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Sample records for diffraction based residual

  1. Method for improve x-ray diffraction determinations of residual stress in nickel-base alloys

    DOEpatents

    Berman, Robert M.; Cohen, Isadore

    1990-01-01

    A process for improving the technique of measuring residual stress by x-ray diffraction in pieces of nickel-base alloys which comprises covering part of a predetermined area of the surface of a nickel-base alloy with a dispersion, exposing the covered and uncovered portions of the surface of the alloy to x-rays by way of an x-ray diffractometry apparatus, making x-ray diffraction determinations of the exposed surface, and measuring the residual stress in the alloy based on these determinations. The dispersion is opaque to x-rays and serves a dual purpose since it masks off unsatisfactory signals such that only a small portion of the surface is measured, and it supplies an internal standard by providing diffractogram peaks comparable to the peaks of the nickel alloy so that the alloy peaks can be very accurately located regardless of any sources of error external to the sample.

  2. Method for improving x-ray diffraction determinations of residual stress in nickel-base alloys

    DOEpatents

    Berman, R.M.; Cohen, I.

    1988-04-26

    A process for improving the technique of measuring residual stress by x-ray diffraction in pieces of nickel-base alloys is discussed. Part of a predetermined area of the surface of a nickel-base alloy is covered with a dispersion. This exposes the covered and uncovered portions of the surface of the alloy to x-rays by way of an x-ray diffractometry apparatus, making x-ray diffraction determinations of the exposed surface, and measuring the residual stress in the alloy based on these determinations. The dispersion is opaque to x-rays and serves a dual purpose, since it masks off unsatisfactory signals such that only a small portion of the surface is measured, and it supplies an internal standard by providing diffractogram peaks comparable to the peaks of the nickel alloy so that the alloy peaks can be very accurately located regardless of any sources of error external to the sample. 2 figs.

  3. Diffraction-based optical correlator

    NASA Technical Reports Server (NTRS)

    Spremo, Stevan M. (Inventor); Fuhr, Peter L. (Inventor); Schipper, John F. (Inventor)

    2005-01-01

    Method and system for wavelength-based processing of a light beam. A light beam, produced at a chemical or physical reaction site and having at least first and second wavelengths, ?1 and ?2, is received and diffracted at a first diffraction grating to provide first and second diffracted beams, which are received and analyzed in terms of wavelength and/or time at two spaced apart light detectors. In a second embodiment, light from first and second sources is diffracted and compared in terms of wavelength and/or time to determine if the two beams arise from the same source. In a third embodiment, a light beam is split and diffracted and passed through first and second environments to study differential effects. In a fourth embodiment, diffracted light beam components, having first and second wavelengths, are received sequentially at a reaction site to determine whether a specified reaction is promoted, based on order of receipt of the beams. In a fifth embodiment, a cylindrically shaped diffraction grating (uniform or chirped) is rotated and translated to provide a sequence of diffracted beams with different wavelengths. In a sixth embodiment, incident light, representing one or more symbols, is successively diffracted from first and second diffraction gratings and is received at different light detectors, depending upon the wavelengths present in the incident light.

  4. Effects of oxygen partial pressure and annealing temperature on the residual stress of hafnium oxide thin-films on silicon using synchrotron-based grazing incidence X-ray diffraction

    NASA Astrophysics Data System (ADS)

    Biswas, Debaleen; Sinha, Anil Kumar; Chakraborty, Supratic

    2016-10-01

    Synchrotron radiation-based grazing incidence X-ray diffraction (GI-XRD) technique is employed here to estimate the residual stress of < 10 nm thin hafnium oxide film deposited on Si (100) substrate at different argon/oxygen ratios using reactive rf sputtering. A decrease in residual stress, tensile in nature, is observed at higher annealing temperature for the samples deposited with increasing argon ratio in the Ar/O2 plasma. The residual stress of the films deposited at higher pAr (Ar:O2 = 4:1) is also found to be decreased with increasing annealing temperature. But the stress is more or less constant with annealing temperature for the films deposited at lower Ar/O2 (1:4) ratio. All the above phenomena can be explained on the basis of swelling of the interfacial layer and enhanced structural relaxation in the presence of excess Hf in hafnium oxide film during deposition.

  5. Neutron Diffraction Characterization of Residual Strain in Welded Inconel 718 for NASA Space Shuttle Flow Liners

    SciTech Connect

    Rathod, C.R.; Vaidyanathan, R.; Livescu, V.; Clausen, B.; Bourke, M. A. M.; Notardonato, W.U.; Femminineo, M.

    2004-06-28

    This work quantitatively assesses residual strains and stresses associated with the weld repair process used to repair cracks on NASA's space shuttle flow liners. The coupons used in this investigation were made of the same INCONEL 718 alloy used for the flow liners. They were subjected to identical welding and certification procedures that were carried out on the space shuttle. Neutron diffraction measurements at Los Alamos National Laboratory determined residual strains at selected locations in a welded coupon at 293 K and 135 K. The weld repair process introduced Mises effective residual stresses of up to 555 MPa. On comparing the measurements at 293 K and 135 K, no significant change to the residual strain profile was noted at the low temperature. This indicated minimal mismatch in the coefficients of thermal expansion between the base metal and the weld.

  6. X-ray diffraction analysis of residual stress in zirconia dental composites

    NASA Astrophysics Data System (ADS)

    Allahkarami, Masoud

    Dental restoration ceramic is a complex system to be characterized. Beside its essential biocompatibility, and pleasant appearance, it requires being mechanically strong in a catastrophic loading environment. Any design is restricted with geometry boundary and material property limits. Inspired by natural teeth, a multilayer ceramic is a smart way of achieving an enhanced restoration. Bi-layers of zirconia core covered by porcelain are known as one of the best multilayer restorations. Residual stresses may be introduced into a bi-layer dental ceramic restoration during its entire manufacturing process due to thermal expansion and elastic property mismatch. It is impossible to achieve a free of residual stresses bi-layer zirconia-porcelain restoration. The idea is to take the advantage of residual stress in design in such a way to prevent the crack initiation and progression. The hypothesis is a compressive residual stress at external contact surface would be enabling the restoration to endure a greater tensile stress. Optimizing the layers thickness, manufacturing process, and validating 3D simulations require development of new techniques of thickness, residual stresses and phase transformation measurement. In the present work, a combined mirco-tomography and finite element based method were adapted for thickness measurement. Two new 2D X-ray diffraction based techniques were adapted for phase transformation area mapping and combined phase transformation and residual stress measurement. Concerning the complex geometry of crown, an efficient method for X-ray diffraction data collection mapping on a given curved surface was developed. Finally a novel method for 3D dimensional x-ray diffraction data collection and visualization were introduced.

  7. Residual stress measurements in forced convective quenched steel bars by means of neutron diffraction

    SciTech Connect

    Hernandez-Morales, B.; Hawbolt, B.E.; Brimacombe, J.K.

    1996-12-31

    The residual stress distributions in 38.1 mm-dia., forced convective quenched bars of interstitial-free (IF), 1045 carbon, and alloyed steels were determined by neutron diffraction. The IF and 1045 carbon steel quenched bars exhibited compressive axial and circumferential (hoop) residual stresses near the surface and tensile values at the center. The radial residual stresses were tensile at all radial positions, decreasing towards zero near the surface. In contrast, the measured axial and circumferential components of the residual stress tensor in the alloyed eutectoid steel quenched bar were tensile near the surface and decreased to compressive values at the center. The radial component showed a maximum compressive value at the center and approached zero close to the surface. Metallographic analysis and hardness testing of the three steel specimens, revealed that the IF steel had transformed completely to ferrite, while the 1045 carbon steel bar transformed to martensite near the surface and a mixture of pearlite, ferrite and martensite at the center. On the other hand, the alloyed eutectoid steel specimen transformed entirely to martensite with small amounts of bainite near the center of the rod. The observed differences in the residual stress distributions in the three steels were explained based on the sequence of phase transformations that took place during quenching.

  8. Mapping of residual strains of a ceramic-to-metal joint using X-ray diffraction

    SciTech Connect

    Watkins, T.R.; Wang, X.L.; Spooner, S.; Hubbard, C.R.; Vance, S.J.; Rabin, B.H.; Williamson, R.L.

    1994-03-01

    In this study, the residual strains in the iron layer of a zirconia-iron joint, brazed with a metal alloy, were measured with X-ray diffraction as a function of distance from the joint. The residual strains were measured at various key locations indicated by a finite element model (FEM). The X-ray residual strain mapping results were compared to neutron diffraction mapping results. These data were combined to provide a complete residual strain profile of these samples and were compared with results of FEM.

  9. Neutron diffraction measurements of residual stresses in friction stir welding: a review

    SciTech Connect

    Woo, Wan Chuck; Feng, Zhili; Wang, Xun-Li; David, Stan A

    2011-01-01

    Significant amounts of residual stresses are often generated during welding and result in critical degradation of the structural integrity and performance of components. Neutron diffraction has become a well established technique for the determination of residual stresses in welds because of the unique deep penetration, three-dimensional mapping capability, and volume averaged bulk measurements characteristic of the scattering neutron beam. Friction stir welding has gained prominence in recent years. The authors reviewed a number of neutron diffraction measurements of residual stresses in friction stir welds and highlighted examples addressing how the microstructures and residual stresses are correlated with each other. An example of in situ neutron diffraction measurement result shows the evolution of the residual stresses during welding.

  10. Neutron diffraction residual stress studies for aero-engine component applications

    NASA Astrophysics Data System (ADS)

    Clay, K.; Small, C.

    1991-12-01

    Computer graphics for a presentation describing how Rolls-Royce is refining the method of residual stress measurement by neutron diffraction to suit the characteristic stress fields of components are presented. Results to date are given. An outline of how this residual stress data is to be used in developing stress models for critical rotating components is given.

  11. Volumetric measurement of residual stress using high energy x-ray diffraction

    NASA Astrophysics Data System (ADS)

    Whitesell, R.; McKenna, A.; Wendt, S.; Gray, J.

    2016-02-01

    We present results and recent developments from our laboratory, bench-top high energy x-ray diffraction system (HEXRD), between diffraction energies 50 and 150 KeV, to measure internal strain of moderately sized objects. Traditional x-ray strain measurements are limited to a few microns depth due to the use of Cu Kα1 Mo Kα1 radiation. The use of high energy x-rays for volumetric measurements of strain is typically the domain of synchrotron sources. We discuss the use of industrial 320kVp tube sources to generate a brighter x-ray beam along with a method using the intrinsic 43 eV width of the Kα1 characteristic peak of tungsten to measure volumetric strains in a number of industrially relevant materials. We will present volumetric strain measurements from two examples, first, additive manufacturing (AM) parts with various build configurations and, secondly, residual strain depth profiles from shot peened surface treatments. The spatial resolution of these depth profiles is ˜75 microns. The development of a faster method as compared to energy dispersive or θ-2θ scans is based on the intensity variation measurement of the strain using the aforementioned 43 eV characteristic tungsten kα line. We will present recent results on the development of this new tool and on x-ray diffraction measurements at high energy.

  12. Residual stress characterization of welds and post-weld processes using x-ray diffraction techniques

    NASA Astrophysics Data System (ADS)

    Brauss, Michael E.; Pineault, James A.; Eckersley, John S.

    1998-03-01

    This paper illustrates the importance of residual stress characterization in welds and post weld processes. The failure to characterize residual stresses created during welding and/or post weld processes can lead to unexpected occurrences of stress corrosion cracking, distortion, fatigue cracking as well as instances of over design or over processing. The development of automated residual stress mapping and the availability of portable and fast equipment have now made the characterization of residual stresses using x-ray diffraction practical for process control and optimization. The paper presents examples where x-ray diffraction residual stress characterization techniques were applied on various kinds of welds including arc welds, TIG welds, resistance welds, laser welds and electron beam welds. The nondestructive nature of the x-ray diffraction technique has made the residual stress characterization of welds a useful tool for process optimization and failure analysis, particularly since components can be measured before and after welding and post welding processes. Some examples presented show the residual stresses before and after the application of post weld processes such as shot peening, grinding and heat treatment.

  13. X-ray diffraction measurement of residual stresses in thick, multi-pass steel weldments

    SciTech Connect

    Ruud, C.O.; Di Mascio, P.S.; Pangborn, R.N.; Snoha, D.J.

    1985-05-01

    A unique X-ray diffraction instrument for residual stress measurement has been developed that provides for speed, ease of measurement, accuracy, and economy of surface stress measurement. Application of this instrument with a material removal technique, e.g., electropolishing, has facilitated detailed, high resolution studies of three-dimensional stress fields. This paper describes the instrumentation and techniques applied to conduct the residual stress measurement and presents maps of the residual stress data obtained for the surfaces of a heavy 21/4 Cr 1 Mo steel plate weldment.

  14. Experimental determination of residual stress by neutron diffraction in a boiling water reactor core shroud

    SciTech Connect

    Payzant, A.; Spooner, S.; Zhu, Xiaojing; Hubbard, C.R.

    1996-06-01

    Residual strains in a 51 mm (2-inch) thick 304L stainless steel plate have been measured by neutron diffraction and interpreted in terms of residual stress. The plate, measuring (300 mm) in area, was removed from a 6m (20-ft.) diameter unirradiated boiling water reactor core shroud, and included a multiple-pass horizontal weld which joined two of the cylindrical shells which comprise the core shroud. Residual stress mapping was undertaken in the heat affected zone, concentrating on the outside half of the plate thickness. Variations in residual stresses with location appeared consistent with trends expected from finite element calculations, considering that a large fraction of the residual hoop stress was released upon removal of the plate from the core shroud cylinder.

  15. Determination of the residual stress tensor in textured zirconium alloy by neutron diffraction

    NASA Astrophysics Data System (ADS)

    Sumin, V. V.; Papushkin, I. V.; Vasin, R. N.; Venter, А. M.; Balagurov, А. М.

    2012-02-01

    Results of neutron diffraction studies of crystallographic texture and residual stress tensor components in cold-worked and annealed cylindrical components made from E-110 zirconium alloy are presented. Those components are used as plugs in the fuel elements of the VVER-type reactors; the resident residual stresses influence the durability and safety of the fuel elements. The experiments were carried out on the neutron diffractometers at Dubna (the IBR-2 pulsed reactor) and Berlin Helmholtz-Zentrum (the BER II research reactor). It is shown that the samples have fiber texture that is changed considerably with annealing. The type I residual stress tensors for both samples were calculated by the BulkPathGEO model. The cold worked component has 136-166 MPa tensile residual stress in the radial direction and zero stress along the axial direction. Residual stress values in the annealed component are close to zero.

  16. Characterisation of Residual Stresses Generated by Laser Shock Peening by Neutron and Synchrotron Diffraction

    NASA Astrophysics Data System (ADS)

    Evans, Alexander Dominic; King, Andrew; Pirling, Thilo; Peyre, Patrice; Withers, Phillip John

    The fatigue behaviour of engineering alloys can be significantly improved through the application of mechanical surface treatments. These processes generate significant compressive residual stresses near surface by inhomogeneous plastic deformation. In the case of mechanical surface treatments such as laser shock peening, certain burnishing and rolling techniques and ultrasonic impact treatment (UIT), the compressive residual stress layer can extend to a depth of the order of millimeters, with balancing tensile stresses located deeper. Techniques to characterise the residual stresses generated by such mechanical surface treatments non-destructively are mainly limited to diffraction methods using penetrating neutron and synchrotron X-ray radiations. The application of these radiation sources is illustrated here by the characterisation of residual strain distributions in a two types of specimens treated with laser shock peening (LSP). Analyses of diffraction peak broadening provide qualitative information concerning the depth to which the plastic deformation of the treatments extends. Two case studies of laser shock peening of titanium and aluminium alloys is presented to demonstrate the capabilities of neutron and synchrotron diffraction techniques in the field of residual stress characterisation of surface engineered material non-destructively.

  17. Neutron diffraction analysis of residual strain/stress distribution in the vicinity of high strength welds

    NASA Astrophysics Data System (ADS)

    Mráz, L.; Karlsson, L.; Hamák, I.; Vrána, M.; Mikula, P.

    2010-06-01

    Residual stresses resulting from non homogeneous heat distribution during welding process belong to most significant factor influencing behavior of welded structures. These stresses are responsible for defect occurrence during welding and they are also responsible for crack initiation and propagation at the either static or dynamic load. The significant effect of weld metal chemical composition as well as the effect of fatigue load and local plastic deformation on residual stress distribution and fatigue life have been recognized for high strength steels welds. The changes in residual stress distribution have then positive effect on cold cracking behavior and also on fatigue properties of the welds [1-3]. Several experimental methods, both destructive and non-destructive, such as hole drilling method, X-ray diffraction, neutron diffraction and others, have been used to examine residual stress distribution in all three significant orientations in the vicinity of the welds. The present contribution summarizes the results of neutron diffraction measurements of residual stress distribution in the vicinity of single-pass high-strength-steel welds having different chemical composition as well as the influence of fatigue load and local plastic deformation. It has been observed that the chemical composition of the weld metal has a significant influence on the stress distribution around the weld. Similarly, by aplying both cyclic load or pre-stress load on the specimens, stress relaxation was observed even in the region of approximately 40 mm far from the weld toe.

  18. In Situ Tensile Deformation and Residual Stress Measurement by Neutron Diffraction in Modified 9Cr-1Mo Steel

    NASA Astrophysics Data System (ADS)

    Shrestha, Triratna; Charit, Indrajit; Potirniche, Gabriel

    2015-12-01

    The deformation behavior of monolithic modified 9Cr-1Mo (Grade 91) steel during uniaxial tensile loading was studied using the in situ neutron diffraction technique. The residual stress distribution across gas tungsten arc welds in the Grade 91 steel was measured by the time-of-flight neutron diffraction method using the SMARTS diffractometer at Lujan Neutron Scattering Center, Los Alamos National Laboratory. Grade 91 plates were welded using the gas tungsten arc welding (GTAW) technique. The load sharing by different grain orientations was observed during the tensile loading. The residual stresses along three orthogonal directions were determined at the mid-thickness, 4.35 and 2.35 mm below the surface of both the as-welded and post-weld heat-treated plates. The residual stresses of the as-welded plates were compared with those of the post-weld heat-treated plates. The post-weld heat treatment significantly reduced the residual stress level in the base metal, the heat-affected zone, and the weld zone. Vickers microhardness across the weld zone of the as-welded and post-weld heat-treated specimens was evaluated and correlated with the observed residual stress profile and microstructure.

  19. Neutron diffraction measurements and modeling of residual strains in metal matrix composites

    NASA Technical Reports Server (NTRS)

    Saigal, A.; Leisk, G. G.; Hubbard, C. R.; Misture, S. T.; Wang, X. L.

    1996-01-01

    Neutron diffraction measurements at room temperature are used to characterize the residual strains in tungsten fiber-reinforced copper matrix, tungsten fiber-reinforced Kanthal matrix, and diamond particulate-reinforced copper matrix composites. Results of finite element modeling are compared with the neutron diffraction data. In tungsten/Kanthal composites, the fibers are in compression, the matrix is in tension, and the thermal residual strains are a strong function of the volume fraction of fibers. In copper matrix composites, the matrix is in tension and the stresses are independent of the volume fraction of tungsten fibers or diamond particles and the assumed stress free temperature because of the low yield strength of the matrix phase.

  20. Neutron diffraction measurements and modeling of residual strains in metal matrix composites

    SciTech Connect

    Saigal, A.; Leisk, G.G.; Hubbard, C.R.; Misture, S.T.; Wang, X.L.

    1996-04-01

    Neutron diffraction measurements at room temperature are used to characterize the residual strains in tungsten fiber-reinforced copper matrix, tungsten fiber-reinforced Kanthal matrix, and diamond particulate-reinforced copper matrix composites. Results of finite element modeling are compared with the neutron diffraction data. In tungsten/Kanthal composites, the fibers are in compression, the matrix is in tension, and the thermal residual strains are a strong function of the volume fraction of fibers. In copper matrix composites, the matrix is in tension and the stresses are independent of the volume fraction of tungsten fibers or diamond particles and the assumed stress free temperature because of the low yield strength of the matrix phase.

  1. Metagratings for Diffraction Based, Compact, Holographic Imaging

    NASA Astrophysics Data System (ADS)

    Inampudi, Sandeep; Podolskiy, Viktor; Multiscale Electromagnetics Group Team

    2013-03-01

    Recent developments in semiconductor technology brought to life a new generation of highly-compact visible-frequency cameras. Unfortunately, straight forward extension of this progress to low-frequency domains (such as mid-IR imaging) is impossible since the pixel size at these frequencies is limited by free-space diffraction limit. Here we present an approach to realize highly-compact imaging systems at lower frequencies. Our approach takes advantage of high refractive index of materials commonly utilized in semiconductor detectors of mid-IR radiation, accompanied by metagratings, structures with engineered diffraction properties, to achieve a 10-fold reduction in the pixel size. In contrast to conventional refraction-based imaging, the approach essentially produces a digital hologram - a 2D projection of the 3D optical field, enabling a post-imaging ``refocusing'' of the picture. The perspectives of numerical recovery of the optical field and the stability of such recovery are discussed.

  2. Verification of residual stresses in flash-butt-weld rails using neutron diffraction

    NASA Astrophysics Data System (ADS)

    Tawfik, David; Kirstein, Oliver; Mutton, Peter John; Chiu, Wing Kong

    2006-11-01

    Residual stresses developed during flash-butt welding may play a crucial role in prolonging the fatigue life of the welded tracks under service loading conditions. The finished welds typically exhibit high levels of tensile residual stresses in the web region of the weld. Moreover, the surface condition of the web may contain shear drag or other defects resulting from the shearing process which may lead to the initiation and propagation of fatigue cracks in a horizontal split web failure mode under high axle loads. However, a comprehensive understanding into the residual stress behaviour throughout the complex weld geometry remains unclear and is considered necessary to establish the correct localised post-weld heat treatment modifications intended to lower tensile residual stresses. This investigation used the neutron diffraction technique to analyse residual stresses in an AS60 flash-butt-welded rail cooled under normal operating conditions. The findings will ultimately contribute to developing modifications to the flash-butt-welding procedure to lower tensile residual stresses which may then improve rail performance under high axle load.

  3. INTERFACE RESIDUAL STRESSES IN DENTAL ZIRCONIA USING LAUE MICRO-DIFFRACTION

    SciTech Connect

    Bale, H. A.; Tamura, N.; Coelho, P.G.; Hanan, J. C.

    2009-01-01

    Due to their aesthetic value and high compressive strength, dentists have recently employed ceramics for restoration materials. Among the ceramic materials, zirconia provides high toughness and crack resistant characteristics. Residual stresses develop in processing due to factors including grain anisotropy and thermal coefficient mismatch. In the present study, polychromatic X-ray (Laue) micro-diffraction provided grain orientation and residual stresses on a clinically relevant zirconia model ceramic disk. A 0.5 mm x 0.024 mm region on zirconia was examined on a 500 nm scale for residual stresses using a focused poly-chromatic synchrotron X-ray beam. Large stresses ranging from - to + 1GPa were observed at some grains. On average, the method suggests a relatively small compressive stress at the surface between 47 and 75 MPa depending on direction.

  4. Neutron diffraction determination of the residual stress redistribution in cracked autofrettaged tubing

    SciTech Connect

    Bourke, M.A. ); McGillivray, H.J.; Webster, G.A. . Dept. of Mechanical Engineering); Webster, P.J. . Dept. of Civil Engineering)

    1991-01-01

    Neutron diffraction has been used to measure the residual stress distributions in uncracked and fatigue cracked rings taken from a high strength, low alloy steel autofrettage tube with a bore diameter of 60mm and a wall thickness of 32mm. Stresses were determined to a precision of {plus minus} 10MPa. Three crack sixes were examines. No appreciable stress redistribution was observed until the crack was grown into a region which originally contained tensile residual hoop stress. When this occurred an increase in residual hoop tension was observed ahead of the crick tip. Qualitative agreement was achieved between the measured hoop stress distribution and values predicted using a boundary element method. 9 refs., 12 figs.

  5. Measurement of residual stress fields in FHPP welding: a comparison between DSPI combined with hole-drilling and neutron diffraction

    NASA Astrophysics Data System (ADS)

    Viotti, Matias R.; Albertazzi, Armando; Staron, Peter; Pisa, Marcelo

    2013-04-01

    This paper shows a portable device to measure mainly residual stress fields outside the optical bench. This system combines the traditional hole drilling technique with Digital Speckle Pattern Interferometry. The novel feature of this device is the high degree of compaction since only one base supports simultaneously the measurement module and the hole-drilling device. The portable device allows the measurement of non-uniform residual stresses in accordance with the ASTM standard. In oil and gas offshore industries, alternative welding procedures among them, the friction hydro pillar processing (FHPP) is highlighted and nowadays is an important maintenance tool since it has the capability to produce structure repairs without risk of explosions. In this process a hole is drilled and filled with a consumable rod of the same material. The rod, which could be cylindrical or conical, is rotated and pressed against the hole, leading to frictional heating. In order to assess features about the residual stress distribution generated by the weld into the rod as well as into the base material around the rod, welded samples were evaluated by neutron diffraction and by the hole drilling technique having a comparison between them. For the hole drilling technique some layers were removed by using electrical discharge machining (EDM) after diffraction measurements in order to assess the bulk stress distribution. Results have shown a good agreement between techniques.

  6. Migration velocity analysis using residual diffraction moveout: a real-data example

    NASA Astrophysics Data System (ADS)

    Gonzalez, Jaime A. C.; de Figueiredo, José J. S.; Coimbra, Tiago A.; Schleicher, Jörg; Novais, Amélia

    2016-08-01

    Unfocused seismic diffraction events carry direct information about errors in the migration-velocity model. The residual-diffraction-moveout (RDM) migration-velocity-analysis (MVA) method is a recent technique that extracts this information by means of adjusting ellipses or hyperbolas to uncollapsed migrated diffractions. In this paper, we apply this method, which has been tested so far only on synthetic data, to a real data set from the Viking Graben. After application of a plane-wave-destruction (PWD) filter to attenuate the reflected energy, the diffractions in the real data become interpretable and can be used for the RDM method. Our analysis demonstrates that the reflections need not be completely removed for this purpose. Beyond the need to identify and select diffraction events in post-stack migrated sections in the depth domain, the method has a very low computational cost and processing time. To reach an acceptable velocity model of comparable quality as one obtained with common-midpoint (CMP) processing, only two iterations were necessary.

  7. Calculation of the diffraction efficiency on concave gratings based on Fresnel-Kirchhoff's diffraction formula.

    PubMed

    Huang, Yuanshen; Li, Ting; Xu, Banglian; Hong, Ruijin; Tao, Chunxian; Ling, Jinzhong; Li, Baicheng; Zhang, Dawei; Ni, Zhengji; Zhuang, Songlin

    2013-02-10

    Fraunhofer diffraction formula cannot be applied to calculate the diffraction wave energy distribution of concave gratings like plane gratings because their grooves are distributed on a concave spherical surface. In this paper, a method based on the Kirchhoff diffraction theory is proposed to calculate the diffraction efficiency on concave gratings by considering the curvature of the whole concave spherical surface. According to this approach, each groove surface is divided into several limited small planes, on which the Kirchhoff diffraction field distribution is calculated, and then the diffraction field of whole concave grating can be obtained by superimposition. Formulas to calculate the diffraction efficiency of Rowland-type and flat-field concave gratings are deduced from practical applications. Experimental results showed strong agreement with theoretical computations. With the proposed method, light energy can be optimized to the expected diffraction wave range while implementing aberration-corrected design of concave gratings, particularly for the concave blazed gratings. PMID:23400074

  8. REVIEW ARTICLE: Determination of residual stresses in materials and industrial components by neutron diffraction

    NASA Astrophysics Data System (ADS)

    Albertini, Gianni; Bruno, Giovanni; Carradò, Adele; Fiori, Fabrizio; Rogante, Massimo; Rustichelli, Franco

    1999-03-01

    We present a review of the determination of residual stresses in materials and components of industrial interest by using the non-destructive technique of neutron diffraction. The fundamental aspects are discussed, together with a brief description of the experimental facilities. Several experimental results are then reported, particularly concerning applications to materials and components for power plants (CrMo steel, AISI304 stainless steel and 2.25Cr1Mo ferritic steel), aerospace and automotive technology (Al alloys, metal matrix composites, nickel superalloy gas-turbine components) and fusion-reactor technology (AISI316L for the first wall). A few thermomechanical treatments are considered, such as welding, cold-expanded holes, thermoelastic coupling and thermal and mechanical fatigue. Moreover, a few applications to general industrial problems are shown, namely brazed ceramic-steel components, coatings and fatigue-cracked samples. In some cases, experimental results are compared with numerical models or results from x-ray diffraction measurements.

  9. Residual Stress Analysis of Overspeeded Disk with Central Hole by X-ray Diffraction

    NASA Technical Reports Server (NTRS)

    Good, James N

    1948-01-01

    An X-ray - diffraction analysis of residual surface stresses after plastic strain was introduced in a parallel-sided 3S-O aluminum disk with a central hole by two types of centrifugal overspeed is reported. Both tangential and radial stresses were generally tensile with large local variations near the hole where surface stresses may have been partly superficial. These stresses were both tensile and compressive dependent on the distance from the disk center when mass compression was effected near the hole.

  10. Determination of the residual stress in a centrifuge bowl by neutron diffraction

    NASA Astrophysics Data System (ADS)

    Albertini, G.; Giuliani, A.; Lin Peng, R.; Manescu, A.; Ponzetti, A.

    An experimental study of the stress field in centrifuges for food processing and for agricultural applications was undertaken. The model, the dimensions and the material of the sample are those of the most recent line of production of the Nuova M.A.I.P. company. The rotor is also one of the largest rotors produced by that firm. The residual strains and stresses were determined by using neutron-diffraction techniques before centrifugation and after centrifugation, to evaluate the evolution of stress induced by centrifuging. The upper part of the rotating bowl is investigated, where the highest stress field during centrifugation is theoretically forecast to occur. A data elaboration aiming at avoiding systematic errors leads to the conclusion that no appreciable residual stress is induced by centrifugation.

  11. Nondestructive evaluation of residual stress in short-fiber reinforced plastics by x-ray diffraction

    NASA Astrophysics Data System (ADS)

    Tanaka, Keisuke; Tokoro, Syouhei; Akiniwa, Yoshiaki; Egami, Noboru

    2014-06-01

    The X-ray diffraction method is used to measure the residual stress in injection-molded plates of short-fiber reinforced plastics (SFRP) made of crystalline thermoplastics, polyphenylene sulphide (PPS), reinforced by carbon fibers with 30 mass%. Based on the orientation of carbon fibers, injection molded plates can be modeled as three-layered lamella where the core layer is sandwiched by skin layers. The stress in the matrix in the skin layer was measured using Cr-Kα radiation with the sin2Ψ method. Since the X-ray penetration depth is shallow, the state of stresses measured by X-rays in FRP can be assumed to be plane stress. The X-ray measurement of stress in carbon fibers was not possible because of high texture. A new method was proposed to evaluate the macrostress in SFRP from the measurement of the matrix stress. According to micromechanics analysis of SFRP, the matrix stresses in the fiber direction, σ1m, and perpendicular to the fiber direction, σ2m, and shear stress τ12m can be expressed as the functions of the applied (macro-) stresses, σ1A, σ2A , τ12A as follows: σ1m = α11σ1A +α12σ2A, σ2m = α21σ1A + α22σ2A, τ12m = α66τ12A, where α11 ,α12, α21, α22, α66 are stress-partitioning coefficients. Using skin-layer strips cut parallel, perpendicular and 45° to the molding direction, the stress in the matrix was measured under the uniaxial applied stress and the stress-partitioning coefficients of the above equations were determined. Once these relations are established, the macrostress in SFRP can be determined from the measurements of the matrix stresses by X-rays.

  12. NEUTRON DIFFRACTION MEASUREMENT OF RESIDUAL STRESSES IN FRICTION STIR PROCESSED NANOCOMPOSITE SURFACE LAYER

    SciTech Connect

    Xu, Hanbing; Hubbard, Camden R; An, Ke; Wang, Xun-Li; Feng, Zhili; Qu, Jun

    2009-01-01

    Friction stir processing (FSP) was successfully used to stir and mix nano-sized Al2O3 particles into a Al6061-T6 aluminum plate to form a nanocomposite layer up to 3 mm thick. This nanocomposite surface has demonstrated significantly improved surface hardness, yield strength, and wear-resistance without sacrificing the substrate ductility and conductivity. Neutron diffraction analysis was conducted to determine the residual stress distribution in the nanocomposite surface layer. For comparison, the residual stress of the aluminum surface that was processed similarly but had no particle involved was also measured. Results showed that the macro-level residual stresses in the FSP zone without particles are low due to the annealing effect induced by the long heating time and large heat input. The macro-level residual stresses in the FSP-processed Al-Al2O3 nanocomposite zone are tensile up to 100 MPa in all three directions. The details of the results will be further discussed in the paper.

  13. Residual Stresses in DC cast Aluminum Billet: Neutron Diffraction Measurements and Thermomechanical Modeling

    SciTech Connect

    Drezet, J.-M.; Evans, A.; Pirling, T.

    2011-05-04

    Thermally-induced residual stresses, generated during the industrial Direct Chill casting process of aluminum alloys, can cause both significant safety concerns as well as the formation of defects during down-stream processing. Although these thermally induced strains can be partially relieved by permanent deformation, cracks will be generated either during solidification (hot tears) or post-solidification cooling (cold cracks) when stresses exceed the deformation limit of the alloy. Furthermore, the thermally induced strains result in the presence of large internal stresses within the billet before further processing steps. Although numerical models have been previously developed to compute these residual stresses, most of the computations have been validated only against measured surface distortions. In the present work, the variation in residual elastic strains and stresses in the steady state regime of casting has been measured as a function of radial position using neutron diffraction in an AA6063 grain-refined cylindrical billet. These measurements have been carried out on the same billet section at Poldi at PSI-Villigen and at Salsa at ILL-Grenoble and compare favorably. The results are used to validate a thermo-mechanical finite element casting model and to assess the level of stored elastic energy within the billet.

