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Sample records for fiber-reinforced bismaleimide materials

  1. Application of fiber-reinforced bismaleimide materials to aircraft nacelle structures

    NASA Technical Reports Server (NTRS)

    Peros, Vasilios; Ruth, John; Trawinski, David

    1992-01-01

    Existing aircraft engine nacelle structures employ advanced composite materials to reduce weight and thereby increase overall performance. Use of advanced composite materials on existing aircraft nacelle structures includes fiber-reinforced epoxy structures and has typically been limited to regions furthest away from the hot engine core. Portions of the nacelle structure that are closer to the engine require materials with a higher temperature capability. In these portions, existing nacelle structures employ aluminum sandwich construction and skin/stringer construction. The aluminum structure is composed of many detail parts and assemblies and is usually protected by some form of ablative, insulator, or metallic thermal shield. A one-piece composite inner cowl for a new-generation engine nacelle structure has been designed using fiber-reinforced bismaleimide (BMI) materials and honeycomb core in a sandwich construction. The new composite design has many advantages over the existing aluminum structure. Multiple details were integrated into the one-piece composite design, thereby significantly reducing the number of detail parts and fasteners. The use of lightweight materials and the reduction of the number of joints result in a significant weight reduction over the aluminum design; manufacturing labor and the overall number of tools required have also been reduced. Several significant technical issues were addressed in the development of a BMI composite design. Technical evaluation of the available BMI systems led to the selection of a toughened BMI material which was resistant to microcracking under thermal cyclic loading and enhanced the damage tolerance of the structure. Technical evaluation of the degradation of BMI materials in contact with aluminum and other metals validated methods for isolation of the various materials. Graphite-reinforced BMI in contact with aluminum and some steels was found to degrade in salt spray testing. Isolation techniques such as

  2. Neutron imaging of fiber-reinforced materials

    NASA Astrophysics Data System (ADS)

    Bastürk, M.; Kardjilov, N.; Rauch, H.; Vontobel, P.

    2005-04-01

    Glass-fiber-reinforced plastic laminates used for the insulation of Toroidal Field (TF) magnet-coils and fiber-reinforced silicon carbide ceramic composites used as structural material for the self-cooled Pb-17Li blanket module are attractive candidate materials for fusion reactors because of their high performance under extreme conditions. Porosity, which depends on the manufacturing process, and swelling of fiber-reinforced materials due to the high flux of radiation are the main problems. The aim of this study is to describe the experimental procedures of different imaging methods, and also to decide the most efficient imaging method for the investigations of the complex microstructure of fiber-reinforced materials. In this work, the fiber-reinforced composites were inspected with neutron and X-ray radiographies at ATI-Vienna and also at PSI-Villigen. A contrast enhancement at the edges can be achieved by means of phase contrast neutron radiography (NR), which is based on the wave properties of neutrons and arises from the neutron refraction (rather than attenuation). Elements having different refractive index within a sample cause a phase shift between coherent neutron waves. The degree of coherence can be determined by means of the coherence pattern caused by the sample, when a point source (pinhole) is used and the distance between source and sample is varied.

  3. Fatigue of continuous fiber reinforced metallic materials

    NASA Technical Reports Server (NTRS)

    Johnson, W. S.; Mirdamadi, M.; Bakuckas, J. G., Jr.

    1993-01-01

    The complex damage mechanisms that occur in fiber reinforced advanced metallic materials are discussed. As examples, results for several layups of SCS-6/Ti-15-3 composites are presented. Fatigue tests were conducted and analyzed for both notched and unnotched specimens at room and elevated temperatures. Test conditions included isothermal, non-isothermal, and simulated mission profile thermomechanical fatigue. Test results indicated that the stress in the 0 degree fibers is the controlling factor for fatigue life for a given test condition. An effective strain approach is presented for predicting crack initiation at notches. Fiber bridging models were applied to crack growth behavior.

  4. Method of preparing fiber reinforced ceramic material

    NASA Technical Reports Server (NTRS)

    Bhatt, Ramakrishna T. (Inventor)

    1987-01-01

    Alternate layers of mats of specially coated SiC fibers and silicon monotapes are hot pressed in two stages to form a fiber reinforced ceramic material. In the first stage a die is heated to about 600 C in a vacuum furnace and maintained at this temperature for about one-half hour to remove fugitive binder. In the second stage the die temperature is raised to about 1000 C and the layers are pressed at between 35 and 138 MPa. The resulting preform is placed in a reactor tube where a nitriding gas is flowed past the preform at 1100 to 1400 C to nitride the same.

  5. Tuning the mechanical properties of glass fiber-reinforced bismaleimide-triazine resin composites by constructing a flexible bridge at the interface

    NASA Astrophysics Data System (ADS)

    Zeng, Xiaoliang; Yu, Shuhui; Lai, Maobai; Sun, Rong; Wong, Ching-Ping

    2013-12-01

    We demonstrate a new method that can simultaneously improve the strength and toughness of the glass fiber-reinforced bismaleimide-triazine (BT) resin composites by using polyethylene glycol (PEG) to construct a flexible bridge at the interface. The mechanical properties, including the elongation, ultimate tensile stress, Young's modulus, toughness and dynamical mechanical properties were studied as a function of the length of PEG molecular chain. It was found that the PEG molecule acts as a bridge to link BT resin and glass fiber through covalent and non-covalent bondings, respectively, resulting in improved interfacial bonding. The incorporation of PEG produces an increase in elongation, ultimate tensile stress and toughness. The Young's modulus and Tg were slightly reduced when the length of the PEG molecular chain was high. The elongation of the PEG-modified glass fiber-reinforced composites containing 5 wt% PEG-8000 increased by 67.1%, the ultimate tensile stress by 17.9% and the toughness by 78.2% compared to the unmodified one. This approach provides an efficient way to develop substrate material with improved strength and toughness for integrated circuit packaging applications.

  6. Material Properties for Fiber-Reinforced Silica Aerogels

    NASA Technical Reports Server (NTRS)

    White, Susan; Rouanet, Stephane; Moses, John; Arnold, James O. (Technical Monitor)

    1994-01-01

    Ceramic fiber-reinforced silica aerogels are novel materials for high performance insulation, including thermal protection materials. Experimental data are presented for the thermal and mechanical properties, showing the trends exhibited over a range of fiber loadings and silica aerogel densities. Test results are compared to that of unreinforced bulk aerogels.

  7. NDE Elastic Properties of Fiber-Reinforced Composite Materials

    NASA Technical Reports Server (NTRS)

    Bar-Cohen, Y.

    1995-01-01

    Fiber-reinforced composites are increasingly replacing metallic alloys as structural materials for primary components of fracture-critical structures. This trend is a result of the growing understanding of material behavior and recognition of the desirable properties of composites. A research program was conducted on NDE methods for determining the elastic properties of composites.

  8. Automobile materials competition: energy implications of fiber-reinforced plastics

    SciTech Connect

    Cummings-Saxton, J.

    1981-10-01

    The embodied energy, structural weight, and transportation energy (fuel requirement) characteristics of steel, fiber-reinforced plastics, and aluminum were assessed to determine the overall energy savings of materials substitution in automobiles. In body panels, a 1.0-lb steel component with an associated 0.5 lb in secondary weight is structurally equivalent to a 0.6-lb fiber-reinforced plastic component with 0.3 lb in associated secondary weight or a 0.5-lb aluminum component with 0.25 lb of secondary weight. (Secondary weight refers to the combined weight of the vehicle's support structure, engine, braking system, and drive train, all of which can be reduced in response to a decrease in total vehicle weight.) The life cycle transportation energy requirements of structurally equivalent body panels (including their associated secondary weights) are 174.4 x 10/sup 3/ Btu for steel, 104.6 x 10/sup 3/ Btu for fiber-reinforced plastics, and 87.2 x 10/sup 3/ Btu for aluminum. The embodied energy requirements are 37.2 x 10/sup 3/ Btu for steel, 22.1 x 10/sup 3/ Btu for fiber-reinforced plastics, and 87.1 x 10/sup 3/ Btu for aluminum. These results can be combined to yield total energy requirements of 211.6 x 10/sup 3/ Btu for steel, 126.7 x 10/sup 3/ Btu for fiber-reinforced plastics, and 174.3 x 10/sup 3/ Btu for aluminum. Fiber-reinforced plastics offer the greatest improvements over steel in both embodied and total energy requirements. Aluminum achieves the greatest savings in transportation energy.

  9. Basalt fiber reinforced porous aggregates-geopolymer based cellular material

    NASA Astrophysics Data System (ADS)

    Luo, Xin; Xu, Jin-Yu; Li, Weimin

    2015-09-01

    Basalt fiber reinforced porous aggregates-geopolymer based cellular material (BFRPGCM) was prepared. The stress-strain curve has been worked out. The ideal energy-absorbing efficiency has been analyzed and the application prospect has been explored. The results show the following: fiber reinforced cellular material has successively sized pore structures; the stress-strain curve has two stages: elastic stage and yielding plateau stage; the greatest value of the ideal energy-absorbing efficiency of BFRPGCM is 89.11%, which suggests BFRPGCM has excellent energy-absorbing property. Thus, it can be seen that BFRPGCM is easy and simple to make, has high plasticity, low density and excellent energy-absorbing features. So, BFRPGCM is a promising energy-absorbing material used especially in civil defense engineering.

  10. Fiber Reinforced Composite Materials Used for Tankage

    NASA Technical Reports Server (NTRS)

    Cunningham, Christy

    2005-01-01

    The Nonmetallic Materials and Processes Group is presently working on several projects to optimize cost while providing effect materials for the space program. One factor that must be considered is that these materials must meet certain weight requirements. Composites contribute greatly to this effort. Through the use of composites the cost of launching payloads into orbit will be reduced to one-tenth of the current cost. This research project involved composites used for aluminum pressure vessels. These tanks are used to store cryogenic liquids during flight. The tanks need some type of reinforcement. Steel was considered, but added too much weight. As a result, fiber was chosen. Presently, only carbon fibers with epoxy resin are wrapped around the vessels as a primary source of reinforcement. Carbon fibers are lightweight, yet high strength. The carbon fibers are wet wound onto the pressure vessels. This was done using the ENTEC Filament Winding Machine. It was thought that an additional layer of fiber would aid in reinforcement as well as containment and impact reduction. Kevlar was selected because it is light weight, but five times stronger that steel. This is the same fiber that is used to make bullet-proof vests trampolines, and tennis rackets.

  11. Process simulation for the compression moulding of fiber reinforced materials

    SciTech Connect

    Michaeli, W.; Goedel, M.; Heber, M.

    1994-12-31

    This paper will give a short overview about the activities of the compression moulding simulation for GMTs and SMCs. The simulation of the compression moulding process avoids the prototyping of new moulds for optimizing the process itself. That helps saving time and money. In compression moulding, a distinction is drawn between the more widespread ``Sheet Moulding Compound`` (SMC) and ``Glass Mat reinforced Thermoplastics`` (GMT). SMC is a glass fiber reinforced thermoset, while GMT has a thermoplastic matrix which is generally polypropylene. Both materials contain fibers with a fiber length of 12 to 25 mm. The fibers are not joined together in form of a fabric.

  12. Natural Kenaf Fiber Reinforced Composites as Engineered Structural Materials

    NASA Astrophysics Data System (ADS)

    Dittenber, David B.

    The objective of this work was to provide a comprehensive evaluation of natural fiber reinforced polymer (NFRP)'s ability to act as a structural material. As a chemical treatment, aligned kenaf fibers were treated with sodium hydroxide (alkalization) in different concentrations and durations and then manufactured into kenaf fiber / vinyl ester composite plates. Single fiber tensile properties and composite flexural properties, both in dry and saturated environments, were assessed. Based on ASTM standard testing, a comparison of flexural, tensile, compressive, and shear mechanical properties was also made between an untreated kenaf fiber reinforced composite, a chemically treated kenaf fiber reinforced composite, a glass fiber reinforced composite, and oriented strand board (OSB). The mechanical properties were evaluated for dry samples, samples immersed in water for 50 hours, and samples immersed in water until saturation (~2700 hours). Since NFRPs are more vulnerable to environmental effects than synthetic fiber composites, a series of weathering and environmental tests were conducted on the kenaf fiber composites. The environmental conditions studied include real-time outdoor weathering, elevated temperatures, immersion in different pH solutions, and UV exposure. In all of these tests, degradation was found to be more pronounced in the NFRPs than in the glass FRPs; however, in nearly every case the degradation was less than 50% of the flexural strength or stiffness. Using a method of overlapping and meshing discontinuous fiber ends, large mats of fiber bundles were manufactured into composite facesheets for structural insulated panels (SIPs). The polyisocyanurate foam cores proved to be poorly matched to the strength and stiffness of the NFRP facesheets, leading to premature core shear or delamination failures in both flexure and compressive testing. The NFRPs were found to match well with the theoretical stiffness prediction methods of classical lamination

  13. Composite structural materials. [fiber reinforced composites for aircraft structures

    NASA Technical Reports Server (NTRS)

    Ansell, G. S.; Loewy, R. G.; Wiberly, S. E.

    1981-01-01

    Physical properties of fiber reinforced composites; structural concepts and analysis; manufacturing; reliability; and life prediction are subjects of research conducted to determine the long term integrity of composite aircraft structures under conditions pertinent to service use. Progress is reported in (1) characterizing homogeneity in composite materials; (2) developing methods for analyzing composite materials; (3) studying fatigue in composite materials; (4) determining the temperature and moisture effects on the mechanical properties of laminates; (5) numerically analyzing moisture effects; (6) numerically analyzing the micromechanics of composite fracture; (7) constructing the 727 elevator attachment rib; (8) developing the L-1011 engine drag strut (CAPCOMP 2 program); (9) analyzing mechanical joints in composites; (10) developing computer software; and (11) processing science and technology, with emphasis on the sailplane project.

  14. Corrosion and tribological properties of basalt fiber reinforced composite materials

    NASA Astrophysics Data System (ADS)

    Ha, Jin Cheol; Kim, Yun-Hae; Lee, Myeong-Hoon; Moon, Kyung-Man; Park, Se-Ho

    2015-03-01

    This experiment has examined the corrosion and tribological properties of basalt fiber reinforced composite materials. There were slight changes of weight after the occurring of corrosion based on time and H2SO4 concentration, but in general, the weight increased. It is assumed that this happens due to the basalt fiber precipitate. Prior to the corrosion, friction-wear behavior showed irregular patterns compared to metallic materials, and when it was compared with the behavior after the corrosion, the coefficient of friction was 2 to 3 times greater. The coefficient of friction of all test specimen ranged from 0.1 to 0.2. Such a result has proven that the basalt fiber, similar to the resin rubber, shows regular patterns regardless of time and H2SO4 concentration because of the space made between resins and reinforced materials.

  15. The Application of Fiber-Reinforced Materials in Disc Repair

    PubMed Central

    Pei, Bao-Qing; Li, Hui; Zhu, Gang; Li, De-Yu; Fan, Yu-Bo; Wu, Shu-Qin

    2013-01-01

    The intervertebral disc degeneration and injury are the most common spinal diseases with tremendous financial and social implications. Regenerative therapies for disc repair are promising treatments. Fiber-reinforced materials (FRMs) are a kind of composites by embedding the fibers into the matrix materials. FRMs can maintain the original properties of the matrix and enhance the mechanical properties. By now, there are still some problems for disc repair such as the unsatisfied static strength and dynamic properties for disc implants. The application of FRMs may resolve these problems to some extent. In this review, six parts such as background of FRMs in tissue repair, the comparison of mechanical properties between natural disc and some typical FRMs, the repair standard and FRMs applications in disc repair, and the possible research directions for FRMs' in the future are stated. PMID:24383057

  16. MULTIPHASE MATERIAL OPTIMIZATION FOR FIBER REINFORCED COMPOSITES CONSIDERING STRAIN SOFTENING

    NASA Astrophysics Data System (ADS)

    Kato, Junji; Ramm, Ekkehard; Terada, Kenjiro; Kyoya, Takashi

    The present paper addresses an optimization strategy of textile fiber reinforced concrete (FRC) with emphasis on its special failure behavior. Since both concrete and fiber are brittle materials, a prominent objective for FRC structures is concerned with the improvement of structural ductility, which may be defined as energy absorption capacity. Despite above unfavorable characteristics, the interface between fiber and matrix plays a substantial role in the structural response. This favorable 'composite effect' is related to material parameters involved in the interface and the material layout on the small scale level. Therefore the purpose of the present paper is to improve the structural ductility of FRC at the macroscopic level applying an optimization method with respect to significant material parameters at the small scale level. The method discussed is based on multiphase material optimization. This methodology is extended to a damage formulation. The performance of the proposed method is demonstrated in a series of numerical examples; it is verified that the structural ductility can be considerably improved.

  17. Mixture for producing fracture-resistant, fiber-reinforced ceramic material by microwave heating

    DOEpatents

    Meek, T.T.; Blake, R.D.

    1985-04-03

    A fracture-resistant, fiber-reinforced ceramic substrate is produced by a method which involves preparing a ceramic precursor mixture comprising glass material, a coupling agent, and resilient fibers, and then exposing the mixture to microwave energy. The microwave field orients the fibers in the resulting ceramic material in a desired pattern wherein heat later generated in or on the substrate can be dissipated in a desired geometric pattern parallel to the fiber pattern. Additionally, the shunt capacitance of the fracture-resistant, fiber-reinforced ceramic substrate is lower which provides for a quicker transit time for electronic pulses in any conducting pathway etched into the ceramic substrate.

  18. Mixture for producing fracture-resistant, fiber-reinforced ceramic material by microwave heating

    DOEpatents

    Meek, T.T.; Blake, R.D.

    1987-09-22

    A fracture-resistant, fiber-reinforced ceramic substrate is produced by a method which involves preparing a ceramic precursor mixture comprising glass material, a coupling agent, and resilient fibers, and then exposing the mixture to microwave energy. The microwave field orients the fibers in the resulting ceramic material in a desired pattern wherein heat later generated in or on the substrate can be dissipated in a desired geometric pattern parallel to the fiber pattern. Additionally, the shunt capacitance of the fracture-resistant, fiber-reinforced ceramic substrate is lower which provides for a quicker transit time for electronic pulses in any conducting pathway etched into the ceramic substrate. 2 figs.

  19. Mixture for producing fracture-resistant, fiber-reinforced ceramic material by microwave heating

    DOEpatents

    Meek, Thomas T.; Blake, Rodger D.

    1987-01-01

    A fracture-resistant, fiber-reinforced ceramic substrate is produced by a method which involves preparing a ceramic precursor mixture comprising glass material, a coupling agent, and resilient fibers, and then exposing the mixture to microwave energy. The microwave field orients the fibers in the resulting ceramic material in a desired pattern wherein heat later generated in or on the substrate can be dissipated in a desired geometric pattern parallel to the fiber pattern. Additionally, the shunt capacitance of the fracture-resistant, fiber-reinforced ceramic substrate is lower which provides for a quicker transit time for electronic pulses in any conducting pathway etched into the ceramic substrate.

  20. MATERIAL SHAPE OPTIMIZATION FOR FIBER REINFORCED COMPOSITES APPLYING A DAMAGE FORMULATION

    NASA Astrophysics Data System (ADS)

    Kato, Junji; Ramm, Ekkehard; Terada, Kenjiro; Kyoya, Takashi

    The present contribution deals with an optimization strategy of fiber reinforced composites. Although the methodical concept is very general we concentrate on Fiber Reinforced Concrete with a complex failure mechanism resulting from material brittleness of both constituents matrix and fibers. The purpose of the present paper is to improve the structural ductility of the fiber reinforced composites applying an optimization method with respect to the geometrical layout of continuous long textile fibers. The method proposed is achieved by applying a so-called embedded reinforcement formulation. This methodology is extended to a damage formulation in order to represent a realistic structural behavior. For the optimization problem a gradient-based optimization scheme is assumed. An optimality criteria method is applied because of its numerically high efficiency and robustness. The performance of the method is demonstrated by a series of numerical examples; it is verified that the ductility can be substantially improved.

  1. Micromechanical model of crack growth in fiber reinforced brittle materials

    NASA Technical Reports Server (NTRS)

    Rubinstein, Asher A.; Xu, Kang

    1990-01-01

    A model based on the micromechanical mechanism of crack growth resistance in fiber reinforced ceramics is presented. The formulation of the model is based on a small scale geometry of a macrocrack with a bridging zone, the process zone, which governs the resistance mechanism. The effect of high toughness of the fibers in retardation of the crack advance, and the significance of the fiber pullout mechanism on the crack growth resistance, are reflected in this model. The model allows one to address issues such as influence of fiber spacing, fiber flexibility, and fiber matrix friction. Two approaches were used. One represents the fracture initiation and concentrated on the development of the first microcracks between fibers. An exact closed form solution was obtained for this case. The second case deals with the development of an array of microcracks between fibers forming the bridging zone. An implicit exact solution is formed for this case. In both cases, a discrete fiber distribution is incorporated into the solution.

  2. Ceramic fiber-reinforced monoclinic celsian phase glass-ceramic matrix composite material

    NASA Technical Reports Server (NTRS)

    Bansal, Narottam P. (Inventor); Dicarlo, James A. (Inventor)

    1994-01-01

    A hyridopolysilazane-derived ceramic fiber reinforced monoclinic celsian phase barium aluminum silicate glass-ceramic matrix composite material is prepared by ball-milling an aqueous slurry of BAS glass powder and fine monoclinic celsian seeds. The fibers improve the mechanical strength and fracture toughness and with the matrix provide superior dielectric properties.

  3. Yeh-Stratton Criterion for Stress Concentrations on Fiber-Reinforced Composite Materials

    NASA Technical Reports Server (NTRS)

    Yeh, Hsien-Yang; Richards, W. Lance

    1996-01-01

    This study investigated the Yeh-Stratton Failure Criterion with the stress concentrations on fiber-reinforced composites materials under tensile stresses. The Yeh-Stratton Failure Criterion was developed from the initial yielding of materials based on macromechanics. To investigate this criterion, the influence of the materials anisotropic properties and far field loading on the composite materials with central hole and normal crack were studied. Special emphasis was placed on defining the crack tip stress fields and their applications. The study of Yeh-Stratton criterion for damage zone stress fields on fiber-reinforced composites under tensile loading was compared with several fracture criteria; Tsai-Wu Theory, Hoffman Theory, Fischer Theory, and Cowin Theory. Theoretical predictions from these criteria are examined using experimental results.

  4. Fracture mechanics in fiber reinforced composite materials, taking as examples B/A1 and CRFP

    NASA Technical Reports Server (NTRS)

    Peters, P. W. M.

    1982-01-01

    The validity of linear elastic fracture mechanics and other fracture criteria was investigated with laminates of boron fiber reinforced aluminum (R/A1) and of carbon fiber reinforced epoxide (CFRP). Cracks are assessed by fracture strength Kc or Kmax (critical or maximum value of the stress intensity factor). The Whitney and Nuismer point stress criterion and average stress criterion often show that Kmax of fiber composite materials increases with increasing crack length; however, for R/A1 and CFRP the curve showing fracture strength as a function of crack length is only applicable in a small domain. For R/A1, the reason is clearly the extension of the plastic zone (or the damage zone n the case of CFRP) which cannot be described with a stress intensity factor.

  5. Design and analysis of a novel latch system implementing fiber-reinforced composite materials

    NASA Astrophysics Data System (ADS)

    Guevara Arreola, Francisco Javier

    The use of fiber-reinforced composite materials have increased in the last four decades in high technology applications due to their exceptional mechanical properties and low weight. In the automotive industry carbon fiber have become popular exclusively in luxury cars because of its high cost. However, Carbon-glass hybrid composites offer an effective alternative to designers to implement fiber-reinforced composites into several conventional applications without a considerable price increase maintaining most of their mechanical properties. A door latch system is a complex mechanism that is under high loading conditions during car accidents such as side impacts and rollovers. Therefore, the Department of Transportation in The United States developed a series of tests that every door latch system comply in order to be installed in a vehicle. The implementation of fiber-reinforced composite materials in a door latch system was studied by analyzing the material behavior during the FMVSS No. 206 transverse test using computational efforts and experimental testing. Firstly, a computational model of the current forkbolt and detent structure was developed. Several efforts were conducted in order to create an effective and time efficient model. Two simplified models were implemented with two different contact interaction approaches. 9 composite materials were studied in forkbolt and 5 in detent including woven carbon fiber, unidirectional carbon fiber, woven carbon-glass fiber hybrid composites and unidirectional carbon-glass fiber hybrid composites. The computational model results showed that woven fiber-reinforced composite materials were stiffer than the unidirectional fiber-reinforced composite materials. For instance, a forkbolt made of woven carbon fibers was 20% stiffer than a forkbolt made of unidirectional fibers symmetrically stacked in 0° and 90° alternating directions. Furthermore, Hybrid composite materials behaved as expected in forkbolt noticing a decline

  6. Fungal degradation of fiber-reinforced composite materials

    NASA Technical Reports Server (NTRS)

    Gu, J. D.; Lu, C.; Mitchell, R.; Thorp, K.; Crasto, A.

    1997-01-01

    As described in a previous report, a fungal consortium isolated from degraded polymeric materials was capable of growth on presterilized coupons of five composites, resulting in deep penetration into the interior of all materials within five weeks. Data describing the utilization of composite constituents as nutrients for the microflora are described in this article. Increased microbial growth was observed when composite extract was incubated with the fungal inoculum at ambient temperatures. Scanning electron microscopic observation of carbon fibers incubated with a naturally developed population of microorganisms showed the formation of bacterial biofilms on the fiber surfaces, suggesting possible utilization of the fiber chemical sizing as carbon and energy sources. Electrochemical impedance spectroscopy was used to monitor the phenomena occurring at the fiber-matrix interfaces. Significant differences were observed between inoculated and sterile panels of the composite materials. A progressive decline in impedance was detected in the inoculated panels. Several reaction steps may be involved in the degradation process. Initial ingress of water into the resin matrix appeared to be followed by degradation of fiber surfaces, and separation of fibers from the resin matrix. This investigation suggested that composite materials are susceptible to microbial attack by providing nutrients for growth.

  7. Compressive strength of fiber-reinforced composite materials

    NASA Technical Reports Server (NTRS)

    Davis, J. G., Jr.

    1975-01-01

    Results of an experimental and analytical investigation of the compressive strength of unidirectional boron-epoxy composite material are presented. Observation of fiber coordinates in a boron-epoxy composite indicates that the fibers contain initial curvature. Combined axial compression and torsion tests were conducted on boron-epoxy tubes and it was shown that the shear modulus is a function of axial compressive stress. An analytical model which includes initial curvature in the fibers and permits an estimate of the effect of curvature on compressive strength is proposed. Two modes of failure which may result from the application of axial compressive stress are analyzed - delamination and shear instability. Based on tests and analysis, failure of boron-epoxy under axial compressive load is due to shear instability.

