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Sample records for creep deformation characteristics

  1. Creep deformation of TD-nickel chromium

    NASA Technical Reports Server (NTRS)

    Kane, R. D.; Ebert, L. J.

    1976-01-01

    An investigation was conducted of the mechanical behavioral characteristics of thoria-dispersed (TD) NiCr materials at elevated temperatures. The experimental procedure used is discussed along with the significance of the obtained results. Attention is given to basic creep behavior and creep thermal activation parameter measurements. It is found that the overall creep behavior of TD-NiCr can be explained on the basis of the relative contributions of two parallel-concurrent deformation mechanisms, including diffusion controlled grain boundary sliding and dislocation motion.

  2. The role of grain boundary sliding on creep deformation characteristics of discontinuous reinforced composites

    SciTech Connect

    Biner, S.B.

    1994-10-01

    In this study, the grain boundary sliding behavior in discontinuous reinforced composites is investigated numerically. Results indicate that the stress enhancement factor for the composite is much larger than the one observed for the matrix material. In the composite, the increase in the strain rates as a result of grain boundary sliding occurs in a wider stress range in comparison to the matrix. It is shown that the experimentally observed large scale triple point grain boundary cavitation in the composites could occur as a result of large grain rotations resulting from grain boundary sliding and evolution of triaxial stress state. Also, the observed larger creep exponent values or stress dependent creep exponent values for the composites may not be explained solely by the mechanism of grain boundary sliding.

  3. Creep Deformation of B2 Alumindes

    NASA Technical Reports Server (NTRS)

    Nathal, M. V.

    1991-01-01

    The creep resistance and elevated temperature deformation mechanisms in CoAl, FeAl, and NiAl are reviewed. The stress and temperature dependencies of the steady state creep rate, the primary creep behavior, the dislocation substructure, and the response during transient tests are used as the main indicators of the deformation processes. In single phase intermetallics, the influence of grain size, stoichiometry, and solid solution hardening have been examined. In addition, the effect of adding dispersoids, precipitates, and other types of reinforcements to improve creep strength are compared.

  4. Creep fracture during solute-drag creep and superplastic deformation

    SciTech Connect

    Taleff, E.M.; Lesuer, D.R.; Syn, C.K.; Henshall, G.A.

    1996-10-01

    Creep fracture behavior has been studied in Al-Mg and Al-Mg-Mn alloys undergoing solute-drag creep and in microduplex stainless steel undergoing both solute-drag creep and superplastic deformation. Failure in these materials is found to be controlled by two mechanisms, neck formation and cavitation. The mechanism of creep fracture during solute-drag creep in Al-Mg is found to change from necking-controlled fracture to cavitation-controlled fracture as Mn content is increased. Binary Al-Mg material fails by neck formation during solute-drag creep, and cavities are formed primarily in the neck region due to high hydrostatic stresses. Ternary alloys of Al-Mg- Mn containing 0.25 and 0.50 wt % Mn exhibit more uniform cavitation, with the 0.50 Mn alloy clearly failing by cavity interlinkage. Failure in the microduplex stainless steel is dominated by neck formation during solute-drag creep deformation but is controlled by cavity growth and interlinkage during superplastic deformation. Cavitation was measured at several strains, and found to increase as an exponential function of strain. An important aspect of cavity growth in the stainless steel is the long latency time before significant cavitation occurs. For a short latency period, cavitation acts to significantly reduce ductility below that allowed by neck growth alone. This effect is most pronounced in materials with a high strain-rate sensitivity, for which neck growth occurs very slowly.

  5. Creep deformation of a soft magnetic iron-cobalt alloy

    NASA Astrophysics Data System (ADS)

    Fingers, R. T.; Coate, J. E.; Dowling, N. E.

    1999-04-01

    The U.S. Air Force is in the process of developing magnetic bearings, as well as an aircraft integrated power unit and an internal starter/generator for main propulsion engines. These developments are the driving force for the new emphasis on the development of high saturation, low loss magnets capable of maintaining structural integrity in high stress and high temperature environments. It is this combination of desired material characteristics that is the motivation of this effort to measure, model, and predict the creep behavior of such advanced magnetic materials. Hiperco Alloy 50HS, manufactured by Carpenter Technology Corporation, is one of the leading candidates for these applications. Material specimens were subjected to a battery of mechanical tests in order to study and characterize their behaviors. Tensile tests provided stress versus strain behaviors that clearly indicated: a yield point, a heterogeneous deformation described as Lders elongation, the Portevin-LeChatelier effect at elevated temperatures, and most often a section of homogeneous deformation that concluded with necking and fracture. Creep testing indicated three distinct types of behavior. Two types resembled a traditional response with primary, secondary, and tertiary stages; while the third type can be characterized by an abrupt increase in strain rate that acts as a transition from one steady-state behavior to another. The relationships between the tensile and creep responses are discussed. Analyses of the mechanical behavior include double linear regression of empirically modeled data, and constant strain rate testing to bridge the tensile and creep test parameters.

  6. Estimating creep deformation of glass-fiber-reinforced polycarbonate

    NASA Astrophysics Data System (ADS)

    Sakai, Takenobu; Somiya, Satoshi

    2006-09-01

    Thermoplastic resin and fiber-reinforced thermo-plastics (FRTPs) were used without post-cure treatment as molded material. For such materials, creep behavior and physical aging occur simultaneously. This study examined the creep behavior of polycarbonate (PC) and glass-fiber-reinforced polycarbonate (GFRPC) injection moldings, including the effect of physical aging and fiber content, and determined that the time temperature superposition principle could be applied to the creep behavior for different fiber contents. The effects of physical aging on creep behavior were evaluated quantitatively on pure resin and with various fiber contents without heat treatment. We found that the effect of physical aging could be evaluated with the proposed factor, aging shift rate. To discuss the linearity of viscoelasticity in FRTPs, this study used two shift factors: time and modulus shift factors. The fiber content affected creep behavior by both retarding and restraining it through changing the elastic modulus. This was shown by generating a grand master curve of creep compliance, which included the effects of time, temperature, and fiber content. Using the grand master curve of creep compliance and shift factors, it was possible to estimate the creep deformation of molded materials under varying conditions and fiber contents. The estimated creep deformation gave a very good fit to the experimental creep deformation.

  7. Nucleation and growth characteristics of cavities during the early stages of tensile creep deformation in a superplastic zirconia-20 wt% alumina composite

    SciTech Connect

    Owen, D.M.; Chokshi, A.H.; Nutt, S.R.

    1997-09-01

    Constant-stress tensile creep experiments on a superplastic 3-mol%-yttria-stabilized tetragonal zirconia composite with 20 wt% alumina revealed that cavities nucleate relatively early during tensile deformation. The number of cavities nucleated increases with increasing imposed stress. The cavities nucleate at triple points associated largely with an alumina grain, and then grow rapidly in a cracklike manner to attain dimensions on the order of the grain facet size. It is suggested that coarser-grained superplastic ceramics exhibit lower ductility due to the ease in formation of such grain boundary facet-cracks and their interlinkage to form a macroscopic crack of critical dimensions.

  8. Finite Element Analysis of Plastic Deformation During Impression Creep

    NASA Astrophysics Data System (ADS)

    Naveena; Ganesh Kumar, J.; Mathew, M. D.

    2015-04-01

    Finite element (FE) analysis of plastic deformation associated with impression creep deformation of 316LN stainless steel was carried out. An axisymmetric FE model of 10 10 10 mm specimen with 1-mm-diameter rigid cylindrical flat punch was developed. FE simulation of impression creep deformation was performed by assuming elastic-plastic-power-law creep deformation behavior. Evolution of the stress with time under the punch during elastic, plastic, and creep processes was analyzed. The onset of plastic deformation was found to occur at a nominal stress about 1.12 times the yield stress of the material. The size of the developed plastic zone was predicted to be about three times the radius of the punch. The material flow behavior and the pile-up on specimen surface have been modeled.

  9. Tantalum alloys resist creep deformation at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Buckman, R. W., Jr.

    1966-01-01

    Dispersion-strengthened tantalum-base alloys possess high strength and good resistance to creep deformation at elevated temperatures in high vacuum environments. They also have ease of fabrication, good weldability, and corrosion resistance to molten alkali metals.

  10. On the creep deformation of nickel foams under compression

    NASA Astrophysics Data System (ADS)

    Burteau, Anthony; Bartout, Jean-Dominique; Bienvenu, Yves; Forest, Samuel

    2014-10-01

    A finite-element computational strategy is developed to study the viscoplastic deformation mechanisms at work in a nickel foam sample under compression creep. The constitutive law for pure nickel accounts for both diffusional and dislocation creep mechanisms. The finite-element results show the competition between both mechanisms due to the strong heterogeneity of the stress distribution in the foam. The initiation of the viscoplastic buckling phenomenon leading to cell crushing in tertiary creep is illustrated. The overall model prediction is compared to the results of compression creep tests performed in vacuo at 900 C. xml:lang="fr"

  11. Effect of Tungsten on Primary Creep Deformation and Minimum Creep Rate of Reduced Activation Ferritic-Martensitic Steel

    NASA Astrophysics Data System (ADS)

    Vanaja, J.; Laha, Kinkar; Mathew, M. D.

    2014-10-01

    Effect of tungsten on transient creep deformation and minimum creep rate of reduced activation ferritic-martensitic (RAFM) steel has been assessed. Tungsten content in the 9Cr-RAFM steel has been varied between 1 and 2 wt pct, and creep tests were carried out over the stress range of 180 and 260 MPa at 823 K (550 C). The tempered martensitic steel exhibited primary creep followed by tertiary stage of creep deformation with a minimum in creep deformation rate. The primary creep behavior has been assessed based on the Garofalo relationship, , considering minimum creep rate instead of steady-state creep rate . The relationships between (i) rate of exhaustion of transient creep r' with minimum creep rate, (ii) rate of exhaustion of transient creep r' with time to reach minimum creep rate, and (iii) initial creep rate with minimum creep rate revealed that the first-order reaction-rate theory has prevailed throughout the transient region of the RAFM steel having different tungsten contents. The rate of exhaustion of transient creep r' and minimum creep rate decreased, whereas the transient strain ? T increased with increase in tungsten content. A master transient creep curve of the steels has been developed considering the variation of with . The effect of tungsten on the variation of minimum creep rate with applied stress has been rationalized by invoking the back-stress concept.

  12. Creep Behavior, Deformation Mechanisms, and Creep Life of Mod.9Cr-1Mo Steel

    NASA Astrophysics Data System (ADS)

    ABE, Fujio

    2015-12-01

    The creep behavior, deformation mechanisms, and the correlation between creep deformation parameters and creep life have been investigated for Mod.9Cr-1Mo steel (Gr.91, 9Cr-1Mo-VNb) by analyzing creep strain data at 723 K to 998 K (450 C to 725 C), 40 to 450 MPa, and t r = 11.4 to 68,755 hours in NIMS Creep Data Sheet. The time to rupture t r is reasonably correlated with the minimum creep rate {dot{\\varepsilon }}_{ min } and the acceleration of creep rate by strain in the acceleration region dln {dot{\\varepsilon }} /d ?, as t r = 1.5/[ {dot{\\varepsilon }}_{ min } ( dln {dot{\\varepsilon }} /d ?)], where {dot{\\varepsilon }}_{ min } and dln {dot{\\varepsilon }} /d ? reflect the creep behavior in the transient and acceleration regions, respectively. The {dot{\\varepsilon }}_{ min } is inversely proportional to the time to minimum creep rate t m, while it is proportional to the strain to minimum creep rate ? m, as {dot{\\varepsilon }}_{ min } = 0.54 ( ? m/ t m). The ? m decreases with decreasing stress, suggesting that the creep deformation in the transient region becomes localized in the vicinity of prior austenite grain boundaries with decreasing stress. The duration of acceleration region is proportional to the duration of transient region, while the dln {dot{\\varepsilon }} /d ? is inversely proportional to the ? m. The t r is also correlated with the t m, as t r = g t m, where g is a constant. The present creep life equations reasonably predict the degradation in creep rupture strength at long times. The downward deviation takes place in the t r vs {dot{\\varepsilon }}_{ min } curves (Monkman-Grant plot). At the same {dot{\\varepsilon }}_{ min } , both the ? m and t m change upon the condition of t m ? ? m. The decrease in ? m with decreasing stress, corresponding to decreasing {dot{\\varepsilon }}_{ min } , causes a decrease in t m, indicating the downward deviation of the t r vs {dot{\\varepsilon }}_{ min } curves.

  13. Sharp interface model of creep deformation in crystalline solids

    NASA Astrophysics Data System (ADS)

    Mishin, Y.; McFadden, G. B.; Sekerka, R. F.; Boettinger, W. J.

    2015-08-01

    We present a rigorous irreversible thermodynamics treatment of creep deformation of solid materials with interfaces described as geometric surfaces capable of vacancy generation and absorption and moving under the influence of local thermodynamic forces. The free energy dissipation rate derived in this work permits clear identification of thermodynamic driving forces for all stages of the creep process and formulation of kinetic equations of creep deformation and microstructure evolution. The theory incorporates capillary effects and reveals the different roles played by the interface free energy and interface stress. To describe the interaction of grain boundaries with stresses, we classify grain boundaries into coherent, incoherent and semicoherent, depending on their mechanical response to the stress. To prepare for future applications, we specialize the general equations to a particular case of a linear-elastic solid with a small concentration of vacancies. The proposed theory creates a thermodynamic framework for addressing more complex cases, such as creep in multicomponent alloys and cross-effects among vacancy generation/absorption and grain boundary motion and sliding.

  14. Assessment of Tungsten Content on Tertiary Creep Deformation Behavior of Reduced Activation Ferritic-Martensitic Steel

    NASA Astrophysics Data System (ADS)

    Vanaja, J.; Laha, Kinkar

    2015-10-01

    Tertiary creep deformation behavior of reduced activation ferritic-martensitic (RAFM) steels having different tungsten contents has been assessed. Creep tests were carried out at 823 K (550 C) over a stress range of 180 to 260 MPa on three heats of the RAFM steel (9Cr-W-0.06Ta-0.22V) with tungsten content of 1, 1.4, and 2.0 wt pct. With creep exposure, the steels exhibited minimum in creep rate followed by progressive increase in creep rate until fracture. The minimum creep rate decreased, rupture life increased, and the onset of tertiary stage of creep deformation delayed with the increase in tungsten content. The tertiary creep behavior has been assessed based on the relationship, , considering minimum creep rate () instead of steady-state creep rate. The increase in tungsten content was found to decrease the rate of acceleration of tertiary parameter ` p.' The relationships between (1) tertiary parameter `p' with minimum creep rate and time spent in tertiary creep deformation and (2) the final creep rate with minimum creep rate revealed that the same first-order reaction rate theory prevailed in the minimum creep rate as well as throughout the tertiary creep deformation behavior of the steel. A master tertiary creep curve of the steels has been developed. Scanning electron microscopic investigation revealed enhanced coarsening resistance of carbides in the steel on creep exposure with increase in tungsten content. The decrease in tertiary parameter ` p' with tungsten content with the consequent decrease in minimum creep rate and increase in rupture life has been attributed to the enhanced microstructural stability of the steel.

  15. Deformation Microstructures and Creep Mechanisms in Advanced ZR-Based Cladding Under Biazal Loading

    SciTech Connect

    K. Linga Murty

    2008-08-11

    Investigate creep behavior of Zr-based cladding tubes with attention to basic creep mechanisms and transitions in them at low stresses and/or temperatures and study the dislocation microstructures of deformed samples for correlation with the underlying micromechanism of creep

  16. Multimechanism-Deformation Parameters of Domal Salts Using Transient Creep Analysis

    SciTech Connect

    MUNSON, DARRELL E

    1999-09-01

    Use of Gulf Coast salt domes for construction of very large storage caverns by solution mining has grown significantly in the last several decades. In fact, among the largest developers of storage caverns along the Gulf Coast is the Strategic Petroleum Reserve (SPR) which has purchased or constructed 62 crude oil storage caverns in four storage sites (domes). Although SPR and commercial caverns have been operated economically for many years, the caverns still exhibit some relatively poorly understood behaviors, especially involving creep closure volume loss and hanging string damage from salt falls. Since it is possible to postulate that some of these behaviors stem from geomechanical or reformational aspects of the salt, a method of correlating the cavern response to mechanical creep behavior as determined in the laboratory could be of considerable value. Recently, detailed study of the creep response of domal salts has cast some insight into the influence of different salt origins on cavern behavior. The study used a simple graphical analysis of limited non-steady state data to establish an approach or bound to steady state, as an estimate of the steady state behavior of a given salt. This permitted analysis of sparse creep databases for domal salts. It appears that a shortcoming of this steady state analysis method is that it obscures some critical differences of the salt material behavior. In an attempt to overcome the steady state analysis shortcomings, a method was developed based on integration of the Multimechanism-Deformation (M-D) creep constitutive model to obtain fits to the transient response. This integration process permits definition of all the material sensitive parameters of the model, while those parameters that are constants or material insensitive parameters are fixed independently. The transient analysis method has proven more sensitive to differences in the creep characteristics and has provided a way of defining different behaviors within a given dome. Characteristics defined by the transient analysis are related quantitatively to the volume loss creep rate of the SPR caverns. This increase in understanding of the domal material creep response already has pointed to the possibility y of delineating the existence of material spines within a specific dome. Further definition of the domal geology and structure seems possible only through expansion of the creep databases for domal salts.

  17. Creep model of unsaturated sliding zone soils and long-term deformation analysis of landslides

    NASA Astrophysics Data System (ADS)

    Zou, Liangchao; Wang, Shimei; Zhang, Yeming

    2015-04-01

    Sliding zone soil is a special soil layer formed in the development of a landslide. Its creep behavior plays a significant role in long-term deformation of landslides. Due to rainfall infiltration and reservoir water level fluctuation, the soils in the slide zone are often in unsaturated state. Therefore, the investigation of creep behaviors of the unsaturated sliding zone soils is of great importance for understanding the mechanism of the long-term deformation of a landslide in reservoir areas. In this study, the full-process creep curves of the unsaturated soils in the sliding zone in different net confining pressure, matric suctions and stress levels were obtained from a large number of laboratory triaxial creep tests. A nonlinear creep model for unsaturated soils and its three-dimensional form was then deduced based on the component model theory and unsaturated soil mechanics. This creep model was validated with laboratory creep data. The results show that this creep model can effectively and accurately describe the nonlinear creep behaviors of the unsaturated sliding zone soils. In order to apply this creep model to predict the long-term deformation process of landslides, a numerical model for simulating the coupled seepage and creep deformation of unsaturated sliding zone soils was developed based on this creep model through the finite element method (FEM). By using this numerical model, we simulated the deformation process of the Shuping landslide located in the Three Gorges reservoir area, under the cycling reservoir water level fluctuation during one year. The simulation results of creep displacement were then compared with the field deformation monitoring data, showing a good agreement in trend. The results show that the creeping deformations of landslides have strong connections with the changes of reservoir water level. The creep model of unsaturated sliding zone soils and the findings obtained by numerical simulations in this study are conducive to reveal the mechanisms of the dynamic process of landslide deformation, and serve as an important basis for the prediction and evaluation of landslides.

  18. Modelling of anisotropic creep deformation and damage in single crystal superalloys

    SciTech Connect

    Li, S.X.; Smith, D.J.

    1995-09-01

    Previous studies on the creep behavior of single crystal nickel base superalloys reveal that both creep deformation behavior and stress rupture properties of single crystal alloys are strongly dependent on crystal orientation and temperature. A physical model of creep deformation in single crystal superalloys has been proposed by Ghosh et al. This model accounts for the anisotropy and asymmetry of creep by viscous glide on specific crystallographic slip systems and for the tertiary creep behavior through a damage parameter that is related to the accumulation of mobile dislocations in each slip system. The model has been applied to analyze the creep curves of the single crystal nickel base superalloy SRR99, with particular reference to [001] and [111] orientations. The model also attempts to predict the change in the anisotropy of creep behavior with stress and temperature, and the changes in the orientation and specimen cross-section with creep strain. The creep model proposed by Ghosh et al has been modified and extended to describe the anisotropic creep behavior of single crystal superalloys for multiaxial stress states. The equations must be used with a general transformation procedure to relate the crystallographic deformation to the global loading directions. Three creep rupture criteria based on material damage in single crystal superalloys have been suggested. The creep damage criterion that takes into account of the different effects of damage on octahedral and cubic slip system and includes interaction effects between the two types of slip provided the best predictions of creep rupture life for the single crystal nickel base superalloy SRR99.

  19. Creep deformation in near-γ TiAl: Part 1. the influence of microstructure on creep deformation in Ti-49Al-1V

    NASA Astrophysics Data System (ADS)

    Worth, Brian D.; Jones, J. Wayne; Allison, John E.

    1995-11-01

    The influence of microstructure on creep deformation was examined in the near-y TiAl alloy Ti-49A1-1V. Specifically, microstructures with varying volume fractions of lamellar constituent were produced through thermomechanical processing. Creep studies were conducted on these various microstructures under constant load in air at temperatures between 760 °C and 870 °C and at stresses ranging from 50 to 200 MPa. Microstructure significantly influences the creep behavior of this alloy, with a fully lamellar microstructure yielding the highest creep resistance of the microstructures examined. Creep resistance is dependent on the volume fraction of lamellar constituent, with the lowest creep resistance observed at intermediate lamellar volume fractions. Examination of the creep deformation structure revealed planar slip of dislocations in the equiaxed y microstructure, while subboundary formation was observed in the duplex microstructure. The decrease in creep resistance of the duplex microstructure, compared with the equiaxed y microstructure, is attributed to an increase in dislocation mobility within the equiaxed y constituent, that results from partitioning of oxygen from the γ phase to the α2 phase. Dislocation motion in the fully lamellar microstructure was confined to the individual lamellae, with no evidence of shearing of γ/γ or γ/α2 interfaces. This suggests that the high creep resistance of the fully lamellar microstructure is a result of the fine spacing of the lamellar structure, which results in a decreased effective slip length for dislocation motion over that found in the duplex and equiaxed y microstructures.

  20. Creep Behavior and Deformation Mechanisms for Nanocluster-Strengthened Ferritic Steels

    SciTech Connect

    Brandes, Matthew C; Kovarik, L.; Miller, Michael K; Daehn, Glenn; Mills, Michael J.

    2011-01-01

    Mechanically alloyed, nanostructured ferritic steels represent a class of alloys that can display high resistance to radiation and creep deformation, which are derived from the presence of nanoclusters, precipitates and solute segregation to the grain boundaries. The creep responses for a 14YWT nanostructured ferritic steel were measured over a range of temperatures and stress levels. The stress exponent was observed to vary non-linearly with applied stress; stress exponents were found to decrease with decreasing stress approaching unity at low stress. Transmission electron microscopy studies clearly demonstrated that creep deformation proceeds by a dislocation glide within nanoscale grains and that glide dislocations are attracted to and pinned by nanoclusters. In light of these observations, a new model of the creep response, inspired by the Kocks-Argon-Ashby model, is developed to explain the low creep rates and small stress exponents that are exhibited by these alloys.

  1. Plastic deformation and creep damage evaluations of type 316 austenitic stainless steels by EBSD

    SciTech Connect

    Yoda, Rika; Yokomaku, Toshinori; Tsuji, Nobuhiro

    2010-10-15

    The inspection method of plastic and/or creep deformations has been required as the quantitative damage estimation procedure for structural components especially used in electric power plants. In this study, the method using electron backscatter diffraction (EBSD) was applied to the deformation and damage evaluation of austenitic stainless steels strained by tension or compression at room temperature and also tested in creep at high temperature. It was found that the value of Grain Average Misorientation (GAM) which showed the average misorientation for the whole observed area including over several dozen grains, was a very useful parameter for quantifying the microstructural change as either the plastic or creep strain increased. The unique linear correlation was obtained between GAM and plastic strain in tension and compression. For creep damage evaluation, the difference of grain average misorientation from the value of the unstrained specimen ({Delta}GAM) showed an excellent correlation with the inelastic strain below strain at which the tertiary creep began.

  2. On the creep deformation mechanisms of an advanced disk nickel-base superalloy

    NASA Astrophysics Data System (ADS)

    Unocic, Raymond R.

    The main objective of this research was aimed at investigating the fundamental relationship between microstructure and creep deformation mechanisms using a variety of electron microscopy characterization techniques. The alloy used in this research, Rene 104, is a newer generation powder metallurgy Ni-base superalloy that was developed specifically for aircraft gas turbine disk applications with extended service durability at temperatures exceeding 650C. The influence of stress and temperature was studied first and it was found that during creep deformation at temperatures between 677--815C and stresses between 345--724MPa a variety of distinctly different creep deformation mechanisms were operative. In addition to identifying the creep deformation mechanisms an attempt was made to determine the creep rate limiting process so that an improved understanding of the fundamental processes that control deformation can be better understood. Microtwinning was found to the dominant deformation mechanism following creep at 677C/690MPa and 704C/724MPa. Microtwins form by the motion of paired a/6<112> Shockley partial dislocations that shear both the gamma matrix and gamma' precipitates. The rate limiting process in this mechanism is diffusion mediated atomic reordering that occurs in the wake of the shearing, twinning partial dislocations in order to maintain the ordered L12 structure of the gamma' precipitates. This reordering process helps to fundamentally explain the temperature and rate dependence of microtwinning under creep conditions within this temperature and stress regime. At a slightly higher temperature but lower stress (760C and 345MPa), a stacking fault related shearing mechanism, which typically spanned only a few micrometers in length, was the principle deformation mode. The faults left behind in the gamma' precipitates determined to be extrinsic in nature. During creep at the highest temperature and lowest stress (815C and 345MPa) a thermally activated climb/bypass mechanism of a/2<110> dislocations were found to be the dominant deformation mechanism. In this mechanism, the gamma' precipitates were not sheared but instead were bypassed by a/2<110> matrix dislocations. In addition to the identification of creep deformation mechanisms as a function of stress and temperature, characterization of the post creep gamma' precipitate microstructure revealed that microstructural evolution of the gamma' precipitates has occurred during creep at the higher test temperatures where the secondary gamma' precipitates have coarsened and the tertiary gamma' precipitates have dissolved. In combination with creep at low stress and high temperature, the microstructural evolution may have contributed to the transition from one deformation mode to another. In an attempt to link the influence of microstructure (gamma' precipitate size scale, distribution, volume fraction, and gamma channel width spacing) on creep deformation behavior and creep deformation mechanisms, specimens with different size scaled microstructural features were crept at the same temperature and stress (677C and 724MPa) in order to provide a direct comparison between differences in microstructure. It was found that a microstructure consisting of a bimodal distribution of gamma' precipitates with coarse secondary gamma' precipitates, a high volume fraction of tertiary gamma' precipitates and a wide gamma channel width spacing results in a less creep resistance microstructure that deformed primary by a/2<110> dislocation activity in the gamma matrix at small strain and secondary gamma' shearing via superlattice intrinsic stacking faults at higher strains. The more creep resistant microstructure consisted of a bimodal distribution of gamma' precipitates with a finer secondary gamma' precipitate size, low volume fraction of gamma' and narrow gamma channel width spacing. The combination of these microstructural features promoted a/2<110> dislocation dissociation and decorrelation of a/6<112> Shockley partial di

  3. Deformation mechanism for high temperature creep of a directionally solidified nickel-base superalloy

    SciTech Connect

    Yuan, C.; Guo, J.T.; Wang, S.H.; Yang, H.C.

    1998-09-04

    Modern nickel-base superalloys, which contain a high volume fraction of hard cubical {gamma}{prime} precipitates embedded coherently in a softer {gamma} matrix, are used as turbine blade material due to their good resistance to creep deformation at high temperature. In this present study, the authors will analyze the relationship between the steady-state creep rate and the applied stress of DZ17G, a modern DS cast nickel-base superalloy used for producing turbine blades and vanes for aeroengine applications. On the basis of TEM observations and calculations of the threshold stress for different deformation mechanism, the authors finally propose the deformation mechanism for creep of DZ17G superalloy at high temperature.

  4. Creep deformation in near-{gamma} TiAl. 2: Influence of carbon on creep deformation in Ti-48Al-1V-0.3C

    SciTech Connect

    Worth, B.D.; Jones, J.W.; Allison, J.E.

    1995-11-01

    The influence of interstitial strengthening and microstructure on creep deformation has been examined in the near-{gamma} TiAl alloy Ti-48Al-1V-0.3C. Creep studies were conducted under constant load in air at 815 c in the stress range of 50 to 200 MPa. Significant improvement in creep resistance was observed in this alloy compared with a similar alloy (Ti-49Al-1V) containing low levels of carbon (0.07 at. pct). The degree of strengthening resulting from the addition of carbon was found to be dependent on microstructure. At 815 C and 150 MPa, the addition of carbon reduced the minimum creep rate by a factor of approximately 20 in the equiaxed {gamma} and duplex microstructures and by a factor of 3 in the fully lamellar microstructures. Carbide precipitation occurred in this alloy when aged in the temperature range of 700 C to 950 C. The addition of carbon leads to a decease in the stress exponent from 4 to 3 in the duplex and equiaxed {gamma} microstructures and the inhibition of sub-boundary formation in the duplex microstructure. This suggests that solute/dislocation interaction mechanisms, rather than a direct effect of carbide precipitates, are responsible for the significant increase in creep resistance observed in this alloy.

  5. Brittle creep in basalt and its application to time-dependent volcano deformation

    NASA Astrophysics Data System (ADS)

    Heap, M. J.; Baud, P.; Meredith, P. G.; Vinciguerra, S.; Bell, A. F.; Main, I. G.

    2011-07-01

    Time-dependent brittle deformation is a fundamental and pervasive process operating in the Earth's upper crust. Its characterization is a pre-requisite to understanding and unraveling the complexities of crustal evolution and dynamics. The preferential chemical interaction between pore fluids and strained atomic bonds at crack tips, a mechanism known as stress corrosion, allows rock to fail under a constant stress that is well below its short-term strength over an extended period of time; a process known as brittle creep. Here we present the first experimental measurements of brittle creep in a basic igneous rock (a basalt from Mt. Etna volcano) under triaxial stress conditions. Results from conventional creep experiments show that creep strain rates are highly dependent on the level of applied stress (and can be equally well fit by a power law or an exponential law); with a 20% increase in stress producing close to three orders of magnitude increase in creep strain rate. Results from stress-stepping creep experiments show that creep strain rates are also influenced by the imposed effective confining pressure. We show that only part of this change can be attributed to the purely mechanical influence of an increase in effective pressure, with the remainder interpreted as due to a reduction in stress corrosion reactions; the result of a reduction in crack aperture that restricts the rate of transport of reactive species to crack tips. Overall, our results also suggest that a critical level of crack damage is required before the deformation starts to accelerate to failure, regardless of the level of applied stress and the time taken to reach this point. The experimental results are discussed in terms of microstructural observations and fits to a macroscopic creep law, and compared with the observed deformation history at Mt. Etna volcano.

  6. Post- and interseismic deformation due to both localized and distributed creep at depth (Invited)

    NASA Astrophysics Data System (ADS)

    Hetland, E. A.; Zhang, G.; Hines, T.

    2013-12-01

    There are two end-member representations of the ductile lithosphere (i.e., the lower crust and uppermost mantle) commonly used in models of post- and interseismic deformation around strike-slip faults: either (1) laterally homogeneous ductile layers, with sharp contrasts in rheological properties between the layers, in which creep is distributed; or (2) discrete extensions of the fault at depth in which creep is fully localized. The most realistic representation of the ductile lithosphere on earthquake cycle time scales likely falls between these two end-members. Researchers have considered both distributed and localized creep when interpreting post- and interseismic deformation, although the two mechanisms are most commonly treated separately, with the localized creep often approximated by kinematic slip on planar faults. There are a few noteworthy models that considered the feedback between both distributed and localized creep, although those models were largely constrained to 2D geometries of infinite length faults. The thickness of shear zones in the ductile lithosphere may be comparable to the locking depth of the fault, and the existence of a deep shear zone does not preclude the possibility that some distributed creep occurs in the surrounding lithosphere. Furthermore, variations in rheology, including both rheological models and their parameters, may be more subtle than the discrete contrasts typically assumed. In this presentation, we consider models of postseismic deformation following a finite length, strike-slip fault, as well as models of interseismic deformation around an infinite length strike-slip fault. Both sets of models are capable of localized and distributed creep at depth, and use Maxwell viscoelasticity. We show that the horizontal surface velocities during the early postseismic period are most sensitive to the viscosity of the shear zone; however during much of the interseismic period the shear zone is not apparent from the surface deformation, which is consistent with very large uniform viscosities in the ductile lithosphere. On the other hand, the vertical postseismic surface deformation is highly sensitive to the depth-dependent distribution of viscosities, regardless of whether the model contains purely distributed creep or also includes a component of localized creep. Hence, vertical postseismic deformation can discriminate vertical contrasts in viscosity, but is not a good discriminant of localized vs. distributed creep at depth. Models that contain components of both localized and distributed creep predict transient postseismic deformation, characterized by a fast relaxation phase followed by a slower relaxation phase, even when the model only contains steady Maxwell viscosities. This transience is equivalent to that predicted in models that approximate the ductile lithosphere with transient viscoelasticity, and we discuss the implication on the lithosphere rheology inferred from deformation following the 1997 Manyi, China, earthquake. Finally, we address the mechanism in which shear zones might develop under strike-slip faults and the implication of power-law creep rheologies.

  7. Constrained cavity growth models of longitudinal creep deformation of oxide dispersion strengthened alloys

    NASA Astrophysics Data System (ADS)

    Stephens, J. J.; Nix, W. D.

    1986-02-01

    Two models of constrained cavity growth are developed to describe the long-term longitudinal creep behavior of nickel based oxide dispersion strengthened (ODS) alloys. For both models the rupture time is taken as the time for a transverse grain boundary to cavitate fully. A diffusive cavity growth law is assumed to govern cavitation. The applicability of the respective models is determined by the particular grain morphology achieved by thermal-mechanical processing. The first model assumes that longitudinal grain boundaries are unable to slide; hence displacements due to cavitation must be matched by displacements due to dislocation creep in adjoining grains. This model predicts a low stress exponent at the transition from single crystal to cavitation creep behavior, and higher stress exponents at stresses below this transition. Good agreement is found between the model predictions and creep data for MA 754 at 1000 and 1093 °C. A second model considers a grain morphology wherein longitudinal grain boundaries are able to slide by means of deformation of pockets of fine grains. Cavitation of transverse grain boundaries is thus controlled by grain boundary sliding. This model predicts a stress exponent of 1 at low stresses, and serves as an upper bound for the creep rate when a duplex grain morphology is present. Model predictions are in good agreement with creep data for a heat of MA 754 with a duplex grain morphology.

  8. Creep Properties and Deformation Mechanisms of a FGH95 Ni-based Superalloy

    NASA Astrophysics Data System (ADS)

    Xie, Jun; Tian, Su-gui; Zhou, Xiao-ming

    2013-07-01

    By means of full heat treatment, microstructure observation, lattice parameters determination, and the measurement of creep curves, an investigation has been conducted into the microstructure and creep mechanisms of FGH95 Ni-based superalloy. Results show that after the alloy is hot isostatically pressed, coarse ?' phase discontinuously distributes along the previous particle boundaries. After solution treatment at high temperature and aging, the grain size has no obvious change, and the amount of coarse ?' phase decreases, and a high volume fraction of fine ?' phase dispersedly precipitates in the ? matrix. Moreover, the granular carbides are found to be precipitated along grain boundaries, which can hinder the grain boundaries' sliding and enhance the creep resistance of the alloy. By x-ray diffraction analysis, it is indicated that the lattice misfit between the ? and ?' phases decreases in the alloy after full heat treatment. In the ranges of experimental temperatures and applied stresses, the creep activation energy of the alloy is measured to be 630.4 kJ/mol. During creep, the deformation mechanisms of the alloy are that dislocations slip in the ? matrix or shear into the ?' phase. Thereinto, the creep dislocations move over the ?' phase by the Orowan mechanism, and the < { 1 10 } rangle super-dislocation shearing into the ?' phase can be decomposed to form the configuration of (1/3) < { 1 12 } rangle super-Shockleys' partials and the stacking fault.

  9. Microstructures of beta silicon carbide after irradiation creep deformation at elevated temperatures

    SciTech Connect

    Katoh, Yutai; Kondo, Sosuke; Snead, Lance Lewis

    2008-01-01

    Microstructures of silicon carbide were examined by transmission electron microscopy (TEM) after creep deformation under neutron irradiation. Thin strip specimens of polycrystalline and monocrystalline, chemically vapor-deposited, beta-phase silicon carbide were irradiated in the high flux isotope reactor to 0.7-4.2 dpa at nominal temperatures of 640-1080 C in an elastically pre-strained bend stress relaxation configuration with the initial stress of {approx}100 MPa. Irradiation creep caused permanent strains of 0.6 to 2.3 x 10{sup -4}. Tensile-loaded near-surface portions of the crept specimens were examined by TEM. The main microstructural features observed were dislocation loops in all samples, and appeared similar to those observed in samples irradiated in non-stressed conditions. Slight but statistically significant anisotropy in dislocation loop microstructure was observed in one irradiation condition, and accounted for at least a fraction of the creep strain derived from the stress relaxation. The estimated total volume of loops accounted for 10-45% of the estimated total swelling. The results imply that the early irradiation creep deformation of SiC observed in this work was driven by anisotropic evolutions of extrinsic dislocation loops and matrix defects with undetectable sizes.

  10. A microstructural study of creep and thermal fatigue deformation in 60Sn-40Pb solder joints

    SciTech Connect

    Tribula, D.

    1990-06-02

    Thermal fatigue failures of solder joints in electronic devices often arise from cyclic shear strains imposed by the mismatched thermal expansion coefficients of the materials that bind the joint as temperature changes are encountered. Increased solder joint reliability demands a fundamental understanding of the metallurigical mechanisms that control the fatigue to design accurate accelerated probative tests and new, more fatigue resistant solder alloys. The high temperatures and slow strain rates that pertain to thermal fatigue imply that creep is an important deformation mode in the thermal fatigue cycle. In this work, the creep behaviour of a solder joint is studied to determine the solder's microstructural response to this type of deformation and to relate this to the more complex problem of thermal fatigue. It is shown that creep failures arise from the inherent inhomogeneity and instability of the solder microstructure and suggest that small compositional changes of the binary near-eutectic Pn-Sn alloy may defeat the observed failure mechanisms. This work presents creep and thermal fatigue data for several near-eutectic Pb-Sn solder compositions and concludes that a 58Sn-40Pb-2In and a 58Sn-40Pb-2Cd alloy show significantly enhanced fatigue resistance over that of the simple binary material. 80 refs., 33 figs., 1 tab.

  11. Elevated temperature flow strength, creep resistance and diffusion welding characteristics of Ti-6Al-2Nb-1Ta-0.8Mo

    NASA Technical Reports Server (NTRS)

    Whittenberger, J. D.; Moore, T. J.

    1979-01-01

    A study of the flow strength, creep resistance and diffusion welding characteristics of the titanium alloy Ti-6Al-2Nb-1Ta-0.8Mo has been conducted. Two mill-processed forms of this alloy were examined. The forged material had been processed above the beta transus (approximately 1275 K) while the rolled form had been subjected to work below the beta transus. Between 1150 and 1250 K, the forged material was stronger and more creep resistant than the rolled alloy. Both forms exhibit superplastic characteristics in this temperature range. Strain measurements during diffusion welding experiments at 1200 K reveal that weld interfaces have no measurable effect on the overall creep deformation. Significant deformation appears to be necessary to produce a quality diffusion weld between superplastic materials. A 'soft' interlayer inserted between faying surfaces would seemingly allow manufacture of quality diffusion welds with little overall deformation.

  12. Elevated-temperature flow strength, creep resistance and diffusion welding characteristics of Ti-gAl-2Nb-1Ta-0.8Mo

    NASA Technical Reports Server (NTRS)

    Whittenberger, J. D.; Moore, T. J.

    1977-01-01

    A study of the flow strength, creep resistance and diffusion welding characteristics of the titanium alloy Ti-6Al-2Nb-1Ta-0.8Mo was conducted. Two mill-processed forms of this alloy were examined. The forged material was essentially processed above the beta transus while the rolled form was subjected to considerable work below the beta transus. Between 1150 and 1250 K, the forged material was stronger and more creep resistant than the rolled alloy. Both forms exhibit superplastic characteristics in this temperature range. Strain measurements during diffusion welding experiments at 1200 K reveal that weld interfaces have no measurable effect on the overall creep deformation. Significant deformation appears to be necessary to produce a quality diffusion weld between superplastic materials. A 'soft' interlayer inserted between faying surfaces would seemingly allow manufacture of quality diffusion welds with little overall deformation.

  13. Fatigue and Creep-Fatigue Deformation of an Ultra-Fine Precipitate Strengthened Advanced Austenitic Alloy

    SciTech Connect

    M.C. Carroll; L.J. Carroll

    2012-10-01

    An advanced austenitic alloy, HT-UPS (high-temperature ultrafine-precipitation-strengthened), has been identified as an ideal candidate material for the structural components of fast reactors and energy-conversion systems. HT-UPS alloys demonstrate improved creep resistance relative to 316 stainless steel (SS) through additions of Ti and Nb, which precipitate to form a widespread dispersion of stable nanoscale metallic carbide (MC) particles in the austenitic matrix. The low-cycle fatigue and creep-fatigue behavior of an HT-UPS alloy have been investigated at 650 C and a 1.0% total strain, with an R-ratio of -1 and hold times at peak tensile strain as long as 150 min. The cyclic deformation response of HT-UPS is directly compared to that of standard 316 SS. The measured values for total cycles to failure are similar, despite differences in peak stress profiles and in qualitative observations of the deformed microstructures. Crack propagation is primarily transgranular in fatigue and creep-fatigue of both alloys at the investigated conditions. Internal grain boundary damage in the form of fine cracks resulting from the tensile hold is present for hold times of 60 min and longer, and substantially more internal cracks are quantifiable in 316 SS than in HT-UPS. The dislocation substructures observed in the deformed material differ significantly; an equiaxed cellular structure is observed in 316 SS, whereas in HT-UPS the microstructure takes the form of widespread and relatively homogenous tangles of dislocations pinned by the nanoscale MC precipitates. The significant effect of the fine distribution of precipitates on observed fatigue and creep-fatigue response is described in three distinct behavioral regions as it evolves with continued cycling.

  14. Understanding creep in sandstone reservoirs - theoretical deformation mechanism maps for pressure solution in granular materials

    NASA Astrophysics Data System (ADS)

    Hangx, Suzanne; Spiers, Christopher

    2014-05-01

    Subsurface exploitation of the Earth's natural resources removes the natural system from its chemical and physical equilibrium. As such, groundwater extraction and hydrocarbon production from subsurface reservoirs frequently causes surface subsidence and induces (micro)seismicity. These effects are not only a problem in onshore (e.g. Groningen, the Netherlands) and offshore hydrocarbon fields (e.g. Ekofisk, Norway), but also in urban areas with extensive groundwater pumping (e.g. Venice, Italy). It is known that fluid extraction inevitably leads to (poro)elastic compaction of reservoirs, hence subsidence and occasional fault reactivation, and causes significant technical, economic and ecological impact. However, such effects often exceed what is expected from purely elastic reservoir behaviour and may continue long after exploitation has ceased. This is most likely due to time-dependent compaction, or 'creep deformation', of such reservoirs, driven by the reduction in pore fluid pressure compared with the rock overburden. Given the societal and ecological impact of surface subsidence, as well as the current interest in developing geothermal energy and unconventional gas resources in densely populated areas, there is much need for obtaining better quantitative understanding of creep in sediments to improve the predictability of the impact of geo-energy and groundwater production. The key problem in developing a reliable, quantitative description of the creep behaviour of sediments, such as sands and sandstones, is that the operative deformation mechanisms are poorly known and poorly quantified. While grain-scale brittle fracturing plus intergranular sliding play an important role in the early stages of compaction, these time-independent, brittle-frictional processes give way to compaction creep on longer time-scales. Thermally-activated mass transfer processes, like pressure solution, can cause creep via dissolution of material at stressed grain contacts, grain-boundary diffusion and precipitation on pore walls. As a first step to better describe creep in sands and sandstones, we have derived a simple model for intergranular pressure solution (IPS) within an ordered pack of spherical grains, employing existing IPS rate models, such as those derived by Renard et al. (1999) and Spiers et al. (2004). This universal model is able to predict the conditions under which each of the respective pressure solution serial processes, i.e. diffusion, precipitation or dissolution, is dominant. In essence, this creates generic deformation mechanism maps for any granular material. We have used our model to predict the amount and rate of compaction for sandstone reservoirs, and compared our predictions to known subsidence rates for reservoirs around the world. This gives a first order-comparison to verify whether or not IPS is an important mechanism in controlling reservoir compaction.

  15. Cell structure in cold worked and creep deformed phosphorus alloyed copper

    SciTech Connect

    Wu, Rui; Pettersson, Niklas; Martinsson, Åsa; Sandström, Rolf

    2014-04-01

    Transmission electron microscopy (TEM) examinations on as-received, cold worked, as well as cold worked and creep tested phosphorus-alloyed oxygen-free copper (Cu-OFP) have been carried out to study the role of the cell structure. The cell size decreased linearly with increasing plastic deformation in tension. The flow stress in the tests could also be correlated to the cell size. The observed relation between the flow stress and the cell size was in excellent agreement with previously published results. The dense dislocation walls that appeared after cold work in tension is likely to be the main reason for the dramatic increase in creep strength. The dense dislocation walls act as barriers against dislocation motion and their presence also reduces the recovery rate due to an unbalanced dislocation content.

  16. Pressure sintering and creep deformation: a joint modeling approach. Final report

    SciTech Connect

    Notis, M.R.

    1983-01-01

    Goal was to understand the mechanisms and microstructure affecting hot-pressing and creep processes. CoO was hot-pressed to different porosity levels and densification maps drawn. Creep experiments were carried out on pure CoO. Dislocation structure of deformed CoO was studied. Grain growth rates in CoO changes from a square dependence with time to a cubic dependence as porosity drops below 2 to 3%. Pores tend to remain on grain boundaries during both final and intermediate-stage densification. A wide variety of ceramics were examined for segregation of impurities: NiO-MgO, NiO-Cr/sub 2/O/sub 3/, NiO-TiO/sub 2/, Ni-Al/sub 2/O/sub 3/. Precipitation processes are being studied in NiO-Cr/sub 2/O/sub 3/ and in magnesium aluminate spinel.

  17. Analysis of Mining Terrain Deformation Characteristics with Deformation Information System

    NASA Astrophysics Data System (ADS)

    Blachowski, Jan; Milczarek, Wojciech; Grzempowski, Piotr

    2014-05-01

    Mapping and prediction of mining related deformations of the earth surface is an important measure for minimising threat to surface infrastructure, human population, the environment and safety of the mining operation itself arising from underground extraction of useful minerals. The number of methods and techniques used for monitoring and analysis of mining terrain deformations is wide and increasing with the development of geographical information technologies. These include for example: terrestrial geodetic measurements, global positioning systems, remote sensing, spatial interpolation, finite element method modelling, GIS based modelling, geological modelling, empirical modelling using the Knothe theory, artificial neural networks, fuzzy logic calculations and other. The aim of this paper is to introduce the concept of an integrated Deformation Information System (DIS) developed in geographic information systems environment for analysis and modelling of various spatial data related to mining activity and demonstrate its applications for mapping and visualising, as well as identifying possible mining terrain deformation areas with various spatial modelling methods. The DIS concept is based on connected modules that include: the spatial database - the core of the system, the spatial data collection module formed by: terrestrial, satellite and remote sensing measurements of the ground changes, the spatial data mining module for data discovery and extraction, the geological modelling module, the spatial data modeling module with data processing algorithms for spatio-temporal analysis and mapping of mining deformations and their characteristics (e.g. deformation parameters: tilt, curvature and horizontal strain), the multivariate spatial data classification module and the visualization module allowing two-dimensional interactive and static mapping and three-dimensional visualizations of mining ground characteristics. The Systems's functionality has been presented on the case study of a coal mining region in SW Poland where it has been applied to study characteristics and map mining induced ground deformations in a city in the last two decades of underground coal extraction and in the first decade after the end of mining. The mining subsidence area and its deformation parameters (tilt and curvature) have been calculated and the latter classified and mapped according to the Polish regulations. In addition possible areas of ground deformation have been indicated based on multivariate spatial data analysis of geological and mining operation characteristics with the geographically weighted regression method.

  18. An experimental and theoretical investigation of the low temperature creep deformation behavior of single phase titanium alloys

    NASA Astrophysics Data System (ADS)

    Oberson, P. Gregory

    Titanium alloys are used for many applications due to their desirable properties, including its high strength-to-weight ratio, corrosion resistance, and biocompatibility. Titanium alloys are used extensively for aerospace, chemical, nuclear, industrial, biomedical, and consumer applications. In many applications, titanium components may be subject to stresses for extended periods of time. It has long been known that single-phase hexagonally close-packed (HCP) alpha and body-centered cubic (BCC) beta titanium alloys deform over time, or creep, at low temperatures (<0.25*Tm). As such, creep is an important factor to consider when assessing the structural reliability of titanium components. However, the factors that affect creep behavior such as grain size and alloy chemistry and the deformation mechanisms associated with creep such as slip and twinning are not well understood. The aim of this investigation is to experimentally and theoretically study the creep deformation behavior of single-phase alpha and beta titanium alloys. The first part of the investigation concerns alpha-Ti alloys. The low temperature creep behavior was studied experimentally, using alpha-Ti-1.6wt.%V as the model alloy. Creep testing was performed at a range of temperatures and slip and twinning were identified as creep deformation mechanisms by optical, SEM and TEM microscopy. The activation energy for creep was measured for the first time for an alpha-Ti than deforms by twinning. The activation energy was found to increase as a function of creep strain, suggesting that there is a change in the predominant deformation mechanism from slip at low strain to twinning at high strain. The reason for this change is explained by a model for twin nucleation caused by dislocation pileups. The theoretical aspect of the study of alpha-Ti, concerns the phenomenon of slow twin growth (time-dependent twinning) during low temperature creep. This phenomenon is unusual and poorly understood as twins in bulk, polycrystalline metals are expected to grow very fast. It was suggested that interstitial atoms, particularly oxygen could be responsible for time-dependent twinning but there were no models to explain this. As such, crystallographic models were developed for the HCP-lattice of alpha-Ti to show how the octahedral interstitial sites where atoms such as oxygen can reside are eliminated by the atomic movements associated with twinning. As such, the rate of twin growth, and in turn the creep strain rate is controlled by the diffusion of oxygen away from these eliminated sites. The second part of the investigation builds on experimental work from a previous investigation to extend the theoretical model for time-dependent twinning to the BCC lattice of beta-Ti. Similar to the case for alpha-Ti alloys, twin growth is rate limited by the diffusion of oxygen atoms away from eliminated interstitial sites. The results of these findings are very valuable when designing Ti alloys for improved creep resistance and mechanical reliability. This is critical because creep can directly alter dimensional tolerances and creep deformation products can contribute to crack nucleation leading to catastrophic failure. This work was supported by the National Science Foundation under Grant Number DMR-0513751.

  19. Stiffness and damping characteristics of aluminum in creep

    NASA Technical Reports Server (NTRS)

    Berkovits, A.

    1977-01-01

    Tensile creep tests conducted at 200 C were performed on annealed commercially pure aluminum specimens in order to measure the dominant elevated temperature dislocation processes. Testing consisted of applying small lateral loads to measure flexural stiffness, and vibrating the specimens laterally in order to measure dynamic modulus and internal damping. It was concluded that (1) the strain hardening increased static stiffness and decreased internal damping during early creep, and (2) the dynamic modulus remained essentially constant at the elastic value during creep. These results imply that primary creep may constitute a mechanism of recovery of dislocatory disorder induced by yielding the material during loading, and that the inelastic modulus utilized as a mathematical concept in several creep buckling theories is not a directly measurable material property.

  20. Creep deformation and rupture behavior of CLAM steel at 823 K and 873 K

    NASA Astrophysics Data System (ADS)

    Zhong, Boyu; Huang, Bo; Li, Chunjing; Liu, Shaojun; Xu, Gang; Zhao, Yanyun; Huang, Qunying

    2014-12-01

    China Low Activation Martensitic (CLAM) steel is selected as the candidate structural material in Fusion Design Study (FDS) series fusion reactor conceptual designs. The creep property of CLAM steel has been studied in this paper. Creep tests have been carried out at 823 K and 873 K over a stress range of 150-230 MPa. The creep curves showed three creep regimes, primary creep, steady-state creep and tertiary creep. The relationship between minimum creep rate (ε˙min) and the applied stress (σ) could be described by Norton power law, and the stress exponent n was decreased with the increase of the creep temperature. The creep mechanism was analyzed with the fractographes of the rupture specimens which were examined by scanning electron microscopy (SEM). The coarsening of precipitates observed with transmission electron microscope (TEM) indicated the microstructural degradation after creep test.

  1. Dynamic Deformation Characteristics of Sedimentary Soft Rock

    NASA Astrophysics Data System (ADS)

    Fukumoto, Shun'ichi; Yoshida, Nozomu; Sahara, Mamoru

    Soil under the engineering seismic base layer is treated as elastic material in the engineering practice, however, evidence that its nonlinear behavior affects surface response begins to appear. Test data on dynamic deformation characteristics and tri-axial compression test on sedimentary soft rock are collected and compiled to consider its nonlinearity. In addition, nonlinear characteristics of soft rock and note on practical use are described. Static tri-axial compression test of the sample taken by means of diamond core drill is first carried out by using a LDT (Local deformation transducer), and shear modulus is found to keep nearly constant up to strain of about 10-3 for the undisturbed sample, whereas that decreases significantly even at strain of 10-5. Secondly, dynamic deformation test data on Pleistocene and Tertiary soft rock with SPT-N value greater than 30 or shear wave velocity greater than 300 m/s is collected and compiled. It is found that there exist data that shows similar behavior of static test described in the preceding. These samples is supposed be undisturbed, which means there exists many disturbed samples even if they are retrieved by, so called, undisturbed sampling method. Shear modulus at shear strain of 10-3, which is used as index of nonlinearity, is independent from effective confining stress, but it has positive correlation with plastic index. Finally, dynamic deformation characteristics of undisturbed samples are shown to be modeled by Ramberg-Osgood model well.

  2. Characteristics of irradiation creep in the first wall of a fusion reactor

    SciTech Connect

    Coghlan, W.A.; Mansur, L.K.

    1981-01-01

    A number of significant differences in the irradiation environment of a fusion reactor are expected with respect to the fission reactor irradiation environment. These differences are expected to affect the characteristics of irradiation creep in the fusion reactor. Special conditions of importance are identified as the (1) large number of defects produced per pka, (2) high helium production rate, (3) cyclic operation, (4) unique stress histories, and (5) low temperature operations. Existing experimental data from the fission reactor environment is analyzed to shed light on irradiation creep under fusion conditions. Theoretical considerations are used to deduce additional characteristics of irradiation creep in the fusion reactor environment for which no experimental data are available.

  3. Creep mechanisms and interface-enhanced deformation twinning in a two-phase lamellar TiAl alloy

    SciTech Connect

    Hsiung, L.M., LLNL

    1997-03-01

    Deformation mechanisms and the role of interfaces in deformation twinning of a two-phase [TiAl({gamma})/Ti{sub 3}Al({alpha}{sub 2})] lamellar alloy creep deformed at elevated temperatures have been investigated. Since the multiplication of lattice dislocations within both {gamma} and {alpha}{sub 2} lamellae is very limited at a low stress level due to a refined lamellar microstructure, the glide of interfacial dislocations on both {gamma}/{alpha}{sub 2} and {gamma}/{gamma} interfaces (i.e interface sliding) becomes an important deformation mode. Obstacles such as impinged lattice dislocations can impede the movement of interfacial dislocations, which glide in a cooperative fashion along the lamellar interfaces. The impediment of dislocation motion subsequently causes a dislocation pile-up in front of obstacles as creep strain accumulates. When the crystals deform at high stress level, deformation twinning becomes a predominant deformation mode. Deformation twins are found to nucleate from the interfaces as a result of a local stress concentration generated from dislocation pile-ups. It is suggested that the deformation twinning in lamellar TiAl/Ti{sub 3}Al crystals can be vieived as a stress relaxation process for the concentration of stress at the head of each dislocation pile-up. An interface-assisted twinning mechanism is accordingly proposed and discussed.

  4. Dislocation creep accommodated Grain Boundary Sliding: A high strain rate/low temperature deformation mechanism in calcite ultramylonites

    NASA Astrophysics Data System (ADS)

    Rogowitz, Anna; Grasemann, Bernhard

    2014-05-01

    Grain boundary sliding (GBS) is an important grain size sensitive deformation mechanism that is often associated with extreme strain localization and superplasticity. Another mechanism has to operate simultaneously to GBS in order to prevent overlaps and voids between sliding grains. One of the most common accommodating mechanisms is diffusional creep but, recently, dislocation creep has been reported to operate simultaneous to GBS. Due to the formation of a flanking structure in nearly pure calcite marble on Syros (Cyclades, Greece) at lower greenschist facies conditions, an extremely fine grained ultramylonite developed. The microstructure of the layer is characterized by (1) calcite grains with an average grain size of 3.6 m (developed by low temperature/high strain rate grain boundary migration recrystallization, BLG), (2) grain boundary triple junctions with nearly 120 angles and (3) small cavities preferentially located at triple junctions and at grain boundaries in extension. These features suggest that the dominant deformation mechanism was GBS. In order to get more information on the accommodation mechanism detailed microstructural and textural analyses have been performed on a FEI Quanta 3D FEG instrument equipped with an EDAX Digiview IV EBSD camera. The misorientation distribution curves for correlated and uncorrelated grains follow almost perfect the calculated theoretical curve for a random distribution, which is typical for polycrystalline material deformed by GBS. However, the crystallographic preferred orientation indicates that dislocation creep might have operated simultaneously. We also report Zener-Stroh cracks resulting from dislocation pile up, indicating that dislocation movement was active. We, therefore, conclude that the dominant deformation mechanism was dislocation creep accommodated grain boundary sliding. This is consistent with the observed grain size range that plots at the field boundary between grain size insensitive and grain size sensitive creep, in a deformation mechanism map for calcite.

  5. Quantitative analysis of microstructure deformation in creep fenomena of ferritic SA-213 T22 and austenitic SA-213 TP304H material

    NASA Astrophysics Data System (ADS)

    Mulyana, Cukup; Taufik, Ahmad; Gunawan, Agus Yodi; Siregar, Rustam Efendi

    2013-09-01

    The failure of critical component of fossil fired power plant that operated in creep range (high stress, high temperature and in the long term) depends on its microstructure characteristics. Ferritic low carbon steel (2.25Cr-1Mo) and Austenitic stainless alloy (18Cr-8Ni) are used as a boiler tube in the secondary superheater outlet header to deliver steam before entering the turbin. The tube failure is occurred in a form of rupture, resulting trip that disrupts the continuity of the electrical generation. The research in quantification of the microstructure deformation has been done in predicting the remaining life of the tube through interrupted accelerated creep test. For Austenitic Stainless Alloy (18Cr-8Ni), creep test was done in 550°C with the stress 424.5 MPa and for Ferritic Low Carbon Steel (2.25Cr-1Mo) in 570°C with the stress 189 MPa. The interrupted accelerated creep test was done by stopping the observation in condition 60%, 70%, 80% and 90% of remaining life, the creep test fracture was done before. Then the micro hardness test, photo micro, SEM and EDS were obtained from those samples. Refer to ASTM E122, microstructure parameters were calculated. The results indicated that there are a consistency of decreasing their grain diameters, increasing their grain size numbers, micro hardness, and the length of crack or void number per unit area with the decreasing of remaining life. While morphology of grain (stated in parameter α=LV/LH) relatively constant for austenitic. However, for ferritic the change of morphology revealed significantly. Fracture mode propagation of ferritic material is growth with voids transgranular and intergranular crack, and for austenitic material the fracture growth with intergranular creep fracture void and wedge crack. In this research, it was proposed a formulation of mathematical model for creep behavior corresponding their curve fitting resulted for the primary, secondary and tertiary in accelerated creep test. In addition, it was also developed a new method for predicting the remaining life using quantification of microstructure and using expansion of parameter Larson Miller from Taylor series for critical component in high temperature in industry. It was found that the proposed method was easier to be applied in field with the results more accurate then Larson Miller Method.

  6. The knes rockslide: Characteristics of subsurface deformation

    NASA Astrophysics Data System (ADS)

    Blikra, Lars; Lovisolo, Mario; Kristensen, Lene

    2010-05-01

    The knes rockslide represents a possible collapse of 20-55 million cubic metres, moving with a velocity of up to 10 cm/year. The risk is associated with the generation of catastrophic tsunamis, having run-up potential of up to 80 m in nearby villages. The surface monitoring systems is today based on extensometers/crackmeters, tiltmeters, single lasers, GPS, total station and a microseismic network, in addition to a climate station. Large efforts have been paid to the establishment of subsurface investigations and monitoring systems in deep boreholes. Tree boreholes have been instrumented with 50 to 120 m long active multiparametric in place columns (DMS system: Differential Monitoring of Stability). The system consists of 1 m long modules connected by special flexible junctions being free to move. Each module contains of a biaxial inclinometric sensor, a temperature sensor, and selected modules have a piezometric sensor. Also digital compass is emplaced in specific modules for controlling the direction of column. Measurements are continuous and are automatically downloaded. The DMS data has documented a well-defined upper sliding zone in two boreholes at depth of 35 and 50 m depth. This is above the water-level measured in open standpipes. The video inspection before instrumentation and the core data shows distinct fracture zones in this upper part, in addition to water inflow at some parts. The continuous temperature data from the DMS columns can also be used to measure the inflow of water through time, by the fact that the flow of water influences the temperatures. The deformation data also show that there are creeping movements in lower part, down to below 120 m depth. The mode of deformation is varying from continuous displacements through time to suddenly and abrupt steps in movement rates. Also, it is possible to detect a series of different displacements rates during small time windows. For examples, in the upper borehole, the movement velocity at 49-51 m depth beginning from November 2009 to middle of January 2010 depicts 3 velocity trends. This range from 0,1 mm/day the first month, decreasing to 0,05 mm/day the next month, and finally reducing to 0,02 mm/day the last half month. This velocity change seems to correlate broadly with the decreasing water level during the transition from relative wet autumn to colder winter conditions.

  7. Creep deformation and fracture behavior of types 316 and 316L(N) stainless steels and their weld metals

    NASA Astrophysics Data System (ADS)

    Sasikala, G.; Mannan, S. L.; Mathew, M. D.; Rao, K. Bhanu

    2000-04-01

    The creep properties of a nuclear-grade type 316(L) stainless steel (SS) alloyed with nitrogen (316L(N) SS) and its weld metal were studied at 873 and 923 K in the range of applied stresses from 100 to 335 MPa. The results were compared with those obtained on a nuclear-grade type 316 SS, which is lean in nitrogen. The creep rupture lives of the weld metals were found to be lower than those of the respective base metals by a factor of 5 to 10. Both the base and weld metals of 316L(N) SS exhibited better resistance to creep deformation compared to their 316 SS counterparts at identical test conditions. A power-law relationship between the minimum creep rate and applied stress was found to be obeyed for both the base and weld metals. Both the weld metals generally exhibited lower rupture elongation than the respective base metals; however, at 873 K, the 316 SS base and weld metals had similar rupture elongation at identical applied stresses. Comparison of the rupture lives of the two steels to the ASME curves for the expected minimum stress to rupture for 316 SS base and weld metals showed that, for 316L(N) SS, the specifications for maximum allowable stresses based on data for 316 SS could prove overconservative. The influence of nitrogen on the creep deformation and fracture behavior, especially in terms of its modifying the precipitation kinetics, is discussed in light of the microstructural observations. In welds containing ? ferrite, the kinetics of its transformation and the nature of the transformation products control the deformation and fracture behavior. The influence of nitrogen on the ? ferrite transformation behavior and coarsening kinetics is also discussed, on the basis of extensive characterization by metallographic techniques.

  8. The sliding mode control for different shapes and dimensions of IPMC on resisting its creep characteristics

    NASA Astrophysics Data System (ADS)

    Hao, Lina; Chen, Yang; Sun, Zhiyong

    2015-04-01

    Ionic polymer metal composite (IPMC) is a novel smart material which has been widely implemented in MEMS, biomimetic mechanical and electrical integrated system and micro operation system. While the IPMC with different shapes and dimensions has been implemented in many different types of biomechanical integrated systems, one of its inherent properties called creep characteristic is difficult to be handled, which limits the further application of different IPMCs in integrated systems. A promising control method called sliding mode control (SMC) is proposed to resist the creep characteristics in this paper. The SMC controller can regulate IPMC actuators with different shapes and dimensions effectively to resist the creep characteristics without changing parameters of the control system. Experiments of four different types of IPMC actuators were conducted on the semi-physical SMC experimental platform. All the experimental results confirm the feasibility of the SMC control approach on regulating the multi-IPMCs with different shapes and dimensions based integrated system.

  9. Creeping Deformation by the Precise Leveling Survey at the central part of the Longitudinal valley fault, Southeast Taiwan

    NASA Astrophysics Data System (ADS)

    Matta, N.; Murase, M.; Ishiguro, S.; Ozawa, K.; Lin, J.; Chen, W.; Lin, C.

    2011-12-01

    We would like to know the distributed asperity for seismic hazard and forecast. It is closely related to slip distribution on the fault in interseismic. We focused on the accumulating process of the stress at the boundary between the creeping and the locking zone, to clear the behavior on the fault. The Longitudinal Valley Fault (LVF), 150 km long and NNE-SSW striking, passes through the eastern Taiwan, and represents the obvious surface expression of the collision boundary between the Philippine Sea plate and the Eurasian continental plate. Owing to such a high deformation rate, many earthquakes have occurred along the LVF. The 1951 earthquake sequence represents a good example. The southern of LVF segment is observed to be high speed creeping based on the creep meter and leveling survey etc. The northern of LVF segment is not observed to be creeping and are found huge earthquakes evidence by paleo-seismology study in the trench. Yuili fault is one of the active segments of the longitudinal valley faults, is located around the boundary between creeping and locking area. It is reverse fault with east dip. We established about 30km leveling route from Yuli to Changbin to detect the vertical deformation in detail. Murase et al. (2009, 2010, and 2011) established about 30 km densely leveling route from Yuli to Changbin to detect the vertical deformation across the LVF for two years. As a result, the vertical displacement is 1.7 cm in 200 m across the LVF and 2.7 cm in 1000 m, referred to the west end of our route. In addition, a synclinal deformation is detected on the hanging wall side of the fault. This result is caused by the geometry of and the slipping distribution on the fault. The deformation detected in the period from 2009 to 2010 denotes the same tendency and rate of that from 2008 to 2009. We compared to the airphotographs which are taken by Taiwanese government at different age (1978 and 2007). If the creeping on the fault has continued for 30 years, the accumulation of displacement reaches about 1m, which is significantly-distinguishable by photogrammetric method. We measure profiles across the fault on 1978 and 2007 air-photograph by photogrammetric system respectively. The comparing result is shown that there are regional differences in deformation in relatively narrow region. About this result, we think two possibility; one is the creeping is not uniformity along the fault, second is the photogrammetry is not enough quality. We should actually check the creeping or not. We made thee new leveling survey lines in last year. In this August , we carried out second leveling survey in three area. We can show the variation of the deformation pattern and uplift rate across the LVF in this presentation.

  10. The effect of environment on the creep deformation of ultra-high purity nickel-chromium-iron alloys at 360 degrees Celcius

    NASA Astrophysics Data System (ADS)

    Paraventi, Denise Jean

    2000-10-01

    Steam generators in pressurized water nuclear power plants have experienced significant problems with intergranular stress corrosion cracking (IGSCC) on the inner diameter of steam generator tubing for over 25 years. In the course of research to understand IGSCC, it has been shown that creep deformation may play a significant role in the cracking of commercial Alloy 600 (Ni-16Cr-9Fe-0.03C). The primary water environment can cause decreases in creep resistance (i.e., faster creep rates, shorter time to failure, and higher creep strains). During corrosion under the conditions of interest, both hydrogen reduction and metal dissolution occur. One or both may contribute to the enhancement of creep. The purpose of this work was to isolate the mechanism by which the water environment causes the creep deformation to increase. Activation area and activation enthalpy for glide were measured in argon and primary water on high purity Ni-16Cr-9Fe alloys. The results indicated that the activation area was reduced by primary water, consistent with a hydrogen enhanced plasticity mechanism for enhanced creep. The stress dependence of creep was also examined in argon and primary water. The results indicated that the internal stress of the alloy is reduced by the primary water environment. Lower internal stress is consistent with both a hydrogen model as well as a vacancy-aided climb model for enhanced creep. To isolate the effect of hydrogen on the creep of the alloy, experiments were conducted in a dissociated hydrogen environment. The results indicated that hydrogen would only increase the steady state creep rate if present before loading of the samples. However, if the sample was already in steady state creep and hydrogen introduced, a transient in the creep strain was observed. The creep rate returned to the original steady state rate in a short time. The results indicate that while hydrogen does affect the steady state creep to an extent, hydrogen cannot completely account for the increase in creep rate observed in primary water. Also, the presence of the aggressive environment before loading appears to be required to increase the creep rate, indicating that the effect of environment may be significant in the primary creep regime.

  11. Effects of cold rolling deformation on microstructure, hardness, and creep behavior of high nitrogen austenitic stainless steel

    NASA Astrophysics Data System (ADS)

    Sun, Shi-Cheng; Sun, Gui-Xun; Jiang, Zhong-Hao; Ji, Chang-Tao; Liu, Jia-An; Lian, Jian-She

    2014-02-01

    Effects of cold rolling deformation on the microstructure, hardness, and creep behavior of high nitrogen austenitic stainless steel (HNASS) are investigated. Microstructure characterization shows that 70% cold rolling deformation results in significant refinement of the microstructure of this steel, with its average twin thickness reducing from 6.4 ?m to 14 nm. Nanoindentation tests at different strain rates demonstrate that the hardness of the steel with nano-scale twins (nt-HNASS) is about 2 times as high as that of steel with micro-scale twins (mt-HNASS). The hardness of nt-HNASS exhibits a pronounced strain rate dependence with a strain rate sensitivity (m value) of 0.0319, which is far higher than that of mt-HNASS (m = 0.0029). nt-HNASS shows more significant load plateaus and a higher creep rate than mt-HNASS. Analysis reveals that higher hardness and larger m value of nt-HNASS arise from stronger strain hardening role, which is caused by the higher storage rate of dislocations and the interactions between dislocations and high density twins. The more significant load plateaus and higher creep rates of nt-HNASS are due to the rapid relaxation of the dislocation structures generated during loading.

  12. Elevated Temperature Creep Deformation in Solid Solution <001> NiAL-3.6Ti Single Crystals

    NASA Technical Reports Server (NTRS)

    Whittenberger, J. Daniel; Noebe, Ronald D.; Darolia, Ram

    2003-01-01

    The 1100 to 1500 K slow plastic strain rate compressive properties of <001> oriented NiAl-3.6Ti single crystals have been measured, and the results suggests that two deformation processes exist. While the intermediate temperature/faster strain rate mechanism is uncertain, plastic flow at elevated temperature/slower strain rates in NiAl-3.6Ti appears to be controlled by solute drag as described by the Cottrell-Jaswon solute drag model for gliding b = a(sub 0)<101> dislocations. While the calculated activation energy of deformation is much higher (approximately 480 kJ/mol) than the activation energy for diffusion (approximately 290 kJ/mol) used in the Cottrell-Jaswon creep model, a forced temperature compensated - power law fit using the activation energy for diffusion was able to adequately (greater than 90%) predict the observed creep properties. Thus we conclude that the rejection of a diffusion controlled mechanism can not be simply based on a large numerical difference between the activation energies for deformation and diffusion.

  13. The high temperature creep deformation of Si3N4-6Y2O3-2Al2O3

    NASA Technical Reports Server (NTRS)

    Todd, J. A.; Xu, Zhi-Yue

    1988-01-01

    The creep properties of silicon nitride containing 6 wt percent yttria and 2 wt percent alumina have been determined in the temperature range 1573 to 1673 K. The stress exponent, n, in the equation epsilon dot varies as sigma sup n, was determined to be 2.00 + or - 0.15 and the true activation energy was found to be 692 + or - 25 kJ/mol. Transmission electron microscopy studies showed that deformation occurred in the grain boundary glassy phase accompanied by microcrack formation and cavitation. The steady state creep results are consistent with a diffusion controlled creep mechanism involving nitrogen diffusion through the grain boundary glassy phase.

  14. The high temperature creep deformation of Si3N4-6Y2O3-2Al2O3

    NASA Technical Reports Server (NTRS)

    Todd, J. A.; Xu, Zhi-Yue

    1989-01-01

    The creep properties of silicon nitride containing 6 wt percent yttria and 2 wt percent alumina have been determined in the temperature range 1573 to 1673 K. The stress exponent, n, in the equation epsilon dot varies as sigma sup n, was determined to be 2.00 + or - 0.15 and the true activation energy was found to be 692 + or - 25 kJ/mol. Transmission electron microscopy studies showed that deformation occurred in the grain boundary glassy phase accompanied by microcrack formation and cavitation. The steady state creep results are consistent with a diffusion controlled creep mechanism involving nitrogen diffusion through the grain boundary glassy phase.

  15. Madelung deformity and Madelung-type deformities: a review of the clinical and radiological characteristics.

    PubMed

    Ali, Sayed; Kaplan, Summer; Kaufman, Theresa; Fenerty, Sarah; Kozin, Scott; Zlotolow, Dan A

    2015-11-01

    Madelung deformity of the distal radius results from premature closure of the medial volar aspect of the distal radial physis, leading to increased volar tilt and increased inclination of the radial articular surface, triangulation of the carpus with proximal migration of the lunate and dorsal displacement of the distal ulna. The deformity is particularly common in Leri-Weill dyschondrosteosis, but it may also occur in isolation. True Madelung deformity can be differentiated from Madelung-type deformities by the presence of an anomalous radiolunate ligament (Vickers ligament). In this article, we will review the imaging characteristics of true Madelung deformity, including the common "distal radius" variant, the less common "entire radius" variant and "reverse" Madelung deformity. We will discuss the role of the Vickers ligament in disease pathogenesis and its use in differentiating true Madelung deformity from Madelung-type deformities arising from trauma or multiple hereditary exostoses. Surgical management of these patients will also be addressed. PMID:26135644

  16. Microstructural Evolution of an Extensional Shear Zone: the Transition from Dislocation Creep to Grain Boundary Sliding in Naturally Deformed Plagioclase

    NASA Astrophysics Data System (ADS)

    Miranda, E.; Hirth, G.; John, B. E.