  14. Residual Stresses in DC cast Aluminum Billet: Neutron Diffraction Measurements and Thermomechanical Modeling

    NASA Astrophysics Data System (ADS)

    Drezet, J.-M.; Evans, A.; Pirling, T.

    2011-05-01

    Thermally-induced residual stresses, generated during the industrial Direct Chill casting process of aluminum alloys, can cause both significant safety concerns as well as the formation of defects during down-stream processing. Although these thermally induced strains can be partially relieved by permanent deformation, cracks will be generated either during solidification (hot tears) or post-solidification cooling (cold cracks) when stresses exceed the deformation limit of the alloy. Furthermore, the thermally induced strains result in the presence of large internal stresses within the billet before further processing steps. Although numerical models have been previously developed to compute these residual stresses, most of the computations have been validated only against measured surface distortions. In the present work, the variation in residual elastic strains and stresses in the steady state regime of casting has been measured as a function of radial position using neutron diffraction in an AA6063 grain-refined cylindrical billet. These measurements have been carried out on the same billet section at Poldi at PSI-Villigen and at Salsa at ILL-Grenoble and compare favorably. The results are used to validate a thermo-mechanical finite element casting model and to assess the level of stored elastic energy within the billet.

  15. Residual stresses in a shape welded steel tube by neutron diffraction

    NASA Astrophysics Data System (ADS)

    Taran, Yu V.; Balagurov, A. M.; Schreiber, J.; Stuhr, U.

    2008-03-01

    Measurements of the triaxial residual strains in a composite tube from an austenitic stainless steel as a parent material and a shape welded ferritic steel were carried out by the time-of-flight neutron diffraction method on the POLDI instrument at the PSI SINQ neutron pulsed facility. The shape weld is used to build compressive stresses and, as a result, to suppress stress corrosion. Investigations of the residual stresses in such composite tubes are important for developing optimal welding techniques. Calculation of the residual stresses was performed using measurement results with a comb-sample, machined from the tube by the electro-discharge method, as the stress free reference sample. The results of the POLDI measurements of the stress state in the composite tube are presented and compared to the results of the destructive turning out method and theoretical predictions of calculations by the finite element method. Semiquantitative agreement between all the used methods was only observed for the tangential component of the stress tensor. In this case, the ferrite cladding produced a tangential compressive stress of about 800 MPa on the austenitic tube.

  16. Structure-based identification of catalytic residues

    PubMed Central

    Yahalom, Ran; Reshef, Dan; Wiener, Ayana; Frankel, Sagiv; Kalisman, Nir; Lerner, Boaz; Keasar, Chen

    2011-01-01

    The identification of catalytic residues is an essential step in functional characterization of enzymes. We present a purely structural approach to this problem, which is motivated by the difficulty of evolution-based methods to annotate structural genomics targets that have few or no homologs in the databases. Our approach combines a state-of-the-art support vector machine (SVM) classifier with novel structural features that augment structural clues by spatial averaging and Z-scoring. Special attention is paid to the class imbalance problem that stems from the overwhelming number of non-catalytic residues in enzymes compared to catalytic residues. This problem is tackled by: 1) optimizing the classifier to maximize a performance criterion that considers both type I and type II errors in the classification of catalytic and non-catalytic residues; 2) under-sampling non-catalytic residues before SVM training; and 3) during SVM training, penalizing errors in learning catalytic residues more than errors in learning non-catalytic residues. Tested on four enzyme datasets – one specifically designed by us to mimic the structural genomics scenario and three previously-evaluated datasets – our structure-based classifier is never inferior to similar structure-based classifiers and comparable to classifiers that use both structural and evolutionary features. In addition to evaluation of the performance of catalytic residue identification, we also present detailed case studies on three proteins. This analysis suggests that many false positive predictions may correspond to binding sites and other functional residues. A web server that implements the method, our own-designed database, and the source code of the programs are publicly available at http://www.cs.bgu.ac.il/~meshi/functionPrediction. PMID:21491495

  17. Structure-based identification of catalytic residues.

    PubMed

    Yahalom, Ran; Reshef, Dan; Wiener, Ayana; Frankel, Sagiv; Kalisman, Nir; Lerner, Boaz; Keasar, Chen

    2011-06-01

    The identification of catalytic residues is an essential step in functional characterization of enzymes. We present a purely structural approach to this problem, which is motivated by the difficulty of evolution-based methods to annotate structural genomics targets that have few or no homologs in the databases. Our approach combines a state-of-the-art support vector machine (SVM) classifier with novel structural features that augment structural clues by spatial averaging and Z scoring. Special attention is paid to the class imbalance problem that stems from the overwhelming number of non-catalytic residues in enzymes compared to catalytic residues. This problem is tackled by: (1) optimizing the classifier to maximize a performance criterion that considers both Type I and Type II errors in the classification of catalytic and non-catalytic residues; (2) under-sampling non-catalytic residues before SVM training; and (3) during SVM training, penalizing errors in learning catalytic residues more than errors in learning non-catalytic residues. Tested on four enzyme datasets, one specifically designed by us to mimic the structural genomics scenario and three previously evaluated datasets, our structure-based classifier is never inferior to similar structure-based classifiers and comparable to classifiers that use both structural and evolutionary features. In addition to the evaluation of the performance of catalytic residue identification, we also present detailed case studies on three proteins. This analysis suggests that many false positive predictions may correspond to binding sites and other functional residues. A web server that implements the method, our own-designed database, and the source code of the programs are publicly available at http://www.cs.bgu.ac.il/∼meshi/functionPrediction. PMID:21491495

  18. Quantitative measurement of phase variation amplitude of ultrasonic diffraction grating based on diffraction spectral analysis

    SciTech Connect

    Pan, Meiyan Zeng, Yingzhi; Huang, Zuohua

    2014-09-15

    A new method based on diffraction spectral analysis is proposed for the quantitative measurement of the phase variation amplitude of an ultrasonic diffraction grating. For a traveling wave, the phase variation amplitude of the grating depends on the intensity of the zeroth- and first-order diffraction waves. By contrast, for a standing wave, this amplitude depends on the intensity of the zeroth-, first-, and second-order diffraction waves. The proposed method is verified experimentally. The measured phase variation amplitude ranges from 0 to 2π, with a relative error of approximately 5%. A nearly linear relation exists between the phase variation amplitude and driving voltage. Our proposed method can also be applied to ordinary sinusoidal phase grating.

  19. Pulsed photothermal deflection and diffraction effects: numerical modeling based on Fresnel diffraction theory

    NASA Astrophysics Data System (ADS)

    Han, Yue; Wu, Z. L.; Rosenshein, Joseph S.; Thomsen, Marshall; Zhao, Qiang; Moncur, Kent

    1999-12-01

    We present a comprehensive theoretical model suitable for treating the effect of pulsed collinear photothermal deflection spectroscopy (PDS). The work is an extension of the theoretical model previously developed for the mirage effect, which can take into account both photothermal deflection and photothermal diffraction effects based on the Fresnel diffraction theory. With the diffraction model, both the collinear PDS and the photothermal lensing spectroscopy techniques can be treated in a unified manner. The model provides a detailed analysis of the laser-induced optical diffraction effect and can be used to optimize experimental parameters. The modeled results are presented in detail, with an emphasis on the advantages of using a near-field detection scheme for achieving the best sensitivity to local temperature change and better experimental stability against environmental noise.

  20. Residual stress measurements on thick plate low-alloy steel narrow gap weldments by x-ray diffraction

    SciTech Connect

    Rund, C.O.; DiMascio, P.S.; Pangborn, R.N.; Snoha, D.J.

    1984-06-01

    A unique x-ray diffraction instrument for residual stress measurement has been developed that provides for speed, ease of measurement, accuracy, and economy of surface stress measurement. Application of this instrument with a material removal technique, e.g., electropolishing, has facilitated detailed, high resolution studies of three-dimensional stress fields. This paper describes the instrumentation and techniques applied to conduct the residual stress measurement and presents maps of the residual stress data obtained for the surfaces of a heavy 2 1/4 Cr 1 Mo steel plate weldment.

  1. Neutron diffraction measurement of residual stresses in Al-clad U-10Mo fuel plates

    NASA Astrophysics Data System (ADS)

    Brown, D. W.; Okuniewski, M. A.; Clausen, B.; Moore, G. A.; Sisneros, T. A.

    2016-06-01

    Neutron diffraction was used to determine residual stress in monolithic two Al-clad U 10 weight percent Mo mini-fuel plates and a full sized fuel plate. One mini-plate was cooled following hot isostatic pressing at a rate of 6.75 °C/min, the second at 0.675 °C/min. A non-traditional method of calibrating the neutron diffractometer at each measurement point was necessitated by the thin nature of the sample. The in-plane stresses in the U-10Mo foils are relatively large, -250 MPa in the U-10Mo foil of the fast cooled mini-plate,-150 MPa in the slow cooled mini-plate and -275 MPa in the full-sized plate. Likewise, the in-plane stresses in the Al-cladding of the fast-cooled mini-plate and full-sized plate were determined to reach ∼50 MPa, while in the slow-cooled sample the stresses in the Al cladding were on the level of the measurement uncertainty. The in-plane stresses in the Zr diffusion barrier were estimated to be as large as -300 MPa.

  2. Procedure for Computing Residual Stresses from Neutron Diffraction Data and its Application to Multi-Pass Dissimilar Weld

    SciTech Connect

    Zhang, Wei; Feng, Zhili; Crooker, Paul

    2011-01-01

    Neutron diffraction is a powerful tool for non-destructive measurement of internal residual stresses of welded structures. The conventional approach for determination of residual stresses requires the knowledge of stress-free lattice spacing a priori. For multiple-pass dissimilar metal welds common to nuclear reactor pipeline systems, the stress-free lattice parameter is a complex function of position due to the chemistry inhomogeneity in the weld region and can be challenging to determine experimentally. This paper presents a new approach to calculate the residual stress field in dissimilar welds without the use of stress-free lattice parameter. The theoretical basis takes advantage of the fact that the normal component of welding residual stresses is typically small for thin plate or pipe welds. The applicability of the new approach is examined and justified in a multi-pass dissimilar metal weld consisting of a stainless steel plate and a nickel alloy filler metal. The level of uncertainties associated with this new approach is assessed. Neutron diffraction experiment is carried out to measure the lattice spacing at various locations in the dissimilar weld. A comb-shaped specimen, electro-discharge machined from a companion weld, is used to determine the stress-free lattice spacing. The calculated results from the new approach are consistent with those from the conventional approach. The new approach is found to be a practical method for determining the two in-plane residual stress components in thin plate or pipe dissimilar metal welds.

  3. Magnetic Barkhausen Noise and Neutron Diffraction Techniques for the Study of Intergranular Residual Strains in Mild Steel

    SciTech Connect

    Hutanu, Roxana; Clapham, Lynann; Rogge, Ronald

    2004-02-26

    Intergranular residual stresses (IS) are microscopic residual stresses which have been found to accumulate along the <100> direction in steels. The <100> direction is also the magnetic easy axis direction in steel. This work involved Magnetic Barkhausen Noise (MBN) studies on steel samples, deformed uniaxially to increasing levels of strain. The MBN results indicated that a bulk magnetic easy axis was produced by the deformation process, and neutron diffraction experiments showed that this easy axis was correlated with the tensile strain in grains oriented in the <100> direction.

  4. Angle-resolved diffraction grating biosensor based on porous silicon

    NASA Astrophysics Data System (ADS)

    Lv, Changwu; Jia, Zhenhong; Liu, Yajun; Mo, Jiaqing; Li, Peng; Lv, Xiaoyi

    2016-03-01

    In this study, an optical biosensor based on a porous silicon composite structure was fabricated using a simple method. This structure consists of a thin, porous silicon surface diffraction grating and a one-dimensional porous silicon photonic crystal. An angle-resolved diffraction efficiency spectrum was obtained by measuring the diffraction efficiency at a range of incident angles. The angle-resolved diffraction efficiency of the 2nd and 3rd orders was studied experimentally and theoretically. The device was sensitive to the change of refractive index in the presence of a biomolecule indicated by the shift of the diffraction efficiency spectrum. The sensitivity of this sensor was investigated through use of an 8 base pair antifreeze protein DNA hybridization. The shifts of the angle-resolved diffraction efficiency spectrum showed a relationship with the change of the refractive index, and the detection limit of the biosensor reached 41.7 nM. This optical device is highly sensitive, inexpensive, and simple to fabricate. Using shifts in diffraction efficiency spectrum to detect biological molecules has not yet been explored, so this study establishes a foundation for future work.

  5. Feasibility Study on Neutron Diffraction Method for Evaluation of Residual Strain Distribution of Regenerative Cooled Combustion Chamber

    NASA Astrophysics Data System (ADS)

    Masuoka, Tadashi; Moriya, Shin-Ichi; Sato, Masaki; Yoshida, Makoto; Tsuchiya, Yoshinori; Suzuki, Hiroshi

    The regenerative cooled combustion chamber of a cryogenic liquid rocket engine is exposed to a large temperature difference between the hot gas (about 3500K) and the liquid hydrogen (about 20K). This induces thermal stress, and strain is accumulated in the chamber wall throughout the cyclic firing tests. Evaluation of the stress and the strain distribution in a chamber wall is essential since chamber life is usually related to such stress and strain. In this study, the residual strain in a regenerative cooled combustion chamber wall was measured by applying the neutron diffraction method and the X-ray diffraction method. The measured data were compared with the numerical data by finite element analysis, and the feasibility of the neutron diffraction method for the regenerative cooled combustion chamber of a cryogenic liquid rocket engine was evaluated.

  6. Effect of Young's modulus evolution on residual stress measurement of thermal barrier coatings by X-ray diffraction

    NASA Astrophysics Data System (ADS)

    Chen, Q.; Mao, W. G.; Zhou, Y. C.; Lu, C.

    2010-09-01

    Subjected to thermal cycling, the apparent Young's modulus of air plasma-sprayed (APS) 8 wt.% Y 2O 3-stabilized ZrO 2 (8YSZ) thermal barrier coatings (TBCs) was measured by nanoindentation. Owing to the effects of sintering and porous microstructure, the apparent Young's modulus follows a Weibull distribution and changes from 50 to 93 GPa with an increase of thermal cycling. The evolution of residual stresses in the top coating of an 8YSZ TBC system was determined by X-ray diffraction (XRD). The residual stresses derived from the XRD data are well consistent with that obtained by the Vickers indention. It is shown that the evolution of Young's modulus plays an important role in improving the measurement precision of residual stresses in TBCs by XRD.

  7. rf streak camera based ultrafast relativistic electron diffraction.

    PubMed

    Musumeci, P; Moody, J T; Scoby, C M; Gutierrez, M S; Tran, T

    2009-01-01

    We theoretically and experimentally investigate the possibility of using a rf streak camera to time resolve in a single shot structural changes at the sub-100 fs time scale via relativistic electron diffraction. We experimentally tested this novel concept at the UCLA Pegasus rf photoinjector. Time-resolved diffraction patterns from thin Al foil are recorded. Averaging over 50 shots is required in order to get statistics sufficient to uncover a variation in time of the diffraction patterns. In the absence of an external pump laser, this is explained as due to the energy chirp on the beam out of the electron gun. With further improvements to the electron source, rf streak camera based ultrafast electron diffraction has the potential to yield truly single shot measurements of ultrafast processes. PMID:19191429

  8. Six Classes of Diffraction-Based Optoelectronic Instruments

    NASA Technical Reports Server (NTRS)

    Spremo, Stevan; Fuhr, Peter; Schipper, John

    2003-01-01

    Six classes of diffraction-based optoelectronic instruments have been invented as means for wavelength-based processing of light. One family of anticipated applications lies in scientific instrumentation for studying chemical and physical reactions that affect and/or are affected differently by light of different wavelengths or different combinations of wavelengths. Another family of anticipated applications lies in optoelectronic communication systems.

  9. As-Cast Residual Stresses in an Aluminum Alloy AA6063 Billet: Neutron Diffraction Measurements and Finite Element Modeling

    NASA Astrophysics Data System (ADS)

    Drezet, J.-M.; Phillion, A. B.

    2010-12-01

    The presence of thermally induced residual stresses, created during the industrial direct chill (DC) casting process of aluminum alloys, can cause both significant safety concerns and the formation of defects during downstream processing. Although numerical models have been previously developed to compute these residual stresses, most of the computations have been validated only against measured surface distortions. Recently, the variation in residual elastic strains in the steady-state regime of casting has been measured as a function of radial position using neutron diffraction (ND) in an AA6063 grain-refined cylindrical billet. In the present study, these measurements are used to show that a well-designed thermomechanical finite element (FE) process model can reproduce relatively well the experimental results. A sensitivity analysis is then carried out to determine the relative effect of the various mechanical parameters when computing the as-cast residual stresses in a cylindrical billet. Two model parameters have been investigated: the temperature when the alloy starts to thermally contract and the plasticity behavior. It is shown that the mechanical properties at low temperatures have a much larger influence on the residual stresses than those at high temperatures.

  10. Neutron Diffraction Residual Strain Tensor Measurements Within The Phase IA Weld Mock-up Plate P-5

    SciTech Connect

    Hubbard, Camden R

    2011-09-01

    Oak Ridge National Laboratory (ORNL) has worked with NRC and EPRI to apply neutron and X-ray diffraction methods to characterize the residual stresses in a number of dissimilar metal weld mockups and samples. The design of the Phase IA specimens aimed to enable stress measurements by several methods and computational modeling of the weld residual stresses. The partial groove in the 304L stainless steel plate was filled with weld beads of Alloy 82. A summary of the weld conditions for each plate is provided in Table 1. The plates were constrained along the long edges during and after welding by bolts with spring-loaded washers attached to the 1-inch thick Al backing plate. The purpose was to avoid stress relief due to bending of the welded stainless steel plate. The neutron diffraction method was one of the methods selected by EPRI for non-destructive through thickness strain and stress measurement. Four different plates (P-3 to P-6) were studied by neutron diffraction strain mapping, representing four different welding conditions. Through thickness neutron diffraction strain mappings at NRSF2 for the four plates and associated strain-free d-zero specimens involved measurement along seven lines across the weld and at six to seven depths. The mountings of each plate for neutron diffraction measurements were such that the diffraction vector was parallel to each of the three primary orthogonal directions of the plate: two in-plane directions, longitudinal and transverse, and the direction normal to the plate (shown in left figure within Table 1). From the three orthogonal strains for each location, the residual stresses along the three plate directions were calculated. The principal axes of the strain and stress tensors, however, need not necessarily align with the plate coordinate system. To explore this, plate P-5 was selected for examination of the possibility that the principal axes of strain are not along the sample coordinate system axes. If adequate data could

  11. Residual stress measurements of welded components using synchrotron and neutron diffraction.

    SciTech Connect

    Paradowska, A. M.; Price, J. W .H; Finlayson, T. R.; Lienert, U.; Ibrahim, R.; Monash Univ.; Univ. of Melbourne

    2007-01-01

    Residual stress remains the single largest unknown in industrial damage situations. Residual stresses have a significant effect on corrosion, fracture resistance, creep and corrosion/fatigue performance and a reduction of these stresses is normally desirable. In this research high energy synchrotron (70 keV) radiation (at the Advanced Photon Source) and thermal neutrons (at the Lucas Heights Research Reactor) have been employed to investigate and compare the residual stress characteristics in fully restrained samples with different numbers of weld beads. The aim of the research was to characterize the residual stress distribution which arises in a welded component with increasing number of beads. The number and resolution of the measurements carried out in this work reveal significant features of the residual stress pattern in single bead in the as-welded condition and after post-weld heat treatment. The intention is to provide key data for the validation of design, fitness-for-purpose methodologies and finite-element tools. In this presentation the details of the synchrotron X-ray and neutron techniques will be compared and contrasted, utilizing results from a number of weldment samples.

  12. MEMS-based diffractive optical-beam-steering technology

    NASA Astrophysics Data System (ADS)

    Winick, David A.; Duewer, Bruce E.; Chaudhury, Som; Wilson, John M.; Tucker, John; Eksi, Umut; Franzon, Paul D.

    1998-03-01

    This paper presents some results from phase-1 research into developing a beam steerer based on micro-mechanical diffractive elements. The position of these elements is electrostatically controlled, to allow dynamic programming of a 2D phase function. Feasibility prototypes were constructed in the MUMPs polysilicon surface micromachine process.

  13. FEA predictions of residual stress in stainless steel compared to neutron and x-ray diffraction measurements. [Finite element analysis

    SciTech Connect

    Flower, E.C.; MacEwen, S.R.; Holden, T.M.

    1987-05-01

    Residual stresses in a body arise from nonuniform plastic deformation and continue to be an important consideration in the design and the fabrication of metal components. The finite element method offers a potentially powerful tool for predicting these stresses. However, it is important to first verify this method through careful analysis and experimentation. This paper describes experiments using neutron and x-ray diffraction to provide quantitative data to compare to finite element analysis predictions of deformation induced residual stress in a plane stress austenitic stainless steel ring. Good agreement was found between the experimental results and the numerical predictions. Effects of the formulation of the finite element model on the analysis, constitutive parameters and effects of machining damage in the experiments are addressed.

  14. X-Ray Diffraction Analysis of Residual Stress in Thin Polycrystalline Anatase Films and Elastic Anisotropy of Anatase

    NASA Astrophysics Data System (ADS)

    Matěj, Z.; Kužel, R.; Nichtová, L.

    2011-11-01

    The importance of residual stress in anatase thin films for their photo-induced hydrophilicity was proved recently. Detailed X-ray diffraction (XRD) studies of residual stresses in titanium dioxide films are presented here. Measurements including multiple hkl reflections on several series of these films revealed the presence of tensile stresses in the films that were obtained by crystallization from amorphous state. Significant anisotropy of the strain was also found and compared with that of anatase, resulting from its theoretically calculated single-crystal elastic constants. The XRD data support the experimental evidence of the hypothesis that the [00 l] axis is the elastically soft anatase direction, whereas the directions in the [ h00] × [ hk0] plane are elastically stiff. This is in agreement with the anisotropy predicted by single-crystal elastic constants that are obtained from ab-initio calculations. Residual stress analysis for materials with tetragonal symmetry is described and the theory is used to analyze the data. The anisotropy is very different from that for the rutile phase, and the experimental results agree well with the values calculated for anatase. A simplified method of XRD residual stress analysis in thin anatase films by total pattern fitting (TPF) is also presented. Tensile stresses are formed during the crystallization process and increase rapidly with reduced film thickness. They inhibit crystallization, which is then very slow in the thinnest films.

  15. High spatial resolution, high energy synchrotron x-ray diffraction characterization of residual strains and stresses in laser shock peened Inconel 718SPF alloy

    NASA Astrophysics Data System (ADS)

    Gill, Amrinder S.; Zhou, Zhong; Lienert, Ulrich; Almer, Jonathan; Lahrman, David F.; Mannava, S. R.; Qian, Dong; Vasudevan, Vijay K.

    2012-04-01

    Laser shock peening (LSP) is an advanced surface enhancement technique used to enhance the fatigue strength of metal parts by imparting deep compressive residual stresses. In the present study, LSP was performed on IN718 SPF alloy, a fine grained nickel-based superalloy, with three different power densities and depth resolved residual strain and stress characterization was conducted using high energy synchrotron x-ray diffraction in beam line 1-ID-C at the Advanced Photon Source at the Argonne National laboratory. A fine probe size and conical slits were used to non-destructively obtain data from specific gauge volumes in the samples, allowing for high-resolution strain measurements. The results show that LSP introduces deep compressive residual stresses and the magnitude and depth of these stresses depend on the energy density of the laser. The LSP induced residual stresses were also simulated using three-dimensional nonlinear finite element analysis, with employment of the Johnson-Cook model for describing the nonlinear materials constitutive behavior. Good agreement between the experimental and simulated data was obtained. These various results are presented and discussed.

  16. Relationship between dislocations and residual stresses in cold-drawn pearlitic steel analyzed by energy-dispersive X-ray diffraction

    SciTech Connect

    Sato, Shigeo; Wagatsuma, Kazuaki; Suzuki, Shigeru; Kumagai, Masayoshi; Imafuku, Muneyuki; Tashiro, Hitoshi; Kajiwara, Kentaro; Shobu, Takahiasa

    2013-09-15

    We analyzed the dislocation distribution of cold-drawn pearlitic-steel wire by using the line-profile analysis based on the energy dispersive X-ray diffraction (EDXD). Although this line-profile analysis requires a high resolution in reciprocal space, the resolution for EDXD is generally poor due to the energy resolution of the detector. Our analysis demonstrated that the resolution in the reciprocal space can be maximized at small scattering angles. Using the line-profile analysis based on the EDXD, the microstructural parameters such as the crystallite size and the dislocation density of the ferrite phase in the pearlitic steel were successfully analyzed. In addition, the distribution of the residual stress of the ferrite phase of a pearlitic steel wire was also analyzed using the EDXD measurement. - Highlights: • Energy dispersive X-ray diffraction is applied to the line-profile analysis. • Distribution of dislocations in ferrite in the pearlitic steel wire is analyzed. • Relationship between dislocations and residual stress is discussed.

  17. Tolerance analysis of multilayer diffractive optics based on polychromatic integral diffraction efficiency.

    PubMed

    Mao, Shan; Cui, Qingfeng; Piao, Mingxu

    2015-11-10

    Multilayer diffractive optical elements (MLDOEs) can achieve high diffraction efficiency for broadband wavelength. Polychromatic integral diffraction efficiency (PIDE) is the key concern for evaluating diffraction efficiency over the waveband. The modulation transfer function of a hybrid refractive-diffractive optical system is directly affected by the PIDE. The relationship between PIDE and continuous manufacturing errors for microstructure heights and periodic widths of MLDOEs is studied theoretically in this paper, and an example of MLDOEs is discussed in the visible waveband. The analysis results can be used for manufacturing error control in microstructure heights and periodic widths. PMID:26560782

  18. Residual stress measurements in a zircaloy-4 weld by neutron diffraction

    SciTech Connect

    Carr, D.G.; Ripley, M.I.; Holden, T.M.; Brown, D.W.; Vogel, S.C

    2004-08-16

    The macroscopic stress distribution across a Zircaloy-4 gas tungsten arc weld was measured by time-of-flight neutron diffraction at the SMARTS diffractometer at Los Alamos National Laboratory. The method enabled the measurement of strain for all the available reflections permitted by the rolling texture of the plate and the modified texture in the weld-metal and heat affected zone. A maximum longitudinal stress of 220 {+-} 40 MPa was observed in the weld compared with the 0.2% yield stress of 390 MPa of the plate. A maximum transverse stress of 60 {+-} 40 MPa was observed in the weld. Textures were measured at the HIPPO diffractometer.

  19. An EUV beamsplitter based on conical grazing incidence diffraction.

    PubMed

    Braig, C; Fritzsch, L; Käsebier, T; Kley, E-B; Laubis, C; Liu, Y; Scholze, F; Tünnermann, A

    2012-01-16

    We present an innovative grating design based on conical diffraction which acts as an almost perfect and low-loss beamsplitter for extreme ultraviolet radiation. The scheme is based on a binary profile operated in grazing incidence along the grating bars under total external reflection. It is shown that periods of a few 10(2) nm may permit an exclusive (±1)(st) order diffraction with efficiencies up to ~ 35% in each of them, whereas higher evanescent orders vanish. In contrast, destructive interference eliminates the 0(th) order. For a sample made of SiO(2) on silicon, measured data and simulated results from rigorous coupled wave analysis procedures are given. PMID:22274527

  20. Goniometer-based femtosecond X-ray diffraction of mutant 30S ribosomal subunit crystals.

    PubMed

    Dao, E Han; Sierra, Raymond G; Laksmono, Hartawan; Lemke, Henrik T; Alonso-Mori, Roberto; Coey, Aaron; Larsen, Kevin; Baxter, Elizabeth L; Cohen, Aina E; Soltis, S Michael; DeMirci, Hasan

    2015-07-01

    In this work, we collected radiation-damage-free data from a set of cryo-cooled crystals for a novel 30S ribosomal subunit mutant using goniometer-based femtosecond crystallography. Crystal quality assessment for these samples was conducted at the X-ray Pump Probe end-station of the Linac Coherent Light Source (LCLS) using recently introduced goniometer-based instrumentation. These 30S subunit crystals were genetically engineered to omit a 26-residue protein, Thx, which is present in the wild-type Thermus thermophilus 30S ribosomal subunit. We are primarily interested in elucidating the contribution of this ribosomal protein to the overall 30S subunit structure. To assess the viability of this study, femtosecond X-ray diffraction patterns from these crystals were recorded at the LCLS during a protein crystal screening beam time. During our data collection, we successfully observed diffraction from these difficult-to-grow 30S ribosomal subunit crystals. Most of our crystals were found to diffract to low resolution, while one crystal diffracted to 3.2 Å resolution. These data suggest the feasibility of pursuing high-resolution data collection as well as the need to improve sample preparation and handling in order to collect a complete radiation-damage-free data set using an X-ray Free Electron Laser. PMID:26798805

  1. Goniometer-based femtosecond X-ray diffraction of mutant 30S ribosomal subunit crystals

    SciTech Connect

    Dao, E. Han; Sierra, Raymond G.; Laksmono, Hartawan; Lemke, Henrik T.; Alonso-Mori, Roberto; Coey, Aaron; Larsen, Kevin; Baxter, Elizabeth L.; Cohen, Aina E.; Soltis, S. Michael; DeMirci, Hasan

    2015-04-30

    In this work, we collected radiation-damage-free data from a set of cryo-cooled crystals for a novel 30S ribosomal subunit mutant using goniometer-based femtosecond crystallography. Crystal quality assessment for these samples was conducted at the X-ray Pump Probe end-station of the Linac Coherent Light Source (LCLS) using recently introduced goniometer-based instrumentation. These 30S subunit crystals were genetically engineered to omit a 26-residue protein, Thx, which is present in the wild-type Thermus thermophilus 30S ribosomal subunit. We are primarily interested in elucidating the contribution of this ribosomal protein to the overall 30S subunit structure. To assess the viability of this study, femtosecond X-ray diffraction patterns from these crystals were recorded at the LCLS during a protein crystal screening beam time. During our data collection, we successfully observed diffraction from these difficult-to-grow 30S ribosomal subunit crystals. Most of our crystals were found to diffract to low resolution, while one crystal diffracted to 3.2 Å resolution. These data suggest the feasibility of pursuing high-resolution data collection as well as the need to improve sample preparation and handling in order to collect a complete radiation-damage-free data set using an X-ray Free Electron Laser.

  2. Goniometer-based femtosecond X-ray diffraction of mutant 30S ribosomal subunit crystals

    DOE PAGESBeta

    Dao, E. Han; Sierra, Raymond G.; Laksmono, Hartawan; Lemke, Henrik T.; Alonso-Mori, Roberto; Coey, Aaron; Larsen, Kevin; Baxter, Elizabeth L.; Cohen, Aina E.; Soltis, S. Michael; et al

    2015-04-30

    In this work, we collected radiation-damage-free data from a set of cryo-cooled crystals for a novel 30S ribosomal subunit mutant using goniometer-based femtosecond crystallography. Crystal quality assessment for these samples was conducted at the X-ray Pump Probe end-station of the Linac Coherent Light Source (LCLS) using recently introduced goniometer-based instrumentation. These 30S subunit crystals were genetically engineered to omit a 26-residue protein, Thx, which is present in the wild-type Thermus thermophilus 30S ribosomal subunit. We are primarily interested in elucidating the contribution of this ribosomal protein to the overall 30S subunit structure. To assess the viability of this study, femtosecondmore » X-ray diffraction patterns from these crystals were recorded at the LCLS during a protein crystal screening beam time. During our data collection, we successfully observed diffraction from these difficult-to-grow 30S ribosomal subunit crystals. Most of our crystals were found to diffract to low resolution, while one crystal diffracted to 3.2 Å resolution. These data suggest the feasibility of pursuing high-resolution data collection as well as the need to improve sample preparation and handling in order to collect a complete radiation-damage-free data set using an X-ray Free Electron Laser.« less

  3. Evaluation on double-wall-tube residual stress distribution of sodium-heated steam generator by neutron diffraction and numerical analysis

    SciTech Connect

    Kisohara, N.; Suzuki, H.; Akita, K.; Kasahara, N.