  8. Chemical Processing and Characterization of Fiber Reinforced Nanocomposite Silica Materials

    NASA Astrophysics Data System (ADS)

    Burnett, Steven Shannon

    Ultrasound techniques, acoustic and electroacoustic spectroscopy, are used to investigate and characterize concentrated fluid phase nanocomposites. In particular, the data obtained from ultrasound methods are used as tools to improve the understanding of the fundamental process chemistry of concentrated, multicomponent, nanomaterial dispersions. Silicon nitride nanofibers embedded in silica are particularly interesting for lightweight nanocomposites, because silicon nitride is isostructural to carbon nitride, a super hard material. However, the major challenge with processing these composites is retarding particle-particle aggregation, to maintain highly dispersed systems. Therefore, a systematic approach was developed to evaluate the affect of process parameters on particle-particle aggregation, and improving the chemical kinetics for gelation. From the acoustic analysis of the nanofibers, this thesis was able to deduce that changes in aspect ratio affects the ultrasound propagation. In particular, higher aspect ratio fibers attenuate the ultrasound wave greater than lower aspect fibers of the same material. Furthermore, our results confirm that changes in attenuation depend on the hydrodynamical interactions between particles, the aspect ratio, and the morphology of the dispersant. The results indicate that the attenuation is greater for fumed silica due to its elastic nature and its size, when compared to silica Ludox. Namely, the larger the size, the greater the attenuation. This attenuation is mostly the result of scattering loss in the higher frequency range. In addition, the silica nanofibers exhibit greater attenuation than their nanoparticle counterparts because of their aspect ratio influences their interaction with the ultrasound wave. In addition, this study observed how 3M NH 4 Cl's acoustic properties changes during the gelation process, and during that change, the frequency dependency deviates from the expected squared of the frequency, until the

  9. Adherence of Streptococcus mutans to Fiber-Reinforced Filling Composite and Conventional Restorative Materials

    PubMed Central

    Lassila, Lippo V.J; Garoushi, Sufyan; Tanner, Johanna; Vallittu, Pekka K; Söderling, Eva

    2009-01-01

    Objectives. The aim was to investigate the adhesion of Streptococcus mutans (S. mutans) to a short glass fibers reinforced semi-IPN polymer matrix composite resin. The effect of surface roughness on adhesion was also studied. For comparison, different commercial restorative materials were also evaluated. Materials and Methods. Experimental composite FC resin was prepared by mixing 22.5 wt% of short E-glass fibers, 22.5 wt% of IPN-resin and 55 wt% of silane treated silica fillers using high speed mixing machine. Three direct composite resins (Z250, Grandio and Nulite), resin-modified glass ionomers (Fuji II LC), amalgam (ANA 2000), fiber-reinforced composite (FRC) (everStick and Ribbond), and pre-fabricated ceramic filling insert (Cerana class 1) were tested in this study. Enamel and dentin were used as controls. The specimens (n=3/group) with or without saliva were incubated in a suspension of S. mutans allowing initial adhesion to occur. For the enumeration of cells on the disc surfaces as colony forming units (CFU) the vials with the microbe samples were thoroughly Vortex-treated and after serial dilutions grown anaerobically for 2 days at +37°C on Mitis salivarius agars (Difco) containing bacitracin. Bacterial adhesion was also evaluated by using scanning electron microscopy. Surface roughness (Ra) of the materials was also determined using a surface profilometer. All results were statistically analyzed with one-way analysis of variance (ANOVA). Results. Composite FC resin and other commercial restorative materials showed similar adhesion of S. mutans, while adhesion to dentin and enamel was significantly higher (p<0.05). Surface roughness had no effect on bacterial adhesion. Saliva coating significantly decreased the adhesion for all materials (p<0.05). Composite FC resin had a significantly higher Ra value than control groups (p<0.05). Conclusions. Short fiber-reinforced composite with semi-IPN polymer matrix revealed similar S. mutans adhesion than

  10. Adherence of Streptococcus mutans to Fiber-Reinforced Filling Composite and Conventional Restorative Materials.

    PubMed

    Lassila, Lippo V J; Garoushi, Sufyan; Tanner, Johanna; Vallittu, Pekka K; Söderling, Eva

    2009-01-01

    OBJECTIVES.: The aim was to investigate the adhesion of Streptococcus mutans (S. mutans) to a short glass fibers reinforced semi-IPN polymer matrix composite resin. The effect of surface roughness on adhesion was also studied. For comparison, different commercial restorative materials were also evaluated. MATERIALS AND METHODS.: Experimental composite FC resin was prepared by mixing 22.5 wt% of short E-glass fibers, 22.5 wt% of IPN-resin and 55 wt% of silane treated silica fillers using high speed mixing machine. Three direct composite resins (Z250, Grandio and Nulite), resin-modified glass ionomers (Fuji II LC), amalgam (ANA 2000), fiber-reinforced composite (FRC) (everStick and Ribbond), and pre-fabricated ceramic filling insert (Cerana class 1) were tested in this study. Enamel and dentin were used as controls. The specimens (n=3/group) with or without saliva were incubated in a suspension of S. mutans allowing initial adhesion to occur. For the enumeration of cells on the disc surfaces as colony forming units (CFU) the vials with the microbe samples were thoroughly Vortex-treated and after serial dilutions grown anaerobically for 2 days at +37 degrees C on Mitis salivarius agars (Difco) containing bacitracin. Bacterial adhesion was also evaluated by using scanning electron microscopy. Surface roughness (Ra) of the materials was also determined using a surface profilometer. All results were statistically analyzed with one-way analysis of variance (ANOVA). RESULTS.: Composite FC resin and other commercial restorative materials showed similar adhesion of S. mutans, while adhesion to dentin and enamel was significantly higher (p<0.05). Surface roughness had no effect on bacterial adhesion. Saliva coating significantly decreased the adhesion for all materials (p<0.05). Composite FC resin had a significantly higher Ra value than control groups (p<0.05). CONCLUSIONS.: Short fiber-reinforced composite with semi-IPN polymer matrix revealed similar S. mutans adhesion

  11. A study of fiber materials for use in temperature resistant fiber reinforced composites

    NASA Technical Reports Server (NTRS)

    Bachowsky, M. J.; Anderson, R. N.

    1982-01-01

    This study has been directed at characterizing the micro-properties of candidate ceramics and glasses for use in making fibers used in fiber reinforced material composites. Particular emphasis has been given into developing techniques to guide the optimization of fiber properties. The Scanning Electron Microscope (SEM) and X-ray Diffractometer (XRD) have been used to help collate the method of synthesis, crystal structure and surface morphology with physical performance parameters. As a result, progress has been made in characterizing such materials. This increased understanding makes the previous research worthy of further study.

  12. Determination of Material Parameters for Microbuckling Analysis of Fiber Reinforced Polymer Matrix Composites

    NASA Astrophysics Data System (ADS)

    Romanowicz, M.

    2015-05-01

    This research focuses on studying the effect of the constitutive law adopted for a matrix material on the compressive response of a unidirectional fiber reinforced polymer matrix composite. To investigate this effect, a periodic unit cell model of a unidirectional composite with an initial fiber waviness and inelastic behavior of the matrix was used. The sensitivity of the compressive strength to the hydrostatic pressure, the flow rule and the fiber misalignment angle were presented. The model was verified against an analytical solution and experimental data. Results of this study indicate that a micromechanical model with correctly identified material parameters provides a useful alternative to theoretical models and experimentation.

  13. Damage threshold study of sonic IR imaging on carbon-fiber reinforced laminated composite materials

    NASA Astrophysics Data System (ADS)

    Han, Xiaoyan; He, Qi; Zhang, Ding; Ashbaugh, Mike; Favro, Lawrence D.; Newaz, Golam; Thomas, Robert L.

    2013-01-01

    Sonic Infrared Imaging, as a young NDE technology, has drawn a lot of attentions due to it's fast, wide-area evaluation capability, and due to its broad applications in different materials such as metal/metal alloy, composites and detection of various types of defects: surface, subsurface, cracks, delaminations/disbonds. Sonic IR Imaging combines pulsed ultrasound excitation and infrared imaging to detect defects in materials. The sound pulse causes rubbing due to non-unison motion between faces of defects, and infrared sensors image the temperature map over the target to identify defects. However, concerns have also been brought up about possible damages which might occur at the contact spots between the ultrasound transducer from the external excitation source and the target materials. In this paper, we present our results from a series of systematically designed experiments on carbon-fiber reinforced laminated composite panels to address the concerns.

  14. Surface modification of fiber reinforced polymer composites and their attachment to bone simulating material.

    PubMed

    Hautamäki, M P; Puska, M; Aho, A J; Kopperud, H M; Vallittu, P K

    2013-05-01

    The purpose of this study was to investigate the effect of fiber orientation of a fiber-reinforced composite (FRC) made of poly-methyl-methacrylate (PMMA) and E-glass to the surface fabrication process by solvent dissolution. Intention of the dissolution process was to expose the fibers and create a macroporous surface onto the FRC to enhance bone bonding of the material. The effect of dissolution and fiber direction to the bone bonding capability of the FRC material was also tested. Three groups of FRC specimens (n = 18/group) were made of PMMA and E-glass fiber reinforcement: (a) group with continuous fibers parallel to the surface of the specimen, (b) continuous fibers oriented perpendicularly to the surface, (c) randomly oriented short (discontinuous) fibers. Fourth specimen group (n = 18) made of plain PMMA served as controls. The specimens were subjected to a solvent treatment by tetrahydrofuran (THF) of either 5, 15 or 30 min of time (n = 6/time point), and the advancement of the dissolution (front) was measured. The solvent treatment also exposed the fibers and created a surface roughness on to the specimens. The solvent treated specimens were embedded into plaster of Paris to simulate bone bonding by mechanical locking and a pull-out test was undertaken to determine the strength of the attachment. All the FRC specimens dissolved as function of time, as the control group showed no marked dissolution during the study period. The specimens with fibers along the direction of long axis of specimen began to dissolve significantly faster than specimens in other groups, but the test specimens with randomly oriented short fibers showed the greatest depth of dissolution after 30 min. The pull-out test showed that the PMMA specimens with fibers were retained better by the plaster of Paris than specimens without fibers. However, direction of the fibers considerably influenced the force of attachment. The fiber reinforcement increases significantly the

  15. Optimization of the hot pressing parameters to fabricate the fiber reinforced material (FRM)

    SciTech Connect

    Takahashi, Kunio; Onzawa, Tadao

    1995-11-01

    When hot pressing is used to fabricate the fiber reinforced materials (FRM), the deformation and the adhesion of the matrix foil must be completed and the thickness of the reaction layer at the matrix/fiber interface must be smaller than the critical value derived from the Ochiai`s theory. A simulation model was proposed to predict the deformation of matrix foils, where plastic and creep deformations were taken into account. These calculations provide a consistent and unified interpretation of experimental data for Ti-matrix FRM, while the creep constants of Ti are known. A method is proposed to estimate the creep constants from some experimental trial for the matrix materials whose creep constants are unknown. By using this method, to types of Ti{sub 3}Al matrix FRM were formed to demonstrate the applicability of the algorithm. The tensile strength of the FRM was examined.

  16. Aging characteristics of short glass fiber reinforced ZA-27 alloy composite materials

    NASA Astrophysics Data System (ADS)

    Sharma, S. C.; Girish, B. M.; Satish, B. M.; Kamath, R.

    1998-12-01

    Aging characteristics of short glass fiber reinforced ZA-27 alloy composite materials have been evaluated in the present study. The liquid metallurgy technique was used to fabricate the composites, in which preheated short glass fibers were introduced into the ZA-27 alloy melt above its liquidus temperature. The aging temperature employed was 125 °C for 6, 12,18, and 24 h. The aged alloy (no fibers) reached the peak hardness after 18 h, while the composites (regardless of filler content) reached the same hardness in 12 h. It is hypothesized that the aging treatment of a composite improves the strength of the interface between the short fibers and the matrix. This is confirmed by the tensile fractograph analysis, which indicates that at a given aging temperature, the composites aged for 18 h exhibit short fibers that remain attached to the metal matrix, while those aged for 6 h undergo debonding.

  17. Investigation of Polymer Resin/Fiber Compatibility in Natural Fiber Reinforced Composite Automotive Materials

    SciTech Connect

    Fifield, Leonard S.; Huang, Cheng; Simmons, Kevin L.

    2010-01-01

    Natural fibers represent a lower density and potentially lower cost alternative to glass fibers for reinforcement of polymers in automotive composites. The high specific modulus and strength of bast fibers make them an attractive option to replace glass not only in non-structural automotive components, but also in semi-structural and structural components. Significant barriers to insertion of bast fibers in the fiber reinforced automotive composite market include the high moisture uptake of this lignocellulosic material relative to glass and the weak inherent interface between natural fibers and automotive resins. This work seeks to improve the moisture uptake and resin interfacing properties of natural fibers through improved fundamental understanding of fiber physiochemical architecture and development of tailored fiber surface modification strategies.

  18. Effect of the coating properties on crack propagation in fiber-reinforced materials

    SciTech Connect

    Kumar, S.; Singh, R.N.

    1996-12-31

    A finite element technique is used to study the effects of the coating properties on the crack propagation in fiber-reinforced materials. Crack opening stresses and energy release rates for the crack penetration and deflection have been studied in SCS6 (fiber) -C/BN (coating) - Zircon (matrix) composites. Effect of the coating thickness on crack propagation has been also studied. In general, no significant changes are found in stress ratio (ratio of hoop stresses along the crack and at the interface) and energy release rate ratio (ratio of energy release rates for the crack penetration and crack deflection), but the magnitudes of the stresses and energy release rates change substantially with the change in the coating thickness.

  19. Conservative Approach for Restoring Posterior Missing Tooth with Fiber Reinforcement Materials: Four Clinical Reports

    PubMed Central

    Karaarslan, Emine Sirin; Ertas, Ertan; Ozsevik, Semih; Usumez, Aslihan

    2011-01-01

    Adhesively luted, fiber-reinforced, composite-inlay, retained fixed-partial dentures can be a clinical alternative for the replacement of missing posterior teeth in selective situations. This type of restoration allows for satisfactory esthetics and reduced tooth preparation compared to a conventional, fixed-partial denture. This clinical report describes the use of a fiber-reinforced, composite-inlay, retained fixed-partial denture as a conservative alternative for the replacement of missing posterior teeth. PMID:21912503

  20. Modeling of the Indentation of Fiber Reinforced Materials Using Spherical Indenters

    SciTech Connect

    Gountsidou, V.; Polatoglou, H. M.

    2010-01-21

    Following the enormous development of the technology there is a great need for complex engineering materials to be studied in multilayered films at the nano-level. Careful modeling of the structure of engineering materials, using finite element analysis may reveal specific behavior of the component materials and the filling materials, such as mortars, which are the important boundaries of all the engineering materials. The instruments used for experiments are expensive and their utilization is hindered by many unexpected factors. With the help of computer programs it is possible to achieve virtual nanoindentation, a widely known non-destructive method. It is easy to model structures in whatever shape or dimensions we wish, with one or more layers and with linear or nonlinear materials in order to obtain stress, strain, displacement curves, study microhardness, etc. The purpose of this paper is to model the nanoindentation process for fiber-reinforced concrete and to study the mechanical properties as a function of the distance of a particular fibre.

  1. Processing and Material Characterization of Continuous Basalt Fiber Reinforced Ceramic Matrix Composites Using Polymer Derived Ceramics.

    NASA Technical Reports Server (NTRS)

    Cox, Sarah B.

    2014-01-01

    The need for high performance vehicles in the aerospace industry requires materials which can withstand high loads and high temperatures. New developments in launch pads and infrastructure must also be made to handle this intense environment with lightweight, reusable, structural materials. By using more functional materials, better performance can be seen in the launch environment, and launch vehicle designs which have not been previously used can be considered. The development of high temperature structural composite materials has been very limited due to the high cost of the materials and the processing needed. Polymer matrix composites can be used for temperatures up to 260C. Ceramics can take much higher temperatures, but they are difficult to produce and form in bulk volumes. Polymer Derived Ceramics (PDCs) begin as a polymer matrix, allowing a shape to be formed and cured and then to be pyrolized in order to obtain a ceramic with the associated thermal and mechanical properties. The use of basalt in structural and high temperature applications has been under development for over 50 years, yet there has been little published research on the incorporation of basalt fibers as a reinforcement in the composites. In this study, continuous basalt fiber reinforced PDCs have been fabricated and tested for the applicability of this composite system as a high temperature structural composite material. The oxyacetylene torch testing and three point bend testing have been performed on test panels and the test results are presented.

  2. On constitutive equations for thermoelastic analysis of fiber-reinforced composites with isotropic matrix material

    NASA Astrophysics Data System (ADS)

    Usal, Melek; Usal, Mustafa Reşit; Esendemir, Ümran

    2013-01-01

    This paper is concerned with developing constitutive equations for the thermoelastic analysis of composites consisting of an isotropic matrix reinforced by independent and inextensible two families of fibers having an arbitrary distribution. The composite medium is assumed to be incompressible, dependent on temperature gradient, and showing linear elastic behavior. The reaction of the composite material subject to external loads is expressed in stress tensor and heat flux vector. The matrix material made of elastic material involving an artificial anisotropy due to fibers reinforcing by arbitrary distributions has been assumed as an isotropic medium. The theory is formulated within the scope of continuum mechanics. As a result of thermodynamic constraints, it has been determined that the stress potential function is dependent on the deformation tensor, the fiber fields vectors and the temperature, while the heat flux vector function is dependent on the deformation tensor, the fiber fields vectors, the temperature and temperature gradient. To determine arguments of the constitutive functionals, findings relating to the theory of invariants have been used as a method because of that isotropy constraint is imposed on the material. The constitutive equations of stress and heat flux vector have been written in terms of different coordinate descriptions.

  3. The Use of Carbon-Fiber-Reinforced (CFR) PEEK Material in Orthopedic Implants: A Systematic Review.

    PubMed

    Li, Chuan Silvia; Vannabouathong, Christopher; Sprague, Sheila; Bhandari, Mohit

    2015-01-01

    Carbon-fiber-reinforced polyetheretherketone (CFR-PEEK) has been successfully used in orthopedic implants. The aim of this systematic review is to investigate the properties, technical data, and safety of CFR-PEEK biomaterial and to evaluate its potential for new innovation in the design of articulating medical devices. A comprehensive search in PubMed and EMBASE was conducted to identify articles relevant to the outcomes of CFR-PEEK orthopedic implants. The search was also expanded by reviewing the reference sections of selected papers and references and benchmark reports provided by content experts. A total of 23 articles were included in this review. There is limited literature available assessing the performance of CFR-PEEK, specifically as an implant material for arthroplasty systems. Nevertheless, available studies strongly support CFR-PEEK as a promising and suitable material for orthopedic implants because of its biocompatibility, material characteristics, and mechanical durability. Future studies should continue to investigate CFR-PEEK's potential benefits. PMID:25780341

  4. Mechanical properties of neat polymer matrix materials and their unidirectional carbon fiber-reinforced composites

    NASA Technical Reports Server (NTRS)

    Zimmerman, Richard S.; Adams, Donald F.

    1988-01-01

    The mechanical properties of two neat resin systems for use in carbon fiber epoxy composites were characterized. This included tensile and shear stiffness and strengths, coefficients of thermal and moisture expansion, and fracture toughness. Tests were conducted on specimens in the dry and moisture-saturated states, at temperatures of 23, 82 and 121 C. The neat resins tested were American Cyanamid 1806 and Union Carbide ERX-4901B(MPDA). Results were compared to previously tested neat resins. Four unidirectional carbon fiber reinforced composites were mechanically characterized. Axial and transverse tension and in-plane shear strengths and stiffness were measured, as well as transverse coefficients of thermal and moisture expansion. Tests were conducted on dry specimens only at 23 and 100 C. The materials tested were AS4/3502, AS6/5245-C, T300/BP907, and C6000/1806 unidirectional composites. Scanning electron microscopic examination of fracture surfaces was performed to permit the correlation of observed failure modes with the environmental test conditions.

  5. Fiber-reinforced glass

    SciTech Connect

    Beier, W.; Markman, S.

    1997-12-01

    Fiber-reinforced glass composites are glass or glass ceramic matrices reinforced with long fibers of carbon or silicon carbide. These composites are lighter than steel but just as strong as many steel grades, and can resist higher temperatures. They also have outstanding resistance to impact, thermal shock, and wear, and can be formulated to control thermal and electrical conductivity. With proper tooling, operations such as drilling, grinding, and turning can be completed in half the time required for non-reinforced glass. Currently, fiber-reinforced glass components are primarily used for handling hot glass or molten aluminum during manufacturing operations. But FRG is also under test as an engineering material in a variety of markets, including the aerospace, automotive, and semiconductor industries. Toward this end, research is being carried out to increase the size of components that can be delivered on a production basis, to develop economical methods of achieving complex near-net shapes, and to reduce the cycle time for production of specific shapes. This article focuses on the properties and applications of fiber-reinforced glass composites.

  6. Analytical modeling in support of the development of fiber reinforced ceramic composite materials for re-heater burners

    SciTech Connect

    Kibler, J.J.; DiPietro, S.G.

    1995-10-01

    Development of Continuous Fiber reinforced Ceramic Composite (CFCC) materials is a process of identifying components which will benefit from CFCC properties, and defining appropriate composite constructions which will provide materials which will meet the structural and thermal requirements of the application. Materials Sciences Corporation (MSC) has been providing analytical support to Textron Specialty Materials in the development of re-heated tubes for metal reheating furnaces. As part of this support, a study has been made of the sensitivity of composite properties to fiber orientation as well as a number of matrix properties which control the stress-strain behavior of the composite.

  7. Recovery of microfields in fiber-reinforced composite materials: Principles and limitations

    NASA Astrophysics Data System (ADS)

    Ritchey, Andrew J.

    A detailed investigation of the limitations and errors induced by modeling a composite layer composed of straight carbon fibers embedded in an epoxy matrix as an homogenous layer with Cauchy effective moduli is performed. Specifically, the material system studied has IM7 carbon fibers arranged in a square array and bonded together with 8552 epoxy resin (IM7/8552). The finite element method is used to study the effect of free surfaces on the local elastic fields in 0°, 45° and 90° laminae, in which as many as 256 individual fibers are modeled. Through these analyses, it is shown that a micro-boundary layer, analogous to the macro-boundary layer observed in composite laminates, is developed at the microlevel. Additionally, [0/90]s and [90/0]s laminates are studied to investigate the joint action of the macro- and micro-boundary layers. Unless otherwise noted, fiber volume fractions of Vƒ=0.20 and Vƒ=0.65 are selected and the domains are subjected to uniform axial extension. Although this study is done for a highly idealized geometry (i.e. with a single material system and under a simple loading condition) the principles of periodicity, symmetry and antisymmetry used to efficiently perform a direct numerical simulation with a large number of fiber inclusions is general, and can be applied to more complicated geometries and boundary conditions. The purpose of the current work is to be the first step in a building block approach to understanding the interaction of multiple scales in fiber-reinforced composites through direct numerical simulations. The main part of the current manuscript focuses on the characterization of a micro-boundary layer that develops in fiber reinforced composite layers. This phenomena results from the changing constraints on the constituent phases as a result of discontinuities, such as free surfaces or ply interfaces. The effect is most pronounced in laminae that have a fiber termination intersecting a free surface, and appears to be

  8. Feasibility study of prestressed natural fiber-reinforced polylactic acid (pla) composite materials

    NASA Astrophysics Data System (ADS)

    Hinchcliffe, Sean A.

    The feasibility of manufacturing prestressed natural-fiber reinforced biopolymer composites is demonstrated in this work. The objective of this study was to illustrate that the specific mechanical properties of biopolymers can be enhanced by leveraging a combination of additive manufacturing (3D printing) and post-tensioning of continuous natural fiber reinforcement. Tensile and flexural PLA specimens were 3D-printed with and without post-tensioning ducts. The mechanical properties of reinforcing fibers jute and flax were characterized prior to post-tensioning. The effect of matrix cross-sectional geometry and post-tensioning on the specific mechanical properties of PLA were investigated using mechanical testing. Numerical and analytical models were developed to predict the experimental results, which confirm that 3D-printed matrices improve the specific mechanical properties of PLA composites and are further improved via initial fiber prestressing. The results suggest that both additive manufacturing and fiber prestressing represent viable new methods for improving the mechanical performance of natural fiber-reinforced polymeric composites.

  9. Laser-Generated Lamb Waves Propagation in Multilayered Plates Composed of Viscoelastic Fiber-reinforced Composite Materials

    NASA Astrophysics Data System (ADS)

    Sun, Hong-xiang; Zhang, Shu-yi; Yuan, Shou-qi; Guan, Yi-jun; Ge, Yong

    2016-07-01

    The propagation characteristics of laser-generated Lamb waves in multilayered fiber-reinforced composite plates with different fiber orientations and number of layers have been investigated quantitatively. Considering the viscoelasticity of the composite materials, we have set up finite element models for simulating the laser-generated Lamb waves in two types of the multilayered composite plates. In the first type, different fiber orientations are adopted. In the second one, different number of layers are considered. The results illustrate the occurrence of attenuation and dispersion, which is induced by the viscoelasticity and multilayer structure, respectively.

  10. Process for curing bismaleimide resins

    NASA Technical Reports Server (NTRS)

    Parker, John A. (Inventor); OTHY S.imides alone. (Inventor)

    1986-01-01

    This invention relates to vinyl pyridine group containing compounds and oligomers, their advantageous copolymerization with bismaleimide resins, and the formation of reinforced composites based on these copolymers. When vinyl pyridines including vinyl stilbazole materials and vinyl styrylpyridine oligomer materials are admixed with bismaleimides and cured to form copolymers the cure temperatures of the copolymers are substantially below the cure temperatures of the bismaleimides alone.

  11. Matched excitation for thermal nondestructive testing of carbon fiber reinforced plastic materials

    NASA Astrophysics Data System (ADS)

    Mulaveesala, Ravibabu; Subbarao, Ghali Venkata; Amarnath, Muniyappa

    2012-06-01

    Active thermographic studies proved their capabilities for detection of deeper subsurface details with reduced non uniform emissivity problems for defect detection. In this contribution analysis of subsurface anomalies has been carried out by probing a suitable frequency component with sufficient energy. This paper highlights the comparative analysis of different non-stationary thermographic schemes on the basis of probing equal energy to the chosen frequency component used for the analysis of a carbon fiber reinforced plastic (CFRP) sample used in experimentation. Experiments have been carried out to find the detection ability of different excitation schemes and comparisons have been made by taking signal to noise ratio (SNR) of the defects into consideration.

  12. Improvement and optimization of internal damping in fiber-reinforced composite materials. Final report, June 1983-November 1985

    SciTech Connect

    Gibson, R.F.; Suarez, S.A.

    1986-03-03

    The objective of this research were to study the effects of such parameters as fiber aspect ratio, fiber orientation and fiber/matrix properties on damping in fiber-reinforced polymer composites. These objectives were to be met by using both experimental and analytical approaches. The development of improved techniques for fabrication and testing of specimens and the development of relatively simple design equations for prediction of damping were desirable goals that were also met. Two new computer-aided testing techniques based on the impulse frequency-response approach were developed. Specimens of graphite/epoxy, boron/epoxy and Kevlar aramid/epoxy were fabricated by using an autoclave-style press cure which was developed specifically for this program. Although a number of parameters were studied, the emphasis was on the influence of fiber length, fiber orientation, and fiber material on damping of polymer composites. Experimental results show that, as predicted, very low fiber aspect ratios are required to produce significant improvements in damping. Of the three fiber types tested, the Kevlar aramid fiber composite was found to have much better damping than graphite or boron fiber composites. Measurements and predictions also indicate that the control of fiber orientation in a continuous fiber reinforced laminate may be a better approach to the improvement of damping than the control of fiber aspect ratio.

  13. Preliminary development of a fundamental analysis model for crack growth in a fiber reinforced composite material

    NASA Technical Reports Server (NTRS)

    Kanninen, M. F.; Rybicki, E. F.; Griffith, W. I.

    1977-01-01

    A mathematical model for the strength of fiber reinforced composites containing specific flaws is described. The approach is to embed a local heterogeneous region surrounding the crack tip in an anisotropic elastic continuum. By consideration of the individual failure events activated near the flaw tip, a strength prediction can be made from basic properties of the composite constituents. Computations for arbitrary flaw size and orientation have been performed for unidirectional composites with linear elastic-brittle constituent behavior. The mechanical properties were those of graphite epoxy. With the rupture properties arbitrarily varied to test the capability of the model to reflect real fracture modes in fiber composites, it is shown that fiber breakage, matrix crazing, crack bridging, matrix-fiber debonding, and axial splitting all can occur during gradually increasing load prior to catastrophic fracture. Qualitative comparisons with experimental results on edge-notched unidirectional graphite epoxy specimens have also been made.

  14. Fiber-reinforced syntactic foams

    NASA Astrophysics Data System (ADS)

    Huang, Yi-Jen

    Long fibers are generally preferred for reinforcing foams for performance reasons. However, uniform dispersion is difficult to achieve because they must be mixed with liquid resin prior to foam expansion. New approaches aiming to overcome such problem have been developed at USC's Composites Center. Fiber-reinforced syntactic foams with long fibers (over 6 mm in length) manufactured at USC's Composites Center have achieved promising mechanical properties and demonstrated lower density relative to conventional composite foams. Fiber-reinforced syntactic foams were synthesized from thermosetting polymeric microspheres (amino and phenolic microspheres), as well as thermoplastic PVC heat expandable microspheres (HEMs). Carbon and/or aramid fibers were used to reinforce the syntactic foams. Basic mechanical properties, including shear, tensile, and compression, were measured in syntactic foams and fiber-reinforced syntactic foams. Microstructure and crack propagation behavior were investigated by scanning electron microscope and light microscopy. Failure mechanisms and reinforcing mechanisms of fiber-reinforced syntactic foams were also analyzed. As expected, additions of fiber reinforcements to foams enhanced both tensile and shear properties. However, only limited enhancement in compression properties was observed, and fiber reinforcement was of limited benefit in this regard. Therefore, a hybrid foam design was explored and evaluated in an attempt to enhance compression properties. HEMs were blended with glass microspheres to produce hybrid foams, and hybrid foams were subsequently reinforced with continuous aramid fibers to produce fiber-reinforced hybrid foams. Mechanical properties of these foams were evaluated. Findings indicated that the production of hybrid foams was an effective way to enhance the compressive properties of syntactic foams, while the addition of fiber reinforcements enhanced the shear and tensile performance of syntactic foams. Another approach

  15. Matrix toughness, long-term behavior, and damage tolerance of notched graphite fiber-reinforced composite materials

    NASA Technical Reports Server (NTRS)

    Bakis, C. E.; Simonds, R. A.; Stinchcomb, W. W.; Vick, L. W.

