrophysics Data System (ADS)

    Pigott, Jeffrey S.; Ditmer, Derek A.; Fischer, Rebecca A.; Reaman, Daniel M.; Hrubiak, Rostislav; Meng, Yue; Davis, Robert J.; Panero, Wendy R.

    2015-12-01

    We have fabricated novel controlled-geometry samples for the laser-heated diamond-anvil cell (LHDAC) in which a transparent oxide layer (SiO2) is sandwiched between two laser-absorbing layers (Ni) in a single, cohesive sample. The samples were mass manufactured (>104 samples) using a combination of physical vapor deposition, photolithography, and wet and plasma etching. The double hot-plate arrangement of the samples, coupled with the chemical and spatial homogeneity of the laser-absorbing layers, addresses problems of spatial temperature heterogeneities encountered in previous studies where simple mechanical mixtures of transparent and opaque materials were used. Here we report thermal equations of state (EOS) for nickel to 100 GPa and 3000 K and stishovite to 50 GPa and 2400 K obtained using the LHDAC and in situ synchrotron X-ray microdiffraction. We discuss the inner core composition and the stagnation of subducted slabs in the mantle based on our refined thermal EOS.

  20. Hot pressing of Cr{sub 2}O{sub 3} powder with thin hexagonal plate particles

    SciTech Connect

    Komeda, T.; Fukumoto, Y.; Yoshinaka, M.; Hirota, K.; Yamaguchi, O.

    1996-08-01

    Chromium oxide (Cr{sub 2}O{sub 3}) powders with thin hexagonal plate particles have been obtained at 1,200 C to 1,400 C from an amorphous material prepared by adding hydrazine monohydrate to the aqueous solution of chromium nitrate. Tablets molded by wet-uniaxial-pressing were hot-pressed for 2 h at 1,500 C and 30 MPa. The dense sintered Cr{sub 2}O{sub 3} ceramics (>98% of theoretical) obtained had crystal-orientation, in which a <001> axis was parallel to the pressing direction. They exhibited an anisotropy in electrical conductivity, s; the values measured at 700 C in the perpendicular and parallel directions for the <001> axis were 5.5 and 0.58 S-m{sup {minus}1}, respectively. Vickers hardness, HV, and fracture toughness, KIC, were 24.1 GPa and 4.6 MPa{center_dot}m{sup 1/2}, respectively.

  1. Microchannel-plate-based x-ray optics

    NASA Astrophysics Data System (ADS)

    Beijersbergen, Marco W.; Bavdaz, Markos; Peacock, Anthony J.; Tomaselli, Enrico; Fraser, G.; Brunton, A.; Flyckt, E.; Krumrey, Michael K.; Souvorov, Alexei

    1999-10-01

    X-ray optics based on micro-channel plates (MCPs) offer some distinctive advantages over conventional technologies used to produce imagin optics for astrophysics applications. Such micro-pore optics (MPOs) are far lighter and allow a larger stacking density than optics based on metallic foils or plates. Until recent, x-ray optics based on MCPs were not feasible or useful because of the limited quality of the MCPs. We have produced thick square pore MPOs of improved quality and have developed methods to stack the channels in a radial pattern, as required for imagin optics based on Wolter type I or II designs. The individual plates were tested in synchrotron radiation facilities and conventional beam lines to determine their geometric and surface scattering properties.

  2. Detection system for inclusion defects in hot-rolled steel plates using MFLT with two different magnetizing strengths

    NASA Astrophysics Data System (ADS)

    Yotsuji, Junichi; Koshihara, Takahiro

    2014-02-01

    Recently, steel can manufacturing requires higher quality because otherwise minute non-metallic inclusions in thin sheets cause cracks and result in a burst during pressurization after the pressing process. Quality testing systems have already been installed in the final process in steel plants, but if there were another inspection in an earlier step, for example, at the hot strip mill, the mass manufacture of nonconforming products could be avoided and maintaining quality control would be more efficient. In order to detect inclusion defects in hot-rolled steel plates, the authors developed a new technique for MFLT (Magnetic Flux Leakage Testing) using different magnetizing forces. According to an analysis of the noise factors in MFLT, it was found that the signals generated from the scale layer on a steel surface are dominant. A different magnetizing force method is the used to decrease this overpowering noise level in MFLT. In this paper, it was confirmed that inclusions larger than 160μm in diameter and less than 0.45mm in depth can be detected utilizing this method.

  3. MANTLE CONVECTION, PLATE TECTONICS, AND VOLCANISM ON HOT EXO-EARTHS

    SciTech Connect

    Van Summeren, Joost; Conrad, Clinton P.; Gaidos, Eric

    2011-07-20

    Recently discovered exoplanets on close-in orbits should have surface temperatures of hundreds to thousands of Kelvin. They are likely tidally locked and synchronously rotating around their parent stars and, if an atmosphere is absent, have surface temperature contrasts of many hundreds to thousands of Kelvin between permanent day and night sides. We investigated the effect of elevated surface temperature and strong surface temperature contrasts for Earth-mass planets on the (1) pattern of mantle convection, (2) tectonic regime, and (3) rate and distribution of partial melting, using numerical simulations of mantle convection with a composite viscous/pseudo-plastic rheology. Our simulations indicate that if a close-in rocky exoplanet lacks an atmosphere to redistribute heat, a {approx}>400 K surface temperature contrast can maintain an asymmetric degree 1 pattern of mantle convection in which the surface of the planet moves preferentially toward subduction zones on the cold night side. The planetary surface features a hemispheric dichotomy, with plate-like tectonics on the night side and a continuously evolving mobile lid on the day side with diffuse surface deformation and vigorous volcanism. If volcanic outgassing establishes an atmosphere and redistributes heat, plate tectonics is globally replaced by diffuse surface deformation and volcanism accelerates and becomes distributed more uniformly across the planetary surface.

  4. Aperture-based antihydrogen gravity experiment: Parallel plate geometry

    SciTech Connect

    Rocha, J. R.; Hedlof, R. M.; Ordonez, C. A.

    2013-10-15

    An analytical model and a Monte Carlo simulation are presented of an experiment that could be used to determine the direction of the acceleration of antihydrogen due to gravity. The experiment would rely on methods developed by existing antihydrogen research collaborations. The configuration consists of two circular, parallel plates that have an axis of symmetry directed away from the center of the earth. The plates are separated by a small vertical distance, and include one or more pairs of circular barriers that protrude from the upper and lower plates, thereby forming an aperture between the plates. Antihydrogen annihilations that occur just beyond each barrier, within a “shadow” region, are asymmetric on the upper plate relative to the lower plate. The probability for such annihilations is determined for a point, line and spheroidal source of antihydrogen. The production of 100,000 antiatoms is predicted to be necessary for the aperture-based experiment to indicate the direction of free fall acceleration of antimatter, provided that antihydrogen is produced within a sufficiently small antiproton plasma at a temperature of 4 K.

  5. Grid base plate for an electrode plate for a storage battery and method of manufacture thereof

    SciTech Connect

    Sano, I.; Suzuki, Y.

    1981-06-02

    A grid base plate and its method of manufacture is described. The method is comprised of intermittently conveying a thin elongated metallic sheet longitudinally in one direction through successive first, second and third stations, the sheet being stopped in each of the stations between successive conveying steps. In the first station , the sheet is bent to form a peripheral upwardly projecting portion in a frame region surrounding an inner grid region. In the second station, a plurality of openings are punched in the grid region and in the third station, the sheet is punched along an outer peripheral edge surface to separate the base plate from the sheet. The upwardly projecting portion forms a space with the grid region which is filled with an active material of a thickness determined by the height of the upwardly projecting portion. The upwardly projecting portion has an outer bend region with an end surface constituting a peripheral edge of the frame which faces laterally outwards and is disposed vertically. The outer bend region has a lower surface disposed in the same horizontal plane as a lower surface of an inner region in the vicinity of the juncture of the projecting portion and the grid region. Thereby, when the base plate is placed on a horizontal planar surface, the peripheral frame region will rest on the horizontal surface along two lines of contact respectively at the bottom of the edge surface and at the lower surface at the juncture of the frame region and the grid region.

  6. Embrittlement of surface mount solder joints by hot solder-dipped, gold-plated leads

    SciTech Connect

    Vianco, P.T.

    1993-07-01

    The detachment of beam-leaded transistors from several surface mount circuit boards following modest thermal cycling was examined. Microstructural analysis of the package leads and bonding pads from the failed units indicated that gold embrittlement was responsible for a loss of solder joint mechanical integrity that caused detachment of transistors from the circuit boards. An analysis of the hot dipping process used to remove gold from the leads prior to assembly demonstrated that the gold, although dissolved from the lead, remained in the nearby solder and was subsequently retained in the coating formed on the lead upon withdrawal from the bath. This scenario allowed gold to enter the circuit board solder joints. It was hypothesized, and later confirmed by experimental trials, that increasing the number of dips prevented gold from entering the solder coatings.

  7. Hierarchic plate and shell models based on p-extension

    NASA Technical Reports Server (NTRS)

    Szabo, Barna A.; Sahrmann, Glenn J.

    1988-01-01

    Formulations of finite element models for beams, arches, plates and shells based on the principle of virtual work was studied. The focus is on computer implementation of hierarchic sequences of finite element models suitable for numerical solution of a large variety of practical problems which may concurrently contain thin and thick plates and shells, stiffeners, and regions where three dimensional representation is required. The approximate solutions corresponding to the hierarchic sequence of models converge to the exact solution of the fully three dimensional model. The stopping criterion is based on: (1) estimation of the relative error in energy norm; (2) equilibrium tests, and (3) observation of the convergence of quantities of interest.

  8. Microtiter plate-based antibody microarrays for bacteria and toxins

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Research has focused on the development of rapid biosensor-based, high-throughput, and multiplexed detection of pathogenic bacteria in foods. Specifically, antibody microarrays in 96-well microtiter plates have been generated for the purpose of selective detection of Shiga toxin-producing E. coli (...

  9. Gasoline identifier based on SH0 plate acoustic waves.

    PubMed

    Kuznetsova, Iren E; Zaitsev, Boris D; Seleznev, Eugenii P; Verona, Enrico

    2016-08-01

    The present paper is devoted to the development of gasoline identifier based on zero order shear-horizontal (SH0) acoustic wave propagating in piezoelectric plate. It has been found that the permittivity of gasoline is increased when its octane number rises. The development of such identifier is experimentally demonstrated to be possible. PMID:27125559

  10. Juan Fernández Ridge (Nazca Plate): petrology and thermochronology of a rejuvenated hot spot trail

    NASA Astrophysics Data System (ADS)

    Reyes, J.; Lara, L. E.

    2012-04-01

    The Juan Fernández Ridge on the oceanic Nazca plate is thought to be a classic hot spot trail because of the apparent westward rejuvenation of the eruptive ages. However, geochronological data is still scarce and there are a few constrains to support this hypothesis like the ca. 9 Ma Ar-Ar age of the O'Higgins seamount (115 km from the Chile-Perú trench), some published K-Ar ages of ca. 3-4 Ma in Robinson Crusoe island (580 km from the trench) and ca. 1 Ma in Alejandro Selkirk (180 km further west). New reconnaissance K-Ar ages and specially the ongoing Ar-Ar dating effort in Robinson Crusoe define a ca. 1-4 Ma time span, which partially overlap with the age of Alejandro Selkirk, breaking the expected age progression given that the Nazca plate moves eastwards at ca. 6-8 cm/yr. In addition, new geological mapping shows a sharp unconformity between the older (ca. 4 Ma), strongly altered sequences and the more recent (ca. 1 Ma), post-erosional volcanic piles, where the proximal facies are still preserved. Petrological evidence also supports this evolution pattern. In fact, the partially altered older sequence is tholeiitic (Ba/Yb=12.70; La/Yb=8.12; Ba/Y=6.51; Ba/Zr=0.89). The shield stage (ca. 1-3 Ma) is transicional from tholeiitic to alkaline (Ba/Yb=18.07-8.32; La/Yb=4.59-9.84; Ba/Y=4.24-8.18; Ba/Zr=0.73-1.09) and the younger (ca. 1 Ma) is mostly alkaline (Ba/Yb=38.15; La/Yb=15.66; Ba/Y=20.27; Ba/Zr=2.31). A fixed deep-mantle plume origin for Pacific hot spots has been widely debated and concurrent phenomena arose as a possible explanation for non-linear age progressions and/or long-lived volcanic activity. In fact, intraplate regional tectonics, plume displacement, and mantle heterogeneities could be the main factor of the ridge architecture or the mask for a first-order linear trend. An ongoing mapping and dating effort is aimed to understand the evolution of the Juan Fernández Ridge, testing the main hypothesis. This research is supported by FONDECYT Project

  11. A titer plate-based polymer microfluidic platform for high throughput nucleic acid purification.

    PubMed

    Park, D S-W; Hupert, M L; Witek, M A; You, B H; Datta, P; Guy, J; Lee, J-B; Soper, S A; Nikitopoulos, D E; Murphy, M C

    2008-02-01

    A 96-well solid-phase reversible immobilization (SPRI) reactor plate was designed to demonstrate functional titer plate-based microfluidic platforms. Nickel, large area mold inserts were fabricated using an SU-8 based, UV-LIGA technique on 150 mm diameter silicon substrates. Prior to UV exposure, the prebaked SU-8 resist was flycut to reduce the total thickness variation to less than 5 mum. Excellent UV lithography results, with highly vertical sidewalls, were obtained in the SU-8 by using an UV filter to remove high absorbance wavelengths below 350 nm. Overplating of nickel in the SU-8 patterns produced high quality, high precision, metal mold inserts, which were used to replicate titer plate-based SPRI reactors using hot embossing of polycarbonate (PC). Optimized molding conditions yielded good feature replication fidelity and feature location integrity over the entire surface area. Thermal fusion bonding of the molded PC chips at 150 degrees C resulted in leak-free sealing, which was verified in leakage tests using a fluorescent dye. The assembled SPRI reactor was used for simple, fast purification of genomic DNA from whole cell lysates of several bacterial species, which was verified by PCR amplification of the purified genomic DNA. PMID:17659445

  12. Development of a System to Measure Recrystallization Ratio of Plate Steel Using Laser-Based Ultrasonics

    SciTech Connect

    Nagata, Y.; Yamada, H.; Hamada, N.; Lim, C. S.; Yi, J. K.; Hong, S. T.; Choi, S. G.; Oh, K. J.

    2007-03-21

    In this study, a material property measurement system of plate steel using laser-based ultrasonics has been developed. The system consists of pulsed Nd:YAG laser for ultrasonic generation, CW single frequency laser and Fabry-Perot interferometer for ultrasonic detection. The system generates and detects shear waves and precisely calculates anisotropy parameter values of shear wave velocities of test samples. At first, the relationship between anisotropy parameter and recrystallization ratio was investigated in the laboratory experiments. Quenching the test samples just after the ultrasonic measurement, recrystallization ratio values were measured by the conventional microscopic method. According to the experimental results, the anisotropy parameter values showed a good correlation with actual recrystallization ratio values. To evaluate the applicability of the system to real steel production line, the system was installed in hot rolling pilot plant of plate steel. As the results, it was demonstrated that the system could measure the recrystallization ratio using the anisotropy parameter values of shear wave velocities, even in the environment of hot rolling pilot plant.

  13. Development of a System to Measure Austenite Grain Size of Plate Steel Using Laser-Based Ultrasonics

    SciTech Connect

    Lim, C. S.; Hong, S. T.; Yi, J. K.; Choi, S. G.; Oh, K. J.; Nagata, Y.; Yamada, H.; Hamada, N.

    2007-03-21

    A measurement system for austenite grain size of plate steel using laser-based ultrasonics has been developed. At first, the relationship between the ultrasonic attenuation coefficients using longitudinal waves and austenite grain size of samples was investigated in the laboratory experiments. According to the experimental results, the ultrasonic attenuation coefficients showed a good correlation with actual austenite grain sizes. For the next step, the system was installed in a hot rolling pilot plant of plate steel, and it was verified that the austenite grain size could be measured even in the environment of a hot rolling pilot plant. In the experiments, it was also confirmed that the fiber delivery system could deliver Nd:YAG laser beam of 810 mJ/pulse and ultrasonic signals could be obtained successfully.

  14. Plate-Based Fuel Processing System Final Report

    SciTech Connect

    Carlos Faz; Helen Liu; Jacques Nicole; David Yee

    2005-12-22

    took the initial steam reforming plate-reactor concept and advanced it towards an integrated fuel processing system. A substantial amount of modeling was performed to guide the catalyst development and prototype hardware design and fabrication efforts. The plate-reactor mechanical design was studied in detail to establish design guidelines which would help the plate reactor survive the stresses of repeated thermal cycles (from start-ups and shut-downs). Integrated system performance modeling was performed to predict system efficiencies and determine the parameters with the most significant impact on efficiency. In conjunction with the modeling effort, a significant effort was directed towards catalyst development. CESI developed a highly active, sulfur tolerant, coke resistant, precious metal based reforming catalyst. CESI also developed its own non-precious metal based water-gas shift catalyst and demonstrated the catalysts durability over several thousands of hours of testing. CESI also developed a unique preferential oxidation catalyst capable of reducing 1% CO to < 10 ppm CO over a 35 C operating window through a single pass plate-based reactor. Finally, CESI combined the modeling results and steam reforming catalyst development efforts into prototype hardware. The first generation 3kW(e) prototype was fabricated from existing heat-exchanger plates to expedite the fabrication process. This prototype demonstrated steady state operation ranging from 5 to 100% load conditions. The prototype also demonstrated a 20:1 turndown ratio, 10:1 load transient operation and rapid start-up capability.

  15. Cancer incidence among population utilizing geothermal hot water: a census-based cohort study.

    PubMed

    Kristbjornsdottir, Adalbjorg; Rafnsson, Vilhjalmur

    2013-12-15

    The aim of the study was to assess whether utilization of geothermal hot-water is associated with risk of cancer. The cohort from census was followed from 1981 to 2010 in nation-wide death and cancer registries. The moving apart of American-Eurasian tectonic plates, observed in Iceland, results in high volcanic activity. The definition of the study populations was based on geological information. The target population was inhabitants of communities located on bedrock younger than 3.3 million years, utilizing hot-water supply generated from geothermal wells since 1972. The two reference populations were inhabitants of communities without this hot-water supply located on areas with less volcanic/geothermal activity, and bedrock older than 3.3 million years. Hazard ratio (HR), and 95% confidence intervals (CI) were adjusted for age, gender, education, housing, reproductive factors and smoking. HR in the geothermal hot-water supply areas for all cancer was 1.15 (95% CI 1.05-1.25) as compared with nongeothermal areas. The HR for breast cancer was 1.40 (1.12-1.75), prostate cancer 1.61 (1.29-2.00), kidney cancer 1.64 (1.11-2.41), lymphatic and haematopoietic tissue cancers 1.45 (1.08-1.95), and for basal cell carcinoma (BCC) of the skin 1.46 (1.16-1.82). Positive exposure-response relations were observed between the risk of these cancers and the degree of volcanic/geothermal activity in the reference areas. Increased incidence of all cancers, breast, prostate, kidney cancer and BCC of the skin was found among the population utilizing geothermal hot-water for decades. More precise information on exposure is needed in future studies. PMID:23733434

  16. Fabrication of tunable plasmonic substrates using a table-top gold coater and a hot plate, their optical characterization, and surface enhanced Raman activity

    NASA Astrophysics Data System (ADS)

    Arora, A.; Krishnan, A.

    2015-10-01

    We present a simple scalable technique for repeatable fabrication of large area (cm2) electromagnetic hot spots using tunable Localized Surface Plasmon Resonance (LSPR) substrates and their k-space microscopic imaging characterization. The substrates were fabricated simply using a low vacuum air plasma scanning electron microscope gold coater and annealing using a hot plate. The measured permittivity profile and optical transmission characteristics of such substrates showed large changes before and after annealing, with clear changes in the occurrence and position of the LSPR in the visible spectrum. Furthermore, the LSPR wavelength of these substrates was tuned from 537 nm to 630 nm using cyclic deposition and annealing. It was observed that every anneal step could be used to blue shift the resonance, while a deposition step could be used to red shift the resonance, thus giving rise to a wide tunability. We also present the k-space images of the substrates using narrowband fluorescence leakage radiation microscopy and broadband polarization microscopy. The enhanced scattering in these substrates was clearly imaged in the k-space, and the color content in the broadband k-space images correlates well with the spectral characteristics of these substrates that can be used in commercial quality testing without a spectrometer. The optical characteristics of the substrates were attributed to the morphology evolution verified using scanning probe microscopy. A single particle model based simulation was used to evaluate the optical response. The substrates were then tested for surface enhanced Raman spectroscopy (SERS) activity using control experiments involving Rhodamine 6G dye in PMMA matrix of different concentrations with analyte volumes of approximately 200 pl and analytical enhancements of >3 ×104 (net enhancement >1.8 ×107 ) were obtained. The limit of detection was ≈ 10-8 M in low volume (≈200 pl) analyte, reaching the regime of few molecule detection. To

  17. Hot spot management through design based metrology: measurement and filtering

    NASA Astrophysics Data System (ADS)

    Lee, Taehyeong; Yang, Hyunjo; Kim, Jungchan; Jung, Areum; Yoo, Gyun; Yim, Donggyu; Park, Sungki; Ishikawa, Akio; Yamamoto, Masahiro; Vikram, Abhishek

    2009-12-01

    Recently several Design Based Metrologies (DBMs) are introduced and being in use for wafer verification. The major applications of DBM are OPC accuracy improvement, DFM feed-back through Process Window Qualification (PWQ) and advanced process control. In general, however, the amount of output data from DBM is normally so large that it is very hard to handle the data for valuable feed-back. In case of PWQ, more than thousands of hot spots are detected on a single chip at the edge of process window. So, it takes much time and labor to review and analyze all the hot spots detected at PWQ. Design-related systematic defects, however, will be found repeatedly and if they can be classified into groups, it would be possible to save a lot of time for the analysis. We have demonstrated an EDA tool which can handle the large amount of output data from DBM by classifying pattern defects into groups. It can classify millions of patterns into less than thousands of pattern groups. It has been evaluated on the analysis of PWQ of metal layer in NAND Flash memory device and random contact hole patterns in a DRAM device. Also, verification was tuned to specific needs of the designer as well as defect analysis engineers by use of EDA tool's 'Pattern Matching Function'. The verification result was well within the required specification of the designer as well as the analysis engineer. The procedures of Hot Spot Management through Design Based Metrology are presented in detail.

  18. Fabrication of a Guarded-Hot-Plate Apparatus for Use over an Extended Temperature Expansion Symposium in St. Andrews-by-the-Sea, New Brunswick, Canada 6/26-29/2005

    SciTech Connect

    R.R. Zarr, D.R. Flynn, J. W. Hettenhouser

    2005-07-01

    NIST has initial a program to design and fabricate a 500 mm diameter guarded-hot-plate apparatus for the eventual development of thermal insulation reference materials for greater temperature and pressure ranges than are currently available.

  19. Irradiation Performance of U-Mo Alloy Based ‘Monolithic’ Plate-Type Fuel – Design Selection

    SciTech Connect

    A. B. Robinson; G. S. Chang; D. D. Keiser, Jr.; D. M. Wachs; D. L. Porter

    2009-08-01

    A down-selection process has been applied to the U-Mo fuel alloy based monolithic plate fuel design, supported by irradiation testing of small fuel plates containing various design parameters. The irradiation testing provided data on fuel performance issues such as swelling, fuel-cladding interaction (interdiffusion), blister formation at elevated temperatures, and fuel/cladding bond quality and effectiveness. U-10Mo (wt%) was selected as the fuel alloy of choice, accepting a somewhat lower uranium density for the benefits of phase stability. U-7Mo could be used, with a barrier, where the trade-off for uranium density is critical to nuclear performance. A zirconium foil barrier between fuel and cladding was chosen to provide a predictable, well-bonded, fuel-cladding interface, allowing little or no fuel-cladding interaction. The fuel plate testing conducted to inform this selection was based on the use of U-10Mo foils fabricated by hot co-rolling with a Zr foil. The foils were subsequently bonded to Al-6061 cladding by hot isostatic pressing or friction stir bonding.

  20. Acoustic Plate Mode sensing in liquids based on free and electrically shorted plate surfaces.

    PubMed

    Anisimkin, V I; Caliendo, C; Verona, E

    2016-05-01

    The sensing behavior to liquids for Acoustic Plate Modes (APMs) propagating along 64°Y, 90°X LiNbO3 plate was investigated vs. two electric boundary conditions. The changes in the APMs phase velocity and attenuation were measured upon exposure to different liquids wetting one of the surfaces of the plate, either free or electrically shorted by a thin conductive Al layer. The experimental data confirm that the presence of a metallic layer covering one of the plate surfaces affects the viscosity and temperature sensitivity of the device. The differences between the sensor response for various liquids, with free or metalized faces, are interpreted in terms of the APM polarization. PMID:26901669

  1. Hot corrosion of S-57, 1 cobalt-base alloy

    NASA Technical Reports Server (NTRS)

    Santoro, G. J.

    1977-01-01

    A cobalt base alloy, S-57, was hot corrosion tested in Mach 0.3 burner rig combustion gases at maximum alloy temperatures of 900 and 1000 C. Various salt concentrations were injected into the burner: 0.5, 2, 5, and 10 ppm synthetic sea salt and 4 ppm sodium sulfate (Na2SO4). S-57 underwent accelerated corrosion only under the most severe test conditions, for example, 4 ppm Na2SO4 at 900 C. The process of the accelerated corrosion was primarily sulfidation.

  2. Hot blast stove process model and model-based controller

    SciTech Connect

    Muske, K.R.; Howse, J.W.; Hansen, G.A.; Cagliostro, D.J.; Chaubal, P.C.

    1998-12-31

    This paper describes the process model and model-based control techniques implemented on the hot blast stoves for the No. 7 Blast Furnace at the Inland Steel facility in East Chicago, Indiana. A detailed heat transfer model of the stoves is developed and verified using plant data. This model is used as part of a predictive control scheme to determine the minimum amount of fuel necessary to achieve the blast air requirements. The model is also used to predict maximum and minimum temperature constraint violations within the stove so that the controller can take corrective actions while still achieving the required stove performance.

  3. The ERESE Project: Modeling Inquiry-Based Plate Tectonic Lessons

    NASA Astrophysics Data System (ADS)

    Symons, C. M.; Helly, M.; Helly, J.; Miller, S. P.; Staudigel, H.; Koppers, A.

    2004-12-01

    The Enduring Resources for Earth Science Education (ERESE) project is a collaborative effort between earth scientists, educators, librarians and data archive managers. Its goal is to develop and maintain a persistent online research and education archive in a digital library environment that supports earth science education in plate tectonics. A key to the library's effectiveness as an educational tool is the efficiency with which educators can access, use and contribute to the library. We have created a master template that educators use to develop inquiry-based curriculum. The central components of the master template include a teacher log, a student log and resource matrices. The teacher's log is divided into stages that reflect our approach to inquiry. This approach was used during a workshop as scientists worked with the teachers to model a reasonable pedagogical analog to scientific inquiry. The student log is similar in structure to a scientific method lab report. There are currently 17 resource matrices that directly access canonical education objects in the digital library, 3 of which relate to expedition planning and 14 to plate tectonics. The structure of the resource matrices allows teachers and students to traverse manageable packets of information relating to a specific topic by expert level (rows) and information type (columns). Teachers download and customize the master template using any web composer and are then invited to upload their lessons through a simple interface at Earthref.org. Once uploaded the lessons become part of the ERESE digital library collection. The upload process allows teachers to define keywords and metadata to allow useful searches by topic, concept or educational standard. The use of a single master template for inquiry lesson design means library contributions will share a common format as well as exploit identical plate tectonic resources.

  4. Individual based simulations of bacterial growth on agar plates

    NASA Astrophysics Data System (ADS)

    Ginovart, M.; López, D.; Valls, J.; Silbert, M.

    2002-03-01

    The individual based simulator, INDividual DIScrete SIMulations (INDISIM) has been used to study the behaviour of the growth of bacterial colonies on a finite dish. The simulations reproduce the qualitative trends of pattern formation that appear during the growth of Bacillus subtilis on an agar plate under different initial conditions of nutrient peptone concentration, the amount of agar on the plate, and the temperature. The simulations are carried out by imposing closed boundary conditions on a square lattice divided into square spatial cells. The simulator studies the temporal evolution of the bacterial population possible by setting rules of behaviour for each bacterium, such as its uptake, metabolism and reproduction, as well as rules for the medium in which the bacterial cells grow, such as concentration of nutrient particles and their diffusion. The determining factors that characterize the structure of the bacterial colony patterns in the presents simulations, are the initial concentrations of nutrient particles, that mimic the amount of peptone in the experiments, and the set of values for the microscopic diffusion parameter related, in the experiments, to the amount of the agar medium.

  5. Time Dependent Antinociceptive Effects of Morphine and Tramadol in the Hot Plate Test: Using Different Methods of Drug Administration in Female Rats

    PubMed Central

    Gholami, Morteza; Saboory, Ehsan; Mehraban, Sogol; Niakani, Afsaneh; Banihabib, Nafiseh; Azad, Mohamad-Reza; Fereidoni, Javid

    2015-01-01

    Morphine and tramadol which have analgesic effects can be administered acutely or chronically. This study tried to investigate the effect of these drugs at various times by using different methods of administration (intraperitoneal, oral, acute and chronic). Sixty adult female rats were divided into six groups. They received saline, morphine or tramadol (20 to 125 mg/Kg) daily for 15 days. A hot plate test was performed for the rats at the 1st, 8th and 15th days. After drug withdrawal, the hot plate test was repeated at the 17th, 19th, and 22nd days. There was a significant correlation between the day, drug, group, and their interaction (P<0.001). At 1st day (d1), both morphine, and tramadol caused an increase in the hot plate time comparing to the saline groups (P<0.001), while there was no correlation between drug administration methods of morphine and/or tramadol. At the 8th day (d8), morphine and tramadol led to the most powerful analgesic effect comparing to the other experimental days (P<0.001). At the 15th day (d15), their effects diminished comparing to the d8. After drug withdrawal, analgesic effect of morphine, and tramadol disappeared. It can be concluded that the analgesic effect of morphine and tramadol increases with the repeated use of them. Thereafter, it may gradually decrease and reach to a level compatible to d1. The present data also indicated that although the analgesic effect of morphine and tramadol is dose-and-time dependent, but chronic exposure to them may not lead to altered nociceptive responses later in life. PMID:25561936

  6. Sensor network based vehicle classification and license plate identification system

    SciTech Connect

    Frigo, Janette Rose; Brennan, Sean M; Rosten, Edward J; Raby, Eric Y; Kulathumani, Vinod K

    2009-01-01

    Typically, for energy efficiency and scalability purposes, sensor networks have been used in the context of environmental and traffic monitoring applications in which operations at the sensor level are not computationally intensive. But increasingly, sensor network applications require data and compute intensive sensors such video cameras and microphones. In this paper, we describe the design and implementation of two such systems: a vehicle classifier based on acoustic signals and a license plate identification system using a camera. The systems are implemented in an energy-efficient manner to the extent possible using commercially available hardware, the Mica motes and the Stargate platform. Our experience in designing these systems leads us to consider an alternate more flexible, modular, low-power mote architecture that uses a combination of FPGAs, specialized embedded processing units and sensor data acquisition systems.

  7. A corrosion resistant cerium oxide based coating on aluminum alloy 2024 prepared by brush plating

    NASA Astrophysics Data System (ADS)

    Tang, Junlei; Han, Zhongzhi; Zuo, Yu; Tang, Yuming

    2011-01-01

    Cerium oxide based coatings were prepared on AA2024 Al alloy by brush plating. The characteristic of this technology is that hydrogen peroxide, which usually causes the plating solution to be unstable, is not necessary in the plating electrolyte. The coating showed laminated structures and good adhesive strength with the substrate. X-ray diffraction and X-ray photoelectron spectroscopy analysis showed that the coatings were composed of Ce(III) and Ce(IV) oxides. The brush plated coatings on Al alloys improved corrosion resistance. The influence of plating parameters on structure and corrosion resistance of the cerium oxide based coating was studied.

  8. Stability and natural vibration analysis of laminated plates by using a mixed element based on a refined plate theory

    NASA Technical Reports Server (NTRS)

    Putcha, N. S.; Reddy, J. N.

    1986-01-01

    A mixed shear flexible finite element, with relaxed continuity, is developed for the geometrically linear and nonlinear analysis of layered anisotropic plates. The element formulation is based on a refined higher order theory which satisfies the zero transverse shear stress boundary conditions on the top and bottom faces of the plate and requires no shear correction coefficients. The mixed finite element developed herein consists of eleven degrees of freedom per node which include three displacements, two rotations and six moment resultants. The element is evaluated for its accuracy in the analysis of the stability and vibration of anisotropic rectangular plates with different lamination schemes and boundary conditions. The mixed finite element described here for the higher order theory gives very accurate results for buckling loads and natural frequencies.

  9. Laser-Based Hot-Melt Bonding of Thermosetting GFRP

    NASA Astrophysics Data System (ADS)

    Amend, P.; Pillach, B.; Frick, T.; Schmidt, M.

    In the future the use of tailored multi-material components will increase because of lightweight constructions. However for an optimal integration of different materials suitable joining techniques are necessary. This paper presents results of joining thermosetting composites to thermoplastics by means of laser-based hot-melt bonding. First the joining process of glass fiber reinforced plastics (GFRP) to thermoplastics is analyzed with regard to appropriate material selection of the thermoplastic joining partner. Then experiments are performed to join two thermosetting GFRP composites using a thermoplastic interlayer. All joined specimens are characterized by tensile shear tests whereby the influences of the used peel ply and the thermoplastic joining partner on the tensile shear strength are analyzed. Finally climate tests are performed to investigate the long-term durability of the joint connections.

  10. Plate-like iron particles based bidisperse magnetorheological fluid

    NASA Astrophysics Data System (ADS)

    Shah, Kruti; Oh, Jong-Seok; Choi, Seung-Bok; Upadhyay, R. V.

    2013-12-01

    Magnetorheological (MR) properties are experimentally investigated for bi-dispersion suspension of plate-like iron magnetic particles dispersed in carrier liquid to see the influence of small size particle on large size MR fluid. As a first step, structural, magnetic, and morphology of two different micron size magnetic particles are described in details. The three different weight fractions of MR fluid samples are then prepared, followed by measuring their magneto-viscous and visco-elastic properties. In the steady-state shear, the Bingham yield stress obtained by extrapolating the shear stress to the zero shear rate increases by augmenting the weight fraction of small micron size magnetic particles and the strength of magnetic field. In the oscillatory strain sweep test at an angular frequency of 10 rad s-1, a transition from visco-elastic solid to visco-elastic liquid is observed and a strong chain formation is proposed to explain the mechanism for transition. The storage modulus also increases with increasing weight fraction. From the frequency sweep test, the storage modulus is seen as independent of frequency, but depends on the magnetic field strength and weight fraction. The magneto-viscous sweep test indicates that both shear modulus and complex viscosity are independent with weight fraction at a high magnetic field. This experimental study reveals some very important physical parameters, rheological properties, and storage modulus of the plate-like iron particles based on MR fluid. The formation of less compact because of the anisotropy in iron particle creates weak sedimentation and good redispersibility of MR fluid. The results presented in this work are the key factors for devising how mechanical applications operated under static and dynamic conditions.

  11. Assessment of Uncertainties for the NIST 1016 mm Guarded-Hot-Plate Apparatus: Extended Analysis for Low-Density Fibrous-Glass Thermal Insulation

    PubMed Central

    Zarr, Robert R.

    2010-01-01

    An assessment of uncertainties for the National Institute of Standards and Technology (NIST) 1016 mm Guarded-Hot-Plate apparatus is presented. The uncertainties are reported in a format consistent with current NIST policy on the expression of measurement uncertainty. The report describes a procedure for determination of component uncertainties for thermal conductivity and thermal resistance for the apparatus under operation in either the double-sided or single-sided mode of operation. An extensive example for computation of uncertainties for the single-sided mode of operation is provided for a low-density fibrous-glass blanket thermal insulation. For this material, the relative expanded uncertainty for thermal resistance increases from 1 % for a thickness of 25.4 mm to 3 % for a thickness of 228.6 mm. Although these uncertainties have been developed for a particular insulation material, the procedure and, to a lesser extent, the results are applicable to other insulation materials measured at a mean temperature close to 297 K (23.9 °C, 75 °F). The analysis identifies dominant components of uncertainty and, thus, potential areas for future improvement in the measurement process. For the NIST 1016 mm Guarded-Hot-Plate apparatus, considerable improvement, especially at higher values of thermal resistance, may be realized by developing better control strategies for guarding that include better measurement techniques for the guard gap thermopile voltage and the temperature sensors. PMID:27134779

  12. RBFNN-based hole identification system in conducting plates.

    PubMed

    Simone, G; Morabito, F C

    2001-01-01

    A neural-based signal processing system that exploits radial basis function neural network (RBFNN) is proposed to solve the problem of detecting and locating circular holes in conducting plates by means of nondestructive eddy currents testing. The capabilities of basic multilayer perceptron and radial basis function (RBF) schemes are first investigated. Since the achieved performance revealed insufficient, a two-step procedure is then analyzed: in the first step, an RBFNN is used to estimate the distances between the hole's center and the eddy current magnetic sensors; a least square algorithm is then exploited in order to locate the hole starting from the previously estimated distances. The performance of the proposed system are tested on a database of simulated experiments based on the a priori knowledge of the corresponding boundary value direct problem solution, by taking advantage of the closed-form analytical expression of the solution in order to generate a wide range of possible sensor-hole configurations. Both noiseless and noisy measurements are taken into account for assessing the system robustness. The main result achieved is discussed. PMID:18249972

  13. Development Of Hot Surface Polysilicon-Based Chemical Sensor And Actuator With Integrated Catalytic Micropatterns For Gas Sensing Applications

    NASA Astrophysics Data System (ADS)

    Vereshchagina, E.; Gardeniers, J. G. E.

    2009-05-01

    Over the last twenty years, we have followed a rapid expansion in the development of chemical sensors and microreactors for detection and analysis of volatile organic compounds. However, for many of the developed gas sensors poor sensitivity and selectivity, and high-power consumption remain among one of the main drawbacks. One promising approach to increase selectivity at lower power consumption is calorimetric sensing, performed in a pulsed regime and using specific catalytic materials. In this work, we study kinetics of various catalytic oxidation reactions using micromachined hot surface polysilicon-based sensor containing sensitive and selective catalysts. The sensor acts as both thermal actuator of chemical and biochemical reactions on hot-surfaces and detector of heats (enthalpies) associated with these reactions. Using novel deposition techniques we integrated selective catalysts in an array of hot plates such that they can be thermally actuated and sensed individually. This allows selective detection and analysis of dangerous gas compounds in a mixture, specifically hydrocarbons at concentrations down to low ppm level. In this contribution we compare various techniques for the local immobilization of catalytic material on hot spots of the sensor in terms of process compatibility, mechanical stress, stability and cost.

  14. Methods for testing Zernike phase plates and a report on silicon-based phase plates with reduced charging and improved ageing characteristics

    PubMed Central

    Marko, Michael; Meng, Xing; Hsieh, Chyongere; Roussie, James; Striemer, Christopher

    2013-01-01

    Imaging with Zernike phase plates is increasingly being used in cryo-TEM tomography and cryo-EM single-particle applications. However, rapid ageing of the phase plates, together with the cost and effort in producing them, present serious obstacles to widespread adoption. We are experimenting with phase plates based on silicon chips that have thin windows; such phase plates could be mass-produced and made available at moderate cost. The windows are coated with conductive layers to reduce charging, and this considerably extends the useful life of the phase plates compared to traditional pure-carbon phase plates. However, a compromise must be reached between robustness and transmission through the phase-plate film. Details are given on testing phase-plate performance by means of imaging an amorphous thin film and evaluating the power spectra of the images. PMID:23994351

  15. CEMS using hot wet extractive method based on DOAS

    NASA Astrophysics Data System (ADS)

    Sun, Bo; Zhang, Chi; Sun, Changku

    2011-11-01

    A continuous emission monitoring system (CEMS) using hot wet extractive method based on differential optical absorption spectroscopy (DOAS) is designed. The developed system is applied to retrieving the concentration of SO2 and NOx in flue gas on-site. The flue gas is carried along a heated sample line into the sample pool at a constant temperature above the dew point. In this case, the adverse impact of water vapor on measurement accuracy is reduced greatly, and the on-line calibration is implemented. And then the flue gas is discharged from the sample pool after the measuring process is complete. The on-site applicability of the system is enhanced by using Programmable Logic Controller (PLC) to control each valve in the system during the measuring and on-line calibration process. The concentration retrieving method used in the system is based on the partial least squares (PLS) regression nonlinear method. The relationship between the known concentration and the differential absorption feature gathered by the PLS nonlinear method can be figured out after the on-line calibration process. Then the concentration measurement of SO2 and NOx can be easily implemented according to the definite relationship. The concentration retrieving method can identify the information and noise effectively, which improves the measuring accuracy of the system. SO2 with four different concentrations are measured by the system under laboratory conditions. The results proved that the full-scale error of this system is less than 2%FS.

  16. Bioavailability of starch based hot stage extrusion formulations.

    PubMed

    Henrist, D; Lefebvre, R A; Remon, J P

    1999-10-01

    The aim of the study was to develop a starch based hot stage extrusion formulation for controlled drug delivery and to evaluate its in vivo behavior. The extrusion mixture consisted of 53% corn starch as the matrix forming agent, 15% sorbitol as a plasticizer, 30% theophylline monohydrate as the model drug and 2% glyceryl monostearate as a lubricant. The extrudates were produced by means of a corotating twin screw extruder of APV Baker equipped with a twin screw powder feeder and a 3-mm cylindrical die. During extrusion 20% water (based on the wet mass) was added to the powder mixture. The extrudates were dried in an oven at 60 degrees C during 48 h, cut and filled out in hard gelatine capsules, in a way that the content of two capsules corresponded with a dose of 300 mg anhydrous theophylline. The dissolution profile of the experimental dosage form was retarded with a drug release of around 80% in 8 h. The in vivo behavior of the experimental formulation was evaluated in a randomized crossover design study (n=8) with a commercially available multiple unit sustained release product as the reference formulation. The plasma samples were analyzed by a validated HPLC-UV method with solid phase extraction for the sample preparation. It was clear that the experimental formulation exhibited sustained release behavior, but that it performed less well than the multiple unit dosage form. PMID:10502624

  17. Hot coal gas desulfurization with manganese-based sorbents

    SciTech Connect

    Lynch, D.; Hepworth, M.T.

    1993-09-01

    The focus of work being performed on Hot Coal Gas Desulfurization is primarily in the use of zinc ferrite and zinc titanate sorbents; however, prior studies at the US Steel Fundamental Research Laboratories in Monroeville, PA, by E.T. Turkdogan indicated that an alternate sorbent, manganese dioxide-containing ore in mixture with alumina (75 wt % ore + 25 wt % Al{sub 2}/O{sub 3}) may be a viable alternative to zinc-based sorbents. Manganese, for example, has a lower vapor pressure in the elemental state than zinc hence it is not as likely to undergo depletion from the sorbent surface upon loading and regeneration cycles. Also manganese oxide is less readily reduced to the elemental state than iron hence the range of reduction potentials for oxygen is somewhat greater than for zinc ferrite. In addition, thermodynamic analysis of the manganese-oxygen-sulfur system shows it to be less amenable to sulfation than zinc ferrite. Potential also exists for utilization of manganese higher temperatures than zinc ferrite or zinc titanate. This presentation gives the thermodynamic background for consideration of manganese-based sorbents as an alternative to zinc ferrite. To date the work which has been in progress for nine months is limited at this stage to thermogravimetric testing of four formulations of manganese-alumina sorbents to determine the optimum conditions of pelletization and induration to produce reactive pellets.

  18. Plasma heating and hot ion sustaining in mirror based hybrids

    SciTech Connect

    Moiseenko, V. E.; Agren, O.

    2012-06-19

    Possibilities of plasma heating and sloshing ion sustaining in mirror based hybrids are briefly reviewed. Sloshing ions, i.e. energetic ions with a velocity distribution concentrated to a certain pitch-angle, play an important role in plasma confinement and generation of fusion neutrons in mirror machines. Neutral beam injection (NBI) is first discussed as a method to generate sloshing ions. Numerical results of NBI modeling for a stellarator-mirror hybrid are analyzed. The sloshing ions could alternatively be sustained by RF heating. Fast wave heating schemes, i.e. magnetic beach, minority and second harmonic heating, are addressed and their similarities and differences are described. Characteristic features of wave propagation in mirror hybrid devices including both fundamental harmonic minority and second harmonic heating are examined. Minority heating is efficient for a wide range of minority concentration and plasma densities; it allows one to place the antenna aside from the hot ion location. A simple-design strap antenna suitable for this has good performance. However, this scenario is appropriate only for light minority ions. The second harmonic heating can be applied for the heavy ion component. Arrangements are similar for minority and second harmonic heating. The efficiency of second harmonic heating is influenced by a weaker wave damping than for minority heating. Numerical calculations show that in a hybrid reactor scaled mirror machine the deuterium sloshing ions could be heated within the minority heating scheme, while the tritium ions could be sustained by second harmonic heating.

  19. Hot coal gas desulfurization with manganese-based sorbents

    SciTech Connect

    Hepworth, M.T.; Ben-Slimane, R.

    1994-12-01

    The focus of work being performed on Hot Coal Gas Desulfurization at the Morgantown Energy Technology Center is primarily in the use of zinc ferrite and zinc titanate sorbents; however, prior studies indicated that an alternate sorbent, manganese dioxide-containing ore in mixture with alumina (75 wt % ore + 25 wt % Al{sub 2}O{sub 3}) may be a viable alternative to zinc-based sorbents. Manganese, for example, has a lower vapor pressure in the elemental state than zinc hence it is not as likely to undergo depletion from the sorbent surface upon loading and regeneration cycles. Also manganese oxide is less readily reduced to the elemental state than iron hence the range of reduction potentials for oxygen is somewhat greater than for zinc ferrite. In addition, thermodynamic analysis of the manganese-oxygen-sulfur system shows it to be less amenable to sulfation than zinc ferrite. Potential also exists for utilization of manganese at higher temperatures than zinc ferrite or zinc titanate. This annual topical report documents progress in pelletizing and testing via thermo-gravimetric analysis of individual pellet formulations of manganese ore/alumina combinations and also manganese carbonate/alumina with two binders, dextrin and bentonite.

  20. VLBI detection of crustal plate motion using DSN antennas as base stations

    NASA Astrophysics Data System (ADS)

    Morabito, D. D.; Claflin, E. S.; Steinberg, C. J.

    1980-04-01

    Crustal plate motion data are presented with respect to each of the three Deep Space Network sites, Goldstone, Madrid and Canberra, based on a plate motion model. The technique of very long baseline interferometry (VLBI) is examined and its capabilities are discussed. The estimated crustal movement predicted by the model is compared with apparent movement measured by a transportable BLBI system across a plate boundary in Southern California.

  1. Slender Compressed Plate in Component Based Finite Element Model

    NASA Astrophysics Data System (ADS)

    Kurejková, M.; Wald, F.; Kabeláč, J.; Šabatka, L.

    2015-11-01

    The paper presents an advance design model of a slender plate in the structural steel joint. Finite element methods and material models are described and design procedure for slender plates in numerical models of steel joints is proposed. The design procedure is demonstrated on examples. The results are verified with an analytical model according to European standards. A compressed beam with slender web and beam-to-column joint are studied by numerical analysis, buckling resistances are determined and results verified. The verification shows very good agreement.

  2. Validation of the DIFFAL, HPAC and HotSpot Dispersion Models Using the Full-Scale Radiological Dispersal Device (FSRDD) Field Trials Witness Plate Deposition Dataset.

    PubMed

    Purves, Murray; Parkes, David

    2016-05-01

    Three atmospheric dispersion models--DIFFAL, HPAC, and HotSpot--of differing complexities have been validated against the witness plate deposition dataset taken during the Full-Scale Radiological Dispersal Device (FSRDD) Field Trials. The small-scale nature of these trials in comparison to many other historical radiological dispersion trials provides a unique opportunity to evaluate the near-field performance of the models considered. This paper performs validation of these models using two graphical methods of comparison: deposition contour plots and hotline profile graphs. All of the models tested are assessed to perform well, especially considering that previous model developments and validations have been focused on larger-scale scenarios. Of the models, HPAC generally produced the most accurate results, especially at locations within ∼100 m of GZ. Features present within the observed data, such as hot spots, were not well modeled by any of the codes considered. Additionally, it was found that an increase in the complexity of the meteorological data input to the models did not necessarily lead to an improvement in model accuracy; this is potentially due to the small-scale nature of the trials. PMID:27023035

  3. Sound insulation and energy harvesting based on acoustic metamaterial plate

    NASA Astrophysics Data System (ADS)

    Assouar, Badreddine; Oudich, Mourad; Zhou, Xiaoming

    2015-03-01

    The emergence of artificially designed sub-wavelength acoustic materials, denoted acoustic metamaterials (AMM), has significantly broadened the range of materials responses found in nature. These engineered materials can indeed manipulate sound/vibration in surprising ways, which include vibration/sound insulation, focusing, cloaking, acoustic energy harvesting …. In this work, we report both on the analysis of the airborne sound transmission loss (STL) through a thin metamaterial plate and on the possibility of acoustic energy harvesting. We first provide a theoretical study of the airborne STL and confronted them to the structure-borne dispersion of a metamaterial plate. Second, we propose to investigate the acoustic energy harvesting capability of the plate-type AMM. We have developed semi-analytical and numerical methods to investigate the STL performances of a plate-type AMM with an airborne sound excitation having different incident angles. The AMM is made of silicone rubber stubs squarely arranged in a thin aluminum plate, and the STL is calculated at low-frequency range [100Hz to 3kHz] for an incoming incident sound pressure wave. The obtained analytical and numerical STL present a very good agreement confirming the reliability of developed approaches. A comparison between computed STL and the band structure of the considered AMM shows an excellent agreement and gives a physical understanding of the observed behavior. On another hand, the acoustic energy confinement in AMM with created defects with suitable geometry was investigated. The first results give a general view for assessing the acoustic energy harvesting performances making use of AMM.

  4. A seismic reflection image for the base of a tectonic plate.

    PubMed

    Stern, T A; Henrys, S A; Okaya, D; Louie, J N; Savage, M K; Lamb, S; Sato, H; Sutherland, R; Iwasaki, T

    2015-02-01

    Plate tectonics successfully describes the surface of Earth as a mosaic of moving lithospheric plates. But it is not clear what happens at the base of the plates, the lithosphere-asthenosphere boundary (LAB). The LAB has been well imaged with converted teleseismic waves, whose 10-40-kilometre wavelength controls the structural resolution. Here we use explosion-generated seismic waves (of about 0.5-kilometre wavelength) to form a high-resolution image for the base of an oceanic plate that is subducting beneath North Island, New Zealand. Our 80-kilometre-wide image is based on P-wave reflections and shows an approximately 15° dipping, abrupt, seismic wave-speed transition (less than 1 kilometre thick) at a depth of about 100 kilometres. The boundary is parallel to the top of the plate and seismic attributes indicate a P-wave speed decrease of at least 8 ± 3 per cent across it. A parallel reflection event approximately 10 kilometres deeper shows that the decrease in P-wave speed is confined to a channel at the base of the plate, which we interpret as a sheared zone of ponded partial melts or volatiles. This is independent, high-resolution evidence for a low-viscosity channel at the LAB that decouples plates from mantle flow beneath, and allows plate tectonics to work. PMID:25653000

  5. TYPICAL HOT WATER DRAW PATTERNS BASED ON FIELD DATA

    SciTech Connect

    Lutz, Jim; Melody, Moya

    2012-11-08

    There is significant variation in hot water use and draw patterns among households. This report describes typical hot water use patterns in single-family residences in North America. We found that daily hot water use is highly variable both among residences and within the same residence. We compared the results of our analysis of the field data to the conditions and draw patterns established in the current U.S. Department of Energy (DOE) test procedure for residential water heaters. The results show a higher number of smaller draws at lower flow rates than used in the test procedure. The data from which the draw patterns were developed were obtained from 12 separate field studies. This report describes the ways in which we managed, cleaned, and analyzed the data and the results of our data analysis. After preparing the data, we used the complete data set to analyze inlet and outlet water temperatures. Then we divided the data into three clusters reflecting house configurations that demonstrated small, medium, or large median daily hot water use. We developed the three clusters partly to reflect efforts of the ASHRAE standard project committee (SPC) 118.2 to revise the test procedure for residential water heaters to incorporate a range of draw patterns. ASHRAE SPC 118.2 has identified the need to separately evaluate at least three, and perhaps as many as five, different water heater capacities. We analyzed the daily hot water use data within each cluster in terms of volume and number of hot water draws. The daily draw patterns in each cluster were characterized using distributions for volume of draws, duration of draws, time since previous draw, and flow rates.

  6. Dual-mode operation of 2D material-base hot electron transistors

    PubMed Central

    Lan, Yann-Wen; Torres, Jr., Carlos M.; Zhu, Xiaodan; Qasem, Hussam; Adleman, James R.; Lerner, Mitchell B.; Tsai, Shin-Hung; Shi, Yumeng; Li, Lain-Jong; Yeh, Wen-Kuan; Wang, Kang L.

    2016-01-01

    Vertical hot electron transistors incorporating atomically-thin 2D materials, such as graphene or MoS2, in the base region have been proposed and demonstrated in the development of electronic and optoelectronic applications. To the best of our knowledge, all previous 2D material-base hot electron transistors only considered applying a positive collector-base potential (VCB > 0) as is necessary for the typical unipolar hot-electron transistor behavior. Here we demonstrate a novel functionality, specifically a dual-mode operation, in our 2D material-base hot electron transistors (e.g. with either graphene or MoS2 in the base region) with the application of a negative collector-base potential (VCB < 0). That is, our 2D material-base hot electron transistors can operate in either a hot-electron or a reverse-current dominating mode depending upon the particular polarity of VCB. Furthermore, these devices operate at room temperature and their current gains can be dynamically tuned by varying VCB. We anticipate our multi-functional dual-mode transistors will pave the way towards the realization of novel flexible 2D material-based high-density and low-energy hot-carrier electronic applications. PMID:27581550

  7. Dual-mode operation of 2D material-base hot electron transistors.

    PubMed

    Lan, Yann-Wen; Torres, Carlos M; Zhu, Xiaodan; Qasem, Hussam; Adleman, James R; Lerner, Mitchell B; Tsai, Shin-Hung; Shi, Yumeng; Li, Lain-Jong; Yeh, Wen-Kuan; Wang, Kang L

    2016-01-01

    Vertical hot electron transistors incorporating atomically-thin 2D materials, such as graphene or MoS2, in the base region have been proposed and demonstrated in the development of electronic and optoelectronic applications. To the best of our knowledge, all previous 2D material-base hot electron transistors only considered applying a positive collector-base potential (VCB > 0) as is necessary for the typical unipolar hot-electron transistor behavior. Here we demonstrate a novel functionality, specifically a dual-mode operation, in our 2D material-base hot electron transistors (e.g. with either graphene or MoS2 in the base region) with the application of a negative collector-base potential (VCB < 0). That is, our 2D material-base hot electron transistors can operate in either a hot-electron or a reverse-current dominating mode depending upon the particular polarity of VCB. Furthermore, these devices operate at room temperature and their current gains can be dynamically tuned by varying VCB. We anticipate our multi-functional dual-mode transistors will pave the way towards the realization of novel flexible 2D material-based high-density and low-energy hot-carrier electronic applications. PMID:27581550

  8. Physics-Based 3-D Simulation for Earthquake Generation Cycles at Plate Interfaces in Subduction Zones

    NASA Astrophysics Data System (ADS)

    Hashimoto, Chihiro; Fukuyama, Eiichi; Matsu'ura, Mitsuhiro

    2014-08-01

    The generation of interplate earthquakes can be regarded as a process of tectonic stress accumulation and release, driven by relative plate motion. We completed a physics-based simulation system for earthquake generation cycles at plate interfaces in the Japan region, where the Pacific plate is descending beneath the North American and Philippine Sea plates, and the Philippine Sea plate is descending beneath the North American and Eurasian plates. The system is composed of a quasi-static tectonic loading model and a dynamic rupture propagation model, developed on a realistic 3-D plate interface model. The driving force of the system is relative plate motion. In the quasi-static tectonic loading model, mechanical interaction at plate interfaces is rationally represented by the increase of tangential displacement discontinuity (fault slip) across them on the basis of dislocation theory for an elastic surface layer overlying Maxwell-type viscoelastic half-space. In the dynamic rupture propagation model, stress changes due to fault slip motion on non-planar plate interfaces are evaluated with the boundary integral equation method. The progress of seismic (dynamic) or aseismic (quasi-static) fault slip on plate interfaces is governed by a slip- and time-dependent fault constitutive law. As an example, we numerically simulated earthquake generation cycles at the source region of the 1968 Tokachi-oki earthquake on the North American-Pacific plate interface. From the numerical simulation, we can see that postseismic stress relaxation in the asthenosphere accelerates stress accumulation in the source region. When the stress state of the source region is close to a critical level, dynamic rupture is rapidly accelerated and develops over the whole source region. When the stress state is much lower than the critical level, the rupture is not accelerated. This means that the stress state realized by interseismic tectonic loading essentially controls the subsequent dynamic

  9. A Compact Immunoassay Platform Based on a Multicapillary Glass Plate

    PubMed Central

    Xue, Shuhua; Zeng, Hulie; Yang, Jianmin; Nakajima, Hizuru; Uchiyama, Katsumi

    2014-01-01

    A highly sensitive, rapid immunoassay performed in the multi-channels of a micro-well array consisting of a multicapillary glass plate (MCP) and a polydimethylsiloxane (PDMS) slide is described. The micro-dimensions and large surface area of the MCP permitted the diffusion distance to be decreased and the reaction efficiency to be increased. To confirm the concept of the method, human immunoglobulin A (h-IgA) was measured using both the proposed immunoassay system and the traditional 96-well plate method. The proposed method resulted in a 1/5-fold decrease of immunoassay time, and a 1/56-fold cut in reagent consumption with a 0.05 ng/mL of limit of detection (LOD) for IgA. The method was also applied to saliva samples obtained from healthy volunteers. The results correlated well to those obtained by the 96-well plate method. The method has the potential for use in disease diagnostic or on-site immunoassays. PMID:24859022

  10. The Earth's Hot Spots.

    ERIC Educational Resources Information Center

    Vink, Gregory E.; And Others

    1985-01-01

    Hot spots are isolated areas of geologic activity where volcanic eruptions, earthquakes, and upwelling currents occur far from plate boundaries. These mantle plumes are relatively stable and crustal plates drift over them. The nature and location of hot spots (with particular attention to the Hawaiian Islands and Iceland) are discussed. (DH)

  11. A feature-based approach to modeling protein-protein interaction hot spots.

    PubMed

    Cho, Kyu-il; Kim, Dongsup; Lee, Doheon

    2009-05-01

    Identifying features that effectively represent the energetic contribution of an individual interface residue to the interactions between proteins remains problematic. Here, we present several new features and show that they are more effective than conventional features. By combining the proposed features with conventional features, we develop a predictive model for interaction hot spots. Initially, 54 multifaceted features, composed of different levels of information including structure, sequence and molecular interaction information, are quantified. Then, to identify the best subset of features for predicting hot spots, feature selection is performed using a decision tree. Based on the selected features, a predictive model for hot spots is created using support vector machine (SVM) and tested on an independent test set. Our model shows better overall predictive accuracy than previous methods such as the alanine scanning methods Robetta and FOLDEF, and the knowledge-based method KFC. Subsequent analysis yields several findings about hot spots. As expected, hot spots have a larger relative surface area burial and are more hydrophobic than other residues. Unexpectedly, however, residue conservation displays a rather complicated tendency depending on the types of protein complexes, indicating that this feature is not good for identifying hot spots. Of the selected features, the weighted atomic packing density, relative surface area burial and weighted hydrophobicity are the top 3, with the weighted atomic packing density proving to be the most effective feature for predicting hot spots. Notably, we find that hot spots are closely related to pi-related interactions, especially pi . . . pi interactions. PMID:19273533

  12. Dynamic programming-based hot spot identification approach for pedestrian crashes.

    PubMed

    Medury, Aditya; Grembek, Offer

    2016-08-01

    Network screening techniques are widely used by state agencies to identify locations with high collision concentration, also referred to as hot spots. However, most of the research in this regard has focused on identifying highway segments that are of concern to automobile collisions. In comparison, pedestrian hot spot detection has typically focused on analyzing pedestrian crashes in specific locations, such as at/near intersections, mid-blocks, and/or other crossings, as opposed to long stretches of roadway. In this context, the efficiency of the some of the widely used network screening methods has not been tested. Hence, in order to address this issue, a dynamic programming-based hot spot identification approach is proposed which provides efficient hot spot definitions for pedestrian crashes. The proposed approach is compared with the sliding window method and an intersection buffer-based approach. The results reveal that the dynamic programming method generates more hot spots with a higher number of crashes, while providing small hot spot segment lengths. In comparison, the sliding window method is shown to suffer from shortcomings due to a first-come-first-serve approach vis-à-vis hot spot identification and a fixed hot spot window length assumption. PMID:27209154

  13. Plate Tectonics and Taiwan Orogeny based on TAIGER Experiments

    NASA Astrophysics Data System (ADS)

    Wu, F. T.; Kuochen, H.; McIntosh, K. D.

    2014-12-01

    Plate tectonics framework is usually complex in a collision zone, where continental lithosphere is involved. In the young Taiwan orogeny, with geologic understanding and large new geodetic and subsurface datasets now available an environment has been created for testing tectonic hypotheses regarding collision and orogeny. Against the background of the commonly accepted view of Taiwan as a southward propagating, self-similar 2-D orogen, a fully 3-D structure is envisaged. Along the whole length of the island the convergence of the Eurasian plate (EUP) the Philippine Sea plate (PSP) takes shape with different plate configurations. In northern Taiwan the convergence occurs with simultaneous collision of the oceanic PSP with continental EUP and the northward subduction of the PSP; in the south, EUP, in the guise of the South China Sea rifted Eurasian continent, subducts toward the east; in central Taiwan collision of oceanic PSP with continental EUP dominates. When relocated seismicity and focal mechanisms are superposed on subsurface P and Vp/Vs velocity images the configurations and the kinematics of the PSP and EUP collision and subduction become clear. While in northern Taiwan the subduction/collision explains well the high peaks and their dwindling (accompanied by crustal thinning) toward the north. In the south, mountains rise above the east-dipping EUP subduction zone as the Eurasian continental shelf veers toward the southwest, divergent from the trend of the Luzon Arc - calling into question the frequently cited arc-continent collision model of Taiwan orogeny. High velocity anomaly and Benioff seismicity coexist in the south. Going north toward Central Taiwan the high velocity anomaly persists for another 150 km or so, but it becomes seismically quiescent. Above the quiescent section the PSP and EUP collide to build the main part of the Central Range and its parallel neighbor the eastern Coastal Range. Key implications regarding orogeny include: 1) Significant

  14. Colorful holographic imaging reconstruction based on one thin phase plate

    NASA Astrophysics Data System (ADS)

    Zhu, Jing; Song, Qiang; Wang, Jian; Yue, Weirui; Zhang, Fang; Huang, Huijie

    2014-11-01

    One method of realizing color holographic imaging using one thin diffractive optical element (DOE) is proposed. This method can reconstruct a two-dimensional color image with one phase plate at user defined distance from DOE. For improving the resolution ratio of reproduced color images, the DOE is optimized by combining Gerchberg-Saxton algorithm and compensation algorithm. To accelerate the computational process, the Graphic Processing Unit (GPU) is used. In the end, the simulation result was analyzed to verify the validity of this method.

  15. Inverse methods-based estimation of plate coupling in a plate motion model governed by mantle flow

    NASA Astrophysics Data System (ADS)

    Ratnaswamy, V.; Stadler, G.; Gurnis, M.

    2013-12-01

    Plate motion is primarily controlled by buoyancy (slab pull) which occurs at convergent plate margins where oceanic plates undergo deformation near the seismogenic zone. Yielding within subducting plates, lateral variations in viscosity, and the strength of seismic coupling between plate margins likely have an important control on plate motion. Here, we wish to infer the inter-plate coupling for different subduction zones, and develop a method for inferring it as a PDE-constrained optimization problem, where the cost functional is the misfit in plate velocities and is constrained by the nonlinear Stokes equation. The inverse models have well resolved slabs, plates, and plate margins in addition to a power law rheology with yielding in the upper mantle. Additionally, a Newton method is used to solve the nonlinear Stokes equation with viscosity bounds. We infer plate boundary strength using an inexact Gauss-Newton method with line search for backtracking. Each inverse model is applied to two simple 2-D scenarios (each with three subduction zones), one with back-arc spreading and one without. For each case we examine the sensitivity of the inversion to the amount of surface velocity used: 1) full surface velocity data and 2) surface velocity data simplified using a single scalar average (2-D equivalent to an Euler pole) for each plate. We can recover plate boundary strength in each case, even in the presence of highly nonlinear flow with extreme variations in viscosity. Additionally, we ascribe an uncertainty in each plate's velocity and perform an uncertainty quantification (UQ) through the Hessian of the misfit in plate velocities. We find that as plate boundaries become strongly coupled, the uncertainty in the inferred plate boundary strength decreases. For very weak, uncoupled subduction zones, the uncertainty of inferred plate margin strength increases since there is little sensitivity between plate margin strength and plate velocity. This result is significant

  16. Microstructural anomalies in hot-isostatic pressed U–10wt.% Mo fuel plates with Zr diffusion barrier

    SciTech Connect

    Park, Y.; Eriksson, N.; Keiser, D. D.; Jue, J.; Rabin, B.; Moore, G.; Sohn, Y. H.

    2015-05-01

    Microstructural anomalies in the co-rolled-and-HIP'ed U–10 wt.% Mo (U10Mo) metallic fuel plate with Zr diffusion barrier assembly were examined as a function of HIP temperature (from 520 to 580 °C) and duration (45, 60, 90, 180 and 345 min) by scanning and transmission electron microscopy. The anomalies observed in this study are carbide/oxide inclusions within the U10Mo fuel alloy, and regions of limited interaction between the U10Mo alloy and Zr barrier, frequently associated with carbide/oxide inclusions. In the U10Mo alloy, the cF8, Fm3m (225) UC phase (a=4.955 Å) and cF12, Fm3m (225) UO2 phase (a=5.467 Å) were observed throughout the U10Mo alloy with an approximate volume percent of 0.5 to 1.8. The volume percent of the UC–UO2 inclusions within the U10Mo alloy did not change as functions of HIP temperature and time. These inclusion phases, located near the surface of the U10Mo alloy, were frequently observed to impede the development of interdiffusion and reaction between the U10Mo alloy and Zr diffusion barrier. The regions of limited interaction between the U10Mo and Zr barrier decreased with an increase in HIP temperature, however no noticeable trend was observed with an increase in HIP duration at constant temperature of 560 °C.

  17. Structure and hot hardness of RuAl-based alloys produced by reactive sintering using hot isostatic pressing

    NASA Astrophysics Data System (ADS)

    Povarova, K. B.; Morozov, A. E.; Padalko, A. G.; Drozdov, A. A.

    2008-04-01

    The structure and hot hardness (at temperatures up to 1100°C) of RuAl-based powder alloys with 1 3 at % Ni, Mo, Re, or Ru are studied. The alloys are produced by the reactive sintering of cold-compacted bars and subsequent threefold isostatic pressing with intermediate annealing at 1500°C performed after the first hot isostatic pressing. The samples have a residual pore content of 1 2.5 vol % and are characterized by a micrononuniform distribution of base and alloying elements. The alloys with refractory metals, such as Re, Mo, or Ru, are found to have the maximum hardness at all temperatures under study. At low temperatures, the effect is more substantial; the hardness of the Re-containing alloys exceeds that of the other alloys by a factor of 1.3 3.6. The increase in the hardness related to solid-solution alloying becomes more substantial owing to the microinhomogeneity of the sintered powder alloys and weakens because of microporosity. Recommendations that allow the uniformity of the distribution of the base and alloying elements to be increased are given.

  18. Effects of selected cooking procedures on the survival of Escherichia coli O157:H7 in inoculated steaks cooked on a hot plate or gas barbecue grill.