    2012-07-01

    A double-wall-tube is nominated for the steam generator heat transfer tube of future sodium fast reactors (SFRs) in Japan, to decrease the possibility of sodium/water reaction. The double-wall-tube consists of an inner tube and an outer tube, and they are mechanically contacted to keep the heat transfer of the interface between the inner and outer tubes by their residual stress. During long term SG operation, the contact stress at the interface gradually falls down due to stress relaxation. This phenomenon might increase the thermal resistance of the interface and degrade the tube heat transfer performance. The contact stress relaxation can be predicted by numerical analysis, and the analysis requires the data of the initial residual stress distributions in the tubes. However, unclear initial residual stress distributions prevent precious relaxation evaluation. In order to resolve this issue, a neutron diffraction method was employed to reveal the tri-axial (radius, hoop and longitudinal) initial residual stress distributions in the double-wall-tube. Strain gauges also were used to evaluate the contact stress. The measurement results were analyzed using a JAEA's structural computer code to determine the initial residual stress distributions. Based on the stress distributions, the structural computer code has predicted the transition of the relaxation and the decrease of the contact stress. The radial and longitudinal temperature distributions in the tubes were input to the structural analysis model. Since the radial thermal expansion difference between the inner (colder) and outer (hotter) tube reduces the contact stress and the tube inside steam pressure contributes to increasing it, the analytical model also took these effects into consideration. It has been conduced that the inner and outer tubes are contacted with sufficient stresses during the plant life time, and that effective heat transfer degradation dose not occur in the double-wall-tube SG. (authors)

  4. Diffraction based overlay metrology for α-carbon applications

    NASA Astrophysics Data System (ADS)

    Saravanan, Chandra Saru; Tan, Asher; Dasari, Prasad; Goelzer, Gary; Smith, Nigel; Woo, Seouk-Hoon; Shin, Jang Ho; Kang, Hyun Jae; Kim, Ho Chul

    2008-03-01

    Applications that require overlay measurement between layers separated by absorbing interlayer films (such as α- carbon) pose significant challenges for sub-50nm processes. In this paper scatterometry methods are investigated as an alternative to meet these stringent overlay metrology requirements. In this article, a spectroscopic Diffraction Based Overlay (DBO) measurement technique is used where registration errors are extracted from specially designed diffraction targets. DBO measurements are performed on detailed set of wafers with varying α-carbon (ACL) thicknesses. The correlation in overlay values between wafers with varying ACL thicknesses will be discussed. The total measurement uncertainty (TMU) requirements for these layers are discussed and the DBO TMU results from sub-50nm samples are reviewed.

  5. A vectorial ray-based diffraction integral for optical systems

    NASA Astrophysics Data System (ADS)

    Andreas, Birk

    2015-09-01

    The propagation of coherent laser light in optical systems is simulated by the vectorial ray-based diffraction integral (VRBDI) method which utilizes vectorial diffraction theory, ray aiming, differential ray tracing and matrix optics. On a global scale the method is not restricted to the paraxial approximation, whereas it is properly used for a local representation of the wavefront close to an aimed detection location. First, the field of a monochromatic continuous wave on an input plane is decomposed into spherical or plane wave components. Then, these components are represented by aimed ray tubes and traced through an optical system. Finally, the contributions are added coherently on an output plane whose position has to be chosen according to ray-aiming requirements. Provided that the apertures in the optical system are large with respect to the wavelength the results are fairly accurate.

  6. Tunable-microlens-based multipoint diffraction strain sensor

    NASA Astrophysics Data System (ADS)

    Zhu, Hui; Asundi, Anand

    2009-12-01

    Multipoint Diffraction Strain Sensor (MDSS) is a novel and promising strain sensing system to acquire whole field strain information with high accuracy without the need for numerical differentiation. Compared to traditional optical diffraction strain sensors, the main advantage of MDSS is the use of micro-lens array to get whole field information. Both tilt and in-plane strain can be acquired separately by using two symmetric incident laser beams. However, it is costly and troublesome to fabricate, adjust or replace lens arrays for different applications. A practical way to solve this problem is to use a liquid crystal lens as spatial light modulator which displays Diffractive Optical Element (DOE) based lens array. This liquid crystal lens is software controlled capable to display any user designed DOE pattern. The sensitivity and field of interrogation is thus tuneable by changing focal length of lens arrays. Moreover arbitrary size or shape of lens arrays can be designed to measure certain part of the specimen in most interest. Experimental results with different lens arrays are demonstrated for uniform rotations.

  7. Diffractive Optical Elements based in Diamond Like Carbon (DLC) films

    NASA Astrophysics Data System (ADS)

    Sparvoli, M. Marina; Mansano, Ronaldo D.

    2008-04-01

    In this work was developed a Diffractive Optical Elements (DOEs) based in amorphous hydrogenated carbon (Diamond Like Carbon) films. DOEs can be built in large scale with high reproducibility and eliminating almost stages used in optical elements tradicional fabrication, as abrasion and burnishing. These devices had been built by the etching of DLC deposited by sputtering process. The characterizations of these devices are realized by optical analyzes with a 633 nm HeNe laser. The DLC films roughness and etch rate after process were measured by high step meter.

  8. X-ray diffraction study of residual stresses in metal-matrix composite-jacketed steel cylinders subjected to internal pressure. Final report

    SciTech Connect

    Lee, S.L.; Doxbeck, M.; Capsimalis, G.

    1992-03-01

    The study of aluminum/silicon carbide metal matrix composite (MMC)-jacketed steel structural components was made because of their light weight and high stiffness. Steel 'liner' cylinders were wrapped with MMC 'jackets' with an all-hoop layup and put through various degrees of hydraulic autofrettage and thermal soak. In this report, the results from our x-ray diffraction residual stress measurements on cylinders using a position-sensitive scintillation detection system are discussed. Our experimental results are compared with theoretical predictions from a model based on the elastic-plastic analysis of a thick-walled cylinder subjected to internal pressure. Interpretation of the interference effect caused by the MMC jacket on the steel liner is also discussed.

  9. Diffraction measurements with a boron-based GEM neutron detector

    NASA Astrophysics Data System (ADS)

    Croci, Gabriele; Albani, Giorgia; Cazzaniga, Carlo; Perelli Cippo, Enrico; Schooneveld, Erik; Claps, Gerardo; Cremona, Anna; Grosso, Giovanni; Muraro, Andrea; Murtas, Fabrizio; Rebai, Marica; Scherillo, Antonella; Tardocchi, Marco; Gorini, Giuseppe

    2014-07-01

    The research of reliable substitutes of 3He detectors is an important task for the affordability of new neutron scattering instrumentation for future spallation sources like the European Spallation Source. GEM (Gas Electron Multiplier)-based detectors represent a valid alternative since they can combine high-rate capability, coverage of up to 1\\ \\text{m}^{2} area and good intrinsic spatial resolution (for this detector class it can be better than 0.5 mm). The first neutron diffraction measurements performed using a borated GEM detector are reported. The detector has an active area of 10 \\times 5\\ \\text{cm}^{2} and is equipped with a borated cathode. The GEM detector was read out using the standard ISIS Data Acquisition System. The comparison with measurements performed with standard 3He detectors shows that the broadening of the peaks measured on the diffractogram obtained with the GEM is 20-30% wider than the one obtained by 3He tubes but the active area of the GEM is twice that of 3He tubes. The GEM resolution is improved if half of its active area is considered. The signal-to-background ratio of the GEM is about 1.5 to 2 times lower than that of 3He. This measurement proves that GEM detectors can be used for neutron diffraction measurements and paves the way for their use at future neutron spallation sources.

  10. Binaural Sound Localizer for Azimuthal Movement Detection Based on Diffraction

    PubMed Central

    Kim, Keonwook; Choi, Anthony

    2012-01-01

    Sound localization can be realized by utilizing the physics of acoustics in various methods. This paper investigates a novel detection architecture for the azimuthal movement of sound source based on the interaural level difference (ILD) between two receivers. One of the microphones in the system is surrounded by barriers of various heights in order to cast the direction dependent diffraction of the incoming signal. The gradient analysis of the ILD between the structured and unstructured microphone demonstrates the rotation directions as clockwise, counter clockwise, and no rotation of the sound source. Acoustic experiments with different types of sound source over a wide range of target movements show that the average true positive and false positive rates are 67% and 16%, respectively. Spectral analysis demonstrates that the low frequency delivers decreased true and false positive rates and the high frequency presents increases of both rates, overall. PMID:23112617

  11. Residual stress mapping by micro X-ray diffraction: Application to the study of thin film buckling

    SciTech Connect

    Goudeau, P.; Villain, P.; Tamura, N.; Celestre, R.S.; Padmore, H.A.

    2002-11-06

    Thin films deposited by Physical Vapour Deposition techniques on substrates generally exhibit large residual stresses which may be responsible of spontaneous detachment of the film from its substrate and in the case of compressive stresses, thin film buckling. Although these effects are undesirable for future applications, one may take benefit of it for thin film mechanical properties investigation. Since the 80's, a lot of theoretical works have been done to develop mechanical models with the aim to get a better understanding of driven mechanisms giving rise to this phenomenon and thus to propose solutions to avoid such problems. Nevertheless, only a few experimental works have been done on this subject to support these theoretical results and nothing concerning local stress/strain measurement mainly because of the small dimension of the buckling (few tenth mm). This paper deals with the application of micro beam x-ray diffraction available on synchrotron radiation sources for stress/ strain mapping analysis of gold thin film buckling.

  12. Large Diffractive Optics for GEo-Based Earth Surveillance

    SciTech Connect

    Hyde, R A

    2003-09-11

    in diameter, building ten-fold larger ones for GEO applications (let alone delivering and operating them there) presents major difficulties. However, since the challenges of fielding large platforms in GEO are matched by the benefits of continuous coverage, we propose a program to develop such optical platforms. In this section, we will examine a particular form of large aperture optic, using a flat diffractive lens instead of the more conventional curved reflectors considered elsewhere in this report. We will discuss both the development of this type of large aperture optics, as well as the steps necessary to use it for GEO-based Earth surveillance. In a later section of this report we will discuss another use for large diffractive optics, their application for global-reach laser weapons.

  13. Diffraction leveraged modulation of X-ray pulses using MEMS-based X-ray optics

    DOEpatents

    Lopez, Daniel; Shenoy, Gopal; Wang, Jin; Walko, Donald A.; Jung, Il-Woong; Mukhopadhyay, Deepkishore

    2016-08-09

    A method and apparatus are provided for implementing Bragg-diffraction leveraged modulation of X-ray pulses using MicroElectroMechanical systems (MEMS) based diffractive optics. An oscillating crystalline MEMS device generates a controllable time-window for diffraction of the incident X-ray radiation. The Bragg-diffraction leveraged modulation of X-ray pulses includes isolating a particular pulse, spatially separating individual pulses, and spreading a single pulse from an X-ray pulse-train.

  14. Twenty Meter Space Telescope Based on Diffractive Fresnel Lens

    SciTech Connect

    Early, J; Hyde, R; Baron, R

    2003-06-26

    Diffractive lenses offer two potential advantages for very large aperture space telescopes; very loose surface-figure tolerances and physical implementation as thin, flat optical elements. In order to actually realize these advantages one must be able to build large diffractive lenses with adequate optical precision and also to compactly stow the lens for launch and then fully deploy it in space. We will discuss the recent fabrication and assembly demonstration of a 5m glass diffractive Fresnel lens at LLNL. Optical performance data from smaller full telescopes with diffractive lens and corrective optics show diffraction limited performance with broad bandwidths. A systems design for a 20m space telescope will be presented. The primary optic can be rolled to fit inside of the standard fairings of the Delta IV vehicle. This configuration has a simple deployment and requires no orbital assembly. A twenty meter visible telescope could have a significant impact in conventional astronomy with eight times the resolution of Hubble and over sixty times the light gathering capacity. If the light scattering is made acceptable, this telescope could also be used in the search for terrestrial planets.

  15. Silica Nanowire Arrays for Diffraction-Based Bioaffinity Sensing

    PubMed Central

    Loget, Gabriel; Corn, Robert M.

    2014-01-01

    Arrays of electrodeposited silica nanowires (SiO2 NWs) have been fabricated over large areas (cm2) on fluoropolymer thin films attached to glass substrates by a combination of photolithography and electrochemically triggered sol-gel nanoscale deposition. Optical and SEM measurements revealed that the SiO2 NW arrays had an average spacing of 10 micrometers and an average width of 700 nm with a significant grain structure that was a result of the sol-gel deposition process. The optical diffraction properties at 633 nm of the SiO2 NWs arrays were characterized when placed in contact with solutions using a prism-coupled total internal reflection geometry; quantification of changes in these diffraction properties was applied in various sensing applications. Bulk refractive index sensing using the SiO2 NWs grating was demonstrated with a refractive index resolution of 1.30 × 10−5 RIU. Toposelectively chemically-modified SiO2 NW arrays were used for diffraction biosensing measurements of surface binding events, such as the electrostatic adsorption of gold nanoparticles and the bioaffinity adsorption of streptavidin onto a biotin monolayer. Finally, the application of the SiO2 NWs arrays for practical medical diagnostic applications was demonstrated by monitoring the diffraction of SiO2 NWs arrays functionalized with a single-stranded DNA aptamer in order to detect human α-thrombin from solutions at sub-pathologic nanomolar concentrations. PMID:24590560

  16. Silica nanowire arrays for diffraction-based bioaffinity sensing.

    PubMed

    Loget, Gabriel; Corn, Robert M

    2014-08-18

    Arrays of electrodeposited silica nanowires (SiO2 NWs) have been fabricated over large areas (cm(2)) on fluoropolymer thin films attached to glass substrates by a combination of photolithography and electrochemically triggered sol-gel nanoscale deposition. Optical and scanning electron microscopy (SEM) measurements revealed that the SiO2 NW arrays had an average spacing of ten micrometers and an average width of 700 nm with a significant grain structure that was a result of the sol-gel deposition process. The optical diffraction properties at 633 nm of the SiO2 NW arrays were characterized when placed in contact with solutions by using a prism-coupled total internal reflection geometry; quantification of changes in these diffraction properties was applied in various sensing applications. Bulk refractive index sensing by using the SiO2 NW grating was demonstrated with a sensitivity of 1.30×10(-5) RIU. Toposelectively chemically modified SiO2 NW arrays were used for diffraction biosensing measurements of surface binding events, such as the electrostatic adsorption of gold nanoparticles and the bioaffinity adsorption of streptavidin onto a biotin monolayer. Finally, the application of the SiO2 NW arrays for practical medical-diagnostic applications was demonstrated by monitoring the diffraction of SiO2 NW arrays functionalized with a single-stranded (ss)DNA aptamer to detect human α-thrombin from solutions at sub-pathologic nanomolar concentrations. PMID:24590560

  17. Evaluation of local structure alphabets based on residue burial.

    PubMed

    Karchin, Rachel; Cline, Melissa; Karplus, Kevin

    2004-05-15

    Residue burial, which describes a protein residue's exposure to solvent and neighboring atoms, is key to protein structure prediction, modeling, and analysis. We assessed 21 alphabets representing residue burial, according to their predictability from amino acid sequence, conservation in structural alignments, and utility in one fold-recognition scenario. This follows upon our previous work in assessing nine representations of backbone geometry.1 The alphabet found to be most effective overall has seven states and is based on a count of C(beta) atoms within a 14 A-radius sphere centered at the C(beta) of a residue of interest. When incorporated into a hidden Markov model (HMM), this alphabet gave us a 38% performance boost in fold recognition and 23% in alignment quality. PMID:15103615

  18. Three-dimensional welding residual stresses evaluation based on the eigenstrain methodology via X-ray measurements at the surface

    NASA Astrophysics Data System (ADS)

    Ogawa, Masaru

    2014-12-01

    In order to assure structural integrity for operating welded structures, it is necessary to evaluate crack growth rate and crack propagation direction for each observed crack non-destructively. Here, three dimensional (3D) welding residual stresses must be evaluated to predict crack propagation. Today, X-ray diffraction is used and the ultrasonic method has been proposed as non-destructive method to measure residual stresses. However, it is impossible to determine residual stress distributions in the thickness direction. Although residual stresses through a depth of several tens of millimeters can be evaluated non-destructively by neutron diffraction, it cannot be used as an on-site measurement technique. This is because neutron diffraction is only available in special irradiation facilities. Author pays attention to the bead flush method based on the eigenstrain methodology. In this method, 3D welding residual stresses are calculated by an elastic Finite Element Method (FEM) analysis from eigenstrains which are evaluated by an inverse analysis from released strains by strain gauges in the removal of the reinforcement of the weld. Here, the removal of the excess metal can be regarded as non-destructive treatment because toe of weld which may become crack starters can be eliminated. The effectiveness of the method has been proven for welded plates and pipes even with relatively lower bead height. In actual measurements, stress evaluation accuracy becomes poorer because measured values of strain gauges are affected by processing strains on the machined surface. In the previous studies, the author has developed the bead flush method that is free from the influence of the affecting strains by using residual strains on surface by X-ray diffraction. However, stress evaluation accuracy is not good enough because of relatively poor measurement accuracy of X-ray diffraction. In this study, a method to improve the estimation accuracy of residual stresses in this method is

  19. Layered holographic stereogram based on inverse Fresnel diffraction.

    PubMed

    Zhang, Hao; Zhao, Yan; Cao, Liangcai; Jin, Guofan

    2016-01-20

    We propose an efficient algorithm using layered holographic stereogram for three-dimensional (3D) computer-generated holograms. The hologram is spatially partitioned into multiple holographic elements (hogels) to provide the occlusion effect and motion parallax by use of multiple viewpoint rendering. Each hogel is calculated with inverse Fresnel diffraction by slicing the viewing frustum according to the depth image. The sliced layers can provide accurate depth cues for reconstruction since the geometric information of the 3D scene is faithfully matched. The algorithm is compatible with computer graphics rendering techniques and robust for holograms with different parameters. When the hogel size equals 1 mm, the signal-to-noise ratio of the diffraction calculation is above 39 dB with a propagation distance longer than 10 mm. Numerical simulations and optical experiments have demonstrated that the proposed method can reconstruct quality 3D images with reduced computational load. PMID:26835948

  20. Dedicated spectrometers based on diffractive optics: design, modelling and evaluation

    NASA Astrophysics Data System (ADS)

    Løvhaugen, O.; Johansen, I.-R.; Bakke, K. A. H.; Fismen, B. G.; Nicolas, S.

    The described design of diffractive optical elements for low cost IR-spectrometers gives a built-in wavelength reference and allows 'spectral arithmetic' to be implemented in the optical performance of the DOE. The diffractive element combines the function of the lenses and the grating and eliminates the need for alignment of those components in the standard scanned grating spectrometer design. The element gives out a set of foci, each with one spectral component, which are scanned across a detector, thus relaxing the demands for scan angle control. It can thus be regarded as an alternative solution to a beam splitter and band pass filter instrument. Software tools have been designed to ease the adaptation of the design to different applications. To model the performance of the spectrometers we have implemented a scalar Rayleigh-Sommerfeldt diffraction model. The gold-coated elements are produced by injection moulding using a compact disc (CD) moulding technique and mould inlays mastered by e-beam lithography. The optimized selection of wavelength bands and the classification of the measured signal use a combination of principal component analysis and robust statistical methods. Typical applications will be material characterization of recycled plastics and gas monitoring. Spectrometers for two different applications have been built and tested. Comparisons between the design goals and the measured performance have been made and show good agreements.

  1. Model-checking techniques based on cumulative residuals.

    PubMed

    Lin, D Y; Wei, L J; Ying, Z

    2002-03-01

    Residuals have long been used for graphical and numerical examinations of the adequacy of regression models. Conventional residual analysis based on the plots of raw residuals or their smoothed curves is highly subjective, whereas most numerical goodness-of-fit tests provide little information about the nature of model misspecification. In this paper, we develop objective and informative model-checking techniques by taking the cumulative sums of residuals over certain coordinates (e.g., covariates or fitted values) or by considering some related aggregates of residuals, such as moving sums and moving averages. For a variety of statistical models and data structures, including generalized linear models with independent or dependent observations, the distributions of these stochastic processes tinder the assumed model can be approximated by the distributions of certain zero-mean Gaussian processes whose realizations can be easily generated by computer simulation. Each observed process can then be compared, both graphically and numerically, with a number of realizations from the Gaussian process. Such comparisons enable one to assess objectively whether a trend seen in a residual plot reflects model misspecification or natural variation. The proposed techniques are particularly useful in checking the functional form of a covariate and the link function. Illustrations with several medical studies are provided. PMID:11890304

  2. High energy X-ray diffraction measurement of residual stresses in a monolithic aluminum clad uranium–10 wt% molybdenum fuel plate assembly

    SciTech Connect

    D. W. Brown; M. A. Okuniewski; J. D. Almer; L. Balogh; B. Clausen; J. S. Okasinski; B. H. Rabin

    2013-10-01

    Residual stresses are expected in monolithic, aluminum clad uranium 10 wt% molybdenum (U–10Mo) nuclear fuel plates because of the large mismatch in thermal expansion between the two bonded materials. The full residual stress tensor of the U–10Mo foil in a fuel plate assembly was mapped with 0.1 mm resolution using high-energy (86 keV) X-ray diffraction. The in-plane stresses in the U–10Mo foil are strongly compressive, roughly -250 MPa in the longitudinal direction and -140 MPa in the transverse direction near the center of the fuel foil. The normal component of the stress is weakly compressive near the center of the foil and tensile near the corner. The disparity in the residual stress between the two in-plane directions far from the edges and the tensile normal stress suggest that plastic deformation in the aluminum cladding during fabrication by hot isostatic pressing also contributes to the residual stress field. A tensile in-plane residual stress is presumed to be present in the aluminum cladding to balance the large in-plane compressive stresses in the U–10Mo fuel foil, but cannot be directly measured with the current technique due to large grain size.

  3. Selenium adsorption to aluminum-based water treatment residuals

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Aluminum-based water treatment residuals (WTR) can adsorb water- and soil-borne P, As(V), As(III), and perchlorate, and may be able to adsorb excess environmental selenium. WTR, clay minerals, and amorphous aluminum hydroxide were shaken for 24 hours in selenate or selenite solutions at pH values o...

  4. Selenium Adsorption To Aluminum-Based Water Treatment Residuals

    EPA Science Inventory

    Aluminum-based water treatment residuals (WTR) can adsorb water-and soil-borne P, As(V), As(III), and perchlorate, and may be able to adsorb excess environmental selenium. WTR, clay minerals, and amorphous aluminum hydroxide were shaken for 24 hours in selenate or selenite solut...

  5. Folding simulations of alanine-based peptides with lysine residues.

    PubMed Central

    Sung, S S

    1995-01-01

    The folding of short alanine-based peptides with different numbers of lysine residues is simulated at constant temperature (274 K) using the rigid-element Monte Carlo method. The solvent-referenced potential has prevented the multiple-minima problem in helix folding. From various initial structures, the peptides with three lysine residues fold into helix-dominated conformations with the calculated average helicity in the range of 60-80%. The peptide with six lysine residues shows only 8-14% helicity. These results agree well with experimental observations. The intramolecular electrostatic interaction of the charged lysine side chains and their electrostatic hydration destabilize the helical conformations of the peptide with six lysine residues, whereas these effects on the peptides with three lysine residues are small. The simulations provide insight into the helix-folding mechanism, including the beta-bend intermediate in helix initiation, the (i, i + 3) hydrogen bonds, the asymmetrical helix propagation, and the asymmetrical helicities in the N- and C-terminal regions. These findings are consistent with previous studies. PMID:7756550

  6. Residual stress determination from a laser-based curvature measurement

    SciTech Connect

    W. D. Swank; R. A. Gavalya; J. K. Wright; R. N. Wright

    2000-05-08

    Thermally sprayed coating characteristics and mechanical properties are in part a result of the residual stress developed during the fabrication process. The total stress state in a coating/substrate is comprised of the quench stress and the coefficient of thermal expansion (CTE) mismatch stress. The quench stress is developed when molten particles impact the substrate and rapidly cool and solidify. The CTE mismatch stress results from a large difference in the thermal expansion coefficients of the coating and substrate material. It comes into effect when the substrate/coating combination cools from the equilibrated deposit temperature to room temperature. This paper describes a laser-based technique for measuring the curvature of a coated substrate and the analysis required to determine residual stress from curvature measurements. Quench stresses were determined by heating the specimen back to the deposit temperature thus removing the CTE mismatch stress. By subtracting the quench stress from the total residual stress at room temperature, the CTE mismatch stress was estimated. Residual stress measurements for thick (>1mm) spinel coatings with a Ni-Al bond coat on 304 stainless steel substrates were made. It was determined that a significant portion of the residual stress results from the quenching stress of the bond coat and that the spinel coating produces a larger CTE mismatch stress than quench stress.

  7. Residual Stress Determination from a Laser-Based Curvature Measurement

    SciTech Connect

    Swank, William David; Gavalya, Rick Allen; Wright, Julie Knibloe; Wright, Richard Neil

    2000-05-01

    Thermally sprayed coating characteristics and mechanical properties are in part a result of the residual stress developed during the fabrication process. The total stress state in a coating/substrate is comprised of the quench stress and the coefficient of thermal expansion (CTE) mismatch stress. The quench stress is developed when molten particles impact the substrate and rapidly cool and solidify. The CTE mismatch stress results from a large difference in the thermal expansion coefficients of the coating and substrate material. It comes into effect when the substrate/coating combination cools from the equilibrated deposit temperature to room temperature. This paper describes a laser-based technique for measuring the curvature of a coated substrate and the analysis required to determine residual stress from curvature measurements. Quench stresses were determined by heating the specimen back to the deposit temperature thus removing the CTE mismatch stress. By subtracting the quench stress from the total residual stress at room temperature, the CTE mismatch stress was estimated. Residual stress measurements for thick (>1mm) spinel coatings with a Ni-Al bond coat on 304 stainless steel substrates were made. It was determined that a significant portion of the residual stress results from the quenching stress of the bond coat and that the spinel coating produces a larger CTE mismatch stress than quench stress.

  8. Determination and mitigation of the uncertainty of neutron diffraction measurements of residual strain in large-grained polycrystalline material

    PubMed Central

    Holden, Tom M.; Traore, Yeli; James, Jon; Kelleher, Joe; Bouchard, P. John

    2015-01-01

    For large-grained samples it is advantageous to perform pairs of neutron diffraction measurements at the same spatial location but rotated 180° around the geometric centre of the gauge volume as a means of minimizing the scatter coming from the random positioning of grains within the gauge volume. PMID:25844082

  9. Non destructive neutron diffraction measurements of cavities, inhomogeneities, and residual strain in bronzes of Ghiberti's relief from the Gates of Paradise

    SciTech Connect

    Festa, G.; Senesi, R.; Alessandroni, M.; Andreani, C.; Vitali, G.; Porcinai, S.; Giusti, A. M.; Materna, T.; Paradowska, A. M.

    2011-03-15

    Quantitative neutron studies of cultural heritage objects provide access to microscopic, mesoscopic, and macroscopic structures in a nondestructive manner. In this paper we present a neutron diffraction investigation of a Ghiberti Renaissance gilded bronze relief devoted to the measurement of cavities and inhomogeneities in the bulk of the sample, along with the bulk phase composition and residual strain distribution. The quantitative measurements allowed the determination of the re-melting parts extension, as well as improving current knowledge about the manufacturing process. The study provides significant and unique information to conservators and restorators about the history of the relief.

  10. An OFDM-Based Speech Encryption System without Residual Intelligibility

    NASA Astrophysics Data System (ADS)

    Tseng, Der-Chang; Chiu, Jung-Hui

    Since an FFT-based speech encryption system retains a considerable residual intelligibility, such as talk spurts and the original intonation in the encrypted speech, this makes it easy for eavesdroppers to deduce the information contents from the encrypted speech. In this letter, we propose a new technique based on the combination of an orthogonal frequency division multiplexing (OFDM) scheme and an appropriate QAM mapping method to remove the residual intelligibility from the encrypted speech by permuting several frequency components. In addition, the proposed OFDM-based speech encryption system needs only two FFT operations instead of the four required by the FFT-based speech encryption system. Simulation results are presented to show the effectiveness of this proposed technique.

  11. Optical refractometry based on Fresnel diffraction from a phase wedge.

    PubMed

    Tavassoly, M Taghi; Saber, Ahad

    2010-11-01

    A method that utilizes the Fresnel diffraction of light from the phase step formed by a transparent wedge is introduced for measuring the refractive indices of transparent solids, liquids, and solutions. It is shown that, as a transparent wedge of small apex angle is illuminated perpendicular to its surface by a monochromatic parallel beam of light, the Fresnel fringes, caused by abrupt change in refractive index at the wedge lateral boundary, are formed on a screen held perpendicular to the beam propagation direction. The visibility of the fringes varies periodically between zero and 1 in the direction normal to the wedge apex. For a known or measured apex angle, the wedge refractive index is obtained by measuring the period length by a CCD. To measure the refractive index of a transparent liquid or solution, the wedge is installed in a transparent rectangle cell containing the sample. Then, the cell is illuminated perpendicularly and the visibility period is measured. By using modest optics, one can measure the refractive index at a relative uncertainty level of 10(-5). There is no limitation on the refractive index range. The method can be applied easily with no mechanical manipulation. The measuring apparatus can be very compact with low mechanical and optical noises. PMID:21042389

  12. Microcontroller based spectrophotometer using compact disc as diffraction grid

    NASA Astrophysics Data System (ADS)

    Bano, Saleha; Altaf, Talat; Akbar, Sunila

    2010-12-01

    This paper describes the design and implementation of a portable, inexpensive and cost effective spectrophotometer. The device combines the use of compact disc (CD) media as diffraction grid and 60 watt bulb as a light source. Moreover it employs a moving slit along with stepper motor for obtaining a monochromatic light, photocell with spectral sensitivity in visible region to determine the intensity of light and an amplifier with a very high gain as well as an advanced virtual RISC (AVR) microcontroller ATmega32 as a control unit. The device was successfully applied to determine the absorbance and transmittance of KMnO4 and the unknown concentration of KMnO4 with the help of calibration curve. For comparison purpose a commercial spectrophotometer was used. There are not significant differences between the absorbance and transmittance values estimated by the two instruments. Furthermore, good results are obtained at all visible wavelengths of light. Therefore, the designed instrument offers an economically feasible alternative for spectrophotometric sample analysis in small routine, research and teaching laboratories, because the components used in the designing of the device are cheap and of easy acquisition.

  13. Image cloning beyond diffraction based on coherent population trapping in a hot rubidium vapor.

    PubMed

    Ding, Dong-Sheng; Zhou, Zhi-Yuan; Shi, Bao-Sen

    2014-01-15

    Following recent theoretical predictions, we report on an experimental realization of image cloning beyond usual diffraction, through the coherent population trapping (CPT) effect in a hot rubidium vapor. In our experiment, an alphabet letter image was transferred from a coupling field to a probe field, based on the CPT effect. Furthermore, we demonstrate that the cloned probe field carrying the image is transmitted without the usual diffraction. To our best knowledge, this is the first experimental report about image cloning beyond diffraction. We believe this mechanism, based on CPT, has definite and important applications in image metrology, image processing, and biomedical imaging. PMID:24562116

  14. Residuals and the Residual-Based Statistic for Testing Goodness of Fit of Structural Equation Models

    ERIC Educational Resources Information Center

    Foldnes, Njal; Foss, Tron; Olsson, Ulf Henning

    2012-01-01

    The residuals obtained from fitting a structural equation model are crucial ingredients in obtaining chi-square goodness-of-fit statistics for the model. The authors present a didactic discussion of the residuals, obtaining a geometrical interpretation by recognizing the residuals as the result of oblique projections. This sheds light on the…

  15. Neutron Diffraction Measurement of Residual Stresses, Dislocation Density and Texture in Zr-bonded U-10Mo ''Mini'' Fuel Foils and Plates

    SciTech Connect

    Brown, Donald W.; Okuniewski, M. A.; Sisneros, Thomas A.; Clausen, Bjorn; Moore, G. A.; Balogh, L

    2014-08-07

    Aluminum clad monolithic uranium 10 weight percent molybdenum (U-10Mo) fuel plates are being considered for conversion of several research and test nuclear reactors from high-enriched to low-enriched uranium fuel due to the inherently high density of fissile material. Comprehensive neutron diffraction measurements of the evolution of the textures, residual phase stresses, and dislocation densities in the individual phases of the mini-foils throughout several processing steps and following hot-isostatic pressing to the Al cladding, have been completed. Recovery and recrystallization of the bare U-10Mo fuel foil, as indicated by the dislocation density and texture, are observed depending on the state of the material prior to annealing and the duration and temperature of the annealing process. In general, the HIP procedure significantly reduces the dislocation density, but the final state of the clad plate, both texture and dislocation density, depends strongly on the final processing step of the fuel foil. In contrast, the residual stresses in the clad fuel plate do not depend strongly on the final processing step of the bare foil prior to HIP bonding. Rather, the residual stresses are dominated by the thermal expansion mismatch of the constituent materials of the fuel plate.

  16. The Role of Cold Work in Eddy Current Residual Stress Measurements in Shot-Peened Nickel-Base Superalloys

    SciTech Connect

    Yu, F.; Nagy, P. B.

    2006-03-06

    Recently, it was shown that eddy current methods can be adapted to residual stress measurement in shot-peened nickel-base superalloys. However, experimental evidence indicates that the piezoresistivity effect is simply not high enough to account for the observed apparent eddy current conductivity (AECC) increase. At the same time, X-ray diffraction data indicates that 'cold work' lingers even when the residual stress is fully relaxed and the excess AECC is completely gone. It is impossible to account for both observations with a single coherent explanation unless we assume that instead of a single 'cold work' effect, there are two varieties of cold work; type-A and type-B. Type-A cold work (e.g., changes in the microscopic homogeneity of the material) is not detected by X-ray diffraction as it does not significantly affect the beam width, but causes substantial conductivity change and exhibits strong thermal relaxation. Type-B cold work (e.g., dislocations) is detected by X-ray, but causes little or no conductivity change and exhibits weak thermal relaxation. Based on the assumption of two separate cold-work variables and that X-ray diffraction results indicate the presence of type-B, but not type-A, all observed phenomena can be explained. If this working hypothesis is proven right, the separation of residual stress and type-A cold work is less critical because they both relax much earlier and much faster than type-B cold work.