    1990-01-01

    The long-term behavior of notched graphite-fiber-reinforced composite laminates with brittle or tough matrix materials and different fiber architectures was investigated using damage measurements and stiffness change, residual strength, and life data. The fiber/matrix materials included T300/5208, AS4/3501-6, AS4/1808, AS4/PEEK, and C3000/PMR-15 matrices and unidirectional tape and woven cloth fiber architectures. Results of damage evaluation and of residual strength measurements during the fatigue damage development showed that the long-term behavior and damage tolerance are controlled by a number of interacting factors such as the matrix toughness, fiber architecture, loading levels, and damage types and distributions.

  16. Non-destructive evaluation of porosity and its effect on mechanical properties of carbon fiber reinforced polymer composite materials

    NASA Astrophysics Data System (ADS)

    Bhat, M. R.; Binoy, M. P.; Surya, N. M.; Murthy, C. R. L.; Engelbart, R. W.

    2012-05-01

    In this work, an attempt is made to induce porosity of varied levels in carbon fiber reinforced epoxy based polymer composite laminates fabricated using prepregs by varying the fabrication parameters such as applied vacuum, autoclave pressure and curing temperature. Different NDE tools have been utilized to evaluate the porosity content and correlate with measurable parameters of different NDE techniques. Primarily, ultrasonic imaging and real time digital X-ray imaging have been tried to obtain a measurable parameter which can represent or reflect the amount of porosity contained in the composite laminate. Also, effect of varied porosity content on mechanical properties of the CFRP composite materials is investigated through a series of experimental investigations. The outcome of the experimental approach has yielded interesting and encouraging trend as a first step towards developing an NDE tool for quantification of effect of varied porosity in the polymer composite materials.

  17. Non-linear finite element-based material constitutive law for zero slump steel fiber reinforced concrete pipe structures

    NASA Astrophysics Data System (ADS)

    Mikhaylova, Alena

    This study presents a comprehensive investigation of performance and behavior of steel-fiber reinforced concrete pipes (SFRCP). The main goal of this study is to develop the material constitutive model for steel fiber reinforced concrete used in dry-cast application. To accomplish this goal a range of pipe sizes varying from 15 in. (400 mm) to 48 in. (1200 mm) in diameter and fiber content of 0.17%, 0.25%, 0.33%, 0.5%, 0.67% and 83% by volume were produced. The pipes were tested in three-edge bearing condition to obtain the load-deformation response and overall performance of the pipe. The pipes were also subjected to hydrostatic joint and joint shear tests to evaluate the performance of the fiber-pipe joints for water tightness and under differential displacements, respectively. In addition, testing on hardened concrete was performed to obtain the basic mechanical material properties. High variation in the test results for material testing was identified as a part of experimental investigation. A three-dimensional non-linear finite element model of the pipe under the three edge bearing condition was developed to identify the constitutive material relations of fiber-concrete composite. A constitutive model of concrete implementing the concrete plasticity and continuum fracture mechanics was considered for defining the complex non-linear behavior of fiber-concrete. Three main concrete damage algorithms were examined: concrete brittle cracking, concrete damaged plasticity with adaptive meshing technique and concrete damaged plasticity with visco-plastic regularization. The latter was identified as the most robust and efficient to model the post-cracking behavior of fiber reinforced concrete and was used in the subsequent studies. The tension stiffening material constitutive law for composite concrete was determined by converging the FEM solution of load-deformation response with the results of experimental testing. This was achieved by iteratively modifying the non

  18. Self-sealing of thermal fatigue and mechanical damage in fiber-reinforced composite materials

    NASA Astrophysics Data System (ADS)

    Moll, Jericho L.

    Fiber reinforced composite tanks provide a promising method of storage for liquid oxygen and hydrogen for aerospace applications. The inherent thermal fatigue of these vessels leads to the formation of microcracks, which allow gas phase leakage across the tank walls. In this dissertation, self-healing functionality is imparted to a structural composite to effectively seal microcracks induced by both mechanical and thermal loading cycles. Two different microencapsulated healing chemistries are investigated in woven glass fiber/epoxy and uni-weave carbon fiber/epoxy composites. Self-healing of mechanically induced damage was first studied in a room temperature cured plain weave E-glass/epoxy composite with encapsulated dicyclopentadiene (DCPD) monomer and wax protected Grubbs' catalyst healing components. A controlled amount of microcracking was introduced through cyclic indentation of opposing surfaces of the composite. The resulting damage zone was proportional to the indentation load. Healing was assessed through the use of a pressure cell apparatus to detect nitrogen flow through the thickness direction of the damaged composite. Successful healing resulted in a perfect seal, with no measurable gas flow. The effect of DCPD microcapsule size (51 microm and 18 microm) and concentration (0--12.2 wt%) on the self-sealing ability was investigated. Composite specimens with 6.5 wt% 51 microm capsules sealed 67% of the time, compared to 13% for the control panels without healing components. A thermally stable, dual microcapsule healing chemistry comprised of silanol terminated poly(dimethyl siloxane) plus a crosslinking agent and a tin catalyst was employed to allow higher composite processing temperatures. The microcapsules were incorporated into a satin weave E-glass fiber/epoxy composite processed at 120°C to yield a glass transition temperature of 127°C. Self-sealing ability after mechanical damage was assessed for different microcapsule sizees (25 microm and 42

  19. Fiber reinforced PMR polyimide composites

    NASA Technical Reports Server (NTRS)

    Cavano, P. J.; Winters, W. E.

    1978-01-01

    Commercially obtained PMR-15 polyimide prepregs with S-glass and graphite fiber reinforcements were evaluated along with in-house prepared glass and graphite cloth PMR 2 materials. A novel autoclave approach was conceived and used to demonstrate that both the PMR systems respond to 1.4 MPa (200 psi) autoclave pressures to produce void free composites equivalent to die molded laminates. Isothermal gravimetric analysis and subsequent mechanical property tests indicated that the PMR 2 system was significantly superior in thermo-oxidative stability, and that S-glass reinforcements may contribute to the accelerated degradation of composites at 316 C (600 F) when compared to graphite fiber reinforced composites. Fully reversed bending fatigue experiments were conducted with a type of fixture unused for organic matrix composites. These studies indicated that the graphite fiber composites were clearly superior in fatigue resistance to the glass fiber reinforced material and that PMR matrix composite systems yield performance of the same order as composite materials employing other families of matrices.

  20. A Comparative Evaluation of Effect of Different Chemical Solvents on the Shear Bond Strength of Glass Fiber reinforced Post to Core Material

    PubMed Central

    Samadi, Firoza; Jaiswal, JN; Saha, Sonali

    2014-01-01

    ABSTRACT% Aim: To compare the effect of different chemical solvents on glass fiber reinforced posts and to study the effect of these solvents on the shear bond strength of glass fiber reinforced post to core material. Materials and methods: This study was conducted to evaluate the effect of three chemical solvents, i.e. silane coupling agent, 6% H2O2 and 37% phosphoric acid on the shear bond strength of glass fiber post to a composite resin restorative material. The changes in post surface characteristics after different treatments were also observed, using scanning electron microscopy (SEM) and shear bond strength was analyzed using universal testing machine (UTM). Results: Surface treatment with hydrogen peroxide had greatest impact on the post surface followed by 37% phosphoric acid and silane. On evaluation of the shear bond strength, 6% H2O2 exhibited the maximum shear bond strength followed in descending order by 37% phosphoric acid and silane respectively. Conclusion: The surface treatment of glass fiber post enhances the adhesion between the post and composite resin which is used as core material. Failure of a fiber post and composite resin core often occurs at the junction between the two materials. This failure process requires better characterization. How to cite this article: Sharma A, Samadi F, Jaiswal JN, Saha S. A Comparative Evaluation of Effect of Different Chemical Solvents on the Shear Bond Strength of Glass Fiber Reinforced Post to Core Material. Int J Clin Pediatr Dent 2014;7(3):192-196. PMID:25709300

  1. Computational efficiency of numerical approximations of tangent moduli for finite element implementation of a fiber-reinforced hyperelastic material model.

    PubMed

    Liu, Haofei; Sun, Wei

    2016-01-01

    In this study, we evaluated computational efficiency of finite element (FE) simulations when a numerical approximation method was used to obtain the tangent moduli. A fiber-reinforced hyperelastic material model for nearly incompressible soft tissues was implemented for 3D solid elements using both the approximation method and the closed-form analytical method, and validated by comparing the components of the tangent modulus tensor (also referred to as the material Jacobian) between the two methods. The computational efficiency of the approximation method was evaluated with different perturbation parameters and approximation schemes, and quantified by the number of iteration steps and CPU time required to complete these simulations. From the simulation results, it can be seen that the overall accuracy of the approximation method is improved by adopting the central difference approximation scheme compared to the forward Euler approximation scheme. For small-scale simulations with about 10,000 DOFs, the approximation schemes could reduce the CPU time substantially compared to the closed-form solution, due to the fact that fewer calculation steps are needed at each integration point. However, for a large-scale simulation with about 300,000 DOFs, the advantages of the approximation schemes diminish because the factorization of the stiffness matrix will dominate the solution time. Overall, as it is material model independent, the approximation method simplifies the FE implementation of a complex constitutive model with comparable accuracy and computational efficiency to the closed-form solution, which makes it attractive in FE simulations with complex material models. PMID:26692168

  2. Computer modeling of the mechanical behavior of composites -- Interfacial cracks in fiber-reinforced materials

    SciTech Connect

    Schmauder, S.; Haake, S. |; Mueller, W.H. |

    1996-06-15

    Computer modeling of materials and especially modeling the mechanical behavior of composites became increasingly popular in the past few years. Among them are examples of micromechanical modeling of real structures as well as idealized model structures of linear elastic and elasto-plastic material response. In this paper, Erdogan`s Integral Equation Method (IEM) is chosen as an example for a powerful method providing principle insight into elastic fracture mechanical situations. IEM or, alternatively, complex function techniques sometimes even allow for deriving analytical solutions such as in the case of a circumferential crack along a fiber/matrix interface. The analytical formulae of this interface crack will be analyzed numerically and typical results will be presented graphically.

  3. Mechanical properties of several neat polymer matrix materials and unidirectional carbon fiber-reinforced composites

    NASA Technical Reports Server (NTRS)

    Coguill, Scott L.; Adams, Donald F.

    1989-01-01

    The mechanical and physical properties of three neat matrix materials, i.e., PEEK (polyetheretherketone) thermoplastic, Hexcel F155 rubber-toughened epoxy and Hercules 8551-7 rubber-toughened epoxy, were experimentally determined. Twelve unidirectional carbon fiber composites, incorporating matrix materials characterized in this or earlier studies (with one exception; the PISO(sub 2)-TPI matrix itself was not characterized), were also tested. These composite systems included AS4/2220-1, AS4/2220-3, T500/R914, IM6/HX1504, T300/4901A (MDA), T700/4901A (MDA), T300/4901B (MPDA), T700/4901B (MPDA), APC2 (AS4/PEEK, ICI), APC2 (AS4/PEEK, Langley Research Center), AS4/8551-7, and AS4/PISO(sub 2)-TPI. For the neat matrix materials, the tensile, shear, fracture toughness, coefficient of thermal expansion, and coefficient of moisture expansion properties were measured as a function of both temperature and moisture content. For the unidirectional composites, axial and transverse tensile, longitudinal shear, coefficient of thermal expansion, and coefficient of moisture expansion properties were determined, at room temperature and 100 C.

  4. Acoustic emission and acousto-ultrasonic signature analysis of failure mechanisms in carbon fiber reinforced polymer materials

    NASA Astrophysics Data System (ADS)

    Carey, Shawn Allen

    Fiber reinforced polymer composite materials, particularly carbon (CFRPs), are being used for primary structural applications, particularly in the aerospace and naval industries. Advantages of CFRP materials, compared to traditional materials such as steel and aluminum, include: light weight, high strength to weight ratio, corrosion resistance, and long life expectancy. A concern with CFRPs is that despite quality control during fabrication, the material can contain many hidden internal flaws. These flaws in combination with unseen damage due to fatigue and low velocity impact have led to catastrophic failure of structures and components. Therefore a large amount of research has been conducted regarding nondestructive testing (NDT) and structural health monitoring (SHM) of CFRP materials. The principal objective of this research program was to develop methods to characterize failure mechanisms in CFRP materials used by the U.S. Army using acoustic emission (AE) and/or acousto-ultrasonic (AU) data. Failure mechanisms addressed include fiber breakage, matrix cracking, and delamination due to shear between layers. CFRP specimens were fabricated and tested in uniaxial tension to obtain AE and AU data. The specimens were designed with carbon fibers in different orientations to produce the different failure mechanisms. Some specimens were impacted with a blunt indenter prior to testing to simulate low-velocity impact. A signature analysis program was developed to characterize the AE data based on data examination using visual pattern recognition techniques. It was determined that it was important to characterize the AE event , using the location of the event as a parameter, rather than just the AE hit (signal recorded by an AE sensor). A back propagation neural network was also trained based on the results of the signature analysis program. Damage observed on the specimens visually with the aid of a scanning electron microscope agreed with the damage type assigned by the

  5. Studies of Matrix/Fiber Reinforced Composite Materials for the High Speed Research (HSR) Program

    NASA Technical Reports Server (NTRS)

    Orwoll, Robert A.

    1998-01-01

    The research on the curing mechanism of the phenylethynyl terminated imide matrix resins was the primary focus of this research. The ability to process high performance polymers into useful adhesives and high quality composites has been significantly advanced by synthetic techniques in which oligomers terminated with reactive groups cure or crosslink at elevated temperature after the article has been fabricated. The research used a variety of analytical techniques. Many stable products were isolated, and attempts at identification were made. This research was intended to provide fundamental insight into the molecular structure of these new engineering materials.

  6. Thermo-mechanical characterization of nano filled and fiber reinforced brake friction materials

    NASA Astrophysics Data System (ADS)

    Singh, Tej; Patnaik, Amar; Satapathy, Bhabani K.

    2013-06-01

    Brake friction materials filled with multiwalled carbon nanotubes (MWCNT) and nanoclay have been fabricated and characterize for thermo-mechanical properties. Thermo gravimetric analysis (TGA) show that the stability of the friction composites increased with increase in MWCNT and nanoclay contents. Dynamic mechanical analysis (DMA) of the composite have been carried out to characterize the storage modulus (E'), loss modulus (E″) and damping factor (Tan δ) as a function of temperature. The storage and loss modulus show a maxima at lower content of MWCNT and nanoclay.

  7. Tungsten fiber reinforced FeCralY: A first generation composite turbine blade material

    NASA Technical Reports Server (NTRS)

    Petrasek, D. W.; Winsa, E. A.; Westfall, L. J.; Signorelli, R. A.

    1979-01-01

    Tungsten-fiber/FeCrAlY (W/FeCrAlY) was identified as a promising aircraft engine, first generation, turbine blade composite material. Based on available data, W/FeCrAlY should have the stress-rupture, creep, tensile, fatigue, and impact strengths required for turbine blades operating from 1250 to 1370 K. It should also have adequate oxidation, hot corrosion, and thermal cycling damage resistance as well as high thermal conductivity. Concepts for potentially low cost blade fabrication were developed. These concepts were used to design a first stage JT9D convection cooled turbine blade having a calculated 50 K use-temperature advantage over the directionally solidified superalloy blade.

  8. Compressive strength of fiber reinforced composite materials. [composed of boron and epoxy

    NASA Technical Reports Server (NTRS)

    Davis, J. G., Jr.

    1974-01-01

    Results of an experimental and analytical investigation of the compressive strength of unidirectional boron-epoxy composite material are presented. Observation of fiber coordinates in a boron-epoxy composite indicates that the fibers contain initial curvature. Combined axial compression and torsion tests were conducted on boron-epoxy tubes, and it was shown that the shear modulus is a function of axial compressive stress. An analytical model which includes initial curvature in the fibers and permits an estimate of the effect of curvature on compressive strength is proposed. Two modes of failure which may result from the application of axial compressive stress are analyzed, delamination and shear instability. Based on tests and analysis, failure of boron-epoxy under axial compressive load is due to shear instability.

  9. An overview of long fiber reinforced thermoplastics

    SciTech Connect

    Bockstedt, R.J.; Skarlupka, R.J.

    1995-12-01

    Long fiber reinforced thermoplastics (LFRTP) are a class of injection molding materials that extend the physical property envelope of thermoplastics polymers. These materials are manufactured by pulling continuous fiber tows through a thermoplastic polymer melt in a specialized processing die. The strands are subsequently cooled and chopped into pellets of equal length. LFRTP materials are available in virtually every common thermoplastic resin with glass, aramid, stainless steel, or carbon fiber reinforcement at levels up to 60% by weight. Unlike short fiber reinforced thermoplastics manufactured by conventional screw compounding processes, LFRTP exhibit simultaneous improvements in both flexural modulus and impact resistance. Improvements in load transfer, creep resistance at elevated temperatures, and dimensional stability can also be attributed to the long fiber network formed in the molded part. This unique combination of properties makes LFRTP the material of choice for replacement of metal structural assemblies in many automotive, industrial, consumer and recreational applications.

  10. Resonant Ultrasound Spectroscopy, as Applied to Nondestructive Evaluation and Characterization of Carbon Fiber Reinforced Epoxy Composite Materials.

    NASA Astrophysics Data System (ADS)

    Whitney, Timothy Marvin

    1996-08-01

    Resonant ultrasound spectroscopy (RUS) can be an elegantly simple nondestructive evaluation tool. The resonance spectrum of any specimen is dependent on, and sensitive at ppm levels to, its density, geometry, elastic and thermal properties, and boundary conditions. The measurement of spectrum is fast, taking between 15 and 90 seconds with state-of-the-art instrumentation, making it appropriate for following properties as a function of temperature. Parts per million changes in specimen density, geometry, elastic moduli, temperature, and boundary conditions are detected with RUS. A novel apparatus is presented for driving and detecting the mechanical resonance of objects with major dimensions ranging from 0.1 cm to 33 cm. The noise floor of the apparatus is characterized using a high Q titanium alloy and a low Q graphite/epoxy composite. The apparatus is used to measure the amplitude/frequency resonance spectra of right rectangular parallelepiped (RRP) specimens of four different lay-ups of AS4/3501-6 carbon fiber reinforced epoxy (CFRE) composite material at room temperature and at one degree C intervals between -177^circC and 25 ^circC. It is important to know the mechanical properties of this material at low temperatures for underwater, polar, and space applications. The temperature dependence of the second order elastic moduli are calculated from the resonance spectra of the AS4/3501-6 RRPs. High power ultrasound is used to enhance the cure of AS4/3501-6 CFRE composite. Composite panels are insonified through the caul plate, by a high power ultrasonic horn, while curing. Stiffness enhancements of five percent are observed. The resonance spectrum of a steel caul plate is used to monitor the degree of cure of AS4/3501-6 CFRE composite panels in real time. Because the curing composite acts to change the boundary conditions, the resonance spectrum changes as the composite cures. RUS is used to screen a variety of high precision engineered parts for mechanical defects

  11. Microstructural characterization of fiber-reinforced composites

    SciTech Connect

    Summerscales, J.

    1998-12-31

    In the past 50 years, great progress has been made in developing artificial fiber-reinforced composite materials, generally using filaments with microscopic diameters. An array of reinforcement forms can be used in commercial applications--with the microstructure being a critical factor in realizing the required properties in a material. This book comprehensively examines the application of advanced microstructural characterization techniques to fiber-reinforced composites. Its contents include: (1) flexible textile composite microstructure; (2) 3-D confocal microscopy of glass fiber-reinforced composites; (3) geometric modeling of yarn and fiber assemblies; (4) characterization of yarn shape in woven fabric composites; (5) quantitative microstructural analysis for continuous fiber composites; (6) electron microscopy of polymer composites; (7) micromechanics of reinforcement using laser raman spectroscopy; and (8) acoustic microscopy of ceramic fiber composites.

  12. Tensile strength of fiber reinforced plastics at 77K irradiated by various radiation sources

    SciTech Connect

    Humer, K.; Weber, H.W.; Tschegg, E.K.; Egusa, S.; Birtcher, R.C.; Gerstenberg, H.

    1993-08-01

    The influence of radiation damage on the mechanical properties of fiber reinforced plastics (FRPs), which are considered as candidate materials for the insulation of superconducting magnets for nuclear fusion reactors, has been investigated. Different types of FRPs (epoxies, bismaleimides; two- and three-dimensional reinforcement structures with E-, S-, or T-glass fibers) has been included in the test program. Three aspects of our present results will be discussed in detail. The first is related to an assessment of the tensile strength and its radiation dependence under the influence of strongly varying radiation conditions. The second aspect refers to low temperature ({approx}5 K) reactor irradiation of selected materials. In this case, identical sets of tensile test samples were transferred into the tensile testing machine, one without warming-up to room temperature and the other after an annealing cycle to room temperature. Finally, a comparison between the radiation response of different materials is made. It turns out that the three-dimensionally reinforced bismaleimide shows the smallest degradation of its tensile properties under all irradiation conditions.

  13. Frequency-modulated thermal wave imaging for non-destructive testing of carbon fiber-reinforced plastic materials

    NASA Astrophysics Data System (ADS)

    Ghali, V. S.; Mulaveesala, R.; Takei, M.

    2011-10-01

    Phase-based methods of active thermographic studies provide deeper subsurface details and reduce non-uniform emissivity problems in defect detection. In this contribution analysis of subsurface anomalies has been carried out by probing a suitable frequency component with sufficient energy. This paper highlights the comparative analysis of different thermographic schemes on the basis of supplying equal energy to the chosen frequency used for the analysis of a given carbon fiber-reinforced plastic sample used in experimentation. Experiments have been carried out to find the detection ability of different excitation schemes, and comparisons have been made by taking the signal-to-noise ratio of the defects into consideration.

  14. Fiber reinforced superalloys

    NASA Technical Reports Server (NTRS)

    Petrasek, Donald W.; Signorelli, Robert A.; Caulfield, Thomas; Tien, John K.

    1987-01-01

    Improved performance of heat engines is largely dependent upon maximum cycle temperatures. Tungsten fiber reinforced superalloys (TFRS) are the first of a family of high temperature composites that offer the potential for significantly raising hot component operating temperatures and thus leading to improved heat engine performance. This status review of TFRS research emphasizes the promising property data developed to date, the status of TFRS composite airfoil fabrication technology, and the areas requiring more attention to assure their applicability to hot section components of aircraft gas turbine engines.

  15. Damping behavior of Discontinuous Fiber Reinforced Thermoplastic Composites

    NASA Astrophysics Data System (ADS)

    Haldar, Amit Kumar; Aggarwal, Ishan; Batra, N. K.

    2010-11-01

    Discontinuous fiber reinforced composites are being used in many antivibration applications due to their time and temperature dependent specific mechanical properties. For utilization of this material to specific engineering applications there is a need to understand the damping behavior of composites under dynamic loading. For this work, unreinforced and 20% long and short reinforced glass fiber polypropylene composite materials were tested for free transverse vibration damping characteristics under static as well as fatigue loading conditions. The damping characteristics are quantified by decay pattern and natural frequency. Presence of reinforced fibers increases the damping capacity. Among reinforcements, short fiber reinforced polypropylene shows increased damping capacity then long glass fiber reinforced polypropylene.

  16. Quantitative radiographic analysis of fiber reinforced polymer composites.

    PubMed

    Baidya, K P; Ramakrishna, S; Rahman, M; Ritchie, A

    2001-01-01

    X-ray radiographic examination of the bone fracture healing process is a widely used method in the treatment and management of patients. Medical devices made of metallic alloys reportedly produce considerable artifacts that make the interpretation of radiographs difficult. Fiber reinforced polymer composite materials have been proposed to replace metallic alloys in certain medical devices because of their radiolucency, light weight, and tailorable mechanical properties. The primary objective of this paper is to provide a comparable radiographic analysis of different fiber reinforced polymer composites that are considered suitable for biomedical applications. Composite materials investigated consist of glass, aramid (Kevlar-29), and carbon reinforcement fibers, and epoxy and polyether-ether-ketone (PEEK) matrices. The total mass attenuation coefficient of each material was measured using clinical X-rays (50 kev). The carbon fiber reinforced composites were found to be more radiolucent than the glass and kevlar fiber reinforced composites. PMID:11261603

  17. X-ray photoelectron spectroscopic studies of graphitic materials and interfacial interactions in carbon-fiber-reinforced polymer composites

    NASA Astrophysics Data System (ADS)

    Viswanathan, Hema L.

    This dissertation involves the X-ray photoelectron spectroscopic (XPS) study of the chemistry associated with carbon fiber-reinforced composites fabricated using PAN-based carbon fibers and a thermoplastic polyimide resin. The mechanical properties of the ultimate composite are significantly affected by the nature of the fiber/matrix interface. Interfacial interaction can be promoted by the electrochemical modification of the fiber surface. The determination of carbon fiber microstructure was conducted through angle-resolved valence band photoemission studies of highly ordered graphite. The change in orientation of the basal planes and reactive edge sites with take-off angle provided a method for the determination of surface microstructure. The electronic structure of solid-state graphite was described using a band structure model and the results obtained were compared with the multiple scattered wave X a calculations. PAN-based fibers were electrochemically oxidized and studied using monochromatic X-radiation. The extremely narrow natural linewidth of the monochromatized Al K a radiation allowed previously unresolved features to be seen. In addition, sample decomposition due to radiative heat from the X-ray source is eliminated. Fibers that were pretreated by the manufacturer were subjected to further electrochemical oxidation. The fibers behaved in an erratic and non-reproducible manner. The surface treatment was removed by heating the fibers in vacuum, followed by XPS analysis and electrochemical oxidation. The fiber/matrix interface was simulated by coating a very thin layer of the polyimide resin on the surface of the fiber followed by XPS analysis. The validity of a proposed structure for the resin was confirmed by comparison with ab initio calculations conducted on the resin repeat unit. A high level of fiber/matrix interaction was observed for electrochemically oxidized fibers. The possibility of solvent interaction with the fiber surface was eliminated by

  18. Bismaleimide compounds

    DOEpatents

    Adams, Johnnie E.; Jamieson, Donald R.

    1986-01-14

    Bismaleimides of the formula ##STR1## wherein R.sub.1 and R.sub.2 each independently is H, C.sub.1-4 -alkyl, C.sub.1-4 -alkoxy, C1 or Br, or R.sub.1 and R.sub.2 together form a fused 6-membered hydrocarbon aromatic ring, with the proviso that R.sub.1 and R.sub.2 are not t-butyl or t-butoxy; X is O, S or Se; n is 1-3; and the alkylene bridging group, optionally, is substituted by 1-3 methyl groups or by fluorine, form polybismaleimide resins which have valuable physical properties. Uniquely, these compounds permit extended cure times, i.e., they remain fluid for a time sufficient to permit the formation of a homogeneous melt prior to curing.

  19. Bismaleimide compounds

    DOEpatents

    Adams, J.E.; Jamieson, D.R.

    1986-01-14

    Bismaleimides of the formula shown in the diagram wherein R[sub 1] and R[sub 2] each independently is H, C[sub 1-4]-alkyl, C[sub 1-4]-alkoxy, Cl or Br, or R[sub 1] and R[sub 2] together form a fused 6-membered hydrocarbon aromatic ring, with the proviso that R[sub 1] and R[sub 2] are not t-butyl or t-butoxy; X is O, S or Se; n is 1--3; and the alkylene bridging group, optionally, is substituted by 1--3 methyl groups or by fluorine, form polybismaleimide resins which have valuable physical properties. Uniquely, these compounds permit extended cure times, i.e., they remain fluid for a time sufficient to permit the formation of a homogeneous melt prior to curing.