    2014-12-01

    We present microstructural, LPO, and misorientation data from EBSD analyses to interpret the deformation mechanisms of naturally deformed plagioclase in an amphibolite-facies extensional shear zone within oceanic crust. Textural data and mineral chemistry data for thermometry were acquired on samples of gabbro mylonite collected from the footwall of the Atlantis Bank oceanic core complex; we focus on a monophase plagioclase layer with a high ratio of recrystallized matrix grains to porphyroclasts. Sample microstructures are subdivided into three regions: seven porphyroclasts, recrystallized grains immediately adjacent to those porphyroclasts, and the population of recrystallized matrix grains. All porphyroclasts exhibit subgrain development and show clustering of low-angle (3-10º) misorientation axes within the {010} plane, consistent with slip on {010}. However, only one porphyroclast is oriented for operation of the {010}<001> easy slip system. The small recrystallized grains immediately adjacent to the porphyroclasts do not show a host control relationship with their respective porphyroclasts, and these grains are also smaller than the subgrains of the porphyroclasts. Recrystallized matrix grains are fine-grained (mean grain size 8 μm) and slightly elongate parallel to foliation, with local misorientations concentrated along grain boundaries and junctions. They exhibit a weak, nonrandom LPO suggesting the activity of the {111}<110> slip system, and their neighbor-pair misorientations are shifted towards higher angles. We interpret the distinctive relationships between the three regions as evidence of a transition from dislocation creep to dislocation-accommodated grain boundary sliding (DisGBS). Porphyroclast subgrains and misorientation axes suggest the operation of dislocation creep, but the lack of host control in the adjacent recrystallized grains precludes grain size reduction through subgrain rotation recrystallization alone. High driving force bulge nucleation likely contributed to the grain size reduction and recrystallization of matrix grains, triggering the onset of grain size sensitive DisGBS. We suggest that the transition between deformation mechanisms is an effective weakening mechanism that contributed to development of the shear zone.

  17. Creep Measurement Video Extensometer

    NASA Technical Reports Server (NTRS)

    Jaster, Mark; Vickerman, Mary; Padula, Santo, II; Juhas, John

    2011-01-01

    Understanding material behavior under load is critical to the efficient and accurate design of advanced aircraft and spacecraft. Technologies such as the one disclosed here allow accurate creep measurements to be taken automatically, reducing error. The goal was to develop a non-contact, automated system capable of capturing images that could subsequently be processed to obtain the strain characteristics of these materials during deformation, while maintaining adequate resolution to capture the true deformation response of the material. The measurement system comprises a high-resolution digital camera, computer, and software that work collectively to interpret the image.

  18. The effect of low angle boundary misorientation on creep deformation in the superalloy CM 247 LC

    NASA Astrophysics Data System (ADS)

    Kirsch, Mathew

    The effect of low angle boundary misorientation on the creep properties of superalloy CM 247LC bicrystals has been investigated in the medium temperature - medium stress creep regime. Constant load tensile creep tests were performed on mixed Low Angle Boundary (LAB) samples with misorientations ranging from 3o-16o; the LABs where the boundaries were oriented approximately transverse to the tensile axis. Five repeats of each LAB sample were ruptured with an initial stress of 300 MPa and three repeats of each LAB sample were ruptured with an initial stress of 200 MPa, both at 950°C. A drastic decrease in creep rupture life and strain to failure was observed in bicrystals with misorientations greater than ˜10°. Fractography of the fracture surfaces indicated that a transition from ductile transgranular fracture to intergranular fracture coincided with the decrease in creep properties. The decrease in strain to failure was correlated to a decrease in the slip compatibility factor m'. Specimens of several misorientations were also interrupted prior to failure at strains of 2%, 5% and 10% and examined by electron microscopy techniques in an effort to better understand the sequences leading to failure. For samples that fractured intergranularly, voids formed adjacent to large MC carbides located at the LABs and propagated along the boundary, ultimately linking to cracks that initiated at the specimen edge. Electron Back Scattered Diffraction (EBSD) scans were performed and Crystal reference Orientation (CO) maps were generated from the partially crept specimens. An increase in misorientation from the crystal reference orientation was observed with increasing LAB misorientation for a given interrupted strain level indicative of the poorer slip compatibility at the higher misorientations Two bicrystals with nearly identical scalar misorientation, both ˜10°, exhibited surprisingly different behavior with one failing intergranularly at low strain to failure and the other failing transgranularly at high strain to failure; these differences were related to the different slip compatibilities as determined by an analysis of the nature of their misorientations. In addition, grain boundary migration was prevalent in the samples that fractured transgranularly, but was rarely observed on any specimen that fractured intergranularly. Based on the collective observations, it is concluded that (1) it is necessary to consider more than just the scalar misorientation when considering whether a single crystal containing LABs should be rejected and (2) characterization of the properties of superalloy bicrystals grown using traditional Bridgman methods is difficult due to the complex, non-planar nature of the resulting LABs that is associated with their dendritic growth.

  19. Evaluation of Permanent Deformation of CRM-Reinforced SMA and Its Correlation with Dynamic Stiffness and Dynamic Creep

    PubMed Central

    Mashaan, Nuha Salim; Karim, Mohamed Rehan

    2013-01-01

    Today, rapid economic and industrial growth generates increasing amounts of waste materials such as waste tyre rubber. Attempts to inspire a green technology which is more environmentally friendly that can produce economic value are a major consideration in the utilization of waste materials. The aim of this study is to evaluate the effect of waste tyre rubber (crumb rubber modifier (CRM)), in stone mastic asphalt (SMA 20) performance. The virgin bitumen (80/100) penetration grade was used, modified with crumb rubber at four different modification levels, namely, 6%, 12%, 16%, and 20% by weight of the bitumen. The testing undertaken on the asphalt mix comprises the indirect tensile (dynamic stiffness), dynamic creep, and wheel tracking tests. By the experimentation, the appropriate amount of CRM was found to be 16% by weight of bitumen. The results show that the addition of CRM into the mixture has an obvious significant effect on the performance properties of SMA which could improve the mixture's resistance against permanent deformation. Further, higher correlation coefficient was obtained between the rut depth and permanent strain as compared to resilient modulus; thus dynamic creep test might be a more reliable test in evaluating the rut resistance of asphalt mixture. PMID:24302883

  20. Modelling and analysis of creep deformation and fracture in a 1 Cr 1/2 Mo ferritic steel

    NASA Astrophysics Data System (ADS)

    Dyson, B. F.; Osgerby, D.

    A quantitative model, based upon a proposed new mechanism of creep deformation in particle-hardened alloys, has been validated by analysis of creep data from a 13CrMo 4 4 (1Cr 1/2 Mo) material tested under a range of stresses and temperatures. The methodology that has been used to extract the model parameters quantifies, as a first approximation, only the main degradation (damage) processes - in the case of the 1CR 1/2 Mo steel, these are considered to be the parallel operation of particle-coarsening and a progressively increasing stress due to a constant-load boundary condition. These 'global' model parameters can then be modified (only slightly) as required to obtain a detailed description and 'fit' to the rupture lifetime and strain/time trajectory of any individual test. The global model parameter approach may be thought of as predicting average behavior and the detailed fits as taking account of uncertainties (scatter) due to variability in the material. Using the global parameter dataset, predictions have also been made of behavior under biaxial stressing; constant straining rate; constant total strain (stress relaxation) and the likely success or otherwise of metallographic and mechanical remanent lifetime procedures.

  1. Elastic phase-strain distribution in a particulate-reinforced metal-matrix composite deforming by slip or creep

    SciTech Connect

    Daymond, M.R.; Lund, C.; Bourke, M.A.M.; Dunand, D.C.

    1999-11-01

    The macroscopic load-bearing capability of a composite is directly related to the strain partitioning due to load transfer between the component phases. Using neutron diffraction, the elastic mean phase strains were measured during in-situ loading of a Cu-15 vol pct Mo particulate metal-matrix composite (MMC) at 25 C, 300 C, and 350 C. The degree of load sharing at each temperature was compared to finite-element (FE) results. The load transfer from the matrix to reinforcement is both qualitatively and quantitatively different at low and high temperatures. When the matrix creeps, load transfer is less effective than when the matrix deforms by slip; also, load transfer at elevated temperatures decreases with increasing applied stress.

  2. On The Creep Behavior and Deformation Mechanisms Found in an Advanced Polycrystalline Nickel-Base Superalloy at High Temperatures

    NASA Astrophysics Data System (ADS)

    Deutchman, Hallee Zox

    Polycrystalline Ni-base superalloys are used as turbine disks in the hot section in jet engines, placing them in a high temperature and stress environment. As operating temperatures increase in search of better fuel efficiency, it becomes important to understand how these higher temperatures are affecting mechanical behavior and active deformation mechanisms in the substructure. Not only are operating temperatures increasing, but there is a drive to design next generation alloys in shorter time periods using predictive modeling capabilities. This dissertation focuses on mechanical behavior and active deformation mechanisms found in two different advanced polycrystalline alloy systems, information which will then be used to build advanced predictive models to design the next generation of alloys. The first part of this dissertation discusses the creep behavior and identifying active deformation mechanisms in an advanced polycrystalline Ni-based superalloy (ME3) that is currently in operation, but at higher temperatures and stresses than are experienced in current engines. Monotonic creep tests were run at 700C and between 655-793MPa at 34MPa increments, on two microstructures (called M1 and M2) produced by different heat treatments. All tests were crept to 0.5% plastic strain. Transient temperature and transient stress tests were used determine activation energy and stress exponents of the M1 microstructure. Constant strain rate tests (at 10-4s-1) were performed on both microstructures as well. Following creep testing, both M1 and M2 microstructures were fully characterized using Scanning Electron Microscopy (SEM) for basic microstructure information, and Scanning Transmission Electron Microscopy (STEM) to determine active deformation mechanism. It was found that in the M1 microstructure, reorder mediated activity (such as discontinuous faulting and microtwinning) is dominant at low stresses (655-724 MPa). Dislocations in the gamma matrix, and overall planar dislocation activity were also present. At higher stresses (758-793MPa), there is still planar activity present, but now non-planar "wavy" slip appears. Wavy slip was also present in the constant strain rate sample of the M1 microstructure. M2 showed much of the same activity as M1, but wavy slip was not present in either the high stress creep conditions or the constant strain rate conditions. The second part of this dissertation focused on Alloy X, which is a next generation alloy system. Three variants were examined (decreased levels of Cr and Co, decreased levels of Cr and Co with added Hf, and decreased levels of Cr and Co with added Hf and a faster cooling rate). The variants were all tested at 700C/690MPa, 760C/490MPa, and 815C/345MPa, to various strains. In Alloy X, the dominant mechanisms that appear throughout all strains, stresses, and temperatures are unpaired dislocations and discontinuous stacking faults. In the Hf bearing variants, , unpaired dislocations appear to start at grain boundaries and move in to the grains with increasing strain and temperature. Through 3D stereo imaging using STEM images, it appears that the dislocations are able to climb over precipitates at larger strains. It is postulated that the decreasing levels of Cr and Co have changed the stacking fault energy so it is unfavorable to form microtwins anymore. This was discussed in terms of the Dislocation Activity Diagram (DAD).

  3. Aftershocks resulting from creeping sections in a heterogeneous fault

    NASA Astrophysics Data System (ADS)

    Zller, G.; Hainzl, S.; Holschneider, M.; Ben-Zion, Y.

    2005-02-01

    We show that realistic aftershock sequences with space-time characteristics compatible with observations are generated by a model consisting of brittle fault segments separated by creeping zones. The dynamics of the brittle regions is governed by static/kinetic friction, 3D elastic stress transfer and small creep deformation. The creeping parts are characterized by high ongoing creep velocities. These regions store stress during earthquake failures and then release it in the interseismic periods. The resulting postseismic deformation leads to aftershock sequences following the modified Omori law. The ratio of creep coefficients in the brittle and creeping sections determines the duration of the postseismic transients and the exponent p of the modified Omori law.

  4. Characteristics of Creep Damage for 60Sn-40Pb Solder Material

    SciTech Connect

    Wei, Y.; Chow, C.L.; Fang, H.E.; Neilsen, M.K.

    1999-08-26

    This paper presents a viscoplasticity model taking into account the effects of change in grain or phase size and damage on the characterization of creep damage in 60Sn-40Pb solder. Based on the theory of damage mechanics, a two-scalar damage model is developed for isotropic materials by introducing the free energy equivalence principle. The damage evolution equations are derived in terms of the damage energy release rates. In addition, a failure criterion is developed based on the postulation that a material element is said to have ruptured when the total damage accumulated in the element reaches a critical value. The damage coupled viscoplasticity model is discretized and coded in a general-purpose finite element program known as ABAQUS through its user-defined material subroutine UMAT. To illustrate the application of the model, several example cases are introduced to analyze, both numerically and experimentally, the tensile creep behaviors of the material at three stress levels. The model is then applied to predict the deformation of a notched specimen under monotonic tension at room temperature (22 C). The results demonstrate that the proposed model can successfully predict the viscoplastic behavior of the solder material.

  5. Creep and the corrosion characteristics of Incoloy Alloy 800 in molten nitrate salts

    SciTech Connect

    Goods, S.H.

    1981-03-01

    Incoloy Alloy 800 (I800) has been proposed for use in the receiver tube panel arrays in a number of advanced solar central receiver (SCR) concepts. Because of their high heat capacity and high thermal energy density, several designs require the use of molten sodium and potassium nitrate salt mixture to act as the cooling or heat transfer fluid. The effects of deformation on the corrosion resistance of Incoloy Alloy 800 in sodium nitrate and potassium nitrate salt mixtures have been studied. Hollow tube specimens filled with the salt mixture (60%-NaNO/sub 3/-40% KNO/sub 3/) were tested in constant load tension creep at elevated temperatures (550/sup 0/ less than or equal to T less than or equal to 670/sup 0/C). Depending on the temperature and initial stress, fracture times (and therefore salt exposure times) ranged between 300 and 1000 hours. While the fracture strain of specimens tested to failure was only slightly reduced when exposed to the salt environment, metallographic observations of polished cross-sections revealed severe surface oxidation. In order to characterize the effect of total imposed strain on oxide morphology a number of creep tests were terminated prior to fracture. Increasing deformation resulted in a more extensively damaged surface oxide as well as a more rapid rate of corrosion. EDX analysis revealed that the oxide was multiphase, with a near surface iron rich oxide above a chromium-rich oxide layer. Below 630/sup 0/C the oxide-metal interface was well defined (although irregular). Above 630/sup 0/C the interface was more diffuse with fine oxide intrusions growing into the base metal and small particles of the alloy visible in the oxide near the base metal interface.

  6. Creep deformation and rupture behavior of 2.25Cr-1Mo steel weldments and its constituents (base metal, weld metal and simulated heat affected zones)

    SciTech Connect

    Laha, K.; Chandravathi, K.S.; Rao, K.B.S.; Mannan, S.L.

    1995-12-31

    Microstructure across a weldment base metal through transformed heat-affected zone (HAZ) to cast weld metal. HAZ of 2.25Cr-1Mo weldment consists of coarse-grain bainite, fine-grain bainite and intercritical region. These HAZ microstructures were simulated by isothermal heat-treatments. Creep tests were carried out on base metal, weld metal, weldment and the simulated HAZ structures. Creep deformation and fracture behavior of 2.25Cr-1Mo weldments has been assessed based on the properties of its constituents. Coarse-grain bainite with low ductility and intercritical structure with low strength are the critical components of HAZ determining performance of the weldments.

  7. Evidence of post-seismic creep type deformations derived by tilt and acoustic emission monitoring of mining induced seismic events

    NASA Astrophysics Data System (ADS)

    Milev, Alexander; Share, Pieter-Ewald; Naoi, Makoto; Durrheim, Raymond; Yabe, Yasuo; Ogasawara, Hiroshi; Nakatani, Masao

    2015-04-01

    In this study we try to understand pre- and post-failure rock behavior associated with mining induced seismic events. This involves underground installation of various high precision instruments, including geophones, acoustic emission sensors, tilt- and strain-meters at a number of sites in deep level South African gold mines. The rate of tilt, strain and the seismic ground motion were analysed in order to understand the coseismic and aseismic deformation of the rocks. A good correspondence between the coseismic and the aseismic deformations was found. The rate of coseismic and aseismic tilt, as well as seismicity recorded by the mine seismic network, are approximately constant until the daily blasting time, which takes place from about 19:30 until shortly before 21:00. During the blasting time and the subsequent seismic events, the coseismic tilt and strain shows a rapid increase. Much of the aseismic deformation, however, occurs independently of the seismic events and blasting. In an attempt to distinguish between the different mechanisms of tilting two types of events were recognized. The "fast" seismic events characterized with sharp increase of the tilt during the seismic rupture and "slow" seismic events characterized by creep type post seismic deformations. Tilt behaviour before and after a seismic event was also analysed. The fact that no recognizable aftertilt was observed for more of the "fast" seismic events means that there is no gradual release of stress and an associated continuous strain rate change afterwards. It can therefore be concluded that a large seismic event causes a rapid change in the state of stress rather than a gradual change in the strain rate During the monitoring period a seismic event with MW 2.2 occurred in the vicinity of the instrumented site. This event was recorded by both the CSIR integrated monitoring system and JAGUARS acoustic emission network. More than 21,000 AE aftershocks were located in the first 150 hours after the main event. Using the distribution of the AE events the position of the fault in the source area was successfully delineated. The rupture area, elastic properties of the rock, the state of stress before the event occurred and frictional parameters of the rupture were used as input parameters to both numerical and analytical tools to reproduce the expected tilt. The calculated values were compared with the real values as recorded by the installed tiltmeters. A good correlation between the calculated and monitored amount of tilt was found. The tilt changes associated with this event showed a well pronounced after-tilt. The distribution of the AE events following the main shock was related to after tilt in order to quantify post slip behavior of the source. There was no evidence found for coseismic expansion of the source after the main slip. Therefore the hypothesis of the post-seismic creep behaviour of the source was proposed to explain the large amount of tilt following the main shock.

  8. Compilation of Surface Creep on California Faults and Comparison of WGCEP 2007 Deformation Model to Pacific-North American Plate Motion

    USGS Publications Warehouse

    Wisely, Beth A.; Schmidt, David A.; Weldon, Ray J., II

    2008-01-01

    This Appendix contains 3 sections that 1) documents published observations of surface creep on California faults, 2) constructs line integrals across the WG-07 deformation model to compare to the Pacific ? North America plate motion, and 3) constructs strain tensors of volumes across the WG-07 deformation model to compare to the Pacific ? North America plate motion. Observation of creep on faults is a critical part of our earthquake rupture model because if a fault is observed to creep the moment released as earthquakes is reduced from what would be inferred directly from the fault?s slip rate. There is considerable debate about how representative creep measured at the surface during a short time period is of the whole fault surface through the entire seismic cycle (e.g. Hudnut and Clark, 1989). Observationally, it is clear that the amount of creep varies spatially and temporally on a fault. However, from a practical point of view a single creep rate is associated with a fault section and the reduction in seismic moment generated by the fault is accommodated in seismic hazard models by reducing the surface area that generates earthquakes or by reducing the slip rate that is converted into seismic energy. WG-07 decided to follow the practice of past Working Groups and the National Seismic Hazard Map and used creep rate (where it was judged to be interseismic, see Table P1) to reduce the area of the fault surface that generates seismic events. In addition to following past practice, this decision allowed the Working Group to use a reduction of slip rate as a separate factor to accommodate aftershocks, post seismic slip, possible aseismic permanent deformation along fault zones and other processes that are inferred to affect the entire surface area of a fault, and thus are better modeled as a reduction in slip rate. C-zones are also handled by a reduction in slip rate, because they are inferred to include regions of widely distributed shear that is not completely expressed as earthquakes large enough to model. Because the ratio of the rate of creep relative to the total slip rate is often used to infer the average depth of creep, the ?depth? of creep can be calculated and used to reduce the surface area of a fault that generates earthquakes in our model. This reduction of surface area of rupture is described by an ?aseismicity factor,? assigned to each creeping fault in Appendix A. An aseismicity factor of less than 1 is only assigned to faults that are inferred to creep during the entire interseismic period. A single aseismicity factor was chosen for each section of the fault that creeps by expert opinion from the observations documented here. Uncertainties were not determined for the aseismicity factor, and thus it represents an unmodeled (and difficult to model) source of error. This Appendix simply provides the documentation of known creep, the type and precision of its measurement, and attempts to characterize the creep as interseismic, afterslip, transient or triggered. Parts 2 and 3 of this Appendix compare the WG-07 deformation model and the seismic source model it generates to the strain generated by the Pacific - North American plate motion. The concept is that plate motion generates essentially all of the elastic strain in the vicinity of the plate boundary that can be released as earthquakes. Adding up the slip rates on faults and all others sources of deformation (such as C-zones and distributed ?background? seismicity) should approximately yield the plate motion. This addition is usually accomplished by one of four approaches: 1) line integrals that sum deformation along discrete paths through the deforming zone between the two plates, 2) seismic moment tensors that add up seismic moment of a representative set of earthquakes generated by a crustal volume spanning the plate boundary, 3) strain tensors generated by adding up the strain associated with all of the faults in a crustal volume spanning the plate

  9. Microstructural changes of CM186LC single-crystal superalloy during creep deformation at 750 degrees C.

    PubMed

    Dubiel, B; Czyrska-Filemonowicz, A

    2006-10-01

    The microstructure of creep-tested CM186LC Ni-base single-crystal alloy was studied to assess its suitability for use in the gas turbine environment. Creep tests were conducted at 750 degrees C and at stresses of 560 and 675 MPa up to 11 440 h. The microstructure of fractured and terminated specimens was investigated by light microscopy, scanning electron microscopy and analytical transmission electron microscopy. Microstructural analysis revealed the differences in the microstructure of creep-tested CM186LC depending on the stress applied during creep at 750 degrees C. PMID:17100893

  10. Viscous Creep in Dry Unconsolidated Gulf of Mexico Shale

    NASA Astrophysics Data System (ADS)

    Chang, C.; Zoback, M. D.

    2002-12-01

    We conducted laboratory experiments to investigate creep characteristics of dry unconsolidated shale recovered from the pathfinder well, Gulf of Mexico (GOM). We subjected jacketed cylindrical specimens (25.4 mm diameter) to hydrostatic pressure that increased from 10 to 50 MPa in steps of 5 MPa. We kept the pressure constant in each step for at least 6 hours and measured axial and lateral strains (provided by LVDTs) and ultrasonic velocities (provided by seismic-wave transducers). The dry shale exhibited pronounced creep strain at all pressure levels, indicating that the dry frame of the shale possesses an intrinsic viscous property. Interestingly, the creep behavior of the shale is different above and below 30 MPa confining pressure. Above 30 MPa, the amount of creep strain in 6 hours is nearly constant with equal pressurization steps, indicating a linear viscous rheology. Below 30 MPa, the amount of creep increases linearly as pressure is raised in constant incremental steps, suggesting that the creep deformation accelerates as pressure increases within this pressure range. Thus, the general creep behavior of the GOM shale is characterized by a bilinear dependence on pressure magnitude. This creep characteristic is quite different from that observed in unconsolidated reservoir sands (Hagin and Zoback, 2002), which exhibited nearly constant amount of creep regardless of the pressure magnitude for equal increasing steps of pressure. The shale exhibits a lack of creep (and nearly negligible strain recovery) when unloaded, suggesting that the creep strain is irrecoverable and can be considered viscoplastic deformation. SEM observations show that the major mechanism of compaction of the dry shale appears to be packing of clay and a progressive collapse of pore (void) spaces. Creep compaction is considerably more significant than compaction that occurs instantaneously, indicating that the process of shale compaction is largely time-dependent.

  11. In-situ scanning electron microscopy (sem) observations of the tensile and tensile-creep deformation of Titanium-8Aluminum-1mo-1v (wt.%) alloy

    NASA Astrophysics Data System (ADS)

    Ghosh Dastidar, Indraroop

    Titanium (Ti) and titanium alloys (Ti alloys) are attractive for structural applications, such as in the aerospace and automotive industries due to their high specific strength, excellent corrosion resistance and good ability to withstand elevated temperatures. To develop Ti alloys with better mechanical properties, it is necessary to comprehend the deformation behavior of available Ti alloys. Previous studies performed by another graduate student, Dr. Hongmei Li, involved investigation of the deformation behavior of commercially pure (CP) Ti, Ti-5Al-2.5Sn (wt.%), Ti-3Al-2.5V (wt.%) and Ti-6Al-4V (wt.%) alloys. The current thesis focused on investigating the deformation behavior of Ti-8Al-1Mo-1V (wt.%). In-situ tensile and tensile-creep experiments were performed at temperatures ranging from room temperature (RT) to 650OC inside a scanning electron microscope (SEM), which allowed for the observation of the surface deformation evolution. Electron Back Scattered Diffraction (EBSD) was used to identify the distribution of the active deformation systems. In this thesis efforts were made to characterize the various deformation modes of the Ti-8Al-1Mo-1V (wt.%) alloy as a function of the testing conditions (stress and temperature). It was observed that prismatic slip made up the majority of the observed slip systems during the RT tensile deformation, while basal and prismatic slip were almost equally active during the 455OC tensile deformation. Grain boundary ledges were observed during the elevated temperature tensile-creep deformation and from this observation it was suggested that grain boundary sliding was an active deformation mode. This work also involved estimating the Critical Resolved Shear Stress (CRSS) ratios of the alpha-phase deformation modes. The CRSS ratios were compared with the CRSS ratios of CP Ti and other Ti alloys. Overall, this work was intended to add more data to the scientific literature of Ti alloys in order to better comprehend their deformation modes, so as to design and develop higher performance Ti alloys.

  12. Microstructure, creep, and tensile deformation in Ti-6Al-2Nb-1Ta-0.8Mo

    NASA Astrophysics Data System (ADS)

    Miller, W. H.; Chen, R. T.; Starke, E. A.

    1987-08-01

    The effects of microstructure, temperature, and stress level on the creep response of Ti-6211 have been investigated. A variety of microstructures simulating the heat affected zone of a weld (HAZ), as well as the as-received structure, were tested in a temperature range of 298 K to 873 K. At stress levels below the tensile yield strength, creep curves saturate in the ambient temperature regime. The colony type Widmanstätten alpha + beta as-received structure exhibited the highest creep strains at ambient temperatures. Long slip lengths associated with the large colony size, and sliding along various interfaces account for the relatively high creep strains to saturation. Planar arrays of straight dislocations operating on a single slip system were observed for samples crept at 298 K while thermally activated cross slip was observed for samples crept at 453 K. Beta-annealed martensitic micro-structures displayed enhanced creep resistance, out-performing other recrystallized HAZ structures. Above 778 K the activation energy of creep is close to that for self-diffusion in titanium, suggesting that diffusion-controlled dislocation mechanisms are the rate-controlling processes at elevated temperatures. Creep rupture at elevated temperatures occurred by microvoid nucleation and growth. Fracture occurred along colony boundaries in the as-received structure but appear to be intergranular with the crack propagating along G. B. alpha/matrix interfaces in the equiaxed microstructures. Sliding along alpha/beta interfaces, colony boundaries, prior beta grain boundaries, and slip traces contributed to the creep strain and rupture process. Cyclic creep with a loading-unloading sequence was also performed at room temperature and cyclic creep acceleration was observed.

  13. Creep deformation and fracture of a Cr/Mo/V bolting steel containing selected trace-element additions

    NASA Astrophysics Data System (ADS)

    Larouk, Z.; Pilkington, R.

    1999-08-01

    The article reports the creep behavior, at 565 C, of 1Cr1Mo0.75V (Ti, B) (Durehete D1055) steel, in each of two grain sizes and doped with individual trace elements such as P, As, and Sn, in comparison to a reference cast of the base material containing 0.08 wt pct Ti. The addition of the trace elements P, As, or Sn (each <0.045 wt pct) appears to produce no significant effect on creep strength or creep crack-growth resistance at 565 C. The fine-grained material shows low creep strength but notch strengthening, while the coarse-grained material shows higher creep strength and exhibits notch weakening for test times up to 2750 hours. From creep crack-growth tests, it appears that the C* parameter is not appropriate for correlating the creep crack-growth rate under the present test conditions. The parameters K I or ? net are found to correlate better, but, from the present data, it is not possible to judge which of these parameters is more appropriate for general use. It is suggested that the presence of Ti in CrMoV steels has an inhibiting effect on trace-element embrittlement.

  14. Numerical creep analysis

    SciTech Connect

    Anderson, C.A.

    1984-01-01

    A large deformation creep algorithm is presented that includes pore pressure and fluid migration effects. Its application is illustrated by the numericl analysis of rock folding with attendant fluid migration. 6 references, 2 figures. (ACR)

  15. Investigation of creep mechanical characteristics of femoral prostheses by simulated hip replacement

    PubMed Central

    LIU, GUANG-YAO; JIN, YAN; LI, PENG

    2013-01-01

    In order to provide creep mechanical parameters for the clinical application of both traditional and reserved anatomy femoral artificial joint replacements, simulated hip replacement femoral stress relaxation and creep experiments were performed. Twenty-four corpse femoral specimens were obtained, with 8 specimens being randomly assigned to the control group and 8 specimens being randomly assigned to the traditional prosthesis group. Our results showed that the retaining femoral neck prosthesis and traditional prosthesis groups have different stress relaxation and creep mechanical properties. PMID:23596489

  16. Correlation of Creep Behavior of Domal Salts

    SciTech Connect

    Munson, D.E.

    1999-02-16

    The experimentally determined creep responses of a number of domal salts have been reported in, the literature. Some of these creep results were obtained using standard (conventional) creep tests. However, more typically, the creep data have come from multistage creep tests, where the number of specimens available for testing was small. An incremental test uses abrupt changes in stress and temperature to produce several time increments (stages) of different creep conditions. Clearly, the ability to analyze these limited data and to correlate them with each other could be of considerable potential value in establishing the mechanical characteristics of salt domes, both generally and specifically. In any analysis, it is necessary to have a framework of rules to provide consistency. The basis for the framework is the Multimechanism-Deformation (M-D) constitutive model. This model utilizes considerable general knowledge of material creep deformation to supplement specific knowledge of the material response of salt. Because the creep of salt is controlled by just a few micromechanical mechanisms, regardless of the origin of the salt, certain of the material parameters are values that can be considered universal to salt. Actual data analysis utilizes the methodology developed for the Waste Isolation Pilot Plant (WIPP) program, and the response of a bedded pure WIPP salt as the baseline for comparison of the domal salts. Creep data from Weeks Island, Bryan Mound, West Hackberry, Bayou Choctaw, and Big Hill salt domes, which are all sites of Strategic Petroleum Reserve (SPR) storage caverns, were analyzed, as were data from the Avery Island, Moss Bluff, and Jennings salt domes. The analysis permits the parameter value sets for the domal salts to be determined in terms of the M-D model with various degrees of completeness. In turn this permits detailed numerical calculations simulating cavern response. Where the set is incomplete because of the sparse database, reasonable assumptions permit the set to be completed. From the analysis, two distinct response groups were evident, with the salts of one group measurably more creep resistant than the other group. Interestingly, these groups correspond well with the indirectly determined creep closure of the SPR storage caverns, a correlation that probably should be expected. Certainly, the results suggest a simple laboratory determination of the creep characteristics of a salt material from a dome site can indicate the relative behavior of any potential cavern placed within that dome.

  17. Creep Deformation, Rupture Analysis, Heat Treatment and Residual Stress Measurement of Monolithic and Welded Grade 91 Steel for Power Plant Components

    NASA Astrophysics Data System (ADS)

    Shrestha, Triratna

    Modified 9Cr-1 Mo (Grade 91) steel is currently considered as a candidate material for reactor pressure vessels (RPVs) and reactor internals for the Very High Temperature Reactor (VHTR), and in fossil-fuel fired power plants at higher temperatures and stresses. The tensile creep behavior of Grade 91 steel was studied in the temperature range of 600°C to 750°C and stresses between 35 MPa and 350 MPa. Heat treatment of Grade 91 steel was studied by normalizing and tempering the steel at various temperatures and times. Moreover, Thermo-Ca1c(TM) calculation was used to predict the precipitate stability and their evolution, and construct carbon isopleths of Grade 91 steel. Residual stress distribution across gas tungsten arc welds (GTAW) in Grade 91 steel was measured by the time-of-flight neutron diffraction using the Spectrometer for Materials Research at Temperature and Stress (SMARTS) diffractometer at Lujan Neutron Scattering Center, Los Alamos National Laboratory, Los Alamos, NM, USA. Analysis of creep results yielded stress exponents of ˜9-11 in the higher stress regime and ˜1 in the lower stress regime. The creep behavior of Grade 91 steel was described by the modified Bird-Mukherjee-Dorn relation. The rate-controlling creep deformation mechanism in the high stress regime was identified as the edge dislocation climb with a stress exponent of n = 5. On the other hand, the deformation mechanism in the Newtonian viscous creep regime (n = 1) was identified as the Nabarro-Herring creep. Creep rupture data were analyzed in terms of Monkman-Grant relation and Larson-Miller parameter. Creep damage tolerance factor and stress exponent were used to identify the cause of creep damage. The fracture surface morphology of the ruptured specimens was studied by scanning electron microscopy to elucidate the failure mechanisms. Fracture mechanism map for Grade 91 steel was developed based on the available material parameters and experimental observations. The microstructural evolution of heat treated steel was correlated with the differential scanning calorimetric study. The combination of microstructural studies with optical microscopy, scanning and transmission electron microscopy, microhardness profiles, and calorimetric plots helped in the understanding of the evolution of microstructure and precipitates in Grade 91 steel. The residual stresses were determined at the mid-thickness of the plate, 4.35 mm and 2.35 mm below the surface of the as-welded and post-weld heat treated plate. The residual stresses of the as-welded plate were compared with the post-weld heat treated plate. The post-weld heat treatment significantly reduced the residual stress in the base metal, heat affected zone, and the weld zone. Vickers microhardness profiles of the as-welded, and post-weld heat treated specimens were also determined and correlated with the observed residual stress profile and microstructure.

  18. ACCEPT: a three-dimensional finite element program for large deformation elastic-plastic-creep analysis of pressurized tubes (LWBR/AWBA Development Program)

    SciTech Connect

    Hutula, D.N.; Wiancko, B.E.

    1980-03-01

    ACCEPT is a three-dimensional finite element computer program for analysis of large-deformation elastic-plastic-creep response of Zircaloy tubes subjected to temperature, surface pressures, and axial force. A twenty-mode, tri-quadratic, isoparametric element is used along with a Zircaloy materials model. A linear time-incremental procedure with residual force correction is used to solve for the time-dependent response. The program features an algorithm which automatically chooses the time step sizes to control the accuracy and numerical stability of the solution. A contact-separation capability allows modeling of interaction of reactor fuel rod cladding with fuel pellets or external supports.

  19. Creep: Long-term Time-Dependent Rock Deformation in a Deep-sea Laboratory in the Ionian sea: a Pilot Study

    NASA Astrophysics Data System (ADS)

    Meredith, P. G.; Boon, S.; Vinciguerra, S.; Bowles, J.; NEMO Group,.

    2003-12-01

    Time-dependent brittle rock deformation is of first-order importance for understanding the long-term behavior of water saturated rocks in the Earth's upper crust. Interpretation of results from traditional laboratory brittle creep experiments have generally been in terms of three individual creep phases; primary (decelerating), secondary (constant strain rate or quasi-steady-state) and tertiary (accelerating or unstable). The deformation may be distributed during the first two, but localizes onto a fault plane during phase three. More recently, models have been proposed that explain the trimodal shape of creep curves in terms of the competition between a weakening mechanism and a strengthening mechanism, with the weakening mechanism eventually dominating and leading to localized failure. However, a major problem is that it is difficult to distinguish between these competing mechanisms and models given the lower limit of strain rates achievable in laboratory experiments over practicable time scales. This study aims to address that problem directly by extending significantly the range of achievable strain rates through much longer-term experiments conducted in a deep-sea laboratory in the Ionian sea. The project takes advantage of a collaboration with the NEMO Group-INFN, a consortium that is developing a large volume (1 km3) deep-sea detector for high-energy (>1019 eV) cosmic neutrinos. A suitable test site has been identified, some 20km north-east of Catania in Sicily, at a depth of 2100m. Within the CREEP deformation apparatus, confining pressure is provided by the ambient water pressure (>22MPa), and the constant axial stress is provided by an actuator that amplifies this pressure. Measurement transducers and a data acquisition system are sealed internally, with power provided for up to 6 months by an internal battery pack. The great advantage of operating in the deep sea in this way is that the system is essentially passive, has few moving parts, and requires no maintenance. The apparatus is held in place by a disposable cast-iron anchor and supported above the seabed by a deep-sea buoyage system. On completion of each experiment, an acoustic release detaches from the anchor and allows the apparatus to float to the surface to be recovered by the oceanographic research vessel.

  20. Deformation characteristics and time-dependent notch sensitivity of Udimet 700 at intermediate temperatures

    NASA Technical Reports Server (NTRS)

    Wilson, D. J.

    1974-01-01

    Time dependent notch sensitivity was observed in Udimet 700 sheet, bar, and investment castings between 1000 and 1400 F (538 -760 C), but not at 1600 F (871 C). As was the case for modified Waspaloy, Waspaloy and Inconel 718, it occurred in notched specimens loaded below the yield strength when the creep deformation was localized. For each alloy and notched specimen geometry, a stress-average particle size zone can be defined that characterizes the notch sensitive behavior.

  1. Effect of temperature on tensile and creep characteristics of PRD49 fiber/epoxy composites

    NASA Technical Reports Server (NTRS)

    Hanson, M. P.

    1972-01-01

    Tensile and creep data of PRD49-1 and 3 fiber/epoxy-resin composites are presented. Tensile data were obtained from 20 to 477 K (-423 to 400 F). Tensile strengths and moduli were determined at selected temperatures. Creep data are presented for fiber composites at 297, 422 and 450 K (75, 300, and 350 F) for as long as 1000 hours at stress levels of approximately 50 and 80 percent of the ultimate tensile strength at 297 K (75 F). Details of tensile specimens and test procedures used in the investigation are presented.

  2. Brittle and compaction creep in porous sandstone

    NASA Astrophysics Data System (ADS)

    Heap, Michael; Brantut, Nicolas; Baud, Patrick; Meredith, Philip

    2015-04-01

    Strain localisation in the Earth's crust occurs at all scales, from the fracture of grains at the microscale to crustal-scale faulting. Over the last fifty years, laboratory rock deformation studies have exposed the variety of deformation mechanisms and failure modes of rock. Broadly speaking, rock failure can be described as either dilatant (brittle) or compactive. While dilatant failure in porous sandstones is manifest as shear fracturing, their failure in the compactant regime can be characterised by either distributed cataclastic flow or the formation of localised compaction bands. To better understand the time-dependency of strain localisation (shear fracturing and compaction band growth), we performed triaxial deformation experiments on water-saturated Bleurswiller sandstone (porosity = 24%) under a constant stress (creep) in the dilatant and compactive regimes, with particular focus on time-dependent compaction band formation in the compactive regime. Our experiments show that inelastic strain accumulates at a constant stress in the brittle and compactive regimes leading to the development of shear fractures and compaction bands, respectively. While creep in the dilatant regime is characterised by an increase in porosity and, ultimately, an acceleration in axial strain to shear failure (as observed in previous studies), compaction creep is characterised by a reduction in porosity and a gradual deceleration in axial strain. The overall deceleration in axial strain, AE activity, and porosity change during creep compaction is punctuated by excursions interpreted as the formation of compaction bands. The growth rate of compaction bands formed during creep is lower as the applied differential stress, and hence background creep strain rate, is decreased, although the inelastic strain required for a compaction band remains constant over strain rates spanning several orders of magnitude. We find that, despite the large differences in strain rate and growth rate (from both creep and constant strain rate experiments), the characteristics (geometry, thickness) of a compaction band remain essentially the same. Several lines of evidence, notably the similarity between the differential stress dependence of creep strain rate in the dilatant and compactive regimes, suggest that, as for dilatant creep, compactant creep is driven by subcritical stress corrosion cracking. We highlight the attendant implications for time-dependent porosity loss, subsidence, and permeability reduction in sandstone reservoirs.

  3. Effect of ultrasound on the characteristics of superplastic deformation

    NASA Astrophysics Data System (ADS)

    Myshlyaev, M. M.; Shpeizman, V. V.; Klubovich, V. V.; Kulak, M. M.; Lyu, G.

    2015-12-01

    The deformation of aluminum-lithium alloy 1420 is investigated in the region of temperatures of its superplasticity T = 320-395C under the simultaneous action of stretching load and axial ultrasonic vibrations. The estimates of the activation parameters of deformation show that the activation energy of deformation during stretching with ultrasonic vibrations and without them are close both at the stage of hardening and at the stage of softening. It is concluded that the ultrasonic vibrations facilitate intragranular deformation at the hardening stage and promote an increase in its contribution to the total deformation without changing the deformation mechanisms.

  4. Creep of rocksalt

    NASA Astrophysics Data System (ADS)

    Carter, Neville L.; Hansen, Francis D.

    1983-03-01

    A review is presented of the fundamental flow properties and processes in experimentally deformed natural and synthetic halite single crystals and polycrystalline aggregates. Included in the summary are discussions of: (a) microstructures induced during steady-state creep; (b) creep-rupture of rocksalt; (c) experiments associated with "Project Salt Vault" and more recent field studies; and (d) brine migration. A representative steady-state flow law determined for natural aggregates and maximum natural deviatoric stresses deduced from subgrain sizes are applied briefly to considerations of creep in waste repositories and of salt dome dynamics. While the mechanical behavior of rocksalt is probably better understood than for all other rock types, further investigations, especially on load path, stress history and creep-rupture are clearly mandated. Furthermore, additional investigations of brine migration and of bench and field-scale deformations are needed, the latter incorporating realistic rocksalt flow properties into numerical simulations of natural rock-mass response.

  5. Memory characteristics of hysteresis and creep in multi-layer piezoelectric actuators: An experimental analysis

    NASA Astrophysics Data System (ADS)

    Biggio, Matteo; Butcher, Mark; Giustiniani, Alessandro; Masi, Alessandro; Storace, Marco

    2014-02-01

    In this paper we provide an experimental characterization of creep and hysteresis in a multi-layer piezoelectric actuator (PEA), taking into account their relationships in terms of memory structure. We fit the well-known log-t model to the response of the PEA when driven by piecewise-constant signals, and find that both the instantaneous and the delayed response of the PEA display hysteretic dependence on the voltage level. We investigate experimentally the dependence of the creep coefficient on the input history, by driving the PEA along first-order reversal curves and congruent minor loops, and find that it displays peculiar features like strict congruence of the minor loops and discontinuities. We finally explain the observed experimental behaviors in terms of a slow relaxation of the staircase interface line in the Preisach plane.

  6. Clash of Porphyroblasts - Mechanical and chemical interaction of strong objects in a weak deforming matrix and the acceleration of dissolution precipitation creep

    NASA Astrophysics Data System (ADS)

    Bender, Hagen; Huet, Benjamin; Grasemann, Bernhard; Schuster, Ralf

    2015-04-01

    The presence of porphyroblasts in metamorphic rocks has a strong influence on the microstructures that develop during deformation. Valuable as gauges for the sense of shear, single isolated porphyroblasts and -clasts have attracted enormous attention and vigorous discussion in the geological community. Naturally, however, porphyroblasts often occur in populations. Therefore, the understanding of multi-porphyroblast interaction is of great significance. We use amphibolite-facies garnet mica schists from the Upper Austroalpine Wlz Complex for a case study. The microstructure of mm-cm sized, densely distributed garnet porphyroblasts indicates interference of the blasts. Blasts are subjected to convergence parallel to the instantaneous shortening axis, causing (i) accumulation and deformation of strain caps, (ii) fracturing of the garnets and (iii) dissolution of garnet at collision sites. Parallel to the instantaneous stretching axis, (i) cone-shaped strain shadows are linked between neighbouring garnets and (ii) separation of garnet clusters occurs preferably. Dissolution precipitation creep accommodates the major part of deformation. Consequently, the matrix separates due to the dense population of porphyroblasts. The matrix differentiates to dissolution sites and precipitation sites in the respective quadrants of stretching and shortening around the blasts. Quantitative chemical analysis and thermodynamic modelling are utilised to examine compositional variations in minerals within the stretching and shortening domains. The results show that the present-day assemblage in these rocks records no deviations from lithostatic pressure.

  7. Active disturbance rejection control for output force creep characteristics of ionic polymer metal composites

    NASA Astrophysics Data System (ADS)

    Xiong, Yan; Chen, Yang; Sun, Zhiyong; Hao, Lina; Dong, Jie

    2014-07-01

    Ionic polymer metal composites (IPMCs) are a type of electroactive polymer (EAP) that can be used as both sensors and actuators. An IPMC has enormous potential application in the field of biomimetic robotics, medical devices, and so on. However, an IPMC actuator has a great number of disadvantages, such as creep and time-variation, making it vulnerable to external disturbances. In addition, the complex actuation mechanism makes it difficult to model and the demand of the control algorithm is laborious to implement. In this paper, we obtain a creep model of the IPMC by means of model identification based on the method of creep operator linear superposition. Although the mathematical model is not approximate to the IPMC accurate model, it is accurate enough to be used in MATLAB to prove the control algorithm. A controller based on the active disturbance rejection control (ADRC) method is designed to solve the drawbacks previously given. Because the ADRC controller is separate from the mathematical model of the controlled plant, the control algorithm has the ability to complete disturbance estimation and compensation. Some factors, such as all external disturbances, uncertainty factors, the inaccuracy of the identification model and different kinds of IPMCs, have little effect on controlling the output block force of the IPMC. Furthermore, we use the particle swarm optimization algorithm to adjust ADRC parameters so that the IPMC actuator can approach the desired block force with unknown external disturbances. Simulations and experimental examples validate the effectiveness of the ADRC controller.

  8. Part 2: The creep behavior of Ti-Al-Nb O + bcc orthorhombic alloys

    SciTech Connect

    Boehlert, C.J.; Miracle, D.B.

    1999-09-01

    The intermediate-temperature (650 C to 760 C) creep behavior of orthorhombic (O) + bcc alloys containing 50 at. pct Ti was studied. Ti-25Al-25Nb, Ti-23Al-27Nb, and Ti-12Al-38Nb ingots were processed and heat treated to obtain a wide variety of microstructures. Creep deformation mechanisms and the effects of grain size, phase volume fraction, tension vs compression and aging on creep rates were examined. Unaged microstructures, which transformed during the creep experiments, exhibited larger primary creep strains than transformed microstructure, which were crept after long-term aging. The deformation observations and calculated creep exponents and activation energies suggested that separate creep mechanisms, dependent on the applied stress level, were dominating the secondary creep behavior. Coble creep characteristics, including relatively low activation energies and dislocation densities as well as stress exponents close to unity, were exhibited at low applied stresses. Experiments on fiducially marked specimens indicated that grain-boundary sliding was occurring for intermediate applied stresses. In this regime, the minimum creep rates were proportional to the applied stress squared and inversely proportional to the grain size. Overall, the minimum creep rates were dependent on microstructure and stress. Within the low-to-intermediate stress regimes, subtransus processed and heat-treated microstructures, which contained much finer grain sizes than supertransus microstructures, exhibited the poorest creep resistance. The influence of grain size was not as significant within the high-stress regime. It is shown that for low-to-intermediate stress levels, grain size is the dominant microstructural feature influencing the creep behavior of O + bcc alloys.

  9. Extreme ductile deformation of fine-grained salt by coupled solution-precipitation creep and microcracking: Microstructural evidence from perennial Zechstein sequence (Neuhof salt mine, Germany)

    NASA Astrophysics Data System (ADS)

    Závada, Prokop; Desbois, Guillaume; Schwedt, Alexander; Lexa, Ondrej; Urai, Janos L.

    2012-04-01

    Microstructural study revealed that the ductile flow of intensely folded fine-grained salt exposed in an underground mine (Zechstein-Werra salt sequence, Neuhof mine, Germany) was accommodated by coupled activity of solution-precipitation (SP) creep and microcracking of the halite grains. The grain cores of the halite aggregates contain remnants of sedimentary microstructures with straight and chevron shaped fluid inclusion trails (FITs) and are surrounded by two concentric mantles reflecting different events of salt precipitation. Numerous intra-granular or transgranular microcracks originate at the tips of FITs and propagate preferentially along the interface between sedimentary cores and the surrounding mantle of reprecipitated halite. These microcracks are interpreted as tensional Griffith cracks. Microcracks starting at grain boundary triple junctions or grain boundary ledges form due to stress concentrations generated by grain boundary sliding (GBS). Solid or fluid inclusions frequently alter the course of the propagating microcracks or the cracks terminate at these inclusions. Because the inner mantle containing the microcracks is corroded and is surrounded by microcrack-free outer mantle, microcracking is interpreted to reflect transient failure of the aggregate. Microcracking is argued to play a fundamental role in the continuation and enhancement of the SP-GBS creep during halokinesis of the Werra salt, because the transgranular cracks (1) provide the ingress of additional fluid in the grain boundary network when cross-cutting the FITs and (2) decrease grain size by splitting the grains. More over, the ingress of additional fluids into grain boundaries is also provided by non-conservative grain boundary migration that advanced into FITs bearing cores of grains. Described readjustments of the microstructure and mechanical and chemical feedbacks for the grain boundary diffusion flow in halite-brine system are proposed to be comparable to other rock-fluid or rock-melt aggregates deforming by the grain boundary sliding (GBS) coupled deformation mechanisms.

  10. Some deformation trends and topographic characteristics of tesserae on Venus

    NASA Technical Reports Server (NTRS)

    Price, Maribeth; Suppe, John

    1993-01-01

    Mapping of dominant trends of deformation and topographic analysis of tesserae reveal that (1) consistant patterns of deformation exist between individual tesserae; (2) regional deformation associated with coronae and rifts commonly overprints tesserae fabrics; (3) normalized area frequency plots of tesserae display a strongly bimodal distribution between -70 to 70 degrees latitude; and (4) the relief at tessera margins is relatively constant and independent of tessera elevation. We are continuing to expand these observations and test their implications for the formation of tesserae and for global models of deformation on Venus.

  11. Characteristics of tsunamis generated by 3D deformable granular landslides

    NASA Astrophysics Data System (ADS)

    Mohammed, F.; Fritz, H. M.; McFall, B.

    2010-12-01

    Landslides can trigger tsunamis with locally high amplitudes and runup, which can cause devastating effects in the near field region. The events of 1958 Lituya Bay, 1998 Papua New Guinea and 2006 Java tsunamis are reminders of the hazards associated with impulse waves. Tsunamis generated by granular landslides were studied in the three dimensional NEES tsunami wave basin (TWB) at Oregon State University (OSU) based on the generalized Froude similarity. A novel pneumatic landslide generator was deployed to simulate landslides with varying geometry and kinematics. Granular materials were used to model deformable landslides. Measurement techniques such as particle image velocimetry (PIV), multiple above and underwater video cameras, multiple acoustic transducer arrays (MTA), as well as resistance wave and runup gauges were applied. Tsunami wave generation and propagation is studied off a hill slope, in fjords and around curved headlands. The wave generation was characterized by an extremely unsteady three phase flow consisting of the slide granulate, water and air entrained into the flow. Landslide deformation is quantified and the slide kinematics with reference to slide surface velocity distribution and slide front velocity is obtained. Empirical equations for predicting the wave amplitude, period and wavelength are obtained. The generated waves depend on determined non-dimensional landslide and water body parameters such as the slide Froude number and relative slide shape at impact, among others. Attenuation functions of the leading wave crest amplitude, the lateral wave runup on the hill slope, the wave length and the time period were obtained to describe the wave behavior in the near field and to quantify the wave amplitude decay away from the landslide source. The measured wave celerity of the leading wave corresponds well to the solitary wave speed while the trailing waves are considerably slower in propagation. The individual waves in the wave train span from shallow to deep water depth regime. The energy conversion between landslide and waves is lower compared with 2D and solid block landslides due to radial spread of unidirectional landslide energy by the wave front. The slide characteristics measured in the experiment provide the landslide source for numerical landslide tsunami modeling. The measured landslide and tsunami data serve the validation and advancement of 3-dimensional numerical landslide tsunami and prediction models. Landslide impact and tsunami generation (Photo credit: Devin K. Daniels)

  12. Deterministic Multiaxial Creep and Creep Rupture Enhancements for CARES/Creep Integrated Design Code

    NASA Technical Reports Server (NTRS)

    Jadaan, Osama M.

    1998-01-01

    High temperature and long duration applications of monolithic ceramics can place their failure mode in the creep rupture regime. A previous model advanced by the authors described a methodology by which the creep rupture life of a loaded component can be predicted. That model was based on the life fraction damage accumulation rule in association with the modified Monkman-Grant creep rupture criterion. However, that model did not take into account the deteriorating state of the material due to creep damage (e.g., cavitation) as time elapsed. In addition, the material creep parameters used in that life prediction methodology, were based on uniaxial creep curves displaying primary and secondary creep behavior, with no tertiary regime. The objective of this paper is to present a creep life prediction methodology based on a modified form of the Kachanov-Rabotnov continuum damage mechanics (CDM) theory. In this theory, the uniaxial creep rate is described in terms of sum, temperature, time, and the current state of material damage. This scalar damage state parameter is basically an abstract measure of the current state of material damage due to creep deformation. The damage rate is assumed to vary with stress, temperature, time, and the current state of damage itself. Multiaxial creep and creep rupture formulations of the CDM approach are presented in this paper. Parameter estimation methodologies based on nonlinear regression analysis are also described for both, isothermal constant stress states and anisothermal variable stress conditions This creep life prediction methodology was preliminarily added to the integrated design code CARES/Creep (Ceramics Analysis and Reliability Evaluation of Structures/Creep), which is a postprocessor program to commercially available finite element analysis (FEA) packages. Two examples, showing comparisons between experimental and predicted creep lives of ceramic specimens, are used to demonstrate the viability of Ns methodology and the CARES/Creep program.

  13. Postseismic relaxation and transient creep

    NASA Astrophysics Data System (ADS)

    Savage, J. C.; Svarc, J. L.; Yu, Shui-Beih

    2005-11-01

    Postseismic deformation has been observed in the epicentral area following the 1992 Landers (M = 7.3), 1999 Chi-Chi (M = 7.6), 1999 Hector Mine (M = 7.1), 2002 Denali (M = 7.9), 2003 San Simeon (M = 6.5), and 2004 Parkfield (M = 6.0) earthquakes. The observations consist of repeated GPS measurements of the position of one monument relative to another (separation 100 km). The early observations (t < 0.1 year) are well fit by the function a' + c'log(t), where t is the time after the earthquake and a' and c' are constants chosen to fit the data. Because a log(t) time dependence is characteristic of transient (primary) creep, the early postseismic response may be governed by transient creep as Benioff proposed in 1951. That inference is provisional as the stress conditions prevailing in postseismic relaxation are not identical to the constant stress condition in creep experiments. The observed logarithmic time dependence includes no characteristic time that might aid in identifying the micromechanical cause.

  14. Postseismic relaxation and transient creep

    USGS Publications Warehouse

    Savage, J.C.; Svarc, J.L.; Yu, S.-B.

    2005-01-01

    Postseismic deformation has been observed in the epicentral area following the 1992 Landers (M = 7.3), 1999 Chi-Chi (M = 7.6), 1999 Hector Mine (M = 7.1), 2002 Denali (M = 7.9), 2003 San Simeon (M = 6.5), and 2004 Parkfield (M = 6.0) earthquakes. The observations consist of repeated GPS measurements of the position of one monument relative to another (separation ???100 km). The early observations (t < 0.1 year) are well fit by the function a' + c'log(t), where t is the time after the earthquake and a' and c' are constants chosen to fit the data. Because a log(t) time dependence is characteristic of transient (primary) creep, the early postseismic response may be governed by transient creep as Benioff proposed in 1951. That inference is provisional as the stress conditions prevailing in postseismic relaxation are not identical to the constant stress condition in creep experiments. The observed logarithmic time dependence includes no characteristic time that might aid in identifying the micromechanical cause.

  15. Deformation characteristics and time-dependent notch sensitivity of Udimet 700 at intermediate temperatures

    NASA Technical Reports Server (NTRS)

    Wilson, D. J.

    1975-01-01

    Time-dependent notch sensitivity of Udimet 700 sheet, bar, and investment castings was observed between 1000 and 1400 F (538-760 C) but not at 1600 F (871 C). As was the case for Modified Waspaloy, Waspaloy, Rene 41, Inconel 718, and TD-NiCr, it occurred when notched specimens were loaded below the yield strength and when creep deformation was localized. For each gamma-prime strengthened alloy and notched specimen geometry, a stress-average particle size zone can be defined to characterize the notch-sensitive behavior.

  16. Assessing the P-wave attenuation and phase velocity characteristics of fractured media based on creep and relaxation tests

    NASA Astrophysics Data System (ADS)

    Milani, Marco; Germn Rubino, J.; Mller, Tobias M.; Quintal, Beatriz; Holliger, Klaus

    2014-05-01

    Fractures are present in most geological formations and they tend to dominate not only their mechanical but also, and in particular, their hydraulic properties. For these reasons, the detection and characterization of fractures are of great interest in several fields of Earth sciences. Seismic attenuation has been recognized as a key attribute for this purpose, as both laboratory and field experiments indicate that the presence of fractures typically produces significant energy dissipation and that this attribute tends to increase with increasing fracture density. This energy loss is generally considered to be primarily due to wave-induced pressure diffusion between the fractures and the embedding porous matrix. That is, due to the strong compressibility contrast between these two domains, the propagation of seismic waves can generate a strong fluid pressure gradient and associated pressure diffusion, which leads to fluid flow and in turn results in frictional energy dissipation. Numerical simulations based on Biot's poroelastic wave equations are computationally very expensive. Alternative approaches consist in performing numerical relaxation or creep tests on representative elementary volumes (REV) of the considered medium. These tests are typically based on Biot's consolidation equations. Assuming that the heterogeneous poroelastic medium can be replaced by an effective, homogeneous viscoelastic solid, these numerical creep and relaxation tests allow for computing the equivalent seismic P-wave attenuation and phase velocity. From a practical point of view, an REV is typically characterized by the smallest volume for which rock physical properties are statistically stationary and representative of the probed medium in its entirety. A more general definition in the context of wavefield attributes is to consider an REV as the smallest volume over which the P-wave attenuation and phase velocity dispersion are independent of the applied boundary conditions. That is, the corresponding results obtained from creep and relaxation tests must be equivalent. For most analyses of media characterized by patchy saturation or double-porosity-type structures these two definitions are equivalent. It is, however, not clear whether this equivalence remains true in the presence of strong material contrasts as those prevailing in fractured rocks. In this work, we explore this question for periodically fractured media. To this end, we build a medium composed of infinite replicas of a unit volume containing one fracture. This unit volume coincides with the smallest possible volume that is statistically representative of the whole. Then, we perform several creep and relaxation tests on samples composed of an increasing number of these unit volumes. We find that the wave field signatures determined from relaxation tests are independent from the number of unit volumes. Conversely, the P-wave attenuation and phase velocity characteristics inferred from creep tests are different and vary with the number of unit volumes considered. Quite interestingly, the creep test results converge with those of the relaxation tests as the number of unit volumes increases. These findings are expected to have direct implications for corresponding laboratory measurements as well as for our understanding of seismic wave propagation in fractured media.

  17. Analysis of Slip Activity and Deformation Modes in Tension and Tension-Creep Tests of Cast Mg-10Gd-3Y-0.5Zr (Wt Pct) at Elevated Temperatures Using In Situ SEM Experiments

    NASA Astrophysics Data System (ADS)

    Wang, Huan; Boehlert, Carl J.; Wang, Qudong; Yin, Dongdi; Ding, Wenjiang

    2016-03-01

    The tension and tension-creep deformation behavior at elevated temperatures of a cast Mg-10Gd-3Y-0.5Zr (wt pct, GW103) alloy was investigated using in situ scanning electron microscopy. The tests were performed at temperatures ranging from 473 K to 598 K (200 °C to 325 °C). The active slip systems were identified using an EBSD-based slip trace analysis methodology. The results showed that for all of the tests, basal slip was the most likely system to be activated, and non-basal slip was activated to some extent depending on the temperature. No twinning was observed. For the tension tests, non-basal slip consisted of ~35 pct of the deformation modes at low temperatures (473 K and 523 K (200 °C and 250 °C)), while non-basal slip accounted for 12 and 7 pct of the deformation modes at high temperatures (573 K and 598 K (300 °C and 325 °C)), respectively. For the tension-creep tests, non-basal slip accounted for 31 pct of the total slip systems at low temperatures, while this value decreased to 10 to 16 pct at high temperatures. For a given temperature, the relative activity for prismatic slip in the tension-creep tests was slightly greater than that for the tension tests, while the activity for pyramidal slip was lower. Slip-transfer in neighboring grains was observed for the low-temperature tests. Intergranular cracking was the main cracking mode, while some intragranular cracks were observed for the tension-creep tests at high temperature and low stress. Grain boundary ledges were prevalently observed for both the tension and tension-creep tests at high temperatures, which suggests that besides dislocation slip, grain boundary sliding also contributed to the deformation.

  18. Microstructure and creep characteristics of dissimilar T91/TP316H martensitic/austenitic welded joint with Ni-based weld metal

    SciTech Connect

    Falat, Ladislav; Svoboda, Milan; Vyrostkova, Anna; Petryshynets, Ivan; Sopko, Martin

    2012-10-15

    This paper deals with characterization of microstructure and creep behavior of dissimilar weldment between the tempered martensitic steel T91 and the non-stabilized austenitic steel TP316H with Ni-based weld metal (Ni WM). Microstructure analyses were performed using light microscopy, scanning and transmission electron microscopy and energy-dispersive X-ray spectroscopy. The martensitic part of the welded joint exhibited a wide heat-affected zone (HAZ) with typical microstructural gradient from its coarse-grained to the fine-grained/intercritical region. In contrast, the HAZ of austenitic steel was limited to only a narrow region with coarsened polygonal grains. The microstructure of Ni WM was found to be very heterogeneous with respect to the size, morphology and distribution of grain boundaries and MC-type precipitates as a result of strong weld metal dilution effects and fast non-equilibrium solidification. Cross-weld creep tests were carried out in a temperature range from 600 to 650 Degree-Sign C at applied stresses from 60 to 140 MPa. The obtained values of apparent stress exponents and creep activation energies indicate thermally activated dislocation glide to be the governing creep deformation mechanism within the range of used testing conditions. The creep samples ruptured in the T91 intercritical HAZ region by the 'type IV cracking' failure mode and the creep fracture mechanism was identified to be the intergranular dimple tearing by microvoid coalescence at grain boundaries. The TEM observations revealed pronounced microstructural differences between the critical HAZ region and the T91 base material before as well as after the creep exposure. - Highlights: Black-Right-Pointing-Pointer Phase transformations affect the microstructures of T91 and TP316H HAZ regions. Black-Right-Pointing-Pointer High weld metal dilution results in heterogeneous microstructure with MC carbides. Black-Right-Pointing-Pointer Creep behavior of the studied weldment is controlled by its martensitic T91 part. Black-Right-Pointing-Pointer The lowest hardness of T91 ICHAZ region corresponds with its lowest creep strength.

  19. Small Strain Deformation Characteristics of Granular Materials in Torsional Shear and Triaxial Tests with Local Deformation Measurements

    NASA Astrophysics Data System (ADS)

    Kiyota, T.; De Silva, L. I. N.; Sato, T.; Koseki, J.

    The soil behaviour under normal working loads usually mobilizes strain increments that are less than 0.1 %. Therefore it is very important to measure the small deformation of soil by laboratory experiments accurately. Among others, the local deformation transducer (LDT) has been used to measure locally small deformation of cylindrical or rectangular specimens in triaxial tests. In this study, a hollow cylindrical specimen was used in torsional shear and triaxial tests. By using a modified version of LDT, called PLDT (Pin-typed LDT), to comply with shear deformation of hollow cylindrical specimen under torsional loading, it was confirmed that the modified version could be successfully used to evaluate quasi-elastic deformation properties. The small deformation characteristics of Toyoura sand, Hime gravel and glass beads were investigated using both PLDTs for the local static measurement and gap sensors and a potentiometer for the external static measurement. In addition, a dynamic measurement system by using a set of small triggers and accelerometers was used to evaluate S wave velocity of glass beads. The specimens at different densities were subjected to small vertical and torsional cyclic loadings during otherwise isotropic consolidation from 50 kPa to 400 kPa and isotropic unloading from 400 kPa to 50 or 100 kPa.

  20. Transient Creep of a Composite Lower Crust. 2; A Polymineralic Basis for Rapidly Evolving Postseismic Deformation Modes

    NASA Technical Reports Server (NTRS)

    Ivins, Erik R.

    1996-01-01

    Postseismic horizontal strain and displacement following the June 28, 1992, Landers, California, earthquake (M(sub W) 7.3) is broad scale and cannot be explained solely by delayed afterslip located at the rupturing fault trace. Both the observed strain at Pifion Flat Observatory (PFO) and observed Global Positioning System receiver velocities evolve rapidly after the Landers-Big Bear earthquake sequence. The observed exponential decay of these motions, with timescales of 4-34 days, may reflect a soft creep rheology in the lower crust and brittle-ductile transition zone or even within the seismogenic crust itself. Here a simple model of a two-dimensional screw dislocation in a layered Maxwell viscoelastic Earth is employed in conjunction with a composite rheology to demonstrate that the short timescale transient response modes (approx. = 4-34 days) are consistent with the behavior of a biviscous lower crust. The lowest viscosity of this system is derivable from laboratory experimental data on the long-term creep of natural quarztites, and the highest viscosity is consistent with isostasy-related lower crustal flow in a continental extensional tectonic environment. The model predicts significant stress relaxation at the base of the seismogenic crust. Near the base of the seismogenic zone, and about 4 km away from the mainshock, the rate of predicted relaxation is of the order of 0.01 MPa/ d during the first 20 days of postseismic flow. Oblate spheroidal inclusions at 5% concentration levels that are both aligned and fairly flat in shape and that have a viscosity of 3-4 x 10(exp 15) Pa s are consistent with both the amplitude and decay time of horizontal crustal strain observed at PFO after the Landers mainshock. It is speculated that the structures exposed in cross sections and in seismic reflection profiles of the lower crust that have mylonitic associations are, in part, the cause of such rapid postseismic evolution in southeastern California. Unmylonitized quartz-rich rock at sufficiently elevated temperatures could also contribute to the rapid decay modes.

  1. Increased Variability of Bone Tissue Mineral Density Resulting from Estrogen Deficiency Influences Creep Behavior in a Rat Vertebral Body

    PubMed Central

    Kim, Do-Gyoon; Navalgund, Anand R.; Tee, Boon Ching; Noble, Garrett J.; Hart, Richard T.; Lee, Hye Ri

    2012-01-01

    Progressive vertebral deformation increases the fracture risk of a vertebral body in the postmenopausal patient. Many studies have observed that bone can demonstrate creep behavior, defined as continued time-dependent deformation even when mechanical loading is held constant. Creep is a characteristic of viscoelastic behavior, which is common in biological materials. We hypothesized that estrogen deficiency-dependent alteration of the mineral distribution of bone at the tissue level could influence the progressive postmenopausal vertebral deformity that is observed as the creep response at the organ level. The objective of this study was thus to examine whether the creep behavior of vertebral bone is changed by estrogen deficiency, and to determine which bone property parameters are responsible for the creep response of vertebral bone at physiological loading levels using an ovariectomized (OVX) rat model. Correlations of creep parameters with bone mineral density (BMD), tissue mineral density (TMD) and architectural parameters of both OVX and sham surgery vertebral bone were tested. As the vertebral creep was not fully recovered during the post-creep unloading period, there was substantial residual displacement for both the sham and OVX groups. A strong positive correlation between loading creep and residual displacement was found (r=0.868, p<0.001). Of the various parameters studied, TMD variability was the parameter that best predicted the creep behavior of the OVX group (p<0.038). The current results indicated that creep caused progressive, permanent reduction in vertebral height for both the sham and OVX groups. In addition, estrogen deficiency-induced active bone remodeling increased variability of trabecular TMD in the OVX group. Taken together, these results suggest that increased variability of trabecular TMD resulting from high bone turnover influence creep behavior of the OVX vertebrae. PMID:22944606

  2. Creep and creep-rupture behavior of Alloy 718

    SciTech Connect

    Brinkman, C.R.; Booker, M.K.; Ding, J.L.

    1991-01-01

    Data obtained from creep and creep-rupture tests conducted on 18 heats of Alloy 718 were used to formulate models for predicting high temperature time dependent behavior of this alloy. Creep tests were conducted on specimens taken from a number of commercial product forms including plate, bar, and forgoing material that had been procured and heat treated in accordance with ASTM specifications B-670 or B-637. Data were obtained over the temperature range of 427 to 760{degree}C ad at test times to about 87,000 h. Comparisons are given between experimental data and the analytical models. The analytical models for creep-rupture included one based on lot-centering regression analysis and two based on the Minimum Commitment Method. A master'' curve approach was used to develop and equation for estimating creep deformation up to the onset of tertiary creep. 11 refs., 13 figs.

  3. Fracture Morphology and Local Deformation Characteristics in the Metallic Glass Matrix Composite Under Tension

    NASA Astrophysics Data System (ADS)

    Wang, Y. S.; Sun, X. H.; Hao, G. J.; Guo, Z. X.; Zhang, Y.; Lin, J. P.; Sui, M. L.; Qiao, J. W.

    2015-11-01

    Fracture and deformation characteristics of the Ti-based metallic glass matrix composite have been studied by the tensile test and the in situ TEM tension test. Typically, the composite exhibits the high strength and considerable plasticity. Microscopically, it was found that shear deformation zone formed at the crack tip in glass phase, which can bring about quick propagation of shear bands. However, the plastic deformation zone nearby the crack tip in dendrites will postpone or retard the crack extension by dislocations. The attributions of micro-deformations to mechanical properties of composites were discussed.

  4. Creep and creep fracture of zirconium and zirconium alloys

    NASA Astrophysics Data System (ADS)

    Hayes, Troy Allyn

    The creep and creep failure mechanisms for zirconium and zirconium alloys have not been established, yet these properties are required to establish safe conditions for the interim dry storage of spent nuclear fuel. The purpose of this research, then, is to determine the relevant creep and creep fracture mechanisms controlling the deformation and failure of zirconium and zirconium alloys at elevated temperatures. Currently, the maximum allowable temperatures for the storage of spent nuclear fuel are defined by the Nuclear Regulatory Commission based on a limited set of experimental data. Recent changes in regulations will be evaluated and recommendations made regarding their applicability. Various studies in the past have reported that zirconium and zirconium alloys exhibit anomalous creep properties. A detailed analysis of the creep properties of zirconium and zirconium alloys is presented based on an extensive literature review. Next, developments in creep fracture phenomena in engineering materials over the past several decades will be discussed and related to the creep fracture of zirconium alloys. As will be discussed, the mechanism for plasticity can be intimately tied to the fracture mechanism. The results of uniaxial creep tests on zirconium at temperatures of 350--700C and stresses of 8--70 MPa and uniaxial creep tests on Zircaloy-2 at temperatures of 300--600C and stresses of 24--382 MPa and subsequent microstructural investigation using a scanning electron microscope will be discussed, particularly as relevant to the fracture mechanisms for this alloy.

  5. Micromechanisms of creep in clay-rich gouge from the Central Deforming Zone of the San Andreas Fault

    NASA Astrophysics Data System (ADS)

    French, M. E.; Chester, F. M.; Chester, J. S.

    2015-02-01

    We report the strength and constitutive behavior of gouge sampled from the Central Deforming Zone (CDZ) of the San Andreas Fault. Layers of flaked CDZ gouge were sheared in the triaxial saw cut configuration using the stress relaxation technique to measure the gouge strength over 4 orders of magnitude in shear strain rate and at rates as low as 5 10-10s-1 and within an order of magnitude of in situ rates. Deformation conditions correspond to the in situ effective normal stress (100 MPa) and temperature (65 to 120C) at the sampling depth of 2.7 km. Gouge was sheared dry and with brine pore fluid at 25 MPa pore pressure. Dry gouge is stronger and more rate strengthening than brine-saturated gouge. Brine-saturated CDZ gouge strengthens with increasing strain rate and decreasing temperature, and the dependencies of strength on strain rate and temperature increase at rates below 5 10-9s-1. At strain rates greater than 5 10-9s-1, the rate dependence is consistent with previous studies on the CDZ gouge conducted at even higher rates. The increase in rate dependence below 5 10-9s-1 indicates a change in the rate-controlling deformation mechanism. The magnitude of the friction rate dependence parameter, a, and the temperature sensitivity of a are consistent with crystal plasticity of the phyllosilicates. We hypothesize a micromechanical model for the CDZ gouge whereby a transition from fracture and delamination-accommodated frictional flow to crystal plasticity-accommodated frictional flow occurs with decreasing strain rate.

  6. Influence of the Temperature of Gases on the Deformation Characteristics of Moving Water Droplets

    NASA Astrophysics Data System (ADS)

    Antonov, D. V.; Volkov, R. S.; Zhdanova, A. O.; Kuznetsov, G. V.; Strizhak, P. A.

    2015-07-01

    An experimental analysis of the influence of the temperature of gases on the deformation characteristics of water droplets moving through them is carried out. High-speed (up to 105 frames per second) photography with video cameras and cross-correlation complexes, as well as panoramic optical methods of recording the motion parameters of gaseous and liquid flows, were used. The laws governing the movement of water droplets through gases with a temperature of about 1100 K and in air at relatively low (to 280 K) and moderate (about 300 K) temperatures have been studied. The principal characteristics of the deformation of water droplets (duration, extension, and amplitudes of "deformation cycles") have been established. The differences in the characteristic shapes of droplets during their motion in gaseous media (at different temperatures of the latter) have been determined. The times during which droplets retain a certain shape in the deformation process have been calculated.

  7. Present-day deformation along the El Pilar Fault in eastern Venezuela: Evidence of creep along a major transform boundary

    NASA Astrophysics Data System (ADS)

    Jouanne, Franois; Audemard, Franck A.; Beck, Christian; Van Welden, Aurlien; Ollarves, Reinaldo; Reinoza, Carlos

    2011-05-01

    The right-lateral strike-slip El Pilar Fault is one of the major structures that accommodate the relative displacement between the Caribbean and South-America Plates. This fault, which trends East-West along the northeastern Venezuela margin, is a seismogenic source, and shows numerous evidence for active tectonics, including deformation of the Quaternary sediments filling the Cariaco Gulf. Because the main El Pilar Fault strand belongs to a set of strike-slip faults and thrusts between the stable Guyana shield (South) and the Caribbean oceanic floor (North), a GPS network was designed and installed to measure the relative motion of the El Pilar Fault and other faults. The results obtained from the comparison of 2003 and 2005 surveys indicate: (i) a lack of significant displacement (especially shortening) in the Serrania del Interior (Neogene cordillera overthrusted above the Guyana craton), (ii) an eastward displacement (relative to fixed south America plate) up to 22 mm/year of benchmarks located north of the El Pilar Fault. Velocities simulations using dislocations in an elastic half-space show: (1) the concentration along the El Pilar Fault of the whole Caribbean-South America relative displacement, (2) the existence of an important component of aseismic displacement along the upper part of the El Pilar Fault. Between 12 km depth and the surface, only 40% of displacement is locked for the western segment and 50% for the eastern segment. This last phenomenon may be related to the existence of serpentinite lenses along the fault zone as observed for segments of San Andreas and North Anatolian faults.

  8. Deformations of classical Lie algebras with homogeneous root system in characteristic two. I

    NASA Astrophysics Data System (ADS)

    Chebochko, N. G.