  17. Leaching characteristics of calcium-based compounds in MSWI Residues: From the viewpoint of clogging risk.

    PubMed

    Xia, Yi; Zhang, Hua; Phoungthong, Khamphe; Shi, Dong-Xiao; Shen, Wen-Hui; Shao, Li-Ming; He, Pin-Jing

    2015-08-01

    Leachate collection system (LCS) clogging caused by calcium precipitation would be disadvantageous to landfill stability and operation. Meanwhile, calcium-based compounds are the main constituents in both municipal solid waste incineration bottom ash (MSWIBA) and stabilized air pollution control residues (SAPCR), which would increase the risk of LCS clogging once these calcium-rich residues were disposed in landfills. The leaching behaviors of calcium from the four compounds and municipal solid waste incineration (MSWI) residues were studied, and the influencing factors on leaching were discussed. The results showed that pH was the crucial factor in the calcium leaching process. CaCO3 and CaSiO3 began leaching when the leachate pH decreased to less than 7 and 10, respectively, while Ca3(PO4)2 leached at pH<12. CaSO4 could hardly dissolve in the experimental conditions. Moreover, the sequence of the leaching rate for the different calcium-based compounds is as follows: CaSiO3>Ca3(PO4)2>CaCO3. The calcium leaching from the MSWIBA and SAPCR separately started from pH<7 and pH<12, resulting from CaCO3 and Ca3(PO4)2 leaching respectively, which was proven by the X-ray diffraction results. Based on the leaching characteristics of the different calcium compounds and the mineral phase of calcium in the incineration residues, simulated computation of their clogging potential was conducted, providing the theoretical basis for the risk assessment pertaining to LCS clogging in landfills. PMID:25934218

  18. Diffractive optics based on modulated subwavelength-domain V-ridge gratings

    NASA Astrophysics Data System (ADS)

    Bose, Gaurav; Verhoeven, Antonie; Vartiainen, Ismo; Roussey, Matthieu; Kuittinen, Markku; Tervo, Jani; Turunen, Jari

    2016-08-01

    We study the properties of reflection-type V-ridge gratings in the subwavelength domain and describe a method to realize diffractive optical elements by using such gratings as signal carriers. In particular, we utilize a coding scheme based on position modulation of a high-frequency V-ridge carrier grating. We design and demonstrate beam splitting elements using this coding scheme, electron-beam lithography, anisotropic wet etching of silicon, hot embossing of polymer, and metal deposition. These elements have the outstanding property of operating over a large spectral range from 406 to 520 nm. The measured diffraction patterns show excellent agreement with theoretical results given by rigorous diffraction theory.

  19. Leaching characteristics of calcium-based compounds in MSWI Residues: From the viewpoint of clogging risk

    SciTech Connect

    Xia, Yi; Zhang, Hua; Phoungthong, Khamphe; Shi, Dong-Xiao; Shen, Wen-Hui; Shao, Li-Ming; He, Pin-Jing

    2015-08-15

    Highlights: • The leaching behavior of Ca-based compounds commonly in MSWI residues was studied. • pH is the crucial factor for calcium leaching process. • CaCO{sub 3} was the most sensitive to leaching temperature and Ca{sub 3}(PO{sub 4}){sub 2} was the least. • Ca leaching of MSWIBA and SAPCR attributed to CaCO{sub 3} and Ca{sub 3}(PO{sub 4}){sub 2} respectively. • Potential clogging ability of MSWI residues leachate in open air was calculated. - Abstract: Leachate collection system (LCS) clogging caused by calcium precipitation would be disadvantageous to landfill stability and operation. Meanwhile, calcium-based compounds are the main constituents in both municipal solid waste incineration bottom ash (MSWIBA) and stabilized air pollution control residues (SAPCR), which would increase the risk of LCS clogging once these calcium-rich residues were disposed in landfills. The leaching behaviors of calcium from the four compounds and municipal solid waste incineration (MSWI) residues were studied, and the influencing factors on leaching were discussed. The results showed that pH was the crucial factor in the calcium leaching process. CaCO{sub 3} and CaSiO{sub 3} began leaching when the leachate pH decreased to less than 7 and 10, respectively, while Ca{sub 3}(PO{sub 4}){sub 2} leached at pH < 12. CaSO{sub 4} could hardly dissolve in the experimental conditions. Moreover, the sequence of the leaching rate for the different calcium-based compounds is as follows: CaSiO{sub 3} > Ca{sub 3}(PO{sub 4}){sub 2} > CaCO{sub 3}. The calcium leaching from the MSWIBA and SAPCR separately started from pH < 7 and pH < 12, resulting from CaCO{sub 3} and Ca{sub 3}(PO{sub 4}){sub 2} leaching respectively, which was proven by the X-ray diffraction results. Based on the leaching characteristics of the different calcium compounds and the mineral phase of calcium in the incineration residues, simulated computation of their clogging potential was conducted, providing the

  20. High sensitivity refractive index sensor based on simple diffraction from phase grating.

    PubMed

    Sahoo, Pankaj K; Joseph, Joby; Yukino, Ryoji; Sandhu, Adarsh

    2016-05-01

    We present a technique for refractive index sensing using a phase grating structure. A grating under normal incidence can be designed such that the first-order diffracted light travels at a diffraction angle of 90° with respect to the zeroth order. The diffracted light, which is along the direction of periodicity, can further be diffracted from the grating and interfere with the zeroth-order light. Under this condition, the π phase difference that arises between the two interfering beams results in a transmission dip. We can tune this dip wavelength for senor applications, based on the grating equation. This Letter presents both simulation and experimental data that show good agreement with each other. PMID:27128084

  1. Neutron diffraction studies towards deciphering the protonation state of catalytic residues in the bacterial KDN9P phosphatase

    PubMed Central

    Bryan, Tyrel; González, Javier M.; Bacik, John P.; DeNunzio, Nicholas J.; Unkefer, Clifford J.; Schrader, Tobias E.; Ostermann, Andreas; Dunaway-Mariano, Debra; Allen, Karen N.; Fisher, S. Zoë

    2013-01-01

    The enzyme 2-keto-3-deoxy-9-O-phosphonononic acid phosphatase (KDN9P phosphatase) functions in the pathway for the production of 2-keto-3-deoxy-d-­glycero-d-galacto-nononic acid, a sialic acid that is important for the survival of commensal bacteria in the human intestine. The enzyme is a member of the haloalkanoate dehalogenase superfamily and represents a good model for the active-site protonation state of family members. Crystals of approximate dimensions 1.5 × 1.0 × 1.0 mm were obtained in space group P21212, with unit-cell parameters a = 83.1, b = 108.9, c = 75.7 Å. A complete neutron data set was collected from a medium-sized H/D-exchanged crystal at BIODIFF at the Heinz Maier-Leibnitz Zentrum (MLZ), Garching, Germany in 18 d. Initial refinement to 2.3 Å resolution using only neutron data showed significant density for catalytically important residues. PMID:23989152

  2. Study of Mechanical Properties of AZ91 Magnesium Alloy Welded by Laser Process Taking into Account the Anisotropy Microhardness and Residual Stresses by X-Ray Diffraction

    NASA Astrophysics Data System (ADS)

    Kouadri, A.; Barrallier, L.

    2011-07-01

    The objective of this investigation was to study the mechanical properties of a magnesium alloy welded by a CO2 laser. Residual stresses were measured by X-ray diffraction. They were calculated by the classic sin2 ψ method in the isotropic zones by using the orientation distribution function (ODF) in the textured zones. The results demonstrated that laser welding results in the formation of several different zones with different microstructural and mechanical properties. Welding principally leads to a reduction in grain size and a new distribution of phases. The most remarkable observation was that of a superficial layer on the surface of the welded zone. This layer has a marked crystallographic texture, a reduction in the level of aluminum, and an elevated microhardness. These characteristics disappear at a depth of 200 μm under the welded zone. These modifications can be explained by the nature of the solidification, which occurs under nonequilibrium conditions resulting in an equiaxial columnar transition. This transition is evident also within the profile of residual tensile stresses, which are at their maximum at the interface between the superficial layer and the rest of the welded zone. These results are explained by the anisotropic properties of the textured layer in relation to the plasticity.

  3. The nature of light: a description of photon diffraction based upon virtual particle exchange

    NASA Astrophysics Data System (ADS)

    Mobley, Michael J.

    2005-08-01

    Any discussion of the nature of light must include a reminder that whenever we make the observation of light (photons), we only observe particle-like properties. This paper provides a reiteration that we don"t need wave-like properties to scattered photons to describe phenomena such as diffraction or refraction of light. This paper updates the original ideas of Duane, later revived by Lande, which provided a description of light diffraction without making reference to a wave nature. These are updated using terminology more common to quantum electrodynamics which describes the interaction of particles in terms of the exchange of virtual photons. Diffraction is described in terms of an ensemble of distinct, probability weighted paths for the scattered photons. The scattering associated with each path results from the quantized momentum exchange with the scattering lattice attributed to the exchange or reflection of virtual photons. The probability for virtual particle exchange/reflection is dependent upon the allowed momentum states of the lattice determined by a Fourier analysis of the lattice geometry. Any scattered photon will exhibit an apparent wavelength inversely proportional to its momentum. Simplified, particle-like descriptions are developed for Young"s double slit diffraction, Fraunhofer diffraction and Fresnel diffraction. This description directly accounts for the quantization of momentum transferred to the scattering lattice and the specific eigenvalues of the lattice based upon the constraints to virtual photon exchange set by the Uncertainty Principle, Δπi = h/ζi.

  4. Physically-based constitutive modelling of residual stress development in welding of aluminium alloy 2024

    SciTech Connect

    Preston, R.V.; Shercliff, H.R. . E-mail: hrs@eng.cam.ac.uk; Withers, P.J.; Smith, S.

    2004-10-04

    A finite element model has been developed to predict the evolution of residual stress and distortion which takes into account the history-dependence of the yield stress-temperature response of heat-treatable aluminium alloys during welding. The model was applied to TIG welding of 2024-T3 aluminium alloy, and the residual strain predictions validated using high resolution X-ray synchrotron diffraction. The goal was to capture the influence of the permanent evolution of the microstructure during the thermal cycle with a straightforward numerical procedure, while retaining a sound physical basis. Hardness and resistivity measurements after isothermal hold-and-quench experiments were used to identify salient temperatures for zero, partial and full dissolution of the initial hardening precipitates, and the extent of softening - both immediately after welding, and after natural ageing. Based on these data, a numerical procedure for weld modelling was proposed for tracking the different yield responses during heating and cooling based on the peak temperature reached locally. This history-dependent model was superior to a conventional model in predicting the peak tensile strains, but otherwise the effect of temperature history was weak for 2024-T3. Predictions of the hardness profile immediately after welding compared with the post-weld naturally aged hardness provided insight into the competition between dissolution and coarsening of the precipitates in the heat-affected zone.

  5. Fatigue investigations of autofrettaged steel cylinders based on neutron-diffraction measurements

    NASA Astrophysics Data System (ADS)

    de Swardt, R. R.; Venter, A. M.; van der Watt, M. W.

    A series of cyclic internal pressurization fatigue experiments was conducted on partially autofrettaged cylinders with multiple internal radial elliptic shaped cracks covering a wide range of possible configurations. A theoretical model was developed to predict the theoretical fatigue life using as input data the actual measured position of the plastic boundary from neutron-diffraction measurements on the failed specimens, as well as a position calculated analytically from the autofrettage pressure. The theoretical fatigue-life predictions based on the neutron-diffraction results were found to give the best correlation with experimental fatigue results.

  6. Optical double-image cryptography based on diffractive imaging with a laterally-translated phase grating.

    PubMed

    Chen, Wen; Chen, Xudong; Sheppard, Colin J R

    2011-10-10

    In this paper, we propose a method using structured-illumination-based diffractive imaging with a laterally-translated phase grating for optical double-image cryptography. An optical cryptosystem is designed, and multiple random phase-only masks are placed in the optical path. When a phase grating is laterally translated just before the plaintexts, several diffraction intensity patterns (i.e., ciphertexts) can be correspondingly obtained. During image decryption, an iterative retrieval algorithm is developed to extract plaintexts from the ciphertexts. In addition, security and advantages of the proposed method are analyzed. Feasibility and effectiveness of the proposed method are demonstrated by numerical simulation results. PMID:22015370

  7. Imaging regenerating bone tissue based on neural networks applied to micro-diffraction measurements

    SciTech Connect

    Campi, G.; Pezzotti, G.; Fratini, M.; Ricci, A.; Burghammer, M.; Cancedda, R.; Mastrogiacomo, M.; Bukreeva, I.; Cedola, A.

    2013-12-16

    We monitored bone regeneration in a tissue engineering approach. To visualize and understand the structural evolution, the samples have been measured by X-ray micro-diffraction. We find that bone tissue regeneration proceeds through a multi-step mechanism, each step providing a specific diffraction signal. The large amount of data have been classified according to their structure and associated to the process they came from combining Neural Networks algorithms with least square pattern analysis. In this way, we obtain spatial maps of the different components of the tissues visualizing the complex kinetic at the base of the bone regeneration.

  8. A system model for ultrasonic NDT based on the Physical Theory of Diffraction (PTD).

    PubMed

    Darmon, M; Dorval, V; Kamta Djakou, A; Fradkin, L; Chatillon, S

    2016-01-01

    Simulation of ultrasonic Non Destructive Testing (NDT) is helpful for evaluating performances of inspection techniques and requires the modelling of waves scattered by defects. Two classical flaw scattering models have been previously usually employed and evaluated to deal with inspection of planar defects, the Kirchhoff approximation (KA) for simulating reflection and the Geometrical Theory of Diffraction (GTD) for simulating diffraction. Combining them so as to retain advantages of both, the Physical Theory of Diffraction (PTD) initially developed in electromagnetism has been recently extended to elastodynamics. In this paper a PTD-based system model is proposed for simulating the ultrasonic response of crack-like defects. It is also extended to provide good description of regions surrounding critical rays where the shear diffracted waves and head waves interfere. Both numerical and experimental validation of the PTD model is carried out in various practical NDT configurations, such as pulse echo and Time of Flight Diffraction (TOFD), involving both crack tip and corner echoes. Numerical validation involves comparison of this model with KA and GTD as well as the Finite-Element Method (FEM). PMID:26323548

  9. Single-order transmission diffraction gratings based on dispersion engineered all-dielectric metasurfaces

    NASA Astrophysics Data System (ADS)

    Gupta, Shulabh

    2016-08-01

    A single-order transmission diffraction grating based on dispersion engineered all-dielectric metasurfaces is proposed and its wavelength discriminating properties have been theoretically described and confirmed using numerical simulations. The metasurface is designed using a 2D array of all-dielectric resonators, which emulates a Huygens source configuration to achieve a perfect match to free-space in broad bandwidth. Using a holey dielectric nanodisk structure as the unit cell, the resonant wavelength is tapered across the metasurface to engineer the wavelength dependent spatial phase gradient, to emulate a dispersive prism. Consequently, different wavelengths are steered towards different directions and thus are discriminated on the output image plane. Due to subwavelength periodicities involved, the wavelength discrimination is achieved directly in the zeroth diffraction order of the device, unlike conventional diffraction gratings, thereby providing a high efficiency wavelength discriminating device.

  10. Micromachined diffraction based optical microphones and intensity probes with electrostatic force feedback

    NASA Astrophysics Data System (ADS)

    Bicen, Baris

    Measuring acoustic pressure gradients is critical in many applications such as directional microphones for hearing aids and sound intensity probes. This measurement is especially challenging with decreasing microphone size, which reduces the sensitivity due to small spacing between the pressure ports. Novel, micromachined biomimetic microphone diaphragms are shown to provide high sensitivity to pressure gradients on one side of the diaphragm with low thermal mechanical noise. These structures have a dominant mode shape with see-saw like motion in the audio band, responding to pressure gradients as well as spurious higher order modes sensitive to pressure. In this dissertation, integration of a diffraction based optical detection method with these novel diaphragm structures to implement a low noise optical pressure gradient microphone is described and experimental characterization results are presented, showing 36 dBA noise level with 1mm port spacing, nearly an order of magnitude better than the current gradient microphones. The optical detection scheme also provides electrostatic actuation capability from both sides of the diaphragm separately which can be used for active force feedback. A 4-port electromechanical equivalent circuit model of this microphone with optical readout is developed to predict the overall response of the device to different acoustic and electrostatic excitations. The model includes the damping due to complex motion of air around the microphone diaphragm, and it calculates the detected optical signal on each side of the diaphragm as a combination of two separate dominant vibration modes. This equivalent circuit model is verified by experiments and used to predict the microphone response with different force feedback schemes. Single sided force feedback is used for active damping to improve the linearity and the frequency response of the microphone. Furthermore, it is shown that using two sided force feedback one can significantly suppress

  11. Structural Assembly of Molecular Complexes Based on Residual Dipolar Couplings

    PubMed Central

    Berlin, Konstantin; O’Leary, Dianne P.; Fushman, David

    2010-01-01

    We present and evaluate a rigid-body molecular docking method, called PATIDOCK, that relies solely on the three-dimensional structure of the individual components and the experimentally derived residual dipolar couplings (RDC) for the complex. We show that, given an accurate ab initio predictor of the alignment tensor from a protein structure, it is possible to accurately assemble a protein-protein complex by utilizing the RDC’s sensitivity to molecular shape to guide the docking. The proposed docking method is robust against experimental errors in the RDCs and computationally efficient. We analyze the accuracy and efficiency of this method using experimental or synthetic RDC data for several proteins, as well as synthetic data for a large variety of protein-protein complexes. We also test our method on two protein systems for which the structure of the complex and steric-alignment data are available (Lys48-linked diubiquitin and a complex of ubiquitin and a ubiquitin-associated domain) and analyze the effect of flexible unstructured tails on the outcome of docking. The results demonstrate that it is fundamentally possible to assemble a protein-protein complex based solely on experimental RDC data and the prediction of the alignment tensor from three-dimensional structures. Thus, despite the purely angular nature of residual dipolar couplings, they can be converted into intermolecular distance/translational constraints. Additionally we show a method for combining RDCs with other experimental data, such as ambiguous constraints from interface mapping, to further improve structure characterization of the protein complexes. PMID:20550109

  12. Determination of pesticide residues in fruit-based soft drinks.

    PubMed

    García-Reyes, Juan F; Gilbert-López, Bienvenida; Molina-Díaz, Antonio; Fernández-Alba, Amadeo R

    2008-12-01

    Here we report the first worldwide reconnaissance study of the presence and occurrence of pesticides in fruit-based soft drinks. While there are strict regulations and exhaustive controls for pesticides in fruits, vegetables, and drinking water, scarce attention has been paid to highly consumed derivate products, which may contain these commodities as ingredients. In the case of the fruit-based soft drinks industry, there are no clear regulations, relating to pesticides, which address them, even when there is significant consumption in vulnerable groups such as children. In this work, we have developed a screening method to search automatically for up to 100 pesticides in fruit-based soft drinks extracts based on the application of liquid chromatography-electrospray time-of-flight mass spectrometry (LC-TOF MS). The sample extracts injected were obtained by a preliminary sample treatment step based on solid-phase extraction using hydrophilic-lipophilic balanced polymer-based reverse phase cartridges and methanol as eluting solvent. Subsequent identification, confirmation, and quantitation were carried out by LC-TOF MS analysis: the confirmation of the target species was based on retention time matching and accurate mass measurements of protonated molecules ([M + H]+) and fragment ions (obtaining accuracy errors typically lower than 2 ppm). With the proposed method, we measured over 100 fruit-based soft drink samples, purchased from 15 different countries from companies with brands distributed worldwide and found relatively large concentration levels of pesticides in most of the samples analyzed. The concentration levels detected were of the micrograms per liter level, low when considering the European maximum residue levels (MRLs) set for fruits but very high (i.e., 300 times) when considering the MRLs for drinking or bottled water. The detected pesticides (carbendazim, thiabendazole, imazalil and its main degradate, prochloraz and its main degradate, malathion, and

  13. Enumerating Pathways of Proton Abstraction Based on a Spatial and Electrostatic Analysis of Residues in the Catalytic Site

    PubMed Central

    Chakraborty, Sandeep

    2012-01-01

    The pathways of proton abstraction (PA), a key aspect of most catalytic reactions, is often controversial and highly debated. Ultrahigh-resolution diffraction studies, molecular dynamics, quantum mechanics and molecular mechanic simulations are often adopted to gain insights in the PA mechanisms in enzymes. These methods require expertise and effort to setup and can be computationally intensive. We present a push button methodology – Proton abstraction Simulation (PRISM) – to enumerate the possible pathways of PA in a protein with known 3D structure based on the spatial and electrostatic properties of residues in the proximity of a given nucleophilic residue. Proton movements are evaluated in the vicinity of this nucleophilic residue based on distances, potential differences, spatial channels and characteristics of the individual residues (polarity, acidic, basic, etc). Modulating these parameters eliminates their empirical nature and also might reveal pathways that originate from conformational changes. We have validated our method using serine proteases and concurred with the dichotomy in PA in Class A β-lactamases, both of which are hydrolases. The PA mechanism in a transferase has also been corroborated. The source code is made available at www.sanchak.com/prism. PMID:22745790

  14. A functional technique based on the Euclidean algorithm with applications to 2-D acoustic diffractal diffusers

    NASA Astrophysics Data System (ADS)

    Cortés-Vega, Luis

    2015-09-01

    We built, based on the Euclidean algorithm, a functional technique, which allows to discover a direct proof of Chinese Remainder Theorem. Afterwards, by using this functional approach, we present some applications to 2-D acoustic diffractal diffusers. The novelty of the method is their functional algorithmic character, which improves ideas, as well as, other results of the author and his collaborators in a previous work.

  15. Change Of Calibration Of Diffraction-Based Particle Suers In Dense Sprays

    NASA Astrophysics Data System (ADS)

    Dodge, Lee G.

    1984-10-01

    A calibration procedure for diffraction-based particle-sizing instru-ments using multielement detectors is briefly reviewed. The effects of multiple scattering due to dense sprays on the calibration of these instruments are then examined over a range of sprays with Sauter mean diameters from 20 to 55 um. An empirical scheme to correct for changes in calibration due to dense sprays or other scattering media is presented.

  16. Modelling of diffraction grating based optical filters for fluorescence detection of biomolecules.

    PubMed

    Kovačič, M; Krč, J; Lipovšek, B; Topič, M

    2014-07-01

    The detection of biomolecules based on fluorescence measurements is a powerful diagnostic tool for the acquisition of genetic, proteomic and cellular information. One key performance limiting factor remains the integrated optical filter, which is designed to reject strong excitation light while transmitting weak emission (fluorescent) light to the photodetector. Conventional filters have several disadvantages. For instance absorbing filters, like those made from amorphous silicon carbide, exhibit low rejection ratios, especially in the case of small Stokes' shift fluorophores (e.g. green fluorescent protein GFP with λ exc = 480 nm and λ em = 510 nm), whereas interference filters comprising many layers require complex fabrication. This paper describes an alternative solution based on dielectric diffraction gratings. These filters are not only highly efficient but require a smaller number of manufacturing steps. Using FEM-based optical modelling as a design optimization tool, three filtering concepts are explored: (i) a diffraction grating fabricated on the surface of an absorbing filter, (ii) a diffraction grating embedded in a host material with a low refractive index, and (iii) a combination of an embedded grating and an absorbing filter. Both concepts involving an embedded grating show high rejection ratios (over 100,000) for the case of GFP, but also high sensitivity to manufacturing errors and variations in the incident angle of the excitation light. Despite this, simulations show that a 60 times improvement in the rejection ratio relative to a conventional flat absorbing filter can be obtained using an optimized embedded diffraction grating fabricated on top of an absorbing filter. PMID:25071964

  17. Cyclic olefin homopolymer-based microfluidics for protein crystallization and in situ X-ray diffraction

    SciTech Connect

    Emamzadah, Soheila; Petty, Tom J.; De Almeida, Victor; Nishimura, Taisuke; Joly, Jacques; Ferrer, Jean-Luc; Halazonetis, Thanos D.

    2009-09-01

    A cyclic olefin homopolymer-based microfluidics system has been established for protein crystallization and in situ X-ray diffraction. Microfluidics is a promising technology for the rapid identification of protein crystallization conditions. However, most of the existing systems utilize silicone elastomers as the chip material which, despite its many benefits, is highly permeable to water vapour. This limits the time available for protein crystallization to less than a week. Here, the use of a cyclic olefin homopolymer-based microfluidics system for protein crystallization and in situ X-ray diffraction is described. Liquid handling in this system is performed in 2 mm thin transparent cards which contain 500 chambers, each with a volume of 320 nl. Microbatch, vapour-diffusion and free-interface diffusion protocols for protein crystallization were implemented and crystals were obtained of a number of proteins, including chicken lysozyme, bovine trypsin, a human p53 protein containing both the DNA-binding and oligomerization domains bound to DNA and a functionally important domain of Arabidopsis Morpheus’ molecule 1 (MOM1). The latter two polypeptides have not been crystallized previously. For X-ray diffraction analysis, either the cards were opened to allow mounting of the crystals on loops or the crystals were exposed to X-rays in situ. For lysozyme, an entire X-ray diffraction data set at 1.5 Å resolution was collected without removing the crystal from the card. Thus, cyclic olefin homopolymer-based microfluidics systems have the potential to further automate protein crystallization and structural genomics efforts.

  18. Spectrometer for hard X-ray free-electron laser based on diffraction focusing.

    PubMed

    Kohn, V G; Gorobtsov, O Y; Vartanyants, I A

    2013-03-01

    X-ray free-electron lasers (XFELs) generate sequences of ultra-short spatially coherent pulses of X-ray radiation. A diffraction focusing spectrometer (DFS), which is able to measure the whole energy spectrum of the radiation of a single XFEL pulse with an energy resolution of ΔE/E 2 × 10(-6), is proposed. This is much better than for most modern X-ray spectrometers. Such resolution allows one to resolve the fine spectral structure of the XFEL pulse. The effect of diffraction focusing occurs in a single-crystal plate due to dynamical scattering, and is similar to focusing in a Pendry lens made from a metamaterial with a negative refraction index. Such a spectrometer is easier to operate than those based on bent crystals. It is shown that the DFS can be used in a wide energy range from 5 keV to 20 keV. PMID:23412482

  19. A fast multispectral light synthesiser based on LEDs and a diffraction grating

    PubMed Central

    Belušič, Gregor; Ilić, Marko; Meglič, Andrej; Pirih, Primož

    2016-01-01

    Optical experiments often require fast-switching light sources with adjustable bandwidths and intensities. We constructed a wavelength combiner based on a reflective planar diffraction grating and light emitting diodes with emission peaks from 350 to 630 nm that were positioned at the angles corresponding to the first diffraction order of the reversed beam. The combined output beam was launched into a fibre. The spacing between 22 equally wide spectral bands was about 15 nm. The time resolution of the pulse-width modulation drivers was 1 ms. The source was validated with a fast intracellular measurement of the spectral sensitivity of blowfly photoreceptors. In hyperspectral imaging of Xenopus skin circulation, the wavelength resolution was adequate to resolve haemoglobin absorption spectra. The device contains no moving parts, has low stray light and is intrinsically capable of multi-band output. Possible applications include visual physiology, biomedical optics, microscopy and spectroscopy. PMID:27558155

  20. A fast multispectral light synthesiser based on LEDs and a diffraction grating.

    PubMed

    Belušič, Gregor; Ilić, Marko; Meglič, Andrej; Pirih, Primož

    2016-01-01

    Optical experiments often require fast-switching light sources with adjustable bandwidths and intensities. We constructed a wavelength combiner based on a reflective planar diffraction grating and light emitting diodes with emission peaks from 350 to 630 nm that were positioned at the angles corresponding to the first diffraction order of the reversed beam. The combined output beam was launched into a fibre. The spacing between 22 equally wide spectral bands was about 15 nm. The time resolution of the pulse-width modulation drivers was 1 ms. The source was validated with a fast intracellular measurement of the spectral sensitivity of blowfly photoreceptors. In hyperspectral imaging of Xenopus skin circulation, the wavelength resolution was adequate to resolve haemoglobin absorption spectra. The device contains no moving parts, has low stray light and is intrinsically capable of multi-band output. Possible applications include visual physiology, biomedical optics, microscopy and spectroscopy. PMID:27558155

  1. Field emitter based extractor gauges and residual gas analyzers

    SciTech Connect

    Changkun Dong; G. Rao Myneni

    1999-04-01

    Attempts at using the Spindt-type molybdenum field emitter arrays in the extractor gauges and a residual gas analyzer are presented in this article. The sensitivity of the fuel emitter gauge is as high as 11 Torr{sup -1}. The departure from linearity of the pressure versus ion current measurements did not exceed 10% over the pressure range of 10{sup -10} - 10{sup -6} Torr. Stable sensitivities for nitrogen, helium, and hydrogen were achieved below 10{sup -7} Torr with the field emitter residual gas analyzer. The slightly reduced emission current and sensitivity, after long-term operation, are of concern and need to be addressed. Residual gas spectra indicate that when using field emitters, the electron stimulated desorption ions (O{sup +}, F{sup +}, and Cl{sup +}) are reduced as compared to those made using a hot filament source.

  2. Use of synchrotron based diffraction enhanced imaging for visualization of soft tissues in invertebrates

    SciTech Connect

    Rao, D.; Zhong, Z.; Swapna, M.; Cesareo, R.; Brunetti, A.; Akatsuka, T.; Yuasa, T.; Takeda, T.; Gigante, G.

    2010-04-04

    Images of terrestrial and marine invertebrates (snails and bivalves) have been obtained by using an X-ray phase-contrast imaging technique, namely, synchrotron-based diffraction-enhanced imaging. Synchrotron X-rays of 20, 30 and 40 keV were used, which penetrate deep enough into animal soft tissues. The phase of X-ray photons shifts slightly as they traverse an object, such as animal soft tissue, and interact with its atoms. Biological features, such as shell morphology and animal physiology, have been visualized. The contrast of the images obtained at 40 keV is the best. This optimum energy provided a clear view of the internal structural organization of the soft tissue with better contrast. The contrast is higher at edges of internal soft-tissue structures. The image improvements achieved with the diffraction-enhanced imaging technique are due to extinction, i.e., elimination of ultra-small-angle scattering. They enabled us to identify a few embedded internal shell features, such as the origin of the apex, which is the firmly attached region of the soft tissue connecting the umbilicus to the external morphology. Diffraction-enhanced imaging can provide high-quality images of soft tissues valuable for biology.

  3. New long trace profiler based on phase plate diffraction for optical metrology of SSRF

    SciTech Connect

    Zeng Danhua; Xiao Tiqiao; Du Guohao; Wen Li; Luo Hongxin; Xia Shaojian; Xu Hongjie

    2006-09-15

    A long trace profiler LTP-1200, with a novel f-{theta} system based on phase plate diffraction and a scanning range up to 1200 mm, has been developed at Shanghai Synchrotron Radiation Facility. The central dark line in the diffraction pattern generated by a {pi} phase plate is taken as the positioning benchmark. A magnet levitated linear rail with very high accuracy is used. A granite bench is employed to reduce deformation due to self-gravity of the rail. The focused diffraction pattern is recorded with an area charge-coupled device. The generalized regression neural network algorithm is adopted to improve the beam positioning precision. The static stability of LTP-1200 in 5 h is 0.14 {mu}rad, and the repeatability reaches 0.05 {mu}rad in a common laboratory without any special control of temperature, air turbulence, etc. Calibration tests were carried out with a high precision autocollimator and a standard spherical mirror, respectively. Results show the high performance and reliability of the LTP-1200.

  4. A Comparison of Residual Stress Development in Inertia Friction Welded Fine Grain and Coarse Grain Nickel-Base Superalloy

    NASA Astrophysics Data System (ADS)

    Iqbal, N.; Rolph, J.; Moat, R.; Hughes, D.; Hofmann, M.; Kelleher, J.; Baxter, G.; Withers, P. J.; Preuss, M.

    2011-12-01

    The effect of the base material microstructure on the development of residual stresses across the weld line in inertia friction welds (IFWs) of high-strength nickel-base superalloy RR1000 was studied using neutron diffraction. A comparison was carried out between tubular IFW specimens generated from RR1000 heat treated below (fine grain (FG) structure) and above (coarse grain (CG) structure) the γ'-solvus. Residual stresses were mapped in the as-welded (AW) condition and, after a postweld heat treatment (PWHT), optimized for maximum alloy strength. The highest tensile stresses were generally found in the hoop direction at the weld line near the inner diameter of the tubular-shaped specimens. A comparison between the residual stresses generated in FG and CG RR1000 suggests that the starting microstructure has little influence on the maximum residual stresses generated in the weld even though different levels of energy must be input to achieve a successful weld in each case. The residual stresses in the postweld heat treated samples were about 35 pct less than for the AW condition. Despite the fact that the high-temperature properties of the two parent microstructures are different, no significant differences in terms of stress relief were found between the FG and CG RR1000 IFWs. Since the actual weld microstructures of FG and CG RR1000 inertia welds are very similar, the results suggest that it is the weld microstructure and its associated high-temperature properties rather than the parent material that affects the overall weld stress distribution and its subsequent stress relief.

  5. Calibration diagnostic and updating strategy based on quantitative modeling of near-infrared spectral residuals.

    PubMed

    Yu, Hua; Small, Gary W

    2015-02-01

    A diagnostic and updating strategy is explored for multivariate calibrations based on near-infrared spectroscopy. For use with calibration models derived from spectral fitting or decomposition techniques, the proposed method constructs models that relate the residual concentrations remaining after a prediction to the residual spectra remaining after the information associated with the calibration model has been extracted. This residual modeling approach is evaluated for use with partial least-squares (PLS) models for predicting physiological levels of glucose in a simulated biological matrix. Residual models are constructed with both PLS and a hybrid technique based on the use of PLS scores as inputs to support vector regression. Calibration and residual models are built with both absorbance and single-beam data collected over 416 days. Effective models for the spectral residuals are built with both types of data and demonstrate the ability to diagnose and correct deviations in performance of the calibration model with time. PMID:25473807

  6. Diffraction-based overlay measurement on dedicated mark using rigorous modeling method

    NASA Astrophysics Data System (ADS)

    Lu, Hailiang; Wang, Fan; Zhang, Qingyun; Chen, Yonghui; Zhou, Chang

    2012-03-01

    Diffraction Based Overlay (DBO) is widely evaluated by numerous authors, results show DBO can provide better performance than Imaging Based Overlay (IBO). However, DBO has its own problems. As well known, Modeling based DBO (mDBO) faces challenges of low measurement sensitivity and crosstalk between various structure parameters, which may result in poor accuracy and precision. Meanwhile, main obstacle encountered by empirical DBO (eDBO) is that a few pads must be employed to gain sufficient information on overlay-induced diffraction signature variations, which consumes more wafer space and costs more measuring time. Also, eDBO may suffer from mark profile asymmetry caused by processes. In this paper, we propose an alternative DBO technology that employs a dedicated overlay mark and takes a rigorous modeling approach. This technology needs only two or three pads for each direction, which is economic and time saving. While overlay measurement error induced by mark profile asymmetry being reduced, this technology is expected to be as accurate and precise as scatterometry technologies.