  20. Fiber reinforced hybrid phenolic foam

    NASA Astrophysics Data System (ADS)

    Desai, Amit

    Hybrid composites in recent times have been developed by using more than one type of fiber reinforcement to bestow synergistic properties of the chosen filler and matrix and also facilitating the design of materials with specific properties matched to end use. However, the studies for hybrid foams have been very limited because of problems related to fiber dispersion in matrix, non uniform mixing due to presence of more than one filler and partially cured foams. An effective approach to synthesize hybrid phenolic foam has been proposed and investigated here. Hybrid composite phenolic foams were reinforced with chopped glass and aramid fibers in varied proportions. On assessing mechanical properties in compression and shear several interesting facts surfaced but overall hybrid phenolic foams exhibited a more graceful failure, greater resistance to cracking and were significantly stiffer and stronger than foams with only glass and aramid fibers. The optimum fiber ratio for the reinforced hybrid phenolic foam system was found to be 1:1 ratio of glass to aramid fibers. Also, the properties of hybrid foam were found to deviate from rule of mixture (ROM) and thus the existing theories of fiber reinforcement fell short in explaining their complex behavior. In an attempt to describe and predict mechanical behavior of hybrid foams a statistical design tool using analysis of variance technique was employed. The utilization of a statistical model for predicting foam properties was found to be an appropriate tool that affords a global perspective of the influence of process variables such as fiber weight fraction, fiber length etc. on foam properties (elastic modulus and strength). Similar approach could be extended to study other fiber composite foam systems such as polyurethane, epoxy etc. and doing so will reduce the number of experimental iterations needed to optimize foam properties and identify critical process variables. Diffusivity, accelerated aging and flammability

  1. Self-cleaning and depollution of fiber reinforced cement materials modified by neutral TiO2/SiO2 hydrosol photoactive coatings

    NASA Astrophysics Data System (ADS)

    Wang, Jian; Lu, ChunHua; Xiong, JiRu

    2014-04-01

    Environmental pollution has an evidently adverse impact on the buildings that are constructed by the glass fiber reinforced cement (GRC) materials. In the present work, the stable, neutral TiO2/SiO2 hydrosols were prepared by using the Ti(SO4)2 as titanium source, HNO3 as peptizing agent, and SiO2 as stabilizer through a simple and low cost process. The morphologies and structures of TiO2/SiO2 hydrosol were further characterized by the TEM, SEM, XRD, and FTIR measurement. In the synthetic hydrosol, lots of nanoparticles with the diameters in the range of 10-20 nm can be observed. Tisbnd Osbnd Si band were formed, as observed from the FTIR spectrum. The Na2O·SiO2 was detected from the SEM. After drying the TiO2/SiO2 hydrosol, the XRD shown that the TiO2 has an anatase structure and the SiO2 is amorphous. The TiO2/SiO2 hydrosol can be compactly coated on the GRC surface due to the existence of Na2O·SiO2 binder and exhibited high photocatalytic activity and stability in the degradation of Rhodamine B.

  2. Fiber-Reinforced Composite Foam

    Technology Transfer Automated Retrieval System (TEKTRAN)

    A two-phase method for making fiber-reinforced compositions was developed to achieve uniform fiber dispersion in a composite matrix. The first phase involved mixing together water, fibers, and a portion of a fiber dispersant to form a viscous composition. The high viscosity imparted by the dispersa...

  3. Fiber-Reinforced Superalloys For Rocket Engines

    NASA Technical Reports Server (NTRS)

    Lewis, Jack R.; Yuen, Jim L.; Petrasek, Donald W.; Stephens, Joseph R.

    1990-01-01

    Report discusses experimental studies of fiber-reinforced superalloy (FRS) composite materials for use in turbine blades in rocket engines. Intended to withstand extreme conditions of high temperature, thermal shock, atmospheres containing hydrogen, high cycle fatigue loading, and thermal fatigue, which tax capabilities of even most-advanced current blade material - directionally-solidified, hafnium-modified MAR M-246 {MAR M-246 (Hf) (DS)}. FRS composites attractive combination of properties for use in turbopump blades of advanced rocket engines at temperatures from 870 to 1,100 degrees C.

  4. Methods for an investigation of the effect of material components on the mechanical characteristics of glass-fiber-reinforced plastics

    NASA Technical Reports Server (NTRS)

    Willax, H. O.

    1980-01-01

    The materials used in the production of glass reinforced plastics are discussed. Specific emphasis is given to matrix polyester materials, the reinforcing glass materials, and aspects of specimen preparation. Various methods of investigation are described, giving attention to optical impregnation and wetting measurements and the gravimetric determination of the angle of contact. Deformation measurements and approaches utilizing a piezoelectric device are also considered.

  5. Strength of anisotropic wood and synthetic materials. [plywood, laminated wood plastics, glass fiber reinforced plastics, polymeric film, and natural wood

    NASA Technical Reports Server (NTRS)

    Ashkenazi, Y. K.

    1981-01-01

    The possibility of using general formulas for determining the strength of different anisotropic materials is considered, and theoretical formulas are applied and confirmed by results of tests on various nonmetallic materials. Data are cited on the strength of wood, plywood, laminated wood plastics, fiber glass-reinforced plastics and directed polymer films.

  6. Mechanical recycling of continuous fiber-reinforced thermoplastic sheets

    NASA Astrophysics Data System (ADS)

    Moritzer, Elmar; Heiderich, Gilmar

    2016-03-01

    This contribution examines possible material recycling of offcuts generated during the production of continuous-fiber-reinforced composite sheets. These sheets consist of a polyamide 6 matrix and glass fiber fabric. In the initial step, the offcut is shredded to obtain particles; following that, the particles are processed in a twin-screw process to produce fiber-reinforced plastic pellets with varying fiber contents. These pellets are intended for use in injection molding processes as a substitution for new raw materials. This investigation centers on the mechanical properties which can be achieved with the recycled material after both the twin-screw process and injection molding.

  7. Fiber reinforced composite resin systems.

    PubMed

    Giordano, R

    2000-01-01

    The Targis/Vectris and Sculpture/FibreKor systems were devised to create a translucent maximally reinforced resin framework for fabrication of crowns, bridges, inlays, and onlays. These materials are esthetic, have translucency similar to castable glass-ceramics such as OPC and Empress, and have fits that are reported to be acceptable in clinical and laboratory trials. These restorations rely on proper bonding to the remaining tooth structure; therefore, careful attention to detail must be paid to this part of the procedure. Cementation procedures should involve silane treatment of the cleaned abraded internal restoration surface, application of bonding agent to the restoration as well as the etched/primed tooth, and finally use of a composite resin. Each manufacturer has a recommended system which has been tested for success with its resin system. These fiber reinforced resins are somewhat different than classical composites, so not all cementation systems will necessarily work with them. Polishing of the restoration can be accomplished using diamond or alumina impregnated rubber wheels followed by diamond paste. The glass fibers can pose a health risk. They are small enough to be inhaled and deposited in the lungs, resulting in a silicosis-type problem. Therefore, if fibers are exposed and ground on, it is extremely important to wear a mask. Also, the fibers can be a skin irritant, so gloves also should be worn. If the fibers become exposed intraorally, they can cause gingival inflammation and may attract plaque. The fibers should be covered with additional composite resin. If this cannot be accomplished, the restoration should be replaced. The bulk of these restorations are formed using a particulate filled resin, similar in structure to conventional composite resins. Therefore, concerns as to wear resistance, color stability, excessive expansion/contraction, and sensitivity remain until these materials are proven in long-term clinical trials. They do hold the

  8. The thermal and mechanical properties of a low-density glass-fiber-reinforced elastomeric ablation material

    NASA Technical Reports Server (NTRS)

    Engelke, W. T.; Robertson, R. W.; Bush, A. L.; Pears, C. D.

    1974-01-01

    An evaluation of the thermal and mechanical properties was performed on a molded low-density elastomeric ablation material designated as Material B. Both the virgin and charred states were examined to provide meaningful inputs to the design of a thermal protection system. Chars representative of the flight chars formed during ablation were prepared in a laboratory furnace from 600 K to 1700 K and properties of effective thermal conductivity, heat capacity, porosity and permeability were determined on the furnace chars formed at various temperature levels within the range. This provided a boxing of the data which will enable the prediction of the transient response of the material during flight ablation.

  9. Effect of different palatal vault shapes on the dimensional stability of glass fiber-reinforced heat-polymerized acrylic resin denture base material

    PubMed Central

    Dalkiz, Mehmet; Arslan, Demet; Tuncdemir, Ali Riza; Bilgin, M.Selim; Aykul, Halil

    2012-01-01

    Objective: The aim of this study was to determine the effect of different palatal vault shapes on the dimensional stability of a glass fiber reinforced heat polymerized acrylic resin denture base material. Methods: Three edentulous maxilla with shallow, deep and medium shaped palatal vaults were selected and elastomeric impressions were obtained. A maxillary cast with four reference points (A, B, C, and D) was prepared to serve as control. Point (A) was marked in the anterior midline of the edentulous ridge in the incisive papillary region, points (B) and (C) were marked in the right and left posterior midlines of the edentulous ridge in the second molar regions, and point (D) was marked in the posterior palatal midline near the fovea palatina media (Figure 2). To determine linear dimensional changes, distances between four reference points (A–B, A–C, A–D and B–C) were initially measured with a metal gauge accurate within 0.1 mm under a binocular stereo light microscope and data (mm) were recorded. Results: No significant difference of interfacial distance was found in sagittal and frontal sections measured 24 h after polymerization and after 30 days of water storage in any of experimental groups (P>.05). Significant difference of linear dimension were found in all experimental groups (P<.01) between measurements made 24 h after polymerization of specimens and 30 days after water storage. Conclusion: Palatal vault shape and fiber impregnation into the acrylic resin bases did not affect the magnitude of interfacial gaps between the bases and the stone cast surfaces. PMID:22229010

  10. Response of fiber reinforced sandwich structures subjected to explosive loading

    SciTech Connect

    Perotti, Luigi E.; El Sayed, Tamer; Deiterding, Ralf; Ortiz, Michael

    2011-01-01

    The capability to numerically simulate the response of sandwich structures to explosive loading constitutes a powerful tool to analyze and optimize their design by investigating the influence of different parameters. In order to achieve this objective, the necessary models for foam core and fiber reinforced materials in finite kinematics have been developed together with a finite element scheme which includes C1 finite elements for shells and cohesive elements able to capture the fracture propagation in composite fiber reinforced materials. This computational capability has been used to investigate the response of fiber reinforced sandwich shells to explosive loading. Based on the dissipated fracture energy resulting from these simulations, a factorial design has been carried out to assess the effect of different parameters on the sandwich shell response creating a tool for its optimization.

  11. Evaluation of Fiber Reinforced Cement Using Digital Image Correlation

    PubMed Central

    Melenka, Garrett W.; Carey, Jason P.

    2015-01-01

    The effect of short fiber reinforcements on the mechanical properties of cement has been examined using a splitting tensile – digital image correlation (DIC) measurement method. Three short fiber reinforcement materials have been used in this study: fiberglass, nylon, and polypropylene. The method outlined provides a simple experimental setup that can be used to evaluate the ultimate tensile strength of brittle materials as well as measure the full field strain across the surface of the splitting tensile test cylindrical specimen. Since the DIC measurement technique is a contact free measurement this method can be used to assess sample failure. PMID:26039590

  12. Evaluation of fiber reinforced cement using digital image correlation.

    PubMed

    Melenka, Garrett W; Carey, Jason P

    2015-01-01

    The effect of short fiber reinforcements on the mechanical properties of cement has been examined using a splitting tensile - digital image correlation (DIC) measurement method. Three short fiber reinforcement materials have been used in this study: fiberglass, nylon, and polypropylene. The method outlined provides a simple experimental setup that can be used to evaluate the ultimate tensile strength of brittle materials as well as measure the full field strain across the surface of the splitting tensile test cylindrical specimen. Since the DIC measurement technique is a contact free measurement this method can be used to assess sample failure. PMID:26039590

  13. Full Mouth Oral Rehabilitation by Maxillary Implant Supported Hybrid Denture Employing a Fiber Reinforced Material Instead of Conventional PMMA

    PubMed Central

    Qamheya, Ala Hassan A.; Yeniyol, Sinem; Arısan, Volkan

    2015-01-01

    Many people have life-long problems with their dentures, such as difficulties with speaking and eating, loose denture, and sore mouth syndrome. The evolution of dental implant supported prosthesis gives these patients normal healthy life for their functional and esthetic advantages. This case report presents the fabrication of maxillary implant supported hybrid prosthesis by using Nanofilled Composite (NFC) material in teeth construction to rehabilitate a complete denture wearer patient. PMID:26557392

  14. The mechanics of delamination in fiber-reinforced composite materials. II - The delamination behavior and fracture mechanics parameters

    NASA Technical Reports Server (NTRS)

    Wang, S. S.; Choi, I.

    1983-01-01

    Based on theories of laminate anisotropic elasticity and interlaminar fracture, the complete solution structure associated with a composite delamination is determined. Fracture mechanics parameters characterizing the interlaminar crack behavior are defined from asymptotic stress solutions for delaminations with different crack-tip deformation configurations. A numerical method employing singular finite elements is developed to study delaminations in fiber composites with any arbitrary combinations of lamination, material, geometric, and crack variables. The special finite elements include the exact delamination stress singularity in its formulation. The method is shown to be computationally accurate and efficient, and operationally simple. To illustrate the basic nature of composite delamination, solutions are shown for edge-delaminated (0/-0/-0/0) and (+ or - 0/+ or - 0/90/90 deg) graphite-epoxy systems under uniform axial extension. Three-dimensional crack-tip stress intensity factors, associated energy release rates, and delamination crack-closure are determined for each individual case. The basic mechanics and mechanisms of composite delamination are studied, and fundamental characteristics unique to recently proposed tests for interlaminar fracture toughness of fiber composite laminates are examined. Previously announced in STAR as N84-13222

  15. The mechanics of delamination in fiber-reinforced composite materials. Part 2: Delamination behavior and fracture mechanics parameters

    NASA Technical Reports Server (NTRS)

    Wang, S. S.; Choi, I.

    1983-01-01

    Based on theories of laminate anisotropic elasticity and interlaminar fracture, the complete solution structure associated with a composite delamination is determined. Fracture mechanics parameters characterizing the interlaminar crack behavior are defined from asymptotic stress solutions for delaminations with different crack-tip deformation configurations. A numerical method employing singular finite elements is developed to study delaminations in fiber composites with any arbitrary combinations of lamination, material, geometric, and crack variables. The special finite elements include the exact delamination stress singularity in its formulation. The method is shown to be computationally accurate and efficient, and operationally simple. To illustrate the basic nature of composite delamination, solutions are shown for edge-delaminated (0/-0/-0/0) and (+ or - 0/+ or - 0/90/90 deg) graphite-epoxy systems under uniform axial extenstion. Three-dimensional crack-tip stress intensity factors, associated energy release rates, and delamination crack-closure are determined for each individual case. The basic mechanics and mechanisms of composite delamination are studied, and fundamental characteristics unique to recently proposed tests for interlaminar fracture toughness of fiber composite laminates are examined.

  16. Fiber-reinforced composites in fixed partial dentures

    PubMed Central

    Vallittu, Pekka

    2006-01-01

    Fiber-reinforced composite resin (FRC) prostheses offer the advantages of good aesthetics, minimal invasive treatment, and an ability to bond to the abutment teeth, thereby compensating for less-than-optimal abutment tooth retention and resistance form. These prostheses are composed of two types of composite materials: fiber composites to build the framework and hybrid or microfill particulate composites to create the external veneer surface. This review concentrates on the use of fiber reinforcement in the fabrication of laboratory or chairsidemade composite-fixed partial dentures of conventional preparation. Other applications of FRC in dentistry are briefly mentioned. The possibilities fiber reinforcement technology offers must be emphasized to the dental community. Rather than limiting discussion to whether FRC prostheses will replace metal-ceramic or full-ceramic prostheses, attention should be focused on the additional treatment options brought by the use of fibers. However, more clinical experience is needed. PMID:21526023

  17. Effect of reinforcement and fiber-matrix interface on dynamic fracture of fiber-reinforced composite materials

    SciTech Connect

    Khanna, S.K.

    1992-01-01

    The experimental technique of dynamic photoelasticity coupled with high speed photography has been used to study the interaction of running cracks with brittle and ductile fibers embedded in a brittle polymeric matrix. The effect of reinforcement and the fiber-matrix interface on dynamic stress intensity factor, crack bridging phenomena, crack surface morphology and toughening mechanisms occurring during dynamic fracturing of reinforced brittle matrix composites has been investigated. It is found that reinforcement reduces the crack velocity and the stress intensity factor. Thus the energy supplied to the crack tip is reduced resulting in reduction of the crack jump distance. Fiber pullout experiments were done to characterize the fiber-matrix interface. Rapid pullout results in an increase in interface shear strength. For rapid pullout of fibers the difference between maximum pullout loads. for well and weakly bonded fibers, is much smaller than for very slow pullout. A fiber-matrix interface which is weaker in the vicinity of the crack path, termed the partly debonded interface, produces higher crack closing forces and lower stress intensity factor compared to well bonded fibers. The former interface condition results in low fracture energy and shorter crack jump compared to the later. The interface condition significantly affects the fracture surface morphology. The fracture surface roughness is lower for reinforced materials compared to monolithic. Further the partly debonded fibers result in lower surface roughness compared to the well bonded fibers. Inclined fibers with various interface conditions have no significant effect on the stress intensity factor. The fiber debonded length, however, decreases, as compared to fibers which are aligned with the loading direction, due to the kinking of the fibers.

  18. Ceramic fiber reinforced filter

    DOEpatents

    Stinton, David P.; McLaughlin, Jerry C.; Lowden, Richard A.

    1991-01-01

    A filter for removing particulate matter from high temperature flowing fluids, and in particular gases, that is reinforced with ceramic fibers. The filter has a ceramic base fiber material in the form of a fabric, felt, paper of the like, with the refractory fibers thereof coated with a thin layer of a protective and bonding refractory applied by chemical vapor deposition techniques. This coating causes each fiber to be physically joined to adjoining fibers so as to prevent movement of the fibers during use and to increase the strength and toughness of the composite filter. Further, the coating can be selected to minimize any reactions between the constituents of the fluids and the fibers. A description is given of the formation of a composite filter using a felt preform of commercial silicon carbide fibers together with the coating of these fibers with pure silicon carbide. Filter efficiency approaching 100% has been demonstrated with these filters. The fiber base material is alternately made from aluminosilicate fibers, zirconia fibers and alumina fibers. Coating with Al.sub.2 O.sub.3 is also described. Advanced configurations for the composite filter are suggested.

  19. An Assessment of Self-Healing Fiber Reinforced Composites

    NASA Technical Reports Server (NTRS)

    Smith, Joseph G., Jr.

    2012-01-01

    Several reviews and books have been written concerning self-healing polymers over the last few years. These have focused primarily on the types of self-healing materials being studied, with minor emphasis given to composite properties. The purpose of this review is to assess the self-healing ability of these materials when utilized in fiber reinforced composites

  20. Fire test method for graphite fiber reinforced plastics

    NASA Technical Reports Server (NTRS)

    Bowles, K. J.

    1980-01-01

    A potential problem in the use of graphite fiber reinforced resin matrix composites is the dispersal of graphite fibers during accidential fires. Airborne, electrically conductive fibers originating from the burning composites could enter and cause shorting in electrical equipment located in surrounding areas. A test method for assessing the burning characteristics of graphite fiber reinforced composites and the effectiveness of the composites in retaining the graphite fibers has been developed. The method utilizes a modified rate of heat release apparatus. The equipment and the testing procedure are described. The application of the test method to the assessment of composite materials is illustrated for two resin matrix/graphite composite systems.

  1. Fire test method for graphite fiber reinforced plastics

    NASA Technical Reports Server (NTRS)

    Bowles, K. J.

    1980-01-01

    A potential problem in the use of graphite fiber reinforced resin matrix composites is the dispersal of graphite fibers during accidental fires. Airborne, electrically conductive fibers originating from the burning composites could enter and cause shorting in electrical equipment located in surrounding areas. A test method for assessing the burning characteristics of graphite fiber reinforced composites and the effectiveness of the composites in retaining the graphite fibers has been developed. The method utilizes a modified Ohio State University Rate of Heat Release apparatus. The equipment and the testing procedure are described. The application of the test method to the assessment of composite materials is illustrated for two resin matrix/graphite composite systems.

  2. Quality assurance of glass fiber reinforced piping systems

    SciTech Connect

    Ende, C.A.M. van den; Bruijn, J.C.M. de

    1997-12-01

    Resin based glass fiber reinforced plastic piping systems have been in use for over 30 years in a variety of industrial purposes, e.g. cooling and potable water, crude oil, gas, etc. Glass fiber reinforced piping systems have considerable advantages over alternative materials for piping systems. This is mainly due to their high corrosion resistance. The use of GRP pipes is limited due to the lack of quality assurance. As with other piping systems the joint is the weakest point. The paper describes the effort made towards a better quality control and understanding of the failure through determination of acceptance criteria and development of nondestructive testing methods for adhesively bounded joints.

  3. Graphite fiber reinforced glass matrix composites for aerospace applications

    NASA Technical Reports Server (NTRS)

    Prewo, K. M.; Bacon, J. F.; Dicus, D. L.

    1979-01-01

    The graphite fiber reinforced glass matrix composite system is described. Although this composite is not yet a mature material, it possesses low density, attractive mechanical properties at elevated temperatures, and good environmental stability. Properties are reported for a borosilicate glass matrix unidirectionally reinforced with 60 volume percent HMS graphite fiber. The flexural strength and fatigue characteristics at room and elevated temperature, resistance to thermal cycling and continuous high temperature oxidation, and thermal expansion characteristics of the composite are reported. The properties of this new composite are compared to those of advanced resin and metal matrix composites showing that graphite fiber reinforced glass matrix composites are attractive for aerospace applications.

  4. Micromechanical analysis of fiber-reinforced composites with interfacial phenomena. I - Modeling and analysis of discontinuous fiber-reinforced composites

    NASA Astrophysics Data System (ADS)

    Saito, Kenji; Iwamoto, Masaharu; Araki, Shigetoshi; Yano, Tadayoshi

    1992-04-01

    A mechanical analysis is presented of fiber-reinforced composite material exhibiting matrix cracking and/or interface sliding between a fiber and a matrix, i.e., the problem of a bridging fiber, by the method of micromechanics. In the case where there are many kinds of inhomogeneities, the interaction between the inhomogeneities, which are neglected in Eshelby's (1961) generally used method, must be taken into consideration. The present method is the extension of the method of Taya and Chou (1981) to the analysis of fiber-reinforced composites with interfacial sliding.

  5. Graphite fiber reinforced thermoplastic resins

    NASA Technical Reports Server (NTRS)

    Novak, R. C.

    1975-01-01

    Mechanical properties of neat resin samples and graphite fiber reinforced samples of thermoplastic resins were characterized with particular emphasis directed to the effects of environmental exposure (humidity, temperature and ultraviolet radiation). Tensile, flexural, interlaminar shear, creep and impact strengths were measured for polysulfone, polyarylsulfone and a state-of-the-art epoxy resin samples. In general, the thermoplastic resins exhibited environmental degradation resistance equal to or superior to the reference epoxy resin. Demonstration of the utility and quality of a graphite/thermoplastic resin system was accomplished by successfully thermoforming a simulated compressor blade and a fan exit guide vane.

  6. Covering of fiber-reinforced composite bars by adhesive materials, is it necessary to improve the bond strength of lingual retainers?

    PubMed Central

    Heravi, Farzin; Kerayechian, Navid; Moazzami, Saied Mostafa; Shafaee, Hooman; Heravi, Parya

    2015-01-01

    Objectives: The objectives were to evaluate the shear bond strength (SBS) of fiber-reinforced composite (FRC) retainers when bonding them to teeth with and without covering the FRC bars using two different adhesive systems. Materials and Methods: Hundred and twenty extracted human maxillary premolars were randomly divided into eight groups (n = 15). FRC bars (4 mm length, Everstick Ortho®, Stick Tech, Oy, Turku, Finland) were bonded to the proximal (distal) surfaces of the teeth using two different adhesives (Tetric Flow [TF, Ivoclar Vivadent, Switzerland] and resin-modified glass ionomer cement [RMGIC, ODP, Vista, CA, USA]) with and without covering with the same adhesive. Specimens were exposed to thermocycling (625 cycles per day [5–55°C, intervals: 30 s] for 8 days). The SBS test was then performed using the universal testing machine (Zwick, GMBH, Ulm, Germany). After debonding, the remaining adhesive on the teeth was recorded by the adhesive remnant index (0–3). Results: The lowest mean SBS (standard deviation) was found in the TF group without covering with adhesive (12.6 [2.11] MPa), and the highest bond strength was in the TF group with covering with adhesive (16.01 [1.09] MPa). Overall, the uncovered RMGIC (15.65 [3.57] MPa) provided a higher SBS compared to the uncovered TF. Covering of FRC with TF led to a significant increase in SBS (P = 0.001), but this was not true for RMGIC (P = 0.807). Thermal cycling did not significantly change the SBS values (P = 0.537). Overall, eight groups were statistically different (ANOVA test, F = 3.32, P = 0.034), but no significant differences in bond failure locations were found between the groups (Fisher's exact tests, P = 0.92). Conclusions: The present findings showed no significant differences between SBS of FRC bars with and without covering by RMGIC. However, when using TF, there was a significant difference in SBS measurements between covering and noncovering groups. Therefore, the use of RMGIC without

  7. Tungsten fiber reinforced superalloys - A status review

    NASA Technical Reports Server (NTRS)

    Petrasek, D. W.; Signorelli, R. A.

    1981-01-01

    After a review of refractory metal fiber/alloy matrix composite development, a discussion is presented of the fabrication techniques used in production of tungsten fiber reinforced superalloys (TFRS), their most significant properties, and their potential applications in the hot section components of gas turbine engines. Emphasis is given the development of airfoil-fabrication technology, with a view to the production of TFRS turbine blades, and attention is given the first-generation TFRS material, a tungsten alloy fiber/FeCrAlY composite currently under evaluation. Detailed properties, design criteria and cost data are presented for this material. Among the properties covered are stress-rupture strength, high and low cycle fatigue, thermal fatigue, impact strength, oxidation and corrosion and thermal conductivity.

  8. Fiber Reinforced Composite Cores and Panels

    NASA Technical Reports Server (NTRS)

    Day, Stephen W. (Inventor); Campbell, G. Scott (Inventor); Tilton, Danny E. (Inventor); Stoll, Frederick (Inventor); Sheppard, Michael (Inventor); Banerjee, Robin (Inventor)

    2013-01-01

    A fiber reinforced core panel is formed from strips of plastics foam helically wound with layers of rovings to form webs which may extend in a wave pattern or may intersect transverse webs. Hollow tubes may replace foam strips. Axial rovings cooperate with overlying helically wound rovings to form a beam or a column. Wound roving patterns may vary along strips for structural efficiency. Wound strips may alternate with spaced strips, and spacers between the strips enhance web buckling strength. Continuously wound rovings between spaced strips permit folding to form panels with reinforced edges. Continuously wound strips are helically wrapped to form annular structures, and composite panels may combine both thermoset and thermoplastic resins. Continuously wound strips or strip sections may be continuously fed either longitudinally or laterally into molding apparatus which may receive skin materials to form reinforced composite panels.

  9. Toughness of fiber reinforced shotcrete

    SciTech Connect

    Morgan, D.R.; Chen, L.; Beaupre, D.

    1995-12-31

    Fibers are added to shotcrete to improve energy absorption and impact resistance, to provide crack resistance and crack control, and to provide apparent ductility, i.e., an ability to continue to carry load after the shotcrete matrix has cracked. In order to be able to quantify the benefits of fiber addition, a variety of different toughness measuring systems have been developed in different countries. Most commonly used are flexural toughness systems which determine load vs. deflection responses and relate the area under the curve to some absolute or dimensionless index energy parameter. In North America the ASTM C1018 test method is most commonly used. In Japan the JSCE-SF4 test procedure is used. A variety of procedures have been used in Europe, but the template approach of the Norwegian Guidelines NBP No. 7, seems to be finding favor. This paper briefly assesses the relative advantages and disadvantages of the various methods of characterizing toughness. It then provides recommendations for a new procedure which uses the ASTM C1018 test method for generating the flexural load vs. deflection curve, but analyzes the data using a modified version of the Norwegian template approach. The load vs. deflection curve is directly compared against four residual strength curves and the fiber reinforced shotcrete assigned one of four toughness performance levels. It is believed that this new procedure should provide suitable within and between laboratory reproducibility and be more suitable for purposes of differentiating between different fiber types and addition rates and specifying toughness for fiber reinforced shotcrete products than any of the existing methods.

  10. Forming of fiber reinforced thermoplastic sheets

    SciTech Connect

    Bhattacharyya, D.; Burt, C.R.; Martin, T.A.

    1993-12-31

    The development of fiber reinforced thermoplastic (FRTP) sheets has added a new dimension to the manufacturing industry. The ability of the thermoplastic matrix to soften and melt with the application of heat allows secondary processing of these composites. The material can be formed into components using conventional sheet metal forming processes with necessary modification. Ideally this opens the way for low cycle-time, non-labor intensive manufacturing processes. However, before there can be any wide scale application of the fiber reinforced sheet material, a better understanding is required regarding the formability of these reinforced sheets and the parameters influencing their forming characteristics. In sheet metal industry the term formability is described as the ease of forming and can be judged by various factors which may vary with the needs of a particular manufacturer. It is not always easy to prejudge formability as in many instances the actual sheet forming mechanism is quite complex. However, often a reasonable understanding of the process characteristics can be obtained through some relatively simple laboratory experiments. The present paper describes the results of a series of such tests namely hemispherical dome forming, cup drawing and vee bending using mainly polypropylene/glass fiber composite sheets with various fiber architecture, forming temperature and speed. Grid strain analysis has been applied to measure the magnitudes and directions of the principal strains and how they are influenced by fiber orientation. A kinematic approach has been shown to theoretically predict the deformation pattern with reasonable accuracy. Some salient features such as fiber buckling, sheet wrinkling, springback have been discussed in the context of forming process variables.