    PubMed

    Gill, C O; Devos, J; Youssef, M K; Yang, X

    2014-06-01

    Beef steaks (2 cm thick) were each inoculated at three sites in the central plane with Escherichia coli O157:H7 at 5.9 ± 0.3 log CFU per site. Temperatures at steak centers were monitored during cooking on a hot plate or the grill of a gas barbeque. Steaks were cooked in groups of five using the same procedures and cooking each steak to the same temperature, and surviving E. coli O157:H7 at each site was enumerated. When steaks cooked on the hot plate were turned over every 2 or 4 min during cooking to between 56 and 62°C, no E. coli O157:H7 was recovered from steaks cooked to ≥58 or 62°C, respectively. When steaks were cooked to ≤71°C and turned over once during cooking, E. coli O157:H7 was recovered from steaks in groups turned over after ≤8 min but not from steaks turned over after 10 or 12 min. E. coli O157:H7 was recovered in similar numbers from steaks that were not held or were held for 3 min after cooking when steaks were turned over once after 4 or 6 min during cooking. When steaks were cooked on the grill with the barbeque lid open and turned over every 2 or 4 min during cooking to 63 or 56°C, E. coli O157:H7 was recovered from only those steaks turned over at 4-min intervals and cooked to 56°C. E. coli O157:H7 was recovered from some steaks turned over once during cooking on the grill and held or not held after cooking to 63°C. E. coli O157:H7 was not recovered from steaks turned over after 4 min during cooking to 60°C on the grill with the barbeque lid closed or when the lid was closed after 6 min. Apparently, the microbiological safety of mechanically tenderized steaks can be assured by turning steaks over at intervals of about 2 min during cooking to ≥60°C in an open skillet or on a barbecue grill. When steaks are turned over only once during cooking to ≥60°C, microbiological safety may be assured by covering the skillet or grill with a lid during at least the final minutes of cooking. PMID:24853513

  19. Towards a laboratory-based calibration of the Swiss plate geophone bedload monitoring system

    NASA Astrophysics Data System (ADS)

    Rodrigo Wyss, Carlos; Rickenmann, Dieter; Fritschi, Bruno; Turowski, Jens Martin; Weitbrecht, Volker; Boes, Robert Michael

    2015-04-01

    The Swiss plate geophone is an indirect bedload monitoring device that is used to continuously monitor bedload transport. The Swiss plate geophone consists of a geophone sensor that measures the elastic deformation of a steel plate induced by the collision of a bedload particle. Differences between bedload particle shape and sizes as well as in-situ hydraulic conditions control the particle transport mode, and these elements have so far required a field calibration of the Swiss plate geophone. In this study, we performed flume experiments with varying bedload transport parameters like particle size and mean flow velocity with natural bedload particles from the Erlenbach stream, Central Switzerland. The impulses, i.e. the number of times the signal recorded by the Swiss plate geophone exceeds a predefined threshold, and wave packets representing a single impact are used to compute laboratory-based calibration curves. These calibration curves are then used as a framework to estimate bedload mass from the impulses and packets registered in the field. Estimated and measured bedload mass are compared for more than 50 bedload samples taken by the automatic basket samplers at the Erlenbach. The results emphasize the sensitivity of the Swiss plate geophone to different hydraulic parameters, in particular mean flow velocity and bed roughness. We conclude that to calibrate the Swiss plate geophone in the laboratory, the hydraulic conditions like bed roughness and Froude numbers have to be replicated. Keywords: Swiss plate geophone, calibration, flume experiments, bedload transport, indirect measurement.

  20. Growth kinetics and microstructural evolution during hot isostatic pressing of U-10 wt.% Mo monolithic fuel plate in AA6061 cladding with Zr diffusion barrier

    SciTech Connect

    Y. Park; J. Yoo; K. Huang; D. D. Keiser, Jr.; J. F. Jue; B. Rabin; G. Moore; Y. H. Sohn

    2014-04-01

    Phase constituents and microstructure changes in RERTR fuel plate assemblies as functions of temperature and duration of hot-isostatic pressing (HIP) during fabrication were examined. The HIP process was carried out as functions of temperature (520, 540, 560 and 580 °C for 90 min) and time (45–345 min at 560 °C) to bond 6061 Al-alloy to the Zr diffusion barrier that had been co-rolled with U-10 wt.% Mo (U10Mo) fuel monolith prior to the HIP process. Scanning and transmission electron microscopies were employed to examine the phase constituents, microstructure and layer thickness of interaction products from interdiffusion. At the interface between the U10Mo and Zr, following the co-rolling, the UZr2 phase was observed to develop adjacent to Zr, and the a-U phase was found between the UZr2 and U10Mo, while the Mo2Zr was found as precipitates mostly within the a-U phase. The phase constituents and thickness of the interaction layer at the U10Mo-Zr interface remained unchanged regardless of HIP processing variation. Observable growth due to HIP was only observed for the (Al,Si)3Zr phase found at the Zr/AA6061 interface, however, with a large activation energy of 457 ± 28 kJ/mole. Thus, HIP can be carried to improve the adhesion quality of fuel plate without concern for the excessive growth of the interaction layer, particularly at the U10Mo-Zr interface with the a-U, Mo2Zr, and UZr2 phases.

  1. Growth kinetics and microstructural evolution during hot isostatic pressing of U-10 wt.% Mo monolithic fuel plate in AA6061 cladding with Zr diffusion barrier

    NASA Astrophysics Data System (ADS)

    Park, Y.; Yoo, J.; Huang, K.; Keiser, D. D.; Jue, J. F.; Rabin, B.; Moore, G.; Sohn, Y. H.

    2014-04-01

    Phase constituents and microstructure changes in RERTR fuel plate assemblies as functions of temperature and duration of hot-isostatic pressing (HIP) during fabrication were examined. The HIP process was carried out as functions of temperature (520, 540, 560 and 580 °C for 90 min) and time (45-345 min at 560 °C) to bond 6061 Al-alloy to the Zr diffusion barrier that had been co-rolled with U-10 wt.% Mo (U10Mo) fuel monolith prior to the HIP process. Scanning and transmission electron microscopies were employed to examine the phase constituents, microstructure and layer thickness of interaction products from interdiffusion. At the interface between the U10Mo and Zr, following the co-rolling, the UZr2 phase was observed to develop adjacent to Zr, and the α-U phase was found between the UZr2 and U10Mo, while the Mo2Zr was found as precipitates mostly within the α-U phase. The phase constituents and thickness of the interaction layer at the U10Mo-Zr interface remained unchanged regardless of HIP processing variation. Observable growth due to HIP was only observed for the (Al,Si)3Zr phase found at the Zr/AA6061 interface, however, with a large activation energy of 457 ± 28 kJ/mole. Thus, HIP can be carried to improve the adhesion quality of fuel plate without concern for the excessive growth of the interaction layer, particularly at the U10Mo-Zr interface with the α-U, Mo2Zr, and UZr2 phases.

  2. Demonstration of 12 nm resolution Fresnel zone plate lens based soft x-ray microscopy

    SciTech Connect

    Chao, W.; Kim, J.; Rekawa, S.; Fischer, P.; Anderson, E. H.

    2009-06-05

    To extend soft x-ray microscopy to a resolution of order 10 nm or better, we developed a new nanofabrication process for Fresnel zone plate lenses. The new process, based on the double patterning technique, has enabled us to fabricate high quality gold zone plates with 12 nm outer zones. Testing of the zone plate with the full-field transmission x-ray microscope, XM-1, in Berkeley, showed that the lens clearly resolved 12 nm lines and spaces. This result represents a significant step towards 10 nm resolution and beyond.

  3. Developing a Basal Texture with Two Peaks Tilting Towards the Transverse Direction in Hot Rolled Mg-5.7Zn-0.5Zr Plates

    NASA Astrophysics Data System (ADS)

    Wang, Yannan; Xin, Yunchang; Chapuis, Adrien; Yu, Huihui; Liu, Qing

    2016-08-01

    Rolled Mg alloys often present a basal texture with the (0002) poles slightly tilting from the normal direction (ND) towards the rolling direction. The current work systematically studies the formation of a double-peaked basal texture tilting from the ND towards the transverse direction (TD) of Mg-5.7Zn-0.5Zr (ZK60) plates hot rolled from the as-cast condition. Our results show that a basal texture forms with the two peaks obviously tilting from the ND towards the TD after rolling to reductions over 19 pct at 673 K (400 °C), but does not appear after rolling at 293 K (20 °C). The TD-tilted double peaks of basal poles disappear after annealing, developing a stronger peak of basal poles around the ND. The microstructural examination indicates that this TD-tilted basal texture mainly results from rolling deformation rather than dynamic recrystallization. Crystal plasticity simulation using the VPSC model was used to understand the effect of slips and twinning on the formation of this TD-tilted basal texture. Simulation demonstrates that, compared to prismatic slip, pyramidal slip is more efficient to generate the basal texture tilting towards the TD. The possible mechanisms affecting the activity of non-basal slips are discussed.

  4. Hot Plate Annealing at a Low Temperature of a Thin Ferroelectric P(VDF-TrFE) Film with an Improved Crystalline Structure for Sensors and Actuators

    PubMed Central

    Mahdi, Rahman Ismael; Gan, W.C.; Abd. Majid, W. H.

    2014-01-01

    Ferroelectric poly(vinylidene fluoride-trifluoroethylene) (P(VDF-TrFE)) copolymer 70/30 thin films are prepared by spin coating. The crystalline structure of these films is investigated by varying the annealing temperature from the ferroelectric phase to the paraelectric phase. A hot plate was used to produce a direct and an efficient annealing effect on the thin film. The dielectric, ferroelectric and pyroelectric properties of the P(VDF-TrFE) thin films are measured as a function of different annealing temperatures (80 to 140 °C). It was found that an annealing temperature of 100 °C (slightly above the Curie temperature, Tc) has induced a highly crystalline β phase with a rod-like crystal structure, as examined by X-ray. Such a crystal structure yields a high remanent polarization, Pr = 94 mC/m2, and pyroelectric constant, p = 24 μC/m2K. A higher annealing temperature exhibits an elongated needle-like crystal domain, resulting in a decrease in the crystalline structure and the functional electrical properties. This study revealed that highly crystalline P(VDF-TrFE) thin films could be induced at 100 °C by annealing the thin film with a simple and cheap method. PMID:25317763

  5. Highly sensitive hot electron bolometer based on disordered graphene.

    PubMed

    Han, Qi; Gao, Teng; Zhang, Rui; Chen, Yi; Chen, Jianhui; Liu, Gerui; Zhang, Yanfeng; Liu, Zhongfan; Wu, Xiaosong; Yu, Dapeng

    2013-01-01

    A bolometer is a device that makes an electrical resistive response to the electromagnetic radiation resulted from a raise of temperature due to heating. The combination of the extremely weak electron-phonon interactions along with its small electron heat capacity makes graphene an ideal material for applications in ultra-fast and sensitive hot electron bolometer. However, a major issue is that the resistance of pristine graphene weakly depends on the electronic temperature. We propose using disordered graphene to obtain a strongly temperature dependent resistance. The measured electrical responsivity of the disordered graphene bolometer reaches 6 × 10(6) V/W at 1.5 K, corresponding to an optical responsivity of 1.6 × 10(5) V/W. The deduced electrical noise equivalent power is 1.2 fW/√Hz, corresponding to the optical noise equivalent power of 44 fW/√Hz. The minimal device structure and no requirement for high mobility graphene make a step forward towards the applications of graphene hot electron bolometers. PMID:24346418

  6. Highly sensitive hot electron bolometer based on disordered graphene

    PubMed Central

    Han, Qi; Gao, Teng; Zhang, Rui; Chen, Yi; Chen, Jianhui; Liu, Gerui; Zhang, Yanfeng; Liu, Zhongfan; Wu, Xiaosong; Yu, Dapeng

    2013-01-01

    A bolometer is a device that makes an electrical resistive response to the electromagnetic radiation resulted from a raise of temperature due to heating. The combination of the extremely weak electron-phonon interactions along with its small electron heat capacity makes graphene an ideal material for applications in ultra-fast and sensitive hot electron bolometer. However, a major issue is that the resistance of pristine graphene weakly depends on the electronic temperature. We propose using disordered graphene to obtain a strongly temperature dependent resistance. The measured electrical responsivity of the disordered graphene bolometer reaches 6 × 106 V/W at 1.5 K, corresponding to an optical responsivity of 1.6 × 105 V/W. The deduced electrical noise equivalent power is 1.2 , corresponding to the optical noise equivalent power of 44 . The minimal device structure and no requirement for high mobility graphene make a step forward towards the applications of graphene hot electron bolometers. PMID:24346418

  7. Numerical Analysis of Residual Stress for Copper Base Brazed Stainless Steel Plate-Fin Structure

    NASA Astrophysics Data System (ADS)

    Xie, Qiaoyun; Ling, Xiang

    2010-07-01

    Copper base stainless steel plate-fin structure has been widely used as a heat exchanger in many fields. The nonlinear thermal reaction on the residual stress in brazing process of the plate-fin structure was studied in this paper. A finite element model (FEM) was proposed to simulate the heat transfer and the sequential residual stress generated in the plate-fin and filler metals based on thermal elastic-plastic theory. By the stress distribution in four paths marked in the structure obtained from FEM results, it is found that the maximum residual tensile stress occurs in the brazed joint next to the plate side and a crack would initiate in this region. Also, the first principle stresses of reference nodes were calculated and the conclusion is consistent with the simulation results. These results would provide some constructive instructions in the practical brazing procedure.

  8. Multifrequency multi-qubit entanglement based on plasmonic hot spots

    PubMed Central

    Ren, Jun; Wu, Tong; Zhang, Xiangdong

    2015-01-01

    The theoretical method to study strong coupling between an ensemble of quantum emitters (QEs) and surface plasmons excited by the nanoparticle cluster has been presented by using a rigorous first-principles electromagnetic Green’s tensor technique. We have demonstrated that multi-qubit entanglements for two-level QEs can be produced at different coupling resonance frequencies, when they locate in the hot spots of the metallic nanoparticle cluster. The duration of quantum beats for such an entanglement can reach two orders longer than that for the entanglement in a photonic cavity. The phenomenon originates from collective coupling resonance excitation of the cluster. At the frequency of single scattering resonance, the entanglement cannot be produced although the single QE spontaneous decay rate is very big. PMID:26350051

  9. Hot coal gas desulfurization with manganese-based sorbents

    SciTech Connect

    Hepworth, M.T.; Ben-Slimane, R.

    1995-11-01

    The primary major deposit of manganese in the US which can be readily mined by an in situ process is located in the Emily district of Minnesota. The US Bureau of Mines Research Centers at both the Twin Cities and Salt Lake City have developed a process for extracting and refining manganese in the form of a high-purity carbonate product. This product has been formulated into pellets by a multi-step process of drying, calcination, and induration to produce relatively high-strength formulations which are capable of being used for hot fuel gas desulfurization. These pellets, which have been developed at the University of Minnesota under joint sponsorship of the US Department of Energy and the US Bureau of Mines, appear superior to other, more expensive, formulations of zinc titanate and zinc ferrite which have previously been studied for multi-cycle loading (desulfurization) and regeneration (evolution of high-strength SO{sub 2} and restoration of pellet reactivity). Although these other formulations have been under development for the past twelve years, their prices still exceed $7 per pound. If manganese pellets perform as predicted in fixed bed testing, and if a significant number of utilities which burn high-sulfur coals incorporate combined-cycle gasification with hot coal gas desulfurization as a viable means of increasing conversion efficiencies, then the potential market for manganese pellets may be as high as 200,000 tons per year at a price not less than $3 per pound. This paper discusses the role of manganese pellets in the desulfurization process with respect to the integrated gasification combined-cycle (IGCC) for power generation.

  10. Degradation behaviour of LAE442-based plate-screw-systems in an in vitro bone model.

    PubMed

    Wolters, Leonie; Besdo, Silke; Angrisani, Nina; Wriggers, Peter; Hering, Britta; Seitz, Jan-Marten; Reifenrath, Janin

    2015-04-01

    The use of absorbable implant materials for fixation after bone fracture helps to avoid a second surgery for implant removal and the risks and costs involved. Magnesium (Mg) is well known as a potential metallic material for degradable implants. The aim of the present in vitro study was to evaluate if degradable LAE442-based magnesium plate-screw-systems are suitable candidates for osteosynthesis implants in load-bearing bones. The corrosion behaviour was tested concerning the influence of different surface treatments, coatings and screw torques. Steel plates and screws of the same size served as control. Plates without special treatment screwed on up to a specified torque of 15cNm or 7cNm, NaOH treated plates (15cNm), magnesium fluoride coated plates (15cNm) and steel plates as control (15cNm) were examined in pH-buffered, temperature-controlled SBF solution for two weeks. The experimental results indicate that the LAE442 plates and screws coated with magnesium fluoride revealed a lower hydrogen evolution in SBF solution as well as a lower weight loss and volume decrease in μ-computed tomography (μCT). The nanoindentation and SEM/EDX measurements at several plate areas showed no significant differences. Summarized, the different screw torques did not affect the corrosion behaviour differently. Also the NaOH treatment seemed to have no essential influence on the degradation kinetics. The plates coated with magnesium fluoride showed a decreased corrosion rate. Hence, it is recommended to consider this coating for the next in vivo study. PMID:25686954

  11. An efficient Mindlin finite strip plate element based on assumed strain distribution

    NASA Technical Reports Server (NTRS)

    Chulya, Abhisak; Thompson, Robert L.

    1988-01-01

    A simple two node, linear, finite strip plate bending element based on Mindlin-Reissner plate theory for the analysis of very thin to thick bridges, plates, and axisymmetric shells is presented. The new transverse shear strains are assumed for constant distribution in the two node linear strip. The important aspect is the choice of the points that relate the nodal displacements and rotations through the locking transverse shear strains. The element stiffness matrix is explicitly formulated for efficient computation and ease in computer implementation. Numerical results showing the efficiency and predictive capability of the element for analyzing plates with different supports, loading conditions, and a wide range of thicknesses are given. The results show no sign of the shear locking phenomenon.

  12. A 3-D elasticity theory based model for acoustic radiation from multilayered anisotropic plates.

    PubMed

    Shen, C; Xin, F X; Lu, T J

    2014-05-01

    A theoretical model built upon three-dimensional elasticity theory is developed to investigate the acoustic radiation from multilayered anisotropic plates subjected to a harmonic point force excitation. Fourier transform technique and stationary phase method are combined to predict the far-field radiated sound pressure of one-side water immersed plate. Compared to equivalent single-layer plate models, the present model based on elasticity theory can differentiate radiated sound pressure between dry-side and wet-side excited cases, as well as discrepancies induced by different layer sequences for multilayered anisotropic plates. These results highlight the superiority of the present theoretical model especially for handling multilayered anisotropic structures. PMID:24815294

  13. Electroplated Fe-Co-Ni films prepared from deep-eutectic-solvent-based plating baths

    NASA Astrophysics Data System (ADS)

    Yanai, Takeshi; Shiraishi, Kotaro; Akiyoshi, Toshiki; Azuma, Keita; Watanabe, Yoshimasa; Ohgai, Takeshi; Morimura, Takao; Nakano, Masaki; Fukunaga, Hirotoshi

    2016-05-01

    We fabricated soft magnetic films from DES-based plating baths, and investigated magnetic properties of the plated films. The plating baths were obtained by stirring the mixture of choline chloride, ethylene glycol, FeCl2 ṡ 4H2O, NiCl2 ṡ 6H2O and CoCl2 ṡ 6H2O. The composition of the electroplated film depended on the amount of the reagent in the plating bath, and we consequently obtained the films with various composition. The current efficiency of the plating process shows high values (> 88 %) in the wide composition range. The soft magnetic films with low coercivity were obtained at the Fe compositions of ≈ 30 at.% and > 80 at.%, and we found that low coercivity could be realized by the control of the film composition. We also found that the Fe-rich films prepared from DES-based plating bath have some advantages as a soft magnetic phase for a nanocomposite magnet due to their high saturation magnetization and very fine crystal structure.

  14. Magnetic Fe-Co films electroplated in a deep-eutectic-solvent-based plating bath

    NASA Astrophysics Data System (ADS)

    Yanai, T.; Shiraishi, K.; Watanabe, Y.; Ohgai, T.; Nakano, M.; Suzuki, K.; Fukunaga, H.

    2015-05-01

    We fabricated Fe-Co films from a deep eutectic solvent (DES)-based plating bath and investigated magnetic properties of the plated films. The plating baths were obtained by stirring the mixture of choline chloride, ethylene glycol, FeCl2.4H2O, and CoCl2.6H2O. The composition of the plated films depended on the amount of FeCl2.4H2O in the plating bath, and Fe content of the films was varied from 0 to 100 at. %. Depending on the Fe content, the saturation magnetization and the coercivity of the films varied. The Fe76Co24 film shows high saturation magnetization and smooth surface, and the change in the saturation magnetization shows good agreement with the expected change by the Slater-Pauling curve. High current efficiency (>90%) could be obtained in the wide film composition. From these results, we concluded that the DES-based plating bath is one of effective baths for the Fe-Co films with high current efficiency.

  15. Computer animation of Phanerozoic plate motions

    SciTech Connect

    Scotese, C.R. . Dept. of Geology)

    1992-01-01

    Since 1985, the PALEOMAP Project, in collaboration with research groups both in the US and abroad, has assembled a digital model that describes global plate motions during the last 600 million years. In this paper the authors present a series of computer animations that dynamically illustrates the movement of continents and terranes, and the evolution of the ocean basins since the breakup of the late Precambrian supercontinent. These animations depict the motion of the plates from both equatorial and polar perspectives. Mesozoic and Cenozoic plate tectonic reconstructions are based on a synthesis of linear magnetic anomalies, fracture zone locations, intracontinental rifts, collision and thrust belts, and zones of strike-slip. Paleozoic plate reconstructions, though more speculative, are based on evidence of past subduction, continental collision, and inferred sea floor spreading. The relative longitudinal positions of the continents during the Paleozoic and the width of intervening oceans have been adjusted to best explain changing biogeographic and paleoclimatic patterns. A new paleomagnetic/hot spot reference frame has been constructed that combines paleomagnetic data compiled by Rob Van der Voo (1992) with inferred motion relative to a fixed frame of hot spots. Using probable Early Mesozoic and Paleozoic hot spot tracks on the major continents, the authors have extended plate motions relative to the hot spot reference frame back to 400 million years.

  16. Metalizing reduction and magnetic separation of vanadium titano-magnetite based on hot briquetting

    NASA Astrophysics Data System (ADS)

    Chen, Shuang-yin; Chu, Man-sheng

    2014-03-01

    To achieve high efficiency utilization of Panzhihua vanadium titano-magnetite, a new process of metalizing reduction and magnetic separation based on hot briquetting is proposed, and factors that affect the cold strength of the hot-briquetting products and the efficiency of reduction and magnetic separation are successively investigated through laboratory experiments. The relevant mechanisms are elucidated on the basis of microstructural observations. Experimental results show that the optimal process parameters for hot briquetting include a hot briquetting temperature of 475°C, a carbon ratio of 1.2, ore and coal particle sizes of less than 74 μm. Additionally, with respect to metalizing reduction and magnetic separation, the rational parameters include a magnetic field intensity of 50 mT, a reduction temperature of 1350°C, a reduction time of 60 min, and a carbon ratio of 1.2. Under these above conditions, the crushing strength of the hot-briquetting agglomerates is 1480 N, and the recovery ratios of iron, vanadium, and titanium are as high as 91.19%, 61.82%, and 85.31%, respectively. The new process of metalizing reduction and magnetic separation based on hot briquetting demonstrates the evident technological advantages of high efficiency separation of iron from other valuable elements in the vanadium titano-magnetite.

  17. Hot Electron-Based Near-Infrared Photodetection Using Bilayer MoS2.

    PubMed

    Wang, Wenyi; Klots, Andrey; Prasai, Dhiraj; Yang, Yuanmu; Bolotin, Kirill I; Valentine, Jason

    2015-11-11

    Recently, there has been much interest in the extraction of hot electrons generated from surface plasmon decay, as this process can be used to achieve additional bandwidth for both photodetectors and photovoltaics. Hot electrons are typically injected into semiconductors over a Schottky barrier between the metal and semiconductor, enabling generation of photocurrent with below bandgap photon illumination. As a two-dimensional semiconductor single and few layer molybdenum disulfide (MoS2) has been demonstrated to exhibit internal photogain and therefore becomes an attractive hot electron acceptor. Here, we investigate hot electron-based photodetection in a device consisting of bilayer MoS2 integrated with a plasmonic antenna array. We demonstrate sub-bandgap photocurrent originating from the injection of hot electrons into MoS2 as well as photoamplification that yields a photogain of 10(5). The large photogain results in a photoresponsivity of 5.2 A/W at 1070 nm, which is far above similar silicon-based hot electron photodetectors in which no photoamplification is present. This technique is expected to have potential use in future ultracompact near-infrared photodetection and optical memory devices. PMID:26426510

  18. Hot coal gas desulfurization with manganese-based sorbents

    SciTech Connect

    Hepworth, M.T.; Ben-Slimane, R.

    1994-10-01

    In this paper, the physical and chemical behavior of several sorbent formulations fabricated from a manganese-containing compound, alundum (Al{sub 2}O{sub 3}), and a binder are addressed. The thermodynamic feasibility of hydrogen sulfide (H{sub 2}S)-removal from hot-simulated coal-gases using these sorbents and their subsequent regeneration with air are established. A formulation, FORM4-A, which consists of MnCO{sub 3}, alundum, and bentonite exhibits the best combination of capacity and reactivity; whereas, FORM1-A, which consists of Mn-ore, alundum, and dextrin exhibits the best combination of strength and reactivity. One important finding is that the capacity of the pellets for sulfur pickup from a H{sub 2}/H{sub 2}S mixture (at 950{degrees}C) and the kinetics of reduction, sulfidation and regeneration (at 1000{degrees}C) improve with recycling without compromising the strength. The leading formulation, FORM4-A, was subjected to 20 consecutive cycles of sulfidation and regeneration at 900{degrees}C in a 2-inch fixed bed reactor. The sulfidation gas was a simulated Tampella U-gas with an increased hydrogen sulfide content of 3% by volume to accelerate the rate of breakthrough, arbitrarily taken as 500 ppmv. Consistent with thermo-gravimetric analysis (TGA) on individual pellets, the fixed bed tests show small improvement in capacity and kinetics with the sulfur-loading capacity being about 22% by weight of the original pellet, which corresponds to approximately 90% bed utilization.

  19. Superconductor-Base Hot-Electron Transistor. II. Fabrication and Electrical Measurement

    NASA Astrophysics Data System (ADS)

    Sakai, Hiroyuki; Kurita, Yoshiyuki; Tonouchi, Masayoshi; Kobayashi, Takeshi

    1986-06-01

    Superconductor-base hot-electron transistors (Super-HETs) comprising n+-GaAs/Nb(or NbN)/α-InSb/Au multiplelayers were fabricated and electrical measurements were made at liquid-helium temperature. The observed hot-electron transport efficiency was as high as 80% for a device with a 200Å thick Nb base, close to the theoretical 90%. A device with a 600Å NbN base exhibited an efficiency of 60%. The sputtered InSb film served as a suitable collector barrier with a lower barrier height and an extremely reduced quantum mechanical reflection for incident hot-electrons. However, the space-charge limited current was still limited to the lower value, probably due to residual defects.

  20. Constitutive Description of 7075 Aluminum Alloy During Hot Deformation by Apparent and Physically-Based Approaches

    NASA Astrophysics Data System (ADS)

    Mirzadeh, Hamed

    2015-03-01

    Hot flow stress of 7075 aluminum alloy during compressive hot deformation was correlated to the Zener-Hollomon parameter through constitutive analyses based on the apparent approach and the proposed physically-based approach which accounts for the dependence of the Young's modulus and the self-diffusion coefficient of aluminum on temperature. It was shown that the latter approach not only results in a more reliable constitutive equation, but also significantly simplifies the constitutive analysis, which in turn makes it possible to conduct comparative hot working studies. It was also demonstrated that the theoretical exponent of 5 and the lattice self-diffusion activation energy of aluminum (142 kJ/mol) can be set in the hyperbolic sine law to describe the peak flow stresses and the resulting constitutive equation was found to be consistent with that resulted from the proposed physically-based approach.

  1. Evaluation of Transverse Thermal Stresses in Composite Plates Based on First-Order Shear Deformation Theory

    NASA Technical Reports Server (NTRS)

    Rolfes, R.; Noor, A. K.; Sparr, H.

    1998-01-01

    A postprocessing procedure is presented for the evaluation of the transverse thermal stresses in laminated plates. The analytical formulation is based on the first-order shear deformation theory and the plate is discretized by using a single-field displacement finite element model. The procedure is based on neglecting the derivatives of the in-plane forces and the twisting moments, as well as the mixed derivatives of the bending moments, with respect to the in-plane coordinates. The calculated transverse shear stiffnesses reflect the actual stacking sequence of the composite plate. The distributions of the transverse stresses through-the-thickness are evaluated by using only the transverse shear forces and the thermal effects resulting from the finite element analysis. The procedure is implemented into a postprocessing routine which can be easily incorporated into existing commercial finite element codes. Numerical results are presented for four- and ten-layer cross-ply laminates subjected to mechanical and thermal loads.

  2. LQR-based optimization of multiple tuned resonators for plate sound radiation reduction

    NASA Astrophysics Data System (ADS)

    Michielsen, J.; Arteaga, I. Lopez; Nijmeijer, H.

    2016-02-01

    A linear quadratic regulator based optimization problem is formulated in order to minimize the broad-band low-frequency domain vibration and acoustic response of a baffled simply supported plate by means of multiple optimally tuned mass-spring-damper systems. To this end, we propose a robust method to obtain a (stable) state-space model describing the far-field radiated sound power, also known as the radiation filter. The Kirchhoff plate equation, which describes the plate vibrations, is discretized based on the Rayleigh-Ritz method. The resulting state-space models of the plate and the mass-springdamper systems are coupled to the radiation filter. Finally, the optimal spring stiffness and damping values of each mass-spring-damper system are successfully obtained by minimizing the kinetic energy or the far-field radiated sound power of the plate for low computational cost. In general, the results indicate that tuned mass-spring-damper systems have great potential to reduce the broadband low frequency vibration and acoustic response of vibro-acoustic systems. From the results, it can be concluded that there are fundamental differences between the optimal TMD systems if one minimizes the kinetic energy or the far-field radiated sound power.

  3. Hot corrosion behavior of platinum-modified nickel- and cobalt-based alloys and coatings

    NASA Astrophysics Data System (ADS)

    Deodeshmukh, Vinay Prakash

    High temperature degradation by hot corrosion (650-1000°C) and/or oxidation (>1000°C) can severely reduce the longevity of advanced gas turbine engine components. The protection of high-temperature components against hot corrosion or oxidation is typically conferred by the application of either a diffusion or overlay metallic coating that is able to form a continuous, adherent, and slow-growing oxide scale. There are currently no coatings that provide adequate protection to both hot corrosion and oxidation. Indeed, there is a particular need for such protective coatings because many advanced aero, marine, and industrial gas-turbines operate in both hot corrosion and oxidation regimes in their duty cycle. Recent work at Iowa State University (ISU) has showed that a wide range Pt+Hf-modified gamma'-Ni3Al + gamma-Ni alloy compositions form a very adherent and slow-growing Al 2O3 scale. In fact, the results reported suggest that Pt+Hf-modified gamma' + gamma coatings offer a viable superior alternative to beta-NiAl(Pt)-based coatings. The main thrust of this study was to assess and establish optimum target gamma' + gamma coating compositions for extending the service life of high-temperature gas turbine components exposed to hot corrosion and oxidation conditions. Both high temperature hot-corrosion (HTHC-900°C) and low temperature hot-corrosion (LTHC-705°C) behaviors of the Pt+Hf-modified gamma' + gamma alloys were assessed. The salt used to bring about hot corrosion was Na 2SO4. Quite interestingly, it was found that the HTHC resistance of gamma' + gamma alloys improved with up to about 10 at.% Pt addition, but then decreased significantly with increasing Pt content up to 30 at.% (the maximum level studied); however, under LTHC conditions the resistance of gamma' + gamma alloys improved with increasing Pt content up to 30 at.%. To further improve hot corrosion resistance of Pt+Hf-modified gamma' + gamma alloys, the effects of systematic additions of Cr, Si, and

  4. Tandem-structured, hot electron based photovoltaic cell with double Schottky barriers

    PubMed Central

    Lee, Young Keun; Lee, Hyosun; Park, Jeong Young

    2014-01-01

    We demonstrate a tandem-structured, hot electron based photovoltaic cell with double Schottky barriers. The tandem-structured, hot electron based photovoltaic cell is composed of two metal/semiconductor interfaces. Two types of tandem cells were fabricated using TiO2/Au/Si and TiO2/Au/TiO2, and photocurrent enhancement was detected. The double Schottky barriers lead to an additional pathway for harvesting hot electrons, which is enhanced through multiple reflections between the two barriers with different energy ranges. In addition, light absorption is improved by the band-to-band excitation of both semiconductors with different band gaps. Short-circuit current and energy conversion efficiency of the tandem-structured TiO2/Au/Si increased by 86% and 70%, respectively, compared with Au/Si metal/semiconductor nanodiodes, showing an overall solar energy conversion efficiency of 5.3%. PMID:24694838

  5. Empirical study on neural network based predictive techniques for automatic number plate recognition

    NASA Astrophysics Data System (ADS)

    Shashidhara, M. S.; Indrakumar, S. S.

    2011-10-01

    The objective of this study is to provide an easy, accurate and effective technology for the Bangalore city traffic control. This is based on the techniques of image processing and laser beam technology. The core concept chosen here is an image processing technology by the method of automatic number plate recognition system. First number plate is recognized if any vehicle breaks the traffic rules in the signals. The number is fetched from the database of the RTO office by the process of automatic database fetching. Next this sends the notice and penalty related information to the vehicle owner email-id and an SMS sent to vehicle owner. In this paper, we use of cameras with zooming options & laser beams to get accurate pictures further applied image processing techniques such as Edge detection to understand the vehicle, Identifying the location of the number plate, Identifying the number plate for further use, Plain plate number, Number plate with additional information, Number plates in the different fonts. Accessing the database of the vehicle registration office to identify the name and address and other information of the vehicle number. The updates to be made to the database for the recording of the violation and penalty issues. A feed forward artificial neural network is used for OCR. This procedure is particularly important for glyphs that are visually similar such as '8' and '9' and results in training sets of between 25,000 and 40,000 training samples. Over training of the neural network is prevented by Bayesian regularization. The neural network output value is set to 0.05 when the input is not desired glyph, and 0.95 for correct input.

  6. Ballistic Hot Electron Transport in Heteroepitaxial SrRuO3 Metal-Base Transistors

    NASA Astrophysics Data System (ADS)

    Kim, Brian; Hikita, Yasuyuki; Yajima, Takeaki; Bell, Christopher; Hwang, Harold

    Perovskite oxide heterostructures is a rapidly emerging field significant for interface-induced electronic and magnetic reconstructions, resulting in novel phases distinct from those found in the bulk counterparts. Notably, utilizing device structures is an effective way to probe these interface-induced phases. One of the most prevalent device structures that has been adopted so far is a three-terminal field-effect geometry, used to probe in-plane electronic transport properties. However, the out-of-plane three-terminal device geometry, though less studied due to its complexity, is also useful in many aspects. In the metal-base transistor (MBT), for instance, ballistic transport of hot electrons injected across a Schottky diode emitter can be used to probe hot electron properties of the metal-base, providing information on inelastic scattering mechanisms, electron confinement effects, and intervalley transfer. One promising model system for the metal-base is SrRuO3 (SRO), characterized by intermediate electron correlations with unusual transport properties. Here we present an all-perovskite oxide heteroepitaxial MBT using SRO as a metal-base layer. Successful MBT operation for various metal-base layer thicknesses was achieved, from which the hot electron attenuation length of SRO was deduced. These results form a foundation on which to examine the properties of hot electrons in strongly correlated systems using the out-of-plane three-terminal device geometry.

  7. Identification and quantification of leachable substances from polymer-based orthodontic base-plate materials.

    PubMed

    Kopperud, Hilde Molvig; Kleven, Inger Sjøvik; Wellendorf, Hanne

    2011-02-01

    The aim of this study was to analyse leachable monomers, additives, and degradation products from polymer-based orthodontic base-plate materials. One heat-cured resin (Orthocryl), one light-cured (Triad VLC), and three thermoplastic materials (Biocryl C, Essix A+, and Essix Embrace) were investigated. Elution was performed in water at 37°C for 10 days. The extract medium was changed and analysed daily. Chromatographic methods were used to identify and quantify the leachables. In addition, the content of residual methyl methacrylate (MMA) was quantified in the poly(methyl methacrylate) (PMMA)-based materials. Statistical analysis of the quantitative results was performed using a t-test for comparison of two independent samples. Monomers and additives leached from the materials polymerized in situ and from the thermoplastic PMMA-based material. No leachable substances were found in the extracts from the other thermoplastic materials. Accumulated over 10 days, a larger amount of MMA leached from the powder-and-liquid material, Orthocryl (42 μg/cm(2)), than from the thermoplastic material, Biocryl C (0.49 μg/cm(2)). The accumulated amounts of monomers leached from Triad VLC were 91 μg/cm(2) of urethane dimethacrylate and 2.2 μg/cm(2) of 2-hydroxyethyl methacrylate. Formaldehyde was found to leach from methacrylate-based materials: 3.2 μg/cm(2) from Orthocryl and 0.16 μg/cm(2) from Triad VLC. However, formaldehyde was not detectable in extracts from Biocryl C. Residual MMA was 5.4 wt % in Orthocryl and 0.4 wt % in Biocryl C. No phthalates were detected in the tested materials. In this in vitro study, minimal leaching was found from the thermoplastic materials, while leaching of methacrylates and formaldehyde was observed from the powder-and-liquid type and the paste material. Within the limitations of this study, the results suggest that prefabricated thermoplastic plates should be preferred for patients with an allergy to methacrylates. PMID:20624754

  8. Voluntary access to a warm plate reduces hyperactivity in activity-based anorexia.

    PubMed

    Hillebrand, Jacquelien J G; de Rijke, Corine E; Brakkee, Jan H; Kas, Martien J H; Adan, Roger A H

    2005-06-01

    Activity-based anorexia (ABA) is considered an animal model of anorexia nervosa. In ABA, scheduled feeding in combination with voluntary wheel running leads to hyperactivity, reduced food intake, severe body weight loss and hypothermia. In this study it was investigated whether hyperactivity in ABA could be reduced by introducing a warm plate (which was voluntary accessible and did not influence ambient temperature) into a part of the cage. In ad libitum fed rats, the presence of the warm plate did not influence body temperature, running wheel activity (RWA), body weight or food intake. During ABA, however, rats preferred the warm plate and hypothermia was prevented, while hyperactivity and body weight loss were significantly reduced when compared to ABA rats without a plate. Correlation analysis revealed a significant association between basal body temperature and RWA during the light phase in ABA rats. However, there was no evidence that initiation of light phase RWA was a result of hypothermia. These data suggest that ABA rats prefer to prevent hypothermia passively by choosing a warm plate rather than actively regulating body temperature by hyperactivity. PMID:15924912

  9. Identification of Impact Location in a Plate Based on Elastodynamics and Higher Order Time Frequency Method

    NASA Astrophysics Data System (ADS)

    Lee, S. K.; Kim, S. J.

    In a nuclear power plant, impact force due to loose part is related to the structural damage in the plant. In general, the steam generator of the nuclear power plant is structured by thick plate. The paper presents a novel approach to locate an impact load in a thick plate. The approach is based on the analysis of the acoustic waveforms measured by a sensor array located on the plate surface. For accurate estimation of the location of the impact source, the time differences in the arrival times of the waves at the sensors and their propagation velocities are determined. The dispersion curves for multi modes of Lamb wave are calculated by using exact plate theory and SDPT. It is difficult to measure directly the group velocity for Lamb mode of acoustic waveform in the thick plate because they are dispersive wave. However, most of the energy in the wave is carried by the flexural waves (A0 mode), the group velocity of this mode is extracted using the CHOTF technique for estimating the impact source location. The estimates are shown to be in excellent agreement with the actual locations and it is applied to the damage analysis due to the loose part in a nuclear power plant.

  10. Virtual plate pre-bending for the long bone fracture based on axis pre-alignment.

    PubMed

    Liu, Bin; Luo, Xinjian; Huang, Rui; Wan, Chao; Zhang, Bingbing; Hu, Weihua; Yue, Zongge

    2014-06-01

    In this paper, a modeling and visualizing system for assisting surgeons in correctly registering for the closed fracture reduction surgery is presented. By using this system, the geometric parameters of the target fixation plate before the long bone fracture operation can be obtained. The main processing scheme consists of following steps: firstly (image data process), utilize the Curvelet transform to denoise the CT images of fracture part and then reconstruct the 3D models of the broken bones. Secondly (pre-alignment), extract the axial lines of the broken bones and spatially align them. Then drive the broken bone models to be pre-aligned. Thirdly (mesh segmentation), a method based on vertex normal feature is utilized to obtain the broken bone cross-sections mesh models. Fourthly (fine registration), the ICP (Iterative Closest Point) algorithm is used to register the cross-sections and the broken bone models are driven to achieve the fine registration posture. Lastly (plate fitting), an accurate NURBS surface fitting method is used to construct the virtual plate. The experiment proved that the obtained models of the pre-bended plates were closely bonded to the surface of the registered long bone models. Finally, the lengths, angles and other interested geometric parameters can be measured on the plate models. PMID:24598409

  11. Design of Stress-Strain Measuring System for Bulldozing Plate Based on Virtual Instrument Technology

    NASA Astrophysics Data System (ADS)

    Xu, S. C.; Li, J. Q.; Zhang, R.

    2006-10-01

    Soil is a kind of discrete, multiphase compound that is composed of soil particles, liquid and air. When soil is disturbed by bulldozing plate, the mechanical behavior of the soil will become very complex. Based on the law of action and reaction, the dynamic mechanical behavior of disturbed soil was indirectly analyzed by measuring and studying the forces on the bulldozing plate by soil currently, so a stress-strain virtual measuring system for bulldozing plate, which was designed by the graphical programming language DASYLab, was used to measure the horizontal force Fz acting on the bulldozing plate. In addition, during the course of design, the experimental complexities and the interferential factors influencing on signal logging were analyzed when bulldozing plate worked, so the anti-jamming methods of hardware and software technology were adopted correlatively. In the end, the horizontal force Fz was analyzed with Error Theory, the result shown that the quantificational analysis of Fz were identical to the qualitative results of soil well, and the error of the whole test system is under 5 percent, so the tress-strain virtual measuring system was stable and credible.

  12. A variable-order laminated plate theory based on the variational-asymptotical method

    NASA Technical Reports Server (NTRS)

    Lee, Bok W.; Sutyrin, Vladislav G.; Hodges, Dewey H.

    1993-01-01

    The variational-asymptotical method is a mathematical technique by which the three-dimensional analysis of laminated plate deformation can be split into a linear, one-dimensional, through-the-thickness analysis and a nonlinear, two-dimensional, plate analysis. The elastic constants used in the plate analysis are obtained from the through-the-thickness analysis, along with approximate, closed-form three-dimensional distributions of displacement, strain, and stress. In this paper, a theory based on this technique is developed which is capable of approximating three-dimensional elasticity to any accuracy desired. The asymptotical method allows for the approximation of the through-the-thickness behavior in terms of the eigenfunctions of a certain Sturm-Liouville problem associated with the thickness coordinate. These eigenfunctions contain all the necessary information about the nonhomogeneities along the thickness coordinate of the plate and thus possess the appropriate discontinuities in the derivatives of displacement. The theory is presented in this paper along with numerical results for the eigenfunctions of various laminated plates.

  13. Efficient alignment scheme for zone-plates-based transmission soft X-ray microscope

    NASA Astrophysics Data System (ADS)

    Lim, Jun; Shin, Hyun-Joon; Hong, Chung Ki

    2010-12-01

    Alignment and operation of a zone-plate (ZP)-based transmission soft X-ray microscope (TXM) is difficult and time consuming, especially when the TXM has no dedicated X-ray source. We introduce here an efficient TXM alignment scheme. The TXM employed is a simple in-situ-experiment-capable setup. It includes ultrahigh-vacuum (UHV)-compatible conflat flanges and is mountable in tandem with any soft X-ray synchrotron radiation beamlines. Obtaining zeroth- and first-order diffracted (condenser-zone-plate [CZP]-focused) beams simultaneously by means of the objective zone plate (OZP) is the most essential step in the alignment scheme. We were able to acquire, in one hour at a radiation wavelength of 2.49 nm, an image of 50 nm spatial resolution.

  14. An investigation of the initiation stage of hot corrosion in Ni-base alloys

    NASA Technical Reports Server (NTRS)

    Huang, T. T.; Meier, G. H.

    1979-01-01

    The commercial nickel base alloy, IN-738, and high purity laboratory alloys were prepared to simulate the effects of the major elements in IN-738. Results indicate that the initiation of hot corrosion attack of IN-738 and other similar alloys is the result of local penetration of molten salt through the protective oxide scale.

  15. A Reusable Calcium-Based Sorbent for Desulfurizing Hot Coal Gas

    SciTech Connect

    Wheelock, T.D.; Hasler, D.J.L.

    2002-09-19

    The overall objective of this project has been to develop a superior, regenerable, calcium-based sorbent for desulfurizing hot coal gas. The sorbent should be strong, durable, inexpensive to manufacture, and capable of being reused many times. To achieve these objectives the project has focused on the development of the very promising core-in-shell sorbent.

  16. Automated methodology for selecting hot and cold pixel for remote sensing based evapotranspiration mapping

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Surface energy fluxes, especially the latent heat flux from evapotranspiration (ET), determine exchanges of energy and mass between the hydrosphere, atmosphere, and biosphere. There are numerous remote sensing-based energy balance approaches such as METRIC and SEBAL that use hot and cold pixels from...

  17. A Hot-Wire Method Based Thermal Conductivity Measurement Apparatus for Teaching Purposes

    ERIC Educational Resources Information Center

    Alvarado, S.; Marin, E.; Juarez, A. G.; Calderon, A.; Ivanov, R.

    2012-01-01

    The implementation of an automated system based on the hot-wire technique is described for the measurement of the thermal conductivity of liquids using equipment easily available in modern physics laboratories at high schools and universities (basically a precision current source and a voltage meter, a data acquisition card, a personal computer…

  18. Hot-electron-based solar energy conversion with metal-semiconductor nanodiodes.

    PubMed

    Lee, Young Keun; Lee, Hyosun; Lee, Changhwan; Hwang, Euyheon; Park, Jeong Young

    2016-06-29

    Energy dissipation at metal surfaces or interfaces between a metal and a dielectric generally results from elementary excitations, including phonons and electronic excitation, once external energy is deposited to the surface/interface during exothermic chemical processes or an electromagnetic wave incident. In this paper, we outline recent research activities to develop energy conversion devices based on hot electrons. We found that photon energy can be directly converted to hot electrons and that hot electrons flow through the interface of metal-semiconductor nanodiodes where a Schottky barrier is formed and the energy barrier is much lower than the work function of the metal. The detection of hot electron flow can be successfully measured using the photocurrent; we measured the photoyield of photoemission with incident photons-to-current conversion efficiency (IPCE). We also show that surface plasmons (i.e. the collective oscillation of conduction band electrons induced by interaction with an electromagnetic field) are excited on a rough metal surface and subsequently decay into secondary electrons, which gives rise to enhancement of the IPCE. Furthermore, the unique optical behavior of surface plasmons can be coupled with dye molecules, suggesting the possibility for producing additional channels for hot electron generation. PMID:27168177

  19. Hot-electron-based solar energy conversion with metal–semiconductor nanodiodes

    NASA Astrophysics Data System (ADS)

    Lee, Young Keun; Lee, Hyosun; Lee, Changhwan; Hwang, Euyheon; Park, Jeong Young

    2016-06-01

    Energy dissipation at metal surfaces or interfaces between a metal and a dielectric generally results from elementary excitations, including phonons and electronic excitation, once external energy is deposited to the surface/interface during exothermic chemical processes or an electromagnetic wave incident. In this paper, we outline recent research activities to develop energy conversion devices based on hot electrons. We found that photon energy can be directly converted to hot electrons and that hot electrons flow through the interface of metal–semiconductor nanodiodes where a Schottky barrier is formed and the energy barrier is much lower than the work function of the metal. The detection of hot electron flow can be successfully measured using the photocurrent; we measured the photoyield of photoemission with incident photons-to-current conversion efficiency (IPCE). We also show that surface plasmons (i.e. the collective oscillation of conduction band electrons induced by interaction with an electromagnetic field) are excited on a rough metal surface and subsequently decay into secondary electrons, which gives rise to enhancement of the IPCE. Furthermore, the unique optical behavior of surface plasmons can be coupled with dye molecules, suggesting the possibility for producing additional channels for hot electron generation.

  20. Lessons from Hot Spot Analysis for Fragment-Based Drug Discovery.

    PubMed

    Hall, David R; Kozakov, Dima; Whitty, Adrian; Vajda, Sandor

    2015-11-01

    Analysis of binding energy hot spots at protein surfaces can provide crucial insights into the prospects for successful application of fragment-based drug discovery (FBDD), and whether a fragment hit can be advanced into a high-affinity, drug-like ligand. The key factor is the strength of the top ranking hot spot, and how well a given fragment complements it. We show that published data are sufficient to provide a sophisticated and quantitative understanding of how hot spots derive from a protein 3D structure, and how their strength, number, and spatial arrangement govern the potential for a surface site to bind to fragment-sized and larger ligands. This improved understanding provides important guidance for the effective application of FBDD in drug discovery. PMID:26538314

  1. Selective mode multiplexer based on phase plates and Mach-Zehnder interferometer with image inversion function.

    PubMed

    Igarashi, Koji; Souma, Daiki; Takeshima, Koki; Tsuritani, Takehiro

    2015-01-12

    We propose a novel mode multiplexer based on phase plates followed by a Mach-Zehnder interferometer (MZI) with image inversion. After the higher-order modes are selectively converted from fundamental linear-polarized (LP) modes by the phase plates, the converted modes are coupled without fundamental loss using MZI with image inversion, in which the original spatial pattern and inverted pattern of the optical signal are interfered. Our scheme is also applicable to the coupling of degenerated LP modes such as LP(11a) and LP(11b). First, we numerically and experimentally evaluate the performance of the mode converter based on phase plates. The mode converter is suitable as long as the five LP modes such as LP(01), LP(11ab) and LP(21ab) are sustained in a few-mode fiber (FMF), although the crosstalk due to excitation of undesirable modes is unavoidable when the higher-order modes over LP(02) are sustained in FMF. Next, we develop and characterize the proposed mode multiplexers based on phase plates and MZIs with image inversion. The insertion loss is suppressed to around 3 dB for mode multiplexing of LP(11a) and LP(11b). Using a fabricated mode multiplexer for LP(31a) and LP(31b), we measure the bit-error rate performance of single-polarization mode-multiplexed quadrature-phase shift keying optical signals. PMID:25835665

  2. Seismic and Geodynamic Constraints on Compositional Heterogeneity in the Lower Mantle: Implications for Deeply-Rooted Hot Upwellings Under the African and Pacific Plates

    NASA Astrophysics Data System (ADS)

    Forte, A. M.; Glisovic, P.; Rowley, D. B.; Simmons, N. A.; Grand, S. P.; Lu, C.

    2014-12-01

    We present the results of a series of tests that probe the possible existence of compositionally distinct material in the central core of the LLSVPs under the African and Pacific plates using tomography-based mantle flow models that employ several independently-derived viscosity profiles (Mitrovica & Forte 2004, Behn et al. 2004, Steinberger & Calderwood 2006, Forte et al. 2010). We also consider four global tomography models derived from seismic shear velocity data alone (Grand 2002, Panning & Romanowicz 2006, Kustowski et al. 2008, Ritsema et al. 2011). The possible combinations of viscosity and tomography models yield 16 different tests for compositional heterogeneity inside the LLSVPs. In all tests we begin with a mineral physical scaling between lower-mantle shear velocity and density anomalies that assumes thermal effects are dominant everywhere, including within the LLSVPs. We find it is not possible, in any of the tests, to obtain a satisfactory fit to surface geodynamic data, especially the global, long-wavelength gravity anomalies and space-geodetic inferences of excess CMB flattening with a purely thermal interpretation of lower-mantle heterogeneity. If we introduce compositionally-distinct material in the central portions of the LLSVPs, all tests show a notable improvement in the fit to the gravity anomaly and CMB ellipticity data. An optimal reconciliation of the gravity and CMB data is obtained by extending compositional heterogeneity upwards, with maximum-amplitude in the seismic D"-layer and tapering off to negligible values in the mid-mantle. A robust assessment of the dynamical impact of this deeply-rooted compositional heterogeneity is obtained with maps of "mean" convective flow, by averaging the results of all 16 test cases. We find (see map below) dominant lower-mantle upwellings below the axis of the East Pacific Rise (EPR), and under the Caroline Islands in the Western Pacific. Under the African plate we find large-scale upwellings under the

  3. High-Current Gain Two-Dimensional MoS₂-Base Hot-Electron Transistors.

    PubMed

    Torres, Carlos M; Lan, Yann-Wen; Zeng, Caifu; Chen, Jyun-Hong; Kou, Xufeng; Navabi, Aryan; Tang, Jianshi; Montazeri, Mohammad; Adleman, James R; Lerner, Mitchell B; Zhong, Yuan-Liang; Li, Lain-Jong; Chen, Chii-Dong; Wang, Kang L

    2015-12-01

    The vertical transport of nonequilibrium charge carriers through semiconductor heterostructures has led to milestones in electronics with the development of the hot-electron transistor. Recently, significant advances have been made with atomically sharp heterostructures implementing various two-dimensional materials. Although graphene-base hot-electron transistors show great promise for electronic switching at high frequencies, they are limited by their low current gain. Here we show that, by choosing MoS2 and HfO2 for the filter barrier interface and using a noncrystalline semiconductor such as ITO for the collector, we can achieve an unprecedentedly high-current gain (α ∼ 0.95) in our hot-electron transistors operating at room temperature. Furthermore, the current gain can be tuned over 2 orders of magnitude with the collector-base voltage albeit this feature currently presents a drawback in the transistor performance metrics such as poor output resistance and poor intrinsic voltage gain. We anticipate our transistors will pave the way toward the realization of novel flexible 2D material-based high-density, low-energy, and high-frequency hot-carrier electronic applications. PMID:26524388

  4. Assessment of coal gasification/hot gas cleanup based advanced gas turbine systems

    SciTech Connect

    Not Available

    1990-12-01

    The major objectives of the joint SCS/DOE study of air-blown gasification power plants with hot gas cleanup are to: (1) Evaluate various power plant configurations to determine if an air-blown gasification-based power plant with hot gas cleanup can compete against pulverized coal with flue gas desulfurization for baseload expansion at Georgia Power Company's Plant Wansley; (2) determine if air-blown gasification with hot gas cleanup is more cost effective than oxygen-blown IGCC with cold gas cleanup; (3) perform Second-Law/Thermoeconomic Analysis of air-blown IGCC with hot gas cleanup and oxygen-blown IGCC with cold gas cleanup; (4) compare cost, performance, and reliability of IGCC based on industrial gas turbines and ISTIG power island configurations based on aeroderivative gas turbines; (5) compare cost, performance, and reliability of large (400 MW) and small (100 to 200 MW) gasification power plants; and (6) compare cost, performance, and reliability of air-blown gasification power plants using fluidized-bed gasifiers to air-blown IGCC using transport gasification and pressurized combustion.

  5. Nd:YAG Pulsed Laser based flaw imaging techniques for noncontact NDE of an aluminum plate

    NASA Astrophysics Data System (ADS)

    Park, Woong-Ki; Lee, Changgil; Park, Seunghee

    2012-04-01

    Recently, the longitudinal, shear and surface waves have been very widely used as a kind of ultrasonic wave exploration methods to identify internal defects of metallic structures. The ultrasonic wave-based non-destructive testing (NDT) is one of main non-destructive inspection techniques for a health assessment about nuclear power plant, aircraft, ships, and/or automobile manufacturing. In this study, a noncontact pulsed laser-based flaw imaging NDT technique is implemented to detect the damage of a plate-like structure and to identify the location of the damage. To achieve this goal, the Nd:YAG pulsed laser equipment is used to generate a guided wave and scans a specific area to find damage location. The Nd: YAG pulsed laser is used to generate Lamb wave and piezoelectric sensors are installed to measure structural responses. Ann aluminum plate is investigated to verify the effectiveness and the robustness of the proposed NDT approach. A notch is a target to detect, which is inflicted on the surface of an aluminum plate. The damagesensitive features are extracted by comparing the time of flight of the guided wave obtained from an acoustic emission (AE) sensor and make use of the flaw imaging techniques of the aluminum plate.

  6. Hot news recommendation system from heterogeneous websites based on bayesian model.

    PubMed

    Xia, Zhengyou; Xu, Shengwu; Liu, Ningzhong; Zhao, Zhengkang

    2014-01-01

    The most current news recommendations are suitable for news which comes from a single news website, not for news from different heterogeneous news websites. Previous researches about news recommender systems based on different strategies have been proposed to provide news personalization services for online news readers. However, little research work has been reported on utilizing hundreds of heterogeneous news websites to provide top hot news services for group customers (e.g., government staffs). In this paper, we propose a hot news recommendation model based on Bayesian model, which is from hundreds of different news websites. In the model, we determine whether the news is hot news by calculating the joint probability of the news. We evaluate and compare our proposed recommendation model with the results of human experts on the real data sets. Experimental results demonstrate the reliability and effectiveness of our method. We also implement this model in hot news recommendation system of Hangzhou city government in year 2013, which achieves very good results. PMID:25093207

  7. A neural network based artificial vision system for licence plate recognition.

    PubMed

    Draghici, S

    1997-02-01

    This paper presents a neural network based artificial vision system able to analyze the image of a car given by a camera, locate the registration plate and recognize the registration number of the car. The paper describes in detail various practical problems encountered in implementing this particular application and the solutions used to solve them. The main features of the system presented are: controlled stability-plasticity behavior, controlled reliability threshold, both off-line and on-line learning, self assessment of the output reliability and high reliability based on high level multiple feedback. The system has been designed using a modular approach. Sub-modules can be upgraded and/or substituted independently, thus making the system potentially suitable in a large variety of vision applications. The OCR engine was designed as an interchangeable plug-in module. This allows the user to choose an OCR engine which is suited to the particular application and to upgrade it easily in the future. At present, there are several versions of this OCR engine. One of them is based on a fully connected feedforward artificial neural network with sigmoidal activation functions. This network can be trained with various training algorithms such as error backpropagation. An alternative OCR engine is based on the constraint based decomposition (CBD) training architecture. The system has showed the following performances (on average) on real-world data: successful plate location and segmentation about 99%, successful character recognition about 98% and successful recognition of complete registration plates about 80%. PMID:9228583

  8. Waves on Thin Plates: A New (Energy Based) Method on Localization

    NASA Astrophysics Data System (ADS)

    Turkaya, Semih; Toussaint, Renaud; Kvalheim Eriksen, Fredrik; Lengliné, Olivier; Daniel, Guillaume; Grude Flekkøy, Eirik; Jørgen Måløy, Knut

    2016-04-01

    Noisy acoustic signal localization is a difficult problem having a wide range of application. We propose a new localization method applicable for thin plates which is based on energy amplitude attenuation and inversed source amplitude comparison. This inversion is tested on synthetic data using a direct model of Lamb wave propagation and on experimental dataset (recorded with 4 Brüel & Kjær Type 4374 miniature piezoelectric shock accelerometers, 1 - 26 kHz frequency range). We compare the performance of this technique with classical source localization algorithms, arrival time localization, time reversal localization, localization based on energy amplitude. The experimental setup consist of a glass / plexiglass plate having dimensions of 80 cm x 40 cm x 1 cm equipped with four accelerometers and an acquisition card. Signals are generated using a steel, glass or polyamide ball (having different sizes) quasi perpendicular hit (from a height of 2-3 cm) on the plate. Signals are captured by sensors placed on the plate on different locations. We measure and compare the accuracy of these techniques as function of sampling rate, dynamic range, array geometry, signal to noise ratio and computational time. We show that this new technique, which is very versatile, works better than conventional techniques over a range of sampling rates 8 kHz - 1 MHz. It is possible to have a decent resolution (3cm mean error) using a very cheap equipment set. The numerical simulations allow us to track the contributions of different error sources in different methods. The effect of the reflections is also included in our simulation by using the imaginary sources outside the plate boundaries. This proposed method can easily be extended for applications in three dimensional environments, to monitor industrial activities (e.g boreholes drilling/production activities) or natural brittle systems (e.g earthquakes, volcanoes, avalanches).

  9. Adjoint-based optimization for the understanding of the aerodynamics of a flapping plate

    NASA Astrophysics Data System (ADS)

    Wei, Mingjun; Xu, Min

    2015-11-01

    An adjoint-based optimization is applied on a rigid flapping plate and a flexible flapping plate for drag reduction and for propulsive efficiency. Non-cylindrical calculus is introduced to handle the moving boundary. The rigid plate has a combined plunging and pitching motion with incoming flow, the control parameter is the phase delay which is considered first as a constant then as an arbitrary time-varying function. The optimal controls with different cost functions provide different strategies to reach maximum drag reduction or propulsive efficiency. The flexible plate has plunging, pitching, and deformation which is defined by the first two natural modes. With the same optimization goals, the control is instead the amplitude and phase delay of the pitching, the first eigen mode, and the second eigen mode. Similar analyses are taken to understand the conditions for drag reduction and propulsive efficiency when flexibility is involved. It is also shown that the flexibility plays a more important role at lower Reynolds number. Supported by AFOSR.

  10. Superior long-term stability of a glucose biosensor based on inserted barrel plating gold electrodes.

    PubMed

    Hsu, Cheng-Teng; Hsiao, Hung-Chan; Fang, Mei-Yen; Zen, Jyh-Myng

    2009-10-15

    Disposable one shot usage blood glucose strips are routinely used in the diagnosis and management of diabetes mellitus and their performance can vary greatly. In this paper we critically evaluated the long-term stability of glucose strips made of barrel plating gold electrodes. Compared to other glucose biosensing platforms of vapor deposited palladium and screen printed carbon electrodes, the proposed glucose biosensor was found to show the best stability among the three biosensing platforms in thermal acceleration experiments at 40 degrees C for 6 months with an average bias of 3.4% at glucose concentrations of 5-20 mM. The precision test of this barrel plating gold glucose biosensor also showed the best performance (coefficients of variation in the range of 1.4-2.4%) in thermal acceleration experiments at 40 degrees C, 50 degrees C and 70 degrees C for 27 days. Error grid analysis revealed that all measurements fell in zone A and zone B. Regression analysis showed no significant difference between the proposed biosensor and the reference method at 99% confidence level. The amperometric glucose biosensor fabricated by inserting two barrel plating gold electrodes onto an injection-molding plastic base followed by immobilizing with a bio-reagent layer and membrane was very impressive with a long-term stability up to 2.5 years at 25 degrees C. Overall, these results indicated that the glucose oxidase/barrel plating gold biosensing platform is ideal for long-term accurate glycemic control. PMID:19729292

  11. Discovering Plate Boundaries Update: Builds Content Knowledge and Models Inquiry-based Learning

    NASA Astrophysics Data System (ADS)

    Sawyer, D. S.; Pringle, M. S.; Henning, A. T.

    2009-12-01

    Discovering Plate Boundaries (DPB) is a jigsaw-structured classroom exercise in which students explore the fundamental datasets from which plate boundary processes were discovered. The exercise has been widely used in the past ten years as a classroom activity for students in fifth grade through high school, and for Earth Science major and general education courses in college. Perhaps more importantly, the exercise has been used extensively for professional development of in-service and pre-service K-12 science teachers, where it simultaneously builds content knowledge in plate boundary processes (including natural hazards), models an effective data-rich, inquiry-based pedagogy, and provides a set of lesson plans and materials which teachers can port directly into their own classroom (see Pringle, et al, this session for a specific example). DPB is based on 4 “specialty” data maps, 1) earthquake locations, 2) modern volcanic activity, 3) seafloor age, and 4) topography and bathymetry, plus a fifth map of (undifferentiated) plate boundary locations. The jigsaw is structured so that students are first split into one of the four “specialties,” then re-arranged into groups with each of the four specialties to describe the boundaries of a particular plate. We have taken the original DPB materials, used the latest digital data sets to update all the basic maps, and expanded the opportunities for further student and teacher learning. The earthquake maps now cover the recent period including the deadly Banda Aceh event. The topography/bathymetry map now has global coverage and uses ice-free elevations, which can, for example, extend to further inquiry about mantle viscosity and loading processes (why are significant portions of the bedrock surface of Greenland and Antarctica below sea level?). The volcanic activity map now differentiates volcano type and primary volcanic lithology, allowing a more elaborate understanding of volcanism at different plate boundaries

  12. Physics-Based Predictive Simulation Models for Earthquake Generation at Plate Boundaries

    NASA Astrophysics Data System (ADS)

    Matsu'Ura, M.

    2002-12-01

    In the last decade there has been great progress in the physics of earthquake generation; that is, the introduction of laboratory-based fault constitutive laws as a basic equation governing earthquake rupture and the quantitative description of tectonic loading driven by plate motion. Incorporating a fault constitutive law into continuum mechanics, we can develop a physics-based_@simulation model for the entire earthquake generation process. For realistic simulation of earthquake generation, however, we need a very large, high-speed computer system. In Japan, fortunately, the Earth Simulator, which is a high performance, massively parallel-processing computer system with 10 TB memories and 40 TFLOPS peak speed, has been completed. The completion of the Earth Simulator and advance in numerical simulation methodology are bringing our vision within reach. In general, the earthquake generation cycle consists of tectonic loading due to relative plate motion, quasi-static rupture nucleation, dynamic rupture propagation and stop, and restoration of fault strength. The basic equations governing the entire earthquake generation cycle consists of an elastic/viscoelastic slip-response function that relates fault slip to shear stress change and a fault constitutive law that prescribes change in shear strength with fault slip and contact time. The shear stress and the shear strength are related with each other through the boundary conditions on the fault. The driving force of this system is observed relative plate motion. The system to describe the earthquake generation cycle is conceptually quite simple. The complexity in practical modelling mainly comes from complexity in structure of the real earth. Since 1998 our group have conducted the Crustal Activity Modelling Program (CAMP), which is one of the three main programs composing the Solid Earth Simulator project. The aim of CAMP is to develop a physics-based predictive simulation model for the entire earthquake generation

  13. KFC2: a knowledge-based hot spot prediction method based on interface solvation, atomic density, and plasticity features.

    PubMed

    Zhu, Xiaolei; Mitchell, Julie C

    2011-09-01

    Hot spots constitute a small fraction of protein-protein interface residues, yet they account for a large fraction of the binding affinity. Based on our previous method (KFC), we present two new methods (KFC2a and KFC2b) that outperform other methods at hot spot prediction. A number of improvements were made in developing these new methods. First, we created a training data set that contained a similar number of hot spot and non-hot spot residues. In addition, we generated 47 different features, and different numbers of features were used to train the models to avoid over-fitting. Finally, two feature combinations were selected: One (used in KFC2a) is composed of eight features that are mainly related to solvent accessible surface area and local plasticity; the other (KFC2b) is composed of seven features, only two of which are identical to those used in KFC2a. The two models were built using support vector machines (SVM). The two KFC2 models were then tested on a mixed independent test set, and compared with other methods such as Robetta, FOLDEF, HotPoint, MINERVA, and KFC. KFC2a showed the highest predictive accuracy for hot spot residues (True Positive Rate: TPR = 0.85); however, the false positive rate was somewhat higher than for other models. KFC2b showed the best predictive accuracy for hot spot residues (True Positive Rate: TPR = 0.62) among all methods other than KFC2a, and the False Positive Rate (FPR = 0.15) was comparable with other highly predictive methods. PMID:21735484

  14. On a simple triangular Reissner/Mindlin plate element based on incompatible modes and discrete constraints

    NASA Astrophysics Data System (ADS)

    Batoz, Jean-Louis; Katili, Irwan

    1992-11-01

    In this paper the formulation of a new triangular element based on the Reissner/Mindlin plate theory is presented. The element has three nodes and three d.o.f. per node only. It is based on constant bending modes plus incompatible energy orthogonal higher order bending modes. The transverse shear effects are represented using the moment equilibrium and the constitutive equations. Discrete (collocation) shear constraints are considered on each side to relate the kinematical and the independent shear strains. The element has a proper rank, is completely locking free, passes all constant patch-tests exactly. The detailed numerical evaluation shows that the element, called DST-BK, is a robust and high-performance element for thick and thin plates.