  7. A Protein Solvation Model Based on Residue Burial.

    PubMed

    Ceres, Nicoletta; Pasi, Marco; Lavery, Richard

    2012-06-12

    The influence of solvent on the individual amino acids of a protein depends not simply on their surface exposure but rather on the degree of their burial within the structure. This property can be related to a simple geometrical measure termed circular variance. Circular variance depends on the spatial distribution of neighboring residues and varies from zero to one as a residue becomes buried. Its only adjustable parameter is a cutoff distance for selecting neighbors. Here, we show that circular variance can be used to build a fast and effective model of protein solvation energies. For this, we combine a coarse-grain protein representation with statistical potentials derived by Boltzmann inversion of circular variance probability distributions for different classes of pseudoatom within a large protein structure database. The method is shown to work well for distinguishing native protein structures from decoy structures generated in a variety of ways. It can also be used to detect specific residues in unfavorable solvent environments. Compared to surface accessibility, circular variance calculations are faster, less sensitive to small conformational changes, and able to account for the longer-range interactions that characterize the electrostatic component of solvent effects. The resulting solvation energies can be used alone or as part of a more general coarse-grain protein model. PMID:26593844

  8. Nondestructive characterization of residual stress within CMOS-based composite microcantilevers

    NASA Astrophysics Data System (ADS)

    Rendon-Hernandez, Adrian A.; Camacho-Leon, Sergio; Martinez-Chapa, Sergio O.

    2013-04-01

    Residual stress can affect the performance of thin-film micromachined structures and lead to curling in cantilevers as well as distortion in the frequency of resonant devices. As the origin of residual stress is dependent on the fabrication processes, a nondestructive method for characterization of residual stress independent of processes conditions is desirable for supporting the design of microcantilever-based microsystems. In this paper we present a nondestructive characterization of the residual stress within composite microcantilever beams providing valuable insights toward predicting their deflection profile after mechanical releasing from the substrate. The approach relies on the assumption of a linear gradient stress and a quadratic deflection profile across a composite microcantilever.

  9. Performance enhancement of thin film silicon solar cells based on distributed Bragg reflector and diffraction grating

    SciTech Connect

    Dubey, R. S.; Saravanan, S.; Kalainathan, S.

    2014-12-15

    The influence of various designing parameters were investigated and explored for high performance solar cells. Single layer grating based solar cell of 50 μm thickness gives maximum efficiency up to 24 % whereas same efficiency is achieved with the use of three bilayers grating based solar cell of 30 μm thickness. Remarkably, bilayer grating based solar cell design not only gives broadband absorption but also enhancement in efficiency with reduced cell thickness requirement. This absorption enhancement is attributed to the high reflection and diffraction from DBR and grating respectively. The obtained short-circuit current were 29.6, 32.9, 34.6 and 36.05 mA/cm{sup 2} of 5, 10, 20 and 30 μm cell thicknesses respectively. These presented designing efforts would be helpful to design and realize new generation of solar cells.

  10. Microstructure and residual stress of laser rapid formed Inconel 718 nickel-base superalloy

    NASA Astrophysics Data System (ADS)

    Liu, Fencheng; Lin, Xin; Yang, Gaolin; Song, Menghua; Chen, Jing; Huang, Weidong

    2011-02-01

    The microstructure and residual stress of laser rapid formed (LRFed) nickel-base superalloy Inconel 718 was investigated. The as-deposited microstructure of an LRFed Inconel 718 alloy is composed of columnar dendrites growing epitaxially along the deposition direction, and the columnar dendrites transformed to unevenly distributed equiaxed grains after annealing treatment at high temperature. Residual stress evaluation in microstructure scale by Vickers micro-indentation method indicates that the residual thermal stress is unevenly distributed in the LRFed sample, and it has a significant effect on the recrystallization during solution annealing treatment. The residual stress is introduced by rapid heating and cooling during laser rapid forming. There is an alternative distribution between high residual stress regions and low residual stress regions, within a single deposited layer, resulting in a similar distribution of recrystallized grain size.

  11. Optical cryptosystem based on phase-truncated Fresnel diffraction and transport of intensity equation.

    PubMed

    Zhang, Chenggong; He, Wenqi; Wu, Jiachen; Peng, Xiang

    2015-04-01

    A novel optical cryptosystem based on phase-truncated Fresnel diffraction (PTFD) and transport of intensity equation (TIE) is proposed. By using the phase truncation technique, a phase-encoded plaintext could be encrypted into a real-valued noise-like intensity distribution by employing a random amplitude mask (RAM) and a random phase mask (RPM), which are regarded as two secret keys. For decryption, a generalized amplitude-phase retrieval (GAPR) algorithm combined with the TIE method are proposed to recover the plaintext with the help of two keys. Different from the current phase-truncated-based optical cryptosystems which need record the truncated phase as decryption keys, our scheme do not need the truncated phase because of the introducing of the TIE method. Moreover, the proposed scheme is expected to against existing attacks. A set of numerical simulation results show the feasibility and security of the proposed method. PMID:25968722

  12. Radius of curvature measurement based on wavefront difference method by the point diffraction interferometer

    NASA Astrophysics Data System (ADS)

    Yang, Zhongming; Gao, Zhishan; Yuan, Qun; Ye, Jingfei; Li, Minjue

    2014-05-01

    A method for measuring the radius of curvature with a pinhole point diffraction interferometer (PDI) is proposed. Using the wavefront difference method and the Gaussian imaging equation, the longitudinal displacement of the converging rays passing through a standard plane-parallel-plate sample in PDI interference cavity is determined. Based on this longitudinal displacement, a precise formula for radius of curvature calculation is deduced. An experimental system for radius of curvature measurements is set up to verify the principle. With this testing system, the radius of curvature of spherical mirrors and the surface figure can be measured in a higher precision simultaneously. Some sources of uncertainty in measurement are discussed based on detailed error analysis. The experimental results indicate that the measurement accuracy ΔR/R0 is in the order of 10-4.

  13. Novel copyright information hiding method based on random phase matrix of Fresnel diffraction transforms

    NASA Astrophysics Data System (ADS)

    Cao, Chao; Chen, Ru-jun

    2009-10-01

    In this paper, we present a new copyright information hide method for digital images in Moiré fringe formats. The copyright information is embedded into the protected image and the detecting image based on Fresnel phase matrix. Firstly, using Fresnel diffraction transform, the random phase matrix of copyright information is generated. Then, according to Moiré fringe principle, the protected image and the detecting image are modulated respectively based on the random phase matrix, and the copyright information is embedded into them. When the protected image and the detecting image are overlapped, the copyright information can reappear. Experiment results show that our method has good concealment performance, and is a new way for copyright protection.

  14. Mechanical characterization of nanowires based on optical diffraction images of the bent shape.

    PubMed

    Muraoka, Mikio; Tobe, Ryohei

    2009-08-01

    A mechanical characterization technique for nanowires (NWs) longer than approximately 10 microm is proposed, based on optical microscopic observations under bending test. Low flexural rigidity of NWs often results in large deflection, which rules out the use of linear beam theory; however, the largely bent shape is optically visible as a diffraction image under transmitted illumination. The NW standing on a rod-like substrate was deflected by means of a micro-cantilever, where interactive forces, such as van der Waals forces, provide sufficient adhesion for fixing the free end of the NW. The reactive force was measured from the cantilever deflection and detected by a laser interferometer. The luminance profile of the diffraction image provided a good measure of the NW diameter. Inverse analysis using geometrically nonlinear mechanics for the bent shape enabled successful evaluation of the Young's modulus. In addition, a fracture test was conducted by manipulating the cantilever for intense deformation of the NW, such as buckling. The maximum curvature was observed at the freely suspended part of the bent NW where fracture was assured. The bending strength was determined from observation of the curvature at the fracture. Examples for CuO NWs of 40 nm to 190 nm in diameter indicated dependence of the Young's modulus and strength on the NW diameter. PMID:19928119

  15. Automatic decomposition of a complex hologram based on the virtual diffraction plane framework

    NASA Astrophysics Data System (ADS)

    Jiao, A. S. M.; Tsang, P. W. M.; Poon, T.-C.; Liu, J.-P.; Lee, C.-C.; Lam, Y. K.

    2014-07-01

    Holography is a technique for capturing the hologram of a three-dimensional scene. In many applications, it is often pertinent to retain specific items of interest in the hologram, rather than retaining the full information, which may cause distraction in the analytical process that follows. For a real optical image that is captured with a camera or scanner, this process can be realized by applying image segmentation algorithms to decompose an image into its constituent entities. However, because it is different from an optical image, classic image segmentation methods cannot be applied directly to a hologram, as each pixel in the hologram carries holistic, rather than local, information of the object scene. In this paper, we propose a method to perform automatic decomposition of a complex hologram based on a recently proposed technique called the virtual diffraction plane (VDP) framework. Briefly, a complex hologram is back-propagated to a hypothetical plane known as the VDP. Next, the image on the VDP is automatically decomposed, through the use of the segmentation on the magnitude of the VDP image, into multiple sub-VDP images, each representing the diffracted waves of an isolated entity in the scene. Finally, each sub-VDP image is reverted back to a hologram. As such, a complex hologram can be decomposed into a plurality of subholograms, each representing a discrete object in the scene. We have demonstrated the successful performance of our proposed method by decomposing a complex hologram that is captured through the optical scanning holography (OSH) technique.

  16. 100-watt fiber-based green laser with near diffraction-limited beam quality

    NASA Astrophysics Data System (ADS)

    Hu, Dan; Eisenberg, Eric; Brar, Khush; Yilmaz, Tolga; Honea, Eric

    2010-02-01

    An air-cooled, light-weight, fiber-based, high power green laser has been prototyped. The system consists of an all-fibercoupled IR pump laser at 1064 nm and a frequency-conversion module in a compact and flexible configuration. The IR laser operates in QCW mode, with 10 MHz pulse repetition frequency and 3-5 ns pulse width, to generate sufficient peak power for frequency doubling in the converter module. The IR laser can produce more than 200 W in a linearlypolarized diffraction-limited output beam with high spectral brightness for frequency conversion. The converter module has an input telescope and an oven with a nonlinear crystal to efficiently convert the 1064-nm IR fiber laser output to 532-nm green output. The IR laser and conversion module are connected via a stainless-steel protected delivery fiber for optical beam delivery and an electrical cable harness for electrical power delivery and system control. The beam quality of the 532 nm output remains near diffraction-limited, with M2<1.4. Up to 101 W of 532 nm output was demonstrated and multi-hour runs were characterized at 75 W output. The weights of the IR laser package and doubler are 69 lbs and 14 lbs respectively. An overview of the system and full characterization results will be presented. Such compact, highbrightness green laser sources are expected to enable various scientific, defense and industrial applications.

  17. FISH TISSUE RESIDUE-BASED WILDLIFE VALUES FOR PISCIVOUOUS WILDLIFE: CHLORDANE, DDT, DIELDRIN, HEXACHLOROBENZENE

    EPA Science Inventory

    Fish tissue residue-based wildlife values were derived for chlordane, DDT, dieldrin, endrin, hexachlorobenzene, mercury and PCBs. Piscivorous wildlife for which these benchmarks were derived include belted kingfisher, river otter and mink. Toxic endpoint selection, criteria for t...

  18. High efficiency near diffraction-limited mid-infrared flat lenses based on metasurface reflectarrays.

    PubMed

    Zhang, Shuyan; Kim, Myoung-Hwan; Aieta, Francesco; She, Alan; Mansuripur, Tobias; Gabay, Ilan; Khorasaninejad, Mohammadreza; Rousso, David; Wang, Xiaojun; Troccoli, Mariano; Yu, Nanfang; Capasso, Federico

    2016-08-01

    We report the first demonstration of a mid-IR reflection-based flat lens with high efficiency and near diffraction-limited focusing. Focusing efficiency as high as 80%, in good agreement with simulations (83%), has been achieved at 45° incidence angle at λ = 4.6 μm. The off-axis geometry considerably simplifies the optical arrangement compared to the common geometry of normal incidence in reflection mode which requires beam splitters. Simulations show that the effects of incidence angle are small compared to parabolic mirrors with the same NA. The use of single-step photolithography allows large scale fabrication. Such a device is important in the development of compact telescopes, microscopes, and spectroscopic designs. PMID:27505769

  19. A study of swing-curve physics in diffraction-based overlay

    NASA Astrophysics Data System (ADS)

    Bhattacharyya, Kaustuve; den Boef, Arie; Storms, Greet; van Heijst, Joost; Noot, Marc; An, Kevin; Park, Noh-Kyoung; Jeon, Se-Ra; Oh, Nang-Lyeom; McNamara, Elliott; van de Mast, Frank; Oh, SeungHwa; Lee, Seung Yoon; Hwang, Chan; Lee, Kuntack

    2016-03-01

    With the increase of process complexity in advanced nodes, the requirements of process robustness in overlay metrology continues to tighten. Especially with the introduction of newer materials in the film-stack along with typical stack variations (thickness, optical properties, profile asymmetry etc.), the signal formation physics in diffraction-based overlay (DBO) becomes an important aspect to apply in overlay metrology target and recipe selection. In order to address the signal formation physics, an effort is made towards studying the swing-curve phenomena through wavelength and polarizations on production stacks using simulations as well as experimental technique using DBO. The results provide a wealth of information on target and recipe selection for robustness. Details from simulation and measurements will be reported in this technical publication.

  20. Digital focusing of OCT images based on scalar diffraction theory and information entropy

    PubMed Central

    Liu, Guozhong; Zhi, Zhongwei; Wang, Ruikang K.

    2012-01-01

    This paper describes a digital method that is capable of automatically focusing optical coherence tomography (OCT) en face images without prior knowledge of the point spread function of the imaging system. The method utilizes a scalar diffraction model to simulate wave propagation from out-of-focus scatter to the focal plane, from which the propagation distance between the out-of-focus plane and the focal plane is determined automatically via an image-definition-evaluation criterion based on information entropy theory. By use of the proposed approach, we demonstrate that the lateral resolution close to that at the focal plane can be recovered from the imaging planes outside the depth of field region with minimal loss of resolution. Fresh onion tissues and mouse fat tissues are used in the experiments to show the performance of the proposed method. PMID:23162717

  1. High efficiency near diffraction-limited mid-infrared flat lenses based on metasurface reflectarrays

    NASA Astrophysics Data System (ADS)

    Zhang, Shuyan; Kim, Myoung-Hwan; Aieta, Francesco; She, Alan; Mansuripur, Tobias; Gabay, Ilan; Khorasaninejad, Mohammadreza; Rousso, David; Wang, Xiaojun; Troccoli, Mariano; Yu, Nanfang; Capasso, Federico

    2016-08-01

    A limiting factor in the development of mid-infrared optics is the lack of abundant materials that are transparent, low cost, lightweight, and easy to machine. In this paper, we demonstrate a metasurface device that circumvents these limitations. A flat lens based on antenna reflectarrays was designed to achieve near diffraction-limited focusing with a high efficiency (experiment: 80%, simulation: 83%) at 45(o) incidence angle at {\\lambda} = 4.6 {\\mu}m. This geometry considerably simplifies the experimental arrangement compared to the common geometry of normal incidence which requires beam splitters. Simulations show that the effect of comatic aberrations is small compared to parabolic mirrors. The use of single-step photolithography allows large scale fabrication.

  2. High-speed miniaturized swept sources based on resonant MEMS mirrors and diffraction gratings

    NASA Astrophysics Data System (ADS)

    Gloor, S.; Bachmann, A. H.; Epitaux, M.; von Niederhäusern, T.; Vorreau, P.; Matuschek, N.; Hsu, K.; Duelk, M.; Vélez, C.

    2013-03-01

    We show a broad range of swept source performances based on a highly-flexible external cavity laser architecture. Specifically, we demonstrate a 40-kHz 1300-nm swept source with 10 mm coherence length realized in a compact butterfly package. Fast wavelength sweeping is achieved through a 1D 20-kHz MEMS mirror in combination with an advanced diffraction grating. The MEMS mirror is a resonant electrostatic mirror that performs harmonic oscillation only within a narrow frequency range, resulting in low-jitter and long-term phase-stable sinusoidal bidirectional sweep operation with an A-scan rate of 40 kHz. The source achieves a coherence length of 10 mm for both the up- and downsweep and an OCT sensitivity of 105 dB.

  3. Measurement of four-degree-of-freedom error motions based on non-diffracting beam

    NASA Astrophysics Data System (ADS)

    Zhai, Zhongsheng; Lv, Qinghua; Wang, Xuanze; Shang, Yiyuan; Yang, Liangen; Kuang, Zheng; Bennett, Peter

    2016-05-01

    A measuring method for the determination of error motions of linear stages based on non-diffracting beams (NDB) is presented. A right-angle prism and a beam splitter are adopted as the measuring head, which is fixed on the moving stage in order to sense the straightness and angular errors. Two CCDs are used to capture the NDB patterns that are carrying the errors. Four different types error s, the vertical straightness error and three rotational errors (the pitch, roll and yaw errors), can be separated and distinguished through theoretical analysis of the shift in the centre positions in the two cameras. Simulation results show that the proposed method using NDB can measure four-degrees-of-freedom errors for the linear stage.

  4. Quantification of Pharmaceutical Compounds Based on Powder X-Ray Diffraction with Chemometrics.

    PubMed

    Otsuka, Yuta; Ito, Akira; Matsumura, Saki; Takeuchi, Masaki; Pal, Suvra; Tanaka, Hideji

    2016-01-01

    We propose an approach for the simultaneous determination of multiple components in pharmaceutical mixed powder based on powder X-ray diffraction (PXRD) method coupled with chemometrics. Caffeine anhydrate, acetaminophen and lactose monohydrate were mixed at various ratios. The samples were analyzed by PXRD method in the ranges of 2θ=5.00-30.0 and 35.0-45.0 degrees. Obtained diffractograms were analyzed by conventional peak intensity method, multi curve resolution (MCR)-alternating least squares (ALS) method and partial least squares (PLS) method. Constructed PLS models can most accurately predict the concentrations among different methods used. Each regression vector of PLS correlates not only to the compound of interest but also to the coexisting compounds. The combination of PXRD and PLS methods is concluded to be powerful approach for analyzing multi components in pharmaceutical formulations. PMID:27477651

  5. A projection-based approach to diffraction tomography on curved boundaries

    PubMed Central

    Clement, Gregory T.

    2014-01-01

    An approach to diffraction tomography is investigated for two-dimensional image reconstruction of objects surrounded by an arbitrarily-shaped curve of sources and receivers. Based on the integral theorem of Helmholtz and Kirchhoff, the approach relies upon a valid choice of the Green’s functions for selected conditions along the (possibly-irregular) boundary. This allows field projections from the receivers to an arbitrary external location. When performed over all source locations, it will be shown that the field caused by a hypothetical source at this external location is also known along the boundary. This field can then be projected to new external points that may serve as a virtual receiver. Under such a reformation, data may be put in a form suitable for image construction by synthetic aperture methods. Foundations of the approach are shown, followed by a mapping technique optimized for the approach. Examples formed from synthetic data are provided. PMID:25598570

  6. Two-degree-of-freedom displacement measurement system based on double diffraction gratings

    NASA Astrophysics Data System (ADS)

    Lu, Zhengang; Wei, Peipei; Wang, Chaoqun; Jing, Jialei; Tan, Jiubin; Zhao, Xiping

    2016-07-01

    A two-degree-of-freedom (2-DOF) displacement measurement system based on double diffraction gratings is proposed in this paper, which consists of a reflective-type scale grating and a grating read head with a scanning transmission grating. Combining the traditional three-grating interference principle with the Michelson interference principle, the system can measure the displacements of a precision stage along the horizontal direction (X-axis, in the scanning grating plane and vertical to the scanning grating lines) and vertical direction (Z-axis, vertical to the scanning grating plane) simultaneously. The system has the merits of compact structure and uncoupled interference signals in the two axes. By simulating the output signals of the system and comparing them with the experimental results, the validity and feasibility of the system have been verified. The 2-DOF system will be favorable in the displacement measurement of multi-dimensional stages and multi-DOF machines.

  7. Melting of iron at Earth's inner core boundary based on fast X-ray diffraction.

    PubMed

    Anzellini, S; Dewaele, A; Mezouar, M; Loubeyre, P; Morard, G

    2013-04-26

    Earth's core is structured in a solid inner core, mainly composed of iron, and a liquid outer core. The temperature at the inner core boundary is expected to be close to the melting point of iron at 330 gigapascal (GPa). Despite intensive experimental and theoretical efforts, there is little consensus on the melting behavior of iron at these extreme pressures and temperatures. We present static laser-heated diamond anvil cell experiments up to 200 GPa using synchrotron-based fast x-ray diffraction as a primary melting diagnostic. When extrapolating to higher pressures, we conclude that the melting temperature of iron at the inner core boundary is 6230 ± 500 kelvin. This estimation favors a high heat flux at the core-mantle boundary with a possible partial melting of the mantle. PMID:23620049

  8. Temporal contrast improvement based on the self-diffraction process with a cylinder mirror

    NASA Astrophysics Data System (ADS)

    Li, Fangjia; Shen, Xiong; Wang, Peng; Li, Yanyan; Liu, Jun; Wang, Zhanshan; Li, Ruxin

    2016-05-01

    A cylinder reflective mirror was used to increase incident pulse energy to multi-millijoules in the research of temporal contrast enhancement based on a self-diffraction (SD) process. A 170 μJ first-order SD pulse with temporal contrast improved by 4 orders of magnitude was obtained when incident pulse energy was 5.1 mJ. In order to improve energy-conversion efficiency, a 67/33 beam splitter was used to replace the original 50/50 one. A 265 μJ first-order SD signal was achieved without damage of the glass plate at 3.7 mJ input pulse energy with an energy-conversion efficiency of about 7.1%. The generated SD pulse is expected to be used as the seed of high-contrast and high-power laser systems.

  9. Harmonic Components Based Post-Filter Design for Residual Echo Suppression

    NASA Astrophysics Data System (ADS)

    Lee, Minwoo; Lee, Yoonjae; Kim, Kihyeon; Ko, Hanseok

    In this Letter, a residual acoustic echo suppression method is proposed to enhance the speech quality of hands-free communication in an automobile environment. The echo signal is normally a human voice with harmonic characteristics in a hands-free communication environment. The proposed algorithm estimates the residual echo signal by emphasizing its harmonic components. The estimated residual echo is used to obtain the signal-to-interference ratio (SIR) information at the acoustic echo canceller output. Then, the SIR based Wiener post-filter is constructed to reduce both the residual echo and noise. The experimental results confirm that the proposed algorithm is superior to the conventional residual echo suppression algorithm in terms of the echo return loss enhancement (ERLE) and the segmental signal-to-noise ratio (SEGSNR).

  10. Diffraction-Based Techniques For High Contrast X-ray Imaging

    NASA Astrophysics Data System (ADS)

    Peerzada, Lubna Naseem

    Two X-ray diffraction based techniques for high contrast were explored to improve contrast in radiology: diffraction enhanced imaging (DEI) and coherent scatter imaging. DEI produces contrast in images based upon the difference in the X-ray refractive indices of materials or tissues. Two DEI systems were devised. Both were comprised of a conventional polychromatic copper X-ray source, polycapillary collimating optics and two silicon crystals.Lucite step phantoms and nylon tubing were imaged. No fringe effects were observed. The lack of observable edge enhancement may have been due to the optic structure which obscured refraction effects. Better results might have been achieved if a higher resolution detector or phantom of larger step size or larger diameter thin walled tubing had been used. The second technique was coherent scatter X-ray imaging. The purpose of this work was to differentiate between healthy and diseased human breast tissues. For instance, breast carcinoma is known to have a peak coherent scattering angle at 12.2° for Mo Ka radiation at 17.5 keV, whereas fatty tissue peaks around 9°. A system which would be compatible with screening mammography was developed. The system was expanded to include sample scanning to allow for a larger image area. The modulation transfer function was computed for static and scanned images of a resolution phantom. These showed good agreement, indicating that the scanning was properly aligned and timed. Static and scanned images of phantoms were taken and the contrast was calculated for a series of experimental parameters including, grid tilt angle. A complex phantom was also then imaged. It was possible to distinguish tissue-equivalent phantom types. Good contrast resolution scanned images were obtained which is promising for a diagnostic system.

  11. Performance improvements of MOEMS-based diffractive arrays: address isolation and optical switching

    NASA Astrophysics Data System (ADS)

    Panaman, Ganesh; Madison, Seth; Sano, Michael; Castracane, James

    2005-01-01

    Micro-Opto-Electro-Mechanical Systems (MOEMS) have found a variety of applications in fields such as telecommunications, spectroscopy and display technology. MOEMS-based optical switching is currently under investigation for the increased flexibility that such devices provide for reconfiguration of the I/O network for inter-chip communication applications. This potential not only adds an additional degree of freedom for adjustment of transmitter/receiver links but also allows for fine alignment of individual channels in the network link. Further, this use of diffractive arrays for specific applications combines beam steering/adjustment capabilities with the inherent wavelength dependence of the diffractive approach for channel separation and de-multiplexing. Research and development has been concentrated on the progression from single MOEMS components to parallel arrays integrated with optical source arrays for a successful feasibility demonstration. Successful development of such an approach will have a major impact of the next generation communication protocols. This paper will focus on the current status of the MOEMS research program for Free Space Optical inter-chip communication at the College of NanoScale Science and Engineering, University at Albany-SUNY (CNSE). New versions of diffractive arrays stemming from the basic MEMS Compound Grating (MCG; patent #5,999,319) have been produced through various fabrication methods including the MUMPs process1. Most MEMS components relying on electrostatic actuation tend to require high actuation voltages (>20V) compared to the typical 5V levels prevalent in conventional integrated circuits. The specific goal is to yield improved performance while minimizing the power consumption of the components. Structural modifications through the variation in the ruling/electrode spacing distance and array wiring layout through individually addressable gratings have been studied to understand effects on the actuation voltage and

  12. A diffraction based study of the deformation mechanisms in anomalously ductile B2 intermetallics

    NASA Astrophysics Data System (ADS)

    Mulay, Rupalee Prashant

    For many decades, the brittle nature of most intermetallic compounds (e.g. NiAl) has been the limiting factor in their practical application. Many B2 (CsCl prototypical structure) intermetallics are known to exhibit slip on the <001>{110} slip mode, which provides only 3 independent slip systems and, hence, is unable to satisfy the von Mises (a.k.a. Taylor) criterion for polycrystalline ductility. As a result, inherent polycrystalline ductility is unexpected. Recent discovery of a number of ductile B2 intermetallics has raised questions about possible violation of the von Mises criterion by these alloys. These ductile intermetallic compounds are MR (metal (M) combined with a rare earth metal or group IV refractory metal (R)) alloys and are stoichiometric, ordered compounds. Single crystal slip trace analyses have only identified the presence of <100>{011} or <100>{010} slip systems. More than 100 other B2 MR compounds are known to exist and many of them have already been shown to be ductile (e.g., CuY, AgY, CuDy, CoZr, CoTi, etc.). Furthermore, these alloys exhibit a large Bauschinger effect. The present work uses several diffraction based techniques including electron back scattered diffraction (EBSD), X-ray diffraction (XRD) and in-situ neutron diffraction; in conjunction with scanning electron microscopy (SEM), transmission electron microscopy (TEM), mechanical testing, and crystal plasticity modeling, to elucidate the reason for ductility in select B2 alloys, explore the spread of this ductility over the B2 family, and understand the Bauschinger effect in these alloys. Several possible explanations (e.g., slip of <111> dislocations, strong texture, phase transformations and twinning) for the anomalous ductility were explored. An X-ray diffraction based analysis ruled out texture, phase purity and departure from order as explanations for the anomalous ductility in MR alloys. In-situ neutron diffraction and post deformation SEM, EBSD, and TEM were unable to

  13. Focal construct geometry for high intensity energy dispersive x-ray diffraction based on x-ray capillary optics.

    PubMed

    Li, Fangzuo; Liu, Zhiguo; Sun, Tianxi; Jiang, Bowen; Zhu, Yu

    2016-03-14

    We presented a focal construct geometry (FCG) method for high intensity energy dispersive X-ray diffraction by utilizing a home-made ellipsoidal single-bounce capillary (ESBC) and a polycapillary parallel X-ray lens (PPXRL). The ESBC was employed to focus the X-rays from a conventional laboratory source into a small focal spot and to produce an annular X-ray beam in the far-field. Additionally, diffracted polychromatic X-rays were confocally collected by the PPXRL attached to a stationary energy-resolved detector. Our FCG method based on ESBC and PPXRL had achieved relatively high intensity diffraction peaks and effectively narrowed the diffraction peak width which was helpful in improving the potential d-spacing resolution for material phase analysis. PMID:26979685

  14. Focal construct geometry for high intensity energy dispersive x-ray diffraction based on x-ray capillary optics

    NASA Astrophysics Data System (ADS)

    Li, Fangzuo; Liu, Zhiguo; Sun, Tianxi; Jiang, Bowen; Zhu, Yu

    2016-03-01

    We presented a focal construct geometry (FCG) method for high intensity energy dispersive X-ray diffraction by utilizing a home-made ellipsoidal single-bounce capillary (ESBC) and a polycapillary parallel X-ray lens (PPXRL). The ESBC was employed to focus the X-rays from a conventional laboratory source into a small focal spot and to produce an annular X-ray beam in the far-field. Additionally, diffracted polychromatic X-rays were confocally collected by the PPXRL attached to a stationary energy-resolved detector. Our FCG method based on ESBC and PPXRL had achieved relatively high intensity diffraction peaks and effectively narrowed the diffraction peak width which was helpful in improving the potential d-spacing resolution for material phase analysis.

  15. [Relationship among coagulation effect of Al-based coagulant, content and speciation of residual aluminum].

    PubMed

    Yang, Zhong-Lian; Gao, Bao-Yu; Yue, Qin-Yan; Jiang, Yi-Shuai

    2010-06-01

    The application of AlCl3, Al2 (SO4)3 and poly-aluminum chloride (PAC) in humic acid-kaolin simulated water was studied in this article. It is intended to discuss the relationship among coagulation effect of Al-based coagulants in humic acid-kaolin simulated water and content and speciation of residual aluminum. It was found that, the turbidity removal efficiency and UV254 removal efficiency could reach about 90% at the tested dosage. At higher dosage, PAC gave better coagulation effect. The residual total aluminum content and residual aluminum ratio of PAC, which was 0.9 mg/L and - 3.0% or so respectively, were greatly lower than those of AlCl3 and Al2 (SO4)3. The residual total dissolved aluminum was the predominant content in the effluent after coagulation and sedimentation by the three Al-based coagulants. For the total dissolved aluminum, the proportion of dissolved organic aluminum was significantly higher than that of other aluminum speciation. With respect to humic acid-kaolin simulated water, the content of residual total aluminum in the effluent after coagulation and sedimentation by PAC decreased obviously compared to AlCl3 and Al2 (SO4)3. PAC could effectively decrease the content of residual dissolved aluminum speciation which has higher toxicity. The content of residual total dissolved aluminum in the effluent after coagulation and sedimentation by PAC was about 0.6 mg/L. PMID:20698270

  16. Model-based calibration of an interferometric setup with a diffractive zoom-lens

    NASA Astrophysics Data System (ADS)

    Bielke, Alexander; Baer, Goran; Pruss, Christof; Osten, Wolfgang

    2015-08-01

    The fabrication of aspheres and freeform surfaces requires a high-precision shape measurement of these elements. In terms of accuracy, interferometric systems provide the best performance for specular surfaces. To test aspherical lenses, it is necessary to adapt or partially adapt the test wavefront to the surface under test. Recently, we have proposed an interferometric setup with a diffractive zoom-lens that includes two computer generated holograms for this purpose.1 Their surface phases are a combination of a cubic function for the adaption of aberrations and correction terms necessary to compensate substrate-induced errors. With this system based on Alvarez design a variable defocus and astigmatism controlled by a lateral shift of the second element is achieved. One of the main challenges is the calibration of the system. We use a black-box model2 recently introduced for a non-null test interferometer, the so called tilted wave interferometer3 (TWI). With it, the calibration data are calculated by solving an inverse problem. The system is divided in the two parts of illumination and imaging optics. By the solution of an inverse problem, we get a set of data, which describes separately the wavefronts of the illumination and imaging optics. The main difference to the TWI is the flexible diffractive element, which can be used in continuous positions. To combine the calibration data of a couple of positions with the exact placement, we designed alignment structures on the hologram. We will show the general functionality of this calibration and first simulation results.