    2005-10-01

    Spaces of local deformations of classical Lie algebras with a homogeneous root system over a field K of characteristic 2 are studied. By a classical Lie algebra over a field K we mean the Lie algebra of a simple algebraic Lie group or its quotient algebra by the centre. The description of deformations of Lie algebras is interesting in connection with the classification of the simple Lie algebras.

  9. Powder metallurgy processing and deformation characteristics of bulk multimodal nickel

    SciTech Connect

    Farbaniec, L.; Dirras, G.; Krawczynska, A.; Mompiou, F.; Couque, H.; Naimi, F.; Bernard, F.; Tingaud, D.

    2014-08-15

    Spark plasma sintering was used to process bulk nickel samples from a blend of three powder types. The resulting multimodal microstructure was made of coarse (average size ∼ 135 μm) spherical microcrystalline entities (the core) surrounded by a fine-grained matrix (average grain size ∼ 1.5 μm) or a thick rim (the shell) distinguishable from the matrix. Tensile tests revealed yield strength of ∼ 470 MPa that was accompanied by limited ductility (∼ 2.8% plastic strain). Microstructure observation after testing showed debonding at interfaces between the matrix and the coarse entities, but in many instances, shallow dimples within the rim were observed indicating local ductile events in the shell. Dislocation emission and annihilation at grain boundaries and twinning at crack tip were the main deformation mechanisms taking place within the fine-grained matrix as revealed by in-situ transmission electron microscopy. Estimation of the stress from loop's curvature and dislocation pile-up indicates that dislocation emission from grain boundaries and grain boundary overcoming largely contributes to the flow stress. - Highlights: • Bulk multi-modal Ni was processed by SPS from a powder blend. • Ultrafine-grained matrix or rim observed around spherical microcrystalline entities • Yield strength (470 MPa) and ductility (2.8% plastic strain) were measured. • Debonding was found at the matrix/microcrystalline entity interfaces. • In-situ TEM showed twinning, dislocation emission and annihilation at grain boundaries.

  10. Analysis of creep behavior in thermoplastics based on visco-elastic theory

    NASA Astrophysics Data System (ADS)

    Sakai, Takenobu; Somiya, Satoshi

    2011-08-01

    Plastics and fiber-reinforced plastics (FRP) are used in the aerospace industry because of their mechanical properties. However, despite their excellent high-temperature mechanical properties, plastics and FRP eventually deform visco-elastically at high temperatures. Most of the research has focused on the creep behavior of FRPs, but few studies have investigated the linear visco-elastic behavior. Linear visco-elastic behavior and non-linear visco-elastic behavior occur with physical aging in these plastics. In this study, the non-linear visco-elastic behavior of plastics and FRP was investigated based on the bending creep deformation of polycarbonate (PC) and polyoxymethylene (POM). Moreover, the effects of the fiber volume fraction on the creep characteristics were investigated using glass fiber-reinforced polycarbonate (GFRPC). The creep deformation was calculated using the linear visco-elastic theory based on these effects, and comparison between experimental and estimated data showed that the creep analysis sufficiently predicted the creep behavior.

  11. Constraining the characteristics of tsunami waves from deformable submarine slides

    NASA Astrophysics Data System (ADS)

    Weiss, R.; Krastel, S.; Anasetti, A.; Wuennemann, K.

    2012-12-01

    As a marine hazard, submarine slope failures have the potential to directly destroy offshore infrastructure, and, if a tsunami is generated, it also endangers the life of those who live and work at the coastline. The hazard and risk from tsunamis generated by submarine mass failure is difficult to quantify and evaluate due to difficulties to estimate the time of trigger for submarine slide bodies, and the problems to constrain the characteristics of the triggered submarine landslide. The missing age constraint and the unconstrained tsunami-wave characteristics generate unquantifiable uncertainties in hazard assessments. To lower the uncertainty from the unconstrained tsunami-characteristic, we present a method that determines material parameters for the slide body to constrain the generated tsunami waves with an iterative method. Our method employs the mapped distribution of landslide run-out masses and their comparison with simulations. It assumes that the slide material can be approximated by bulk values during the slide motion. The free parameter that will be changed during in iterations is the viscosity of the slide body. The goal of the procedure is to find the optimal viscosity, which represents the viscosity for which the slide body matches well with the mapped slide run-out masses. The tsunami waves generated in the simulations employing the optimal viscosity are then considered constrained within the framework of our work. While we understand that viscosity does not accurately describe the dynamics of the slide body, we argue that viscosity can be employed as a first-order approximation to constrain the tsunami wave characteristics. To demonstrate our method, we make use of Valdes slide run-out masses off the Chilean coast. We show the difference in tsunami characteristics for slides whose viscosity is too low, too high and optimal. Furthermore, we will present an overview on how these differences result in dramatically different wave amplitudes as functions of the distance to the landslide-trigger area in general and for the Chilean coast due to the Valdes slide.

  12. Precipitation Behavior in the Heat-Affected Zone of Boron-Added 9Cr-3W-3Co Steel During Post-Weld Heat Treatment and Creep Deformation

    NASA Astrophysics Data System (ADS)

    Liu, Yuan; Tsukamoto, Susumu; Sawada, Kota; Tabuchi, Masaaki; Abe, Fujio

    2015-05-01

    In the previous paper, we demonstrated that the addition of boron was effective in preventing type IV failure due to suppression of grain refinement in the heat-affected zone at the peak temperature of around AC3 (AC3 HAZ). However, some fine prior austenite grains (PAGs) still remained around the coarse PAG boundaries, and these fine PAGs may affect the creep property of the welded joint. In the present study, the effect of these fine PAGs on the creep property of the boron-added 9Cr-3Co-3W steel (B steel) Ac3 HAZ is investigated. Different heat treatments are carried out on B steel base metal to form different Ac3 HAZ-simulated microstructures of coarse PAG with and without fine PAGs. Ac3 HAZ microstructure shows that a lot of M23C6 carbides are formed at the block boundary in the interior of coarse PAG. On the other hand, few M23C6 carbides are formed at the fine PAG boundaries, but a number of ? phases (W6Fe7 type) cover the boundary. The formation of ? phase retards the recovery of dislocation at the fine PAG boundary and contributes to stabilizing the microstructure in the primary and transient creep regions. The ? phase transforms to the Laves phase during creep. As the growth rate of Laves phase is higher than that of M23C6 carbides during creep, the creep strength of fine PAG boundary, which is strengthened only by Laves phase, becomes a little bit lower than the other boundaries strengthened by M23C6 carbides after long-term creep. The mismatch of creep strength between the fine PAG boundary and the matrix should be taken into account to attain an excellent long-term creep property of the B steel welded joint.

  13. Analysis of the Deformation Behavior in Tension and Tension-Creep of Ti-3Al-2.5V (wt pct) at 296 K and 728 K (23 C and 455 C) Using In Situ SEM Experiments

    NASA Astrophysics Data System (ADS)

    Li, Hongmei; Boehlert, Carl J.; Bieler, Thomas R.; Crimp, Martin A.

    2014-12-01

    The deformation behavior of a Ti-3Al-2.5V (wt pct) near-? alloy was investigated during in situ deformation inside a scanning electron microscopy (SEM). Two plates with distinct textures were examined. Tensile experiments were performed at 296 K and 728 K (455 C) (~0.4 T m), while a tensile-creep experiment was performed at 728 K (455 C) and 180 MPa ( ?/ ? ys = 0.72). The active deformation systems were identified in the ? phase using electron backscattered diffraction based slip-trace analysis and SEM images of the surface. Prismatic slip deformation was the dominant slip mode observed for all the experiments in both plates, which was supported by a critical resolved shear stress (CRSS) ratio analysis. However, due to the texture of plate 1, which strongly favored the activation of prismatic slip, the percentages of prismatic slip activity for specimens from plate 1 tested at 296 K and 728 K (23 C and 455 C) were higher than the specimens from plate 2 under the same testing conditions. T1 twinning was an active deformation mode at both 296 K and 728 K (23 C and 455 C), but the extent of twinning activity decreased with increased temperature. T1 twinning was more frequently observed in specimens from plate 2, which exhibited a higher fraction of twinning systems favoring activation at both 296 K and 728 K (23 C and 455 C). The tension-creep experiment revealed less slip and more grain boundary sliding than in the higher strain rate tensile experiments. Using a previously demonstrated bootstrapping statistical analysis methodology, the relative CRSS ratios of prismatic, pyramidal < a>, pyramidal < c+ a>, and T1 twinning deformation systems compared with basal slip were calculated and discussed in light of similar measurements made on CP Ti and Ti-5Al-2.5Sn (wt pct).

  14. Deterministic and Probabilistic Creep and Creep Rupture Enhancement to CARES/Creep: Multiaxial Creep Life Prediction of Ceramic Structures Using Continuum Damage Mechanics and the Finite Element Method

    NASA Technical Reports Server (NTRS)

    Jadaan, Osama M.; Powers, Lynn M.; Gyekenyesi, John P.

    1998-01-01

    High temperature and long duration applications of monolithic ceramics can place their failure mode in the creep rupture regime. A previous model advanced by the authors described a methodology by which the creep rupture life of a loaded component can be predicted. That model was based on the life fraction damage accumulation rule in association with the modified Monkman-Grant creep ripture criterion However, that model did not take into account the deteriorating state of the material due to creep damage (e.g., cavitation) as time elapsed. In addition, the material creep parameters used in that life prediction methodology, were based on uniaxial creep curves displaying primary and secondary creep behavior, with no tertiary regime. The objective of this paper is to present a creep life prediction methodology based on a modified form of the Kachanov-Rabotnov continuum damage mechanics (CDM) theory. In this theory, the uniaxial creep rate is described in terms of stress, temperature, time, and the current state of material damage. This scalar damage state parameter is basically an abstract measure of the current state of material damage due to creep deformation. The damage rate is assumed to vary with stress, temperature, time, and the current state of damage itself. Multiaxial creep and creep rupture formulations of the CDM approach are presented in this paper. Parameter estimation methodologies based on nonlinear regression analysis are also described for both, isothermal constant stress states and anisothermal variable stress conditions This creep life prediction methodology was preliminarily added to the integrated design code CARES/Creep (Ceramics Analysis and Reliability Evaluation of Structures/Creep), which is a postprocessor program to commercially available finite element analysis (FEA) packages. Two examples, showing comparisons between experimental and predicted creep lives of ceramic specimens, are used to demonstrate the viability of this methodology and the CARES/Creep program.

  15. Nanogranular origin of concrete creep

    PubMed Central

    Vandamme, Matthieu; Ulm, Franz-Josef

    2009-01-01

    Concrete, the solid that forms at room temperature from mixing Portland cement with water, sand, and aggregates, suffers from time-dependent deformation under load. This creep occurs at a rate that deteriorates the durability and truncates the lifespan of concrete structures. However, despite decades of research, the origin of concrete creep remains unknown. Here, we measure the in situ creep behavior of calcium–silicate–hydrates (C–S–H), the nano-meter sized particles that form the fundamental building block of Portland cement concrete. We show that C–S–H exhibits a logarithmic creep that depends only on the packing of 3 structurally distinct but compositionally similar C–S–H forms: low density, high density, ultra-high density. We demonstrate that the creep rate (≈1/t) is likely due to the rearrangement of nanoscale particles around limit packing densities following the free-volume dynamics theory of granular physics. These findings could lead to a new basis for nanoengineering concrete materials and structures with minimal creep rates monitored by packing density distributions of nanoscale particles, and predicted by nanoscale creep measurements in some minute time, which are as exact as macroscopic creep tests carried out over years. PMID:19541652

  16. Utilizing microstructural characteristics to derive insights into deformation and annealing behaviour: Numerical simulations, experiments and nature

    NASA Astrophysics Data System (ADS)

    Piazolo, Sandra; Montagnat, Maurine; Prakash, Abhishek; Borthwick, Verity; Evans, Lynn; Griera, Albert; Bons, Paul D.; Svahnberg, Henrik; Prior, David J.

    2015-04-01

    Understanding the influence of the pre-existing microstructure on subsequent microstructural development is pivotal for the correct interpretation of rocks and ice that stayed at high homologous temperatures over a significant period of time. The microstructural behaviour of these materials through time has an important bearing on the interpretation of characteristics such as grain size, for example, using grain size statistics to detect former high strain zones that remain at high temperatures but low stress. We present a coupled experimental and modelling approach to better understand the evolution of recrystallization characteristics as a function of deformation-annealing time paths in a material with a high viscoplastic anisotropy e.g. polycrystalline ice and magnesium alloys. Deformation microstructures such as crystal bending, subgrain boundaries, grain size variation significantly influence the deformation and annealing behaviour of crystalline material. For numerical simulations we utilize the microdynamic modelling platform, Elle (www.elle.ws), taking local microstructural evolution into account to simulate the following processes: recovery within grains, rotational recrystallization, grain boundary migration and nucleation. We first test the validity of the numerical simulations against experiments, and then use the model to interpret microstructural features in natural examples. In-situ experiments are performed on laboratory grown and deformed ice and magnesium alloy. Our natural example is a deformed then recrystallized anorthosite from SW Greenland. The presented approach can be applied to many other minerals and crystalline materials.

  17. EBSD investigation of the microstructure and texture characteristics of hot deformed duplex stainless steel.

    PubMed

    Cizek, P; Wynne, B P; Rainforth, W M

    2006-05-01

    The microstructure and crystallographic texture characteristics were studied in a 22Cr-6Ni-3Mo duplex stainless steel subjected to plastic deformation in torsion at a temperature of 1000 degrees C using a strain rate of 1 s(-1). High-resolution EBSD was successfully used for precise phase and substructural characterization of this steel. The austenite/ferrite ratio and phase morphology as well as the crystallographic texture, subgrain size, misorientation angles and misorientation gradients corresponding to each phase were determined over large sample areas. The deformation mechanisms in each phase and the interrelationship between the two are discussed. PMID:16774517

  18. Vortex and characteristics of prestrained type-II deformable superconductors under magnetic fields

    NASA Astrophysics Data System (ADS)

    Ma, Zeling; Wang, Xingzhe; Zhou, Youhe

    2016-04-01

    Based on the time-dependent Ginzburg-Landau (TDGL) theory and the linear deformation theory, we present a numerical investigation of magnetic vortex characteristics of a type-II deformable superconductor with prestrain. The effect of prestrain on the wave function, vortex dynamics and energy density of a superconducting film is analyzed by solving the nonlinear TDGL equations in the presence of magnetic field. The results show that the prestrain has a remarkable influence on the magnetic vortex distribution and the vortex dynamics, as well as value of wave function of the superconductor. The different prestrains, i.e., pre-given compression and tension strains, result in dissimilar characteristics on a half-plane of deformable superconductor in an applied magnetic field, and the vortex distribution and entrance in a two dimensional superconducting film. The studies demonstrated that the compression prestrain may speed up the vortexes entering into the region of the superconducting film and increases the vortex number in comparison with those of free-prestrain case, while the tension prestrain shows the reversal features. The energy density and spectrum in the superconductor are further demonstrated numerically and discussed. The present investigation is an attempt to give insight into the superconductivity and electromagnetic characteristics taking into account the elastic deformation in superconductors.

  19. Deformation characteristics of {delta} phase in the delta-processed Inconel 718 alloy

    SciTech Connect

    Zhang, H.Y.; Zhang, S.H.; Cheng, M.; Li, Z.X.

    2010-01-15

    The hot working characteristics of {delta} phase in the delta-processed Inconel 718 alloy during isothermal compression deformation at temperature of 950 deg. C and strain rate of 0.005 s{sup -1}, were studied by using optical microscope, scanning electron microscope and quantitative X-ray diffraction technique. The results showed that the dissolution of plate-like {delta} phase and the precipitation of spherical {delta} phase particles coexisted during the deformation, and the content of {delta} phase decreased from 7.05 wt.% to 5.14 wt.%. As a result of deformation breakage and dissolution breakage, the plate-like {delta} phase was spheroidized and transferred to spherical {delta} phase particles. In the center with largest strain, the plate-like {delta} phase disappeared and spherical {delta} phase appeared in the interior of grains and grain boundaries.

  20. Estyuninky's Deformation Characteristics of the Iron-Ore Deposit by Gravimetric Means

    NASA Astrophysics Data System (ADS)

    Vandysheva, Ksenya; Filatov, Vladimir

    2013-04-01

    Gravitation is the main energy source of many processes which happen in crust. Gravity possesses the leading role in structurization; it defines a tectonic broken state and permeability of the geological medium, having significant importance at an ore deposition. Because of the gravitation density naturally changes, permeability and other properties of the geological medium changes too. Presence in crust of density heterogeneity of a various form and the sizes and properties change, show its compound stress of deformation condition. Studying of the deformations caused by gravitation, represents great expected and research interest. Theoretical basis of studying of these deformations consists on ratios between components of a pure tensor deformation and its first invariant -dilatation and results of measurement of gravity force. The method of deformation studying of the geological medium, developed on this basis, was called a method of the tektonophysic analysis of a gravitational field (MTPAGF). The detailed analysis of results of MTPAGF was made for the region of the Estyuninsky iron-ore deposit. The deposit region is characterized by a reversed dilatation. The zero isoline of dilatation divides it into two parts. To the east of this isoline where there is a deposit, a dilatation positive and rather small size. To the west - a dilatation negative and it increases as approaching a protrusion. Thus, to the east of the zero isoline the geological medium is in stretching mode, which promote relative expansion of the medium, improvement of its permeability. Thanks to it favorable conditions for an ore deposition here were created. To the west f the zero isoline medium is in a compression mode. Therefore it is characterized by smaller permeability. The border of change of a sign of a dilatation probably was important a role of the peculiar deformation barrier blocking migration through it of ore substance. It is possible to make the following conclusion of the analysis of deformation characteristics of the geological medium: small values of principal values of deformation and positive dilatation and, as a result, low level of specific energy of volume deformation, can evidence and to rather low tendency of the medium to destruction. As the deposit is located in the medium with such deformation properties, so there is some optimum broken state (permeability) of the medium optimum for an ore deposition. Extreme cases: very small and very big permeability complicate development of this process. In a little permeable medium it doesn't go at all, in very permeable - (at lack of screens) the disseminated or interspersed mineralization is formed. That work was supported by grant RFBR 10-05-00013.

  1. Electrochemical control of creep in nanoporous gold

    SciTech Connect

    Ye, Xing-Long; Jin, Hai-Jun

    2013-11-11

    We have investigated the mechanical stability of nanoporous gold (npg) in an electrochemical environment, using in situ dilatometry and compression experiments. It is demonstrated that the gold nano-ligaments creep under the action of surface stress which leads to spontaneous volume contractions in macroscopic npg samples. The creep of npg, under or without external forces, can be controlled electrochemically. The creep rate increases with increasing potential in double-layer potential region, and deceases to almost zero when the gold surface is adsorbed with oxygen. Surprisingly, we also noticed a correlation between creep and surface diffusivity, which links the deformation of nanocrystals to mobility of surface atoms.

  2. Creep behavior of uranium carbide-based alloys

    NASA Technical Reports Server (NTRS)

    Seltzer, M. S.; Wright, T. R.; Moak, D. P.

    1975-01-01

    The present work gives the results of experiments on the influence of zirconium carbide and tungsten on the creep properties of uranium carbide. The creep behavior of high-density UC samples follows the classical time-dependence pattern of (1) an instantaneous deformation, (2) a primary creep region, and (3) a period of steady-state creep. Creep rates for unalloyed UC-1.01 and UC-1.05 are several orders of magnitude greater than those measured for carbide alloys containing a Zr-C and/or W dispersoid. The difference in creep strength between alloyed and unalloyed materials varies with temperature and applied stress.

  3. Automatic Deformation Inspection Method for Digital Aerial Imagery Based on Statistical Characteristics

    NASA Astrophysics Data System (ADS)

    Yaohua, Y.; Yuan, Y.; Hai, S.; Mingjing, M.

    2013-05-01

    The geometric distortion of the push-broom digital aerial imagery can be rectified according to the data of the inertial measurement unit (IMU). The low precision of IMU data will cause the undulant wavelike twist deformations of the push-broom digital aerial images after geometric rectification, directly influencing the authenticity and liability of images and their practical applications. At present, the image deformation diagnosis mainly depends on the subjective judgement of human being, which costs much time and manpower. In the paper, an automatic deformation inspection method based on statistical characteristics for digital aerial imagery is proposed to inspect the distortion caused by the low IMU data accuracy. For the undulant wavelike deformation image has the characteristic of pixel displacement in the regularly same direction, there will be a lot of wave curves in the same direction appeared in the image after geometric correction. Therefore, in the method, the positions of the wave curves in the image will be located by the extreme points of curvature of the contour lines, and then the wavelike deformations can be judged automatically through the distribution statistics of the open directions of the wave curves. The specific implement method can be described as follows: firstly, the edges of the image are detected with Canny edge detector and the vector contour lines are obtained by tracing the edges to get contour lines and fitting them with the cubic spline curve method. Then, the extreme points of curvature of the contour lines are calculated, and some of these points are determined to be the vertexes of the wave curves by judging the positional relations between each extreme point and the points around it, thus constituting a vertex set. Afterwards, the perpendicular directions of the tangent of the vertexes are used as the directions of the wave curves, and then the direction histograms of all the wave curves in the image are obtained by statistical analysis. Finally, the existence of the deformation phenomenon in the image due to the low precision of IMU data is able to be judged based on whether the directions of the wave curves are centralized in a certain direction or not. Experimental results showed that the automatic deformation inspection method presented in this paper can detect the deformation of the digital aerial images effectively caused by low accuracy of IMU data with 95% accuracy.

  4. Creep-rupture characteristics of Type 304 stainless steel weldments with Type 308 stainless steel welds at 1100/sup 0/F

    SciTech Connect

    Manjoine, M.J.

    1985-06-01

    This paper describes the creep of Type 304 stainless steel plate weldments as influenced by the level of ferrite and the geometries of the Type 308 stainless steel weld metal. The method of testing enabled multiple determinations of the strains for weld metal, heat-affected zone (HAZ), and base metal at crack initiation and rupture. The tests of weldments included two levels of ferrite, 2 FN and 9 FN, and two weld geometries-75 deg V-groove weld and a single, square groove weld made from one side with a backing plate at the weld root. All tests were performed at 24 ksi (165 MPa) and 1100/sup 0/F (593/sup 0/C). The weldments with a central axial weld and constraints at the ends of the gage section were tensile loaded. Therefore, all zones of the weld are subjected to the same overall axial deformation. This loading and constraint is similar to a circumferential weld in a pipe or vessel. The failure mode was a function at all three of the following: The relative strengths and ductilities of the weld metal, heat-affected zone (HAZ) and the base metal. The residual stresses and deformations from the welding process. The stress and strain histories under loading.

  5. Deformation characteristics during Y-shaped tube hydroforming of 6061 aluminum alloy

    NASA Astrophysics Data System (ADS)

    Chu, Guannan; Li, Feng; Liu, Wenjian

    2011-02-01

    To manufacture lightweight tube components for aerospace oil circuit systems, an experiment was run to investigate the deformation characteristics on Y-shaped tube hydroforming of 6061 aluminum alloy. Both strain state and metallurgical structure indicate that there are four kinds of prevailing defects during Y-shaped tube hydroforming: bursting, lack of cylindricity, wrinkling, and thinning due to the poor plastic property of 6061 aluminum alloy. The danger of bursting prevails at the early stage of the operation as a result of excessively high internal pressure. In contrast, wrinkling prevails after the middle stage of the operation as a result of excessively axial feeding and cannot be eliminated during subsequent deformation. Lack of cylindricity is mainly because of insufficient axial feeding and internal pressure but can be eliminated by increasing internal pressure. Elongation and compression deformations are originated on protrusion and main pipe of Y-shape tube respectively all the way through the bulging process. Consequently, minimum and maximum thicknesses are at the top of protrusion and the bottom of Y-shape tube respectively, which induces a V-shape borderline of thickness distribution. According to the excessive plastic deformation, microstructure evolution is originated. Crystal grain of protrusion is elongated and its grain size is about 150 ?m. In contrast, crystal grain of the middle zone of main tube is refined greatly, which grain size is 50 ?m, decreased by 75%. These are useful to improve the component.

  6. The Creep of Single Crystals of Aluminum

    NASA Technical Reports Server (NTRS)

    Johnson, R D; Shober, F R; Schwope, A D

    1953-01-01

    The creep of single crystals of high-purity aluminum was investigated in the range of temperatures from room temperature to 400 F and at resolved-shear-stress levels of 200, 300, and 400 psi. The tests were designed in an attempt to produce data regarding the relation between the rate of strain and the mechanism of deformation. The creep data are analyzed in terms of shear strain rate and the results are discussed with regard to existing creep theories. Stress-strain curves were determined for the crystals in tinsel and constant-load-rate tests in the same temperature range to supplement the study of plastic deformation by creep with information regarding the part played by crystal orientation, differences in strain markings, and other variables in plastic deformation.

  7. Creep of plasma sprayed zirconia

    NASA Technical Reports Server (NTRS)

    Firestone, R. F.; Logan, W. R.; Adams, J. W.

    1982-01-01

    Specimens of plasma-sprayed zirconia thermal barrier coatings with three different porosities and different initial particle sizes were deformed in compression at initial loads of 1000, 2000, and 3500 psi and temperatures of 1100 C, 1250 C, and 1400 C. The coatings were stabilized with lime, magnesia, and two different concentrations of yttria. Creep began as soon as the load was applied and continued at a constantly decreasing rate until the load was removed. Temperature and stabilization had a pronounced effect on creep rate. The creep rate for 20% Y2O3-80% ZrO2 was 1/3 to 1/2 that of 8% Y2O3-92% ZrO2. Both magnesia and calcia stabilized ZrO2 crept at a rate 5 to 10 times that of the 20% Y2O3 material. A near proportionality between creep rate and applied stress was observed. The rate controlling process appeared to be thermally activated, with an activation energy of approximately 100 cal/gm mole K. Creep deformation was due to cracking and particle sliding.

  8. Surface loading affects internal pressure source characteristics derived from volcano deformation signals

    NASA Astrophysics Data System (ADS)

    Grapenthin, Ronni; Sigmundsson, Freysteinn; Ofeigsson, Benedikt; Sturkell, Erik

    2010-05-01

    Deformation of the Earth's surface provides critical information about the migration of material beneath a volcano. The resulting displacements, recorded by geodetic techniques such as GPS or InSAR, are used to infer characteristics of the volcanic plumbing system which are critical for hazard mitigation in volcanic regions. Given some deformation data, we search for the source model that explains the data best. Discussions of the results usually focus on the validity of the chosen model and the underlying assumptions regarding crustal composition, e.g. the level of inhomogeneity, elastic versus plastic deformation, thermal effects, depth vs. volume trade offs of the applied analytical models, or the (in-)compressibility of materials. Surface loads such as lava flows, however, provide an additional source of deformation. The initial elastic response due to a load on the surface of the Earth is followed by a visco-elastic response of the ductile crust below the uppermost elastic layer. Thus, a deformation signal recorded in the vicinity of a volcano is often composed of at least two contributors: an internal pressure source (the magma chamber) and a surface load (e.g., a composition of previously erupted lava flows) - at the extreme the volcanic edifice and its glaciers. A test case for a circular lava flow on top of a deflating magma chamber shows that the crust will adjust to the load towards final relaxed response. During this relaxation process gradual subsidence occurs that may mistakenly be interpreted as due to pressure decrease in a magma chamber since the deformation pattern of both processes are very similar. This poses a problem when characteristics of a magma chamber are to be derived. Based on the ratio of horizontal and vertical displacement and a combination of model results (Green's functions and Mogi model), we can estimate the composition of observed deformation signals. This method is applied to the Icelandic volcano Mt. Hekla where we investigate InSAR observations prior to the Hekla 2000 eruption that show circular pattern of near field subsidence and far field inflation. We compare these data to the deformation pattern expected from pressure changes in a hypothetical, shallow magma reservoir. We estimate surface loading at the volcano to account for a displacement of 13.5mm-yr based on a comparison of expected Mogi source and observed InSAR line of sight velocity. From this we estimate an effective relaxation time of tr = 100yrs for this region. We infer an elastic plate thickness of H = 3.5km which controls the 15 - 20km radius of subsidence. We find that surface load signals in volcanic regions affect magmatic source model estimates significantly ; to the point of changing the preferred source model. This effect should be considered in virtually any volcanic region that shows lava flow emplacement, glacier dynamics, or sudden load removal (i.e., lateral blasts). Deformation data that remains uncorrected will most likely result in an overestimation of depth and volume of a magma reservoir. We find that the ratio of displacements aids the identification of composite signals and suggest that the ratio for GPS data be employed more rigorously in future studies since this allows volume independent source depth estimates.

  9. The characteristics of cavitation during superplastic deformation of a warm-rolled Al-Li-Cu-Mg-Zr alloy

    SciTech Connect

    Liu, Q. ); Huang, X.; Yang, J.; Yao, M. )

    1991-01-01

    The process of superplastic forming has become important in numerous commercial applications. However, there may be some deleterious defects on the properties of superplastically-formed components due to the presence of minor levels of cavitation introduced during the forming process. Thus, it is important to obtain information on nucleation, growth and interlinkage of cavities in a wide range of superplastic materials. Two different thermomechanical processing routes may be employed to develop fine grain sizes conducive to superlasticity in Al-Li alloys. In one of them, a fine grain size microstructure is obtained by static recrystallization prior to superplastic deformation, and in another, a fine grain size microstructure is obtained by deformation-induced recrystallization during the initial stage of superplastic deformation. The deformation-induced recrystallization of a cold (or warm)-rolled Al-Li alloy is strongly dependent on the strain rate microstructural change during the initial stage of superplastic deformation due to deformation-induced recrystallization. There have been some studies dealing with cavitation in superplastic Al-Li alloys. However, there is no research work reported on the effect of deformation-induced recrystallization on the characteristics of cavitation during superplastic deformation of a warm-rolled Al-Li alloy. This paper deals with the relationship between deformation-induced recrystallization and cavitation characteristics during superplastic deformation of a warm-rolled Al-Li-Cu-Mg-Zr alloy. The results show that there are three kinds of cavities. The first includes the fine cavities formed at the beginning stage of deformation, the second the large cavities formed around the intermetallic particles and the third the grain boundary cavities. All three kinds of cavities are closely related to deformation-induced recrystallization.

  10. Comparison of cleaning efficiency and deformation characteristics of Twisted File and ProTaper rotary instruments

    PubMed Central

    Li, Hang; Zhang, Chenzheng; Li, Qing; Wang, Changning; Song, Yaling

    2014-01-01

    Objective: The objective of the following study is to compare the cleaning efficiency and deformation characteristics of Twisted File (TF) and ProTaper (PT) nickel-titanium rotary instruments in root canal preparation. Materials and Methods: A total of 52 canals from 26 extracted maxillary first molars were randomly assigned into two groups of each including 13 mesiobuccal and 12 distobuccal (DB) canals. Two DB canals were as blank controls. After preparation with TF and PT, we recorded the preparation time and evaluate the amounts of debris and smear layer at apical, middle and coronal canals under scanning electron microscopy (SEM). Three cross-sections of canals at 3 mm, 5 mm and 7 mm from the apex foramens were scanned before and after preparation under micro-computed tomography. Changes of the cross-section area (CSA) at the three levels were calculated with Photoshop CS4. File deformation was also investigated under SEM. Two groups were statistically compared with Mann-Whitney test and independent sample t-test. Results: Less debris and smear layer were found in coronal regions of canals prepared with TF (P = 0.006, P = 0.001, respectively). TF group displayed more CSA change than PT group (P = 0.045) at cross-sections of 5 mm from the apex foramens and took significantly less preparation time than PT group did (P = 9.06 10?28). All five TF files without obvious micro-cracks and two out of 25 PT files with many micro-cracks showed visible unwound deformation. Conclusion: Neither TF nor PT achieves complete cleanliness of canal walls. Their deformation features might indicate different fracture resistance. TF single-file technique would substantially shorten the time of root canal preparation. PMID:24966769

  11. Combination of metamorphism and deformation affect the nano-scale pore structures and macromolecule characteristics of high-rank deformed coals

    NASA Astrophysics Data System (ADS)

    Zhang, W.; Li, H.; Ju, Y.

    2013-12-01

    Coal constitutes a large proportion of total energy supply in the world. Coalbed Methane (CBM) composes the greenhouse gases, which has attracted more and more scientists' concern and attention. The adsorption/desorption characteristics and mechanism of CBM on high-rank deformed coals are in favor of enhancing gas recovery, reducing coal mining accidents and carbon emission. Although the influence factors of CBM adsorption/desorption on different coals have been intensively studied, the combined action of metamorphism and deformation on high-rank coals have been rarely researched. Nevertheless. Metamorphism and deformation are the most fundamental driving forces that cause the changes of inner structures and compositions in coal strata, and then alter the adsorption/desorption capacities of CBM on different coalbeds. South of Qinshui Basin in Shanxi province developed with abundant high-rank coals is the first demonstrate area of CBM development in China. Meanwhile Southwest of Fujian province represents high metamorphic-deformed coals region due to the intense volcanic activities. Therefore samples were taken in both areas to elaborate the adsorption/desorption characteristics and mechanism of CBM. Based on hand specimens description, coal macerals testing, proximate analysis, ultimate analysis and vitrinite reflectance testing, the physical properties and composition characteristics of high-rank deformed coals have been studied. Combined with liquid nitrogen adsorption experiments, Transmission Electron Microscopy (TEM) observation, Fourier Transform Infrared Spectrometry (FTIR) and Nuclear Magnetic Resonance (NMR) experiments, the results show that nano-pores increase and become homogenization with metamorphic-deformation enhancement, stacking of the macromolecular basic structural units (BSU) enhances, aromatic compound increases while aliphatic chain compound and oxygen-containing function groups decrease. Comparing to coal adsorption/desorption isotherm experiments indicates that adsorption/desorption capacity shows a 'U' type with nano-pores volume and specific surface area, coals with best adsorption capacity contained both vitrinite and inertinite with an approximate ratio of 4:1 or 1:4, the increase of aromatic and aliphatic content individually facilitated the adsorption of CBM. Generally speaking, the adsorption/desorption capacity of ductile deformed coals is higher than that of brittle ones, but metamorphism could dramatically affects the final results. To enhance CBM production and reduce carbon emission, the appropriate coal-bearing strata need to be chosen. Our research shows that metamorphism and deformation affect the nano-scale pore structures and macromolecule characteristics of different coals. Therefore brittle-ductile superposed zone with medium-high rank coals has high gas content and permeability which is promising to exploit and helpful to environmental protection.

  12. Nonlinear dynamic characteristics of a dielectric elastomer membrane undergoing in-plane deformation

    NASA Astrophysics Data System (ADS)

    Sheng, Junjie; Chen, Hualing; Li, Bo; Wang, Yongquan

    2014-04-01

    This paper proposes a free energy model to study the dynamic characteristics of a dielectric elastomer membrane undergoing in-plane deformation, subject to the combined loads of a mechanical press and an electric field. The natural frequency of the small-amplitude perturbation around the state of equilibrium is calculated with focus on the damping effects and the resonance phenomenon. The numerical results, such as the oscillation, phase diagrams and Poincar maps, are presented to show the influence of the damping on the nonlinear dynamic characteristics of the dielectric elastomer. The numerical results indicate that pre-stresses, damping effects and applied voltages could tune the natural frequency and modify the dynamic behavior of the dielectric elastomer. There is a stability transition when taking the damping effect into account. The damping effect could cause the dynamic responses to constant vibration and decrease the amplitude. These conclusions may guide the exploration of high-performance dielectric elastomers under dynamic mechanical and electrical loads.

  13. Irradiation creep in structural materials at ITER operating conditions

    SciTech Connect

    Grossbeck, M.L.

    1994-09-01

    Irradiation creep is plastic deformation of a material under the influence of irradiation and stress. Below the regime of thermal creep, there remains a deformation mechanism under irradiation that is weakly temperature dependent and clearly different from thermal creep. This is irradiation creep. Both stress and irradiation are required for irradiation creep. Irradiation creep studies for applications in the past focused mostly on liquid metal fast breeder reactors where temperatures are usually above 400{degrees}C. Fusion reactors, especially nearterm devices such as the ITER will have components operating at temperatures as low as 100{degrees}C exposed to high neutron fluxes. Theories of irradiation creep based on steady-state point defect concentrations do not predict significant irradiation creep deformation at these temperatures; however, data from research reactors show that irradiation creep strains at 60{degrees}C are as high or higher than at temperatures above 300{degrees}C for austenitic stainless steels. Irradiation creep of nickel has also been observed at cryogenic temperatures.

  14. Analysis of crustal deformation and strain characteristics in the Tianshan Mountains with least-squares collocation

    NASA Astrophysics Data System (ADS)

    Li, S. P.; Chen, G.; Li, J. W.

    2015-11-01

    By fitting the observed velocity field of the Tianshan Mountains from 1992 to 2006 with least-squares collocation, we established a velocity field model in this region. The velocity field model reflects the crustal deformation characteristics of the Tianshan reasonably well. From the Tarim Basin to the Junggar Basin and Kazakh platform, the crustal deformation decreases gradually. Divided at 82° E, the convergence rates in the west are obviously higher than those in the east. We also calculated the parameter values for crustal strain in the Tianshan Mountains. The results for maximum shear strain exhibited a concentration of significantly high values at Wuqia and its western regions, and the values reached a maxima of 4.4×10-8 a-1. According to isogram distributions for the surface expansion rate, we found evidence that the Tianshan Mountains have been suffering from strong lateral extrusion by the basin on both sides. Combining this analysis with existing results for focal mechanism solutions from 1976 to 2014, we conclude that it should be easy for a concentration of earthquake events to occur in regions where maximum shear strains accumulate or mutate. For the Tianshan Mountains, the possibility of strong earthquakes in Wuqia-Jiashi and Lake Issyk-Kul will persist over the long term.

  15. High-temperature creep of Nb-Al-V alloys

    SciTech Connect

    Rong, T.S.; Aindow, M.

    1999-07-01

    Nb-15Al-20V alloys with about 45% by volume of an A15 phase in a B2 matrix have been subjected to creep deformation at temperatures between 1,000 C and 1,200 C and stresses from 80 MPa to 240 MPa in vacuum. The creep curves show a rapid transition from primary to steady-state creep with a well-defined activation energy. Microstructural observations show that the creep deformation occurs mainly in the B2 matrix and is controlled by dislocation mechanisms. Samples which had been cold-rolled and annealed to reduce the size of A15 precipitates and increase the yield strength were found to have lower creep resistance than those with unrefined microstructures. The significance of these observations for the creep mechanisms is discussed.

  16. Study on creep properties of Japonica cooked rice and its relationship with rice chemical compositions and sensory evaluation

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Creep properties of four varieties japonica cooked rice were tested using a Dynamic Mechanical Analyser (DMA Q800). The creep curve was described by Burgers model. The creep process of japonica cooked rice mainly consisted of retarded elastic deformation, epsilonR and viscous flow deformation, epsil...

  17. Geodetic characteristic of the postseismic deformation following the interplate large earthquake along the Japan Trench (Invited)

    NASA Astrophysics Data System (ADS)

    Ohta, Y.; Hino, R.; Ariyoshi, K.; Matsuzawa, T.; Mishina, M.; Sato, T.; Inazu, D.; Ito, Y.; Tachibana, K.; Demachi, T.; Miura, S.

    2013-12-01

    On March 9, 2011 at 2:45 (UTC), an M7.3 interplate earthquake (hereafter foreshock) occurred ~45 km northeast of the epicenter of the M9.0 2011 Tohoku earthquake. This foreshock preceded the 2011 Tohoku earthquake by 51 hours. Ohta et al., (2012, GRL) estimated co- and postseismic afterslip distribution based on a dense GPS network and ocean bottom pressure gauge sites. They found the afterslip distribution was mainly concentrated in the up-dip extension of the coseismic slip. The coseismic slip and afterslip distribution of the foreshock were also located in the slip deficit region (between 20-40m slip) of the coiseismic slip of the M9.0 mainshock. The slip amount for the afterslip is roughly consistent with that determined by repeating earthquake analysis carried out in a previous study (Kato et al., 2012, Science). The estimated moment release for the afterslip reached magnitude 6.8, even within a short time period of 51 hours. They also pointed out that a volumetric strainmeter time series suggests that this event advanced with a rapid decay time constant (4.8 h) compared with other typical large earthquakes. The decay time constant of the afterslip may reflect the frictional property of the plate interface, especially effective normal stress controlled by fluid. For verification of the short decay time constant of the foreshock, we investigated the postseismic deformation characteristic following the 1989 and 1992 Sanriku-Oki earthquakes (M7.1 and M6.9), 2003 and 2005 Miyagi-Oki earthquakes (M6.8 and M7.2), and 2008 Fukushima-Oki earthquake (M6.9). We used four components extensometer at Miyako (39.59N, 141.98E) on the Sanriku coast for 1989 and 1992 event. For 2003, 2005 and 2008 events, we used volumetric strainmeter at Kinka-zan (38.27N, 141.58E) and Enoshima (38.27N, 141.60E). To extract the characteristics of the postseismic deformation, we fitted the logarithmic function. The estimated decay time constants for each earthquake had almost similar range (1-15 h) with the foreshock of the 2011 Tohoku earthquake (4.8h), but relatively small compared with the typical interplate earthquakes. The comparison of decay time constant with other typical large interplate earthquakes is very difficult because of difference in the observation sensors such as GPS and strainmeter. In any case, decay time constant of postseismic deformation for the foreshock of the 2011 Tohoku earthquake is not anomalous compared with other events in this region.

  18. Quantitative analysis of tissue deformation dynamics reveals three characteristic growth modes and globally aligned anisotropic tissue deformation during chick limb development

    PubMed Central

    Morishita, Yoshihiro; Kuroiwa, Atsushi; Suzuki, Takayuki

    2015-01-01

    Tissue-level characterization of deformation dynamics is crucial for understanding organ morphogenetic mechanisms, especially the interhierarchical links among molecular activities, cellular behaviors and tissue/organ morphogenetic processes. Limb development is a well-studied topic in vertebrate organogenesis. Nevertheless, there is still little understanding of tissue-level deformation relative to molecular and cellular dynamics. This is mainly because live recording of detailed cell behaviors in whole tissues is technically difficult. To overcome this limitation, by applying a recently developed Bayesian approach, we here constructed tissue deformation maps for chick limb development with high precision, based on snapshot lineage tracing using dye injection. The precision of the constructed maps was validated with a clear statistical criterion. From the geometrical analysis of the map, we identified three characteristic tissue growth modes in the limb and showed that they are consistent with local growth factor activity and cell cycle length. In particular, we report that SHH signaling activity changes dynamically with developmental stage and strongly correlates with the dynamic shift in the tissue growth mode. We also found anisotropic tissue deformation along the proximal-distal axis. Morphogenetic simulation and experimental studies suggested that this directional tissue elongation, and not local growth, has the greatest impact on limb shaping. This result was supported by the novel finding that anisotropic tissue elongation along the proximal-distal axis occurs independently of cell proliferation. Our study marks a pivotal point for multi-scale system understanding in vertebrate development. PMID:25858459

  19. Quantitative analysis of tissue deformation dynamics reveals three characteristic growth modes and globally aligned anisotropic tissue deformation during chick limb development.

    PubMed

    Morishita, Yoshihiro; Kuroiwa, Atsushi; Suzuki, Takayuki

    2015-05-01

    Tissue-level characterization of deformation dynamics is crucial for understanding organ morphogenetic mechanisms, especially the interhierarchical links among molecular activities, cellular behaviors and tissue/organ morphogenetic processes. Limb development is a well-studied topic in vertebrate organogenesis. Nevertheless, there is still little understanding of tissue-level deformation relative to molecular and cellular dynamics. This is mainly because live recording of detailed cell behaviors in whole tissues is technically difficult. To overcome this limitation, by applying a recently developed Bayesian approach, we here constructed tissue deformation maps for chick limb development with high precision, based on snapshot lineage tracing using dye injection. The precision of the constructed maps was validated with a clear statistical criterion. From the geometrical analysis of the map, we identified three characteristic tissue growth modes in the limb and showed that they are consistent with local growth factor activity and cell cycle length. In particular, we report that SHH signaling activity changes dynamically with developmental stage and strongly correlates with the dynamic shift in the tissue growth mode. We also found anisotropic tissue deformation along the proximal-distal axis. Morphogenetic simulation and experimental studies suggested that this directional tissue elongation, and not local growth, has the greatest impact on limb shaping. This result was supported by the novel finding that anisotropic tissue elongation along the proximal-distal axis occurs independently of cell proliferation. Our study marks a pivotal point for multi-scale system understanding in vertebrate development. PMID:25858459

  20. Low Temperature Creep of Hot-Extruded Near-Stoichiometric NiTi Shape Memory Alloy. Part I; Isothermal Creep

    NASA Technical Reports Server (NTRS)

    Raj, S. V.; Noebe, R. D.

    2013-01-01

    This two-part paper is the first published report on the long term, low temperature creep of hot-extruded near-stoichiometric NiTi. Constant load tensile creep tests were conducted on hot-extruded near-stoichiometric NiTi at 300, 373 and 473 K under initial applied stresses varying between 200 and 350 MPa as long as 15 months. These temperatures corresponded to the martensitic, two-phase and austenitic phase regions, respectively. Normal primary creep lasting several months was observed under all conditions indicating dislocation activity. Although steady-state creep was not observed under these conditions, the estimated creep rates varied between 10(exp -10) and 10(exp -9)/s. The creep behavior of the two phases showed significant differences. The martensitic phase exhibited a large strain on loading followed by a primary creep region accumulating a small amount of strain over a period of several months. The loading strain was attributed to the detwinning of the martensitic phase whereas the subsequent strain accumulation was attributed to dislocation glide-controlled creep. An "incubation period" was observed before the occurrence of detwinning. In contrast, the austenitic phase exhibited a relatively smaller loading strain followed by a primary creep region, where the creep strain continued to increase over several months. It is concluded that the creep of the austenitic phase occurs by a dislocation glide-controlled creep mechanism as well as by the nucleation and growth of deformation twins.

  1. Creep in electronic ceramics

    SciTech Connect

    Routbort, J. L.; Goretta, K. C.; Arellano-Lopez, A. R.

    2000-04-27

    High-temperature creep measurements combined with microstructural investigations can be used to elucidate deformation mechanisms that can be related to the diffusion kinetics and defect chemistry of the minority species. This paper will review the theoretical basis for this correlation and illustrate it with examples from some important electronic ceramics having a perovskite structure. Recent results on BaTiO{sub 3}, (La{sub 1{minus}x}Sr){sub 1{minus}y}MnO{sub 3+{delta}}, YBa{sub 2}Cu{sub 3}O{sub x}, Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub x}, (Bi,Pb){sub 2}Sr{sub 2}Ca{sub 2}Cu{sub 3}O{sub x} and Sr(Fe,Co){sub 1.5}O{sub x} will be presented.

  2. Creep of trabecular bone from the human proximal tibia

    PubMed Central

    Novitskaya, Ekaterina; Zin, Carolyn; Chang, Neil; Cory, Esther; Chen, Peter; D'Lima, Darryl; Sah, Robert L.; McKittrick, Joanna

    2014-01-01

    Creep is the deformation that occurs under a prolonged, sustained load and can lead to permanent damage in bone. Creep in bone is a complex phenomenon and varies with type of loading and local mechanical properties. Human trabecular bone samples from proximal tibia were harvested from a 71-year old female cadaver with osteoporosis. The samples were initially subjected to one cycle load up to 1% strain to determine the creep load. Samples were then loaded in compression under a constant stress for two hours and immediately unloaded. All tests were conducted with the specimens soaked in phosphate buffered saline with proteinase inhibitors at 37C. Steady state creep rate and final creep strain were estimated from mechanical testing and compared with published data. The steady state creep rate correlated well with values obtained from bovine tibial and human vertebral trabecular bone, and was higher for lower density samples. Tissue architecture was analyzed by micro-computed tomography (?CT) both before and after creep testing to assess creep deformation and damage accumulated. Quantitative morphometric analysis indicated that creep induced changes in trabecular separation and the structural model index. A main mode of deformation was bending of trabeculae. PMID:24857486

  3. Effect of unloading time on interrupted creep in copper

    SciTech Connect

    Chandler, H.D. . School of Mechanical Engineering)

    1994-06-01

    The effect of unloading time on the interrupted creep behavior of polycrystalline copper specimens was investigated over the temperature range 298--773 K. Up to 553 K, cyclic creep acceleration could be explained in terms of deformation and hardening using a dislocation glide model with recovery during unloading being due to dislocation climb. At higher temperatures, recrystallization effects probably influence behavior.

  4. The search for creep on the faults of northern California

    NASA Astrophysics Data System (ADS)

    Funning, Gareth; Jin, Lizhen

    2013-04-01

    Shallow aseismic fault creep is a behaviour exhibited by very few faults in the world. Instead of the stick-slip frictional regime that most faults follow, creeping faults move, steadily or episodically, throughout the interseismic period of the earthquake cycle. Creep effectively reduces the fault surface area capable of rupture in earthquakes, and thus knowledge of its extent is critical for the correct assessment of seismic hazard. In addition, by comparing the geographical locations of creeping fault areas with mapped lithologies, we may be able to better understand the underlying causes or mechanisms. We present here the results of our ongoing research into the distribution of creeping fault areas in northern California, where the majority of reported cases are located. We map the surface deformation field of the plate boundary system south and north of the San Francisco Bay Area using persistent scatterer InSAR, which provides a dense spatial coverage of surface deformation measurements across the region, and 'ground truth' these, where possible, with additional surface deformation measurements from GPS. In so doing, we identify deformation consistent with right-lateral shallow creep on sections of five major faults (the Hayward, Calaveras, San Andreas, Rodgers Creek and Concord faults). On the Hayward fault, we are able to map both the extent and distribution of creep rates at depth, constraining the location of a locked zone that is presumably the source of major earthquakes on the fault. We are not able to identify a consistent lithological control for the creep behaviour.

  5. Deformation characteristics of the near-surface layers of zirconia ceramics implanted with aluminum ions

    NASA Astrophysics Data System (ADS)

    Ghyngazov, S. A.; Vasiliev, I. P.; Frangulyan, T. S.; Chernyavski, A. V.

    2015-10-01

    The effect of ion treatment on the phase composition and mechanical properties of the near-surface layers of zirconium ceramic composition 97 ZrO2-3Y2O3 (mol%) was studied. Irradiation of the samples was carried out by accelerated ions of aluminum with using vacuum-arc source Mevva 5-Ru. Ion beam had the following parameters: the energy of the accelerated ions E = 78 keV, the pulse current density Ji = 4mA / cm2, current pulse duration equal τ = 250 mcs, pulse repetition frequency f = 5 Hz. Exposure doses (fluence) were 1016 и 1017 ion/cm2. The depth distribution implanted ions was studied by SIMS method. It is shown that the maximum projected range of the implanted ions is equal to 250 nm. Near-surface layers were investigated by X-ray diffraction (XRD) at fixed glancing incidence angle. It is shown that implantation of aluminum ions into the ceramics does not lead to a change in the phase composition of the near-surface layer. The influence of implanted ions on mechanical properties of ceramic near-surface layers was studied by the method of dynamic nanoindentation using small loads on the indenter P=300 mN. It is shown that in ion- implanted ceramic layer the processes of material recovery in the deformed region in the unloading mode proceeds with higher efficiency as compared with the initial material state. The deformation characteristics of samples before and after ion treatment have been determined from interpretation of the resulting P-h curves within the loading and unloading sections by the technique proposed by Oliver and Pharr. It was found that implantation of aluminum ions in the near-surface layer of zirconia ceramics increases nanohardness and reduces the Young's modulus.

  6. Quantitative investigation of the tensile plastic deformation characteristic and microstructure for friction stir welded 2024 aluminum alloy

    SciTech Connect

    Hu, Z.L.; Wang, X.S.; Yuan, S.J.

    2012-11-15

    The effect of the microstructure heterogeneity on the tensile plastic deformation characteristic of friction stir welded (FSW) 2024 aluminum alloy was investigated for the potential applications on light weight design of vehicles. The microstructure characteristics of the FSW joints, such as the grain structure, dislocation density and the distribution of precipitation, were studied by electron backscattered diffraction (EBSD) and transmission electron microscopy (TEM). The tensile deformation characteristic of the FSW joints was examined using the automatic strain measuring system (ASAME) by mapping the global and local strain distribution, and then was analyzed by mechanics calculation. It is found that the tensile deformation of the FSW joints is highly heterogeneous leading to a significant decrease in global ductility. The FSW joints mainly contain two typical deformation zones, which show great effect on the regional inhomogeneous deformation. One is the nugget zone (NZ) with a region of 8 mm in width, and the other is part of the BM with a region of 10 mm in width. The BM of the joints is the weakest region where the strain localizes early and this localization extends until fracture with a strain over 30%, while the strain in the NZ is only 4%. Differences in regional strain of FSW joints, which are essentially controlled by grain structure, the distribution of precipitation and dislocation density, result in decrease on the overall mechanical properties. - Highlights: Black-Right-Pointing-Pointer Microstructure heterogeneity of welds on tensile deformation behavior is studied. Black-Right-Pointing-Pointer The welds contain two typical deformation zones, affecting the global ductility. Black-Right-Pointing-Pointer Regional strain of welds is controlled by grain structure and dislocation density. Black-Right-Pointing-Pointer Theoretical calculation is in good agreement with experimental result.

  7. Diffusion creep of enstatite at high pressures

    NASA Astrophysics Data System (ADS)

    Zhang, G.; Mei, S.; Kohlstedt, D. L.

    2014-12-01

    Deformation behavior of fine-grained enstatite (g.s. ~ 8 μm) was investigated with triaxial compressive creep experiments at high pressures (4.2 - 6.9 GPa) and high temperatures (1373 - 1573 K) using a deformation-DIA apparatus. Experiments were carried out under anhydrous conditions. In each experiment, a sample column composed of a sample and alumina pistons was assembled with a boron nitride sleeve and graphite resistance heater into a 6.2-mm edge length cubic pressure medium. Experiments were carried out at the National Synchrotron Light Source at Brookhaven National Laboratory. In a run, differential stress and sample displacement were monitored in-situ using synchrotron x-ray diffraction and radiography, respectively. Based on results from this study, the deformation behavior of enstatite under anhydrous conditions has been quantitatively presented in the form of a flow law that describes the dependence of deformation rate on stress, temperature, and pressure. Specifically, data fitting yields the dependence of creep rate on stress with an exponent of n ≈ 1; indicating samples were deformed in the regime of diffusion creep. Experimental results also yield the dependences of creep rate on temperature and pressure with an activation energy of ~250 kJ/mol and activation volume of ~3.5×10-6 m3/mol, respectively. The flow laws for enstatite, one important constituent component for the upper mantle, quantified from this study provides a necessary constraint for modeling the dynamic activities occurring within Earth's interior.

  8. Creep-fatigue interactions in eutectic tin-lead-based solder alloys. Ph.D. Thesis

    SciTech Connect

    Kuo, C.W.

    1994-01-01

    Eutectic tin-lead solder alloys subjected to cyclic loading at room temperature experience creep-fatigue interactions due to high homologous temperature. At temperature above 0.5 melting point, the dominant damage mechanism can be cavity nucleation and growth, especially for alloys that have fine grain structure and a large volume fraction of dispersoids. The objective of the present study is to model the damage evolution during creep-fatigue interactions and experimentally validate the damage evolution based life predictions in rapidly solidified solder alloys. Four types of solder alloys were considered in this research, namely, conventional 63Sn-37Pb, rapidly solidified 63Sn-37Pb, dispersion-strengthened eutectic solders, and solid solution strengthened eutectic solders. Mechanical properties of the solder alloys and the life times under creep-fatigue conditions were evaluated. Damage produced in the course of creep or fatigue deformation was studied by metallography, scanning electron microscopy, precision density measurement, and the observation of grain boundary sliding. Based on the damage characteristics, the dominant failure mechanism was proved to be cavity growth. Three cavity growth models were applied to four types of solder alloys to predict creep-fatigue life by taking into account the tensile loading component as well as the compressive loading component when reversed process can occur. An algorithm to calculate cavity growth in each fatigue cycle is used to predict the number of fatigue cycles to failure, where failure is defined as a critical cavity size. Calculated lives are compared to experimental data under six types of creep-fatigue loading histories. The method predicts the creep-fatigue lives within a factor of two with the incorporation of appropriate compressive healing factor. Discrepancy between calculated lives and experimental results is discussed.

  9. Some problems on the theory of creep

    NASA Technical Reports Server (NTRS)

    Rabotnov, Y N

    1953-01-01

    The term creep of metals is applied to the phenomenon in which, at temperatures beyond a certain limit, the metal subjected to a load slowly undergoes deformation with time. For the case of steel, the creep phenomenon must be taken into account at temperatures above 400 degrees C. Very slow deformations for a prolonged period are cumulative and lead either to inadmissible changes in the dimensions of a structural part or to its failure. The theory of creep constitutes part of the mechanics of dense media and the mechanical formulation of the problem may be given as the following: a body is subjected to the action of a given system of forces, or initial displacements are prescribed on its surface. It is required to find the stress distribution in the body and the changes or its deformations with time. For the solution of the problem of creep as thus formulated, a mechanical theory of creep is required. Such theory must necessarily bear an external, overall character based, not on the investigation of microprocesses, but on the results of mechanical tests.

  10. Water weakening of clinopyroxenite in diffusion creep

    NASA Astrophysics Data System (ADS)

    Hier-Majumder, Saswata; Mei, Shenghua; Kohlstedt, David L.

    2005-07-01

    We performed triaxial compressive creep tests to study water weakening of clinopyroxenite in the diffusion creep regime. All tests were carried out on fine-grained samples at confining pressures between 100 and 300 MPa at temperatures of 1321 to 1421 K for water-saturated and 1398 to 1508 K for anhydrous conditions. Samples were prepared by hot-pressing ground powder of Sleaford Bay clinopyroxenite. Water was added to the sample during the run by dehydration of a talc sleeve. Water-saturated aggregates crept 30 times faster than aggregates under anhydrous conditions at a temperature of 1400 K and a pressure of 300 MPa. The stress exponent in both cases was 1, and the activation energies under water-saturated and anhydrous conditions were 340 30 and 760 20 kJ/mol, respectively. Under water-saturated conditions creep rate increased with increasing water fugacity to the power 1.4 0.2 with an activation volume for creep of 14 6 10-6 m3/mol. Comparison of the water weakening in aggregates of clinopyroxene, olivine, and anorthite deformed in the diffusion creep regime indicates that the creep strength of clinopyroxene has a stronger dependence on the water fugacity than do the creep strengths of olivine and anorthite. In water-rich environments, clinopyroxene will be the weakest component in polycrystalline rocks composed of these phases.

  11. Phenomenology of the creep process of a precipitation-hardenable AlMgSi alloy wires for overhead power lines. Experimental tests. Simulation

    NASA Astrophysics Data System (ADS)

    Knych, Tadeusz; Mamala, Andrzej; Smyrak, Beata

    2009-05-01

    The article presents the results of the experimental test on the creep process of AlMgSi alloy wires (series 6xxx) under the conditions of variable stress. A theoretical analysis of equivalency rheological results of stress and temperature changes by means of Bayley-Norton function, which describes well the low-temperature aluminum alloys creep, was carried out. Therefore, the described issue became one-dimensional. On the basis of experimental tests, it has been proved that negative gradients of stress and temperature may generate three types of rheological behaviour, such as: Temporary decrease of creep speed (type 1), Temporary stop of creep deformation (dead time)type 2 and reverse after creep (type 3). The applicable nature of tests is placed in overhead power lines, which undergo cyclical stress- and time-dependent operation. Such a nature of conductor operation creates favourable conditions to decrease creep intensity, whereas its history and value and speed of stress and temperature lowering decide whether conductor rheological activity loss will take place. The actual material parameter controlling the conductor rheological behaviour is stress and temperature rheological equivalent. The article contains exemplary results of current-carrying capacity changes of AlMgSi alloy conductor on a given temperature range, and the calculations include actual creep characteristic and cumulated rheological inactivity caused by negative gradients of stress and temperature.

  12. Creep Mechanisms of a Ni-Co-Based-Wrought Superalloy with Low Stacking Fault Energy

    NASA Astrophysics Data System (ADS)

    Tian, Chenggang; Xu, Ling; Cui, Chuanyong; Sun, Xiaofeng

    2015-10-01

    In order to study the influences of stress and temperature on the creep deformation mechanisms of a newly developed Ni-Co-based superalloy with low stacking fault energy, creep experiments were carried out under a stress range of 345 to 840 MPa and a temperature range of 923 K to 1088 K (650 °C to 815 °C). The mechanisms operated under the various creep conditions were identified and the reasons for their transformation were well discussed. A deformation mechanism map under different creep conditions was summarized, which provides a qualitative representation of the operative creep mechanisms as a function of stress and temperature.

  13. Change in characteristics of superplastic deformation of the aluminum-lithium alloy under the effect of ultrasonic vibrations

    NASA Astrophysics Data System (ADS)

    Myshlyaev, M. M.; Shpeizman, V. V.; Klubovich, V. V.; Kulak, M. M.; Lyu, G.

    2015-10-01

    The tension of samples of aluminum-lithium alloy 1420 in the superplasticity temperature region T = 320-395C and the influence of ultrasonic vibrations on deformation characteristics have been investigated. It has been shown that the effect of ultrasound manifests itself in a decrease in resistance to deformation and an increase in total strain. The tension curves plotted in the coordinates true stresses-true strains, in contrast to the standard stress-strain curves, have an extended hardening region, the magnitude of which is larger for the samples deformed with the ultrasound. The stress-rate sensitivity coefficients m have been determined from stress jumps with variations in the tension rate. It has been shown that the quantity m can be assumed to be constant over the entire superplasticity temperature region for different strains with ultrasound and without it, m = 0.46 0.04, and, correspondingly, the stress exponent in the formula for the strain rate is = 2.21 0.23. The activation energies of the deformation process have been evaluated, and it has been concluded that the dislocation motion during the intragrain deformation that is characteristic of the hardening stage is facilitated under the effect of ultrasound.

  14. Creep rupture of fiber bundles: A molecular dynamics investigation.

    PubMed

    Linga, G; Ballone, P; Hansen, Alex

    2015-08-01

    The creep deformation and eventual breaking of polymeric samples under a constant tensile load F is investigated by molecular dynamics based on a particle representation of the fiber bundle model. The results of the virtual testing of fibrous samples consisting of 40000 particles arranged on Nc=400 chains reproduce characteristic stages seen in the experimental investigations of creep in polymeric materials. A logarithmic plot of the bundle lifetime τ versus load F displays a marked curvature, ruling out a simple power-law dependence of τ on F. A power law τ∼F-4, however, is recovered at high load. We discuss the role of reversible bond breaking and formation on the eventual fate of the sample and simulate a different type of creep testing, imposing a constant stress rate on the sample up to its breaking point. Our simulations, relying on a coarse-grained representation of the polymer structure, introduce new features into the standard fiber bundle model, such as real-time dynamics, inertia, and entropy, and open the way to more detailed models, aiming at material science aspects of polymeric fibers, investigated within a sound statistical mechanics framework. PMID:26382414

  15. Creep rupture of fiber bundles: A molecular dynamics investigation

    NASA Astrophysics Data System (ADS)

    Linga, G.; Ballone, P.; Hansen, Alex

    2015-08-01

    The creep deformation and eventual breaking of polymeric samples under a constant tensile load F is investigated by molecular dynamics based on a particle representation of the fiber bundle model. The results of the virtual testing of fibrous samples consisting of 40 000 particles arranged on Nc=400 chains reproduce characteristic stages seen in the experimental investigations of creep in polymeric materials. A logarithmic plot of the bundle lifetime τ versus load F displays a marked curvature, ruling out a simple power-law dependence of τ on F . A power law τ ˜F-4 , however, is recovered at high load. We discuss the role of reversible bond breaking and formation on the eventual fate of the sample and simulate a different type of creep testing, imposing a constant stress rate on the sample up to its breaking point. Our simulations, relying on a coarse-grained representation of the polymer structure, introduce new features into the standard fiber bundle model, such as real-time dynamics, inertia, and entropy, and open the way to more detailed models, aiming at material science aspects of polymeric fibers, investigated within a sound statistical mechanics framework.

  16. Spatial and Temporal Characteristics of Propagating Deformation Bands in AA5182 Alloy at Room Temperature

    NASA Astrophysics Data System (ADS)

    de Codes, R. Nogueira; Hopperstad, O. S.; Engler, O.; Lademo, O.-G.; Embury, J. D.; Benallal, A.

    2011-11-01

    The spatial and temporal characteristics of propagating deformation bands in the Al-Mg alloy AA5182 in O temper were studied experimentally at room temperature. Tensile tests were carried out on flat specimens at strain rates in the range from 10-5 to 10-1 s-1. Digital image correlation (DIC) and digital infrared thermography (DIT) were applied to monitor the propagating bands. It was found that the material exhibits a sharp yield point, and Lders bands were seen at all the strain rates. Jerky flow took place all along the Lders plateau. It thus seems that the Portevin-Le Chatelier (PLC) effect starts at incipient yielding and that there is no critical strain. At the end of the Lders plateau, PLC bands immediately started to propagate back and forth along the gage section of the specimen. The work hardening of the material decreased consistently with increasing strain rate, while the flow stress on the Lders plateau was rather unaffected by the strain rate. This indicates that the dynamic strain aging (DSA) mainly affects the strength of the interaction between mobile and forest dislocations. The strain to necking was found to decrease gradually with strain rate for this alloy, which is consistent with the lower work-hardening rate at the higher strain rates.

  17. Creep behavior of thin laminates of iron-cobalt alloys for use in switched reluctance motors and generators

    NASA Astrophysics Data System (ADS)

    Fingers, Richard Todd

    The United States Air Force is in the process of developing magnetic bearings as well as an aircraft Integrated Power Unit and an Internal Starter/Generator for main propulsion engines. These developments are the driving force behind a new emphasis on high temperature, high strength magnetic materials for power applications. Analytical work, utilizing elasticity theory, in conjunction with design requirements, indicates a need for magnetic materials to have strengths in excess of 80 ksi up to about 1000sp°F. It is this combination of desired material characteristics that is the motivation for this effort to measure, model, and predict the creep behavior of such advanced magnetic materials. Hipercosp°ler Alloy 50HS, manufactured by Carpenter Technology Corporation, is one of the leading candidates for application and is studied in this effort by subjecting mechanical test specimens to a battery of tensile and creep tests. The tensile tests provide stress versus strain behaviors that clearly indicate: a yield point, a heterogeneous deformation described as Luders elongation, the Portevin-LeChatelier effect at elevated temperatures, and, most often, a section of homogeneous deformation that concluded with necking and fracture. Creep testing indicated two distinct types of behavior. The first was a traditional response with primary, secondary and tertiary stages, while the second type could be characterized by an abrupt increase in strain rate that acted as a transition from one steady state behavior to another. This second linear region was then followed by the tertiary stage. The relationship between the tensile response and the creep responses is discussed. Analyses of the mechanical behavior includes double linear regression of empirically modeled data, scanning electron microscopy for microstructural investigations, isochronous stress-strain relations, and constant strain rate testing to relate the tensile and creep test parameters. Also, elastic and creep deformation analyses are done, which incorporate material property data and material constants determined along with stress and displacement profiles for a specific Air Force design configuration.

  18. Deformation characteristics of 2-3 km buried Hota accretionary complex, central Japan

    NASA Astrophysics Data System (ADS)

    Yamamoto, Y.; Yamaguchi, H.; Kameda, J.

    2008-12-01

    The lower to middle Miocene Hota accretionary complex is a unique example of on land accretionary complex, representing deformation and its physical/chemical properties of sediments just prior to entering the seismogenic realm. The maximum paleotemperature was estimated approximately 55-70C (based on vitrinite reflectance) indicative of a maximum burial depth about 2-3 km assuming a paleo-geothermal gradient as 25-35C/km. Accretionary complex in this temperature/depth range corresponds with an intermediate range between the core samples collected from the modern accretionary prism (e.g. Nankai, Barbados, and so on) and rocks in the ancient accretionary complexes on land. Deformation and physical/chemical properties of accretionary complex in this range were poorly understood because the appropriate samples have not been collected yet (scientific drilling has never reached there and most of ancient examples experienced the deeper burial depth and suffered thermal and physical overprinting). This presentation will treat the detailed structural and chemical analyses of the Hota accretionary complex to construct deformation properties of accretionary complex in its 2-3 km depth range and to discuss the interrelation between the early diagenesis (hydrocarbon/cations generation and sediment dewatering, etc.) and transition of the deformation properties. The deformation in this accretionary complex is characterized by two deformation styles: one is a few centimeter-scale phacoidal deformation representing clay minerals preferred orientation in the outer rim, whereas random fabric in the core, quite similar texture to the rocks in the present-Nankai dcollement zone. The other is S-C style deformation (similar deformation to the mlanges in ancient accretionary complex on land) exhibiting block-in-matrix texture and quite intense clay minerals preferred orientation in the matrix, cutting the phacoidal deformation. Positive anomaly of illite/smectite ratio and vitrinite reflectance data (Ro) inside the latter S-C structure infers frictional heating during the deformation. Carbonate cement and calcite/dolomite-filled breccias above the S- C deformation and sandstone clasts representing hydro-fractured texture in the deformation are indicative that calcareous cement and pore-fluid pressure fluctuations seemed to be an essential control of the transition of the deformation style and position of the S-C style deformation.

  19. Experimental and Numerical Study of Ceramic Breeder Pebble Bed Thermal Deformation Behavior

    SciTech Connect

    An Zhiyong; Ying, Alice; Abdou, Mohamed

    2005-05-15

    Experiments on thermomechanics interactions between clad and pebble beds have been performed with overstoichiometric lithium orthosilicate pebbles (pebble diameters between 0.25 and 0.63 mm) at temperatures of 700-800 deg. C. The experimental results show that the thermal deformation of our pebble bed system is nonlinear and when the operating temperature is higher than 600 deg. C, thermal creep deformation is generated. In this paper, constitutive equations of the elastic and creep deformation are derived from the experimental results. Incorporating the effective constitutive equations in finite element method (FEM), numerical investigations presenting the elastic and plastic deformation characteristics of pebble bed system are comparable to the experimental behaviors. In addition, discrete element method (DEM) is underdevelopment to derive constitutive equations for different pebble beds. The preliminary results of DEM show the stress distribution inside the pebble beds at steady or transient states, which helps us to identify the destructive region in a pebble bed system.

  20. Irradiation creep of nano-powder sintered silicon carbide at low neutron fluences

    SciTech Connect

    Koyanagi, Takaaki; Shimoda, Kazuya; Kondo, Sosuke; Hinoki, Tatsuya; Ozawa, Kazumi; Katoh, Yutai

    2014-12-01

    The irradiation creep behavior of nano-powder sintered silicon carbide was investigated using the bend stress relaxation method under neutron irradiation up to 1.9 dpa. The creep deformation was observed at all temperatures ranging from 380 to 1180 °C mainly from the irradiation creep but with the increasing contributions from the thermal creep at higher temperatures. Microstructural observation and data analysis were performed.

  1. Threshold Stress Creep Behavior of Alloy 617 at Intermediate Temperatures

    NASA Astrophysics Data System (ADS)

    Benz, Julian K.; Carroll, Laura J.; Wright, Jill K.; Wright, Richard N.; Lillo, Thomas M.

    2014-06-01

    Creep of Alloy 617, a solid solution Ni-Cr-Mo alloy, was studied in the temperature range of 1023 K to 1273 K (750 C to 1000 C). Typical power-law creep behavior with a stress exponent of approximately 5 is observed at temperatures from 1073 K to 1273 K (800 C to 1000 C). Creep at 1023 K (750 C), however, exhibits threshold stress behavior coinciding with the temperature at which a low volume fraction of ordered coherent ?' precipitates forms. The threshold stress is determined experimentally to be around 70 MPa at 1023 K (750 C) and is verified to be near zero at 1173 K (900 C)temperatures directly correlating to the formation and dissolution of ?' precipitates, respectively. The ?' precipitates provide an obstacle to continued dislocation motion and result in the presence of a threshold stress. TEM analysis of specimens crept at 1023 K (750 C) to various strains, and modeling of stresses necessary for ?' precipitate dislocation bypass, suggests that the climb of dislocations around the ?' precipitates is the controlling factor for continued deformation at the end of primary creep and into the tertiary creep regime. As creep deformation proceeds at an applied stress of 121 MPa and the precipitates coarsen, the stress required for Orowan bowing is reached and this mechanism becomes active. At the minimum creep rate at an applied stress of 145 MPa, the finer precipitate size results in higher Orowan bowing stresses and the creep deformation is dominated by the climb of dislocations around the ?' precipitates.

  2. Creep of chemically vapour deposited SiC fibres

    NASA Technical Reports Server (NTRS)

    Dicarlo, J. A.

    1986-01-01

    The creep, thermal expansion, and elastic modulus properties for chemically vapor deposited SiC fibers were measured between 1000 and 1500 C. Creep strain was observed to increase logarithmically with time, monotonically with temperature, and linearly with tensile stress up to 600 MPa. The controlling activation energy was 480 + or - 20 kJ/mole. Thermal pretreatments near 1200 and 1450 C were found to significantly reduce fiber creep. These results coupled with creep recovery observations indicate that below 1400 C fiber creep is anelastic with negligible plastic component. This allowed a simple predictive method to be developed for describing fiber total deformation as a function of time, temperature, and stress. Mechanistic analysis of the property data suggests that fiber creep is the result of beta-SiC grain boundary sliding controlled by a small percent of free silicon in the grain boundaries.

  3. Creep of chemically vapor deposited SiC fibers

    NASA Technical Reports Server (NTRS)

    Dicarlo, J. A.

    1984-01-01

    The creep, thermal expansion, and elastic modulus properties for chemically vapor deposited SiC fibers were measured between 1000 and 1500 C. Creep strain was observed to increase logarithmically with time, monotonically with temperature, and linearly with tensile stress up to 600 MPa. The controlling activation energy was 480 + or - 20 kJ/mole. Thermal pretreatments near 1200 and 1450 C were found to significantly reduce fiber creep. These results coupled with creep recovery observations indicate that below 1400 C fiber creep is anelastic with neglible plastic component. This allowed a simple predictive method to be developed for describing fiber total deformation as a function of time, temperature, and stress. Mechanistic analysis of the property data suggests that fiber creep is the result of beta-SiC grain boundary sliding controlled by a small percent of free silicon in the grain boundaries.

  4. In-situ Creep Testing Capability Development for Advanced Test Reactor

    SciTech Connect

    B. G. Kim; J. L. Rempe; D. L. Knudson; K. G. Condie; B. H. Sencer

    2010-08-01

    Creep is the slow, time-dependent strain that occurs in a material under a constant strees (or load) at high temperature. High temperature is a relative term, dependent on the materials being evaluated. A typical creep curve is shown in Figure 1-1. In a creep test, a constant load is applied to a tensile specimen maintained at a constant temperature. Strain is then measured over a period of time. The slope of the curve, identified in the figure below, is the strain rate of the test during Stage II or the creep rate of the material. Primary creep, Stage I, is a period of decreasing creep rate due to work hardening of the material. Primary creep is a period of primarily transient creep. During this period, deformation takes place and the resistance to creep increases until Stage II, Secondary creep. Stage II creep is a period with a roughly constant creep rate. Stage II is referred to as steady-state creep because a balance is achieved between the work hardening and annealing (thermal softening) processes. Tertiary creep, Stage III, occurs when there is a reduction in cross sectional area due to necking or effective reduction in area due to internal void formation; that is, the creep rate increases due to necking of the specimen and the associated increase in local stress.