  11. Bismaleimide Copolymer Matrix Resins

    NASA Technical Reports Server (NTRS)

    Parker, John A.; Heimbuch, Alvin H.; Hsu, Ming-Ta S.; Chen, Timothy S.

    1987-01-01

    Graphite composites, prepared from 1:1 copolymer of two new bismaleimides based on N,N'-m-phenylene-bis(m-amino-benzamide) structure have mechanical properties superior to those prepared from other bismaleimide-type resins. New heat-resistant composites replace metal in some structural applications. Monomers used to form copolymers with superior mechanical properties prepared by reaction of MMAB with maleic or citraconic anhydride.

  12. Experimental study on mixed mode fracture in unidirectional fiber reinforced composites

    NASA Astrophysics Data System (ADS)

    Gong, Kezhuang; Li, Zheng; Fu, Bin

    2008-11-01

    Fiber reinforced composites are applied broadly in aeronautic and astronautic fields as a structural material. But the investigation in dynamic fracture behavior of fiber reinforced composite stands in the breach for scientists due to a large number of aircraft disasters. In this paper, the mixed mode fracture problems in fiber reinforced composites under impact are studied. First, based on the theory of the reflective dynamic caustic method for mixed mode fracture, corresponding experiments are carried out to study the dynamic fracture behaviors of unidirectional fiber reinforced composites under two kinds load conditions. By recording and analyzing the shadow spot patterns during the crack propagation process carefully, the dynamic fracture toughness and crack growth velocity of fiber reinforced composites are obtained. Via the observation of the crack growth routes and fracture sections, we further reveal the fracture mechanism of unidirectional fiber reinforced composites. It concludes that opening mode still is the easier fracture type for the pre-crack initiation in fiber reinforced composites, while the interface between fibers and matrix becomes the fatal vulnerability during the crack propagation.

  13. Fiber reinforced superalloys for rocket engines

    NASA Technical Reports Server (NTRS)

    Petrasek, Donald W.; Stephens, Joseph R.

    1989-01-01

    High pressure turbopumps for advanced reusable liquid propellant rocket engines such as that for the Space Shuttle Main Engine (SSME) require turbine blade materials that operate under extreme conditions of temperature, hydrogen environment, high-cycle fatigue loading, thermal fatigue and thermal shock. Such requirements tax the capabilities of current blade materials. Based on projections of properties for tungsten fiber reinforced superalloy (FRS) composites, it was concluded that FRS turbine blades offer the potential of a several fold increase in life and over a 200 C increase in temperature capability over the current SSME blade material. FRS composites were evaluated with respect to mechanical property requirements for SSME blade applications. Compared to the current blade material, the thermal shock resistance of FRS materials is excellent, two to nine times better, and their thermal fatigue resistance is equal to or higher than the current blade material. FRS materials had excellent low and high-cycle fatigue strengths, and thermal shock-induced surface microcracks had no influence on their fatigue strength. The material also exhibited negligible embrittlement when exposed to a hydrogen environment.

  14. Fiber reinforced superalloys for rocket engines

    NASA Technical Reports Server (NTRS)

    Petrasek, Donald W.; Stephens, Joseph R.

    1988-01-01

    High-pressure turbopumps for advanced reusable liquid-propellant rocket engines such as that for the Space Shuttle Main Engine (SSME) require turbine blade materials that operate under extreme conditions of temperature, hydrogen environment, high-cycle fatigue loading, thermal fatigue and thermal shock. Such requirements tax the capabilities of current blade materials. Based on projections of properties for tungsten fiber reinforced superalloy (FRS) composites, it was concluded that FRS turbine blades offer the potential of a several-fold increase in life and over a 200C increase in temperature capability over current SSME blade material. FRS composites were evaluated with respect to mechanical property requirements for SSME blade applications. Compared to the current blade material, the thermal shock resistance of FRS materials is excellent, two to nine times better, and their thermal fatigue resistance is equal to or higher than the current blade material. FRS materials had excellent low and high-cycle fatigue strengths, and thermal shock-induced surface microcracks had no influence on their fatigue strength. The material also exhibited negligible embrittlement when exposed to a hydrogen environment.

  15. Rate dependent constitutive models for fiber reinforced polymer composites

    NASA Technical Reports Server (NTRS)

    Gates, Thomas S.

    1990-01-01

    A literature survey was conducted to assess the state-of-the-art in rate dependent constitutive models for continuous fiber reinforced polymer matrix composite (PMC) materials. Several recent models which include formulations for describing plasticity, viscoelasticity, viscoplasticity, and rate-dependent phenomenon such as creep and stress relaxation are outlined and compared. When appropriate, these comparisons include brief descriptions of the mathematical formulations, the test procedures required for generating material constants, and details of available data comparing test results to analytical predictions.

  16. Laser transmission welding of long glass fiber reinforced thermoplastics

    NASA Astrophysics Data System (ADS)

    van der Straeten, Kira; Engelmann, Christoph; Olowinsky, Alexander; Gillner, Arnold

    2015-03-01

    Joining fiber reinforced polymers is an important topic for lightweight construction. Since classical laser transmission welding techniques for polymers have been studied and established in industry for many years joint-strengths within the range of the base material can be achieved. Until now these processes are only used for unfilled and short glass fiber-reinforced thermoplastics using laser absorbing and laser transparent matrices. This knowledge is now transferred to joining long glass fiber reinforced PA6 with high fiber contents without any adhesive additives. As the polymer matrix and glass fibers increase the scattering of the laser beam inside the material, their optical properties, changing with material thickness and fiber content, influence the welding process and require high power lasers. In this article the influence of these material properties (fiber content, material thickness) and the welding parameters like joining speed, laser power and clamping pressure are researched and discussed in detail. The process is also investigated regarding its limitations. Additionally the gap bridging ability of the process is shown in relation to material properties and joining speed.

  17. Fiber-reinforced superalloy composites provide an added performance edge

    NASA Technical Reports Server (NTRS)

    Petrasek, D. W.; Mcdaniels, D. L.; Westfall, L. J.; Stephens, J. R.

    1986-01-01

    Fiber reinforcements are being explored as a means to increasing the performance of superalloys past 980 C. Fiber-reinforced superalloys (FRS), particularly tungsten FRS (TFRS) are candidate materials for rocket-engine turbopump blades for advanced Shuttle engines and in airbreathing and other rocket engines. Refractory metal wires are the reinforcement of choice due to tolerance to fiber/matrix interactions. W alloy fibers have a maximum tensile strength of 2165 MPa at 1095 C and a 100 hr creep rupture strength at stresses up to 1400 MPa. A TFRS has the potential of a service temperature 110 C over the strongest superalloy. Manufacturing processes being evaluated to realize the FRS components are summarized, together with design features which will be introduced in turbine blades to take advantage of the FRS materials and to extend their surface life.

  18. Ceramic fiber reinforced glass-ceramic matrix composite

    NASA Technical Reports Server (NTRS)

    Bansal, Narottam P. (Inventor)

    1993-01-01

    A slurry of BSAS glass powders is cast into tapes which are cut to predetermined sizes. Mats of continuous chemical vapor deposition (CVD)-SiC fibers are alternately stacked with these matrix tapes. This tape-mat stack is warm-pressed to produce a 'green' composite which is heated to burn out organic constituents. The remaining interim material is then hot-pressed to form a BSAS glass-ceramic fiber-reinforced composite.

  19. Fretting maps of glass fiber-reinforced composites

    SciTech Connect

    Turki, C.; Salvia, M.; Vincent, L.

    1993-12-31

    Industrial development of new materials are often limited due to an insufficient knowledge in their functional properties. The paper deals with fretting behavior of glass fiber reinforced epoxy/metal contacts. Fretting is a plague for all industries, especially in the case of quasi-static loadings. Furthermore friction testing under small displacements appeared well fitted to understand the effect of fiber orientations and to relate results to microstructure (fiber, matrix and interface).

  20. CODIFICATION OF FIBER REINFORCED COMPOSITE PIPING

    SciTech Connect

    Rawls, G.

    2012-10-10

    The goal of the overall project is to successfully adapt spoolable FRP currently used in the oil industry for use in hydrogen pipelines. The use of FRP materials for hydrogen service will rely on the demonstrated compatibility of these materials for pipeline service environments and operating conditions. The ability of the polymer piping to withstand degradation while in service, and development of the tools and data required for life management are imperative for successful implementation of these materials for hydrogen pipeline. The information and data provided in this report provides the technical basis for the codification for fiber reinforced piping (FRP) for hydrogen service. The DOE has invested in the evaluation of FRP for the delivery for gaseous hydrogen to support the development of a hydrogen infrastructure. The codification plan calls for detailed investigation of the following areas: System design and applicable codes and standards; Service degradation of FRP; Flaw tolerance and flaw detection; Integrity management plan; Leak detection and operational controls evaluation; Repair evaluation. The FRP codification process started with commercially available products that had extensive use in the oil and gas industry. These products have been evaluated to assure that sufficient structural integrity is available for a gaseous hydrogen environment.

  1. Durability of waste glass flax fiber reinforced mortar

    SciTech Connect

    Aly, M.; Hashmi, M. S. J.; Olabi, A. G.; Messeiry, M.

    2011-01-17

    The main concern for natural fibre reinforced mortar composites is the durability of the fibres in the alkaline environment of cement. The composites may undergo a reduction in strength as a result of weakening of the fibres by a combination of alkali attack and fibre mineralisation. In order to enhance the durability of natural fiber reinforced cement composites several approaches have been studied including fiber impregnation, sealing of the matrix pore system and reduction of matrix alkalinity through the use of pozzolanic materials. In this study waste glass powder was used as a pozzolanic additive to improve the durability performance of flax fiber reinforced mortar (FFRM). The durability of the FFRM was studied by determining the effects of ageing in water and exposure to wetting and drying cycles; on the microstructures and flexural behaviour of the composites. The mortar tests demonstrated that the waste glass powder has significant effect on improving the durability of FFRM.

  2. Durability of Waste Glass Flax Fiber Reinforced Mortar

    NASA Astrophysics Data System (ADS)

    Aly, M.; Hashmi, M. S. J.; Olabi, A. G.; Messeiry, M.

    2011-01-01

    The main concern for natural fibre reinforced mortar composites is the durability of the fibres in the alkaline environment of cement. The composites may undergo a reduction in strength as a result of weakening of the fibres by a combination of alkali attack and fibre mineralisation. In order to enhance the durability of natural fiber reinforced cement composites several approaches have been studied including fiber impregnation, sealing of the matrix pore system and reduction of matrix alkalinity through the use of pozzolanic materials. In this study waste glass powder was used as a pozzolanic additive to improve the durability performance of flax fiber reinforced mortar (FFRM). The durability of the FFRM was studied by determining the effects of ageing in water and exposure to wetting and drying cycles; on the microstructures and flexural behaviour of the composites. The mortar tests demonstrated that the waste glass powder has significant effect on improving the durability of FFRM.

  3. CREATION OF MUSIC WITH FIBER REINFORCED CONCRETE

    NASA Astrophysics Data System (ADS)

    Kato, Hayato; Takeuchi, Masaki; Ogura, Naoyuki; Kitahara, Yukiko; Okamoto, Takahisa

    This research focuses on the Fiber Reinforcement Concrete(FRC) and its performance on musical tones. Thepossibility of future musical instruments made of this concrete is discussed. Recently, the technical properties of FRC had been improved and the different production styles, such as unit weight of binding material and volume of fiber in the structure, hardly affects the results of the acoustics. However, the board thickness in the FRC instruments is directly related with the variety of musical tone. The FRC musical effects were compared with those produced with wood on wind instruments. The sounds were compared with those produced with woodwind instruments. The sound pressure level was affected by the material and it becomes remarkably notorious in the high frequency levels. These differences had great influence on the spectrum analysis of the tone in the wind instruments and the sensory test. The results from the sensory test show dominant performances of brightness, beauty and power in the FRC instruments compared with those made of wood.

  4. Delayed cure bismaleimide resins

    DOEpatents

    Not Available

    1982-08-12

    Prior art polybismaleimides begin to polymerize at or just above the melting point of the monomer. This patent describes new bismaleimide resins which have an increased pot life and provide longer time periods in which the monomer remains fluid. The resins can be polymerized into molded articles with a high uniformity of properties. (DLC)

  5. Tensile and shear fracture behavior of fiber reinforced plastics at 77K irradiated by various radiation sources

    SciTech Connect

    Humer, K.; Weber, H.W.; Tschegg, E.K.; Egusa, Shigenori; Birtcher, R.C.; Gerstenberg, H.

    1993-08-01

    Influence of radiation damage (gamma, electron, neutron) on mechanical properties of fiber reinforced plastics (FRPs) has been investigated. Different types of FRPs (two or three dimensional E-, S- or T-glass fiber reinforcement, epoxy or bismaleimide resin) have been irradiated at room temperature with 2 MeV electrons and {sup 6O}Co {gamma}-rays up to 1.8 {times} 1 0{sup 8} Gy as well as with different reactor spectra up to a fast neutron fluence of 5 {times} lO{sup 22} m{sup {minus}2} (E > 0.1 MeV). Tensile and intralaminar shear tests were carried out on the irradiated samples at 77 K. Some samples were irradiated at 5 K and tested at 77 K with and without an annealing cycle to room temperature. Results on the influence of these radiation conditions and of warm-up cycles on the mechanical properties of FRPs are compared and discussed.

  6. Advance study of fiber-reinforced self-compacting concrete

    SciTech Connect

    Mironova, M. Ivanova, M. Naidenov, V.; Georgiev, I.; Stary, J.

    2015-10-28

    Incorporation in concrete composition of steel macro- and micro – fiber reinforcement with structural function increases the degree of ductility of typically brittle cement-containing composites, which in some cases can replace completely or partially conventional steel reinforcement in the form of rods and meshes. Thus, that can reduce manufacturing, detailing and placement of conventional reinforcement, which enhances productivity and economic efficiency of the building process. In this paper, six fiber-reinforced with different amounts of steel fiber cement-containing self-compacting compositions are investigated. The results of some of their main strength-deformation characteristics are presented. Advance approach for the study of structural and material properties of these type composites is proposed by using the methods of industrial computed tomography. The obtained original tomography results about the microstructure and characteristics of individual structural components make it possible to analyze the effective macro-characteristics of the studied composites. The resulting analytical data are relevant for the purposes of multi-dimensional modeling of these systems. Multifactor structure-mechanical analysis of the obtained with different methods original scientific results is proposed. It is presented a conclusion of the capabilities and effectiveness of complex analysis in the studies to characterize the properties of self-compacting fiber-reinforced concrete.

  7. Advance study of fiber-reinforced self-compacting concrete

    NASA Astrophysics Data System (ADS)

    Mironova, M.; Ivanova, M.; Naidenov, V.; Georgiev, I.; Stary, J.

    2015-10-01

    Incorporation in concrete composition of steel macro- and micro - fiber reinforcement with structural function increases the degree of ductility of typically brittle cement-containing composites, which in some cases can replace completely or partially conventional steel reinforcement in the form of rods and meshes. Thus, that can reduce manufacturing, detailing and placement of conventional reinforcement, which enhances productivity and economic efficiency of the building process. In this paper, six fiber-reinforced with different amounts of steel fiber cement-containing self-compacting compositions are investigated. The results of some of their main strength-deformation characteristics are presented. Advance approach for the study of structural and material properties of these type composites is proposed by using the methods of industrial computed tomography. The obtained original tomography results about the microstructure and characteristics of individual structural components make it possible to analyze the effective macro-characteristics of the studied composites. The resulting analytical data are relevant for the purposes of multi-dimensional modeling of these systems. Multifactor structure-mechanical analysis of the obtained with different methods original scientific results is proposed. It is presented a conclusion of the capabilities and effectiveness of complex analysis in the studies to characterize the properties of self-compacting fiber-reinforced concrete.

  8. Fire test methodology for aerospace materials. 1: Thermal and smoke toxicological assessments of graphite/bismaleimide and graphite/epoxy systems

    NASA Technical Reports Server (NTRS)

    Kanakia, M. D.; Switzer, W. G.; Hartzell, G. E.; Kaplan, H. L.

    1980-01-01

    Both materials possess a high degree of thermal stability, with total heat release values being essentially identical under piloted ignition conditions over a range of 5 to 10 W/sq cm incident heat flux. The graphite/epoxy material had a tendency to auto-ignite at a lower heat flux (about 7 W/sq cm) and produced about 23 percent higher peak heat release rates, approximately 42 percent more carbon monoxide and considerably more smoke than the graphite/bismaleimide under conditions of piloted ignition. Toxicological potencies of smoke produced from the two composites were equivalent for 30 minute exposures. Potencies were also comparable to many common materials, such as wood. There was no evidence for the formation of an "unusual toxicant" nor for any short term post-exposure toxicological effects.

  9. Recent developments in polyimide and bismaleimide adhesives

    NASA Technical Reports Server (NTRS)

    Politi, R. E.

    1985-01-01

    Research on high temperature resin systems has intensified. In the Aerospace Industry, the motivation for this increased activity has been to replace heat resistant alloys of aluminum, stainless steel and titanium by lighter weight glass and carbon fiber reinforced composites. Applications for these structures include: (1) engine nacelles involving long time exposure (thousands of hours) to temperatures in the 150 to 300 C range, (2) supersonic military aircraft involving moderately long exposure (hundreds of hours) to temperatures of 150 to 200 C, and (3) missile applications involving only brief exposure (seconds or minutes) to temperatures up to 500 C and above. Because of fatigue considerations, whenever possible, it is preferable to bond rather than mechanically fasten composite structures. For this reason, the increased usage of high temperature resin matrix systems for composites has necessitated the devlopment of compatible and equally heat stable adhesive systems. The performance of high temperature epoxy, epoxy phenolic and condensation polyimide adhesives is reviewed. This is followed by a discussion of three recently developed types of adhesives: (1) condensation reaction polyimides having improved processing characteristics; (2) addition reaction polyimides; and (3) bismaleimides.

  10. Mechanical Properties of Continuous Fiber Reinforced Zirconium Diboride Matrix Composites

    NASA Technical Reports Server (NTRS)

    Stuffle, Kevin; Creegan, Peter; Nowell, Steven; Bull, Jeffrey D.; Rasky, Daniel J. (Technical Monitor)

    1995-01-01

    Continuous fiber reinforced zirconium diboride matrix composites, SCS-9a-(RBSiCZrB2)matrix, are being developed for leading edge, rocket nozzle and turbine engine applications. Recently, the composite materials have been characterized for tensile properties to 1250 C, the highest temperature tested. The tensile properties are fiber dominated as the matrix is microcracked on fabrication, but favorable failure characteristic are observed. Compression and shear mechanical testing results will be reported if completed. The effects of fiber volume fraction and matrix density on mechanical properties will be discussed. The target applications of the materials will be discussed. Specific testing being performed towards qualification for these applications will be included.

  11. The recycling of comminuted glass-fiber-reinforced resin from electronic waste.

    PubMed

    Duan, Huabo; Jia, Weifeng; Li, Jinhui

    2010-05-01

    The reuse of comminuted glass-fiber-reinforced resin with various granularities gathered from printed circuit manufacturing residues was investigated. As fillers, these residues were converted into polymeric composite board by an extrusion and injection process using polypropylene as a bonding agent. The mechanical properties of the reproduced composite board were examined by considering the effects of mass fraction and glass-fiber distribution. Interfacial-layer micrograph analysis of the composite material fracture surface was used to study the fiber reinforcement mechanism. Results showed that using comminuted glass-fiber-reinforced resin as a filler material greatly enhanced the performance properties of the composite board. Although the length and diameter of filler varied, these variations had no appreciable effect on the mechanical properties of the processed board. Maximum values of 48.30 MPa for flexural strength, 31.34 MPa for tensile strength, and 31.34 J/m for impact strength were achieved from a composite board containing mass fractions of 30, 10, and 20% glass-fiber-reinforced resin waste, respectively. It was found that the maximum amount of recyclate that could be added to a composite board was 30% of weight. Beyond these percentages, the materials blend became unmanageable and the mixture less amenable to impregnation with fiber. Presented studies indicated that comminuted glass-fiber-reinforced resin waste-filled polypropylene composites are promising candidates for structural applications where high stiffness and fracture resistance are required. PMID:20480852

  12. Glass matrix composites. I - Graphite fiber reinforced glass

    NASA Technical Reports Server (NTRS)

    Prewo, K. M.; Bacon, J. F.

    1978-01-01

    An experimental program is described in which graphite fibers of Hercules HMS and HTS, Thornel 300, and Celanese DG-12 were used to reinforce, both uniaxially and biaxially, borosilicate pyrex glass. Composite flexural strength distribution, strength as a function of test temperature, fracture toughness and oxidative stability were determined and shown to be primarily a function of fiber type and the quality of fiber-matrix bond formed during composite fabrication. It is demonstrated that the graphite fiber reinforced glass system offers unique possibilities as a high performance structural material.

  13. SiC Fiber-Reinforced Celsian Composites

    NASA Technical Reports Server (NTRS)

    Bansal, Narottam P.

    2003-01-01

    Celsian is a promising matrix material for fiber-reinforced composites for high temperature structural applications. Processing and fabrication of small diameter multifilament silicon carbide tow reinforced celsian matrix composites are described. Mechanical and microstructural properties of these composites at ambient and elevated temperatures are presented. Effects of high-temperature exposures in air on the mechanical behavior of these composites are also given. The composites show mechanical integrity up to 1100 C but degrade at higher temperatures in oxidizing atmospheres. A model has been proposed for the degradation of these composites in oxidizing atmospheres at high temperatures.

  14. Fiber reinforced composites in prosthodontics – A systematic review

    PubMed Central

    Nayar, Sanjna; Ganesh, R.; Santhosh, S.

    2015-01-01

    Fiber-reinforced composite (FRC), prostheses offer the potential advantages of optimized esthetics, low wear of the opposing dentition and the ability to bond the prosthesis to the abutment teeth, thereby compensating for less-than-optimal abutment tooth retention and resistance form. These prostheses are composed of two types of composite materials: Fiber-composites to build the substructure and hybrid or micro fill particulate composites to create the external veneer surface. This article reviews the various types of FRCs and its mechanical properties. PMID:26015717

  15. Suppression of electromechanical instability in fiber-reinforced dielectric elastomers

    NASA Astrophysics Data System (ADS)

    Xiao, Rui; Gou, Xiaofan; Chen, Wen

    2016-03-01

    The electromechanical instability of dielectric elastomers has been a major challenge for the application of this class of active materials. In this work, we demonstrate that dielectric elastomers filled with soft fiber can suppress the electromechanical instability and achieve large deformation. Specifically, we developed a constitutive model to describe the dielectric and mechanical behaviors of fiber-reinforced elastomers. The model was applied to study the influence of stiffness, nonlinearity properties and the distribution of fiber on the instability of dielectric membrane under an electric field. The results show that there exists an optimal fiber distribution condition to achieve the maximum deformation before failure.

  16. Carbon Fiber Reinforced Ceramic Composites for Propulsion Applications

    NASA Technical Reports Server (NTRS)

    Shivakumar, Kunigal; Argade, Shyam

    2003-01-01

    This report presents a critical review of the processing techniques for fabricating continuous fiber-reinforced CMCs for possible applications at elevated temperatures. Some of the issues affecting durability of the composite materials such as fiber coatings and cracking of the matrix because of shrinkage in PIP-process are also examined. An assessment of the potential inexpensive processes is also provided. Finally three potential routes of manufacturing C/SiC composites using a technology that NC A&T developed for carbon/carbon composites are outlined. Challenges that will be encountered are also listed.

  17. EXPERIMENTAL STUDY ON THE APPLICATION OF HIGH STRENGTH FIBER REINFORCED MORTAR TO PRESTRESSED CONCRETE STRUCTURES

    NASA Astrophysics Data System (ADS)

    Sakurada, Michihiro; Mori, Takuya; Ohyama, Hiroaki; Seki, Hiroshi

    In order to study the application of high strength fiber reinforced mortar which has design compressive strength 120N/mm2 to prestressed concrete structures, the authors carried out material tests, bending tests and shear tests of prestressed concrete beam specimens. From the material tests, we obtained material properties for the design of prestressed concrete structures such as compressive strength, tensile strength, Young's modulus, coefficient of creep, dry shrinkage and so on. The results of the bending tests and the shear tests of prestressed concrete beam specimen shows that experimental flexural strength and shear strength of prestressed concrete beam using high strength fiber reinforced mortar exceeds strength calculated by traditional design method. It is confirmed that high strength fiber reinforced mortar can be applied to prestressed concrete structures.

  18. Reversible dielectric property degradation in moisture-contaminated fiber-reinforced laminates

    NASA Astrophysics Data System (ADS)

    Rodriguez, Luis A.; García, Carla; Fittipaldi, Mauro; Grace, Landon R.

    2016-03-01

    The potential for recovery of dielectric properties of three water-contaminated fiber-reinforced laminates is investigated using a split-post dielectric resonant technique at X-band (10 GHz). The three material systems investigated are bismaleimide (BMI) reinforced with an eight-harness satin weave quartz fabric, an epoxy resin reinforced with an eight- harness satin weave glass fabric (style 7781), and the same epoxy reinforced with a four-harness woven glass fabric (style 4180). A direct correlation between moisture content, dielectric constant, and loss tangent was observed during moisture absorption by immersion in distilled water at 25 °C for five equivalent samples of each material system. This trend is observed through at least 0.72% water content by weight for all three systems. The absorption of water into the BMI, 7781 epoxy, and 4180 epoxy laminates resulted in a 4.66%, 3.35%, and 4.01% increase in dielectric constant for a 0.679%, 0.608%, and 0.719% increase in water content by weight, respectively. Likewise, a significant increase was noticed in loss tangent for each material. The same water content is responsible for a 228%, 71.4%, and 64.1% increase in loss tangent, respectively. Subsequent to full desorption through drying at elevated temperature, the dielectric constant and loss tangent of each laminate exhibited minimal change from the dry, pre-absorption state. The dielectric constant and loss tangent change after the absorption and desorption cycle, relative to the initial state, was 0.144 % and 2.63% in the BMI, 0.084% and 1.71% in the style 7781 epoxy, and 0.003% and 4.51% in the style 4180 epoxy at near-zero moisture content. The similarity of dielectric constant and loss tangent in samples prior to absorption and after desorption suggests that any chemical or morphological changes induced by the presence of water have not caused irreversible changes in the dielectric properties of the laminates.

  19. CO2-Laser Cutting Fiber Reinforced Polymers

    NASA Astrophysics Data System (ADS)

    Mueller, R.; Nuss, Rudolf; Geiger, Manfred

    1989-10-01

    Guided by experimental investigations laser cutting of glass fiber reinforced reactive injection moulded (RRIM)-polyurethanes which are used e.g. in car industry for bumpers, spoilers, and further components is described. A Comparison with other cutting techniques as there are water jet cutting, milling, punching, sawing, cutting with conventional knife and with ultrasonic excited knife is given. Parameters which mainly influence cutting results e.g. laser power, cutting speed, gas nature and pressure will be discussed. The problematic nature in characterising micro and macro geometry of laser cut edges of fiber reinforced plastic (FRP) is explained. The topography of cut edges is described and several characteristic values are introduced to specify the obtained working quality. The surface roughness of laser cut edges is measured by both, an optical and a mechanical sensor and their reliabilities are compared.

  20. Long-short fiber reinforced thermoplastics

    SciTech Connect

    Gore, C.R.; Cuff, G.; Cianelli, D.A.; Travis, J.E.

    1986-01-01

    This paper presents information on a new family of fiber-reinforced thermoplastic compounds developed by ICI PLC and now produced by LNP under the trade mark ''Verton.'' Production is by a pultrusion process, rather than by the usual compounding extruder, which enables a high level of impregnation to be achieved without damaging the fibers. The result in molded parts is a 0.24-0.40 inch (6-10 mm) typical fiber length versus 0.008-0.016 inches (0.2-0.4 mm) for conventional short fiber products. Consequently, this enables fabricators to achieve typically a 10 to 20-fold increase in average fiber length in the finished component. These long-short fiber reinforced compounds exhibit substantial property improvements over short fiber system. Processing conditions are similar to corresponding short fiber compounds.