  17. Sparsity-based super-resolved coherent diffraction imaging of one-dimensional objects

    PubMed Central

    Sidorenko, Pavel; Kfir, Ofer; Shechtman, Yoav; Fleischer, Avner; Eldar, Yonina C.; Segev, Mordechai; Cohen, Oren

    2015-01-01

    Phase-retrieval problems of one-dimensional (1D) signals are known to suffer from ambiguity that hampers their recovery from measurements of their Fourier magnitude, even when their support (a region that confines the signal) is known. Here we demonstrate sparsity-based coherent diffraction imaging of 1D objects using extreme-ultraviolet radiation produced from high harmonic generation. Using sparsity as prior information removes the ambiguity in many cases and enhances the resolution beyond the physical limit of the microscope. Our approach may be used in a variety of problems, such as diagnostics of defects in microelectronic chips. Importantly, this is the first demonstration of sparsity-based 1D phase retrieval from actual experiments, hence it paves the way for greatly improving the performance of Fourier-based measurement systems where 1D signals are inherent, such as diagnostics of ultrashort laser pulses, deciphering the complex time-dependent response functions (for example, time-dependent permittivity and permeability) from spectral measurements and vice versa. PMID:26345495

  18. Relation between the Rayleigh equation in diffraction theory and the equation based on Green's formula

    NASA Astrophysics Data System (ADS)

    Tatarskii, V. I.

    1995-06-01

    The steps necessary to produce the Rayleigh equation that is based on the Rayleigh hypothesis from the equation that is based on the Green's formula are shown. First a definition is given for the scattering amplitude that is true not only in the far zone of diffraction but also near the scattering surface. With this definition the Rayleigh equation coincides with the rigorous equation for the surface secondary sources that is based on Green's formula. The Rayleigh hypothesis is equivalent to substituting the far-zone expression of the scattering amplitude into this rigorous equation. In this case it turns out to be the equation not for the sources but directly for the scattering amplitude, which is the main advantage of this method. For comparing the Rayleigh equation with the initial rigorous equation, the Rayleigh equation is represented in terms of secondary sources. The kernel of this equation contains an integral that converges for positive and diverges for negative values of some parameter. It is shown that if we regularize this integral, defining it for the negative values of this parameter as an analytical continuation from the domain of positive values, this kernel becomes equal to the kernel of the initial rigorous equation. It follows that the formal perturbation series for the scattering amplitude obtained from the Rayleigh equation and from Green's equation always coincide. This means that convergence of the perturbation series is a sufficient condition

  19. Sparsity-based super-resolved coherent diffraction imaging of one-dimensional objects

    NASA Astrophysics Data System (ADS)

    Sidorenko, Pavel; Kfir, Ofer; Shechtman, Yoav; Fleischer, Avner; Eldar, Yonina C.; Segev, Mordechai; Cohen, Oren

    2015-09-01

    Phase-retrieval problems of one-dimensional (1D) signals are known to suffer from ambiguity that hampers their recovery from measurements of their Fourier magnitude, even when their support (a region that confines the signal) is known. Here we demonstrate sparsity-based coherent diffraction imaging of 1D objects using extreme-ultraviolet radiation produced from high harmonic generation. Using sparsity as prior information removes the ambiguity in many cases and enhances the resolution beyond the physical limit of the microscope. Our approach may be used in a variety of problems, such as diagnostics of defects in microelectronic chips. Importantly, this is the first demonstration of sparsity-based 1D phase retrieval from actual experiments, hence it paves the way for greatly improving the performance of Fourier-based measurement systems where 1D signals are inherent, such as diagnostics of ultrashort laser pulses, deciphering the complex time-dependent response functions (for example, time-dependent permittivity and permeability) from spectral measurements and vice versa.

  20. A phase retrieval algorithm based on three-dimensionally translated diffraction patterns

    NASA Astrophysics Data System (ADS)

    Loetgering, L.; Hammoud, R.; Juschkin, L.; Wilhein, T.

    2015-09-01

    An iterative phase retrieval method is proposed that combines alternating projections and registration of three-dimensionally translated near-field diffraction patterns. This method allows to enhance resolution limited by a finite detector size and automatically stitches the assembled data while avoiding the need for a priori knowledge or scanning of the object as encountered in coherent diffraction imaging or ptychography.

  1. Pharyngeal Residue Severity Rating Scales Based on Fiberoptic Endoscopic Evaluation of Swallowing: A Systematic Review.

    PubMed

    Neubauer, Paul D; Hersey, Denise P; Leder, Steven B

    2016-06-01

    Identification of pharyngeal residue severity located in the valleculae and pyriform sinuses has always been a primary goal during fiberoptic endoscopic evaluation of swallowing (FEES). Pharyngeal residue is a clinical sign of potential prandial aspiration making an accurate description of its severity an important but difficult challenge. A reliable, validated, and generalizable pharyngeal residue severity rating scale for FEES would be beneficial. A systematic review of the published English language literature since 1995 was conducted to determine the quality of existing pharyngeal residue severity rating scales based on FEES. Databases were searched using controlled vocabulary words and synonymous free text words for topics of interest (deglutition disorders, pharyngeal residue, endoscopy, videofluoroscopy, fiberoptic technology, aspiration, etc.) and outcomes of interest (scores, scales, grades, tests, FEES, etc.). Search strategies were adjusted for syntax appropriate for each database/platform. Data sources included MEDLINE (OvidSP 1946-April Week 3 2015), Embase (OvidSP 1974-2015 April 20), Scopus (Elsevier), and the unindexed material in PubMed (NLM/NIH) were searched for relevant articles. Supplementary efforts to identify studies included checking reference lists of articles retrieved. Scales were compared using qualitative properties (sample size, severity definitions, number of raters, and raters' experience and training) and psychometric analyses (randomization, intra- and inter-rater reliability, and construct validity). Seven articles describing pharyngeal residue severity rating scales met inclusion criteria. Six of seven scales had insufficient data to support their use as evidenced by methodological weaknesses with both qualitative properties and psychometric analyses. There is a need for qualitative and psychometrically reliable, validated, and generalizable pharyngeal residue severity rating scales that are anatomically specific, image-based

  2. Residual stress and crack initiation in laser clad composite layer with Co-based alloy and WC + NiCr

    NASA Astrophysics Data System (ADS)

    Lee, Changmin; Park, Hyungkwon; Yoo, Jaehong; Lee, Changhee; Woo, WanChuck; Park, Sunhong

    2015-08-01

    Although laser cladding process has been widely used to improve the wear and corrosion resistance, there are unwanted cracking issues during and/or after laser cladding. This study investigates the tendency of Co-based WC + NiCr composite layers to cracking during the laser cladding process. Residual stress distributions of the specimen are measured using neutron diffraction and elucidate the correlation between the residual stress and the cracking in three types of cylindrical specimens; (i) no cladding substrate only, (ii) cladding with 100% stellite#6, and (iii) cladding with 55% stellite#6 and 45% technolase40s. The microstructure of the clad layer was composed of Co-based dendrite and brittle eutectic phases at the dendritic boundaries. And WC particles were distributed on the matrix forming intermediate composition region by partial melting of the surface of particles. The overlaid specimen exhibited tensile residual stress, which was accumulated through the beads due to contraction of the coating layer generated by rapid solidification, while the non-clad specimen showed compressive. Also, the specimen overlaid with 55 wt% stellite#6 and 45 wt% technolase40s showed a tensile stress higher than the specimen overlaid with 100% stellite#6 possibly, due to the difference between thermal expansion coefficients of the matrix and WC particles. Such tensile stresses can be potential driving force to provide an easy crack path ways for large brittle fractures combined with the crack initiation sites such as the fractured WC particles, pores and solidification cracks. WC particles directly caused clad cracks by particle fracture under the tensile stress. The pores and solidification cracks also affected as initiation sites and provided an easy crack path ways for large brittle fractures.

  3. Limited-angle hybrid optical diffraction tomography system with total-variation-minimization-based reconstruction

    NASA Astrophysics Data System (ADS)

    Krauze, Wojciech; Kuś, Arkadiusz; Kujawinska, Malgorzata

    2015-05-01

    The case of diffraction tomography with limited angle of projections is discussed from the algorithmic and experimental points of view. To reconstruct a three-dimensional distribution of refractive index of a micro-object under study, we use a hybrid approach based on the simultaneous algebraic reconstruction technique (SART) enhanced by a compressed sensing reconstruction technique. It enables us to apply the standard computed tomography algorithms (which assume that the rays are traveling in straight lines through the object) for phase data obtained by means of digital holography. We present the results of analysis of a phantom and real objects obtained by applying SART with anisotropic total variation (ATV) minimization. The real data are acquired from an experimental setup based on a Mach-Zehnder interferometer configuration. Also, it is proven that in the case of simulated data, the limited number of projections captured in a limited angular range can be compensated by a higher number of iterations of the algorithm. We also show that the SART + ATV method applied for experimental data gives better results than the data replenishment algorithm.

  4. Tunable Diffractive Optical Elements Based on Shape-Memory Polymers Fabricated via Hot Embossing.

    PubMed

    Schauer, Senta; Meier, Tobias; Reinhard, Maximilian; Röhrig, Michael; Schneider, Marc; Heilig, Markus; Kolew, Alexander; Worgull, Matthias; Hölscher, Hendrik

    2016-04-13

    We introduce actively tunable diffractive optical elements fabricated from shape-memory polymers (SMPs). By utilizing the shape-memory effect of the polymer, at least one crucial attribute of the diffractive optical element (DOE) is tunable and adjustable subsequent to the completed fabrication process. A thermoplastic, transparent, thermoresponsive polyurethane SMP was structured with diverse diffractive microstructures via hot embossing. The tunability was enabled by programming a second, temporary shape into the diffractive optical element by mechanical deformation, either by stretching or a second embossing cycle at low temperatures. Upon exposure to the stimulus heat, the structures change continuously and controllable in a predefined way. We establish the novel concept of shape-memory diffractive optical elements by illustrating their capabilities, with regard to tunability, by displaying the morphing diffractive pattern of a height tunable and a period tunable structure, respectively. A sample where an arbitrary structure is transformed to a second, disparate one is illustrated as well. To prove the applicability of our tunable shape-memory diffractive optical elements, we verified their long-term stability and demonstrated the precise adjustability with a detailed analysis of the recovery dynamics, in terms of temperature dependence and spatially resolved, time-dependent recovery. PMID:26998646

  5. Holographic diffraction gratings with enhanced sensitivity based on epoxy-resin photopolymers.

    PubMed

    Jeong, Yong-Cheol; Lee, Seungwoo; Park, Jung-Ki

    2007-02-19

    Photopolymers are interesting materials to obtain high-quality performance for the volume holographic data storage with a low noise and high diffraction efficiency. In this paper, the recording of holographic diffraction gratings with a spatial frequency of 1285lines/mm in photopolymerizable epoxy resin materials is experimentally demonstrated. Diffraction efficiency near 92% and an energetic sensitivity of 11.7 x 10-3cm2/J are achieved by designing the proper structure of matrix and also optimizing photopolymer compositions. The effect of photopolymer compositions on the fundamental optical properties is also discussed. PMID:19532382

  6. Paraxial-domain diffractive elements with 100% efficiency based on polarization gratings.

    PubMed

    Tervo, J; Turunen, J

    2000-06-01

    The concept of polarization freedom is employed to design diffraction gratings that are capable of transforming an electromagnetic plane wave into two or three diffraction orders with an arbitrary efficiency distribution among them, such that the combined efficiency of the signal orders is always equal to 100%. As a special case we consider paraxial-domain duplicators and triplicators with 100% efficiency, which is not possible for illumination by scalar waves: Diffractive elements that are capable of performing the required wave transformation must modulate the state of polarization of the incident field. PMID:18064183

  7. In-line metrology setup for periodic nanostructures based on sub-wavelength diffraction

    NASA Astrophysics Data System (ADS)

    Kreuzer, Martin; Gomis Bresco, Jordi; Sledzinska, Marianna; Sotomayor Torres, Clivia M.

    2015-09-01

    The analysis of diffracted light from periodic structures is shown to be a versatile metrology technique applicable to inline metrology for periodic nanostructures. We show that 10 nm changes in periodic structures can be traced optically by means of sub-wavelength diffraction. Polymer gratings were fabricated by electron beam lithography. The gratings have a common periodicity of 6 μm, but different line width, ranging from 370 to 550 nm in 10 nm steps. A comparison between the resulting diffraction patterns shows marked differences in intensity which are used to sense nanometre scale deviations in periodic structures.

  8. Production of apple-based baby food: changes in pesticide residues.

    PubMed

    Kovacova, Jana; Kocourek, Vladimir; Kohoutkova, Jana; Lansky, Miroslav; Hajslova, Jana

    2014-01-01

    Apples represent the main component of most fruit-based baby food products. Since not only fruit from organic farming, but also conventionally grown fruit is used for baby food production, the occurrence of pesticide residues in the final product is of high concern. To learn more about the fate of these hazardous compounds during processing of contaminated raw material, apples containing altogether 21 pesticide residues were used for preparation of a baby food purée both in the household and at industrial scale (in the baby food production facility). Within both studies, pesticide residues were determined in raw apples as well as in final products. Intermediate product and by-product were also analysed during the industrial process. Determination of residues was performed by a sensitive multi-detection analytical method based on liquid or gas chromatography coupled with mass spectrometry. The household procedure involved mainly the cooking of unpeeled apples, and the decrease of residues was not extensive enough for most of the studied pesticides; only residues of captan, dithianon and thiram dropped significantly (processing factors less than 0.04). On the other hand, changes in pesticide levels were substantial for all tested pesticides during apple processing in the industrial baby food production facility. The most important operation affecting the reduction of residues was removal of the by-products after pulping (rest of the peel, stem, pips etc.), while subsequent sterilisation has an insignificant effect. Also in this case, captan, dithianon and thiram were identified as pesticides with the most evident decrease of residues. PMID:24720736

  9. Diffraction-based optical sensor detection system for capture-restricted environments

    NASA Astrophysics Data System (ADS)

    Khandekar, Rahul M.; Nikulin, Vladimir V.

    2008-04-01

    The use of digital cameras and camcorders in prohibited areas presents a growing problem. Piracy in the movie theaters results in huge revenue loss to the motion picture industry every year, but still image and video capture may present even a bigger threat if performed in high-security locations. While several attempts are being made to address this issue, an effective solution is yet to be found. We propose to approach this problem using a very commonly observed optical phenomenon. Cameras and camcorders use CCD and CMOS sensors, which include a number of photosensitive elements/pixels arranged in a certain fashion. Those are photosites in CCD sensors and semiconductor elements in CMOS sensors. They are known to reflect a small fraction of incident light, but could also act as a diffraction grating, resulting in the optical response that could be utilized to identify the presence of such a sensor. A laser-based detection system is proposed that accounts for the elements in the optical train of the camera, as well as the eye-safety of the people who could be exposed to optical beam radiation. This paper presents preliminary experimental data, as well as the proof-of-concept simulation results.

  10. Reflective off-axis point-diffraction interferometer based on Michelson architecture

    NASA Astrophysics Data System (ADS)

    Bai, Hongyi; Guo, Lili; Zhong, Zhi; Shan, Mingguang; Zhang, Yabin

    2015-02-01

    A reflective off-axis point-diffraction interferometer based on Michelson architecture is built to measure static and dynamic quantitative phase in a single shot. The interferometer is constructed by a beam-splitter, a pinhole mirror, a reflective mirror and two lenses to build a 4f optical system. The pinhole mirror is used as a low-pass spatial filter to generate reference wave. By tilting the reflective mirror, a small angle is created between the object beam and the reference beam to enable an off-axis interferogram. To reconstruct an interferogram with a few fringes, Kreis Fourier method is used to recovery the specimen phase. Using a plano-convex cylinder lens and an evaporative alcohol drop as the specimens, experiments are run to verify the effectiveness and robustness with this interferometer. Experimental results show that this interferometer has not only simple setup and good anti-interference performance, but also good real-time ability, which makes it suitable for dynamic phase measurement.

  11. Nondestructive evaluation of near-surface residual stress in shot-peened nickel-base superalloys

    NASA Astrophysics Data System (ADS)

    Yu, Feng

    Surface enhancement methods, which produce beneficial compressive residual stresses and increased hardness in a shallow near-surface region, are widely used in a number of industrial applications, including gas-turbine engines. Nondestructive evaluation of residual stress gradients in surface-enhanced materials has great significance for turbine engine component life extension and their reliability in service. It has been recently found that, in sharp contrast with most other materials, shot-peened nickel-base superalloys exhibit an apparent increase in electrical conductivity at increasing inspection frequencies, which can be exploited for nondestructive residual stress assessment. The primary goal of this research is to develop a quantitative eddy current method for nondestructive residual stress profiles in surface-treated nickel-base superalloys. Our work have been focused on five different aspects of this issue, namely, (i) validating the noncontacting eddy current technique for electroelastic coefficients calibration, (ii) developing inversion procedures for determining the subsurface residual stress profiles from the measured apparent eddy current conductivity (AECC), (iii) predicting the adverse effect of surface roughness on the eddy current characterization of shot-peened metals, (iv) separating excess AECC caused by the primary residual stress effect from intrinsic conductivity variations caused by material inhomogeneity, and (v) investigating different mechanisms through which cold work could influence the AECC in surface-treated nickel-base superalloys. The results of this dissertation have led to a better understanding of the underlying physical phenomenon of the measured excess AECC on nickel-base engine alloys, and solved a few critical applied issues in eddy current nondestructive residual stress assessment in surface-treated engine components and, ultimately, contributed to the better utilization and safer operation of the Air Force's aging

  12. Free-Suspension Residual Flexibility Testing of Space Station Pathfinder: Comparison to Fixed-Base Results

    NASA Technical Reports Server (NTRS)

    Tinker, Michael L.

    1998-01-01

    Application of the free-suspension residual flexibility modal test method to the International Space Station Pathfinder structure is described. The Pathfinder, a large structure of the general size and weight of Space Station module elements, was also tested in a large fixed-base fixture to simulate Shuttle Orbiter payload constraints. After correlation of the Pathfinder finite element model to residual flexibility test data, the model was coupled to a fixture model, and constrained modes and frequencies were compared to fixed-base test. modes. The residual flexibility model compared very favorably to results of the fixed-base test. This is the first known direct comparison of free-suspension residual flexibility and fixed-base test results for a large structure. The model correlation approach used by the author for residual flexibility data is presented. Frequency response functions (FRF) for the regions of the structure that interface with the environment (a test fixture or another structure) are shown to be the primary tools for model correlation that distinguish or characterize the residual flexibility approach. A number of critical issues related to use of the structure interface FRF for correlating the model are then identified and discussed, including (1) the requirement of prominent stiffness lines, (2) overcoming problems with measurement noise which makes the antiresonances or minima in the functions difficult to identify, and (3) the use of interface stiffness and lumped mass perturbations to bring the analytical responses into agreement with test data. It is shown that good comparison of analytical-to-experimental FRF is the key to obtaining good agreement of the residual flexibility values.

  13. MICROCARD: a micro-camera based on a circular diffraction grating for MWIR and LWIR imagery

    NASA Astrophysics Data System (ADS)

    Druart, Guillaume; Guérineau, Nicolas; Tauvy, Michel; Rommeluère, Sylvain; Primot, Jérôme; Deschamps, Joël; Fendler, Manuel; Cigna, Jean-Charles; Taboury, Jean

    2008-09-01

    Circular diffraction gratings (also called diffractive axicons) are optical components producing achromatic non-diffracting beams. They thus produce a focal line rather than a focal point for classical lenses. We have recently shown in the visible spectral range that this property can be used to design a simple imaging system with a long depth of focus and a linear variable zoom by using and translating a diffractive axicon as the only component. We have then adapted this principle for the mid-wavelength infrared (MWIR) spectral range and the long-wavelength infrared (LWIR) spectral range. A LWIR low-cost micro-camera, called MICROCARD, has been designed and realized. First images from this camera will be shown. Moreover a way to design a compact MWIR micro-camera with moveable parts integrated directly into the cryostat will be presented.

  14. Prediction of protein secondary structure based on residue pair types and conformational states using dynamic programming algorithm.

    PubMed

    Sadeghi, Mehdi; Parto, Sahar; Arab, Shahriar; Ranjbar, Bijan

    2005-06-20

    We have used a statistical approach for protein secondary structure prediction based on information theory and simultaneously taking into consideration pairwise residue types and conformational states. Since the prediction of residue secondary structure by one residue window sliding make ambiguity in state prediction, we used a dynamic programming algorithm to find the path with maximum score. A score system for residue pairs in particular conformations is derived for adjacent neighbors up to ten residue apart in sequence. The three state overall per-residue accuracy, Q3, of this method in a jackknife test with dataset created from PDBSELECT is more than 70%. PMID:15936021

  15. Mindful mood balance: a case report of Web-based treatment of residual depressive symptoms.

    PubMed

    Felder, Jennifer; Dimidjian, Sona; Beck, Arne; Boggs, Jennifer M; Segal, Zindel

    2014-01-01

    Residual depressive symptoms are associated with increased risk for relapse and impaired functioning. Although there is no definitive treatment for residual depressive symptoms, Mindfulness-Based Cognitive Therapy has been shown to be effective, but access is limited. Mindful Mood Balance (MMB), a Web-based adaptation of Mindfulness-Based Cognitive Therapy, was designed to address this care gap. In this case study, we describe a composite case that is representative of the course of intervention with MMB and its implementation in a large integrated delivery system. Specifically, we describe the content of each of eight weekly sessions, and the self-management skills developed by participating in this program. MMB may be a cost-effective and scalable option in primary care for increasing access to treatments for patients with residual depressive symptoms. PMID:25141988

  16. Mindful Mood Balance: A Case Report of Web-Based Treatment of Residual Depressive Symptoms

    PubMed Central

    Felder, Jennifer; Dimidjian, Sona; Beck, Arne; Boggs, Jennifer M; Segal, Zindel

    2014-01-01

    Residual depressive symptoms are associated with increased risk for relapse and impaired functioning. Although there is no definitive treatment for residual depressive symptoms, Mindfulness-Based Cognitive Therapy has been shown to be effective, but access is limited. Mindful Mood Balance (MMB), a Web-based adaptation of Mindfulness-Based Cognitive Therapy, was designed to address this care gap. In this case study, we describe a composite case that is representative of the course of intervention with MMB and its implementation in a large integrated delivery system. Specifically, we describe the content of each of eight weekly sessions, and the self-management skills developed by participating in this program. MMB may be a cost-effective and scalable option in primary care for increasing access to treatments for patients with residual depressive symptoms. PMID:25141988

  17. Fast GPU-based absolute intensity determination for energy-dispersive X-ray Laue diffraction

    NASA Astrophysics Data System (ADS)

    Alghabi, F.; Send, S.; Schipper, U.; Abboud, A.; Pietsch, U.; Kolb, A.

    2016-01-01

    This paper presents a novel method for fast determination of absolute intensities in the sites of Laue spots generated by a tetragonal hen egg-white lysozyme crystal after exposure to white synchrotron radiation during an energy-dispersive X-ray Laue diffraction experiment. The Laue spots are taken by means of an energy-dispersive X-ray 2D pnCCD detector. Current pnCCD detectors have a spatial resolution of 384 × 384 pixels of size 75 × 75 μm2 each and operate at a maximum of 400 Hz. Future devices are going to have higher spatial resolution and frame rates. The proposed method runs on a computer equipped with multiple Graphics Processing Units (GPUs) which provide fast and parallel processing capabilities. Accordingly, our GPU-based algorithm exploits these capabilities to further analyse the Laue spots of the sample. The main contribution of the paper is therefore an alternative algorithm for determining absolute intensities of Laue spots which are themselves computed from a sequence of pnCCD frames. Moreover, a new method for integrating spectral peak intensities and improved background correction, a different way of calculating mean count rate of the background signal and also a new method for n-dimensional Poisson fitting are presented.We present a comparison of the quality of results from the GPU-based algorithm with the quality of results from a prior (base) algorithm running on CPU. This comparison shows that our algorithm is able to produce results with at least the same quality as the base algorithm. Furthermore, the GPU-based algorithm is able to speed up one of the most time-consuming parts of the base algorithm, which is n-dimensional Poisson fitting, by a factor of more than 3. Also, the entire procedure of extracting Laue spots' positions, energies and absolute intensities from a raw dataset of pnCCD frames is accelerated by a factor of more than 3.

  18. Multiple Bragg diffraction in opal-based photonic crystals: Spectral and spatial dispersion

    NASA Astrophysics Data System (ADS)

    Shishkin, I. I.; Rybin, M. V.; Samusev, K. B.; Golubev, V. G.; Limonov, M. F.

    2014-01-01

    We present an experimental and theoretical study of multiple Bragg diffraction from synthetic opals. An original setup permits us to overcome the problem of the total internal light reflection in an opal film and to investigate the diffraction from both the (111) and (1¯11) systems of planes responsible for the effect. As a result, angle- and frequency-resolved diffraction and transmission measurements create a picture of multiple Bragg diffraction that includes general agreement between dips in the transmission spectra and diffraction peaks for each incident white light angle and a twin-peak structure at frequencies of the photonic stop band edges. Two opposite cases of the interference are discussed: an interference of two narrow Bragg bands that leads to multiple Bragg diffraction with anticrossing regime for dispersion photonic branches and an interference of a narrow Bragg band and broad disorder-induced Mie background that results in a Fano resonance. A good quantitative agreement between the experimental data and calculated photonic band structure has been obtained.

  19. Applications of on-product diffraction-based focus metrology in logic high volume manufacturing

    NASA Astrophysics Data System (ADS)

    Noyes, Ben F.; Mokaberi, Babak; Bolton, David; Li, Chen; Palande, Ashwin; Park, Kevin; Noot, Marc; Kea, Marc

    2016-03-01

    The integration of on-product diffraction-based focus (DBF) capability into the majority of immersion lithography layers in leading edge logic manufacturing has enabled new applications targeted towards improving cycle time and yield. A CD-based detection method is the process of record (POR) for excursion detection. The drawback of this method is increased cycle time and limited sampling due to CD-SEM metrology capacity constraints. The DBFbased method allows the addition of focus metrology samples to the existing overlay measurements on the integrated metrology (IM) system. The result enables the addition of measured focus to the SPC system, allowing a faster excursion detection method. For focus targeting, the current method involves using a dedicated focus-exposure matrix (FEM) on all scanners, resulting in lengthy analysis times and uncertainty in the best focus. The DBF method allows the measurement to occur on the IM system, on a regular production wafer, and at the same time as the exposure. This results in a cycle time gain as well as a less subjective determination of best focus. A third application aims to use the novel onproduct focus metrology data in order to apply per-exposure focus corrections to the scanner. These corrections are particularly effective at the edge of the wafer, where systematic layer-dependent effects can be removed using DBFbased scanner feedback. This paper will discuss the development of a methodology to accomplish each of these applications in a high-volume production environment. The new focus metrology method, sampling schemes, feedback mechanisms and analysis methods lead to improved focus control, as well as earlier detection of failures.

  20. Sound Velocity and Diffraction Intensity Measurements Based on Raman-Nath Theory of the Interaction of Light and Ultrasound

    ERIC Educational Resources Information Center

    Neeson, John F.; Austin, Stephen

    1975-01-01

    Describes a method for the measurement of the velocity of sound in various liquids based on the Raman-Nath theory of light-sound interaction. Utilizes an analog computer program to calculate the intensity of light scattered into various diffraction orders. (CP)

  1. An Inquiry-Based Project Focused on the X-Ray Powder Diffraction Analysis of Common Household Solids

    ERIC Educational Resources Information Center

    Hulien, Molly L.; Lekse, Jonathan W.; Rosmus, Kimberly A.; Devlin, Kasey P.; Glenn, Jennifer R.; Wisneski, Stephen D.; Wildfong, Peter; Lake, Charles H.; MacNeil, Joseph H.; Aitken, Jennifer A.

    2015-01-01

    While X-ray powder diffraction (XRPD) is a fundamental analytical technique used by solid-state laboratories across a breadth of disciplines, it is still underrepresented in most undergraduate curricula. In this work, we incorporate XRPD analysis into an inquiry-based project that requires students to identify the crystalline component(s) of…

  2. Visualization of soft tissues by highly sensitive X-ray crystal analyzer-based multi diffraction enhanced imaging

    NASA Astrophysics Data System (ADS)

    Wu, Yanlin; Sunaguchi, Naoki; Lin, Xiaojie; Wang, Yongting; Yuasa, Tetsuya; Hirano, Keiichi; Hyodo, Kazuyuki

    2015-09-01

    In this paper, we propose a novel multi diffraction enhanced imaging (MDEI) technique to improve contrast resolution owning to the sharp rise of the reflectivity curve and high contrast-to-noise ratio (CNR). MDEI is derived from the diffraction enhanced imaging (DEI) technique. Here, DEI and MDEI phase contrast tomograms are compared. The results show that MDEI offers higher contrast resolution, while DEI has higher spatial resolution. This study provided indications for developments and applications of X-ray crystal analyzer-based imaging to obtain a higher contrast resolution.

  3. Residual Motion and Duty Time in Respiratory Gating Radiotherapy Using Individualized or Population-Based Windows

    SciTech Connect

    Fuji, Hiroshi Asada, Yoshihiro; Numano, Masumi; Yamashita, Haruo; Nishimura, Tetsuo; Hashimoto, Takayuki; Harada, Hideyuki; Asakura, Hirofumi; Murayama, Shigeyuki

    2009-10-01

    Purpose: The efficiency and precision of respiratory gated radiation therapy for tumors is affected by variations in respiration-induced tumor motion. We evaluated the use of individualized and population-based parameters for such treatment. Methods and Materials: External respiratory signal records and images of respiration-induced tumor motion were obtained from 42 patients undergoing respiratory gated radiation therapy for liver tumors. Gating window widths were calculated for each patient, with 2, 4, and 10 mm of residual motion, and the mean was defined as the population-based window width. Residual motions based on population-based and predefined window widths were compared. Duty times based on whole treatment sessions, at various window levels, were calculated. The window level giving the longest duty time was defined as the individualized most efficient level (MEL). MELs were also calculated based on the first 10 breathing cycles. The duty times for population-based MELs (defined as mean MELs) and individualized MELs were compared. Results: Tracks of respiration-induced tumor motion ranged from 3 to 50 mm. Half of the patients had larger actual residual motions than the assigned residual motions. Duty times were greater when based on individualized, rather than population-based, window widths. The MELs established during whole treatment sessions for 2 mm and 4 mm of residual motion gave significantly increased duty times, whereas those calculated using the first 10 breathing cycles showed only marginal increases. Conclusions: Using individualized window widths and levels provided more precise and efficient respiratory gated radiation therapy. However, methods for predicting individualized window levels before treatment remain to be explored.

  4. Synchrotron-based crystal structure, associated morphology of snail and bivalve shells by X-ray diffraction

    NASA Astrophysics Data System (ADS)

    Rao, D. V.; Gigante, G. E.; Kumar, Y. Manoj; Cesareo, R.; Brunetti, A.; Schiavon, N.; Akatsuka, T.; Yuasa, T.; Takeda, T.

    2016-10-01

    Synchrotron-based high-resolution X-ray powder diffraction spectra from the body parts of a snail and bivalve (CaCO3), have been recorded with Pilatus area detector. Experiments were performed at Desy, Hamburg, Germany, utilizing the Resonant and Diffraction beamline (P9), with 15 keV X-rays (λ=0.82666 Å). The external shell of these living organisms, is composed of calcium carbonate, which carries strong biological signal. It consists of some light elements, such as, Ca, C and O, which constitute part of the soft tissue and other trace elements. The knowledge of these diffraction patterns and hence the understanding of structures at molecular level are enormous. The application of synchrotron radiation to powder diffraction is well suited for samples of biological nature via changes in their patterns and also to investigate crystallographic phase composition. With the use of Rietveld refinement procedure, to the high-resolution diffraction spectra, we were able to extract the lattice parameters of orthorhombic polymorph of CaCO3, the most abundant mineral produced by these living organisms. The small size of the crystallite is a very important factor related to the biological structure. The natural model presents a combination of organic and inorganic phases with nanometer size. For the present study, we also used the scanning electron microscopy (SEM) to explore the associated morphology of the snail and bivalve.

  5. Numerical Analysis of Residual Stress for Copper Base Brazed Stainless Steel Plate-Fin Structure

    NASA Astrophysics Data System (ADS)

    Xie, Qiaoyun; Ling, Xiang

    2010-07-01

    Copper base stainless steel plate-fin structure has been widely used as a heat exchanger in many fields. The nonlinear thermal reaction on the residual stress in brazing process of the plate-fin structure was studied in this paper. A finite element model (FEM) was proposed to simulate the heat transfer and the sequential residual stress generated in the plate-fin and filler metals based on thermal elastic-plastic theory. By the stress distribution in four paths marked in the structure obtained from FEM results, it is found that the maximum residual tensile stress occurs in the brazed joint next to the plate side and a crack would initiate in this region. Also, the first principle stresses of reference nodes were calculated and the conclusion is consistent with the simulation results. These results would provide some constructive instructions in the practical brazing procedure.

  6. Near-Surface Residual Stress Assessment in Inhomogeneous Nickel-Base Superalloys

    NASA Astrophysics Data System (ADS)

    Yu, F.; Nagy, P. B.

    2006-03-01

    Recently, it has been shown that shot-peened nickel-base superalloys exhibit an approximately 1% increase in apparent eddy current conductivity at high inspection frequencies, which can be exploited for nondestructive subsurface residual stress assessment. Unfortunately, microstructural inhomogeneity in certain as-forged and precipitation hardened nickel-base superalloys, like Waspaloy, can lead to significantly larger electrical conductivity variations of as much as 4-6%. This intrinsic conductivity variation adversely affects the accuracy of residual stress evaluation in shot-peened and subsequently thermal-relaxed specimens, but does not completely prevent it. Experimental results are presented to demonstrate that the conductivity variation resulting from volumetric inhomogeneities in as-forged engine alloys do not display significant frequency dependence. This characteristic independence of frequency can be exploited to distinguish these inhomogeneities from near-surface residual stress and cold work effects caused by surface treatment, which, in contrast, are strongly frequency-dependent.