  5. Modeling creep behavior in a directionally solidified nickel base superalloy

    NASA Astrophysics Data System (ADS)

    Ibanez, Alejandro R.

    Directionally solidified (DS) nickel-base superalloys provide significant improvements relative to the limitations inherent to equiaxed materials in the areas of creep resistance, oxidation, and low and high cycle fatigue resistance. Since these materials are being pushed to the limits of their capability in gas turbine applications, accurate mathematical models are needed to predict the service lives of the hot-section components to prevent unscheduled outages due to sudden mechanical failures. The objectives of this study are to perform critical experiments and investigate the high temperature tensile, fracture toughness, creep deformation, creep rupture and creep crack growth behavior of DS GTD111 as well as to apply creep deformation, rupture and crack growth models that will enable the accurate representation of the life times of the DS GTD111 superalloy gas turbine components that are exposed to high temperatures under sustained tensile stresses. The applied models will be capable of accurately representing the creep deformation, rupture and crack growth behavior as a function of stress, time and temperature. The yield strength and fracture toughness behavior with temperature is governed by the gamma particles. The longitudinal direction showed higher ductility and strength than the transverse direction. The TL direction exhibited higher fracture toughness than the LT orientation because the crack follows a more tortuous path. The longitudinal direction showed higher creep ductility, lower minimum strain rates and longer creep rupture times than the transverse direction. The results in the transverse direction were similar to the ones for the equiaxed version of this superalloy. Two models for creep deformation have been evaluated. The power-law model includes a secondary and a tertiary creep term with the primary creep represented by a constant. A theta-projection model has also been evaluated and it appears to provide a more accurate representation of creep deformation over a wide range of stress, time and temperature conditions. The Monkman-Grant relationship, the Larson-Miller parameter and the theta projection model have been successfully used to predict the time to rupture for different orientation-temperature-stress conditions. The time dependent fracture mechanics approach is used to model creep crack growth behavior. The creep crack grows faster at higher temperatures and in the LT orientation, but the crack advance rate is uniquely characterized by Ct independent of the orientation and temperature.

  6. CREEP AND CREEP-FATIGUE OF ALLOY 617 WELDMENTS

    SciTech Connect

    Wright, Jill; Carroll, Laura; Wright, Richard

    2014-08-01

    The Very High Temperature Reactor (VHTR) Intermediate Heat Exchanger (IHX) may be joined to piping or other components by welding. Creep-fatigue deformation is expected to be a predominant failure mechanism of the IHX1 and thus weldments used in its fabrication will experience varying cyclic stresses interrupted by periods of elevated temperature deformation. These periods of elevated temperature deformation are greatly influenced by a materials’ creep behavior. The nickel-base solid solution strengthened alloy, Alloy 617, is the primary material candidate for a VHTR-type IHX, and it is expected that Alloy 617 filler metal will be used for welds. Alloy 617 is not yet been integrated into Section III of the Boiler and Pressure Vessel Code, however, nuclear component design with Alloy 617 requires ASME (American Society of Mechanical Engineers) Code qualification. The Code will dictate design for welded construction through significant performance reductions. Despite the similar compositions of the weldment and base material, significantly different microstructures and mechanical properties are inevitable. Experience of nickel alloy welds in structural applications suggests that most high temperature failures occur at the weldments or in the heat-affected zone. Reliably guarding against this type of failure is particularly challenging at high temperatures due to the variations in the inelastic response of the constituent parts of the weldment (i.e., weld metal, heat-affected zone, and base metal) [ref]. This work focuses on the creep-fatigue behavior of nickel-based weldments, a need noted during the development of the draft Alloy 617 ASME Code Case. An understanding of Alloy 617 weldments when subjected to this important deformation mode will enable determination of the appropriate design parameters associated with their use. Specifically, the three main areas emphasized are the performance reduction due to a weld discontinuity in terms of the reduced number of the cycles to failure and whether a saturation in reduced cycle life with increased hold times is observed, the microstructural stability over long cycle times, and finally, the location of the generated weldment data on a creep-fatigue damage diagram (D-diagram).

  7. Plasticity and diffusion creep of dolomite

    NASA Astrophysics Data System (ADS)

    Davis, N. E.; Kronenberg, A. K.; Newman, J.

    2008-08-01

    Natural and synthetic dolomites have been shortened in triaxial compression experiments at temperatures of 400-850 C, equilibrium CO 2 pore pressures, effective confining pressures of 50-400 MPa, and strain rates of 10 - 4 to 10 - 7 s - 1 . At low temperatures ( T < 700 C) natural and synthetic dolomites exhibit high crystal-plastic strengths (> 600 MPa), both for coarse-grained (240 ?m) and fine-grained (2 ?m and 12 ?m) samples; differential stresses vary little with strain rate or temperature and microstructures of coarse-grained samples are dominated by f-twins and undulatory extinction. An exponential relation ( ?? = ??o exp[ ?( ?1 - ?3)] between strain rate ?? and differential stress ( ?1 - ?3) describes the crystal plasticity of dolomite at a fixed Pe and T, with ? = 0.079 ( 0.01) MPa - 1 and 0.023 ( 07.03) MPa - 1 for coarse- and fine-grained materials, respectively. However, measured values of ( ?1 - ?3) increase with increasing temperature, a trend that has been observed for dolomite single crystals but cannot be described by an Arrhenius relation. At high temperatures ( T ? 800 C for coarse, T ? 700 C for fine), dolomite strengths are reduced with increasing temperature and decreasing strain rate, but the mechanisms of deformation differ depending on grain size. High temperature flow strengths of coarse-grained dolomite can be described by a power law ?? = ??o[( ?1 - ?3) / ?] nexp(- H* / RT) with a large value of n (> 5) and a ratio of parameters H* / n = 60 ( 6) kJ/mol. Microstructures of coarse-grained samples deformed at T ? 800 C show evidence of dislocation creep with little mechanical twinning. High temperature flow strengths of fine-grained synthetic dolomite fit a thermally activated Newtonian law, where the effective n = 1.28 ( 0.15) and H* = 280 ( 45 kJ/mol), consistent with diffusion creep. The change in mechanical response of coarse-grained natural dolomite with increasing temperature represents a transition from twinning and slip with little or no recovery to dislocation creep, while the change in response of fine-grained synthetic dolomite represents a transition from crystal plasticity to diffusion creep. The combined results for coarse- and fine-grained dolomites define a deformation mechanism map with fields of crystal plasticity, dislocation creep, and diffusion creep. Strengths of coarse-grained dolomite in the crystal plastic and dislocation creep fields are much larger than strengths of calcite rocks deformed by similar mechanisms. In contrast, strengths of fine-grained dolomite deformed by diffusion creep are more comparable to those of fine-grained calcite, suggesting little contrast in rheology.

  8. Effect of Preaging Deformation on Aging Characteristics of 2507 Super Duplex Stainless Steel

    NASA Astrophysics Data System (ADS)

    Mishra, M. K.; Rao, A. G.; Sarkar, R.; Kashyap, B. P.; Prabhu, N.

    2016-01-01

    In the present study, precipitation of sigma (?) phase was investigated over the temperature range of 700-850 C in undeformed and deformed (60% cold rolling) samples of 2507 super duplex stainless steel. The fraction of sigma phase formed as a result of the transformation ? ? ? + ?2 increases with increasing time and temperature. The increase in sigma phase leads to increase in yield strength and decrease in ductility. Preaging deformation leads to accelerated precipitation of sigma phase. The activation energy for sigma phase precipitation in deformed sample is found to be lower than that in undeformed sample.

  9. Effect of Preaging Deformation on Aging Characteristics of 2507 Super Duplex Stainless Steel

    NASA Astrophysics Data System (ADS)

    Mishra, M. K.; Rao, A. G.; Sarkar, R.; Kashyap, B. P.; Prabhu, N.

    2016-02-01

    In the present study, precipitation of sigma (σ) phase was investigated over the temperature range of 700-850 °C in undeformed and deformed (60% cold rolling) samples of 2507 super duplex stainless steel. The fraction of sigma phase formed as a result of the transformation α → σ + γ2 increases with increasing time and temperature. The increase in sigma phase leads to increase in yield strength and decrease in ductility. Preaging deformation leads to accelerated precipitation of sigma phase. The activation energy for sigma phase precipitation in deformed sample is found to be lower than that in undeformed sample.

  10. Influence of phosphorus on the creep ductility of copper

    NASA Astrophysics Data System (ADS)

    Sandstrm, Rolf; Wu, Rui

    2013-10-01

    Around 1990 it was discovered that pure copper could have extra low creep ductility in the temperature interval 180-250 C. The material was intended for use in canisters for nuclear waste disposal. Although extra low creep ductility was not observed much below 180 C and the temperature in the canister will never exceed 100 C, it was feared that the creep ductility could reach low values at lower temperatures after long term exposure. If 50 ppm phosphorus was added to the copper the low creep ductility disappeared. A creep cavitation model is presented that can quantitatively describe the cavitation behaviour in uniaxial and multiaxial creep tests as well as the observed creep ductility for copper with and without phosphorus. A so-called double ledge model has been introduced that demonstrates why the nucleation rate of creep cavities is often proportional to the creep rate. The phosphorus agglomerates at the grain boundaries and limits their local deformation and thereby reduces the formation and growth of cavities. This explains why extra low creep ductility does not occur in phosphorus alloyed copper.

  11. Creep relaxation and fully reversible creep of foam core sandwich composites in seawater

    NASA Astrophysics Data System (ADS)

    de la Paz, Ismael; Shafiq, Basir

    2015-12-01

    Foam core sandwich composites were subjected to (i) creep to failure, (ii) cyclic creep-relaxation and (iii) fully reversible cyclic creep loading in seawater in order to mimic an actual ship hull's service lifetime scenario. The results indicate a strong dependence of lifetime on the mode of loading. A significant reduction in the overall life was observed under cyclic creep as compared with the conventional creep to failure. Creep relaxation (R=1) tests were performed at loading-relaxation periods of 24/24, 24/12, 24/6, 12/12 and 6/6 h, while the fully reversible (R=-1) creep tests were conducted at loading-reversed loading times of 36/36, 24/24, 12/12, 6/6, and 3/3 h. The results suggest that creep-relaxation lifetime characteristics depend predominantly on the relaxation time as opposed to loading times, i.e. longer relaxation periods lead to shorter life. Whereas, fully reversible creep appears to be dependent upon the number of reversals whereby, life is observed to reduce as the number of reversals increase. These significant observations are explained in terms of various possible paths to interface cell wall collapse. Modes of failure were predominantly indentation and core compression in the vicinity of the loading site.

  12. Molecular dynamics simulations of the atom packing characteristics of three deformed silver nanoparticles at room temperature.

    PubMed

    Zhang, Lin

    2016-03-14

    Deformation is of significance in controlling the shape of materials, but the key structural information of metal nanoparticles is still limited. Molecular dynamics simulations are performed to explore the microscopic details of atom packing differences in three deformed silver nanoparticles with one atom difference. Analytical tools are used to demonstrate the effects of external load and surface atoms of particles on the packing patterns in these deformed nanoparticles including internal energy per atom, pair numbers, and pair distribution functions as well as cross-sectional images. The simulation results show that under small compression, the particles present elastic behaviors. The increasing compression results in the sliding of the atoms in different parts of these particles, and some interfaces are formed between these parts. As the external load becomes large, these deformed particles are compressed into the thickness of several atomic layers. The unloaded particles present different behaviors. PMID:26899951

  13. Unified creep-plasticity model for halite

    SciTech Connect

    Krieg, R. D.

    1980-11-01

    There are two national energy programs which are considering caverns in geological salt (NaCl) as a storage repository. One is the disposal of nuclear wastes and the other is the storage of oil. Both short-time and long-time structural deformations and stresses must be predictable for these applications. At 300K, the nominal initial temperature for both applications, the salt is at 0.28 of the melting temperature and exhibits a significant time dependent behavior. A constitutive model has been developed which describes the behavior observed in an extensive set of triaxial creep tests. Analysis of these tests showed that a single deformation mechanism seems to be operative over the stress and temperature range of interest so that the secondary creep data can be represented by a power of the stress over the entire test range. This simple behavior allowed a new unified creep-plasticity model to be applied with some confidence. The resulting model recognizes no inherent difference between plastic and creep strains yet models the total inelastic strain reasonably well including primary and secondary creep and reverse loadings. A multiaxial formulation is applied with a back stress. A Bauschinger effect is exhibited as a consequence and is present regardless of the time scale over which the loading is applied. The model would be interpreted as kinematic hardening in the sense of classical plasticity. Comparisons are made between test data and model behavior.

  14. Creep Laboratory manual

    NASA Astrophysics Data System (ADS)

    Osgerby, S.; Loveday, M. S.

    1992-06-01

    A manual for the NPL Creep Laboratory, a collective name given to two testing laboratories, the Uniaxial Creep Laboratory and the Advanced High Temperature Mechanical Testing Laboratory, is presented. The first laboratory is devoted to uniaxial creep testing and houses approximately 50 high sensitivity creep machines including 10 constant stress cam lever machines. The second laboratory houses a low cycle fatigue testing machine of 100 kN capacity driven by a servo-electric actuator, five machines for uniaxial tensile creep testing of engineering ceramics at temperatures up to 1600C, and an electronic creep machine. Details of the operational procedures for carrying out uniaxial creep testing are given. Calibration procedures to be followed in order to comply with the specifications laid down by British standards, and to provide traceability back to the primary standards are described.

  15. Small Two-Bar Specimen Creep Testing of Grade P91 Steel at 650°C

    NASA Astrophysics Data System (ADS)

    Ali, Balhassn S. M.; Hyde, Tom H.; Sun, Wei

    2016-03-01

    Commonly used small creep specimen types, such as ring and impression creep specimens, are capable of providing minimum creep strain rate data from small volumes of material. However, these test types are unable to provide the creep rupture data. In this paper the recently developed two-bar specimen type, which can be used to obtain minimum creep strain rate and creep rupture creep data from small volumes of material, is described. Conversion relationships are used to convert (i) the applied load to the equivalent uniaxial stress, and (ii) the load line deformation rate to the equivalent uniaxial creep strain rate. The effects of the specimen dimension ratios on the conversion factors are also discussed in this paper. This paper also shows comparisons between two-bar specimen creep test data and the corresponding uniaxial creep test data, for grade P91 steel at 650°C.

  16. Material Parameters for Creep Rupture of Austenitic Stainless Steel Foils

    NASA Astrophysics Data System (ADS)

    Osman, H.; Borhana, A.; Tamin, M. N.

    2014-08-01

    Creep rupture properties of austenitic stainless steel foil, 347SS, used in compact recuperators have been evaluated at 700 C in the stress range of 54-221 MPa to establish the baseline behavior for its extended use. Creep curves of the foil show that the primary creep stage is brief and creep life is dominated by tertiary creep deformation with rupture lives in the range of 10-2000 h. Results are compared with properties of bulk specimens tested at 98 and 162 MPa. Thin foil 347SS specimens were found to have higher creep rates and higher rupture ductility than their bulk specimen counterparts. Power law relationship was obtained between the minimum creep rate and the applied stress with stress exponent value, n = 5.7. The value of the stress exponent is indicative of the rate-controlling deformation mechanism associated with dislocation creep. Nucleation of voids mainly occurred at second-phase particles (chromium-rich M23C6 carbides) that are present in the metal matrix by decohesion of the particle-matrix interface. The improvement in strength is attributed to the precipitation of fine niobium carbides in the matrix that act as obstacles to the movement of dislocations.

  17. Central Cascadia subduction zone creep

    NASA Astrophysics Data System (ADS)

    Schmalzle, Gina M.; McCaffrey, Robert; Creager, Kenneth C.

    2014-04-01

    Cascadia between 43N and 46N has reduced interseismic uplift observed in geodetic data and coseismic subsidence seen in multiple thrust earthquakes, suggesting elevated persistent fault creep in this section of the subduction zone. We estimate subduction thrust "decade-scale" locking and crustal block rotations from three-component continuous Global Positioning System (GPS) time series from 1997 to 2013, as well as 80 year tide gauge and leveling-derived uplift rates. Geodetic observations indicate coastal central Oregon is rising at a slower rate than coastal Washington, southern Oregon and northern California. Modeled locking distributions suggest a wide locking transition zone that extends inland under central Oregon. Paleoseismic records of multiple great earthquakes along Cascadia indicate less subsidence in central Oregon. The Cascade thrust under central Oregon may be partially creeping for at least 6500 years (the length of the paleoseismic record) reducing interseismic uplift and resulting in reduced coseismic subsidence. Large accretions of Eocene age basalt (Siletzia terrane) between 43N and 46N may be less permeable compared to surrounding terranes, potentially increasing pore fluid pressures along the fault interface resulting in a wide zone of persistent fault creep. In a separate inversion, three-component GPS time series from 1 July 2005 to 1 January 2011 are used to estimate upper plate deformation, locking between slow-slip events (SSEs), slip from 16 SSEs and an earthquake mechanism. Cumulative SSEs and tectonic tremor are weakest between 43N and 46N where partial fault creep is increased and Siletzia terrane is thick, suggesting that surrounding rock properties may influence the mode of slip.

  18. Transient Analysis for the Multimechanism-Deformation Parameters of Several Domal Salts

    SciTech Connect

    Munson, Darrell E.

    1999-08-16

    Use of Gulf Coast salt domes for construction of very large storage caverns by solution mining has grown significantly in the last several decades. In fact, a nationally important Strategic Petroleum Reserve (SPR) storage occurs in large cavern arrays in some of these domes. Although caverns have been operated economically for these many years, these caverns have a range of relatively poorly understood behaviors, involving creep closure fluid loss and damage from salt falls. It is certainly possible to postulate that many of these behaviors stem from geomechanical or deformational aspects of the salt response. As a result, a method of correlating the cavern response to mechanical creep behavior as determined in the laboratory could be of considerable importance. Recently, detailed study of the creep response of domal salts has cast some insight into the influence of different salt origins on cavern behavior. The study used a simple graphical analysis of the limited non-steady state data to give a bound, or an approach to steady state, as an estimate of the steady state behavior of a given domal salt. This permitted the analysis of sparse creep databases for domal salts. It appears that a shortcoming of the steady state analysis was in masking some of the salt material differences. In an attempt to overcome the steady state analysis shortcomings, a method was developed based on the integration of the Multimechanism-Deformation (M-D) creep constitutive model to fit the transient response. This integration process essentially permits definition of the material sensitive parameters of the model, while those parameters that are either constants or material insensitive parameters are fixed independently. The transient analysis method has proven more sensitive to differences in the creep characteristics and has provided a way of defining different behaviors within a given dome. Creep characteristics, as defined by the transient analysis of the creep rate, are related quantitatively to the volume loss creep rate of the caverns. This type of understanding of the domal material creep response already has pointed to the possibility of establishing various distinct material spines within a given dome. Furthermore, if the creep databases for domal salts can be expanded, one could expect additional definition of domal geology and structure.

  19. Probabilistic models for creep-fatigue in a steel alloy

    NASA Astrophysics Data System (ADS)

    Ibisoglu, Fatmagul

    In high temperature components subjected to long term cyclic operation, simultaneous creep and fatigue damage occur. A new methodology for creep-fatigue life assessment has been adopted without the need to separate creep and fatigue damage or expended life. Probabilistic models, described by hold times in tension and total strain range at temperature, have been derived based on the creep rupture behavior of a steel alloy. These models have been validated with the observed creep-fatigue life of the material with a scatter band close to a factor of 2. Uncertainties of the creep-fatigue model parameters have been estimated with WinBUGS which is an open source Bayesian analysis software tool that uses Markov Chain Monte Carlo method to fit statistical models. Secondly, creep deformation in stress relaxation data has been analyzed. Well performing creep equations have been validated with the observed data. The creep model with the highest goodness of fit among the validated models has been used to estimate probability of exceedance at 0.6% strain level for the steel alloy.

  20. Effect of Phosphorous Inoculation on Creep Behavior of a Hypereutectic Al-Si Alloy

    NASA Astrophysics Data System (ADS)

    Faraji, Masoumeh; Khalilpour, Hamid

    2014-10-01

    Creep behavior of Al-Si hypereutectic alloys inoculated with phosphorus was investigated using the impression creep testing. The results showed that at stress regimes of up to 400-450 MPa and temperatures up to 300 C, no significant creep deformation occurred in both uninoculated and inoculated specimens; however, at temperatures above 300 C, the inoculated alloys presented better creep properties. Creep data were used to calculate the stress exponent of steady-state creep rate, n, and creep activation energy, Q, for different additive conditions where n was found varied between 5 and 8. Owing to the fact that most alloys have lower values for n (4, 5), threshold stress was estimated for studied conditions. The creep governing mechanisms for different conditions are discussed here, with a particular attention to the effect of phosphorous addition on the microstructural features, including number of primary silicon particles, mean primary silicon spacing, and morphology and distribution of eutectic silicon.

  1. Analysis of Faulting and Sediment Velocity Characteristics Outboard of the Cascadia Deformation Front from Multi-Channel Seismic Data.

    NASA Astrophysics Data System (ADS)

    Gibson, J. C.; Carbotte, S. M.; Han, S.; Nedimovic, M. R.; Canales, J. P.; Carton, H. D.

    2014-12-01

    Faulting of the sediment section on the downgoing Juan de Fuca Plate (JdF) outboard of the Cascadia deformation front is explored using multi-channel seismic (MCS) data collected in 2012 during the JdF Ridge to Trench Survey (MGL1211). MCS data were collected along two full plate transects ("Oregon" (ORT) and "Washington" (WAT)) and one trench parallel line. Sediment velocity analysis is conducted via semblance spectrums on common mid-point super gathers spaced at a 625 m interval. Higher sediment velocities are found in the north, which may reflect the regional differences in sediment composition evident in existing drill holes located along our transects (DSDP site 174 - ORT and ODP site 1027 - WAT) that indicate higher smectite content along the ORT (bulk composition +44%). Accordingly, observations of fault frequency, dip, and throw along both transects show significant differences in faulting characteristics across the JdF plate. Faulting extends ~175 km (8.2 - 1.9 Ma plate age) from the deformation front along the WAT, and reaches a maximum fault density of ~0.48 fault/km in the region between 25 - 113 km (7.5 - 4 Ma plate age). Evidence of faulting extends ~300 km (8.9 - 2.6 Ma plate age) from the deformation front along the ORT and reaches a similar high fault density of ~0.48 fault/km in the region between 113 - 138 km (7.07 - 5.96 Ma plate age). Analysis of fault offset indicates growth faults along both transects. Along the ORT, maximum fault throws remain ~uniform at 10 - 15 m for crustal ages of 7.07 - 5.96 Ma and beginning ~75 km from the deformation front increase landward to maximum throws of 30 m, consistent with increasing fault strain due to flexural bending of the downgoing plate. In contrast, along the WAT, there is no evidence of increasing fault throw toward the deformation front. High fault dips (45 - 70°) are found in the region of highest fault density on both transects. Lower dips (35 - 60°) are measured in the region of increasing fault strain near the deformation front along the ORT. Overall, fault characteristics indicate greater subduction-bend related faulting along the ORT. Additionally, complex intra-plate stresses and/or differential compaction may contribute to the abundant faulting found within the plate interior to young crustal ages along both transects.

  2. Creep-assisted slow crack growth in bio-inspired dental multilayers.

    PubMed

    Du, Jing; Niu, Xinrui; Soboyejo, Wole

    2015-06-01

    Ceramic crown structures under occlusal contact are often idealized as flat multilayered structures that are deformed under Hertzian contact loading. Previous models treated each layer as linear elastic materials and resulted in differences between the measured and predicted critical loads. This paper examines the combined effects of creep (in the adhesive and substrate layers) and creep-assisted slow crack growth (in the ceramic layer) on the contact-induced deformation of bio-inspired, functionally graded multilayer (FGM) structures and the conventional tri-layers. The time-dependent moduli of each of the layers were determined from constant load creep tests. The resulting modulus-time characteristics were modeled using Prony series. These were then incorporated into a finite element model for the computation of stress distributions in the sub-surface regions of the top ceramic layer, in which sub-surface radial cracks, are observed as the clinical failure mode. The time-dependent stresses are incorporated into a slow crack growth (SCG) model that is used to predict the critical loads of the dental multilayers under Hertzian contact loading. The predicted loading rate dependence of the critical loads is shown to be consistent with experimental results. The implications of the results are then discussed for the design of robust dental multilayers. PMID:25771255

  3. Relationship between creep, gamma 2, and marginal fracture of dental amalgams.

    PubMed

    Sarkar, N K; Eyer, C S; Norling, B K

    1983-11-01

    The effect of gamma 1 and gamma 2 on the creep deformation of dental amalgams has been investigated. It has been shown that the creep of a conventional amalgam is not dependent on gamma 1 as was previously reported. Rather it is strongly influenced by gamma 2 and its volume fraction. It has been speculated that Sn-rich grain boundaries also enhance creep by facilitating grain boundary sliding. The reported correlation between creep and marginal fracture has been explained in terms of this dependence of creep on corrosion-prone Sn-rich microstructural constituents of amalgams. PMID:6580405

  4. Development of a constitutive model for creep and life prediction of advanced silicon nitride ceramics

    SciTech Connect

    Ding, J.L.; Liu, K.C.; Brinkman, C.R.

    1992-12-31

    A constitutive model capable of describing deformation and predicting rupture life was developed for high temperature ceramic materials under general thermal-mechanical loading conditions. The model was developed based on the deformation and fracture behavior observed from a systematic experimental study on an advanced silicon nitride (Si{sub 3}N{sub 4}) ceramic material. Validity of the model was evaluated with reference to creep and creep rupture data obtained under constant and stepwise-varied loading conditions, including the effects of annealing on creep and creep rupture behavior.

  5. Creep of PEEK-graphite fibre composite material

    NASA Astrophysics Data System (ADS)

    Enns, Jonathan; Cahoon, J. R.

    1991-05-01

    The thermoplastic matrix composites are a relatively new class of materials and their mechanical properties have not yet been fully characterized. Therefore, a study was initiated to determine the high temperature creep behavior of polyether ether ketone (PEEK) matrix-graphite fiber composites, one of the new thermoplastic matrix composites. The samples were tested in the longitudinal direction (direction of maximum strength) using 3-point bending with a span length of 2.5 inches. Tests were conducted at 8 temperatures from 20 C to 220 C. Creep tests were conducted for period of time ranging from a few hours to a few days. The Larson-Miller parameter method shows some promise for predicting long term creep behavior of PEEK-graphite fiber composite material. Creep failure occurs suddenly after very small creep deformations of only 0.01-0.04 percent at high temperatures and is, therefore, quite insidious in nature since imminent failure is most difficult to detect.

  6. Wear characteristics of severely deformed aluminum sheets by accumulative roll bonding (ARB) process

    SciTech Connect

    Talachi, A. Kazemi; Eizadjou, M. Manesh, H. Danesh; Janghorban, K.

    2011-01-15

    Wear behavior of severely deformed aluminum sheets by accumulative roll bonding (ARB) process was characterized using a pin on disc wear machine at different conditions. The sheets were processed up to eight ARB cycles in order to induce a high strain ({approx} 6.4) to the samples. EBSD results showed that after eight cycles of ARB, sheets were found to contain ultrafine grains with high fraction of high angle grain boundaries. Wear experiments were conducted under different loading and operating conditions, including dry and immersion lubrication, and rotation speeds. Wear was continuously monitored by measuring the wear rates and morphologies of worn surfaces by scanning electron microscope (SEM). Contrary to expectation, the wear resistance of the ARBed Al sheets was less than the non-processed sheets. Wear rates of the ARBed Al sheets increased by increasing wear load and rotation speed, while, immersion lubrication decreased the wear rate significantly. Based on the observation and results, a model for the wear of the ARBed Al was proposed. - Research Highlights: {yields}The wear rate of the ARBed Al was higher than that of the non-processed alloy. {yields}This unexpected behavior was related to the low strain hardening capability and evolution of the ARB subsurface microstructure during the wear process. {yields}Sliding wear of the ARBed Al proceeded by surface deformation, and progressed by delamination of the deformed surface layer. {yields}The wear rate of ARBed Al increased by increasing applied load and sliding speed.

  7. Changes in the expression of genetic characteristics across cohorts in skeletal deformations of farmed salmonids

    PubMed Central

    Kause, Antti; Ritola, Ossi; Paananen, Tuija

    2007-01-01

    Genetic analysis of disorder incidence in farmed animals is challenged by two factors. Disorders in different cohorts and environments could be caused by different factors, leading to changes in heritability and to less than unity genetic correlations across cohorts. Moreover, due to computational limitations, liability scale heritabilities at very low incidence may differ from those estimated at higher incidence. We tested whether these two dilemmas occur in skeletal deformations of farmed salmonids using multigeneration data from the Finnish rainbow trout breeding programme and previous salmonid studies. The results showed that heritability was close to zero in cohorts in which management practices maintained incidence at a low level. When there was a management failure and incidence was unusually high, heritability was elevated. This may be due to computational limitations at very low incidence and/or because deformations are induced by different factors in different cohorts. Most genetic correlations between deformations recorded in different generations were weakly to strongly positive. However, also negative correlations between generations were present, showing that high liability at one time can be genetically connected to low liability at another time. The results emphasise that genetic architecture of binary traits can be influenced by trait expression. PMID:17897595

  8. Novel characteristics of energy spectrum for 3D Dirac oscillator analyzed via Lorentz covariant deformed algebra

    PubMed Central

    Betrouche, Malika; Maamache, Mustapha; Choi, Jeong Ryeol

    2013-01-01

    We investigate the Lorentz-covariant deformed algebra for Dirac oscillator problem, which is a generalization of Kempf deformed algebra in 3 + 1 dimension of space-time, where Lorentz symmetry are preserved. The energy spectrum of the system is analyzed by taking advantage of the corresponding wave functions with explicit spin state. We obtained entirely new results from our development based on Kempf algebra in comparison to the studies carried out with the non-Lorentz-covariant deformed one. A novel result of this research is that the quantized relativistic energy of the system in the presence of minimal length cannot grow indefinitely as quantum number n increases, but converges to a finite value, where c is the speed of light and ? is a parameter that determines the scale of noncommutativity in space. If we consider the fact that the energy levels of ordinary oscillator is equally spaced, which leads to monotonic growth of quantized energy with the increment of n, this result is very interesting. The physical meaning of this consequence is discussed in detail. PMID:24225900

  9. Diffusional creep and diffusion-controlled dislocation creep and their relation to denuded zones in Mg-ZrH{sub 2} materials

    SciTech Connect

    Ruano, O.A.; Sherby, O.D.; Wadsworth, J.; Wolfenstine, J.

    1998-03-13

    Langdon`s contention that creep of Mg-0.5 wt% Zr is well characterized by diffusional creep at 400 C is in error. It is shown that Langdon and Gifkins` single analysis of denuded zones formed during creep at 2 MPa, purporting to occur as a result of diffusional creep, in fact, took place in the power-law dislocation creep range where solute atoms are interacting with moving dislocations. This observation supports the earlier conclusions made for creep and denuded zones observed in the hydrided Mg-Zr alloy at 500 C. Furthermore, it is shown that Pickles` data at stresses below 2 MPa at 400 C are not related to diffusional creep as considered by Langdon. In this region, denuded zones appear in both longitudinal and transverse boundaries indicating that grain boundary sliding, accompanied by grain boundary migration, is the principal deformation process. It is proposed that denuded zones are caused by dissolution of precipitates at moving grain boundaries.

  10. EBSD and TEM investigation of the hot deformation substructure characteristics of a type 316L austenitic stainless steel.

    PubMed

    Cizek, P; Whiteman, J A; Rainforth, W M; Beynon, J H

    2004-03-01

    The evolution of crystallographic texture and deformation substructure was studied in a type 316L austenitic stainless steel, deformed in rolling at 900 degrees C to true strain levels of about 0.3 and 0.7. Electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM) were used in the investigation and a comparison of the substructural characteristics obtained by these techniques was made. At the lower strain level, the deformation substructure observed by EBSD appeared to be rather poorly developed. There was considerable evidence of a rotation of the pre-existing twin boundaries from their original orientation relationship, as well as the formation of highly distorted grain boundary regions. In TEM, at this strain level, the substructure was more clearly revealed, although it appeared rather inhomogeneously developed from grain to grain. The subgrains were frequently elongated and their boundaries often approximated to traces of [111] slip planes. The corresponding misorientations were small and largely displayed a non-cumulative character. At the larger strain, the substructure within most grains became well developed and the corresponding misorientations increased. This resulted in better detection of sub-boundaries by EBSD, although the percentage of indexing slightly decreased. TEM revealed splitting of some sub-boundaries to form fine microbands, as well as the localized formation of microshear bands. The substructural characteristics observed by EBSD, in particular at the larger strain, generally appeared to compare well with those obtained using TEM. With increased strain level, the mean subgrain size became finer, the corresponding mean misorientation angle increased and both these characteristics became less dependent on a particular grain orientation. The statistically representative data obtained will assist in the development of physically based models of microstructural evolution during thermomechanical processing of austenitic stainless steels. PMID:15009696

  11. Tension-Compression Asymmetry of Creep and Unilateral Creep Damage in Aluminum for Isothermal and Nonisothermal Processes

    NASA Astrophysics Data System (ADS)

    Zolochevsky, Alexander; Obataya, Yoichi

    A constitutive model is proposed to describe the damage development in aluminum alloys under creep conditions for both isothermal and nonisothermal processes. Special emphasis is laid on four specific phenomena: tension-compression asymmetry of creep, damage induced anisotropy, unilateral creep damage and damage deactivation. Within the framework of the phenomenological approach in the Continuum Damage Mechanics, the nonlinear tensor constitutive equation for creep deformation and damage evolution equation are proposed to account for different orientation of microcracks in aluminum alloys under tensile and compressive loading types. After a determination of the material parameters in the obtained constitutive equation and damage growth equation, the proposed model is applied to the describing creep behavior of the aluminum alloy under uniaxial nonproportional and multiaxial nonproportional loading for both isothermal and nonisothermal processes.

  12. Mathematical model of creep for a microinhomogeneous nonlinearly elastic material

    NASA Astrophysics Data System (ADS)

    Radchenko, V. P.; Shapievskii, D. V.

    2008-05-01

    A mathematical model is proposed to describe the experimentally observed creep effect on the instantaneous elastic deformation of physically nonlinear elastic microinhomogeneous materials. Using a structural model of the medium, it is shown that, during unloading of a sample after creep at constant stress, the elastic strain can be both larger and smaller than the elastic strain during loading. It is shown that calculation results for a biocomposite material are in good agreement with experimental data.

  13. A loading system for creep testing under constant compressive stress

    NASA Technical Reports Server (NTRS)

    Dobes, F.; Zverina, O.; Cadek, J.

    1987-01-01

    A critical analysis is made of layouts assuring constant stress under creep, pointing out the difficulties of using these layouts for compressive testing. A new mechanical system to maintain stress during creep testing is proposed. Constant stress is achieved by a definite motion of the load. The proposed system can be used in tensile or compressive testing. Practical measurements reveal that the stress constancy error is not greater than plus or minus 1.5 percent up to relative deformation of 30 percent.

  14. An Evaluation for Creep of 3013 Inner Can Lids

    SciTech Connect

    DAUGHERTY, W. L.; GIBBS, K. M.; LOUTHAN JR., M. R.; DUNN, K. A.

    2005-09-01

    The deflection of Type 304L austenitic stainless steel can lids on inner 3013 containers is monitored to identify any buildup of pressure within the container. This paper provides the technical basis to conclude that creep-induced deformation of these lids will be insignificant unless the temperature of storage exceeds 400 C. This conclusion is based on experimental literature data for Types 304 and 316 stainless steel and on a phenomenological evaluation of potential creep processes.

  15. Continuous deformation versus episodic deformation at high stress - the microstructural record

    NASA Astrophysics Data System (ADS)

    Trepmann, C. A.; Stckhert, B.

    2009-04-01

    The microstructural record of continuous high stress deformation is compared to that of episodic high stress deformation on two examples: 1. Folding of quartz veins in metagreywacke from Pacheco Pass, California, undergoing deformation by dissolution precipitation creep at temperatures of 300 50C. The microfabric of the folded quartz veins indicates deformation by dislocation creep accompanied by subgrain rotation. The small recrystallized grain size of ~86 m in average implies relatively high differential stresses of a few hundred MPa. The stress concentration in the vein is due to a high contrast in effective viscosities between the single phase material and the polyphase fine-grained host metagreywacke deforming by dissolution precipitation creep. Smoothly curved, but generally not sutured, grain boundaries as well as the small size and a relatively high dislocation density of recrystallized grains suggest that strain-induced grain boundary migration was of minor importance. This is suspected to be a consequence of low strain gradients, which are due to the relative rates of dynamic recovery and continuous dislocation production during climb-controlled creep, at high stress and the given low temperature. Subgrain rotation recrystallization is thus proposed to be characteristic for continuous deformation at high differential stress. 2. Episodic deformation in the middle crust at the tip of a seismic active fault zone. The microfabric of mid-crustal rocks exhumed in tectonically active regions can record episodic high stress deformation at the base of the seismogenic layer. The quartz veins from St. Paul la Roche in the Massif Central, France, are very coarse grained. On the scale of a thin section they are basically single crystalline. However, they show a very heterogeneous microstructure with a system of healed microcracks that are decorated by subgrains and more rarely by small recrystallized grains. Undulating deformation lamellae that do not show a preferred crystallographic orientation are found by transmission electron microscopy to represent dislocation walls with a high density of dislocations. They are interpreted as a modified microstructure that reflects a stage of initial high stress deformation with restricted dynamic recovery. The missing aggregates of recrystallized grains rule out dynamic recrystallization, which is proposed to be due to a high strain rate, preventing effective dislocation climb. Instead, localized single grains in random orientations that are aligned along fractures indicate quasi-static recrystallization and recovery at a subsequent stage of low stress and temperatures of ~300 50C. Such a microstructure is characteristic of initial short-term high stress glide-controlled deformation accompanied by microcracking during coseismic loading and subsequent modification by recovery and recrystallization at rapidly decreasing stresses during postseismic relaxation in the middle crust below the seismogenic layer. Both examples indicate deformation of quartz at similar conditions in terms of temperature (~300 50C) and high stress. However, the deformation and recrystallization processes and the resulting microfabrics are completely different due to the different loading time and rate.

  16. Characterization of the groundwater response to rainfall on a hillslope with fractured bedrock by creep deformation and its implication for the generation of deep-seated landslides on Mt. Wanitsuka, Kyushu Island

    NASA Astrophysics Data System (ADS)

    Padilla, Cristobal; Onda, Yuichi; Iida, Tomoyuki; Takahashi, Shinya; Uchida, Taro

    2014-01-01

    In this study, the hydrogeological response of a hillslope affected by gravitational deformation was analyzed based on the data obtained for two observation boreholes: a 10-m borehole representing a relatively superficial section of the hillslope dominated by soil and old landslide deposits and a 40-m borehole representing the bedrock aquifer. For this analysis, the precipitation events in the area, groundwater levels of the two boreholes, electrical conductivity and isotopic concentration (oxygen and hydrogen) of the groundwater in the boreholes and rainfall samples were measured. Derived from the rainfall data, the antecedent precipitation index (API) with a 6-h half-life offers a good correlation with the peaks in the groundwater levels in the bedrock aquifer. The characteristics of the groundwater response suggest the existence of a single structure in the bedrock that controls the response of the hillslope. The structure serves as a conduit, which rapidly drives the rainfall water (recharge) into the bedrock. Evidently, this process is unrelated to the superficial section represented by the observations in the 10-m borehole. The structure is associated with an area of high hydraulic conductivity in the bedrock caused by the gravitational deformation in the hillslope. The strong control of this structure in the hillslope's hydrogeological response makes it responsible for the hillslope's stability during high-precipitation events. This information is highly relevant to areas featuring the generation of several deep-seated landslides under heavy-rain conditions.

  17. Plastic Deformation Characteristics Of AZ31 Magnesium Alloy Sheets At Elevated Temperature

    SciTech Connect

    Park, Jingee; Lee, Jongshin; You, Bongsun; Choi, Seogou; Kim, Youngsuk

    2007-05-17

    Using lightweight materials is the emerging need in order to reduce the vehicle's energy consumption and pollutant emissions. Being a lightweight material, magnesium alloys are increasingly employed in the fabrication of automotive and electronic parts. Presently, magnesium alloys used in automotive and electronic parts are mainly processed by die casting. The die casting technology allows the manufacturing of parts with complex geometry. However, the mechanical properties of these parts often do not meet the requirements concerning the mechanical properties (e.g. endurance strength and ductility). A promising alternative can be forming process. The parts manufactured by forming could have fine-grained structure without porosity and improved mechanical properties such as endurance strength and ductility. Because magnesium alloy has low formability resulted form its small slip system at room temperature it is usually formed at elevated temperature. Due to a rapid increase of usage of magnesium sheets in automotive and electronic industry it is necessary to assure database for sheet metal formability and plastic yielding properties in order to optimize its usage. Especially, plastic yielding criterion is a critical property to predict plastic deformation of sheet metal parts in optimizing process using CAE simulation. Von-Mises yield criterion generally well predicts plastic deformation of steel sheets and Hill'1979 yield criterion predicts plastic deformation of aluminum sheets. In this study, using biaxial tensile test machine yield loci of AZ31 magnesium alloy sheet were obtained at elevated temperature. The yield loci ensured experimentally were compared with the theoretical predictions based on the Von-Mises, Hill, Logan-Hosford, and Barlat model.

  18. Creep behaviour of Cu-30 percent Zn at intermediate temperatures

    NASA Technical Reports Server (NTRS)

    Raj, S. V.

    1991-01-01

    The present, intermediate-temperature (573-823 K) range investigation of creep properties for single-phase Cu-30 percent Zn alpha-brass observed inverse, linear, and sigmoidal primary-creep transients above 573 K under stresses that yield minimum creep rates in the 10 to the -7th to 2 x 10 to the -4th range; normal primary creep occurred in all other conditions. In conjunction with a review of the pertinent literature, a detailed analysis of these data suggests that no clearly defined, classes M-to-A-to-M transition exists in this alloy notwithstanding the presence of both classes' characteristics under nominally similar stresses and temperatures.

  19. An Investigation into Hot Deformation Characteristics and Processing Maps of High-Strength Armor Steel

    NASA Astrophysics Data System (ADS)

    Bobbili, Ravindranadh; Madhu, V.

    2015-12-01

    The isothermal hot compression tests of high-strength armor steel over wide ranges of strain rates (0.01-10 /s) and deformation temperatures (950-1100 °C) are carried out using Gleeble thermo-simulation machine. The true stress-strain data obtained from the experiments are employed to establish the constitutive equations based on the strain-compensated Arrhenius model. With strain-compensated Arrhenius model, good agreement between the experimental and predicted values is achieved, which represents the highest accuracy in comparison with the other models. The hot deformation activation energy is estimated to be 512 kJ/mol. By employing dynamic material model, the processing maps of high-strength armor steel at various strains are established. A maximum efficiency of about 45% of power dissipation is obtained at high temperature and low strain rate. Due to the high power dissipation efficiency and excellent processing ability in dynamic recrystallization zone for metal material, the optimum processing conditions are selected such that the temperature range is between 1050 and 1100°C and the strain rate range is between 0.01 and 0.1/s. Transmission electron microscopy observations show that the dislocation density is directly associated with the value of processing efficiency.

  20. An Investigation into Hot Deformation Characteristics and Processing Maps of High-Strength Armor Steel

    NASA Astrophysics Data System (ADS)

    Bobbili, Ravindranadh; Madhu, V.

    2015-11-01

    The isothermal hot compression tests of high-strength armor steel over wide ranges of strain rates (0.01-10 /s) and deformation temperatures (950-1100 C) are carried out using Gleeble thermo-simulation machine. The true stress-strain data obtained from the experiments are employed to establish the constitutive equations based on the strain-compensated Arrhenius model. With strain-compensated Arrhenius model, good agreement between the experimental and predicted values is achieved, which represents the highest accuracy in comparison with the other models. The hot deformation activation energy is estimated to be 512 kJ/mol. By employing dynamic material model, the processing maps of high-strength armor steel at various strains are established. A maximum efficiency of about 45% of power dissipation is obtained at high temperature and low strain rate. Due to the high power dissipation efficiency and excellent processing ability in dynamic recrystallization zone for metal material, the optimum processing conditions are selected such that the temperature range is between 1050 and 1100C and the strain rate range is between 0.01 and 0.1/s. Transmission electron microscopy observations show that the dislocation density is directly associated with the value of processing efficiency.

  1. Research of dynamical Characteristics of slow deformation Waves as Massif Responses on Explosions

    NASA Astrophysics Data System (ADS)

    Hachay, Olga; Khachay, Oleg; Shipeev, Oleg

    2013-04-01

    The research of massif state with use of approaches of open system theory [1-3] was developed for investigation the criterions of dissipation regimes for real rock massifs, which are under heavy man-caused influence. For realization of that research we used the data of seismic catalogue of Tashtagol mine. As a result of the analyze of that data we defined character morphology of phase trajectories of massif response, which was locally in time in a stable state: on the phase plane with coordinates released by the massif during the dynamic event energy E and lg(dE/dt) there is a local area as a ball of twisted trajectories and some not great bursts from that ball, which are not greater than 105 joules. In some time intervals that burst can be larger, than 105 joules, achieving 106 joules and yet 109 joules. [3]. Evidently there are two reciprocal depend processes: the energy accumulation in the attracted phase trajectories area and resonance fault of the accumulated energy. But after the fault the system returns again to the same attracted phase trajectories area. For analyzing of the thin structure of the chaotic area we decided to add the method of processing of the seismic monitoring data by new parameters. We shall consider each point of explosion as a source of seismic or deformation waves. Using the kinematic approach of seismic information processing we shall each point of the massif response use as a time point of the first arrival of the deformation wave for calculation of the wave velocity, because additionally we know the coordinates of the fixed response and the coordinates of explosion. The use of additional parameter-velocity of slow deformation wave propagation allowed us with use method of phase diagrams identify their hierarchic structure, which allow us to use that information for modeling and interpretation the propagation seismic and deformation waves in hierarchic structures. It is researched with use of that suggested processing method the thin structure of the chaotic area for two responses of the massif on a high energetic explosion in the northern and southern parts of it. The results are significant for understanding the high energetic rock shock and evaluation a criterion for massif stability estimation. The work is supported by the grant RFBR 10-05-00013 and Integration Project 2012-2014 with SB RAS Key words: massif response, slow deformation waves, seismic mine catalogue, analyze of observed data, phase diagrams. References 1. Naimark Y.I.,Landa P.S. Stochastic and chaotic oscillations//Moscow: Book House "LIBROKOM", 2009.-p.424. 2. Chulichkov A.I. Mathematical models of nonlinear dynamics.Moscow: Fizmatlit, 2003.-p.294. 3. Hachay O.A.,Khachay O.Y.,Klimko V.K.,Shipeev O.V. Reflection of synergetic features of rock massif state under man-caused influence after the data of mine seismological catalogue.// Mine informational and analytical bulletin MSMU,6, 2010,p.259-271.

  2. Error correction for Moir based creep measurement system

    NASA Astrophysics Data System (ADS)

    Liao, Yi; Harding, Kevin G.; Nieters, Edward J.; Tait, Robert W.; Hasz, Wayne C.; Piche, Nicole

    2014-05-01

    Due to the high temperatures and stresses present in the high-pressure section of a gas turbine, the airfoils experience creep or radial stretching. Nowadays manufacturers are putting in place condition-based maintenance programs in which the condition of individual components is assessed to determine their remaining lives. To accurately track this creep effect and predict the impact on part life, the ability to accurately assess creep has become an important engineering challenge. One approach for measuring creep is using moir imaging. Using pad-print technology, a grating pattern can be directly printed on a turbine bucket, and it compares against a reference pattern built in the creep measurement system to create moir interference pattern. The authors assembled a creep measurement prototype for this application. By measuring the frequency change of the moir fringes, it is then possible to determine the local creep distribution. However, since the sensitivity requirement for the creep measurement is very stringent (0.1 micron), the measurement result can be easily offset due to optical system aberrations, tilts and magnification. In this paper, a mechanical specimen subjected to a tensile test to induce plastic deformation up to 4% in the gage was used to evaluate the system. The results show some offset compared to the readings from a strain gage and an extensometer. By using a new grating pattern with two subset patterns, it was possible to correct these offset errors.

  3. Buckling Analysis in Creep Conditions: Review and Comparison

    SciTech Connect

    Turbat, Andre; Drubay, Bernard

    2002-07-01

    In the case of structures operating at high temperature in normal or accidental conditions, the influence of creep has to be considered at the design stage because this phenomenon may reduce the lifetime significantly. This is true in particular for buckling analysis: in creep conditions, the buckling sometimes occurs after a long period under a compressive load which is lower than the critical load assessed when considering an instantaneous buckling. The main reason is that creep deformations induce an amplification of the initial geometrical imperfections and consequently a reduction of the buckling load. Some Design Codes incorporate special rules and/or methods to take creep buckling into account. Creep buckling analysis methods aim at evaluating critical loading for a given hold period with creep or alternatively critical creep time for a given loading. The Codes where creep buckling is considered also define margins with respect to critical loading: it shall be demonstrated that creep instability will not occur during the whole lifetime when multiplying the specified loading by a coefficient (design factor) depending on the situation level. For the design of NPP, specific creep buckling rules exist in the US, France and Russia. In the US, ASME, Section III, Subsection NH, which is dedicated to high temperature components design, provides limits which are applicable to general geometrical configurations and loading conditions that may cause buckling due to creep behaviour of the material. For load-controlled time-dependent creep buckling, the design factors to apply to the specified loadings are 1.5 for levels A, B or C service loadings and 1.25 for level D service loadings. A design factor is not required in the case of purely strain-controlled buckling. No specific method is provided to obtain critical loading or critical time for creep instability. In France, creep buckling rules included in RCC-MR, Chapter RB or RC 3200 are similar to those of ASME, Subsection NH. In addition, a new simplified method has been developed recently to assess critical creep loading/time for a shell under mechanical loading. Diagrams, presently valid for 316 austenitic steel, have been established from a ring model with perfect plasticity. Creep buckling load is determined applying a reduction factor to Euler instantaneous buckling load, depending on temperature, hold time, thinness of the structure and geometrical imperfection amplitude. This method has been validated by experimental tests and finite element results. It will be included in Appendix A7 of RCC-MR, Edition 2000. In Russia, the document PNAE G-7-002-86 applicable to NPP equipment and pipeline strength analysis, presents stability check analytical calculations to be performed to determine the allowable loading or allowable operation lifetime for typical geometries (cylindrical shells, dished ends) and loadings (external pressure, axial force). In the case of stability analysis under creep, creep deformation is assessed using a Norton law. In Germany, a KTA project including an analytical method for creep buckling analysis had also been proposed at the beginning of 90's to be used in HTR development. Finally, in India, a creep buckling analysis method has been proposed in the framework of PFBR project. As per this approach, elastic-plastic analysis should be performed replacing the instantaneous stress-strain curve at the design temperature by the isochronous curve for the time corresponding to the lifetime of the component and the same temperature. These methods are applied in the case of cylindrical shells under external pressure and comparative results are provided. The RCC-MR method appears to be reasonably conservative and applicable with several creep law types. (authors)

  4. On creep mechanisms in amalgams.

    PubMed

    Her, H

    1983-01-01

    Creep mechanisms have been investigated in both conventional and non-gamma 2 amalgams. The back stress during steady-state creep was measured by the "stress-dip" technique, and pre-polished vertical surfaces of nearly cylindrical specimens were studied after creep. Indications of both superplastic flow and dislocation creep were observed. PMID:6571853

  5. New constraints on upper mantle creep mechanism inferred from silicon grain-boundary diffusion rates

    NASA Astrophysics Data System (ADS)

    Fei, Hongzhan; Koizumi, Sanae; Sakamoto, Naoya; Hashiguchi, Minako; Yurimoto, Hisayoshi; Marquardt, Katharina; Miyajima, Nobuyoshi; Yamazaki, Daisuke; Katsura, Tomoo

    2016-01-01

    The creep in the Earth's interior is dominated either by diffusion creep which causes Newtonian mantle flow, or by dislocation creep which results in non-Newtonian mantle flow. Although previous deformation studies on olivine claimed a transition from dislocation creep to diffusion creep with depth in the upper mantle, they might misunderstand the creep rates due to experimental difficulties. Since creep in olivine is controlled by silicon diffusion, we measured the silicon grain-boundary diffusion coefficient in well-sintered iron-free olivine aggregates as a function of temperature, pressure, and water content, showing activation energy, activation volume, and water content exponent of 220 30 kJ /mol, 4.0 0.7 cm3 /mol, and 0.26 0.07, respectively. Our results based on Si diffusion in forsterite predict that diffusion creep dominates at low pressures and low temperatures, whereas dislocation creep dominates under high pressure and high temperature conditions. Water has negligible effects on both diffusion and dislocation creep. There is a transition from diffusion creep in the shallow upper mantle to dislocation creep in deeper regions. This explains the seismic anisotropy increases at the Gutenberg discontinuity beneath oceans and at the mid-lithosphere discontinuity beneath continents.

  6. Threshold Stress Creep Behavior of Alloy 617 at Intermediate Temperatures

    SciTech Connect

    J.K. Benz; L.J. Carroll; J.K. Wright; R.N. Wright; T. Lillo

    2014-06-01

    Creep of Alloy 617, a solid solution Ni-Cr-Mo alloy, was studied in the temperature range of 1023 K to 1273 K (750 °C to 1000 °C). Typical power-law creep behavior with a stress exponent of approximately 5 is observed at temperatures from 1073 K to 1273 K (800 °C to 1000 °C). Creep at 1023 K (750 °C), however, exhibits threshold stress behavior coinciding with the temperature at which a low volume fraction of ordered coherent y' precipitates forms. The threshold stress is determined experimentally to be around 70 MPa at 1023 K (750 °C) and is verified to be near zero at 1173 K (900 °C)—temperatures directly correlating to the formation and dissolution of y' precipitates, respectively. The y' precipitates provide an obstacle to continued dislocation motion and result in the presence of a threshold stress. TEM analysis of specimens crept at 1023 K (750 °C) to various strains, and modeling of stresses necessary for y' precipitate dislocation bypass, suggests that the climb of dislocations around the y' precipitates is the controlling factor for continued deformation at the end of primary creep and into the tertiary creep regime. As creep deformation proceeds at an applied stress of 121 MPa and the precipitates coarsen, the stress required for Orowan bowing is reached and this mechanism becomes active. At the minimum creep rate at an applied stress of 145 MPa, the finer precipitate size results in higher Orowan bowing stresses and the creep deformation is dominated by the climb of dislocations around the y' precipitates.

  7. Thiel-fixation preserves the non-linear load-deformation characteristic of spinal motion segments, but increases their flexibility.

    PubMed

    Wilke, Hans-Joachim; Werner, Karin; Hussler, Kim; Reinehr, Michael; Bckers, Tobias M

    2011-11-01

    Human cadaveric specimens are recommended as the best option for in-vitro tests. However, fresh human spine specimens are often difficult to obtain. Further problems are the potential risk of infection and they can only be used over a limited test period. Therefore, the use of embalmed specimens is often discussed. The most common method is formalin fixation. However, this type of embalming can result in failure, because the biomechanical properties of the tissue is partially influenced. In recent years the development of the new method, the fixation according to Thiel, could provide an alternative to fresh or formalin-fixed specimens. The aim of the present study is to compare the biomechanical properties between fresh and Thiel-fixed spine specimens, and to compare the data to previous data of a test with formalin fixation. For the study, six L1-L2 spinal segments from 16-week-old calves were biomechanically tested. The parameters, range of motion and neutral zone, were determined in flexion/extension, right/left lateral bending and left/right axial rotation. The results showed that the specimens kept their non-linear load-deformation-characteristic after Thiel fixation. The range of motion of Thiel-fixed specimens increased relative to the unembalmed state by approximately 22% in flexion-extension, 23% in lateral bending (p<0.05) and 45% in axial rotation (p<0.05). In conclusion, the results still suggest a preference for fresh cadaveric spine specimens for quantitative biomechanical in-vitro testing, because they provide the best physiological conditions. However, for preliminary tests, which may only be used for orientation, embalmed specimens using the Thiel fixation method might serve as an alternative. Compared to formalin-fixated specimens which become approximately 5 times stiffer and completely lose their non-linear load-deformation-characteristic, as found in a previous study; the Thiel fixation maintains the non-linear load-deformation-characteristic but increases the range of motion. PMID:22098913

  8. Irradiation Induced Creep of Graphite

    SciTech Connect

    Burchell, Timothy D; Murty, Prof K.L.; Eapen, Dr. Jacob

    2010-01-01

    The current status of graphite irradiation induced creep strain prediction is reviewed and the major creep models are described. The ability of the models to quantitatively predict the irradiation induced creep strain of graphite is reported. Potential mechanisms of in-crystal creep are reviewed as are mechanisms of pore generation under stress. The case for further experimental work is made and the need for improved creep models across multi-scales is highlighted.

  9. Diffusion creep in the mantle may create and maintain anisotropy

    NASA Astrophysics Data System (ADS)

    Wheeler, John

    2014-05-01

    Diffusion creep is thought to play an important role in lower mantle deformation and hence must be understood in detail if Earth behaviour is to be explained. It is commonly claimed that diffusion creep gives rise to equant grain shapes and destroys any crystallographic preferred orientation (CPO), so all physical properties would be isotropic. Some experiments on olivine support the first assertion but other minerals, and polyphase rocks, commonly show inequant grain shapes in nature and experiment even when diffusion creep is thought to be a major contribution to strain. Numerical models allow rigorous exploration of the effects of deformation under conditions not easily reached in experiments. A numerical model named 'DiffForm' (Wheeler & Ford 2007) gives insight into how grain shapes and microstructures evolve during diffusion creep. Modelling shows that whilst grains may initially rotate in apparently chaotic fashion during diffusion creep, such rotations slow down as grains become inequant. Consequently, an initial CPO (formed, for example, by dislocation creep at higher strain rates) will be decreased in intensity but not destroyed. Seismic anisotropy will decrease but not disappear (Wheeler 2009). Diffusion creep is also predicted to have intense mechanical anisotropy. In simple models diffusion creep is controlled entirely by diffusion and sliding along grain boundaries; there is no crystallographic influence. An aggregate of equant grains must then be mechanically isotropic, but a model microstructure with inequant grains has marked mechanical anisotropy (Wheeler 2010) - an effect related to the fact that grain boundary sliding is an intrinsic part of diffusion creep. That work was based on a very simple microstructure with a single inequant grain shape but I present here new results showing that for more complicated microstructures, mechanical anisotropy is intense even for quite modest grain elongations. There will be feedback between strain and rheology which may control overall mantle strength. This theoretical development and some recent experiments indicate that diffusion creep is quite a different process to what was envisaged 10 years ago. This means that its relationship to seismic and mechanical anisotropy in the Earth requires reappraisal. .Wheeler, J. 2009. The preservation of seismic anisotropy in the Earth's mantle during diffusion creep. Geophysical Journal International 178, 1723-1732. Wheeler, J. 2010. Anisotropic rheology during grain boundary diffusion creep and its relation to grain rotation, grain boundary sliding and superplasticity. Philosophical Magazine 90, 2841-2864. Wheeler, J. & Ford, J. M. 2007. Diffusion Creep. In: Microdynamic simulation - From microprocess to patterns in rocks (edited by Bons, P. D., Jessell, M. & Koehn, D.). Lecture Notes in Earth Science. Springer, Berlin / Heidelberg, 161-169.

  10. Bend stress relaxation and tensile primary creep of a polycrystalline alpha-SiC fiber

    NASA Technical Reports Server (NTRS)

    Hee Man, Yun; Goldsby, Jon C.; Morscher, Gregory N.

    1995-01-01

    Understanding the thermomechanical behavior (creep and stress relaxation) of ceramic fibers is of both practical and basic interest. On the practical level, ceramic fibers are the reinforcement for ceramic matrix composites which are being developed for use in high temperature applications. It is important to understand and model the total creep of fibers at low strain levels where creep is predominantly in the primary stage. In addition, there are many applications where the component will only be subjected to thermal strains. Therefore, the stress relaxation of composite consituents in such circumstances will be an important factor in composite design and performance. The objective of this paper is to compare and analyze bend stress relaxation and tensile creep data for alpha-SiC fibers produced by the Carborundum Co. (Niagara Falls, NY). This fiber is of current technical interest and is similar in composition to bulk alpha-SiC which has been studied under compressive creep conditions. The temperature, time, and stress dependences will be discussed for the stress relaxation and creep results. In addition, some creep and relaxation recovery experiments were performed in order to understand the complete viscoelastic behavior, i.e. both recoverable and nonrecoverable creep components of these materials. The data will be presented in order to model the deformation behavior and compare relaxation and/or creep behavior for relatively low deformation strain conditions of practical concern. Where applicable, the tensile creep results will be compared to bend stress relaxation data.

  11. Modeling the Role of Dislocation Substructure During Class M and Exponential Creep. Revised

    NASA Technical Reports Server (NTRS)

    Raj, S. V.; Iskovitz, Ilana Seiden; Freed, A. D.

    1995-01-01

    The different substructures that form in the power-law and exponential creep regimes for single phase crystalline materials under various conditions of stress, temperature and strain are reviewed. The microstructure is correlated both qualitatively and quantitatively with power-law and exponential creep as well as with steady state and non-steady state deformation behavior. These observations suggest that creep is influenced by a complex interaction between several elements of the microstructure, such as dislocations, cells and subgrains. The stability of the creep substructure is examined in both of these creep regimes during stress and temperature change experiments. These observations are rationalized on the basis of a phenomenological model, where normal primary creep is interpreted as a series of constant structure exponential creep rate-stress relationships. The implications of this viewpoint on the magnitude of the stress exponent and steady state behavior are discussed. A theory is developed to predict the macroscopic creep behavior of a single phase material using quantitative microstructural data. In this technique the thermally activated deformation mechanisms proposed by dislocation physics are interlinked with a previously developed multiphase, three-dimensional. dislocation substructure creep model. This procedure leads to several coupled differential equations interrelating macroscopic creep plasticity with microstructural evolution.

  12. An Evaluation of the Potential for Creep of 3013 Inner Can Lids

    SciTech Connect

    KERRY, DUNN

    2005-03-15

    This report provides the technical basis to conclude that creep induced deformation of Type 304L austenitic stainless steel can lids on inner 3013 containers will be insignificant unless the temperature of storage exceeds 400 C. This conclusion is based on experimental literature data for Types 304 and 316 stainless steel and on a phenomenological evaluation of potential creep processes.

  13. Biaxial Creep Specimen Fabrication

    SciTech Connect

    JL Bump; RF Luther

    2006-02-09

    This report documents the results of the weld development and abbreviated weld qualification efforts performed by Pacific Northwest National Laboratory (PNNL) for refractory metal and superalloy biaxial creep specimens. Biaxial creep specimens were to be assembled, electron beam welded, laser-seal welded, and pressurized at PNNL for both in-pile (JOYO reactor, O-arai, Japan) and out-of-pile creep testing. The objective of this test campaign was to evaluate the creep behavior of primary cladding and structural alloys under consideration for the Prometheus space reactor. PNNL successfully developed electron beam weld parameters for six of these materials prior to the termination of the Naval Reactors program effort to deliver a space reactor for Project Prometheus. These materials were FS-85, ASTAR-811C, T-111, Alloy 617, Haynes 230, and Nirnonic PE16. Early termination of the NR space program precluded the development of laser welding parameters for post-pressurization seal weldments.

  14. Irradiation Creep in Graphite

    SciTech Connect

    Ubic, Rick; Butt, Darryl; Windes, William

    2014-03-13

    An understanding of the underlying mechanisms of irradiation creep in graphite material is required to correctly interpret experimental data, explain micromechanical modeling results, and predict whole-core behavior. This project will focus on experimental microscopic data to demonstrate the mechanism of irradiation creep. High-resolution transmission electron microscopy should be able to image both the dislocations in graphite and the irradiation-induced interstitial clusters that pin those dislocations. The team will first prepare and characterize nanoscale samples of virgin nuclear graphite in a transmission electron microscope. Additional samples will be irradiated to varying degrees at the Advanced Test Reactor (ATR) facility and similarly characterized. Researchers will record microstructures and crystal defects and suggest a mechanism for irradiation creep based on the results. In addition, the purchase of a tensile holder for a transmission electron microscope will allow, for the first time, in situ observation of creep behavior on the microstructure and crystallographic defects.

  15. Analysis of Multistage and Other Creep Data for Domal Salts

    SciTech Connect

    Munson, D.E.

    1998-10-01

    There have existed for some time relatively sparse creep databases for a number of domal salts. Although all of these data were analyzed at the time they were reported, to date there has not been a comprehensive, overall evaluation within the same analysis framework. Such an evaluation may prove of value. The analysis methodology is based on the Multimechanism Deformation (M-D) description of salt creep and the corresponding model parameters determined from conventional creep tests. The constitutive model of creep wss formulated through application of principles involved in micromechanical modeling. It was possible, at minimum, to obtain the steady state parameters of the creep model from the data on the domal salts. When this was done, the creep of the domal salts, as compared to the well-defined Waste Isolation Pilot Plant (WIPP) bedded clean salt, was either essentially identical to, or significantly harder (more creep resistant) than WIPP salt. Interestingly, the domal salts form two distinct groups, either sofl or hard, where the difference is roughly a factor often in creep rate between the twcl groups. As might be expected, this classification corresponds quite well to the differences in magnitude of effective creep volume losses of the Strategic Petroleum Reserve (SPR) caverns as determined by the CAVEMAN cavern pressure history analysis, depending upon the specific dome or region within the dome. Creep response shoulcl also correlate to interior cavern conditions that produce salt falls. WMle, in general, the caverns in hard sah have a noticeably greater propensity for salt falls, a smaller number of similar events are exhibited even in the caverns in soft salt.

  16. Bond characteristics of steel fiber and deformed reinforcing steel bar embedded in steel fiber reinforced self-compacting concrete (SFRSCC)

    NASA Astrophysics Data System (ADS)

    Aslani, Farhad; Nejadi, Shami

    2012-09-01

    Steel fiber reinforced self-compacting concrete (SFRSCC) is a relatively new composite material which congregates the benefits of the self-compacting concrete (SCC) technology with the profits derived from the fiber addition to a brittle cementitious matrix. Steel fibers improve many of the properties of SCC elements including tensile strength, ductility, toughness, energy absorption capacity, fracture toughness and cracking. Although the available research regarding the influence of steel fibers on the properties of SFRSCC is limited, this paper investigates the bond characteristics between steel fiber and SCC firstly. Based on the available experimental results, the current analytical steel fiber pullout model (Dubey 1999) is modified by considering the different SCC properties and different fiber types (smooth, hooked) and inclination. In order to take into account the effect of fiber inclination in the pullout model, apparent shear strengths (? (app)) and slip coefficient (?) are incorporated to express the variation of pullout peak load and the augmentation of peak slip as the inclined angle increases. These variables are expressed as functions of the inclined angle (?). Furthurmore, steel-concrete composite floors, reinforced concrete floors supported by columns or walls and floors on an elastic foundations belong to the category of structural elements in which the conventional steel reinforcement can be partially replaced by the use of steel fibers. When discussing deformation capacity of structural elements or civil engineering structures manufactured using SFRSCC, one must be able to describe thoroughly both the behavior of the concrete matrix reinforced with steel fibers and the interaction between this composite matrix and discrete steel reinforcement of the conventional type. However, even though the knowledge on bond behavior is essential for evaluating the overall behavior of structural components containing reinforcement and steel fibers, information is hardly available in this area. In this study, bond characteristics of deformed reinforcing steel bars embedded in SFRSCC is investigated secondly.

  17. Bond characteristics of steel fiber and deformed reinforcing steel bar embedded in steel fiber reinforced self-compacting concrete (SFRSCC)

    NASA Astrophysics Data System (ADS)

    Aslani, Farhad; Nejadi, Shami

    2012-09-01

    Steel fiber reinforced self-compacting concrete (SFRSCC) is a relatively new composite material which congregates the benefits of the self-compacting concrete (SCC) technology with the profits derived from the fiber addition to a brittle cementitious matrix. Steel fibers improve many of the properties of SCC elements including tensile strength, ductility, toughness, energy absorption capacity, fracture toughness and cracking. Although the available research regarding the influence of steel fibers on the properties of SFRSCC is limited, this paper investigates the bond characteristics between steel fiber and SCC firstly. Based on the available experimental results, the current analytical steel fiber pullout model (Dubey 1999) is modified by considering the different SCC properties and different fiber types (smooth, hooked) and inclination. In order to take into account the effect of fiber inclination in the pullout model, apparent shear strengths ( ? ( app)) and slip coefficient ( ?) are incorporated to express the variation of pullout peak load and the augmentation of peak slip as the inclined angle increases. These variables are expressed as functions of the inclined angle ( ?). Furthurmore, steel-concrete composite floors, reinforced concrete floors supported by columns or walls and floors on an elastic foundations belong to the category of structural elements in which the conventional steel reinforcement can be partially replaced by the use of steel fibers. When discussing deformation capacity of structural elements or civil engineering structures manufactured using SFRSCC, one must be able to describe thoroughly both the behavior of the concrete matrix reinforced with steel fibers and the interaction between this composite matrix and discrete steel reinforcement of the conventional type. However, even though the knowledge on bond behavior is essential for evaluating the overall behavior of structural components containing reinforcement and steel fibers, information is hardly available in this area. In this study, bond characteristics of deformed reinforcing steel bars embedded in SFRSCC is investigated secondly.

  18. Creep Resistant Zinc Alloy

    SciTech Connect

    Frank E. Goodwin

    2002-12-31

    This report covers the development of Hot Chamber Die Castable Zinc Alloys with High Creep Strengths. This project commenced in 2000, with the primary objective of developing a hot chamber zinc die-casting alloy, capable of satisfactory service at 140 C. The core objectives of the development program were to: (1) fill in missing alloy data areas and develop a more complete empirical model of the influence of alloy composition on creep strength and other selected properties, and (2) based on the results from this model, examine promising alloy composition areas, for further development and for meeting the property combination targets, with the view to designing an optimized alloy composition. The target properties identified by ILZRO for an improved creep resistant zinc die-casting alloy were identified as follows: (1) temperature capability of 1470 C; (2) creep stress of 31 MPa (4500 psi); (3) exposure time of 1000 hours; and (4) maximum creep elongation under these conditions of 1%. The project was broadly divided into three tasks: (1) Task 1--General and Modeling, covering Experimental design of a first batch of alloys, alloy preparation and characterization. (2) Task 2--Refinement and Optimization, covering Experimental design of a second batch of alloys. (3) Task 3--Creep Testing and Technology transfer, covering the finalization of testing and the transfer of technology to the Zinc industry should have at least one improved alloy result from this work.

  19. Transient creep and semibrittle behavior of crystalline rocks

    USGS Publications Warehouse

    Carter, N.L.; Kirby, S.H.

    1978-01-01

    We review transient creep and semibrittle behavior of crystalline solids. The results are expected to be pertinent to crystalline rocks undergoing deformation in the depth range 5 to 20 km, corresponding to depths of focus of many major earthquakes. Transient creep data for crystalline rocks at elevated temperatures are analyzed but are poorly understood because of lack of information on the deformation processes which, at low to moderate pressure, are likely to be semibrittle in nature. Activation energies for transient creep at high effective confining pressure are much higher than those found for atmospheric pressure tests in which thermally-activated microfracturing probably dominates the creep rate. Empirical transient creep equations are extrapolated at 200?? to 600??C, stresses from 0.1 to 1.0 kbar, to times ranging from 3.17??102 to 3.17??108 years. At the higher temperatures, appreciable transient creep strains may take place but the physical significance of the results is in question because the flow mechanisms have not been determined. The purpose of this paper is to stimulate careful research on this important topic. ?? 1978 Birkha??user Verlag.

  20. A model of compaction creep in carbonates

    NASA Astrophysics Data System (ADS)

    Keszthelyi, Daniel; Jamtveit, Bjørn; Dysthe, Dag Kristian

    2015-04-01

    Rocks in compressional stress conditions are subject to long-term creep deformations. We created a simple conceptual micomechanical model of creep in rocks combining microscopic fracturing and pressure solution. This was then scaled up to macroscopic scale by a statistical mechanical approach to predict strain rate at core scale. The model uses no fitting parameter and have a few input parameters: effective stress, porosity, pore size distribution, temperature and water saturation. Internal parameters are Young's modulus, interfacial energy of wet calcite and dissolution rates of calcite, all of which are measurable independently. Existing long-term creep experiments were used to verify the model which was able to predict the magnitude of the resulting strain in largely different effective stress, temperature and water saturation conditions. The model was also able to predict the compaction of a producing chalk reservoir with a good agreement. Further generalization of the model might function as a general theory of long-term creep of rocks in compressional settings.

  1. A unified creep-plasticity model suitable for thermo-mechanical loading

    NASA Technical Reports Server (NTRS)

    Slavik, D.; Sehitoglu, H.

    1988-01-01

    An experimentally based unified creep-plasticity constitutive model was implemented for 1070 steel. Accurate rate and temperature effects were obtained for isothermal and thermo-mechanical loading by incorporating deformation mechanisms into the constitutive equations in a simple way.

  2. Time-dependent deformations on marine clays on submarine slopes

    SciTech Connect

    Silva, A.J.; Brandes, H.; Sadd, M.H.; Tian, W.M. )

    1990-06-01

    Evidence from geological and geophysical records indicates that time-dependent deformations occur on or within many submarine slopes. Laboratory studies on marine clays from the slope/rise and the ocean's basin have shown that these clays are generally quite viscous and therefore can be expected to deform in the field even under such small stresses as those caused by the downslope component of gravity on relatively gentle slopes. The nature and extent of these deformations has important geologic and engineering applications and depends on a number of factors. A research program at the University of Rhode Island is under way to study these factors, make predictions on rates of displacement, and identify environmental conditions that may lead to catastrophic mass failures. A laboratory testing program on the time-dependent characteristics of marine clays has been under way for a number of years. The data include, among others, long-term drained triaxial, one-dimensional, and direct simple shear creep tests. These results along with practical considerations are used to select a constitutive model for inclusion in the numerical code. Sediment deposits encountered on the continental slope and rise can vary substantially both in composition and behavior over relatively short distances. To analyze the integrated behavior of such a continuum, the authors have selected the finite element method. The code being developed will initially include a numerical model proposed by other investigators. With the aid of the developed methodology, creep deformations can be studied for a number of field cases of interest.