  15. Measurements of strain at plate boundaries using space based geodetic techniques

    NASA Technical Reports Server (NTRS)

    Robaudo, Stefano; Harrison, Christopher G. A.

    1993-01-01

    We have used the space based geodetic techniques of Satellite Laser Ranging (SLR) and VLBI to study strain along subduction and transform plate boundaries and have interpreted the results using a simple elastic dislocation model. Six stations located behind island arcs were analyzed as representative of subduction zones while 13 sites located on either side of the San Andreas fault were used for the transcurrent zones. The length deformation scale was then calculated for both tectonic margins by fitting the relative strain to an exponentially decreasing function of distance from the plate boundary. Results show that space-based data for the transcurrent boundary along the San Andreas fault help to define better the deformation length scale in the area while fitting nicely the elastic half-space earth model. For subduction type bonndaries the analysis indicates that there is no single scale length which uniquely describes the deformation. This is mainly due to the difference in subduction characteristics for the different areas.

  16. HotEye (tm) Based Coordinate Measuring Machine for Forging Industry

    SciTech Connect

    OG Technologies

    2003-06-09

    The objective of this project is to develop a 3 dimensional measurement system for the domestic forging industry based on HotEye{trademark}. This technology will allow high definition camera to accurately image a red hot object. The project marries conventional Coordinate Measurement Machine ''CMM'' technology to HotEye{trademark} technology to permit the accurate measurement of forged parts while they are at high temperature. Being able to take such measurements will dramatically reduce the amount of scrap produced by the domestic forging industry. This industry wastes a significant amount of energy because of the high rate of scrap it produces. OGT will: (1) Develop a 3D measurement sensor head that will work on a part at a temperature up to 1,450 C with an accuracy of 0.1mm or better and with a scanning speed of less than 10 seconds for an area of 100mm x 100mm. (2) Develop a Virtual-Fixturing software package to alleviate the need of precise hard fixturing. (3) Integrate the 3D measurement sensor head and the Virtual-Fixturing software into a standard CMM, both hardware (replacing the probes) and software (data format and user interface match) so that the system can automatically perform a complete preprogrammed measurement of a hot product. (4) Test and evaluate the system in a forging facility.

  17. Investigation on the effect of MR elastomer based adaptive vibration absorbers on the radiated sound from circular elastic plates

    NASA Astrophysics Data System (ADS)

    Hemmatian, M.; Sedaghati, R.

    2016-04-01

    This study aims to investigate the effect of using magnetorheological elastomer (MRE)-based adaptive tuned vibration absorbers (ATVA) on the sound transmission in an elastic plate. Sound transmission loss (STL) of an elastic circular thin plate is analytically studied. The plate is excited by a plane acoustic wave as an incident sound and the displacement of the plate is calculated using corresponding mode shapes of the system for clamped boundary condition. Rayleigh integral approach is used to express the transmitted sound pressure in terms of the plate's displacement modal amplitude. In order to increase sound transmission loss of the plate, the MRE-based ATVA is considered. The basic idea is to be able to change the stiffness of the ATVA by varying magnetic field in order to reduce the transmitted acoustic energy of the host structure in a wide frequency range. Here, a MRE-based ATVA under the shear mode consisting of an oscillator mass, magnetic conductor, coils and MRE is investigated. In order to predict the viscoelastic characteristics of the field-dependent MRE based on the applied magnetic field, the double pole model is used. Finally, MRE-based ATVAs are integrated with the plate to absorb the plate energy with the aim of decreasing the transmitted sound power. Results show that plate with integrated MRE-based ATVAs suppresses the axisymmetric vibration of the plate and thus considerably improves the STL. Parametric studies on the influence of the position of MRE-based ATVAs and the effects of applied current on their performance are also presented.

  18. Fabrication and characterization of monolithically integrated microchannel plates based on amorphous silicon

    PubMed Central

    Franco, Andrea; Geissbühler, Jonas; Wyrsch, Nicolas; Ballif, Christophe

    2014-01-01

    Microchannel plates are vacuum-based electron multipliers for particle—in particular, photon— detection, with applications ranging from image intensifiers to single-photon detectors. Their key strengths are large signal amplification, large active area, micrometric spatial resolution and picosecond temporal resolution. Here, we present the first microchannel plate made of hydrogenated amorphous silicon (a-Si:H) instead of lead glass. The breakthrough lies in the possibility of realizing amorphous silicon-based microchannel plates (AMCPs) on any kind of substrate. This achievement is based on mastering the deposition of an ultra-thick (80–120 μm) stress-controlled a-Si:H layer from the gas phase at temperatures of about 200°C and micromachining the channels by dry etching. We fabricated AMCPs that are vertically integrated on metallic anodes of test structures, proving the feasibility of monolithic integration of, for instance, AMCPs on application-specific integrated circuits for signal processing. We show an electron multiplication factor exceeding 30 for an aspect ratio, namely channel length over aperture, of 12.5:1. This result was achieved for input photoelectron currents up to 100 pA, in the continuous illumination regime, which provides a first evidence of the a-Si:H effectiveness in replenishing the electrons dispensed in the multiplication process. PMID:24698955

  19. Reevaluation of plate motion models based on hotspot tracks in the Atlantic and Indian Oceans

    SciTech Connect

    Baksi, A.K.

    1999-01-01

    Plate motion models based on hotspot tracks in the Atlantic and Indian Oceans predict minimal movement (less than a few millimeters per year) between these hotspots and their counterparts in the Pacific Ocean for the past {approximately}100 m.yr., whereas plate circuit exercises indicate relative motions of {approximately}20 mm/yr. Hotspot-based models also suggest that the Rajmahal Traps, India, were located {approximately}1,000 km away from the Kerguelen hotspot at {approximately}115 Ma, and the Deccan Traps, India, were located a similar distance from the Reunion hotspot at {approximately}65 Ma; this is at odds with conclusions derived from paleomagnetism, plate circuits, and geochemical parameters that suggest a genetic link between flood basalt provinces in India and hotspots in the Indian Ocean. These divergent views may be explained by plume action {approximately}1,000 km from its center or errors in the hotspot motion models. The latter hypothesis is scrutinized in this article by examination of the radiometric ages for hotspot tracks in the Atlantic and Indian Oceans. The {sup 40}/{sup 39}Ar step-heating data for rocks defining the tracks of the Reunion and Kerguelen hotspots in the Indian Ocean and the Great Metero and Tristan da Cunha hotspots in the Atlantic Ocean are critically reexamined. Of {approximately}35 such ages utilized for deriving plate motion models for the past 130 m.yr., at best, only three ({approximately}32, {approximately}50, and {approximately}52 Ma) in the Indian Ocean and one ({approximately}65 Ma) for the Atlantic Ocean may be treated as crystallization ages. Conclusions based on hotspot track modeling for Late Cretaceous to Eocene time are suspect, and those for the Early to Late Cretaceous period are untenable. In the absence of precise age data for the tracks of hotspots in the Atlantic and Indian Oceans, and inconsistent age progressions noted within a single volcanic chain, plate circuit models serve as the superior technique

  20. Generalized Constitutive-Based Theoretical and Empirical Models for Hot Working Behavior of Functionally Graded Steels

    NASA Astrophysics Data System (ADS)

    Vanini, Seyed Ali Sadough; Abolghasemzadeh, Mohammad; Assadi, Abbas

    2013-07-01

    Functionally graded steels with graded ferritic and austenitic regions including bainite and martensite intermediate layers produced by electroslag remelting have attracted much attention in recent years. In this article, an empirical model based on the Zener-Hollomon (Z-H) constitutive equation with generalized material constants is presented to investigate the effects of temperature and strain rate on the hot working behavior of functionally graded steels. Next, a theoretical model, generalized by strain compensation, is developed for the flow stress estimation of functionally graded steels under hot compression based on the phase mixture rule and boundary layer characteristics. The model is used for different strains and grading configurations. Specifically, the results for αβγMγ steels from empirical and theoretical models showed excellent agreement with those of experiments of other references within acceptable error.

  1. X-ray imaging plate performance investigation based on a Monte Carlo simulation tool

    NASA Astrophysics Data System (ADS)

    Yao, M.; Duvauchelle, Ph.; Kaftandjian, V.; Peterzol-Parmentier, A.; Schumm, A.

    2015-01-01

    Computed radiography (CR) based on imaging plate (IP) technology represents a potential replacement technique for traditional film-based industrial radiography. For investigating the IP performance especially at high energies, a Monte Carlo simulation tool based on PENELOPE has been developed. This tool tracks separately direct and secondary radiations, and monitors the behavior of different particles. The simulation output provides 3D distribution of deposited energy in IP and evaluation of radiation spectrum propagation allowing us to visualize the behavior of different particles and the influence of different elements. A detailed analysis, on the spectral and spatial responses of IP at different energies up to MeV, has been performed.

  2. Mechanism of beneficial effect of tantalum in hot corrosion of nickel-base superalloys

    NASA Technical Reports Server (NTRS)

    Fryburg, G. C.; Stearns, C. A.; Kohl, F. J.

    1977-01-01

    X-ray diffraction and electron microprobe analyses were used to examine a prominent NaTaO3 pattern formed in a number of nickel-base superalloys. It is found that a beneficial effect of tantalum with respect to hot corrosion attack arises from the ability of Ta2O5 to tie up Na2O and prevent the formation of a molten Na2MoO4 phase.

  3. Miniaturization of mitotic index cell-based assay using "wall-less" plate technology.

    PubMed

    Le Guezennec, Xavier; Phong, Mark; Nor, Liyana; Kim, Namyong

    2014-03-01

    The use of microscopic imaging for the accurate assessment of cells in mitosis is hampered by the round morphology of mitotic cells, which renders them poorly adherent and highly susceptible to loss during the washing stage of cell-based assays. Here, to circumvent these limitations, we make use of DropArray, a recent technology that allows high retention of weakly adherent cells and suspension cells. DropArray offers the competitive advantage of maintaining the classic high throughput format of microtiter plates while reducing classic microwell volume by up to 90% by using a drop format. Here, we present a mitotic index cell-based assay using the mitosis marker phospho histone H3 at serine 10 on a DropArray 384-well plate format. Dose-response curve analysis of the mitotic index assay with an antimitotic drug (docetaxel) on DropArray is presented that shows an effective dosage compared to previous established results similar to those obtained with conventional microtiter plates. The mitotic index assay with DropArray showed a Z-factor >0.6. Our results validate DropArray as a suitable platform for high throughput screening for compounds affecting mitosis or the cell cycle. PMID:24611478

  4. Electrodeposited Fe-Co films prepared from a citric-acid-based plating bath

    NASA Astrophysics Data System (ADS)

    Yanai, T.; Uto, H.; Shimokawa, T.; Nakano, M.; Fukunaga, H.; Suzuki, K.

    2013-06-01

    Electrodeposited Fe-Co films are commonly prepared in a boric-acid-based bath. In this research, we applied citric acid instead of boric acid for the plating of Fe-Co films because boron in the waste bath is restricted by environmental-protection regulations in Japan. We evaluated the effect of citric acid on the magnetic and structural properties of the films. The saturation magnetization of the Fe-Co films slightly increased while the Fe content in the Fe-Co films decreased with increasing citric acid concentration. The lowest coercivity value of 240 A/m was obtained at a citric acid concentration of 100 g/L. The plating bath with this citric acid concentration enabled us to obtain Fe-Co films with high saturation magnetizations and smooth surface morphologies.

  5. Performance evaluation of dual-frequency driving plate ultrasonic motor based on an analytical model.

    PubMed

    Pang, Yafei; Yang, Ming; Chen, Xuying; He, Wei; Li, Shiyang; Li, Chaodong

    2011-08-01

    An analytical model is presented to explain the effects of dual-frequency drive on the plate ultrasonic motor in this paper. The experimental prototype is a plate ultrasonic motor using single-phase asymmetric excitation, which can work under a single vibration or multiple vibration modes. Based on the linear superposition of vibrations with two different excitation frequencies, an analytical model is established using the classic Coulomb friction model, and the non-load rotation speed and maximum stall torque are deduced. Moreover, some crucial parameters such as preload and dead-zone in dual-frequency superposition model are identified or modified automatically by searching for the maximum correlation coefficient between simulation and experimental data using single-frequency drive. It is found that simulation and experiment results agree well when no excitation frequency component is at resonance. PMID:21859583

  6. Chip-based optical microscopy for imaging membrane sieve plates of liver scavenger cells

    NASA Astrophysics Data System (ADS)

    Helle, Øystein I.; Øie, Cristina I.; McCourt, Peter; Ahluwalia, Balpreet S.

    2015-08-01

    The evanescent field on top of optical waveguides is used to image membrane network and sieve-plates of liver endothelial cells. In waveguide excitation, the evanescent field is dominant only near the surface (~100-150 nm) providing a default optical sectioning by illuminating fluorophores in close proximity to the surface and thus benefiting higher signal-to-noise ratio. The sieve plates of liver sinusoidal endothelial cells are present on the cell membrane, thus near-field waveguide chip-based microscopy configuration is preferred over epi-fluorescence. The waveguide chip is compatible with optical fiber components allowing easy multiplexing to different wavelengths. In this paper, we will discuss the challenges and opportunities provided by integrated optical microscopy for imaging cell membranes.

  7. Calibration of a microchannel plate based extreme ultraviolet grazing incident spectrometer at the Advanced Light Source.

    PubMed

    Bakeman, M S; van Tilborg, J; Sokollik, T; Baum, D; Ybarrolaza, N; Duarte, R; Toth, C; Leemans, W P

    2010-10-01

    We present the design and calibration of a microchannel plate based extreme ultraviolet spectrometer. Calibration was performed at the Advance Light Source (ALS) at the Lawrence Berkeley National Laboratory (LBNL). This spectrometer will be used to record the single shot spectrum of radiation emitted by the tapered hybrid undulator (THUNDER) undulator installed at the LOASIS GeV-class laser-plasma-accelerator. The spectrometer uses an aberration-corrected concave grating with 1200 lines/mm covering 11-62 nm and a microchannel plate detector with a CsI coated photocathode for increased quantum efficiency in the extreme ultraviolet. A touch screen interface controls the grating angle, aperture size, and placement of the detector in vacuum, allowing for high-resolution measurements over the entire spectral range. PMID:21034012

  8. Extended Kalman Filter Based Neural Networks Controller For Hot Strip Rolling mill

    NASA Astrophysics Data System (ADS)

    Moussaoui, A. K.; Abbassi, H. A.; Bouazza, S.

    2008-06-01

    The present paper deals with the application of an Extended Kalman filter based adaptive Neural-Network control scheme to improve the performance of a hot strip rolling mill. The suggested Neural Network model was implemented using Bayesian Evidence based training algorithm. The control input was estimated iteratively by an on-line extended Kalman filter updating scheme basing on the inversion of the learned neural networks model. The performance of the controller is evaluated using an accurate model estimated from real rolling mill input/output data, and the usefulness of the suggested method is proved.

  9. Extended Kalman Filter Based Neural Networks Controller For Hot Strip Rolling mill

    SciTech Connect

    Moussaoui, A. K.; Abbassi, H. A.; Bouazza, S.

    2008-06-12

    The present paper deals with the application of an Extended Kalman filter based adaptive Neural-Network control scheme to improve the performance of a hot strip rolling mill. The suggested Neural Network model was implemented using Bayesian Evidence based training algorithm. The control input was estimated iteratively by an on-line extended Kalman filter updating scheme basing on the inversion of the learned neural networks model. The performance of the controller is evaluated using an accurate model estimated from real rolling mill input/output data, and the usefulness of the suggested method is proved.

  10. Study on load relaxation based on hot bending and sizing of Ti6Al4V alloy sheet

    NASA Astrophysics Data System (ADS)

    Po, Liu; Yingying, Zong; Debin, Shan; Bin, Guo

    2013-05-01

    The mechanism of hot sizing following sheet thermal forming of titanium alloy is considered as stress relaxation based on creep flow. A certain amount of internal stress in sheet metal parts can be relaxed during hot-sizing stage and hence the springback can be markedly reduced. Hot v-bending of Ti6Al4V sheet were carried out to study the behavior of load relaxation and springback in specimens after hot sizing, also known as shape retention. Experimental results reveal that load relaxation occurs during hot sizing following sheet v-bending. Reduction of springback angle obtained using hot sizing is obviously larger than that obtained without hot sizing under the same thermal environment. During hot sizing, springback angle decreases with increase in temperature and time, respectively. Load relaxation behavior is affected by loading method, namely constant velocity and two step loading. The linear relation between creep rate and load relaxation rate was deduced in hot-sizing stage. The calculated ratio shows good agreement with experimental data obtained by two-step loading. V-bending and sizing together with appropriate loading method are demonstrated as a good approach for stress relaxation analysis.

  11. Seismic Probing of the Base of a Tectonic Plate from Subduction Zone to Trench Outer Rise: Hikurangi Margin, New Zealand

    NASA Astrophysics Data System (ADS)

    Louie, J. N.; Kent, G. M.; Lamb, S. H.; Savage, M. K.; Stern, T. A.; Stratford, W. R.

    2015-12-01

    The nature of the base of a tectonic plate (LAB) is the 3rd dimension of plate tectonics. Recent seismic studies of the LAB have revealed planar features that show very different characteristics. In the oceans, the top of the S-wave low velocity zone shows a systematic deepening with plate age that fits plate-cooling models. However, the change in radial anisotropy has a markedly constant depth of ~70 km, regardless of plate age. A recent land-based study (SAHKE 2) of the subducted Pacific Plate in the southern Hikurangi margin has imaged a pair of distinct reflectors defining a ~10 km thick channel parallel to and ~70 km below the top of the ~15° dipping plate. Low velocities indicate that the channel is a zone of partial melt or high volatile content, acting as a weak base to the plate. Receiver function studies along the Japan margin have also imaged layers at these depths, parallel to the top of the plate and dipping up to 45°. We propose probing the base of the tectonic plate by tracing potential LAB seismic reflectors from their dipping portions in the subduction zone to where they bend in the trench outer rise. If the seismically identified boundary represents a 'frozen-in' feature, created at the mid ocean ridge, then it will remain parallel to the top of the plate, and its nature will remain unchanged as it is tracked over the outer rise. Alternatively, if the base of the plate is a thin channel of partial melt, then one would expect thickening of the channel beneath the outer rise due to melt ponding in the core of the flexure; this melt ponding may be the source of volcanic activity. A 500-km survey will trace the Pacific plate LAB from the subduction zone into the trench outer rise. The deeper part of the line coincides with the part of the plate where the ~10 km thick 'melt' channel was clearly imaged with the SAHKE 2 experiment. We show with synthetic experiments that given seismic energy scatter and attenuation comparable to that observed in the

  12. Physical Simulation of Friction Stir Welding and Processing of Nickel-Base Alloys Using Hot Torsion

    NASA Astrophysics Data System (ADS)

    Rule, James R.; Lippold, John C.

    2013-08-01

    The Gleeble hot torsion test was utilized in an attempt to simulate the friction stir-processed microstructure of three Ni-base alloys: Hastelloy X, Alloy 625, and Alloy 718. The simulation temperatures were based on actual thermal cycles measured by embedded thermocouples during friction stir processing of these alloys. Peak process temperatures were determined to be approximately 1423 K (1150 °C) for Hastelloy X and Alloy 625 K and 1373 K (352 °C and 1100 °C) for Alloy 718. The peak temperature and cooling rates were programed into the Gleeble™ 3800 thermo-mechanical simulator to reproduce the stir zone and thermo-mechanically affected zone (TMAZ) microstructures. The TMAZ was successfully simulated using this technique, but the stir zone microstructure could not be accurately reproduced, with hot torsion samples exhibiting larger grain size than actual friction stir processing trials. Shear stress and strain rates as a function of temperature were determined for each material using hot torsion simulation.

  13. Hot Workability of CuZr-Based Shape Memory Alloys for Potential High-Temperature Applications

    NASA Astrophysics Data System (ADS)

    Biffi, Carlo Alberto; Tuissi, Ausonio

    2014-07-01

    The research on high-temperature shape memory alloys has been growing because of the interest of several potential industrial fields, such as automotive, aerospace, mechanical, and control systems. One suitable candidate is given by the CuZr system, because of its relative low price in comparison with others, like the NiTi-based one. In this context, the goal of this work is the study of hot workability of some CuZr-based shape memory alloys. In particular, this study addresses on the effect of hot rolling process on the metallurgical and calorimetric properties of the CuZr system. The addition of some alloying elements (Cr, Co, Ni, and Ti) is taken into account and their effect is also put in comparison with each other. The alloys were produced by means of an arc melting furnace in inert atmosphere under the shape of cigars. Due to the high reactivity of these alloys at high temperature, the cigars were sealed in a stainless steel can before the processing and two different procedures of hot rolling were tested. The characterization of the rolled alloys is performed using discrete scanning calorimetry in terms of evolution of the martensitic transformation and scanning electron microscopy for the microstructural investigations. Additionally, preliminary tests of laser interaction has been also proposed on the alloy more interesting for potential applications, characterized by high transformation temperatures and its good thermal stability.

  14. Hybrid Semiloof elements for plates and shells based upon a modified Hu-Washizu principle

    NASA Technical Reports Server (NTRS)

    Pian, T. H. H.; Sumihara, K.

    1984-01-01

    Hybrid SemiLoof elements for plates and shells are developed based upon modified Hu-Washizu principle. In the new version of the assumed stress hybrid formulation the equilibrium equations are satisfied through the introduction of internal displacement parameters as Lagrange multipliers. The inversion of the resulting H-matrices is simplified particularly when the stresses are expressed in terms of natural coordinates. A 24-DOF triangular element and a 32-DOF quadrilateral element based on shallow shell theory are derived and evaluated.

  15. Boattail Plates With Non-Rectangular Geometries For Reducing Aerodynamic Base Drag Of A Bluff Body In Ground Effect

    DOEpatents

    Ortega, Jason M.; Sabari, Kambiz

    2006-03-07

    An apparatus for reducing the aerodynamic base drag of a bluff body having a leading end, a trailing end, a top surface, opposing left and right side surfaces, and a base surface at the trailing end substantially normal to a longitudinal centerline of the bluff body, with the base surface joined (1) to the left side surface at a left trailing edge, (2) to the right side surface at a right trailing edge, and (3) to the top surface at a top trailing edge. The apparatus includes left and right vertical boattail plates which are orthogonally attached to the base surface of the bluff body and inwardly offset from the left and right trailing edges, respectively. This produces left and right vertical channels which generate, in a flowstream substantially parallel to the longitudinal centerline, respective left and right vertically-aligned vortical structures, with the left and right vertical boattail plates each having a plate width defined by a rear edge of the plate spaced from the base surface. Each plate also has a peak plate width at a location between top and bottom ends of the plate corresponding to a peak vortex of the respective vertically-aligned vortical structures.

  16. Hot coal gas desulfurization with manganese-based sorbents. Final report, September 1992--December 1994

    SciTech Connect

    Hepworth, M.T.; Slimane, R.B.

    1994-11-01

    The focus of much current work being performed by the Morgantown Energy Technology Center (METC) of the Department of Energy on hot coal-derived fuel gas desulfurization is in the use of zinc-based sorbents. METC has shown interest in formulating and testing manganese-based pellets as alternative effective sulfur sorbents in the 700 to 1200{degree}C temperature range. To substantiate the potential superiority of Mn-based pellets, a systematic approach toward the evaluation of the desulfurizing power of single-metal sorbents is developed based on thermodynamic considerations. This novel procedure considered several metal-based sorbents and singled out manganese oxide as a prime candidate sorbent capable of being utilized under a wide temperature range, irrespective of the reducing power (determined by CO{sub 2}/CO ratio) of the fuel gas. Then, the thermodynamic feasibility of using Mn-based pellets for the removal of H{sub 2}S from hot-coal derived fuel gases, and the subsequent oxidative regeneration of loaded (sulfided) pellets was established. It was concluded that MnO is the stable form of manganese for virtually all commercially available coal-derived fuel gases. In addition, the objective of reducing the H{sub 2}S concentration below 150 ppMv to satisfy the integrated gasification combined cycle system requirement was shown to be thermodynamically feasible. A novel process is developed for the manufacture of Mn-based spherical pellets which have the desired physical and chemical characteristics required.

  17. Effective microwell plate-based screening method for microbes producing cellulase and xylanase and its application.

    PubMed

    Kim, Jennifer Jooyoun; Kwon, Young-Kyung; Kim, Ji Hyung; Heo, Soo-Jin; Lee, Youngdeuk; Lee, Su-Jin; Shim, Won-Bo; Jung, Won-Kyo; Hyun, Jung-Ho; Kwon, Kae Kyoung; Kang, Do-Hyung; Oh, Chulhong

    2014-11-28

    Cellulase and xylanase are main hydrolysis enzymes for the degradation of cellulosic and hemicellulosic biomass, respectively. In this study, our aim was to develop and test the efficacy of a rapid, high-throughput method to screen hydrolytic-enzyme-producing microbes. To accomplish this, we modified the 3,5-dinitrosalicylic acid (DNS) method for microwell plate-based screening. Targeted microbial samples were initially cultured on agar plates with both cellulose and xylan as substrates. Then, isolated colonies were subcultured in broth media containing yeast extract and either cellulose or xylan. The supernatants of the culture broth were tested with our modified DNS screening method in a 96-microwell plate, with a 200 μl total reaction volume. In addition, the stability and reliability of glucose and xylose standards, which were used to determine the enzymatic activity, were studied at 100°C for different time intervals in a dry oven. It was concluded that the minimum incubation time required for stable color development of the standard solution is 20 min. With this technique, we successfully screened 21 and 31 cellulase- and xylanase-producing strains, respectively, in a single experimental trial. Among the identified strains, 19 showed both cellulose and xylan hydrolyzing activities. These microbes can be applied to bioethanol production from cellulosic and hemicellulosic biomass. PMID:25085570

  18. Guided-wave-based detections of weld and crack in steel plates

    NASA Astrophysics Data System (ADS)

    Lu, Mingyu; Lu, Xi; Zhou, Limin; Su, Zhongqing; Ye, Lin

    2009-07-01

    The guided-wave-based damage detection techniques using structurally integrated Lead-zirconate-titanate (PZT) patches for structural health monitoring (SHM) have been developed for many years. However, the method is still in its formative years and one of the main challenges is the application in real-word complicated structures. It's very important to widely study the techniques in the structures with simple geometries which can be used to construct more complicated structures for practical applications. In this paper, different steel plates of the same dimensions were used for detecting a 2mm-gap through-crack in welded zone and studying the effects of different impurities such as water, alcohol, epoxy and mud in the crack on wave propagations. Advanced signal processing and pattern recognition techniques such as the wavelet transform (WT) especially continuous wavelet transform (CWT) and Hilbert transform (HT) were used to enhance the efficiency of damage detections in the steel plates. Some simulation results were obtained to validate of experimental results. The results from both the experiments and simulations show the validity of the proposed method and the effects of different factors on the damage detection of the steel plates.

  19. Imaging-based optical caliper for objects in hot manufacturing processes

    SciTech Connect

    Huang, Howard

    2013-04-03

    OG Technologies, Inc. (OGT), in conjunction with its industrial and academic partners, proposes to develop an Imaging-Based Optical Caliper (hereafter referred to as OC) for Objects in Hot Manufacturing Processes. The goal is to develop and demonstrate the OC with the synergy of OGT's current technological pool and other innovations to provide a light weight, robust, safe and accurate portable dimensional measurement device for hot objects with integrated wireless communication capacity to enable real time process control. The technical areas of interest in this project are the combination of advanced imaging, Sensor Fusion, and process control. OGT believes that the synergistic interactions between its current set of technologies and other innovations could deliver products that are viable and have high impact in the hot manufacture processes, such as steel making, steel rolling, open die forging, and glass industries, resulting in a new energy efficient control paradigm in the operations through improved yield, prolonged tool life and improved quality. In-line dimension measurement and control is of interest to the steel makers, yet current industry focus is on the final product dimension only instead of whole process due to the limit of man power, system cost and operator safety concerns. As sensor technologies advances, the industry started to see the need to enforce better dimensional control throughout the process, but lack the proper tools to do so. OGT along with its industrial partners represent the indigenous effort of technological development to serve the US steel industry. The immediate market that can use and get benefited from the proposed OC is the Steel Industry. The deployment of the OC has the potential to provide benefits in reduction of energy waste, CO2 emission, waste water amount, toxic waste, and so forth. The potential market after further expended function includes Hot Forging and Freight Industries. The OC prototypes were fabricated, and

  20. Effects of cobalt on the hot workability of nickel-base superalloys

    NASA Technical Reports Server (NTRS)

    Jarrett, R. N.; Collier, J. P.; Tien, J. K.

    1984-01-01

    The effect of cobalt on the workability of nickel-base superalloys is examined with reference to experimental results for four heats of alloys based on the Nimonic 115 composition with varying amounts of nickel substituted for the nominal 14 percent cobalt. It is shown that Co lowers the gamma-prime solvus, which in turn lowers the Cr23C6 carbide solvus. It is further shown that these solvus temperatures bracket the hot working range for the alloys. However, thermomechanical processing modifications reflecting the effect of Co on the gamma-prime and carbide solvi are shown to restore the workability and the properties of alloys with little or no cobalt.

  1. Image cloning beyond diffraction based on coherent population trapping in a hot rubidium vapor.

    PubMed

    Ding, Dong-Sheng; Zhou, Zhi-Yuan; Shi, Bao-Sen

    2014-01-15

    Following recent theoretical predictions, we report on an experimental realization of image cloning beyond usual diffraction, through the coherent population trapping (CPT) effect in a hot rubidium vapor. In our experiment, an alphabet letter image was transferred from a coupling field to a probe field, based on the CPT effect. Furthermore, we demonstrate that the cloned probe field carrying the image is transmitted without the usual diffraction. To our best knowledge, this is the first experimental report about image cloning beyond diffraction. We believe this mechanism, based on CPT, has definite and important applications in image metrology, image processing, and biomedical imaging. PMID:24562116

  2. Burner Rig Hot Corrosion of Five Ni-Base Alloys Including Mar-M247

    NASA Technical Reports Server (NTRS)

    Nesbitt, James A.; Helmink, R.; Harris, K.; Erickson, G.

    2000-01-01

    The hot corrosion resistance of four new Ni-base superalloys was compared to that of Mar-M247 by testing in a Mach 0.3 burner rig at 900 C for 300 1-hr cycles. While the Al content was held the same as in the Mar-M247, the Cr and Co levels in the four new alloys were decreased while other strengthening elements (Re, Ta) were increased. Surprisingly, despite their lower Cr and Co contents, the hot corrosion behavior of all four new alloys was superior to that of the Mar-M247 alloy. The Mar-M247 alloy began to lose weight almost immediately whereas the other four alloys appeared to undergo an incubation period of 50-150 1-hr cycles. Examination of the cross-sectional microstructures showed regions of rampant corrosion attack (propagation stage) in all five alloys after 300 1-hr cycles . This rampant corrosion morphology was similar for each of the alloys with Ni and Cr sulfides located in an inner subscale region. The morphology of the attack suggests a classic "Type I", or high temperature, hot corrosion attack.

  3. DEVELOPMENT OF A CALCIUM-BASED SORBENT FOR HOT GAS CLEANUP

    SciTech Connect

    T.D. Wheelock; L.K. Doraiswamy; K. Constant

    1999-10-01

    The development and testing of potential calcium-based sorbents for hot gas cleanup continued. One of the most promising materials combines powdered limestone and a calcium aluminate cement by two step pelletization followed by steam curing. Reasonably strong pellets are produced with good adsorption characteristics by incorporating 20 wt.% cement in the core and 40 wt.% cement in the shell. The resulting 4.76 mm diameter pellets are capable of withstanding a crushing force approaching 11.5 N/mm before breaking and are also capable of removing H{sub 2}S from dilute, hot gas streams. The pellets are also regenerable and reusable. Another promising material combines calcium carbonate powder and finely ground calcined alumina in tablet form. The small tablets are prepared by mixing the materials with water to form a thick paste which is then molded and dried. The tablets are hardened by calcining at either 1000 to 1100 C. The resulting tablets are strong and capable of removing H{sub 2}S from a dilute, hot gas stream.

  4. Prediction of Proper Temperatures for the Hot Stamping Process Based on the Kinetics Models

    NASA Astrophysics Data System (ADS)

    Samadian, P.; Parsa, M. H.; Mirzadeh, H.

    2015-02-01

    Nowadays, the application of kinetics models for predicting microstructures of steels subjected to thermo-mechanical treatments has increased to minimize direct experimentation, which is costly and time consuming. In the current work, the final microstructures of AISI 4140 steel sheets after the hot stamping process were predicted using the Kirkaldy and Li kinetics models combined with new thermodynamically based models in order for the determination of the appropriate process temperatures. In this way, the effect of deformation during hot stamping on the Ae3, Acm, and Ae1 temperatures was considered, and then the equilibrium volume fractions of phases at different temperatures were calculated. Moreover, the ferrite transformation rate equations of the Kirkaldy and Li models were modified by a term proposed by Åkerström to consider the influence of plastic deformation. Results showed that the modified Kirkaldy model is satisfactory for the determination of appropriate austenitization temperatures for the hot stamping process of AISI 4140 steel sheets because of agreeable microstructure predictions in comparison with the experimental observations.

  5. In vitro evaluation of the antifungal efficacy of poloxamer 407-based formulations in an infected nail plate model.

    PubMed

    Täuber, Anja; Müller-Goymann, Christel C

    2016-05-30

    The in vitro efficacy of poloxamer 407-based formulations with antifungal ciclopirox olamine has been analysed in an infected nail plate model. As artificial nail plates, keratin films made of human hair keratin and slices from bovine hooves have been utilised. Several poloxamer 407-based formulations with 1 % active ingredient indicated complete growth inhibition of the dermatophyte fungus Trichophyton rubrum after 6days of incubation. PMID:26992819

  6. One-dimensional plate impact experiments on the cyclotetramethylene tetranitramine (HMX) based explosive EDC32

    NASA Astrophysics Data System (ADS)

    Burns, Malcolm J.; Gustavsen, Richard L.; Bartram, Brian D.

    2012-09-01

    Eight one-dimensional plate impact experiments have been performed to study both the Shock to Detonation Transition and Hugoniot state in the cyclotetramethylene tetranitramine (HMX) based explosive EDC32. The experiments covered shock pressures ranging from 0.59 to 7.5 GPa with sustained shocks, double shocks, and short pulse shocks. Experiments were instrumented with embedded magnetic particle velocity gauges. Results include; (1) wave profiles of particle velocity vs. time vs. depth in the explosive, (2) time-distance coordinates for onset of detonation vs. initial shock pressure (aka the Pop-plot), (3) a reactants Hugoniot, and (4) measurement of the Hugoniot Elastic Limit of 0.22.GPa.

  7. Model-based auralizations of violin sound trends accompanying plate-bridge tuning or holding.

    PubMed

    Bissinger, George; Mores, Robert

    2015-04-01

    To expose systematic trends in violin sound accompanying "tuning" only the plates or only the bridge, the first structural acoustics-based model auralizations of violin sound were created by passing a bowed-string driving force measured at the bridge of a solid body violin through the dynamic filter (DF) model radiativity profile "filter" RDF(f) (frequency-dependent pressure per unit driving force, free-free suspension, anechoic chamber). DF model auralizations for the more realistic case of a violin held/played in a reverberant auditorium reveal that holding the violin greatly diminishes its low frequency response, an effect only weakly compensated for by auditorium reverberation. PMID:25920880

  8. Architectural Blueprint for Plate Boundary Observatories based on interoperable Data Management Platforms

    NASA Astrophysics Data System (ADS)

    Kerschke, D. I.; Häner, R.; Schurr, B.; Oncken, O.; Wächter, J.

    2014-12-01

    Interoperable data management platforms play an increasing role in the advancement of knowledge and technology in many scientific disciplines. Through high quality services they support the establishment of efficient and innovative research environments. Well-designed research environments can facilitate the sustainable utilization, exchange, and re-use of scientific data and functionality by using standardized community models. Together with innovative 3D/4D visualization, these concepts provide added value in improving scientific knowledge-gain, even across the boundaries of disciplines. A project benefiting from the added value is the Integrated Plate boundary Observatory in Chile (IPOC). IPOC is a European-South American network to study earthquakes and deformation at the Chilean continental margin and to monitor the plate boundary system for capturing an anticipated great earthquake in a seismic gap. In contrast to conventional observatories that monitor individual signals only, IPOC captures a large range of different processes through various observation methods (e.g., seismographs, GPS, magneto-telluric sensors, creep-meter, accelerometer, InSAR). For IPOC a conceptual design has been devised that comprises an architectural blueprint for a data management platform based on common and standardized data models, protocols, and encodings as well as on an exclusive use of Free and Open Source Software (FOSS) including visualization components. Following the principles of event-driven service-oriented architectures, the design enables novel processes by sharing and re-using functionality and information on the basis of innovative data mining and data fusion technologies. This platform can help to improve the understanding of the physical processes underlying plate deformations as well as the natural hazards induced by them. Through the use of standards, this blueprint can not only be facilitated for other plate observing systems (e.g., the European Plate

  9. Multi-damage localization in plate structure using frequency response function-based indices

    NASA Astrophysics Data System (ADS)

    Gao, Hai-yang; Guo, Xing-lin; Ouyang, Huajiang; Yang, Xiu-ming

    2015-07-01

    Vibration signal and its derivative have shown some promise in structural damage detection in previous research. However, the theoretical and practical difficulties of multi-damage detection in plate structures based on dynamic responses remain. In this paper, an efficient damage localization index based on frequency response function (FRF) is presented. The imaginary part of FRF (IFRF) is extracted to derive the new localization index due to its relation to modal flexibility. For avoiding the finite element model error, two-dimensional gapped smoothing method (GSM) is employed without the need for baseline data from a presumably undamaged structure. Experimental studies on a steel plate with two localized defects in different boundary conditions are performed. The results are compared with some typical damage indices in the literature, such as mode shapes, uniform load surface and IFRF. In order to mitigate the inherent disadvantages of GSM in anti-noise ability, a simple statistical treatment based on Thompson outlier analysis is finally used for noise suppression. The effect of damage level and boundary condition on the detection results is also investigated.

  10. A prerecognition model for hot topic discovery based on microblogging data.

    PubMed

    Zhu, Tongyu; Yu, Jianjun

    2014-01-01

    The microblogging is prevailing since its easy and anonymous information sharing at Internet, which also brings the issue of dispersing negative topics, or even rumors. Many researchers have focused on how to find and trace emerging topics for analysis. When adopting topic detection and tracking techniques to find hot topics with streamed microblogging data, it will meet obstacles like streamed microblogging data clustering, topic hotness definition, and emerging hot topic discovery. This paper schemes a novel prerecognition model for hot topic discovery. In this model, the concepts of the topic life cycle, the hot velocity, and the hot acceleration are promoted to calculate the change of topic hotness, which aims to discover those emerging hot topics before they boost and break out. Our experiments show that this new model would help to discover potential hot topics efficiently and achieve considerable performance. PMID:25254235

  11. A Prerecognition Model for Hot Topic Discovery Based on Microblogging Data

    PubMed Central

    Zhu, Tongyu

    2014-01-01

    The microblogging is prevailing since its easy and anonymous information sharing at Internet, which also brings the issue of dispersing negative topics, or even rumors. Many researchers have focused on how to find and trace emerging topics for analysis. When adopting topic detection and tracking techniques to find hot topics with streamed microblogging data, it will meet obstacles like streamed microblogging data clustering, topic hotness definition, and emerging hot topic discovery. This paper schemes a novel prerecognition model for hot topic discovery. In this model, the concepts of the topic life cycle, the hot velocity, and the hot acceleration are promoted to calculate the change of topic hotness, which aims to discover those emerging hot topics before they boost and break out. Our experiments show that this new model would help to discover potential hot topics efficiently and achieve considerable performance. PMID:25254235

  12. Flexible carbon nanotube-based composite plates as efficient monolithic counter electrodes for dye solar cells.

    PubMed

    Malara, Francesco; Manca, Michele; De Marco, Luisa; Pareo, Paola; Gigli, Giuseppe

    2011-09-01

    We demonstrate a general approach to fabricate a novel low-cost, lightweight and flexible nanocomposite foil that can be effectively implemented as a monolithic counter-electrode in dye solar cells. The pivotal aim of this work was to replace not only the platinum catalyzer film, but even the underlying transparent conductive oxide-coated substrate, by means of a monolithic counter electrode based on carbonaceous materials. According to our approach, a proper dispersion of multiwalled carbon nanotubes (MWCNTs) has been added to a dilute polypropylene solution in toluene. The composite solution has been then adequately mixed and subsequently dried by means of a controlled solvent evaporation process; the resulting powder has been modeled by compression molding into thin plates. Four different series of plates have been realized by tuning the carbon nanotubes concentration from 5 wt % to 20 wt %. Finally, a specifically setup reactive ion etching treatment with oxygen plasma has been carried out onto the plate surface to remove the residual polymeric capping layer and allow the embedded CNTs to protrude on top of the surface. A fine-tuning of the morphological features has been made possible by adjusting the plasma etching conditions. For all the treated surfaces, the most meaningful electrochemical parameters have been quantitatively analyzed by means of both electrochemical impedance spectroscopy and cyclic voltammetry measurements. An as high as 13.8 mA/cm(2) photocurrent density, along with a solar conversion efficiency of 6.67%, has been measured for a dye solar cell mounting a counter-electrode based on a 20 wt % CNT nanocomposite. PMID:21870845

  13. An evaluation of displacement-based finite element models used for free vibration analysis of homogeneous and composite plates

    NASA Astrophysics Data System (ADS)

    Burlayenko, V. N.; Altenbach, H.; Sadowski, T.

    2015-12-01

    The finite element vibration analysis of plates has become one of the classical problems over the past several decades. Different finite element plate models based on classical, standard and improved shear deformable plate theories, three-dimensional elasticity equations or their combinations have been developed. The ability and accuracy of each such model can be established by validating it against analytical models, if it is possible, or other numerical models. In this paper, a comparative study of different plate finite element models used for the free vibration analysis of homogeneous isotropic and anisotropic, composite laminated and sandwich thin and thick plates with different boundary conditions is presented. The aim of the study is to find out the weaknesses and strengths of each model used and to pick out their interchangeability for the finite element calculations. For comparisons, the plate models based on classical and first-order shear deformation theories within the framework of both single-layer and layer-wise concept and three-dimensional theory of elasticity are used. The models are created using the finite element package ABAQUSTM. Natural frequencies obtained by the authors are compared with results known in the literature from different analytical or approximate solutions and, then, the correlation between them is discussed in detail. At the end, conclusions are drawn concerning the utility of each model considered for vibration predictions of plates.

  14. OUT Success Stories: Solar Hot Water Technology

    DOE R&D Accomplishments Database

    Clyne, R.

    2000-08-01

    Solar hot water technology was made great strides in the past two decades. Every home, commercial building, and industrial facility requires hot water. DOE has helped to develop reliable and durable solar hot water systems. For industrial applications, the growth potential lies in large-scale systems, using flat-plate and trough-type collectors. Flat-plate collectors are commonly used in residential hot water systems and can be integrated into the architectural design of the building.

  15. Validation of the Hot Strip Mill Model

    SciTech Connect

    Richard Shulkosky; David Rosberg; Jerrud Chapman

    2005-03-30

    The Hot Strip Mill Model (HSMM) is an off-line, PC based software originally developed by the University of British Columbia (UBC) and the National Institute of Standards and Technology (NIST) under the AISI/DOE Advanced Process Control Program. The HSMM was developed to predict the temperatures, deformations, microstructure evolution and mechanical properties of steel strip or plate rolled in a hot mill. INTEG process group inc. undertook the current task of enhancing and validating the technology. With the support of 5 North American steel producers, INTEG process group tested and validated the model using actual operating data from the steel plants and enhanced the model to improve prediction results.

  16. A Novel Diagnosis Method for a Hall Plates-Based Rotary Encoder with a Magnetic Concentrator

    PubMed Central

    Meng, Bumin; Wang, Yaonan; Sun, Wei; Yuan, Xiaofang

    2014-01-01

    In the last few years, rotary encoders based on two-dimensional complementary metal oxide semiconductors (CMOS) Hall plates with a magnetic concentrator have been developed to measure contactless absolute angle. There are various error factors influencing the measuring accuracy, which are difficult to locate after the assembly of encoder. In this paper, a model-based rapid diagnosis method is presented. Based on an analysis of the error mechanism, an error model is built to compare minimum residual angle error and to quantify the error factors. Additionally, a modified particle swarm optimization (PSO) algorithm is used to reduce the calculated amount. The simulation and experimental results show that this diagnosis method is feasible to quantify the causes of the error and to reduce iteration significantly. PMID:25090417

  17. A novel diagnosis method for a Hall plates-based rotary encoder with a magnetic concentrator.

    PubMed

    Meng, Bumin; Wang, Yaonan; Sun, Wei; Yuan, Xiaofang

    2014-01-01

    In the last few years, rotary encoders based on two-dimensional complementary metal oxide semiconductors (CMOS) Hall plates with a magnetic concentrator have been developed to measure contactless absolute angle. There are various error factors influencing the measuring accuracy, which are difficult to locate after the assembly of encoder. In this paper, a model-based rapid diagnosis method is presented. Based on an analysis of the error mechanism, an error model is built to compare minimum residual angle error and to quantify the error factors. Additionally, a modified particle swarm optimization (PSO) algorithm is used to reduce the calculated amount. The simulation and experimental results show that this diagnosis method is feasible to quantify the causes of the error and to reduce iteration significantly. PMID:25090417

  18. On the limits of applicability of drift-diffusion based hot carrier degradation modeling

    NASA Astrophysics Data System (ADS)

    Jech, Markus; Sharma, Prateek; Tyaginov, Stanislav; Rudolf, Florian; Grasser, Tibor

    2016-04-01

    We study the limits of the applicability of a drift-diffusion (DD) based model for hot-carrier degradation (HCD). In this approach the rigorous but computationally expensive solution of the Boltzmann transport equation is replaced by an analytic expression for the carrier energy distribution function. On the one hand, we already showed that the simplified version of our HCD model is quite successful for LDMOS devices. On the other hand, hot carrier degradation models based on the drift-diffusion and energy transport schemes were shown to fail for planar MOSFETs with gate lengths of 0.5-2.0 µm. To investigate the limits of validity of the DD-based HCD model, we use planar nMOSFETs of an identical topology but with different gate lengths of 2.0, 1.5, and 1.0 µm. We show that, although the model is able to adequately represent the linear and saturation drain current changes in the 2.0 µm transistor, it starts to fail for gate lengths shorter than 1.5 µm and becomes completely inadequate for the 1.0 µm device.

  19. Metallurgical evaluation of SRAM II/SRAM A programmer base plates

    SciTech Connect

    Damkroger, B.K.; Maguire, M.C.; Robino, C.V.

    1993-05-01

    Ten MC4073/4369 programmer base plates were analyzed. This component, a programmer base plate for the SRAM II (and later the SRAM A), is specified as a Grade C quality casting made of aluminum Alloy A356, heat treated to the T6 condition. A concern was expressed regarding the choice of an A356 casting for this application, given the complexity and severity of the loading environment. Preliminary tests and analyses suggested that the design was adequate, but noted the uncertainty involved in a number of their underlying assumptions. The uncertainty was compounded by the discovery that the casting used in the original series of mechanical tests failed. In this investigation, several production castings were examined and found to be of a quality superior to that required under current specifications. Their defect content and microstructure were studied and compared with published data to establish a mechanical property data base. The data base was supplemented with a series of X-direction static tests, which characterized the loading environment and measured the overall casting performance. It was found that the mechanical properties of the supplied castings were adequate for the anticipated X-direction loading environment, but the component is not over-designed. The established data base further indicates that a reduction in casting quality to the allowable level could result in failure of the component. Recommendations were made including (1) change the component specification to require higher casting quality in highly stressed areas, (2) supplement the inspection procedures to ensure adequate quality in critical regions, (3) alter the component design to reduce the stress levels in the mounting feet, (4) substitute a modified A356 alloy to improve the mechanical properties and their consistency, and (5) more thoroughly establish a data base for the mechanical property consequences of levels and configurations of casting defects.

  20. Analyzing excitation forces acting on a plate based on measured acoustic pressure.

    PubMed

    Wu, Sean F; Zhou, Pan

    2016-07-01

    This paper presents a theoretical study on "seeing" through an elastic structure to uncover the root cause of sound and vibration by using nearfield acoustical holography (NAH) and normal modes expansion. This approach is of generality because vibro-acoustic responses on the surface of a vibrating structure can always be reconstructed, exactly or approximately. With these vibro-acoustic responses, excitation forces acting on the structure can always be determined, analytically or numerically, given any set of boundary conditions. As an example, the explicit formulations for reconstructing time-harmonic excitation forces, including point, line and surface forces, and their arbitrary combinations acting on a rectangular thin plate in vacuum mounted on an infinite baffle are presented. The reason for choosing this example is that the analytic solutions to vibro-acoustic responses are available, and in-depth analyses of results are possible. Results demonstrate that this approach allows one to identify excitation forces based on measured acoustic pressures and reveal their characteristics such as locations, types and amplitudes, as if one could "see" excitation forces acting behind the plate based on acoustic pressure measured on the opposite side. This approach is extendable to general elastic structures, except that in such circumstance numerical results must be sought. PMID:27475174

  1. Factors Affecting the Morphology of Pb-Based Glass Frit Coated with Ag Material Prepared by Electroless Silver Plating

    NASA Astrophysics Data System (ADS)

    Huang, Bei; Gan, Weiping; Zhou, Jian; Li, Yingfen; Lin, Tao; Liu, Xiaogang

    2014-05-01

    Pb-based glass frit coated with nanosilver material for Si solar cell applications has been directly prepared by electroless silver plating. Activation of the glass frit was accomplished by using glycol, with the aim of reducing the silver ions to elemental silver on the surface of the glass frit. Electroless silver plating onto the glass frit was successfully realized using two kinds of electroless plating bath. However, the morphology of the composite powder greatly affected the modality, sheet resistance, series resistance, and photoelectric conversion efficiency of the conducting silver films. We found that the activation temperature affected the number and distribution of silver nanoparticles. Meanwhile, the average grain size of the silver particles and the silver content in the Pb-based glass frit coated with Ag material could be controlled by adjusting the pH value and loading capacity, respectively, during plating.

  2. Finite element method for the rising and the slip of column-plate base for usual connections

    NASA Astrophysics Data System (ADS)

    Hamizi, M.; Aider, H. Ait; Alliche, A.; Hannachi, N. E.

    2010-06-01

    In the present paper, a finite element approach calculating the rising and the relative slip of steel base plate connections is proposed. Two types of connections are studied, the first consists on a base plate welded to the column end and attached to the reinforced concrete foundation by two anchor bolts. These bolts are placed on the major axis of the I shaped section used as column, one anchor bolt on each side of the web. In the second configuration, the connection includes a plate base and four anchor bolts placed out side the flanges of the I shaped section or hallow form. To take in account the real behaviour of this connection, a model by finite elements which considers count geometrical and material no linearties of the contact and cracking in the concrete foundation. To study the rising of the base plate, an approach treating problems of contact-friction between the base plate and the foundation is developed. This approach is based on a unilateral contact law in which a Coulomb friction is added. The numerical resolution is ensured by the increased Lagrangien method. For the behaviour of the concrete foundation, the developed model is based of a compressive elastoplastic model. The heights rising-rotations and the heights rising- slip displacements curves are plotted.

  3. MICROSCOPY CHARACTERIZATION OF U-MO BEARING MINI-PLATES FABRICATED BY HOT ISOSTATIC PRESSING (HIPPING) WITH A LONG THERMAL CYCLE

    SciTech Connect

    Jan-Fong Jue

    2007-07-01

    The RERTR Program has formed the Production Development Team to coordinate fabrication efforts to produce the fuel elements for the qualifying irradiation tests. These fuel elements will be fabricated in production facilities. Fabrication development data will be shared with all participants on the development team. The INL has been developing a method of cladding using a Hot Isostatic Press (HIP). The operating parameters were varied to understand the impact of time, pressure and temperature on the reaction between the fuel and the cladding. This report details some of the data produced to date.

  4. ASP (AntiSubmarine Penetrator) base plate redesign and explosive bolt test

    SciTech Connect

    Cole, J.K.; Wolfe, W.P.

    1988-10-01

    This report presents the results of a post-flight investigation of the Rocket Antisubmarine Penetrator (RAP) tests of the AntiSubmarine Penetrator (ASP). It focuses on the cause for the premature deployment of the on-board recovery system and the failure of the base pressure transducers. As a result of the investigation, the base plate of the ASP vehicle was modified to increase its structural stiffness. Also, an instrumented test was conducted to assess the environment that is created when the three explosive bolts are activated to separate the vehicle from the interstage adapter and the rocket booster. The results of this test are presented and discussed. 5 refs., 15 figs.

  5. Adjustable low frequency and broadband metamaterial absorber based on magnetic rubber plate and cross resonator

    NASA Astrophysics Data System (ADS)

    Cheng, Yongzhi; Nie, Yan; Wang, Xian; Gong, Rongzhou

    2014-02-01

    In this paper, the magnetic rubber plate absorber (MRPA) and metamaterial absorber (MA) based on MRP substrate were proposed and studied numerically and experimentally. Based on the characteristic of L-C resonances, experimental results show that the MA composed of cross resonator (CR) embedded single layer MRP could be adjustable easily by changing the wire length and width of CR structure and MRP thickness. Finally, experimental results show that the MA composed of CR-embedded two layers MRP with the total thickness of 2.42 mm exhibit a -10 dB absorption bandwidth from 1.65 GHz to 3.7 GHz, which is 1.86 times wider than the same thickness MRPA.

  6. Composite plate low energy impact localization system based on FBG sensing network and hybrid algorithm

    NASA Astrophysics Data System (ADS)

    Sai, Yaozhang; Jiang, Mingshun; Sui, Qingmei; Lu, Shizeng; Jia, Lei

    2015-08-01

    This paper proposed an impact localization system using fiber Bragg grating (FBG) network which is based on quasi-Newton algorithm and particle swarm optimization (PSO) algorithm. The FBG sensing network, formed by eight FBGs, was used to detect impact signals. And Shannon wavelet transform was employed to extract time differences. According to time differences and the coordinates of FBGs, nonlinear equations model of impact localization was established. Based on quasi-Newton algorithm and PSO algorithm, the nonlinear equations can be solved to obtain the coordinate of impact source. Testing experiments were carried out on a composite plate within 400 mm × 400 mm monitoring area. The experimental results showed that the maximum and average errors are 3.2 mm and 1.73 mm, respectively. The computational time is less than 2 s.

  7. Design of plate directional heat transmission structure based on layered thermal metamaterials

    NASA Astrophysics Data System (ADS)

    Sun, L. K.; Yu, Z. F.; Huang, J.

    2016-02-01

    Invisibility cloaks based on transformation optics are often closed structures; however, such a structure limits the kinds of objects that can be placed in the cloak. In this work, we adopt a transformation thermodynamics approach to design an "open cloak", called a plate directional heat transmission structure, which is capable of guiding heat fluxes to the flank region of the metamaterial device. The most fascinating and unique feature of the device is that the lower surface can remain at a lower temperature compared with the SiO2 aerogel thermal insulation material. Our results are expected to markedly enhance capabilities in thermal protection, thermal-energy utilization, and domains beyond. In addition to the theoretical analysis, the present design is demonstrated in numerical simulations based on finite element calculations.

  8. Iron-based alloy and nitridation treatment for PEM fuel cell bipolar plates

    DOEpatents

    Brady, Michael P [Oak Ridge, TN; Yang, Bing [Oak Ridge, TN; Maziasz, Philip J [Oak Ridge, TN

    2010-11-09

    A corrosion resistant electrically conductive component that can be used as a bipolar plate in a PEM fuel cell application is composed of an alloy substrate which has 10-30 wt. % Cr, 0.5 to 7 wt. % V, and base metal being Fe, and a continuous surface layer of chromium nitride and vanadium nitride essentially free of base metal. A oxide layer of chromium vanadium oxide can be disposed between the alloy substrate and the continuous surface nitride layer. A method to prepare the corrosion resistant electrically conductive component involves a two-step nitridization sequence by exposing the alloy to a oxygen containing gas at an elevated temperature, and subsequently exposing the alloy to an oxygen free nitrogen containing gas at an elevated temperature to yield a component where a continuous chromium nitride layer free of iron has formed at the surface.

  9. Nanofocusing of hard X-ray free electron laser pulses using diamond based Fresnel zone plates

    NASA Astrophysics Data System (ADS)

    David, C.; Gorelick, S.; Rutishauser, S.; Krzywinski, J.; Vila-Comamala, J.; Guzenko, V. A.; Bunk, O.; Färm, E.; Ritala, M.; Cammarata, M.; Fritz, D. M.; Barrett, R.; Samoylova, L.; Grünert, J.; Sinn, H.

    2011-08-01

    A growing number of X-ray sources based on the free-electron laser (XFEL) principle are presently under construction or have recently started operation. The intense, ultrashort pulses of these sources will enable new insights in many different fields of science. A key problem is to provide x-ray optical elements capable of collecting the largest possible fraction of the radiation and to focus into the smallest possible focus. As a key step towards this goal, we demonstrate here the first nanofocusing of hard XFEL pulses. We developed diamond based Fresnel zone plates capable of withstanding the full beam of the world's most powerful x-ray laser. Using an imprint technique, we measured the focal spot size, which was limited to 320 nm FWHM by the spectral band width of the source. A peak power density in the focal spot of 4×1017 W/cm2 was obtained at 70 fs pulse length.

  10. Nanofocusing of hard X-ray free electron laser pulses using diamond based Fresnel zone plates.

    PubMed

    David, C; Gorelick, S; Rutishauser, S; Krzywinski, J; Vila-Comamala, J; Guzenko, V A; Bunk, O; Färm, E; Ritala, M; Cammarata, M; Fritz, D M; Barrett, R; Samoylova, L; Grünert, J; Sinn, H

    2011-01-01

    A growing number of X-ray sources based on the free-electron laser (XFEL) principle are presently under construction or have recently started operation. The intense, ultrashort pulses of these sources will enable new insights in many different fields of science. A key problem is to provide x-ray optical elements capable of collecting the largest possible fraction of the radiation and to focus into the smallest possible focus. As a key step towards this goal, we demonstrate here the first nanofocusing of hard XFEL pulses. We developed diamond based Fresnel zone plates capable of withstanding the full beam of the world's most powerful x-ray laser. Using an imprint technique, we measured the focal spot size, which was limited to 320 nm FWHM by the spectral band width of the source. A peak power density in the focal spot of 4×10(17)W/cm(2) was obtained at 70 fs pulse length. PMID:22355576

  11. A Catalog of 1.5273 um Diffuse Interstellar Bands Based on APOGEE Hot Telluric Calibrators

    NASA Astrophysics Data System (ADS)

    Elyajouri, M.; Monreal-Ibero, A.; Remy, Q.; Lallement, R.

    2016-08-01

    High resolution stellar spectroscopic surveys provide massive amounts of diffuse interstellar bands (DIBs) measurements. Data can be used to study the distribution of the DIB carriers and those environmental conditions that favor their formation. In parallel, recent studies have also proved that DIBs extracted from stellar spectra constitute new tools for building the 3D structure of the Galactic interstellar medium (ISM). The amount of details on the structure depends directly on the quantity of available lines of sight. Therefore there is a need to construct databases of high-quality DIB measurements as large as possible. We aim at providing the community with a catalog of high-quality measurements of the 1.5273 μm DIB toward a large fraction of the Apache Point Observatory Galactic Evolution Experiment (APOGEE) hot stars observed to correct for the telluric absorption and not used for ISM studies so far. This catalog would complement the extensive database recently extracted from the APOGEE observations and used for 3D ISM mapping. We devised a method to fit the stellar continuum of the hot calibration stars and extracted the DIB from the normalized spectrum. Severe selection criteria based on the absorption characteristics are applied to the results. In particular limiting constraints on the DIB widths and Doppler shifts are deduced from the H i 21 cm measurements, following a new technique of decomposition of the emission spectra. From ∼16,000 available hot telluric spectra we have extracted ∼6700 DIB measurements and their associated uncertainties. The statistical properties of the extracted absorptions are examined and our selection criteria are shown to provide a robust dataset. The resulting catalog contains the DIB total equivalent widths, central wavelengths and widths. We briefly illustrate its potential use for the stellar and interstellar communities.

  12. A Catalog of 1.5273 um Diffuse Interstellar Bands Based on APOGEE Hot Telluric Calibrators

    NASA Astrophysics Data System (ADS)

    Elyajouri, M.; Monreal-Ibero, A.; Remy, Q.; Lallement, R.

    2016-08-01

    High resolution stellar spectroscopic surveys provide massive amounts of diffuse interstellar bands (DIBs) measurements. Data can be used to study the distribution of the DIB carriers and those environmental conditions that favor their formation. In parallel, recent studies have also proved that DIBs extracted from stellar spectra constitute new tools for building the 3D structure of the Galactic interstellar medium (ISM). The amount of details on the structure depends directly on the quantity of available lines of sight. Therefore there is a need to construct databases of high-quality DIB measurements as large as possible. We aim at providing the community with a catalog of high-quality measurements of the 1.5273 μm DIB toward a large fraction of the Apache Point Observatory Galactic Evolution Experiment (APOGEE) hot stars observed to correct for the telluric absorption and not used for ISM studies so far. This catalog would complement the extensive database recently extracted from the APOGEE observations and used for 3D ISM mapping. We devised a method to fit the stellar continuum of the hot calibration stars and extracted the DIB from the normalized spectrum. Severe selection criteria based on the absorption characteristics are applied to the results. In particular limiting constraints on the DIB widths and Doppler shifts are deduced from the H i 21 cm measurements, following a new technique of decomposition of the emission spectra. From ˜16,000 available hot telluric spectra we have extracted ˜6700 DIB measurements and their associated uncertainties. The statistical properties of the extracted absorptions are examined and our selection criteria are shown to provide a robust dataset. The resulting catalog contains the DIB total equivalent widths, central wavelengths and widths. We briefly illustrate its potential use for the stellar and interstellar communities.

  13. Canadian Arctic Plate Reconstructions based on revised geological and geophysical data

    NASA Astrophysics Data System (ADS)

    Torsvik, Trond H.; Gaina, Carmen

    2015-04-01

    We present a revised rifting and seafloor spreading history around Greenland based on geological and geophysical constraints. Palaeomagnetic data from (i) Neoproterozoic dykes and sills in North America, NW Greenland, Devon and SW Ellesmere (Franklin and Clarence Head), (ii) Early Permian volcanism (Esayoo unit) in Ellesmere and (iii) Cretaceous volcanism and intrusive activity (Isachsen and Strandfjord Formations) in Axel Heiberg and Ellesmere have also been re-evaluated and used to develop a new Canadian Arctic plate model from Silurian to Paleogene times. We have tentatively divided the Canadian Arctic into seven tectonic units, including Pearya, which accreted to the northern sectors of Ellesmere and Axel Heiberg islands as part of the mid-Silurian Caledonide Orogeny. The Canadian Arctic was variable deformed during the Late Devonian Ellesmere and the Tertiary Eurekean events, the latter including c. 250 km of shortening and ultimately amalgamating all the Canadian Arctic units in the Late Eocene. Two of the units, Devon and SW Ellesmere must have been closely tied to NW Greenland (the 'Greenland Plate') in order to minimize Palaeocene-Eocene deformation across the Nares Strait during Labrador Sea and Baffin Bay seafloor spreading. We model 100 and 60 km of Late Cretaceous-Eocene transtension/extension in the Lancaster and Jones Sounds but in order to avoid too much continental overlap between Devon and North America (Lancaster Sound) we must include 150 km of pure strike-slip faulting along the Nares Strait.

  14. Defect detection in anisotropic plates based on the instantaneous phase of signals.

    PubMed

    Prado, Vander Teixeira; Granja, Silvio Cesar Garcia; Higuti, Ricardo Tokio; Kitano, Cláudio; Martínez-Graullera, Óscar; Segura, Luis Elvira

    2015-10-01

    Anisotropic materials are widely employed in industry and engineering, and efficient nondestructive testing techniques are important to guarantee the structural integrity of the involved parts. A simple technique is proposed to detect defects in anisotropic plates using ultrasonic guided waves and arrays. The technique is based on the application of an objective threshold to a synthetic aperture image obtained from the instantaneous phase (IP) of the emitter-receiver signal combinations. In a previous work the method was evaluated for isotropic materials, and in this paper it is shown that with some considerations the technique can also be applied to anisotropic plates. These considerations, which should be taken into account in beamforming, are (1) group velocity dependence with propagation direction, and (2) elastic focusing, which results in energy concentration in some propagation directions, with the practical consequence that not all aperture signals effectively contribute to the image. When compared with conventional delay-and-sum image beamforming techniques, the proposed IP technique results in significant improvements relative to defect detection and artifacts/dead zone reduction. PMID:26470050

  15. New long trace profiler based on phase plate diffraction for optical metrology of SSRF

    SciTech Connect

    Zeng Danhua; Xiao Tiqiao; Du Guohao; Wen Li; Luo Hongxin; Xia Shaojian; Xu Hongjie

    2006-09-15

    A long trace profiler LTP-1200, with a novel f-{theta} system based on phase plate diffraction and a scanning range up to 1200 mm, has been developed at Shanghai Synchrotron Radiation Facility. The central dark line in the diffraction pattern generated by a {pi} phase plate is taken as the positioning benchmark. A magnet levitated linear rail with very high accuracy is used. A granite bench is employed to reduce deformation due to self-gravity of the rail. The focused diffraction pattern is recorded with an area charge-coupled device. The generalized regression neural network algorithm is adopted to improve the beam positioning precision. The static stability of LTP-1200 in 5 h is 0.14 {mu}rad, and the repeatability reaches 0.05 {mu}rad in a common laboratory without any special control of temperature, air turbulence, etc. Calibration tests were carried out with a high precision autocollimator and a standard spherical mirror, respectively. Results show the high performance and reliability of the LTP-1200.

  16. Toward a generalized plate motion reference frame

    NASA Astrophysics Data System (ADS)

    Becker, T. W.; Schaeffer, A. J.; Lebedev, S.; Conrad, C. P.

    2015-05-01

    An absolute plate motion (APM) model is required to address issues such as the thermochemical evolution of Earth's mantle. All APM models have to rely on indirect inferences, including those based on hot spots and seismic anisotropy, each with their own set of uncertainties. Here, we explore a seafloor spreading-aligned reference frame. We show that this reference frame fits azimuthal seismic anisotropy in the uppermost mantle very well. The corresponding Euler pole is close to those of hot spot reference frames, ridge motion minimizing models, and geodynamic estimates of net rotation and predicts clear trench motion patterns. We conclude that a net rotation pole guided by the spreading-aligned model (at 64°E, 61°S, with moderate rotation of ˜ 0.2 … 0.3°/Myr) could indeed represent a standard, comprehensive reference frame for present-day plate motions with respect to the deep mantle.

  17. An assessment of four-noded plate finite elements based on a generalized third-order theory

    NASA Technical Reports Server (NTRS)

    Averill, R. C.; Reddy, J. N.

    1992-01-01

    Plate finite elements based on the generalized third-order theory of Reddy and the first-order shear deformation theory are analyzed and compared on the basis of thick and thin plate modeling behavior, distortion sensitivity, overall accuracy, reliability, and efficiency. In particular, several four-noded Reddy-type elements and the nine-noded Lagrangian and heterosis (Mindlin-type) plate elements are analyzed to assess their behavior in bending, vibration, and stability of isotropic and laminated composite plates. A four-noded Reddy-type element is identified which is free of all spurious stiffness and zero energy modes, computationally efficient, and suitable for use in any general-purpose finite element program.

  18. Hot corrosion studies of four nickel-base superalloys - B-1900, NASA-TRW VIA, 713C and IN738

    NASA Technical Reports Server (NTRS)

    Fryburg, G. C.; Kohl, F. J.; Stearns, C. A.