  1. Preparation of tungsten fiber reinforced-tungsten/copper composite for plasma facing component

    NASA Astrophysics Data System (ADS)

    He, Gang; Xu, Kunyuan; Guo, Shibin; Qian, Xueqiang; Yang, Zengchao; Liu, Guanghua; Li, Jiangtao

    2014-12-01

    W fiber reinforced-W/Cu composite is designed as a transition layer between CuCrZr heat sink material and W plasma facing material. A novel method was developed for the preparation of W fiber reinforced-W/Cu composite by combining combustion synthesis with centrifugal infiltration. Cu melt with a transient temperature over 2000 °C produced by the thermite reaction was infiltrated into the W powder and fiber bed with the assistance of a high gravity field. It was found that the W particles were sintered and bonded to the W fibers due to the high temperature produced by the thermite reaction. The bending strength of W/Cu composite improved 12.7% through W fibers reinforcement.

  2. High-frequency components made of carbon-fiber reinforced plastics for satellite payloads

    NASA Astrophysics Data System (ADS)

    Saulich, G.

    1981-06-01

    The design and the material characteristics of carbon-fiber reinforced plastics (CFRP) are discussed, taking into account characteristic data for various types of fibers and details of material construction. Waveguide filters made of carbon-fiber reinforced plastics are considered. These filters are used in satellite transponders in connection with the high resonator quality required. Attention is given to tubes and plates of CFRF, aspects of metallization, and adhesive bonding. Reflector antennas of CFRP are discussed, taking into account the design of CFRP reflectors, the reflection characteristics of CFRP reflectors, CFRP laminate characteristics, reflector coatings, and selection criteria for the design of CFRP reflectors.

  3. Tribological study of non-asbestos fiber reinforced phenolic composites for braking applications

    SciTech Connect

    Gopal, P.; Dharani, L.R.; Blum, F.D.

    1994-12-31

    A cashew modified phenolic resin was used as the binder to prepare several different nonasbestos fiber reinforced composite friction materials. Friction-wear tests were conducted at various loads, speeds and temperatures on a Chase friction testing machine. The fade and wear characteristics of glass and carbon fiber reinforced friction materials were studied. The wear rates of hybrid composites containing Kevlar{reg_sign} (registered trademark of E.I. duPont de Nemours) pulp were compared to those of control composites without Kevlar{reg_sign} pulp.

  4. Modeling of short fiber reinforced injection moulded composite

    NASA Astrophysics Data System (ADS)

    Kulkarni, A.; Aswini, N.; Dandekar, C. R.; Makhe, S.

    2012-09-01

    A micromechanics based finite element model (FEM) is developed to facilitate the design of a new production quality fiber reinforced plastic injection molded part. The composite part under study is composed of a polyetheretherketone (PEEK) matrix reinforced with 30% by volume fraction of short carbon fibers. The constitutive material models are obtained by using micromechanics based homogenization theories. The analysis is carried out by successfully coupling two commercial codes, Moldflow and ANSYS. Moldflow software is used to predict the fiber orientation by considering the flow kinetics and molding parameters. Material models are inputted into the commercial software ANSYS as per the predicted fiber orientation and the structural analysis is carried out. Thus in the present approach a coupling between two commercial codes namely Moldflow and ANSYS has been established to enable the analysis of the short fiber reinforced injection moulded composite parts. The load-deflection curve is obtained based on three constitutive material model namely an isotropy, transversely isotropy and orthotropy. Average values of the predicted quantities are compared to experimental results, obtaining a good correlation. In this manner, the coupled Moldflow-ANSYS model successfully predicts the load deflection curve of a composite injection molded part.

  5. Tungsten fiber reinforced copper matrix composites: A review

    NASA Technical Reports Server (NTRS)

    Mcdanels, David L.

    1989-01-01

    Tungsten fiber reinforced copper matrix (W/Cu) composites have served as an ideal model system with which to analyze the properties of metal matrix composites. A series of research programs were conducted to investigate the stress-strain behavior of W/Cu composites; the effect of fiber content on the strength, modulus, and conductivity of W/Cu composites; and the effect of alloying elements on the behavior of tungsten wire and of W/Cu composites. Later programs investigated the stress-rupture, creep, and impact behavior of these composites at elevated temperatures. Analysis of the results of these programs as allows prediction of the effects of fiber properties, matrix properties, and fiber content on the properties of W/Cu composites. These analyses form the basis for the rule-of-mixtures prediction of composite properties which was universally adopted as the criteria for measuring composite efficiency. In addition, the analyses allows extrapolation of potential properties of other metal matrix composites and are used to select candidate fibers and matrices for development of tungsten fiber reinforced superalloy composite materials for high temperature aircraft and rocket engine turbine applications. The W/Cu composite efforts are summarized, some of the results obtained are described, and an update is provided on more recent work using W/Cu composites as high strength, high thermal conductivity composite materials for high heat flux, elevated temperature applications.

  6. Asymptotic Analysis of Fiber-Reinforced Composites of Hexagonal Structure

    NASA Astrophysics Data System (ADS)

    Kalamkarov, Alexander L.; Andrianov, Igor V.; Pacheco, Pedro M. C. L.; Savi, Marcelo A.; Starushenko, Galina A.

    2016-08-01

    The fiber-reinforced composite materials with periodic cylindrical inclusions of a circular cross-section arranged in a hexagonal array are analyzed. The governing analytical relations of the thermal conductivity problem for such composites are obtained using the asymptotic homogenization method. The lubrication theory is applied for the asymptotic solution of the unit cell problems in the cases of inclusions of large and close to limit diameters, and for inclusions with high conductivity. The lubrication method is further generalized to the cases of finite values of the physical properties of inclusions, as well as for the cases of medium-sized inclusions. The analytical formulas for the effective coefficient of thermal conductivity of the fiber-reinforced composite materials of a hexagonal structure are derived in the cases of small conductivity of inclusions, as well as in the cases of extremely low conductivity of inclusions. The three-phase composite model (TPhM) is applied for solving the unit cell problems in the cases of the inclusions with small diameters, and the asymptotic analysis of the obtained solutions is performed for inclusions of small sizes. The obtained results are analyzed and illustrated graphically, and the limits of their applicability are evaluated. They are compared with the known numerical and asymptotic data in some particular cases, and very good agreement is demonstrated.

  7. NDE of Fiber Reinforced Foam Composite Structures for Future Aerospace Vehicles

    NASA Technical Reports Server (NTRS)

    Walker, james; Roth, Don; Hopkins, Dale

    2010-01-01

    This slide presentation reviews the complexities of non-destructive evaluation (NDE) of fiber reinforced foam composite structures to be used for aerospace vehicles in the future.Various views of fiber reinforced foam materials are shown and described. Conventional methods of NDE for composites are reviewed such as Micro-computed X-Ray Tomography, Thermography, Shearography, and Phased Array Ultrasonics (PAUT). These meth0ods appear to work well on the face sheet and face sheet ot core bond, they do not provide adequate coverage for the webs. There is a need for additional methods that will examine the webs and web to foam core bond.

  8. High performance addition-type thermoplastics (ATTs) - Evidence for the formation of a Diels-Alder adduct in the reaction of an acetylene-terminated material and a bismaleimide

    NASA Technical Reports Server (NTRS)

    Pater, R. H.; Soucek, M. D.; Chang, A. C.; Partos, R. D.

    1991-01-01

    Recently, the concept and demonstration of a new versatile synthetic reaction for making a large number of high-performance addition-type thermoplastics (ATTs) were reported. The synthesis shows promise for providing polymers having an attractive combination of easy processability, good toughness, respectable high temperature mechanical performance, and excellent thermo-oxidative stability. The new chemistry involves the reaction of an acetylene-terminated material with a bismaleimide or benzoquinone. In order to clarify the reaction mechanism, model compound studies were undertaken in solutions as well as in the solid state. The reaction products were purified by flash chromatography and characterized by conventional analytical techniques including NMR, FT-IR, UV-visible, mass spectroscopy, and high pressure liquid chromatography. The results are presented of the model compound studies which strongly support the formation of a Diels-Alder adduct in the reaction of an acetylene-terminated compound and a bismaleimide or benzoquinone.

  9. Fracture of fiber-reinforced composites analyzed via acoustic emission.

    PubMed

    Ereifej, Nadia S; Oweis, Yara G; Altarawneh, Sandra K

    2015-01-01

    This study investigated the fracture resistance of composite resins using a three-point bending test and acoustic emission (AE) analysis. Three groups of specimens (n=15) were prepared: non-reinforced BelleGlass HP composite (NRC), unidirectional (UFRC) and multidirectional (MFRC) fiber-reinforced groups which respectively incorporated unidirectional Stick and multidirectional StickNet fibers. Specimens were loaded to failure in a universal testing machine while an AE system was used to detect audible signals. Initial fracture strengths and AE amplitudes were significantly lower than those at final fracture in all groups (p<0.05). Initial fracture strength of UFRC (170.0 MPa) was significantly higher than MFRC (124.6 MPa) and NRC (87.9 MPa). Final fracture strength of UFRC (198.1 MPa) was also significantly higher than MFRC (151.0 MPa) and NRC (109.2 MPa). Initial and final fracture strengths were significantly correlated (r=0.971). It was concluded that fiber reinforcement improved the fracture resistance of composite resin materials and the monitoring of acoustic signals revealed significant information regarding the fracture process. PMID:25904176

  10. A micromorphic model for steel fiber reinforced concrete.

    PubMed

    Oliver, J; Mora, D F; Huespe, A E; Weyler, R

    2012-10-15

    A new formulation to model the mechanical behavior of high performance fiber reinforced cement composites with arbitrarily oriented short fibers is presented. The formulation can be considered as a two scale approach, in which the macroscopic model, at the structural level, takes into account the mesostructural phenomenon associated with the fiber-matrix interface bond/slip process. This phenomenon is contemplated by including, in the macroscopic description, a micromorphic field representing the relative fiber-cement displacement. Then, the theoretical framework, from which the governing equations of the problem are derived, can be assimilated to a specific case of the material multifield theory. The balance equation derived for this model, connecting the micro stresses with the micromorphic forces, has a physical meaning related with the fiber-matrix bond slip mechanism. Differently to previous procedures in the literature, addressed to model fiber reinforced composites, where this equation has been added as an additional independent ingredient of the methodology, in the present approach it arises as a natural result derived from the multifield theory. Every component of the composite is defined with a specific free energy and constitutive relation. The mixture theory is adopted to define the overall free energy of the composite, which is assumed to be homogeneously constituted, in the sense that every infinitesimal volume is occupied by all the components in a proportion given by the corresponding volume fraction. The numerical model is assessed by means of a selected set of experiments that prove the viability of the present approach. PMID:24049211

  11. Tungsten fiber reinforced superalloys: A status review

    NASA Technical Reports Server (NTRS)

    Petrasek, D. W.; Signorelli, R. A.

    1981-01-01

    Improved performance of heat engines is largely dependent upon maximum cycle temperatures. Tungsten fiber reinforced superalloys (TFRS) are the first of a family of high temperature composites that offer the potential for significantly raising hot component operating temperatures and thus leading to improved heat engine performance. This status review of TFRS research emphasizes the promising property data developed to date, the status of TFRS composite airfoil fabrication technology, and the areas requiring more attention to assure their applicability to hot section components of aircraft gas turbine engines.

  12. Mechanics of advanced fiber reinforced lattice composites

    NASA Astrophysics Data System (ADS)

    Fan, Hua-Lin; Zeng, Tao; Fang, Dai-Ning; Yang, Wei

    2010-12-01

    Fiber reinforced lattice composites are light-weight attractive due to their high specific strength and specific stiffness. In the past 10 years, researchers developed three-dimensional (3D) lattice trusses and two-dimensional (2D) lattice grids by various methods including interlacing, weaving, interlocking, filament winding and molding hot-press. The lattice composites have been applied in the fields of radar cross-section reduction, explosive absorption and heat-resistance. In this paper, topologies of the lattice composites, their manufacturing routes, as well as their mechanical and multifunctional applications, were surveyed.

  13. Three-dimensional printing fiber reinforced hydrogel composites.

    PubMed

    Bakarich, Shannon E; Gorkin, Robert; in het Panhuis, Marc; Spinks, Geoffrey M

    2014-09-24

    An additive manufacturing process that combines digital modeling and 3D printing was used to prepare fiber reinforced hydrogels in a single-step process. The composite materials were fabricated by selectively pattering a combination of alginate/acrylamide gel precursor solution and an epoxy based UV-curable adhesive (Emax 904 Gel-SC) with an extrusion printer. UV irradiation was used to cure the two inks into a single composite material. Spatial control of fiber distribution within the digital models allowed for the fabrication of a series of materials with a spectrum of swelling behavior and mechanical properties with physical characteristics ranging from soft and wet to hard and dry. A comparison with the "rule of mixtures" was used to show that the swollen composite materials adhere to standard composite theory. A prototype meniscus cartilage was prepared to illustrate the potential application in bioengineering. PMID:25197745

  14. Homogenization of long fiber reinforced composites including fiber bending effects

    NASA Astrophysics Data System (ADS)

    Poulios, Konstantinos; Niordson, Christian F.

    2016-09-01

    This paper presents a homogenization method, which accounts for intrinsic size effects related to the fiber diameter in long fiber reinforced composite materials with two independent constitutive models for the matrix and fiber materials. A new choice of internal kinematic variables allows to maintain the kinematics of the two material phases independent from the assumed constitutive models, so that stress-deformation relationships, can be expressed in the framework of hyper-elasticity and hyper-elastoplasticity for the fiber and the matrix materials respectively. The bending stiffness of the reinforcing fibers is captured by higher order strain terms, resulting in an accurate representation of the micro-mechanical behavior of the composite. Numerical examples show that the accuracy of the proposed model is very close to a non-homogenized finite-element model with an explicit discretization of the matrix and the fibers.

  15. Electrical Insulation Characteristics of Glass Fiber Reinforced Resins

    SciTech Connect

    Tuncer, Enis; Sauers, Isidor; James, David Randy; Ellis, Alvin R

    2009-01-01

    Non-metallic structural materials that act as an electrical insulation are needed for cryogenic power applications. One of the extensively utilized materials is glass fiber reinforced resins (GFRR) and may also be known as GFRP and FRP. They are created from glass fiber cloth that are impregnated with an epoxy resin under pressure and heat. Although the materials based on GFRR have been employed extensively, reports about their dielectric properties at cryogenic temperatures and larger thicknesses are generally lacking in the literature. Therefore to guide electrical apparatus designers for cryogenic applications, GFRR samples with different thicknesses are tested in a liquid nitrogen bath. Scaling relation between the dielectric breakdown strength and the GFFR thickness is established. Their loss tangents are also reported at various frequencies.

  16. A New Generation of Sub Mm Telescopes, Made of Carbon Fiber Reinforced Plastic

    NASA Technical Reports Server (NTRS)

    Mezger, P.; Baars, J. W. M.; Ulich, B. L.

    1984-01-01

    Carbon fiber reinforced plastic (CFRP) appears to be the material most suited for the construction of submillimeter telescopes (SMT) not only for ground-based use but also for space applications. The accuracy of the CFRP reflectors needs to be improved beyond value of the 17 micron rms envisaged for the 10 m SMT.

  17. Fiber reinforced glasses and glass-ceramics for high performance applications

    NASA Technical Reports Server (NTRS)

    Prewo, K. M.; Brennan, J. J.; Layden, G. K.

    1986-01-01

    The development of fiber reinforced glass and glass-ceramic matrix composites is described. The general concepts involved in composite fabrication and resultant composite properties are given for a broad range of fiber and matrix combinations. It is shown that composite materials can be tailored to achieve high levels of toughness, strength, and elastic stiffness, as well as wear resistance and dimensional stability.

  18. Dielectric strength of irradiated fiber reinforced plastics

    NASA Astrophysics Data System (ADS)

    Humer, Karl; Weber, Harald W.; Hastik, Ronald; Hauser, Hans; Gerstenberg, Heiko

    2001-05-01

    The insulation system for the toroidal field model coil of international thermonuclear experimental reactor is a fiber reinforced plastic (FRP) laminate, which consists of a combined Kapton/R-glass-fiber reinforcement tape, vacuum-impregnated with an epoxy DGEBA system. Pure disk-shaped laminates, disk-shaped FRP/stainless-steel sandwiches, and conductor insulation prototypes were irradiated at 5 K in a fission reactor up to a fast neutron fluence of 10 22 m -2 ( E>0.1 MeV) to investigate the radiation induced degradation of the dielectric strength of the insulation system. After warm-up to room temperature, swelling, weight loss, and the breakdown strength were measured at 77 K. The sandwich swells by 4% at a fluence of 5×10 21 m -2 and by 9% at 1×10 22 m -2. The weight loss of the FRP is 2% at 1×10 22 m -2. The dielectric strength remained unchanged over the whole dose range.

  19. Cohesive fracture model for functionally graded fiber reinforced concrete

    SciTech Connect

    Park, Kyoungsoo; Paulino, Glaucio H.; Roesler, Jeffery

    2010-06-15

    A simple, effective, and practical constitutive model for cohesive fracture of fiber reinforced concrete is proposed by differentiating the aggregate bridging zone and the fiber bridging zone. The aggregate bridging zone is related to the total fracture energy of plain concrete, while the fiber bridging zone is associated with the difference between the total fracture energy of fiber reinforced concrete and the total fracture energy of plain concrete. The cohesive fracture model is defined by experimental fracture parameters, which are obtained through three-point bending and split tensile tests. As expected, the model describes fracture behavior of plain concrete beams. In addition, it predicts the fracture behavior of either fiber reinforced concrete beams or a combination of plain and fiber reinforced concrete functionally layered in a single beam specimen. The validated model is also applied to investigate continuously, functionally graded fiber reinforced concrete composites.

  20. Fracture Behavior and Properties of Functionally Graded Fiber-Reinforced Concrete

    SciTech Connect

    Roesler, Jeffery; Bordelon, Amanda; Gaedicke, Cristian; Park, Kyoungsoo; Paulino, Glaucio

    2008-02-15

    In concrete pavements, a single concrete mixture design is selected to resist mechanical loading without attempting to adversely affect the concrete pavement shrinkage, ride quality, or noise attenuation. An alternative approach is to design distinct layers within the concrete pavement surface which have specific functions thus achieving higher performance at a lower cost. The objective of this research was to address the structural benefits of functionally graded concrete materials (FGCM) for rigid pavements by testing and modeling the fracture behavior of different combinations of layered plain and synthetic fiber-reinforced concrete materials. Fracture parameters and the post-peak softening behavior were obtained for each FGCM beam configuration by the three point bending beam test. The peak loads and initial fracture energy between the plain, fiber-reinforced, and FGCM signified similar crack initiation. The total fracture energy indicated improvements in fracture behavior of FGCM relative to full-depth plain concrete. The fracture behavior of FGCM depended on the position of the fiber-reinforced layer relative to the starter notch. The fracture parameters of both fiber-reinforced and plain concrete were embedded into a finite element-based cohesive zone model. The model successfully captured the experimental behavior of the FGCMs and predicted the fracture behavior of proposed FGCM configurations and structures. This integrated approach (testing and modeling) demonstrates the viability of FGCM for designing layered concrete pavements system.

  1. Puncture-Healing Thermoplastic Resin Carbon-Fiber-Reinforced Composites

    NASA Technical Reports Server (NTRS)

    Gordon, Keith L. (Inventor); Siochi, Emilie J. (Inventor); Grimsley, Brian W. (Inventor); Cano, Roberto J. (Inventor); Czabaj, Michael W. (Inventor)

    2015-01-01

    A composite comprising a combination of a self-healing polymer matrix and a carbon fiber reinforcement is described. In one embodiment, the matrix is a polybutadiene graft copolymer matrix, such as polybutadiene graft copolymer comprising poly(butadiene)-graft-poly(methyl acrylate-co-acrylonitrile). A method of fabricating the composite is also described, comprising the steps of manufacturing a pre-impregnated unidirectional carbon fiber preform by wetting a plurality of carbon fibers with a solution, the solution comprising a self-healing polymer and a solvent, and curing the preform. A method of repairing a structure made from the composite of the invention is described. A novel prepreg material used to manufacture the composite of the invention is described.

  2. Ballistic impact fatigue behavior of spectra fiber-reinforced composites

    SciTech Connect

    Song, J.W.; Lee, B.L.

    1994-12-31

    The study examined the penetration failure mechanisms of Spectra fiber-reinforced composites under ballistic impact and assessed the roles played by resin matrix properties in controlling the process of impact damage propagation. In order to observe gradual propagation of damage, a concept of impact fatigue was introduced by subjecting the composite plates to a multiple number of repeated ballistic impact. When the striking velocity of,a projectile was below the ballistic limit, repeated impact resulted in a progressive growth of local delamination until full penetration of the projectile occurs. Preliminary results indicated that the vinyl ester resin matrix composites have a higher ballistic limit and longer impact fatigue life at a given striking velocity than the polyurethane matrix composites. Based on the test results of dynamic mechanical properties, more localized delamination of polyurethane matrix composites was attributed to a greater degree of stress wave attenuation and lower bending stiffness of material system.

  3. Creep behavior of tungsten fiber reinforced niobium metal matrix composites

    NASA Technical Reports Server (NTRS)

    Grobstein, T. L.

    1989-01-01

    Tungsten fiber reinforced niobium metal matrix composites were evaluated for use in space nuclear power conversion systems. The composite panels were fabricated using the arc-spray monotape technique at the NASA Lewis Research Center. The creep behavior of W/Nb composite material was determined at 1400 and 1500 K in vacuum over a wide range of applied loads. The time to reach 1 percent strain, the time to rupture, and the minimum creep rate were measured. The W/Nb composites exceeded the properties of monolithic niobium alloys significantly even when compared on a strength to density basis. The effect of fiber orientation on the creep strength also was evaluated. Kirkendall void formation was observed at the fiber/matrix interface; the void distribution differed depending on the fiber orientation relative to the stress axis. A relationship was found between the fiber orientation and the creep strength.

  4. Creep behavior of tungsten fiber reinforced niobium metal matrix composites

    NASA Technical Reports Server (NTRS)

    Grobstein, Toni L.

    1992-01-01

    Tungsten fiber reinforced niobium metal matrix composites were evaluated for use in space nuclear power conversion systems. The composite panels were fabricated using the arc-spray monotape technique at the NASA Lewis Research Center. The creep behavior of W/Nb composite material was determined at 1400 and 1500 K in vacuum over a wide range of applied loads. The time to reach 1 percent strain, the time to rupture, and the minimum creep rate were measured. The W/Nb composites exceeded the properties of monolithic niobium alloys significantly even when compared creep strength also was evaluated. Kirkendall void formation was observed at the fiber/matrix interface; the void distribution differed depending the fiber orientation relative to the stress axis. A relationship was found between the fiber orientation and the creep strength.

  5. Shear degradation in fiber reinforced laminates due to matrix damage

    NASA Astrophysics Data System (ADS)

    Salavatian, Mohammedmahdi

    The objective of this study was to develop and implement a shear modulus degradation model to improve the failure analysis of the fiber reinforced composite structures. Matrix damage, involving transverse and shear cracks, is a common failure mode for composite structures, yet little is known concerning their interaction. To understand the material behavior after matrix failure, the nonlinear response of the composite laminate was studied using pressure vessels made from a [+/-o] bias orientation, which tend to exhibit a matrix dominated failure. The result of this work showed laminate matrix hardening in shear and softening in the transverse direction. A modified Iosipescu coupon was proposed to study the evolution of shear and transverse damage and their mutual effects. The proposed method showed good agreement with tubular results and has advantages of simplified specimen fabrication using standard test fixtures. The proposed method was extended by introducing a novel experimental technique to study the shear degradation model under biaxial loading. Experimental results of the transverse modulus reduction were in good agreement with material degradation models, while the predicted shear modulus reduction was higher than experiment. The discrepancy between available models and observations was due to the presence of a traction between the crack surfaces. Accordingly, a closed form solution was proposed for the shear stress-strain field of a cracked laminate by replacing the cracks with cohesive zones. The constitutive equations of the crack laminate were derived including the effects of internal tractions and transverse stress on the shear modulus. The proposed analytical model was shown to be the most comprehensive model for shear modulus degradation reduction of the fiber reinforced laminates. A numerical implementation of the shear degradation model was done using continuum damage mechanics. Through this work it was shown the common assumption of a linear

  6. Basalt fiber reinforced polymer composites: Processing and properties

    NASA Astrophysics Data System (ADS)

    Liu, Qiang

    A high efficiency rig was designed and built for in-plane permeability measurement of fabric materials. A new data derivation procedure to acquire the flow fluid pattern in the experiment was developed. The measurement results of the in-plane permeability for basalt twill 31 fabric material showed that a high correlation exists between the two principal permeability values for this fabric at 35% fiber volume fraction. This may be the most important scientific contribution made in this thesis. The results from radial measurements corresponded quite well with those from Unidirectional (UD) measurements, which is a well-established technique. No significant differences in mechanical properties were found between basalt fabric reinforced polymer composites and glass composites reinforced by a fabric of similar weave pattern. Aging results indicate that the interfacial region in basalt composites may be more vulnerable to environmental damage than that in glass composites. However, the basalt/epoxy interface may have been more durable than the glass/epoxy interface in tension-tension fatigue because the basalt composites have significantly longer fatigue life. In this thesis, chapter I reviews the literature on fiber reinforced polymer composites, with concentration on permeability measurement, mechanical properties and durability. Chapter II discusses the design of the new rig for in-plane permeability measurement, the new derivation procedure for monitoring of the fluid flow pattern, and the permeability measurement results. Chapter III compares the mechanical properties and durability between basalt fiber and glass fiber reinforced polymer composites. Lastly, chapter IV gives some suggestions and recommendations for future work.

  7. Thermal oxidation induced degradation of carbon fiber reinforced composites and carbon nanotube sheet enhanced fiber/matrix interface for high temperature aerospace structural applications

    NASA Astrophysics Data System (ADS)

    Haque, Mohammad Hamidul

    Recent increase in the use of carbon fiber reinforced polymer matrix composite, especially for high temperature applications in aerospace primary and secondary structures along with wind energy and automotive industries, have generated new challenges to predict its failure mechanisms and service life. This dissertation reports the experimental study of a unidirectional carbon fiber reinforced bismaleimide (BMI) composites (CFRC), an excellent candidate for high temperature aerospace components, undergoing thermal oxidation at 260 °C in air for over 3000 hours. The key focus of the work is to investigate the mechanical properties of the carbon fiber BMI composite subjected to thermal aging in three key aspects - first, studying its bulk flexural properties (in macro scale), second, characterizing the crack propagation along the fiber direction, representing the interfacial bonding strength between fiber and matrix (in micro scale), and third, introducing nano-structured materials to modify the interface (in nano scale) between the carbon fiber and BMI resin and mechanical characterization to study its influence on mitigating the aging effect. Under the first category, weight loss and flexural properties have been monitored as the oxidation propagates through the fiber/matrix interface. Dynamic mechanical analysis and micro-computed tomography analysis have been performed to analyze the aging effects. In the second category, the long-term effects of thermal oxidation on the delamination (between the composite plies) and debonding (between fiber and matrix) type fracture toughness have been characterized by preparing two distinct types of double cantilever beam specimens. Digital image correlation has been used to determine the deformation field and strain distribution around the crack propagation path. Finally the resin system and the fiber/matrix interface have been modified using nanomaterials to mitigate the degradations caused by oxidation. Nanoclay modified

  8. Carbon fiber reinforced thermoplastic composites for future automotive applications

    NASA Astrophysics Data System (ADS)

    Friedrich, K.

    2016-05-01

    After a brief introduction to polymer composite properties and markets, the state of the art activities in the field of manufacturing of advanced composites for automotive applications are elucidated. These include (a) long fiber reinforced thermoplastics (LFT) for secondary automotive components, and (b) continuous carbon fiber reinforced thermosetting composites for car body applications. It is followed by future possibilities of carbon fiber reinforced thermoplastic composites for e.g. (i) crash elements, (ii) racing car seats, and (iii) production and recycling of automotive fenders.

  9. Replacement of a tooth with a fiber-reinforced direct bonded restoration.

    PubMed

    Shuman, I E

    2000-01-01

    Today's methods and materials for tooth replacement are multiple and varied. Modern materials now allow for highly conservative abutment preparations that can retain bonded single tooth replacement fixed prostheses. A case report is presented in which fiber reinforced with composite resin was used for placement of a three-unit fixed long-term provisional restoration, providing fracture resistance while achieving an esthetically pleasing, durable restoration. PMID:11199598

  10. Energy Dependent Processing of Fiber Reinforced Plastics with Ultra Short Laser Pulses

    NASA Astrophysics Data System (ADS)

    Schilling, N.; Lasagni, A.; Klotzbach, U.

    In this paper the processing of a fiber reinforced plastic consisting of glass fibers embedded in polypropylene with ultra short laser systems is shown. Focus of the study is on the dependence of working wavelength (1064 nm, 532 nm and 355 nm) and pulse duration (500 fs to 10 ps) on the laser ablation characteristic of the treated material. Depending on the energy density and the material properties, two different process regions could be identified.

  11. [Fiber-reinforced composite in fixed prosthodontics].