  3. A method of tuning viscoelastic creep in charge-controlled dielectric elastomer actuation

    NASA Astrophysics Data System (ADS)

    Zhang, Junshi; Chen, Hualing; Li, Bo

    2014-12-01

    Deformation in charge-controlled dielectric elastomer actuation eliminates pull-in instability, but the performance is affected by dissipative characteristics, such as viscoelasticity and leakage current. This letter focuses on the modeling of the dissipative performance in charge-controlled dielectric elastomer actuation. The effects of the initial surface charge and the ratios between viscoelastic relaxation time and resistor-capacitor time constant are investigated. By spraying charge to compensate the leakage and adjusting the surface charge, the viscoelastic relaxation is dispelled and the invariable deformation is tuned. The rate of spraying charge to suppress viscoelastic creep is determined by the difference between the value of the leakage current and the rate of the change of the surface charge.

  4. Elevated temperature creep-rupture behavior of the single crystal nickel-base superalloy NASAIR 100

    NASA Astrophysics Data System (ADS)

    Nathal, M. V.; Ebert, L. J.

    1985-03-01

    The creep and rupture behavior of [001] oriented single crystals of the nickel-base superalloy NASAIR 100 was investigated at temperatures of 925 and 1000 °C. In the stress and temperature ranges studied, the steady state creep rate, time to failure, time to the onset of secondary creep, and the time to the onset of tertiary creep all exhibited power law dependencies on the applied stress. The creep rate exponents for this alloy were between seven and eight, and the modulus-corrected activation energy for creep was approximately 350 kjoule/mole, which was comparable to the measured activa-tion energy for Ostwald ripening of the γ' precipitates. Oriented γ' coarsening to form lamellae perpendicular to the applied stress was very prominent during creep. At 1000 °C, the formation of a continuous γ-γ' lamellar structure was completed during the primary creep stage. Shear through the γ-γ ' interface is considered to be the rate limiting step in the deformation process. Gradual thickening of the lamellae appeared to be the cause of the onset of tertiary creep. At 925 °C, the fully developed lamellar structure was not achieved until the secondary or tertiary creep stages. At this temperature, the γ-γ' lamellar structure did not appear to be as beneficial for creep resistance as at the higher temperature.

  5. Elevated temperature creep-rupture behavior of the single crystal nickel-base superalloy NASAIR 100

    NASA Technical Reports Server (NTRS)

    Nathal, M. V.; Ebert, L. J.

    1985-01-01

    The creep and rupture behavior of 001-line-oriented single crystals of the nickel-base superalloy NASAIR 100 was investigated at temperatures of 925 and 1000 C. In the stress and temperature ranges studied, the steady state creep rate, time to failure, time to the onset of secondary creep, and the time to the onset of tertiary creep all exhibited power law dependencies on the applied stress. The creep rate exponents for this alloy were between seven and eight, and the modulus-corrected activation energy for creep was approximately 350 kjoule/mole, which was comparable to the measured activation energy for Ostwald ripening of the gamma-prime precipitates. Oriented gamma-prime coarsening to form lamellae perpendicular to the applied stress was very prominent during creep. At 1000 C, the formation of a continuous gamma-gamma-prime lamellar structure was completed during the primary creep stage. Shear through the gamma-gamma-prime interface is considerd to be the rate limiting step in the deformation process. Gradual thickening of the lamellae appeared to be the cause of the onset of tertiary creep. At 925 C, the fully developed lamellar structure was not achieved until the secondary or tertiary creep stages. At this temperature, the gamma-gamma-prime lamellar structure did not appear to be as beneficial for creep resistance as at the higher temperature.

  6. Creep properties of catalyst coated membranes for polymer electrolyte fuel cells

    NASA Astrophysics Data System (ADS)

    Sadeghi Alavijeh, Alireza; Khorasany, Ramin M. H.; Habisch, Aronne; Wang, G. Gary; Kjeang, Erik

    2015-07-01

    Creep as a time-dependent mechanical damage acting either independently or in conjunction with other degradation mechanisms is known to reduce the membrane durability of polymer electrolyte fuel cells (PEFCs). Due to the important ionomer coupling of membrane and catalyst layers in PEFCs, the present work evaluates membrane creep when constrained within a catalyst coated membrane (CCM). Three key factors dominating creep life in commonly used perfluorosulfonic acid (PFSA) ionomer membranes, including creep stress, temperature, and relative humidity, were investigated by applying ex-situ creep loading and unloading experiments under controlled temperature and humidity conditions. The creep strain and recovery of the CCM were found to be highly dependent on the environmental conditions and applied stress levels, where the temperature effect on creep strain was the most significant. Repetitive creep - recovery cycles revealed that significant creep damage can accumulate in the material over time. This accumulated creep damage was found to be independent of the loading frequency while both peak strain and permanent deformation increased with the stress duration. Based on the present findings, it is recommended to reduce the operating temperature and ensure adequate membrane hydration in order to mitigate harmful creep effects in PEFCs.

  7. Creep behavior of 6 micrometer linear low density polyethylene film

    NASA Technical Reports Server (NTRS)

    Simpson, J. M.; Schur, W. W.

    1993-01-01

    Creep tests were performed to provide material characteristics for a 6.4-micron polyethylene film used to construct high altitude balloons. Results suggest simple power law relationships are adequate for stresses below about 4.83 MPa.

  8. Sources of Variation in Creep Testing

    NASA Technical Reports Server (NTRS)

    Loewenthal, William S.; Ellis, David L.

    2011-01-01

    Creep rupture is an important material characteristic for the design of rocket engines. It was observed during the characterization of GRCop-84 that the complete data set had nearly 4 orders of magnitude of scatter. This scatter likely confounded attempts to determine how creep performance was influenced by manufacturing. It was unclear if this variation was from the testing, the material, or both. Sources of variation were examined by conducting tests on identically processed specimens at the same specified stresses and temperatures. Significant differences existed between the five constant-load creep frames. The specimen temperature was higher than the desired temperature by as much as 43 C. It was also observed that the temperature gradient was up to 44 C. Improved specimen temperature control minimized temperature variations. The data from additional tests demonstrated that the results from all five frames were comparable. The variation decreased to 1/2 order of magnitude from 2 orders of magnitude for the baseline data set. Independent determination of creep rates in a reference load frame closely matched the creep rates determined after the modifications. Testing in helium tended to decrease the sample temperature gradient, but helium was not a significant improvement over vacuum.

  9. Superplastic Deformation of ice: Experimental Observations

    NASA Technical Reports Server (NTRS)

    Goldsby, D. L.; Kohlstedt, D. L.

    2001-01-01

    Creep experiments on fine-grained ice reveal the existence of three creep regimes: (1) a dislocation creep regime; (2) a superplastic flow regime in which grain boundary sliding is an important deformation process; and (3) a basal slip creep regime in which the strain rate is limited by basal slip. Dislocation creep in ice is likely climb-limited, is characterized by a stress exponent of 4.0, and is independent of grain size. Superplastic flow is characterized by a stress exponent of 1.8 and depends inversely on grain size to the 1.4 power. Basal slip limited creep is characterized by a stress exponent of 2.4 and is independent of grain size. A fourth creep mechanism, diffusional flow, which usually occurs at very low stresses, is inaccessible at practical laboratory strain rates even for our finest grain sizes of approximately 3 micrometers. A constitutive equation based on these experimental results that includes flow laws for these four creep mechanisms is described. This equation is in excellent agreement with published laboratory creep data for coarse-grained samples at high temperatures. Superplastic flow of ice is the rate-limiting creep mechanism over a wide range of temperatures and grain sizes at stresses less than or equal to 0.1 MPa, conditions which overlap those occurring in glaciers, ice sheets, and icy planetary interiors.

  10. Damage and permiability evolution in creep-failed microgranite

    NASA Astrophysics Data System (ADS)

    Odling, N.; Elphick, S.; Main, I.; Meredith, P.; Ngwenya, B.

    2003-04-01

    The importance of crack generation during deformation is now becoming widely recognized as one of the key factors that control important processes involving fluid flow in rocks of low permeability e.g., hydro-thermal circulation at mid-ocean ridges, energy recovery from geothermal reservoirs, and accelerating deformation preceding volcanic eruptions. Here we describe experiments that extend the study of Meredith et al. (2000) by examining the relationship between slow deformation, the growth of micro-fractures, and permeability in Ailsa Craig microgranite (ACM) close to the fracture interconnection percolation threshold. To examine the inter-relationship between the above factors we have undertaken creep experiments on cores of ACM during which we have measured acoustic emissions, solute breakthrough curves, and electrical impedance (EI), at a strain rate of 10e(-6). The initial network of distributed damage was generated in a 38mm-diameter core of ACM by heating at 1C/hr to 900C then cooling to room temperature at the same rate. The treated core was then placed in a Hasler cell with integral acoustic emission and electrical impedance sensors and initially loaded to 20MPa. To measure breakthrough curves, solutions of deionized/distilled/degassed water was alternated with a degassed 1M NaCl solution at a flow rate of 1cc/hr. Differential fluid pressures were monitored by piezoelectric pressure gauges and the strain in the sample was monitored by LVDTs attached to the pistons. Initial 'breakthrough' tests under hydrostatic conditions show that the EI response detects first a linear change in impedance as the solute front advances through the core followed by a more gradual decrease as the front breaks out of the core end. The EI response, therefore, describes both the advection and dispersion terms associated with the solute front in the core. The data allow the inter-relationship between crack generation/growth, effective cumulative aperture, permeability and hydraulic dispersion to be examined during the process of creep deformation. Of particular interest is the behaviour of the system close to failure, where rapid changes in fracture network characteristics occur.

  11. Deformation Failure Characteristics of Coal Body and Mining Induced Stress Evolution Law

    PubMed Central

    Wen, Zhijie; Wen, Jinhao; Shi, Yongkui; Jia, Chuanyang

    2014-01-01

    The results of the interaction between coal failure and mining pressure field evolution during mining are presented. Not only the mechanical model of stope and its relative structure division, but also the failure and behavior characteristic of coal body under different mining stages are built and demonstrated. Namely, the breaking arch and stress arch which influence the mining area are quantified calculated. A systematic method of stress field distribution is worked out. All this indicates that the pore distribution of coal body with different compressed volume has fractal character; it appears to be the linear relationship between propagation range of internal stress field and compressed volume of coal body and nonlinear relationship between the range of outburst coal mass and the number of pores which is influenced by mining pressure. The results provide theory reference for the research on the range of mining-induced stress and broken coal wall. PMID:24967438

  12. Nano-mesoscopic structural characterization of 9Cr-ODS martensitic steel for improving creep strength

    NASA Astrophysics Data System (ADS)

    Ohtsuka, S.; Ukai, S.; Sakasegawa, H.; Fujiwara, M.; Kaito, T.; Narita, T.

    2007-08-01

    This paper describes the effect on creep strength and microstructure of 9Cr-oxide dispersion strengthened martensitic steel (9Cr-ODS steel) produced by differences in titanium concentration and consolidation temperature. The increase of titanium concentration to 0.30-0.35 wt% was shown to provide considerable improvement of creep strength accompanied by the increase of residual-? ferrite. The elevation of hot-extrusion temperature degraded the creep strength, however, it appeared to increase the volume fraction of residual-? ferrite. The creep deformation process of 9Cr-ODS steel was discussed to explain these results based on microstructure observations.

  13. A creep apparatus to explore the quenching and ageing phenomena of PVC films

    NASA Technical Reports Server (NTRS)

    Lee, H. H. D.; Mcgarry, F. J.

    1991-01-01

    A creep apparatus has been constructed for an in situ determination of length and length change. Using this apparatus, the creep behavior of PVC thin films associated with quenching and aging was studied. The more severe the quench through the glass transition temperature, the greater is the instantaneous elastic deformation and the subsequent creep behavior. As aging proceeds, the quenched films gradually lose the ductility incurred by quenching. These results agree well with the well-known phenomena of physical aging. Thus, the changes reflecting molecular mobilities due to quenching and aging can be properly monitored by such a creep apparatus.

  14. A constitutive model for representing coupled creep, fracture, and healing in rock salt

    SciTech Connect

    Chan, K.S.; Bodner, S.R.; Munson, D.E.; Fossum, A.F.

    1996-03-01

    The development of a constitutive model for representing inelastic flow due to coupled creep, damage, and healing in rock salt is present in this paper. This model, referred to as Multimechanism Deformation Coupled Fracture model, has been formulated by considering individual mechanisms that include dislocation creep, shear damage, tensile damage, and damage healing. Applications of the model to representing the inelastic flow and fracture behavior of WIPP salt subjected to creep, quasi-static loading, and damage healing conditions are illustrated with comparisons of model calculations against experimental creep curves, stress-strain curves, strain recovery curves, time-to-rupture data, and fracture mechanism maps.

  15. ORNL irradiation creep facility

    SciTech Connect

    Reiley, T.C.; Auble, R.L.; Beckers, R.M.; Bloom, E.E.; Duncan, M.G.; Saltmarsh, M.J.; Shannon, R.H.

    1980-09-01

    A machine was developed at ORNL to measure the rates of elongation observed under irradiation in stressed materials. The source of radiation is a beam of 60 MeV alpha particles from the Oak Ridge Isochronous Cyclotron (ORIC). This choice allows experiments to be performed which simulate the effects of fast neutrons. A brief review of irradiation creep and experimental constraints associated with each measurement technique is given. Factors are presented which lead to the experimental choices made for the Irradiation Creep Facility (ICF). The ICF consists of a helium-filled chamber which houses a high-precision mechanical testing device. The specimen to be tested must be thermally stabilized with respect to the temperature fluctuations imposed by the particle beam which passes through the specimen. Electrical resistance of the specimen is the temperature control parameter chosen. Very high precision in length measurement and temperature control are required to detect the small elongation rates relevant to irradiation creep in the test periods available (approx. 1 day). The apparatus components and features required for the above are presented in some detail, along with the experimental procedures. The damage processes associated with light ions are discussed and displacement rates are calculated. Recent irradiation creep results are given, demonstrating the suitability of the apparatus for high resolution experiments. Also discussed is the suitability of the ICF for making high precision thermal creep measurements.

  16. Strain localization and grain size reduction during high-stress low-temperature plasticity and subsequent creep below the seismogenic zone

    NASA Astrophysics Data System (ADS)

    Trepmann, Claudia

    2014-05-01

    A sequence of high-stress crystal-plasticity with accompanying microcracking and subsequent creep at low stresses in the plastosphere can be triggered by the rupture of a fault in a major earthquake within the overlying seismogenic zone. In this study, microfabrics are analyzed by polarized light microscopy and electron microscopic techniques (SEM/EBSD, FIB, TEM) in rocks (vein quartz, peridotite) experimentally deformed at conditions that correspond to those prevailing in the upper plastosphere following a major earthquake. The experiments are carried out in a Griggs-type solid medium apparatus with a deformation stage at low temperature (300 to 600 °C) and high stress ("kick") followed by a stage at higher temperature (900 to 1000 °C) and isostatic ("cook") or low stress ("creep"). The resulting microfabrics show amazing resemblance to those observed in rocks from natural deep continuations of seismically active fault zones (i.e., shear zones). Localized zones of small new grains (a few µm in diameter) without systematic crystallographic preferred orientation within deformed host grains occur. The new grains develop by grain-boundary migration driven by the reduction in surface and strain energies at low stresses from highly damaged zones formed by initial low-temperature plasticity with associated cataclasis at high-stress deformation. A high variability in grain size is observed with the smallest grain size in the center of the highly damaged zones. The grain size reduction is controlled by strain during the initial high-stress deformation and growth is occurring only during the low-stress stage - rendering conventional grain size piezometers inappropriate. In large remnant host grains, short-wavelength undulatory extinction is reflecting low-stress modification (recovery) outside the highly damaged zones but in areas of original high dislocation densities formed at high-stress low-temperature plasticity. Extrapolation to natural conditions suggests that the observed characteristic microstructures may develop within as little as tens of years and less than ten thousands of years. The characteristic deformation and recrystallization microstructures can be expected to be stable over geological time scales, since driving forces for further modification are not sufficient to erase the characteristic heterogeneities. Thus, they are diagnostic for a past sequence of high-stress deformation (a combination of brittle failure and low-temperature plasticity) followed by creep at low stresses (recovery and recrystallization) in shear zones as deep continuations of seismically active fault zones. Such a sequence can explain initial grain size reduction localized along highly damaged zones during high-stress crystal-plasticity further leading to localized recrystallization during subsequent low-stress creep.

  17. Creep of oxide dispersion strengthened materials (with special reference to TD nichrome)

    NASA Technical Reports Server (NTRS)

    Lin, J.; Sherby, O. D.

    1978-01-01

    It was shown that the creep behavior of oxide dispersion strengthened (ODS) alloys is controlled principally by the creep properties of the matrix of the alloy devoid of particles. Thus, diffusion controlled slip process determine the rate controlling step in such materials. The role of the particles is to stabilize a fine substructure which is invariant with the creep stress over a wide range of stress. This characteristic leads to negligible strain hardening during creep and suggests that creep relations developed for pure metals and many solid solution alloys at constant structure should be used to describe the creep of ODS alloys. A second characteristics of the ODS alloys is that a stress may exist below which creep will not occur (threshold stress).

  18. Steady-State Creep of Rock Salt: Improved Approaches for Lab Determination and Modelling

    NASA Astrophysics Data System (ADS)

    Günther, R.-M.; Salzer, K.; Popp, T.; Lüdeling, C.

    2015-11-01

    Actual problems in geotechnical design, e.g., of underground openings for radioactive waste repositories or high-pressure gas storages, require sophisticated constitutive models and consistent parameters for rock salt that facilitate reliable prognosis of stress-dependent deformation and associated damage. Predictions have to comprise the active mining phase with open excavations as well as the long-term development of the backfilled mine or repository. While convergence-induced damage occurs mostly in the vicinity of openings, the long-term behaviour of the backfilled system is dominated by the damage-free steady-state creep. However, because in experiments the time necessary to reach truly stationary creep rates can range from few days to years, depending mainly on temperature and stress, an innovative but simple creep testing approach is suggested to obtain more reliable results: A series of multi-step tests with loading and unloading cycles allows a more reliable estimate of stationary creep rate in a reasonable time. For modelling, we use the advanced strain-hardening approach of Günther-Salzer, which comprehensively describes all relevant deformation properties of rock salt such as creep and damage-induced rock failure within the scope of an unified creep ansatz. The capability of the combination of improved creep testing procedures and accompanied modelling is demonstrated by recalculating multi-step creep tests at different loading and temperature conditions. Thus reliable extrapolations relevant to in-situ creep rates (10^{-9} to 10^{-13} s^{-1}) become possible.

  19. Creep Strain and Strain Rate Response of 2219 Al Alloy at High Stress Levels

    NASA Technical Reports Server (NTRS)

    Taminger, Karen M. B.; Wagner, John A.; Lisagor, W. Barry

    1998-01-01

    As a result of high localized plastic deformation experienced during proof testing in an International Space Station connecting module, a study was undertaken to determine the deformation response of a 2219-T851 roll forging. After prestraining 2219-T851 Al specimens to simulate strains observed during the proof testing, creep tests were conducted in the temperature range from ambient temperature to 107 C (225 F) at stress levels approaching the ultimate tensile strength of 2219-T851 Al. Strain-time histories and strain rate responses were examined. The strain rate response was extremely high initially, but decayed rapidly, spanning as much as five orders of magnitude during primary creep. Select specimens were subjected to incremental step loading and exhibited initial creep rates of similar magnitude for each load step. Although the creep rates decreased quickly at all loads, the creep rates dropped faster and reached lower strain rate levels for lower applied loads. The initial creep rate and creep rate decay associated with primary creep were similar for specimens with and without prestrain; however, prestraining (strain hardening) the specimens, as in the aforementioned proof test, resulted in significantly longer creep life.

  20. Impression Creep Behavior of a Cast AZ91 Magnesium Alloy

    NASA Astrophysics Data System (ADS)

    Kabirian, F.; Mahmudi, R.

    2009-01-01

    The creep behavior of the cast AZ91 magnesium alloy was investigated by impression testing. The tests were carried out under constant punching stress in the range 100 to 650 MPa, corresponding to 0.007 ? ? imp/ G ? 0.044, at temperatures in the range 425 to 570 K. Assuming a power-law relationship between the impression velocity and stress, depending on the testing temperature, stress exponents of 4.2 to 6.0 were obtained. When the experimental creep rates were normalized to the grain size and effective diffusion coefficient, a stress exponent of approximately 5 was obtained, which is in complete agreement with stress exponents determined by the conventional creep testing of the same material reported in the literature. Calculation of the activation energy showed a slight decrease in the activation energy with increasing stress such that the creep-activation energy of 122.9 kJ/mol at ? imp/ G = 0.020 decreases to 94.0 kJ/mol at ? imp/ G = 0.040. Based on the obtained stress exponents and activation energy data, it is proposed that dislocation climb is the controlling creep mechanism. However, due to the decreasing trend of creep-activation energy with stress, it is suggested that two parallel mechanisms of lattice and pipe-diffusion-controlled dislocation climb are competing. To elucidate the contribution of each mechanism to the overall creep deformation, the creep rates were calculated based on the effective activation energy. This yielded a criterion that showed that, in the high-stress regimes, the experimental activation energies fall in the range in which the operative creep mechanism is dislocation climb controlled by dislocation pipe diffusion. In the low-stress regime, however, the lattice-diffusion dislocation climb is dominant.

  1. The effect of cement creep and cement fatigue damage on the micromechanics of the cement-bone interface

    PubMed Central

    Waanders, Daan; Janssen, Dennis; Mann, Kenneth A.; Verdonschot, Nico

    2010-01-01

    The cement-bone interface provides fixation for the cement mantle within the bone. The cement-bone interface is affected by fatigue loading in terms of fatigue damage, or micro cracks, and creep, both mostly in the cement. This study investigates how fatigue damage and cement creep separately affect the mechanical response of the cement-bone interface at various load levels in terms of plastic displacement and crack formation. Two FEA models were created, which were based on micro-computed tomography data of two physical cement-bone interface specimens. These models were subjected to tensile fatigue loads with four different magnitudes. Three deformation modes of the cement were considered; only creep, only damage or creep and damage. The interfacial plastic deformation, the crack reduction as a result of creep and the interfacial stresses in the bone were monitored. The results demonstrate that, although some models failed early, the majority of plastic displacement was caused by fatigue damage, rather than cement creep. However, cement creep does decrease the crack formation in the cement up to 20%. Finally, while cement creep hardly influences the stress levels in the bone, fatigue damage of the cement considerably increases the stress levels in the bone. We conclude that at low load levels the plastic displacement is mainly caused by creep. At moderate to high load levels, however, the plastic displacement is dominated by fatigue damage and is hardly affected by creep, although creep reduced the number of cracks in moderate to high load region. PMID:20692663

  2. The effect of neutron irradiation on the fatigue and fatigue-creep behaviour of structural material

    NASA Astrophysics Data System (ADS)

    van der Schaaf, B.

    1988-07-01

    The primary circuit of a pulsed type fusion reactor will be subjected to cyclic loads at high temperature. Deformation rates will be in the range from below 10 -6 s -1 (creep) to 1 s -1 (fatigue) leading to creep-fatigue interaction in the neutron irradiated structural materials. The effects of neutron irradiation on fatigue and fatigue-creep interaction are reviewed. The study of austenitic stainless steel is most advanced, but the test conditions are still far from the first wall operating conditions, leaving a lot of uncertainties. It is expected that irradiation reduces the fatigue-creep endurance of austenites to very low levels, because of enhanced intergranular cracking. Two classes of alloys in an early stage of development, low activation steels and vanadium base alloys, hold the promise to be more fatigue-creep resistant due to their more ductile creep behaviour.

  3. On the stability of the creep substructure in NaCl single crystals

    NASA Technical Reports Server (NTRS)

    Raj, S. V.; Whittenberger, J. D.; Pharr, G. M.

    1989-01-01

    Microstructural observations were conducted on NaCl single crystals after creep. The microstructure after a stress increase followed by a stress decrease consisted primarily of cells; no significant number of subgrains were observed although they were present in the microstructures produced during uninterrupted tests. Prestraining in the exponential creep regime produced an uniform distribution of dislocations and a few subboundaries which transformed to equiaxed subgrains when tested in the power law creep region. This substructure was similar to that observed in an as-received specimen deformed to an equivalent strain. Prior creep in the power law creep region produced equiaxed subgrains whose boundaries were found to be mechanically stable when the specimen was retested in the exponential creep region. The role of subboundary migration in the formation of new subgrains is discussed.

  4. Creep and recovery behaviors of magnetorheological elastomer based on polyurethane/epoxy resin IPNs matrix

    NASA Astrophysics Data System (ADS)

    Qi, S.; Yu, M.; Fu, J.; Li, P. D.; Zhu, M.

    2016-01-01

    This paper mainly investigated the creep and recovery behaviors of magnetorheological elastomers (MRE) based on polyurethane/epoxy resin (EP) graft interpenetrating polymer networks (IPNs). The influences of constant stress level, content of EP, particle distribution, magnetic field and temperature on the creep and recovery behaviors were systematically investigated. As expected, results suggested that the presence of IPNs leads to a significant improvement of creep resistance of MRE, and creep and recovery behaviors of MRE were highly dependent on magnetic field and temperature. To further understand its deformation mechanism, several models (i.e., Findley’s power law model, Burgers model, and Weibull distribution equation) were used to fit the measured creep and recovery data. Results showed that the modeling of creep and recovery of samples was satisfactorily conducted by using these models. The influences of content of EP and magnetic field on fitting parameters were discussed, and relevant physical mechanism was proposed to explain it qualitatively.

  5. Analysis of the Creep Behavior of P92 Steel Welded Joint

    NASA Astrophysics Data System (ADS)

    An, Junchao; Jing, Hongyang; Xiao, Guangchun; Zhao, Lei; Xu, Lianyong

    2011-11-01

    Different regions of heat-affected zone (HAZ) were simulated by heat treatment to investigate the mechanisms of the Type IV fracture of P92 (9Cr-2W) steel weldments. Creep deformation of simulated HAZ specimens with uniform microstructures was investigated and compared with those of the base metal (BM) and the weld metal (WM) specimens. The results show that the creep strain rate of the fine-grained HAZ (FGHAZ) is much higher than that of the BM, WM, the coarse-grained HAZ (CGHAZ), and the inter-critical HAZ (ICHAZ). According to the metallurgical investigation of stress-rupture, the FGHAZ and the ICHAZ have the most severely cavitated zones. During creep process, carbides become coarser, and form on grain boundaries again, leading to the deterioration of creep property and the decline of creep strength. In addition, the crack grows along the FGHAZ adjacent to the BM in the creep crack growth test (CCG) of HAZ.

  6. Creep of Uncoated and Cu-Cr Coated NARloy-Z

    NASA Technical Reports Server (NTRS)

    Walter, R. J.; Chiang, K. T.

    1998-01-01

    Stress rupture creep tests were performed on uncoated and Cu-30vol%Cr coated NARloy-Z copper alloy specimens exposed to air at 482 C to 704 C. The results showed that creep failure in air of unprotected NARloy-Z was precipitated by brittle intergranular surface cracking produced by strain assisted grain boundary oxidation (SAGBO) which in turn caused early onset of tertiary creep. For the protected specimens, the Cu-Cr coating remained adherent throughout the tests and was effective in slowing down the rate of oxygen absorption, particularly at the higher temperatures, by formation of a continuous chromium oxide scale. As the result of reducing oxygen ingress, the coating prevented SAGBO initiated early creep failure, extended creep deformation and increased the creep rupture life of NARloy-Z over the entire 482 C to 704 C test temperature range.

  7. Arctic underwater noise transients from sea ice deformation: Characteristics, annual time series, and forcing in Beaufort Sea.

    PubMed

    Kinda, G Bazile; Simard, Yvan; Gervaise, Cédric; Mars, Jérôme I; Fortier, Louis

    2015-10-01

    A 13-month time series of Arctic Ocean noise from the marginal ice zone of the Eastern Beaufort Sea is analyzed to detect under-ice acoustic transients isolated from ambient noise with a dedicated algorithm. Noise transients due to ice cracking, fracturing, shearing, and ridging are sorted out into three categories: broadband impulses, frequency modulated (FM) tones, and high-frequency broadband noise. Their temporal and acoustic characteristics over the 8-month ice covered period, from November 2005 to mid-June 2006, are presented and their generation mechanisms are discussed. Correlations analyses showed that the occurrence of these ice transients responded to large-scale ice motion and deformation rates forced by meteorological events, often leading to opening of large-scale leads at main discontinuities in the ice cover. Such a sequence, resulting in the opening of a large lead, hundreds by tens of kilometers in size, along the margin of landfast ice and multiyear ice plume in the Beaufort-Chukchi seas is detailed. These ice transients largely contribute to the soundscape properties of the Arctic Ocean, for both its ambient and total noise components. Some FM tonal transients can be confounded with marine mammal songs, especially when they are repeated, with periods similar to wind generated waves. PMID:26520287

  8. Irradiation creep of the US Heat 832665 of V-4Cr-4Ti

    SciTech Connect

    Li, Meimei; Hoelzer, D. T.; Grossbeck, Martin L.; Rowcliffe, A. F.; Zinkle, Steven J.; Kurtz, Richard J.

    2009-04-30

    The paper presents irradiation creep data for V-4Cr-4Ti irradiated to 3.7 dpa at 425 and 600 _C in the HFIR-17J experiment. Creep deformation was characterized by measuring diametral changes of pressur-ized creep tubes before and after irradiation. It was found that the creep strain rate of the US Heat 832665 of V-4Cr-4Ti exhibited a linear relationship with stress up to _180 MPa at 425 _C with a creep coefficient of 2.50 _10_6 MPa_1 dpa_1. A linear relationship between creep rate and applied stress was observed below _110 MPa at 600 _C with a creep coefficient of 5.41 _10_6 MPa_1 dpa_1; non-linear creep behavior was observed above _110 MPa, and it may not be fully accounted by invoking thermal creep. The bilinear creep behavior observed in the same alloy irradiated in BR-10 was not observed in this study.

  9. Study of creep behavior of ultra-high-molecular-weight polyethylene systems.

    PubMed

    Deng, M; Latour, R A; Ogale, A A; Shalaby, S W

    1998-05-01

    The short- and long-term creep behaviors of ultra-high-molecular-weight polyethylene (UHMWPE) systems (compression-molded UHMWPE sheets and self-reinforced UHMWPE composites) have been investigated. The short-term (30-120 min) creep experiment was conducted at a load of 1 MPa and a temperature range of 37-62 degrees C. Based on short-term creep data, the long-term creep behavior of UHMWPE systems at 1 MPa and 37 degrees C was predicted using time-temperature superposition and analytical formulas. Compared to actual long-term creep experiments of up to 110 days, the predicted creep values were found to well describe the creep properties of the materials. The creep behaviors of the UHMWPE systems were then evaluated for a creep time of longer than 10 years, and it was found that most creep deformation occurs in the early periods. The shift factors associated with time-temperature superposition were found to increase with increasing temperature, as per the Arrhenius equation. The effects of temperature, materials, and load on the shift factors could be explained by the classical free volume theory. PMID:9549616

  10. Transient Deformation at the Seismic-Aseismic Transition in a Mature Plate Boundary Fault Zone - New Zealand's Alpine Fault

    NASA Astrophysics Data System (ADS)

    Toy, V. G.; Norris, R. J.; Prior, D. J.

    2008-12-01

    During the seismic cycle, stresses and strain rates fluctuate in the viscously-deforming zones down-dip of large faults. These transient events produce geological records that can be preserved in exhumed fault zones that have experienced single ruptures (e.g. Sesia Zone, European Western Alps). On the other hand, in major faults that have not experienced a simple, single rupture history, coseismic structures are likely to be destroyed during subsequent cycles of postseismic creep. New Zealand's active Alpine Fault has likely experienced upwards of 20,000 Mw~8 earthquakes, on average one every 200-300 years, over the last ≥5 million years of dextral-reverse slip. Fault rocks generated during these events are exhumed in the hangingwall, exposing materials deformed throughout the seismogenic zone at the surface. We have recognised a structural record of transient events in these rocks that differs from that previously reported elsewhere. Mylonites were formed by viscous shearing of a metasedimentary protolith downdip of the seismogenic structure. Rheological models predict these mylonites should have passed through a crustal strength peak (τ ≥100 MPa) around the brittle-viscous transition. Immediately prior to passing through this transition, they should have developed a small recrystallised grainsize (~10-15μm) and a crystallographic preferred orientation (CPO) indicating slip on the basal system during quartz dislocation creep, as well as a retrograde greenschist-facies mineralogy. However, the high-strain mylonites preserve a large recrystallised grainsize (>~30μm), amphibolite-facies mineralogy and CPO characteristic of prism slip. This suggests they were not significantly deformed at temperatures below ~450°C, significantly above the lower temperature limit for quartz crystal-plasticity at steady-state strain rates in the fault zone Microstructural observations and textural data indicate variable deformation style through the seismic cycle. Large fault ruptures propagated down-dip of the interseismically locked portion of the fault, so that a significant amount of deformation within the shear zone was released by slip on a single surface or surfaces, sometimes generating pseudotachylyte. High-stress immediate post-seismic creep resulted in activation of the uncharacteristic (harder?) prism slip system during quartz dislocation creep. On the other hand, creep strain rates in the interseismic period were much lower, so flow stresses were an order of magnitude less than expected if the shear zone deformation was evenly distributed over time. This postseismic creep must have been sufficient to develop a steady-state microstructure, so that the large quartz recrystallised grainsize developed while the ratio of recovery to deformation was high, but may have been insufficient to modify the prism CPO.

  11. Avoiding Project Creep.

    ERIC Educational Resources Information Center

    Kennerknecht, Norbert J.; Scarnati, James T.

    1998-01-01

    Discusses how to keep school district capital-improvement projects within budget. Examines areas where runaway costs creep into a project and ways of cutting or lessening these costs, such as using standard agreements, controlling architect's expense reimbursements, developing a quality-control process, and reducing document duplication. (GR)

  12. Bending induced by creeping of plasticized poly(vinyl chloride) gel

    NASA Astrophysics Data System (ADS)

    Hirai, Toshihiro; Kobayashi, Shigeyuki; Hirai, Mitsuhiro; Yamaguchi, Masaki; Uddin, Md. Zulhash; Watanabe, Masashi; Shirai, Hirofusa

    2004-07-01

    Poly(vinyl chloride) (PVC) plasticized with large amount of plasticizer has been investigated as a material for artificial muscle or actuator that can be actuated by applying an electric field. This material shows "creep deformation" on an electrode. The deformation looks like a pseudopodial deformation of amoeba. The deformation can be utilized for swift bending motility. In this paper, we investigated the mechanism of the creep deformation. Microscopic Raman spectroscopy revealed that the orientation of polymer network or plasticizer molecule was hardly detectable under the experimental conditions employed for the electrical actuation. Orientation of plasticizer was detected only slightly at higher field application. Small angle X-ray scattering analysis clarified that the PVC gel (plasticized PVC) sustains network structure even at the very high plasticizer content like 90wt%. With the increase of plasticizer content, space distance increased linearly, implying the network structure is sustained. This nature of the PVC gel plays a critical roll in the elastic creep deformation. The network structure of the gel depends on the chemical nature of the plasticizer itself. When the increase of plasticizer content caused serious deterioration of the physical network of PVC polymer chain, the PVC gel only deformed irreversibly by creep. The bending deformation also investigated from the viewpoint of electrode asymmetry. The results suggest effective charge injection and the charge concentration on the electrode is the controlling factor of this amoeba-like deformation.

  13. Relation between creep compliance and elastic modulus in organic-rich shales observed through laboratory experiments.

    NASA Astrophysics Data System (ADS)

    Sone, Hiroki; Zoback, Mark

    2013-04-01

    We studied the ductile creep behavior of organic-rich shales from shale gas reservoirs in North America through laboratory triaxial experiments to better understand controls on the physical behavior of these rocks over time and the effect of creep on other rock properties. Laboratory experiments conducted at room-temperature conditions show that creep deformation observed at in-situ differential stress conditions is approximately linear with the applied differential pressure. The creep behavior is also anisotropic such that creep occurs more in the bedding-perpendicular direction than in the bedding-parallel direction. The reduction in sample volume during creep suggests that the creep is accommodated by a small amount of pore compaction occurring in the clay-aggregates and/or the relatively porous kerogen in the rock. Thus, the tendency to creep (creep compliance) is generally observed to increases with clay and kerogen volume. However, the strongest correlation is found between creep compliance and Young's modulus. A strong negative correlation between creep compliance and elastic Young's modulus exists regardless of the sample orientation and despite the wide range of sample mineralogy (5-50% clay, 5-60% quartz-feldspar-pyrite, 0-80% carbonates). This correlation is quite interesting as inelastic creep and elastic stiffness depend on somewhat different physical attributes. We attempt to quantitatively explain the correlation between creep behavior and elastic stiffness by appealing to a stress-partitioning that occurs between the soft components (clay and kerogen) and stiff components (quartz, feldspar, pyrite, carbonates) of the shale rock. First, the stress-partitioning occurring within the soft and stiff components is quantified based on the rock composition, elastic properties of the individual components, and the overall average Young's modulus of the rock. By combining the stress-partitioning behavior with knowledge that the creep behavior is linear against the applied stress, we forward calculate the creep compliance of the whole rock. Results show that when creep is linear against stress, a unique relation between creep compliance and elastic modulus can be established for rocks with similar mineral assemblages, consistent with our laboratory results. Thus, our results provide insights into how creep behaviors of poly-mineralic rocks can be re-constructed from the creep properties of the individual phases composing the rock.

  14. Creep behavior of submarine sediments

    USGS Publications Warehouse

    Silva, Armand J.; Booth, J.S.

    1984-01-01

    A series of experiments on drained creep of marine sediment indicates that strength degradation results from the creep process, which implies an associated reduction in slope stability. Furthermore, the highest creep potential of a sediment may be at its preconsolidation stress. Results from the experiments on samples from Georges Bank continental slope were also used in conjunction with a preliminary theoretical model to predict creep displacements. For the case illustrated in this report, steep slopes (>20??) and thick sections (>30 m) give rise to substantial creep and probable creep rupture; as angles or thicknesses decrease, displacements rapidly become negligible. Creep may be a significant geologic process on many marine slopes. Not only can it cause major displacements of surface sediment, but it may also be the precursor to numerous slope failures. ?? 1985 Springer-Verlag New York Inc.

  15. Effect of Creep and Oxidation on Reduced Creep-Fatigue life of Ni-based Alloy 617 at 850 C

    SciTech Connect

    Chen, Xiang; Yang, Zhiqing; Sokolov, Mikhail A; ERDMAN III, DONALD L; Mo, Kun; Stubbins, James

    2014-01-01

    Low cycle fatigue (LCF) and creep fatigue testing of Ni-based alloy 617 was carried out at 850 C. Compared with its LCF life, the material s creep fatigue life decreases to different extents depending on test conditions. To elucidate the microstructure-fatigue property relationship for alloy 617 and the effect of creep and oxidation on its fatigue life, systematic microstructural investigations were carried out using scanning electron microscopy, energy-dispersive X-ray spectroscopy, and electron backscatter diffraction (EBSD). In LCF tests, as the total strain range increased, deformations concentrated near high angle grain boundaries (HAGBs). The strain hold period in the creep fatigue tests introduced additional creep damage to the material, which revealed the detrimental effect of the strain hold time on the material fatigue life in two ways. First, the strain hold time enhanced the localized deformation near HAGBs, resulting in the promotion of intergranular cracking of alloy 617. Second, the strain hold time encouraged grain boundary sliding, which resulted in interior intergranular cracking of the material. Oxidation accelerated the initiation of intergranular cracking in alloy 617. In the crack propagation stage, if oxidation was promoted and the cyclic oxidation damage was greater than the fatigue damage, oxidation-assisted intergranular crack growth resulted in a significant reduction in the material s fatigue life.

  16. Characteristics of the Cenozoic crustal deformations in SE Korea and its vicinity due to major tectonic events

    NASA Astrophysics Data System (ADS)

    Son, M.; Kim, J.; Song, C.; Sohn, Y.; Kim, I.

    2010-12-01

    The southeastern Korean Peninsula has experienced multiple crustal deformations according to changes of global tectonic setting during the Cenozoic. Characteristics of the crustal deformations in relation to major Cenozoic tectonic events are summarized as follows. (1) Collision of Indian and Eurasian continents and abrupt change of movement direction of the Pacific plate (50 ~ 43 Ma): The collision of Indian and Eurasian continents caused the eastward extrusion of East Asia block as a trench-rollback, and then the movement direction of the Pacific plate was abruptly changed from NNW to WNW. As a result, the strong suction-force along the plate boundary produced a tensional stress field trending EW or WNW-ESE in southeastern Korea, which resultantly induced the passive intrusion of NS or NNE trending mafic dike swarm pervasively. (2) Opening of the East Sea (25 ~ 16 Ma): The NS or NNW-SSE trending opening of the East Sea generated a dextral shear stress regime trending NNW-SSE along the eastern coast line of the Korean Peninsula. As a result, pull-apart basins were developed in right bending and overstepping parts along major dextral strike slip faults trending NNW-SSE in southeastern Korea. The basins can be divided into two types on the basis of geometry and kinematics: Parallelogram-shaped basin (rhombochasm) and wedged-shaped basin (sphenochasm), respectively. At that time, the basins and adjacent basement blocks experienced clockwise rotation and northwestward tilting, and the eastward propagating rifting also occurred. At about 17 Ma, the Yeonil Tectonic Line, which is the westernmost border fault of the Miocene crustal deformation in southeastern Korea, began to move as a major dextral strike slip fault. (3) Clockwise rotation of southeastern Japan Island (16~15 Ma): The collision of the Izu-Bonin Arc and southeastern Japan Island, as a result of northward movement of the Philippine sea-plate, induced the clockwise rotation of southeastern Japan Islands. The event caused a NW-SE compression in the Korea Strait as a tectonic inversion, which resultantly terminated the basin extension and caused locally counterclockwise rotation of blocks in southeastern Korea. At that time, the folding of the San'in folded zone commenced. The folding in the Tsushima Island was almost completely accomplished at about 15 Ma and then an extensive intrusion of felsic magma occurred in the southern part of the island which led the island to be tilted about 20 into northeast. Simultaneously, the Tsushima-Goto fault was reactivated as major sinistral strike-slip faults owing to the accumulated NNW-trending compressional stress. The adjacent blocks to the fault were rotated horizontally about 28 counterclockwise due to the sinistral movement, and resultantly the western part of the San'in folded zone was dragged counterclockwise. (4) E-W compression in the East Asia (after about 5 Ma): Decreasing subduction angle of the Pacific plate and eastward movement of the Amurian plate have constructed the-top-to-west thrusts and become a major cause for earthquakes in southeastern Korea.

  17. Creep-constitutive behavior of Sn-3.8Ag-0.7Cu solder using an internal stress approach

    NASA Astrophysics Data System (ADS)

    Rist, Martin A.; Plumbridge, W. J.; Cooper, S.

    2006-05-01

    The experimental tensile creep deformation of bulk Sn-3.8Ag-0.7Cu solder at temperatures between 263 K and 398 K, covering lifetimes up to 3,500 h, has been rationalized using constitutive equations that incorporate structure-related internal state variables. Primary creep is accounted for using an evolving internal back stress, due to the interaction between the soft matrix phase and a more creep-resistant particle phase. Steady-state creep is incorporated using a conventional power law, modified to include the steady-state value of internal stress. It is demonstrated that the observed behavior is well-fitted using creep constants for pure tin in the modified creep power law. A preliminary analysis of damage-induced tertiary creep is also presented.

  18. Stress versus temperature dependence of activation energies for creep

    NASA Technical Reports Server (NTRS)

    Freed, A. D.; Raj, S. V.; Walker, K. P.

    1992-01-01

    The activation energy for creep at low stresses and elevated temperatures is associated with lattice diffusion, where the rate controlling mechanism for deformation is dislocation climb. At higher stresses and intermediate temperatures, the rate controlling mechanism changes from dislocation climb to obstacle-controlled dislocation glide. Along with this change in deformation mechanism occurs a change in the activation energy. When the rate controlling mechanism for deformation is obstacle-controlled dislocation glide, it is shown that a temperature-dependent Gibbs free energy does better than a stress-dependent Gibbs free energy in correlating steady-state creep data for both copper and LiF-22mol percent CaF2 hypereutectic salt.

  19. Creep behaviour and creep mechanisms of normal and healing ligaments

    NASA Astrophysics Data System (ADS)

    Thornton, Gail Marilyn

    Patients with knee ligament injuries often undergo ligament reconstructions to restore joint stability and, potentially, abate osteoarthritis. Careful literature review suggests that in 10% to 40% of these patients the graft tissue "stretches out". Some graft elongation is likely due to creep (increased elongation of tissue under repeated or sustained load). Quantifying creep behaviour and identifying creep mechanisms in both normal and healing ligaments is important for finding clinically relevant means to prevent creep. Ligament creep was accurately predicted using a novel yet simple structural model that incorporated both collagen fibre recruitment and fibre creep. Using the inverse stress relaxation function to model fibre creep in conjunction with fibre recruitment produced a superior prediction of ligament creep than that obtained from the inverse stress relaxation function alone. This implied mechanistic role of fibre recruitment during creep was supported using a new approach to quantify crimp patterns at stresses in the toe region (increasing stiffness) and linear region (constant stiffness) of the stress-strain curve. Ligament creep was relatively insensitive to increases in stress in the toe region; however, creep strain increased significantly when tested at the linear region stress. Concomitantly, fibre recruitment was evident at the toe region stresses; however, recruitment was limited at the linear region stress. Elevating the water content of normal ligament using phosphate buffered saline increased the creep response. Therefore, both water content and fibre recruitment are important mechanistic factors involved in creep of normal ligaments. Ligament scars had inferior creep behaviour compared to normal ligaments even after 14 weeks. In addition to inferior collagen properties affecting fibre recruitment and increased water content, increased glycosaminoglycan content and flaws in scar tissue were implicated as potential mechanisms of scar creep. Similarly, ligament autografts had persistently abnormal creep behaviour and creep recovery after 2 years likely due to infiltration by scar tissue. Short-term immobilization of autografts had long-term detrimental consequences perhaps due to re-injury of the graft at remobilization. Treatments that restore normal properties to these mechanistic factors in order to control creep would improve joint healing by restoring joint kinematics and maintaining normal joint loading.

  20. FTIR Maps and Spatial Distributions of OH in Caledonide and Himalayan Shear Zones: Implications for Dislocation Creep and Water Weakening

    NASA Astrophysics Data System (ADS)

    Kronenberg, A. K.; Hasnan, H. F. B.; Holyoke, C. W., III; Kronenberg, J. A.; Law, R. D.; Thomas, J. B.

    2014-12-01

    FTIR measurements of quartz mylonites from the Moine Thrust of the NW Scotland Caledonides and the Main Central Thrust of the Himalaya reveal spatial variations in OH absorptions that correspond to deformation temperature, tectonic level within the thrust, intragranular shear, and recrystallization. Infrared spectra measured with apertures of 10-100 ?m exhibit OH absorptions characteristic of hydrogen point defects, fine fluid inclusions and micas within quartz grain interiors, and hydrous phases at grain boundaries. Moine Thrust quartzites, deformed at greenschist conditions (T ~ 350C) by Regime II, BLG/SGR dislocation creep, have pervasive broad OH absorptions due to fine fluid inclusions and sharp OH bands that appear locally due to finely dispersed micas. Mean OH contents vary from 2250 (+/-1500) ppm (106 OH/Si) in mylonitic quartzites 2.5 m below the thrust surface to 4080 (+/-1400) ppm in weakly deformed Cambrian quartzites 70 m below the thrust. Spatial variations in OH due to fine fluid inclusions are complex, with water contents that differ significantly between neighboring grains and correlate with grain strain and recrystallization. OH absorption bands mapped at a resolution of 10 ?m vary from 280 to 9000 ppm, well above and below concentrations known to weaken quartz.Himalayan mylonites in the hanging wall of the Main Central Thrust of the Sutlej region were deformed at upper amphibolite conditions (T ~ 600C) by Regime III, GBM dislocation creep. Given their extensive deformation and dislocation creep microstructures, quartz grains of these rocks are remarkably dry. Quartz grain spectra are dominated by sharp OH bands due to hydrogen interstitials with OH contents from 350 (+/-250) ppm (T = 600C) to 119 (+/-62) ppm (T = 640 - 740C). These results offer challenges to the application of experimental flow laws for water-weakened quartz to the high-grade dislocation creep of Himalayan mylonites. Much lower water contents may be sufficient for water weakening at upper amphibolite conditions and natural strain rates than are needed at experimental strain rates. Alternatively, hydrogen defects that enhance dislocation motion at these conditions may be sourced from grain boundaries or micas, diffusing over longer distances than are possible at greenschist conditions or laboratory rates.

  1. Creep and fracture of dispersion-strengthened materials

    NASA Technical Reports Server (NTRS)

    Raj, Sai V.

    1991-01-01

    The creep and fracture of dispersion strengthened materials is reviewed. A compilation of creep data on several alloys showed that the reported values of the stress exponent for creep varied between 3.5 and 100. The activation energy for creep exceeded that for lattice self diffusion in the matrix in the case of some materials and a threshold stress behavior was generally reported in these instances. The threshold stress is shown to be dependent on the interparticle spacing and it is significantly affected by the initial microstructure. The effect of particle size and the nature of the dispersoid on the threshold stress is not well understood at the present time. In general, most studies indicate that the microstructure after creep is similar to that before testing and very few dislocations are usually observed. It is shown that the stress acting on a dispersoid due to a rapidly moving dislocation can exceed the particle yield strength of the G sub p/1000, where G sub p is the shear modulus of the dispersoid. The case when the particle deforms is examined and it is suggested that the dislocation creep threshold stress of the alloy is equal to the yield strength of the dispersoid under these conditions. These results indicate that the possibility that the dispersoid creep threshold stress is determined by either the particle yield strength or the stress required to detach a dislocation from the dispersoid matrix interface. The conditions under which the threshold stress is influenced by one or the other mechanism are discussed and it is shown that the particle yield strength is important until the extent of dislocation core relaxation at the dispersoid matrix interface exceeds about 25 pct. depending on the nature of the particle matrix combination. Finally, the effect of grain boundaries and grain morphology on the creep and fracture behavior of dispersoid strengthened alloys is examined.

  2. Characterisation of Laves phase precipitation and its correlation to creep rupture strength of ferritic steels

    SciTech Connect

    Zhu, S.; Yang, M.; Song, X.L.; Tang, S.; Xiang, Z.D.

    2014-12-15

    The Laves phase precipitation process was characterised by means of field emission scanning electron microscopy to demonstrate its effect on creep rupture strength of steels with a fully ferritic matrix. To eliminate the effects of carbide and carbonitride precipitations so that the creep rupture data can be analysed exclusively in relation to the Laves phase precipitation process, an alloy Fe–9Cr–3Co–3W (wt.%) without C and N additions was used for the study. Creep rupture strengths were measured and volume fraction and particle size of Laves phase precipitates in the ruptured specimens were analysed. It was found that the creep rupture strength started to collapse (or decrease more rapidly) long before the Laves phase precipitation reached equilibrium fraction. This was related to the onset of the coarsening of Laves phase particles, which precipitated only on grain boundaries and hence contributed little to precipitation strengthening. Creep deformation had no effect either on the precipitation kinetics or on the growth kinetics of Laves phase particles. - Highlights: • Laves phase precipitation at 650 °C was characterised for Fe–9Cr–3W–3Co alloy. • Laves phase precipitated predominantly on grain boundaries. • Creep deformation had no effect on Laves phase precipitation and growth kinetics. • Creep strength started to collapse long before Laves phase precipitation is ended. • Collapse of creep strength was attributed to the coarsening of Laves phase particles.

  3. Microscopic evaluation of creep-fatigue interaction in a nickel-based superalloy

    SciTech Connect

    Santella, Michael L; Yamamoto, Masato; Shingledecker, John P; Boehlert, C. J.; Ogata, Takashi

    2009-01-01

    In order to verify the applicability of Nickel-based alloy Alloy 263 for the thick component, a series of creep, fatigue and creep-fatigue experiments were carried out. To investigate the detailed damage process under the creep-fatigue condition, simple aged, crept, fatigued, and creep-fatigued specimens were subjected to electron back scattering diffraction (EBSD) pattern observation in the SEM. While the simple aged and fatigued specimens showed no remarkable local change in orientation (less than 1deg), the crept specimen exhibited inhomogeneous change of crystallographic orientation, at most 5 degrees, within the grains. This shows that the creep strain is inhomogeneously distributed in the grains due to the effect of relative constraint among the grains. The creep-fatigued specimen exhibited similar local inhomogeniety in strain distribution compared to the crept sample near the center of the grains. However, the creep-fatigued specimen showed remarkable local change in orientation at the vicinity of grain boundaries up to 15 degrees, indicating the occurrence of high strain concentration nearby the grain boundaries. A detailed observation of creep-fatigue damage evolution process in SEM revealed that the inhomogeneous grain deformation precedes the remarkable inhomogeneous deformation nearby the grain boundaries, and followed by the grain boundary cracking.

  4. Helium effects on creep properties of Fe-14CrWTi ODS steel at 650 C

    NASA Astrophysics Data System (ADS)

    Chen, J.; Jung, P.; Rebac, T.; Duval, F.; Sauvage, T.; de Carlan, Y.; Barthe, M. F.

    2014-10-01

    In the present paper, the effects of helium on creep properties of Fe-14CrWTi ODS steel were studied by in-beam and post He-implantation creep tests. In-situ creep was performed in an in-beam creep device under uniaxial tensile stresses from 350 to 370 MPa during homogeneous helium implantation. Helium ions of energies varying from 0 to 25 MeV were implanted at a rate of 6 10-3 appm/s (corresponding to a displacement dose rate of 1.5 10-6 dpa/s). The average temperature was controlled to 650 C within 2 C. In addition, post He-implantation creep tests were conducted at 650 C as well. Subsequently, fracture surfaces and helium bubble evolution were studied in detail by SEM and TEM observations, respectively. Preliminary creep results show that helium slightly shortens the creep life time of ODS steel at 650 C. Fracture surfaces of reference as well as implanted specimens, show areas with various grades of deformation. Areas of highest deformation can be interpreted as necking, while areas of low deformation show in helium implanted specimens a more granular structure. The results are discussed in terms of possible embrittlement of ODS steels by helium.

  5. Copper, Boron, and Cerium Additions in Type 347 Austenitic Steel to Improve Creep Rupture Strength

    NASA Astrophysics Data System (ADS)

    Laha, Kinkar; Kyono, J.; Shinya, Norio

    2012-04-01

    Type 347 austenitic stainless steel (18Cr-12Ni-Nb) was alloyed with copper (3 wt pct), boron (0.01 to 0.06 wt pct), and cerium (0.01 wt pct) with an aim to increase the creep rupture strength of the steel through the improved deformation and cavitation resistance. Short-term creep rupture strength was found to increase with the addition of copper in the 347 steel, but the long-term strength was inferior. Extensive creep cavitation deprived the steel of the beneficial effect of creep deformation resistance induced by nano-size copper particles. Boron and cerium additions in the copper-containing steel increased its creep rupture strength and ductility, which were more for higher boron content. Creep deformation, grain boundary sliding, and creep cavity nucleation and growth in the steel were found to be suppressed by microalloying the copper-containing steel with boron and cerium, and the suppression was more for higher boron content. An auger electron spectroscopic study revealed the segregation of boron instead of sulfur on the cavity surface of the boron- and cerium-microalloyed steel. Cerium acted as a scavenger for soluble sulfur in the steels through the precipitation of cerium sulfide (CeS). This inhibited the segregation of sulfur and facilitated the segregation of boron on cavity surface. Boron segregation on the nucleated cavity surface reduced its growth rate. Microalloying the copper-containing 347 steel with boron and cerium thus enabled to use the full extent of creep deformation resistance rendered by copper nano-size particle by increase in creep rupture strength and ductility.

  6. Muscle Activity Adaptations to Spinal Tissue Creep in the Presence of Muscle Fatigue

    PubMed Central

    Nougarou, François

    2016-01-01

    Aim The aim of this study was to identify adaptations in muscle activity distribution to spinal tissue creep in presence of muscle fatigue. Methods Twenty-three healthy participants performed a fatigue task before and after 30 minutes of passive spinal tissue deformation in flexion. Right and left erector spinae activity was recorded using large-arrays surface electromyography (EMG). To characterize muscle activity distribution, dispersion was used. During the fatigue task, EMG amplitude root mean square (RMS), median frequency and dispersion in x- and y-axis were compared before and after spinal creep. Results Important fatigue-related changes in EMG median frequency were observed during muscle fatigue. Median frequency values showed a significant main creep effect, with lower median frequency values on the left side under the creep condition (p≤0.0001). A significant main creep effect on RMS values was also observed as RMS values were higher after creep deformation on the right side (p = 0.014); a similar tendency, although not significant, was observed on the left side (p = 0.06). A significant creep effects for x-axis dispersion values was observed, with higher dispersion values following the deformation protocol on the left side (p≤0.001). Regarding y-axis dispersion values, a significant creep x fatigue interaction effect was observed on the left side (p = 0.016); a similar tendency, although not significant, was observed on the right side (p = 0.08). Conclusion Combined muscle fatigue and creep deformation of spinal tissues led to changes in muscle activity amplitude, frequency domain and distribution. PMID:26866911

  7. Deformation processes in forging ceramics

    NASA Technical Reports Server (NTRS)

    Cannon, R. M.; Rhodes, W. H.

    1973-01-01

    The deformation processes involved in the forging of refractory ceramic oxides were investigated. A combination of mechanical testing and forging was utilized to investigate both the flow and fracture processes involved. Deformation studies of very fine grain Al203 revealed an apparent transition in behavior, characterized by a shift in the strain rate sensitivity from 0.5 at low stresses to near unity at higher stresses. The behavior is indicative of a shift in control between two dependent mechanisms, one of which is indicated to be cation limited diffusional creep with significant boundary enhancement. The possible contributions of slip, indicated by crystallographic texture, interface control of the diffusional creep and inhomogeneous boundary sliding are also discussed. Additional experiments indicated an independence of deformation behavior on MgO doping and retained hot pressing impurities, at least for ultrafine grained material, and also an independence of test atmosphere.

  8. Prediction and verification of creep behavior in metallic materials and components, for the space shuttle thermal protection system. Volume 1, phase 1: Cyclic materials creep predictions

    NASA Technical Reports Server (NTRS)

    Davis, J. W.; Cramer, B. A.

    1974-01-01

    Cyclic creep response was investigated and design methods applicable to thermal protection system structures were developed. The steady-state (constant temperature and load) and cyclic creep response characteristics of four alloys were studied. Steady-state creep data were gathered through a literature survey to establish reference data bases. These data bases were used to develop empirical equations describing creep as a function of time, temperature, and stress and as a basis of comparison for test data. Steady-state creep tests and tensile cyclic tests were conducted. The following factors were investigated: material thickness and rolling direction; material cyclic creep response under varying loads and temperatures; constant stress and temperature cycles representing flight conditions; changing stresses present in a creeping beam as a result of stress redistribution; and complex stress and temperature profiles representative of space shuttle orbiter trajectories. A computer program was written, applying creep hardening theories and empirical equations for creep, to aid in analysis of test data. Results are considered applicable to a variety of structures which are cyclicly exposed to creep producing thermal environments.

  9. The effects of computed tomography image characteristics and knot spacing on the spatial accuracy of B-spline deformable image registration in the head and neck geometry

    PubMed Central

    2014-01-01

    Objectives To explore the effects of computed tomography (CT) image characteristics and B-spline knot spacing (BKS) on the spatial accuracy of a B-spline deformable image registration (DIR) in the head-and-neck geometry. Methods The effect of image feature content, image contrast, noise, and BKS on the spatial accuracy of a B-spline DIR was studied. Phantom images were created with varying feature content and varying contrast-to-noise ratio (CNR), and deformed using a known smooth B-spline deformation. Subsequently, the deformed images were repeatedly registered with the original images using different BKSs. The quality of the DIR was expressed as the mean residual displacement (MRD) between the known imposed deformation and the result of the B-spline DIR. Finally, for three patients, head-and-neck planning CT scans were deformed with a realistic deformation field derived from a rescan CT of the same patient, resulting in a simulated deformed image and an a-priori known deformation field. Hence, a B-spline DIR was performed between the simulated image and the planning CT at different BKSs. Similar to the phantom cases, the DIR accuracy was evaluated by means of MRD. Results In total, 162 phantom registrations were performed with varying CNR and BKSs. MRD-values < 1.0 mm were observed with a BKS between 1020 mm for image contrast ? 250 HU and noise < 200 HU. Decreasing the image feature content resulted in increased MRD-values at all BKSs. Using BKS = 15 mm for the three clinical cases resulted in an average MRD < 1.0 mm. Conclusions For synthetically generated phantoms and three real CT cases the highest DIR accuracy was obtained for a BKS between 1020 mm. The accuracy decreased with decreasing image feature content, decreasing image contrast, and higher noise levels. Our results indicate that DIR accuracy in clinical CT images (typical noise levels < 100 HU) will not be effected by the amount of image noise. PMID:25074293

  10. Experimental deformation of rocksalt

    NASA Astrophysics Data System (ADS)

    Handin, J.; Russell, J. E.; Carter, N. L.

    Using newly designed apparatus for triaxial-compression testing of 10 by 20-cm cores of Avery Island rocksalt at constant strain-rates between 10-4 and 10-6/s, temperatures between 100° and 200°C, and confining pressures of 3.4 and 20 MPa, comparing our data with those of other workers on the same material, and observing natural deformations of rocksalt, we find that (1) constant-strain-rate and quasi-constant stress-rate tests (both often called quasi-static compression tests) yield essentially similar stress-strain relations, and these depend strongly on strain rate and temperature, but not confining pressure; (2) fracture excluded, the deformation mechanisms observed for differential stresses between 0.5 and 20 MPa are intracrystal-line slip (dislocation glide and cross-slip) and polygonization (dislocation glide and climb by ion-vacancy pipe diffusion); (3) the same steady-state strain rate ɛ., and flow stress are reached at the same temperature in both constant-strain-rate and constant-stress (creep) tests, but the strain-time data from transient creep tests do not match the strain-hardening data unless the initial strain, ɛ0 (time-dependent in rocksalt) is accounted for; in creep tests the clock is not started until the desired constant stress is reached; (4) because the stress-strain curve contains the entire history of the deformation, the constant-strain-rate test rather than the creep test may well be preferred as the source of constitutive data; (5) furthermore, if the stress or temperature of the creep test is too low to achieve the steady state in laboratory time, one cannot predict the steady-state flow stress or strain rate from the transient response alone, whereas we can estimate them rather well from constant-strain-rate data even when strain rates are too high or temperatures too low to reach the steady state within a few hours; (6) the so-called "baseline creep law", giving creep strain, ɛ = ea[1-exp(-ξt)]+ɛ. ss t, where ea, ξ, and ɛ. ss are regarded as material properties as well as fitting parameters, can be valid, if at all, only over intervals of stress and temperature where the same deformation mechanisms operate and only if it is independent of structural changes, that is of loading path, and it poorly predicts constant-stress-rate response in triaxial-compression tests and long-term, low-stress response from data taken over short time at high stress; (7) a potentially more useful, semi-empirical constitutive model, incorporating stress (σ), strain (ɛ), strain rate (ɛ.), and absolute temperature (T), and capable of matching at least limited constant-strain-rate, constant-stress-rate, constant-stress (creep), and relaxation (nearly constant strain) data even though constant structure is assumed, is σ=Kɛ. q exp(B/T)[1={exp(-r1ɛ) + exp(-r2ɛ)}/2], where K, q, B, r1, and r2 are to be treated as fitting parameters until their physical significance is better understood; (8) however, we doubt that any single, perfectly general constitutive equation can be written to satisfy all conditions pertinent to repository design, say 25° ≤ T ≤ 300°C and 1 ≤ σ ≤ 20 MPa, and also to be workable in numerical modeling; (9) hence, no matter how abundant and precise site-specific laboratory data may become, one can expect only to approximate the rheological behavior of the prototype.

  11. Testing the inference of creep on Rodgers Creek Fault

    NASA Astrophysics Data System (ADS)

    Jin, L.; Funning, G. J.

    2010-12-01

    The Rodgers Creek fault (RCF), one of the major through-going structures in the northern San Francisco Bay area, links two known active creeping faults - the Hayward fault and the Maacama fault. Historic earthquakes that occurred on the fault prove that this fault is seismically active. However, whether or not it creeps like its neighbors remains a question. A previous study (Funning et al., 2007) identified a right-lateral fault creep at rates up to 6 mm/yr between 1992 and 2001. The estimate remains controversial, however, since the evidence on the ground is limited. Another explanation for the velocity step is a vertical hydrological signal. Here, we use Permanent Scaterers InSAR data from both ascending and descending viewing geometries to test these two hypotheses. Under the assumption that fault-related deformation acts in the fault-parallel direction, it is possible to separate the deformation measured in the two viewing geometries into its horizontal and vertical components. Therefore, we put our efforts to validate/refute our initial hypothesis of creep on RCF by processing a 39-image ascending track dataset (track 478, frame 765) and a 33-image descending track dataset (track 342, frame 2835) from the ESA Envisat satellite spanning the interval 2003-2010, using the StaMPS/MTI code (Hooper, 2008). Assuming there is a creep on RCF, we would expect to see vertical deformations in both datasets but horizontal deformations only in track 342. In order to compare the PS velocities on either side of the fault, we plot cross-fault profiles through both datasets at ~5 km intervals and detrend the profiles by fitting parallel straight lines to windows of datapoints either side of the fault. The gradients of the lines reflect the regional component of deformation, along with any residual error in satellite orbital position, while the separations represent fault offset rates. Our preliminary results show positive (towards the satellite) velocities in the Cotati Basin and negative (away from the satellite) in the Santa Rosa plain in both datasets. In these areas, we believe, the ground is experiencing vertical deformations due to the subsurface fluid exchanges. Also, the results exhibit velocities change from negative to positive from west to east crossing RCF near the Foutaingrove Lake (FL) and the Annadel State Park (ASP), but in track 342 only. Based on the results, we find that our data are consistent with creep on RCF between FL and ASP from 2003 to 2010.

  12. The constant-hardness creep compliance of polycrystalline ice

    NASA Astrophysics Data System (ADS)

    Caswell, Tess E.; Cooper, Reid F.; Goldsby, David L.

    2015-08-01

    We have performed creep and stress-reduction experiments on polycrystalline ice (grain sizes, d ? 30 and ? 245 m) in the grain boundary sliding and dislocation creep regimes (stresses ? = 0.5-5 MPa, temperature T = 233 K) to determine the constant-hardness creep compliance under these conditions. Our results are consistent with a microstructural state-variable description of dislocation-effected deformation whose rate is accelerated by grain boundary sliding. The fine-grained specimens reveal no subgrain boundaries, indicating that the stress-sensitive microstructural feature upon which the state-variable behavior is founded may be the dislocation structure of the grain boundaries. Deviations of our constant-hardness data from the behavior predicted by the state-variable formulation allow estimation of the viscosity of the grain boundaries, which is ~4.8 106 Pa s at this temperature.

  13. Can Competition Between Frictional Sliding and Viscous Creep Determine Megathrust Fault Slip Style?

    NASA Astrophysics Data System (ADS)

    Fagereng, A.

    2014-12-01

    In exhumed megathrust analogues, deformation is partitioned between continuous and discontinuous deformation structures, commonly reflecting partitioning between concurrent frictional and viscous shear. This partitioning is a function of material properties, strain rate, and fluid pressure distribution. Mineral strength and preferred deformation mechanism vary down-dip as a function of temperature and pressure; however, incoming sediment composition, roughness of the sea floor, and the relative proportions of competent and incompetent material, all affect bulk rheology, and may vary both with depth and along strike. Fluid pressure varies with depth, but also along strike if fluid sources and/or permeability vary along the margin. At the locations of major dehydration reactions, localized peaks in fluid pressure occur if permeability is low. These zones of low effective stress may allow for frictional sliding in rocks normally deforming by viscous shearing flow, and could relate to zones of tremor and slow slip. Frictional sliding and possible associated tensile fractures would, however, allow fluid escape, resulting in fluid pressure fluctuations and a time-dependent interplay between continuous and discontinuous deformation. Locally elevated effective stress increases frictional strength, promoting failure by viscous mechanisms. If this is true, and representative of large-scale megathrust behavior, then decreased fluid pressure may promote creep. In a fluid-saturated, tabular fault zone with small grain size, this creep can take place by pressure solution creep at subgreenschist conditions. If pressure solution is the active mineral deformation mechanism, and shear is distributed though a tabular zone, viscous shearing flow at plate boundary rates is possible at temperatures significantly less than required for the onset of dislocation creep in quartzofeldspathic rocks. In a wide shear zone, such viscous flow may occur at low differential stress. A hypothesis to consider, consistent with field observations of coexisting frictional sliding and pressure solution creep, is then that locked megathrust segments have relatively low effective stress and prefer frictional over viscous deformation, whereas creeping segments have higher effective stress and dominantly deform viscously.

  14. SAR interferometry and optical remote sensing for analysis of co-seismic deformation, source characteristics and mass wasting pattern of Lushan (China, April 2013) earthquake

    NASA Astrophysics Data System (ADS)

    Mathew, John; Majumdar, Ritwik; Kumar, K. Vinod

    2015-03-01

    Co-seismic deformation associated with the Lushan (China) earthquake that occurred along the south-western segment of the Longmenshan Fault Zone (LFZ) on the 20th April 2013 has been estimated by differential interferometric SAR (DInSAR) technique using Radarsat-2 data. The Lushan earthquake resulted in the deformation of the Sichuan basin and the Longmenshan ranges in proximity to the LFZ. The line of sight (LOS) displacement values obtained from DInSAR technique mainly range between -4.0 cm to +3.0 cm. The western Sichuan basin shows oblique westward movement with predominant downward component in areas farther from LFZ and predominant westward component over the downward movement in areas closer to the source fault. Inversion modelling has been used to derive the seismic source characteristics from DInSAR derived deformation values using elastic dislocation source type. The linear inversion model converged at a double-fault source solution consisting of a deeper, steep, NW dipping fault plane-1 of 60 km 16 km dimension and a shallower, gentle, NW dipping fault plane-2 of 60 km 15 km dimension, with distributed slip values varying between 0 to 2.26 m. These fault planes (fault planes-1 and -2) coincide with the Dachuan-Shuangshi fault and the buried Range Front Fault, respectively. The inversion model gives a moment magnitude of 6.81 and the geodetic moment of 2.07 1019 Nm, comparable to those given in literature, derived using teleseismic body wave data. Thus DInSAR technique helped to quantify the co-seismic deformation and to retrieve the source characteristics from the estimated deformation values. The study also evaluated the distribution pattern of earthquake induced landslides (EIL) triggered fresh or re-activated during the Lushan earthquake and found that they show spatial association with the seismic source zone and also with various pre-conditioning factors of slope instability.

  15. An Experimental study of the initial volumetric strain rate effect on the creep behaviour of reconstituted clays

    NASA Astrophysics Data System (ADS)

    Bagheri, M.; Rezania, M.; Nezhad, M. M.

    2015-09-01

    Clayey soils tend to undergo continuous compression with time, even after excess pore pressures have substantially dissipated. The effect of time on deformation and mechanical response of these soft soils has been the subject of numerous studies. Based on these studies, the observed time-dependent behaviour of clays is mainly related to the evolution of soil volume and strength characteristics with time, which are classified as creep and/or relaxation properties of the soil. Apart from many empirical relationships that have been proposed in the literature to capture the rheological behaviour of clays, a number of viscid constitutive relationships have also been developed which have more attractive theoretical attributes. A particular feature of these viscid models is that their creep parameters often have clear physical meaning (e.g. coefficient of secondary compression, C?). Sometimes with these models, a parameter referred to as initial/reference volumetric strain rate, has also been alluded as a model parameter. However, unlike C?, the determination of and its variations with stress level is not properly documented in the literature. In an attempt to better understand , this paper presents an experimental investigation of the reference volumetric strain rate in reconstituted clay specimens. A long-term triaxial creep test, at different shear stress levels and different strain rates, was performed on clay specimen whereby the volumetric strain rate was measured. The obtained results indicated the stress-level dependency and non-linear variation of with time.

  16. High temperature tensile and creep behaviour of low pressure plasma-sprayed Ni-Co-Cr-Al-Y coating alloy

    NASA Technical Reports Server (NTRS)

    Hebsur, M. G.; Miner, R. V.

    1986-01-01

    The high temperature tensile and creep behavior of low pressure plasma-sprayed plates of a typical Ni-Co-Cr-Al-Y alloy has been studied. From room temperature to 800 K, the Ni-Co-Cr-Al-Y alloy studied has nearly a constant low ductility and a high strength. At higher temperatures, it becomes weak and highly ductile. At and above 1123 K, the behavior is highly dependent on strain rate and exhibits classic superplastic characteristics with a high ductility at intermediate strain rates and a strain rate sensitivity of about 0.5. At either higher or lower strain rates, the ductility decreases and the strain rate sensitivities are about 0.2. In the superplastic deformation range, the activation energy for creep is 120 + or - 20 kJ/mol, suggesting a diffusion-aided grain boundary sliding mechanism. Outside the superplastic range, the activation energy for creep is calculated to be 290 + or - 20 kJ/mol.

  17. THE INFLUENCE OF COLD?WORK LEVEL ON THE IRRADIATION CREEP AND The Influence of Cold?Work Level on The Irradiation Creep and Swelling of AISI 316 Stainless Steel Irradiated as Pressurized Tubes In The EBR-II Fast Reactor

    SciTech Connect

    Gilbert, Edgar R.; Garner, Francis A.

    2006-09-01

    Pressurized tubes of AISI 316 stainless steel irradiated in the P-1 experiment in the EBR-II fast reactor have been measured to determine the dependence of irradiation-induced strains resulting from plastic deformation, irradiation creep, void swelling and precipitation. It is shown that the Soderberg relation predicting no axial creep strains in biaxially-loaded tubes is correct for both plastic and creep strains. Swelling strains are shown to be isotropically distributed both for stress-free and stress-affected swelling, while precipitation strains are somewhat anisotropic in their distribution. When corrected for stress-enhancement of swelling, the derived irradiation creep strains appear to be identical for both annealed and 20% cold-worked specimens, and also for tubes strained by rise to power increases in pressure. For relatively small creep strains it is often difficult to separate the creep and non-creep components of deformation.

  18. An Investigation of the Strength and Deformation Characteristics of Rock masses: A Case Study in an Excavation of Eskişehir-Köseköy Tunnels, Turkey

    NASA Astrophysics Data System (ADS)

    Beyhan, Sunay; Abiddin Erguler, Zeynal; Ogul, Kenan

    2015-04-01

    With increasing of high-speed rail technology in last decades, Turkey has developed many big engineering projects to connect major cities. Excavations conducted for these projects provide very important contributions in term of understanding the strength and deformation characteristics of weak rock masses belongs to various geological materials. The Ankara-Istanbul high-speed railway known as a significant project among these projects was designed in two different phases. To discuss the outcomes, experiences and challenging geological materials during construction of this tunnel, the geotechnical properties of rock masses of a tunnel named as T19 are evaluated and discussed in this study. The T19 tunnel was excavated in stratified and heavily fractured four different geological formations. Rock mass rating (RMR) system, and tunnelling quality index (Q) were utilized for the preliminary design stages of this tunnel. These engineering rock mass classifications were utilized in 135 different locations to find representative RMR and Q values for encountered rock masses during excavation. The RMR and Q values, which range between 18-52 and changing between 0.017 and 1.6 respectively, indicate that the T19 tunnel was mainly constructed in very poor and poor rock masses. Thus, shotcrete immediately was applied after face advance to prevent the fall of loose rock fragments and to minimize excessive deformation in rock, particular in very poor and poor rock masses. In addition, the deformation characteristics of the tunnel were also carefully monitored and measured by 3D-optical measuring system and conventional tape extensometer, and then required further supports were installed. Finally, the rock mass-support interactions of different geological formations were comprehensively evaluated in this study for understanding strength and deformation characteristics of weak and stratified rock masses. Keywords: Convergence, high-speed rail, rock mass, support, tunnel

  19. Observations of orientation dependent creep of Ni{sub 3}Al

    SciTech Connect

    Knobloch, C.; Glock, K.; Glatzel, U.