    1976-01-01

    The susceptibility to hot corrosion of four nickel-base superalloys has been studied at 900 and 1000 C in one atmosphere of slowly flowing oxygen. Hot corrosion was induced by coating the samples with known doses of Na2SO4 and oxidizing the coated samples isothermally on a sensitive microbalance. In order of decending susceptibility to hot corrosion, these alloys were ranked: B-1900, 713C, NASA-TRW VIA, IN738. This order corresponds to the order of decreasing molybdenum content of the alloys. Chemical evidence for B-1900 indicates that hot corrosion is instigated by acid fluxing of the protective Al2O3 coating by MoO3.

  19. Hot roller embossing system equipped with a temperature margin-based controller

    NASA Astrophysics Data System (ADS)

    Kim, Seyoung; Son, Youngsu; Lee, Sunghee; Ham, Sangyong; Kim, Byungin

    2014-08-01

    A temperature control system was proposed for hot roller embossing. The roll surface was heated using induction coils and cooled with a circulating chilled water system. The temperature of the roll surface was precisely controlled by a temperature margin-based control algorithm that we developed. Implementation of the control system reduced deviations in the roll surface temperature to less than ±2 °C. The tight temperature control and the ability to rapidly increase and decrease the roll temperature will allow optimum operating parameters to be developed quickly. The temperature margin-based controller could also be used to optimize the time course of electrical power and shorten the cooling time by choosing an appropriate temperature margin, possibly for limited power consumption. The chiller-equipped heating roll with the proposed control algorithm is expected to decrease the time needed to determine the optimal embossing process.

  20. Hot roller embossing system equipped with a temperature margin-based controller.

    PubMed

    Kim, Seyoung; Son, Youngsu; Lee, Sunghee; Ham, Sangyong; Kim, Byungin

    2014-08-01

    A temperature control system was proposed for hot roller embossing. The roll surface was heated using induction coils and cooled with a circulating chilled water system. The temperature of the roll surface was precisely controlled by a temperature margin-based control algorithm that we developed. Implementation of the control system reduced deviations in the roll surface temperature to less than ±2 °C. The tight temperature control and the ability to rapidly increase and decrease the roll temperature will allow optimum operating parameters to be developed quickly. The temperature margin-based controller could also be used to optimize the time course of electrical power and shorten the cooling time by choosing an appropriate temperature margin, possibly for limited power consumption. The chiller-equipped heating roll with the proposed control algorithm is expected to decrease the time needed to determine the optimal embossing process. PMID:25173322

  1. Hot roller embossing system equipped with a temperature margin-based controller

    SciTech Connect

    Kim, Seyoung Son, Youngsu; Lee, Sunghee; Ham, Sangyong; Kim, Byungin

    2014-08-15

    A temperature control system was proposed for hot roller embossing. The roll surface was heated using induction coils and cooled with a circulating chilled water system. The temperature of the roll surface was precisely controlled by a temperature margin-based control algorithm that we developed. Implementation of the control system reduced deviations in the roll surface temperature to less than ±2 °C. The tight temperature control and the ability to rapidly increase and decrease the roll temperature will allow optimum operating parameters to be developed quickly. The temperature margin-based controller could also be used to optimize the time course of electrical power and shorten the cooling time by choosing an appropriate temperature margin, possibly for limited power consumption. The chiller-equipped heating roll with the proposed control algorithm is expected to decrease the time needed to determine the optimal embossing process.

  2. INL HIP Plate Fabrication

    SciTech Connect

    B. H. Park; C. R. Clark; J. F. Jue

    2010-02-01

    This document outlines the process used to bond monolithic fuel plates by Hot Isostatic Pressing (HIP). This method was developed at Idaho National Laboratory (INL) for the Reduced Enrichment for Research and Test Reactors (RERTR) program. These foils have been used in a number of irradiation experiments in support of the United States Global Threat Reduction Initiative (GTRI) program.

  3. Hot Deformation Processing Map and Microstructural Evaluation of the Ni-Based Superalloy IN-738LC

    NASA Astrophysics Data System (ADS)

    Sajjadi, S. A.; Chaichi, A.; Ezatpour, H. R.; Maghsoudlou, A.; Kalaie, M. A.

    2016-04-01

    Hot deformation behavior of the Ni-based superalloy IN-738LC was investigated by means of hot compression tests over the temperature range of 1000-1200 °C and strain rate range of 0.01-1 s-1. The obtained peak flow stresses were related to strain rate and temperature through the hyperbolic sine equation with activation energy of 950 kJ/mol. Dynamic material model was used to obtain the processing map of IN-738LC. Analysis of the microstructure was carried out in order to study each domain's characteristic represented by the processing map. The results showed that dynamic recrystallization occurs in the temperature range of 1150-1200 °C and strain rate of 0.1 s-1 with the maximum power dissipation efficiency of 35%. The unstable domain was exhibited in the temperature range of 1000-1200 °C and strain rate of 1 s-1 on the occurrence of severe deformation bands and grain boundary cracking.

  4. Microfluidic flowmeter based on micro "hot-wire" sandwiched Fabry-Perot interferometer.

    PubMed

    Li, Ying; Yan, Guofeng; Zhang, Liang; He, Sailing

    2015-04-01

    We present a compact microfluidic flowmeter based on Fabry-Perot interferometer (FPI). The FPI was composed by a pair of fiber Bragg grating reflectors and a micro Co(2+)-doped optical fiber cavity, acting as a "hot-wire" sensor. Microfluidic channels made from commercial silica capillaries were integrated with the FPIs on a chip to realize flow-rate sensing system. By utilizing a tunable pump laser with wavelength of 1480 nm, the proposed flowmeter was experimentally demonstrated. The flow rate of the liquid sample is determined by the induced resonance wavelength shift of the FPI. The effect of the pump power, microfluidic channel scale and temperature on the performance of our flowmeter was investigated. The dynamic response was also measured under different flow-rate conditions. The experimental results achieve a sensitivity of 70 pm/(μL/s), a dynamic range up to 1.1 μL/s and response time in the level of seconds, with a spatial resolution ~200 μm. Such good performance renders the sensor a promising supplementary component in microfluidic biochemical sensing system. Furthermore, simulation modal was built up to analyze the heat distribution of the "hot-wire" cavity and optimize the FPI structure as well. PMID:25968776

  5. Sentiment Diffusion of Public Opinions about Hot Events: Based on Complex Network.

    PubMed

    Hao, Xiaoqing; An, Haizhong; Zhang, Lijia; Li, Huajiao; Wei, Guannan

    2015-01-01

    To study the sentiment diffusion of online public opinions about hot events, we collected people's posts through web data mining techniques. We calculated the sentiment value of each post based on a sentiment dictionary. Next, we divided those posts into five different orientations of sentiments: strongly positive (P), weakly positive (p), neutral (o), weakly negative (n), and strongly negative (N). These sentiments are combined into modes through coarse graining. We constructed sentiment mode complex network of online public opinions (SMCOP) with modes as nodes and the conversion relation in chronological order between different types of modes as edges. We calculated the strength, k-plex clique, clustering coefficient and betweenness centrality of the SMCOP. The results show that the strength distribution obeys power law. Most posts' sentiments are weakly positive and neutral, whereas few are strongly negative. There are weakly positive subgroups and neutral subgroups with ppppp and ooooo as the core mode, respectively. Few modes have larger betweenness centrality values and most modes convert to each other with these higher betweenness centrality modes as mediums. Therefore, the relevant person or institutes can take measures to lead people's sentiments regarding online hot events according to the sentiment diffusion mechanism. PMID:26462230

  6. Hot-isostatic pressing of silicon carbide based multiphase composed materials

    SciTech Connect

    Jiang, D.L.; She, J.H.

    1995-10-01

    Silicon carbide (SiC) based ceramic composites with improved fracture toughness and increased flexure strength have been developed by incorporating some other non-oxide and oxide particles or some whiskers and fibers. Hot-Isostatic Pressing (HIP) has been identified as an important technology for strengthening carbide by surface modification. In this paper, Hot-pressed SiC-TiC with different densities and HIP-SiC/SiC(w) composites were post HIPped under a N{sub 2}-pressure of 200 MPa at 1,850 C for 1 h. The results showed that the open pores were closed and physical and mechanical properties such as density, flexure strength and toughness were obviously improved. For the SiC-TiC composites, the final density can be reached above 985 theoretical density, flexure strength and fracture toughness were increased by 100% and 30--50%, respectively. For the SiC/5vol%-SiC(w) composites, the final flexure strength and fracture toughness were increased from 595 MPa and 6.7 MPa {center_dot} m{sup 1/2} to 920 MPa and 8.5 MPa {center_dot} m{sup 1/2} separately. A possible reaction-HIP densification mechanism for SiC ceramics with open pores is proposed.

  7. Sentiment Diffusion of Public Opinions about Hot Events: Based on Complex Network

    PubMed Central

    Hao, Xiaoqing; An, Haizhong; Zhang, Lijia; Li, Huajiao; Wei, Guannan

    2015-01-01

    To study the sentiment diffusion of online public opinions about hot events, we collected people’s posts through web data mining techniques. We calculated the sentiment value of each post based on a sentiment dictionary. Next, we divided those posts into five different orientations of sentiments: strongly positive (P), weakly positive (p), neutral (o), weakly negative (n), and strongly negative (N). These sentiments are combined into modes through coarse graining. We constructed sentiment mode complex network of online public opinions (SMCOP) with modes as nodes and the conversion relation in chronological order between different types of modes as edges. We calculated the strength, k-plex clique, clustering coefficient and betweenness centrality of the SMCOP. The results show that the strength distribution obeys power law. Most posts’ sentiments are weakly positive and neutral, whereas few are strongly negative. There are weakly positive subgroups and neutral subgroups with ppppp and ooooo as the core mode, respectively. Few modes have larger betweenness centrality values and most modes convert to each other with these higher betweenness centrality modes as mediums. Therefore, the relevant person or institutes can take measures to lead people’s sentiments regarding online hot events according to the sentiment diffusion mechanism. PMID:26462230

  8. FEA Based Tool Life Quantity Estimation of Hot Forging Dies Under Cyclic Thermo-Mechanical Loads

    NASA Astrophysics Data System (ADS)

    Behrens, B.-A.; Bouguecha, A.; Schäfer, F.; Hadifi, T.

    2011-01-01

    Hot forging dies are exposed during service to a combination of cyclic thermo-mechanical, tribological and chemical loads. Besides abrasive and adhesive wear on the die surface, fatigue crack initiation with subsequent fracture is one of the most frequent causes of failure. In order to extend the tool life, the finite element analysis (FEA) may serve as a means for process design and process optimisation. So far the FEA based estimation of the production cycles until initial cracking is limited as tool material behaviour due to repeated loading is not captured with the required accuracy. Material models which are able to account for cyclic effects are not verified for the fatigue life predictions of forging dies. Furthermore fatigue properties from strain controlled fatigue tests of relevant hot work steels are to date not available to allow for a close-to-reality fatigue life prediction. Two industrial forging processes, where clear fatigue crack initiation has been observed are considered for a fatigue analysis. For this purpose the relevant tool components are modelled with elasto-plastic material behaviour. The predicted sites, where crack initiation occurs, agree with the ones observed on the real die component.

  9. Fabrication of lotus-leaf-like superhydrophobic surfaces via Ni-based nano-composite electro-brush plating

    NASA Astrophysics Data System (ADS)

    Liu, Hongtao; Wang, Xuemei; Ji, Hongmin

    2014-01-01

    Superhydrophobic surface has become a research hot topic in recent years due to its excellent performance and wide application prospect. This paper investigates the method to fabricate superhydrophobic surface on carbon steel substrate via two-layer nano-composite electro-brush plating and subsequent surface modification with low free energy materials. The hydrophobic properties of as-prepared coatings were characterized by a water sliding angle (SA) and a water contact angle (CA) measured by the Surface tension instrument. A Scanning electron microscope was used to analyze the surface structure of plating coatings. Anti-corrosion performance of the superhydrophobic coating was characterized by a potentiodynamic polarization curve measured by the Electrochemical workstation. The research result shows that: the superhydrophobic structure can be successfully prepared by plating nano-C/Ni and nano-Cu/Ni two-layer coating on carbon steel substrate under appropriate technology and has similarity with lotus-leaf-like micro/nano composite structure; the contact angle of the as-prepared superhydrophobic coating can be up to 155.5°, the sliding angle is 5°; the coating has better anti-corrosion performance compared with substrate.

  10. Web-based monitoring tools for Resistive Plate Chambers in the CMS experiment at CERN

    NASA Astrophysics Data System (ADS)

    Kim, M. S.; Ban, Y.; Cai, J.; Li, Q.; Liu, S.; Qian, S.; Wang, D.; Xu, Z.; Zhang, F.; Choi, Y.; Kim, D.; Goh, J.; Choi, S.; Hong, B.; Kang, J. W.; Kang, M.; Kwon, J. H.; Lee, K. S.; Lee, S. K.; Park, S. K.; Pant, L. M.; Mohanty, A. K.; Chudasama, R.; Singh, J. B.; Bhatnagar, V.; Mehta, A.; Kumar, R.; Cauwenbergh, S.; Costantini, S.; Cimmino, A.; Crucy, S.; Fagot, A.; Garcia, G.; Ocampo, A.; Poyraz, D.; Salva, S.; Thyssen, F.; Tytgat, M.; Zaganidis, N.; Doninck, W. V.; Cabrera, A.; Chaparro, L.; Gomez, J. P.; Gomez, B.; Sanabria, J. C.; Avila, C.; Ahmad, A.; Muhammad, S.; Shoaib, M.; Hoorani, H.; Awan, I.; Ali, I.; Ahmed, W.; Asghar, M. I.; Shahzad, H.; Sayed, A.; Ibrahim, A.; Aly, S.; Assran, Y.; Radi, A.; Elkafrawy, T.; Sharma, A.; Colafranceschi, S.; Abbrescia, M.; Calabria, C.; Colaleo, A.; Iaselli, G.; Loddo, F.; Maggi, M.; Nuzzo, S.; Pugliese, G.; Radogna, R.; Venditti, R.; Verwillingen, P.; Benussi, L.; Bianco, S.; Piccolo, D.; Paolucci, P.; Buontempo, S.; Cavallo, N.; Merola, M.; Fabozzi, F.; Iorio, O. M.; Braghieri, A.; Montagna, P.; Riccardi, C.; Salvini, P.; Vitulo, P.; Vai, I.; Magnani, A.; Dimitrov, A.; Litov, L.; Pavlov, B.; Petkov, P.; Aleksandrov, A.; Genchev, V.; Iaydjiev, P.; Rodozov, M.; Sultanov, G.; Vutova, M.; Stoykova, S.; Hadjiiska, R.; Ibargüen, H. S.; Morales, M. I. P.; Bernardino, S. C.; Bagaturia, I.; Tsamalaidze, Z.; Crotty, I.

    2014-10-01

    The Resistive Plate Chambers (RPC) are used in the CMS experiment at the trigger level and also in the standard offline muon reconstruction. In order to guarantee the quality of the data collected and to monitor online the detector performance, a set of tools has been developed in CMS which is heavily used in the RPC system. The Web-based monitoring (WBM) is a set of java servlets that allows users to check the performance of the hardware during data taking, providing distributions and history plots of all the parameters. The functionalities of the RPC WBM monitoring tools are presented along with studies of the detector performance as a function of growing luminosity and environmental conditions that are tracked over time.

  11. Photon-counting detector arrays based on microchannel array plates. [for image enhancement

    NASA Technical Reports Server (NTRS)

    Timothy, J. G.

    1975-01-01

    The recent development of the channel electron multiplier (CEM) and its miniaturization into the microchannel array plate (MCP) offers the possibility of fully combining the advantages of the photographic and photoelectric detection systems. The MCP has an image-intensifying capability and the potential of being developed to yield signal outputs superior to those of conventional photomultipliers. In particular, the MCP has a photon-counting capability with a negligible dark-count rate. Furthermore, the MCP can operate stably and efficiently at extreme-ultraviolet and soft X-ray wavelengths in a windowless configuration or can be integrated with a photo-cathode in a sealed tube for use at ultraviolet and visible wavelengths. The operation of one- and two-dimensional photon-counting detector arrays based on the MCP at extreme-ultraviolet wavelengths is described, and the design of sealed arrays for use at ultraviolet and visible wavelengths is briefly discussed.

  12. Ultra lightweight PMMA-based composite plates with robust super-hydrophobic surfaces.

    PubMed

    Pareo, Paola; De Gregorio, Gian Luca; Manca, Michele; Pianesi, Maria Savina; De Marco, Luisa; Cavallaro, Francesco; Mari, Margherita; Pappadà, Silvio; Ciccarella, Giuseppe; Gigli, Giuseppe

    2011-11-15

    Extremely lightweight plates made of an engineered PMMA-based composite material loaded with hollow glass micro-sized spheres, nano-sized silica particles and aluminum hydroxide prismatic micro-flakes were realized by cast molding. Their interesting bulk mechanical properties were combined to properly tailored surface topography compatible with the achievement of a superhydrophobic behavior after the deposition of a specifically designed hydrophobic coating. With this aim, we synthesized two different species of fluoromethacrylic polymers functionalized with methoxysilane anchoring groups to be covalently grafted onto the surface protruding inorganic fillers. By modulating the feed composition of the reacting monomers, it was possible to combine the hydrophobic character of the polymer with an high adhesion strength to the substrate and hence to maximize both the water contact angle (up to 157°) and the durability of the easy-to-clean effect (up to 2000 h long outdoor exposure). PMID:21855889

  13. Exergy efficiency analysis of a flat plate solar collector using graphene based nanofluid

    NASA Astrophysics Data System (ADS)

    Said, Z.; Alim, M. A.; Janajreh, Isam

    2015-10-01

    The thermal efficiency of a flat plate solar thermal collector is largely affected by the thermal conductivity of the fluid used. In this paper, we theoretically analyzed the heat transfer performance, the entropy generation rate, and the exergy efficiency of the two different graphene based nanofluids (graphene/Acetone and graphene/water). From the analyses, it is revealed that by inserting a small amount of graphene nanoparticles in water, exergy efficiency could be enhanced by 21%, comparing to conventional fluids and entropy generation is decreased by 4%. However, the graphene/water nanofluid shows a lower entropy generation. This characteristic suggests that graphene/water nanofluid is a better candidate for flat solar thermal application.

  14. Ultra-thin optical vortex phase plate based on the metasurface and the angular momentum transformation

    NASA Astrophysics Data System (ADS)

    Wang, Wei; Li, Yan; Guo, Zhongyi; Li, Rongzhen; Zhang, Jingran; Zhang, Anjun; Qu, Shiliang

    2015-04-01

    The ultra-thin optical vortex phase plate (VPP) has been designed and investigated based on the metasurface of the metal rectangular split-ring resonators (MRSRRs) array. The circularly polarized incident light can convert into corresponding cross-polarization transmission light, and the phase and the amplitude of cross-polarization transmission light can be simultaneously governed by modulating two arms of the MRSRR. The MRSRR has been arranged in a special order for forming an ultra-thin optical VPP that can covert a plane wave into a vortex beam with a variety of the topological charges, and the transformation between spin angular momentum (SAM) and orbital angular momentum (OAM) has been discussed in detail. The multi-spectral characteristics of the VPP have also been investigated, and the operating bandwidth of the designed VPP is 190 nm (in the range of 710-900 nm), which enable a potential implication for integrated optics and vortex optics.

  15. A novel silver-coated solid-phase microextraction metal fiber based on electroless plating technique.

    PubMed

    Feng, Juanjuan; Sun, Min; Li, Jubai; Liu, Xia; Jiang, Shengxiang

    2011-09-01

    A novel silver-coated solid-phase microextraction fiber was prepared based on electroless plating technique. Good extraction performance of the fiber for model compounds including phthalate esters (dibutyl phthalate, dioctyl phthalate, dicyclohexyl phthalate and diallyl phthalate) and polycyclic aromatic hydrocarbons (naphthalene, fluorene, phenanthrene, fluoranthene) in aqueous solution was obtained. Under the optimized conditions (extraction temperature, extraction time, ionic strength and desorption temperature), the proposed SPME-GC method showed wide linear ranges with correlation coefficients (R(2)) ranging from 0.9745 to 0.9984. The limits of detection were at the range of 0.02 to 0.1 μg L(-1). Single fiber repeatability and fiber-to-fiber reproducibility as well as stability to acid, alkali and high temperature were studied and the results were all satisfactory. The method was applied successfully to the aqueous extracts of disposable paper cup and instant noodle barrel. Several kinds of analytes were detected and quantified. PMID:21801885

  16. Tunable broadband terahertz wave plate based on one-dimensional superconductor-dielectric photonic crystals

    NASA Astrophysics Data System (ADS)

    Liu, Yang; Liu, Ming; Hu, Xin-Guang; Yu, Li; Xie, Yan-Ding; Yi, Lin

    2016-04-01

    The reflection phase difference between transverse electric (TE) and transverse magnetic (TM) waves in a one-dimensional superconductor-dielectric photonic crystal is studied by the transfer matrix method. The simulation results indicate that wide frequency regions exist within the terahertz range, in which the reflection phase differences can remain constant for a fixed incident angle and can vary continuously from 0 to π (or 0 to -π ) by increasing the incident angle. The shift and the number of such wide frequency regions can be manipulated through changing the thickness of the dielectric layers. The influences of temperature and the normal conducting electrons on the properties of the reflection phase difference are also numerically investigated. Based on these properties, a continuously tunable broadband terahertz wave plate can be designed.

  17. A model of convergent plate margins based on the recent tectonics of Shikoku, Japan

    NASA Technical Reports Server (NTRS)

    Bischke, R. E.

    1974-01-01

    A viscoelastic finite element plate tectonic model is applied to displacement data for the island of Shikoku, Japan. The flow properties and geometry of the upper portions of the earth are assumed known from geophysical evidence, and the loading characteristics are determined from the model. The nature of the forces acting on the Philippine Sea plate, particularly in the vicinity of the Nankai trough, is determined. Seismic displacement data related to the 1946 Nankaido earthquake are modeled in terms of a thick elastic plate overlying a fluidlike substratum. The sequence of preseismic and seismic displacements can be explained in terms of two independent processes operating on elastic lithospheric plates: a strain accumulation process caused by vertical downward forces acting on or within the lithosphere in the vicinity of the trench, and a strain release process caused by plate failure along a preexisting zone on weakness. This is a restatement of Reid's elastic rebound theory in terms of elastic lithospheric plates.

  18. Microstructural Stability and Hot Deformation of γ- γ'- δ Ni-Base Superalloys

    NASA Astrophysics Data System (ADS)

    Detrois, Martin; Helmink, Randolph C.; Tin, Sammy

    2014-11-01

    Nickel-base superalloys exhibit excellent high-temperature mechanical and physical properties and remain the first choice for structural components in advanced gas turbine engines for the aerospace propulsion and power generation applications. In response to the increasing demand for more efficient solutions and tighter requirements linked to gas turbine technologies, the properties of nickel-base superalloys can be improved by modification of their thermo-mechanical and/or compositional attributes. Recent investigations have revealed the potential use of ternary eutectic γ- γ'- δ Ni-base superalloys in advanced gas turbines due to high temperature mechanical properties that are comparable to state-of-the-art polycrystalline Ni-base superalloys. With properties largely dependent on microstructural strengthening mechanisms, both the composition and thermo-mechanical processing parameters of this novel class of alloys need to be optimized concurrently. The hot deformation characteristics of four γ- γ'- δ Ni-base superalloys with varying levels of Nb were evaluated at temperatures and strain rates between 1353 K and 1433 K (1080 °C and 1160 °C) and 0.01 to 0.001/s, respectively. Evidence of dislocation-based plasticity was observed following deformation at low temperatures and high strain rates, while high temperatures and low strain rates promoted superplasticity in these alloys. The extent of the microstructural changes and the magnitude of the cavitation damage which occurred during deformation was found to vary as a function of the alloy composition.

  19. Predicting hot spots in protein interfaces based on protrusion index, pseudo hydrophobicity and electron-ion interaction pseudopotential features

    PubMed Central

    Xia, Junfeng; Yue, Zhenyu; Di, Yunqiang; Zhu, Xiaolei; Zheng, Chun-Hou

    2016-01-01

    The identification of hot spots, a small subset of protein interfaces that accounts for the majority of binding free energy, is becoming more important for the research of drug design and cancer development. Based on our previous methods (APIS and KFC2), here we proposed a novel hot spot prediction method. For each hot spot residue, we firstly constructed a wide variety of 108 sequence, structural, and neighborhood features to characterize potential hot spot residues, including conventional ones and new one (pseudo hydrophobicity) exploited in this study. We then selected 3 top-ranking features that contribute the most in the classification by a two-step feature selection process consisting of minimal-redundancy-maximal-relevance algorithm and an exhaustive search method. We used support vector machines to build our final prediction model. When testing our model on an independent test set, our method showed the highest F1-score of 0.70 and MCC of 0.46 comparing with the existing state-of-the-art hot spot prediction methods. Our results indicate that these features are more effective than the conventional features considered previously, and that the combination of our and traditional features may support the creation of a discriminative feature set for efficient prediction of hot spots in protein interfaces. PMID:26934646

  20. Hot hollow cathode gun assembly

    DOEpatents

    Zeren, J.D.

    1983-11-22

    A hot hollow cathode deposition gun assembly includes a hollow body having a cylindrical outer surface and an end plate for holding an adjustable heat sink, the hot hollow cathode gun, two magnets for steering the plasma from the gun into a crucible on the heat sink, and a shutter for selectively covering and uncovering the crucible.

  1. A material based approach to creating wear resistant surfaces for hot forging

    NASA Astrophysics Data System (ADS)

    Babu, Sailesh

    Tools and dies used in metal forming are characterized by extremely high temperatures at the interface, high local pressures and large metal to metal sliding. These harsh conditions result in accelerated wear of tooling. Lubrication of tools, done to improve metal flow drastically quenches the surface layers of the tools and compounds the tool failure problem. This phenomenon becomes a serious issue when parts forged at complex and are expected to meet tight tolerances. Unpredictable and hence uncontrolled wear and degradation of tooling result in poor part quality and premature tool failure that result in high scrap, shop downtime, poor efficiency and high cost. The objective of this dissertation is to develop a computer-based methodology for analyzing the requirements hot forging tooling to resist wear and plastic deformation and wear and predicting life cycle of forge tooling. Development of such is a system is complicated by the fact that wear and degradation of tooling is influenced by not only the die material used but also numerous process controls like lubricant, dilution ratio, forging temperature, equipment used, tool geometries among others. Phenomenological models available u1 the literature give us a good thumb rule to selecting materials but do not provide a way to evaluate pits performance in field. Once a material is chosen, there are no proven approaches to create surfaces out of these materials. Coating approaches like PVD and CVD cannot generate thick coatings necessary to withstand the conditions under hot forging. Welding cannot generate complex surfaces without several secondary operations like heat treating and machining. If careful procedures are not followed, welds crack and seldom survive forging loads. There is a strong need for an approach to selectively, reliably and precisely deposit material of choice reliably on an existing surface which exhibit not only good tribological properties but also good adhesion to the substrate

  2. Process improvement in laser hot wire cladding for martensitic stainless steel based on the Taguchi method

    NASA Astrophysics Data System (ADS)

    Huang, Zilin; Wang, Gang; Wei, Shaopeng; Li, Changhong; Rong, Yiming

    2016-07-01

    Laser hot wire cladding, with the prominent features of low heat input, high energy efficiency, and high precision, is widely used for remanufacturing metal parts. The cladding process, however, needs to be improved by using a quantitative method. In this work, volumetric defect ratio was proposed as the criterion to describe the integrity of forming quality for cladding layers. Laser deposition experiments with FV520B, one of martensitic stainless steels, were designed by using the Taguchi method. Four process variables, namely, laser power (P), scanning speed (V s), wire feed rate (V f), and wire current (I), were optimized based on the analysis of signal-to-noise (S/N) ratio. Metallurgic observation of cladding layer was conducted to compare the forming quality and to validate the analysis method. A stable and continuous process with the optimum parameter combination produced uniform microstructure with minimal defects and cracks, which resulted in a good metallurgical bonding interface.

  3. Studying a multilayer material based on stainless steels and produced by hot pack rolling

    NASA Astrophysics Data System (ADS)

    Tabatchikova, T. I.; Yakovleva, I. L.; Plokhikh, A. I.; Del'gado Reina, S. Yu.

    2014-04-01

    The structure of a multilayer metal material produced from a composite blank based on sheets of the 08Kh18 and 08Kh18N10 steels by hot pack rolling has been studied using optical microscopy, as well as scanning and transmission electron microscopy. It has been found that two processing cycles are completed in the formation of a laminated structure that is characterized by structural and chemical inhomogeneities due to diffusion and relaxation processes. It has been shown that, during pack rolling, an ultradispersed structure is formed, which is a mixture of ferrite layers elongated in the direction of rolling and of packet martensite layers or layers of carbide-free bainite that has a subgrain structure.

  4. An investigation of the initiation stage of hot corrosion in Ni-base alloys

    NASA Technical Reports Server (NTRS)

    Huang, T. T.; Meier, G. H.

    1979-01-01

    The mechanisms which lead to the destruction of a normally protective scale during the initial stages of hot corrosion of 14 nickel-base alloys contaminated with Na2SO4 and other condensed deposits were investigated. A continuous reading microbalance was used to record weight changes at temperatures between 900 C and 1000 C at 1 atmosphere pressure of slowly flowing oxygen. The reaction was initiated by raising a preheated furnace around the quartz tube in which the specimen was supported with oxygen flowing. The furnace was raised in a time period of seconds. At 900 C, the system and specimen came to thermal equilibrium in less than one minute. Oxidized specimens were studied using optical and scanning electron metallography and X-ray diffraction techniques. Transmission electron microscopy and electron diffraction spectroscopy were also used to identify the structure of carbides in some of the commercial alloys.

  5. Long rod penetration test of hot isostatically pressed Ti-based targets

    NASA Astrophysics Data System (ADS)

    Nesterenko, Vitali F.; Indrakanti, Sastry S.; Brar, Singh; Gu, YaBei

    2000-04-01

    Hot Isostatic Pressing (HIP) is one of the most efficient techniques to produce high quality materials from powders. Nevertheless there is a shortage of data on high-strain-rate behavior and penetration resistance of such materials. In this paper the results of penetration test with tungsten (93%) heavy alloy penetrators of solid and porous composite samples of Ti-6Al-4V alloy with different microstructures (Widmanstatten pattern and equiaxed) are presented. Penetration depth for HIPed materials is smaller than in baseline samples of Ti-6Al-4V alloy (forged rod MIL-T-9047G). Composite materials with alumina rods and tubes filled with B4C powders demonstrated a new features of penetration: projectile deflection with self sealing of hole and forced shear localization caused by tubes fracture. The results demonstrate the applicability of HIPing for Ti-based armor materials.

  6. Hot, cold, and annual reference atmospheres for Edwards Air Force Base, California (1975 version)

    NASA Technical Reports Server (NTRS)

    Johnson, D. L.

    1975-01-01

    Reference atmospheres pertaining to summer (hot), winter (cold), and mean annual conditions for Edwards Air Force Base, California, are presented from surface to 90 km altitude (700 km for the annual model). Computed values of pressure, kinetic temperature, virtual temperature, and density and relative differences percentage departure from the Edwards reference atmospheres, 1975 (ERA-75) of the atmospheric parameters versus altitude are tabulated in 250 m increments. Hydrostatic and gas law equations were used in conjunction with radiosonde and rocketsonde thermodynamic data in determining the vertical structure of these atmospheric models. The thermodynamic parameters were all subjected to a fifth degree least-squares curve-fit procedure, and the resulting coefficients were incorporated into Univac 1108 computer subroutines so that any quantity may be recomputed at any desired altitude using these subroutines.

  7. Wind-Based Navigation of a Hot-air Balloon on Titan: A Feasibility Study

    NASA Technical Reports Server (NTRS)

    Furfaro, Roberto; Lunine, Jonathan I.; Elfes, Alberto; Reh, Kim

    2008-01-01

    Current analysis of data streamed back to Earth by the Cassini spacecraft features Titan as one of the most exciting places in the solar system. NASA centers and universities around the US, as well as the European Space Agency, are studying the possibility of sending, as part of the next mission to this giant moon of Saturn, a hot-air balloon (Montgolfier-type) for further and more in-depth exploration. The basic idea would be to design a reliable, semi-autonomous, and yet cheap Montgolfier capable of using continuous flow of waste heat from a power source to lift the balloon and sustain its altitude in the Titan environment. In this paper we study the problem of locally navigating a hot-air balloon in the nitrogen-based Titan atmosphere. The basic idea is to define a strategy (i.e. design of a suitable guidance system) that allows autonomous and semi-autonomous navigation of the balloon using the available (and partial) knowledge of the wind structure blowing on the saturnian satellite surface. Starting from first principles we determined the appropriate thermal and dynamical models describing (a) the vertical dynamics of the balloon and (b) the dynamics of the balloon moving on a vertical plane (2-D motion). Next, various non-linear fuzzy-based control strategies have been evaluated, analyzed and implemented in MATLAB to numerically simulate the capability of the system to simultaneously maintain altitude, as well as a scientifically desirable trajectory. We also looked at the ability of the balloon to perform station keeping. The results of the simulation are encouraging and show the effectiveness of such a system to cheaply and effectively perform semiautonomous exploration of Titan.

  8. The ERESE Project: Enactment of Digital Library Inquiry-Based Plate Tectonic Lessons

    NASA Astrophysics Data System (ADS)

    Helly, M.; Symons, C. M.; Dow, N.; Miller, S. P.; Helly, J.; Staudigel, H.; Koppers, A.

    2004-12-01

    The Enduring Resources for Earth Science Education (ERESE) project is a collaborative effort between earth scientists, educators, librarians and data archive managers. Its goal is to develop and maintain a persistent online research and education archive in a digital library environment that supports earth science education in plate tectonics. A major contribution from educators has been the development of inquiry lessons included in the digital library. Fourteen middle and high school teachers from across the country participated in the ERESE Workshop in July 2004. The goal of the workshop was three-fold: to provide the teachers with a research experience based on the digital library materials, to model an inquiry process and to support teachers as they develop inquiry lessons for their students. This process was led by a team of scientists and expert educators. The team used a master template to facilitate the teacher's lesson development. The pedagogical approach outlined in the template reflects a model of scientific thinking the goal of which is to shift from direction by the teacher at the onset of a lesson to a self-directed experience on the part of the student as they engage in the inquiry process and complete the lesson. Two examples of inquiry lessons produced as part of the workshop are reported here. The first investigates the symmetry of magnetic stripes at the northern East Pacific Rise using real marine geophysical data from the digital library. The second inquiry lesson was developed by a participant teacher and has been implemented this academic year by a high school marine science teacher. The lesson investigates the evidence that supports plate tectonics on the basis of the Pangea model. Having already been implemented in the classroom this lesson provides a rigorous testing of the inquiry process and the robustness of the scientific content of the digital library.

  9. Well plate-based perfusion culture device for tissue and tumor microenvironment replication.

    PubMed

    Zhang, W; Gu, Y; Hao, Y; Sun, Q; Konior, K; Wang, H; Zilberberg, J; Lee, W Y

    2015-07-01

    There are significant challenges in developing in vitro human tissue and tumor models that can be used to support new drug development and evaluate personalized therapeutics. The challenges include: (1) working with primary cells which are often difficult to maintain ex vivo, (2) mimicking native microenvironments from which primary cells are harvested, and (3) the lack of culture devices that can support these microenvironments to evaluate drug responses in a high-throughput manner. Here we report a versatile well plate-based perfusion culture device that was designed, fabricated and used to: (1) ascertain the role of perfusion in facilitating the expansion of human multiple myeloma cells and evaluate drug response of the cells, (2) preserve the physiological phenotype of primary murine osteocytes by reconstructing the 3D cellular network of osteocytes, and (3) circulate primary murine T cells through a layer of primary murine intestine epithelial cells to recapitulate the interaction of the immune cells with the epithelial cells. Through these diverse case studies, we demonstrate the device's design features to support: (1) the convenient and spatiotemporal placement of cells and biomaterials into the culture wells of the device; (2) the replication of tissues and tumor microenvironments using perfusion, stromal cells, and/or biomaterials; (3) the circulation of non-adherent cells through the culture chambers; and (4) conventional tissue and cell characterization by plate reading, histology, and flow cytometry. Future challenges are identified and discussed from the perspective of manufacturing the device and making its operation for routine and wide use. PMID:26021852

  10. Design of quasi-static piezoelectric plate based transducers by using topology optimization

    NASA Astrophysics Data System (ADS)

    Motta Mello, Luis Augusto; Yukishigue Kiyono, César; Henrique Nakasone, Paulo; Nelli Silva, Emílio Carlos

    2014-02-01

    Sensors and actuators based on piezoelectric plates have shown relevance in the field of smart structures. Recently, modern design techniques such as the topology optimization method have been applied to design laminated piezoelectric transducers, and design requirements such as maximizing static displacements (actuator design) and output voltages (sensor design) have been employed. However, it may be desirable to keep the transducer working range before its first resonance frequency. In this case, the (displacement or voltage) amplitude is expected to be constant with excitation frequency, which may not be the case when only static design requirements are employed. Thus, considering sensor design, if the amplitude is constant, an undetected change in the excitation frequency would cause a small measurement error. Regarding actuators, on the other hand, if the first resonance frequency is small, oscillations in the response to a step excitation (which is usually applied in quasi-static applications, i.e. applications in which the transducer operates under the first resonance frequency) could be high, ultimately causing overshoot, for instance. Thus, in this work, the topology optimization method has been applied to design piezoelectric transducers considering quasi-static operation, by distributing piezoelectric material over a metallic plate and by selecting the material polarization sign, in order to fulfil quasi-static design requirements. This is achieved by maximizing an objective function that depends on both displacements (for actuators) or output voltages (for sensors), and first resonance frequencies. The applied methodology, which encompasses the optimization problem formulation and numerical implementation, is presented. The achieved computational results, corresponding to the design of different types of transducers, clearly show the potential of the proposed methodology to increase the quasi-static working frequency range.

  11. A study of Gd-based parallel plate avalanche counter for thermal neutrons by MC simulation

    NASA Astrophysics Data System (ADS)

    Rhee, J. T.; Kim, H. G.; Ahmad, Farzana; Jeon, Y. J.; Jamil, M.

    2013-12-01

    In this work, we demonstrate the feasibility and characteristics of a single-gap parallel plate avalanche counter (PPAC) as a low energy neutron detector, based on Gd-converter coating. Upon falling on the Gd-converter surface, the incident low energy neutrons produce internal conversion electrons which are evaluated and detected. For estimating the performance of the Gd-based PPAC, a simulation study has been performed using GEANT4 Monte Carlo (MC) code. The detector response as a function of incident neutron energies in the range of 25-100 meV has been evaluated with two different physics lists. Using the QGSP_BIC_HP physics list and assuming 5 μm converter thickness, 11.8%, 18.48%, and 30.28% detection efficiencies have been achieved for the forward-, the backward-, and the total response of the converter-based PPAC. On the other hand, considering the same converter thickness and detector configuration, with the QGSP_BERT_HP physics list efficiencies of 12.19%, 18.62%, and 30.81%, respectively, were obtained. These simulation results are briefly discussed.

  12. Analytical and experimental investigation of the dispersion process during rapid transients for the aluminum-based nuclear fuel plates

    SciTech Connect

    Georgevich, V.; Taleyarkhan, R.P.; Kim, S.H.; Fuketa, T.; Soyama, K.; Ishijima, K.

    1995-06-01

    A thermally induced fuel-plate dispersion model was developed to analyze for dispersive potential and determine the onset of fuel plate dispersion for aluminum-based research and test reactor fuels. The effect of rapid energy deposition in a fuel plate was simulated. Several data types for aluminum-based fuels tested in the Nuclear Safety Research Reactor (NSRR) facility in Japan and in the Transient Reactor Test (TREAT) facility in Idaho, US, were reviewed. Analyses of experiments show that the onset of fuel dispersion is clearly linked to a sharp rise in the predicted strain rate, which further coincides with the onset of aluminum vaporization. Analysis also shows that aluminum oxidation and exothermal chemical reaction between the fuel and aluminum can significantly affect: the energy deposition characteristics and, therefore dispersion onset connected with aluminum vaporization, and the onset of aluminum vaporization.

  13. Physiological responses of dogs on exposure to hot, arid conditions. Acid-base status.

    PubMed

    Krausz, S; Marder, J

    1977-09-16

    Acid-base parameters were determined in chronically cannulated dogs exposed to ambient temperatures increasing from 25-47 degrees C (with relative humidity below 30%). pH increased from 7.409 +/- 0.004 (S.E.M.) to 7.538 +/- 0.017, PaCO2 decreased from 33.0 +/- 0.5 to 20.9 +/- 1.2 torr, and [HCO3-] decreased from 20.9 +/- 0.3 to 17.2 +/- 0.4 mEq/l. Minimal base excess change, together with a rapid return to normal parameters upon recooling to 25 degrees C, suggests that the stress is almost exclusively respiratory, with little metabolic involvement. Analysis of serial exposures shows no acclimatization effect in acid-base status. This suggests the possible existence of natural acclimation to heat in dogs maintained in a warm climate, permitting excellent tolerance of hot, arid conditions with limited acid-base disturbance. PMID:563058

  14. Kinetics of MN based sorbents for hot coal gas. Quarterly report, September--December 1996

    SciTech Connect

    1996-12-31

    Manganese-based sorbents have been investigated for the removal of hydrogen sulfide (the primary sulfur bearing compound) from hot coal gases prior to its use in combined cycle turbines. Four formulations of Mn-based sorbents were tested in an ambient-pressure fixed-bed reactor to determine steady state H{sub 2}S concentrations, breakthrough times and effectiveness of the sorbent when subjected to cyclic sulfidation and regeneration testing. In a previous report, the sulfidation results were presented. Manganese-based sorbents with molar ratios > 1:1 Mn:Substrate were effective in reducing the H{sub 2}S concentration in simulated coal gases to less than 100 ppmv over five cycles. Actual breakthrough time for formulation C6-2-1100 was as high as 73% of breakthrough time based on wt% Mn in sorbent. In this report, the regeneration results will be presented. Regeneration tests determined that loaded pellets can be fully regenerated in air/steam mixture at 750{degrees}C with minimal sulfate formation. 16 refs., 9 figs., 5 tabs.

  15. Free vibration analysis of plate assemblies using the dynamic stiffness method based on the higher order shear deformation theory

    NASA Astrophysics Data System (ADS)

    Kolarevic, Nevenka; Marjanović, Miroslav; Nefovska-Danilovic, Marija; Petronijevic, Mira

    2016-03-01

    This paper deals with the free vibration analysis of isotropic plate assemblies using the dynamic stiffness method (DSM) based on the Reddy's higher-order shear deformation theory (HSDT). Using the proposed method, the isotropic rectangular plate assemblies of non-uniform thickness and material properties can be analyzed. The proposed model does not have any restrictions regarding the boundary conditions or the frequency limitations. It enables free vibration analysis of both thin and thick plates, making it advantageous in comparison with the conventional finite element method (FEM) regarding the computational cost and the accuracy of the results. Three coupled Euler-Lagrange equations of motion based on the HSDT have been transformed into two uncoupled equations of motion introducing a boundary layer function. The dynamic stiffness matrix for a completely free rectangular plate element has been derived using the superposition and the projection method. The proposed numerical model has been applied in the free vibration analysis of rectangular plate assemblies. Along with the convergence study, the results for natural frequencies have been validated against the existing data from the literature, the previous results from the authors as well as the results obtained by using the finite element software Abaqus. Excellent agreement has been obtained. Finally, a variety of new results is provided as a benchmark for future investigations.

  16. Glued Joint Behavior of Ribs for Wood-Based Composite Plates

    NASA Astrophysics Data System (ADS)

    Frolovs, G.; Rocens, K.; Sliseris, J.

    2015-11-01

    This article presents experimental investigations of composite sandwich plywood plates with cell type core and their connections between skin layers of birch plywood and a core of straight and curved plywood honeycomb-type ribs. This shape of core ribs provides several improvements for these plates in the manufacturing process as well as improves the mechanical properties of plywood plates. This specific form of ribs allows simplifying the manufacturing of these plates although it should be detailed and improved. The most typical cases (series of specimens) were compared to the results obtained from FEM (ANSYS) simulations. All thicknesses of elements are chosen according to plywood supplier assortment. Standard birch plywood (Riga Ply) plates were used - three layer plywood was chosen for skin elements (Surfaces) and three or five layer plywood was chosen for edge elements. Different bond pressures were taken to compare their influence on joint strength and stiffness.

  17. A reactive burn model for shock initiation in a PBX: scaling and separability based on the hot spot concept

    SciTech Connect

    Show, Milton S; Menikoff, Ralph

    2010-01-01

    In the formulation of a reactive burn model for shock initiation, we endeavor to incorporate a number of effects based on the underlying physical concept of hot spot ignition followed by the growth of reaction due to diverging deflagration fronts. The passage of a shock front sets the initial condition for reaction, leading to a fraction of the hot spots that completely burn while others will quench. The form of the rate model is chosen to incorporate approximations based on the physical picture. In particular, the approximations imply scaling relations that are then used to mathematically separate various contributions. That is, the model is modular and refinements can be applied separately without changing the other contributions. For example, the effect of initial temperature, porosity, etc. predominantly enter the characterization of the non-quenching hot spot distribution. A large collection of velocity gauge data is shown to be well represented by the model with a very small number of parameters.

  18. Finite difference based vibration simulation analysis of a segmented distributed piezoelectric structronic plate system

    NASA Astrophysics Data System (ADS)

    Ren, B. Y.; Wang, L.; Tzou, H. S.; Yue, H. H.

    2010-08-01

    Electrical modeling of piezoelectric structronic systems by analog circuits has the disadvantages of huge circuit structure and low precision. However, studies of electrical simulation of segmented distributed piezoelectric structronic plate systems (PSPSs) by using output voltage signals of high-speed digital circuits to evaluate the real-time dynamic displacements are scarce in the literature. Therefore, an equivalent dynamic model based on the finite difference method (FDM) is presented to simulate the actual physical model of the segmented distributed PSPS with simply supported boundary conditions. By means of the FDM, the four-ordered dynamic partial differential equations (PDEs) of the main structure/segmented distributed sensor signals/control moments of the segmented distributed actuator of the PSPS are transformed to finite difference equations. A dynamics matrix model based on the Newmark-β integration method is established. The output voltage signal characteristics of the lower modes (m <= 3, n <= 3) with different finite difference mesh dimensions and different integration time steps are analyzed by digital signal processing (DSP) circuit simulation software. The control effects of segmented distributed actuators with different effective areas are consistent with the results of the analytical model in relevant references. Therefore, the method of digital simulation for vibration analysis of segmented distributed PSPSs presented in this paper can provide a reference for further research into the electrical simulation of PSPSs.

  19. A Pressure Plate-Based Method for the Automatic Assessment of Foot Strike Patterns During Running.

    PubMed

    Santuz, Alessandro; Ekizos, Antonis; Arampatzis, Adamantios

    2016-05-01

    The foot strike pattern (FSP, description of how the foot touches the ground at impact) is recognized to be a predictor of both performance and injury risk. The objective of the current investigation was to validate an original foot strike pattern assessment technique based on the numerical analysis of foot pressure distribution. We analyzed the strike patterns during running of 145 healthy men and women (85 male, 60 female). The participants ran on a treadmill with integrated pressure plate at three different speeds: preferred (shod and barefoot 2.8 ± 0.4 m/s), faster (shod 3.5 ± 0.6 m/s) and slower (shod 2.3 ± 0.3 m/s). A custom-designed algorithm allowed the automatic footprint recognition and FSP evaluation. Incomplete footprints were simultaneously identified and corrected from the software itself. The widely used technique of analyzing high-speed video recordings was checked for its reliability and has been used to validate the numerical technique. The automatic numerical approach showed a good conformity with the reference video-based technique (ICC = 0.93, p < 0.01). The great improvement in data throughput and the increased completeness of results allow the use of this software as a powerful feedback tool in a simple experimental setup. PMID:26471786

  20. A Cell-based PDE4 Assay in 1536-well Plate format for High Throughput Screening

    PubMed Central

    Titus, Steven A.; Li, Xiao; Southall, Noel; Lu, Jianming; Inglese, James; Brasch, Michael; Austin, Christopher P.; Zheng, Wei

    2009-01-01

    The cyclic nucleotide phosphodiesterases (PDEs) are intracellular enzymes that catalyze the hydrolysis of 3', 5'-cyclic nucleotides, such as cyclic adenosine monophosphate (cAMP) and cyclic guanosine monophosphate (cGMP), to their corresponding 5'-nucleotide monophosphates. These enzymes play an important role in controlling cellular concentrations of cyclic nucleotides and thus regulate a variety of cellular signaling events. PDEs are emerging as drug targets for several diseases including asthma, cardiovascular disease, ADHD, Parkinson’s disease, and Alzheimer’s disease. Though biochemical assays with purified recombinant PDE enzymes and cAMP or cGMP substrate are commonly used for compound screening, cell-based assays would provide a better assessment of compound activity in a more physiological context. Here we report the development and validation of a new cell-based PDE4 assay using a constitutively active GPCR as a driving force for cAMP production and a cyclic nucleotide gated (CNG) cation channel as a biosensor in 1536-well plates. PMID:18591513

  1. Analytical modeling of a sandwiched plate piezoelectric transformer-based acoustic-electric transmission channel.

    PubMed

    Lawry, Tristan J; Wilt, Kyle R; Scarton, Henry A; Saulnier, Gary J

    2012-11-01

    The linear propagation of electromagnetic and dilatational waves through a sandwiched plate piezoelectric transformer (SPPT)-based acoustic-electric transmission channel is modeled using the transfer matrix method with mixed-domain two-port ABCD parameters. This SPPT structure is of great interest because it has been explored in recent years as a mechanism for wireless transmission of electrical signals through solid metallic barriers using ultrasound. The model we present is developed to allow for accurate channel performance prediction while greatly reducing the computational complexity associated with 2- and 3-dimensional finite element analysis. As a result, the model primarily considers 1-dimensional wave propagation; however, approximate solutions for higher-dimensional phenomena (e.g., diffraction in the SPPT's metallic core layer) are also incorporated. The model is then assessed by comparing it to the measured wideband frequency response of a physical SPPT-based channel from our previous work. Very strong agreement between the modeled and measured data is observed, confirming the accuracy and utility of the presented model. PMID:23192811

  2. Nanofocusing of hard X-ray free electron laser pulses using diamond based Fresnel zone plates

    PubMed Central

    David, C.; Gorelick, S.; Rutishauser, S.; Krzywinski, J.; Vila-Comamala, J.; Guzenko, V. A.; Bunk, O.; Färm, E.; Ritala, M.; Cammarata, M.; Fritz, D. M.; Barrett, R.; Samoylova, L.; Grünert, J.; Sinn, H.

    2011-01-01

    A growing number of X-ray sources based on the free-electron laser (XFEL) principle are presently under construction or have recently started operation. The intense, ultrashort pulses of these sources will enable new insights in many different fields of science. A key problem is to provide x-ray optical elements capable of collecting the largest possible fraction of the radiation and to focus into the smallest possible focus. As a key step towards this goal, we demonstrate here the first nanofocusing of hard XFEL pulses. We developed diamond based Fresnel zone plates capable of withstanding the full beam of the world's most powerful x-ray laser. Using an imprint technique, we measured the focal spot size, which was limited to 320 nm FWHM by the spectral band width of the source. A peak power density in the focal spot of 4×1017 W/cm2 was obtained at 70 fs pulse length. PMID:22355576

  3. Control of supersonic axisymmetric base flows using passive splitter plates and pulsed plasma actuators

    NASA Astrophysics Data System (ADS)

    Reedy, Todd Mitchell

    An experimental investigation evaluating the effects of flow control on the near-wake downstream of a blunt-based axisymmetric body in supersonic flow has been conducted. To better understand and control the physical phenomena that govern these massively separated high-speed flows, this research examined both passive and active flow-control methodologies designed to alter the stability characteristics and structure of the near-wake. The passive control investigation consisted of inserting splitter plates into the recirculation region. The active control technique utilized energy deposition from multiple electric-arc plasma discharges placed around the base. The flow-control authority of both methodologies was evaluated with experimental diagnostics including particle image velocimetry, schlieren photography, surface flow visualization, pressure-sensitive paint, and discrete surface pressure measurements. Using a blowdown-type wind tunnel reconstructed specifically for these studies, baseline axisymmetric experiments without control were conducted for a nominal approach Mach number of 2.5. In addition to traditional base pressure measurements, mean velocity and turbulence quantities were acquired using two-component, planar particle image velocimetry. As a result, substantial insight was gained regarding the time-averaged and instantaneous near-wake flow fields. This dataset will supplement the previous benchmark point-wise laser Doppler velocimetry data of Herrin and Dutton (1994) for comparison with new computational predictive techniques. Next, experiments were conducted to study the effects of passive triangular splitter plates placed in the recirculation region behind a blunt-based axisymmetric body. By dividing the near-wake into 1/2, 1/3, and 1/4 cylindrical regions, the time-averaged base pressure distribution, time-series pressure fluctuations, and presumably the stability characteristics were altered. While the spatial base pressure distribution was

  4. Can we safely deform a plate to fit every bone? Population-based fit assessment and finite element deformation of a distal tibial plate.

    PubMed

    Harith, Hazreen; Schmutz, Beat; Malekani, Javad; Schuetz, Michael A; Yarlagadda, Prasad K

    2016-03-01

    Anatomically precontoured plates are commonly used to treat periarticular fractures. A well-fitting plate can be used as a tool for anatomical reduction of the fractured bone. Recent studies highlighted that some plates fit poorly for many patients due to considerable shape variations between bones of the same anatomical site. While it is impossible to design one shape that fits all, it is also burdensome for the manufacturers and hospitals to produce, store and manage multiple plate shapes without the certainty of utilization by a patient population. In this study, we investigated the number of shapes required for maximum fit within a given dataset, and if they could be obtained by manually deforming the original plate. A distal medial tibial plate was automatically positioned on 45 individual tibiae, and the optimal deformation was determined iteratively using finite element analysis simulation. Within the studied dataset, we found that: (i) 89% fit could be achieved with four shapes, (ii) 100% fit was impossible through mechanical deformation, and (iii) the deformations required to obtain the four plate shapes were safe for the stainless steel plate for further clinical use. The proposed framework is easily transferable to other orthopaedic plates. PMID:26739124

  5. Surface modification and performance of inexpensive Fe-based bipolar plates for proton exchange membrane fuel cells

    NASA Astrophysics Data System (ADS)

    Bai, Ching-Yuan; Wen, Tse-Min; Huang, Mao-Suan; Hou, Kung-Hsu; Ger, Ming-Der; Lee, Shuo-Jen

    A reforming pack chromization with rolling pretreatment process is utilized to develop inexpensive and high-performance Fe-based metal bipolar plates (SS 420, SS 430, and SS 316 stainless steels) for PEMFC systems. Rolling process is previously performed to reduce the chromizing temperature and generate a coating possessing excellent conductivity and corrosion resistance on the steels during chromization. The power efficiencies of rolled-chromized and simple chromized bipolar plates are compared with graphite bipolar plates employed in PEMFCs. The results show that the rolled-chromized bipolar plates have a corrosion current (I corr) of 7.87 × 10 -8 A cm -2 and an interfacial contact resistance of 9.7 mΩ cm 2. Moreover, the power density of the single cell assembled with rolled-chromized bipolar plates is 0.46 W cm -2, which is very close to that of graphite (0.50 W cm -2), in the tested conditions of this study.

  6. Numerical determination of statistical energy analysis parameters of directly coupled composite plates using a modal-based approach

    NASA Astrophysics Data System (ADS)

    Seçgin, Abdullah

    2013-01-01

    Statistical energy analysis (SEA) parameters such as average modal spacing, coupling loss factor and input power are numerically determined for point connected, directly coupled symmetrically laminated composite plates using a modal-based approach. The approach is an enhancement of classical wave transmission formula. Unlike most of the existing numerical or experimental techniques, the approach uses uncoupled plate modal information and treats substructure by means of averaged modal impedances. The procedure introduced here is verified using analytical definitions of infinite orthotropic plates which physically resemble to laminated plates for (under) specific conditions, and is tested by performing experimental power injection method (PIM) for an actual, right-angled composite structure. In the development process, force and moment transmissions are individually considered in order to be consistent with analytical formulations. Modal information of composite plates is statistically evaluated by the discrete singular convolution method with random boundary conditions. Proposed methodology not only provides an efficient use of SEA method in high frequency vibration analysis of composite structures, but also enhances SEA accuracy in mid frequency region in which conventional SEA fails. Furthermore, the effect of orientation angles of laminations on SEA parameters are also discussed in mid and high frequency regions.

  7. Radiopacity of resin-based materials measured in film radiographs and storage phosphor plate (Digora).

    PubMed

    Sabbagh, Joseph; Vreven, José; Leloup, Gaetane

    2004-01-01

    This study compared the radiopacity of 41 resin-based materials using conventional dental x-ray film (Ultraspeed-D) and a digital system (Digora) based on storage phosphor plate technology. For the film-based technique, optical density measurements were carried out using an X-Rite densitometer. Al equivalents (mm) were calculated as described in the literature using a calibration curve of Optical Density versus the thickness of aluminum. Regarding the digital system after exposures of 0.16 and 0.32 seconds, the images were exported to an image processing software (NIH Image Engineering). An approach similar to that used for optical density was used to generate a calibration curve for gray pixel values. Linear correlations were found between the percentage of fillers by weight and x-ray film radiopacity and the Digora system, and the same coefficient of estimation was recorded (r=0.60; p< or = 0.05). A linear correlation was also observed between the conventional x-ray film technique and the Digora system (r=0.93;p< or = 0.05). Using two different exposure times did not affect the radiopacity. Considerable differences were found among materials of the same category. Flowable resin composites were more radiopaque than dentin, while microfine composites were "radiolucent." Most of the available resin-based materials were more radiopaque than enamel. The radiopacity of resin composites depended on their fillers (percentage and type). Using elements with low atomic numbers (Si) resulted in radiolucent materials, while adding elements with high molecular numbers (Ba, Y, Yb), resulted in radiopaque resin composites. Despite the numerous benefits offered by the digital imaging system (low irradiation dose, instant image, image manipulation), the conventional x-ray film technique seems to be more accurate for radiopacity measurements. PMID:15646224

  8. Paper microzone plates.

    PubMed

    Carrilho, Emanuel; Phillips, Scott T; Vella, Sarah J; Martinez, Andres W; Whitesides, George M

    2009-08-01

    This paper describes 96- and 384-microzone plates fabricated in paper as alternatives to conventional multiwell plates fabricated in molded polymers. Paper-based plates are functionally related to plastic well plates, but they offer new capabilities. For example, paper-microzone plates are thin (approximately 180 microm), require small volumes of sample (5 microL per zone), and can be manufactured from inexpensive materials ($0.05 per plate). The paper-based plates are fabricated by patterning sheets of paper, using photolithography, into hydrophilic zones surrounded by hydrophobic polymeric barriers. This photolithography used an inexpensive formulation photoresist that allows rapid (approximately 15 min) prototyping of paper-based plates. These plates are compatible with conventional microplate readers for quantitative absorbance and fluorescence measurements. The limit of detection per zone loaded for fluorescence was 125 fmol for fluorescein isothiocyanate-labeled bovine serum albumin, and this level corresponds to 0.02 the quantity of analyte per well used to achieve comparable signal-to-noise in a 96-well plastic plate (using a solution of 25 nM labeled protein). The limits of detection for absorbance on paper was approximately 50 pmol per zone for both Coomassie Brilliant Blue and Amaranth dyes; these values were 0.4 that required for the plastic plate. Demonstration of quantitative colorimetric correlations using a scanner or camera to image the zones and to measure the intensity of color, makes it possible to conduct assays without a microplate reader. PMID:19572563

  9. A 1.5 THz hot-electron bolometer mixer operated by a planar diode based local oscillator

    NASA Technical Reports Server (NTRS)

    Tong, C. Y. E.; Meledin, D.; Blundell, R.; Erickson, N.; Mehdi, I.; Goltsman, G.

    2003-01-01

    We have developed a 1.5 THz superconducting NbN Hot-Electron Bolometer mixer. It is oprated by an all-solid-state Local Oscillator comprising of a cascade of 4 planar doublers following an MMIC based W-band power amplifier.

  10. Economic Assessment of Home Co-generation System with PEFC Based on Survey of Hot-water Demand

    NASA Astrophysics Data System (ADS)

    Kato, Takeyoshi; Hino, Norio; Kasugai, Shiori; Suzuoki, Yasuo

    This paper provides a case study of the performance and the economy of micro co-generation system (μCGS) for residential use based on a time series data on the hot-water demand obtained with 1 minute interval for one year. Assuming a simple constant output operation of PEFC, we calculated the composition of hot-water supply from PEFC and backup boiler. When μCGS is equipped with 100L hot-water storage tank, many portions of hot-water output of the PEFC were wasted although the backup boiler must assist to meet the demand concentrated within a short period. Annually, about 88% of the hot-water demand was met by the PEFC and the rest 12% was met by the backup boiler. Even in this case, the primary energy consumption was small as compared to the conventional energy system, because the electricity output from the PEFC could be fully utilized in the household or grid. However, because of a relatively higher price of city gas, the variable energy cost in μCGS was higher than that in the conventional system in the summer season. When the unit cost of PEFC is reduced to about 120, 000 yen/kWe by a mass production, the annual cost on μCGS could be small relative to the conventional system.

  11. Experimental estimation of the hot spot size in Nb-based Josephson tunnel junctions using Abrikosov vortices

    SciTech Connect

    Cristiano, R.; Frunzio, L.; Pagano, S.; Palmieri, V.G.; Lisitskii, M.P.

    1997-11-01

    We report on a new experimental approach to the size estimation of the hot spot induced by ionizing particles in a Josephson tunnel junction. Here, in contrast to the case of a superconducting strip, it is possible to investigate the hot spot dynamics in absence of effects due to the heating induced by the bias current. The reported experiment is based on the motion of Abrikosov vortices, trapped in the thin films constituting the junction electrodes, under 5.6 MeV {alpha}-particle irradiation. The fast time evolution of a hot spot, combined with the presence of Abrikosov vortices, produces a change of the static magnetic field in the junction area and thus a change of the critical current value, I{sub c}. Measurements of I{sub c} during the {alpha}-particle irradiation and in presence of trapped Abrikosov vortices allow to determine the rate of appearance of those I{sub c} changes. The behavior of the average appearance rate as function of the Abrikosov vortices density provides a direct determination of the maximum hot spot area. The experiment is performed on a high quality Nb/Al{endash}AlO{sub x}/Nb junction of circular geometry and with {open_quotes}small{close_quotes} dimensions with respect to the Josephson penetration depth. A value of 4.7{plus_minus}1.2{mu}m{sup 2} is found for the maximum hot spot area. {copyright} {ital 1997 American Institute of Physics.}

  12. Hot corrosion studies of four nickel-base superalloys: B-1900, NASA-TRW VIA, 713C and IN738

    NASA Technical Reports Server (NTRS)

    Fryburg, G. C.; Kohl, F. J.; Stearns, C. A.

    1976-01-01

    The susceptibility to hot corrosion of four nickel base superalloys has been studied at 900 deg and 1000 deg C in one atmosphere of slowly flowing oxygen. Hot corrosion was induced by coating the samples with known doses of NaSO4 and oxidizing the coated samples isothermally on a sensitive microbalance. In general, the order of susceptibility found was: B-1900 is greater than 713C is greater than NASA-TRW VIA and is greater than IN738. This order corresponds to the order of decreasing molybdenum content of the alloys. Chemical evidence for B-1900 indicates that hot corrosion is instigated by acid fluxing of the protective Al2O3 coating by MoO3.

  13. Shotgun metagenomic sequencing based microbial diversity assessment of Lasundra hot spring, India.

    PubMed

    Mangrola, Amit V; Dudhagara, Pravin; Koringa, Prakash; Joshi, C G; Patel, Rajesh K

    2015-06-01

    This is the first report on the metagenomic approach for unveiling the microbial diversity of Lasundra hot spring, Gujarat State, India. High-throughput sequencing of community DNA was performed on an Ion Torrent PGM platform. Metagenome consisted of 606,867 sequences represent 98,567,305 bps size with an average length of 162 bps and 46% G + C content. Metagenome sequence information is available at EBI under EBI Metagenomic database with accession no. ERP009313. MG-RAST assisted community analysis revealed that 99.21% sequences were bacterial origin, 0.43% was fit to eukaryotes and 0.11% belongs to archaea. A total of 29 bacterial, 20 eukaryotic and 4 archaeal phyla were detected. Abundant genera were Bacillus (86.7%), Geobacillus (2.4%), Paenibacillus (1.0%), Clostridium (0.7%) and Listeria (0.5%), that represent 91.52% in metagenome. In functional analysis, Cluster of Orthologous Group (COG) based annotation revealed that 45.4% was metabolism connected and 19.6% falls in poorly characterized group. Subsystem based annotation approach suggests that the 14.0% was carbohydrates, 7.0% was protein metabolism and 3.0% genes for various stress responses together with the versatile presence of commercially useful traits. PMID:26484181

  14. Shotgun metagenomic sequencing based microbial diversity assessment of Lasundra hot spring, India

    PubMed Central

    Mangrola, Amit V.; Dudhagara, Pravin; Koringa, Prakash; Joshi, C.G.; Patel, Rajesh K.

    2015-01-01

    This is the first report on the metagenomic approach for unveiling the microbial diversity of Lasundra hot spring, Gujarat State, India. High-throughput sequencing of community DNA was performed on an Ion Torrent PGM platform. Metagenome consisted of 606,867 sequences represent 98,567,305 bps size with an average length of 162 bps and 46% G + C content. Metagenome sequence information is available at EBI under EBI Metagenomic database with accession no. ERP009313. MG-RAST assisted community analysis revealed that 99.21% sequences were bacterial origin, 0.43% was fit to eukaryotes and 0.11% belongs to archaea. A total of 29 bacterial, 20 eukaryotic and 4 archaeal phyla were detected. Abundant genera were Bacillus (86.7%), Geobacillus (2.4%), Paenibacillus (1.0%), Clostridium (0.7%) and Listeria (0.5%), that represent 91.52% in metagenome. In functional analysis, Cluster of Orthologous Group (COG) based annotation revealed that 45.4% was metabolism connected and 19.6% falls in poorly characterized group. Subsystem based annotation approach suggests that the 14.0% was carbohydrates, 7.0% was protein metabolism and 3.0% genes for various stress responses together with the versatile presence of commercially useful traits. PMID:26484181

  15. Plate motion

    SciTech Connect

    Gordon, R.G. )

    1991-01-01

    The motion of tectonic plates on the earth is characterized in a critical review of U.S. research from the period 1987-1990. Topics addressed include the NUVEL-1 global model of current plate motions, diffuse plate boundaries and the oceanic lithosphere, the relation between plate motions and distributed deformations, accelerations and the steadiness of plate motions, the distribution of current Pacific-North America motion across western North America and its margin, plate reconstructions and their uncertainties, hotspots, and plate dynamics. A comprehensive bibliography is provided. 126 refs.