  7. Near-Surface Residual Stress Assessment in Inhomogeneous Nickel-Base Superalloys

    SciTech Connect

    Yu, F.; Nagy, P. B.

    2006-03-06

    Recently, it has been shown that shot-peened nickel-base superalloys exhibit an approximately 1% increase in apparent eddy current conductivity at high inspection frequencies, which can be exploited for nondestructive subsurface residual stress assessment. Unfortunately, microstructural inhomogeneity in certain as-forged and precipitation hardened nickel-base superalloys, like Waspaloy, can lead to significantly larger electrical conductivity variations of as much as 4-6%. This intrinsic conductivity variation adversely affects the accuracy of residual stress evaluation in shot-peened and subsequently thermal-relaxed specimens, but does not completely prevent it. Experimental results are presented to demonstrate that the conductivity variation resulting from volumetric inhomogeneities in as-forged engine alloys do not display significant frequency dependence. This characteristic independence of frequency can be exploited to distinguish these inhomogeneities from near-surface residual stress and cold work effects caused by surface treatment, which, in contrast, are strongly frequency-dependent.

  8. Computer-based classification of bacteria species by analysis of their colonies Fresnel diffraction patterns

    NASA Astrophysics Data System (ADS)

    Suchwalko, Agnieszka; Buzalewicz, Igor; Podbielska, Halina

    2012-01-01

    In the presented paper the optical system with converging spherical wave illumination for classification of bacteria species, is proposed. It allows for compression of the observation space, observation of Fresnel patterns, diffraction pattern scaling and low level of optical aberrations, which are not possessed by other optical configurations. Obtained experimental results have shown that colonies of specific bacteria species generate unique diffraction signatures. Analysis of Fresnel diffraction patterns of bacteria colonies can be fast and reliable method for classification and recognition of bacteria species. To determine the unique features of bacteria colonies diffraction patterns the image processing analysis was proposed. Classification can be performed by analyzing the spatial structure of diffraction patterns, which can be characterized by set of concentric rings. The characteristics of such rings depends on the bacteria species. In the paper, the influence of basic features and ring partitioning number on the bacteria classification, is analyzed. It is demonstrated that Fresnel patterns can be used for classification of following species: Salmonella enteritidis, Staplyococcus aureus, Proteus mirabilis and Citrobacter freundii. Image processing is performed by free ImageJ software, for which a special macro with human interaction, was written. LDA classification, CV method, ANOVA and PCA visualizations preceded by image data extraction were conducted using the free software R.

  9. A new approach to calculating powder diffraction patterns based on the Debye scattering equation.

    PubMed

    Thomas, Noel William

    2010-01-01

    A new method is defined for the calculation of X-ray and neutron powder diffraction patterns from the Debye scattering equation (DSE). Pairwise atomic interactions are split into two contributions, the first from lattice-pair vectors and the second from cell-pair vectors. Since the frequencies of lattice-pair vectors can be directly related to crystallite size, application of the DSE is thereby extended to crystallites of lengths up to approximately 200 nm. The input data correspond to unit-cell parameters, atomic coordinates and displacement factors. The calculated diffraction patterns are characterized by full backgrounds as well as complete reflection profiles. Four illustrative systems are considered: sodium chloride (NaCl), alpha-quartz, monoclinic lead zirconate titanate (PZT) and kaolinite. The effects of varying crystallite size on diffraction patterns are calculated for NaCl, quartz and kaolinite, and a method of modelling static structural disorder is defined for kaolinite. The idea of partial diffraction patterns is introduced and a treatment of atomic displacement parameters is included. Although the method uses pair distribution functions as an intermediate stage, it is anticipated that further progress in reducing computational times will be made by proceeding directly from crystal structure to diffraction pattern. PMID:20029134

  10. Diffractive optics in large sizes: computer-generated holograms (CGH) based on Bayfol HX photopolymer

    NASA Astrophysics Data System (ADS)

    Bruder, Friedrich-Karl; Fäcke, Thomas; Hagen, Rainer; Hönel, Dennis; Kleinschmidt, Tim Patrick; Orselli, Enrico; Rewitz, Christian; Rölle, Thomas; Walze, Günther

    2015-03-01

    Volume Holographic Optical Elements (vHOE) offer angular and spectral Bragg selectivity that can be tuned by film thickness and holographic recording conditions. With the option to integrate complex optical function in a very thin plastic layer formerly heavy refractive optics can be made thin and lightweight especially for large area applications like liquid crystal displays, projection screens or photovoltaic. Additionally their Bragg selectivity enables the integration of several completely separated optical functions in the same film. The new instant developing photopolymer film (Bayfol® HX) paves the way towards new cost effective diffractive large optics, due to its easy holographic recording and environmental stability. A major bottleneck for large area applications has been the master hologram recording which traditionally needs expensive, large high precision optical equipment and high power laser with long coherence length. Further the recording setup needs to be rearranged for a change in optical design. In this paper we describe an alternative method for large area holographic master recording, using standard optics and low power lasers in combination with an x, y-translation stage. In this setup small sub-holograms generated by a phase only spatial light modulator (SLM) are recorded next to each other to generate a large size vHOE. The setup is flexible to generate various types of HOEs without the need of a change in the mechanical and optical construction by convenient SLM programming. One Application example and parameter studies for printed vHOEs based on Bayfol® HX Photopolymer will be given.

  11. Optical pendulum effect in one-dimensional diffraction-thick porous silicon based photonic crystals

    SciTech Connect

    Novikov, V. B. Svyakhovskiy, S. E.; Maydykovskiy, A. I.; Murzina, T. V.; Mantsyzov, B. I.

    2015-11-21

    We present the realization of the multiperiodic optical pendulum effect in 1D porous silicon photonic crystals (PhCs) under dynamical Bragg diffraction in the Laue scheme. The diffraction-thick PhC contained 360 spatial periods with a large variation of the refractive index of adjacent layers of 0.4. The experiments reveal switching of the light leaving the PhC between the two spatial directions, which correspond to Laue diffraction maxima, as the fundamental wavelength or polarization of the incident light is varied. A similar effect can be achieved when the temperature of the sample or the intensity of the additional laser beam illuminating the crystal are changed. We show that in our PhC structures, the spectral period of the pendulum effect is down to 5 nm, while the thermal period is about 10 °C.

  12. Optical cryptography topology based on a three-dimensional particle-like distribution and diffractive imaging.

    PubMed

    Chen, Wen; Chen, Xudong

    2011-05-01

    In recent years, coherent diffractive imaging has been considered as a promising alternative for information retrieval instead of conventional interference methods. Coherent diffractive imaging using the X-ray light source has opened up a new research perspective for the measurement of non-crystalline and biological specimens, and can achieve unprecedentedly high resolutions. In this paper, we show how a three-dimensional (3D) particle-like distribution and coherent diffractive imaging can be applied for a study of optical cryptography. An optical multiple-random-phase-mask encoding approach is used, and the plaintext is considered as a series of particles distributed in a 3D space. A topology concept is also introduced into the proposed optical cryptosystem. During image decryption, a retrieval algorithm is developed to extract the plaintext from the ciphertexts. In addition, security and advantages of the proposed optical cryptography topology are also analyzed. PMID:21643154

  13. Optical pendulum effect in one-dimensional diffraction-thick porous silicon based photonic crystals

    NASA Astrophysics Data System (ADS)

    Novikov, V. B.; Svyakhovskiy, S. E.; Maydykovskiy, A. I.; Murzina, T. V.; Mantsyzov, B. I.

    2015-11-01

    We present the realization of the multiperiodic optical pendulum effect in 1D porous silicon photonic crystals (PhCs) under dynamical Bragg diffraction in the Laue scheme. The diffraction-thick PhC contained 360 spatial periods with a large variation of the refractive index of adjacent layers of 0.4. The experiments reveal switching of the light leaving the PhC between the two spatial directions, which correspond to Laue diffraction maxima, as the fundamental wavelength or polarization of the incident light is varied. A similar effect can be achieved when the temperature of the sample or the intensity of the additional laser beam illuminating the crystal are changed. We show that in our PhC structures, the spectral period of the pendulum effect is down to 5 nm, while the thermal period is about 10 °C.

  14. Multiwavelength anomalous diffraction analyses of protein structures based on xenon and selenium resonances

    NASA Astrophysics Data System (ADS)

    Slama, Betty Nicole

    The 'phase problem' is central to X-ray crystallography, and multiwavelength anomalous diffraction (MAD) provides an elegant and broadly accessible solution. In the first part, the use of MAD at the xenon L3 edge is explored, as an alternative to the well established selenium K-edge phasing. In the second part, the structure of the bacterial protein Vibrio cholerae LuxQ, part of a two component signaling system involved in quorum sensing, is solved and analyzed. Keywords: anomalous scattering, x-ray diffraction, phasing, protein structure.

  15. Isoelectric Point, Electric Charge, and Nomenclature of the Acid-Base Residues of Proteins

    ERIC Educational Resources Information Center

    Maldonado, Andres A.; Ribeiro, Joao M.; Sillero, Antonio

    2010-01-01

    The main object of this work is to present the pedagogical usefulness of the theoretical methods, developed in this laboratory, for the determination of the isoelectric point (pI) and the net electric charge of proteins together with some comments on the naming of the acid-base residues of proteins. (Contains 8 figures and 4 tables.)

  16. Analysis of oxytetracycline residue in salmon muscle using a portable analyzer based on Eu III luminescence

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Oxytetracycline (OTC), one of tetracycline (TC) antibiotics, is the most prominent therapeutant in aquaculture worldwide. In this work, OTC residue in salmon muscle is determined by europium-sensitized luminescence (ESL) using an LED-based portable analyzer. OTC is extracted in EDTA-McIlvaine buff...

  17. Post-extraction algal residue in steam-flaked corn-based diets for beef cattle

    Technology Transfer Automated Retrieval System (TEKTRAN)

    The effects of post-extraction algal residue (PEAR) as N source 23 in steam-flaked corn-based (SFC) beef cattle finishing diets on intake, duodenal flow, digestion, ruminal microbial efficiency, ruminal parameters, and blood constituents were evaluated. Ruminally and duodenally cannulated steers (BW...

  18. Far-field sub-diffraction focusing lens based on binary amplitude-phase mask for linearly polarized light.

    PubMed

    Chen, Gang; Zhang, Kun; Yu, Anping; Wang, Xianyou; Zhang, Zhihai; Li, Yuyan; Wen, Zhongquan; Li, Chen; Dai, Luru; Jiang, Senling; Lin, Feng

    2016-05-16

    Planar lenses are attractive photonic devices due to its minimized size and easy to integrate. However, planar lenses designed in traditional ways are restricted by the diffraction limit. They have difficulties in further reducing the focal spot size beyond the diffraction limit. Super-oscillation provides a possible way to solve the problem. However, lenses based on super-oscillation have always been affected by huge sidelobes, which resulted in limited field of view and difficulties in real applications. To address the problem, in the paper, a far-field sub-diffraction lens based on binary amplitude-phase mask was demonstrated under illumination of linearly polarized plane wave at wavelength 632.8 nm. The lens realized a long focal length of 148λ (94 µm), and the full width at half maximum of the focal line was 0.406λ, which was super-oscillatory. More important is that such a flat lens has small sidelobes and wide field of view. Within the measured range of [-132λ, + 120λ], the maximum sidelobe observed on the focal plane was less than 22% of the central peak. Such binary amplitude-phase planar lens can also be extended to long focal length far-field sub-diffraction focusing lens for other spectrum ranges. PMID:27409922

  19. Generalization of the residual cutting method based on the Krylov subspace

    NASA Astrophysics Data System (ADS)

    Abe, Toshihiko; Sekine, Yoshihito; Kikuchi, Kazuo

    2016-06-01

    The residual cutting (RC) method has been reported to have superior converging characteristics in numerically solving elliptic partial differential equations. However, its application is limited to linear problems with diagonal-dominant matrices in general, for which convergence of a relaxation method such as SOR is guaranteed. In this study, we propose the generalized residual cutting (GRC) method, which is based on the Krylov subspace and applicable to general unsymmetric linear problems. Also, we perform numerical experiments with various coefficient matrices, and show that the GRC method has some desirable properties such as convergence characteristics and memory usage, in comparison to the conventional RC, BiCGSTAB and GMRES methods.

  20. Plane-wave Fresnel diffraction by elliptic apertures: a Fourier-based approach.

    PubMed

    Borghi, Riccardo

    2014-10-01

    A simple theoretical approach to evaluate the scalar wavefield, produced, within paraxial approximation, by the diffraction of monochromatic plane waves impinging on elliptic apertures or obstacles is presented. We find that the diffracted field can be mathematically described in terms of a Fourier series with respect to an angular variable suitably related to the elliptic parametrization of the observation plane. The convergence features of such Fourier series are analyzed, and a priori truncation criterion is also proposed. Two-dimensional maps of the optical intensity diffraction patterns are then numerically generated and compared, at a visual level, with several experimental pictures produced in the past. The last part of this work is devoted to carrying out an analytical investigation of the diffracted field along the ellipse axis. A uniform approximation is derived on applying a method originally developed by Schwarzschild, and an asymptotic estimate, valid in the limit of small eccentricities, is also obtained via the Maggi-Rubinowicz boundary wave theory. PMID:25401234

  1. Ophthalmic compensation of visual ametropia based on a programmable diffractive lens

    NASA Astrophysics Data System (ADS)

    Millán, Maria S.; Pérez-Cabré, Elisabet; Romero, Lenny A.; Ramírez, Natalia

    2013-11-01

    Pixelated liquid crystal displays have been widely used as spatial light modulators to implement programmable diffractive optical elements (DOEs), particularly diffractive lenses. Many different applications of such components have been developed in information optics and optical processors that take advantage of their properties of great flexibility, easy and fast refreshment, and multiplexing capability in comparison with equivalent conventional refractive lenses. In this paper, we explore the application of programmable diffractive lenses displayed on the pixelated screen of a liquid crystal on silicon spatial light modulator (LCoS-SLM) to ophthalmic optics. In particular, we consider the use of programmable diffractive lenses for the visual compensation of some refractive errors (myopia, hyperopia). The theoretical principles of compensation are described and sketched using geometrical optics and paraxial ray tracing. A series of experiments with artificial eye in optical bench are conducted to analyze the compensation accuracy in terms of optical power and to compare the results with those obtained by means of conventional ophthalmic lenses. Practical considerations oriented to feasible applications are provided.

  2. Generation of High-Density Electrons Based on Plasma Grating Induced Bragg Diffraction in Air

    SciTech Connect

    Shi Liping; Li Wenxue; Wang Yongdong; Lu Xin; Ding Liang'en; Zeng Heping

    2011-08-26

    Efficient nonlinear Bragg diffraction was observed as an intense infrared femtosecond pulse was focused on a plasma grating induced by interference between two ultraviolet femtosecond laser pulses in air. The preformed electrons inside the plasma grating were accelerated by subsequent intense infrared laser pulses, inducing further collisional ionization and significantly enhancing the local electron density.

  3. Diffraction-based study of fatigue crack initiation and propagation in aerospace aluminum alloys

    NASA Astrophysics Data System (ADS)

    Gupta, Vipul K.

    The crack initiation sites and microstructure-sensitive growth of small fatigue cracks are experimentally characterized in two precipitation-hardened aluminum alloys, 7075-T651 and 7050-T7451, stressed in ambient temperature moist-air (warm-humid) and -50°C dry N2 (cold-dry) environmental conditions. Backscattered electron imaging (BSE) and energy dispersive spectroscopy (EDS) of the fracture surfaces showed that Fe-Cu rich constituent particle clusters are the most common initiation sites within both alloys stressed in either environment. The crack growth within each alloy, on average, was observed to be slowed in the cold-dry environment than in the warm-humid environment, but only at longer crack lengths. Although no overwhelming effects of grain boundaries and grain orientations on small-crack growth were observed, crack growth data showed local fluctuations within individual grains. These observations are understood as crack propagation through the underlying substructure at the crack surface and frequent interaction with low/high-angle grain and subgrain boundaries, during cyclic loading, and, are further attributed to periodic changes in crack propagation path and multiple occurrences of crack-branching observed in the current study. SEM-based stereology in combination with electron backscattered diffraction (EBSD) established fatigue crack surface crystallography within the region from ˜1 to 50 mum of crack initiating particle clusters. Fatigue crack facets were parallel to a wide variety of crystallographic planes, with pole orientations distributed broadly across the irreducible stereographic triangle between the {001} and {101}-poles within both warm-humid and cold-dry environments. The results indicate environmentally affected fatigue cracking in both cases, given the similarity between the observed morphology and crystallography with that of a variety of aerospace aluminum alloys cracked in the presence of moist-air. There was no evidence of

  4. Eddy Current Nondestructive Residual Stress Assessment in Shot-Peened Nickel-Base Superalloys

    SciTech Connect

    Blodgett, M.P.; Yu, F.; Nagy, P.B.

    2005-04-09

    Shot peening and other mechanical surface enhancement methods improve the fatigue resistance and foreign-object damage tolerance of metallic components by introducing beneficial near-surface compressive residual stresses and hardening the surface. However, the fatigue life improvement gained via surface enhancement is not explicitly accounted for in current engine component life prediction models because of the lack of accurate and reliable nondestructive methods that could verify the presence of compressive near-surface residual stresses in shot-peened hardware. In light of its frequency-dependent penetration depth, the measurement of eddy current conductivity has been suggested as a possible means to allow the nondestructive evaluation of subsurface residual stresses in surface-treated components. This technique is based on the so-called piezoresistivity effect, i.e., the stress-dependence of electrical resistivity. We found that, in contrast with most other materials, surface-treated nickel-base superalloys exhibit an apparent increase in electrical conductivity at increasing inspection frequencies, i.e., at decreasing penetration depths. Experimental results are presented to illustrate that the excess frequency-dependent apparent eddy current conductivity of shot-peened nickel-base superalloys can be used to estimate the absolute level and penetration depth of the compressive residual stress layer both before and after partial thermal relaxation.

  5. A CMOS active pixel sensor system for laboratory- based x-ray diffraction studies of biological tissue.

    PubMed

    Bohndiek, Sarah E; Cook, Emily J; Arvanitis, Costas D; Olivo, Alessandro; Royle, Gary J; Clark, Andy T; Prydderch, Mark L; Turchetta, Renato; Speller, Robert D

    2008-02-01

    X-ray diffraction studies give material-specific information about biological tissue. Ideally, a large area, low noise, wide dynamic range digital x-ray detector is required for laboratory-based x-ray diffraction studies. The goal of this work is to introduce a novel imaging technology, the CMOS active pixel sensor (APS) that has the potential to fulfil all these requirements, and demonstrate its feasibility for coherent scatter imaging. A prototype CMOS APS has been included in an x-ray diffraction demonstration system. An industrial x-ray source with appropriate beam filtration is used to perform angle dispersive x-ray diffraction (ADXRD). Optimization of the experimental set-up is detailed including collimator options and detector operating parameters. Scatter signatures are measured for 11 different materials, covering three medical applications: breast cancer diagnosis, kidney stone identification and bone mineral density calculations. Scatter signatures are also recorded for three mixed samples of known composition. Results are verified using two independent models for predicting the APS scatter signature: (1) a linear systems model of the APS and (2) a linear superposition integral combining known monochromatic scatter signatures with the input polychromatic spectrum used in this case. Cross validation of experimental, modelled and literature results proves that APS are able to record biologically relevant scatter signatures. Coherent scatter signatures are sensitive to multiple materials present in a sample and provide a means to quantify composition. In the future, production of a bespoke APS imager for x-ray diffraction studies could enable simultaneous collection of the transmitted beam and scattered radiation in a laboratory-based coherent scatter system, making clinical transfer of the technique attainable. PMID:18199908

  6. Approach to improve beam quality of inter-satellite optical communication system based on diffractive optical elements.

    PubMed

    Tan, Liying; Yu, Jianjie; Ma, Jing; Yang, Yuqiang; Li, Mi; Jiang, Yijun; Liu, Jianfeng; Han, Qiqi

    2009-04-13

    For inter-satellite optical communication transmitter with reflective telescope of two-mirrors on axis, a large mount of the transmitted energy will be blocked by central obscuration of the secondary mirror. In this paper, a novel scheme based on diffractive optical element (DOE) is introduced to avoid it. This scheme includes one diffractive beam shaper and another diffractive phase corrector, which can diffract the obscured part of transmitted beam into the domain unobscured by the secondary mirror. The proposed approach is firstly researched with a fixed obscuration ratio of 1/4. Numerical simulation shows that the emission efficiency of new figuration is 99.99%; the beam divergence from the novel inter-satellite optical communication transmitter is unchanged; and the peak intensity of receiver plane is increased about 31% compared with the typical configuration. Then the intensy patterns of receiver plane are analyzed with various obscuration ratio, the corresponding numerical modelling reveals that the intensity patterns with various obscuration ratio are nearly identical, but the amplify of relative peak intensity is getting down with the growth of obscuration ratio. This work can improve the beam quality of inter-satellite optical communication system without affecting any other functionality. PMID:19365457

  7. SeO II addition on PVA-based photopolymer for improving photostorage stabilities and diffraction efficiencies

    NASA Astrophysics Data System (ADS)

    Kim, Daeheum; Nam, Seungwoong; Yeo, Seungbyung; Lim, Jiyun

    2006-08-01

    Polyvinyl alcohol/Acrylamide(PVA/AA)based photopolymer systems modified with SeO II crystals were prepared and photostorage characteristics mainly including diffraction efficiencies were examined and compared with pure PVA/AA films using green laser light (532nm). The photosensitive films were composed of polymeric film-forming binder (PVA), monomer (acrylamide, AA), photoinitiator (triethanol amine, TEA), photosensitizer (Eosin YR), and SeO II crystals. The best optical recording characteristics were observed at the composition of: polymer binder (PVA) : AA : TEA : SeO II : Eosin Y = 1.0 : 0.3 : 0.225 : 0.1 : 0.0015. Diffraction efficiencies as high as 85% with energetic sensitivity of 0.5 mW/cm2 have been obtained in the photopolymer film, and the photopolymer film with SeO II showed higher diffraction efficiencies and lower initial sensitivity than the photopolymer film without SeO II. The morphology of SeO II was expected to be nano crystals since they didn't scatter optical lights and didn't show any peaks in X-ray diffraction spectra.

  8. High-resolution diffraction for residual stress determination in the NiCrMoV wheel of an axial compressor for a heavy-duty gas turbine

    NASA Astrophysics Data System (ADS)

    Rogante, M.; Török, G.; Ceschini, G. F.; Tognarelli, L.; Füzesy, I.; Rosta, L.

    2004-07-01

    The wheel of an axial compressor for a heavy-duty gas turbine has been investigated for residual stresses (RS) evaluation of the teeth-section where SANS measurements have previously been performed. Such a component can contain internal RS, either due to the manufacturing process, or to the operating cycles fatigue. The constitutive material is a NiCrMoV steel to ASTM A 471 (type 2) norms (equivalent to B50A420B10); this material is usually adopted in the manufacturing of forged components for gas turbines. Internal radial and hoop RS have been determined, whose values are under the limit of 200kPa. Hoop RS, in general, resulted in higher value than the radial ones. The present experiment represents a particularly important step in the RS determination for gas turbine components, since the measurements reveal that the fatigue of the wheel is also a lifetime limiting factor although, in the same technological field, the available data in the actual neutron techniques literature mainly concern turbine buckets.

  9. Diffraction techniques in engineering applications

    SciTech Connect

    Kozarczek, K.J.; Hubbard, C.R.; Watkins, T.R.; Wang, X.L.; Spooner, S.

    1995-12-31

    Diffraction techniques applied to crystalline materials provide quantitative information about the crystallographic structure and mechanical condition of the material. Those two characteristics influence the chemical, physical, and mechanical properties of a Component. A concerted application of x-ray and neutron diffraction allows one to comprehensively study the bulk and subsurface variations of such material characteristics as crystallographic texture, residual stress, and cold work. The Residual Stress User Center at the Oak Ridge National Laboratory offers academic and industrial researchers both neutron and x-ray diffraction capabilities. Recent examples of the application of work related to thin film, metal, ceramic and composite material technologies are presented.

  10. Leaching of nitrogen and base cations from calcareous soil amended with organic residues.

    PubMed

    Zarabi, Mahboubeh; Jalali, Mohsen

    2012-01-01

    The potential for groundwater and surface water pollution by nutrients in organic residues, primarily nitrogen (N) and base cations (K+, Na+, Ca2+, Mg2+), is a consideration when applying such residues to land. In this study, we used a laboratory column leaching procedure to examine the leaching of N, K+, Na+, Ca2+ and Mg2+ in soils treated with two types of raw organic residues (poultry manure and potato residues) and one municipal waste compost, which are currently recycled on agricultural land in Iran. Each organic residue was thoroughly mixed with two different soils (sandy loam and clay) at the rate of 3%. Soil columns were leached at 4-d intervals for 92 d with distilled water, and effluents were analysed for pH, EC, nitrate (NO3(-)-N), ammonium (NH4(+)-N) K+, Na+, Ca2+ and Mg2+. The results indicated that the amounts of NO3(-)-N and NH4(+)-N leached from the poultry manure and potato residues could represent very important economic losses of N and pose an environmental threat under field conditions. The sandy loam soil amended with poultry manure lost the highest amount of NO3(-)-N (206.4 kg ha(-1)), and clay soil amended with poultry manure lost the highest amounts of NH4(+)-N (454.3 kg ha(-1)). The results showed that a treatment incorporating 3% of municipal waste compost could be used without negative effects to groundwater N concentration in clay soil. Significant amounts of K+, Na+, Ca2+, and Mg2+ were leached owing to the application of poultry manure, potato and municipal waste compost to soils. There was a positive relationship between K+, Na+, Ca2+, and Mg2+ with NO3(-)-N and NH4(+)-N leached in soils. Analysis of variance detected significant effects of amendment, soil type and time on the leaching NO3(-)-N, NH4(+)-N, K+, Na+, Ca2+ and Mg2+. PMID:22988618

  11. X-ray diffraction and EXAFS analysis of materials for lithium-based rechargeable batteries

    SciTech Connect

    Sharkov, M. D. Boiko, M. E.; Bobyl, A. V.; Ershenko, E. M.; Terukov, E. I.; Zubavichus, Y. V.

    2013-12-15

    Lithium iron phosphate LiFePO{sub 4} (triphylite) and lithium titanate Li{sub 4}Ti{sub 5}O{sub 12} are used as components of a number of active materials in modern rechargeable batteries. Samples of these materials are studied by X-ray diffraction and extended X-ray absorption fine structure (EXAFS) spectroscopy. Hypotheses about the phase composition of the analyzed samples are formulated.

  12. Sub-millimeter Bunch Length Non-invasive Diagnostic Based on the Diffraction and Cherenkov Radiation

    NASA Astrophysics Data System (ADS)

    Shevelev, M.; Deng, H.; Potylitsyn, A.; Naumenko, G.; Zhang, J.; Lu, Sh; Gogolev, S.; Shkitov, D.

    2012-05-01

    A layout for the investigation the coherent Cherenkov radiation from a dielectric target with a large spectral dispersion and the coherent diffraction radiation from a conducting screen as a tool for non-invasive longitudinal electron beam profile diagnostics are proposed for the 20~30MeV Linac at Shanghai Institute of Applied Physics (SINAP). In this paper the status of the joint experiment and future plans are presented.

  13. A laboratory based system for Laue micro x-ray diffraction

    SciTech Connect

    Advanced Light Source; Tamura, Nobumichi; Lynch, P.A.; Stevenson, A.W.; Liang, D.; Parry, D.; Wilkins, S.; Tamura, N.

    2007-02-28

    A laboratory diffraction system capable of illuminating individual grains in a polycrystalline matrix is described. Using a microfocus x-ray source equipped with a tungsten anode and prefigured monocapillary optic, a micro-x-ray diffraction system with a 10 mum beam was developed. The beam profile generated by the ellipsoidal capillary was determined using the"knife edge" approach. Measurement of the capillary performance, indicated a beam divergence of 14 mrad and a useable energy bandpass from 5.5 to 19 keV. Utilizing the polychromatic nature of the incident x-ray beam and application of the Laue indexing software package X-Ray Micro-Diffraction Analysis Software, the orientation and deviatoric strain of single grains in a polycrystalline material can be studied. To highlight the system potential the grain orientation and strain distribution of individual grains in a polycrystalline magnesium alloy (Mg 0.2 wt percent Nd) was mapped before and after tensile loading. A basal (0002) orientation was identified in the as-rolled annealed alloy; after tensile loading some grains were observed to undergo an orientation change of 30 degrees with respect to (0002). The applied uniaxial load was measured as an increase in the deviatoric tensile strain parallel to the load axis (37 References).

  14. Diffraction anomalies in hybrid structures based on chalcogenide Ge2Sb2Te5-coated opal photonic crystals

    NASA Astrophysics Data System (ADS)

    Voronov, M. M.; Pevtsov, A. B.; Yakovlev, S. A.; Kurdyukov, D. A.; Golubev, V. G.

    2014-01-01

    The results of spectroscopic studies of the diffraction anomalies (the so-called resonant Wood anomalies) in spatially periodic hybrid structures based on chalcogenide Ge2Sb2Te5-coated opal films of various thickness are presented. A theoretical analysis of spectral-angular dependencies of the Wood anomalies has been made by means of a phenomenological approach using the concept of the effective refractive index of the waveguiding surface layer.

  15. Polylactide-based renewable green composites from agricultural residues and their hybrids.

    PubMed

    Nyambo, Calistor; Mohanty, Amar K; Misra, Manjusri

    2010-06-14

    Agricultural natural fibers like jute, kenaf, sisal, flax, and industrial hemp have been extensively studied in green composites. The continuous supply of biofibers in high volumes to automotive part makers has raised concerns. Because extrusion followed by injection molding drastically reduces the aspect ratio of biofibers, the mechanical performance of injection molded agricultural residue and agricultural fiber-based composites are comparable. Here, the use of inexpensive agricultural residues and their hybrids that are 8-10 times cheaper than agricultural fibers is demonstrated to be a better way of getting sustainable materials with better performance. Green renewable composites from polylactide (PLA), agricultural residues (wheat straw, corn stover, soy stalks, and their hybrids) were successfully prepared through twin-screw extrusion, followed by injection molding. The effect on mechanical properties of varying the wheat straw amount from 10 to 40 wt % in PLA-wheat straw composites was studied. Tensile moduli were compared with theoretical calculations from the rule of mixture (ROM). Combination of agricultural residues as hybrids is proved to reduce the supply chain concerns for injection molded green composites. Densities of the green composites were found to be lower than those of conventional glass fiber composites. PMID:20499931

  16. Preliminary design of a zone plate based hard X-ray monochromatic diffraction nanoprobe for materials studies at APS

    NASA Astrophysics Data System (ADS)

    Cai, Zhonghou; Liu, Wenjun; Tischler, Jonathan Z.; Shu, Deming; Xu, Ruqing; Schmidt, Oliver

    2013-09-01

    Aiming at studies of the micro/nano-structures of a broad range materials and electronic devices, Advance Photon Source (APS) is developing a dedicated diffraction nanoprobe (DNP) beamline for the needs arising from a multidiscipline research community. As a part of the APS Upgrade Project, the planed facility, named Sub-micron 3-D Diffraction (S3DD) beamline1, integrates the K-B mirror based polychromatic Laue diffraction and the Fresnel zone-plate based monochromatic diffraction techniques that currently support 3D/2D microdiffraction programs at the 34-ID-E and 2-ID-D of the APS, respectively. Both diffraction nanoprobes are designed to have a 50-nm or better special resolution. The zone-plate based monochromatic DNP has been preliminarily designed and will be constructed at the sector 34-ID. It uses an APS-3.0-cm period or APS-3.3-cm period undulator, a liquid-nitrogen cooled mirror as its first optics, and a water cooled small gap silicon double-crystal monochromator with an energy range of 5-30 keV. A set of zone plates have been designed to optimize for focusing efficiency and the working distance based on the attainable beamline length and the beam coherence. To ensure the nanoprobe performance, high stiffness and high precision flexure stage systems have been designed or demonstrated for optics mounting and sample scanning, and high precision temperature control of the experimental station will be implemented to reduce thermal instability. Designed nanoprobe beamline has a good management on thermal power loading on optical components and allows high degree of the preservation of beam brilliance for high focal flux and coherence. Integrated with variety of X-ray techniques, planed facility provides nano-XRD capability with the maximum reciprocal space accessibility and allows micro/nano-spectroscopy studies with K-edge electron binding energies of most elements down to Vanadium in the periodic table. We will discuss the preliminary design of the zone

  17. Two States Mapping Based Time Series Neural Network Model for Compensation Prediction Residual Error

    NASA Astrophysics Data System (ADS)

    Jung, Insung; Koo, Lockjo; Wang, Gi-Nam

    2008-11-01

    The objective of this paper was to design a model of human bio signal data prediction system for decreasing of prediction error using two states mapping based time series neural network BP (back-propagation) model. Normally, a lot of the industry has been applied neural network model by training them in a supervised manner with the error back-propagation algorithm for time series prediction systems. However, it still has got a residual error between real value and prediction result. Therefore, we designed two states of neural network model for compensation residual error which is possible to use in the prevention of sudden death and metabolic syndrome disease such as hypertension disease and obesity. We determined that most of the simulation cases were satisfied by the two states mapping based time series prediction model. In particular, small sample size of times series were more accurate than the standard MLP model.