    1999-07-01

    The influence of crystal orientation on the high temperature creep behavior of Ni{sub 3}(Al Ti Ta) was investigated by tensile creep testing under a constant load at a temperature of 1,123K. The single crystals were oriented close to [001], [011], [111], [557] and [012]. The results show an increasing stationary creep rate from [111] over [011] to [001]. The evolution of the microstructure during creep deformation was studied, using transmission electron microscopy (TEM). Only few systems are active in the primary regime, whereas several slip systems operate in the secondary stage. habit planes of dislocation pairs separated by an antiphase boundary were examined and compared with anisotropic elastic calculations, explaining the good creep response of [111] oriented using crystals.

  20. Correlation between permanent deformation-related performance parameters of asphalt concrete mixes and binders

    NASA Astrophysics Data System (ADS)

    Adorjányi, Kálmán; Füleki, Péter

    2013-09-01

    This paper examines methods to predict the performance of hot asphalt concrete mixes based on performance parameters of binders. Specifically, relationships between binder parameters determined from multiple stress creep and recovery tests were correlated to the creep parameters of hot asphalt concrete mixes obtained from cyclic load compression testing. For the determination of creep parameters, a modified expression of the creep curve is proposed to cover the entire spectrum of permanent deformation; including the tertiary creep phase. Non-recoverable compliance, unrecovered strain, and recoverable strain of binders show good correlation to creep parameters of hot asphalt concrete mixes such as creep rate and high temperature performance ratio. Additionally, unrecovered strain and non-recoverable compliance of binders correlates well with mean rut depth of asphalt concrete mixes. However, no correlation has been detected between the difference in non-recoverable compliance of binders and permanent deformation parameters of asphalt concrete mixes.

  1. The plastic deformation behaviour of ceramic nuclear fuels at stress changes

    NASA Astrophysics Data System (ADS)

    Mller-Lyda, I.

    1980-01-01

    The irradiation creep experiments of the BR2 Mol-12 series in capsules allowing an in-pile variation of the stress applied on the fuel specimen showed a typical accelerated deformation of mixed oxide as well as mixed carbide fuel. Quantitative relations for the accelerated deformation depending upon the irradiation parameters are derived from the measured creep data. Magnitude and time dependence of the accelerated deformation effects are discussed and compared with the steady-state creep and swelling. Accelerated fuel deformations due to stress changes can be a beneficial effect lowering the fuel/ cladding mechanical interaction during load-follow-on operation.

  2. Propagation of Crack in Glasses under Creep Conditions

    NASA Astrophysics Data System (ADS)

    Mallet, C.; Fortin, J.; Guguen, Y.; Schubnel, A.

    2012-04-01

    The context of our study is the observation of the mechanical behaviour of glass used for the storage of radioactive wastes. This implies to measure the crack propagation characteristics in glass. Results on the investigation of the micromechanics of creep under triaxial loading conditions are presented in the framework of this study. We performed the experiments in a triaxial cell, with pore fluid pressure, on boro-silicate glass. The chemical composition of the investigated glass is very close to the composition of waste vitrified packages. The matrix of the original glass (OG) is perfectly amorphous, without porosity. A few isolated air bubbles are trapped during the glass flow. Cracks are introduced in the OG through thermal shocks. The evolution of deformation (axial and radial strain) is measured using strain gages. The elastic P and S wave velocities and the acoustic emissions (AE) are also recorded. An experiment in dry conditions was performed (the pore fluid was argon gas) with a confining pressure fixed at 15 MPa. Stress step tests were performed in order to get creep data. A similar experiment was performed in water saturated conditions. Crack-closure is first observed at very low strains. Then elastic deformation is observed up to a stress level where elastic anisotropy develops. This can be clearly detected from ? Thomsen parameter increase. At last, at a deviatoric stress of 175 MPa (in dry conditions), we observe dilatancy. This behaviour has never been observed in original glass. Indeed, the OG behaviour is perfectly elastic and brittle. In addition, the constant stress tests show that dilatancy develops during a time constant that depends on the stress level. It can be inferred that crack propagation takes place during the constant stress steps. This behaviour is under investigation. We are also quantifying the velocity of the crack propagation by modelling this phenomenon. Indeed, the crack density can be expressed as a volumic strain, ?v = ???c. Then, using a model of penny shaped cracks of a radius, "a", we can express the crack density as: ?c = N/V a3 (for N cracks in a volume V). Knowing that ? is the crack aspect ratio we can estimate ?v using in a first approximation that ? is a constant. Thus the variation of ?v with time can be directly related to crack propagation ȧ.

  3. Creep Strength of Nb-1Zr for SP-100 Applications

    NASA Astrophysics Data System (ADS)

    Horak, James A.; Egner, Larry K.

    1994-07-01

    Power systems that are used to provide electrical power in space are designed to optimize conversion of thermal energy to electrical energy and to minimize the mass and volume that must be launched. Only refractory metals and their alloys have sufficient long-term strength for several years of uninterrupted operation at the required temperatures of 1200 K and above. The high power densities and temperatures at which these reactors must operate require the use of liquid-metal coolants. The alloy Nb-1 wt % Zr (Nb-lZr), which exhibits excellent corrosion resistance to alkali liquid-metals at high temperatures, is being considered for the fuel cladding, reactor structural, and heat-transport systems for the SP-100 reactor system. Useful lifetime of this system is limited by creep deformation in the reactor core. Nb-lZr sheet procured to American Society for Testing and Materials (ASTM) specifications for reactor grade and commercial grade has been processed by several different cold work and annealing treatments to attempt to produce the grain structure (size, shape, and distribution of sizes) that provides the maximum creep strength of this alloy at temperatures from 1250 to 1450 K. The effects of grain size, differences in oxygen concentrations, tungsten concentrations, and electron beam and gas tungsten arc weldments on creep strength were studied. Grain size has a large effect on creep strength at 1450 K but only material with a very large grain size (150 ?m) exhibits significantly higher creep strength at 1350 K. Differences in oxygen or tungsten concentrations did not affect creep strength, and the creep strengths of weldments were equal to, or greater than, those for base metal.

  4. Creep behavior of slate slopes explained with numerical modeling

    NASA Astrophysics Data System (ADS)

    Chang, K.-T.

    2012-04-01

    Geological structures such as folds, shearing and contortion of cleavage are commonly observed in the fields of slate slopes. These features may result from creep of gradual weathered rock slopes under gravity in long geological time. This study uses the finite element method to simulate the geological features in slate areas. The material behavior is described by a creep or an anisotropic model calibrated by the investigation of a landslide site in a slate area. Time and strength reduction with respect to the two material models cause deformation of slope models. The numerical modeling illuminates causes and processes of the creep behavior of rock slopes, which cannot be observed in short human life. The results show different creep patterns that are associated with different causes such as weathering near the slope surface and shearing or sliding along discontinuities in rock mass. Also, creep is more likely to appear in slopes with steeper or higher relief. The geological structures observed in the slate slopes can be explained by the numerical modeling and mechanics concepts.

  5. Continuous turbine blade creep measurement based on Moir

    NASA Astrophysics Data System (ADS)

    Liao, Yi; Tait, Robert; Harding, Kevin; Nieters, Edward J.; Hasz, Wayne C.; Piche, Nicole

    2012-11-01

    Moir imaging has been used to measure creep in the airfoil section of gas turbine blades. The ability to accurately assess creep and other failure modes has become an important engineering challenge, because gas turbine manufacturers are putting in place condition-based maintenance programs. In such maintenance programs, the condition of individual components is assessed to determine their remaining lives. Using pad-print technology, a grating pattern was printed directly on a turbine blade for localized creep detection using the spacing change of moir pattern fringes. A creep measurement prototype was assembled for this application which contained a lens, reference grating, camera and lighting module. This prototype comprised a bench-top camera system that can read moir patterns from the turbine blade sensor at shutdown to determine creep level in individual parts by analyzing the moir fringes. Sensitivity analyses and noise factor studies were performed to evaluate the system. Analysis software was also developed. A correlation study with strain gages was performed and the measurement results from the moir system align well with the strain gage readings. A mechanical specimen subjected to a one cycle tensile test at high temperature to induce plastic deformation in the gage was used to evaluate the system and the result of this test exhibited good correlation to extensometer readings.

  6. Creep behavior of Fe-bearing olivine under hydrous conditions

    NASA Astrophysics Data System (ADS)

    Tasaka, Miki; Zimmerman, Mark E.; Kohlstedt, David L.

    2015-09-01

    To understand the effect of iron content on the creep behavior of olivine, (MgxFe(1 - x))2SiO4, under hydrous conditions, we have conducted tri-axial compressive creep experiments on samples of polycrystalline olivine with Mg contents of x = 0.53, 0.77, 0.90, and 1. Samples were deformed at stresses of 25 to 320 MPa, temperatures of 1050 to 1200C, a confining pressure of 300 MPa, and a water fugacity of 300 MPa using a gas-medium high-pressure apparatus. Under hydrous conditions, our results yield the following expression for strain rate as a function of iron content for 0.53 ? x ? 0.90 in the dislocation creep regime: ??=??0.90((1-x/0.1))1/2exp[2261030.9-x/RT]. In this equation, the strain rate of San Carlos olivine, ??0.90, is a function of T, ?, and fH2O. As previously shown for anhydrous conditions, an increase in iron content directly increases creep rate. In addition, an increase in iron content increases hydrogen solubility and therefore indirectly increases creep rate. This flow law allows us to extrapolate our results to a wide range of mantle conditions, not only for Earth's mantle but also for the mantle of Mars.

  7. MOLECULAR DYNAMICS STUDY OF DIFFUSIONAL CREEP IN NANOCRYSTALLINE UO2

    SciTech Connect

    Tapan G. Desai; Paul C. Millett; Dieter Wolf

    2008-09-01

    We present the results of molecular dynamics (MD) simulations to study hightemperature deformation of nanocrystalline UO2. In qualitative agreement with experimental observations, the oxygen sub-lattice undergoes a structural transition at a temperature of about 2200 K (i.e., well below the melting point of 3450 K of our model system), whereas the uranium sub-lattice remains unchanged all the way up to melting. At temperatures well above this structural transition, columnar nanocrystalline model microstructures with a uniform grain size and grain shape were subjected to constantstress loading at levels low enough to avoid microcracking and dislocation nucleation from the GBs. Our simulations reveal that in the absence of grain growth, the material deforms via GB diffusion creep (also known as Coble creep). Analysis of the underlying self-diffusion behavior in undeformed nanocrystalline UO2 reveals that, on our MD time scale, the uranium ions diffuse only via the grain boundaries (GBs) whereas the much faster moving oxygen ions diffuse through both the lattice and the GBs. As expected for the Coble-creep mechanism, the creep activation energy agrees well with that for GB diffusion of the slowest moving species, i.e., of the uranium ions.

  8. Field theory and diffusion creep predictions in polycrystalline aggregates

    NASA Astrophysics Data System (ADS)

    Villani, A.; Busso, E. P.; Forest, S.

    2015-07-01

    In polycrystals, stress-driven vacancy diffusion at high homologous temperatures leads to inelastic deformation. In this work, a novel continuum mechanics framework is proposed to describe the strain fields resulting from such a diffusion-driven process in a polycrystalline aggregate where grains and grain boundaries are explicitly considered. The choice of an anisotropic eigenstrain in the grain boundary region provides the driving force for the diffusive creep processes. The corresponding inelastic strain rate is shown to be related to the gradient of the vacancy flux. Dislocation driven deformation is then introduced as an additional mechanism, through standard crystal plasticity constitutive equations. The fully coupled diffusion-mechanical model is implemented into the finite element method and then used to describe the biaxial creep behaviour of FCC polycrystalline aggregates. The corresponding results revealed for the first time that such a coupled diffusion-stress approach, involving the gradient of the vacancy flux, can accurately predict the well-known macroscopic strain rate dependency on stress and grain size in the diffusion creep regime. They also predict strongly heterogeneous viscoplastic strain fields, especially close to grain boundaries triple junctions. Finally, a smooth transition from Herring and Coble to dislocation creep behaviour is predicted and compared to experimental results for copper.

  9. Non-Contact Measurements of Creep Properties of Refractory Materials

    NASA Technical Reports Server (NTRS)

    Lee, Jonghyun; Bradshaw, Richard C.; Hyers, Robert W.; Rogers, Jan R.; Rathz, Thomas J.; Wall, James J.; Choo, Hahn; Liaw, Peter

    2006-01-01

    State-of-the-art technologies for hypersonic aircraft, nuclear electric/thermal propulsion for spacecraft, and more efficient jet engines are driving ever more demanding needs for high-temperature (>2000 C) materials. At such high temperatures, creep rises as one of the most important design factors to be considered. Since conventional measurement techniques for creep resistance are limited to about 17OO0C, a new technique is in demand for higher temperatures. This paper presents a non-contact method using electrostatic levitation (ESL) which is applicable to both metallic and non-metallic materials. The samples were rotated quickly enough to cause creep deformation by centrifugal acceleration. The deformation of the samples was captured with a high speed camera and then the images were analyzed to estimate creep resistance. Finite element analyses were performed and compared to the experiments to verify the new method. Results are presented for niobium and tungsten, representative refractory materials at 2300 C and 2700 C respectively.

  10. Creep-fatigue life prediction of in situ composite solders

    SciTech Connect

    Kuo, C.G.; Sastry, S.M.L.; Jerina, K.L.

    1995-12-01

    Eutectic tin-lead solder alloys subjected to cyclic loading at room temperature experience creep-fatigue interactions due to high homologous temperature. Intermetallic reinforcements of Ni{sub 3}Sn{sub 4} and Cu{sub 6}Sn{sub 5} are incorporated into eutectic tin-lead alloy by rapid solidification processes to form in situ composite solders. In this study, the in situ composite solders were subjected to combined creep and fatigue deformation at room temperature. Under cyclic deformation, the dominant damage mechanism of in situ composite solders is proposed to be growth of cavities. A constrained cavity growth model is applied to predict creep-fatigue life by taking into account the tensile loading component as well as the compressive loading component when reversed processes can occur. An algorithm to calculate cavity growth in each fatigue cycle is used to predict the number of fatigue cycles to failure, based on a critical cavity size of failure. Calculated lives are compared to experimental data under several fatigue histories, which include fully reversed stress-controlled fatigue, zero-tension stress-controlled fatigue, stress-controlled fatigue with tension hold time, fully reversed strain-controlled fatigue, and zero-tension strain-controlled fatigue. The model predicts the creep-fatigue lives within a factor of 2 with the incorporation of an appropriate compressive healing factor in most cases. Discrepancy between calculated lives and experimental results is discussed.

  11. Effects of NaCl, pH, and Potential on the Static Creep Behavior of AA1100

    NASA Astrophysics Data System (ADS)

    Wan, Quanhe; Quesnel, David J.

    2013-03-01

    The creep rates of AA1100 are measured during exposure to a variety of aggressive environments. NaCl solutions of various concentrations have no influence on the steady-state creep behavior, producing creep rates comparable to those measured in lab air at room temperature. However, after an initial incubation period of steady strain rate, a dramatic increase of strain rate is observed on exposure to HCl solutions and NaOH solutions, as well as during cathodic polarization of specimens in NaCl solutions. Creep strain produces a continuous deformation and elongation of the sample surface that is comparable to slow strain rates at crack tips thought to control the kinetics of crack growth during stress corrosion cracking (SCC). In this experiment, we separate the strain and surface deformation from the complex geometry of the crack tip to better understand the processes at work. Based on this concept, two possible explanations for the environmental influences on creep strain rates are discussed relating to the anodic dissolution of the free surface and hydrogen influences on deformation mechanisms. Consistencies of pH dependence between corrosion creep and SCC at low pH prove a creep-involved SCC mechanism, while the discrepancies between corrosion creep behavior and previous SCC results at high pH indicate a rate-limit step change in the crack propagation of the SCC process.

  12. Probability distributions for parameters of the Munson-Dawson salt creep model

    SciTech Connect

    Fossum, A.F.; Pfeifle, T.W.; Mellegard, K.D.

    1993-12-31

    Stress-related probability distribution functions are determined for the random variable material model parameters of the Munson-Dawson multi-mechanism deformation creep model for salt. These functions are obtained indirectly from experimental creep data for clean salt. The parameter distribution functions will form the basis for numerical calculations to generate an appropriate distribution function for room closure. Also included is a table that gives the values of the parameters for individual specimens of clean salt under different stresses.

  13. Elevated temperature deformation of TD-nickel base alloys

    NASA Technical Reports Server (NTRS)

    Petrovic, J. J.; Kane, R. D.; Ebert, L. J.

    1972-01-01

    Sensitivity of the elevated temperature deformation of TD-nickel to grain size and shape was examined in both tension and creep. Elevated temperature strength increased with increasing grain diameter and increasing L/D ratio. Measured activation enthalpies in tension and creep were not the same. In tension, the internal stress was not proportional to the shear modulus. Creep activation enthalpies increased with increasing L/D ratio and increasing grain diameter, to high values compared with that of the self diffusion enthalpy. It has been postulated that two concurrent processes contribute to the elevated temperature deformation of polycrystalline TD-nickel: (1) diffusion controlled grain boundary sliding, and (2) dislocation motion.

  14. Experimental and Numerical Studies on Mudstone's Creep Behavior During Water Injection and Its Effect on Casing Damage

    NASA Astrophysics Data System (ADS)

    Huang, X. L.; Yang, C. H.; Liu, J. J.; He, X.; Xiong, J.

    2008-07-01

    During the process of water injection production in oilfield, when water cuts into the mudstone, as a result, large numbers of casings are damaged because of mudstone's creep characteristic. In order to analyze this phenomenon, the uniaxial compression experiments and creep experiments of mudstone from Daqing Oil Field under different saturation conditions were done, it was studied that how the mudstone's mechanical parameters and creep characteristic would change with the increment of water contents. The results indicate that the rock strength and elastic modulus are decreased rapidly with the increment of water contents, on the other hand, the creep strain and steady state creep strain rate are increased with the increment of water contents, and also the steady state creep strain rate is enhanced with the increment of deviatoric stress. Through the creep characteristic curves, a nonlinear creeping constitutive equation of mudstone considering the changes of water contents was established. In the deep stratum of the oilfield, the calculation model of casing-cement sheath-mudstone was built, based on the experiment results of mudstone and its creep constitutive equation, mudstone's creep pressure with time under different water contents was simulated. The simulation results show that the increasing water content accelerates the incremental rate of the creep pressure of mudstone, so the time of reaching yield state of casing will descend greatly, which means service time of casing becomes much shorter.

  15. Non-contact Creep Resistance Measurement for Ultra-High Temperature Materials

    NASA Technical Reports Server (NTRS)

    Lee, J.; Bradshaw, C.; Rogers, J. R.; Rathz, T. J.; Wall, J. J.; Choo, H.; Liaw, P. K.; Hyers, R. W.

    2005-01-01

    Conventional techniques for measuring creep are limited to about 1700 C, so a new technique is required for higher temperatures. This technique is based on electrostatic levitation (ESL) of a spherical sample, which is rotated quickly enough to cause creep deformation by centrifugal acceleration. Creep of samples has been demonstrated at up to 2300 C in the ESL facility at NASA MSFC, while ESL itself has been applied at over 3000 C, and has no theoretical maximum temperature. The preliminary results and future directions of this NASA-funded research collaboration will be presented.

  16. Long-term performance of ceramic matrix composites at elevated temperatures: Modelling of creep and creep rupture

    SciTech Connect

    Curtin, W.A.; Fabeny, B.; Ibnabdeljalil, M.; Iyengar, N.; Reifsnider, K.L.

    1996-07-31

    The models developed, contain explicit dependences on constituent material properties and their changes with time, so that composite performance can be predicted. Three critical processes in ceramic composites at elevated temperatures have been modeled: (1) creep deformation of composite vs stress and time-dependent creep of fibers and matrix, and failure of these components; (2) creep deformation of ``interface`` around broken fibers; and (3) lifetime of the composite under conditions of fiber strength loss over time at temperature. In (1), general evolution formulas are derived for relaxation time of matrix stresses and steady-state creep rate of composite; the model is tested against recent data on Ti-MMCs. Calculations on a composite of Hi-Nicalon fibers in a melt-infiltrated SiC matrix are presented. In (2), numerical simulations of composite failure were made to map out time-to-failure vs applied load for several sets of material parameters. In (3), simple approximate relations are obtained between fiber life and composite life that should be useful for fiber developers and testers. Strength degradation data on Hi-Nicalon fibers is used to assess composite lifetime vs fiber lifetime for Hi-Nicalon fiber composites.

  17. Rate- and strain-dependent brittle deformation of rocks

    NASA Astrophysics Data System (ADS)

    Brantut, N.; Heap, M. J.; Baud, P.; Meredith, P. G.

    2014-03-01

    We develop a unifying framework to quantify rate-dependent deformation in the brittle field and establish links between the microscale time-dependent crack growth processes and the macroscopically observed rate dependency. Triaxial deformation experiments have been performed under both constant strain rate and constant stress (creep) conditions on three types of sandstone. The measured relative evolution of P wave speeds as a function of inelastic axial strain is similar for both types of test, despite differences in strain rate of up to 3 orders of magnitude. This similarity indicates that there exists a direct, time-independent link between the microstructural state (as reflected by the variations in P wave speed) and the inelastic axial strain. Comparison of applied stresses between constant strain rate and creep experiments as a function of inelastic strain indicates that creep deformation requires less mechanical work to bring the sample to failure. This energy deficit corresponds to a stress deficit, which can be related to a deficit in energy release rate of the microcracks. We establish empirically that the creep strain rate is given by ???exp(?Q/??), where ?Q is the stress deficit (negative) and ?? is an activation stress. This empirical exponential relation between creep strain rate and stress deficit is analogous to rate-and-state friction law. We develop a micromechanical approach based on fracture mechanics to determine the evolution of an effective stress intensity factor at crack tips during creep deformation and estimate the activation volume of the stress corrosion reaction responsible for brittle creep.

  18. Mechanisms of time-dependent deformation in porous limestone

    NASA Astrophysics Data System (ADS)

    Brantut, Nicolas; Heap, Michael J.; Baud, Patrick; Meredith, Philip G.

    2014-07-01

    We performed triaxial deformation experiments on a water-saturated porous limestone under constant strain rate and constant stress (creep) conditions. The tests were conducted at room temperature and at low effective pressures Peff=10 and Peff=20 MPa, in a regime where the rock is nominally brittle when tested at a constant strain rate of 10-5 s-1. Under these conditions and at constant stress, the phenomenon of brittle creep occurs. At Peff=10 MPa, brittle creep follows similar trends as those observed in other rock types (e.g., sandstones and granites): only small strains are accumulated before failure, and damage accumulation with increasing strain (as monitored by P wave speeds measurements during the tests) is not strongly dependent on the applied stresses. At Peff=20 MPa, brittle creep is also macroscopically observed, but when the creep strain rate is lower than ?10-7 s-1, we observe that (1) much larger strains are accumulated, (2) less damage is accumulated with increasing strain, and (3) the deformation tends to be more compactant. These observations can be understood by considering that another deformation mechanism, different from crack growth, is active at low strain rates. We explore this possibility by constructing a deformation mechanism map that includes both subcritical crack growth and pressure solution creep processes; the increasing contribution of pressure solution creep at low strain rates is consistent with our observations.

  19. On the determination of vortex creep parameters in superconductors using standard magnetization relaxation data

    NASA Astrophysics Data System (ADS)

    Ivan, I.; Miu, D.; Popa, S.; Jakob, G.; Miu, L.

    2011-09-01

    The relaxation of the irreversible magnetic moment m(t) in YBa2Cu3O7 (YBCO) films was investigated as a function of temperature T and the external magnetic field H along the c axis applied in zero-field cooling conditions, for the determination of vortex creep parameters. The data analysis was performed using the T and current density dependence of the normalized vortex creep activation energy, or by the fit of the m(t) data with the well known interpolation formula in the framework of the general vortex creep equation. It was found that (i) even for specimens with strong static pinning the characteristic pinning energy remains small in the low-T range, where the vortex creep appearing in standard magnetization measurements is elastic, (ii) the observed strong increase of the time scale for creep and the decrease of the creep exponent with increasing H beyond the theoretical predictions can be attributed to the crossover elastic-creep-plastic-creep generated by the macroscopic currents induced in the specimen during magnetization measurements, and (iii) the creep parameters extracted with the interpolation formula are highly affected by the m(t) data registered at short t, which may lead to unphysical creep parameter values.

  20. A deformation-mechanism material model for NIKE 3-D

    SciTech Connect

    Raboin, P.J.

    1993-01-04

    The structural, finite element code, NIKE2D has a, new material model called the Deformation-Mechanism Model (DMM). This model uses kinetic equations to predict deformation rates for specific deformation-mechanisms. These mechanisms depend on temperature, applied stress, a strength parameter and grain size. Five kinetic equations are available, and they model Obstacle Controlled Plasticity, Power Law Creep, Power Law Breakdown, Diffusion Controlled Deformation and Slip Creep. A strength parameter models isotropic strain hardening and dynamic recovery. Grain size changes are modeled with a dynamic grain growth equation which depends on temperature, current grain size and the deformation rate. These kinetic equations and their evolutionary parameters are capable of predicting rate-dependent deformation behavior for many metals. In addition, multiple deformation-mechanisms can be combined in this material model to predict the rate dependent behavior of a material across several regimes of deformation behavior.

  1. Deformation mechanisms and grain size evolution in the Bohemian granulites - a computational study

    NASA Astrophysics Data System (ADS)

    Maierova, Petra; Lexa, Ondrej; Je?bek, Petr; Fran?k, Jan; Schulmann, Karel

    2015-04-01

    A dominant deformation mechanism in crustal rocks (e.g., dislocation and diffusion creep, grain boundary sliding, solution-precipitation) depends on many parameters such as temperature, major minerals, differential stress, strain rate and grain size. An exemplary sequence of deformation mechanisms was identified in the largest felsic granulite massifs in the southern Moldanubian domain (Bohemian Massif, central European Variscides). These massifs were interpreted to result from collision-related forced diapiric ascent of lower crust and its subsequent lateral spreading at mid-crustal levels. Three types of microstructures were distinguished. The oldest relict microstructure (S1) with large grains (>1000 ?m) of feldspar deformed probably by dislocation creep at peak HT eclogite facies conditions. Subsequently at HP granulite-facies conditions, chemically- and deformation- induced recrystallization of feldspar porphyroclasts led to development of a fine-grained microstructure (S2, ~50 ?m grain size) indicating deformation via diffusion creep, probably assisted by melt-enhanced grain-boundary sliding. This microstructure was associated with flow in the lower crust and/or its diapiric ascent. The latest microstructure (S3, ~100 ?m grain size) is related to the final lateral spreading of retrograde granulites, and shows deformation by dislocation creep at amphibolite-facies conditions. The S2-S3 switch and coarsening was interpreted to be related with a significant decrease in strain rate. From this microstructural sequence it appears that it is the grain size that is critically linked with specific mechanical behavior of these rocks. Thus in this study, we focused on the interplay between grain size and deformation with the aim to numerically simulate and reinterpret the observed microstructural sequence. We tested several different mathematical descriptions of the grain size evolution, each of which gave qualitatively different results. We selected the two most elaborated and at the same time the most promising descriptions: thermodynamics-based models with and without Zener pinning. For conditions compatible with the S1 and S2 microstructures (~800 C and strain rate ~10-13 s-1), the calculated stable grain sizes are ~30 ?m and >300 ?m in the models with and without Zener pinning, respectively. This is in agreement with the contrasting grain sizes associated with S1 and S2 microstructures implying that mainly chemically induced recrystallization of S1 feldspar porphyroclasts must had played a fundamental role in the transition into the diffusion creep. The model with pinning also explains only minor changes of mean grain size associated with S2 microstructure. The S2-S3 switch from the diffusion to dislocation creep is difficult to explain when assuming reasonable temperature and strain rate (or stress). However, a simple incorporation of the effect of melt solidification into the model with pinning can mimic this observed switch. Besides the above mentioned simple models with prescribed temperature and strain rate, we implemented the grain size evolution laws into in a 2D thermo-mechanical model setup, where stress, strain rate and temperature evolve in a more natural manner. This setup simulates a collisional evolution of an orogenic root with anomalous lower crust. The lower-crustal material is a source region for diapirs and it deforms via a combination of dislocation and grain-size-sensitive creeps. We tested the influence of selected parameters in the flow laws and in the grain-size evolution laws on the shape and other characteristics of the growing diapirs. The outputs of our simulations were then compared with the geological record from the Moldanubian granulite massifs.

  2. Effect of interconnect creep on long-term performance of SOFC of one cell stacks

    SciTech Connect

    Liu, Wenning N.; Sun, Xin; Khaleel, Mohammad A.

    2008-02-01

    Creep deformation becomes relevant for a material when the operating temperature is near or exceeds half of its melting temperature (in degrees of Kelvin). The operating temperatures for most of the solid oxide fuel cells (SOFC) under development in the SECA program are around 1073oK. High temperature ferritic alloys are potential candidates as interconnect (IC) materials and spacers due to their low cost and CTE compatibility with other SOFC components. Since the melting temperature of most stainless steel is around 1800oK, possible creep deformation of IC under the typical cell operating temperature should not be neglected. In this paper, the effects of interconnect creep behavior on stack geometry change and stress redistribution of different cell components are predicted and summarized. The goal of the study is to investigate the performance of the fuel cell stack by obtaining the fuel and air channel geometry changes due to creep of the ferritic stainless steel interconnect, therefore indicating possible SOFC performance change under long term operations. IC creep models were incorporated into SOFC-MP and Mentat FC, and finite element analyses were performed to quantify the deformed configuration of the SOFC stack under the long term steady state operating temperature. It is found that creep behavior of the ferritic stainless steel IC contributes to narrowing of both the fuel and the air flow channels. In addition, stress re-distribution of the cell components suggests the need for a compliant sealing material that also relaxes at operating temperature.

  3. Deformation behavior of particle-strengthened alloys: A Voronoi mesh approach

    SciTech Connect

    Estrin, Y.; Arndt, S.; Heilmaier, M.; Brechet, Y.

    1999-01-15

    A modelling approach based on the discretization of a particle-strengthened material using a Voronoi mesh is considered. The model is applied to studying the effects of particle arrangement on the deformation behavior of a particle-strengthened alloy, particularly on its creep resistance. On a local scale, i.e., within an individual Voronoi cell containing a single particle, a dislocation density-based constitutive model developed previously is applied. Interaction with adjacent Voronoi cells due to plastic incompatibilities is also included. The model predicts a dependence of the creep resistance on the character of particle distribution, notably, on the degree of particle clustering. Application to oxide dispersion strengthened (ODS) nickel-base alloys MA 754 and PM 1000, which are very similar in their metallurgical characteristics, including the volume fraction of oxide dispersoids, but differ in the dispersoid arrangement, shows an excellent predictive capability of the Voronoi mesh modelling technique.

  4. Autonomous Repair Mechanism of Creep Damage in Fe-Au and Fe-Au-B-N Alloys

    NASA Astrophysics Data System (ADS)

    Zhang, S.; Kwakernaak, C.; Tichelaar, F. D.; Sloof, W. G.; Kuzmina, M.; Herbig, M.; Raabe, D.; Brck, E.; van der Zwaag, S.; van Dijk, N. H.

    2015-12-01

    The autonomous repair mechanism of creep cavitation during high-temperature deformation has been investigated in Fe-Au and Fe-Au-B-N alloys. Combined electron-microscopy techniques and atom probe tomography reveal how the improved creep properties result from Au precipitation within the creep cavities, preferentially formed on grain boundaries oriented perpendicular to the applied stress. The selective precipitation of Au atoms at the free creep cavity surface results in pore filling, and thereby, autonomous repair of the creep damage. The large difference in atomic size between the Au and Fe strongly hampers the nucleation of precipitates in the matrix. As a result, the matrix acts as a reservoir for the supersaturated solute until damage occurs. Grain boundaries and dislocations are found to act as fast transport routes for solute gold from the matrix to the creep cavities. The mechanism responsible for the self-healing can be characterized by a simple model for cavity growth and cavity filling.

  5. Creep-Fatigue Interaction Testing

    NASA Technical Reports Server (NTRS)

    Halford, Gary R.

    2001-01-01

    Fatigue fives in metals are nominally time independent below 0.5 T(sub Melt). At higher temperatures, fatigue lives are altered due to time-dependent, thermally activated creep. Conversely, creep rates are altered by super. imposed fatigue loading. Creep and fatigue generally interact synergistically to reduce material lifetime. Their interaction, therefore, is of importance to structural durability of high-temperature structures such as nuclear reactors, reusable rocket engines, gas turbine engines, terrestrial steam turbines, pressure vessel and piping components, casting dies, molds for plastics, and pollution control devices. Safety and lifecycle costs force designers to quantify these interactions. Analytical and experimental approaches to creep-fatigue began in the era following World War II. In this article experimental and life prediction approaches are reviewed for assessing creep-fatigue interactions of metallic materials. Mechanistic models are also discussed briefly.

  6. Creep cavitation bands control porosity and fluid flow in lower crustal shear zones

    SciTech Connect

    Menegon, Luca; Fusseis, Florian; Stunitz, Holger; Xiao, Xianghui

    2015-03-01

    Shear zones channelize fluid flow in Earth’s crust. However, little is known about deep crustal fluid migration and how fluids are channelized and distributed in a deforming lower crustal shear zone. This study investigates the deformation mechanisms, fluid-rock interaction, and development of porosity in a monzonite ultramylonite from Lofoten, northern Norway. The rock was deformed and transformed into an ultramylonite under lower crustal conditions (temperature = 700–730 °C, pressure = 0.65–0.8 GPa). The ultramylonite consists of feldspathic layers and domains of amphibole + quartz + calcite, which result from hydration reactions of magmatic clinopyroxene. The average grain size in both domains is <25 mm. Microstructural observations and electron backscatter diffraction analysis are consistent with diffusion creep as the dominant deformation mechanism in both domains. Festoons of isolated quartz grains define C'-type bands in feldspathic layers. These quartz grains do not show a crystallographic preferred orientation. The alignment of quartz grains is parallel to the preferred elongation of pores in the ultramylonites, as evidenced from synchrotron X-ray microtomography. Such C'-type bands are interpreted as creep cavitation bands resulting from diffusion creep deformation associated with grain boundary sliding. Mass-balance calculation indicates a 2% volume increase during the protolith-ultramylonite transformation, which is consistent with synkinematic formation of creep cavities producing dilatancy. Thus, this study presents evidence that creep cavitation bands may control deep crustal porosity and fluid flow. Nucleation of new phases in creep cavitation bands inhibits grain growth and enhances the activity of grain size–sensitive creep, thereby stabilizing strain localization in the polymineralic ultramylonites.

  7. Brittle creep and subcritical crack propagation in glass submitted to triaxial conditions

    NASA Astrophysics Data System (ADS)

    Mallet, Céline; Fortin, Jérôme; Guéguen, Yves; Bouyer, Frédéric

    2015-02-01

    An experimental work is presented that aimed at improving our understanding of the mechanical evolution of cracks under brittle creep conditions. Brittle creep may be an important slow deformation process in the Earth's crust. Synthetic glass samples have been used to observe and document brittle creep due to slow crack-propagation. A crack density of 0.05 was introduced in intact synthetic glass samples by thermal shock. Creep tests were performed at constant confining pressure (15 MPa) for water saturated conditions. Data were obtained by maintaining the differential-stress constant in steps of 24 h duration. A set of sensors allowed us to record strains and acoustic emissions during creep. The effect of temperature on creep was investigated from ambient temperature to 70°C. The activation energy for crack growth was found to be 32 kJ/mol. In secondary creep, a large dilatancy was observed that did not occur in constant strain rate tests. This is correlated to acoustic emission activity associated with crack growth. As a consequence, slow crack growth has been evidenced in glass. Beyond secondary creep, failure in tertiary creep was found to be a progressive process. The data are interpreted through a previously developed micromechanical damage model that describes crack propagation. This model allows one to predict the secondary brittle creep phase and also to give an analytical expression for the time to rupture. Comparison between glass and crystalline rock indicates that the brittle creep behavior is probably controlled by the same process even if stress sensitivity for glass is lower than for rocks.

  8. Irradiation Creep of Chemically Vapor Deposited Silicon Carbide as Estimated by Bend Stress Relaxation Method

    SciTech Connect

    Katoh, Yutai; Snead, Lance Lewis; Hinoki, Tatsuya; Kondo, Sosuke; Kohyama, Akira

    2007-01-01

    The bend stress relaxation technique was applied for an irradiation creep study of high purity, chemically vapor-deposited beta-phase silicon carbide (CVD SiC) ceramic. A constant bend strain was applied to thin strip samples during neutron irradiation to fluences 0.2-4.2 dpa at various temperatures in the range {approx}400 to {approx}1080 C. Irradiation creep strain at <0.7 dpa exhibited only a weak dependence on irradiation temperature. However, the creep strain dependence on fluence was non-linear due to the early domination of the initial transient creep, and a transition in creep behavior was found between 950 and 1080 C. Steady-state irradiation creep compliances of polycrystalline CVD SiC at doses >0.7 dpa were estimated to be 2.7({+-}2.6) x 10{sup -7} and 1.5({+-}0.8) x 10{sup -6} (MPa dpa){sup -1} at {approx}600 to {approx}950 C and {approx}1080 C, respectively, whereas linear-averaged creep compliances of 1-2 x 10{sup -6} (MPa dpa){sup -1} were obtained for doses of 0.6-0.7 dpa at all temperatures. Monocrystalline 3C SiC samples exhibited significantly smaller transient creep strain and greater subsequent deformation when loaded along <0 1 1> direction.

  9. Elevated temperature creep properties of the 54Fe-29Ni-17Co "Kovar" alloy.

    SciTech Connect

    Stephens, John Joseph, Jr.; Rejent, Jerome Andrew; Schmale, David T.

    2009-01-22

    The outline of this presentation is: (1) Applications of Kovar Alloy in metal/ceramic brazing; (2) Diffusion bonding of precision-photoetched Kovar parts; (3) Sample composition and annealing conditions; (4) Intermediate temperature creep properties (350-650 C); (5) Power law creep correlations--with and without modulus correction; (6) Compressive stress-strain properties (23-900 C); (7) Effect of creep deformation on grain growth; and (8) Application of the power law creep correlation to the diffusion bonding application. The summary and conclusions are: Elevated temperature creep properties of Kovar from 750-900 C obey a power law creep equation with a stress exponent equal to 4.9, modulus compensated activation energy of 47.96 kcal/mole. Grain growth in Kovar creep samples tested at 750 and 800 C is quite sluggish. Significant grain growth occurs at 850 C and above, this is consistent with isothermal grain growth studies performed on Kovar alloy wires. Finite element analysis of the diffusion bonding of Kovar predict that stresses of 30 MPa and higher are needed for good bonding at 850 C, we believe that 'sintering' effects must be accounted for to allow FEA to be predictive of actual processing conditions. Additional creep tests are planned at 250-650 C.

  10. Extended-time-scale creep measurement on Maraging cantilever blade springs

    NASA Astrophysics Data System (ADS)

    Virdone, Nicole; Agresti, Juri; Bertolini, Alessandro; DeSalvo, Riccardo; Stellacci, Rosalia; Kamp, Justin; Mantovani, Maddalena; Sannibale, Virginio; Tarallo, Marco; Kaltenegger, Lisa

    2008-08-01

    Two controlled temperature facilities were built to induce an accelerated creep rate in a Maraging steel GAS spring and to measure the material's creep over an artificially extended period of time. The data acquisition of the first experiment lasted for almost a year, but then the blades were allowed to creep for six more years before measuring the permanent deformation integrated over time. The data from this first experiment was polluted by a defect in the data acquisition software, but yielded overall creep limits and an evaluation of the Arrhenius acceleration of creep speed with temperature (1.28±0.13 °C -1). The duration of the second experiment was only 1 year but more free of systematic errors. The effective test period of this second experiment (normalized with the Arrhenius acceleration measured in the first experiment) extends in billions of years showing no sign of anomalous creep. The result of both experiments also produced a simple procedure capable of eliminating all practical effects of creep from the Advanced LIGO seismic isolation and suspensions. Measurements of creep under various stress levels, and of the thermal variations of Young's modulus (2.023 (±0.013)×10 -4 °C -1) are reported as well.

  11. Creep of a Silicon Nitride Under Various Specimen/Loading Configurations

    NASA Technical Reports Server (NTRS)

    Choi, Sung R.; Powers, Lynn M.; Holland, Frederic A.; Gyekenyesi, John P.; Holland, F. A. (Technical Monitor)

    2000-01-01

    Extensive creep testing of a hot-pressed silicon nitride (NC132) was performed at 1300 C in air using five different specimen/loading configurations, including pure tension, pure compression, four-point uniaxial flexure, ball-on-ring biaxial flexure, and ring-on-ring biaxial flexure. Nominal creep strain and its rate for a given nominal applied stress were greatest in tension, least in compression, and intermediate in uniaxial and biaxial flexure. Except for the case of compressive loading, nominal creep strain generally decreased with time, resulting in less-defined steady-state condition. Of the four different creep formulations - power-law, hyperbolic sine, step, redistribution models - the conventional power-law model still provides the most convenient and reasonable means to estimate simple, quantitative creep parameters of the material. Predictions of creep deformation for the case of multiaxial stress state (biaxial flexure) were made based on pure tension and compression creep data by using the design code CARES/Creep.

  12. Fragmentation of {alpha}{sub 2} plates in a fully lamellar TiAl during creep

    SciTech Connect

    Wang, J.G.; Hsiung, L.M.; Nieh, T.G.

    1999-07-01

    The fragmentation and spheroidization of {alpha}{sub 2} laths in a fully-lamellar TiAl alloy during creep were examined. Three possible mechanisms, Rayleigh's perturbation model, subgrain boundary groove mechanism and intersection of deformation twins with {alpha}{sub 2} lamellae were presented and discussed. During creep deformation, the pile-up of interfacial dislocations leads to a change of planar interface, which, in turn, causes a difference in local chemical potential, and further results in the spheroidization of {alpha}{sub 2} lamellae. On the other hand, the deformation of the {alpha}{sub 2} phase is expected to be induced by the high local stress concentration introduced by the pile up of interfacial dislocations. The dynamic recovery process may lead to the formation of subgrain boundaries in the {alpha}{sub 2} lamellae, which results in the spheroidization and termination of {alpha}{sub 2} lamellae with the aid of diffusion during creep.

  13. Citation Characteristics of Research Articles under the Center of Cleft Lip-Cleft Palate and Craniofacial Deformities, Khon Kaen University.

    PubMed

    Thanapaisal, Soodjai; Thanapaisal, Chaiwit; Thanapaisal, Sukhumal

    2015-08-01

    Center of Cleft Lip-Cleft Palate and Craniofacial Deformities, Khon Kaen University, has cooperated with the Medical Association of Thailand in publishing the special five issues of JMT (Journal of the Medical Association of Thailand) during the years 2010-2014 in order to promote research activities and working network of related fields in cleft lip-cleft palate and craniofacial deformities. This study aimed to examine the features of 106 research articles in terms of authors and disciplines, and analyze the citations considering sources, country and years after publication. The scope of study also included citations in the form of journal, which was presented as journal ranking compared with impact factors and Bradford's Law on journal citation. The results of study will be useful in developing multidisciplinary research activities of the center and especially assist in the acquisition of academic journals for essential sources of reference. PMID:26742377

  14. The Effects of Ferrite Content and Morphology on the Mechanical Properties and Room Temperature Creep of Quenched and Tempered SAE 4340 Steel

    NASA Astrophysics Data System (ADS)

    Liu, Cheng; Bhole, Sanjiwan; Northwood, Derek

    The room temperature creep behavior is investigated for a commercial SAE 4340 steel containing small amounts of ferrite. Significant creep deformation occurs at stress levels below 1/3 ?0.2 (The yield strength at 0.2% offset strain). Small amounts of ferrite (0% to 4%) have no influence on the hardness and yield strength. However, these small amounts of ferrite play an important role in controlling the creep resistance. The presence of any ferrite leads to a reduction in the creep resistance. The creep deformation at room temperature increases with an increase in the amount of ferrite. The effects of ferrite morphology and an inhomogeneous microstructure on the creep resistance are discussed.

  15. Roof Deformation, Failure Characteristics, and Preventive Techniques of Gob-Side Entry Driving Heading Adjacent to the Advancing Working Face

    NASA Astrophysics Data System (ADS)

    Bai, Jian-biao; Shen, Wen-long; Guo, Guan-long; Wang, Xiang-yu; Yu, Yang

    2015-11-01

    In mining excavation, the roof bending subsidence of gob-side entry driving heading adjacent to the advancing working face (HAWF) can be considerable. Influenced by the original rock pressure, the front and lateral abutment pressure of the adjacent working face, and the front abutment pressure of the current working face, the support body can easily fail, leading to serious instability of the rock mass surrounding the tunnel. To study the stress state and the deformation failure mechanism of the HAWF roof structure, we use on-site survey data, numerical simulation, and theoretical calculations to fit the spatial distribution law of mining abutment pressure piecewise, and establish a dynamic mechanical model of the roof structure. We then propose a roof failure criterion and examine the roof flexure deformation behavioral pattern. We found that the central part of the roof is the main point that controls the surrounding rock. To prevent the deformation and collapse of the roof and rock surrounding the tunnel, we propose techniques that can be applied to HAWF gob-side entry driving, including setting the coal pillar width, the driving stop and restart timing, and other control concepts.

  16. Creep in Topopah Spring Member welded tuff. Yucca Mountain Site Characterization Project

    SciTech Connect

    Martin, R.J. III; Boyd, P.J.; Noel, J.S.; Price, R.H.

    1995-06-01

    A laboratory investigation has been carried out to determine the effects of elevated temperature and stress on the creep deformation of welded tuffs recovered from Busted Butte in the vicinity of Yucca Mountain, Nevada. Water saturated specimens of tuff from thermal/mechanical unit TSw2 were tested in creep at a confining pressure of 5.0 MPa, a pore pressure of 4.5 MPa, and temperatures of 25 and 250 C. At each stress level the load was held constant for a minimum of 2.5 {times} 10{sup 5} seconds and for as long as 1.8 {times} 10{sup 6} seconds. One specimen was tested at a single stress of 80 MPa and a temperature of 250 C. The sample failed after a short time. Subsequent experiments were initiated with an initial differential stress of 50 or 60 MPa; the stress was then increased in 10 MPa increments until failure. The data showed that creep deformation occurred in the form of time-dependent axial and radial strains, particularly beyond 90% of the unconfined, quasi-static fracture strength. There was little dilatancy associated with the deformation of the welded tuff at stresses below 90% of the fracture strength. Insufficient data have been collected in this preliminary study to determine the relationship between temperature, stress, creep deformation to failure, and total failure time at a fixed creep stress.

  17. High temperature indentation creep tests on anhydrite - a promising first look

    NASA Astrophysics Data System (ADS)

    Dorner, D.; Rller, K.; Stckhert, B.

    2014-08-01

    Indentation creep tests are established in materials engineering, providing information on rheology, deformation mechanisms, and related microstructures of materials. Here we explore the potential of this method on natural, polycrystalline anhydrite. The tests are run at atmospheric pressure, temperatures between 700 and 920 C, and reference stresses between 7 and 30 MPa. An activation energy Q of 338 kJ mol-1 and a stress exponent n of 3.9 are derived. Deformation is localized into shear zones bounding a less deformed approximately conical plug underneath the indenter. Shear zone microstructures reveal inhomogeneous crystal-plastic deformation, subgrains, and extensive strain-induced grain boundary migration, while mechanical twinning appears not to be activated. Microstructure and mechanical data are consistent with deformation by dislocation creep.

  18. High temperature indentation creep tests on anhydrite - a promising first look

    NASA Astrophysics Data System (ADS)

    Dorner, D.; Rller, K.; Stckhert, B.

    2013-11-01

    Indentation creep tests are established in materials engineering, providing information on rheology, deformation mechanisms, and related microstructures of materials. Here we explore the potential of this method on natural, polycrystalline anhydrite. The tests are run at atmospheric pressure, temperatures between 700 C and 920 C, and reference stresses between 7 MPa and 30 MPa. An activation energy Q of 338 kJ mol-1 and a stress exponent n of 3.9 are derived. Deformation is localized into shear zones bounding a less deformed approximately conical plug underneath the indenter. Shear zone microstructures reveal inhomogeneous crystal plastic deformation, subgrains, and extensive strain induced grain boundary migration, while mechanical twinning appears not to be activated. Microstructure and mechanical data are consistent with deformation by dislocation creep. Extrapolated to slow natural strain rates, the flow law predicts a high flow strength of anhydrite compared to previous studies.

  19. Variational principles and optimal solutions of the inverse problems of creep bending of plates

    NASA Astrophysics Data System (ADS)

    Bormotin, K. S.; Oleinikov, A. I.

    2012-09-01

    It is shown that inverse problems of steady-state creep bending of plates in both the geometrically linear and nonlinear formulations can be represented in a variational formulation. Steady-state values of the obtained functionals corresponding to the solutions of the problems of inelastic deformation and elastic unloading are determined by applying a finite element procedure to the functionals. Optimal laws of creep deformation are formulated using the criterion of minimizing damage in the functionals of the inverse problems. The formulated problems are reduced to the problems solved by the finite element method using MSC.Marc software.

  20. Back stress in dislocation creep. Part 1: Basic concepts and measuring techniques

    NASA Technical Reports Server (NTRS)

    Cadek, J.

    1984-01-01

    A theory is proposed whereby the plastic deformation of metal materials is determined by the difference between the applied stress and the back stress which characterizes the resistance of the material to plastic deformation. The back stress is usually equivalent to the internal stress or the friction stress and depends on the magnitude of the applied stress and temperature. The concept of back stress is applied to the case of the dislocation creep of precipitation-hardened or dispersion-strengthened metal materials. An additivity rule is formulated which can be useful in interpreting the creep behavior of such materials.

  1. Water weakening of clinopyroxene in the dislocation creep regime

    NASA Astrophysics Data System (ADS)

    Chen, S.; Hiraga, T.; Kohlstedt, D. L.

    2006-08-01

    We performed a series of triaxial compressive creep experiments at two different water fugacities to investigate the effect of water on the creep strength of a natural clinopyroxenite. Samples were deformed under water-saturated conditions at temperatures between 1373 and 1473 K, confining pressures of 150 and 300 MPa, and differential stresses from 34 to 261 MPa. Strain rates were in the range 10-7 to 10-5 s-1. Water fugacity was controlled at either 140 or 280 MPa. The creep results yield a stress exponent of 2.7 0.3 and an activation energy of 670 40 kJ/mol. Compared to dry clinopyroxene, wet samples creep over 100 times faster at a given temperature, confining pressure, water fugacity, and differential stress. The creep rate of clinopyroxene is proportional to the water fugacity to the 3.0 0.6 power, with an activation volume of 0 m3/mol. One possible water-weakening mechanism is an enhancement of the rate of dislocation climb associated with increases in the concentration of jogs and the diffusivity of silicon ions. Compared to other major minerals in Earth's lower crust, specifically olivine and plagioclase, the water-weakening effect is most significant for clinopyroxene. Under hydrous conditions the strengths of clinopyroxene and anorthite are comparable over the investigated stress range, and both phases are weaker than olivine. Since the mineral assemblages in Earth's lower continental crust are often dominated by plagioclase and pyroxene, in places where a wet flow law applies, the mechanical behavior of clinopyroxene will have a substantial effect on creep strength.

  2. High temperature creep resistant austenitic alloy

    DOEpatents

    Maziasz, Philip J.; Swindeman, Robert W.; Goodwin, Gene M.

    1989-01-01

    An improved austenitic alloy having in wt % 19-21 Cr, 30-35 Ni, 1.5-2.5 Mn, 2-3 Mo, 0.1-0.4 Si, 0.3-0.5 Ti, 0.1-0.3 Nb, 0.1-0.5 V, 0.001-0.005 P, 0.08-0.12 C, 0.01-0.03 N, 0.005-0.01 B and the balance iron that is further improved by annealing for up to 1 hour at 1150.degree.-1200.degree. C. and then cold deforming 5-15 %. The alloy exhibits dramatically improved creep rupture resistance and ductility at 700.degree. C.

  3. Defect-mediated creep of structured materials

    NASA Astrophysics Data System (ADS)

    Colby, R. H.; Nentwich, L. M.; Clingman, S. R.; Ober, C. K.

    2001-04-01

    Low-stress creep measurements on a nematic liquid crystal polymer indicate that it is a viscoelastic solid, with a modulus of 100dynes/cm2 and a yield stress of 50dynes/cm2. Both smectics and nematics are viscoelastic solids at very low stress levels, with a modulus that is related to their defect texture. At stress levels somewhat above the yield stress, there is a yielding regime where the deformation rate and defect spacing are power laws in the applied stress. We understand these power laws using the ideas developed long ago by Orowan for the motion of line defects in crystalline solids. The exponents of these power laws are different for nematics and smectics, but the nematic universality class also appears to apply to superplastic metals and ceramics.

  4. Improved high temperature creep resistant austenitic alloy

    DOEpatents

    Maziasz, P.J.; Swindeman, R.W.; Goodwin, G.M.

    1988-05-13

    An improved austenitic alloy having in wt% 19-21 Cr, 30-35 Ni, 1.5-2.5 Mn, 2-3 Mo, 0.1-0.4 Si, 0.3-0.5 Ti, 0.1-0.3 Nb, 0.1-0.5 V, 0.001-0.005 P, 0.08-0.12 C, 0.01-0.03 N, 0.005-0.01 B and the balance iron that is further improved by annealing for up to 1 hour at 1150-1200/degree/C and then cold deforming 5-15%. The alloy exhibits dramatically improved creep rupture resistance and ductility at 700/degree/C. 2 figs.

  5. Numerical and experimental studies on thermal deformation of ceramic breeder pebble bed systems

    NASA Astrophysics Data System (ADS)

    An, Zhiyong

    The goal of this work is to develop modeling capabilities for understanding and predicting thermo-mechanical behavior of ceramic breeder pebble bed systems at elevated temperatures (600-800°C). The thermo-mechanical behavior of solid breeder pebble beds is a critical issue for the solid breeder blanket designs and is different from the behaviors of solid materials. The issue includes potential breakage of pebble materials and change in heat transfer characteristics across the breeder materials and cladding interface. Furthermore, at elevated temperatures, thermal creep deformation plays an uncertain role related to the contact stresses in the pebble beds. To understand these effects, the following efforts have been undertaken: First, experiments of a typical breeder blanket design have been conducted to study the thermal creep behaviors of the pebble bed system. Other than providing data for benchmarking numerical simulation, the experimental results show that the thermal deformation behaviors of typical pebble materials, such as Li2O and Li4SiO4 lithium ceramics, are nonlinear with respect to time and temperature. Under fixed temperatures (higher than 600°C), stresses generated from differential thermal expansion begin to decrease as a result of creep deformation. Second, a new numerical program, based on discrete element method (DEM), has been developed to simulate the fundamental mechanical behaviors of the packed pebble bed system. Considering the effects in a high temperature situation, inelastic contact models have been derived to predict thermal creep deformation. Our DEM program is mainly used to derive the effective mechanical constitutive equations for a pebble bed system. Besides that, it can provide the stress distribution inside the pebble bed and the force evolution related to the changes of boundary loadings. Last, a numerical program based on the finite element analysis (FEA) has been utilized to simulate the stress magnitude and deformation characteristics/evolution of the breeding zone in a fusion blanket. The advantage of FEA modeling is that it can analyze a larger-scale material system, and also provide important information for blanket design and performance evaluation. One of the numerical results has illustrated the thermo-mechanical behaviors of breeding blanket unit cells under pulsed heating operation.

  6. Plasticity and creep of polycrystalline magnesite

    NASA Astrophysics Data System (ADS)

    Ulrich, C. A.; Holyoke, C. W.; Kronenberg, A. K.; Newman, J.

    2011-12-01

    Carbonates may be incorporated in the mantle at collisional plate boundaries by a number of processes, including subduction of weathered oceanic crust and fault-bounded tectonic slivers of seamounts that are not left behind in the accretionary wedge. High-magnesium carbonates, dolomite and magnesite have been observed in ultra-deep metamorphic collisional terrains and they have been observed (or inferred) in mantle xenoliths from well-preserved (or partially back-reacted) inclusions. Magnesite can also be formed in the mantle by reaction with CO2-rich fluids, and is commonly found within serpentinized peridotite bodies. Once magnesite is formed in subducting slabs, it is likely to remain as an important carbon-bearing phase, as its stability extends over a wide range of (upper, transitional and possibly lower) mantle conditions. In order to quantify the mechanical properties of magnesite aggregates, we performed a series of triaxial compression experiments on cylinders of a natural, fine-grained (d~1 μm) magnesite aggregate at temperatures of 400-775°C and strain rates of 10-4/s - 10-6/s at a constant effective pressure of 300 MPa using a Heard-type gas confining medium deformation apparatus. Experiments performed at 1*10-5/s, show that the strength of magnesite is weakly temperature dependent from 400 to 600°C and becomes strongly temperature dependent at T ≥ 600°C as strengths decrease from 500 MPa to 5 MPa (at 775°C). The microstructures in the sample deformed at 500°C include angular grains and pores, similar to those observed in the starting material. However, the grains and pore boundaries in the sample deformed at 775°C are considerably more rounded. These first deformation experiments on polycrystalline magnesite reveal results indicate a transition in the dominant deformation mechanism with increasing temperature. Based on comparisons with deformation mechanisms of other carbonates, and their associated mechanical responses, we expect that magnesite deforms by low-temperature crystal plasticity at temperatures less than 600°C (at 1*10-5/s) and it deforms by diffusion (coble) creep at higher temperatures. Comparisons of magnesite, calcite, dolomite and olivine strengths along a P-T path within a subducting slab indicate that calcite is the weakest phase in the upper 100 km, where it is stable, but magnesite becomes weaker than all of the other phases at greater depths. These results indicate that magnesite may play a significant role as a weak phase that affects the rheology of subducting slabs.

  7. Coupling creep and damage in concrete under high sustained loading: Experimental investigation on bending beams and application of Acoustic Emission technique

    NASA Astrophysics Data System (ADS)

    Saliba, J.; Loukili, A.; Grondin, F.

    2010-06-01

    Creep and damage in concrete govern the long-term deformability of concrete. Thus, it is important to understand the interaction between creep and damage in order to design reliable civil engineering structures subjected to high level loading during a long time. Many investigations have been performed on the influence of concrete mixture, the effect of the bond between the matrix and the aggregates, temperature, aging and the size effect on the cracking mechanism and fracture parameters of concrete. But there is a lack of results on the influence of the creep loading history. In the present paper, an experimental investigation on the fracture properties of concrete beams submitted to three point bending tests with high levels of sustained load that deals with creep is reported. The results aim first to investigate the ranges of variation of the time response due to creep damage coupled effects under constant load and secondly to evaluate the residual capacity after creep. For this purpose a series of tests were carried out on geometrically similar specimens of size 100x200x800mm with notch to depth ratio of 0.2 in all the test specimens. The exchange of moisture was prevented and beams were subjected to a constant load of 70% and 90% of the maximum capacity. Three point bending test were realized on specimen at the age of 28 days to determine the characteristics of concrete and the maximum load so we could load the specimens in creep. Threepoint bend creep tests were performed on frames placed in a climate controlled chamber [1]. Then after four months of loading, the beams subjected to creep were removed from the creep frames and then immediately subjected to three-point bending test loading up to failure with a constant loading rate as per RILEM-FMC 50 recommendations. The residual capacity on the notched beams and the evolution of the characteristics of concrete due to the basic creep was considered. The results show that sustained loading had a strengthening effect on concrete, probably because of the consolidation of the hardened cement paste. The influence of creep on fracture energy, fracture toughness, and characteristic length of concrete is also studied. The fracture energy and the characteristic length of concrete increases slightly when creep occurs prior to failure and the size of the fracture process zone increases too. The load-CMOD relationship is linear in the ascending portion and gradually drops off after the peak value in the descending portion. The length of the tail end portion of the softening curve increases with beams subjected to creep. Relatively more ductile fracture behavior was observed with beams subjected to creep. The contribution of non-destructive and instrumental investigation methods is currently exploited to check and measure the evolution of some negative structural phenomena, such as micro-and macro-cracking, finally resulting in a creep-like behaviour. Among these methods, the non-destructive technique based on acoustic Emission proves to be very effective, especially to check and measure micro-cracking that takes place inside a structure under mechanical loading. Thus as a part of the investigation quantitative acoustic emission techniques were applied to investigate microcracking and damage localization in concrete beams. The AE signals were captured with the AE WIN software and further analyzed with Noesis software analysis of acoustic emission data. AE waveforms were generated as elastic waves in concrete due to crack nucleation. And a multichannel data acquisition system was used to record the AE waveforms. During the three point bending tests, quantitative acoustic emission (AE) techniques were used to monitor crack growth and to deduce micro fracture mechanics in concrete beams before and after creep. Several specimens are experimented in order to match each cluster with corresponding damage mechanism of the material under loading. At the same time acoustic emission was used to investigate characteristic of the fracture process zone (length width and macro crack propagation

  8. Elevated temperature deformation of TD-nickel.

    NASA Technical Reports Server (NTRS)

    Petrovic, J. J.; Ebert, L. J.

    1973-01-01

    Sensitivity of the elevated temperature (above 0.5 Tm) deformation of TD-nickel to grain size and shape was examined in both tension and creep. Elevated temperature strength increased with increasing grain diameter and increasing L/D ratio. Temperature sensitivity of the yield stress, as well as high (compared to self diffusion) apparent tensile activation enthalpies were the result of the internal stress not being proportional to the shear modulus. Creep activation enthalpies increased with increasing L/D ratio and, to a lesser extent, increasing grain diameter, reaching high values which may be apparent values. The thoria particle dispersion may have been altered by elevated temperature tensile and creep deformation.

  9. Effect of Annealing Time on Microstructural Evolution and Deformation Characteristics in 10Mn1.5Al TRIP Steel

    NASA Astrophysics Data System (ADS)

    Han, Qihang; Zhang, Yulong; Wang, Li

    2015-05-01

    To investigate microstructural evolution and its effects on the deformation behaviors of cold-rolled 10Mn1.5Al TRIP steel, a series of intercritical annealing treatments with various holding times from 3 minutes to 48 hours were conducted. With the increase of the holding time from 3 minutes to 12 hours, the elongation was improved from 15 to 42 pct, while the tensile strength was only reduced from 1210 to 1095 MPa; the strength-ductility combination thus exceeded 45 GPa pct. Austenite was found to coexist with martensite within deformed grains, which reduced the strain concentration at the interface. The austenite transformation fraction, as measured from the {220} peaks, after 3 minutes annealing was half that after 12 hours annealing. This is an indication that the slip systems were more easily activated in the micro-scaled grains compared with nano-scaled grains. Therefore, although the stability of austenite would have increased during annealing, size-induced slip suppression was reduced. Thus, more strain was accommodated in the austenite, facilitating a greater strain-induced transformation and better ductility.

  10. Characteristics of lateral electrical surface stimulation (LESS) and its effect on the degree of spinal deformity in idiopathic scoliosis

    NASA Astrophysics Data System (ADS)

    Kowalski, Ireneusz M.; Palko, Tadeusz; Pasniczek, Roman; Szarek, Jozef

    2009-01-01

    Clinical studies were carried out in the period of 2003-2006 at the Provincial Children's Rehabilitation Hospital in Ameryka near Olsztyn (Poland). The study involved a group of children and youth exhibiting spinal deformity progression in idiopathic scoliosis (IS) of more than 5° per year according to the Cobb scale. Four hundred and fifty patients between 4 and 15 years of age were divided into three groups (n = 150). Group I and group II received 2-hour and 9-hour lateral electrical surface stimulation (LESS), respectively, whereas group III (control) was treated only with corrective exercises for 30 minutes twice a day. LESS was performed with the use of a battery-operated SCOL-2 stimulator manufactured by Elmech, Warsaw, Poland. The effectiveness of this method was confirmed in the treatment of spinal IS in children and youth, especially when the initial spinal deformity did not exceed 20° according to the Cobb scale. A short-duration electrostimulation (2 hours daily) was found to produce results similar to those obtained after overnight (9 h) electrostimulation. Moreover, the analysis of the Harrington prognostic index F confirms the positive effect of LESS in both groups of patients (2 h and 9 h of LESS).

  11. Cyclic creep-rupture behavior of three high-temperature alloys.

    NASA Technical Reports Server (NTRS)

    Halford, G. R.

    1972-01-01

    Study of some important characteristics of the cyclic creep-rupture curves for the titanium alloy 6Al-2Sn-4Zr-2Mo at 900 and 1100 F (755 and 865 K), the cobalt-base alloy L-605 at 1180 F (910 K), and for two hardness levels of 316 stainless steel at 1300 F (980 K). The cyclic creep-rupture curve relates tensile stress and tensile time-to-rupture for strain-limited cyclic loading and has been found to be independent of the total strain range and the level of compressive stress employed in the cyclic creep-rupture tests. The cyclic creep-rupture curve was always found to be above and to the right of the conventional (constant load) monotonic creep-rupture curve by factors ranging from 2 to 10 in time-to-rupture. This factor tends to be greatest when the creep ductility is large. Cyclic creep acceleration was observed in every cyclic creep-rupture test conducted. The phenomenon was most pronounced at the highest stress levels and when the tensile and compressive stresses were completely reversed. In general, creep rates were found to be lower in compression than in tension for equal true stresses. The differences, however, were strongly material-dependent.

  12. Invited review paper: Fault creep caused by subduction of rough seafloor relief

    NASA Astrophysics Data System (ADS)

    Wang, Kelin; Bilek, Susan L.

    2014-01-01

    Among the wide range of thermal, petrologic, hydrological, and structural factors that potentially affect subduction earthquakes, the roughness of the subducting seafloor is among the most important. By reviewing seismic and geodetic studies of megathrust locking/creeping state, we find that creeping is the predominant mode of subduction in areas of extremely rugged subducting seafloor such as the Kyushu margin, Manila Trench, northern Hikurangi, and southeastern Costa Rica. In Java and Mariana, megathrust creeping state is not yet constrained by geodetic observations, but the very rugged subducting seafloor and lack of large earthquakes also suggest aseismic creep. Large topographic features on otherwise relatively smooth subducting seafloor such as the Nazca Ridge off Peru, the Investigator Fracture Zone off Sumatra, and the Joban seamount chain in southern Japan Trench also cause creep and often stop the propagation of large ruptures. Similar to all other known giant earthquakes, the Tohoku earthquake of March 2011 occurred in an area of relatively smooth subducting seafloor. The Tohoku event also offers an example of subducting seamounts stopping rupture propagation. Very rugged subducting seafloor not only retards the process of shear localization, but also gives rise to heterogeneous stresses. In this situation, the fault zone creeps because of distributed deformation of fractured rocks, and the creep may take place as transient events of various spatial and temporal scales accompanied with small and medium-size earthquakes. This process cannot be described as stable or unstable friction along a single contact surface. The association of large earthquakes with relatively smooth subducting seafloor and creep with very rugged subducting seafloor calls for further investigation. Seafloor near-trench geodetic monitoring, high-resolution imaging of subduction fault structure, studies of exhumed ancient subduction zones, and laboratory studies of low-temperature creep will greatly improve our understanding of the seismogenic and creep processes and their hazard implications.

  13. Non-contact Creep Resistance Measurement for Ultra-high temperature Materials

    NASA Technical Reports Server (NTRS)

    Hyers, Robert W.; Lee, Jonghuyn; Bradshaw, Richard C.; Rogers, Jan; Rathz, Thomas J.; Wall, James J.; Choo, Hahn; Liaw, Peter K.

    2005-01-01

    Continuing pressures for higher performance and efficiency in propulsion are driving ever more demanding needs for high-temperature materials. Some immediate applications in spaceflight include combustion chambers for advanced chemical rockets and turbomachinery for jet engines and power conversion in nuclear-electric propulsion. In the case of rockets, the combination of high stresses and high temperatures make the characterization of creep properties very important. Creep is even more important in the turbomachinery, where a long service life is an additional constraint. Some very high-temperature materials are being developed, including platinum group metals, carbides, borides, and silicides. But the measurement of creep properties at very high temperatures is itself problematic, because the testing instrument must operate at such high temperatures. Conventional techniques are limited to about 1700 C. A new, containerless technique for measuring creep deformation has been developed. This technique is based on electrostatic levitation (ESL) of a spherical sample, which is heated to the measurement temperature and rotated at a rate such that the centrifugal acceleration causes creep deformation. Creep of samples has been demonstrated at up to 2300 C in the ESL facility at NASA MSFC, while ESL itself has been applied at over 3000 C, and has no theoretical maximum temperature. The preliminary results and future directions of this NASA-funded research collaboration will be presented.

  14. Life Estimation and Creep Damage Quantification of Service Exposed Reformer Tube

    NASA Astrophysics Data System (ADS)

    Raj, A.; Roy, N.; Roy, B. N.; Ray, A. K.

    2015-11-01

    This paper deals with evaluation of creep damage of ~11 years service exposed primary hydrogen reformer tube made of HP-40 grade of steel in a petrochemical industry, which has been carried out in terms of Kachanav's continuum damage mechanics (CDM) model (K-model) and Bogdanoff model (B-model) based on Markov process. Residual life of the tubes was estimated based on hot tensile, conventional creep deformation under identical test conditions, optical microscopy and fractography. Accumulation of damage due to creep has been quantified through microstructural studies. The as received tubes did not reveal any degradation in the material like creep cavitation or voids, but there was indeed loss of tensile strength from room temperature to 870C for the bottom portion of the tube due to ageing and overheating. Scatter in creep deformation behaviour of the material is probably due to variation in mode of fracture and scatter in voids. From statistical point of view, Weibull distribution pattern for analysing probability of rupture due to void area shifts with increase in true strain towards the higher population of void. The estimation of mean time to reach a specific damage state from K- model and B-model is in close agreement with that of experimental data and can describe the sudden changes of the creep damage in the tertiary region as well. A remnant life of >10 years is estimated at the operating stress-temperature conditions of the top as well as bottom portion of the tube.

  15. Numerical analysis for elucidation of nonlinear frictional characteristics of a deformed erythrocyte moving on a plate in medium subject to inclined centrifugal force.

    PubMed

    Oshibe, Takashi; Hayase, Toshiyuki; Funamoto, Kenichi; Shirai, Atsushi

    2014-12-01

    Complex interactions between blood cells, plasma proteins, and glycocalyx in the endothelial surface layer are crucial in microcirculation. To obtain measurement data of such interactions, we have previously performed experiments using an inclined centrifuge microscope, which revealed that the nonlinear velocity-friction characteristics of erythrocytes moving on an endothelia-cultured glass plate in medium under inclined centrifugal force are much larger than those on plain or material-coated glass plates. The purpose of this study was to elucidate the nonlinear frictional characteristics of an erythrocyte on plain or material-coated glass plates as the basis to clarify the interaction between the erythrocyte and the endothelial cells. We propose a model in which steady motion of the cell is realized as an equilibrium state of the force and moment due to inclined centrifugal force and hydrodynamic flow force acting on the cell. Other electrochemical effects on the surfaces of the erythrocyte and the plate are ignored for the sake of simplicity. Numerical analysis was performed for a three-dimensional flow of a mixture of plasma and saline around a rigid erythrocyte model of an undeformed biconcave shape and a deformed shape with a concave top surface and a flat bottom surface. A variety of conditions for the concentration of plasma in a medium, the velocity of the cell, and the minimum gap width and the angle of attack of the cell from the plate, were examined to obtain the equilibrium states. A simple flat plate model based on the lubrication theory was also examined to elucidate the physical meaning of the model. The equilibrium angle of attack was obtained only for the deformed cell model and was represented as a power function of the minimum gap width. A simple flat plate model qualitatively explains the power function relation of the frictional characteristics, but it cannot explain the equilibrium relation, confirming the computational result that the deformation of the cell is necessary for the equilibrium. The frictional characteristics obtained from the present computation qualitatively agree with those of former experiments, showing the validity of the proposed model. PMID:25271707

  16. Mechanical Interferometry Imaging for Creep Modeling of the Cornea

    PubMed Central

    Yoo, Lawrence; Reed, Jason; Gimzewski, James K.

    2011-01-01

    Purpose. A novel nanoindentation technique was used to biomechanically characterize each of three main layers of the cornea by using Hertzian viscoelastic formulation of creep, the deformation resulting from sustained-force application. Methods. The nanoindentation method known as mechanical interferometry imaging (MII) with <1-nm displacement precision was used to observe indentation of bovine corneal epithelium, endothelium, and stroma by a spherical ferrous probe in a calibrated magnetic field. For each specimen, creep testing was performed using two different forces for 200 seconds. Measurements for single force were used to build a quantitative Hertzian model that was then used to predict creep behavior for another imposed force. Results. For all three layers, displacement measurements were highly repeatable and were well predicted by Hertzian models. Although short- and long-term stiffnesses of the endothelium were highest of the three layers at 339.2 and 20.2 kPa, respectively, both stromal stiffnesses were lowest at 100.4 and 3.6 kPa, respectively. Stiffnesses for the epithelium were intermediate at 264.6 and 12.2 kPa, respectively. Conclusions. Precise, repeatable measurements of corneal creep behavior can be conveniently obtained using MII at mechanical scale as small as one cell thickness. When interpreted in analytical context of Hertzian viscoelasticity, MII technique proved to be a powerful tool for biomechanical characterization of time-dependent biomechanics of corneal regions. PMID:21969299

  17. Creep fatigue life prediction for engine hot section materials (isotropic)

    NASA Technical Reports Server (NTRS)

    Moreno, Vito; Nissley, David; Lin, Li-Sen Jim

    1985-01-01

    The first two years of a two-phase program aimed at improving the high temperature crack initiation life prediction technology for gas turbine hot section components are discussed. In Phase 1 (baseline) effort, low cycle fatigue (LCF) models, using a data base generated for a cast nickel base gas turbine hot section alloy (B1900+Hf), were evaluated for their ability to predict the crack initiation life for relevant creep-fatigue loading conditions and to define data required for determination of model constants. The variables included strain range and rate, mean strain, strain hold times and temperature. None of the models predicted all of the life trends within reasonable data requirements. A Cycle Damage Accumulation (CDA) was therefore developed which follows an exhaustion of material ductility approach. Material ductility is estimated based on observed similarities of deformation structure between fatigue, tensile and creep tests. The cycle damage function is based on total strain range, maximum stress and stress amplitude and includes both time independent and time dependent components. The CDA model accurately predicts all of the trends in creep-fatigue life with loading conditions. In addition, all of the CDA model constants are determinable from rapid cycle, fully reversed fatigue tests and monotonic tensile and/or creep data.