  16. The application of Fresnel zone plate based projection in optofluidic microscopy

    PubMed Central

    Wu, Jigang; Cui, Xiquan; Lee, Lap Man; Yang, Changhuei

    2009-01-01

    Optofluidic microscopy (OFM) is a novel technique for low-cost, high-resolution on-chip microscopy imaging. In this paper we report the use of the Fresnel zone plate (FZP) based projection in OFM as a cost-effective and compact means for projecting the transmission through an OFM's aperture array onto a sensor grid. We demonstrate this approach by employing a FZP (diameter = 255 μm, focal length = 800 μm) that has been patterned onto a glass slide to project the transmission from an array of apertures (diameter = 1 μm, separation = 10 μm) onto a CMOS sensor. We are able to resolve the contributions from 44 apertures on the sensor under the illumination from a HeNe laser (wavelength = 633 nm). The imaging quality of the FZP determines the effective field-of-view (related to the number of resolvable transmissions from apertures) but not the image resolution of such an OFM system – a key distinction from conventional microscope systems. We demonstrate the capability of the integrated system by flowing the protist Euglena gracilis across the aperture array microfluidically and performing OFM imaging of the samples. PMID:18825198

  17. The application of Fresnel zone plate based projection in optofluidic microscopy.

    PubMed

    Wu, Jigang; Cui, Xiquan; Lee, Lap Man; Yang, Changhuei

    2008-09-29

    Optofluidic microscopy (OFM) is a novel technique for low-cost, high-resolution on-chip microscopy imaging. In this paper we report the use of the Fresnel zone plate (FZP) based projection in OFM as a cost-effective and compact means for projecting the transmission through an OFM's aperture array onto a sensor grid. We demonstrate this approach by employing a FZP (diameter = 255 microm, focal length = 800 microm) that has been patterned onto a glass slide to project the transmission from an array of apertures (diameter = 1 microm, separation = 10 microm) onto a CMOS sensor. We are able to resolve the contributions from 44 apertures on the sensor under the illumination from a HeNe laser (wavelength = 633 nm). The imaging quality of the FZP determines the effective field-of-view (related to the number of resolvable transmissions from apertures) but not the image resolution of such an OFM system--a key distinction from conventional microscope systems. We demonstrate the capability of the integrated system by flowing the protist Euglena gracilis across the aperture array microfluidically and performing OFM imaging of the samples. PMID:18825198

  18. Establishment of ATP-based luciferase viability assay in 96-well plate for Trypanosoma congolense.

    PubMed

    Suganuma, Keisuke; Allamanda, Puttik; Hakimi, Hassan; Zhou, Mo; Angeles, Jose Ma; Kawazu, Shin-ichiro; Inoue, Noboru

    2014-11-01

    Animal African trypanosomosis (AAT), caused by Trypanosoma congolense, is widespread throughout sub-Saharan Africa. There are significant concerns related to the current drugs available for the treatment of AAT due to their limited effectiveness across species and their adverse effects. Moreover, drug resistant trypanosomes have recently been reported in the field. High throughput screening (HTS) of large chemical compound library collections is a promising approach for identifying novel drug candidates. While HTS for Trypanozoon trypanosomes, T. brucei sspp. and T. evansi is well established, no assays have been developed for T. congolense. In the present study, the authors developed an ATP-based luciferase viability assay for T. congolense in a 96-well plate format. The calculated 50% inhibitory concentration (IC50) values for pentamidine and diminazene were 10-100 times higher in T. congolense than in T. brucei. This result suggests that the transporters for the 2 tested compounds differ between T. congolense and T. brucei. This assay could further be applied to screen novel chemical compounds for the treatment of AAT caused by T. congolense. PMID:25056575

  19. Establishment of ATP-Based Luciferase Viability Assay in 96-Well Plate for Trypanosoma congolense

    PubMed Central

    SUGANUMA, Keisuke; ALLAMANDA, Puttik; HAKIMI, Hassan; ZHOU, Mo; ANGELES, Jose Ma.; KAWAZU, Shin-ichiro; INOUE, Noboru

    2014-01-01

    ABSTRACT Animal African trypanosomosis (AAT), caused by Trypanosoma congolense, is widespread throughout sub-Saharan Africa. There are significant concerns related to the current drugs available for the treatment of AAT due to their limited effectiveness across species and their adverse effects. Moreover, drug resistant trypanosomes have recently been reported in the field. High throughput screening (HTS) of large chemical compound library collections is a promising approach for identifying novel drug candidates. While HTS for Trypanozoon trypanosomes, T. brucei sspp. and T. evansi is well established, no assays have been developed for T. congolense. In the present study, the authors developed an ATP-based luciferase viability assay for T. congolense in a 96-well plate format. The calculated 50% inhibitory concentration (IC50) values for pentamidine and diminazene were 10–100 times higher in T. congolense than in T. brucei. This result suggests that the transporters for the 2 tested compounds differ between T. congolense and T. brucei. This assay could further be applied to screen novel chemical compounds for the treatment of AAT caused by T. congolense. PMID:25056575

  20. Vorticity Based Turbulence Model Applied to an Impulsively Moved Flat Plate

    NASA Astrophysics Data System (ADS)

    Kachman, Nicholas

    2009-11-01

    A novel technique to model turbulence by vorticity in solid body rotation is presented. The model is based on simultaneously solving the vorticity equation and the Navier-Stokes equation for a 2-D unsteady boundary layer. Only that vorticity that is in solid body rotation is used to develop perturbation velocities that are then applied to the unsteady boundary layer equations. New vorticity is introduced each time step, when the vorticity equation produces a value different from that calculated by the boundary layer equations. Comparing the numerical results to experimental flow visualization demonstrates similar characteristic traits to a turbulent boundary layer, such as no turbulence until Re ˜ 4.5x10^4, intermittency, velocity ``tubes'' that ejected fluid into and out of the boundary layer, and turbulent decay after leaving the plate. Issues remain with the method. First, the velocity perturbations and boundary layer growth are less than expected. It is believed that this is due to the 2-D nature of the solution and that the move to 3-D and the incorporation of vortex stretching will provide values closer to experimental results. Second, the velocity perturbations cause the mesh Reynolds number to be exceeded, which needs to be addressed in future work.

  1. Efficient finite element modeling of laminated composite plates based on higher-order theory

    NASA Technical Reports Server (NTRS)

    Tessler, Alexander; Saether, Erik

    1990-01-01

    A simple and efficient three-node plate bending element for the analysis of composite laminates is developed from a variational principle. The deformations due to transverse shear and transverse normal effects are accounted for, allowing accurate predictions in the range of thin to thick plates. The methodology incorporates C(exp 0) and C(exp 1) continuous displacement approximations and yields accurate ply-by-ply predictions of all displacement, strain, and stress variables.

  2. GIS-based Reconstruction of Pangaea with Recent Progresses in Plate Tectonics

    NASA Astrophysics Data System (ADS)

    Kwon, O.-H.; Cheong, H.-B.; Lee, Y.-W.

    2012-04-01

    It is now widely accepted that the continents or land masses are constantly, slowly moving, or drifting over the asthenosphere as the sea floors spread in response to the mantle convection. These continents were joined together at one time, some 250 million years ago, in a single giant landmass called Pangaea. Alfred Wegener, who proposed originally the hypothesis of continental drift, succeeded in reconstructing the Pangaea in early 20th century, by gathering evidences such as land features, fossils, and climate change. The shape of Pangaea shown by Wegener is a huge landmass which is in rounded shape close to an oval. The Pangaea of Wegener was found to be in good agreement with the supercontinent which was reconstructed by modern scientists in late 1960s based on concrete and sophisticated sciences such as the plate tectonics. There are a couple of shapes describing the Pangaea by now, other than the Wegener's, that are recognized by the geological community. In spite of profound geological data and development of related-area sciences, uncertainties still remains on the precise shape of Pangaea before the stage of breaking up and drifting apart. In this study, the Pangaea is reconstructed taking the recent progresses of plate tectonics into full consideration with the use of an elaborate Geographical Information System (GIS) mapping technique. For a better visualization of the shape of the supercontinent the equidistant map projection is incorporated to display the Pangaea, where the central point of Pangaea is placed on the center of the map. The Pangaea reconstructed in this way appears in an almost circular shape, which has never been seen in previous studies (Fig. 1). The radius of the circle which circumscribes the Pangaea is about 9 000 km, giving the total area slightly above that of continents and lands of present day, because some of the continental margins were considered as a part of continents. This result suggests us that the Pangaea might have

  3. An Agar-Based Method for Plating Marine Protozoan Parasites of the Genus Perkinsus

    PubMed Central

    Cold, Emma R.; Freyria, Nastasia J.; Martínez Martínez, Joaquín; Fernández Robledo, José A.

    2016-01-01

    The genus Perkinsus includes protozoan parasites of mollusks responsible for losses in the aquaculture industry and hampering the recovery of natural shellfish beds worldwide, and they are a key taxon for understanding intracellular parasitism adaptations. The ability to propagate the parasite in liquid media, in the absence of the host, has been crucial for improving understanding of its biology; however, alternative techniques to grow the parasite are needed to explore other basic aspects of the Perkinsus spp. biology. We optimized a DME: Ham’s F12–5% FBS- containing solid agar medium for plating Perkinsus marinus. This solid medium supported trophozoite propagation both by binary fission and schizogony. Colonies were visible to the naked eye 17 days after plating. We tested the suitability of this method for several applications, including the following: 1) Subcloning P. marinus isolates: single discrete P. marinus colonies were obtained from DME: Ham’s F12–5% FBS– 0.75% agar plates, which could be further propagated in liquid medium; 2) Subcloning engineered Perkinsus mediterraneus MOE[MOE]: GFP by streaking cultures on plates; 3) Chemical susceptibility: Infusing the DME: Ham’s F12–5% FBS– 0.75% agar plates with triclosan resulted in inhibition of the parasite propagation in a dose-dependent manner. Altogether, our plating method has the potential for becoming a key tool for investigating diverse aspects of Perkinsus spp. biology, developing new molecular tools, and for biotechnological applications. PMID:27149378

  4. Dynamic Response of a Rigid Pavement Plate Based on an Inertial Soil

    PubMed Central

    Gibigaye, Mohamed; Yabi, Crespin Prudence; Alloba, I. Ezéchiel

    2016-01-01

    This work presents the dynamic response of a pavement plate resting on a soil whose inertia is taken into account in the design of pavements by rational methods. Thus, the pavement is modeled as a thin plate with finite dimensions, supported longitudinally by dowels and laterally by tie bars. The subgrade is modeled via Pasternak-Vlasov type (three-parameter type) foundation models and the moving traffic load is expressed as a concentrated dynamic load of harmonically varying magnitude, moving straight along the plate with a constant acceleration. The governing equation of the problem is solved using the modified Bolotin method for determining the natural frequencies and the wavenumbers of the system. The orthogonal properties of eigenfunctions are used to find the general solution of the problem. Considering the load over the center of the plate, the results showed that the deflections of the plate are maximum about the middle of the plate but are not null at its edges. It is therefore observed that the deflection decreased 18.33 percent when the inertia of the soil is taken into account. This result shows the possible economic gain when taking into account the inertia of soil in pavement dynamic design. PMID:27382639

  5. Dynamic Response of a Rigid Pavement Plate Based on an Inertial Soil.

    PubMed

    Gibigaye, Mohamed; Yabi, Crespin Prudence; Alloba, I Ezéchiel

    2016-01-01

    This work presents the dynamic response of a pavement plate resting on a soil whose inertia is taken into account in the design of pavements by rational methods. Thus, the pavement is modeled as a thin plate with finite dimensions, supported longitudinally by dowels and laterally by tie bars. The subgrade is modeled via Pasternak-Vlasov type (three-parameter type) foundation models and the moving traffic load is expressed as a concentrated dynamic load of harmonically varying magnitude, moving straight along the plate with a constant acceleration. The governing equation of the problem is solved using the modified Bolotin method for determining the natural frequencies and the wavenumbers of the system. The orthogonal properties of eigenfunctions are used to find the general solution of the problem. Considering the load over the center of the plate, the results showed that the deflections of the plate are maximum about the middle of the plate but are not null at its edges. It is therefore observed that the deflection decreased 18.33 percent when the inertia of the soil is taken into account. This result shows the possible economic gain when taking into account the inertia of soil in pavement dynamic design. PMID:27382639

  6. An Agar-Based Method for Plating Marine Protozoan Parasites of the Genus Perkinsus.

    PubMed

    Cold, Emma R; Freyria, Nastasia J; Martínez Martínez, Joaquín; Fernández Robledo, José A

    2016-01-01

    The genus Perkinsus includes protozoan parasites of mollusks responsible for losses in the aquaculture industry and hampering the recovery of natural shellfish beds worldwide, and they are a key taxon for understanding intracellular parasitism adaptations. The ability to propagate the parasite in liquid media, in the absence of the host, has been crucial for improving understanding of its biology; however, alternative techniques to grow the parasite are needed to explore other basic aspects of the Perkinsus spp. biology. We optimized a DME: Ham's F12-5% FBS- containing solid agar medium for plating Perkinsus marinus. This solid medium supported trophozoite propagation both by binary fission and schizogony. Colonies were visible to the naked eye 17 days after plating. We tested the suitability of this method for several applications, including the following: 1) Subcloning P. marinus isolates: single discrete P. marinus colonies were obtained from DME: Ham's F12-5% FBS- 0.75% agar plates, which could be further propagated in liquid medium; 2) Subcloning engineered Perkinsus mediterraneus MOE[MOE]: GFP by streaking cultures on plates; 3) Chemical susceptibility: Infusing the DME: Ham's F12-5% FBS- 0.75% agar plates with triclosan resulted in inhibition of the parasite propagation in a dose-dependent manner. Altogether, our plating method has the potential for becoming a key tool for investigating diverse aspects of Perkinsus spp. biology, developing new molecular tools, and for biotechnological applications. PMID:27149378

  7. Convenient microtiter plate-based, oxygen-independent activity assays for flavin-dependent oxidoreductases based on different redox dyes

    PubMed Central

    Brugger, Dagmar; Krondorfer, Iris; Zahma, Kawah; Stoisser, Thomas; Bolivar, Juan M; Nidetzky, Bernd; Peterbauer, Clemens K; Haltrich, Dietmar

    2014-01-01

    Flavin-dependent oxidoreductases are increasingly recognized as important biocatalysts for various industrial applications. In order to identify novel activities and to improve these enzymes in engineering approaches, suitable screening methods are necessary. We developed novel microtiter-plate-based assays for flavin-dependent oxidases and dehydrogenases using redox dyes as electron acceptors for these enzymes. 2,6-dichlorophenol-indophenol, methylene green, and thionine show absorption changes between their oxidized and reduced forms in the visible range, making it easy to judge visually changes in activity. A sample set of enzymes containing both flavoprotein oxidases and dehydrogenases – pyranose 2-oxidase, pyranose dehydrogenase, cellobiose dehydrogenase, d-amino acid oxidase, and l-lactate oxidase – was selected. Assays for these enzymes are based on a direct enzymatic reduction of the redox dyes and not on the coupled detection of a reaction product as in the frequently used assays based on hydrogen peroxide formation. The different flavoproteins show low Michaelis constants with these electron acceptor substrates, and therefore these dyes need to be added in only low concentrations to assure substrate saturation. In conclusion, these electron acceptors are useful in selective, reliable and cheap MTP-based screening assays for a range of flavin-dependent oxidoreductases, and offer a robust method for library screening, which could find applications in enzyme engineering programs. PMID:24376171

  8. Investigation of the microbial community in the Odisha hot spring cluster based on the cultivation independent approach

    PubMed Central

    Singh, Archana; Subudhi, Enketeswara; Sahoo, Rajesh Kumar; Gaur, Mahendra

    2016-01-01

    Deulajhari hot spring is located in the Angul district of Odisha. The significance of this hot spring is the presence of the hot spring cluster adjacent to the cold spring which attracts the attention of microbiologists to understand the role of physio-chemical factors of these springs on bacterial community structure. Next-generation sequencing technology helps us to depict the pioneering microflora of any ecological niche based on metagenomic approach. Our study represents the first Illumina based metagenomic study of Deulajhari hot spring DH1, and DH2 of the cluster with temperature 65 °C to 55 °C respectively establishing a difference of 10 °C. Comprehensive study of microbiota of these two hot springs was done using the metagenomic sequencing of 16S rRNA of V3‐V4 region extracting metagenomic DNA from the two hot spring sediments. Sequencing community DNA reported about 28 phyla in spring DH1 of which the majority were Chloroflexi (22.98%), Proteobacteria (15.51%), Acidobacteria (14.51%), Chlorobi (9.52%), Nitrospirae (8.54%), and Armatimonadetes (7.07%), at the existing physiochemical conditions like; temperature 65 °C, pH 8.06, electro conductivity 0.020 dSm− 1, and total organic carbon (TOC) 3.76%. About 40 phyla were detected in cluster DH2 at the existing physiochemical parameters like temperature 55 °C, pH 8.10, electro conductivity 0.019 dSm− 1, and total organic carbon (TOC) 0.58% predominated with Chloroflexi (41.98%), Proteobacteria (10.74%), Nitrospirae (10.01%), Chlorobi (8.73%), Acidobacteria (6.73%) and Planctomycetes (3.73%). Approximately 68 class, 107 order, 171 genus and 184 species were reported in cluster DH1 but 102 class, 180 order, 375 genus and 411 species in cluster DH2. The comparative metagenomics study of the Deulajhari hot spring clusters DH1, and DH2 depicts the differential profile of the microbiota. Metagenome sequences of these two hot spring clusters are deposited to the SRA database and are available in

  9. SHARK: Flight Results of an UHTC-Based Nose Related to USV Hot Structures

    NASA Astrophysics Data System (ADS)

    Gardi, R.; Del Vecchio, A.; Russo, G.; Marino, G.

    2011-05-01

    In the frame of USV program, CIRA is developing different projects aimed to develop new technologies for the future hypersonic vehicles. One of these technological projects is Sharp Hot Structures (SHS) and it is aimed to the realization of innovative thermo- structures, based on innovative material solution, able to sustain the heat loads generated during the hypersonic flight. Because the slender configuration of the USV program vehicles, SHS is focused on sharp geometries, like sharp leading edges and sharp nose cones. CIRA, for many years, is investigating the effectiveness of ultra high temperature ceramic materials (UHTC) by means of numerical simulations, ground testing in plasma torch and in SCIROCCO, the 70MW plasma wind tunnel (PWT) facility at CIRA. More recently CIRA is moving the experimentation in real flight environment, boarding UHTC components on the re-entering space capsules EXPERT and SHARK. The former is a European experimental test bed boarding a couple of UHTC fins, already qualified and integrated on the vehicle. SHARK is a 20kg capsule launched on March the 26th 2010 from Kiruna with the European sounding rocker Maxus-8. During the ascent parabola, the capsule was released and successfully executed its 15 minutes ballistic flight and then re-entered in the atmosphere from a 700km altitude. The capsule has been recovered on July the 1st and all data have been acquired. All the instrumentation worked nicely and the data acquisition continued even after the landing, confirming the robustness of the design.

  10. Resonant plasmonic terahertz detection in vertical graphene-base hot-electron transistors

    SciTech Connect

    Ryzhii, V.; Otsuji, T.; Ryzhii, M.; Mitin, V.; Shur, M. S.

    2015-11-28

    We analyze dynamic properties of vertical graphene-base hot-electron transistors (GB-HETs) and consider their operation as detectors of terahertz (THz) radiation using the developed device model. The GB-HET model accounts for the tunneling electron injection from the emitter, electron propagation across the barrier layers with the partial capture into the GB, and the self-consistent oscillations of the electric potential and the hole density in the GB (plasma oscillations), as well as the quantum capacitance and the electron transit-time effects. Using the proposed device model, we calculate the responsivity of GB-HETs operating as THz detectors as a function of the signal frequency, applied bias voltages, and the structural parameters. The inclusion of the plasmonic effect leads to the possibility of the GB-HET operation at the frequencies significantly exceeding those limited by the characteristic RC-time. It is found that the responsivity of GB-HETs with a sufficiently perfect GB exhibits sharp resonant maxima in the THz range of frequencies associated with the excitation of plasma oscillations. The positions of these maxima are controlled by the applied bias voltages. The GB-HETs can compete with and even surpass other plasmonic THz detectors.

  11. Studies on the hot corrosion of a nickel-base superalloy, Udimet 700

    NASA Technical Reports Server (NTRS)

    Misra, A. K.

    1984-01-01

    The hot corrosion of a nickel-base superalloy, Udimet 700, was studied in the temperature range of 884 to 965 C and with different amounts of Na2SO4. Two different modes of degradation were identified: (1) formation of Na2MoO4 - MoO3 melt and fluxing by this melt, and (2) formation of large interconnected sulfides. The dissolution of Cr2O3, TiO2 in the Na2SO4 melt does not play a significant role in the overall corrosion process. The conditions for the formation of massive interconnected sulfides were identified and a mechanism of degradation due to sulfide formation is described. The formation of Ns2MoO4 - MoO3 melt requires an induction period and various physiochemical processes during the induction period were identified. The factors affecting the length of the induction period were also examined. The melt penetration through the oxide appears to be the prime mode of degradation whether the degradation is due to the formation of sulfides or the formation of the Na2MoO4 - MoO3 melt.

  12. High cycle fatigue and fracture behaviour of a hot isostatically pressed nickel-based superalloy

    NASA Astrophysics Data System (ADS)

    Qiu, Chunlei; Wu, Xinhua

    2014-01-01

    Powder of a nickel-based superalloy, RR1000, has been hot isostatically pressed (HIPped) at a supersolvus temperature and post-HIP heat treated to produce different microstructures. Microstructures were investigated using a scanning electron microscope together with an energy dispersive X-ray spectrometer and a wave-length dispersive X-ray spectrometer. High cycle four-point bending fatigue and tension-tension fatigue tests have been performed on the fabricated samples. It was found that HIPped and aged samples showed the best four-point bending fatigue limit while HIPped and solution-treated and aged samples had the lowest fatigue limit. The four-point bending fatigue crack initiations all occurred from the sample surfaces either at the sites of inclusion clusters or by cleavage through large grains on the surfaces. The tension-tension fatigue crack initiation occurred mainly due to large hafnia inclusion clusters, with lower fatigue lives for samples where inclusions were closer to the surface. Crack initiation at the compact Al2O3 inclusion cluster led to a much higher fatigue life than found when cracks were initiated by large hafnia inclusion clusters. The tension-tension fatigue limits were shown to decrease with increased testing temperature (from room temperature to 700 °C).

  13. Long Rod Penetration Test of Hot Isostatically Pressed Ti-based Targets

    NASA Astrophysics Data System (ADS)

    Nesterenko, Vitali; Indrakanti, Sastry; Singh Brar, N.; Gu, Yabei

    1999-06-01

    Hot Isostatic Pressing (HIP) is one of the most efficient techniques to produce materials from powders. Nevertheless there is a shortage of data on high-strain-rate behavior and penetration resistance of such materials. In this paper the results of penetration test (tungsten rod, velocity 886-960 m/s, diameter D=4.98 mm, L/D=10) with solid and porous composite samples of Ti-6Al-4V alloy with different microstructures (Widmanstatten pattern and equiaxed) will be reported. Milling of rapidly solidified Ti-6Al-4V powders prior to HIPing ensured the equiaxed final microstructure with increased compressive yield strength and microhardness (1180 and 3370 MPa correspondingly). Interstitial content was suitable for armor applications in some of the processing routes. Penetration depth for HIPed materials(14-15 mm) is smaller than in baseline samples of Ti-6Al-4V alloy (forged rod MIL-T-9047G). The results demonstrate the applicability of HIPing for Ti-based composite armor materials.

  14. [A method of temperature measurement for hot forging with surface oxide based on infrared spectroscopy].

    PubMed

    Zhang, Yu-cun; Qi, Yan-de; Fu, Xian-bin

    2012-05-01

    High temperature large forging is covered with a thick oxide during forging. It leads to a big measurement data error. In this paper, a method of measuring temperature based on infrared spectroscopy is presented. It can effectively eliminate the influence of surface oxide on the measurement of temperature. The method can measure the surface temperature and emissivity of the oxide directly using the infrared spectrum. The infrared spectrum is radiated from surface oxide of forging. Then it can derive the real temperature of hot forging covered with the oxide using the heat exchange equation. In order to greatly restrain interference spectroscopy through included in the received infrared radiation spectrum, three interference filter system was proposed, and a group of optimal gap parameter values using spectral simulation were obtained. The precision of temperature measurement was improved. The experimental results show that the method can accurately measure the surface temperature of high temperature forging covered with oxide. It meets the requirements of measurement accuracy, and the temperature measurement method is feasible according to the experiment result. PMID:22827063

  15. Hot coal gas desulfurization with manganese based sorbents. Quarterly report, June--September 1994

    SciTech Connect

    Hepworth, M.T.; Slimane, R.B.

    1994-11-01

    The focus of work being performed on hot coal gas desulfurization at the Morgantown Energy Technology Center is primarily in the use of zinc titanate sorbents; however, prior studies indicated that an alternate sorbent, manganese dioxide-containing ore in mixture with alumina (75 wt% ore + 25 wt% Al{sub 2}O{sub 3}) appears to be a strong contender to zinc-based sorbents. Manganese, for example, has a lower vapor pressure in the elemental state than zinc; hence, it is not as likely to undergo zinc-depletion from the sorbent surface upon loading and regeneration cycles. Also manganese oxide is less readily reduced to the elemental state than iron; hence, the range of reduction potentials for oxygen is somewhat greater than for zinc ferrite. In addition, thermodynamic analysis of the manganese-oxygen-sulfur system shows it to be less amenable to sulfation than zinc ferrite. Also manganese chlorides are much less stable and volatile than zinc chlorides. Potential also exists for utilization of manganese at higher temperatures than zinc ferrite or zinc titanate. This Eighth Quarterly Report documents progress in pelletizing and testing via thermo-gravimetric analysis of individual pellet formulations of manganese ore/alumina combinations and also manganese carbonate/alumina with two binders, dextrin and bentonite.

  16. A high-throughput microtiter plate based method for the determination of peracetic acid and hydrogen peroxide.

    PubMed

    Putt, Karson S; Pugh, Randall B

    2013-01-01

    Peracetic acid is gaining usage in numerous industries who have found a myriad of uses for its antimicrobial activity. However, rapid high throughput quantitation methods for peracetic acid and hydrogen peroxide are lacking. Herein, we describe the development of a high-throughput microtiter plate based assay based upon the well known and trusted titration chemical reactions. The adaptation of these titration chemistries to rapid plate based absorbance methods for the sequential determination of hydrogen peroxide specifically and the total amount of peroxides present in solution are described. The results of these methods were compared to those of a standard titration and found to be in good agreement. Additionally, the utility of the developed method is demonstrated through the generation of degradation curves of both peracetic acid and hydrogen peroxide in a mixed solution. PMID:24260173

  17. Plate reader-based cell viability assays for glioprotection using primary rat optic nerve head astrocytes

    PubMed Central

    Kaja, Simon; Payne, Andrew J.; Naumchuk, Yuliya; Levy, Deborah; Zaidi, Danish H.; Altman, Alexa M.; Nawazish, Saba; Ghuman, Jasleen K.; Gerdes, Bryan C.; Moore, Mark A.; Koulen, Peter

    2015-01-01

    Optic nerve head astrocytes (ONHAs) are the major glia cell type in the non-myelinated optic nerve head where they contribute critically to extracellular matrix synthesis during development and throughout life. In glaucoma, and in related disorders affecting the optic nerve and the optic nerve head, pathological changes include altered astrocyte gene and protein expression resulting in their activation and extracellular matrix remodeling. ONHAs are highly sensitive to mechanical and oxidative stress resulting in the initiation of axon damage early during pathogenesis. Furthermore, ONHAs are crucial for the maintenance of retinal ganglion cell physiology and function. Therefore, glioprotective strategies with the goal to preserve and/or restore the structural and functional viability of ONHA in order to slow glaucoma and related pathologies are of high clinical relevance. Herein, we describe the development of standardized methods that will allow for the systematic advancement of such glioprotective strategies. These include isolation, purification and culture of primary adult rat ONHAs, optimized immunocytochemical protocols for cell type validation, as well as plate reader-based assays determining cellular viability, proliferation and the intracellular redox state. We validated and standardized our protocols by performing a glioprotection study using primary ONHAs. Specifically, we measured protection against exogenously-applied oxidative stress using tert-butylhydroperoxide (tBHP) as a model of disease-mediated oxidative stress in the retina and optic nerve head by the prototypic antioxidant, 6-hydroxy-2,5,7,8-tetramethylchroman-2-carboxylic acid (Trolox). Levels of oxidative stress were increased in the response to exogenously applied tBHP and were assessed by 6-carboxy-2′, 7′ dichlorodihydrofluorescein diacetate (DCFDA) fluorescence. Normalized DCFDA fluorescence showed a maximal 5.1-fold increase; the half-maximal effect (EC50) for tBHP was 212 ± 25

  18. A hot-wire method based thermal conductivity measurement apparatus for teaching purposes

    NASA Astrophysics Data System (ADS)

    Alvarado, S.; Marín, E.; Juárez, A. G.; Calderón, A.; Ivanov, R.

    2012-07-01

    The implementation of an automated system based on the hot-wire technique is described for the measurement of the thermal conductivity of liquids using equipment easily available in modern physics laboratories at high schools and universities (basically a precision current source and a voltage meter, a data acquisition card, a personal computer and a high purity platinum wire). The wire, which is immersed in the investigated sample, is heated by passing a constant electrical current through it, and its temperature evolution, ΔT, is measured as a function of time, t, for several values of the current. A straightforward methodology is then used for data processing in order to obtain the liquid thermal conductivity. The start point is the well known linear relationship between ΔT and ln(t) predicted for long heating times by a model based on a solution of the heat conduction equation for an infinite lineal heat source embedded in an infinite medium into which heat is conducted without convective and radiative heat losses. A criterion is used to verify that the selected linear region is the one that matches the conditions imposed by the theoretical model. As a consequence the method involves least-squares fits in linear, semi-logarithmic (semi-log) and log-log graphs, so that it becomes attractive not only to teach about heat transfer and thermal properties measurement techniques, but also as a good exercise for students of undergraduate courses of physics and engineering learning about these kinds of mathematical functional relationships between variables. The functionality of the experiment was demonstrated by measuring the thermal conductivity in samples of liquids with well known thermal properties.

  19. Hot Coal Gas Desulfurization with manganese-based sorbents. Quarterly report, April--June 1994

    SciTech Connect

    Hepworth, M.T.; Slimane, R.B.

    1994-06-01

    The focus of work being performed on Hot Coal Gas Desulfurization at the Morgantown Energy Technology Center is primarily in the use of zinc titanate sorbents; however, prior studies indicated that an alternate sorbent, manganese dioxide-containing ore in mixture with alumina (75 wt% ore + 25 wt% Al{sub 2}O{sub 3}) appears to be a strong contender to zincbased sorbents. Manganese, for example, has a lower vapor pressure in the elemental state than zinc; hence, it is not as likely to undergo zinc-depletion from the sorbent surface upon loading and regeneration cycles. Also manganese oxide is less readily reduced to the elemental state than iron; hence, the range of reduction potentials for oxygen is somewhat greater than for zinc ferrite. In addition, thermodynamic analysis of the manganese-oxygen-sulfur system shows it to be less amenable to sulfation than zinc ferrite. Also manganese chlorides are much less stable and volatile than zinc chlorides. Potential also exists for utilization of manganese at higher temperatures than zinc ferrite or zinc titanate. This Seventh Quarterly Report documents progress in bench-scale testing of a leading manganese-based sorbent pellets (FORM4-A). This formulation is a high-purity manganese carbonate-based material. This formulation was subjected to 20 consecutive cycles of sulfidation and regeneration at 900{degrees}C in a 2-inch fixed bed reactor. The sulfidation gas was a simulated Tampella U-gas with an increased hydrogen sulfide content of 3% by volume to accelerate the rate of breakthrough, arbitrarily taken as 500 ppmv. Consistent with thermo-gravimetric analysis (TGA) on individual pellets, the fixed bed tests show small improvement in capacity and kinetics with the sulfur-loading capacity being about 22% by weight of the original pellet, which corresponds to approximately 90% bed utilization!

  20. Preparation and characterization of Fe-based bulk metallic glasses in plate form

    NASA Astrophysics Data System (ADS)

    Lavorato, G. C.; Fiore, G.; Castellero, A.; Baricco, M.; Moya, J. A.

    2012-08-01

    Amorphous alloys with composition (at%) Fe48Cr15Mo14C15B6Gd2 (alloy A) and Fe48Cr15Mo14C15B6Y2 (alloy B) were prepared either using pure elements (A and B1) and a commercial AISI430 steel as a base material (B2). When prepared from pure elements both alloys (A and B1) could be cast in plate form with a fixed thickness of 2 mm and variable lengths between 10 and 20 mm by means of copper-mold injection in air atmosphere. In the case of alloy B2, prepared using commercial grade raw materials, rods of 2 mm diameter were obtained. X-ray diffraction and scanning electron microscopy observations confirmed that an amorphous structure was obtained in all the as-cast samples. A minor fraction of crystalline phases (oxides and carbides) was detected on the as-cast surface. Differential scanning calorimetry measurements showed a glass transition temperature at 856 K for alloy A and 841 K for alloy B1, and an onset crystallization temperature of 887 K for alloy A and 885 K for alloy B1. In the case of alloy B2 a slightly different crystallization sequence was observed. Values of hardness (∼13 GPa) and the Young modulus (∼180 GPa) were measured by nanoindentation for both the alloys. The effects of adverse casting conditions (such as air atmosphere, non-conventional injection copper mold casting and partial replacement of pure elements with commercial grade raw materials) on the glass formation and properties of the alloy are discussed.

  1. Total and Viable Legionella pneumophila Cells in Hot and Natural Waters as Measured by Immunofluorescence-Based Assays and Solid-Phase Cytometry ▿†

    PubMed Central

    Parthuisot, N.; Binet, M.; Touron-Bodilis, A.; Pougnard, C.; Lebaron, P.; Baudart, J.

    2011-01-01

    A new method was developed for the rapid and sensitive detection of viable Legionella pneumophila. The method combines specific immunofluorescence (IF) staining using monoclonal antibodies with a bacterial viability marker (ChemChrome V6 cellular esterase activity marker) by means of solid-phase cytometry (SPC). IF methods were applied to the detection and enumeration of both the total and viable L. pneumophila cells in water samples. The sensitivity of the IF methods coupled to SPC was 34 cells liter−1, and the reproducibility was good, with the coefficient of variation generally falling below 30%. IF methods were applied to the enumeration of total and viable L. pneumophila cells in 46 domestic hot water samples as well as in cooling tower water and natural water samples, such as thermal spring water and freshwater samples. Comparison with standard plate counts showed that (i) the total direct counts were always higher than the plate counts and (ii) the viable counts were higher than or close to the plate counts. With domestic hot waters, when the IF assay was combined with the viability test, SPC detected up to 3.4 × 103 viable but nonculturable L. pneumophila cells per liter. These direct IF methods could be a powerful tool for high-frequency monitoring of domestic hot waters or for investigating the occurrence of viable L. pneumophila in both man-made water systems and environmental water samples. PMID:21742913

  2. Total and viable Legionella pneumophila cells in hot and natural waters as measured by immunofluorescence-based assays and solid-phase cytometry.

    PubMed

    Parthuisot, N; Binet, M; Touron-Bodilis, A; Pougnard, C; Lebaron, P; Baudart, J

    2011-09-01

    A new method was developed for the rapid and sensitive detection of viable Legionella pneumophila. The method combines specific immunofluorescence (IF) staining using monoclonal antibodies with a bacterial viability marker (ChemChrome V6 cellular esterase activity marker) by means of solid-phase cytometry (SPC). IF methods were applied to the detection and enumeration of both the total and viable L. pneumophila cells in water samples. The sensitivity of the IF methods coupled to SPC was 34 cells liter(-1), and the reproducibility was good, with the coefficient of variation generally falling below 30%. IF methods were applied to the enumeration of total and viable L. pneumophila cells in 46 domestic hot water samples as well as in cooling tower water and natural water samples, such as thermal spring water and freshwater samples. Comparison with standard plate counts showed that (i) the total direct counts were always higher than the plate counts and (ii) the viable counts were higher than or close to the plate counts. With domestic hot waters, when the IF assay was combined with the viability test, SPC detected up to 3.4 × 10(3) viable but nonculturable L. pneumophila cells per liter. These direct IF methods could be a powerful tool for high-frequency monitoring of domestic hot waters or for investigating the occurrence of viable L. pneumophila in both man-made water systems and environmental water samples. PMID:21742913

  3. Development of a novel bead-based 96-well filtration plate competitive immunoassay for the detection of Gentamycin.

    PubMed

    Ho, Tien Yu Jessica; Chan, Chia-Chung; Chan, KinGho; Wang, Yu Chieh; Lin, Jing-Tang; Chang, Cheng-Ming; Chen, Chien-Sheng

    2013-11-15

    We developed a sensitive, simple, inexpensive and rapid bead-based immunoassay platform, composed of liposomal nanovesicle amplification system, Gentamycin sulfate beads and 96-well filtration plates. In the beginning of the assay, Gentamycin sulfate beads, Gentamycin sulfate and Gentamycin specific antibody were incubated in a bottom-sealed 96-well filtration plate. After incubation, washing was done by running washing buffer through the unsealed filtration plate with only gravity and the antibody-Gentamycin bead complexes were retained in the plate. Fluorescent dye-loaded protein G-liposomal nanovesicles were then added to specifically bind to antibodies on the retained beads. After washing unbound nanovesicles, millions of fluorescent dye molecules were released by adding a detergent solution to lyse liposomal nanovesicles. The limit of detection (LOD) of this novel detection platform in TBS and in skim milk were 52.65 ng/mL and 14.16 ng/mL, which are both sufficient for detecting the 200 ng/mL Codex maximum residual level (MRL). The dynamic ranges were both from each of their LODs to 100 μg/mL. The 50% inhibition concentrations (IC50) in TBS and skim milk were 199.66 ng/mL and 360.81 ng/mL, respectively. We also demonstrated the good specificity of this platform by comparing detection results between pure Gentamycin solution and a mixture solution of 6 different antibiotics including Gentamycin in skim milk. The entire assay with 60 samples was conducted within 2h. In sum, this novel biosensing platform not only fulfilled most benefits of magnetic bead-based assays, but also was inexpensive and convenient by replacing the magnetic separation with filtration plate separation. PMID:23728198

  4. Double channel mechanically tunable terahertz filter based on parallel plate waveguide cavities

    NASA Astrophysics Data System (ADS)

    Chen, Lin; Zhu, Yiming

    2012-12-01

    Theoretical and experimental works were carried out on a double channel mechanically tunable terahertz filter integrated with parallel plate waveguide cavities. The filter includes two rectangular grooves on upper and bottom plates of waveguide, respectively. The filter frequencies can be quasilinearly tuned by altering the overlap length between two rectangle grooves on metal plates. From the experiment, we found low (high) resonant frequency can be adjusted from 0.417(0.346) THz to 0.399(0.374) THz when the overlap length is altered from 0 to 500 μm, respectively. The Q values can reach 46 with the resonant frequency (0.41THz), overlap length (220 μm) and waveguide spacing (650 μm). Theoretical results show good agreement with experiment.

  5. Flyer-Plate-Based Current Diagnostic for Magnetized Liner Inertial Fusion Experiments

    NASA Astrophysics Data System (ADS)

    Reneker, Joseph; Gomez, Matthew; Hess, Mark; Jennings, Christopher

    2015-11-01

    Accurate measurements of the current delivered to Magnetized Liner Inertial Fusion (MagLIF) loads on the Z machine are important for understanding the dynamics of liner implosions. Difficulty acquiring a reliable load current measurement with the standard Z load B-dots has spurred the development of alternative load current diagnostics. Velocimetry of an electromagnetically-accelerated flyer plate can be used to infer the drive current on a flyer surface. A load current diagnostic design is proposed using a cylindrical flyer plate in series with the MagLIF target. Aspects of the flyer plate design were optimized using magnetohydrodynamic simulations. Design and preliminary results will be presented. Sandia National Laboratories is a multi-program laboratory managed and operated by Sandia Corporation, a wholly owned subsidiary of Lockheed Martin Corporation, for the U.S. Department of Energy's National Nuclear Security Administration under contract DE-AC04-94AL85000.

  6. The estimation of material and patch parameters in a PDE-based circular plate model

    NASA Technical Reports Server (NTRS)

    Banks, H. T.; Smith, Ralph C.; Brown, D. E.; Metcalf, Vern L.; Silcox, R. J.

    1995-01-01

    The estimation of material and patch parameters for a system involving a circular plate, to which piezoceramic patches are bonded, is considered. A partial differential equation (PDE) model for the thin circular plate is used with the passive and active contributions form the patches included in the internal and external bending moments. This model contains piecewise constant parameters describing the density, flexural rigidity, Poisson ratio, and Kelvin-Voigt damping for the system as well as patch constants and a coefficient for viscous air damping. Examples demonstrating the estimation of these parameters with experimental acceleration data and a variety of inputs to the experimental plate are presented. By using a physically-derived PDE model to describe the system, parameter sets consistent across experiments are obtained, even when phenomena such as damping due to electric circuits affect the system dynamics.

  7. Caveats and limitations of plate reader-based high-throughput kinetic measurements of intracellular calcium levels

    SciTech Connect

    Heusinkveld, Harm J.; Westerink, Remco H.S.

    2011-08-15

    Calcium plays a crucial role in virtually all cellular processes, including neurotransmission. The intracellular Ca{sup 2+} concentration ([Ca{sup 2+}]{sub i}) is therefore an important readout in neurotoxicological and neuropharmacological studies. Consequently, there is an increasing demand for high-throughput measurements of [Ca{sup 2+}]{sub i}, e.g. using multi-well microplate readers, in hazard characterization, human risk assessment and drug development. However, changes in [Ca{sup 2+}]{sub i} are highly dynamic, thereby creating challenges for high-throughput measurements. Nonetheless, several protocols are now available for real-time kinetic measurement of [Ca{sup 2+}]{sub i} in plate reader systems, though the results of such plate reader-based measurements have been questioned. In view of the increasing use of plate reader systems for measurements of [Ca{sup 2+}]{sub i} a careful evaluation of current technologies is warranted. We therefore performed an extensive set of experiments, using two cell lines (PC12 and B35) and two fluorescent calcium-sensitive dyes (Fluo-4 and Fura-2), for comparison of a linear plate reader system with single cell fluorescence microscopy. Our data demonstrate that the use of plate reader systems for high-throughput real-time kinetic measurements of [Ca{sup 2+}]{sub i} is associated with many pitfalls and limitations, including erroneous sustained increases in fluorescence, limited sensitivity and lack of single cell resolution. Additionally, our data demonstrate that probenecid, which is often used to prevent dye leakage, effectively inhibits the depolarization-evoked increase in [Ca{sup 2+}]{sub i}. Overall, the data indicate that the use of current plate reader-based strategies for high-throughput real-time kinetic measurements of [Ca{sup 2+}]{sub i} is associated with caveats and limitations that require further investigation. - Research Highlights: > The use of plate readers for high-throughput screening of intracellular

  8. Metallic nanofilm half-wave plate based on magnetic plasmon resonance.

    PubMed

    Zhu, Z H; Guo, C C; Liu, K; Ye, W M; Yuan, X D; Yang, B; Ma, T

    2012-02-15

    We proposed and fabricated a nanofilm half-wave plate consisting of periodic arrays of orthogonally coupled slit-hole resonator structures in Au film. Experimental results reveal that 95.2% of energy of the incident linearly polarized light is converted to the perpendicular polarization direction after reflection from the nanostructure. The wave plate is single layer with only 180 nm thickness, which is much thinner than the operation wavelength. Our method can be expanded to other resonant structures or transmitted case. PMID:22344152

  9. Hot N Sour Mantle Soup on Indian Plate During Cretaceous- Evidence from Clumped Isotope and Geochemical Studies of Sung Valley Carbonatite, India

    NASA Astrophysics Data System (ADS)

    Ghosh, P.; Banerjee, Y.; Tiwari, A.; Srivastava, R. K.

    2015-12-01

    Geological processes involved in the formation of Carbonatite rocks are complex and so is the understanding about its formational temperature. Fluid inclusion studies (1) on Carbonatite and their associated Ijolites showed a homogenization temperature of 1000-1100°C for Ijoltes and a temperature (T) range of 200-600°C was assigned to the carbonatite melts. Liquid immiscibility process is held responsible for the origin of parental carbonated (ijolititic/ nephelinitic) magma. The homogenization T signifies about a time interval during which there must be a considerable amount of T dropdown soon after the formation of Ijolite and subsequent crystallization of the residual carbonatite magma. However the lack of information about the T of the primary carbonated melt remains as an important area of petrological research. Experimental studies suggest a T range of 950-1400°C for the primary carbonate melt (2). Advent of Clumped isotope thermometry (3) allowed independent method for estimation of the formational T and provide avenues to derive composition of CO2 in equilibrium with carbonate melt. Earlier attempt involving carbonatites from several locations (4) captured range of T between 83°-416°C . Here we present our observation on calcite growth T in the carbonatites from the Cretaceous Sung valley ultramafic-alkaline-carbonatite complex. Based on stable C,O isotope study and Sr, Nd isotopic composition a mantle origin- genetically linked with the Kerguelen plume was proposed (5). Clumped isotope study on the same samples revealed consistent C and O isotope compositions, providing Δ47 values ranging from 0.32 to 0.48. δ13C and δ18O (in VPDB) values of the present study falls within the "Primary Igneous Carbonatite Field" (6). Using high T thermometry equation (7) we obtained a T range of 137-474 °C for the calcite present in the samples. The T recorded in our study is lower than that deduced experimental values of 960-625°C at 0.1 GPa (8) and fluid inclusion

  10. The propagation of horizontally polarized shear waves in plates bordered with viscous liquid.

    PubMed

    Gitis, Alexander; Sauer, Dirk Uwe

    2016-09-01

    Requirements for ultrasonic horizontally polarized shear waves based viscosity sensors and their applicability for continuous in-line measurement are presented and discussed. The results reveal, that sensors using non-piezoelectric plates as well as wave guides and sensing surface have application-oriented advantages in corrosive and hot liquids. For such non-piezoelectric plate sensors, the dispersion relations are found and the linking equation among propagation velocity as well as attenuation coefficient and Newtonian liquid parameters are obtained. The findings show that in presence of viscous liquids the propagation parameters of horizontally polarized shear waves (HPSW) in non-piezoelectric plate change and a viscosity depending attenuation occurs. It is shown that the measurement sensitivity, in physical terms, of the investigated device highly depends on plate thickness, shear wave impedance of the plate material, and the shear wave impedance of the ambient liquid. Further, reasonable geometrical optimizations and suited plate materials are discussed. PMID:27423968

  11. Hot spot analysis for driving the development of hits into leads in fragment-based drug discovery.

    PubMed

    Hall, David R; Ngan, Chi Ho; Zerbe, Brandon S; Kozakov, Dima; Vajda, Sandor

    2012-01-23

    Fragment-based drug design (FBDD) starts with finding fragment-sized compounds that are highly ligand efficient and can serve as a core moiety for developing high-affinity leads. Although the core-bound structure of a protein facilitates the construction of leads, effective design is far from straightforward. We show that protein mapping, a computational method developed to find binding hot spots and implemented as the FTMap server, provides information that complements the fragment screening results and can drive the evolution of core fragments into larger leads with a minimal loss or, in some cases, even a gain in ligand efficiency. The method places small molecular probes, the size of organic solvents, on a dense grid around the protein and identifies the hot spots as consensus clusters formed by clusters of several probes. The hot spots are ranked based on the number of probe clusters, which predicts the binding propensity of the subsites and hence their importance for drug design. Accordingly, with a single exception the main hot spot identified by FTMap binds the core compound found by fragment screening. The most useful information is provided by the neighboring secondary hot spots, indicating the regions where the core can be extended to increase its affinity. To quantify this information, we calculate the density of probes from mapping, which describes the binding propensity at each point, and show that the change in the correlation between a ligand position and the probe density upon extending or repositioning the core moiety predicts the expected change in ligand efficiency. PMID:22145575

  12. Hot corrosion resistance of high-velocity oxyfuel sprayed coatings on a nickel-base superalloy in molten salt environment

    NASA Astrophysics Data System (ADS)

    Sidhu, T. S.; Prakash, S.; Agrawal, R. D.

    2006-09-01

    No alloy is immune to hot corrosion attack indefinitely. Coatings can extend the lives of substrate materials used at higher temperatures in corrosive environments by forming protective oxides layers that are reasonably effective for long-term applications. This article is concerned with studying the performance of high-velocity oxyfuel (HVOF) sprayed NiCrBSi, Cr3C2-NiCr, Ni-20Cr, and Stellite-6 coatings on a nickel-base superalloy at 900 °C in the molten salt (Na2SO4-60% V2O5) environment under cyclic oxidation conditions. The thermogravimetric technique was used to establish kinetics of corrosion. Optical microscope, x-ray diffraction, scanning electron microscopy/electron dispersive analysis by x-ray (SEM/EDAX), and electron probe microanalysis (EPMA) techniques were used to characterize the as-sprayed coatings and corrosion products. The bare superalloy suffered somewhat accelerated corrosion in the given environmental conditions. whereas hot corrosion resistance of all the coated superalloys was found to be better. Among the coating studied, Ni-20Cr coated superalloy imparted maximum hot corrosion resistance, whereas Stellite-6 coated indicated minimum resistance. The hot corrosion resistance of all the coatings may be attributed to the formation of oxides and spinels of nickel, chromium, or cobalt.

  13. KINETICS OF Mn-BASED SORBENTS FOR HOT COAL GAS DESULFURIZATION

    SciTech Connect

    K.A. SADECKI; M.T. HEPWORTH

    1997-06-15

    Manganese-based sorbents have been investigated for the removal of hydrogen sulfide (the primary sulfur bearing compound) from hot coal gases. Four formulations of Mn-based sorbents were tested in an ambient-pressure fixed-bed reactor to determine steady state H2S concentrations, breakthrough times and effectiveness of the sorbent when subjected to cyclic sulfidation and regeneration testing. In previous reports, the sulfidation and regeneration results from cyclic testing done at 550 and 600 °C were presented. Manganese-based sorbents with molar ratios > 1:1 Mn:Substrate were effective in reducing the H2S concentration in simulated coal gases to less than 100 ppmv over five cycles. Actual breakthrough time for formulation C6-2-1100 was as high as 73% of breakthrough time based on wt% Mn in sorbent at 600 °C. Regeneration tests determined that loaded pellets can be essentially completely regenerated in air/steam mixture at 750 °C with minimal sulfate formation. In this report, the performance of the leading formulation (designated C6-2) was investigated for high temperature removal of H2S from simulated coal-derived fuel gas under varying sorbent induration temperature, reaction temperature, and superficial gas velocity. Sulfidation experiments were performed in an ambient pressure fixed-bed reactor between 500 °C and 600 °C. Four tests were conducted with each test consisting of four cycles of sulfidation and regeneration. Results showed that the induration temperature of the sorbent and the reaction temperature greatly affected the H2S removal capacity of the sorbent while the superficial gas velocity between 1090 and 1635 cm/min had minimal affect on the sorbent's breakthrough capacity. Sorbent also showed 30 to 53% loss of its strength over four cycles of sulfidation and regeneration. The former being sorbent indurated at 1115 °C and the prior being sorbent indurated at 1100 °C.

  14. Air-coupled detection of the S1-ZGV lamb mode in a concrete plate based on backward wave propagation

    NASA Astrophysics Data System (ADS)

    Bjurström, H.; Ryden, N.

    2013-01-01

    Impact Echo is commonly used to determine thickness of concrete plate like structures. The method is based on the generation and detection of the plate thickness resonance frequency, where the group velocity of the first higher symmetric Lamb mode goes to zero (S1-ZGV). When using air-coupled microphones as receivers it is hard to determine the correct resonance frequency due to low signal to noise ratio. In this study multichannel signal processing is used to identify the S1-ZGV frequency, based on backward wave propagation instead of the conventional amplitude spectrum approach. The original PDF file of this article, as supplied to AIP Publishing, contained some minor font problems within Figures 1, 4, 7, 8, and 9. An updated PDF file using the correct font within those figures was issued on June 3, 2013. There are no other changes to the scientific content.

  15. MStern Blotting-High Throughput Polyvinylidene Fluoride (PVDF) Membrane-Based Proteomic Sample Preparation for 96-Well Plates.

    PubMed

    Berger, Sebastian T; Ahmed, Saima; Muntel, Jan; Cuevas Polo, Nerea; Bachur, Richard; Kentsis, Alex; Steen, Judith; Steen, Hanno

    2015-10-01

    We describe a 96-well plate compatible membrane-based proteomic sample processing method, which enables the complete processing of 96 samples (or multiples thereof) within a single workday. This method uses a large-pore hydrophobic PVDF membrane that efficiently adsorbs proteins, resulting in fast liquid transfer through the membrane and significantly reduced sample processing times. Low liquid transfer speeds have prevented the useful 96-well plate implementation of FASP as a widely used membrane-based proteomic sample processing method. We validated our approach on whole-cell lysate and urine and cerebrospinal fluid as clinically relevant body fluids. Without compromising peptide and protein identification, our method uses a vacuum manifold and circumvents the need for digest desalting, making our processing method compatible with standard liquid handling robots. In summary, our new method maintains the strengths of FASP and simultaneously overcomes one of the major limitations of FASP without compromising protein identification and quantification. PMID:26223766

  16. Inkjet-printing- and electroless-plating- based fabrication of RF circuit structures on high-frequency substrates

    NASA Astrophysics Data System (ADS)

    Sridhar, A.; Reiding, J.; Adelaar, H.; Achterhoek, F.; van Dijk, D. J.; Akkerman, R.

    2009-08-01

    In this paper, a method to fabricate radio frequency (RF) circuit structures is described. This method involves inkjet printing of a silver nanoparticle-based ink on a functional substrate material to create the seed track (i.e., the seed layer), onto which copper is subsequently deposited by an electroless plating method, to obtain the desired thickness and conductivity of the RF structures. This process combination was validated by fabricating an S-band filter on a high-frequency substrate and comparing the RF performance of this filter with that of a filter fabricated using the conventional lithography-based method. The adhesion of the circuit structures to the substrate was qualitatively ascertained by the scotch tape test method. The performance of the inkjet-printed-electroless-plated filter was comparable to that of the conventional filter, thus proving the suitability of this novel method for practical RF applications.

  17. A comparison of field-dependent rheological properties between spherical and plate-like carbonyl iron particles-based magneto-rheological fluids

    NASA Astrophysics Data System (ADS)

    Tan Shilan, Salihah; Amri Mazlan, Saiful; Ido, Yasushi; Hajalilou, Abdollah; Jeyadevan, Balachandran; Choi, Seung-Bok; Azhani Yunus, Nurul

    2016-09-01

    This work proposes different sizes of the plate-like particles from conventional spherical carbonyl iron (CI) particles by adjusting milling time in the ball mill process. The ball mill process to make the plate-like particles is called a solid-state powder processing technique which involves repeated welding, fracturing and re-welding of powder particles in a high-energy ball mill. The effect of ball milling process on the magnetic behavior of CI particles is firstly investigated by vibrating sample magnetometer. It is found form this investigation that the plate-like particles have higher saturation magnetization (about 8%) than that of the spherical particles. Subsequently, for the investigation on the sedimentation behavior the cylindrical measurement technique is used. It is observed from this measurement that the plate-like particles show slower sedimentation rate compared to the spherical particles indicating higher stability of the MR fluid. The field-dependent rheological properties of MR fluids based on the plate-like particles are then investigated with respect to the milling time which is directly connected to the size of the plate-like particles. In addition, the field-dependent rheological properties such as the yield stress are evaluated and compared between the plate-like particles based MR fluids and the spherical particles based MR fluid. It is found that the yield shear stress of the plate-like particles based MR fluid is increased up to 270% compared to the spherical particles based MR fluid.

  18. Surface-plasmon enhanced photodetection at communication band based on hot electrons

    NASA Astrophysics Data System (ADS)

    Wu, Kai; Zhan, Yaohui; Wu, Shaolong; Deng, Jiajia; Li, Xiaofeng

    2015-08-01

    Surface plasmons can squeeze light into a deep-subwavelength space and generate abundant hot electrons in the nearby metallic regions, enabling a new paradigm of photoconversion by the way of hot electron collection. Unlike the visible spectral range concerned in previous literatures, we focus on the communication band and design the infrared hot-electron photodetectors with plasmonic metal-insulator-metal configuration by using full-wave finite-element method. Titanium dioxide-silver Schottky interface is employed to boost the low-energy infrared photodetection. The photodetection sensitivity is strongly improved by enhancing the plasmonic excitation from a rationally engineered metallic grating, which enables a strong unidirectional photocurrent. With a five-step electrical simulation, the optimized device exhibits an unbiased responsivity of ˜0.1 mA/W and an ultra-narrow response band (FWHM = 4.66 meV), which promises to be a candidate as the compact photodetector operating in communication band.

  19. Hot Coal Gas Desulfurization with manganese based sorbents. Quarterly report, August 1, 1993--September 30, 1993

    SciTech Connect

    Hepworth, M.T.

    1993-10-01

    The focus of work being performed on Hot Coal Gas Desulfurization at the Morgantown Energy Technology Center is primarily in the use of zinc ferrite and zinc titanate sorbents; however, prior studies at the US Steel Fundamental Research Laboratories in Monroeville, PA, by E. T. Turkdogan indicated that an alternate sorbent, manganese dioxide-containing ore in mixture with alumina (75 wt % ore + 25 wt % Al{sub 2}O{sub 3}) may be a viable alternative to zinc-based sorbents. Manganese, for example, has a lower vapor pressure in the elemental state than zinc hence it is not as likely to undergo depletion from the sorbent surface upon loading and regeneration cycles. Also manganese oxide is less readily reduced to the elemental state than iron hence the range of reduction potentials for oxygen is somewhat greater than for zinc ferrite. In addition, thermodynamic analysis of the manganese-oxygen-sulfur system shows it to be less amenable to sulfation than zinc ferrite. Potential also exists for utilization of manganese at higher temperatures than zinc ferrite or zinc titanate. This report documents progress in pelletizing and testing via thermogravimetric analysis of individual pellet formulations of manganese ore/alumina combinations and also manganese carbonate/alumina with two binders, dextrin and bentonite. Preliminary results indicate that the manganese carbonate material, being of higher purity than the manganese ore, has a higher degree of sulfur capacity and more rapid absorption kinetics. A 2-inch fixed-bed reactor has been fabricated and is now ready for subjecting pellets to cyclic loading and regeneration.

  20. Hot coal gas desulfurization with manganese-based sorbents. Quarterly report, October--December 1993

    SciTech Connect

    Hepworth, M.T.; Slimane, R.B.

    1994-01-01

    The focus of work being performed on Hot Coal Gas Desulfurization at the Morgantown Energy Technology Center is primarily in the use of zinc ferrite and zinc titanate sorbents; however, prior studies indicated that an alternate sorbent, manganese dioxide-containing ore in mixture with alumina (75 wt% ore + 25 wt% Al{sub 2}O{sub 3}) may be a viable alternative to zinc-based sorbents. Manganese, for example, has a lower vapor pressure in the elemental state than zinc hence it is not as likely to undergo depletion from the sorbent surface upon loading and regeneration cycles. Also manganese oxide is less readily reduced to the elemental state than iron hence the range of reduction potentials for oxygen is somewhat greater than for zinc ferrite. In addition, thermodynamic analysis of the manganese-oxygen-sulfur system shows it to be less amenable to sulfation than zinc ferrite. Potential also exists for utilization of manganese at higher temperatures than zinc ferrite or zinc titanate. This Fifth Quarterly Report documents progress in pellet testing via thermogravimetric analysis of pellet formulation FORM4-A of a manganese ore/alumina combination. This formulation, described more fully in the Quarterly Technical Progress Report of October 15, 1993, consists of manganese carbonate combined with alundum. A 2-inch fixed-bed reactor has been fabricated and is now ready for subjecting pellets to cyclic loading and regeneration; however, a minor problem has arisen during the regeneration cycle in that sulfur tends to form and plug the exit tube during the early stage of regeneration. This problem is about to be overcome by increasing the flow rate of air during the regeneration cycle resulting in more oxidizing conditions and hence less tendency for sulfide sulfur (S{sup =}) to oxidize to the intermediate elemental form (S{sup o}) rather than to 4-valent (S{sup +4}).

  1. Hot coal gas desulfurization with manganese-based sorbents. Annual report, September 1992--September 1993

    SciTech Connect

    Hepworth, M.T.

    1993-12-01

    The focus of work being performed on Hot Coal Gas Desulfurization at the Morgantown Energy Technology Center is primarily in the use of zinc ferrite and zinc titanate sorbents; however, prior studies at the US Steel Fundamental Research Laboratories in Monroeville, PA, by E. T. Turkdogan indicated that an alternate sorbent, manganese dioxide-containing ore in mixture with alumina (75 wt % ore + 25 wt % Al{sub 2}O{sub 3}) may be a viable alternative to zinc-based sorbents. Manganese, for example, has a lower vapor pressure in the elemental state than zinc hence it is not as likely to undergo depletion from the sorbent surface upon loading and regeneration cycles. Also manganese oxide is less readily reduced to the elemental state than iron hence the range of reduction potentials for oxygen is somewhat greater than for zinc ferrite. In addition, thermodynamic analysis of the manganese-oxygen-sulfur system shows it to be less amenable to sulfation than zinc ferrite. Potential also exists for utilization of manganese at higher temperatures than zinc ferrite or zinc titanate. This Annual Topical Report documents progress in pelletizing and testing via thermo-gravimetric analysis of individual pellet formulations of manganese ore/ alumina combinations and also manganese carbonate/alumina with two binders, dextrin and bentonite. It includes the prior Quarterly Technical Reports which indicate that the manganese carbonate material, being of higher purity than the manganese ore, has a higher degree of sulfur capacity and more rapid absorption kinetics. A 2-inch fixed-bed reactor has been fabricated and is now ready for subjecting pellets to cyclic loading and regeneration.

  2. Adjoint-based estimation of plate coupling in a non-linear mantle flow model: theory and examples

    NASA Astrophysics Data System (ADS)

    Ratnaswamy, Vishagan; Stadler, Georg; Gurnis, Michael

    2015-08-01

    We develop and validate a systematic approach to infer plate boundary strength and rheological parameters in models of mantle flow from surface velocity observations. Based on a realistic rheological model that includes yielding and strain rate weakening from dislocation creep, we formulate the inverse problem in a Bayesian inference framework. To study the distribution of parameters that are consistent with the observations, we compute the maximum a posteriori (MAP) point, Gaussian approximations of the parameter distribution around that MAP point, and employ Markov Chain Monte Carlo (MCMC) sampling methods. The computation of the MAP point and the Gaussian approximation require first and second derivatives of an objective function subject to non-linear Stokes equations; these derivatives are computed efficiently using adjoint Stokes equations. We set up 2-D numerical experiments with many of the elements expected in a global geophysical inversion. This setup incorporates three subduction zones with slab and weak zone (interplate fault) geometry consistent with average seismic characteristics. With these experiments, we demonstrate that when the temperature field is known, we can recover the strength of plate boundaries, the yield stress and strain rate exponent in the upper mantle. When the number of uncertain parameters increases, there are trade-offs between the inferred parameters. These trade-offs depend on how well the observational data represents the surface velocities, and on the weakness of plate boundaries. As the plate boundary coupling drops below a threshold, the uncertainty of the inferred parameters increases due to insensitivity of plate motion to plate coupling. Comparing the trade-offs between inferred rheological parameters found from the Gaussian approximation of the parameter distribution and from MCMC sampling, we conclude that the Gaussian approximation-which is significantly cheaper to compute-is often a good approximation, in particular

  3. Microstructure and mechanical properties of hip-consolidated Rene 95 powders. [hot-isostatic pressed nickel-based powder metal

    NASA Technical Reports Server (NTRS)

    Shimanuki, Y.; Nishino, Y.; Masui, M.; Doi, H.

    1980-01-01

    The effects of heat-treatments on the microstructure of P/M Rene 95 (a nickel-based powder metal), consolidated by the hot-isostatic pressing (HIP), were examined. The microstructure of as-HIP'd specimen was characterized by highly serrated grain boundaries. Mechanical tests and microstructural observations reveal that the serrated grain boundaries improved ductility at both room and elevated temperatures by retarding crack propagation along grain boundaries.

  4. Homogeneous plate based antibody internalization assay using pH sensor fluorescent dye.

    PubMed

    Nath, Nidhi; Godat, Becky; Zimprich, Chad; Dwight, Stephen J; Corona, Cesear; McDougall, Mark; Urh, Marjeta

    2016-04-01

    Receptor-mediated antibody internalization is a key mechanism underlying several anti-cancer antibody therapeutics. Delivering highly toxic drugs to cancer cells, as in the case of antibody drug conjugates (ADCs), efficient removal of surface receptors from cancer cells and changing the pharmacokinetics profile of the antibody drugs are some of key ways that internalization impacts the therapeutic efficacy of the antibodies. Over the years, several techniques have been used to study antibody internalization including radiolabels, fluorescent microscopy, flow cytometry and cellular toxicity assays. While these methods allow analysis of internalization, they have limitations including a multistep process and limited throughput and are generally endpoint assays. Here, we present a new homogeneous method that enables time and concentration dependent measurements of antibody internalization. The method uses a new hydrophilic and bright pH sensor dye (pHAb dye), which is not fluorescent at neutral pH but becomes highly fluorescent at acidic pH. For receptor mediated antibody internalization studies, antibodies against receptors are conjugated with the pHAb dye and incubated with the cells expressing the receptors. Upon binding to the receptor, the dyes conjugated to the antibody are not fluorescent because of the neutral pH of the media, but upon internalization and trafficking into endosomal and lysosomal vesicles the pH drops and dyes become fluorescent. The enabling attributes of the pHAb dyes are the hydrophilic nature to minimize antibody aggregation and bright fluorescence at acidic pH which allows development of simple plate based assays using a fluorescent reader. Using two different therapeutic antibodies--Trastuzumab (anti-HER2) and Cetuximab (anti-EGFR)--we show labeling with pHAb dye using amine and thiol chemistries and impact of chemistry and dye to antibody ration on internalization. We finally present two new approaches using the pHAb dye, which will be

  5. Hot embossed polyethylene through-hole chips for bead-based microfluidic devices

    PubMed Central

    Chou, Jie; Du, Nan; Ou, Tina; Floriano, Pierre N.; Christodoulides, Nicolaos; McDevitt, John T.