    PubMed

    Pilo, R; Abu Rass, Z; Shmidt, A

    2010-07-01

    Fiber reinforced composite (FRC) is composed of resin matrix and fibers filler. Common types of fibers: polyethylene, carbon and glass. Fibers can be continuous and aligned, discontinuous and aligned, discontinuous and randomly oriented. The architecture of the fibers is unidirectional, woven or braided. The two main types are: dry fibers or impregnated. Inclusion of fibers to resin composite increased its average flexural strength in 100-200 MPa. FRC can be utilized by the dentist in direct approach (splinting, temporary winged bridge) or indirect approach (laboratory made fixed partial denture). Laboratory fixed partial denture (FPD) is made from FRC substructure and Hybrid/Microfill particulate composite veneer. Main indications: interim temporary FPD or FPD in cases of questionable abutment teeth, in aesthetic cases where All Ceram FPD is not feasible. Retention is attained by adhesive cementation to minimally prepared teeth or to conventionally prepared teeth; other options are inlay-onlay bridges or hybrid bridges. Contraindications are: poor hygiene, inability to control humidity, parafunction habits, and more than two pontics. Survival rate of FRC FPD over 5 years is 75%, lower compared to porcelain fused to metal FPD which is 95%. Main reasons for failure are: fracture of framework and delamination of the veneer. Part of the failures is repairable. PMID:21485555

  12. Impact behavior of a SiC fiber-reinforced reaction bonded Si3N4 composite

    NASA Technical Reports Server (NTRS)

    Grady, J.; Bhatt, R.; Klima, S.

    1989-01-01

    Impact tests were performed on a series of ceramic plate specimens. Monolithic (unreinforced) and composite specimens with various fiber layups were tested to determine the effect that the fiber reinforcement has on impact damage initiation and dynamic response of the ceramic materials. Results show that a porous surface layer of Si3N4 on the composite specimens can enhance the energy absorbing capability of the composite specimens. The addition of SiC fiber reinforcement to the RBSN matrix material is also shown to significantly change the mode of failure and reduce the extent of damage due to impact.

  13. Anomaly detection of microstructural defects in continuous fiber reinforced composites

    NASA Astrophysics Data System (ADS)

    Bricker, Stephen; Simmons, J. P.; Przybyla, Craig; Hardie, Russell

    2015-03-01

    Ceramic matrix composites (CMC) with continuous fiber reinforcements have the potential to enable the next generation of high speed hypersonic vehicles and/or significant improvements in gas turbine engine performance due to their exhibited toughness when subjected to high mechanical loads at extreme temperatures (2200F+). Reinforced fiber composites (RFC) provide increased fracture toughness, crack growth resistance, and strength, though little is known about how stochastic variation and imperfections in the material effect material properties. In this work, tools are developed for quantifying anomalies within the microstructure at several scales. The detection and characterization of anomalous microstructure is a critical step in linking production techniques to properties, as well as in accurate material simulation and property prediction for the integrated computation materials engineering (ICME) of RFC based components. It is desired to find statistical outliers for any number of material characteristics such as fibers, fiber coatings, and pores. Here, fiber orientation, or `velocity', and `velocity' gradient are developed and examined for anomalous behavior. Categorizing anomalous behavior in the CMC is approached by multivariate Gaussian mixture modeling. A Gaussian mixture is employed to estimate the probability density function (PDF) of the features in question, and anomalies are classified by their likelihood of belonging to the statistical normal behavior for that feature.

  14. High-temperature testing of high performance fiber reinforced concrete

    NASA Astrophysics Data System (ADS)

    Fořt, Jan; Vejmelková, Eva; Pavlíková, Milena; Trník, Anton; Čítek, David; Kolísko, Jiří; Černý, Robert; Pavlík, Zbyšek

    2016-06-01

    The effect of high-temperature exposure on properties of High Performance Fiber Reinforced Concrete (HPFRC) is researched in the paper. At first, reference measurements are done on HPFRC samples without high-temperature loading. Then, the HPFRC samples are exposed to the temperatures of 200, 400, 600, 800, and 1000 °C. For the temperature loaded samples, measurement of residual mechanical and basic physical properties is done. Linear thermal expansion coefficient as function of temperature is accessed on the basis of measured thermal strain data. Additionally, simultaneous difference scanning calorimetry (DSC) and thermogravimetry (TG) analysis is performed in order to observe and explain material changes at elevated temperature. It is found that the applied high temperature loading significantly increases material porosity due to the physical, chemical and combined damage of material inner structure, and negatively affects also the mechanical strength. Linear thermal expansion coefficient exhibits significant dependence on temperature and changes of material structure. The obtained data will find use as input material parameters for modelling the damage of HPFRC structures exposed to the fire and high temperature action.

  15. The formation of cyclo-addition adducts in the reaction of an acetylene-terminated material with a bismaleimide: A model compound study for addition-type thermoplastics (ATTs) using metal catalysts

    SciTech Connect

    Soucek, M.D., Pater, R.H.; Ritenour, S.L.

    1993-12-31

    A model compound study using an acetylene-terminated material and a bismaleimide has provided evidence that a diruthenium complex Ru{sub 2}(CO){sub 6}[1,2-({mu}-PPh){sub 2}C{sub 6}H{sub 4}] and a rhodium complex Rh(PPh{sub 3}){sub 3}Cl can catalyze a Diels-Alder type cycloaddition in which acetylene-terminated material acts as a diene and the bismaleimide is a dieneophile. The molten state reaction of N-(3-ethynylphenyl) phthalimide and N-(4-phenoxyphenyl) maleimide with Ru{sub 2}(CO){sub 6}[{mu}-(PhP){sub 2}C{sub 6}H{sub 4}] or Rh(PPh{sub 3}){sub 3}Cl heated to 170{degrees}C led to two major products. The spectral data for the first major product is consistent with a 2:1 Diels-Alder adduct formed from two molecules of the acetylene compound and one molecule of the maleimide. The spectral data for the second major product is consistent with a 2:2 Diels-Alder adduct formed from two molecules of each reactant.

  16. Clinical evaluation of carbon fiber reinforced carbon endodontic post, glass fiber reinforced post with cast post and core: A one year comparative clinical study

    PubMed Central

    Preethi, GA; Kala, M

    2008-01-01

    Aim: Restoring endodontically treated teeth is one of the major treatments provided by the dental practitioner. Selection and proper use of restorative materials continues to be a source of frustration for many clinicians. There is controversy surrounding the most suitable choice of restorative material and the placement method that will result in the highest probability of successful treatment. This clinical study compares two different varieties of fiber posts and one cast post and core in terms of mobility of crown margin under finger pressure, recurrent caries detected at the crown margin, fracture of the restoration, fracture of the root and periapical and periodontal pathology requiring crown removal over the period of 12months as evaluated by clinical and radiographical examination. Materials and Methods: 30 root canal treated, single rooted maxillary anterior teeth of 25 patients in the age range of 18–60 years where a post retained crown was indicated were selected for the study between January 2007 and August 2007; and prepared in a standard clinical manner. It was divided into 3 groups of 10 teeth in each group. After post space preparation, the Carbon fiber and Glass fiber reinforced posts were cemented with Scotch bond multipurpose plus bonding agent and RelyX adhesive resin cement in the first and second groups respectively. The Cast post and cores were cemented with Zinc Phosphate cement in the third group. Following post- cementation, the preparation was further refined and a rubber base impression was taken for metal-ceramic crowns which was cemented with Zinc Phosphate cement. A baseline periapical radiograph was taken once each crown was cemented. All patients were evaluated after one week (baseline), 3 months, 6 months and one year for following characteristics mobility of crown margin under finger pressure, recurrent caries detected at the crown margin, fracture of the restoration, fracture of the root and periapical and periodontal pathology

  17. A Different Pontic Design for Fiber-Reinforced Composite Bridgeworks: A Clinical Report

    PubMed Central

    Kumbuloḡlu, Ovul; Özdemir, Niler; Aksoy, Gökhan; User, Atilla

    2007-01-01

    Objectives This clinical report describes a relatively simple but esthetic, non-invasive and functional prosthodontic treatment option for a patient with missing tooth. Methods A patient with a missing maxillary left canine was non-invasively treated with a fiber reinforced composite (FRC) bridgework with an all ceramic (Empress II, Ivoclar Vivadent, Schaan, Liech-tenstein) pontic design, using laboratory technique. Results The restoration has served the patient for 2 year, seemingly without discomfort, and it has not required any maintenance. The patient has kept up with his oral hygiene. Conclusions Although additional clinical experience is necessary, fiber-reinforced composite materials can be used in combination with a lithium disilicate ceramic material in fixed partial dentures. PMID:19212498

  18. Processing and damage recovery of intrinsic self-healing glass fiber reinforced composites

    NASA Astrophysics Data System (ADS)

    Sordo, Federica; Michaud, Véronique

    2016-08-01

    Glass fiber reinforced composites with a self-healing, supramolecular hybrid network matrix were produced using a modified vacuum assisted resin infusion moulding process adapted to high temperature processing. The quality and fiber volume fraction (50%) of the obtained materials were assessed through microscopy and matrix burn-off methods. The thermo-mechanical properties were quantified by means of dynamic mechanical analysis, revealing very high damping properties compared to traditional epoxy-based glass fiber reinforced composites. Self-healing properties were assessed by three-point bending tests. A high recovery of the flexural properties, around 72% for the elastic modulus and 65% of the maximum flexural stress, was achieved after a resting period of 24 h at room temperature. Recovery after low velocity impact events was also visually observed. Applications for this intrinsic and autonomic self-healing highly reinforced composite material point towards semi-structural applications where high damping and/or integrity recovery after impact are required.

  19. Properties of glass/carbon fiber reinforced epoxy hybrid polymer composites

    NASA Astrophysics Data System (ADS)

    Patel, R. H.; Sevkani, V. R.; Patel, B. R.; Patel, V. B.

    2016-05-01

    Composite Materials are well known for their tailor-made properties. For the fabrication of composites different types of reinforcements are used for different applications. Sometimes for a particular application, one type of reinforcement may not fulfill the requirements. Therefore, more than one type of reinforcements may be used. Thus, the idea of hybrid composites arises. Hybrid composites are made by joining two or more different reinforcements with suitable matrix system. It helps to improve the properties of composite materials. In the present work glass/carbon fiber reinforcement have been used with a matrix triglycidyl ether of tris(m-hydroxy phenyl) phosphate epoxy resin using amine curing agent. Different physical and mechanical properties of the glass, carbon and glass/carbon fiber reinforced polymeric systems have been found out.

  20. Studying impact damage on carbon-fiber reinforced aircraft composite panels with sonicir

    SciTech Connect

    Han Xiaoyan; Zhang Ding; He Qi; Song Yuyang; Lubowicki, Anthony; Zhao Xinyue; Newaz, Golam.; Favro, Lawrence D.; Thomas, Robert L.

    2011-06-23

    Composites are becoming more important materials in commercial aircraft structures such as the fuselage and wings with the new B787 Dreamliner from Boeing which has the target to utilize 50% by weight of composite materials. Carbon-fiber reinforced composites are the material of choice in aircraft structures. This is due to their light weight and high strength (high strength-to-weight ratio), high specific stiffness, tailorability of properties, design flexibility etc. Especially, by reducing the aircraft's body weight by using such lighter structures, the cost of fuel can be greatly reduced with the high jet fuel price for commercial airlines. However, these composites are prone to impact damage and the damage may occur without any observable sign on the surface, yet resulting in delaminations and disbonds that may occur well within the layers. We are studying the impact problem with carbon-fiber reinforced composite panels and developing SonicIR for this application as a fast and wide-area NDE technology. In this paper, we present our results in studying composite structures including carbon-fiber reinforced composite materials, and preliminary quantitative studies on delamination type defect depth identification in the panels.

  1. Effect of moisture on hammer-milled glass-fiber-reinforced polyurethane

    SciTech Connect

    Mateen, A.; Siddiqi, S.A.

    1996-10-01

    The effect of moisture on the dynamic properties of hammer-milled glass-fiber-reinforced polyurethane was investigated. Similar investigations were also made on an unfilled polyurethane matrix for comparison. Moisture was found to increase the shear modulus at lower temperature due to the formation of ice. At higher temperatures, however, shear modulus decreased due to the plasticizing effect of water. Moisture also modified the damping properties of the material.

  2. Rapid Prototyping of Continuous Fiber Reinforced Ceramic Matrix Composites

    NASA Technical Reports Server (NTRS)

    Vaidyanathan, R.; Green, C.; Phillips, T.; Cipriani, R.; Yarlagadda, S.; Gillespie, J. W., Jr.; Effinger, M.; Cooper, K. C.

    2003-01-01

    For ceramics to be used as structural components in high temperature applications, their fracture toughness is improved by embedding continuous ceramic fibers. Ceramic matrix composite (CMC) materials allow increasing the overall operating temperature, raising the temperature safety margins, avoiding the need for cooling, and improving the damping capacity, while reducing the weight at the same time. They also need to be reliable and available in large quantities as well. In this paper, an innovative rapid prototyping technique to fabricate continuous fiber reinforced ceramic matrix composites is described. The process is simple, robust and will be widely applicable to a number of high temperature material systems. This technique was originally developed at the University of Delaware Center for Composite Materials (UD-CCM) for rapid fabrication of polymer matrix composites by a technique called automated tow placement or ATP. The results of mechanical properties and microstructural characterization are presented, together with examples of complex shapes and parts. It is believed that the process will be able to create complex shaped parts at an order of magnitude lower cost than current chemical vapor infiltration (CVI) and polymer impregnation and pyrolysis (PIP) processes.

  3. Rapid Prototyping of Continuous Fiber Reinforced Ceramic Matrix Composites

    NASA Technical Reports Server (NTRS)

    Vaidyanathan, R.; Green, C.; Phillips, T.; Cipriani, R.; Yarlagadda, S.; Gillespie, J.; Effinger, M.; Cooper, K. C.; Gordon, Gail (Technical Monitor)

    2002-01-01

    For ceramics to be used as structural components in high temperature applications, their fracture toughness is improved by embedding continuous ceramic fibers. Ceramic matrix composite (CMC) materials allow increasing the overall operating temperature, raising the temperature safety margins, avoiding the need for cooling, and improving the damping capacity, while reducing the weight at the same time. They also need to be reliable and available in large quantities as well. In this paper, an innovative rapid prototyping technique to fabricate continuous fiber reinforced ceramic matrix composites is described. The process is simple, robust and will be widely applicable to a number of high temperature material systems. This technique was originally developed at the University of Delaware Center for Composite Materials (UD-CCM) for rapid fabrication of polymer matrix composites by a technique called automated tow placement or ATP. The results of mechanical properties and microstructural characterization are presented, together with examples of complex shapes and parts. It is believed that the process will be able to create complex shaped parts at an order of magnitude lower cost than current CVI and PIP processes.

  4. New generation fiber reinforced polymer composites incorporating carbon nanotubes

    NASA Astrophysics Data System (ADS)

    Soliman, Eslam

    The last five decades observed an increasing use of fiber reinforced polymer (FRP) composites as alternative construction materials for aerospace and infrastructure. The high specific strength of FRP attracted its use as non-corrosive reinforcement. However, FRP materials were characterized with a relatively low ductility and low shear strength compared with steel reinforcement. On the other hand, carbon nanotubes (CNTs) have been introduced in the last decade as a material with minimal defect that is capable of increasing the mechanical properties of polymer matrices. This dissertation reports experimental investigations on the use of multi-walled carbon nanotubes (MWCNTs) to produce a new generation of FRP composites. The experiments showed significant improvements in the flexure properties of the nanocomposite when functionalized MWCNTs were used. In addition, MWCNTs were used to produce FRP composites in order to examine static, dynamic, and creep behavior. The MWCNTs improved the off-axis tension, off-axis flexure, FRP lap shear joint responses. In addition, they reduced the creep of FRP-concrete interface, enhanced the fracture toughness, and altered the impact resistance significantly. In general, the MWCNTs are found to affect the behaviour of the FRP composites when matrix failure dominates the behaviour. The improvement in the mechanical response with the addition of low contents of MWCNTs would benefit many industrial and military applications such as strengthening structures using FRP composites, composite pipelines, aircrafts, and armoured vehicles.

  5. Fabrication of full-scale fiber reinforced hot-gas filters by chemical vapor deposition. Final technical report

    SciTech Connect

    Smith, R.G.

    1994-04-01

    The goal of this program was to develop and fabricate an initial set of ceramic fiber reinforced, ceramic matrix composite, hot gas candle filters for testing in a simulated pressurized fluidized bed combustion (PFBC) environment. Four full-scale ceramic fiber reinforced candle filters were fabricated in a multi step process. The substrate was filament wound using Nextel{trademark} 312 yarn and then coated with silicon carbide by chemical vapor deposition (CVD) to form a ceramic composite shape that provides the candle`s structural shape, toughness, and strength. Filter layer material was applied over the surface and then bonded with silicon carbide in a chemical vapor infiltration, CVI, step.

  6. Laser processing of glass fiber reinforced thermoplastics with different wavelengths and pulse durations

    NASA Astrophysics Data System (ADS)

    Schilling, N.; Krupop, B.; Klotzbach, U.

    2015-03-01

    In this paper, laser processing of fiber reinforced thermoplastics is investigated with different laser sources. Aim of the study is to determine the process windows in which selective ablation of polymer matrix and homogenous ablation of matrix and fiber occurs. To reach this, laser sources with different wavelengths (10600 nm, 1064 nm and 532 nm) and pulse durations in μs, ns and ps regime are compared on their ablation behavior of natural and black colored glass fiber reinforced polypropylene. Best results were achieved with ns lasers with IR wavelength at black colored material. At this parameter combination a wide process window can be shown where no damage of the reinforcing fibers happens.

  7. Mechanical behavior of a glass-fiber reinforced composite to steel joint for ships

    NASA Astrophysics Data System (ADS)

    Li, Xiaowen; Li, Ping; Lin, Zhuang; Yang, Dongmei

    2015-03-01

    The use of a glass-fiber reinforced composite in marine structures is becoming more common, particularly due to the potential weight savings. The mechanical response of the joint between a glass-fiber reinforced polymer (GRP) superstructure and a steel hull formed is examined and subsequently modified to improve performance through a combined program of modeling and testing. A finite-element model is developed to predict the response of the joint. The model takes into account the contact at the interface between different materials, progressive damage, large deformation theory, and a non-linear stress-strain relationship. To predict the progressive failure, the analysis combines Hashin failure criteria and maximum stress failure criteria. The results show stress response has a great influence on the strength and bearing of the joint. The Balsawood-steel interface is proved to be critical to the mechanical behavior of the joint. Good agreement between experimental results and numerical predictions is observed.

  8. Method of producing a ceramic fiber-reinforced glass-ceramic matrix composite

    NASA Technical Reports Server (NTRS)

    Bansal, Narottam P. (Inventor)

    1994-01-01

    A fiber-reinforced composite composed of a BaO-Al2O3-2SiO2 (BAS) glass ceramic matrix is reinforced with CVD silicon carbide continuous fibers. A slurry of BAS glass powders is prepared and celsian seeds are added during ball melting. The slurry is cast into tapes which are cut to the proper size. Continuous CVD-SiC fibers are formed into mats of the desired size. The matrix tapes and the fiber mats are alternately stacked in the proper orientation. This tape-mat stack is warm pressed to produce a 'green' composite. The 'green' composite is then heated to an elevated temperature to burn out organic constituents. The remaining interim material is then hot pressed to form a silicon carbide fiber-reinforced celsian (BAS) glass-ceramic matrix composite which may be machined to size.

  9. Flexural retrofitting of reinforced concrete structures using Green Natural Fiber Reinforced Polymer plates

    NASA Astrophysics Data System (ADS)

    Cervantes, Ignacio

    An experimental study will be carried out to determine the suitability of Green Natural Fiber Reinforced Polymer plates (GNFRP) manufactured with hemp fibers, with the purpose of using them as structural materials for the flexural strengthening of reinforced concrete (RC) beams. Four identical RC beams, 96 inches long, are tested for the investigation, three control beams and one test beam. The first three beams are used as references; one unreinforced, one with one layer of Carbon Fiber Reinforced Polymer (CFRP), one with two layers of CFRP, and one with n layers of the proposed, environmental-friendly, GNFRP plates. The goal is to determine the number of GNFRP layers needed to match the strength reached with one layer of CFRP and once matched, assess if the system is less expensive than CFRP strengthening, if this is the case, this strengthening system could be an alternative to the currently used, expensive CFRP systems.

  10. Carbon Fiber Reinforced Carbon Composite Valve for an Internal Combustion Engine

    NASA Technical Reports Server (NTRS)

    Rivers, H. Kevin (Inventor); Ransone, Philip O. (Inventor); Northam, G. Burton (Inventor)

    1999-01-01

    A carbon fiber reinforced carbon composite valve for internal combustion engines and the like formed of continuous carbon fibers throughout the valve's stem and head is disclosed. The valve includes braided carbon fiber material over axially aligned unidirectional carbon fibers forming a valve stem; the braided and unidirectional carbon fibers being broomed out at one end of the valve stem forming the shape of the valve head; the valve-shaped structure being densified and rigidized with a matrix of carbon containing discontinuous carbon fibers: and the finished valve being treated to resist oxidation. Also disclosed is a carbon matrix plug containing continuous and discontinuous carbon fibers and forming a net-shape valve head acting as a mandrel over which the unidirectional and braided carbon fibers are formed according to textile processes. Also disclosed are various preform valves and processes for making finished and preform carbon fiber reinforced carbon composite valves.

  11. Seamless metal-clad fiber-reinforced organic matrix composite structures and process for their manufacture

    NASA Technical Reports Server (NTRS)

    Bluck, Raymond M. (Inventor); Bush, Harold G. (Inventor); Johnson, Robert R. (Inventor)

    1990-01-01

    A metallic outer sleeve is provided which is capable of enveloping a hollow metallic inner member having continuous reinforcing fibers attached to the distal end thereof. The inner member is then introduced into outer sleeve until inner member is completely enveloped by outer sleeve. A liquid matrix member is then injected into space between inner member and outer sleeve. A pressurized heat transfer medium is flowed through the inside of inner member, thereby forming a fiber reinforced matrix composite material. The wall thicknesses of both inner member and outer sleeve are then reduced to the appropriate size by chemical etching, to adjust the thermal expansion coefficient of the metal-clad composite structure to the desired value. thereby forming a fiber reinforced matrix composite material. The wall thicknesses of both inner member and outer sleeve are then reduced to the appropriate size by chemical etching, to adjust the thermal expansion coefficient of the metal-clad composite structure to the desired value. The novelty of this invention resides in the development of a efficient method of producing seamless metal clad fiber reinforced organic matrix composite structures.

  12. All-round joining method with carbon fiber reinforced interface

    NASA Astrophysics Data System (ADS)

    Miwa, Noriyoshi; Tanaka, Kazunori; Kamiya, Yoshiko; Nishi, Yoshitake

    2008-08-01

    Carbon fiber reinforced polymer (CFRP) has been recently applied to not only wing, but also fan blades of turbo fan engines. To prevent impact force, leading edge of titanium was often mounted on the CFRP fan blades with adhesive force. In order to enhance the joining strength, a joining method with carbon fiber reinforced interface has been developed. By using nickel-coated carbon fibers, a joining sample with carbon fiber-reinforced interface between CFRP and CFRM has been successfully developed. The joining sample with nickel-coated carbon fiber interface exhibits the high tensile strength, which was about 10 times higher than that with conventional adhesion. On the other hand, Al-welding methods to steel, Cu and Ti with carbon fiber reinforced interface have been successfully developed to lighten the parts of machines of racing car and airplane. Carbon fibers in felt are covered with metals to protect the interfacial reaction. The first step of the welding method is that the Al coated felt is contacted and wrapped with molten aluminum solidified under gravity pressure, whereas the second step is that the felt with double layer of Ni and Al is contacted and wrapped with molten steel (Cu or Ti) solidified under gravity pressure. Tensile strength of Al-Fe (Cu or Ti) welded sample with carbon fiber reinforced interface is higher than those of Al-Fe (Cu or Ti) welded sample.

  13. Structural Behavior of Concrete Beams Reinforced with Basalt Fiber Reinforced Polymer (BFRP) Bars

    NASA Astrophysics Data System (ADS)

    Ovitigala, Thilan

    The main challenge for civil engineers is to provide sustainable, environmentally friendly and financially feasible structures to the society. Finding new materials such as fiber reinforced polymer (FRP) material that can fulfill the above requirements is a must. FRP material was expensive and it was limited to niche markets such as space shuttles and air industry in the 1960s. Over the time, it became cheaper and spread to other industries such as sporting goods in the 1980-1990, and then towards the infrastructure industry. Design and construction guidelines are available for carbon fiber reinforced polymer (CFRP), aramid fiber reinforced polymer (AFRP) and glass fiber reinforced polymer (GFRP) and they are currently used in structural applications. Since FRP is linear elastic brittle material, design guidelines for the steel reinforcement are not valid for FRP materials. Corrosion of steel reinforcement affects the durability of the concrete structures. FRP reinforcement is identified as an alternative to steel reinforcement in corrosive environments. Although basalt fiber reinforced polymer (BFRP) has many advantages over other FRP materials, but limited studies have been done. These studies didn't include larger BFRP bar diameters that are mostly used in practice. Therefore, larger beam sizes with larger BFRP reinforcement bar diameters are needed to investigate the flexural and shear behavior of BFRP reinforced concrete beams. Also, shear behavior of BFRP reinforced concrete beams was not yet studied. Experimental testing of mechanical properties and bond strength of BFRP bars and flexural and shear behavior of BFRP reinforced concrete beams are needed to include BFRP reinforcement bars in the design codes. This study mainly focuses on the use of BFRP bars as internal reinforcement. The test results of the mechanical properties of BFRP reinforcement bars, the bond strength of BFRP reinforcement bars, and the flexural and shear behavior of concrete beams

  14. Effect of stress on ultrasonic pulses in fiber reinforced composites

    NASA Technical Reports Server (NTRS)

    Hemann, J. H.; Baaklini, G. Y.

    1986-01-01

    An acoustical-ultrasonic technique was used to demonstrate relationships existing between changes in attenuation of stress waves and tensile stress on an eight ply 0 degree graphite-epoxy fiber reinforced composite. All tests were conducted in the linear range of the material for which no mechanical or macroscopic damage was evident. Changes in attenuation were measured as a function of tensile stress in the frequency domain and in the time domain. Stress wave propagation in these specimens was dispersive, i.e., the wave speed depends on frequency. Wave speeds varied from 267,400 cm/sec to 680,000 cm/sec as the frequency of the signal was varied from 150 kHz to 1.9 MHz which strongly suggests that flexural/lamb wave modes of propagation exist. The magnitude of the attenuation changes depended strongly on tensile stress. It was further observed that the wave speeds increased slightly for all tested frequencies as the stress was increased.

  15. Life Cycle Assessment of Carbon Fiber-Reinforced Polymer Composites

    SciTech Connect

    Das, Sujit

    2011-01-01

    Carbon fiber-reinforced polymer matrix composites is gaining momentum with the pressure to lightweight vehicles, however energy-intensity and cost remain some of the major barriers before this material could be used in large-scale automotive applications. A representative automotive part, i.e., a 30.8 kg steel floor pan having a 17% weight reduction potential with stringent cash performance requirements has been considered for the life cycle energy and emissions analysis based on the latest developments occurring in the precursor type (conventional textile-based PAN vs. renewable-based lignin), part manufacturing (conventional SMC vs. P4) and fiber recycling technologies. Carbon fiber production is estimated to be about 14 times more energy-intensive than conventional steel production, however life cycle primary energy use is estimated to be quite similar to the conventional part, i.e., 18,500 MJ/part, especially when considering the uncertainty in LCI data that exists from using numerous sources in the literature. Lignin P4 technology offers the most life cycle energy and CO2 emissions benefits compared to a conventional stamped steel technology. With a 20% reduction in energy use in the lignin conversion to carbon fiber and free availability of lignin as a by-product of ethanol and wood production, a 30% reduction in life cycle energy use could be obtained. A similar level of life cycle energy savings could also be obtained with a higher part weight reduction potential of 43%.

  16. Acoustic emission of fire damaged fiber reinforced concrete

    NASA Astrophysics Data System (ADS)

    Mpalaskas, A. C.; Matikas, T. E.; Aggelis, D. G.

    2016-04-01

    The mechanical behavior of a fiber-reinforced concrete after extensive thermal damage is studied in this paper. Undulated steel fibers have been used for reinforcement. After being exposed to direct fire action at the temperature of 850°C, specimens were subjected to bending and compression in order to determine the loss of strength and stiffness in comparison to intact specimens and between the two types. The fire damage was assessed using nondestructive evaluation techniques, specifically ultrasonic pulse velocity (UPV) and acoustic emission (AE). Apart from the strong, well known, correlation of UPV to strength (both bending and compressive), AE parameters based mainly on the frequency and duration of the emitted signals after cracking events showed a similar or, in certain cases, better correlation with the mechanical parameters and temperature. This demonstrates the sensitivity of AE to the fracture incidents which eventually lead to failure of the material and it is encouraging for potential in-situ use of the technique, where it could provide indices with additional characterization capability concerning the mechanical performance of concrete after it subjected to fire.