  18. Mechanical Behavior of Low Porosity Carbonate Rock: From Brittle Creep to Ductile Creep.

    NASA Astrophysics Data System (ADS)

    Nicolas, A.; Fortin, J.; Gueguen, Y.

    2014-12-01

    Mechanical compaction and associated porosity reduction play an important role in the diagenesis of porous rocks. They may also affect reservoir rocks during hydrocarbon production, as the pore pressure field is modified. This inelastic compaction can lead to subsidence, cause casing failure, trigger earthquake, or change the fluid transport properties. In addition, inelastic deformation can be time - dependent. In particular, brittle creep phenomena have been deeply investigated since the 90s, especially in sandstones. However knowledge of carbonates behavior is still insufficient. In this study, we focus on the mechanical behavior of a 14.7% porosity white Tavel (France) carbonate rock (>98% calcite). The samples were deformed in a triaxial cell at effective confining pressures ranging from 0 MPa to 85 MPa at room temperature and 70C. Experiments were carried under dry and water saturated conditions in order to explore the role played by the pore fluids. Two types of experiments have been carried out: (1) a first series in order to investigate the rupture envelopes, and (2) a second series with creep experiments. During the experiments, elastic wave velocities (P and S) were measured to infer crack density evolution. Permeability was also measured during creep experiments. Our results show two different mechanical behaviors: (1) brittle behavior is observed at low confining pressures, whereas (2) ductile behavior is observed at higher confining pressures. During creep experiments, these two behaviors have a different signature in term of elastic wave velocities and permeability changes, due to two different mechanisms: development of micro-cracks at low confining pressures and competition between cracks and microplasticity at high confining pressure. The attached figure is a summary of 20 triaxial experiments performed on Tavel limestone under different conditions. Stress states C',C* and C*' and brittle strength are shown in the P-Q space: (a) 20C and dry, (b) 20C and water saturated samples, (c) 70C dry and (d) summary of all the experiments. Three regimes of inelastic and failure modes are observed: brittle failure, shear-enhanced compaction and dilatant cataclastic flow.

  19. In situ tensile and creep testing of lithiated silicon nanowires

    SciTech Connect

    Boles, Steven T.; Kraft, Oliver; Thompson, Carl V.; Mönig, Reiner; Helmholtz Institute Ulm for Electrochemical Energy Storage , 89069 Ulm

    2013-12-23

    We present experimental results for uniaxial tensile and creep testing of fully lithiated silicon nanowires. A reduction in the elastic modulus is observed when silicon nanowires are alloyed with lithium and plastic deformation becomes possible when the wires are saturated with lithium. Creep testing was performed at fixed force levels above and below the tensile strength of the material. A linear dependence of the strain-rate on the applied stress was evident below the yield stress of the alloy, indicating viscous deformation behavior. The observed inverse exponential relationship between wire radius and strain rate below the yield stress indicates that material transport was controlled by diffusion. At stress levels approaching the yield strength of fully lithiated silicon, power-law creep appears to govern the strain-rate dependence on stress. These results have direct implications on the cycling conditions, rate-capabilities, and charge capacity of silicon and should prove useful for the design and construction of future silicon-based electrodes.

  20. Tectonic creep in the Hayward fault zone, California

    USGS Publications Warehouse

    Radbruch-Hall, Dorothy H.; Bonilla, M.G.

    1966-01-01

    Tectonic creep is slight apparently continuous movement along a fault. Evidence of creep has been noted at several places within the Hayward fault zone--a zone trending northwestward near the western front of the hills bordering the east side of San Francisco Bay. D. H. Radbruch of the Geological Survey and B. J. Lennert, consulting engineer, confirmed a reported cracking of a culvert under the University of California stadium. F. B. Blanchard and C. L. Laverty of the East Bay Municipal Utility District of Oakland studied cracks in the Claremont water tunnel in Berkeley. M. G. Bonilla of the Geological Survey noted deformation of railroad tracks in the Niles district of Fremont. Six sets of tracks have been bent and shifted. L. S. Cluff of Woodward-Clyde-Sherard and Associates and K. V. Steinbrugge of the Pacific Fire Rating Bureau noted that the concrete walls of a warehouse in the Irvington district of Fremont have been bent and broken, and the columns forced out of line. All the deformations noted have been right lateral and range from about 2 inches in the Claremont tunnel to about 8 inches on the railroad tracks. Tectonic creep almost certainly will continue to damage buildings, tunnels, and other structures that cross the narrow bands of active movement within the Hayward fault zone.

  1. Microstructure and Creep Behavior of a Directional Solidification Nickel-based Superalloy

    NASA Astrophysics Data System (ADS)

    Tian, Ning; Tian, Sugui; Yu, Huichen; Li, Ying; Meng, Xianlin

    2015-07-01

    By means of creep property measurement and microstructure observation, an investigation has been made into microstructure and creep behavior of a directional solidification Ni-based superalloy at high temperatures. Results show that after full heat treatment, small cuboidal ?' precipitates distribute in the dendrite regions, while coarser ones distribute in the inter-dendrite regions. In the primary stage of creep, the ?' phase in alloy is transformed into the rafted structure along the direction vertical to stress axis, and then the creep of alloy enters the steady state stage. And dislocations slipping in the g matrix and climbing over the rafted ?' phase are thought to be the deformation mechanism of the alloy during steady creep stage. At the latter stage of creep, the alternate slipping of dislocations may shear and twist the rafted ?'/? phases, which promotes the initiation and propagation of the micro-cracks along the boundaries near the coarser rafted ?' phase. And the bigger probability of the creep damage occurs in the grain boundaries along 45 angles relative to the stress axis due to them bearing relatively bigger shearing stress.

  2. Creep and shrinkage of high performance lightweight concrete: A multi-scale investigation

    NASA Astrophysics Data System (ADS)

    Lopez, Mauricio

    This multi-scale investigation aimed to provide new knowledge and understanding of creep and shrinkage of high performance lightweight concrete (HPLC) by assessing prestress losses in HPLC prestressed members in a large-scale study; by quantifying the effect of the constituent materials and external conditions on creep and shrinkage in a medium-scale study; and by improving the fundamental understanding of creep and shrinkage in a small-scale study. Creep plus shrinkage prestress losses were between two and eight times lower than those estimated for the design standards and approximately 50% of those measured in similar strength normal weight high performance concrete girders. The lower creep and shrinkage exhibited by HPLC was found to be caused by a synergy between the pre-soaked lightweight aggregate and the low water-to-cementitious material ratio matrix. That is, the water contained in the lightweight aggregate contributes to enhance hydration by providing an internal moist curing. The water in the aggregate also contributes to maintain a high internal relative humidity which reduces or eliminates autogenous shrinkage. This higher internal relative humidity also reduces creep by preventing load-induced water migration. Finally, lightweight aggregate exhibits a better elastic compatibility with the paste than normal weight aggregate. This improved elastic matching and the enhanced hydration are believed to reduce peak deformations at the ITZ which further decreases creep and shrinkage.

  3. Creep-strengthening of steel at high temperatures using nano-sized carbonitride dispersions.

    PubMed

    Taneike, Masaki; Abe, Fujio; Sawada, Kota

    2003-07-17

    Creep is a time-dependent mechanism of plastic deformation, which takes place in a range of materials under low stress-that is, under stresses lower than the yield stress. Metals and alloys can be designed to withstand creep at high temperatures, usually by a process called dispersion strengthening, in which fine particles are evenly distributed throughout the matrix. For example, high-temperature creep-resistant ferritic steels achieve optimal creep strength (at 923 K) through the dispersion of yttrium oxide nanoparticles. However, the oxide particles are introduced by complicated mechanical alloying techniques and, as a result, the production of large-scale industrial components is economically unfeasible. Here we report the production of a 9 per cent Cr martensitic steel dispersed with nanometre-scale carbonitride particles using conventional processing techniques. At 923 K, our dispersion-strengthened material exhibits a time-to-rupture that is increased by two orders of magnitude relative to the current strongest creep-resistant steels. This improvement in creep resistance is attributed to a mechanism of boundary pinning by the thermally stable carbonitride precipitates. The material also demonstrates enough fracture toughness. Our results should lead to improved grades of creep-resistant steels and to the economical manufacture of large-scale steel components for high-temperature applications. PMID:12867976

  4. (Irradiation creep of graphite)

    SciTech Connect

    Kennedy, C.R.

    1990-12-21

    The traveler attended the Conference, International Symposium on Carbon, to present an invited paper, Irradiation Creep of Graphite,'' and chair one of the technical sessions. There were many papers of particular interest to ORNL and HTGR technology presented by the Japanese since they do not have a particular technology embargo and are quite open in describing their work and results. In particular, a paper describing the failure of Minor's law to predict the fatigue life of graphite was presented. Although the conference had an international flavor, it was dominated by the Japanese. This was primarily a result of geography; however, the work presented by the Japanese illustrated an internal program that is very comprehensive. This conference, a result of this program, was better than all other carbon conferences attended by the traveler. This conference emphasizes the need for US participation in international conferences in order to stay abreast of the rapidly expanding HTGR and graphite technology throughout the world. The United States is no longer a leader in some emerging technologies. The traveler was surprised by the Japanese position in their HTGR development. Their reactor is licensed and the major problem in their graphite program is how to eliminate it with the least perturbation now that most of the work has been done.

  5. The development of methods for the prediction of primary creep behavior in metals

    NASA Technical Reports Server (NTRS)

    Zerwekh, R. P.

    1978-01-01

    The applicability of a thermodynamic constitutive theory of deformation to the prediction of primary creep and creep strain relaxation behavior in metals is examined. Constitutive equations derived from the theory are subjected to a parametric analysis in order to determine the influence of several parameters on the curve forms generated by the equations. A computer program is developed which enables the solution of a generalized constitutive equation using experimental data as input. Several metals were tested to form a data base of primary creep and relaxation behavior. The extent to which these materials conformed to the constitutive equation showed wide variability, with the alloy Ti-6Al-4V exhibiting the most consistent results. Accordingly, most of the analysis is concentrated upon data from that alloy, although creep and relaxation data from all the materials tested are presented. Experimental methods are outlined as well as some variations in methods of analysis. Various theoretical and practical implications of the work are discussed.

  6. Energy version of the kinetic equations of isothermal creep and long-term strength

    NASA Astrophysics Data System (ADS)

    Radchenko, V. P.; Saushkin, M. N.; Gorbunov, S. V.

    2014-01-01

    Energy-type kinetic equations of inelastic rheological deformation are proposed in which the elastic, plastic, and creep strains are the additive components of the total strain, and the damage parameter is taken into account. A model of viscoelastic material with a creep kernel of exponential type is considered. The Lyapunov stability of solutions under constant stress is studied. The stability range of the solutions of the differential equations of the mathematical model corresponding to asymptotically bounded creep is established. It is shown that the instability range of the solutions corresponds to the onset of the third stage of creep. The relationship is determined between the Lyapunov stability of the solutions and the stability of the computational algorithm for the numerical solution of the system of equations. The proposed model is experimentally verified. It is shown that the calculated and experimental data are in good agreement.

  7. A nonlocal continuum damage mechanics approach to simulation of creep fracture in ice sheets

    NASA Astrophysics Data System (ADS)

    Duddu, Ravindra; Waisman, Haim

    2013-06-01

    We present a Lagrangian finite element formulation aimed at modeling creep fracture in ice-sheets using nonlocal continuum damage mechanics. The proposed formulation is based on a thermo-viscoelastic constitutive model and a creep damage model for polycrystalline ice with different behavior in tension and compression. In this paper, mainly, we detail the nonlocal numerical implementation of the constitutive damage model into commercial finite element codes (e.g. Abaqus), wherein a procedure to handle the abrupt failure (rupture) of ice under tension is proposed. Then, we present numerical examples of creep fracture under four-point bending, uniaxial tension, and biaxial tension in order to illustrate the viability of the current approach. Finally, we present simulations of creep crack propagation in idealized rectangular ice slabs so as to estimate calving rates at low deformation rates. The examples presented demonstrate the mesh size and mesh directionality independence of the proposed nonlocal implementation.

  8. Creep of Rocksalt: Microstructure and Hart's Mechanical Equation of State

    NASA Astrophysics Data System (ADS)

    Plookphol, T.; Cooper, R. F.; Stone, D. S.

    2001-12-01

    Hart's mechanical equation of state prescribes methods for efficiently gathering and extrapolating data pertaining to time-dependent deformation. The approach relies on the ability to characterize, first, the stress-strain rate behavior of a material at "constant structure," or "hardness state" and, second, the evolution of that structure -- work hardening and recovery -- throughout deformation. Constant structure "Hardness curves" can be generated using load relaxation experiments, which sweep out a spectrum of stress v. strain rate at nearly constant strain. It has been widely observed that hardness curves generated at different levels of work hardening scale with each other, that is, they can be translated in log-log space along lines of fixed slope so that they fit on top of each other. Despite the ubiquity of scaling among many varied materials, there has never been an experimental effort to establish a microscopic basis for such scaling. Too, there has never been a careful effort to establish the relationship between data generated from load relaxation and those obtained from creep tests. The benefit of such efforts would be to provide experimenters with tools for extending experimental techniques to lower strain rates -- short duration load relaxation experiments can routinely achieve 10-8 s-1 and, with effort, 10-10 s-1. Such efforts might also lead to a better understanding of power law creep itself, for which there is no universally accepted microscopic model. In this work we investigated the creep, stress-change, and load relaxation behavior of single crystal rock-salt at 673K and 973K deformed under compression in the [100] orientation. Subgrain size distributions of the specimens deformed at 973K were measured using light microscopy. In load relaxation experiments we found that hardness states correlated uniquely with differences in average subgrain size but not dislocation density. To within measurement error, subgrain size distributions were similar to each other differing only in the mean diameter, depending on stress, but not in the shape of the distributions; it is conjectured that microstructural similarity is the physical basis for scaling in load relaxation. A correspondence rule was established between stress relaxation and creep; the data suggest that during primary creep the material evolves through a range of hardness states until steady state strain rate is achieved.

  9. Characteristic of the postseismic deformation following the 2011 Sanriku-Oki earthquake (Mw 7.2) by comparing the 1989 and 1992 Sanriku-Oki events

    NASA Astrophysics Data System (ADS)

    Ohta, Yusaku; Hino, Ryota; Ariyoshi, Keisuke; Matsuzawa, Toru; Mishina, Masaaki; Sato, Tadahiro; Tachibana, Kenji; Demachi, Tomotsugu; Miura, Satoshi

    2013-04-01

    The March 11, 2011, moment magnitude (Mw) 9.0 Tohoku earthquake (hereafter referred to as the mainshock) generated a large tsunami, which caused devastating damage and the loss of more than 15,800 lives. On March 9, 2011 at 2:45 (UTC), an M7.3 interplate earthquake (hereafter referred to as the foreshock) occurred ~45 km northeast of the epicenter of the Mw9.0 mainshock. The focal mechanism estimated by the National Research Institute for Earth Science and Disaster Prevention (NIED) incorporates reverse fault motion with a west-northwest to east-southeast compression axis. This foreshock preceded the 2011 Tohoku earthquake by 51 h. Kato et al. [Science, 2012] pointed out aftershock migration after the foreshock along the trench axis toward the epicenter of the Mw9.0 mainshock on the basis of an earthquake catalog, which was created using a waveform correlation technique. They also estimated aseismic slip amount by the repeating earthquake analysis. Ohta et al. [GRL, 2012] proposed a coseismic and postseismic afterslip model of the foreshock based on a GPS network and ocean bottom pressure gauge sites. The estimated coseismic slip and afterslip areas show complementary spatial distributions. The slip amount for the afterslip is roughly consistent with that determined by repeating earthquake analysis carried out by Kato et al. [2012]. Ohta et al. [2012] also pointed out a volumetric strainmeter time series suggests that this event advanced with a rapid decay time constant compared with other typical large earthquakes. For verification of this exception, we investigated the postseismic deformation characteristic following the 1989 and 1992 Sanriku-Oki earthquake, which occurred 100-150 km north of the epicenter of the 2011 Sanriku-Oki event. We used four components extensometer of the Tohoku University at Miyako (39.59N, 141.98E) on the Sanriku coast for these events. To extract the characteristics of the postseismic deformation, we fitted the logarithmic function. The estimated decay time constant was relatively small compared with the typical interplate earthquakes in a similar fashion to 2011 Sanriku-Oki event. Our result suggests that the short decay time of the postseismic deformation is characteristic of this region. The exact reason of short decay time for these afterslips is unclear at present, but it was possibly controlled by the frictional property on the plate interface, especially effective normal stress controlled by fluid.

  10. Seismological characteristics of the 2011 unrest in Santorini caldera: Implications for observed deformation and volcano-tectonics

    NASA Astrophysics Data System (ADS)

    Konstantinou, Konstantinos; Evangelidis, Christos; Melis, Nikolaos; Liang, Wen-Tzong

    2013-04-01

    Santorini caldera has experienced several explosive eruptions in the past, the most well-known of these being the Late Bronze Age (ca. 1628 BC) eruption that may have been responsible for the demise of the Minoan civilization. Since the early 1950's the volcano has been dormant without exhibiting any significant activity except from discharge of low-temperature hydrothermal fluids. In January 2011 both deformation and seismic activity increased considerably signaling a period of unrest which however, did not result in an eruption. One permanent and seven temporary seismic stations equipped with three-component sensors were deployed by the National Observatory of Athens. These were combined with seismic stations from the University of Thessaloniki, seven with only a vertical component and four with three-component sensors and all operated under the Hellenic Unified Seismic Network, thus densely monitoring the Santorini Volcano. These seismic stations have recorded the seismic activity from its start up to now. About 290 micro-earthquakes recorded by at least 5 stations were analyzed for the purpose of obtaining accurate epicentral and hypocentral locations using both catalog and differential travel times from waveform cross-correlation. All of these events exhibit clear P- and S-phases indicating that they resulted from shear failure of rock rather than fluid-flow within volcanic conduits. Results show two well-defined clusters in Palea and Nea Kameni islands within the caldera with hypocentral depths ranging between 5-10 km. Interestingly, one more cluster of events with depths between 15-19 km appears near the area of Cape Coloumbo and developed almost simultaneously with the clusters within the caldera. The Mogi source depth inferred from geodetic observations previously is shallower (~4 km) and does not coincide spatially with the clusters within the caldera. This points to the possibility that seismicity and deformation may be excited by deeper pressure changes. Shear wave splitting measurements have also been performed using all available waveform data in order to understand the nature and spatial variation of the stress field during the unrest. Fast polarization directions exhibit some orientations consistent with the regional NW-SE extension in the area, but also orientations along NE-SW that signify the presence of a local stress field as well.

  11. Creep property and microstructure evolution of a nickel-base single crystal superalloy in [011] orientation

    SciTech Connect

    Han, G.M. Yu, J.J.; Hu, Z.Q.; Sun, X.F.

    2013-12-15

    The creep property and microstructure evolution of a single crystal superalloy with [011] orientation were investigated at the temperatures of 700 °C, 900 °C and 1040 °C. It is shown that there exist stages of primary, steady-state, and tertiary creep under the lower temperature 700 °C. As the temperature increases to high temperatures of 900 °C and 1040 °C, steady-state creep stage is reduced or disappears and the shape of creep curves is dominated by an extensive tertiary stage. The minimum creep strain rate exhibits power law dependence on the applied stress; the stress exponents at 700 °C, 900 °C and 1040 °C are 28, 13 and 6.5, respectively. Microstructure observation shows that the morphologies of γ′ phase almost keep original shape at the lower temperature 700 °C and high applied stress. With the increasing creep temperature, γ′ precipitates tend to link together and form lamellar structure at an angle of 45° inclined to the applied stress. Transmission electron microscopy (TEM) investigations reveal that multiple < 110 > (111) slip systems gliding in the matrix channels and shearing γ′ precipitates by stacking faults or bending dislocation pairs are the main deformation mechanism at the lower temperature of 700 °C. At the high temperatures of 900 °C and 1040 °C, dislocation networks are formed at γ/γ′ interfaces and the γ′ rafts are sheared by dislocation pairs. - Highlights: • Creep properties of < 011 >-oriented single crystal superalloys were investigated. • γ′ phases become rafting at an angle of 45° inclined to the applied stress. • Creep deformation mechanisms depend on temperature and stress.

  12. A model for high temperature creep of single crystal superalloys based on nonlocal damage and viscoplastic material behavior

    NASA Astrophysics Data System (ADS)

    Trinh, B. T.; Hackl, K.

    2014-07-01

    A model for high temperature creep of single crystal superalloys is developed, which includes constitutive laws for nonlocal damage and viscoplasticity. It is based on a variational formulation, employing potentials for free energy, and dissipation originating from plasticity and damage. Evolution equations for plastic strain and damage variables are derived from the well-established minimum principle for the dissipation potential. The model is capable of describing the different stages of creep in a unified way. Plastic deformation in superalloys incorporates the evolution of dislocation densities of the different phases present. It results in a time dependence of the creep rate in primary and secondary creep. Tertiary creep is taken into account by introducing local and nonlocal damage. Herein, the nonlocal one is included in order to model strain localization as well as to remove mesh dependence of finite element calculations. Numerical results and comparisons with experimental data of the single crystal superalloy LEK94 are shown.

  13. Remaining Creep Life Assessment Techniques Based on Creep Cavitation Modeling

    NASA Astrophysics Data System (ADS)

    Ankit, Kumar

    2009-05-01

    The boiler and its components are built with assumed nominal design and reasonable life of operation about two to three decades (one or two hundred thousand hours). These units are generally replaced or life is extended at the end of this period. Under normal operating conditions, after the initial period of teething troubles, the reliability of these units remains fairly constant up to about two decades of normal operation. The failure rate then increases as a result of their time-dependent material damage. Further running of these units may become uneconomical and dangerous in some cases. In the following article, step-by-step methodology to quantify creep cavitation based on statistical probability analysis and continuum damage mechanics has been described. The concepts of creep cavity nucleation have also been discussed with a special emphasis on the need for development of a model based on creep cavity growth kinetics.

  14. Transient Creep and Strain Energy Dissipation: An Experimental Perspective

    NASA Astrophysics Data System (ADS)

    Faul, Ulrich; Jackson, Ian

    2015-05-01

    Energy dissipation due to intrinsic attenuation occurs at elevated temperatures in rocks as a result of a range of processes. Examples where small-strain, transient deformation occurs are seismic waves, tidal deformation, and at longer timescales post-glacial rebound and far-field post-seismic deformation. Experiments at mantle temperatures and seismic frequencies show that grain boundary sliding is a key process that results in a broad absorption band, as indicated by seismic observations. Models of grain boundary sliding predict a smooth transition from elastic behavior through an anelastic regime toward viscous (Maxwell) behavior, consistent with experimental observations. Other mechanisms that may contribute to dissipation in Earth, at least locally, are dislocations and melt. Extrapolation of the laboratory data shows that first-order observations of planetary behavior and structure can be explained by the effects of temperature and pressure on transient creep properties, but that locally, additional mechanisms are required.

  15. Observation of Grain Rotations to Elucidate the Development of Crystal Preferred Orientation during Diffusion Creep

    NASA Astrophysics Data System (ADS)

    Maruyama, G.; Hiraga, T.

    2014-12-01

    The seismic anisotropy in Earth's upper mantle is explained by the crystallographic preferred orientation (CPO) of rock-forming minerals, which have anisotropic elasticity. Our team showed that the CPO of forsterite is produced even during diffusion creep (Miyazaki et al. 2013). The purpose of this study is to understand the mechanism of the development of CPO of forsterite by observations of samples surface after the sample deformation where the fine-scale strain markers were imposed.We deformed cylindrical polycrystalline samples of synthesized forsterite plus 20 vol. % diopside at its diffusion creep regime. We polished the lateral side of the sample where we imposed grooves parallel to the compression axis of the sample using a focused ion beam. These marker lines allow us to observe grain rotation due to a plastic deformation of the sample. After the high temperature compression creep experiment under atmosphere, we observed the marker lines under scanning electron microscope.We succeeded to observe the marker lines after the deformation. Strain of bulk sample and of the marker line exhibit the similar value indicating the similar deformation proceeded both at bulk and surface regions of the samples. Grain rotation, which is identified by misfits of the markers at grain boundaries and rotation of intra-granular markers, were observed in all the samples. No distortion of the markers within the grains was found indicating the absence of intragranular deformation process such as a glide of dislocations; however, in the samples deformed at high stress (~300 MPa), curved intra-granular markers were observed, which is consistent with dislocation activity at high stress condition. Our results show the significant grain rotation, which is necessary process for the development of CPO, during diffusion creep as well as the ability of identification of the deformation mechanism of the bulk sample by the observation of the sample surface.

  16. Stress versus temperature dependent activation energies in creep

    NASA Technical Reports Server (NTRS)

    Freed, A. D.; Raj, S. V.; Walker, K. P.

    1990-01-01

    The activation energy for creep at low stresses and elevated temperatures is lattice diffusion, where the rate controlling mechanism for deformation is dislocation climb. At higher stresses and intermediate temperatures, the rate controlling mechanism changes from that of dislocation climb to one of obstacle-controlled dislocation glide. Along with this change, there occurs a change in the activation energy. It is shown that a temperature-dependent Gibbs free energy does a good job of correlating steady-state creep data, while a stress-dependent Gibbs free energy does a less desirable job of correlating the same data. Applications are made to copper and a LiF-22 mol. percent CaF2 hypereutectic salt.

  17. Sandia/Stanford Unified Creep Plasticity Damage Model for ANSYS

    Energy Science and Technology Software Center (ESTSC)

    2006-09-03

    A unified creep plasticity (UCP) model was developed, based upon the time-dependent and time-independent deformation properties of the 95.5Sn-3.9Ag-0.6Cu (wt.%) soldier that were measured at Sandia. Then, a damage parameter, D, was added to the equation to develop the unified creep plasticity damage (UCPD) model. The parameter, D, was parameterized, using data obtained at Sandia from isothermal fatigue experiments on a double-lap shear test. The softwae was validated against a BGA solder joint exposed tomore » thermal cycling. The UCPD model was put into the ANSYS finite element as a subroutine. So, the softwae is the subroutine for ANSYS 8.1.« less

  18. Sandia/Stanford Unified Creep Plasticity Damage Model for ANSYS

    SciTech Connect

    2006-09-03

    A unified creep plasticity (UCP) model was developed, based upon the time-dependent and time-independent deformation properties of the 95.5Sn-3.9Ag-0.6Cu (wt.%) soldier that were measured at Sandia. Then, a damage parameter, D, was added to the equation to develop the unified creep plasticity damage (UCPD) model. The parameter, D, was parameterized, using data obtained at Sandia from isothermal fatigue experiments on a double-lap shear test. The softwae was validated against a BGA solder joint exposed to thermal cycling. The UCPD model was put into the ANSYS finite element as a subroutine. So, the softwae is the subroutine for ANSYS 8.1.

  19. Changes in complex resistivity during creep in granite

    USGS Publications Warehouse

    Lockner, D.A.; Byerlee, J.D.

    1986-01-01

    A sample of Westerly granite was deformed under constant stress conditions: a pore pressure of 5 MPa, a confining pressure of 10 MPa, and an axial load of 170 MPa. Pore volume changes were determined by measuring the volume of pore fluid (0.01 M KClaq) injected into the sample. After 6 days of creep, characterized by accelerating volumetric stain, the sample failed along a macroscopic fault. Measurements of complex resistivity over the frequency range 0.001-300 Hz, taken at various times during creep, showed a gradual increase in both conductivity and permittivity. When analysed in terms of standard induced polarization (IP) techniques, the changing complex resistivity resulted in systematic changes in such parameters as percent frequency effect and chargeability. These results suggest that it may be possible to monitor the development of dilatancy in the source region of an impending earthquake through standard IP techniques. ?? 1986 Birka??user Verlag.

  20. Creep-fatigue criteria and inelastic behavior of modified 9Cr-1Mo steel at elevated temperatures. Final report

    SciTech Connect

    Ruggles, M.B.; Ogata, T.

    1994-02-01

    The ever increasing demand for safety requires that stringent and conservative methodology be developed for design and analysis of reactor components. At present modified 9Cr-1Mo steel is a candidate material for construction of steam generators in fast breeder reactors. Therefore high-temperature material properties and extensive insight into deformation behavior and creep-fatigue life are required to develop design guidelines for use of modified 9Cr-1Mo steel in actual plant components. However, existing information on creep-fatigue and deformation response of modified 9Cr-1Mo steel is insufficient, and further experimental and modeling efforts are needed. A joint effort between the Electric Power Research Institute (EPRI) in the United States and the Central Research Institute of Electric Power Industry (CRIEPI) in Japan was started in 1991 to investigate the inelastic behavior of and to develop creep-fatigue criteria for modified 9Cr-1Mo steel at elevated temperatures. The current program focuses on uniaxial and biaxial fatigue, creep, and creep-fatigue tests. Results of this effort are presented in this report. Section 2 introduces the test material and experimental arrangement. Uniaxial exploratory deformation tests and unified constitutive equations for inelastic analysis of modified 9Cr-1Mo steel are presented in Sections 3 and 4, respectively. Axial fatigue and creep-fatigue test results are discussed in Section 5. Section 6 is devoted to constant stress creep tests. Biaxial fatigue and creep-fatigue tests are described in Section 7. Progress in creep-fatigue life evaluation is reported in Section 8.

  1. Creep Behavior of Near-Stoichiometric Polycrystalline Binary NiAl

    NASA Technical Reports Server (NTRS)

    Raj, S. V.

    2002-01-01

    New and published constant load creep and constant engineering strain rate data on near-stoichiometric binary NiAl in the intermediate temperature range 700 to 1300 K are reviewed. Both normal and inverse primary creep curves are observed depending on stress and temperature. Other characteristics relating to creep of NiAl involving grain size, stress and temperature dependence are critically examined and discussed. At stresses below 25 MPa and temperatures above 1000 K, a new grain boundary sliding mechanism was observed with n approx. 2, Qc approx. 100 kJ/ mol and a grain size exponent of about 2. It is demonstrated that Coble creep and accommodated grain boundary sliding models fail to predict the experimental creep rates by several orders of magnitude.

  2. Pore-scale investigation on stress-dependent characteristics of granular packs and the impact of pore deformation on fluid distribution

    SciTech Connect

    Yoon, Hongkyu; Klise, Katherine A.; Torrealba, Victor A.; Karpyn, Zuleima T.; Crandall, D.

    2015-05-25

    Understanding the effect of changing stress conditions on multiphase flow in porous media is of fundamental importance for many subsurface activities including enhanced oil recovery, water drawdown from aquifers, soil confinement, and geologic carbon storage. Geomechanical properties of complex porous systems are dynamically linked to flow conditions, but their feedback relationship is often oversimplified due to the difficulty of representing pore-scale stress deformation and multiphase flow characteristics in high fidelity. In this work, we performed pore-scale experiments of single- and multiphase flow through bead packs at different confining pressure conditions to elucidate compaction-dependent characteristics of granular packs and their impact on fluid flow. A series of drainage and imbibition cycles were conducted on a water-wet, soda-lime glass bead pack under varying confining stress conditions. Simultaneously, X-ray micro-CT was used to visualize and quantify the degree of deformation and fluid distribution corresponding with each stress condition and injection cycle. Micro-CT images were segmented using a gradient-based method to identify fluids (e.g., oil and water), and solid phase redistribution throughout the different experimental stages. Changes in porosity, tortuosity, and specific surface area were quantified as a function of applied confining pressure. Results demonstrate varying degrees of sensitivity of these properties to confining pressure, which suggests that caution must be taken when considering scalability of these properties for practical modeling purposes. Changes in capillary number with confining pressure are attributed to the increase in pore velocity as a result of pore contraction. Furthermore, this increase in pore velocity was found to have a marginal impact on average phase trapping at different confining pressures.

  3. Pore-scale investigation on stress-dependent characteristics of granular packs and the impact of pore deformation on fluid distribution

    DOE PAGESBeta

    Yoon, Hongkyu; Klise, Katherine A.; Torrealba, Victor A.; Karpyn, Zuleima T.; Crandall, D.

    2015-05-25

    Understanding the effect of changing stress conditions on multiphase flow in porous media is of fundamental importance for many subsurface activities including enhanced oil recovery, water drawdown from aquifers, soil confinement, and geologic carbon storage. Geomechanical properties of complex porous systems are dynamically linked to flow conditions, but their feedback relationship is often oversimplified due to the difficulty of representing pore-scale stress deformation and multiphase flow characteristics in high fidelity. In this work, we performed pore-scale experiments of single- and multiphase flow through bead packs at different confining pressure conditions to elucidate compaction-dependent characteristics of granular packs and their impactmore » on fluid flow. A series of drainage and imbibition cycles were conducted on a water-wet, soda-lime glass bead pack under varying confining stress conditions. Simultaneously, X-ray micro-CT was used to visualize and quantify the degree of deformation and fluid distribution corresponding with each stress condition and injection cycle. Micro-CT images were segmented using a gradient-based method to identify fluids (e.g., oil and water), and solid phase redistribution throughout the different experimental stages. Changes in porosity, tortuosity, and specific surface area were quantified as a function of applied confining pressure. Results demonstrate varying degrees of sensitivity of these properties to confining pressure, which suggests that caution must be taken when considering scalability of these properties for practical modeling purposes. Changes in capillary number with confining pressure are attributed to the increase in pore velocity as a result of pore contraction. Furthermore, this increase in pore velocity was found to have a marginal impact on average phase trapping at different confining pressures.« less

  4. Dimensional change of dental amalgam and a suggested correlation between marginal integrity and creep.

    PubMed

    Paffenbarger, G C; Rupp, N W; Patel, P R

    1979-07-01

    Discussion of a possible correlation of marginal integrity and degree of creep resulting from relative resistance of amalgams to deformation caused by expansion is included in this study of the effect of phase changes on the dimensional stability of amalgams. PMID:379099

  5. Jumplike deformation of ?-irradiated polymethyl methacrylate

    NASA Astrophysics Data System (ADS)

    Peschanskaya, N. N.; Smolyanski?, A. S.; Shvedov, A. S.

    2009-06-01

    Nonuniformity of the microdeformation rate and the parameters of microdeformation jumps were studied in the creep regime for a polymethyl methacrylate irradiated by various dozes of the Co-60 ? radiation. The creep rate during compression of the polymethyl methacrylate was measured by an interferogram on 300-nm deformation increments. It is shown that the periods L of rate oscillations (jumps of deformation) on three scale levels are dependent on the irradiation doze and are also changed after prolonged exposure of samples in air. In the doze range 0 to 330 kGy, both a decrease and an increase in L are observed, which corresponds to the unstable kinetics of radiation chemical processes. The deformation jumps permit estimates of the radiation effect on various structural levels. It is concluded that the effect of radiation on coarser microstructural formations is the largest.

  6. Research the dynamical characteristics of slow deformation waves as a rock massif response to explosions during its outworking

    NASA Astrophysics Data System (ADS)

    Hachay, Olga; Khachay, Oleg; Shipeev, Oleg

    2015-04-01

    As a result of long-term natural geomechanics and geophysical observation data on mines of complex ore rocks, generalization of the non-linear reaction of rock massif to heavy dynamic influences have been established. In addition, pendulum type waves have been observed and the sources of them have been located inside geoblocks of different hierarchic levels (Oparin et al., 2010). At the same time, these waves propagate with wide low (compared with seismic waves) velocity values (Kurlenja et al., 1993; Oparin et al., 2006). Research into the massif state with the use of the dynamic systems theory approach (Naimark et al., 2009; Chulichkov, 2003; Hachay et al., 2010) has been developed to ascertain the criteria of dissipative regimes changing for real rock massifs, which are under heavy man-caused influence. To realize such research we used the data from the seismic record of the Tashtagol mine for the two-year period from June 2006 up to June 2008. We used the space-time coordinates for all dynamic massif event responses, which occurred during that period inside the mine space and for the explosions - values fixed by seismic station energy (Hachay et al., 2010). The phase diagrams of the massif state for the northern and southern parts of the mine space were plotted in coordinates Ev(t) and d(Ev(t))/dt, t - time - in parts of 24 hours, Ev - the dissipated massive seismic energy - in joules. Hachay et al., (2010) analysed the morphology of seismic response phase trajectories on the explosion influences during different serial intervals in the southern part of the mine. In that period, according to data for different explosions in the mine, the majority of the total energy had been injected into the southern part of the mine. Moreover, at the end of 2007, just in the southern part, the strongest rock burst during the whole history of the working mine happened. We developed a new processing method of seismological information in real, which we can use directly in the mine to estimate the changing state of the rock burst in the massif by its outworking. As a result we have selected a typical morphology of massif response phase trajectories, which were locally, over time, in a stable state: on the phase plane the local area presented as a ball of twisted trajectories with some not far removed points from the ball, which had not exceeded energy of more than 105 joules. For some time intervals those removed points exceeded 105 joules, achieving 106 joules and even 109 joules (Hachay et al., 2010). Introduction of the additional velocity parameter of slow deformation wave propagation allowed us, with the use of phase diagrams, to identify the hierarchic structure. Further, we can use that information for the modelling and interpretation of seismic and deformation waves in hierarchic structures (Hachay et al., 2012). That method can be useful in building-up an understanding of the resonance outshooting of catastrophic dynamic events and prevent these events. References 1.Chulichkov A. (2003) Mathematical models of nonlinear dynamics. Moscow: Phismatlit. 294p. 2.Hachay O., Khachay O.Yu., Klimko V., et al. (2010) Reflection of synergetic features of rock massif state under the man-caused influence from the data of a seismological catalogue. Mining Information-Analytic Bulletin, Moscow, Mining book, 6, pp.259-271. 3.Hachay O., Khachay A.Yu. (2012) Research of stress-deforming state of hierarchic medium. Proceedings of the Third Tectonics and Physics Conference at the Institute of the Physics of the Earth 8-12 October 2012, Moscow, IFZ RAS, pp.114-117. 4.Kurlenja M., Oparin V., Vostrikov V. (1993) About forming elastic wave trains by impulse excitation of block medium. Waves of pendulum type Uμ. DAN USSR, V.133, 4, pp.475-481. 5.Naimark Yu., Landa P. (2009). Stochastic and chaotic oscillations. Moscow, Knigniy dom ,'LIBROKOM', 424 p. 7.Oparin V., Vostrikov V., Tapsiev A. et al. (2006) About one kinematic criterion of forecasting of the limiting massif state with use of seismological data , FTPRPI, 6, pp.3-10.

  7. Slow and Go: Pulsing slip rates on the creeping section of the San Andreas Fault

    NASA Astrophysics Data System (ADS)

    Turner, Ryan C.; Shirzaei, Manoochehr; Nadeau, Robert M.; Brgmann, Roland

    2015-08-01

    Rising and falling slip rates on the creeping section of the San Andreas Fault have been inferred from variations of recurrence intervals of characteristically repeating microearthquakes, but this observation has not previously been confirmed using modern geodetic data. Here we report on observations of this "pulsing" slip obtained from advanced multitemporal interferometric synthetic aperture radar (InSAR) data, confirmed using continuous GPS sites of the Plate Boundary Observatory. The surface deformation time series show a strong correlation to the previously documented slip rate variations derived from repeating earthquakes on the fault interface, at various spatial and temporal scales. Time series and spectral analyses of repeating earthquake and InSAR data reveal a quasiperiodic pulsing with a roughly 2 year period along some sections of the fault, with the earthquakes on the fault interface lagging behind the far-field deformation by about 6 months. This suggests a temporal delay between the pulsing crustal strain generated by deep-seated shear and the time-variable slip on the shallow fault interface, and that at least in some places this process may be cyclical. There exist potential impacts for time-dependent seismic hazard forecasting in California and, as it becomes better validated in the richly instrumented natural laboratory of the central San Andreas Fault, the process used here will be even more helpful in characterizing hazard and fault zone rheology in areas without California's geodetic infrastructure.

  8. Temperature-dependent creep buckling of plates

    NASA Technical Reports Server (NTRS)

    Ross, D. A.; Berke, L.

    1981-01-01

    Time-dependent lateral deflection of flat rectangular plates is predicted by the Norton-Bailey (Norton 1929, Bailey 1935) power law for material creep. The plates have a through-thickness steady-state temperature distribution, and the effects are considered by using Maxwell's law to modify the power creep law. Equations are derived for creep exponents of 3 and 5, using the sandwich plate element to predict creep buckling of plates. Predictions of creep buckling with a temperature variation between the inner and outer plate surfaces are found to be somewhat dependent on the creep buckling relationship assumed. When significant scatter justifies a variation in the creep constants up to an order of magnitude, discrepancies in predictions using the two exponents are reasonable, and for one engineering material, the predictions have the same degree of agreement with experimental data as have the respective creep laws.

  9. Characterization of the elastic and viscoelastic properties of dentin by a nanoindentation creep test.

    PubMed

    Chuang, Shu-Fen; Lin, Shih-Yun; Wei, Pal-Jen; Han, Chang-Fu; Lin, Jen-Fin; Chang, Hsien-Chang

    2015-07-16

    Dentin is the main supporting structure of teeth, but its mechanical properties may be adversely affected by pathological demineralization. The purposes of this study were to develop a quantitative approach to characterize the viscoelastic properties of dentin after de- and re-mineralization, and to examine the elastic properties using a nanoindentation creep test. Dentin specimens were prepared to receive both micro- and nano-indentation tests at wet and dry states. These tests were repeatedly performed after demineralization (1% citric acid for 3 days) and remineralization (artificial saliva immersion for 28 days). The nanoindentation test was executed in a creep mode, and the resulting displacement-time responses were disintegrated into primary (transient) and secondary (viscous) creep. The structural changes and mineral densities of dentin were also examined under SEM and microCT, respectively. The results showed that demineralization removed superficial minerals of dentin to the depth of 400 ?m, and affected its micro- and nano-hardness, especially in the hydrate state. Remineralization only repaired the minerals at the surface layer, and partially recovered the nanohardness. Both the primary the secondary creep increased in the demineralized dentin, while the hydration further enhanced creep deformation of untreated and remineralized dentin. Remineralization reduced the primary creep of dentin, but did not effectively increase the viscosity. In conclusion, water plasticization increases the transient and viscous creep strains of demineralized dentin and reduces load sustainability. The nanoindentation creep test is capable of analyzing the elastic and viscoelastic properties of dentin, and reveals crucial information about creep responses. PMID:25911251

  10. Simulation of microstructural evolution during superplastic deformation

    SciTech Connect

    Kim, B.N.; Hiraga, K.

    2000-07-01

    Superplastic tensile deformation is simulated in 2 dimensions by incorporating grain boundary diffusion and concurrent grain growth derived from static and dynamic growth mechanisms. The following relationship is found between microstructural changes and deformation behavior for constant stress conditions. Grain boundary diffusion produces an increase in the aspect ratio of the matrix grains during deformation and the increased aspect ratio causes a change in creep rate parameters: the stress exponent is decreased from the initial value of 1.0 for equiaxed grains and the grain size exponent is increased from the initial value of 3.0. Accelerated grain growth is also found by the present simulation.

  11. Creep-Fatigue Behavior of Alloy 617 at 850°C

    SciTech Connect

    Carroll, Laura

    2015-05-01

    Creep-fatigue deformation is expected to be a significant contributor to the potential factors that limit the useful life of the Intermediate Heat Exchanger (IHX) in the Very High Temperature Reactor (VHTR) nuclear system.[1] The IHX of a high temperature gas reactor will be subjected to a limited number of transient cycles due to start-up and shut-down operations imparting high local stresses on the component. This cycling introduces a creep-fatigue type of interaction as dwell times occur intermittently. The leading candidate alloy for the IHX is a nickel-base solid solution strengthened alloy, Alloy 617, which must safely operate near the expected reactor outlet temperature of up to 950 °C.[1] This solid solution strengthened nickel-base alloy provides an interesting creep-fatigue deformation case study because it has characteristics of two different alloy systems for which the cyclic behavior has been extensively investigated. Compositionally, it resembles nickel-base superalloys, such as Waspalloy, IN100, and IN718, with the exception of its lower levels of Al. At temperatures above 800 °C, the microstructure of Alloy 617, however, does not contain the ordered ?’ or ?’’ phases. Thus microstructurally, it is more similar to an austenitic stainless steel, such as 316 or 304, or Alloy 800H comprised of a predominantly solid solution strengthened matrix phase with a dispersion of inter- and intragranular carbides. Previous studies of the creep-fatigue behavior of Alloy 617 at 950 °C indicate that the fatigue life is reduced when a constant strain dwell is added at peak tensile strain.[2-5] This results from the combination of faster crack initiation occurring at surface-connected grain boundaries due to oxidation from the air environment along with faster, and intergranular, crack propagation resulting from the linking of extensive interior grain boundary cracking.[3] Saturation, defined as the point at which further increases in the strain-controlled hold time duration no longer decreases the cycle life, has been observed for Alloy 617 at 950 °C at least to the investigated hold times[2,3], as illustrated through a plot of cycles to failure v. hold time in Figure 1. The 950 °C creep-fatigue data set generated by Totemeier and Tian[5] at the 0.3% and 1.0% strain range is consistent in magnitude in terms of the cycles to failure data of that of Carroll et al., however, 0.3% strain range data did not exhibit saturation at hold times of up to 10 min. At 1.0% total strain, saturation in the number of cycles to failure was observed within the investigated peak tensile hold times of up to 10 min[5]. The data of Carroll et al.[2,3] in Figure 1 and Totemeier and Tian[5] is also consistent in magnitude with the data of Rao and coworkers[4] investigated at the 0.6% strain range. It should be noted that saturation in the number of cycles to failure is not present in the data published by Rao and coworkers[4] for tensile hold times of up to 120 min. The latter testing was in a simulated primary-circuit helium gas as opposed to air and a single data point is reported for the longer hold time conditions.

  12. An investigation on the creep and fracture behavior of cast nickel-base superalloy IN738LC

    NASA Astrophysics Data System (ADS)

    Jianting, Guo; Ranucci, D.; Picco, E.; Strocchi, P. M.

    1983-11-01

    The creep-rupture properties of cast nickel-base superalloy IN738LC were studied over the temperature range 750 to 950 °C. Our results show that primary and steady-state creep should not be regarded as distinct stages and that they have basically the same deformation mechanism. The dependence of the steady-state creep rate, ɛs, on stress, δ, and on temperature, T, for this superalloy can be described as ɛs = Aδ nexp( -Qc/RT). n = 8.3 - 9.8 and Qc = 570 - 730 kJ mol-1 at high stress levels, whereas n = 4.1 - 4.9 and Qc = 370 - 420 kJ mol-1 at low stress levels. The observations of dislocation structures during steady-state creep confirm that the creep mechanism is different in the high and low stress regimes. The observations of the microstructure show that the initial acceleration in creep rate during the tertiary stage is connected with changes in the size and distribution of γ' particles during creep. Rupture occurs by the propagation of oxidized intergranular cracks which initiate at the specimen surface, and the rate of crack propagation is controlled by the deformation behavior of the superalloy.

  13. The Effect of Holding Time on Nanoindentation Measurements of Creep in Bone

    PubMed Central

    Wu, Ziheng; Baker, Tyler A.; Ovaert, Timothy C.; Niebur, Glen L

    2011-01-01

    Viscoelasticity may affect both the elastic and fracture characteristics of bone. Nanoindentation can be used to measure the creep behavior of bone by fitting the depth vs. time data at constant load to rheological models. However, the creep data may be influenced by latent effects arising during the loading phase of indentation. As such, the loading protocol, particularly the holding time, may affect the measured creep time constants. To characterize the effect of holding time on the measures, four cortical bone samples were prepared from four bovine femora and subjected to nanoindentation to measure the creep behavior. The creep time constants were found by fitting the indentation depth vs. time curve to three different rheological models: the standard linear solid, Burgers model, and a two-dashpot Kelvin model. All three models provided good fits to the data, which were relatively insensitive to the initial parameter estimates. The calculated creep time constants increased monotonically with increasing holding time for all three models. However, the relative differences between measurements within a single osteon, within a single sample, and between samples were maintained for creep holding times over 16 s. Hence, while the creep time constants measured by nanoindentation with hold times up to 30 s may not provide accurate property measurements, comparisons between samples are valid if all are assessed at the same holding time. Considering the long-term viscosity of bone tissue, Burgers model provided the best performance in terms of stability and goodness of fit, and is recommended for future studies. PMID:21353675

  14. "A New Class of Creep Resistant Oxide/Oxide Ceramic Matrix Composites"

    SciTech Connect

    Dr. Mohit Jain, Dr. Ganesh Skandan, Prof. Roger Cannon, Rutgers University

    2007-03-30

    Despite recent progress in the development of SiC-SiC ceramic matrix composites (CMCs), their application in industrial gas turbines for distributed energy (DE) systems has been limited. The poor oxidation resistance of the non-oxide ceramics warrants the use of envrionmental barrier coatings (EBCs), which in turn lead to issues pertaining to life expectancy of the coatings. On the other hand, oxide/oxide CMCs are potential replacements, but their use has been limited until now due to the poor creep resistance at high temperatures, particularly above 1200 oC: the lack of a creep resistant matrix has been a major limiting factor. Using yttrium aluminum garnet (YAG) as the matrix material system, we have advanced the state-of-the-art in oxide/oxide CMCs by introducing innovations in both the structure and composition of the matrix material, thereby leading to high temperature matrix creep properties not achieved until now. An array of YAG-based powders with a unique set of particle characteristics were produced in-house and sintered to full density and compressive creep data was obtained. Aided in part by the composition and the microstructure, the creep rates were found to be two orders of magnitude smaller than the most creep resistant oxide fiber available commercially. Even after accounting for porosity and a smaller matrix grain size in a practical CMC component, the YAG-based matrix material was found to creep slower than the most creep resistant oxide fiber available commercially.

  15. Experimental Creep Life Assessment for the Advanced Stirling Convertor Heater Head

    NASA Technical Reports Server (NTRS)

    Krause, David L.; Kalluri, Sreeramesh; Shah, Ashwin R.; Korovaichuk, Igor

    2010-01-01

    The United States Department of Energy is planning to develop the Advanced Stirling Radioisotope Generator (ASRG) for the National Aeronautics and Space Administration (NASA) for potential use on future space missions. The ASRG provides substantial efficiency and specific power improvements over radioisotope power systems of heritage designs. The ASRG would use General Purpose Heat Source modules as energy sources and the free-piston Advanced Stirling Convertor (ASC) to convert heat into electrical energy. Lockheed Martin Corporation of Valley Forge, Pennsylvania, is integrating the ASRG systems, and Sunpower, Inc., of Athens, Ohio, is designing and building the ASC. NASA Glenn Research Center of Cleveland, Ohio, manages the Sunpower contract and provides technology development in several areas for the ASC. One area is reliability assessment for the ASC heater head, a critical pressure vessel within which heat is converted into mechanical oscillation of a displacer piston. For high system efficiency, the ASC heater head operates at very high temperature (850 C) and therefore is fabricated from an advanced heat-resistant nickel-based superalloy Microcast MarM-247. Since use of MarM-247 in a thin-walled pressure vessel is atypical, much effort is required to assure that the system will operate reliably for its design life of 17 years. One life-limiting structural response for this application is creep; creep deformation is the accumulation of time-dependent inelastic strain under sustained loading over time. If allowed to progress, the deformation eventually results in creep rupture. Since creep material properties are not available in the open literature, a detailed creep life assessment of the ASC heater head effort is underway. This paper presents an overview of that creep life assessment approach, including the reliability-based creep criteria developed from coupon testing, and the associated heater head deterministic and probabilistic analyses. The approach also includes direct benchmark experimental creep assessment. This element provides high-fidelity creep testing of prototypical heater head test articles to investigate the relevant material issues and multiaxial stress state. Benchmark testing provides required data to evaluate the complex life assessment methodology and to validate that analysis. Results from current benchmark heater head tests and newly developed experimental methods are presented. In the concluding remarks, the test results are shown to compare favorably with the creep strain predictions and are the first experimental evidence for a robust ASC heater head creep life.

  16. Microstructural stability and creep of directionally solidified alumina/YAG eutectic monofilaments

    NASA Astrophysics Data System (ADS)

    Matson, Lawrence Edwin

    2000-10-01

    Fiber strength retention and creep currently limit the use of polycrystalline oxide fibers in ceramic matrix composite applications up to 1100°C. Single phase - single crystal fibers show superior creep resistance up to 1500°C but have a significant strength loss at moderate temperatures due to processing flaws, which undergo slow crack growth. In hopes of overcoming these shortcomings, Directionally Solidified Al2O3 - YAG eutectic fibers were grown at various rates by the Edge-defined, Film-fed Growth method (EFG) and their microstructure and mechanical properties were studied in this thesis. It was hypothesized that these two phase - single crystal structures would exhibit an increase in strength and a decrease in slow crack growth rates as the transverse phase size decreases. Additionally, that the creep resistance would increase to single crystal values as the phase aspect ratio increased. A digital microstructural analysis procedure was developed as part of the thesis in order to quantify the various microstructures from the EFG processing study. Microstructural stability plays a significant role in determining the "use temperature and life" of fibers. Coarsening effects the strength, creep resistance, as well as the rupture life. In this work, the kinetics of homogeneous coarsening as well as heterogeneous coarsening on the bare fiber surfaces was investigated. A "site specific" TEM thin foil preparation method was developed so that the mechanism for coarsening could be analysis. A methodology was developed in order to determine if the creep behavior of a fiber was affected by any heterogeneous coarsening defect. Creep data which showed no effects was analyzed for its steady state creep behavior. The creep data showed a significant variation in the stress exponent as a function of test temperature and fiber microstructure. A threshold stress analysis was employed in order to obtain a reasonable effective activation energy of ≅1100 kJ/mole °K. TEM analysis of the crept fibers suggested that the Sapphire phase was deforming by a dislocation mechanism, while the YAG phase deformed by a diffusional mechanism. A creep model was developed which contained geometrical factors for describing the microstructure. Microstructural data from the digital analysis was entered into the creep model and validates the creep hypothesis.

  17. Corrosion and creep of dental amalgam.

    PubMed

    Gjerdet, N R; Espevik, S

    1978-01-01

    The influence of stress on corrosion was investigated by a potentiostatic technique. Amalgrams with low creep, both with and without gamma2-phase, revealed small increases in current with stress application while alloys with high creep exhibited large increases in current. Rupture of protective oxide due to increased strain for high creep alloys may explain the phenomenon. PMID:277492

  18. Advances in Non-contact Measurement of Creep Properties

    NASA Technical Reports Server (NTRS)

    Hyers, Robert W.; Canepari, Stacy; Rogers, Jan. R.

    2009-01-01

    Our team has developed a novel approach to measuring creep at extremely high temperatures using electrostatic levitation (ESL). This method has been demonstrated on niobium up to 2300 C, while ESL has melted tungsten (3400 C). High-precision machined spheres of the sample are levitated in the NASA MSFC ESL, a national user facility, and heated with a laser. The laser is aligned off-center so that the absorbed photons transfer their momentum to the sample, causing it to rotate at up to 250,000+ RPM. The rapid rotation loads the sample through centripetal acceleration, causing it to deform. The deformation of the sample is captured on high-speed video, which is analyzed by machine-vision software from the University of Massachusetts. The deformations are compared to finite element models to determine the constitutive constants in the creep relation. Furthermore, the noncontact method exploits stress gradients within the sample to determine the stress exponent in a single test. This method was validated in collaboration with the University of Tennessee for niobium at 1985 C, with agreement within the uncertainty of the conventional measurements. A similar method is being employed on Ultra-High-Temperature ZrB2- SiC composites, which may see application in rocket nozzles and sharp leading edges for hypersonic vehicles.

  19. Improved Creep Measurements for Ultra-High Temperature Materials

    NASA Technical Reports Server (NTRS)

    Hyers, Robert W.; Ye, X.; Rogers, Jan R.

    2010-01-01

    Our team has developed a novel approach to measuring creep at extremely high temperatures using electrostatic levitation (ESL). This method has been demonstrated on niobium up to 2300 C, while ESL has melted tungsten (3400 C). This method has been extended to lower temperatures and higher stresses and applied to new materials, including a niobium-based superalloy, MASC. High-precision machined spheres of the sample are levitated in the NASA MSFC ESL, a national user facility and heated with a laser. The samples are rotated with an induction motor at up to 30,000 revolutions per second. The rapid rotation loads the sample through centripetal acceleration, producing a shear stress of about 60 MPa at the center, causing the sample to deform. The deformation of the sample is captured on high-speed video, which is analyzed by machine-vision software from the University of Massachusetts. The deformations are compared to finite element models to determine the constitutive constants in the creep relation. Furthermore, the non-contact method exploits stress gradients within the sample to determine the stress exponent in a single test.

  20. Patterns of brittle deformation under extension on Venus

    NASA Technical Reports Server (NTRS)

    Neumann, G. A.; Zuber, M. T.

    1994-01-01

    The development of fractures at regular length scales is a widespread feature of Venusian tectonics. Models of lithospheric deformation under extension based on non-Newtonian viscous flow and brittle-plastic flow develop localized failure at preferred wavelengths that depend on lithospheric thickness and stratification. The characteristic wavelengths seen in rift zones and tessera can therefore provide constraints on crustal and thermal structure. Analytic solutions were obtained for growth rates in infinitesimal perturbations imposed on a one-dimensional, layered rheology. Brittle layers were approximated by perfectly-plastic, uniform strength, overlying ductile layers exhibiting thermally-activated power-law creep. This study investigates the formation of faults under finite amounts of extension, employing a finite-element approach. Our model incorporates non-linear viscous rheology and a Coulomb failure envelope. An initial perturbation in crustal thickness gives rise to necking instabilities. A small amount of velocity weakening serves to localize deformation into planar regions of high strain rate. Such planes are analogous to normal faults seen in terrestrial rift zones. These 'faults' evolve to low angle under finite extension. Fault spacing, orientation and location, and the depth to the brittle-ductile transition, depend in a complex way on lateral variations in crustal thickness. In general, we find that multiple wavelengths of deformation can arise from the interaction of crustal and mantle lithosphere.

  1. High temperature tensile deformation behavior of Grade 92 steel

    NASA Astrophysics Data System (ADS)

    Alsagabi, Sultan; Shrestha, Triratna; Charit, Indrajit

    2014-10-01

    Candidate structural materials for advanced reactors need to have superior high temperature strength and creep-rupture properties among other characteristics. The ferritic-martensitic Grade 92 steel (Fe-9Cr-2W-0.5Mo, wt.%) is considered such a candidate structural material. Tensile tests were performed at temperatures of 600, 650 and 700 C in the strain rate range of 10-5-10-3 s-1. After analyzing the tensile results using the Bird-Mukherjee-Dorn (BMD) equation, a stress exponent of about 9.5 and an activation energy of about 646 kJ/mol were obtained. In the light of high values of the stress exponent and activation energy, the threshold stress concept was used to elucidate the operating high temperature deformation mechanism. As a result of this modification, the true activation energy and stress exponent of the high temperature deformation in Grade 92 steel were found to be about 245 kJ/mol and 5, respectively. Thus, the dominant high temperature deformation mechanism was identified as the high temperature climb of edge dislocations and the appropriate constitutive equation was developed.

  2. Thermal creep model for CWSR zircaloy-4 cladding taking into account the annealing of the irradiation hardening

    SciTech Connect

    Cappelaere, Chantal; Limon, Roger; Duguay, Chrstelle; Pinte, Gerard; Le Breton, Michel; Bouffioux, Pol; Chabretou, Valerie; Miquet, Alain

    2012-02-15

    After irradiation and cooling in a pool, spent nuclear fuel assemblies are either transported for wet storage to a devoted site or loaded in casks for dry storage. During dry transportation or at the beginning of dry storage, the cladding is expected to be submitted to creep deformation under the hoop stress induced by the internal pressure of the fuel rod. The thermal creep is a potential mechanism that might lead to cladding failure. A new creep model was developed, based on a database of creep tests on as-received and irradiated cold-worked stress-relieved Zircaloy-4 cladding in a wide range of temperatures (310 degrees C to 470 degrees C) and hoop stress (80 to 260 MPa). Based on three laws-a flow law, a strain-hardening recovery law, and an annealing of irradiation hardening law this model allows the simulation of not only the transient creep and the steady-state creep, but also the early creep acceleration observed on irradiated samples tested in severe conditions, which was not taken into account in the previous models. The extrapolation of the creep model in the conditions of very long-term creep tests is reassuring, proving the robustness of the chosen formalism. The creep model has been assessed in progressively decreasing stress conditions, more representative of a transport. Set up to predict the cladding creep behavior under variable temperature and stress conditions, this model can easily be implemented into codes in order to simulate the thermomechanical behavior of spent fuel rods in various scenarios of postirradiation phases. (authors)

  3. Seismic anisotropy and mantle creep in young orogens

    USGS Publications Warehouse

    Meissner, R.; Mooney, W.D.; Artemieva, I.

    2002-01-01

    Seismic anisotropy provides evidence for the physical state and tectonic evolution of the lithosphere. We discuss the origin of anisotropy at various depths, and relate it to tectonic stress, geotherms and rheology. The anisotropy of the uppermost mantle is controlled by the orthorhombic mineral olivine, and may result from ductile deformation, dynamic recrystallization or annealing. Anisotropy beneath young orogens has been measured for the seismic phase Pn that propagates in the uppermost mantle. This anisotropy is interpreted as being caused by deformation during the most recent thermotectonic event, and thus provides information on the process of mountain building. Whereas tectonic stress and many structural features in the upper crust are usually orientated perpendicular to the structural axis of mountain belts, Pn anisotropy is aligned parallel to the structural axis. We interpret this to indicate mountain-parallel ductile (i.e. creeping) deformation in the uppermost mantle that is a consequence of mountain-perpendicular compressive stresses. The preferred orientation of the fast axes of some anisotropic minerals, such as olivine, is known to be in the creep direction, a consequence of the anisotropy of strength and viscosity of orientated minerals. In order to explain the anisotropy of the mantle beneath young orogens we extend the concept of crustal 'escape' (or 'extrusion') tectonics to the uppermost mantle. We present rheological model calculations to support this hypothesis. Mountain-perpendicular horizontal stress (determined in the upper crust) and mountain-parallel seismic anisotropy (in the uppermost mantle) require a zone of ductile decoupling in the middle or lower crust of young mountain belts. Examples for stress and mountain-parallel Pn anisotropy are given for Tibet, the Alpine chains, and young mountain ranges in the Americas. Finally, we suggest a simple model for initiating mountain parallel creep.

  4. Testing Protocol for Module Encapsulant Creep (Presentation)

    SciTech Connect

    Kempe, M. D.; Miller, D. C.; Wohlgemuth, J. H.; Kurtz, S. R.; Moseley, J. M.; Shah, Q.; Tamizhmani, G.; Sakurai, K.; Inoue, M.; Doi, T.; Masuda, A.

    2012-02-01

    Recently there has been an interest in the use of thermoplastic encapsulant materials in photovoltaic modules to replace chemically crosslinked materials, e.g., ethylene-vinyl acetate. The related motivations include the desire to: reduce lamination time or temperature; use less moisture-permeable materials; or use materials with better corrosion characteristics. However, the use of any thermoplastic material in a high-temperature environment raises safety and performance concerns, as the standardized tests currently do not expose the modules to temperatures in excess of 85C, yet modules may experience temperatures above 100C in operation. Here we constructed eight pairs of crystalline-silicon modules and eight pairs of glass/encapsulation/glass mock modules using different encapsulation materials of which only two were designed to chemically crosslink. One module set was exposed outdoors with insulation on the back side in Arizona in the summer, and an identical set was exposed in environmental chambers. High precision creep measurements and performance measurements indicate that despite many of these polymeric materials being in the melt state at some of the highest outdoor temperatures achievable, very little creep was seen because of their high viscosity, temperature heterogeneity across the modules, and in the case of the crystalline-silicon modules, the physical restraint of the backsheet. These findings have very important implications for the development of IEC and UL qualification and safety standards, and in regards to the necessary level of cure during the processing of crosslinking encapsulants.

  5. Haglund's Deformity

    MedlinePLUS

    ... Is Haglund’s Deformity? Haglund’s deformity is a bony enlargement on the back of the heel. The soft ... the Achilles tendon becomes irritated when the bony enlargement rubs against shoes. This often leads to painful ...

  6. Life at Mission Creep U

    ERIC Educational Resources Information Center

    Dubrow, Greg; Moseley, Bryan; Dustin, Daniel

    2006-01-01

    The term "mission creep" was originally coined nearly a hundred years ago to describe the gradual process by which a military mission's stated methods and goals change, and recently the term has been applied to incremental organizational changes. In this article, the term is used to describe what happens when a teaching-oriented college or

  7. COMPARISON OF CLADDING CREEP RUPTURE MODELS

    SciTech Connect

    P. Macheret

    2000-06-12

    The objective of this calculation is to compare several creep rupture correlations for use in calculating creep strain accrued by the Zircaloy cladding of spent nuclear fuel when it has been emplaced in the repository. These correlations are used to calculate creep strain values that are then compared to a large set of experimentally measured creep strain data, taken from four different research articles, making it possible to determine the best fitting correlation. The scope of the calculation extends to six different creep rupture correlations.

  8. Creep of CoO single crystals.

    NASA Technical Reports Server (NTRS)

    Clauer, A. H.; Seltzer, M. S.; Wilcox, B. A.

    1971-01-01

    The crystals were creep tested in compression over ranges of temperature, stress, and oxygen pressure. The creep curves were S-shaped, and only the inflection creep rate was analyzed. A formula is presented for the inflection creep rate in the range from 1000 to 1200 C, 850 to 1700 psi, and 0.001 to 1 atm oxygen. Slip was found to occur on two orthogonal slip systems. The presence of subboundaries was observed by optical and transmission electron microscopy. It is suggested that the creep rate is controlled by oxygen diffusion.

  9. Time-dependent deformation in unconsolidated reservoir sands

    NASA Astrophysics Data System (ADS)

    Chang, Carl Tingyu

    1998-12-01

    This dissertation discusses observations, implications, and micromechanical mechanisms of time-dependent deformation in dry reservoir sands from the Wilmington Field, Long Beach, California, and the South Eugene Island Field, Gulf of Mexico, with grain sizes between 10 to 300 mum under elevated pressures. Experimental results obtained in a triaxial loading system at confining pressures of 20-30 MPa and axial stresses of 40 MPa provide evidence of viscoelasticity as indicated by time-dependent deformation and ultrasonic pulse transmission data. Creep strain data suggests that dry sand deformed under high pressures has a fundamental creep and relaxation time constant. These results may provide a mechanism that explains creep, dispersion, and low differential stress observed in unconsolidated reservoir rocks. The combination of creep and relaxation implies that the dry rock matrix is viscoelastic which may result in dispersion even in the absence of pore fluids. The viscoelasticity of the dry sand matrix adds an additional relaxation time constant besides those associated with pore fluid motion thus complicating previous descriptions of frequency dependent moduli. Control groups of Ottawa sand mixed with small amounts of Montmorillonite clay suggest that the phenomena is controlled by the deformation of intergranular clay and not the deformation of quartz grains. Creep tests on synthetic idealized "two grain" models could replicate the creep strain observed in the sands with equal volume fractions of Montmorillonite clay indicating clay's role in the overall matrix rheology. It appears that microporosity reduction in the clays allows the quartz sand matrix to viscously rearrange its grains hence leading to time-dependent deformation.

  10. Madelung Deformity.

    PubMed

    Kozin, Scott H; Zlotolow, Dan A

    2015-10-01

    Madelung deformity of the wrist is more common in females and is often associated with Leri Weill dyschondrosteosis, a mesomelic form of dwarfism. Patients with Madelung deformity often report wrist deformity resulting from the prominence of the relatively long ulna. The typical Madelung deformity is associated with a Vickers ligament that creates a tether across the volar-ulnar radial physis that restricts growth across this segment. The distal radius deforms in the coronal (increasing radial inclination) and the sagittal (increasing volar tilt) planes. There is lunate subsidence and the proximal carpal row adapts to the deformity by forming an upside-down pyramid shape or triangle. Treatment depends on the age at presentation, degree of deformity, and magnitude of symptoms. Mild asymptomatic deformity warrants a period of nonsurgical management with serial x-ray examinations because the natural history is unpredictable. Many patients never require surgical intervention. Progressive deformity in the young child with considerable growth potential remaining requires release of Vickers ligament and radial physiolysis to prevent ongoing deterioration Concomitant ulnar epiphysiodesis may be necessary. Advanced asymptomatic deformity in older children with an unacceptable-appearing wrist or symptomatic deformity are indications for surgery. A dome osteotomy of the radius allows 3-dimensional correction of the deformity. Positive radiographic and clinical results after dome osteotomy have been reported. PMID:26341718

  11. Counter-intuitive Behavior of Subduction Zones: Weak Faults Rupture, Strong Faults Creep

    NASA Astrophysics Data System (ADS)

    Wang, K.; Gao, X.; Bilek, S. L.; Brown, L. N.

    2014-12-01

    Subduction interfaces that produce great earthquakes are often said to be "strongly coupled", and those that creep are said to be "weakly coupled". However, the relation between the strength and seismogenic behavior of subduction faults is far from clear. Seismological and geodetic observations of earthquake rupture usually provide information only on stress change, not fault strength. In this study, we infer fault strength by calculating frictional heating along megathrusts and comparing results with heat flow measurements. We find that stick-slip megathrusts that have produced great earthquakes such as at Japan Trench and northern Sumatra have very low apparent friction coefficients (~ 0.02 - 0.03), but megathrusts that creep such as at Northern Hikurangi and Manila Trench have higher values (up to ~0.13). The differnce cannot be explained by coseismic dynamic weakening of the stick-slip megathrusts, because the average stress drop in great earthquakes is usually less than 5 MPa, equivalent to a coseismic reduction of apparent friction coefficient by less than ~0.01. Therefore our results indicate differences in the static strength of different subduction faults. Why are the creeping faults stronger? We think it is related to their creeping mechanism. Very rugged subducting seafloor tends to cause creep and hinder great earthquake rupture (Wang and Bilek, 2014). In contrast, all giant earthquakes have occurred at subduction zones with relatively smooth subducting seafloor. Large geometrical irregularities such as seamounts generate heterogeneous structure and stresses that promote numerous small and medium size earthquakes and aseismic creep. The creeping is a process of breaking and wearing of geometrical irregularities in a deformation zone and is expected to be against relatively large resistance (strong creep). This is different from the creeping of smooth faults due to the presence of weak fault gouge (weak creep) such as along the creeping segment of the San Andreas fault. The general correlation between subducting seafloor ruggedness, creeping, and greater heat dissipation, if further verified, provides a new perspective in assessing earthquake and tsunami hazards for risk mitigation. Wang, K., and S. L. Bilek. Tectonophysics 610, 1-24 (2014).

  12. Effect of Mg on the Grain Growth and Dislocation Creep of Calcite

    NASA Astrophysics Data System (ADS)

    Xu, L.

    2004-12-01

    We tested the effect of variations in the amount of the solute impurity (Mg) on grain growth and strength of calcite aggregate. Synthetic marbles were produced by hot isostatic pressing mixtures of powders of calcite and dolomite at 850 C and 300 MPa confining pressure for different intervals (2 to 30 hrs). The HIP treatment resulted in homogeneous aggregates of calcite with Mg content from 0.5 to 17 mol%. Stress stepping tests and constant strain rate tests were used to examine the effect of Mg content on the dislocation creep of calcite. The grain growth rate under static conditions was decreased with Mg content from 7 to 17 mol%, indicating perhaps that grain boundary mobility is suppressed by the solute drag effect. In the diffusion creep at stresses below 40 Mpa, the strength of calcite decreases with increasing Mg content owing to the difference in grain size at 800 C and 300 MPa confining pressure. The contribution of dislocation creep increases with increasing stress, and the transition between diffusion and dislocation creep occurs at higher stresses for the samples with higher magnesium content and smaller grain size. The creep data were fit assuming a composite flow law consisting of a linear combination of diffusion and dislocation creep and a single-valued grain size. The best agreement was obtained by using a dislocation creep law with exponential dependence of strain rate on stress (e.g. Peierls law). More evidence from microstructure is needed to identify the dominant deformation mechanism conclusively. Most of the samples were compressed up to strains of 0.25; small recrystallized grains are formed resulting in a bimodal grain size distribution in some of the deformed samples. Preliminary data shows that the recrystallized grain sizes are smaller for Mg-calcite compared with that of pure calcite. This study will help to understand the effect of impurities on grain-growth kinetics and strain weakening in localized shear zones.

  13. Creep Behavior of Glass/Ceramic Sealant Used in Solid Oxide Fuel Cells

    SciTech Connect

    Liu, Wenning N.; Sun, Xin; Koeppel, Brian J.; Khaleel, Mohammad A.

    2010-01-02

    High operating temperature of solid oxide fuel cells require that sealant must function at high temperature between 600o and 900oC and in the oxidizing and reducing environments of fuel and air. It should be noted that creep deformation becomes relevant for a material when the operating temperature is near or exceeds half of its melting temperature (in degrees of Kelvin). The operating temperatures for most of the solid oxide fuel cells (SOFC) under development in the SECA program are around 800oC, which exceeds the glass transition temperature Tg for most glass ceramic materials. The goal of the study is to develop a creep model to capture the creep behavior of glass ceramic materials at high temperature and to investigate the effect of creep of glass ceramic sealant materials on stresses in glass seal and on the various interfaces of glass seal with other layers. The self-consistent creep models were incorporated into SOFC-MP and Mentat FC, and finite element analyses were performed to quantify the stresses in various parts. The stress in glass seals were released due to its creep behavior during the operating environments.

  14. Creep Behavior of High Temperature Alloys for Generation IV Nuclear Energy Systems

    NASA Astrophysics Data System (ADS)

    Wen, Xingshuo

    The Very High Temperature Reactor (VHTR) is one of the leading concepts of the Generation IV nuclear reactor development, which is the core component of Next Generation Nuclear Plant (NGNP). The major challenge in the research and development of NGNP is the performance and reliability of structure materials at high temperature. Alloy 617, with an exceptional combination of high temperature strength and oxidation resistance, has been selected as a primary candidate material for structural use, particularly in Intermediate Heat Exchanger (IHX) which has an outlet temperature in the range of 850 to 950C and an inner pressure from 5 to 20MPa. In order to qualify the material to be used at the operation condition for a designed service life of 60 years, a comprehensive scientific understanding of creep behavior at high temperature and low stress regime is necessary. In addition, the creep mechanism and the impact factors such as precipitates, grain size, and grain boundary characters need to be evaluated for the purpose of alloy design and development. In this study, thermomechanically processed specimens of alloy 617 with different grain sizes were fabricated, and creep tests with a systematic test matrix covering the temperatures of 850 to 1050C and stress levels from 5 to 100MPa were conducted. Creep data was analyzed, and the creep curves were found to be unconventional without a well-defined steady-state creep. Very good linear relationships were determined for minimum creep rate versus stress levels with the stress exponents determined around 3-5 depending on the grain size and test condition. Activation energies were also calculated for different stress levels, and the values are close to 400kJ/mol, which is higher than that for self-diffusion in nickel. Power law dislocation climb-glide mechanism was proposed as the dominant creep mechanism in the test condition regime. Dynamic recrystallization happening at high strain range enhanced dislocation climb and are believed to be responsible for the monotonically increasing creep rates. Apart from dislocation creep, diffusional creep in existence at low stress level in fine-grained (ASTM 8) material also contributed partly to the creep rates. A reasonable prediction on the long term performance of alloy 617 was also made by extrapolation method using optimized parameters based on creep test data. Furthermore, microstructure characterization was performed utilizing Optical Microscopy (OM), Scanning Electron Microscopy (SEM), Electron Backscattered Diffraction (EBSD), Transmission Electron Microscopy (TEM) and related analytical techniques on samples from both before and after creep, with special attention given to grain size effects, grain boundary type, and dislocation substructures. Evidences for dislocation climb and dislocation glide were found through detailed dislocation analysis by TEM, proving the dislocation climb-glide mechanism. The formation of subgrain boundary, the changes in boundary characters and grain sizes was confirmed by EBSD analysis for dynamic recrystallization. The effects of initial grain size and grain boundary character distribution on the creep behavior and mechanism were also evaluated. Through the results obtained from this experimental study, new insights were provided into how changes in microstructure take place during high temperature creep of alloy 617, creep mechanism at different conditions was identified, and the creep deformation model was discussed. The results will also serve to technological and code case development and design of materials for NGNP.