    2013-01-01

    Over the past decade, there has been a growth of interest in the translation of microfluidic systems into real-world clinical practice, especially for use in point-of-care or near patient settings. While initial fabrication advances in microfluidics involved mainly the etching of silicon and glass, the economics of scaling of these materials is not amendable for point-of-care usage where single-test applications forces cost considerations to be kept low and throughput high. As such, a materials base more consistent with point-of-care needs is required. In this manuscript, the fabrication of a hot embossed, through-hole low-density polyethylene ensembles derived from an anisotropically etched silicon wafer is discussed. This semi-opaque polymer that can be easily sterilized and recycled provides low background noise for fluorescence measurements and yields more affordable cost than other thermoplastics commonly used for microfluidic applications such as cyclic olefin copolymer (COC). To fabrication through-hole microchips from this alternative material for microfluidics, a fabrication technique that uses a high-temperature, high-pressure resistant mold is described. This aluminum-based epoxy mold, serving as the positive master mold for embossing, is casted over etched arrays of pyramidal pits in a silicon wafer. Methods of surface treatment of the wafer prior to casting and PDMS casting of the epoxy are discussed to preserve the silicon wafer for future use. Changes in the thickness of polyethylene are observed for varying embossing temperatures. The methodology described herein can quickly fabricate 20 disposable, single use chips in less than 30 minutes with the ability to scale up 4x by using multiple molds simultaneously. When coupled as a platform supporting porous bead sensors, as in the recently developed Programmable Bio-Nano-Chip, this bead chip system can achieve limits of detection, for the cardiac biomarker C-reactive protein, of 0.3 ng/mL, thereby

  6. Hot embossed polyethylene through-hole chips for bead-based microfluidic devices.

    PubMed

    Chou, Jie; Du, Nan; Ou, Tina; Floriano, Pierre N; Christodoulides, Nicolaos; McDevitt, John T

    2013-04-15

    Over the past decade, there has been a growth of interest in the translation of microfluidic systems into real-world clinical practice, especially for use in point-of-care or near patient settings. While initial fabrication advances in microfluidics involved mainly the etching of silicon and glass, the economics of scaling of these materials is not amendable for point-of-care usage where single-test applications force cost considerations to be kept low and throughput high. As such, materials base more consistent with point-of-care needs is required. In this manuscript, the fabrication of a hot embossed, through-hole low-density polyethylene ensembles derived from an anisotropically etched silicon wafer is discussed. This semi-opaque polymer that can be easily sterilized and recycled provides low background noise for fluorescence measurements and yields more affordable cost than other thermoplastics commonly used for microfluidic applications such as cyclic olefin copolymer (COC). To fabrication through-hole microchips from this alternative material for microfluidics, a fabrication technique that uses a high-temperature, high-pressure resistant mold is described. This aluminum-based epoxy mold, serving as the positive master mold for embossing, is casted over etched arrays of pyramidal pits in a silicon wafer. Methods of surface treatment of the wafer prior to casting and PDMS casting of the epoxy are discussed to preserve the silicon wafer for future use. Changes in the thickness of polyethylene are observed for varying embossing temperatures. The methodology described herein can quickly fabricate 20 disposable, single use chips in less than 30 min with the ability to scale up 4 times by using multiple molds simultaneously. When coupled as a platform supporting porous bead sensors, as in the recently developed Programmable Bio-Nano-Chip, this bead chip system can achieve limits of detection, for the cardiac biomarker C-reactive protein, of 0.3 ng/mL, thereby

  7. KINETICS OF Mn-BASED SORBENTS FOR HOT COAL GAS DESULFURIZATION

    SciTech Connect

    J.J. BERNS; K.A. SADECKI; M.T. HEPWORTH

    1997-09-15

    Mixed manganese oxide sorbents have been investigated for high-temperature removal of hydrogen sulfide (the primary sulfur bearing compound) from hot coal gases. The sorbents were screened by thermodynamic equilibrium considerations for sulfidation. Preliminary experimental work using thermogravimetric analysis (TGA) indicated titania to be a superior substrate than alumina. Four formulations showing superior reactivity in a TGA were then tested in an ambient pressure fixed-bed reactor to determine steady state H 2 S concentrations, breakthrough times and effectiveness of the sorbent when subjected to cyclic sulfidation and regeneration testing. Eight tests were conducted with each test consisting of five cycles of sulfidation and regeneration. Sulfidation occurred at 600 o C using a simulated coal gas at an empty-bed space velocity of approximately 12,000 per hour. Manganese-based sorbents with molar ratios > 1:1 Mn:Substrate were effective in reducing the H 2 S concentration in simulated coal gases to less than 100 ppmv over five cycles. Actual breakthrough time for formulation C6-2-1100 was as high as 73% of breakthrough time based on wt% Mn in sorbent at 600 o C. Regeneration tests determined that loaded pellets can be essentially completely regenerated in an air/steam mixture at 750 o C with minimal sulfate formation. The leading formulation (designated C6-2) from the fixed-bed tests was then further tested under varying sorbent induration temperature, sulfidation temperature and superficial gas velocity. Four tests were conducted with each test consisting of four cycles of sulfidation and regeneration. Results showed that the induration temperature of the sorbent and the reaction temperature greatly affected the H 2 S removal capacity of the sorbent while the superficial gas velocity between 1090 and 1635 cm/min had minimal affect on the sorbent's breakthrough capacity. Testing showed that the sorbent's strength was a strong function of the sorbent induration

  8. Fluorescent protein-based cellular assays analyzed by laser-scanning microplate cytometry in 1536-well plate format.

    PubMed

    Auld, Douglas S; Johnson, Ronald L; Zhang, Ya-qin; Veith, Henrike; Jadhav, Ajit; Yasgar, Adam; Simeonov, Anton; Zheng, Wei; Martinez, Elisabeth D; Westwick, John K; Austin, Christopher P; Inglese, James

    2006-01-01

    Microtiter plate readers have evolved from photomultiplier and charged-coupled device-based readers, where a population-averaged signal is detected from each well, to microscope-based imaging systems, where cellular characteristics from individual cells are measured. For these systems, speed and ease of data analysis are inversely proportional to the amount of data collected from each well. Microplate laser cytometry is a technology compatible with a 1536-well plate format and capable of population distribution analysis. Microplate cytometers such as the Acumen Explorer can monitor up to four fluorescent signals from single objects in microtiter plates with densities as high as 1536 wells. These instruments can measure changes in fluorescent protein expression, cell shape, or simple cellular redistribution events such as cytoplasmic to nuclear translocation. To develop high-throughput screening applications using laser-scanning microplate cytometry, we used green fluorescent protein- and yellow fluorescent protein-expressing cell lines designed to measure diverse biological functions such as nuclear translocation, epigenetic signaling, and G protein-coupled receptor activation. This chapter illustrates the application of microplate laser cytometry to these assays in a manner that is suitable for screening large compound collections in high throughput. PMID:17110211

  9. Computer simulation of fast crack propagation and arrest in steel plate with temperature gradient based on local fracture stress criterion

    SciTech Connect

    Machida, Susumu; Yoshinari, Hitoshi; Aihara, Shuji

    1997-12-31

    A fracture mechanics model for fast crack propagation and arrest is proposed based on the local fracture stress criterion. Dynamic fracture toughness (K{sub D}) for a propagating crack is calculated as a function of crack velocity and temperature. The model is extended to incorporate the effect of unbroken ligament (UL) formed near the plate surfaces and crack-front-tunneling. The model simulates acceleration, deceleration and arrest of a crack in a ESSO or a double-tension test plate with temperature-gradient. Calculated arrested crack lengths compare well with experimental results. It is shown that the conventional crack arrest toughness calculated from applied stress and arrested crack length depends on temperature-gradient and the toughness is not a unique material property.

  10. A high-throughput system for two-hybrid screening based on growth curve analysis in microtiter plates.

    PubMed

    Diaz-Camino, Claudia; Risseeuw, Eddy P; Liu, Enwu; Crosby, William L

    2003-05-15

    The yeast two-hybrid system is a powerful tool for identifying novel protein-protein interactions. In general, biochemical marker genes such as lacZ are exploited for indirect quantification of the interaction, and commonly involve the conduct of rather laborious beta-galactosidase assays. This paper describes a simple alternative method based on growth curve analysis of yeast cultures that is amenable to microtiter plate format, and therefore allows the quantification of large numbers of yeast two-hybrid combinations. The analyzed results of yeast cultures grown in microtiter plates were compared with those obtained from the classical beta-galactosidase assay. We conclude that the method presented here is reproducible, of equal or greater sensitivity than the beta-galactosidase assay, and can be further adapted for application to the conduct of large-scale, automated yeast two-hybrid experiments. PMID:12711337

  11. A numerical model based on closed form solution for elastic stability of thin plates

    NASA Astrophysics Data System (ADS)

    Ciaramella, S.; Migliore, M.; Minutolo, V.; Ruocco, E.

    2010-06-01

    An analytical approach for studying the elastic stability of thin rectangular plates under arbitrary boundary conditions is presented. Because the solution is given in closed-form, the approach can be regarded as "exact" under the Kirchhoff-Love assumption. The proposed procedure allows us to obtain the buckling load and modal displacements that do not depend on the number of elements adopted in the numerical discretization using, say, the finite element method.

  12. Parallel double-plate capacitive proximity sensor modelling based on effective theory

    SciTech Connect

    Li, Nan Zhu, Haiye; Wang, Wenyu; Gong, Yu

    2014-02-15

    A semi-analytical model for a double-plate capacitive proximity sensor is presented according to the effective theory. Three physical models are established to derive the final equation of the sensor. Measured data are used to determine the coefficients. The final equation is verified by using measured data. The average relative error of the calculated and the measured sensor capacitance is less than 7.5%. The equation can be used to provide guidance to engineering design of the proximity sensors.

  13. License plate localization in complex scenes based on oriented FAST and rotated BRIEF feature

    NASA Astrophysics Data System (ADS)

    Wang, Ran; Xia, Yuanchun; Wang, Guoyou; Tian, Jiangmin

    2015-09-01

    Within intelligent transportation systems, fast and robust license plate localization (LPL) in complex scenes is still a challenging task. Real-world scenes introduce complexities such as variation in license plate size and orientation, uneven illumination, background clutter, and nonplate objects. These complexities lead to poor performance using traditional LPL features, such as color, edge, and texture. Recently, state-of-the-art performance in LPL has been achieved by applying the scale invariant feature transform (SIFT) descriptor to LPL for visual matching. However, for applications that require fast processing, such as mobile phones, SIFT does not meet the efficiency requirement due to its relatively slow computational speed. To address this problem, a new approach for LPL, which uses the oriented FAST and rotated BRIEF (ORB) feature detector, is proposed. The feature extraction in ORB is much more efficient than in SIFT and is invariant to scale and grayscale as well as rotation changes, and hence is able to provide superior performance for LPL. The potential regions of a license plate are detected by considering spatial and color information simultaneously, which is different from previous approaches. The experimental results on a challenging dataset demonstrate the effectiveness and efficiency of the proposed method.

  14. Simulation of Bacillus subtilis biofilm growth on agar plate by diffusion–reaction based continuum model

    NASA Astrophysics Data System (ADS)

    Zhang, Xianlong; Wang, Xiaoling; Nie, Kai; Li, Mingpeng; Sun, Qingping

    2016-08-01

    Various species of bacteria form highly organized spatially-structured aggregates known as biofilms. To understand how microenvironments impact biofilm growth dynamics, we propose a diffusion–reaction continuum model to simulate the formation of Bacillus subtilis biofilm on an agar plate. The extended finite element method combined with level set method are employed to perform the simulation, numerical results show the quantitative relationship between colony morphologies and nutrient depletion over time. Considering that the production of polysaccharide in wild-type cells may enhance biofilm spreading on the agar plate, we inoculate mutant colony incapable of producing polysaccharide to verify our results. Predictions of the glutamate source biofilm’s shape parameters agree with the experimental mutant colony better than that of glycerol source biofilm, suggesting that glutamate is rate limiting nutrient for Bacillus subtilis biofilm growth on agar plate, and the diffusion-limited is a better description to the experiment. In addition, we find that the diffusion time scale is of the same magnitude as growth process, and the common-employed quasi-steady approximation is not applicable here.

  15. Simulation of Bacillus subtilis biofilm growth on agar plate by diffusion-reaction based continuum model.

    PubMed

    Zhang, Xianlong; Wang, Xiaoling; Nie, Kai; Li, Mingpeng; Sun, Qingping

    2016-01-01

    Various species of bacteria form highly organized spatially-structured aggregates known as biofilms. To understand how microenvironments impact biofilm growth dynamics, we propose a diffusion-reaction continuum model to simulate the formation of Bacillus subtilis biofilm on an agar plate. The extended finite element method combined with level set method are employed to perform the simulation, numerical results show the quantitative relationship between colony morphologies and nutrient depletion over time. Considering that the production of polysaccharide in wild-type cells may enhance biofilm spreading on the agar plate, we inoculate mutant colony incapable of producing polysaccharide to verify our results. Predictions of the glutamate source biofilm's shape parameters agree with the experimental mutant colony better than that of glycerol source biofilm, suggesting that glutamate is rate limiting nutrient for Bacillus subtilis biofilm growth on agar plate, and the diffusion-limited is a better description to the experiment. In addition, we find that the diffusion time scale is of the same magnitude as growth process, and the common-employed quasi-steady approximation is not applicable here. PMID:27434099

  16. Broadband high-efficiency half-wave plate: a supercell-based plasmonic metasurface approach.

    PubMed

    Ding, Fei; Wang, Zhuoxian; He, Sailing; Shalaev, Vladimir M; Kildishev, Alexander V

    2015-04-28

    We design, fabricate, and experimentally demonstrate an ultrathin, broadband half-wave plate in the near-infrared range using a plasmonic metasurface. The simulated results show that the linear polarization conversion efficiency is over 97% with over 90% reflectance across an 800 nm bandwidth. Moreover, simulated and experimental results indicate that such broadband and high-efficiency performance is also sustained over a wide range of incident angles. To further obtain a background-free half-wave plate, we arrange such a plate as a periodic array of integrated supercells made of several plasmonic antennas with high linear polarization conversion efficiency, consequently achieving a reflection-phase gradient for the cross-polarized beam. In this design, the anomalous (cross-polarized) and the normal (copolarized) reflected beams become spatially separated, hence enabling highly efficient and robust, background-free polarization conversion along with broadband operation. Our results provide strategies for creating compact, integrated, and high-performance plasmonic circuits and devices. PMID:25790895

  17. Solar Sail - Fresnel Zone Plate Lens for a Large Space Based Telescope

    SciTech Connect

    Early, J T

    2002-02-13

    A Fresnel zone plate lens made with solar sail material could be used as the primary optic for a very large aperture telescope on deep space probes propelled by solar sails. The large aperture telescope capability could enable significant science on fly-by missions to the asteroids, Pluto, Kuiper belt or the tort cloud and could also enable meaningful interstellar fly-by missions for laser propelled sails. This type of lens may also have some potential for laser communications and as a solar concentrator. The techniques for fabrication of meter size and larger Fresnel phase plate optics are under development at LLNL, and we are extending this technology to amplitude zone plates made from sail materials. Corrector optics to greatly extend the bandwidth of these Fresnel optics will be demonstrated in the future. This novel telescope concept will require new understanding of the fabrication, deployment and control of gossamer space structures. It will also require new materials technology for fabricating these optics and understanding their long term stability in a space environment.

  18. New Constitutive Model for Hot Deformation Behaviors of Ni-Based Superalloy Considering the Effects of Initial δ Phase

    NASA Astrophysics Data System (ADS)

    Lin, Y. C.; He, Min; Zhou, Mi; Wen, Dong-Xu; Chen, Jian

    2015-09-01

    The hot deformation behaviors of a typical Ni-based superalloy are investigated by uniaxial tensile tests over wide ranges of strain rate and deformation temperature. The experimental results show that the flow stress is sensitive to strain, strain rate, and deformation temperature. Especially, initial δ phase (Ni3Nb) has a special effect on the flow stress. The initial δ phase can enhance the work-hardening behavior and result in the increased peak stress at relatively small strains. With the further straining, the initial δ phase can stimulate the dynamic recrystallization and promote the dynamic-softening behaviors. Considering the synthetical effects of deformation temperature, strain, strain rate, and initial δ phase on the hot deformation behaviors, a new phenomenological constitutive model is proposed. In the proposed model, the peak stress and material constant are expressed as functions of Zener-Hollomon parameter and the initial content of δ phase. A good agreement between the predicted and measured results shows that the proposed model can give an accurate and precise estimate of the hot deformation behaviors for the studied Ni-based superalloy.

  19. Hot Coal Gas Desulfurization with manganese-based sorbents. Second [quarterly] technical report, December 1, 1992--March 1, 1993

    SciTech Connect

    Hepworth, M.T.

    1993-03-01

    At present, the focus of work being performed on Hot Coal Gas Desulfurization is primarily in the use of zinc ferrite and zinc titanate sorbents; however studies at the US Steel Fundamental Research Laboratories in Monroeville, PA, by E. T. Turkdogan indicate that an alternate sorbent, manganese dioxide-containing ore in mixture with alumina (75 wt % ore + 25 wt % Al{sub 2}O{sub 3}) may be a preferable alternative to zinc-based sorbents. A significant domestic source of manganese in Minnesota is being explored for an in situ leach process which has potential for producing large tonnages of solutions which may be ideal for precipitation and recovery of pure manganese as a carbonate in a reactive form. In the current program the following studies will be addressed: Preparation of manganese sorbent pellets and characterization tests on pellets for strength and surface area; analysis of the thermodynamics and kinetics of sulfur removal from hot fuel gases by individual sorbent pellets (loading tests) by thermogravimetric testing; regeneration tests via TGA on individual sorbent pellets by oxidation; and bench-scale testing on sorbent beds in a two-inch diameter reactor. The developed information will be of value to METC in its determination of whether or not a manganese-based regenerable sorbent holds real promise for sulfur cleanup of hot fuel gases. This information is necessary prior to pilot-scale testing leading to commercial development is undertaken.

  20. A multiple linear regression analysis of hot corrosion attack on a series of nickel base turbine alloys

    NASA Technical Reports Server (NTRS)

    Barrett, C. A.

    1985-01-01

    Multiple linear regression analysis was used to determine an equation for estimating hot corrosion attack for a series of Ni base cast turbine alloys. The U transform (i.e., 1/sin (% A/100) to the 1/2) was shown to give the best estimate of the dependent variable, y. A complete second degree equation is described for the centered" weight chemistries for the elements Cr, Al, Ti, Mo, W, Cb, Ta, and Co. In addition linear terms for the minor elements C, B, and Zr were added for a basic 47 term equation. The best reduced equation was determined by the stepwise selection method with essentially 13 terms. The Cr term was found to be the most important accounting for 60 percent of the explained variability hot corrosion attack.

  1. High gas velocity oxidation and hot corrosion testing of oxide dispersion-strengthened nickel-base alloys

    NASA Technical Reports Server (NTRS)

    Deadmore, D. L.; Lowell, C. E.

    1975-01-01

    Several oxide dispersion strengthened (ODS) nickel-base alloys were tested in high velocity gases for cyclic oxidation resistance at temperatures to 1200 C and times to 500 hours and for hot corrosion resistance at 900 C for 200 hours. Nickel-chromium-aluminum ODS alloys were found to have superior resistance to oxidation and hot corrosion when compared to bare and coated nickel-chromium ODS alloys. The best of the alloys tested had compositions of nickel - 15.5 to 16 weight percent chromium with aluminum weight percents between 4.5 and 5.0. All of the nickel-chromium-aluminum ODS materials experienced small weight losses (less than 16 mg/sq cm).

  2. Charge coupled devices vs. microchannel plates in the extreme and far ultraviolet - A comparison based on the latest laboratory measurements

    NASA Technical Reports Server (NTRS)

    Vallerga, J.; Lampton, M.

    1988-01-01

    While microchannel plates (MCPs) have been established as imaging photon counters in the EUV and FUV for some years, CCDs are associated with low light level sensing at visible and near-IR wavelengths. Attention is presently given to recent proposals for CCDs' use as EUV and FUV detectors with quantum efficiencies sometimes exceeding those of MCPs; quantum resolution, format size, dynamic range, and long-term stability are also used as bases of comparison, for the cases of both space-based astronomical and spectroscopic applications.

  3. High loading uranium fuel plate

    DOEpatents

    Wiencek, Thomas C.; Domagala, Robert F.; Thresh, Henry R.

    1990-01-01

    Two embodiments of a high uranium fuel plate are disclosed which contain a meat comprising structured uranium compound confined between a pair of diffusion bonded ductile metal cladding plates uniformly covering the meat, the meat having a uniform high fuel loading comprising a content of uranium compound greater than about 45 Vol. % at a porosity not greater than about 10 Vol. %. In a first embodiment, the meat is a plurality of parallel wires of uranium compound. In a second embodiment, the meat is a dispersion compact containing uranium compound. The fuel plates are fabricated by a hot isostatic pressing process.

  4. Development of carbon nanotube and graphite filled polyphenylene sulfide based bipolar plates for all-vanadium redox flow batteries

    NASA Astrophysics Data System (ADS)

    Caglar, Burak; Fischer, Peter; Kauranen, Pertti; Karttunen, Mikko; Elsner, Peter

    2014-06-01

    In this study, synthetic graphite and carbon nanotube (CNT) filled polyphenylene sulfide (PPS) based bipolar plates are produced by using co-rotating twin-screw extruder and injection molding. Graphite is the main conductive filler and CNTs are used as bridging filler between graphite particles. To improve the dispersion of the fillers and the flow behavior of the composite, titanate coupling agent (KR-TTS) is used. The concentration effect of CNTs and coupling agent on the properties of bipolar plates are examined. At 72.5 wt.% total conductive filler concentration, by addition of 2.5 wt.% CNT and 3 wt.% KR-TTS; through-plane and in-plane electrical conductivities increase from 1.42 S cm-1 to 20 S cm-1 and 6.4 S cm-1 to 57.3 S cm-1 respectively compared to sample without CNTs and additive. Extruder torque value and apparent viscosity of samples decrease significantly with coupling agent and as a result; the flow behavior is positively affected. Flexural strength is improved 15% by addition of 1.25 wt.% CNT. Differential scanning calorimeter (DSC) analysis shows nucleating effect of conductive fillers on PPS matrix. Corrosion measurements, cyclic voltammetry and galvanostatic charge-discharge tests are performed to examine the electrochemical stability and the performance of produced bipolar plates in all-vanadium redox flow battery.

  5. Characterization and fixed-bed testing of a nickel-based hot gas desulfurization sorbent

    SciTech Connect

    Gasper-Galvin, L.D.; Swisher, J.H.; Hammerbeck, K.

    1994-10-01

    The objective of this project was to (1) extend a preliminary investigation completed earlier on dispersed nickel sorbents by developing new processing methods, characterizing sorbent materials more extensively, and evaluating the materials in fixed bed reactor tests, and (2) to determine the feasibility of using dispersed nickel sorbents with reductive regeneration for hot gas desulfurization. One of the properties of nickel that is somewhat unique is that it forms a liquid sulfide at sufficiently high temperatures with high sulfur potentials or H{sub 2}S levels. A eutectic exists in the Ni-S phase diagram at 637 C and a composition of 33.4 wt% or 21.5 wt% S. Under controlled conditions, the formation of a liquid phase can be used to advantage in hot gas desulfurization. Sorbent preparation, the experimental unit, and experimental procedure are described. Results from the sorbent, 24Ni-7Cu-Al{sub 2}O{sub 3}, are given.

  6. An on-axis self-calibration approach for precision rotary metrology stages based on an angular artifact plate

    NASA Astrophysics Data System (ADS)

    Hu, Chuxiong; Zhu, Yu; Hu, Jinchun; Xu, Dengfeng; Zhang, Ming

    2013-08-01

    Precision rotary metrology stages need calibration technology to determine the stage error for the compensation and improvement of angle measurement accuracy. Departing from previous perspectives, we present an on-axis angle self-calibration approach for rotary metrology stages with the utilization of an angular artifact plate. Specifically, the artifact plate with angular mark lines, whose accuracy is not precisely known, is first presented as the assistant tool. Then, the artifact plate is placed in the uncalibrated rotary metrology stage with different alignments to construct independent measurement views. The measurement deviation of each mark line from its nominal angle position is rigidly modeled as a combination of stage error, artifact error, misalignment error and random measurement noise. Based on the circle closure principle and the mathematical definition of axis orientation, the misalignment error of each measurement view can be directly determined by algebraic processing. With the comparison of the different measurement views, transitivity and redundancy can be obtained, and a least-squares calculation law is synthesized to determine the stage error and to meet the challenge of random measurement noise. The designed artifact plate is developed for the explanation of a standard angle self-calibration procedure, and a practical description of how to measure the angular marks of different measurement views is also provided in detail. Computer simulation finally validates that the proposed method can realize the stage error accurately even when there exist various random measurement noises. The proposed strategy essentially provides a novel on-axis angle self-calibration approach with accuracy, simplicity and robustness orientation to meet industrial requirements.

  7. Surface-plasmon enhanced photodetection at communication band based on hot electrons

    SciTech Connect

    Wu, Kai; Zhan, Yaohui E-mail: xfli@suda.edu.cn; Wu, Shaolong; Deng, Jiajia; Li, Xiaofeng E-mail: xfli@suda.edu.cn

    2015-08-14

    Surface plasmons can squeeze light into a deep-subwavelength space and generate abundant hot electrons in the nearby metallic regions, enabling a new paradigm of photoconversion by the way of hot electron collection. Unlike the visible spectral range concerned in previous literatures, we focus on the communication band and design the infrared hot-electron photodetectors with plasmonic metal-insulator-metal configuration by using full-wave finite-element method. Titanium dioxide-silver Schottky interface is employed to boost the low-energy infrared photodetection. The photodetection sensitivity is strongly improved by enhancing the plasmonic excitation from a rationally engineered metallic grating, which enables a strong unidirectional photocurrent. With a five-step electrical simulation, the optimized device exhibits an unbiased responsivity of ∼0.1 mA/W and an ultra-narrow response band (FWHM = 4.66 meV), which promises to be a candidate as the compact photodetector operating in communication band.

  8. Kiln for hot-pressing compacts in a continuous manner

    DOEpatents

    Reynolds, C.D Jr.

    1983-08-08

    The invention is directed to a hot pressing furnace or kiln which is capable of preheating, hot pressing, and cooling a plurality of articles in a sequential and continuous manner. The hot pressing furnace of the present invention comprises an elongated, horizontally disposed furnace capable of holding a plurality of displaceable pusher plates each supporting a die body loaded with refractory or ceramic material to be hot pressed. Each of these plates and the die body supported thereby is sequentially pushed through the preheating zone, a temperature stabilizing and a hot pressing zone, and a cooling zone so as to provide a continuous hot-pressing operation of a plurality of articles.

  9. Kiln for hot-pressing compacts in a continuous manner

    DOEpatents

    Reynolds, Jr., Carl D.

    1985-01-01

    The present invention is directed to a hot pressing furnace or kiln which is capable of preheating, hot pressing, and cooling a plurality of articles in a sequential and continuous manner. The hot pressing furnace of the present invention comprises an elongated, horizontally disposed furnace capable of holding a plurality of displaceable pusher plates each supporting a die body loaded with refractory or ceramic material to be hot pressed. Each of these plates and the die body supported thereby is sequentially pushed through the preheating zone, a temperature stabilizing and a hot pressing zone, and a cooling zone so as to provide a continuous hot-pressing operation of a plurality of articles.

  10. A novel unified dislocation density-based model for hot deformation behavior of a nickel-based superalloy under dynamic recrystallization conditions

    NASA Astrophysics Data System (ADS)

    Lin, Y. C.; Wen, Dong-Xu; Chen, Ming-Song; Chen, Xiao-Min

    2016-09-01

    In this study, a novel unified dislocation density-based model is presented for characterizing hot deformation behaviors in a nickel-based superalloy under dynamic recrystallization (DRX) conditions. In the Kocks-Mecking model, a new softening item is proposed to represent the impacts of DRX behavior on dislocation density evolution. The grain size evolution and DRX kinetics are incorporated into the developed model. Material parameters of the developed model are calibrated by a derivative-free method of MATLAB software. Comparisons between experimental and predicted results confirm that the developed unified dislocation density-based model can nicely reproduce hot deformation behavior, DRX kinetics, and grain size evolution in wide scope of initial grain size, strain rate, and deformation temperature. Moreover, the developed unified dislocation density-based model is well employed to analyze the time-variant forming processes of the studied superalloy.

  11. Graphene-based supercapacitors in the parallel-plate electrode configuration: ionic liquids versus organic electrolytes.

    PubMed

    Shim, Youngseon; Kim, Hyung J; Jung, Younjoon

    2012-01-01

    Supercapacitors with two single-sheet graphene electrodes in the parallel plate geometry are studied via molecular dynamics (MD) computer simulations. Pure 1-ethyl-3-methylimidazolium tetrafluoroborate (EMI+BF4-) and a 1.1 M solution of EMI+BF4- in acetonitrile are considered as prototypes of room-temperature ionic liquids (RTILs) and organic electrolytes. Electrolyte structure, charge density and associated electric potential are investigated by varying the charges and separation of the two electrodes. Multiple charge layers formed in the electrolytes in the vicinity of the electrodes are found to screen the electrode surface charge almost completely. As a result, the supercapacitors show nearly an ideal electric double layer behavior, i.e., the electric potential exhibits essentially a plateau behavior in the entire electrolyte region except for sharp changes in screening zones very close to the electrodes. Due to its small size and large charge separation, BF4- is considerably more efficient in shielding electrode charges than EMI+. In the case of the acetonitrile solution, acetonitrile also plays an important role by aligning its dipoles near the electrodes; however, the overall screening mainly arises from ions. Because of the disparity of shielding efficiency between cations and anions, the capacitance of the positively-charged anode is significantly larger than that of the negatively-charged cathode. Therefore, the total cell capacitance in the parallel plate configuration is primarily governed by the cathode. Ion conductivity obtained via the Green-Kubo (GK) method is found to be largely independent of the electrode surface charge. Interestingly, EMI+BF4- shows higher GK ion conductivity than the 1.1 M acetonitrile solution between two parallel plate electrodes. PMID:22455024

  12. [Research on the temperature field detection method of hot forging based on long-wavelength infrared spectrum].

    PubMed

    Zhang, Yu-Cun; Wei, Bin; Fu, Xian-Bin

    2014-02-01

    A temperature field detection method based on long-wavelength infrared spectrum for hot forging is proposed in the present paper. This method combines primary spectrum pyrometry and three-stage FP-cavity LCTF. By optimizing the solutions of three group nonlinear equations in the mathematical model of temperature detection, the errors are reduced, thus measuring results will be more objective and accurate. Then the system of three-stage FP-cavity LCTF was designed on the principle of crystal birefringence. The system realized rapid selection of any wavelength in a certain wavelength range. It makes the response of the temperature measuring system rapid and accurate. As a result, without the emissivity of hot forging, the method can acquire exact information of temperature field and effectively suppress the background light radiation around the hot forging and ambient light that impact the temperature detection accuracy. Finally, the results of MATLAB showed that the infrared spectroscopy through the three-stage FP-cavity LCTF could meet the requirements of design. And experiments verified the feasibility of temperature measuring method. Compared with traditional single-band thermal infrared imager, the accuracy of measuring result was improved. PMID:24822408

  13. Protection of carbon steel against hot corrosion using thermal spray Si- and Cr-base coatings

    SciTech Connect

    Porcayo-Calderon, J.; Gonzalez-Rodriguez, J.G.; Martinez, L.

    1998-02-01

    A Fe75Si thermal spray coating was applied on the surface of a plain carbon steel baffle plate. Beneath this coating, a Ni20Cr coating was applied to give better adherence to the silicon coating. The baffle was installed in the high-temperature, fireside, corrosion zone of a steam generator. At the same time, an uncoated 304 stainless steel baffle was installed nearby for comparison. For 13 months the boiler burned heavy fuel oil with high contents of vanadium. The samples were studied employing scanning electron microscopy, x-ray microanalysis, and x-ray diffraction techniques. After that, it was possible to inspect the structural state of the components, and it was found that the stainless steel baffle plates were destroyed almost completely by corrosion, whereas the carbon steel coated baffle plate did not suffer a significant attack, showing that the performance of the thermal spray coating was outstanding and that the coating was not attacked by vanadium salts of the molten slag.

  14. Tunable terahertz half-wave plate based on hybridization effect in coupled graphene nanodisks

    NASA Astrophysics Data System (ADS)

    Peng, Jialong; Zhu, Zhihong; Zhang, Jianfa; Yuan, Xiaodong; Qin, Shiqiao

    2016-05-01

    We demonstrate a tunable terahertz half-wave plate composed of a periodic array of graphene nanodisk dimers supported on a dielectric spacer backed by a planar gold layer. The polarization conversion phenomena are attributed to the hybridization effect caused by coupling interactions between plasmonic resonances in the graphene nanodisk dimers. By varying the distance between graphene nanodisks, the polarization conversion performance can be controlled. Further, the polarization conversion can be dynamically tuned at different frequencies via electrostatic doping of graphene. Other novel phenomena and applications could be developed from coupled graphene structures in the future.

  15. Optomechanical design of near-null subaperture test system based on counter-rotating CGH plates

    NASA Astrophysics Data System (ADS)

    Li, Yepeng; Chen, Shanyong; Song, Bing; Li, Shengyi

    2014-09-01

    In off-axis subapertures of most convex aspheres, astigmatism and coma dominate the aberrations with approximately quadratic and linear increase as the off-axis distance increases. A pair of counter-rotating computer generated hologram (CGH) plates is proposed to generate variable amount of Zernike terms Z4 and Z6, correcting most of the astigmatism and coma for subapertures located at different positions on surfaces of various aspheric shapes. The residual subaperture aberrations are then reduced within the vertical range of measurement of the interferometer, which enables near-null test of aspheres flexibly. The alignment tolerances for the near-null optics are given with optomechanical analysis. Accordingly a novel design for mounting and aligning the CGH plates is proposed which employs three concentric rigid rings. The CGH plate is mounted in the inner ring which is supported by two couples of ball-end screws in connection with the middle ring. The CGH plate along with the inner ring is hence able to be translated in X-axis and tipped by adjusting the screws. Similarly the middle ring is able to be translated in Y-axis and tilted by another two couples of screws orthogonally arranged and connected to the outer ring. This design is featured by the large center-through hole, compact size and capability of four degrees-of-freedom alignment (lateral shift and tip-tilt). It reduces the height measured in the direction of optical axis as much as possible, which is particularly advantageous for near-null test of convex aspheres. The CGH mounts are then mounted on a pair of center-through tables realizing counter-rotation. Alignment of the interferometer, the CGHs, the tables and the test surface is also discussed with a reasonable layout of the whole test system. The interferometer and the near-null optics are translated by a three-axis stage while the test mirror is rotated and tilted by two rotary tables. Experimental results are finally given to show the near

  16. Preliminary design of a zone plate based hard X-ray monochromatic diffraction nanoprobe for materials studies at APS

    NASA Astrophysics Data System (ADS)

    Cai, Zhonghou; Liu, Wenjun; Tischler, Jonathan Z.; Shu, Deming; Xu, Ruqing; Schmidt, Oliver

    2013-09-01

    Aiming at studies of the micro/nano-structures of a broad range materials and electronic devices, Advance Photon Source (APS) is developing a dedicated diffraction nanoprobe (DNP) beamline for the needs arising from a multidiscipline research community. As a part of the APS Upgrade Project, the planed facility, named Sub-micron 3-D Diffraction (S3DD) beamline1, integrates the K-B mirror based polychromatic Laue diffraction and the Fresnel zone-plate based monochromatic diffraction techniques that currently support 3D/2D microdiffraction programs at the 34-ID-E and 2-ID-D of the APS, respectively. Both diffraction nanoprobes are designed to have a 50-nm or better special resolution. The zone-plate based monochromatic DNP has been preliminarily designed and will be constructed at the sector 34-ID. It uses an APS-3.0-cm period or APS-3.3-cm period undulator, a liquid-nitrogen cooled mirror as its first optics, and a water cooled small gap silicon double-crystal monochromator with an energy range of 5-30 keV. A set of zone plates have been designed to optimize for focusing efficiency and the working distance based on the attainable beamline length and the beam coherence. To ensure the nanoprobe performance, high stiffness and high precision flexure stage systems have been designed or demonstrated for optics mounting and sample scanning, and high precision temperature control of the experimental station will be implemented to reduce thermal instability. Designed nanoprobe beamline has a good management on thermal power loading on optical components and allows high degree of the preservation of beam brilliance for high focal flux and coherence. Integrated with variety of X-ray techniques, planed facility provides nano-XRD capability with the maximum reciprocal space accessibility and allows micro/nano-spectroscopy studies with K-edge electron binding energies of most elements down to Vanadium in the periodic table. We will discuss the preliminary design of the zone-plate

  17. Flat-plate solar-collector performance data base and user's manual

    NASA Astrophysics Data System (ADS)

    Kirkpatrick, D. L.; Kolar, W. A.

    1983-07-01

    The reader is provided with a thorough understanding on the type of collector thermal performance information which is required in active system design and analysis. Thermal performance test data on 109 commercially available solar collectors which were evaluated in a single, uniform test program, the Interim Solar Collector Test (ISCT) Program are given. In addition to recounting the ISCT program and its results, the an introduction is given on the engineering and physics of a flat-plate solar collector operation. A step-by-step analysis of heat gains and losses is provided to help the reader understand both the source and applicability of the parameters used to describe collector thermal performance. A brief description of the engineering basis for the ASHRAE Standard 93-77 test procedure and the method are included. To demonstrate the sensitivity to variations of collector performance parameters of the annual output of representative solar heating systems, three sets of F-Chart (4.0) system performance predictions are given. Finally, a sensitivity analysis study is presented which considers the heat loss and optical gain parameters of flat-plate collectors, in terms of how they affect the overall solar heating system solar fraction.

  18. Outcomes and complications based on experience with resorbable plates in pediatric craniosynostosis patients.

    PubMed

    Ahmad, Nawaiz; Lyles, James; Panchal, Jayesh; Deschamps-Braly, Jordan

    2008-05-01

    The structure and functional relationship of polymers have long been the purview of engineers and polymer chemists. Bioabsorbable fixation devices have been used for decades as dissolvable suture meshes and, recently, routinely by orthopedic surgeons. During the past decade, bioabsorbable fixation systems have become available for use by craniomaxillofacial surgeons for cranial vault remodeling. This study evaluates the application of a bioabsorbable fixation system in reconstructive craniofacial procedures in a pediatric population. We reviewed 146 cases of cranial vault reconstruction including 98 boys and 48 girls ranging from 2 months to 16 years (mean, 15 months) in age. The procedures were performed for 6 years between January 1998 and June 2004. Bioabsorbable plates and screws were used in each case; most of these cases were craniosynostosis reconstructions. There were 69 cases of frontal sagittal craniosynostosis, 36 metopic, 20 unicoronal, 12 bicoronal, 5 lamboid, 2 deformational plagiocephaly, and 2 multiple fusion of sutures. Postoperative evaluation consisted of clinical examination and three-dimensional computed tomography scan reconstructions at 3, 6, and 12 months. Items specifically screened for on the clinical examination included wound healing, signs of infection, and palpability of implant through the skin. Six patients had palpable plates, 2 patients had palpable screw, and 5 patients had infection at the incision site (of which only 3 were treated with inpatient care including incision drainage and intravenous antibiotics). Our experience has been overwhelmingly positive, and we feel that our results suggest that resorbable fixation is a superior option in pediatric plastic and craniofacial surgery. PMID:18520420

  19. r-adaptive methods based on element-level error indicators for parallel analysis of plates and shells

    NASA Technical Reports Server (NTRS)

    Militello, Carmelo; Felippa, Carlos A.

    1992-01-01

    The formulation and application of element-level error indicators based on parametrized variational principles are investigated. These indicators are ideally suited to drive adaptive mesh refinment on parallel computers where access to neighboring elements resident on different processors may incur significant computational overhead. Furthermore, such estimators are not affected by physical jumps at wavefronts or interfaces. An estimator derived from the higher-order element energy is applied to r adaptation of meshes in plates and shell structures where the exact solution is known.

  20. On 3-D inelastic analysis methods for hot section components (base program)

    NASA Technical Reports Server (NTRS)

    Wilson, R. B.; Bak, M. J.; Nakazawa, S.; Banerjee, P. K.

    1986-01-01

    A 3-D Inelastic Analysis Method program is described. This program consists of a series of new computer codes embodying a progression of mathematical models (mechanics of materials, special finite element, boundary element) for streamlined analysis of: (1) combustor liners, (2) turbine blades, and (3) turbine vanes. These models address the effects of high temperatures and thermal/mechanical loadings on the local (stress/strain)and global (dynamics, buckling) structural behavior of the three selected components. Three computer codes, referred to as MOMM (Mechanics of Materials Model), MHOST (Marc-Hot Section Technology), and BEST (Boundary Element Stress Technology), have been developed and are briefly described in this report.

  1. Liquid extraction surface analysis (LESA) of hydrophobic TLC plates coupled to chip-based nanoelectrospray high-resolution mass spectrometry.

    PubMed

    Himmelsbach, Markus; Varesio, Emmanuel; Hopfgartner, Gérard

    2014-01-01

    Direct identification and structural characterization of analyte spots on TLC plates have always been of great interest and the development of interfaces that allow TLC to be combined with MS is making steady progress. The recently introduced liquid extraction surface analysis (LESA) approach has the potential to hyphenate TLC with MS. A mixture of lipid standards was separated on HPTLC RP-18 glass plates using chloroform:methanol :acetonitrile 2:1:1 (v:v:v) as mobile phase. After visualization with primuline dye (0.02% in acetone:water 8:2 (v:v)), LESA was performed, followed by a chip-based nanoflow infusion in combination with FTICRMS. The optimized extraction solvent composition was methanol:chloroform:water:formic acid 52:24:24:0.2 (v:v:v:v). A nanoelectrospray voltage of 1.6 kV and a gas pressure of 0.2 psi were applied in all experiments. All phospholipids were extracted successfully and detected unambiguously using the optimized TLC-LESA-FTICRMS procedure. Sampling the tricaprylin spot gave the most intense signals and also tricaprin was detected. Three other triacylglycerols of higher molecular mass have logP values between 15.5 and 21.6, which are the highest among all investigated compounds and are not detected from their corresponding spots, due to the fact that the solubility of very apolar lipids is not high enough in the extraction solvent. It was demonstrated that TLC can be elegantly combined with mass spectrometry based on the LESA approach. In general, apart from the analysis of lipids, TLC-LESA-MS has a high potential for medium-polar compounds separated on reversed-phase TLC plates, but limitations are present when very apolar compounds have to be extracted. PMID:24801846

  2. Production of hot-wires

    NASA Astrophysics Data System (ADS)

    Dickinson, S. C.

    1983-04-01

    Several methods for producing hot-wire probes are described. Discussion includes the manufacture of probe bodies, soldering plated wires to the prongs etching Walaston type wires, and finishing the probe. This report is written as an instruction manual for researchers who desire to produce or repair their own sensors.

  3. Plate-mantle coupling from post-Pangea plate kinematics

    NASA Astrophysics Data System (ADS)

    Zahirovic, Sabin; Dietmar Müller, R.; Seton, Maria; Flament, Nicolas

    2015-04-01

    keels impinge on asthenospheric flow to increase shear traction, thus anchoring the plate in the more viscous mantle transition zone. However, plates with significant cratonic fragments exhibit short-lived (~10 Myr) accelerations, such as the rapid motion of the Indian plate that is correlated with plume head arrivals as recorded by large igneous province (LIPs) emplacement, highlighting the necessity to analyse plate velocities over long geological timeframes. By evaluating factors controlling plate velocities in the post-Pangea timeframe, simple principles can be applied to highlight potential plate velocity artefacts for Paleozoic and earlier times for which no hotspot tracks, nor in-situ seafloor spreading histories, are preserved. Based on the post-Pangea timeframe, a principle that can be applied to pre-Pangea times is that plates with less than ~50% continental area can reach RMS velocities of ~20 cm/yr, while plates with more than 50% continental fraction do not exceed RMS velocities of ~10 cm/yr. Similarly, plates with large portions of continental or cratonic area with RMS velocities exceeding ~15 cm/yr for more than ~10 Myr should be flagged as potential artefacts requiring further justification of plate driving forces in such scenarios.

  4. Solar Hot Water Heater

    NASA Technical Reports Server (NTRS)

    1978-01-01

    The solar panels pictured below, mounted on a Moscow, Idaho home, are part of a domestic hot water heating system capable of providing up to 100 percent of home or small business hot water needs. Produced by Lennox Industries Inc., Marshalltown, Iowa, the panels are commercial versions of a collector co-developed by NASA. In an effort to conserve energy, NASA has installed solar collectors at a number of its own facilities and is conducting research to develop the most efficient systems. Lewis Research Center teamed with Honeywell Inc., Minneapolis, Minnesota to develop the flat plate collector shown. Key to the collector's efficiency is black chrome coating on the plate developed for use on spacecraft solar cells, the coating prevents sun heat from "reradiating," or escaping outward. The design proved the most effective heat absorber among 23 different types of collectors evaluated in a Lewis test program. The Lennox solar domestic hot water heating system has three main components: the array of collectors, a "solar module" (blue unit pictured) and a conventional water heater. A fluid-ethylene glycol and water-is circulated through the collectors to absorb solar heat. The fluid is then piped to a double-walled jacket around a water tank within the solar module.

  5. Fluorescence microscopy imaging with a Fresnel zone plate array based optofluidic microscope

    PubMed Central

    Han, Chao; Lee, Lap Man; Yang, Changhuei

    2013-01-01

    We report the implementation of an on-chip microscope system, termed fluorescence optofluidic microscope (FOFM), which is capable of fluorescence microscopy imaging of samples in fluid media. The FOFM employs an array of Fresnel zone plates (FZP) to generate an array of focused light spots within a microfluidic channel. As a sample flows through the channel and across the array of focused light spots, the fluorescence emissions are collected by a filter-coated CMOS sensor, which serves as the channel's floor. The collected data can then be processed to render fluorescence microscopy images at a resolution determined by the focused light spot size (experimentally measured as 0.65 μm FWHM). In our experiments, our established resolution was 1.0 μm due to Nyquist criterion consideration. As a demonstration, we show that such a system can be used to image the cell nuclei stained by Acridine Orange and cytoplasm labeled by Qtracker®. PMID:21935556

  6. A novel interferometric vibration measurement sensor with quadrature detection based on 1/8 wave plate

    NASA Astrophysics Data System (ADS)

    Zhen, Shenglai; Chen, Bo; Yuan, Liang; Li, Min; Liang, Jing; Yu, Benli

    2010-03-01

    In-phase and quadrature-phase (I/Q) signals often need to be formed in the laser interferometric vibration measurement technique. To avoid the disadvantages of traditional I/Q signals forming methods such as effect of piezoelectric ceramic (PZT) for generating high frequency carrier, or optical configuration with complicated structure, a novel interferometric vibration measurement sensor with quadrature detection is proposed. The sensor utilizes simple optical configuration which contains 1/8 wave plate to generate two I/Q signals, then the signals were processed by arctangent algorithm which is compiled by Labview software through data acquisition card. Theoretical analysis and experimental Lissajous figures synthesis prove the phase orthogonality of the two signals. The experimental results indicate that the system can measure the vibration displacement accurately.

  7. Development of TOF-PET detectors based on the Multi-Gap Resistive Plate Chambers

    NASA Astrophysics Data System (ADS)

    Amaldi, U.; Borghi, G.; Bucciantonio, M.; Kieffer, R.; Samarati, J.; Sauli, F.; Watts, D.

    2015-04-01

    We describe the development, construction and preliminary results obtained with medium-size Multi-Gap Resistive Plate Chambers prototypes designed to detect and localize 511 keV photons for Positron Emission Tomography imaging applications. The devices are intended for in-beam monitoring of the treatment plans throughout deep tumor therapy with hadron beams; emphasis is put on achieving coincidence time resolutions of few hundred ps, in order to exploit optimized reconstruction algorithm and reduce the heavy non-correlated background contributions distinctive of this operation. Using technologies developed for high energy physics experiments, the detectors can be built for covering large areas, thus leading the way to the conception of full-body PET systems at low cost.

  8. Matrix based system of isotretinoin as nail lacquer to enhance transungal delivery across human nail plate.

    PubMed

    Joshi, Monika; Sharma, Vijay; Pathak, Kamla

    2015-01-15

    The project was aimed at development of isotretinoin nail lacquer and assessment of its penetration efficiency across human nail plate. Preliminary studies (hydration enhancement factor and SEM) aided the selection of thioglycolic acid as permeation and eugenol was selected as local anesthetic in the formulation. The nail lacquer was optimized by 3(2) factorial design and a total of nine formulations were prepared and screened. In vitro adhesion and ex vivo permeation (cumulative drug permeation per unit area (CDP/A) = 6.61 ± 0.57 mg/cm(2)) across bovine hoof guided the selection of F3 as optimized formulation that was improvised. Viscosity adjustments to improve handling characteristics were affected by incorporation of ethyl cellulose (6%; F3M1) that scaled the viscosity to 312.681 cp and insignificantly (p > 0.05) affected CDP/A (6.32 ± 0.45 mg/cm(2)). In comparison to marketed preparation (Retino-A cream) F3M1 afforded two fold increase in CDP/A. The permeation characteristics were defined by Higuchi model (r(2) = 0.964) and flux value of 176 μg/cm(2)/h. Confocal laser scanning microscopy, after 72 h of nail lacquer application, revealed extensive distribution of the fluorescent tracer across the human nail plate in comparison to control that was confined to the top layer. Conclusively, an efficacious and stable nail lacquer of isotretinoin was developed for potential clinical topical use to target the drug to nail bed in treatment of nail psoriasis. PMID:25445993

  9. Gap-plasmon based broadband absorbers for enhanced hot-electron and photocurrent generation

    NASA Astrophysics Data System (ADS)

    Lu, Yuhua; Dong, Wen; Chen, Zhuo; Pors, Anders; Wang, Zhenlin; Bozhevolnyi, Sergey I.

    2016-07-01

    Plasmonic hot-electron generation has recently come into focus as a new scheme for solar energy conversion. So far, however, due to the relatively narrow bandwidth of the surface plasmon resonances and the insufficient resonant light absorption, most of plasmonic photocatalysts show narrow-band spectral responsivities and small solar energy conversion efficiencies. Here we experimentally demonstrate that a three-layered nanostructure, consisting of a monolayer gold-nanoparticles and a gold film separated by a TiO2 gap layer (Au-NPs/TiO2/Au-film), is capable of near-completely absorbing light within the whole visible region. We show that the Au-NPs/TiO2/Au-film device can take advantage of such strong and broadband light absorption to enhance the generation of hot electrons and thus the photocurrent under visible irradiation. As compared to conventional plasmonic photocatalysts such as Au-NPs/TiO2 nanostructures, a 5-fold-enhanced incident photon-to-current conversion efficiency is achieved within the entire wavelength range 450–850 nm in the Au-NPs/TiO2/Au-film device. Simulations show good agreements with the experimental results, demonstrating that only the plasmon-induced losses contribute to the enhanced photocurrent generation of the Au-NPs/TiO2/Au-film device.

  10. Gap-plasmon based broadband absorbers for enhanced hot-electron and photocurrent generation

    PubMed Central

    Lu, Yuhua; Dong, Wen; Chen, Zhuo; Pors, Anders; Wang, Zhenlin; Bozhevolnyi, Sergey I.

    2016-01-01

    Plasmonic hot-electron generation has recently come into focus as a new scheme for solar energy conversion. So far, however, due to the relatively narrow bandwidth of the surface plasmon resonances and the insufficient resonant light absorption, most of plasmonic photocatalysts show narrow-band spectral responsivities and small solar energy conversion efficiencies. Here we experimentally demonstrate that a three-layered nanostructure, consisting of a monolayer gold-nanoparticles and a gold film separated by a TiO2 gap layer (Au-NPs/TiO2/Au-film), is capable of near-completely absorbing light within the whole visible region. We show that the Au-NPs/TiO2/Au-film device can take advantage of such strong and broadband light absorption to enhance the generation of hot electrons and thus the photocurrent under visible irradiation. As compared to conventional plasmonic photocatalysts such as Au-NPs/TiO2 nanostructures, a 5-fold-enhanced incident photon-to-current conversion efficiency is achieved within the entire wavelength range 450–850 nm in the Au-NPs/TiO2/Au-film device. Simulations show good agreements with the experimental results, demonstrating that only the plasmon-induced losses contribute to the enhanced photocurrent generation of the Au-NPs/TiO2/Au-film device. PMID:27470207

  11. Gap-plasmon based broadband absorbers for enhanced hot-electron and photocurrent generation.

    PubMed

    Lu, Yuhua; Dong, Wen; Chen, Zhuo; Pors, Anders; Wang, Zhenlin; Bozhevolnyi, Sergey I

    2016-01-01

    Plasmonic hot-electron generation has recently come into focus as a new scheme for solar energy conversion. So far, however, due to the relatively narrow bandwidth of the surface plasmon resonances and the insufficient resonant light absorption, most of plasmonic photocatalysts show narrow-band spectral responsivities and small solar energy conversion efficiencies. Here we experimentally demonstrate that a three-layered nanostructure, consisting of a monolayer gold-nanoparticles and a gold film separated by a TiO2 gap layer (Au-NPs/TiO2/Au-film), is capable of near-completely absorbing light within the whole visible region. We show that the Au-NPs/TiO2/Au-film device can take advantage of such strong and broadband light absorption to enhance the generation of hot electrons and thus the photocurrent under visible irradiation. As compared to conventional plasmonic photocatalysts such as Au-NPs/TiO2 nanostructures, a 5-fold-enhanced incident photon-to-current conversion efficiency is achieved within the entire wavelength range 450-850 nm in the Au-NPs/TiO2/Au-film device. Simulations show good agreements with the experimental results, demonstrating that only the plasmon-induced losses contribute to the enhanced photocurrent generation of the Au-NPs/TiO2/Au-film device. PMID:27470207

  12. New concepts for chip-supported multi-well-plates: realization of a 24-well-plate with integrated impedance-sensors for functional cellular screening applications and automated microscope aided cell-based assays.

    PubMed

    Ressler, J; Grothe, H; Motrescu, E; Wolf, B

    2004-01-01

    Based on the experience with multiparametric bioelectronic sensor chips for the monitoring of living cells, we have combined the established multi-well-format with the advantages of microelectronic sensors. The result is a 24-well-plate where the bottom of the wells is replaced by glass-based chips with integrated IDES (interdigital electrode structure). By using IDES it is possible to detect adhesion and morphological changes of adherent growing cell cultures. Up to now these measurements were inaccessible in conjunction with multi-well-plates, especially in high throughput applications. If microscopic monitoring of the cell culture is required, the IDES can be fabricated using transparent conductor materials like ITO (indium tin oxide). Both the transparent material for the sensors and the sensor-carrier make the multi-well-plate also applicable for all kinds of fluorescence and luminescence biological tests. In addition to the impedance-sensors optical read-out sensor layers for pH and pO2 can be integrated. For this reason there are many possible fields of application in biological and biomedical areas such as drug screening, chemosensitive testing and environmental toxicology as well as in biosensing for biological and chemical warfare. Especially the possibility of using this multi-well-plate together with automated imaging-systems has the great advantage of combining optical and sensory monitoring accessible to high-throughput-applications. PMID:17272129

  13. Saturn's Hot Plasma Explosions

    NASA Video Gallery

    This animation based on data obtained by NASA's Cassini Spacecraft shows how the "explosions" of hot plasma on the night side (orange and white) periodically inflate Saturn's magnetic field (white ...

  14. Free vibration analysis of laminated plate/shell structures based on FSDT with a stabilized nodal-integrated quadrilateral element

    NASA Astrophysics Data System (ADS)

    Nguyen-Van, H.; Mai-Duy, N.; Tran-Cong, T.

    2008-06-01

    This paper reports numerical analyses of free vibration of laminated composite plate/shell structures of various shapes, span-to-thickness ratios, boundary conditions and lay-up sequences. The method is based on a novel four-node quadrilateral element, namely MISQ20, within the framework of the first-order shear deformation theory (FSDT). The element is built by incorporating a strain smoothing method into the bilinear four-node quadrilateral finite element where the strain smoothing operation is based on mesh-free conforming nodal integration. The bending and membrane stiffness matrices are based on the boundaries of smoothing cells while the shear term is evaluated by 2×2 Gauss quadrature. Through several numerical examples, the capability, efficiency and simplicity of the element are demonstrated. Convergence studies and comparison with other existing solutions in the literature suggest that the present element is robust, computationally inexpensive and free of locking.

  15. Application of electrolyzed acid water to sterilization of denture base part 1. Examination of sterilization effects on resin plate.

    PubMed

    Nagamatsu, Y; Tajima, K; Kakigawa, H; Kozono, Y

    2001-06-01

    Bactericidal activities of electrolyzed strong and weak acid waters for acrylic denture base resin were evaluated in order to discuss the applicability of these waters for sterilization of denture base. Only 1-minute immersion in the electrolyzed strong or weak acid water could completely eliminate the attached bacteria, Staphylococcus aureus 209P, on the resin plate. When the resin was relined with tissue conditioner, 5-minute immersion or 1- to 2-minute ultrasonic cleaning reduced the number of the bacteria from 10(5)/cm2 level to 10(1)/cm2 and no surviving bacteria could be detected after 10-minute treatment. These findings suggest that both the electrolyzed strong and weak acid waters are well applicable to the disinfectant for acrylic denture base showing excellent bactericidal activities in a significantly shorter treatment as compared with the conventional denture cleaning. PMID:11523978

  16. Current gain above 10 in sub-10 nm base III-Nitride tunneling hot electron transistors with GaN/AlN emitter

    NASA Astrophysics Data System (ADS)

    Yang, Zhichao; Zhang, Yuewei; Krishnamoorthy, Sriram; Nath, Digbijoy N.; Khurgin, Jacob B.; Rajan, Siddharth

    2016-05-01

    We report on a tunneling hot electron transistor amplifier with common-emitter current gain greater than 10 at a collector current density in excess of 40 kA/cm2. The use of a wide-bandgap GaN/AlN (111 nm/2.5 nm) emitter was found to greatly improve injection efficiency of the emitter and reduce cold electron leakage. With an ultra-thin (8 nm) base, 93% of the injected hot electrons were collected, enabling a common-emitter current gain up to 14.5. This work improves understanding of the quasi-ballistic hot electron transport and may impact the development of high speed devices based on unipolar hot electron transport.

  17. A Thermodynamic Model for Predicting Phosphorus Partition between CaO-based Slags and Hot Metal during Hot Metal Dephosphorization Pretreatment Process Based on the Ion and Molecule Coexistence Theory

    NASA Astrophysics Data System (ADS)

    Yang, Xue-min; Li, Jin-yan; Chai, Guo-ming; Duan, Dong-ping; Zhang, Jian

    2016-08-01

    A thermodynamic model for predicting phosphorus partition L P between a CaO-based slags and hot metal during hot metal dephosphorization pretreatment process has been developed based on the ion and molecule coexistence theory (IMCT), i.e., the IMCT- L P model. The reaction abilities of structural units or ion couples in the CaO-based slags have been represented by the calculated mass action concentrations N i through the developed IMCT- N i model based on the IMCT. The developed IMCT- L P model has been verified to be valid through comparing with the measured L P as well as the predicted L P by two reported L P models from the literature. Besides the total phosphorus partition L P between the CaO-based slag and hot metal, the respective phosphorus partitions L P, i of nine dephosphorization products as P2O5, 3FeO·P2O5, 4FeO·P2O5, 2CaO·P2O5, 3CaO·P2O5, 4CaO·P2O5, 2MgO·P2O5, 3MgO·P2O5, and 3MnO·P2O5 can also be accurately predicted by the developed IMCT- L P model. The formed 3CaO·P2O5 accounts for 99.20 pct of dephosphorization products comparing with the generated 4CaO·P2O5 for 0.08 pct. The comprehensive effect of CaO+Fe t O, which can be described by the mass percentage ratio (pct Fe t O)/(pct CaO) or the mass action concentration ratio N_{Fe}t O/N_{Fe}t O N_{CaO}. N_{CaO}} as well as the mass percentage product (pct Fe t O) × (pct CaO) or the mass action concentration product N_{{{{Fe}}t {{O}}}}5 × N_{{CaO}}3 , controls dephosphorization ability of the CaO-based slags. A linear relationship of L P against (pct Fe t O)/(pct CaO) can be correlated compared with a parabolic relationship of L P against N_{Fe}t O/N_{Fe}t O N_{CaO}. N_{CaO}, while the linear relationship of L P against (pct Fe t O) × (pct CaO) or N_{Fe}t O5 × N_{CaO}3 can be established. Thus, the mass percentage product (pct Fe t O) × (pct CaO) and the mass action concentration product N_{Fe}t O5 × N_{CaO}3 are recommended to represent the comprehensive effect of CaO+Fe t O on

  18. Scalable 96-well Plate Based iPSC Culture and Production Using a Robotic Liquid Handling System

    PubMed Central

    Conway, Michael K.; Gerger, Michael J.; Balay, Erin E.; O'Connell, Rachel; Hanson, Seth; Daily, Neil J.; Wakatsuki, Tetsuro

    2015-01-01

    Continued advancement in pluripotent stem cell culture is closing the gap between bench and bedside for using these cells in regenerative medicine, drug discovery and safety testing. In order to produce stem cell derived biopharmaceutics and cells for tissue engineering and transplantation, a cost-effective cell-manufacturing technology is essential. Maintenance of pluripotency and stable performance of cells in downstream applications (e.g., cell differentiation) over time is paramount to large scale cell production. Yet that can be difficult to achieve especially if cells are cultured manually where the operator can introduce significant variability as well as be prohibitively expensive to scale-up. To enable high-throughput, large-scale stem cell production and remove operator influence novel stem cell culture protocols using a bench-top multi-channel liquid handling robot were developed that require minimal technician involvement or experience. With these protocols human induced pluripotent stem cells (iPSCs) were cultured in feeder-free conditions directly from a frozen stock and maintained in 96-well plates. Depending on cell line and desired scale-up rate, the operator can easily determine when to passage based on a series of images showing the optimal colony densities for splitting. Then the necessary reagents are prepared to perform a colony split to new plates without a centrifugation step. After 20 passages (~3 months), two iPSC lines maintained stable karyotypes, expressed stem cell markers, and differentiated into cardiomyocytes with high efficiency. The system can perform subsequent high-throughput screening of new differentiation protocols or genetic manipulation designed for 96-well plates. This technology will reduce the labor and technical burden to produce large numbers of identical stem cells for a myriad of applications. PMID:26068617

  19. Parallel-plate lab-on-a-chip based on digital microfluidics for on-chip electrochemical analysis

    NASA Astrophysics Data System (ADS)

    Yu, Yuhua; Chen, Jianfeng; Zhou, Jia

    2014-01-01

    This paper describes an electrowetting on dielectric (EWOD) digital microfluidic-based lab-on-a-chip (LOC) integrated with on-chip electrochemical microsensor by IC compatible fabrication process, and its application for the entire online biosensing process capable of fully automatic analysis for ferrocenemethanol (FcM) and dopamine (DA). In this work, we made full use of the parallel-plate structure of the EWOD digital microfluidic device to fabricate the microfluidic module on the bottom plate and the three-microelectrode-system-integrated electrochemical cell together with patterned ground electrode on the top plate. The proposed LOC possesses the multifunction of: (1) creating, merging and transporting of microliter-level sample droplets, (2) online biosensing, and (3) droplets recycling. The three-electrode-integrated microsensor not only reveals a sensitive electrochemical detection for FcM in a wide concentration range (10 µM-1.0 mM), but also shows good stability, selectivity and reproducibility for surface-controlled detection of DA. The calibration of DA was linear for concentration from 1.0 to 50.0 µM with a high sensitivity of 2145 nA µM-1 cm-2 (R2 = 0.9933) and estimated detection limit of 0.42 µM (signal/noise ratio of 3). This work shows the promise of state-of-the-art digital microfluidic biosensors for fully automatic online bioanalysis in a future LOC to perform on-chip biomedical protocols in vitro diagnostic assays.

  20. Scalable 96-well Plate Based iPSC Culture and Production Using a Robotic Liquid Handling System.

    PubMed

    Conway, Michael K; Gerger, Michael J; Balay, Erin E; O'Connell, Rachel; Hanson, Seth; Daily, Neil J; Wakatsuki, Tetsuro

    2015-01-01

    Continued advancement in pluripotent stem cell culture is closing the gap between bench and bedside for using these cells in regenerative medicine, drug discovery and safety testing. In order to produce stem cell derived biopharmaceutics and cells for tissue engineering and transplantation, a cost-effective cell-manufacturing technology is essential. Maintenance of pluripotency and stable performance of cells in downstream applications (e.g., cell differentiation) over time is paramount to large scale cell production. Yet that can be difficult to achieve especially if cells are cultured manually where the operator can introduce significant variability as well as be prohibitively expensive to scale-up. To enable high-throughput, large-scale stem cell production and remove operator influence novel stem cell culture protocols using a bench-top multi-channel liquid handling robot were developed that require minimal technician involvement or experience. With these protocols human induced pluripotent stem cells (iPSCs) were cultured in feeder-free conditions directly from a frozen stock and maintained in 96-well plates. Depending on cell line and desired scale-up rate, the operator can easily determine when to passage based on a series of images showing the optimal colony densities for splitting. Then the necessary reagents are prepared to perform a colony split to new plates without a centrifugation step. After 20 passages (~3 months), two iPSC lines maintained stable karyotypes, expressed stem cell markers, and differentiated into cardiomyocytes with high efficiency. The system can perform subsequent high-throughput screening of new differentiation protocols or genetic manipulation designed for 96-well plates. This technology will reduce the labor and technical burden to produce large numbers of identical stem cells for a myriad of applications. PMID:26068617

  1. Susceptibility to hot corrosion of four nickel-base superalloys, NASA-TRW VIA, B-1900, 713C and IN-738

    NASA Technical Reports Server (NTRS)

    Stearns, C. A.; Kohl, F. J.; Fryburg, G. C.

    1977-01-01

    The susceptibility to hot corrosion of four nickel-base, cast superalloys has been studied at 900 and 1000 C. The test consisted of coating alloy samples with known amounts of Na2SO4 and oxidizing the coated samples isothermally in 1 atmosphere of slowly flowing oxygen, the weight-gain being monitored on a sensitive recording microbalance. Susceptibility to hot corrosion decreased in the order of decreasing molybdenum content of the alloys. Preoxidation of samples before hot-corrosion testing markedly increased the induction period observed prior to the inception of hot corrosion for all alloys tested. X-ray diffraction analyses of the oxide scales were made. All samples that underwent hot corrosion showed the presence of a (Ni,Co)MoO4 layer near the alloy-oxide interface. Several specimens displayed resistance to hot corrosion and these showed NaTaO3 as a prominent feature in their oxide scale. Our results may be interpreted as indicating that molybdenum in an alloy is detrimental, with respect to hot corrosion, while tantalum is beneficial.

  2. Effect of annealing on the structure and properties of hot-pressed boron carbide base cermets

    SciTech Connect

    Koval'chenko, M.S.; Laptev, A.V.; Zhidov, A.B.

    1986-02-01

    This paper studies the effect of annealing conditions on the structure and some physicomechanical properties of boron carbidealuminum cermets produced by hot pressing under high pressures. The paper also explores the possibility of regulating the properties of such cermets by heat treatment. Cermets were produced using boron carbide powders of particle sizes up to 100 ..mu..m. As metallic binders, PA-3 aluminum powder and powders of aluminum alloys with improving wetting and adhesional interaction were employed. The microstructures of specimens were studied under an MIM-8 optical microscope. X-ray phase analysis was carried out in a URS-501M diffractometer in Cu K-alpha radiation. The authors found that to obtain boron carbidealuminum materials of maximum strength, it is necessary to perform their liquid-phase pressing under high pressures and dispense with subsequent annealing.

  3. DEVELOPMENT OF A CALCIUM-BASED SORBENT FOR HOT GAS CLEANUP

    SciTech Connect

    T.D. Wheelock; L.K. Doraiswamy; K. Constant

    1999-03-31

    The preparation and testing of potential sorbents for removing H{sub 2}S and COS from hot coal gas continued. Two preparation methods received the most consideration. Both methods involve pelletizing powders in a revolving drum under moist conditions followed either by heat treatment or steam curing to harden the pellets, depending on the particle bonding mechanism. One method was used to pelletize mixtures of calcium carbonate and either alumina or a calcium aluminate cement in a single step. Another method was used to pelletize powdered limestone in an initial step followed by the application of a coating consisting of both limestone and a hydraulic cement in a second step. By employing this method, an especially promising material was produced consisting of a limestone core surrounded by a shell consisting initially of 80 wt.% limestone and 20% wt.% calcium aluminate cement. The best material exhibited both an acceptable crushing strength and adsorption capacity for H{sub 2}S.

  4. Mechanical properties of molybdenum disilicide based materials consolidated by hot isostatic pressing (HIP)

    SciTech Connect

    Suryanarayanan, R.; Sastry, S.M.L.; Jerina, K.L. . Dept. of Mechanical Engineering)

    1994-11-01

    The influence of hot isostatic pressing (HIP) consolidation parameters on the mechanical properties of molybdenum disilicide (MoSi[sub 2]) and MoSi[sub 2] reinforced with ductile and brittle reinforcements was studied. MoSi[sub 2], MoSi[sub 2]-20 vol.% coarse and fine niobium powder and MoSi[sub 2]-20 vol.% silicon carbide whiskers consolidated by HIP at 1,200--1,400 C, 207 MPa, for 1 and 4 h were tested in compression for elevated temperature strength and creep resistance. Single-edge-notched specimens of the three materials were tested in a three-point bend configuration for fracture toughness. Mechanical properties were related with consolidation parameters and post-HIP microstructures.

  5. Elastomer based composite materials for bipolar plates in polymer electrolyte membrane fuel cells

    NASA Astrophysics Data System (ADS)

    Petrach, Elaine M.

    2011-07-01

    In most investigations, polymer conductive composite bipolar plates have failed to achieve the low resistivity required for PEMFCs. The goal of this dissertation is to investigate whether a composite of conductive fillers and a two-phase polymeric matrix will achieve low resistivity through preferred distribution of the fillers at the interface of the two phases. The use of an elastomer as one component of the blend will impart fracture resistance. Three types of matrices were investigated, a single phase polyvinyl ester plastic matrix, a compatible one-phase blend of polyvinyl ester (VER) and polyurethane (PU) elastomer, and a two-phase system of polyvinyl ester and ethylene propylene diene monomer (EPDM) elastomer. The different phases were determined by the theory of mixing. When solubility parameters are closer together it is likely that the system will be one phase. The one and two-phase systems were analyzed within the composition containing natural Cytec DKD graphite fibers, Asbury synthetic graphite 4012 flakes and ultra high surface area synthetic graphite TC 307. Phase systems affect the mechanical, electrical, and thermal properties. The percolation theory analysis was applied to determine the optimal percentage of conductive fillers and polymer blends. The optimal composition for composite materials consisted of 35vo1% of conductive fillers and 65vo1% of a two-phase blend matrix. The conductive filler included 3vol% of synthetic graphite TC307, 25.5vol% of Cytec DKD graphite fibers and 6.5vol% of Asbury synthetic graphite 4012 flakes. The two-phase blend matrix included 40vol% of EPDM to 60vol% of VER. This resulted in an electrical resistivity of 0.009O-cm and a thermal conductivity of 11.6W/m-K. The two-phase blend matrix added more ductility to the composition with the ability to withstand a stress of 10MPa with over 1% strain applied to the overall composite bipolar plates. The composition also absorbed 60% more mechanical energy than that

  6. Peen plating

    NASA Technical Reports Server (NTRS)

    Babecki, A. J. (Inventor); Haehner, C. L.