  18. A quantitative method for measurement of HL-60 cell apoptosis based on diffraction imaging flow cytometry technique

    PubMed Central

    Yang, Xu; Feng, Yuanming; Liu, Yahui; Zhang, Ning; Lin, Wang; Sa, Yu; Hu, Xin-Hua

    2014-01-01

    A quantitative method for measurement of apoptosis in HL-60 cells based on polarization diffraction imaging flow cytometry technique is presented in this paper. Through comparative study with existing methods and the analysis of diffraction images by a gray level co-occurrence matrix algorithm (GLCM), we found 4 GLCM parameters of contrast (CON), cluster shade (CLS), correlation (COR) and dissimilarity (DIS) exhibit high sensitivities as the apoptotic rates. It was further demonstrated that the CLS parameter correlates significantly (R2 = 0.899) with the degree of nuclear fragmentation and other three parameters showed a very good correlations (R2 ranges from 0.69 to 0.90). These results demonstrated that the new method has the capability for rapid and accurate extraction of morphological features to quantify cellular apoptosis without the need for cell staining. PMID:25071957

  19. Covariance of lucky images for increasing objects contrast: diffraction-limited images in ground-based telescopes

    NASA Astrophysics Data System (ADS)

    Cagigal, Manuel P.; Valle, Pedro J.; Colodro-Conde, Carlos; Villó-Pérez, Isidro; Pérez-Garrido, Antonio

    2016-01-01

    Images of stars adopt shapes far from the ideal Airy pattern due to atmospheric density fluctuations. Hence, diffraction-limited images can only be achieved by telescopes without atmospheric influence, e.g. spatial telescopes, or by using techniques like adaptive optics or lucky imaging. In this paper, we propose a new computational technique based on the evaluation of the COvariancE of Lucky Images (COELI). This technique allows us to discover companions to main stars by taking advantage of the atmospheric fluctuations. We describe the algorithm and we carry out a theoretical analysis of the improvement in contrast. We have used images taken with 2.2-m Calar Alto telescope as a test bed for the technique resulting that, under certain conditions, telescope diffraction limit is clearly reached.

  20. Theory for Gaussian beam diffraction in 2D inhomogeneous medium, based on the eikonal form of complex geometrical optics

    NASA Astrophysics Data System (ADS)

    Berczynski, P.; Kravtsov, Yu. A.

    2004-10-01

    A simple and effective method to describe Gaussian beams propagation and diffraction in arbitrary smoothly inhomogeneous 2D medium has been developed based on the eikonal form of complex geometrical optics. The method assumes the eikonal equation can be solved in paraxial approximation in curvilinear frame of references, connected with the central ray. The Riccati-type ordinary differential equation is derived for complex parameter characterizing the Gaussian beam width and phase front curvature. The same parameter was proved to define both the modulus and the argument of the complex amplitude. As a result, the problem of the Gaussian beam diffraction in inhomogeneous media has been reduced to the solution of the ordinary differential equation of the first order, which can be readily calculated numerically for arbitrary profile of dielectric permittivity.

  1. Optical study of a spectrum splitting solar concentrator based on a combination of a diffraction grating and a Fresnel lens

    SciTech Connect

    Michel, Céline Habraken, Serge; Loicq, Jérôme; Thibert, Tanguy

    2015-09-28

    This paper presents recent improvements of our new solar concentrator design for space application. The concentrator is based on a combination of a diffraction grating (blazed or lamellar) coupled with a Fresnel lens. Thanks to this diffractive/refractive combination, this optical element splits spatially and spectrally the light and focus approximately respectively visible light and IR light onto electrically independent specific cells. It avoid the use of MJs cells and then also their limitations like current matching and lattice matching conditions, leading theoretically to a more tolerant system. The concept is reminded, with recent optimizations, ideal and more realistic results, and the description of an experimental realization highlighting the feasibility of the concept and the closeness of theoretical and experimental results.

  2. Polarization-independent light-dispersing device based on diffractive optics

    NASA Astrophysics Data System (ADS)

    Amako, J.; Fujii, E.

    2015-03-01

    We report a light-dispersing device comprised of two transmission gratings and a wave plate. The gratings split the light incident at the Bragg angle into two orthogonally polarized components. The wave plate, which is placed between the gratings, functions as a polarization converter for oblique illumination. Appropriate assembly of these optical parts results in efficient diffraction of the unpolarized light with high spectral resolution. Using coupled-wave theories and Mueller matrix analysis, we constructed a device with a grating period of 400 nm for the spectral range of 680 ± 50 nm. We verified the proposed polarization-independent light-dispersing concept from the evaluation of this device.

  3. Study of an ultrafast analog-to-digital conversion scheme based on diffractive optics.

    PubMed

    Johansson, M; Löfving, B; Hård, S; Thylén, L; Mokhtari, M; Westergren, U; Pala, C

    2000-06-10

    A potentially ultrafast optical analog-to-digital (A/D) converter scheme is proposed and was partly studied experimentally. In the A/D converter scheme the input signal controls the wavelength of a diode laser, whose output beam is incident on a grating. The beam from the grating hits a diffractive optical element in an array. The wavelength determines which element is illuminated. Each element fans out a unique spot-pattern bit code to be read out in parallel by individual detectors. In the experiment all patterns but one from 64 array elements were read out correctly. PMID:18345212

  4. Super-Resolved Digital Holography Based on the Coherent Diffraction Imaging Scheme

    NASA Astrophysics Data System (ADS)

    Wang, Bao-Sheng; Pan, Xing-Chen; Wang, Hai-Yan; Cheng, Jun; Gao, Shu-Mei; Liu, Cheng; Zhu, Jian-Qiang

    2013-05-01

    An algorithm is proposed to enhance the resolution of digital holography by retrieving the frequency components lost in common holograms. A pinhole is placed directly behind the specimen to record the hologram, and an iterative scheme commonly used in coherent diffraction imaging is adopted for the reconstruction. Since some of the frequency components lost in common digital holography can be properly retrieved, the resolution of the reconstructed image is remarkably improved. Theoretical analysis and computer simulations are presented to demonstrate the feasibility of this proposed technique.

  5. Microelectromechanical mirrors and electrically-programmable diffraction gratings based on two-stage actuation

    DOEpatents

    Allen, James J.; Sinclair, Michael B.; Dohner, Jeffrey L.

    2005-11-22

    A microelectromechanical (MEM) device for redirecting incident light is disclosed. The MEM device utilizes a pair of electrostatic actuators formed one above the other from different stacked and interconnected layers of polysilicon to move or tilt an overlying light-reflective plate (i.e. a mirror) to provide a reflected component of the incident light which can be shifted in phase or propagation angle. The MEM device, which utilizes leveraged bending to provide a relatively-large vertical displacement up to several microns for the light-reflective plate, has applications for forming an electrically-programmable diffraction grating (i.e. a polychromator) or a micromirror array.

  6. Iodide Residues in Milk Vary between Iodine-Based Teat Disinfectants.

    PubMed

    French, Elizabeth A; Mukai, Motoko; Zurakowski, Michael; Rauch, Bradley; Gioia, Gloria; Hillebrandt, Joseph R; Henderson, Mark; Schukken, Ynte H; Hemling, Thomas C

    2016-07-01

    Majority of iodine found in dairy milk comes from the diet and teat disinfection products used during milking process. The objective of this study was to evaluate the effects of 4 iodine-based teat dips on milk iodide concentrations varying in iodine level (0.25% vs. 0.5%, w/w), normal low viscosity dip versus barrier dip, and application method (dip vs. spray) to ensure safe iodine levels in dairy milk when these products are used. The iodine exposure study was performed during a 2-wk period. The trial farm was purged of all iodine-based disinfection products for 21 d during a prestudy "washout period," which resulted in baseline milk iodide range of 145 to 182 ppb. During the experiment, iodine-based teat dips were used as post-milking teat disinfectants and compared to a non-iodine control disinfectant. Milk iodide residue levels for each treatment was evaluated from composited group samples. Introduction of different iodine-based teat disinfectants increased iodide residue content in milk relative to the control by between 8 and 29 μg/L when averaged across the full trial period. However, residues levels for any treatment remained well below the consumable limit of 500 μg/L. The 0.5% iodine disinfectant increased milk iodide levels by 20 μg/L more compared to the 0.25% iodine. Compared to dip-cup application, spray application significantly increased milk iodide residue by 21 μg/L and utilized approximately 23% more teat dip. This carefully controlled study demonstrated an increase in milk iodide concentrations from iodine disinfectants, but increases were small and within acceptable limits. PMID:27259164

  7. Visual Analysis of Residuals from Data-Based Models in Complex Industrial Processes

    NASA Astrophysics Data System (ADS)

    Ordoñez, Daniel G.; Cuadrado, Abel A.; Díaz, Ignacio; García, Francisco J.; Díez, Alberto B.; Fuertes, Juan J.

    2012-10-01

    The use of data-based models for visualization purposes in an industrial background is discussed. Results using Self-Organizing Maps (SOM) show how through a good design of the model and a proper visualization of the residuals generated by the model itself, the behavior of essential parameters of the process can be easily tracked in a visual way. Real data from a cold rolling facility have been used to prove the advantages of these techniques.

  8. Capacitive micromachined ultrasonic transducers with diffraction-based integrated optical displacement detection.

    PubMed

    Hall, Neal A; Lee, Wook; Degertekin, F Levent

    2003-11-01

    Capacitive detection limits the performance of capacitive micromachined ultrasonic transducers (CMUTs) by providing poor sensitivity below megahertz frequencies and limiting acoustic power output by imposing constraints on the membrane-substrate gap height. In this paper, an integrated optical interferometric detection method for CMUTs, which provides high displacement sensitivity independent of operation frequency and device capacitance, is reported. The method also enables optoelectronics integration in a small volume and provides optoelectronic isolation between transmit and receive electronics. Implementation of the method involves fabricating CMUTs on transparent substrates and shaping the electrode under each individual CMUT membrane in the form of an optical diffraction grating. Each CMUT membrane thus forms a phase-sensitive optical diffraction grating structure that is used to measure membrane displacements down to 2 x 10(-4) A/square root(Hz) level in the dc to 2-MHz range. Test devices are fabricated on quartz substrates, and ultrasonic array imaging in air is performed using a single 4-mm square CMUT consisting of 19 x 19 array of membranes operating at 750 kHz. PMID:14682641

  9. Colorful holographic display of 3D object based on scaled diffraction by using non-uniform fast Fourier transform

    NASA Astrophysics Data System (ADS)

    Chang, Chenliang; Xia, Jun; Lei, Wei

    2015-03-01

    We proposed a new method to calculate the color computer generated hologram of three-dimensional object in holographic display. The three-dimensional object is composed of several tilted planes which are tilted from the hologram. The diffraction from each tilted plane to the hologram plane is calculated based on the coordinate rotation in Fourier spectrum domains. We used the nonuniform fast Fourier transformation (NUFFT) to calculate the nonuniform sampled Fourier spectrum on the tilted plane after coordinate rotation. By using the NUFFT, the diffraction calculation from tilted plane to the hologram plane with variable sampling rates can be achieved, which overcomes the sampling restriction of FFT in the conventional angular spectrum based method. The holograms of red, green and blue component of the polygon-based object are calculated separately by using our NUFFT based method. Then the color hologram is synthesized by placing the red, green and blue component hologram in sequence. The chromatic aberration caused by the wavelength difference can be solved effectively by restricting the sampling rate of the object in the calculation of each wavelength component. The computer simulation shows the feasibility of our method in calculating the color hologram of polygon-based object. The 3D object can be displayed in color with adjustable size and no chromatic aberration in holographic display system, which can be considered as an important application in the colorful holographic three-dimensional display.

  10. Microstructure-Based Modeling of Residual Stresses in WC-12Co-Sprayed Coatings

    NASA Astrophysics Data System (ADS)

    Klusemann, B.; Denzer, R.; Svendsen, B.

    2012-01-01

    In this study, the residual stresses in a thermal-sprayed tungsten carbide-cobalt coating are numerically investigated after a plasma-spraying process and after a subsequent roller-burnishing process. The results from the simulations are compared to the first experimental results obtained by a classical hole-drilling method. First, effective material parameters are identified by a detailed microstructure FE model based on scanning electron microscope (SEM) images of the coating. Then, two types of simulations are performed with regard to thermally induced residual stresses as well as the rolling process. In the first model, the microstructural details like pores, interface, and surface roughness are modeled in detail based on light microscope (LM) images. In the second model, the coating and substrate are assumed to be ideal homogeneous, and the interface and surface to be as planar. Furthermore, two types of boundary conditions are investigated: (1), the periodic boundary conditions for the left and right faces, and, (2) when these faces are free. It is shown that, for large sample sizes, the results nearly coincide. The simulation results show increasing compressive residual stresses in thickness direction after the rolling process, which is in qualitative agreement with the experiment. A layer of tensile stresses is obtained at the surface in the simulation which could not be captured by the hole-drilling method. Furthermore, an investigation with homogeneous material behavior is performed in 3D.

  11. Highly sensitive homogeneous electrochemical aptasensor for antibiotic residues detection based on dual recycling amplification strategy.

    PubMed

    Wang, Xiuzhong; Dong, Shanshan; Gai, Panpan; Duan, Rui; Li, Feng

    2016-08-15

    The ubiquitous presence of antibiotic residues in foodstuff have serious health consequences for consumers from allergic reactions to the evolution of antibiotic-resistant bacteria. To address this problem, a novel homogeneous electrochemical aptasensor with high sensitivity and specificity is designed for antibiotic residues detection based on target-induced and T7 exonuclease-assisted dual recycling signal amplification strategy. It was realized by the remarkable diffusivity difference between hairpin probe and the mononucleotides towards the negatively charged indium tin oxide electrode. For the proof-of-concept experiment, ampicillin, was employed as a model analyte to examine the desirable properties of this assay. A low detection limit of 4.0pM toward ampicillin with an excellent selectivity could be achieved, which has been successfully applied to assay antibiotic in milk. What's more, compared with the immobilization-based electrochemical means, the proposed sensing system avoids the tedious and time-consuming steps of electrode modification, making the experimental processes much simpler and more convenient. With the advantages of high sensitivity, excellent selectivity and simple operation, it is believed that this strategy possesses great potential for the simple, easy and convenient detection of antibiotic residues in food safety field. PMID:27040941

  12. Generalization of the residual cutting method based on the Krylov subspace

    NASA Astrophysics Data System (ADS)

    Abe, Toshihiko; Sekine, Yoshihito; Kikuchi, Kazuo

    2016-06-01

    The residual cutting (RC) method has been reported to have superior converging characteristics in numerically solving elliptic partial differential equations. However, its application is limited to linear problems with diagonal-dominant matrices in general, for which convergence of a relaxation method such as SOR is guaranteed. In this study, we propose the generalized residual cutting (GRC) method, which is based on the Krylov subspace and applicable to general unsymmetric linear problems. Also, we perform numerical experiments with various coefficient matrices, and show that the GRC method has some desirable properties such as convergence characteristics and memory usage, in comparison to the conventional RC, BiCGSTAB and GMRES methods. At the request of the author of this paper, a corrigendum was issued on 22 June 2016 to correct an error in Eq. (2) and Eq. (3).

  13. Rapid detection of pesticide residue in apple based on Raman spectroscopy

    NASA Astrophysics Data System (ADS)

    Li, Yongyu; Sun, Yunyun; Peng, Yankun; Dhakal, Sagar; Chao, Kuanglin; Liu, Qiaoqiao

    2012-05-01

    The potential of Raman spectroscopy in the analysis of low concentration organic contaminants on apples' surface was evidenced in this study. Chlorpyrifos, an organophosphorus pesticide, was used as a probe for this purpose. The characteristic peaks of fingerprints of pesticide on an aluminum substrate and apple fruit cuticle without pesticide residue were acquired first. Then a concentration range of chlorpyrifos (commercial products at 40%) solutions were made using deionised and distilled water. Single 100 μL droplets of the chlorpyrifos solutions were placed gently on apple fruit cuticles and left to dry before analysis. Through comparative analysis of the Raman spectra data collected, 341, 632 and 1237cm-1 were identified to detect the chlorpyrifos pesticide residue on apple surface. Based on the relationship between the Raman intensity of the most prominent peak at around 632cm-1 and the pesticide concentrations, the limit of detection of ordinary Raman spectrum for chlorpyrifos was estimated to be 48ppm.

  14. Schematic representation of residue-based protein context-dependent data: an application to transmembrane proteins.

    PubMed

    Campagne, F; Weinstein, H

    1999-01-01

    An algorithmic method for drawing residue-based schematic diagrams of proteins on a 2D page is presented and illustrated. The method allows the creation of rendering engines dedicated to a given family of sequences, or fold. The initial implementation provides an engine that can produce a 2D diagram representing secondary structure for any transmembrane protein sequence. We present the details of the strategy for automating the drawing of these diagrams. The most important part of this strategy is the development of an algorithm for laying out residues of a loop that connects to arbitrary points of a 2D plane. As implemented, this algorithm is suitable for real-time modification of the loop layout. This work is of interest for the representation and analysis of data from (1) protein databases, (2) mutagenesis results, or (3) various kinds of protein context-dependent annotations or data. PMID:10736778

  15. Fluorescence volume imaging with an axicon: simulation study based on scalar diffraction method.

    PubMed

    Zheng, Juanjuan; Yang, Yanlong; Lei, Ming; Yao, Baoli; Gao, Peng; Ye, Tong

    2012-10-20

    In a two-photon excitation fluorescence volume imaging (TPFVI) system, an axicon is used to generate a Bessel beam and at the same time to collect the generated fluorescence to achieve large depth of field. A slice-by-slice diffraction propagation model in the frame of the angular spectrum method is proposed to simulate the whole imaging process of TPFVI. The simulation reveals that the Bessel beam can penetrate deep in scattering media due to its self-reconstruction ability. The simulation also demonstrates that TPFVI can image a volume of interest in a single raster scan. Two-photon excitation is crucial to eliminate the signals that are generated by the side lobes of Bessel beams; the unwanted signals may be further suppressed by placing a spatial filter in the front of the detector. The simulation method will guide the system design in improving the performance of a TPFVI system. PMID:23089777

  16. Multiple Plane Phase Retrieval Based On Inverse Regularized Imaging and Discrete Diffraction Transform

    NASA Astrophysics Data System (ADS)

    Migukin, Artem; Katkovnik, Vladimir; Astola, Jaakko

    2010-04-01

    The phase retrieval is formulated as an inverse problem, where the forward propagation is defined by Discrete Diffraction Transform (DDT) [1], [2]. This propagation model is precise and aliasing free for pixelwise invariant (pixelated) wave field distributions in the sensor and object planes. Because of finite size of sensors DDT can be ill-conditioned and the regularization is an important component of the inverse. The proposed algorithm is designed for multiple plane observations and can be treated as a generalization of the Gerchberg-Saxton iterative algorithm. The proposed algorithm is studied by numerical experiments produced for phase and amplitude modulated object distributions. Comparison versus the conventional forward propagation models such as the angular spectrum decomposition and the convolutional model used in the algorithm of the same structure shows a clear advantage of DDT enabling better accuracy and better imaging.

  17. Fatigue reliability based on residual strength model with hybrid uncertain parameters

    NASA Astrophysics Data System (ADS)

    Wang, Jun; Qiu, Zhi-Ping

    2012-02-01

    The aim of this paper is to evaluate the fatigue reliability with hybrid uncertain parameters based on a residual strength model. By solving the non-probabilistic set-based reliability problem and analyzing the reliability with randomness, the fatigue reliability with hybrid parameters can be obtained. The presented hybrid model can adequately consider all uncertainties affecting the fatigue reliability with hybrid uncertain parameters. A comparison among the presented hybrid model, non-probabilistic set-theoretic model and the conventional random model is made through two typical numerical examples. The results show that the presented hybrid model, which can ensure structural security, is effective and practical.

  18. Formulation and characterization of functional foods based on fruit and vegetable residue flour.

    PubMed

    Ferreira, Mariana S L; Santos, Mônica C P; Moro, Thaísa M A; Basto, Gabriela J; Andrade, Roberta M S; Gonçalves, Édira C B A

    2015-02-01

    Fruits and vegetables are extensively processed and the residues are often discarded. However, due to their rich composition, they could be used to minimize food waste. This study aimed to develop food products based on the solid residue generated from the manufacture of an isotonic beverage. This beverage was produced based on integral exploitation of several fruits and vegetables: orange, passion fruit, watermelon, lettuce, courgette, carrot, spinach, mint, taro, cucumber and rocket. The remaining residue was processed into flour and its functional properties were evaluated. The fruit and vegetable residue (FVR) flour was incorporated with different levels (20 to 35 %) into biscuits and cereal bars. The proximate composition, microbiological stability until 90 days and consumer acceptance were analyzed. The FVR flour presented a higher water holding capacity than oil holding capacity, respectively 7.43 and 1.91 g g(-1) of flour, probably associated with its high levels of carbohydrates (53 %) and fibres (21.5 %). Biscuits enriched with 35 % of FVR flour presented significantly higher fibre, ranging from 57 % to 118 % and mineral contents, from 25 % to 37 % than when only 20 % was added. Cereal bars presented about 75 % of fibres and variable mineral contents between 14 % and 37 %. The incorporation of FVR did not change the fat content. The microbiological examinations are within acceptable limits according to international regulation. The incorporation of FVR flour did not impair consumer acceptance, the sensory attributes averaged around 6. The chemical, microbiological and sensorial results of the designed products attested for an alternative towards applying and reducing agro-industrial wastes. PMID:25694690

  19. Release time of residual oxygen after dental bleaching with 35% hydrogen peroxide: effect of a catalase-based neutralizing agent.

    PubMed

    Guasso, Bárbara; Salomone, Paloma; Nascimento, Paulo Cícero; Pozzobon, Roselaine Terezinha

    2016-01-01

    This article assessed the effect of a catalase-based agent on residual oxygen (O2) release from teeth exposed to 35% hydrogen peroxide (H2O2). The use of the catalase-based neutralizer agent for 2-3 minutes was able to release residual O2 5 days after exposure to a 35% H2O2-based bleaching gel. PMID:27148658

  20. Optical pressure sensor based on the combined system of a variable liquid lens and a point diffraction interferometer

    NASA Astrophysics Data System (ADS)

    García-Arellano, Anmi; Gómez-García, Manuel; Acosta, Eva

    2011-09-01

    In this work we present an experimental proposal for an efficient optical pressure sensor based on a Variable Liquid Lens (VLL) and a modified Point Diffraction Interferometer (PDI). The working principle of the proposed sensor relies on the fact that a pressure variation induces a change in the lens curvature and hence in its focal length which can be tracked and measured with the interferometer. The pressure is then measured by recording and processing the interferometric images. The calibration of the sensor in this proposal demonstrated a working range of 0-26 kPa with an accuracy of less than 0.1 kPa in the whole range.

  1. Exploring hardness enhancement in superhard tungsten tetraboride-based solid solutions using radial X-ray diffraction

    SciTech Connect

    Xie, Miao; Turner, Christopher L.; Mohammadi, Reza; Kaner, Richard B. E-mail: akavner@ucla.edu Tolbert, Sarah H. E-mail: akavner@ucla.edu; Kavner, Abby E-mail: akavner@ucla.edu

    2015-07-27

    In this work, we explore the hardening mechanisms in WB{sub 4}-based solid solutions upon addition of Ta, Mn, and Cr using in situ radial X-ray diffraction techniques under non-hydrostatic pressure. By examining the lattice-supported differential strain, we provide insights into the mechanism for hardness increase in binary solid solutions at low dopant concentrations. Speculations on the combined effects of electronic structure and atomic size in ternary WB{sub 4} solid solutions containing Ta with Mn or Cr are also included to understand the extremely high hardness of these materials.

  2. Determination of liquid's molecular interference function based on X-ray diffraction and dual-energy CT in security screening.

    PubMed

    Zhang, Li; YangDai, Tianyi

    2016-08-01

    A method for deriving the molecular interference function (MIF) of an unknown liquid for security screening is presented. Based on the effective atomic number reconstructed from dual-energy computed tomography (CT), equivalent molecular formula of the liquid is estimated. After a series of optimizations, the MIF and a new effective atomic number are finally obtained from the X-ray diffraction (XRD) profile. The proposed method generates more accurate results with less sensitivity to the noise and data deficiency of the XRD profile. PMID:27239986

  3. Preparation of Compact Agarose Cell Blocks from the Residues of Liquid-Based Cytology Samples

    PubMed Central

    Choi, Suk Jin; Choi, Yeon Il; Kim, Lucia; Park, In Suh; Han, Jee Young; Kim, Joon Mee; Chu, Young Chae

    2014-01-01

    Background Inevitable loss of diagnostic material should be minimized during cell block preparation. We introduce a modified agarose cell block technique that enables the synthesis of compact cell blocks by using the entirety of a cell pellet without the loss of diagnostic material during cell block preparations. The feasibility of this technique is illustrated by high-throughput immunocytochemistry using high-density cell block microarray (CMA). Methods The cell pellets of Sure- Path residues were pre-embedded in ultra-low gelling temperature agarose gel and re-embedded in standard agarose gel. They were fixed, processed, and embedded in paraffin using the same method as tissue sample processing. The resulting agarose cell blocks were trimmed and represented on a CMA for high-throughput analysis using immunocytochemical staining. Results The SurePath residues were effectively and entirely incorporated into compact agarose cell buttons and embedded in paraffin. Sections of the agarose cell blocks revealed cellularities that correlated well with corresponding SurePath smears and had immunocytochemical features that were sufficient for diagnosis of difficult cases. Conclusions This agarose-based compact cell block technique enables preparation of high-quality cell blocks by using up the residual SurePath samples without loss of diagnostic material during cell block preparation. PMID:25366070

  4. A C. elegans-based foam for rapid on-site detection of residual live virus.

    SciTech Connect

    Negrete, Oscar A.; Branda, Catherine; Hardesty, Jasper O. E.; Tucker, Mark David; Kaiser, Julia N.; Kozina, Carol L.; Chirica, Gabriela S.

    2012-02-01

    In the response to and recovery from a critical homeland security event involving deliberate or accidental release of biological agents, initial decontamination efforts are necessarily followed by tests for the presence of residual live virus or bacteria. Such 'clearance sampling' should be rapid and accurate, to inform decision makers as they take appropriate action to ensure the safety of the public and of operational personnel. However, the current protocol for clearance sampling is extremely time-intensive and costly, and requires significant amounts of laboratory space and capacity. Detection of residual live virus is particularly problematic and time-consuming, as it requires evaluation of replication potential within a eukaryotic host such as chicken embryos. The intention of this project was to develop a new method for clearance sampling, by leveraging Sandia's expertise in the biological and material sciences in order to create a C. elegans-based foam that could be applied directly to the entire contaminated area for quick and accurate detection of any and all residual live virus by means of a fluorescent signal. Such a novel technology for rapid, on-site detection of live virus would greatly interest the DHS, DoD, and EPA, and hold broad commercial potential, especially with regard to the transportation industry.

  5. Measurement of yarn twist based on backward light scattering and small-angle far-field diffraction

    NASA Astrophysics Data System (ADS)

    Pei, Z. G.; Tao, X. M.

    2015-12-01

    This paper presents a non-destructive, non-contact method for measuring the twist of a yarn based on light scattering and diffraction. The surface twist angle is measured by determining the direction of the line with the highest intensity on the backward light scattering pattern which is perpendicular to the surface fibers, which is verified by both theoretical analysis based on Beckmann’s scattering model and experiments. The yarn diameter is measured with good accuracy by using the small-angle far-field diffraction pattern of the yarn body. Yarn twist is then derived from the measured surface twist angle and yarn diameter. Further studies reveal that the measured yarn twists by the proposed method are comparable to those measured based on microscopic images of the yarn. This method requires no high-magnification optics and is able to pick up short-term variations of twist with less labor intensity, indicating its potential application in the on-line measuring of yarn twist and its distribution.

  6. DDT-based indoor residual spraying suboptimal for visceral leishmaniasis elimination in India

    PubMed Central

    Coleman, Michael; Foster, Geraldine M.; Deb, Rinki; Pratap Singh, Rudra; Ismail, Hanafy M.; Shivam, Pushkar; Ghosh, Ayan Kumar; Dunkley, Sophie; Kumar, Vijay; Coleman, Marlize; Hemingway, Janet; Paine, Mark J. I.; Das, Pradeep

    2015-01-01

    Indoor residual spraying (IRS) is used to control visceral leishmaniasis (VL) in India, but it is poorly quality assured. Quality assurance was performed in eight VL endemic districts in Bihar State, India, in 2014. Residual dichlorodiphenyltrichloroethane (DDT) was sampled from walls using Bostik tape discs, and DDT concentrations [grams of active ingredient per square meter (g ai/m2)] were determined using HPLC. Pre-IRS surveys were performed in three districts, and post-IRS surveys were performed in eight districts. A 20% threshold above and below the target spray of 1.0 g ai/m2 was defined as “in range.” The entomological assessments were made in four districts in IRS and non-IRS villages. Vector densities were measured: pre-IRS and 1 and 3 mo post-IRS. Insecticide susceptibility to 4% DDT and 0.05% deltamethrin WHO-impregnated papers was determined with wild-caught sand flies. The majority (329 of 360, 91.3%) of pre-IRS samples had residual DDT concentrations of <0.1 g ai/m2. The mean residual concentration of DDT post-IRS was 0.37 g ai/m2; 84.9% of walls were undersprayed, 7.4% were sprayed in range, and 7.6% were oversprayed. The abundance of sand flies in IRS and non-IRS villages was significantly different at 1 mo post-IRS only. Sand flies were highly resistant to DDT but susceptible to deltamethrin. The Stockholm Convention, ratified by India in 2006, calls for the complete phasing out of DDT as soon as practical, with limited use in the interim where no viable IRS alternatives exist. Given the poor quality of the DDT-based IRS, ready availability of pyrethroids, and susceptibility profile of Indian sand flies, the continued use of DDT in this IRS program is questionable. PMID:26124110

  7. Development and application of recombinant antibody-based immunoassays to tetraconazole residue analysis in fruit juices.

    PubMed

    Plana, Emma; Moreno, Maria-José; Montoya, Ángel; Manclús, Juan J

    2014-01-15

    Tetraconazole is currently used as a fungicide in fruit and vegetables. The aim of this work was the development of immunochemical techniques based on recombinant antibodies for the screening of tetraconazole residues in fruit juices. Recombinant antibodies were produced from a hybridoma cell line secreting a monoclonal antibody specific for tetraconazole and from lymphocytes of mice hyperimmunised with tetraconazole haptens conjugated to bovine serum albumin. From these antibodies, enzyme-linked immunosorbent assays in the conjugate-coated format were developed, which were able to detect tetraconazole standards down to 1ng/mL. From recovery studies with spiked samples, these immunoassays determined tetraconazole in orange and apple juices with acceptable reproducibility (coefficients of variation below 25%) and recoveries (ranging from 78% to 145%) for a screening technique. The analytical performance of RAb-based immunoassays was fairly similar to that of the MAb-based immunoassays. Due to their simplicity and high sample throughput, the developed recombinant-based immunoassays can be valuable analytical tools for the screening of tetraconazole residues in fruit juices at regulatory levels. PMID:24054232

  8. Diffraction-based sensitivity analysis for an external occulter laboratory demonstration.

    PubMed

    Sirbu, Dan; Kim, Yunjong; Jeremy Kasdin, N; Vanderbei, Robert J

    2016-08-01

    An external flower-shaped occulter flying in formation with a space telescope can theoretically provide sufficient starlight suppression to enable direct imaging of an Earth-like planet. Occulter shapes are scaled to enable experimental validation of their performance at laboratory dimensions. Previous experimental results have shown promising performance but have not realized the full theoretical potential of occulter designs. Here, we develop a two-dimensional diffraction model for optical propagations for occulters incorporating experimental errors. We perform a sensitivity analysis, and comparison with experimental results from a scaled-occulter testbed validates the optical model to the 10-10 contrast level. The manufacturing accuracy along the edge of the occulter shape is identified as the limiting factor to achieving the theoretical potential of the occulter design. This hypothesis is experimentally validated using a second occulter mask manufactured with increased edge feature accuracy and resulting in a measured contrast level approaching the 10-12 level-a better than one order of magnitude improvement in performance. PMID:27505392

  9. Determining the Structure of Biomaterials Interfaces using Synchrotron-based X-ray Diffraction

    SciTech Connect

    McBride, M

    2002-01-24

    The purpose of this project is to explore the feasibility of using surface X-ray diffraction (SXRD) to determine the structure of biomineral surfaces in electrolyte solutions and of the adsorbed layer of acidic amino acids that are believed to play a central role in the control of biomineral formation and function. The work is a critical component in the development of an integrated picture of the physical and chemical basis for deposition and dissolution at solid-liquid interfaces in biological systems, and brings a new and very powerful surface-sensitive capability to LLNL. We have chosen as our model systems calcium carbonate and calcium phosphate in aspartic and glutamic acid-bearing solutions. The calcium compounds are ubiquitous among biomineral structures, both those that are beneficial such as bones and teeth, and those that are pathological such as kidney stones, while the two acidic amino acids--both as simple and poly-amino acids--are the dominant constituents of protein mixtures implicated in the control of biomineralization. The goals of the work are: (1) to determine the surface structure of pure calcium phosphate and calcium carbonate surfaces in aqueous solution using SXRD; (2) to determine how those surfaces are modified by the presence of aspartic and glutamic acid, both as the simple amino acids and as poly-aspartate and poly-glutamate and (3) to model the interactions of acidic amino acids with calcite.

  10. Gunshot residue particles formed by using ammunitions that have mercury fulminate based primers.

    PubMed

    Zeichner, A; Levin, N; Dvorachek, M

    1992-11-01

    Ammunition having mercury fulminate-based primers are commonly manufactured by Eastern Bloc countries and used extensively in the Middle East. Gunshot residue (GSR) particles formed by firing these types of ammunition were examined. It was observed that much lower percentage of mercury-containing GSR particles were found in samples taken from a shooter as compared to the percentage of such particles in samples from cartridge cases. This fact must therefore be taken into account when interpreting case results. A plausible explanation for the results described is proposed. PMID:1453170