  15. A study on the creep mechanism of slate slope using model test

    NASA Astrophysics Data System (ADS)

    Weng, Meng-Chia; Lo, Chia-Ming; Wu, Cheng-Hsien; Chuang, Ting-Feng; Su, Yu-Hsuan

    2013-04-01

    Typhoon Morakot struck southern Taiwan in 2009 and brought the most extreme precipitation ever recorded in this area. The extreme amount of rain triggered lots of enormous landslides in the Lawnon River basin. Therefore, this research aims to explore the mechanism of slate slope failure in the Lawnon River basin. When the slate slope is influenced by wet deterioration and gravitation for a long time, significant creep deformation will develop between the foliation of slate and folds and faults will form in the rock mass. To simulate this phenomenon by discrete element method in the future, a series of physical model experiments with simplified mechanism were firstly performed in the laboratory. Based on the experimental setup, the influencing factors of the sliding behaviors, including the volume of rock block, topography, slope, foliation orientation were investigated. The result of this research showed that the creep deformation may deform more quickly under the condition of higher degree of slopes and foliations.

  16. Deformation mechanisms and impact attenuation characteristics of thin-walled collapsible air chambers used in head protection.

    PubMed

    Lamb, L; Hoshizaki, T B

    2009-11-01

    Head injuries are a major cause of morbidity and mortality worldwide, many resulting from sporting activities. There is a constant need in the head protection industry for improved methods to manage impacts and to reduce the risk of mild and severe head injuries. Contemporary head protection primarily consists of foam with several inherent disadvantages, including a limited ability to provide effective energy absorption under both low and high impact velocities. Recently, thin-walled collapsible chambers were engineered to address this problem and have been implemented into sport helmets. The chambers consist of four engineering elements which define their dynamic performance: geometry, air volume, material, and venting system. This research analysed the contribution of air flow through an orifice to the chamber's management of impact energy. The objective of this study was to determine the effect of the chamber's vent diameter and material stiffness on peak force and venting rate during an impact. Two material stiffnesses (thermoplastic polyurethane 45D and thermoplastic polyurethane 90A) and five vent diameters (1 mm, 2 mm, 3 mm, 4 mm, and 5 mm) were tested at three inbound velocities (1.3 m/s, 2.3 m/s, and 3.0 m/s). Each chamber was impacted ten times using a monorail drop system. Analysis of the results revealed that the material stiffness, vent diameter, and inbound velocity all had a significant effect on peak force and venting rate (p < 0.001). Under low inbound velocities the largest vent diameters transmitted a lower force than the smallest vent, while this relationship reversed at high inbound velocities. Under low velocities the air flowrate was negatively correlated and the flow duration was positively correlated to the peak force. Under high velocities, the air flowrate was positively correlated and the duration was negatively correlated to the peak force. This suggested that, under low velocities, chambers performed optimally when air was dissipated quickly, for a short duration; however, as the chamber approached a critical failure region, the increased duration and decreased velocity of air released prevented higher peak forces. This research confirmed that the differences in vent diameter and material stiffness significantly affected the impact force characteristics of engineered thin-walled collapsible chambers. PMID:20092098

  17. Rheological Characteristics of Weak Rock Mass and Effects on the Long-Term Stability of Slopes

    NASA Astrophysics Data System (ADS)

    Yang, Tianhong; Xu, Tao; Liu, Hongyuan; Zhang, Chunming; Wang, Shanyong; Rui, Yongqin; Shen, Li

    2014-11-01

    The creep deformation behavior of the northern slope of an open-pit mine is introduced. Direct shear creep tests are then conducted for the samples taken from the northern slope to study the rheological characteristics of the rock mass. The experimental results are analyzed afterwards using an empirical method to develop a rheological model for the rock mass. The proposed rheological model is finally applied to understand the creep behavior of the northern slope, predict the long-term stability, and guide appropriate measures to be taken at suitable times to increase the factor of safety to ensure stability. Through this study, a failure criterion is proposed to predict the long-term stability of the slope based on the rheological characteristics of the rock mass and a critical deformation rate is adopted to determine when appropriate measures should be taken to ensure slope stability. The method has been successfully applied for stability analysis and engineering management of the toppling and slippage of the northern slope of the open-pit mine. This success in application indicates that it is theoretically accurate, practically feasible, and highly cost-effective.

  18. Effect of subgrain structure on the creep strength of alloy 1207

    NASA Astrophysics Data System (ADS)

    Dudko, V. A.; Kaibyshev, R. O.; Salakhova, E. R.

    2009-01-01

    The effect of severe plastic deformation (SPD) on the creep resistance of the Al-6%Cu-0.48Mn-0.52Mg-0.3Sc-0.1Zr alloy has been examined in a temperature range of 125-180C. It has been shown that SPD performed by the method of equal-channel angular pressing at 300C to a true strain of 1 leads to the formation of a well-defined subgrain structure, which is retained upon solution treatment before quenching because of the presence in the alloy of ultradisperse Al3(Sc, Zr) particles with coherent boundaries. It was established that the creep strength at 125-150C of the as-cast alloy and of the deformed material is approximately the same. At 180C, the creep rate of the deformed aluminum alloy is almost an order of magnitude lower than that of the as-cast alloy. The reasons for the influence of the subgrain structure on the creep strength of the Al-Cu-Sc-Zr alloy are discussed.

  19. Impulsive radon emanation on a creeping segment of the San Andreas fault, California

    USGS Publications Warehouse

    King, C.-Y.

    1985-01-01

    Radon emanation was continuously monitored for several months at two locations along a creeping segment of the San Andreas fault in central California. The recorded emanations showed several impulsive increases that lasted as much as five hours with amplitudes considerably larger than meteorologically induced diurnal variations. Some of the radon increases were accompanied or followed by earthquakes or fault-creep events. They were possibly the result of some sudden outbursts of relatively radon-rich ground gas, sometimes triggered by crustal deformation or vibration. ?? 1985 Birkha??user Verlag.

  20. Non-isothermal elastoviscoplastic snap-through and creep buckling of shallow arches

    NASA Technical Reports Server (NTRS)

    Simitses, G. J.; Riff, R.

    1987-01-01

    The problem of buckling of shallow arches under transient thermomechanical loads is investigated. The analysis is based on nonlinear geometric and constitutive relations, and is expressed in a rate form. The material constitutive equations are capable of reproducing all non-isothermal, elasto-viscoplastic characteristics. The solution scheme is capable of predicting response which includes pre and postbuckling with creep and plastic effects. The solution procedure is demonstrated through several examples which include both creep and snap-through behavior.

  1. Monitoring microstructural evolution of alloy 617 with non-linear acoustics for remaining useful life prediction; multiaxial creep-fatigue and creep-ratcheting

    SciTech Connect

    Lissenden, Cliff; Hassan, Tasnin; Rangari, Vijaya

    2014-10-30

    The research built upon a prior investigation to develop a unified constitutive model for design-­by-­analysis of the intermediate heat exchanger (IHX) for a very high temperature reactor (VHTR) design of next generation nuclear plants (NGNPs). Model development requires a set of failure data from complex mechanical experiments to characterize the material behavior. Therefore uniaxial and multiaxial creep-­fatigue and creep-­ratcheting tests were conducted on the nickel-­base Alloy 617 at 850 and 950°C. The time dependence of material behavior, and the interaction of time dependent behavior (e.g., creep) with ratcheting, which is an increase in the cyclic mean strain under load-­controlled cycling, are major concerns for NGNP design. This research project aimed at characterizing the microstructure evolution mechanisms activated in Alloy 617 by mechanical loading and dwell times at elevated temperature. The acoustic harmonic generation method was researched for microstructural characterization. It is a nonlinear acoustics method with excellent potential for nondestructive evaluation, and even online continuous monitoring once high temperature sensors become available. It is unique because it has the ability to quantitatively characterize microstructural features well before macroscale defects (e.g., cracks) form. The nonlinear acoustics beta parameter was shown to correlate with microstructural evolution using a systematic approach to handle the complexity of multiaxial creep-­fatigue and creep-­ratcheting deformation. Mechanical testing was conducted to provide a full spectrum of data for: thermal aging, tensile creep, uniaxial fatigue, uniaxial creep-­fatigue, uniaxial creep-ratcheting, multiaxial creep-fatigue, and multiaxial creep-­ratcheting. Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM), and Optical Microscopy were conducted to correlate the beta parameter with individual microstructure mechanisms. We researched application of the harmonic generation method to tubular mechanical test specimens and pipes for nondestructive evaluation. Tubular specimens and pipes act as waveguides, thus we applied the acoustic harmonic generation method to guided waves in both plates and shells. Magnetostrictive transducers were used to generate and receive guided wave modes in the shell sample and the received signals were processed to show the sensitivity of higher harmonic generation to microstructure evolution. Modeling was initiated to correlate higher harmonic generation with the microstructure that will lead to development of a life prediction model that is informed by the nonlinear acoustics measurements.

  2. The physics of creep and attenuation in the mantle

    NASA Technical Reports Server (NTRS)

    Anderson, D. L.; Minster, J. B.

    1981-01-01

    The objective is to investigate the role of dislocations in both creep and attenuation. Attenuation in the mantle at seismic frequencies is thought to be caused by the glide of dislocations in the subgrains. Both kink and impurity drag can contribute to the glide time constant. The kink-formation, or Peierls barrier, model for dislocation glide is seen as a low-temperature, high-frequency mechanism most appropriate for pure systems. It is noted that a small amount of impurity drag brings the dislocation glide characteristic time into the seismic band at upper-mantle temperatures. The attenuation and creep behavior of the mantle are related by way of the dislocation structure. Analysis of the various possible mechanisms is facilitated by casting them and the geophysical data in terms of a pre-exponential characteristic time and an activation energy.

  3. Current understanding of superplastic deformation of Y-TZP and its application to joining.

    SciTech Connect

    Dominguez-Rodriguez, A.; Gutierrez-Mora; Jimenez-Melendo, M.; Routbort, J. L.; Chaim, R.; Energy Technology; Univ. de Sevilla; Technion - Israel Inst. of Tech.

    2001-04-15

    A review of the high-temperature, steady-state creep of yttria tetragonal zirconia polycrystals (Y-TZP) as a function of grain size, strain rate, stress, and temperature will be presented in this paper. Data have been analyzed using the standard creep equation incorporating a threshold stress. Microstructural observations of deformed samples indicated that deformation was achieved primarily by grain boundary sliding (GBS). This microscopic characteristic was used to join pieces of these materials. When two pieces of ceramics are compressed in the superplastic regime, GBS will produce a junction between the pieces. Several types of strong junctions have been produced, i.e. between pieces of the same material having different grain sizes, and between pieces of different materials. Scanning electron microscopy of the interfaces showed that each interface was cavity- and crack-free. Vickers indentations and high-temperature mechanical tests indicated that the interfaces were as strong as the matrix. This joining technique allows the construction of a complex shape or a functional gradient material.

  4. Room Temperature Creep Of SiC/SiC Composites

    NASA Technical Reports Server (NTRS)

    Morscher, Gregory N.; Gyekenyesi, Andrew; Levine, Stanley (Technical Monitor)

    2001-01-01

    During a recent experimental study, time dependent deformation was observed for a damaged Hi-Nicalon reinforced, BN interphase, chemically vapor infiltrated SiC matrix composites subjected to static loading at room temperature. The static load curves resembled primary creep curves. In addition, acoustic emission was monitored during the test and significant AE activity was recorded while maintaining a constant load, which suggested matrix cracking or interfacial sliding. For similar composites with carbon interphases, little or no time dependent deformation was observed. Evidently, exposure of the BN interphase to the ambient environment resulted in a reduction in the interfacial mechanical properties, i.e. interfacial shear strength and/or debond energy. These results were in qualitative agreement with observations made by Eldridge of a reduction in interfacial shear stress with time at room temperature as measured by fiber push-in experiments.

  5. Creep cavity observation using liquid metal embrittlement

    SciTech Connect

    Reiley, T.C.

    1981-01-01

    Grain boundary cavities, which form during high-temperature deformation and which may be considered incipient intergranular cracks, have been difficult to observe at the early growth stages. To examine grain boundaries in unfailed specimans one is normally limited to metallographic or transmission electron microscopy (TEM) techniques, the first having resolution limitations (r/sub cavity/approx.l..mu..m) and the second having limitations in the probability of seeing a cavity (especially for large-grained, low-density specimens) or of seeing a cavity which is undisturbed by the thinning process required for TEM. Other observational techniques involving hydrogen attack or low-temperature impact loading have been used to create brittle intergranular failures to observe grain boundary features, such as creep cavities on pre-crept specimens. These techniques are not, however, applicable to most metals, and as such, the need remains for a more general observational technique. Such a new technique employing liquid metal embrittlement (LME) is described below, and, given that most metals are severely embrittled by at least one liquid metal, this approach may satisfy requirements of general applicability.

  6. Rates of surficial rock creep on hillslopes in Western Colorado

    USGS Publications Warehouse

    Schumm, S.A.

    1967-01-01

    The average rate of downshope movement of rock fragments on shale hillslopes is directly proportional to the sine of the slope angle or that component of the gravitational force which acts parallel to the hillslope. The rates of surficial rock creep range from a few millimeters per year on a 3degree slope to almost 70 millimeters per year on a 40-degree slope, but these rates vary with natural variations in soil characteristics and microclimate, as well as with accidental disturbances.

  7. Creep of Structural Nuclear Composites

    SciTech Connect

    Will Windes; R.W. Lloyd

    2005-09-01

    A research program has been established to investigate fiber reinforced ceramic composites to be used as control rod components within a Very High Temperature Reactor (VHTR) design. Two candidate systems have been identified, carbon fiber reinforced carbon (Cf/C) and silicon carbide fiber reinforced silicon carbide (SiCf/SiC) composites. One of the primary degradation mechanisms anticipated for these core components is high temperature thermal and irradiation enhanced creep. As a consequence, high temperature test equipment, testing methodologies, and test samples for very high temperature (up to 1600º C) tensile strength and long duration creep studies have been established. Actual testing of both tubular and flat, "dog-bone"-shaped tensile composite specimens will begin next year. Since there is no precedence for using ceramic composites within a nuclear reactor, ASTM standard test procedures are currently being established from these high temperature mechanical tests.

  8. Proton Irradiation Creep in Pyrocarbon

    SciTech Connect

    Was, Gary S.; Campbell, Anne

    2011-10-01

    This project aims to understand irradiation creep in pyrocarbon using proton irradiation under controlled stresses and temperatures. Experiments will be conducted over a range of temperatures and stresses per the proposal submitted. The work scope will include the preparation of samples, measurement of deposition thickness, thickness uniformity, and anisotropy. The samples produced will be made in strips, which will be used for the creep experiments. Materials used will include pyrolytic carbon (PyC), Highly Oriented Pyrolytic Graphite (HOPG), or graphite strip samples in that order depending upon success. Temperatures tested under will range from 800C to 1200C, and stresses from 6MPa to 20.7MPa. Optional testing may occur at 900C and 1100C and stresses from 6MPa to 20.7MPa if funding is available.

  9. Effects of the regimes of heat treatment and of the magnitude and temperature of the inducing deformation on the characteristics of the shape-memory effect in the 43Ti-46Ni-9Nb-2Zr alloy

    NASA Astrophysics Data System (ADS)

    Popov, N. N.; Sysoeva, T. I.; Shchedrina, E. V.; Presnyakov, D. V.; Grishin, E. N.

    2015-06-01

    The influence of the types and regimes of heat treatment, as well as of the temperature and magnitude of the shape-memory-inducing deformation on the structural changes, martensitic transformations, parameters of the crystal lattice and substructure, and the mechanical and thermomechanical characteristics have been studied in the new shape-memory alloy of composition 43Ti-46Ni-9Nb-2Zr (at %). The conditions of the appearance and realization of the shape-memory effect have been determined. The relationship between the structural features and the values of the thermomechanical characteristics of the alloy has been revealed. The regimes of the heat treatment and of the deformation that induces the shape-memory effect, which provide in this alloy the obtaining of high thermomechanical characteristics, have been determined.

  10. Compression creep of filamentary composites

    NASA Technical Reports Server (NTRS)

    Graesser, D. L.; Tuttle, M. E.

    1988-01-01

    Axial and transverse strain fields induced in composite laminates subjected to compressive creep loading were compared for several types of laminate layups. Unidirectional graphite/epoxy as well as multi-directional graphite/epoxy and graphite/PEEK layups were studied. Specimens with and without holes were tested. The specimens were subjected to compressive creep loading for a 10-hour period. In-plane displacements were measured using moire interferometry. A computer based data reduction scheme was developed which reduces the whole-field displacement fields obtained using moire to whole-field strain contour maps. Only slight viscoelastic response was observed in matrix-dominated laminates, except for one test in which catastrophic specimen failure occurred after a 16-hour period. In this case the specimen response was a complex combination of both viscoelastic and fracture mechanisms. No viscoelastic effects were observed for fiber-dominated laminates over the 10-hour creep time used. The experimental results for specimens with holes were compared with results obtained using a finite-element analysis. The comparison between experiment and theory was generally good. Overall strain distributions were very well predicted. The finite element analysis typically predicted slightly higher strain values at the edge of the hole, and slightly lower strain values at positions removed from the hole, than were observed experimentally. It is hypothesized that these discrepancies are due to nonlinear material behavior at the hole edge, which were not accounted for during the finite-element analysis.

  11. Creep and shrinkage effects on integral abutment bridges

    NASA Astrophysics Data System (ADS)

    Munuswamy, Sivakumar

    Integral abutment bridges provide bridge engineers an economical design alternative to traditional bridges with expansion joints owing to the benefits, arising from elimination of expensive joints installation and reduced maintenance cost. The superstructure for integral abutment bridges is cast integrally with abutments. Time-dependent effects of creep, shrinkage of concrete, relaxation of prestressing steel, temperature gradient, restraints provided by abutment foundation and backfill and statical indeterminacy of the structure introduce time-dependent variations in the redundant forces. An analytical model and numerical procedure to predict instantaneous linear behavior and non-linear time dependent long-term behavior of continuous composite superstructure are developed in which the redundant forces in the integral abutment bridges are derived considering the time-dependent effects. The redistributions of moments due to time-dependent effects have been considered in the analysis. The analysis includes nonlinearity due to cracking of the concrete, as well as the time-dependent deformations. American Concrete Institute (ACI) and American Association of State Highway and Transportation Officials (AASHTO) models for creep and shrinkage are considered in modeling the time dependent material behavior. The variations in the material property of the cross-section corresponding to the constituent materials are incorporated and age-adjusted effective modulus method with relaxation procedure is followed to include the creep behavior of concrete. The partial restraint provided by the abutment-pile-soil system is modeled using discrete spring stiffness as translational and rotational degrees of freedom. Numerical simulation of the behavior is carried out on continuous composite integral abutment bridges and the deformations and stresses due to time-dependent effects due to typical sustained loads are computed. The results from the analytical model are compared with the published laboratory experimental and field data. The behavior of the laterally loaded piles supporting the integral abutments is evaluated and presented in terms of the lateral deflection, bending moment, shear force and stress along the pile depth.

  12. Deformation inside a paleosubduction channel - Insights from microstructures and crystallographic preferred orientations of eclogites and metasediments from the Tauern Window, Austria

    NASA Astrophysics Data System (ADS)

    Keppler, Ruth; Stipp, Michael; Behrmann, Jan H.; Ullemeyer, Klaus; Heidelbach, Florian

    2016-01-01

    The Eclogite Zone, of the Tauern Window is an exhumed subduction channel comprising eclogites with different grades of retrogression in a matrix of high-pressure metasediments. The rocks were exposed to 600 °C and 20-25 kbars, and then retrogressed during their exhumation, first under blueschist facies and later under amphibolite facies metamorphism. To gain insights into the deformation within the subduction channel during subduction and exhumation, both fresh and retrogressed eclogites, as well as the surrounding metasediments were investigated with respect to their deformation microstructures and crystallographic preferred orientations (CPOs). Pristine and retrogressed eclogites show grain boundary migration and subgrain rotation recrystallization microstructures in omphacite. A misorientation axes analysis reveals the activity of complementary deformation mechanisms including grain boundary sliding and dislocation creep. The omphacite CPOs of the eclogites correspond to dominant SL-fabrics characteristic of plane strain deformation, though there are local variations towards flattening or constriction within the paleosubduction channel. The glaucophane CPOs in retrogressed eclogites match those of omphacite, suggesting that a constant strain geometry persisted during exhumation at blueschist facies conditions. Plastic deformation of the host high-pressure metasediments outlasted that of the eclogites, as indicated by white mica fabrics and quartz CPO. The latter is consistently asymmetric, pointing to the operation of non-coaxial deformation. The microstructures and CPO data indicate a continuous plastic deformation cycle with eclogite and blueschist facies metamorphism related to subduction and exhumation of the different rock units.

  13. The Role of Eta Phase Formation on the Creep Strength and Ductility of INCONEL Alloy 740 at 1023 K (750 C)

    NASA Astrophysics Data System (ADS)

    Shingledecker, J. P.; Pharr, G. M.

    2012-06-01

    INCONEL alloy 740 is an age-hardenable nickel-based superalloy proposed for advanced ultrasupercritical steam boiler applications operating at high stress and long times above 973 K (700 C), where creep will be the dominate deformation mode. During high-temperature exposure, the alloy can form eta phase platelets that many have suggested may be detrimental to creep strength and ductility. In this study, creep-rupture tests were conducted on smooth and notched bars of INCONEL alloy 740 at 1023 K (750 C) for times up to 20,000 hours. Examination of the creep-rupture life, creep ductility, failure modes, and microstructure by quantitative electron microscopy shows that a small amount of eta phase does not diminish the creep performance. Applied stress appears to have a minor effect on the precipitation of the eta phase but not its growth rate. Based on the observation that the microstructure after 20,000 hours of creep exposure has reached equilibrium in comparison to thermodynamic calculations, it is concluded that 20,000 hour creep tests are adequate for prediction of long-term creep performance.

  14. The Role of Eta Phase Formation on the Creep Strength and Ductility of INCONEL Alloy 740 t 1023 k (750 Degrees C)

    SciTech Connect

    Shingledecker, John P; Pharr, George Mathews

    2012-01-01

    INCONEL alloy 740 is an age-hardenable nickel-based superalloy proposed for advanced ultrasupercritical steam boiler applications operating at high stress and long times above 973 K (700 C), where creep will be the dominate deformation mode. During high-temperature exposure, the alloy can form eta phase platelets that many have suggested may be detrimental to creep strength and ductility. In this study, creep-rupture tests were conducted on smooth and notched bars of INCONEL alloy 740 at 1023 K (750 C) for times up to 20,000 hours. Examination of the creep-rupture life, creep ductility, failure modes, and microstructure by quantitative electron microscopy shows that a small amount of eta phase does not diminish the creep performance. Applied stress appears to have a minor effect on the precipitation of the eta phase but not its growth rate. Based on the observation that the microstructure after 20,000 hours of creep exposure has reached equilibrium in comparison to thermodynamic calculations, it is concluded that 20,000 hour creep tests are adequate for prediction of long-term creep performance.

  15. Control of epoxy creep using graphene.

    PubMed

    Zandiatashbar, Ardavan; Picu, Catalin R; Koratkar, Nikhil

    2012-06-11

    The creep behavior of epoxy-graphene platelet (GPL) nanocomposites with different weight fractions of filler is investigated by macroscopic testing and nanoindentation. No difference is observed at low stress and ambient temperature between neat epoxy and nanocomposites. At elevated stress and temperature the nanocomposite with the optimal weight fraction, 0.1 wt% GPLs, creeps significantly less than the unfilled polymer. This indicates that thermally activated processes controlling the creep rate are in part inhibited by the presence of GPLs. The phenomenon is qualitatively similar at the macroscale and in nanoindentation tests. The results are compared with the creep of epoxy-single-walled (SWNT) and multi-walled carbon nanotube (MWNT) composites and it is observed that creep in both these systems is similar to that in pure epoxy, that is, faster than creep in the epoxy-GPL system considered in this work. PMID:22378720

  16. Empirical law for fault-creep events

    USGS Publications Warehouse

    Crough, S.T.; Burford, R.O.

    1977-01-01

    Fault-creep events measured on the San Andreas and related faults near Hollister, California, can be described by a rheological model consisting of a spring, power-law dashpotand sliding block connected in series. An empirical creep-event law, derived from many creep-event records analyzed within the constraints of the model, provides a remarkably simple and accurate representation of creep-event behavior. The empirical creep law is expressed by the equation: D(t)= Df [1-1/{ct(n-1)Dfn-1+1}/(n-1)] where D is the value of displacement at time t following the onset of an event, Df is the final equilibrium value of the event displacementand C is a proportionality constant. This discovery should help determine whether the time-displacement character of creep events is controlled by the material properties of fault gouge, or by other parameters. ?? 1977.

  17. Low cycle fatigue and creep-fatigue behavior of Ni-based alloy 230 at 850 C

    SciTech Connect

    Chen, Xiang; Yang, Zhiqing; Sokolov, Mikhail A; ERDMAN III, DONALD L; Mo, Kun; Stubbins, James

    2013-01-01

    Strain-controlled low cycle fatigue (LCF) and creep-fatigue testing of Ni-based alloy 230 were carried out at 850 C. The material creep-fatigue life decreased compared with its low cycle fatigue life at the same total strain range. Longer hold time at peak tensile strain further reduced the material creep-fatigue life. Based on the electron backscatter diffraction, a novel material deformation characterization method was applied, which revealed that in low cycle fatigue testing as the total strain range increased, the deformation was segregated to grain boundaries since the test temperature was higher than the material equicohesive temperature and grain boundaries became weaker regions compared with grains. Creep-fatigue tests enhanced the localized deformation, resulting in material interior intergranular cracking, and accelerated material damage. Precipitation in alloy 230 helped slip dispersion, favorable for fatigue property, but grain boundary cellular precipitates formed after material exposure to the elevated temperature had a deleterious effect on the material low cycle fatigue and creep-fatigue property.

  18. Subsurface Creep and Geometry of the Hayward-Calaveras Stepover

    NASA Astrophysics Data System (ADS)

    Evans, E. L.; Bürgmann, R.; Meade, B.; Houlie, N.; Nadeau, R.; Funning, G. J.

    2008-12-01

    The San Francisco Bay Area has not experienced a major earthquake beneath and urban center since 1906. The Hayward fault is the most populated fault in the area, and 140 years after its last rupture, also has the greatest risk associated with it. A contiguous subsurface stepover connecting the Hayward and the Calaveras faults appears to directly transfer slip between the two faults, and may affect earthquake rupture scenarios on both faults. Although the Hayward fault is partially locked for much of its trace, the southernmost fault creeps up to 9 mm/yr, equal to its long-term slip rate. At the proposed juncture region, the southern Calaveras fault also exhibits a surface creep rate close to total slip rate of 15mm/yr. Although, creep on the northern Calaveras is poorly constrained, its geologic slip rate is about 6 mm/yr, suggesting direct slip transfer from the southern Calaveras to the Hayward fault. Relocated seismicity outlines an eastward-dipping Hayward fault which appears to dip into and merge with the central Calaveras fault at depth. Additionally, characteristic repeating earthquakes through the stepover indicate that subsurface creep occurs between the two faults. Using both continuous GPS and updated GPS campaign data, we re-evaluate slip on Bay Area faults, and map slip through the Hayward-Calaveras stepover using a contiguous fault model. We use background seismicity and repeating earthquakes to constrain the geometry of the stepover, and invert GPS and InSAR data for slip. We interpret our map of creep transfer between the Hayward and Calaveras faults for its implications for seismic rupture through the stepover and seismic hazard in the Bay Area.

  19. On the theory of critical currents and flux flow in superconductors by the mechanism of plastic deformation of the flux-line lattice

    SciTech Connect

    Welch, D.O.

    1999-07-01

    In this paper the author will discuss how the nature of the stress state in the flux-line lattice (FLL) of superconductors arises from the distribution, density, geometry, and strength of pinning centers. Under certain conditions this stress causes the onset of plastic deformation in the FLL for values of the current density below that required for flux-flow by general depinning. He will describe an analytic framework, based on a theory of plasticity of the FLL, which describes the flux-flow characteristics, including the possibility of thermally-activated flow and flux creep.

  20. High temperature creep of SiC densified using a transient liquid phase

    SciTech Connect

    Jou, Z.C.; Virkar, A.V. ); Cutler, R.A. )

    1991-09-01

    Silicon carbide-based ceramics can be rapidly densified above approximately 1850 {degree}C due to a transient liquid phase resulting from the reaction between alumina and aluminum oxycarbides. The resulting ceramics are fine-grained, dense, and exhibit high strength at room temperature. SiC hot pressed at 1875 {degree}C for 10 min in Ar was subjected to creep deformation in bending at elevated temperatures between 1500 and 1650 {degree}C in Ar. Creep was thermally activated with an activation energy of 743 kJ/mol. Creep rates at 1575 {degree}C were between 10{sup {minus}9}/s and 10{sup {minus}7}/s at an applied stress between 38 and 200 MPa, respectively, resulting in a stress exponent of {approx}1.7.

  1. Theoretical and practical differences between creep and relaxation Poisson's ratios in linear viscoelasticity

    NASA Astrophysics Data System (ADS)

    Aili, Abudushalamu; Vandamme, Matthieu; Torrenti, Jean-Michel; Masson, Benoit

    2015-11-01

    Poisson's ratio is a well-defined parameter in elasticity. For time-dependent materials, multiple definitions based on the ratios between lateral and axial deformations are available. Here, we focus ourselves on the two most widely used definitions in the time domain, which define time-dependent functions that we call relaxation Poisson's ratio and creep Poisson's ratio. Those two ratios are theoretically different, but are linked in an exact manner through an equation we derive. We show that those two functions are equal at both initial and large times and that their derivatives with respect to time also are. Based on simple rheological models for both the deviatoric and volumetric creep behaviors, we perform a parametric study and show that the difference between those two time-dependent Poisson's ratios can be significant. However, based on creep data available in the literature, we show that, for cementitious materials, this difference can be negligible or not, depending on the case.

  2. Effect of Nb and Cu on the high temperature creep properties of a high MnN austenitic stainless steel

    SciTech Connect

    Lee, Kyu-Ho; Suh, Jin-Yoo; Huh, Joo-Youl; Park, Dae-Bum; Hong, Sung-Min; Shim, Jae-Hyeok; Jung, Woo-Sang

    2013-09-15

    The effect of Nb and Cu addition on the creep properties of a high MnN austenitic stainless steel was investigated at 600 and 650 C. In the original high MnN steel, which was initially precipitate-free, the precipitation of M{sub 23}C{sub 6} (M = Cr, Fe) and Cr{sub 2}N took place mostly on grain boudaries during creep deformation. On the other hand, the minor addition of Nb resulted in high number density of Z-phases (CrNbN) and MX (M = Nb; X = C, N) carbonitrides inside grains by combining with a high content of N, while suppressing the formation of Cr{sub 2}N. The addition of Cu gave rise to the independent precipitation of nanometer-sized metallic Cu particles. The combination of the different precipitate-forming mechanisms associated with Z-phase, MX and Cu-rich precipitates turned out to improve the creep-resistance significantly. The thermodynamics and kinetics of the precipitation were discussed using thermo-kinetic simulations. - Highlights: The creep rupture life was improved by Nb and Cu addition. The creep resistance of the steel A2 in this study was comparable to that of TP347HFG. The size of Z-phase and MX carbonitride did not change significantly after creep test. The nanometer sized Cu-rich precipitate was observed after creep. The predicted size of precipitates by MatCalc agreed well with measured size.

  3. Triaxial creep measurements on rock salt from the Jennings dome, Louisiana, borehole LA-1, core {number_sign}8

    SciTech Connect

    Wawersik, W.R.; Zimmerer, D.J.

    1994-05-01

    Tejas Power Company requested that facilities in the Rock Mechanics Laboratory at Sandia National Laboratories be used to assess the time-dependent properties of rock salt from the Jennings dome in Acadia Parish, Louisiana. Nominally 2.5-inch diameter slat core from borehole LA-1, core 8 (depth 3924.8 to 3837.8 ft; 1196.8--1197.1 m) was provided to accomplish two tasks: (1) Using the smallest possible number of experiments, evaluate the tendency of Jennings salt to undergo time-dependent deformation (creep) under constant applied stresses, and compare the creep of Jennings salt with creep data for rock salt from other locations. (2) Assess the applicability of published laboratory-derived creep properties for rock salt from several bedded and domal sites in finite element analyses concerning the design of new gas storage caverns in the Jennings dome. The characterization of Jennings salt followed the same strategy that was applied in earlier laboratory experiments on core from the Moss Bluff dome near Houston, Texas. This report summarizes the relevant details of five creep experiments on a sample from depth 3927.5 ft, the results obtained, and how these results compared with laboratory creep measurements gathered on rock salt from other locations including the West Hackberry, Bryan Mound and Moss Bluff domes. The report also considers the estimates of specific creep parameters commonly used in numerical engineering design analyses.

  4. Cumulative creep damage for polycarbonate and polysulfone

    NASA Technical Reports Server (NTRS)

    Zhang, M.; Brinson, H. F.

    1985-01-01

    The literature for creep to failure cumulative damage laws are reviewed. Creep to failure tests performed on polycarbonate and polysulfone under single and two step loadings are discussed. A cumulative damage law or modified time fraction rule is developed using a power law for transient creep response as the starting point. Experimental results are approximated well by the new rule. Damage and failure mechanisms associated with the two materials are suggested.

  5. Plastic Creep and Brittle-Ductile Transition in Hydrated Rocks of the Plate Interface

    NASA Astrophysics Data System (ADS)

    Reynard, B.

    2014-12-01

    Geophysical observations suggest that the formation of hydrous phyllosilicate-bearing rocks such as serpentinites favor aseismic slip on the plate interface. I review our current understanding of deformation of serpentines and similar phyllosilicates in the first 100 km of subduction and discuss some pending questions on measurements and modeling of the behavior and properties of the complex serpentinite rocks. Experimental studies suggest that serpentines have low enough mechanical strength to act as a "stabilizer" of stable creep, but the actual strength of serpentinites will depend on the exact nature of the crystallographic structure and fabric of the stable serpentine variety. Low-temperature, flat-layered lizardite has strong anisotropy in strength. Lizardite-serpentinite strength will depend crystal-preferred orientation (CPO), with isotropic texture having high strength (>300 MPa) and foliated serpentinites having small strength (<100 MPa), independent of temperature, pressure, and strain rate. Thus, the transition between brittle and plastic (or stable creep) behavior may result from progressive deformation. High-temperature serpentine antigorite has a complex corrugated-layered structure, and complex deformation modes were evidenced from experimental studies. Mechanical strength shows a strong stress dependence, suggesting dislocation-creep, and low temperature dependence, suggesting plastic behavior. Extrapolation of experimental results to natural strain rates suggests that antigorite-serpentinites have low strength (<100 MPa or lower), and will favor stable-creep. However, the extrapolation relies on mechanical flow laws that may not apply to serpentine. Electron microscopy observations reveals dislocation-like deformation mechanisms that are not sufficient to explain global deformation of antigorite aggregates, and that are likely accompanied by dissolution-precipitation at low natural strain-rates. Establishing reliable flow laws relevant to the subduction interface in the 30-100 km depth range will require further experimental investigations of such mechanisms.

  6. Structural Benchmark Creep Testing for the Advanced Stirling Convertor Heater Head

    NASA Technical Reports Server (NTRS)

    Krause, David L.; Kalluri, Sreeramesh; Bowman, Randy R.; Shah, Ashwin R.

    2008-01-01

    The National Aeronautics and Space Administration (NASA) has identified the high efficiency Advanced Stirling Radioisotope Generator (ASRG) as a candidate power source for use on long duration Science missions such as lunar applications, Mars rovers, and deep space missions. For the inherent long life times required, a structurally significant design limit for the heater head component of the ASRG Advanced Stirling Convertor (ASC) is creep deformation induced at low stress levels and high temperatures. Demonstrating proof of adequate margins on creep deformation and rupture for the operating conditions and the MarM-247 material of construction is a challenge that the NASA Glenn Research Center is addressing. The combined analytical and experimental program ensures integrity and high reliability of the heater head for its 17-year design life. The life assessment approach starts with an extensive series of uniaxial creep tests on thin MarM-247 specimens that comprise the same chemistry, microstructure, and heat treatment processing as the heater head itself. This effort addresses a scarcity of openly available creep properties for the material as well as for the virtual absence of understanding of the effect on creep properties due to very thin walls, fine grains, low stress levels, and high-temperature fabrication steps. The approach continues with a considerable analytical effort, both deterministically to evaluate the median creep life using nonlinear finite element analysis, and probabilistically to calculate the heater head s reliability to a higher degree. Finally, the approach includes a substantial structural benchmark creep testing activity to calibrate and validate the analytical work. This last element provides high fidelity testing of prototypical heater head test articles; the testing includes the relevant material issues and the essential multiaxial stress state, and applies prototypical and accelerated temperature profiles for timely results in a highly controlled laboratory environment. This paper focuses on the last element and presents a preliminary methodology for creep rate prediction, the experimental methods, test challenges, and results from benchmark testing of a trial MarM-247 heater head test article. The results compare favorably with the analytical strain predictions. A description of other test findings is provided, and recommendations for future test procedures are suggested. The manuscript concludes with describing the potential impact of the heater head creep life assessment and benchmark testing effort on the ASC program.

  7. Micromechanics of brittle creep and implications for the strength of the upper crust

    NASA Astrophysics Data System (ADS)

    Brantut, N.; Baud, P.; Heap, M. J.; Meredith, P. G.

    2012-04-01

    In the upper crust, the chemical influence of pore water or other aqueous solutions promotes time dependent brittle deformation through sub-critical crack growth. Sub-critical crack growth allows rocks to deform and fail at stresses far below their short-term failure strength, and even at constant applied stress ("brittle creep"). Here we present a new micromechanical model describing time dependent brittle creep of water-saturated rocks under triaxial stress conditions. Macroscopic brittle creep is modelled on the basis of microcrack extension under compressive stresses due to sub-critical crack growth. The incremental strains due to the growth of cracks in compression are derived from the sliding wing crack model of Ashby and Sammis (1990). Crack length evolution is computed from Charles' power law description of stress corrosion crack growth. The macroscopic strains and strain rates computed from the model are non-linear and compare well with experimental results obtained on granite, low porosity sandstone and basalt samples. Primary creep (decelerating strain rate) corresponds to decelerating crack growth, due to an initial decrease in stress intensity factor with increasing crack length in compression. Tertiary creep (accelerating strain rate as failure is approached) corresponds to an increase in crack growth rate due to crack interactions. Secondary creep, with apparently constant strain rate, arises as merely an inflexion between these two end-member phases. The strain rate at the inflexion point can be estimated analytically as a function of model parameters, effective confining pressure and temperature conditions, which provides an approximate creep law for the process. The creep law is used to infer the long term differential stress as a function of depth in the upper crust for tectonic loading rates: sub-critical cracking induces an offset of the rock strength, which is equivalent to a decrease in cohesion. For porous rocks, the competition between sub-critical crack growth and pressure solution has also been investigated, and brittle creep appears to be the dominant mechanism only at high (> 10-10 s-1) strain rates and shallow (< 1 km) depth in the crust.

  8. Strain localization during deformation of Westerly granite

    NASA Technical Reports Server (NTRS)

    Brodsky, N. S.; Spetzler, H. A.

    1984-01-01

    A specimen of Westerly granite was cyclically loaded to near failure at 50 MPa confining pressure. Holographic interferometry provided detailed measurements of localized surface deformations during loading and unloading. The data are consistent with deformation occurring primarily elastically at low differential stress; in conjunction with one incipient fault zone between approximately 350 and 520 MPa differential stress; and in conjunction with a second incipient fault zone above 580 MPa and/or during creep. During unloading only one fault zone, that which is active at the intermediate stress levels during loading, is seen to recede.

  9. Model for transient creep of southeastern New Mexico rock salt

    SciTech Connect

    Herrmann, W; Wawersik, W R; Lauson, H S

    1980-11-01

    In a previous analysis, existing experimental data pertaining to creep tests on rock salt from the Salado formation of S.E. New Mexico were fitted to an exponential transient creep law. While very early time portions of creep strain histories were not fitted very well for tests at low temperatures and stresses, initial creep rates in particular generally being underestimated, the exponential creep law has the property that the transient creep strain approaches a finite limit with time, and is therefore desirable from a creep modelling point of view. In this report, an analysis of transient creep is made. It is found that exponential transient creep can be related to steady-state creep through a universal creep curve. The resultant description is convenient for creep analyses where very early time behavior is not important.

  10. Time temperature-stress dependence of boron fiber deformation

    NASA Technical Reports Server (NTRS)

    Dicarlo, J. A.

    1976-01-01

    Flexural stress relaxation (FSR) and flexural internal friction (FIF) techniques were employed to measure the time-dependent deformation of boron fibers from -190 to 800 C. The principal specimens were 203 micrometers diameter fibers commercially produced by chemical vapor deposition (CVD) on a 13 micrometer tungsten substrate. The observation of complete creep strain recovery with time and temperature indicated that CVD boron fibers deform flexurally as anelastic solids with no plastic component.

  11. Behavior of Conductive Particle Networks in Polymer Melts under Deformation

    NASA Astrophysics Data System (ADS)

    Star, Zden?k; Krckel, Johannes; Schubert, Dirk; Mnstedt, Helmut

    2011-07-01

    The electrical properties of the composites containing conductive fillers are given by the structure of the particle network. Therefore, the behavior of these networks under deformation in the molten state is of great interest in order to obtain materials with desirable electrical properties. In this work the composites containing carbon black or carbon fibers were exposed to a shear deformation in two different experimental modesoscillation and creep and the electrical conductivity of the materials was measured simultaneously.

  12. Earthquakes and fault creep on the northern San Andreas fault

    USGS Publications Warehouse

    Nason, R.

    1979-01-01

    At present there is an absence of both fault creep and small earthquakes on the northern San Andreas fault, which had a magnitude 8 earthquake with 5 m of slip in 1906. The fault has apparently been dormant after the 1906 earthquake. One possibility is that the fault is 'locked' in some way and only produces great earthquakes. An alternative possibility, presented here, is that the lack of current activity on the northern San Andreas fault is because of a lack of sufficient elastic strain after the 1906 earthquake. This is indicated by geodetic measurements at Fort Ross in 1874, 1906 (post-earthquake), and 1969, which show that the strain accumulation in 1969 (69 ?? 10-6 engineering strain) was only about one-third of the strain release (rebound) in the 1906 earthquake (200 ?? 10-6 engineering strain). The large difference in seismicity before and after 1906, with many strong local earthquakes from 1836 to 1906, but only a few strong earthquakes from 1906 to 1976, also indicates a difference of elastic strain. The geologic characteristics (serpentine, fault straightness) of most of the northern San Andreas fault are very similar to the characteristics of the fault south of Hollister, where fault creep is occurring. Thus, the current absence of fault creep on the northern fault segment is probably due to a lack of sufficient elastic strain at the present time. ?? 1979.

  13. Progress Report on Long Hold Time Creep Fatigue of Alloy 617 at 850°C

    SciTech Connect

    Carroll, Laura Jill

    2015-10-01

    Alloy 617 is the leading candidate material for an intermediate heat exchanger for the very high temperature reactor. To evaluate the behavior of this material in the expected service conditions, strain-controlled cyclic tests that include long hold times up to 240 minutes at maximum tensile strain were conducted at 850°C. In terms of the total number of cycles to failure, the fatigue resistance decreased when a hold time was added at peak tensile strain. Increases in the tensile hold duration degraded the creep-fatigue resistance, at least to the investigated strain controlled hold time of up to 60 minutes at the 0.3% strain range and 240 minutes at the 1.0% strain range. The creep-fatigue deformation mode is considered relative to the lack of saturation, or continually decreasing number of cycles to failure with increasing hold times. Additionally, preliminary values from the 850°C creep-fatigue data are calculated for the creep-fatigue damage diagram and have higher values of creep damage than those from tests at 950°C.

  14. Creep-fatigue as a possible cause of dental amalgam margin failure.

    PubMed

    Williams, P T; Hedge, G L

    1985-03-01

    Fracture of the margins is the most common cause of failure of dental amalgam restorations. Both corrosion and creep have been identified as possible contributors to this type of failure. The stresses that induce creep may arise from the continued setting expansion of the amalgam, the formation of corrosion products, mastication, or from the thermal expansion of the amalgam during ingestion of hot foods. The latter two are low-frequency cyclic stresses. The amalgams used in dentistry have fusion temperatures only about 40 degrees C above mouth temperature, and they experience grain boundary sliding during creep deformation. Since grain boundary sliding, low-frequency cyclic stresses, and a temperature near the fusion temperature of the alloy are prerequisites for so-called "creep-fatigue fracture", this type of fracture may contribute to amalgam margin failure. Amalgam made from seven different alloys was condensed into stainless steel dies. After being allowed to set for seven days, the specimens were thermally cycled between 4 degrees C and 50 degrees C for 500 and 1000 cycles. Amalgam margin integrity was evaluated by scanning electron microscopy both before and after each cycling period. The amount of margin fracture was calculated after 1000 cycles. Thermal cycling of amalgam restorations placed in stainless steel dies resulted in predominantly intergranular fracturing of the amalgam margins, indicating that creep-fatigue failure may be a significant contributor to in vivo margin fracturing. PMID:3855901

  15. Development of a simplified procedure for rocket engine thrust chamber life prediction with creep

    NASA Technical Reports Server (NTRS)

    Badlani, M. L.; Porowski, J. S.; Odonnell, W. J.; Peterson, D. B.

    1983-01-01

    An analytical method for predicting engine thrust chamber life is developed. The method accounts for high pressure differentials and time-dependent creep effects both of which are significant in limiting the useful life of the shuttle main engine thrust chamber. The hot-gas-wall ligaments connecting adjacent cooling channels ribs and separating the coolant flow from the combustion gas are subjected to a high pressure induced primary stress superimposed on an alternating cyclic thermal strain field. The pressure load combined with strain-controlled cycling produces creep ratcheting and consequent bulging and thinning of these ligaments. This mechanism of creep-enhanced ratcheting is analyzed for determining the hot-gas-wall deformation and accumulated strain. Results are confirmed by inelastic finite element analysis. Fatigue and creep rupture damage as well as plastic tensile instability are evaluated as potential failure modes. It is demonstrated for the NARloy Z cases analyzed that when pressure differentials across the ligament are high, creep rupture damage is often the primary failure mode for the cycle times considered.

  16. Shear Correction Factors in Creep-Damage Analysis of Beams, Plates and Shells

    NASA Astrophysics Data System (ADS)

    Altenbach, Holm; Naumenko, Konstantin

    Modern design rules for thin-walled structures which operate at elevated temperatures are based on the demand that the creep and may be the damage behaviour should be taken into account. In the last four decades various models including the scalar or tensor valued hardening and damage variables are established. These models reflect the influence of the deformation or the damage induced anisotropy on the creep response. One problem in creep analysis of thin-walled structures is the selection of the structural mechanics model which has to be adequate to the choice of the constitutive equations. Considering complex loading conditions the structural mechanics model has to reflect for instance the different constitutive behaviour in tension and compression. Below the applicability of classical engineering models for beams, plates and shells to the creep-damage analysis is discussed. It will be shown that a first improvement of the classical approach can be given within the assumptions of the first order shear deformation theory. Based on the beam equations we demonstrate that the shear correction factors have to be modified within the time-step analysis.

  17. Microstructural study of the partition between seismic and aseismic deformation along the North Anatolian Fault zone, Turkey

    NASA Astrophysics Data System (ADS)

    Kaduri, M.; Gratier, J. P.; Renard, F.; Cakir, Z.; Lasserre, C.

    2014-12-01

    Along the North Anatolian Fault (Turkey), fault sliding is accommodated both by earthquakes and by aseismic creep. The creep processes develop either as transient (post-seismic or interseismic) sliding or as permanent sliding along zones localized on specific segments of the fault. Creep processes relax the stress and contribute to stress redistribution within the seismogenic zone. They participate to the deformation budget during the seismic cycle, sometimes delaying or on the contrary helping triggering the occurrence of large earthquakes. Identifying the mechanisms controlling creep and their evolution with time and space represents a major challenge for predicting the mechanical evolution of active faults. Our goal is to answer three main questions: How to identify at the outcrop scale permanent creep from transient creep? Is aseismic creep controlled by lithology? How does creep evolve before and after earthquakes? The challenge is to understand which key parameters control the shift from seismic to aseismic deformation, such as the effect of fabric, rock lithology, fault roughness, strain-rate, fluid pressure or stress.We collected samples from a dozen of fresh and well-preserved fault outcrops along creeping and locked segments of the North Anatolian Fault. We used various methods such as microscopic and geological observations, SEM, XRD analysis, strain measurements from image processing approaches in order to quantitatively characterize the amount of deformation and the mechanisms involved. Results show different relationships between lithology and mechanisms of deformation: (i) Along the locked segments of the North Anatolian Fault, in massive limestone, we found evidence of large earthquakes followed by pre- or post-seismic (i.e. afterslip) creep. (ii) Along some creeping segments, we observed gouges with weak clay (saponite) that could accommodate (or have accommodated in the past) large permanent creep. (iii) Along other creeping segments, we observed deformed serpentine bodies attesting of creep episodes, the strain values of which remaining to be evaluated, but also evidences of past earthquakes, suggesting in such areas a mixed-mode of seismic and aseismic deformation.

  18. Models for rupture mechanics of plate boundaries and crustal deformation

    NASA Technical Reports Server (NTRS)

    Nur, A.

    1983-01-01

    The role of pull aparts and pushups in transcurrent systems, the rotation of faults and blocks within transcurrent fault systems, the role of accretion tectonics in plate boundary deformation, and power law creep behavior and the yielding at plate boundaries were investigated.

  19. Measurement of Creep Properties of Ultra-High-Temperature Materials by a Novel Non-Contact Technique

    NASA Technical Reports Server (NTRS)

    Hyers, Robert W.; Lee, Jonghyun; Rogers, Jan R.; Liaw, Peter K.

    2007-01-01

    A non-contact technique for measuring the creep properties of materials has been developed and validated as part of a collaboration among the University of Massachusetts, NASA Marshall Space Flight Center Electrostatic Levitation Facility (ESL), and the University of Tennessee. This novel method has several advantages over conventional creep testing. The sample is deformed by the centripetal acceleration from the rapid rotation, and the deformed shapes are analyzed to determine the strain. Since there is no contact with grips, there is no theoretical maximum temperature and no concern about chemical compatibility. Materials may be tested at the service temperature even for extreme environments such as rocket nozzles, or above the service temperature for accelerated testing of materials for applications such as jet engines or turbopumps for liquid-fueled engines. The creep measurements have been demonstrated to 2400 C with niobium, while the test facility, the NASA MSFC ESL, has processed materials up to 3400 C. Furthermore, the ESL creep method employs a distribution of stress to determine the stress exponent from a single test, versus the many tests required by conventional methods. Determination of the stress exponent from the ESL creep tests requires very precise measurement of the surface shape of the deformed sample for comparison to deformations predicted by finite element models for different stress exponents. An error analysis shows that the stress exponent can be determined to about 1% accuracy with the current methods and apparatus. The creep properties of single-crystal niobium at 1985 C showed excellent agreement with conventional tests performed according to ASTM Standard E-139. Tests on other metals, ceramics, and composites relevant to rocket propulsion and turbine engines are underway.

  20. Indentation creep behavior of a direct-filling silver alternative to amalgam.

    PubMed

    Xu, H H; Liao, H; Eichmiller, F C

    1998-12-01

    Amalgam creep has been identified as a key parameter associated with marginal breakdown and corrosion. The aim of this study was to evaluate the time-dependent deformation (creep) of a novel silver filling material as an alternative to amalgam. We made the silver specimens by pressing a precipitated powder at room temperature to a density that can be achieved in clinical hand consolidation. The surface of the silver was either polished or burnished. To examine local contact creep and the effect of surface finishing, we used an indentation creep method in which a Vickers indenter was loaded on the specimen surface at a load of 10 N with dwell times of 5 sec to 6x10(4) sec. We used a bonded-interface technique to examine subsurface creep mechanisms. The flexural strength (mean+/-SD; n = 10) was 86+/-20 MPa for amalgam, 180+/-21 MPa for polished silver, and 209+/-19 MPa for burnished silver-values which are significantly different from each other (family confidence coefficient = 0.95; Tukey's multiple-comparison test). Indentation creep manifested as hardness number decreasing with increased dwell time. With dwell time increasing from 5 sec to 6x10(4) sec, the hardness number of amalgam was reduced by approximately 80%; that of the polished silver and the burnished silver was reduced by only 40%. Subsurface creep in amalgam consisted of the shape change of the alloy particles from spherical to elongated shapes, and the separation of matrix grains from each other, possibly due to grain-boundary sliding. Creep of the polished silver occurred by densification reducing porosity and increasing hardness; that of the burnished silver occurred by the displacement of the burnished layer. These results suggest that, due to creep-induced subsurface work-hardening and densification, the consolidated silver exhibits a higher resistance to indentation creep than does amalgam. The hardness number of silver approaches that of amalgam after prolonged indentation loading. PMID:9839787

  1. Contribution of Grain Boundary Sliding to Diffusion Creep of Forsterite

    NASA Astrophysics Data System (ADS)

    Thompson, E.; Dillman, A. M.; Hansen, L. N.; Kohlstedt, D. L.

    2011-12-01

    Grain boundary sliding (GBS) is an important component of diffusion creep in crystalline materials. Significant advances have been made in numerical simulations that provide insight into microstructural development during diffusion-accommodated GBS. However, the direct observation and measurement of GBS has not been extensively employed for geological materials, which prevents numerical simulations from being properly calibrated. This study aims to quantify the contribution of GBS to the total strain by utilizing atomic force microscopy (AFM) to measure displacements across grain boundaries as a function of strain. High-density samples were synthesized from forsterite powders that were isostatically compressed and subsequently sintered in a vacuum for 5 h at 1400C. After sintering, mean grain sizes ranged from 2 to 6 ?m. The faces of rectangularly shaped samples were were polished to produce flat surfaces. The resulting samples were uniaxially deformed at 1 atm and 1200C with differential stresses of 30-60 MPa. Stress-strain rate data indicate a stress exponent of ~1 demonstrating that deformation occurred in the diffusion creep regime. Samples were periodically removed from the deformation apparatus to monitor microstructural development as a function of strain. Topographical changes were followed with an AFM to characterize GBS. Line profiles created for each data set allowed analysis of displacements across a large number of grain boundaries. Profiles across individual grain surfaces were then fit with a line to reduce the effect of grain curvature that arises due to the shape of the AFM cantilever tip and thermal grooving of the grain boundaries. To calculate the amount of strain due to GBS, the average vertical offset between adjacent grains was measured using the fit lines. Samples deformed to strains of ~2% exhibited vertical displacements as low as 23 nm. These displacements correspond to ratios of GBS to total strain of nearly unity. At a total strain of 6.8%, the percentage of strain due to GBS decreased to ~39%. This decrease in the contribution of GBS with increasing strain may reflect transient deformation at the start of a deformation experiment.

  2. High-Temperature Creep of Fine-Grained Anorthite Aggregate

    NASA Astrophysics Data System (ADS)

    Yabe, K.; Koizumi, S.; Hiraga, T.

    2014-12-01

    Rheology of the lower crust has often been compared to the creep properties of polycrystalline anorthite. Samples that have been used in previous studies (Dimanov et al., 1999; Rybacki and Dresen, 2000) were prepared through crystallization of anorthite glass which can remain in the experiment and also contain some impurities such as absorbed water, TiO2, MgO and Fe2O3. In this study, we synthesized genuinely pure polycrystalline anorthite using the technique that does not allow the contamination of water and glass phase. Also, we prepared anorthite aggregates with glass phase and/or a small amount (1wt%) of MgO to investigate the creep properties of pure and impure anorthite aggregates. Pure anorthite powders were prepared through high temperature reaction of highly pure and nano-sized powders of CaCO3, Al2O3 and SiO2 and then they were vacuum sintered (Koizumi et al., 2010). For MgO doping, we added Mg(OH)2powders at the synthesis of anorthite powders. Glass phase was introduced to the samples by sintering above melting temperature and subsequent quenching. Constant load tests under 1 atmosphere were performed at temperatures ranging from 1150 to 1380?C and stresses of 10 to 120 MPa. We measured Arithmetic mean grain size of specimens by microstructural observations using scanning electron microscopy (SEM) before and after creep tests. Grain sizes of all the specimens were around 1 ?m before and after the creep test. Log stress versus log strain rate showed a linear relationship where its slope gave a stress exponent, n of 1, indicating that all the samples were deformed under diffusion creep. Anorthite containing MgO and glass phase were more than two and one orders of magnitude weaker than genuinely pure anorthite aggregates, respectively. Further, our pure aggregate exhibited three orders of magnitude lager strength compared to the "pure" aggregate used in previous studies. These results indicate that a small amount of glass and/or impurities including water have a great influence on the strength of polycrystalline anorthite aggregates.

  3. Progressive evolution of microfabrics in high-temperature indentation creep experiments

    NASA Astrophysics Data System (ADS)

    Wassmann, S.; Dorner, D.; Stoeckhert, B.

    2014-12-01

    Microfabrics of natural rocks as well as of those deformed in laboratory experiments are studied post-mortem, the history of fabric evolution being inferred from a finite state. This is a major drawback when being interested in modification of fabrics related to progressive deformation. Here we present a novel approach to analyze and compare fabrics in different stages of evolution, taking spatial position to mimic a time series. Using this approach, evolution in time can be investigated on one sample deformed in a single indentation creep test. Such experiments at high temperatures and atmospheric pressure provide information on mechanical properties of rock-forming minerals as well as on microfabrics developed during inhomogeneous deformation underneath the indenter. Using a conventional creep apparatus, a cylindrical alumina indenter, 2 mm in diameter, is driven by a dead load into the flat surface of a specimen. A penetration depth of 1 mm is typically reached after hours to days, depending on material, applied temperature, and load. Previous experiments on natural, polycrystalline anhydrite carried out at temperatures between 700C and 920 C yield a stress exponent of 3.9 indicating deformation in the dislocation creep regime, consistent with microstructural observations (Dorner et al., 2014; Solid Earth). Within a cone-shaped region in front of the indenter, the original microfabric appears entirely unaffected. The neutral cone is mantled by highly deformed shear zones. During progressive indentation this structure of undeformed cone and shear zones propagates into the specimen. Thus, for a homogeneous starting material, serial sections of the deformed specimen normal to the indenter axis provide insight into fabrics in distinct stages of evolution. Microfabrics developed at different distance in front of the approaching indenter can be taken to represent a time series. A disadvantage of the technique is that the history of shear zone deformation is complex, comprising components of tangential stretching and simple shear, which complicates the interpretation of fabrics and crystallographic preferred orientations. Notwithstanding, indentation creep tests seem to be a sound experimental approach to study microstructural evolution in time using a single experimentally deformed sample.

  4. Anatomy of gravitationally deformed slopes

    NASA Astrophysics Data System (ADS)

    Chigira, Masahiro; Yamasaki, Shintaro; Hariyama, Takehiro

    2010-05-01

    Deep-seated gravitational slope deformation is the deformation of rocks as well as slope surfaces, but the internal structures have not been well observed and described before. This is mainly due to the difficulty in obtaining undisturbed samples from underground. We analyzed the internal deformational structures of gravitationally deformed slopes by using high quality drilled cores obtained by hybrid drilling technique, which has been recently developed and can recover very fragile materials that could not be taken by the conventional drilling techniques. Investigated slopes were gravitationally deformed out-facing slopes of pelitic schist and shale. The slope surfaces showed deformational features of small steps, depressions, knobs, and linear depressions, but had no major main scarp and landslide body with well-defined outline. This is indicative of slow, deep-seated gravitational deformation. Most of these small deformational features are hidden by vegetations, but they are detected by using airborne laser scanner. Drilled cores showed that the internal deformation is dominated by the slip and tearing off along foliations. Slippage along foliations is conspicuous in pelitic schist: Pelitic schist is sheared, particularly along black layers, which are rich in graphite and pyrite. Graphite is known to be a solid lubricant in material sciences, which seems to be why shearing occurs along the black layers. Rock mass between two slip layers is sheared, rotated, fractured, and pulverized; undulation of bedding or schistosity could be the nucleation points of fracturing. Tearing off along foliations is also the major deformation mode, which forms jagged morphology of rock fragments within shear zones. Rock fragments with jagged surface are commonly observed in "gouge", which is very different from tectonic gouge. This probably reflects the low confining pressures during their formation. Microscopic to mesoscopic openings along fractures are commonly observed with fractures, which also suggests the low confining pressures. Vertical distribution of gravitational deformation with above features indicates that gravitational shear zones are nucleated in a distributed manner, then gradually connected to each other, and finally cut through the whole slope. This is the transition of gravitational mass rock creep to rock slide. First nucleation points seem to be controlled by the heterogeneity of rock properties. Thick black layers in pelitic schist, shale near thick sandstone beds in sedimentary rocks, were such nuclear points. The geometrical relationships between the distribution of fracture zones and the slope morphology suggest that they are formed in accordance to the valley incision and resultant slope destabilization.

  5. Deformation Mechanisms of Antigorite Serpentinite at Subduction Zone Conditions Determined from Experimentally and Naturally Deformed Rocks

    NASA Astrophysics Data System (ADS)

    Auzende, A. L.; Escartin, J.; Walte, N.; Guillot, S.; Hirth, G.; Frost, D. J.

    2014-12-01

    The rheology of serpentinite, and particularly that of antigorite-bearing rocks, is of prime importance for understanding subduction zone proceses, including decoupling between the downwelling slab and the overriding plate, exhumation of high-pressure rocks, fluids pathways and, more generally, mantle wedge dynamics. We present results from deformation-DIA experiments on antigorite serpentinite performed under conditions relevant of subduction zones (1-3.5 GPa ; 400-650°C). We complemented our study with a sample deformed in a Griggs-type apparatus at 1 GPa and 400°C (Chernak and Hirth, EPSL, 2010), and with natural samples from Cuba and the Alps deformed under blueschist/eclogitic conditions. Our observations on experimental samples of antigorite deformed within its stability field show that deformation is dominated by cataclastic flow; we can only document a minor contribution of plastic deformation. In naturally deformed samples, deformation-related plastic structures largely dominate strain accommodation, but we also document a minor contribution of brittle deformation. When dehydration occurs in experiments, plasticity increases, and is coupled to local embrittlement attributed to hydraulic fracturating due to the migration of dehydration fluids. Our results thus show that semibrittle deformation operates within and above the stability field of antigorite. We also document that the corrugated structure of antigorite has a control on the strain accommodation mechanisms under subduction conditions, with preferred inter and intra-cracking along (001) and gliding along both a and b. Deformation dominated by brittle processes, as observed in experiments, may occur during deformation at elevated (seismic?) strain rates, while plastic deformation, as observed in naturally deformed rocks, may correspond instead to low strain rates instead (aseismic creep?). We also discuss the role of antigorite rheology and mode of deformation on fluid transport.

  6. Materials Science and Technology, Volume 6, Plastic Deformation and Fracture of Materials

    NASA Astrophysics Data System (ADS)

    Mughrabi, Hael

    1996-12-01

    This self-contained handbook focuses on the mechanisms of plastic deformation and fracture affecting a wide variety of materials. From the Contents: Mughrabi: Introduction. Gil Sevillano: Flow Stress and Work Hardening. Leffers/Van Houtte/Aernoudt: Deformation and Textures of Metals at Large Strain. Kubin: Dislocation Patterning. Neuhuser/Schwink: Solid Solution Strengthening. Umakoshi: Deformation of Intermettalic Compounds. Reppich: Particle Strengthening. Blum: High Temperature Deformation and Creep of Crystalline Solids. Mukherjee: Superplasticity in Metals, Ceramics and Intermetallics. Argon: Inelastic Deformation and Fracture of Glassy Solids. Suresh: Cyclic Deformation and Fatigue. Riedel: Frature Mechanisms. Kato: Friction and Wear.

  7. Matrix cracking and creep behavior of monolithic zircon and zircon silicon carbide fiber composites

    NASA Astrophysics Data System (ADS)

    Anandakumar, Umashankar

    In this study, the first matrix cracking behavior and creep behavior of zircon matrix silicon carbide fiber composites were studied, together with the fracture and creep behavior of the monolithic zircon. These behaviors are of engineering and scientific importance, and the study was aimed at understanding the deformation mechanisms at elevated temperatures. The first matrix cracking behavior of zircon matrix uniaxially reinforced with silicon carbide fiber (SCS-6) composites and failure behavior of monolithic zircon were studied as a function of temperature (25C, 500C, and 1200C) and crack length in three point bending mode. A modified vicker's indentation technique was used to vary the initial crack length in monolithic and composite samples. The interfacial shear strength was measured at these temperatures from matrix crack saturation spacing. The composites exhibited steady state and non steady state behaviors at the three different temperatures as predicted by theoretical models, while the failure stress of zircon decreased with increasing stress. The intrinsic properties of the composites were used to numerically determine the results predicted by three different matrix cracking models based on a fracture mechanics approach. The analysis showed that the model based on crack bridging analysis was valid at 25C and 500C, while a model based on statistical fiber failure was valid at 1200C. Microstructural studies showed that fiber failure in the crack wake occurred at or below the matrix cracking stress at 1200C, and no fiber failure occurred at the other two temperatures, which validated the results predicted by the theoretical models. Also, it was shown that the interfacial shear stress corresponding to debonding determined the matrix cracking stress, and not the frictional shear stress. This study showed for the first time, the steady state and non-steady state matrix cracking behavior at elevated temperatures, the difference in behavior between room temperature and elevated temperatures, and the validity of the various models of first matrix cracking behavior. In order to understand the creep behavior of composites, it is important to study the creep behavior of matrix, fiber, and composites under identical conditions to determine the role of various constituents. Creep studies were conducted in an inert atmosphere in four point bending and uniaxial tension modes on zircon and zircon silicon carbide fiber composites at four different temperatures of 1250C, 1300C, 1350C, and 1400C, and over the stress range of 10--200 MPa. The strain rate was measured as a function of the stress and temperature to determine the stress exponent and activation energy, and microstructural analysis was done on crept samples using scanning electron microscopy. The composites exhibited a much lower creep rate than the monolilth, indicating that the major portion of the creep load was carried by the fibers. In flexural mode, both zircon and composite samples exhibited bimodal creep behavior, with the stress exponent (n) increasing with increasing stress. For zircon, at lower-stresses n was in the range of 2.1--2.6 and increased to 7--7.9 at higher stresses. Microstructural studies showed that diffusional creep was the rate controlling mechanism at lower stresses, while the higher stress exponent observed at higher stresses, was due to linkage of cavities and damage accumulation resulting in a higher strain rate. In the case of composites, the stress exponent was ?1 at lower stresses, and increased to 3--5 at higher stresses, indicating that diffusional creep (and grain boundary sliding) was rate controlling at lower stresses, and either creep cavitation and crack growth or dislocation creep was the rate controlling mechanism at higher stresses. Anomalous creep curves with strain jumps were observed for the first time during the creep of ceramic composites at lower temperatures and higher stresses. Microstructural studies showed that matrix cracking during creep results in these strain jumps. These studies showed tha

  8. Rupture and creep behaviours of subduction interface controlled by fault zone heterogeneity

    NASA Astrophysics Data System (ADS)

    Wang, Kelin; Brown, Lonn; Gao, Xiang; Bilek, Susan

    2015-04-01

    The behaviour of fault slip varies tremendously, ranging from seismic rupture to aseismic creep. We explore the role of fault zone heterogeneity in controlling large-scale (> 100 km in strike dimension) rupture and creep behaviours of subduction faults. Geometrically smooth subduction faults can (although not always) provide relatively homogeneous structural and stress conditions to allow large fault patches to be locked over prolonged periods and then rupture in great earthquakes. During the rupture, however, frictional heterogeneities arising from lithological changes, pore-fluid pressure variations, and low-amplitude geometrical irregularities always cause a very heterogeneous distribution of stress drop. Although some parts of the fault may undergo high or complete stress drop (local weakening), many other parts undergo very low stress drop or stress increase (local strengthening). The mixing of stress drop and increase in different parts of the rupture zone makes the average stress drop in each great earthquake very small, of the order of a couple of MPa, as widely observed in seismological studies. We use the 2011 Mw=9 Tohoku-oki earthquake to demonstrate this averaging effect. Geometrically extremely rough subduction faults, such as those featuring multiple subducting seamounts, provide very heterogeneous structural and stress conditions that promote creep and numerous small earthquakes. A global inspection of geodetically constrained locking and creeping states of subduction zones indicates that these extremely rough faults all tend to creep (Wang and Bilek, 2014). Depending on the degree of roughness and other geological conditions (e.g., sediment and fluid), some of the rough faults may host a mixture of seismic and aseismic patches and may exhibit a variety of creep behaviour ranging from steady creep to transient creep pulses (i.e., slow slip events) of different time scales. It can be envisioned that the heterogeneity in these rough faults is generally in the form of 3D deformation in a complex zone of damage along the interface and cannot be adequately approximated by heterogeneous rate-state friction. It is also important to recognize that these creeping rough faults are not "weakly coupled", nor are the highly seismic smooth faults "strongly coupled". A global examination of frictional heating of subduction faults indicate that the creeping rough faults dissipate more heat and are statically stronger, that is, they creep against greater resistance (called strong creep) than the stress required to cause a smooth fault to rupture in great earthquakes (Gao and Wang, 2014). This observation supports the notion that these faults creep as a result of geometrical irregularities forcing through a damage zone, very different from frictional creep due to the presence of week fault gouge (called weak creep). Gao, X., and K. Wang (2014), Science, 345, 1038-1041. Wang, K., and S. L. Bilek (2014), Tectonophysics, 610, 1-24.

  9. Creep buckling of axially compressed circular cylindrical shells of a zirconium alloy: Experiment and computer simulation

    NASA Astrophysics Data System (ADS)

    Korobeynikov, S. N.; Torshenov, N. G.; Lyubashevskaya, I. V.; Larichkin, A. Yu.; Chunikhina, E. V.

    2014-01-01

    Experiments were performed to study the deformation and buckling of axially compressed circular cylindrical shells of Zr2.5Nb zirconium alloy under creep conditions. Computer simulation using the MSC.Marc 2012 software was conducted by step-by-step integration of the equations of quasistatic deformation of thin shells using Norton's law of steady creep. The results of the experiment and computer simulation show that the buckling modes are a combination of axisymmetric bulges located near one end or both ends of the shell and axisymmetric buckling modes with the formation of three or four waves in the circumferential direction. A comparison is made of the time dependences of the axial strain of the shells obtained in the experiment and by computer simulation. It is shown that for large axial compressive stresses, these dependences are in satisfactory agreement. For lower values of these stresses, the difference between the theoretical and experimental dependences is greater.

  10. Evolution of Precipitate Microstructure During Creep of an AA7449 T7651 Aluminum Alloy

    NASA Astrophysics Data System (ADS)

    Fribourg, G.; Brchet, Y.; Chemin, J. L.; Deschamps, A.

    2011-12-01

    Creep forming is a process where plastic deformation is applied at the material's aging temperature. It enables to obtain parts of complex shape with reduced internal stresses and finds applications, for instance, in the aerospace industry. In this article, we report in-situ small-angle X-ray scattering measurements during creep experiments carried out on an AA7449 Al-Zn-Mg-Cu alloy in the T7651 temper. In the range of temperatures of 413 K to 453 K (140 C to 180 C), we show that the initial microstructure is not stable with respect to the applied stress/strain. Accelerated precipitation coarsening is shown to occur, clearly related to the plastic deformation. This strain-induced microstructure evolution is shown to happen even at temperatures well below the aging temperature that has led to the initial temper.

  11. Evolution of Strain Partitioning during Creep of Carrara Marble

    NASA Astrophysics Data System (ADS)

    Quintanilla Terminel, A.; Evans, J. B.; Mainprice, D.; Lebensohn, R.

    2014-12-01

    We measured the local strain and strain heterogeneity produced during creep deformation of split cylinders of Carrara marble under conventional triaxial loading to inelastic strains of 11% at a strain rate of 3x10-5s-1, confining pressure of 300 MPa and 400deformed to strains of 11%, 22% and 36% at 600C and the same rate and confining pressure. Microscale strain mapping at a scale of 10 micrometers (MSSM) show that the partitioning of strain amongst twinning, dislocation slip, and grain boundary sliding mechanisms change with T. Preliminary results using a VPFFT model that gives more importance to dislocation slip predict strain heterogeneities with larger wavelength. Interestingly, at all T, although sliding occurred on some boundaries, on average, strain in regions near boundaries was less than that in grain interiors suggesting the formation of a core-mantle structure observed in naturally deformed rocks. The production of local crystallographic texture also depends on T (and presumably, partitioning amongst the mechanisms). In all the experiments, the texture index (TI) of local areas decreased after deformation, but the path of the evolution differed with changing T. Reductions in TI were greatest for samples deformed at 400C, where twin activity was greatest, and at 700C, where boundary sliding was more prevalent, and less for intermediate T. The wavelength and amplitude of the heterogeneity in local strain decreased with increasing strain at 600C, suggesting that the strain (and perhaps, structures) were being homogenized. From this data and previous observations, we conclude that the evolution of deformation structures in marble takes place over a substantial interval in strain; that the duration of this interval probably depends on strain rate, temperature, and pressure; and that extrapolation of mechanical behavior from lab to natural conditions will need to account for changes in strain partitioning.

  12. Cumulative creep damage for polycarbonate and polysulfone

    NASA Technical Reports Server (NTRS)

    Zhang, M. J.; Straight, M. R.; Brinson, H. F.

    1985-01-01

    Creep to failure tests performed on polycarbonate and polysulfone under single and two step loadings are discussed. A cumulative damage law or modified time fraction rule is developed using a power law for transient creep response as the starting point. Experimental results are approximated well by the new rule. Damage and failure mechanisms associated with the two materials are suggested.