    1973-01-01

    A process for metal plating which comprises spraying a mixture of metallic powder and small peening particles at high velocity against a surface is described. The velocity must be sufficient to impact and bond metallic powder onto the surface. In the case of metal surfaces, the process has as one of its advantages providing mechanical working (hardening) of the surface simultaneously with the metal plating.

  7. Development of Microelectrode Arrays Using Electroless Plating for CMOS-Based Direct Counting of Bacterial and HeLa Cells.

    PubMed

    Niitsu, Kiichi; Ota, Shoko; Gamo, Kohei; Kondo, Hiroki; Hori, Masaru; Nakazato, Kazuo

    2015-10-01

    The development of two new types of high-density, electroless plated microelectrode arrays for CMOS-based high-sensitivity direct bacteria and HeLa cell counting are presented. For emerging high-sensitivity direct pathogen counting, two technical challenges must be addressed. One is the formation of a bacteria-sized microelectrode, and the other is the development of a high-sensitivity and high-speed amperometry circuit. The requirement for microelectrode formation is that the gold microelectrodes are required to be as small as the target cell. By improving a self-aligned electroless plating technique, the dimensions of the microelectrodes on a CMOS sensor chip in this work were successfully reduced to 1.2 μm × 2.05 μm. This is 1/20th of the smallest size reported in the literature. Since a bacteria-sized microelectrode has a severe limitation on the current flow, the amperometry circuit has to have a high sensitivity and high speed with low noise. In this work, a current buffer was inserted to mitigate the potential fluctuation. Three test chips were fabricated using a 0.6- μm CMOS process: two with 1.2 μm × 2.05 μm (1024 × 1024 and 4 × 4) sensor arrays and one with 6- μm square (16 × 16) sensor arrays; and the microelectrodes were formed on them using electroless plating. The uniformity among the 1024 × 1024 electrodes arranged with a pitch of 3.6 μm × 4.45 μm was optically verified. For improving sensitivity, the trenches on each microelectrode were developed and verified optically and electrochemically for the first time. Higher sensitivity can be achieved by introducing a trench structure than by using a conventional microelectrode formed by contact photolithography. Cyclic voltammetry (CV) measurements obtained using the 1.2 μm × 2.05 μm 4 × 4 and 6- μm square 16 × 16 sensor array with electroless-plated microelectrodes successfully demonstrated direct counting of the bacteria-sized microbeads and HeLa cells. PMID:26561481

  8. Development of a New Fast Shower Maximum Detector Based on Microchannel Plates Photomultipliers (MCP-PMT) as an Active Element

    SciTech Connect

    Ronzhin, A.; Los, S.; Ramberg, E.; Spiropulu, M.; Apresyan, A.; Xie, S.; Kim, H.; Zatserklyaniy, A.

    2014-09-21

    One possibility to make a fast and radiation resistant shower maximum (SM) detector is to use a secondary emitter as an active element. We present below test beam results, obtained with different types of photodetectors based on microchannel plates (MCPs) as the secondary emitter. We performed the measurements at the Fermilab Test Beam Facility with 120GeV proton beam and 12GeV and 32GeV secondary beams. The goal of the measurement with 120GeV protons was to determine time resolution for minimum ionizing particles (MIPs). The SM time resolution we obtained for this new type of detector is at the level of 20-30ps. We estimate that a significant contribution to the detector response originates from secondary emission of the MCP. This work can be considered as the first step in building a new type of calorimeter based on this principle.

  9. Development of a new fast shower maximum detector based on microchannel plates photomultipliers (MCP-PMT) as an active element

    NASA Astrophysics Data System (ADS)

    Ronzhin, A.; Los, S.; Ramberg, E.; Spiropulu, M.; Apresyan, A.; Xie, S.; Kim, H.; Zatserklyaniy, A.

    2014-09-01

    One possibility to make a fast and radiation resistant shower maximum (SM) detector is to use a secondary emitter as an active element. We present below test beam results, obtained with different types of photodetectors based on microchannel plates (MCPs) as the secondary emitter. We performed the measurements at the Fermilab Test Beam Facility with 120 GeV proton beam and 12 GeV and 32 GeV secondary beams. The goal of the measurement with 120 GeV protons was to determine time resolution for minimum ionizing particles (MIPs). The SM time resolution we obtained for this new type of detector is at the level of 20-30 ps. We estimate that a significant contribution to the detector response originates from secondary emission of the MCP. This work can be considered as the first step in building a new type of calorimeter based on this principle.

  10. Optically switchable and axially symmetric half-wave plate based on photoaligned liquid crystal films

    NASA Astrophysics Data System (ADS)

    Lin, C.-C.; Huang, T.-C.; Chu, C.-C.; Hsiao, Vincent K. S.

    2016-07-01

    We demonstrate an optically switchable half-wave plate (HWP) composed of a photoaligned and axially symmetric liquid crystal (ASLC) film containing two azobenzene derivatives, methyl red (MR) and 4-butyl-4‧-methoxyazobenzene (BMAB). MR is responsible for photoalignment, and BMAB is used for optical tuning and switching the state of polarization (SOP) of probe beam (633 nm He-Ne laser) passing through the MR/BMAB doped ASLC film. The photoaligned ASLC film is first fabricated using a line-shaped laser beam (532 nm) exposure applied on a rotating LC sample. The fabricated ASLC film can passively change the linearly polarized light. Under UV light exposure, the formation of cis-BMAB (bend-like shape) within the film disrupts the LC molecules, switches the LC orientation, and further changes the SOP of the probe beam. Under laser irradiation (532 nm), the formation of trans-BMAB (rod-like shape) reverts the LC orientation back and simultaneously generates cis-MR, helping anchor the LC in the previously photoaligned orientation. The photoaligned MR/BMAB-doped LC HWP can change the linear SOP under alternating UV and visible light exposure.

  11. Behaviour of plate elements based on the first-order shear deformation theory

    NASA Technical Reports Server (NTRS)

    Averill, R. C.; Reddy, J. N.

    1990-01-01

    A new analytical technique to assess the performance of shear deformable elements is presented, which makes it possible to determine a priori whether a given element will lock when used to model thin structures. The role that shear constraints play in determining the behavior of thin elements was established by comparing the results of key numerical tests with the predictions of element behavior made by studying the form of the shear constraints. Conclusions regarding locking behavior and the effects of reduced integration in thin shear deformable elements are presented, including the findings (1) that singularity of the shear stiffness matrix is not sufficient to avoid locking; (2) that the effect of mesh refinement on an element that contains spurious constraints is two-fold; and (3) that reduced integration does not remove spurious constraints but rather relaxes them. The results of the study are in agreement with previous studies of Mindlin plate elements in regarding Lagrangian elements as superior to serendipity elements when either full or reduced integration is employed.

  12. Image-based fluidic sorting system for automated Zebrafish egg sorting into multiwell plates.

    PubMed

    Graf, Siegfried F; Hötzel, Sebastian; Liebel, Urban; Stemmer, Andreas; Knapp, Helmut F

    2011-04-01

    The global demand for the reduction of animal testing has led to the emergence of Zebrafish eggs/larvae as model organisms to replace current adult animal testing in, for example, toxicity testing. Because of the egg size (diameter 1.6mm) and the relatively easy maintenance of Zebrafish farms the eggs also offer high-throughput screening (HTS). However, the current bottleneck for HTS is the cost-efficient placing of individual organisms into single wells of a multiwell plate (MWP). The system presented here is capable of storing, sorting, and placing individual organisms in a highly reproducible manner. In about 11 min a complete 96-MWP is filled, which corresponds to about 8 sec per egg. The survival rate of fertilized transgenic and wild-type eggs was comparable to the one of the control (control 6.7%, system 7.6%). Furthermore, it was also possible to place dechorionated eggs into individual wells. The results demonstrate that the cost efficient system works gentle and reliable enough to disburden scientists from the exhausting and monotonous job of placing single eggs into single wells, such that they can concentrate on the scientific aspects of their experiments and create results with a higher statistical relevance. PMID:21609691

  13. A modified procedure for replica plating of mammalian cells allowing selection of clones based on gene expression.

    PubMed

    Hornsby, P J; Yang, L; Lala, D S; Cheng, C Y; Salmons, B

    1992-02-01

    The polyester cloth replica-plating technique for selection of mammalian cell clones was modified by growing cells in colonies on a flexible polytetrafluoroethylene membrane and then transferring them completely to polyester cloth (27-microns mesh), from which a replica was made by allowing cells to transfer to a cloth of smaller pore size (17-microns mesh). Using this technique, two phenotype selection methods are demonstrated here: in situ hybridization for detection of a specific mRNA and a photographic film assay for detection of luciferase expression. Cells were transfected with pSV2AL-A delta 5' in which firefly luciferase cDNA is under the control of the simian virus 40 promoter. The luciferase assay was adapted for colonies on polyester cloth; cells were permeabilized with digitonin to allow access of ATP and luciferin to the cell without disruption of colonies. Clones selected for expression or nonexpression of luciferase by the photographic film assay were positive or negative for expression after isolation from the cloth replica and subsequent growth under conventional culture conditions. The replica-plating procedure described here should be generally applicable to most mammalian cell types. The ability to produce replicas of colonies, combined with in situ hybridization or assays that can be adapted to in situ detection, provides phenotype selection for clones based on gene expression independent of growth characteristics. PMID:1616718

  14. Fatigue strength of Al7075 notched plates based on the local SED averaged over a control volume

    NASA Astrophysics Data System (ADS)

    Berto, Filippo; Lazzarin, Paolo

    2014-01-01

    When pointed V-notches weaken structural components, local stresses are singular and their intensities are expressed in terms of the notch stress intensity factors (NSIFs). These parameters have been widely used for fatigue assessments of welded structures under high cycle fatigue and sharp notches in plates made of brittle materials subjected to static loading. Fine meshes are required to capture the asymptotic stress distributions ahead of the notch tip and evaluate the relevant NSIFs. On the other hand, when the aim is to determine the local Strain Energy Density (SED) averaged in a control volume embracing the point of stress singularity, refined meshes are, not at all, necessary. The SED can be evaluated from nodal displacements and regular coarse meshes provide accurate values for the averaged local SED. In the present contribution, the link between the SED and the NSIFs is discussed by considering some typical welded joints and sharp V-notches. The procedure based on the SED has been also proofed to be useful for determining theoretical stress concentration factors of blunt notches and holes. In the second part of this work an application of the strain energy density to the fatigue assessment of Al7075 notched plates is presented. The experimental data are taken from the recent literature and refer to notched specimens subjected to different shot peening treatments aimed to increase the notch fatigue strength with respect to the parent material.

  15. A study of the long-term properties of Jovian hot spots from HST and ground-based observations between 1994 and 1998

    NASA Astrophysics Data System (ADS)

    Arregui, E.; Rojas, J. F.; Sanchez-Lavega, A.; Lecacheux, J.; Colas, F.; Miyazaki, I.; Parker, D.

    2000-10-01

    We have used the HST-WFPC2 archived images of Jupiter in the period 1994-1998 together with a large set of CCD ground based images, to study the zonal distribution, long-term motions, lifetimes, interactions and other properties of the hot spot - plume regions at 7 degrees North. Red and near infrared filters covering the wavelength range 650 - 953 nm have been used since they show the hot spots with a high contrast. We have found that the hot spots have velocities ranging from 95 to 112 m/s and are grouped typically in families of three to six members. We do not found any correlation between their velocity and wavenumber. The long-term survey allowed us to identify mergers and splitting of the hot spots areas. The Spanish team was supported by Gobierno Vasco PI 034/97. The French team was supported by the "Programme National de Planetologie."

  16. Field-based evaluations of horizontal flat-plate fish screens

    USGS Publications Warehouse

    Rose, B.P.; Mesa, M.G.; Barbin-Zydlewski, G.

    2008-01-01

    Diversions from streams are often screened to prevent the loss of or injury to fish. Hydraulic criteria meant to protect fish that encounter screens have been developed, but primarily for screens that are vertical to the water flow rather than horizontal. For this reason, we measured selected hydraulic variables and released wild rainbow trout Oncorhynchus mykiss over two types of horizontal flat-plate fish screens in the field. Our goal was to assess the efficacy of these screens under a variety of conditions in the field and provide information that could be used to develop criteria for safe fish passage. We evaluated three different invertedweir screens over a range of stream (0.24-1.77 m3/s) and diversion flows (0.10-0.31 m3/s). Approach velocities (AVs) ranged from 3 to 8 cm/s and sweeping velocities (SVs) from 69 to 143 cm/s. We also evaluated a simple backwatered screen over stream flows of 0.23-0.79 m3/s and diversion flows of 0.08-0.32 m3/s. The mean SVs for this screen ranged from 15 to 66 cm/s and the mean AVs from 1 to 5 cm/s. The survival rates of fish held for 24 h after passage over these screens exceeded 98%. Overall, the number of fish-screen contacts was low and the injuries related to passage were infrequent and consisted primarily of minor fin injuries. Our results indicate that screens of this type have great potential as safe and effective fish screens for small diversions. Care must be taken, however, to avoid operating conditions that produce shallow or no water over the screen surface, situations of high AVs and low SVs at backwatered screens, and situations producing a localized high AV with spiraling flow. ?? Copyright by the American Fisheries Society 2008.

  17. On the possibility to grow zinc oxide-based transparent conducting oxide films by hot-wire chemical vapor deposition

    SciTech Connect

    Abrutis, Adulfas Silimavicus, Laimis; Kubilius, Virgaudas; Murauskas, Tomas; Saltyte, Zita; Kuprenaite, Sabina; Plausinaitiene, Valentina

    2014-03-15

    Hot-wire chemical vapor deposition (HW-CVD) was applied to grow zinc oxide (ZnO)-based transparent conducting oxide (TCO) films. Indium (In)-doped ZnO films were deposited using a cold wall pulsed liquid injection CVD system with three nichrome wires installed at a distance of 2 cm from the substrate holder. The wires were heated by an AC current in the range of 0–10 A. Zn and In 2,2,6,6-tetramethyl-3,5-heptanedionates dissolved in 1,2-dimethoxyethane were used as precursors. The hot wires had a marked effect on the growth rates of ZnO, In-doped ZnO, and In{sub 2}O{sub 3} films; at a current of 6–10 A, growth rates were increased by a factor of ≈10–20 compared with those of traditional CVD at the same substrate temperature (400 °C). In-doped ZnO films with thickness of ≈150 nm deposited on sapphire-R grown at a wire current of 9 A exhibited a resistivity of ≈2 × 10{sup −3} Ωcm and transparency of >90% in the visible spectral range. These initial results reveal the potential of HW-CVD for the growth of TCOs.

  18. Defect Prediction and Control for Ultra-high-strength Steel Complex Structure in Hot Forming Based on FEM

    NASA Astrophysics Data System (ADS)

    Shang, Xin; Zhou, Jie; Zhuo, Fang; Luo, Yan; Li, Yang

    2015-06-01

    Cracking is the main defect in ultra-high-strength steel (UHSS) forming products. In order to avoid cracking, either adjusting process parameters or changing die's design is usually applied. However, under the condition of forming parts with unreasonable structure design, it makes little difference through the traditional methods of modifying process parameters. In this paper, true stress-strain curves under different strain rates and temperatures are obtained via the hot tensile tests. Then, the material constitutive model of UHSS is introduced into software CAE; this step is used to analyze and predict defects of UHSS hot forming complex structural parts based on FEM. In addition, simulation results of changed structure (open end) are compared with original structure (closed end). The results have shown that both maximum reduction ratio and stress in all directions are sharply reduced, i.e., the forming quality is improved significantly after changing the end structure. Finally, the prediction and control methods of forming defects are verified to be feasible in actual production.

  19. Hot compression deformation behavior and a modified physically-based constitutive model of Cu-6 %Ag alloy

    NASA Astrophysics Data System (ADS)

    Meng, Lie; Wang, Menghan; Liu, Xiao; Wang, Fenglin

    2016-04-01

    In order to reveal the flow characteristics of Cu-6 %Ag alloy on the condition of hot deformation, the isothermal compression experiments are carried out at the temperatures of 973-1123 K under strain rates of 0.01-10 s-1. The effects of deformation condition on the hot compression deformation behavior are investigated. The low instability strain (ɛ i) behavior at high strain rate (10 s-1) is discussed in this paper. According to the experiment results and analyses, the deformation twinning and inhomogeneous grains are thought to be the possible reasons for low strain cracking. Then, a modified physically based constitutive model is established. The strain for maximum softening rate (\\varepsilon_{ *} ) is quoted in the constitutive equation which is proved that there is a nearly linear relationship between { ln }\\varepsilon_{ *} and { ln }Z . What's more, the correlation coefficient (R) and the average absolute relative error (AARE) are used to evaluate the accuracy of the established constitutive model. The values of R and AARE are 0.99612 and 3.47 %, respectively, which show that the modified constitutive model can exactly reveal the flow stress of Cu-6 %Ag alloy.

  20. Solution of boundary heat transfer coefficients between hot stamping die and cooling water based on FEM and optimization method

    NASA Astrophysics Data System (ADS)

    Li, Huiping; He, Lianfang; Zhang, Chunzhi; Cui, Hongzhi

    2016-04-01

    The thermal physical parameters have significant effects on the calculation accuracy of physical fields, and the boundary heat transfer coefficient between the die and water is one of the most important thermal physical parameters in the hot stamping. In order to attain the boundary heat transfer coefficient, the testing devices and test procedures are designed according to the characteristic of heat transfer in the hot stamping die. A method of estimating the temperature-dependent boundary heat transfer coefficient is presented, and an inverse heat conduction software is developed based on finite element method, advance-retreat method and golden section method. The software is used to calculate the boundary heat transfer coefficient according to the temperatures measured by NiCr-NiSi thermocouples in the experiment. The research results show that, the convergence of the method given in the paper is well, the surface temperature of sample has a significant effect on the boundary heat transfer coefficient between the die and water. The boundary heat transfer coefficient increases as the surface temperature of sample reduces, and the variation is nonlinear.

  1. Tunable Diffractive Optical Elements Based on Shape-Memory Polymers Fabricated via Hot Embossing.

    PubMed

    Schauer, Senta; Meier, Tobias; Reinhard, Maximilian; Röhrig, Michael; Schneider, Marc; Heilig, Markus; Kolew, Alexander; Worgull, Matthias; Hölscher, Hendrik

    2016-04-13

    We introduce actively tunable diffractive optical elements fabricated from shape-memory polymers (SMPs). By utilizing the shape-memory effect of the polymer, at least one crucial attribute of the diffractive optical element (DOE) is tunable and adjustable subsequent to the completed fabrication process. A thermoplastic, transparent, thermoresponsive polyurethane SMP was structured with diverse diffractive microstructures via hot embossing. The tunability was enabled by programming a second, temporary shape into the diffractive optical element by mechanical deformation, either by stretching or a second embossing cycle at low temperatures. Upon exposure to the stimulus heat, the structures change continuously and controllable in a predefined way. We establish the novel concept of shape-memory diffractive optical elements by illustrating their capabilities, with regard to tunability, by displaying the morphing diffractive pattern of a height tunable and a period tunable structure, respectively. A sample where an arbitrary structure is transformed to a second, disparate one is illustrated as well. To prove the applicability of our tunable shape-memory diffractive optical elements, we verified their long-term stability and demonstrated the precise adjustability with a detailed analysis of the recovery dynamics, in terms of temperature dependence and spatially resolved, time-dependent recovery. PMID:26998646

  2. Hot corrosion behavior of Ni based Inconel 617 and Inconel 738 superalloys

    NASA Astrophysics Data System (ADS)

    El-Awadi, G. A.; Abdel-Samad, S.; Elshazly, Ezzat S.

    2016-08-01

    Superalloys are extensively used at high temperature applications due to their good oxidation and corrosion resistance properties in addition to their high stability were made at high temperature. Experimental measurements of hot corrosion at high temperature of Inconel 617 and Inconel 738 superalloys. The experiments were carried out at temperatures 700 °C, 800 °C and 900 °C for different exposure times to up to 100 h. The corrosive media was NaCl and Na2SO4 sprayed on the specimens. Seven different specimens were used at each temperature. The corrosion process is endothermic and the spontaneity increased by increasing temperature. The activation energy was found to be Ea = 23.54 and Ea = 25.18 KJ/mol for Inconel 738 and Inconel 617 respectively. X-ray diffraction technique (XRD) was used to analyze the formed scale. The morphology of the specimen and scale were examined by scanning electron microscopy (SEM). The results show that the major corrosion products formed were NiCr2O4, and Co Cr2O4 spinles, in addition to Cr2O3.

  3. Three-dimensional laparoscope based on the manipulation of polarized light by a cellophane half-wave plate

    NASA Astrophysics Data System (ADS)

    Iizuka, Keigo

    2005-11-01

    A three-dimensional laparoscope that can capture three-dimensional images during surgery is reported. The principle is solely based on the manipulation of polarized light by a cellophane half-wave plate rather than computer processing; hence there is no time delay (it operates in real time) and lesions are viewed in true color, which is important for diagnostics. Three-dimensional images are obtained with a single laparoscope. A unique feature of this three-dimensional laparoscope is that it includes a virtual ruler to measure distances without physically touching the affected areas. The structure is simple, sturdy, lightweight, and its diameter is no bigger than a standard 10 mm diam laparoscope.

  4. Phononic plate waves.

    PubMed

    Wu, Tsung-Tsong; Hsu, Jin-Chen; Sun, Jia-Hong

    2011-10-01

    In the past two decades, phononic crystals (PCs) which consist of periodically arranged media have attracted considerable interest because of the existence of complete frequency band gaps and maneuverable band structures. Recently, Lamb waves in thin plates with PC structures have started to receive increasing attention for their potential applications in filters, resonators, and waveguides. This paper presents a review of recent works related to phononic plate waves which have recently been published by the authors and coworkers. Theoretical and experimental studies of Lamb waves in 2-D PC plate structures are covered. On the theoretical side, analyses of Lamb waves in 2-D PC plates using the plane wave expansion (PWE) method, finite-difference time-domain (FDTD) method, and finite-element (FE) method are addressed. These methods were applied to study the complete band gaps of Lamb waves, characteristics of the propagating and localized wave modes, and behavior of anomalous refraction, called negative refraction, in the PC plates. The theoretical analyses demonstrated the effects of PC-based negative refraction, lens, waveguides, and resonant cavities. We also discuss the influences of geometrical parameters on the guiding and resonance efficiency and on the frequencies of waveguide and cavity modes. On the experimental side, the design and fabrication of a silicon-based Lamb wave resonator which utilizes PC plates as reflective gratings to form the resonant cavity are discussed. The measured results showed significant improvement of the insertion losses and quality factors of the resonators when the PCs were applied. PMID:21989878

  5. A novel real-time fuzzy-based diagnostic system of roll eccentricity influence in finishing hot strip mills

    SciTech Connect

    Garcia, D.F.; Lopez, J.M.; Suarez, F.J.; Garcia, J.; Obeso, F.; Gonzalez, J.A.

    1998-11-01

    This paper proposes a method for the diagnosis of the influence of roll eccentricity on the strip thickness at the exit of a finishing hot strip mill (FHSM). Each strip thickness defect on exit is related to a roll of the FHSM, allowing the implementation of an optimal policy for the substitution and maintenance of the rolls, thereby maintaining the required quality level of the strip. This policy allows the minimization of roll changes and the concentration of several changes at the same time, reducing production costs. Fuzzy logic is used to compare spectra, looking for common patterns, which allows for a totally automated diagnostic system. Moreover, an innovative estimate of roll eccentricity based on a least-squares algorithm has been developed, which provides higher accuracy than classical algorithms, as well as a drastic reduction in the time required to perform eccentricity tests.

  6. Effects of silicon on the oxidation, hot-corrosion, and mechanical behavior of two cast nickel-base superalloys

    NASA Technical Reports Server (NTRS)

    Miner, R. V., Jr.

    1977-01-01

    Cast specimens of nickel-base superalloys 713C and Mar-M200 with nominal additions of 0, 0.5, and 1 wt% Si were evaluated for oxidation and corrosion resistance, tensile and stress-rupture properties, microstructure, and phase relations. Results are compared with those of an earlier study of the effects of Si in B-1900. Si had similar effects on all three superalloys. It improves oxidation resistance but the improvement in 713C and Mar-M200 was considerably less than in B-1900. Hot-corrosion resistance is also improved somewhat. Si is, however, detrimental to mechanical properties, in particular, rupture strength and tensile ductility. Si has two obvious microstructural effects. It increases the amount of gamma-prime precipitated in eutectic nodules and promotes a Mo(Ni,Si)2 Laves phase in the alloys containing Mo. These microstructural effects do not appear responsible for the degradation of mechanical properties, however.

  7. HVOF Spraying of Fe-Based MMC Coatings with In Situ Formation of Hard Particles by Hot Isostatic Pressing

    NASA Astrophysics Data System (ADS)

    Röttger, A.; Weber, S. L.; Theisen, W.; Rajasekaran, B.; Vaßen, R.

    2012-03-01

    Thick (2-3 mm) Fe-base coatings with admixed ferrotitanium (Fe30Ti70) were applied to austenitic steel by a high-velocity oxy-fuel process (HVOF). Hot-isostatic pressing (HIP) was carried out to the decrease porosity and to increase the material strength, wear resistance, and adhesive bond strength of the deposited coating to the substrate material. SEM and XRD investigations confirmed the formation of hard titanium carbide (TiC) particles during HIP treatment as a result of strong carbon diffusion out of the metal matrix and into the Fe30Ti70 particles. The mechanical and wear properties of the densified coatings were investigated by means of shear tests, hardness measurements, and abrasive wear tests. A comparison of the coatings in the as-sprayed and the HIPed state showed a large increase in the wear resistance due to in situ TiC formation.

  8. Ultrasensitive SERS detection of trinitrotoluene through capillarity-constructed reversible hot spots based on ZnO-Ag nanorod hybrids

    NASA Astrophysics Data System (ADS)

    He, Xuan; Wang, Hui; Li, Zhongbo; Chen, Dong; Liu, Jiahui; Zhang, Qi

    2015-04-01

    A simple and efficient self-approach strategy was used to apply ultrasensitivity and self-revive ZnO-Ag hybrid surface-enhanced Raman scattering (SERS) sensors for the highly sensitive and selective detection of explosive TNT in both solution and vapour conditions. The good ultrasensitive sensing performance is a result of the abundant Raman hot spots, which were spontaneously formed in a reversible way by the self-approaching of flexible ZnO-Ag hybrid nanorods driven by the capillary force of solvent evaporation. Moreover, the enhancement effect was repeatedly renewed by the reconstruction of molecular bridges, which could selectively detect TNT with a lower limit of 4 × 10-14 M. In addition, TNT vapor was also tested under this sensor, whereby once the ZnO-Ag NRs hybrid substrate was dipped in TNT, this substrate could detect the existence of TNT even in 5 detection cycles via a capillarity-constructed reversible hot spots approach. Compared with other pure Ag-based SERS sensors, this ZnO-Ag hybrid SERS sensor could rapidly self-revive SERS-activity by simple UV light irradiation and could retain stable SERS sensitivity for one month when used for TNT detection. This stable and ultrasensitive SERS substrate demonstrates a new route to eliminate the oxidized inactive problem of traditional Ag-based SERS substrates and suggests promising use in the applications of such hybrids as real-time online sensors for explosives detection.A simple and efficient self-approach strategy was used to apply ultrasensitivity and self-revive ZnO-Ag hybrid surface-enhanced Raman scattering (SERS) sensors for the highly sensitive and selective detection of explosive TNT in both solution and vapour conditions. The good ultrasensitive sensing performance is a result of the abundant Raman hot spots, which were spontaneously formed in a reversible way by the self-approaching of flexible ZnO-Ag hybrid nanorods driven by the capillary force of solvent evaporation. Moreover, the enhancement

  9. The influence of particle size on the rheological properties of plate-like iron particle based magnetorheological fluids

    NASA Astrophysics Data System (ADS)

    Shah, Kruti; Choi, Seung-Bok

    2015-01-01

    This work is devoted to the dependence of particle size on magnetorheological properties of magnetorheological fluid (MRF) consisting of plate-like iron particles suspended in a carrier liquid with two aspects. One aspect is to study the influence of the particle size on the rheological properties of the MRF, and the other is to investigate the influence of small-sized particles on the large-sized MRF. In order to achieve this goal, firstly, two different types of MR suspensions have been constituted by a plate-like iron particle; one is small with an average particle size of 2 μm in diameter, and the other is large with an average particle size of 19 μm in diameter. In this work, these are denoted as S-MRF and L-MRF, respectively. Secondly, in order to check the influence of the small particle size of the large-sized MR fluid, three different weight fractions of bidisperse MRF samples are prepared. The structural and morphology of plate-like iron particles are described in detail. The magnetic properties of these MR fluids are carried out at room temperature using the magnetometer, followed by the investigation on the field-dependent rheological properties of these MR fluids. It is observed that in both the S-MRF and L-MRF, the yield stress and viscosity is increased by the increasing particle size, which directly shows a correlation with the fluid magnetization. It is also identified from the test of the bidisperse MRF samples that the yield and viscosity depend on the weight fraction due to the magnetostatic interaction between the two different sizes of particles. Based on the rheological properties, some figures of merit are derived for the proposed MRF samples, which are important in the design of the application device. The sedimentation experiments for MRF samples are performed to check the stability of the MRF each day. With the basic rheological properties and sedimentation experiments, it is clearly demonstrated that the bidisperse MR suspension with a

  10. Solitary wave-based delamination detection in composite plates using a combined granular crystal sensor and actuator

    NASA Astrophysics Data System (ADS)

    Kim, Eunho; Restuccia, Francesco; Yang, Jinkyu; Daraio, Chiara

    2015-12-01

    We experimentally and numerically investigate a diagnostic method for detecting hidden delamination in composite panels, using highly nonlinear solitary waves. Solitary waves are a type of nonlinear waves with strong energy intensity and non-distortive nature, which can be controllably generated in one-dimensional granular crystals. In this study, we use granular crystals as a combined sensor and actuator to detect hidden delamination in carbon fiber reinforced polymer (CFRP) composite panels. Specifically, we locally excite a CFRP composite specimen using the granular crystal as an actuator and measure the reflected waves that carry the specimen’s diagnostic information using the same device as a sensor. We first investigate the effect of the panel’s boundary conditions on the response of the reflected solitary waves. We then investigate the interactions of a solitary wave with delamination hidden in the CFRP composite specimen. Lastly, we define a damage index based on the solitary waves’ responses to identify the location of the hidden delamination in the CFRP composite panel. The solitary wave-based diagnostic method can provide unique merits, such as portable and fast sensing of composites’ hidden damage, thereby with the potential of being used for hot spot monitoring of composite-based structures.

  11. Evaluation of resistive-plate-chamber-based TOF-PET applied to in-beam particle therapy monitoring

    NASA Astrophysics Data System (ADS)

    Torres-Espallardo, I.; Diblen, F.; Rohling, H.; Solevi, P.; Gillam, J.; Watts, D.; España, S.; Vandenberghe, S.; Fiedler, F.; Rafecas, M.

    2015-05-01

    Particle therapy is a highly conformal radiotherapy technique which reduces the dose deposited to the surrounding normal tissues. In order to fully exploit its advantages, treatment monitoring is necessary to minimize uncertainties related to the dose delivery. Up to now, the only clinically feasible technique for the monitoring of therapeutic irradiation with particle beams is Positron Emission Tomography (PET). In this work we have compared a Resistive Plate Chamber (RPC)-based PET scanner with a scintillation-crystal-based PET scanner for this application. In general, the main advantages of the RPC-PET system are its excellent timing resolution, low cost, and the possibility of building large area systems. We simulated a partial-ring scanner based on an RPC prototype under construction within the Fondazione per Adroterapia Oncologica (TERA). For comparison with the crystal-based PET scanner we have chosen the geometry of a commercially available PET scanner, the Philips Gemini TF. The coincidence time resolution used in the simulations takes into account the current achievable values as well as expected improvements of both technologies. Several scenarios (including patient data) have been simulated to evaluate the performance of different scanners. Initial results have shown that the low sensitivity of the RPC hampers its application to hadron-beam monitoring, which has an intrinsically low positron yield compared to diagnostic PET. In addition, for in-beam PET there is a further data loss due to the partial ring configuration. In order to improve the performance of the RPC-based scanner, an improved version of the RPC detector (modifying the thickness of the gas and glass layers), providing a larger sensitivity, has been simulated and compared with an axially extended version of the crystal-based device. The improved version of the RPC shows better performance than the prototype, but the extended version of the crystal-based PET outperforms all other options.

  12. How mantle slabs drive plate tectonics.

    PubMed

    Conrad, Clinton P; Lithgow-Bertelloni, Carolina

    2002-10-01

    The gravitational pull of subducted slabs is thought to drive the motions of Earth's tectonic plates, but the coupling between slabs and plates is not well established. If a slab is mechanically attached to a subducting plate, it can exert a direct pull on the plate. Alternatively, a detached slab may drive a plate by exciting flow in the mantle that exerts a shear traction on the base of the plate. From the geologic history of subduction, we estimated the relative importance of "pull" versus "suction" for the present-day plates. Observed plate motions are best predicted if slabs in the upper mantle are attached to plates and generate slab pull forces that account for about half of the total driving force on plates. Slabs in the lower mantle are supported by viscous mantle forces and drive plates through slab suction. PMID:12364804

  13. Kinetics of Mn-based sorbents for hot coal gas desulfurization. Quarterly report, September 15 - December 15, 1996

    SciTech Connect

    Hepworth, M.T.

    1996-12-31

    Manganese-based sorbents have been investigated for the removal of hydrogen sulfide (the primary sulfur bearing compound) from hot coal gases prior to its use in combined cycle turbines. Four formulations of Mn-based sorbents were tested in an ambient-pressure fixed-bed reactor to determine steady state H{sub 2}S concentrations, breakthrough times and effectiveness of the sorbent when subjected to cyclic sulfidation and regeneration testing. In a previous report, the sulfidation results were presented. Manganese-based sorbents with molar ratios > 1:1 Mn:Substrate were effective in reducing the H{sub 2}S concentration in simulated coal gases to less than 100 ppmv over five cycles. Actual breakthrough time for formulation C6-2-1100 was as high as 73% of breakthrough time based on wt% Mn in sorbent. In this report, the regeneration results will be presented. Regeneration tests determined that loaded pellets can be fully regenerated in air/steam mixture at 750{degrees}C with minimal sulfate formation. 16 refs., 9 figs., 5 tabs.

  14. Kinetics of MN-based sorbents for hot coal gas desulfurization. Semiannual report, December 15, 1996--March 15, 1997

    SciTech Connect

    Hepworth, M.T.

    1997-03-01

    Manganese-based sorbents have been investigated for the removal of hydrogen sulfide (the primary sulfur bearing compound) from hot coal gases prior to its use in combined cycle turbines. Four formulations of Mn-based sorbents were tested in an ambient-pressure fixed-bed reactor to determine steady state H{sub 2}S concentrations, breakthrough times and effectiveness of the sorbent when subjected to cyclic sulfidation and regeneration testing. In previous reports, the sulfidation and regeneration results from cyclic testing done at 600{degrees}C were presented. Manganese-based sorbents with molar ratios >1:1 Mn:substrate were effective in reducing the H{sub 2}S concentration in simulated coal gases to less than 100 ppmv over five cycles. Actual breakthrough time for formulation C6-2-1100 was as high as 73% of breakthrough time based on wt% Mn in sorbent. Regeneration tests determined that loaded pellets can be fully regenerated in air/steam mixture at 750{degrees}C with minimal sulfate formation. In this report, the results from the cyclic crush strength tests, sulfur profile test, and cyclic testing done after 5 cycles showed decreases in strength from 12.6% to 57.9%. Cyclic testing at 550{degrees}C showed pre-breakthrough concentrations as low as 10 ppmv. Cyclic testing done at 2 L/min and 3 L/min did not show any significant difference in pre-breakthrough concentrations or capacity.

  15. Effect of hot implantation on ON-current enhancement utilizing isoelectronic trap in Si-based tunnel field-effect transistors

    NASA Astrophysics Data System (ADS)

    Mori, Takahiro; Mizubayashi, Wataru; Morita, Yukinori; Migita, Shinji; Fukuda, Koichi; Miyata, Noriyuki; Yasuda, Tetsuji; Masahara, Meishoku; Ota, Hiroyuki

    2015-03-01

    A tunneling-current enhancement technology for Si-based tunnel field-effect transistors (TFETs) utilizing an Al-N isoelectronic trap (IET) has been proposed recently. In this study, we investigate hot implantation as a doping technique for Al-N isoelectronic impurity. Hot implantation reduces the damage induced by Al and N implantation processes, resulting in performance improvement of IET-assisted TFETs, e.g., a 12-fold enhancement in the driving current at an operation voltage of 0.5 V and an approximately one-third reduction in the subthreshold slope. By hot implantation, we can achieve a higher driving current in Si-based TFETs using the IET technology.

  16. Fragment-based identification of druggable ‘hot spots’ of proteins using Fourier domain correlation techniques

    PubMed Central

    Brenke, Ryan; Kozakov, Dima; Chuang, Gwo-Yu; Beglov, Dmitri; Hall, David; Landon, Melissa R.; Mattos, Carla; Vajda, Sandor

    2009-01-01

    Motivation: The binding sites of proteins generally contain smaller regions that provide major contributions to the binding free energy and hence are the prime targets in drug design. Screening libraries of fragment-sized compounds by NMR or X-ray crystallography demonstrates that such ‘hot spot’ regions bind a large variety of small organic molecules, and that a relatively high ‘hit rate’ is predictive of target sites that are likely to bind drug-like ligands with high affinity. Our goal is to determine the ‘hot spots’ computationally rather than experimentally. Results: We have developed the FTMAP algorithm that performs global search of the entire protein surface for regions that bind a number of small organic probe molecules. The search is based on the extremely efficient fast Fourier transform (FFT) correlation approach which can sample billions of probe positions on dense translational and rotational grids, but can use only sums of correlation functions for scoring and hence is generally restricted to very simple energy expressions. The novelty of FTMAP is that we were able to incorporate and represent on grids a detailed energy expression, resulting in a very accurate identification of low-energy probe clusters. Overlapping clusters of different probes are defined as consensus sites (CSs). We show that the largest CS is generally located at the most important subsite of the protein binding site, and the nearby smaller CSs identify other important subsites. Mapping results are presented for elastase whose structure has been solved in aqueous solutions of eight organic solvents, and we show that FTMAP provides very similar information. The second application is to renin, a long-standing pharmaceutical target for the treatment of hypertension, and we show that the major CSs trace out the shape of the first approved renin inhibitor, aliskiren. Availability: FTMAP is available as a server at http://ftmap.bu.edu/. Contact: vajda@bu.edu Supplementary

  17. Detection of plate components defects by surface wave based on transducer arrays

    NASA Astrophysics Data System (ADS)

    Liu, Zhao; Meng, Fanwu; Xu, Chunguang; Li, Xipeng; Zhou, Shiyuan; Xiao, Dingguo

    2013-01-01

    Detection of micro damages in flat components on-site has a significant sense for improving the safety of the equipment. Based on the theory of the surface acoustic wave (SAW) propagation laws in flat components, the micro damage detection in the flat component has been researched. Using wavelet analysis technology and inversed spectrum technology, the microdamages' feature parameters can be extracted out accurately. Utilizing the feature parameters got by every transducer in a transducer arrays, the micro-damages' image can be reconstructed, and the micro-damages' location, outer geometric configuration, and damage level can be showed clearly.

  18. Design of the IXO optics based on thin glass plates connected by reinforcing ribs

    NASA Astrophysics Data System (ADS)

    Parodi, G.; Martelli, F.; Basso, S.; Citterio, O.; Civitani, M.; Conconi, P.; Ghigo, M.; Pareschi, G.; Zambra, A.

    2011-09-01

    Effective area requirements for the large X-ray mirror of the International X-ray Observatory (IXO) are about 3 m2 at 1keV, 0.65 m2 at 6 keV and 150 cm2 at 30 keV. Because of its large dimension, the telescope cannot be realized as a monolithic structure but rather it requires the integration and assembly in the telescope optical bench of a number of basic module units, called X-ray Optical Unit (XOU). We are currently studying a method for the production of these basic units that is based on the slumping technology for the production of thin glass segmented mirrors. It foresees the implementation of a stacking integration concept based on the use of reinforcing ribs connecting the glass segments in order to create very stiff structures. This paper reports on the last design of the single optical module and describe the results of FEM analyses that show how it is possible to use an innovative approach to the integration of the slumped glass foils.

  19. Hot Canyon

    SciTech Connect

    2012-01-01

    This historical film footage, originally produced in the early 1950s as part of a series by WOI-TV, shows atomic research at Ames Laboratory. The work was conducted in a special area of the Laboratory known as the "Hot Canyon."

  20. Hot Tickets

    ERIC Educational Resources Information Center

    Fox, Bette-Lee; Hoffert, Barbara; Kuzyk, Raya; McCormack, Heather; Williams, Wilda

    2008-01-01

    This article describes the highlights of this year's BookExpo America (BEA) held at the Los Angeles Convention Center. The attendees at BEA had not minded that the air was recycled, the lighting was fluorescent, and the food was bad. The first hot book sighting came courtesy of Anne Rice. Michelle Moran, author of newly published novel, "The…

  1. Hot Canyon

    ScienceCinema

    None

    2013-03-01

    This historical film footage, originally produced in the early 1950s as part of a series by WOI-TV, shows atomic research at Ames Laboratory. The work was conducted in a special area of the Laboratory known as the "Hot Canyon."

  2. High-throughput microtitre plate-based assay for DNA topoisomerases.

    PubMed

    Taylor, James A; Burton, Nicolas P; Maxwell, Anthony

    2012-01-01

    We have developed a rapid, high-throughput assay for measuring the catalytic activity (DNA supercoiling or relaxation) of DNA topoisomerases. The assay utilizes intermolecular triplex formation between an immobilized triplex-forming oligo (TFO) and a triplex-forming region inserted into the plasmid substrate (pNO1), and capitalizes on the observation that supercoiled DNA forms triplexes more readily than relaxed DNA. Thus, supercoiled DNA is preferentially retained by the TFO under triplex-forming conditions while relaxed DNA can be washed away. Due to its high speed of sample analysis and reduced sample handling over conventional gel-based techniques, this assay can be used to screen chemical libraries for novel inhibitors of topoisomerases. PMID:22130995

  3. Machinability of hastelloy C-276 using Hot-pressed sintered Ti(C7N3)-based cermet cutting tools

    NASA Astrophysics Data System (ADS)

    Xu, Kaitao; Zou, Bin; Huang, Chuanzhen; Yao, Yang; Zhou, Huijun; Liu, Zhanqiang

    2015-05-01

    C-276 nickel-based alloy is a difficult-to-cut material. In high-speed machining of Hastelloy C-276, notching is a prominent failure mode due to high mechanical properties of work piece, which results in the short tool life and low productivity. In this paper, a newly developed Ti(C7N3)-based cermet insert manufactured by a hot-pressing method is used to machine the C-276 nickel-based alloy, and its cutting performances are studied. Based on orthogonal experiment method, the influence of cutting parameters on tool life, material removal rates and surface roughness are investigated. Experimental research results indicate that the optimal cutting condition is a cutting speed of 50 m/min, depth of cut of 0.4 mm and feed rate of 0.15 mm/r if the tool life and material removal rates are considered comprehensively. In this case, the tool life is 32 min and material removal rates are 3000 mm3/min, which is appropriate to the rough machining. If the tool life and surface roughness are considered, the better cutting condition is a cutting speed of 75 m/min, depth of cut of 0.6 mm and feed rate of 0.1 mm/r. In this case, the surface roughness is 0.59μm. Notch wear, flank wear, chipping at the tool nose, built-up edge(BUE) and micro-cracks are found when Ti(C7N3)-based cermet insert turned Hastelloy C-276. Oxidation, adhesive, abrasive and diffusion are the wear mechanisms, which can be investigated by the observations of scanning electron microscope and energy-dispersive spectroscopy. This research will help to guide studies on the evaluation of machining parameters to further advance the productivity of nickel based alloy Hastelloy C-276 machining.

  4. Operating experience with Grimethorpe Distributor Plate Seal. Part 1. Initial design and first stage modification

    SciTech Connect

    Cavanna, J.; Morsbach, B.; Jack, A.R.

    1981-03-01

    During the early stages of hot commissioning of the Grimethorpe Experimental Facility it was found that the Distributor Plate Seal did not operate correctly. It allowed the upward leakage of fluidizing air and the downward leakage of bed material out of the combustor. The seal was modified and has now performed satisfactorily during a number of hot commissioning trials. Additionally, a further modification involving the elimination of the seal from the base of the combustor is being developed and will be available should the first modification prove to be unacceptable as a long term solution.

  5. A physically-based continuum damage mechanics model for numerical prediction of damage growth in laminated composite plates

    NASA Astrophysics Data System (ADS)

    Williams, Kevin Vaughan

    Rapid growth in use of composite materials in structural applications drives the need for a more detailed understanding of damage tolerant and damage resistant design. Current analytical techniques provide sufficient understanding and predictive capabilities for application in preliminary design, but current numerical models applicable to composites are few and far between and their development into well tested, rigorous material models is currently one of the most challenging fields in composite materials. The present work focuses on the development, implementation, and verification of a plane-stress continuum damage mechanics based model for composite materials. A physical treatment of damage growth based on the extensive body of experimental literature on the subject is combined with the mathematical rigour of a continuum damage mechanics description to form the foundation of the model. The model has been implemented in the LS-DYNA3D commercial finite element hydrocode and the results of the application of the model are shown to be physically meaningful and accurate. Furthermore it is demonstrated that the material characterization parameters can be extracted from the results of standard test methodologies for which a large body of published data already exists for many materials. Two case studies are undertaken to verify the model by comparison with measured experimental data. The first series of analyses demonstrate the ability of the model to predict the extent and growth of damage in T800/3900-2 carbon fibre reinforced polymer (CFRP) plates subjected to normal impacts over a range of impact energy levels. The predicted force-time and force-displacement response of the panels compare well with experimental measurements. The damage growth and stiffness reduction properties of the T800/3900-2 CFRP are derived using published data from a variety of sources without the need for parametric studies. To further demonstrate the physical nature of the model, a IM6

  6. Impact Damage Detection in Composite Plates using a Self-diagnostic Electro-Mechanical Impedance-based Structural Health Monitoring System

    NASA Astrophysics Data System (ADS)

    Sharif-Khodaei, Z.; Ghajari, M.; Aliabadi, M. H.

    2015-03-01

    In this work, application of the electro-mechanical impedance (EMI) method in structural health monitoring as a damage detection technique has been investigated. A damage metric based on the real and imaginary parts of the impedance measures is introduced. Numerical and experimental tests are carried out to investigate the applicability of the method for various types of damage, such as debonding between the transducers and the plate, faulty sensors and impact damage in composite plates. The effect of several parameters, such as environmental effects, frequency sweep, severity of damage, location of damage, etc., on the damage metric has been reported.

  7. Hot-Spots and Holiness: Faith-Based Topics in Freshman Composition.

    ERIC Educational Resources Information Center

    Worth, Jan

    For an instructor of freshman composition at the University of Michigan at Flint, faith-based writing topics offer particular challenges and sometimes intersect in troubling ways with her own prejudices and personal history as a teacher and as a person. But if handled correctly, she believes that a teacher's interaction with students about…

  8. HOT ELUENT CAPILLARY LIQUID CHROMATOGRAPHY USING ZIRCONIA AND TITANIA BASED STATIONARY PHASES. (R825344)

    EPA Science Inventory

    Abstract

    High speed capillary liquid chromatographic separations using a simple home made system constructed from readily available inexpensive components have been studied. Using thermally stable zirconia and titania based packing, the separation of eight alkylbenzene...

  9. Neutron Imager and Flux Monitor Based on Micro Channel Plates (MCP) in Electrostatic Mirror Configuration

    NASA Astrophysics Data System (ADS)

    Variale, V.

    In this paper, a new high transparency device based on MCP for the monitoring the flux and spatial profile of a neutron beam will be described. The assembly consists of a carbon foil with a 6Li deposit, placed in the beam, and a MCP equipped with a phosphor screen readout viewed by a CCD camera, placed outside the beam. Secondary emitted electrons (SEE) produced in the carbon foil by the alpha-particles and tritons from the 6Li+n reaction, are deflected to the MCP detector by means of an electrostatic mirror, suitably designed to preserve the spatial resolution. The conductive layer on the phosphor can be used for neutron counting, and to obtain time-of-flight information. A peculiar feature of this device is that the use of an electrostatic mirror minimizes the perturbation of the neutron beam, i.e. absorption and scattering. It can be used at existing time-of-flight (TOF) facilities, in particular at the n_TOF facility at CERN, for monitoring the flux and special profile of the neutron beam in the thermal and epithermal region. In this work, the device principle and design will be presented, together with the main features in terms of resolution and neutron detection efficiency.

  10. Effect of Mn/S Ratio on the Hot Ductility of Eco-friendly Bi-S based Free Cutting Steel

    NASA Astrophysics Data System (ADS)

    Liu, Haitao; Yu, Yanchong; Chen, Weiqing; Wang, Qingxian; Wang, Guangshun

    2014-12-01

    The hot ductility of eco-friendly Bi-S based free cutting steels with different Mn/S ratios was studied using a Gleeble-1500 thermal-mechanical simulator. The hot ductility of the steel was found to depend on the Mn/S ratio, and the Mn/S ratio of the steel should be greater than 3.5 for hot rolling of billets without crack development. The low Mn/S ratio would inhibit the occurrence of the dynamic recrystallization and cause the formation of the low melting point sulfide Fe-rich (Fe,Mn)S as secondary phases, which could obviously reduce the strength of the grain boundary and resulted in the formation of cracks along the grain boundary. The higher the Mn/S ratio in the steel, the lower the Fe content in the Fe-rich (Fe,Mn)S phases. When the Mn/S ratio in the steel was high enough, the sulfide phases in the steel were mainly MnS as primary inclusions and the low melting point sulfide phases could be effectively avoided forming. While the Mn/S ratio could influence the hot ductility of the steel over the whole temperature range of 900-1200 °C, the segregation of bismuth along grain boundary could be harmful to the hot ductility in addition to the lower Mn/S ratio for the temperature was no more than 1050 °C.

  11. GROUND-BASED TRANSIT SPECTROSCOPY OF THE HOT-JUPITER WASP-19b IN THE NEAR-INFRARED

    SciTech Connect

    Bean, Jacob L.; Seifahrt, Andreas; Desert, Jean-Michel; Madhusudhan, Nikku; Chilingarian, Igor; Szentgyorgyi, Andrew; Homeier, Derek

    2013-07-10

    We present ground-based measurements of the transmission and emission spectra of the hot-Jupiter WASP-19b in nine spectroscopic channels from 1.25 to 2.35 {mu}m. The measurements are based on the combined analysis of time-series spectroscopy obtained during two complete transits and two complete secondary eclipses of the planet. The observations were performed with the MMIRS instrument on the Magellan II telescope using the technique of multi-object spectroscopy with wide slits. We compare the transmission and emission data to theoretical models to constrain the composition and thermal structure of the planet's atmosphere. Our measured transmission spectrum exhibits a scatter that corresponds to 1.3 scale heights of the planet's atmosphere, which is consistent with the size of spectral features predicted by theoretical models for a clear atmosphere. We detect the secondary eclipses of the planet at significances ranging from 2.2{sigma} to 14.4{sigma}. The secondary eclipse depths, and the significances of the detections increase toward longer wavelengths. Our measured emission spectrum is consistent with a 2250 K effectively isothermal one-dimensional model for the planet's dayside atmosphere. This model also matches previously published photometric measurements from the Spitzer Space Telescope and ground-based telescopes. These results demonstrate the important role that ground-based observations using multi-object spectroscopy can play in constraining the properties of exoplanet atmospheres, and they also emphasize the need for high-precision measurements based on observations of multiple transits and eclipses.

  12. Theoretical study on the cooperative exciton dissociation process based on dimensional and hot charge-transfer state effects in an organic photocell

    NASA Astrophysics Data System (ADS)

    Shimazaki, Tomomi; Nakajima, Takahito

    2016-06-01

    This paper discusses the exciton dissociation process at the donor-acceptor interface in organic photocells. In our previous study, we introduced a local temperature to handle the hot charge-transfer (CT) state and calculated the exciton dissociation probability based on the 1D organic semiconductor model [T. Shimazaki and T. Nakajima, Phys. Chem. Chem. Phys. 17, 12538 (2015)]. Although the hot CT state plays an essential role in exciton dissociations, the probabilities calculated are not high enough to efficiently separate bound electron-hole pairs. This paper focuses on the dimensional (entropy) effect together with the hot CT state effect and shows that cooperative behavior between both effects can improve the exciton dissociation process. In addition, we discuss cooperative effects with site-disorders and external-electric-fields.

  13. Theoretical study on the cooperative exciton dissociation process based on dimensional and hot charge-transfer state effects in an organic photocell.

    PubMed

    Shimazaki, Tomomi; Nakajima, Takahito

    2016-06-21

    This paper discusses the exciton dissociation process at the donor-acceptor interface in organic photocells. In our previous study, we introduced a local temperature to handle the hot charge-transfer (CT) state and calculated the exciton dissociation probability based on the 1D organic semiconductor model [T. Shimazaki and T. Nakajima, Phys. Chem. Chem. Phys. 17, 12538 (2015)]. Although the hot CT state plays an essential role in exciton dissociations, the probabilities calculated are not high enough to efficiently separate bound electron-hole pairs. This paper focuses on the dimensional (entropy) effect together with the hot CT state effect and shows that cooperative behavior between both effects can improve the exciton dissociation process. In addition, we discuss cooperative effects with site-disorders and external-electric-fields. PMID:27334193

  14. Fabrication and characterization of silicon based thermal neutron detector with hot wire chemical vapor deposited boron carbide converter

    NASA Astrophysics Data System (ADS)

    Chaudhari, Pradip; Singh, Arvind; Topkar, Anita; Dusane, Rajiv

    2015-04-01

    In order to utilize the well established silicon detector technology for neutron detection application, a silicon based thermal neutron detector was fabricated by integrating a thin boron carbide layer as a neutron converter with a silicon PIN detector. Hot wire chemical vapor deposition (HWCVD), which is a low cost, low temperature process for deposition of thin films with precise thickness was explored as a technique for direct deposition of a boron carbide layer over the metalized front surface of the detector chip. The presence of B-C bonding and 10B isotope in the boron carbide film were confirmed by Fourier transform infrared spectroscopy and secondary ion mass spectrometry respectively. The deposition of HWCVD boron carbide layer being a low temperature process was observed not to cause degradation of the PIN detector. The response of the detector with 0.2 μm and 0.5 μm thick boron carbide layer was examined in a nuclear reactor. The pulse height spectrum shows evidence of thermal neutron response with signature of (n, α) reaction. The results presented in this article indicate that HWCVD boron carbide deposition technique would be suitable for low cost industrial fabrication of PIN based single element or 1D/2D position sensitive thermal neutron detectors.

  15. Hot-melt extruded filaments based on pharmaceutical grade polymers for 3D printing by fused deposition modeling.

    PubMed

    Melocchi, Alice; Parietti, Federico; Maroni, Alessandra; Foppoli, Anastasia; Gazzaniga, Andrea; Zema, Lucia

    2016-07-25

    Fused deposition modeling (FDM) is a 3D printing technique based on the deposition of successive layers of thermoplastic materials following their softening/melting. Such a technique holds huge potential for the manufacturing of pharmaceutical products and is currently under extensive investigation. Challenges in this field are mainly related to the paucity of adequate filaments composed of pharmaceutical grade materials, which are needed for feeding the FDM equipment. Accordingly, a number of polymers of common use in pharmaceutical formulation were evaluated as starting materials for fabrication via hot melt extrusion of filaments suitable for FDM processes. By using a twin-screw extruder, filaments based on insoluble (ethylcellulose, Eudragit(®) RL), promptly soluble (polyethylene oxide, Kollicoat(®) IR), enteric soluble (Eudragit(®) L, hydroxypropyl methylcellulose acetate succinate) and swellable/erodible (hydrophilic cellulose derivatives, polyvinyl alcohol, Soluplus(®)) polymers were successfully produced, and the possibility of employing them for printing 600μm thick disks was demonstrated. The behavior of disks as barriers when in contact with aqueous fluids was shown consistent with the functional application of the relevant polymeric components. The produced filaments were thus considered potentially suitable for printing capsules and coating layers for immediate or modified release, and, when loaded with active ingredients, any type of dosage forms. PMID:27215535

  16. Hot melt extrusion based solid solution approach: Exploring polymer comparison, physicochemical characterization and in-vivo evaluation.

    PubMed

    Fule, Ritesh; Paithankar, Vivek; Amin, Purnima

    2016-02-29

    The objective of this study was to develop solid solution (SSL) using hot-melt extrusion as a continuous manufacturing method. Powder blends of artesunate (ARS) a water insoluble drug with either Soluplus (SOL) or Kollidon VA64 (VA64) and additives in the form of surfactants or plasticizers were extruded to manufacture extrudes. The incorporation of surfactant or plasticizers facilitates smooth extrusion processing of the drug-excipient blend which directly reduced the residence time to form extrudes and works as parameter to control flow of the drug-excipients melt inside the extruder barrel. Differential scanning calorimetry (DSC) and X-ray diffraction (TXRD) analysis revealed the existence of the drug within the extrudes in amorphous state. Scanning electron microscopy (SEM), Raman spectroscopy (RS), Raman imaging (RI) and Atomic force microscopy (AFM) analytical characterization were carry out on the SSL formulations showed a homogeneous drug distribution within the extrudes. (2)D NMR and (1)H NMR studies were undertaken to reveal the possible drug-excipient interactions. The SSL produced via continuous HME processing showed significantly faster release of ARS compared to the pure drug substance. It is observed that F1 SSL (soluplus based) have 66.44 times higher AUC(0-72) and 16.60 times higher Cmax than pure ARS. Also K1 SSL (Kollidon VA64 based) have 62.20 times higher AUC(0-72) and 13.40 times higher Cmax than pure ARS. PMID:26746801

  17. Bilayer insulator tunnel barriers for graphene-based vertical hot-electron transistors.

    PubMed

    Vaziri, S; Belete, M; Dentoni Litta, E; Smith, A D; Lupina, G; Lemme, M C; Östling, M

    2015-08-14

    Vertical graphene-based device concepts that rely on quantum mechanical tunneling are intensely being discussed in the literature for applications in electronics and optoelectronics. In this work, the carrier transport mechanisms in semiconductor-insulator-graphene (SIG) capacitors are investigated with respect to their suitability as electron emitters in vertical graphene base transistors (GBTs). Several dielectric materials as tunnel barriers are compared, including dielectric double layers. Using bilayer dielectrics, we experimentally demonstrate significant improvements in the electron injection current by promoting Fowler-Nordheim tunneling (FNT) and step tunneling (ST) while suppressing defect mediated carrier transport. High injected tunneling current densities approaching 10(3) A cm(-2) (limited by series resistance), and excellent current-voltage nonlinearity and asymmetry are achieved using a 1 nm thick high quality dielectric, thulium silicate (TmSiO), as the first insulator layer, and titanium dioxide (TiO2) as a high electron affinity second layer insulator. We also confirm the feasibility and effectiveness of our approach in a full GBT structure which shows dramatic improvement in the collector on-state current density with respect to the previously reported GBTs. The device design and the fabrication scheme have been selected with future CMOS process compatibility in mind. This work proposes a bilayer tunnel barrier approach as a promising candidate to be used in high performance vertical graphene-based tunneling devices. PMID:26176739

  18. Bilayer insulator tunnel barriers for graphene-based vertical hot-electron transistors

    NASA Astrophysics Data System (ADS)

    Vaziri, S.; Belete, M.; Dentoni Litta, E.; Smith, A. D.; Lupina, G.; Lemme, M. C.; Östling, M.

    2015-07-01

    Vertical graphene-based device concepts that rely on quantum mechanical tunneling are intensely being discussed in the literature for applications in electronics and optoelectronics. In this work, the carrier transport mechanisms in semiconductor-insulator-graphene (SIG) capacitors are investigated with respect to their suitability as electron emitters in vertical graphene base transistors (GBTs). Several dielectric materials as tunnel barriers are compared, including dielectric double layers. Using bilayer dielectrics, we experimentally demonstrate significant improvements in the electron injection current by promoting Fowler-Nordheim tunneling (FNT) and step tunneling (ST) while suppressing defect mediated carrier transport. High injected tunneling current densities approaching 103 A cm-2 (limited by series resistance), and excellent current-voltage nonlinearity and asymmetry are achieved using a 1 nm thick high quality dielectric, thulium silicate (TmSiO), as the first insulator layer, and titanium dioxide (TiO2) as a high electron affinity second layer insulator. We also confirm the feasibility and effectiveness of our approach in a full GBT structure which shows dramatic improvement in the collector on-state current density with respect to the previously reported GBTs. The device design and the fabrication scheme have been selected with future CMOS process compatibility in mind. This work proposes a bilayer tunnel barrier approach as a promising candidate to be used in high performance vertical graphene-based tunneling devices.

  19. Strength and corrosion behavior of SiC - based ceramics in hot coal combustion environments

    SciTech Connect

    Breder, K.; Parten, R.J.

    1996-08-01

    As part of an effort to evaluate the use of advanced ceramics in a new generation of coal-fired power plants, four SiC-based ceramics have been exposed to corrosive coal slag in a laboratory furnace and two pilot scale combustors. Initial results indicate that the laboratory experiments are valuable additions to more expensive pilot plant experiments. The results show increased corrosive attack with increased temperature, and that only slight changes in temperature may significantly alter the degree of strength degradation due to corrosive attack. The present results are part of a larger experimental matrix evaluating the behavior of ceramics in the coal combustion environment.

  20. Kinetics of Mn-based sorbents for hot coal gas desulfurization. Quarterly report, December 15, 1993--March 15, 1997

    SciTech Connect

    Hepworth, M.T.

    1997-03-03

    Manganese-based sorbents have been investigated for the removal of hydrogen sulfide (the primary sulfur bearing compound) from hot coal gases prior to its use in combined cycle turbines. Four formulations of Mn-based sorbents were tested in an ambient-pressure fixed-bed reactor to determine steady state H{sub 2}S concentrations, breakthrough times and effectiveness of the sorbent when subjected to cyclic sulfidation and regeneration testing. In previous reports, the sulfidation and regeneration results from cyclic testing done at 600{degrees}C were presented. Manganese-based sorbents, with molar ratios > 1:1 Mn:Substrate were effective in reducing the H{sub 2}S concentration in simulated coal gases to less than 100 ppmv over five cycles. Actual breakthrough time for formulation C6-2-1100 was as high as 73% of breakthrough time based on wt% Mn in sorbent. Regeneration tests determined that loaded pellets can be fully regenerated in air/steam mixture at 750{degrees}C with minimal sulfate formation. In this report, the results from cyclic crush strength tests, Sulfur profile tests and cyclic testing at 550{degrees}C and lower flowrate cyclic testing are presented. Crush strength testing done after 5 cycles showed decreases in strength from 12.6% to 57.9%. Cyclic testing at 550{degrees}C showed pre breakthrough concentrations as low as 10 ppmv. Cyclic testing done at 2 L/min and 3 L/min did not show any significant difference in pre breakthrough concentrations or capacity.

  1. Droplet-based magnetic bead immunoassay using microchannel-connected multiwell plates (μCHAMPs) for the detection of amyloid beta oligomers.

    PubMed

    Park, Min Cheol; Kim, Moojong; Lim, Gun Taek; Kang, Sung Min; An, Seong Soo A; Kim, Tae Song; Kang, Ji Yoon

    2016-06-21

    Multiwell plates are regularly used in analytical research and clinical diagnosis but often require laborious washing steps and large sample or reagent volumes (typically, 100 μL per well). To overcome such drawbacks in the conventional multiwell plate, we present a novel microchannel-connected multiwell plate (μCHAMP) that can be used for automated disease biomarker detection in a small sample volume by performing droplet-based magnetic bead immunoassay inside the plate. In this μCHAMP-based immunoassay platform, small volumes (30-50 μL) of aqueous-phase working droplets are stably confined within each well by the simple microchannel structure (200-300 μm in height and 0.5-1 mm in width), and magnetic beads are exclusively transported into an adjacent droplet through the oil-filled microchannels assisted by a magnet array aligned beneath and controlled by a XY-motorized stage. Using this μCHAMP-based platform, we were able to perform parallel detection of synthetic amyloid beta (Aβ) oligomers as a model analyte for the early diagnosis of Alzheimer's disease (AD). This platform easily simplified the laborious and consumptive immunoassay procedure by achieving automated parallel immunoassay (32 assays per operation in 3-well connected 96-well plate) within 1 hour and at low sample consumption (less than 10 μL per assay) with no cumbersome manual washing step. Moreover, it could detect synthetic Aβ oligomers even below 10 pg mL(-1) concentration with a calculated detection limit of ∼3 pg mL(-1). Therefore, the μCHAMP and droplet-based magnetic bead immunoassay, with the combination of XY-motorized magnet array, would be a useful platform in the diagnosis of human disease, including AD, which requires low consumption of the patient's body fluid sample and automation of the entire immunoassay procedure for high processing capacity. PMID:27185215

  2. The Plate Tectonics Project

    ERIC Educational Resources Information Center

    Hein, Annamae J.

    2011-01-01

    The Plate Tectonics Project is a multiday, inquiry-based unit that facilitates students as self-motivated learners. Reliable Web sites are offered to assist with lessons, and a summative rubric is used to facilitate the holistic nature of the project. After each topic (parts of the Earth, continental drift, etc.) is covered, the students will…

  3. Cadmium plating replacements

    SciTech Connect

    Nelson, M.J.; Groshart, E.C.

    1995-03-01

    The Boeing Company has been searching for replacements to cadmium plate. Two alloy plating systems seem close to meeting the needs of a cadmium replacement. The two alloys, zinc-nickel and tin-zinc are from alloy plating baths; both baths are neutral pH. The alloys meet the requirements for salt fog corrosion resistance, and both alloys excel as a paint base. Currently, tests are being performed on standard fasteners to compare zinc-nickel and tin-zinc on threaded hardware where cadmium is heavily used. The Hydrogen embrittlement propensity of the zinc-nickel bath has been tested, and just beginning for the tin-zinc bath. Another area of interest is the electrical properties on aluminum for tin-zinc and will be discussed. The zinc-nickel alloy plating bath is in production in Boeing Commercial Airplane Group for non-critical low strength steels. The outlook is promising that these two coatings will help The Boeing Company significantly reduce its dependence on cadmium plating.

  4. Cadmium plating replacements

    NASA Technical Reports Server (NTRS)

    Nelson, Mary J.; Groshart, Earl C.

    1995-01-01

    The Boeing Company has been searching for replacements to cadmium plate. Two alloy plating systems seem close to meeting the needs of a cadmium replacement. The two alloys, zinc-nickel and tin-zinc are from alloy plating baths; both baths are neutral pH. The alloys meet the requirements for salt fog corrosion resistance, and both alloys excel as a paint base. Currently, tests are being performed on standard fasteners to compare zinc-nickel and tin-zinc on threaded hardware where cadmium is heavily used. The Hydrogen embrittlement propensity of the zinc-nickel bath has been tested, and just beginning for the tin-zinc bath. Another area of interest is the electrical properties on aluminum for tin-zinc and will be discussed. The zinc-nickel alloy plating bath is in production in Boeing Commercial Airplane Group for non-critical low strength steels. The outlook is promising that these two coatings will help The Boeing Company significantly reduce its dependence on cadmium plating.

  5. 9. Bronze slide expansion plate at Pier 3, on right, ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    9. Bronze slide expansion plate at Pier 3, on right, fixed end left. - Monongahela Connecting Railroad Company, Hot Metal Bridge, Spanning Monongahela River at mile post 3.1, Pittsburgh, Allegheny County, PA

  6. Near-infrared Thermal Emission Detections of a Number of Hot Jupiters and the Systematics of Ground-based Near-infrared Photometry

    NASA Astrophysics Data System (ADS)

    Croll, Bryce; Albert, Loic; Jayawardhana, Ray; Cushing, Michael; Moutou, Claire; Lafreniere, David; Johnson, John Asher; Bonomo, Aldo S.; Deleuil, Magali; Fortney, Jonathan

    2015-03-01

    We present detections of the near-infrared thermal emission of three hot Jupiters and one brown dwarf using the Wide-field Infrared Camera (WIRCam) on the Canada-France-Hawaii Telescope (CFHT). These include Ks-band secondary eclipse detections of the hot Jupiters WASP-3b and Qatar-1b and the brown dwarf KELT-1b. We also report Y-band, K CONT-band, and two new and one reanalyzed Ks-band detections of the thermal emission of the hot Jupiter WASP-12b. We present a new reduction pipeline for CFHT/WIRCam data, which is optimized for high precision photometry. We also describe novel techniques for constraining systematic errors in ground-based near-infrared photometry, so as to return reliable secondary eclipse depths and uncertainties. We discuss the noise properties of our ground-based photometry for wavelengths spanning the near-infrared (the YJHK bands), for faint and bright stars, and for the same object on several occasions. For the hot Jupiters WASP-3b and WASP-12b we demonstrate the repeatability of our eclipse depth measurements in the Ks band; we therefore place stringent limits on the systematics of ground-based, near-infrared photometry, and also rule out violent weather changes in the deep, high pressure atmospheres of these two hot Jupiters at the epochs of our observations. Based on observations obtained with WIRCam, a joint project of Canada-France-Hawaii Telescope (CFHT), Taiwan, Korea, Canada, France, at the CFHT, which is operated by the National Research Council (NRC) of Canada, the Institute National des Sciences de l'Univers of the Centre National de la Recherche Scientifique of France, and the University of Hawaii.

  7. Geolocating thermal binoculars based on a software defined camera core incorporating HOT MCT grown by MOVPE

    NASA Astrophysics Data System (ADS)

    Pillans, Luke; Harmer, Jack; Edwards, Tim; Richardson, Lee

    2016-05-01

    Geolocation is the process of calculating a target position based on bearing and range relative to the known location of the observer. A high performance thermal imager with integrated geolocation functions is a powerful long range targeting device. Firefly is a software defined camera core incorporating a system-on-a-chip processor running the AndroidTM operating system. The processor has a range of industry standard serial interfaces which were used to interface to peripheral devices including a laser rangefinder and a digital magnetic compass. The core has built in Global Positioning System (GPS) which provides the third variable required for geolocation. The graphical capability of Firefly allowed flexibility in the design of the man-machine interface (MMI), so the finished system can give access to extensive functionality without appearing cumbersome or over-complicated to the user. This paper covers both the hardware and software design of the system, including how the camera core influenced the selection of peripheral hardware, and the MMI design process which incorporated user feedback at various stages.

  8. Multichannel reconfigurable measurement system for hot plasma diagnostics based on GEM-2D detector

    NASA Astrophysics Data System (ADS)

    Wojenski, A. J.; Kasprowicz, G.; Pozniak, K. T.; Byszuk, A.; Chernyshova, M.; Czarski, T.; Jablonski, S.; Juszczyk, B.; Zienkiewicz, P.

    2015-12-01

    In the future magnetically confined fusion research reactors (e.g. ITER tokamak), precise determination of the level of the soft X-ray radiation of plasma with temperature above 30 keV (around 350 mln K) will be very important in plasma parameters optimization. This paper presents the first version of a designed spectrography measurement system. The system is already installed at JET tokamak. Based on the experience gained from the project, the new generation of hardware for spectrography measurements, was designed and also described in the paper. The GEM detector readout structure was changed to 2D in order to perform measurements of i.e. laser generated plasma. The hardware structure of the system was redesigned in order to provide large number of high speed input channels. Finally, this paper also covers the issue of new control software, necessary to set-up a complete system of certain complexity and perform data acquisition. The main goal of the project was to develop a new version of the system, which includes upgraded structure and data transmission infrastructure (i.e. handling large number of measurement channels, high sampling rate).

  9. Structure and plasticity in hot deformed FeAl intermetallic phase base alloy

    SciTech Connect

    Kuc, Dariusz; Niewielski, Grzegorz; Bednarczyk, Iwona

    2009-10-15

    This paper constitutes part of research conducted on the possibility of forming alloys based on intermetallic phases from the Fe-Al system via thermoplastic processing. Insufficient plasticity, which is an inhibitor of further development of these intermetallics as construction materials, makes the range of their applications limited. In the paper, an analysis is conducted of the influence of deformation parameters on the structure of an alloy of Fe-Al with the B2 type structure. Axi-symmetric compression tests were carried out at temperatures ranging from 600 deg. C to 1200 deg. C and at a deformation rate from 0.001 s{sup 1} to 10 s{sup -1}. Structural examination was carried out using light microscopy and transmission electron microscopy. A quantitative evaluation of the structure was made with the use of 'Met-Ilo'. The results obtained will be used for the development of mathematical models determining the influence of deformation parameters on the alloy structure.

  10. Effects of the foil flatness on the stress-strain characteristics of U10Mo alloy based monolithic mini-plates

    SciTech Connect

    Hakan Ozaltun; Pavel Medvedev

    2014-11-01

    The effects of the foil flatness on stress-strain behavior of monolithic fuel mini-plates during fabrication and irradiation were studied. Monolithic plate-type fuels are a new fuel form being developed for research and test reactors to achieve higher uranium densities. This concept facilitates the use of low-enriched uranium fuel in the reactor. These fuel elements are comprised of a high density, low enrichment, U–Mo alloy based fuel foil encapsulated in a cladding material made of Aluminum. To evaluate the effects of the foil flatness on the stress-strain behavior of the plates during fabrication, irradiation and shutdown stages, a representative plate from RERTR-12 experiments (Plate L1P756) was considered. Both fabrication and irradiation processes of the plate were simulated by using actual irradiation parameters. The simulations were repeated for various foil curvatures to observe the effects of the foil flatness on the peak stress and strain magnitudes of the fuel elements. Results of fabrication simulations revealed that the flatness of the foil does not have a considerable impact on the post fabrication stress-strain fields. Furthermore, the irradiation simulations indicated that any post-fabrication stresses in the foil would be relieved relatively fast in the reactor. While, the perfectly flat foil provided the slightly better mechanical performance, overall difference between the flat-foil case and curved-foil case was not significant. Even though the peak stresses are less affected, the foil curvature has several implications on the strain magnitudes in the cladding. It was observed that with an increasing foil curvature, there is a slight increase in the cladding strains.

  11. Design of all-optical, hot-electron current-direction-switching device based on geometrical asymmetry.

    PubMed

    Kumarasinghe, Chathurangi S; Premaratne, Malin; Gunapala, Sarath D; Agrawal, Govind P

    2016-01-01

    We propose a nano-scale current-direction-switching device(CDSD) that operates based on the novel phenomenon of geometrical asymmetry between two hot-electron generating plasmonic nanostructures. The proposed device is easy to fabricate and economical to develop compared to most other existing designs. It also has the ability to function without external wiring in nano or molecular circuitry since it is powered and controlled optically. We consider a such CDSD made of two dissimilar nanorods separated by a thin but finite potential barrier and theoretically derive the frequency-dependent electron/current flow rate. Our analysis takes in to account the quantum dynamics of electrons inside the nanorods under a periodic optical perturbation that are confined by nanorod boundaries, modelled as finite cylindrical potential wells. The influence of design parameters, such as geometric difference between the two nanorods, their volumes and the barrier width on quality parameters such as frequency-sensitivity of the current flow direction, magnitude of the current flow, positive to negative current ratio, and the energy conversion efficiency is discussed by considering a device made of Ag/TiO2/Ag. Theoretical insight and design guidelines presented here are useful for customizing our proposed CDSD for applications such as self-powered logic gates, power supplies, and sensors. PMID:26887286

  12. Design of all-optical, hot-electron current-direction-switching device based on geometrical asymmetry

    PubMed Central

    Kumarasinghe, Chathurangi S.; Premaratne, Malin; Gunapala, Sarath D.; Agrawal, Govind P.

    2016-01-01

    We propose a nano-scale current-direction-switching device(CDSD) that operates based on the novel phenomenon of geometrical asymmetry between two hot-electron generating plasmonic nanostructures. The proposed device is easy to fabricate and economical to develop compared to most other existing designs. It also has the ability to function without external wiring in nano or molecular circuitry since it is powered and controlled optically. We consider a such CDSD made of two dissimilar nanorods separated by a thin but finite potential barrier and theoretically derive the frequency-dependent electron/current flow rate. Our analysis takes in to account the quantum dynamics of electrons inside the nanorods under a periodic optical perturbation that are confined by nanorod boundaries, modelled as finite cylindrical potential wells. The influence of design parameters, such as geometric difference between the two nanorods, their volumes and the barrier width on quality parameters such as frequency-sensitivity of the current flow direction, magnitude of the current flow, positive to negative current ratio, and the energy conversion efficiency is discussed by considering a device made of Ag/TiO2/Ag. Theoretical insight and design guidelines presented here are useful for customizing our proposed CDSD for applications such as self-powered logic gates, power supplies, and sensors. PMID:26887286

  13. Aircraft-based in-situ calibration of a hot-wire anemometer in a compressible flow

    NASA Astrophysics Data System (ADS)

    Hugo, Ronald J.; Nowlin, Scott R.; Hahn, Ila L.; Bishop, Kenneth P.; McCrae, Kimberley A.

    1999-08-01

    High-bandwidth measurements of atmospheric velocity and temperature fluctuations in the high troposphere/low stratosphere using aircraft-based hot-wire anemometers requires calibration. An in-situ calibration characterizing wire sensitivity at high subsonic Mach numbers and relatively low temperatures and pressures was performed. Custom designed constant-temperature and constant-current anemometer equipment has been used for these atmospheric measurements. Two sets of calibration experiments are described, one in a controlled laboratory environment where the Mach number and temperature were varied and the other on board a C-135E aircraft. The aircraft test were conducted by varying the flight Mach number at different pressure altitudes while flying into an upper-level low pressure area, achieving variability in velocity, temperature, and pressure. Results obtained indicate increased sensitivity to velocity while operating the wire at a low overheat ratio. The calibration data was fit to a form of King's law which was found to work well for in-situ calibrations.

  14. Genetic based sensorless hybrid intelligent controller for strip loop formation control between inter-stands in hot steel rolling mills.

    PubMed

    Thangavel, S; Palanisamy, V; Duraiswamy, K

    2008-04-01

    Safe operating environment is essential for all complex industrial processes. The safety issues in steel rolling mill when the hot strip passes through consecutive mill stands have been considered in this paper. Formation of sag in strip is a common problem in the rolling process. The excessive sag can lead to scrap runs and damage to machinery. Conventional controllers for mill actuation system are based on a rolling model. The factors like rise in temperature, aging, wear and tear are not taken into account while designing a conventional controller. Therefore, the conventional controller cannot yield a requisite controlled output. In this paper, a new Genetic-neuro-fuzzy hybrid controller without tension sensor has been proposed to optimize the quantum of excessive sag and reduce it. The performance of the proposed controller has been compared with the performance of fuzzy logic controller, Neuro-fuzzy controller and conventional controller with the help of data collected from the plant. The simulation results depict that the proposed controller has superior performance than the other controllers. PMID:18093589

  15. Design of all-optical, hot-electron current-direction-switching device based on geometrical asymmetry

    NASA Astrophysics Data System (ADS)

    Kumarasinghe, Chathurangi S.; Premaratne, Malin; Gunapala, Sarath D.; Agrawal, Govind P.

    2016-02-01

    We propose a nano-scale current-direction-switching device(CDSD) that operates based on the novel phenomenon of geometrical asymmetry between two hot-electron generating plasmonic nanostructures. The proposed device is easy to fabricate and economical to develop compared to most other existing designs. It also has the ability to function without external wiring in nano or molecular circuitry since it is powered and controlled optically. We consider a such CDSD made of two dissimilar nanorods separated by a thin but finite potential barrier and theoretically derive the frequency-dependent electron/current flow rate. Our analysis takes in to account the quantum dynamics of electrons inside the nanorods under a periodic optical perturbation that are confined by nanorod boundaries, modelled as finite cylindrical potential wells. The influence of design parameters, such as geometric difference between the two nanorods, their volumes and the barrier width on quality parameters such as frequency-sensitivity of the current flow direction, magnitude of the current flow, positive to negative current ratio, and the energy conversion efficiency is discussed by considering a device made of Ag/TiO2/Ag. Theoretical insight and design guidelines presented here are useful for customizing our proposed CDSD for applications such as self-powered logic gates, power supplies, and sensors.

  16. Effect of B, Zr, and C on Hot Tearing of a Directionally Solidified Nickel-Based Superalloy

    NASA Astrophysics Data System (ADS)

    Grodzki, J.; Hartmann, N.; Rettig, R.; Affeldt, E.; Singer, R. F.

    2016-06-01

    The effect of the minor elements B, Zr, and C on the castability of a Nickel-based γ'-strengthened superalloy has been investigated. Tube-like specimens were prepared by directional solidification where the rigid ceramic core leads to hoop stresses and grain boundary cracking. It was found that an important improvement in castability can be achieved by adjusting the minor elemental composition. Too low C (≤0.15 pct) and too high B and Zr contents (≥0.05 pct) lead to material that is very prone to solidification cracking and should be avoided. The results cannot be rationalized on the basis of the current models for solidification cracking. Instead, pronounced hot tearing is observed to occur at high amounts of γ/ γ'-eutectic and high Zr contents. The critical film stage where dendrites at the end of solidification do not touch and are separated by thin liquid films must be avoided. How Zr promotes the film stage will be discussed in the paper.

  17. Evaluation of a photon-counting x-ray imaging detector based on microchannel plates for mammography applications

    NASA Astrophysics Data System (ADS)

    Shikhaliev, Polad M.; Xu, Tong; Molloi, Sabee

    2004-05-01

    Experimental prototype of a photon counting scanning slit X-ray imaging system is being evaluated for potential application in digital mammography. This system is based on a recently developed and tested "edge-on" illuminated Microchannel Plate (MCP) detector. The MCP detectors are well known for providing a combination of capabilities such as direct conversion, physical charge amplification, pulse counting, high spatial and temporal resolution, and very low noise. However, their application for medical imaging was hampered by their low detection efficiency. This limitation was addressed using an "edge-on" illumination mode for MCP. The current experimental prototype was developed to investigate the imaging performance of this detector concept for digital mammography. The current prototype provides a 60 mm field of view, 200 kHz count rate with 20% non-paralysable dead time and >7 lp/mm limiting resolution. A 0.3 mm focal spot W target X-ray tube was used for image acquisition. The detector noise is 0.3 count/pixel for 50x50 micron pixels. The count rate of the current prototype is limited by the delay line readout electronics, which causes long scanning times (minutes) and high tube loading. This problem will be addressed using multichannel ASIC electronics for clinical implementation. However, the current readout architecture is adequate for evaluation of the performance parameters of the new detector concept. It is very simple and provides a maximum intrinsic resolution of 28 micron FWHM. The prototype was evaluated using resolution, contrast detail and breast Phantoms. The MTF and DQE of the system are being evaluated at different tube voltages. The design parameters of a scanning multiple slit mammography system are being evaluated. It is concluded that a photon counting, quantum limited and virtually scatter free digital mammography system can be developed based on the proposed detector.

  18. Heat transfer characteristics of the metal hydride vessel based on the plate-fin type heat exchanger

    NASA Astrophysics Data System (ADS)

    Oi, Tsutomu; Maki, Kohei; Sakaki, Yoshinori

    Heat transfer characteristics of the metal hydride vessel based on the plate-fin type heat exchanger were investigated. Metal hydride beds were filled with AB 2 type hydrogen-storage alloy's particles, Ti 0.42Zr 0.58Cr 0.78Fe 0.57Ni 0.2Mn 0.39Cu 0.03, with a storage capacity of 0.92 wt.%. Heat transfer model in the metal hydride bed based on the heat transfer mechanism for packed bed proposed by Kunii and co-workers is presented. The time-dependent hydrogen absorption/desorption rate and pressure in the metal hydride vessel calculated by the model were compared with the experimental results. During the hydriding, calculated hydrogen absorption rates agreed with measured ones. Calculated thermal equilibrium hydrogen pressures were slightly lower than the measured hydrogen pressures at the inlet of metal hydride vessel. Taking account of the pressure gradient between the inlet of metal hydride vessel and the metal hydride bed, it is considered that this discrepancy is reasonable. During the dehydriding, there were big differences between the calculated hydrogen desorption rates and measured ones. As calculated hydrogen desorption rates were lower than measured ones, there were big differences between the calculated thermal equilibrium hydrogen pressures and the measured hydrogen pressures at the inlet of metal hydride vessel. It is considered that those differences are due to the differences of the heat transfer characteristics such as thermal conductivity of metal hydride particles and porosity between the assumed and actual ones. It is important to obtain the heat transfer characteristics such as thermal conductivity of metal hydride particles and porosity both during the hydriding and dehydriding to design a metal hydride vessel.

  19. Development of an Abuse- and Alcohol-Resistant Formulation Based on Hot-Melt Extrusion and Film Coating.

    PubMed

    Jedinger, Nicole; Schrank, Simone; Fischer, Johannes M; Breinhälter, Karlheinz; Khinast, Johannes; Roblegg, Eva

    2016-02-01

    This study focused on the development of flexible (i.e., deformable) multiple-unit pellets that feature (i) a prolonged drug release, (ii) drug abuse deterrence, and (iii) a minimal risk of alcohol-induced dose dumping (ADD). Deformable pellets were prepared via an advanced continuous one-step hot-melt extrusion (HME) technique, with the drug (i.e., antipyrine and codeine phosphate) fed as an aqueous solution into the molten matrix material (i.e., cornstarch, gum arabic, and xanthan). Formulations that had suitable mechanical characteristics (i.e., high compression strength) were coated with a flexible Aquacoat(®) ARC film to ensure prolonged release and to avoid ADD. The pellets were characterized in terms of their mechanical properties and in vitro drug release behavior in alcoholic media. All formulations were abuse deterrent: they had a high compression strength and grinding the pellets into powder was impossible. Since the pellets comprising gum arabic and xanthan as a matrix did not remain intact during dissolution testing, they had a very fast drug release rate. Cornstarch-based pellets that swelled but remained intact in the dissolution media had a slower drug release. Coated cornstarch-based pellets had a prolonged release over 8 h and resistance to dose dumping in 20 and 40% ethanol. Our results indicate that cornstarch-based pellets manufactured via the advanced HME process followed by coating are a promising formulation that makes tampering difficult due to a high compression strength combined with robustness in alcoholic media. PMID:26206403

  20. Multi-objective shape optimization of plate structure under stress criteria based on sub-structured mixed FEM and genetic algorithms

    NASA Astrophysics Data System (ADS)

    Garambois, Pierre; Besset, Sebastien; Jézéquel, Louis

    2015-07-01

    This paper presents a methodology for the multi-objective (MO) shape optimization of plate structure under stress criteria, based on a mixed Finite Element Model (FEM) enhanced with a sub-structuring method. The optimization is performed with a classical Genetic Algorithm (GA) method based on Pareto-optimal solutions and considers thickness distributions parameters and antagonist objectives among them stress criteria. We implement a displacement-stress Dynamic Mixed FEM (DM-FEM) for plate structure vibrations analysis. Such a model gives a privileged access to the stress within the plate structure compared to primal classical FEM, and features a linear dependence to the thickness parameters. A sub-structuring reduction method is also computed in order to reduce the size of the mixed FEM and split the given structure into smaller ones with their own thickness parameters. Those methods combined enable a fast and stress-wise efficient structure analysis, and improve the performance of the repetitive GA. A few cases of minimizing the mass and the maximum Von Mises stress within a plate structure under a dynamic load put forward the relevance of our method with promising results. It is able to satisfy multiple damage criteria with different thickness distributions, and use a smaller FEM.

  1. SOURCE ASSESSMENT: ASPHALT HOT MIX

    EPA Science Inventory

    This report summarizes data on air emissions from the asphalt hot mix industry. A representative asphalt hot mix plant was defined, based on the results of an industrial survey, to assess the severity of emissions from this industry. Source severity was defined as the ratio of th...

  2. 6. INTERIOR VIEW, HIGH CARBON HOT ROLLED SHEET STEEL FOR ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    6. INTERIOR VIEW, HIGH CARBON HOT ROLLED SHEET STEEL FOR NAIL PLATE BEING LOADED ON THE CRADLE USED DURING THE PICKLING PROCESS - LaBelle Iron Works, Thirtieth & Wood Streets, Wheeling, Ohio County, WV

  3. 5. INTERIOR VIEW, HIGH CARBON HOT ROLLED SHEET STEEL FOR ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    5. INTERIOR VIEW, HIGH CARBON HOT ROLLED SHEET STEEL FOR NAIL PLATE BEING REMOVED FROM THE CRADLE USED DURING THE PICKLING PROCESS - LaBelle Iron Works, Thirtieth & Wood Streets, Wheeling, Ohio County, WV

  4. Chloride-based fast homoepitaxial growth of 4H-SiC films in a vertical hot-wall CVD

    NASA Astrophysics Data System (ADS)

    Guoguo, Yan; Feng, Zhang; Yingxi, Niu; Fei, Yang; Xingfang, Liu; Lei, Wang; Wanshun, Zhao; Guosheng, Sun; Yiping, Zeng

    2016-06-01

    Chloride-based fast homoepitaxial growth of 4H-SiC epilayers was performed on 4° off-axis 4H-SiC substrates in a home-made vertical hot-wall chemical vapor deposition (CVD) system using H2‑SiH4‑C2H4‑HCl. The effect of the SiH4/H2 ratio and reactor pressure on the growth rate of 4H-SiC epilayers has been studied successively. The growth rate increase in proportion to the SiH4/H2 ratio and the influence mechanism of chlorine has been investigated. With the reactor pressure increasing from 40 to 100 Torr, the growth rate increased to 52 μm/hand then decreased to 47 μm/h, which is due to the joint effect of H2 and HCl etching as well as the formation of Si clusters at higher reactor pressure. The surface root mean square (RMS) roughness keeps around 1 nm with the growth rate increasing to 49 μm/h. The scanning electron microscope (SEM), Raman spectroscopy and X-ray diffraction (XRD) demonstrate that 96.7 μm thick 4H-SiC layers of good uniformity in thickness and doping with high crystal quality can be achieved. These results prove that chloride-based fast epitaxy is an advanced growth technique for 4H-SiC homoepitaxy. Project supported by the National High Technology R&D Program of China (No. 2014AA041402), the National Natural Science Foundation of China (Nos. 61474113, 61274007, 61574140), the Beijing Natural Science Foundation of China (Nos. 4132076, 4132074), the Program of State Grid Smart Grid Research Institute (No. SGRI-WD-71-14-004), and the Youth Innovation Promotion Association of CAS.

  5. 0.94-2.42 μm ground-based transmission spectra of the hot Jupiter HD-189733b

    SciTech Connect

    Danielski, C.; Waldmann, I. P.; Hollis, M. D. J.; Tinetti, G.; Deroo, P.; Swain, M. R.

    2014-04-10

    We present here new transmission spectra of the hot Jupiter HD-189733b using the SpeX instrument on the NASA Infrared Telescope Facility. We obtained two nights of observations where we recorded the primary transit of the planet in the J, H, and K bands simultaneously, covering a spectral range from 0.94 to 2.42 μm. We used Fourier analysis and other detrending techniques validated previously on other data sets to clean the data. We tested the statistical significance of our results by calculating the autocorrelation function, and we found that, after the detrending, autocorrelative noise is diminished at most frequencies. Additionally, we repeated our analysis on the out-of-transit data only, showing that the residual telluric contamination is well within the error bars. While these techniques are very efficient when multiple nights of observations are combined together, our results prove that even one good night of observations is enough to provide statistically meaningful data. Our observed spectra are consistent with space-based data recorded in the same wavelength interval by multiple instruments, indicating that ground-based facilities are becoming a viable and complementary option to spaceborne observatories. The best fit to the features in our data was obtained with water vapor. Our error bars are not small enough to address the presence of additional molecules; however, by combining the information contained in other data sets with our results, it is possible to explain all the available observations with a modeled atmospheric spectrum containing water vapor, methane, carbon monoxide, and hazes/clouds.

  6. Kinetics of Mn-based sorbents for hot coal gas desulfurization. Quarterly progress report, March 15, 1995--July 15, 1995

    SciTech Connect

    Hepworth, M.T.

    1995-07-15

    Hot gas desulfurization may be accomplished by using solid sorbents such as oxides of those metals that form stable sulfides. The effectiveness of a desulfurizing agent in treating such gases is related to the predicted equilibrium partial pressure of hydrogen sulfide which will be present in a phase combination of the reduced form of sulfide and oxide phases. The focus of much current work being performed by the Department of Energy on sorbent development is in the use of zinc ferrite, zinc titanate, and Z-Sorb. The latter sorbent is a commercial product consisting of ZnO, a promoter, and a proprietary supporting matrix designed to provide stability and prolong sorbent life. Although these Zn-based sorbents have been the subject of extensive pilot-scale and process development work, all sorbents produced to date still experience structural and reactive degradation over multi-cycle use at relatively moderate temperatures. An effective alternative to zinc-based sorbents could be manganese sorbents which withstand high temperature operation and also maintain structural and reactive integrity over many cycles, as investigations by Ben-Slimane and Hepworth have indicated. Thermodynamic limits may prevent MnO from achieving the low sulfur specifications of the product gas for use in a molten carbonate fuel cell, but under the correct conditions the guideline for IGCC systems can easily be achieved. Furthermore, manganese sorbents could possibly be used in conjunction with a polishing sorbent (such as zinc oxide) possessing more favorable thermodynamic properties to reach levels acceptable for fuel cell applications (< 10 ppmv). Such an arrangement may not require that the zinc sulfide be regenerated since the sulfur concentration of the cleaned gas is low enough that the zinc oxide may be discarded when exhausted.

  7. Evaluation of the light scattering and the turbidity microtiter plate-based methods for the detection of the excipient-mediated drug precipitation inhibition.

    PubMed

    Petruševska, Marija; Urleb, Uroš; Peternel, Luka

    2013-11-01

    The excipient-mediated precipitation inhibition is classically determined by the quantification of the dissolved compound in the solution. In this study, two alternative approaches were evaluated, one is the light scattering (nephelometer) and other is the turbidity (plate reader) microtiter plate-based methods which are based on the quantification of the compound precipitate. Following the optimization of the nephelometer settings (beam focus, laser gain) and the experimental conditions, the screening of 23 excipients on the precipitation inhibition of poorly soluble fenofibrate and dipyridamole was performed. The light scattering method resulted in excellent correlation (r>0.91) between the calculated precipitation inhibitor parameters (PIPs) and the precipitation inhibition index (PI(classical)) obtained by the classical approach for fenofibrate and dipyridamole. Among the evaluated PIPs AUC100 (nephelometer) resulted in only four false positives and lack of false negatives. In the case of the turbidity-based method a good correlation of the PI(classical) was obtained for the PIP maximal optical density (OD(max), r=0.91), however, only for fenofibrate. In the case of the OD(max) (plate reader) five false positives and two false negatives were identified. In conclusion, the light scattering-based method outperformed the turbidity-based one and could be reliably used for identification of novel precipitation inhibitors. PMID:24056092

  8. Hot Cell Window Shielding Analysis Using MCNP

    SciTech Connect

    Chad L. Pope; Wade W. Scates; J. Todd Taylor

    2009-05-01

    The Idaho National Laboratory Materials and Fuels Complex nuclear facilities are undergoing a documented safety analysis upgrade. In conjunction with the upgrade effort, shielding analysis of the Fuel Conditioning Facility (FCF) hot cell windows has been conducted. This paper describes the shielding analysis methodology. Each 4-ft thick window uses nine glass slabs, an oil film between the slabs, numerous steel plates, and packed lead wool. Operations in the hot cell center on used nuclear fuel (UNF) processing. Prior to the shielding analysis, shield testing with a gamma ray source was conducted, and the windows were found to be very effective gamma shields. Despite these results, because the glass contained significant amounts of lead and little neutron absorbing material, some doubt lingered regarding the effectiveness of the windows in neutron shielding situations, such as during an accidental criticality. MCNP was selected as an analysis tool because it could model complicated geometry, and it could track gamma and neutron radiation. A bounding criticality source was developed based on the composition of the UNF. Additionally, a bounding gamma source was developed based on the fission product content of the UNF. Modeling the windows required field inspections and detailed examination of drawings and material specifications. Consistent with the shield testing results, MCNP results demonstrated that the shielding was very effective with respect to gamma radiation, and in addition, the analysis demonstrated that the shielding was also very effective during an accidental criticality.

  9. Analysis of saturated and aromatic hydrocarbons migrating from a polyolefin-based hot-melt adhesive into food.

    PubMed

    Lommatzsch, Martin; Biedermann, Maurus; Grob, Koni; Simat, Thomas J

    2016-03-01

    Hot-melt adhesives are widely utilised to glue cardboard boxes used as food packaging material. They have to comply with the requirements of Article 3 of the European Framework Regulation for food contact materials (1935/2004). The hot melt raw materials analysed mainly consisted of paraffinic waxes, hydrocarbon resins and polyolefins. The hydrocarbon resins, functioning as tackifiers, were the predominant source of hydrocarbons of sufficient volatility to migrate into dry foods: the 18 hydrocarbon resins analysed contained 8.2-118 g kg(-1) saturated and up to 59 g kg(-1) aromatic hydrocarbons eluted from GC between n-C16 and n-C24, substantially more than the paraffinic waxes and the polyolefins. These tackfier resins, especially the oligomers ≤ C24, have been characterised structurally by GC×GC-MS and (1)H-NMR spectroscopy. Migration into food was estimated using a simulating system with polenta as food simulant, which was verified by the analysis of a commercial risotto rice sample packed in a virgin fibre folding box sealed with a hot melt. About 0.5-1.5% of the potentially migrating substances (between n-C16 and n-C24) of a hot melt were found to be transferred into food under storage conditions, which can result in a food contamination in the order of 1 mg kg(-1) food (depending on the amount of potentially migrating substances from the hot melt, the hot melt surface, amount of food, contact time etc.). Migrates from hot melts are easily mistaken for mineral oil hydrocarbons from recycled cardboard. PMID:26744923

  10. A simple calibration approach based on film-casting for confocal Raman microscopy to support the development of a hot-melt extrusion process.

    PubMed

    Netchacovitch, L; Thiry, J; De Bleye, C; Dumont, E; Dispas, A; Hubert, C; Krier, F; Sacré, P-Y; Evrard, B; Hubert, Ph; Ziemons, E

    2016-07-01

    When developing a new formulation, the development, calibration and validation steps of analytical methods based on vibrational spectroscopy are time-consuming. For each new formulation, real samples must be produced and a "reference method" must be used in order to determine the Active Pharmaceutical Ingredient (API) content of each sample. To circumvent this issue, the paper presents a simple approach based on the film-casting technique used as a calibration tool in the framework of hot-melt extrusion process. Confocal Raman microscopic method was successfully validated for the determination of itraconazole content in film-casting samples. Then, hot-melt extrusion was carried out to produce real samples in order to confront the results obtained with confocal Raman microscopy and Ultra High Performance Liquid Chromatography (UHPLC). The agreement between both methods was demonstrated using a comparison study based on the Bland and Altman's plot. PMID:27154691

  11. Volcanism in response to plate flexure.

    PubMed

    Hirano, Naoto; Takahashi, Eiichi; Yamamoto, Junji; Abe, Natsue; Ingle, Stephanie P; Kaneoka, Ichiro; Hirata, Takafumi; Kimura, Jun-Ichi; Ishii, Teruaki; Ogawa, Yujiro; Machida, Shiki; Suyehiro, Kiyoshi

    2006-09-01

    Volcanism on Earth is known to occur in three tectonic settings: divergent plate boundaries (such as mid-ocean ridges), convergent plate boundaries (such as island arcs), and hot spots. We report volcanism on the 135 million-year-old Pacific Plate not belonging to any of these categories. Small alkalic volcanoes form from small percent melts and originate in the asthenosphere, as implied by their trace element geochemistry and noble gas isotopic compositions. We propose that these small volcanoes erupt along lithospheric fractures in response to plate flexure during subduction. Minor extents of asthenospheric melting and the volcanoes' tectonic alignment and age progression in the direction opposite to that of plate motion provide evidence for the presence of a small percent melt in the asthenosphere. PMID:16873612

  12. Characterizing intra and inter annual variability of storm events based on very high frequency monitoring of hydrological and chemical variables: what can we learn about hot spots and hot moments from continuous hydro-chemical sensors ?

    NASA Astrophysics Data System (ADS)

    Fovet, O.; Thelusma, G.; Humbert, G.; Dupas, R.; Jaffrezic, A.; Grimaldi, C.; Faucheux, M.; Gilliet, N.; Hamon, Y.; Gruau, G.

    2015-12-01

    Storm events are hot moments of emission for several dissolved and particulate chemical species at major stake for water quality (e.g. dissolved organic carbon DOC, suspended sediments, phosphorus, NH4). During such events, the solutes or particles are exported from heterogeneous sources through various pathways to stream or are possibly stored in retention hot spots temporary. This leads to specific integrated signals at the outlet at the scale of storm events. The dynamics of such events are also very short especially in headwater catchments where their total duration ranges over 10h to 3 days, with very quick variations in stream flow and concentrations at the outlet occurring in a few hours. Thus for investigating properly event processes, high frequency monitoring of flow and water quality is required. We analysed 103 storm events in a 5 km2 agricultural headwater catchment, part of the AgrHys Observatory, on the basis of a 3-year-long data set which combined meterological (Rainfall), hydrological (flow and piezometry), and water quality (turbidity, conductivity, DOC and NO3 concentrations) data recorded at very high frequencies (from 1 to 20 min) thanks to dedicated sensors. We described the storm events using simple (1 variable) and combined (2 variables) descriptors for characterizing level and dynamics of flow (Q), groundwater levels, and concentrations (C) but also the C-Q relationships. Three intra annual periods have been previously defined for base flow dynamic according to shallow groundwater table variations so that they correspond to different connectivity status in the catchment. The seasonal and inter-annual variability of the storm events have been analysed using the descriptors and based on these predefined periods. Principal component analysis based on storm chemical descriptors led to discriminate these three seasons while storm hydrological descriptors are less variable between them. Finally we used a clustering method to build a typology of

  13. Characteristics of a micro-mechanical thermal flow sensor based on a two hot wires principle with constant temperature operation in a small channel

    NASA Astrophysics Data System (ADS)

    Lange, P.; Weiss, M.; Warnat, S.

    2014-12-01

    A thermal mass flow sensor with high dynamic flow range in silicon bulk micromachining membrane technology is presented. The response behavior of this sensor based on a two hot wire principle is described. This sensor configuration uses two hot wires mounted closely spaced one behind the other within a thin membrane, kept at the same temperature. The power to compensate cooling of and the interaction between the two hot wires are used to calculate mass flows and directionality of flows of gaseous and liquid fluids in a small channel. The response shows both anemometric and calorimetric behavior, depending on fluid, channel height and flow range. The hot wires are heated relative to temperature sensors located also on an isolated membrane on the same chip. Choosing an appropriate evaluation procedure an independence of the signal from the ambient temperature is achieved. This configuration will be discussed in view of the published results of single heater flow sensors, being of calorimetric or anemometric type. A calculation method for the determination of linear and power law range of the response is given.

  14. Distribution of Sequence-Based Types of Legionella pneumophila Serogroup 1 Strains Isolated from Cooling Towers, Hot Springs, and Potable Water Systems in China

    PubMed Central

    Zhou, Haijian; Ren, Hongyu; Guan, Hong; Li, Machao; Zhu, Bingqing

    2014-01-01

    Legionella pneumophila serogroup 1 causes Legionnaires' disease. Water systems contaminated with Legionella are the implicated sources of Legionnaires' disease. This study analyzed L. pneumophila serogroup 1 strains in China using sequence-based typing. Strains were isolated from cooling towers (n = 96), hot springs (n = 42), and potable water systems (n = 26). Isolates from cooling towers, hot springs, and potable water systems were divided into 25 sequence types (STs; index of discrimination [IOD], 0.711), 19 STs (IOD, 0.934), and 3 STs (IOD, 0.151), respectively. The genetic variation among the potable water isolates was lower than that among cooling tower and hot spring isolates. ST1 was the predominant type, accounting for 49.4% of analyzed strains (n = 81), followed by ST154. With the exception of two strains, all potable water isolates (92.3%) belonged to ST1. In contrast, 53.1% (51/96) and only 14.3% (6/42) of cooling tower and hot spring, respectively, isolates belonged to ST1. There were differences in the distributions of clone groups among the water sources. The comparisons among L. pneumophila strains isolated in China, Japan, and South Korea revealed that similar clones (ST1 complex and ST154 complex) exist in these countries. In conclusion, in China, STs had several unique allelic profiles, and ST1 was the most prevalent sequence type of environmental L. pneumophila serogroup 1 isolates, similar to its prevalence in Japan and South Korea. PMID:24463975

  15. Distribution of sequence-based types of legionella pneumophila serogroup 1 strains isolated from cooling towers, hot springs, and potable water systems in China.

    PubMed

    Qin, Tian; Zhou, Haijian; Ren, Hongyu; Guan, Hong; Li, Machao; Zhu, Bingqing; Shao, Zhujun

    2014-04-01

    Legionella pneumophila serogroup 1 causes Legionnaires' disease. Water systems contaminated with Legionella are the implicated sources of Legionnaires' disease. This study analyzed L. pneumophila serogroup 1 strains in China using sequence-based typing. Strains were isolated from cooling towers (n = 96), hot springs (n = 42), and potable water systems (n = 26). Isolates from cooling towers, hot springs, and potable water systems were divided into 25 sequence types (STs; index of discrimination [IOD], 0.711), 19 STs (IOD, 0.934), and 3 STs (IOD, 0.151), respectively. The genetic variation among the potable water isolates was lower than that among cooling tower and hot spring isolates. ST1 was the predominant type, accounting for 49.4% of analyzed strains (n = 81), followed by ST154. With the exception of two strains, all potable water isolates (92.3%) belonged to ST1. In contrast, 53.1% (51/96) and only 14.3% (6/42) of cooling tower and hot spring, respectively, isolates belonged to ST1. There were differences in the distributions of clone groups among the water sources. The comparisons among L. pneumophila strains isolated in China, Japan, and South Korea revealed that similar clones (ST1 complex and ST154 complex) exist in these countries. In conclusion, in China, STs had several unique allelic profiles, and ST1 was the most prevalent sequence type of environmental L. pneumophila serogroup 1 isolates, similar to its prevalence in Japan and South Korea. PMID:24463975

  16. Hot Meetings

    NASA Technical Reports Server (NTRS)

    Chiu, Mary

    2002-01-01

    A colleague walked by my office one time as I was conducting a meeting. There were about five or six members of my team present. The colleague, a man who had been with our institution (The Johns Hopkins Applied Physics Lab, a.k.a. APL) for many years, could not help eavesdropping. He said later it sounded like we we re having a raucous argument, and he wondered whether he should stand by the door in case things got out of hand and someone threw a punch. Our Advanced Composition Explorer (ACE) team was a hot group, to invoke the language that is fashionable today, although we never thought of ourselves in those terms. It was just our modus operandi. The tenor of the discussion got loud and volatile at times, but I prefer to think of it as animated, robust, or just plain collaborative. Mary Chiu and her "hot" team from the Johns Hopkins Applied Physics Laboratory built the Advanced Composition Explorer spacecraft for NASA. Instruments on the spacecraft continue to collect data that inform us about what's happening on our most important star, the Sun.

  17. Using EarthScope Construction of the Plate Boundary Observatory to Provide Locally Based Experiential Education and Outreach

    NASA Astrophysics Data System (ADS)

    Jackson, M.; Eriksson, S.; Barbour, K.; Venator, S.; Mencin, D.; Prescott, W.

    2006-12-01

    EarthScope is an NSF-funded, national science initiative to explore the structure and evolution of the North American continent and to understand the physical processes controlling earthquakes and volcanoes. This large-scale experiment provides locally based opportunities for education and outreach which engage students at various levels and the public. UNAVCO is responsible for the Plate Boundary Observatory (PBO) component of EarthScope. PBO includes the installation and operations and maintenance of large networks of Global Positioning Satellite (GPS), strainmeter, seismometer, and tiltmeter instruments and the acquisition of satellite radar imagery, all of which will be used to measure and map the smallest movements across faults, the magma movement inside active volcanoes and the very wide areas of deformation associated with plate tectonic motion. UNAVCO, through its own education and outreach activities and in collaboration with the EarthScope E&O Program, uses the PBO construction activities to increase the understanding and public appreciation of geodynamics, earth deformation processes, and their relevance to society. These include programs for public outreach via various media, events associated with local installations, a program to employ students in the construction of PBO, and development of curricular materials by use in local schools associated with the EarthScope geographic areas of focus. PBO provides information to the media to serve the needs of various groups and localities, including interpretive centers at national parks and forests, such as Mt. St. Helens. UNAVCO staff contributed to a television special with the Spanish language network Univision Aquí y Ahora program focused on the San Andreas Fault and volcanoes in Alaska. PBO participated in an Education Day at the Pathfinder Ranch Science and Outdoor Education School in Mountain Center, California. Pathfinder Ranch hosts two of the eight EarthScope borehole strainmeters in the Anza

  18. Deformation and recrystallization behavior during hot working of a coarse-grain, nickel-base superalloy ingot material

    NASA Astrophysics Data System (ADS)

    Semiatin, S. L.; Weaver, D. S.; Kramb, R. C.; Fagin, P. N.; Glavicic, M. G.; Goetz, R. L.; Frey, N. D.; Antony, M. M.

    2004-02-01

    The deformation and dynamic recrystallization behavior of Waspaloy-ingot material with coarse, columnar grains was established using isothermal uniaxial and double-cone compression tests. Testing was conducted along different test directions relative to the columnar-grain microstructure at supersolvus temperatures (1066 °C and 1177 °C) and strain rates (0.005 and 0.1 s-1), which bracket typical ingot-breakdown conditions for the material. The flow behavior of axial samples ( i.e., those compressed parallel to the columnar-grain direction) showed an initial strain-hardening transient followed by steady-state flow. In contrast, the stress-strain curves of samples upset transverse to the columnar grains exhibited a peak stress at low strains, whose magnitude was greater than the steady-state flow stress of the axial samples, followed by flow softening. The two distinct flow behaviors were explained on the basis of the solidification texture associated with the starting ingot structure, differences in the kinetics of dynamic recrystallization revealed in the double-cone tests, and the evolution of deformation and recrystallization textures during hot working. Dynamic recrystallization kinetics were measurably faster for the transverse samples as well as specimens oriented at ˜45 deg to the forging direction, an effect partially rationalized based on the initial texture and its effect on the input rate of deformation work driving recrystallization. Despite these differences, the overall strains required for dynamic recrystallization were comparable to those measured previously for fine-grain (wrought) Waspaloy. However, the Avrami exponents (˜2 to 3) were somewhat higher than those for wrought material (˜1 to 2), an effect attributable to the particle-stimulated nucleation in the ingot material.

  19. Oxidation Characterization of Hafnium-Based Ceramics Fabricated by Hot Pressing and Electric Field-Assisted Sintering

    NASA Technical Reports Server (NTRS)

    Gasch, Matt; Johnson, Sylvia; Marschall, Jochen

    2010-01-01

    Ceramic borides, such as hafnium diboride (HfB2) and zirconium diboride (ZrB2), are members of a family of materials with extremely high melting temperatures referred to as Ultra High Temperature Ceramics (UHTCs). UHTCs constitute a class of promising materials for use in high temperature applications, such as sharp leading edges on future-generation hypersonic flight vehicles, because of their high melting points. The controlled development of microstructure has become important to the processing of UHTCs, with the prospect of improving their mechanical and thermal properties. The improved oxidation resistance of HfB2 has also become important if this material is to be successfully used at temperatures above 2000 C. Furthermore, the use of UHTCs on the leading edges of vehicles traveling at hypersonic speeds will mean exposure to a mixed oxidation environment comprised of both molecular and atomic oxygen. The current study has investigated the high-temperature oxidation behavior of HfB2-based materials in a pure O2 environment, as well as in environments containing different levels of dissociated oxygen (O/O2). Materials were processed by two techniques: conventional hot pressing (HP) and electric field-assisted sintering (FAS). Their oxidation behavior was evaluated in both a tube furnace at 1250 C for 3 hours and in a simulated re-entry environment in the Advanced Heating Facility (AHF) arcjet at NASA Ames Research Center, during a 10-minute exposure to a cold wall heat flux of 250W/sq cm and stagnation pressure of 0.1-0.2 atm. The microstructure of the different materials was characterized before and after oxidation using scanning electron microscopy (SEM).

  20. Multiband terahertz quasi-optical balanced hot-electron mixers based on dual-polarization sinuous antennas

    NASA Astrophysics Data System (ADS)

    Jiang, Zhenguo; Rahman, Syed M.; Ruggiero, Steven T.; Fay, Patrick; Liu, Lei

    2014-05-01

    Receivers based on superconducting Hot-Electron Bolometers (HEBs) are widely used for terahertz (THz) sensing owing to their advantages of high sensitivity, low noise, and low LO power requirement. Balanced HEB mixers are superior to single-element ones since the thermal noise and AM noise from the LO injection can be effectively suppressed. Although a 1.3 THz balanced waveguide HEB mixer has been reported, waveguide mixer configurations offer relatively narrow RF bandwidths. We report on the development, fabrication and characterization of a THz quasioptical balanced superconducting HEB mixer utilizing a dual-polarization sinuous antenna that can potentially achieve both multiband operation and ultra-high sensitivity. In the balanced mixer configuration, a lens-coupled four-arm sinuous antenna was designed for operation from 0.2-1.0 THz with a nearly frequency-independent embedding impedance of ~106 Ω. Two identical superconducting niobium HEB devices have been integrated at the antenna feedpoints, connecting each opposing pair of antenna arms to form a balanced mixer configuration. An air-bridge was also fabricated to separate the two mixer branches. The HEB devices were fabricated from 10 nm thick niobium film sputtered on semi-insulating silicon substrates. Each HEB device has dimensions of 80 nm × 240 nm (3 squares) for approaching a resistance of 105 Ω for impedance matching. Mixer properties including antenna radiation patterns, broadband operation and polarization isolation have been characterized. Finally, in order to achieve multiband mixer operation, electronically reconfigurable THz quasi-optical mesh filters are needed. Frequency-tunable antenna elements using Schottky varactor diodes suitable for the above applications have been designed, simulated and demonstrated at Gband (140-220 GHz) showing 50 GHz tuning range.

  1. Quantitation of virus using laser-based scanning of near-infrared fluorophores replaces manual plate reading in a virus titration assay.

    PubMed

    Weldon, Sally K; Mischnick, Shawn L; Urlacher, Teresa M; Ambroz, Kristi L H

    2010-09-01

    A method was developed for quantitation of a virus titration assay for minimally cytopathic and noncytopathic viruses that utilizes laser-based scanning of near-infrared (NIR) fluorophores. This automated method bypasses the need for manual plate reading thus eliminating human bias and error. The image data is translated by LI-COR's Odyssey software into numerical data which is used directly in the virus titer calculations. PMID:20438762

  2. Effects of the shape of the foil corners on the irradiation performance of U10Mo alloy based monolithic mini-plates

    SciTech Connect

    Ozaltun, Hakan; Medvedev, Pavel G

    2015-06-01

    Monolithic plate-type fuel is a fuel form being developed for high performance research and test reactors to minimize the use of enriched material. These fuel elements are comprised of a high density, low enrichment, U-Mo alloy based fuel foil, sandwiched between Zirconium liners and encapsulated in Aluminum cladding. The use of a high density fuel in a foil form presents a number of fabrication and operational concerns, such as: foil centering, flatness of the foil, fuel thickness variation, geometrical tilting, foil corner shape etc. To benchmark this new design, effects of various geometrical and operational variables on irradiation performance have been evaluated. As a part of these series of sensitivity studies, the shape of the foil corners were studied. To understand the effects of the corner shapes of the foil on thermo-mechanical performance of the plates, a behavioral model was developed for a selected plate from RERTR-12 experiments (Plate L1P785). Both fabrication and irradiation processes were simulated. Once the thermo-mechanical behavior the plate is understood for the nominal case, the simulations were repeated for two additional corner shapes to observe the changes in temperature, displacement and stress-strain fields. The results from the fabrication simulations indicated that the foil corners do not alter the post-fabrication stress-strain magnitudes. Furthermore, the irradiation simulations revealed that post-fabrication stresses of the foil would be relieved very quickly in operation. While, foils with chamfered and filleted corners yielded stresses with comparable magnitudes, they are slightly lower in magnitudes, and provided a more favorable mechanical response compared with the foil with sharp corners.

  3. Paleomagnetic evidence from land-based and ODP cores for clockwise rotation and northward translation of the Phillippine Sea plate

    SciTech Connect

    Cisowski, S.M.; Fuller, M.; Haston, R.B.; Koyama, M. )

    1990-06-01

    On-land and deep-sea core paleomagnetic data have been collected from around the Philippine Sea plate. Data from the Palau islands suggest 70{degree} of clockwise rotation and northward translation since the mid-Oligocene. The authors interpret this rotation as a rotation of the West Philippine Sea basin as a whole. New paleomagnetic data from Guam indicate 70{degree} of clockwise rotation and northward translation since the early Oligocene. Although Eocene results have been previously quoted, the new data suggest that there is no reliable Eocene data from Guam. New data from Saipan suggest 50-60{degree} of clockwise rotation since the Late Eocene and 20{degree} of clockwise rotation since the mid-Miocene, along with northward translation. During ODP Leg 126, a new technique utilizing the formation microscanner logging tool was employed to obtain orientated drill cores from the Bonin forearc basin. Preliminary results indicate that 70-110{degree} of clockwise rotation has occurred there since the mid-Oligocene. Inclination studies on cores from ODP Legs 125 and 126 along with the on-land paleomagnetic data support 15{degree} of northward translation of the Philippine Sea plate since the mid-Oligocene. The consistent clockwise rotations found around the Philippine Sea plate suggest that the entire plate, including the Bonin and Mariana arcs, has rotated more than 50{degree} since the mid-Oligocene. The similarity of Oligocene results from the Bonin forearc and Guam suggest that little or no relative rotation has occurred between these two points. This implies that the shape of the Mariana arc is probably not due to rotational deformation. The northward translation and clockwise rotation of the Philippine Sea plate established oblique subduction along the proto-Philippine margin, which could account for the 600 km of subducted slab beneath the eastern Celebes Sea.

  4. Sensitivity Characterization of Pressed Energetic Materials using Flyer Plate Mesoscale Simulations

    NASA Astrophysics Data System (ADS)

    Rai, Nirmal; Udaykumar, H. S.

    Heterogeneous energetic materials like pressed explosives have complicated microstructure and contain various forms of heterogeneities such as pores, micro-cracks, energetic crystals etc. It is widely accepted that the presence of these heterogeneities can affect the sensitivity of these materials under shock load. The interaction of shock load with the microstructural heterogeneities may leads to the formation of local heated regions known as ``hot spots''. Chemical reaction may trigger at the hot spot regions depending on the hot spot temperature and the duration over which the temperature can be maintained before phenomenon like heat conduction, rarefaction waves withdraws energy from it. There are different mechanisms which can lead to the formation of hot spots including void collapse. The current work is focused towards the sensitivity characterization of two HMX based pressed energetic materials using flyer plate mesoscale simulations. The aim of the current work is to develop mesoscale numerical framework which can perform simulations by replicating the laboratory based flyer plate experiments. The current numerical framework uses an image processing approach to represent the microstructural heterogeneities incorporated in a massively parallel Eulerian code SCIMITAR3D. The chemical decomposition of HMX is modeled using Henson-Smilowitz reaction mechanism. The sensitivity characterization is aimed towards obtaining James initiation threshold curve and comparing it with the experimental results.

  5. Holding fixture for a hot stamping press

    NASA Technical Reports Server (NTRS)

    Harris, R. P. (Inventor)

    1983-01-01

    A hand held guide for manually positioning a work piece between the anvil rib and tool of a hot die stamping press is described. A groove completed by interchangeable cover plates attached at one end of the guide conforms to a cross sectional dimension common to similar workpieces and, with a force fit, retentively holds each of the workpieces.

  6. The hot plasma spectrometers on Freja

    NASA Astrophysics Data System (ADS)

    Norberg, O.; Eliasson, L.

    1991-11-01

    The hot plasma instrumentation F3H on the Swedish-German Freja satellite due for launch in 1992 will consist of electron and ion spectrometers. The spectrometer Magnetic imaging Two dimensional Electron (MATE) will measure the two dimensional electron distribution in the spin plane in the energy range 0.1 to 120 keV. The ion mass spectrometer Three dimensional Ion Composition Spectrometer (TICS) measures a full three dimensional distribution in the energy range 0.5 to 15000 eV/q with high mass resolution. The instruments use a particle 'imaging' detector technique based on a large diameter microchannel plate with position sensitive anode. The topics to be studied with the Freja hot plasma spectrometers include auroral particle acceleration, heating and acceleration of ionospheric ions, and the dynamics of auroral arc systems. Of special importance to the scientific objectives is the high data rate from the Freja instrumentation, the MATE and TICS spectrometers will be sampled every 10 ms, corresponding to a spatial resolution better than 70 m at ionospheric heights. The design, simulation, and calibration of the spectrometers are discussed.

  7. Complete metagenome sequencing based bacterial diversity and functional insights from basaltic hot spring of Unkeshwar, Maharashtra, India.

    PubMed

    Mehetre, Gajanan T; Paranjpe, Aditi S; Dastager, Syed G; Dharne, Mahesh S

    2016-03-01

    Unkeshwar hot springs are located at geographical South East Deccan Continental basalt of India. Here, we report the microbial community analysis of this hot spring using whole metagenome shotgun sequencing approach. The analysis revealed a total of 848,096 reads with 212.87 Mbps with 50.87% G + C content. Metagenomic sequences were deposited in SRA database with accession number (SUB1242219). Community analysis revealed 99.98% sequences belonging to bacteria and 0.01% to archaea and 0.01% to Viruses. The data obtained revealed 41 phyla including bacteria and Archaea and including 719 different species. In taxonomic analysis, the dominant phyla were found as, Actinobacteria (56%), Verrucomicrobia (24%), Bacteriodes (13%), Deinococcus-Thermus (3%) and firmicutes (2%) and Viruses (2%). Furthermore, functional annotation using pathway information revealed dynamic potential of hot spring community in terms of metabolism, environmental information processing, cellular processes and other important aspects. Kyoto Encyclopedia of Genes and Genomes (KEGG) pathway analysis of each contig sequence by assigning KEGG Orthology (KO) numbers revealed contig sequences that were assigned to metabolism, organismal system, Environmental Information Processing, cellular processes and human diseases with some unclassified sequences. The Unkeshwar hot springs offer rich phylogenetic diversity and metabolic potential for biotechnological applications. PMID:26981391

  8. Complete metagenome sequencing based bacterial diversity and functional insights from basaltic hot spring of Unkeshwar, Maharashtra, India

    PubMed Central

    Mehetre, Gajanan T.; Paranjpe, Aditi S.; Dastager, Syed G.; Dharne, Mahesh S.

    2015-01-01

    Unkeshwar hot springs are located at geographical South East Deccan Continental basalt of India. Here, we report the microbial community analysis of this hot spring using whole metagenome shotgun sequencing approach. The analysis revealed a total of 848,096 reads with 212.87 Mbps with 50.87% G + C content. Metagenomic sequences were deposited in SRA database with accession number (SUB1242219). Community analysis revealed 99.98% sequences belonging to bacteria and 0.01% to archaea and 0.01% to Viruses. The data obtained revealed 41 phyla including bacteria and Archaea and including 719 different species. In taxonomic analysis, the dominant phyla were found as, Actinobacteria (56%), Verrucomicrobia (24%), Bacteriodes (13%), Deinococcus-Thermus (3%) and firmicutes (2%) and Viruses (2%). Furthermore, functional annotation using pathway information revealed dynamic potential of hot spring community in terms of metabolism, environmental information processing, cellular processes and other important aspects. Kyoto Encyclopedia of Genes and Genomes (KEGG) pathway analysis of each contig sequence by assigning KEGG Orthology (KO) numbers revealed contig sequences that were assigned to metabolism, organismal system, Environmental Information Processing, cellular processes and human diseases with some unclassified sequences. The Unkeshwar hot springs offer rich phylogenetic diversity and metabolic potential for biotechnological applications. PMID:26981391

  9. ELECTROMAGNETISM, OPTICS, ACOUSTICS, HEAT TRANSFER, CLASSICAL MECHANICS, AND FLUID DYNAMICS: On Feasibility of Variable Separation Method Based on Hamiltonian System for a Class of Plate Bending Equations

    NASA Astrophysics Data System (ADS)

    Eburilitu; Alatancang

    2010-03-01

    The eigenfunction system of infinite-dimensional Hamiltonian operators appearing in the bending problem of rectangular plate with two opposites simply supported is studied. At first, the completeness of the extended eigenfunction system in the sense of Cauchy's principal value is proved. Then the incompleteness of the extended eigenfunction system in general sense is proved. So the completeness of the symplectic orthogonal system of the infinite-dimensional Hamiltonian operator of this kind of plate bending equation is proved. At last the general solution of the infinite dimensional Hamiltonian system is equivalent to the solution function system series expansion, so it gives to theoretical basis of the methods of separation of variables based on Hamiltonian system for this kind of equations.

  10. Freestanding GaN-based light-emitting diode membranes on Y3Al5O12:Ce3+ crystal phosphor plate for efficient white light emission

    NASA Astrophysics Data System (ADS)

    Feng, Lungang; Li, Yufeng; Xiong, Han; Wang, Shuai; Wang, Jiangteng; Ding, Wen; Zhang, Ye; Yun, Feng

    2016-08-01

    GaN-based light-emitting diode (LED) membranes were peeled from the substrate using electrochemical etching of the bottom sacrificial layer. The freestanding membranes were transferred onto a Y3Al5O12:Ce3+ (YAG:Ce3+) crystal phosphor plate to realize a compact white light source. Verified by the Raman test, the initial strain within the original GaN layers was greatly released after the exfoliation process, which induced alleviation of the quantum confined stark effect. The electroluminescence measurement of a blue LED membranes-on-YAG:Ce3+ plate-structured device was conducted exhibiting color coordinates and a correlated color temperature of (0.3367,0.4525) and 5450 K at 10 mA, respectively.

  11. Identification of lipid- and protein-based binders in paintings by direct on-plate wet chemistry and matrix-assisted laser desorption ionization mass spectrometry.

    PubMed

    Calvano, Cosima Damiana; van der Werf, Inez Dorothé; Palmisano, Francesco; Sabbatini, Luigia

    2015-01-01

    Direct on-target plate processing of small (ca. 100 μg) fragments of paint samples for MALDI-MS identification of lipid- and protein-based binders is described. Fragments were fixed on a conventional stainless steel target plate by colloidal graphite followed by in situ fast tryptic digestion and matrix addition. The new protocol was first developed on paint replicas composed of chicken egg, collagen, and cow milk mixed with inorganic pigments and then successfully applied on historical paint samples taken from a fifteenth century Italian panel painting. The present work contributes a step forward in the simplification of binder identification in very small paint samples since no conventional solvent extraction is required, speeding up the whole sample preparation to 10 min and reducing lipid/protein loss. PMID:25433687

  12. Real-time thermal imaging of microwave accelerated metal-enhanced fluorescence (MAMEF) based assays on sapphire plates.

    PubMed

    Previte, Michael J R; Zhang, Yongxia; Aslan, Kadir; Geddes, Chris D

    2007-11-01

    In this paper, we describe an optical geometry that facilitates our further characterization of the temperature changes above silver island films (SiFs) on sapphire plates, when exposed to microwave radiation. Since sapphire transmits IR, we designed an optical scheme to capture real-time temperature images of a thin water film on sapphire plates with and without SiFs during the application of a short microwave pulse. Using this optical scheme, we can accurately determine the temperature profile of solvents in proximity to metal structures when exposed to microwave irradiation. We believe that this optical scheme will provide us with a basis for further studies in designing metal structures to further improve plasmonic-fluorescence clinical sensing applications, such as those used in microwave accelerated metal-enhanced fluorescence (MAMEF). PMID:17902038

  13. Plate impact experiments on the TATB based explosive PBX 9502 at pressures near the Chapman-Jouguet state

    NASA Astrophysics Data System (ADS)

    Gustavsen, R. L.; Aslam, T. D.; Bartram, B. D.; Hollowell, B. C.

    2014-05-01

    A series of two-stage gus-gun driven plate impact experiments on PBX 9502 (95 wt.% tri-amino-trinitro-benzene, 5 wt.% Kel-F800 plastic binder) was completed in the 28-34 GPa pressure range. This is just above the Chapman-Jouguet state of ≈ 28 GPa. The experiments consisted of a thick oxygen free high conductivity copper (OFHC Cu) flyer plate impacting a PBX 9502 sample backed by a Lithium Fluoride (LiF) window. Photonic Doppler Velocimetry (PDV) was used to measure velocity histories (wave profiles) at the PBX 9502/LiF interface. Shock transit times and sample thicknesses were converted to shock velocities, Us. Particle velocities, up, were calculated by way of impedance matching. Lastly, the measured wave profiles were compared with numerical simulations of the experiments using the Wescott-Stewart-Davis reactive-burn model.

  14. Experience of the Indirect Neutron Radiography Method Based on the X-ray Imaging Plate at CARR

    NASA Astrophysics Data System (ADS)

    Wei, Guohai; Han, Songbai; Wang, Hongli; He, Linfeng; Wang, Yu; Wu, Meimei; Liu, Yuntao; Chen, Dongfeng

    Indirect neutron radiography (INR) experiments by X-ray imaging plate were carried out at the China Advanced Research Reactor (CARR). The key experiment parameters were optimized, especially the exposure time of the neutron converter andimaging plate. The optimized total exposure time is 37.25 min, it is two-fifths of the timebased on the film method under the same experimental conditions. The qualitative and quantitativeinspections were tested with dummy nuclear fuel rods and a water temperaturesensor ofa motor vehicle. The spring in the sensor and the defects of the dummy fuel rod's pellets can be qualitatively detected. The thickness of the tape at one position on the cladding of the dummy nuclear fuel rodwas quantitatively calculated to be 9.57 layers with the relative error of ±4.3%.

  15. APD-based X-ray imaging telescope using fresnel zone plates for extremely high Spatial Resolution

    NASA Astrophysics Data System (ADS)

    Squillante, Michael R.; Myers, Richard A.; Woodring, Mitchell; Christian, James F.; Robertson, Frank; Farrell, Richard; Kogan, Alexander I.; Tiernan, Timothy C.; Entine, Gerald

    2005-09-01

    A method for constructing an x-ray telescope with exceedingly hgh spatial resolution is to use a pair of coaxial, Fresnel zone plates aligned with an imaging x-ray detector. This combination allows the high sensitivity imaging of x-ray and gamma-ray sources ranging in energy from 1 keV to several hundred keV over a field of view of several degrees with spatial resolution of a fraction of an arc minute. We have implemented a version of such a telescope using several relatively new technologies. These include specialized techniques for constructing Fresnel zone plates from thin sheets of tungsten, a 64-element, avalanche photodiode (APD) array coupled to a matching, segmented, CsI(T1) scintillator, a new ASIC which provides 16-channels of low noise amplification, and image processing software that provides the user not only with localized intensity information, but also with localized spectral information.

  16. Fabrication of a Near-Field Optical Fiber Probe Based on Electroless Nickel Plating under Ultrasonic Irradiation

    NASA Astrophysics Data System (ADS)

    Mononobe, Shuji; Saito, Yuichi; Ohtsu, Motoichi; Honma, Hideo

    2004-05-01

    We present a method of fabricating a near-field optical probe with a nickel film whose thickness gradually decreases to a few tens of nanometers toward the apex. This method involves etching an optical fiber and electroless nickel plating with ultrasonic agitation. Using 1 MHz ceramic transducers, we have reproducibly fabricated the probe with a tip diameter of less than 40 nm. This reproducibility is high compared to those for Langevin-type transducers.

  17. Mantle convection with plates and mobile, faulted plate margins.

    PubMed

    Zhong, S; Gurnis, M

    1995-02-10

    A finite-element formulation of faults has been incorporated into time-dependent models of mantle convection with realistic rheology, continents, and phase changes. Realistic tectonic plates naturally form with self-consistent coupling between plate and mantle dynamics. After the initiation of subduction, trenches rapidly roll back with subducted slabs temporarily laid out along the base of the transition zone. After the slabs have penetrated into the lower mantle, the velocity of trench migration decreases markedly. The inhibition of slab penetration into the lower mantle by the 670-kilometer phase change is greatly reduced in these models as compared to models without tectonic plates. PMID:17813909

  18. Probability-based classifications for spatially characterizing the water temperatures and discharge rates of hot springs in the Tatun Volcanic Region, Taiwan.

    PubMed

    Jang, Cheng-Shin

    2015-05-01

    Accurately classifying the spatial features of the water temperatures and discharge rates of hot springs is crucial for environmental resources use and management. This study spatially characterized classifications of the water temperatures and discharge rates of hot springs in the Tatun Volcanic Region of Northern Taiwan by using indicator kriging (IK). The water temperatures and discharge rates of the springs were first assigned to high, moderate, and low categories according to the two thresholds of the proposed spring classification criteria. IK was then used to model the occurrence probabilities of the water temperatures and discharge rates of the springs and probabilistically determine their categories. Finally, nine combinations were acquired from the probability-based classifications for the spatial features of the water temperatures and discharge rates of the springs. Moreover, various combinations of spring water features were examined according to seven subzones of spring use in the study region. The research results reveal that probability-based classifications using IK provide practicable insights related to propagating the uncertainty of classifications according to the spatial features of the water temperatures and discharge rates of the springs. The springs in the Beitou (BT), Xingyi Road (XYR), Zhongshanlou (ZSL), and Lengshuikeng (LSK) subzones are suitable for supplying tourism hotels with a sufficient quantity of spring water because they have high or moderate discharge rates. Furthermore, natural hot springs in riverbeds and valleys should be developed in the Dingbeitou (DBT), ZSL, Xiayoukeng (XYK), and Macao (MC) subzones because of low discharge rates and low or moderate water temperatures. PMID:25917185

  19. Vibration control of a flexible clamped-clamped plate based on an improved FULMS algorithm and laser displacement measurement

    NASA Astrophysics Data System (ADS)

    Xie, Lingbo; Qiu, Zhi-cheng; Zhang, Xian-min

    2016-06-01

    This paper presents a novel active resonant vibration control experiment of a flexible clamped-clamped plate using an improved filtered-U least mean square (FULMS) algorithm and laser displacement measurement. Different from the widely used PZT sensors or acceleration transducers, the vibration of the flexible clamped-clamped plate is measured by a non-contact laser displacement measurement sensor with higher measurement accuracy and without additional load to the plate. The conventional FULMS algorithm often uses fixed step size and needs reference signal related to the external disturbance signal. However, the fixed step size method cannot obtain a fast convergence speed and it will result in a low residual error. Thus, a variable step size method is investigated. In addition, it is difficult to extract reference signal related to the vibration source directly in the practical application. Therefore, it is practically useful that a reference signal is constructed by both the controller parameters and the vibration residual signal. The experimental results demonstrate that the improved FULMS algorithm has better vibration control effect than the proportional derivative (PD) feedback control algorithm and the fixed step-size control algorithm.

  20. Concentrator hot-spot testing, phase 1

    NASA Technical Reports Server (NTRS)

    Gonzalez, C. C.

    1987-01-01

    Results of a study to determine the hot-spot susceptibility of concentrator cells, to provide a hot-spot qualification test for concentrator modules, and to provide guidelines for reducing hot-spot susceptibility are presented. Hot-spot heating occurs in a photovoltaic module when the short-circuit current of a cell is lower than the string operating current forcing the cell into reverse bias with a concurrent power dissipation. Although the basis for the concentrator module hot-spot qualification test is the test developed for flat-plate modules, issues, such as providing cell illumination, introduce additional complexities into the testing procedure. The same general guidelines apply for protecting concentrator modules from hot-spot stressing as apply to flat-plate modules. Therefore, recommendations are made on the number of bypass diodes required per given number of series cells per module or source circuit. In addition, a new method for determining the cell temperature in the laboratory or in the field is discussed.