  17. New Fiber Reinforced Waterless Concrete for Extraterrestrial Structural Applications

    NASA Technical Reports Server (NTRS)

    Toutanji, H.; Tucker, D.; Ethridge, E.

    2005-01-01

    Commercial use of sulfur concrete on Earth is well established, particularly in corrosive, e.g., acid and salt, environments. Having found troilite (FeS) on the Moon raises the question of using extracted sulfur as a lunar construction mate: iii an attractive alternative to conventional concrete as it does not require water For the purpose of this paper it is assumed that lunar ore is mined, refined, and the raw sulfur processed with appropriate lunar regolith to form, for example, brick and beam elements. Glass fibers produced from regolith were used as a reinforcement to improve the mechanical properties of the sulfur concrete. Glass fibers and glass rebar were produced by melting the lunar regolith simulant. Lunar regolith stimulant was melted in a 25 cc Pt-Rh crucible in a Sybron Thermoline 46100 high temperature MoSi2 furnace at melting temperatures of 1450 to 1600G. The glass melt wets the ceramic rod and long continuous glass fibers were easily hand drawn. The glass fibers were immediately coated with a protective polymer to maintain the mechanical strength. The viability of sulfur concrete as a construction material for extraterrestrial application is presented. The mechanical properties of the glass fiber reinforced sulfur concrete were investigated.

  18. Single-sitting, fiber-reinforced fixed bridges for the missing lateral or central incisors in adolescent patients.

    PubMed

    Belvedere, P C

    1998-10-01

    Many materials, methods, and techniques for the reinforcing of composites to bond a pontic onto abutment teeth have been tried and promoted. In this article, the author examines the use of fiber reinforcement in fixed bridges, describing the various steps performed by the dentist during the procedure. PMID:9891649

  19. Fabrication of fiber-reinforced composites by chemical vapor infiltration

    SciTech Connect

    Besmann, T.M.; McLaughlin, J.C.; Probst, K.J.; Anderson, T.J.; Starr, T.L.

    1997-12-01

    Silicon carbide-based heat exchanger tubes are of interest to energy production and conversion systems due to their excellent high temperature properties. Fiber-reinforced SiC is of particular importance for these applications since it is substantially tougher than monolithic SiC, and therefore more damage and thermal shock tolerant. This paper reviews a program to develop a scaled-up system for the chemical vapor infiltration of tubular shapes of fiber-reinforced SiC. The efforts include producing a unique furnace design, extensive process and system modeling, and experimental efforts to demonstrate tube fabrication.

  20. Damping properties of fiber reinforced composite suitable for stayed cable

    NASA Astrophysics Data System (ADS)

    Li, Jianzhi; Sun, Baochen; Du, Yanliang

    2011-11-01

    Carbon fiber reinforced plastics (CFRP) cables were initially most investigated to replace steel cables. To further explore the advantages of FRP cables, the potential ability of vibration control is studied in this paper emphasizing the designable characteristic of hybrid FRP cables. Fiber reinforced vinyl ester composites and fiber reinforced epoxy composites were prepared by the pultrusion method. Due to the extensive application of fiber reinforced composites, the temperature spectrum and frequency spectrum of loss factor for the composite were tested using dynamic mechanical analysis (DMA) equipment. The damping properties and damping mechanism of the composite were investigated and discussed at different temperatures and frequencies. The result indicates that the loss factor of the composites is increasing with the increase of the frequency from 0.1Hz to 2 Hz and decreasing with the decrease of the temperature from -20°C to 60°C. The loss factor of the carbon fiber composite is higher than that of the glass fiber for the same matrix. The loss factor of the vinyl ester composite is higher than that of the epoxy composite for the same fiber.

  1. Damping properties of fiber reinforced composite suitable for stayed cable

    NASA Astrophysics Data System (ADS)

    Li, Jianzhi; Sun, Baochen; Du, Yanliang

    2012-04-01

    Carbon fiber reinforced plastics (CFRP) cables were initially most investigated to replace steel cables. To further explore the advantages of FRP cables, the potential ability of vibration control is studied in this paper emphasizing the designable characteristic of hybrid FRP cables. Fiber reinforced vinyl ester composites and fiber reinforced epoxy composites were prepared by the pultrusion method. Due to the extensive application of fiber reinforced composites, the temperature spectrum and frequency spectrum of loss factor for the composite were tested using dynamic mechanical analysis (DMA) equipment. The damping properties and damping mechanism of the composite were investigated and discussed at different temperatures and frequencies. The result indicates that the loss factor of the composites is increasing with the increase of the frequency from 0.1Hz to 2 Hz and decreasing with the decrease of the temperature from -20°C to 60°C. The loss factor of the carbon fiber composite is higher than that of the glass fiber for the same matrix. The loss factor of the vinyl ester composite is higher than that of the epoxy composite for the same fiber.

  2. Characterization and design of steel fiber reinforced shotcrete in tunnelling

    SciTech Connect

    Casanova, P.A.; Rossi, P.C.

    1995-12-31

    A design procedure of steel fiber reinforced shotcrete tunnel linings is proposed. It is based on the analysis of a cracked section. The tensile behavior of shotcrete after cracking is obtained by a uniaxial tension test on cored notched samples. As for usual reinforced concrete structures an interaction diagram (moment-axial load) is determined.

  3. Design Guide for glass fiber reinforced metal pressure vessel

    NASA Technical Reports Server (NTRS)

    Landes, R. E.

    1973-01-01

    Design Guide has been prepared for pressure vessel engineers concerned with specific glass fiber reinforced metal tank design or general tank tradeoff study. Design philosophy, general equations, and curves are provided for safelife design of tanks operating under anticipated space shuttle service conditions.

  4. Comparison of fracture resistance of endodontically treated teeth restored with nanohybrid, silorane, and fiber reinforced composite: An in vitro study

    PubMed Central

    Bilgi, Priyanka Shripad; Shah, Nimisha Chinmay; Patel, Parth Pinakinbhai; Vaid, Deepa S

    2016-01-01

    Background: The present study was undertaken to evaluate the most suitable restorative for badly mutilated endodontically treated teeth. Aims: To evaluate and compare the fracture resistance of endodontically treated premolars restored with conventional nanohybrid, silorane composite with glass fibers and newer fiber-reinforced composite in mesio-occluso-distal (MOD) cavities. Materials and Methods: Sixty extracted human maxillary premolars were selected. Fifteen intact teeth served as positive controls (Group 1). Endodontic therapy was done in the remaining 45 teeth. MOD cavities were prepared in all the teeth with standardized dimensions and were randomly divided into three groups (Group 2 - nanohybrid + glass fibers, Group 3 - silorane + glass fibers, and Group 4 – fiber-reinforced composite). Restorations were done for all groups. Fracture resistance was measured by Instron universal testing machine. Statistical Analysis Used: One-way anova test and Tukey's post hoc test. Results: Highest fracture resistance was shown by intact teeth group followed by fiber-reinforced composite, nanohybrid, and silorane, respectively. Statistically Significant difference was revealed by anova test (P < 0.0001) and Tukey's post hoc test (P < 0.0001). Conclusions: Among the experimental groups, fiber-reinforced composite showed the highest fracture resistance. Statistically significant difference was observed for all the groups. PMID:27563188

  5. The effect of different fiber reinforcements on flexural strength of provisional restorative resins: an in-vitro study

    PubMed Central

    Parkhedkar, Rambhau D.; Mowade, Tushar Krishnarao

    2012-01-01

    PURPOSE The aim of this study was to compare the flexural strength of polymethyl methacrylate (PMMA) and bis-acryl composite resin reinforced with polyethylene and glass fibers. MATERIALS AND METHODS Three groups of rectangular test specimens (n = 15) of each of the two resin/fiber reinforcement were prepared for flexural strength test and unreinforced group served as the control. Specimens were loaded in a universal testing machine until fracture. The mean flexural strengths (MPa) was compared by one way ANOVA test, followed by Scheffe analysis, using a significance level of 0.05. Flexural strength between fiber-reinforced resin groups were compared by independent samples t-test. RESULTS For control groups, the flexural strength for PMMA (215.53 MPa) was significantly lower than for bis-acryl composite resin (240.09 MPa). Glass fiber reinforcement produced significantly higher flexural strength for both PMMA (267.01 MPa) and bis-acryl composite resin (305.65 MPa), but the polyethylene fibers showed no significant difference (PMMA resin-218.55 MPa and bis-acryl composite resin-241.66 MPa). Among the reinforced groups, silane impregnated glass fibers showed highest flexural strength for bis-acryl composite resin (305.65 MPa). CONCLUSION Of two fiber reinforcement methods evaluated, glass fiber reinforcement for the PMMA resin and bis-acryl composite resin materials produced highest flexural strength. Clinical implications On the basis of this in-vitro study, the use of glass and polyethylene fibers may be an effective way to reinforce provisional restorative resins. When esthetics and space are of concern, glass fiber seems to be the most appropriate method for reinforcing provisional restorative resins. PMID:22439093

  6. Effect of polyester fiber reinforcement on the mechanical properties of interim fixed partial dentures

    PubMed Central

    Gopichander, N.; Halini Kumarai, K.V.; Vasanthakumar, M.

    2015-01-01

    Background Different reinforcements currently available for interim fixed partial denture (FPD) materials do not provide the ideal strength for long-term use. Therefore, the aim of this investigation was to develop a more ideal provisional material for long-term use with better mechanical properties. This study evaluated the effectiveness of polyester fiber reinforcement on different interim FPD materials. Methods Thirty resin-bonded FPDs were constructed from three provisional interim FPD materials. Specimens were tested with a universal testing machine (UTM). The modulus of elasticity and flexural strength were recorded in MPa. The compressive strength and degree of deflection were calculated from the obtained values, and a two-way analysis of variance (ANOVA) was used to determine the significance. Results The polyester fiber reinforcement increased the mechanical properties. The modulus of elasticity for heat-polymerized polymethyl methacrylate (PMMA) was 624 MPa, compared to 700.2 MPa for the reinforced heat-cured sample. The flexural strengths of the bis-acrylic and cold-polymerized reinforced samples increased significantly to 2807 MPa and 979.86 MPa, respectively, compared to the nonreinforced samples. The mean compressive strength of the reinforced cold-polymerized PMMA samples was 439.17 MPa; and for the reinforced heat-polymerized PMMA samples, it was 1117.41 MPa. The degree of deflection was significantly greater (P < 0.05) in the reinforced bis-acrylic sample (5.03 MPa), compared with the nonreinforced bis-acrylic sample (2.95 MPa). Conclusion Within the limitations of this study, polyester fiber reinforcements improved the mechanical properties of heat-polymerized PMMA, cold-polymerized PMMA, and bis-acrylic provisional FPD materials. PMID:26644754

  7. Laser cutting of carbon fiber reinforced plastics (CFRP) by UV pulsed laser ablation

    NASA Astrophysics Data System (ADS)

    Niino, Hiroyuki; Kurosaki, Ryozo

    2011-03-01

    In this paper, we report on a micro-cutting of carbon fiber reinforced plastics (CFRP) by nanosecond-pulsed laser ablation with a diode-pumped solid state UV laser (DPSS UV laser, λ= 355nm). A well-defined cutting of CFRP which were free of debris and thermal-damages around the grooves, were performed by the laser ablation with a multiple-scanpass irradiation method. CFRP is a high strength composite material with a lightweight, and is increasingly being used various applications. UV pulsed laser ablation is suitable for laser cutting process of CFRP materials, which drastically reduces a thermal damage at cut regions.

  8. Predicted inlet gas temperatures for tungsten fiber reinforced superalloy turbine blades

    NASA Technical Reports Server (NTRS)

    Winsa, E. A.; Westfall, L. J.; Petrasek, D. W.

    1978-01-01

    Tungsten fiber reinforced superalloy composite (TFRS) impingement cooled turbine blade inlet gas temperatures were calculated taking into account material spanwise strength, thermal conductivity, material oxidation resistance, fiber-matrix interaction, and coolant flow. Measured values of TFRS thermal conductivities are presented. Calculations indicate that blades made of 30 volume percent fiber content TFRS having a 12,000 N-m/kg stress-to-density ratio while operating at 40 atmospheres and a 0.06 coolant flow ratio could permit a turbine blade inlet gas temperature of over 1900K. This is more than 150K greater than similar superalloy blades.

  9. Simulations of Fiber Distribution Effects in Fiber-Reinforced Cement Composites

    SciTech Connect

    Bolander, John E.; Lim, Yun Mook

    2008-02-15

    This paper describes a lattice model for coupled moisture transport/stress analyses of fiber-reinforced cement composites (FRCC). Each fiber, and its interface with the matrix material, is explicitly represented within the three-dimensional material volume. This enables the direct study of fiber orientation and distribution effects on composite performance. Realistic, nonuniform fiber distributions can be specified as model input. Basic applications of the model are presented, with emphasis toward simulating the durability mechanics of FRCC exposed to drying environments. The modeling of functionally graded FRCC is an obvious potential extension of this work.

  10. Performance and stability of advanced monolithic and fiber reinforced composite candle filters during PCFBC operation

    SciTech Connect

    Alvin, M.A.

    1996-12-31

    Advanced clay bonded silicon carbide, alumina/mullite and CVI-SiC fiber reinforced composite porous ceramic candle filters have been identified for use in pressurized circulating fluidized-bed combustion (PCFBC) systems where operating temperatures approach 870--900 C. In this paper the author will discuss the performance of these filter elements, and explore the response and stability of the advanced filter materials after 540 hours of operation in Foster Wheeler`s PCFBC system in Karhula, Finland. The potential use of the advanced filter materials for extended operating life in high temperature, pressurized, coal-fired process applications will also be addressed.

  11. Study of fracture mechanisms of short fiber reinforced AS composite by acoustic emission technique

    SciTech Connect

    Kida, Sotoaki; Suzuki, Megumu

    1995-11-01

    The fracture mechanisms of short fiber reinforced AS composites are studied by acoustic emission technique for examining the effects of fiber contents. The loads P{sub b} and P{sub c} which the damage mechanisms change are obtained at the inflection points of the total AE energy curve the energy gradient method. The damages are generated by fiber breaking at the load point of P{sub b} and P{sub c} in B material, and by the fiber breaking and the debonding between resin and fiber at the load points of P{sub b} and P{sub c} in C material.

  12. Passive vibration damping of carbon fiber reinforced plastic with PZT particles and SMA powder

    NASA Astrophysics Data System (ADS)

    Jung, Jaemin; Lee, Woo Il; Lee, Dasom; Park, Sungho; Moon, Sungnam

    2016-04-01

    Carbon fiber reinforced plastic (CFRP) has been used various industrial fields, because of high strength, light weight, corrosion resistance and other properties. In this study, lead zirconate titanate (PZT) ceramic particles which is one of typical piezoelectric material and shape memory alloy powder dispersed in CFRP laminate in order to improve the vibration damping by dissipating vibration energy quickly. The loss factor (tanδ) is measured in Dynamic mechanical analyzer (DMA) which is used to measure the viscoelastic behavior of a material to verify the change in vibration damping. The results show that there exists difference on vibration damping ability between CFRP with PZT ceramic particles and CFRP with SMA powder.

  13. Evaluation of residual strength in the basalt fiber reinforced composites under impact damage

    NASA Astrophysics Data System (ADS)

    Kim, Yun-Hae; Lee, Jin-Woo; Moon, Kyung-Man; Yoon, Sung-Won; Baek, Tae-Sil; Hwang, Kwang-Il

    2015-03-01

    Composites are vulnerable to the impact damage by the collision as to the thickness direction, because composites are being manufactured by laminating the fiber. The understanding about the retained strength after the impact damage of the material is essential in order to secure the reliability of the structure design using the composites. In this paper, we have tried to evaluate the motion of the material according to the kinetic energy and potential energy and the retained strength after impact damage by testing the free fall test of the basalt fiber reinforced composite in the limelight as the environment friendly characteristic.

  14. In Vitro Study of Transverse Strength of Fiber Reinforced Composites

    PubMed Central

    Mosharraf, R.; Hashemi, Z.; Torkan, S.

    2011-01-01

    Objective Reinforcement with fiber is an effective method for considerable improvement in flexural properties of indirect composite resin restorations. The aim of this in-vitro study was to compare the transverse strength of composite resin bars reinforced with pre-impregnated and non-impregnated fibers. Materials and Methods Thirty six bar type composite resin specimens (3×2×25 mm) were constructed in three groups. The first group was the control group (C) without any fiber reinforcement. The specimens in the second group (P) were reinforced with pre-impregnated fibers and the third group (N) with non-impregnated fibers. These specimens were tested by the three-point bending method to measure primary transverse strength. Data were statistically analyzed with one way ANOVA and Tukey’s tests. Results There was a significant difference among the mean primary transverse strength in the three groups (P<0.001). The post-hoc (Tukey) test showed that there was a significant difference between the pre-impregnated and control groups in their primary transverse strength (P<0.001). Regarding deflection, there was also a significant difference among the three groups (P=0.001). There were significant differences among the mean deflection of the control group and two other groups (PC&N<.001 and PC&P=.004), but there was no significant difference between the non-and pre-impregnated groups (PN&P=.813). Conclusion Within the limitations of this study, it was concluded that reinforcement with fiber considerably increased the transverse strength of composite resin specimens, but impregnation of the fiber used implemented no significant difference in the transverse strength of composite resin samples. PMID:22457836

  15. Discrete fiber-reinforced polyurea systems for infrastructure strengthening and blast mitigation

    NASA Astrophysics Data System (ADS)

    Carey, Natalia L.

    The research presented in this dissertation focused on evaluating the effectiveness of various blast mitigation materials and coating technologies to be used for enhancing blast resistance of structural members. Mechanical properties and blast mitigation performance of different discrete fiber-reinforced polyurea (DFRP) systems were investigated through experimental and analytical work. Four technical papers discuss the research efforts conducted within this dissertation. The first paper examined the development and characterization of different DFRP systems for infrastructure strengthening and blast retrofit. The behavior of various systems which consisted of chopped E-glass fibers discretely integrated in with the polyurea matrix was evaluated through coupon tensile testing. The addition of glass fiber to a polymer coating provided improved stiffness and strength to the composite system while the polyurea base material provided ductility. The second paper evaluated the behavior of hybrid, plain, and steel fiber-reinforced concrete panels coated with various polyurea and DFRP systems under blast loading. Hybrid panels demonstrated higher blast mitigation performance compared to plain and steel fiber-reinforced concrete panels due to sacrificial hybrid layer. The addition of plain polyurea or DFRP systems on the tension side improved panel performance by containing fragmentation during a blast event. The third paper presents an analytical investigation conducted using the explicit finite element program LS-DYNA to model panel and coating response under blast loading. Several modeling solutions were undertaken and compared for concrete formulation. Modeling results were analyzed and compared to the experimental work to validate the conclusions. The final paper describes an internal equilibrium mechanics based model developed to predict the flexural capacity of reinforced concrete beams strengthened with various DFRP systems. The developed model was validated using

  16. Simplified analyses of a fiber-reinforced plastic joint for filament-wound pipes

    SciTech Connect

    Estrada, H.; Parsons, I.D.

    1999-08-01

    A simplified analysis procedure is described for a fiber-reinforced plastic (FRP) stub-flanged joint which addresses some of the problems with current FRP joints. The joint consists of a tapered hub that is filament-wound with the pipe. A separate stub is used to connect the two halves of the joint. This system avoids material discontinuities at the flange-pipe intersection and pull-back of the flange. The joint is modeled following the Taylor Forge approach used in metallic joint analysis. The analytical model is verified using finite element analysis; the results are in excellent agreement.

  17. High-temperature tensile properties of fiber reinforced reaction bonded silicon nitride

    NASA Technical Reports Server (NTRS)

    Jablonski, David A.; Bhatt, Ramakrishna T.

    1990-01-01

    Measurements of tensile properties of unidirectional silicon carbide fiber-reinforced reaction-bonded silicon nitride (SiC/RBSN) composite specimens were carried out in air at 25, 1300, and 1500 C, using a new testing technique and a specially designed gripping system that minimizes bending moment and assures that failure always occurred in the gage section. The material was found to display metallike stress-strain behavior at all temperatures tested, and a noncatastrophic failure beyond the matrix fracture. The tensile properties were found to be temperature dependent, with the values of the ultimate tensile strength decreasing with temperature, from 543 MPa at 25 C to 169 at 1500 C.

  18. Carbon Fiber Reinforced Carbon Composites Rotary Valves for Internal Combustion Engines

    NASA Technical Reports Server (NTRS)

    Northam, G. Burton (Inventor); Ransone, Philip O. (Inventor); Rivers, H. Kevin (Inventor)

    1999-01-01

    Carbon fiber reinforced carbon composite rotary, sleeve, and disc valves for internal combustion engines and the like are disclosed. The valves are formed from knitted or braided or warp-locked carbon fiber shapes. Also disclosed are valves fabricated from woven carbon fibers and from molded carbon matrix material. The valves of the present invention with their very low coefficient of thermal expansion and excellent thermal and self-lubrication properties, do not present the sealing and lubrication problems that have prevented rotary, sleeve, and disc valves from operating efficiently and reliably in the past. Also disclosed are a sealing tang to further improve sealing capabilities and anti-oxidation treatments.

  19. Carbon Fiber Reinforced Carbon Composite Rotary Valve for an Internal Combustion Engine

    NASA Technical Reports Server (NTRS)

    Northam, G.Burton (Inventor); Ransone, Philip O. (Inventor); Rivers, H. Kevin (Inventor)

    2000-01-01

    Carbon fiber reinforced carbon composite rotary sleeve, and disc valves for internal combustion engines and the like are disclosed. The valves are formed from knitted or braided or wrap-locked carbon fiber shapes. Also disclosed are valves fabricated from woven carbon fibers and from molded carbon matrix material. The valves of the present invention with their very low coefficient of thermal expansion and excellent thermal and self-lubrication properties do not present the sealing and lubrication problems that have prevented rotary sleeve and disc valves from operating efficiently and reliably in the past. Also disclosed are a sealing tang to further improve sealing capabilities and anti-oxidation treatments.

  20. Mechanical properties of long carbon fiber reinforced thermoplastic (LFT) at elevated temperature

    NASA Astrophysics Data System (ADS)

    Wang, Qiushi

    Long fiber reinforced thermoplastics (LFT) possess high specific modulus and strength, superior damage tolerance and fracture toughness and have found increasing use in transportation, military, and aerospace applications. However, one of the impediments to utilizing these materials is the lack of performance data in harsh conditions, especially at elevated temperature. In order to quantify the effect of temperature on the mechanical properties of carbon fiber reinforced thermoplastic composites, carbon fiber PAA composite plates containing 20% and 30% carbon fiber were produced using extrusion/compression molding process and tested at three representative temperatures, room temperature (RT 26°C), middle temperature (MID 60°C) and glass transition temperature (Tg 80°C). A heating chamber was designed and fabricated for the testing at elevated temperature. As temperature increases, flexural modulus, flexural strength, tensile modulus and tensile strength decrease. The highest reduction observed in stiffness (modulus) values of 30% CF/PAA at Tg in the 00 orientation is 75%. The reduction values were larger for the transverse (perpendicular to flow direction) samples than the longitudinal (flow direction) samples. The property reduction in 30% CF/PAA is larger than 20% CF/PAA. Furthermore, an innovative method was developed to calculate the fiber content in carbon fiber reinforced composites by burning off the neat resin and sample in a tube furnace. This method was proved to be accurate (within 1.5 wt. % deviation) by using burning off data obtained from CF/Epoxy and CF/Vinyl Ester samples. 20% and 30% carbon/PAA samples were burned off and carbon fiber content was obtained using this method. The results of the present study will be helpful in determining the end-user applications of these composite materials. Keywords: Long Carbon Fibers, Elevated Temperature, Mechanical Properties, Burn off Test.

  1. Stabilized fiber-reinforced pavement base course with recycled aggregate

    NASA Astrophysics Data System (ADS)

    Sobhan, Khaled

    's assumptions for rigid pavements), which has been found to explain reasonably well the field behavior of unreinforced and fiber-reinforced concrete slabs on grade. Finally, a preliminary cost analysis demonstrated that the use of stabilized recycled aggregate instead of a standard crushed stone base course can result in a meaningful economic savings.

  2. Unified micromechanics of damping for unidirectional fiber reinforced composites

    NASA Technical Reports Server (NTRS)

    Saravanos, D. A.; Chamis, C. C.

    1989-01-01

    An integrated micromechanics methodology for the prediction of damping capacity in fiber-reinforced polymer matrix unidirectional composites has been developed. Explicit micromechanics equations based on hysteretic damping are presented relating the on-axis damping capacities to the fiber and matrix properties and volume fraction. The damping capacities of unidirectional composites subjected to off-axis loading are synthesized from thermal effect on the damping performance of unidirectional composites due to temperature and moisture variations is also modeled. The damping contributions from interfacial friction between broken fibers and matrix are incorporated. Finally, the temperature rise in continuously vibrating composite plies is estimated. Application examples illustrate the significance of various parameters on the damping performance of unidirectional and off-axis fiber reinforced composites.

  3. Studies on natural fiber reinforced polymer matrix composites

    NASA Astrophysics Data System (ADS)

    Patel, R. H.; Kapatel, P. M.; Machchhar, A. D.; Kapatel, Y. A.

    2016-05-01

    Natural fiber reinforced composites show increasing importance in day to days applications because of their low cost, lightweight, easy availability, non-toxicity, biodegradability and environment friendly nature. But these fibers are hydrophilic in nature. Thus they have very low reactivity and poor compatibility with polymers. To overcome these limitations chemical modifications of the fibers have been carried out. Therefore, in the present work jute fibers have chemically modified by treating with sodium hydroxide (NaOH) solutions. These treated jute fibers have been used to fabricate jute fiber reinforced epoxy composites. Mechanical properties like tensile strength, flexural strength and impact strength have been found out. Alkali treated composites show better properties compare to untreated composites.

  4. Fabrication of fiber-reinforced composites by chemical vapor infiltration

    SciTech Connect

    Besmann, T.M.; Stinton, D.P.; Matlin, W.M.; Liaw, P.K.

    1996-08-01

    Processing equipment for the infiltration of fiber-reinforced composite tubes is being designed that incorporates improvements over the equipment used to infiltrate disks. A computer-controlled machine-man interface is being developed to allow for total control of all processing variables. Additionally, several improvements are being made to the furnace that will reduce the complexity and cost of the process. These improvements include the incorporation of free standing preforms, cast mandrels, and simpler graphite heating elements.

  5. Dynamic tensile strength of glass fiber reinforced pultruded composites

    SciTech Connect

    Dutta, P.K.; Kumar, M.M.; Hui, D.

    1994-12-31

    This paper discusses the stress-strain behavior, fracture strength, influence of low temperature, and energy absorption in the diametral tensile splitting fracturing of a Glass Fiber Reinforced Polymer Composite. Experiments were conducted at low-temperature in a thermal chamber installed on a servo-hydraulic universal testing machine. The tensile strength was determined by diametral compression of disc samples at 24, {minus}5 and {minus}40 C.

  6. Elastic/viscoplastic behavior of fiber-reinforced thermoplastic composites

    NASA Technical Reports Server (NTRS)

    Wang, C.; Sun, C. T.; Gates, T. S.

    1990-01-01

    An elastic/viscoplastic constitutive model was used to characterize the nonlinear and rate dependent behavior of a continuous fiber-reinforced thermoplastic composite. This model was incorporated into a finite element program for the analysis of laminated plates and shells. Details on the finite element formulation with the proposed constitutive model were presented. The numerical results were compared with experimental data for uniaxial tension and three-point bending tests of (+ or - 45 deg)3s APC-2 laminates.

  7. Carbon fiber reinforced composites: their structural and thermal properties

    NASA Astrophysics Data System (ADS)

    Cheng, Jingquan; Yang, Dehua

    2010-07-01

    More and more astronomical telescopes use carbon fiber reinforced composites (CFRP). CFRP has high stiffness, high strength, and low thermal expansion. However, they are not isotropic in performance. Their properties are direction dependent. This paper discusses, in detail, the structural and thermal properties of carbon fiber structure members, such as tubes, plates, and honeycomb sandwich structures. Comparisons are provided both from the structural point of view and from the thermal point of view.

  8. Fabrication of fiber-reinforced composites by chemical vapor infiltration

    SciTech Connect

    Besmann, T.M.; Matlin, W.M.; Stinton, D.P.; Liaw, P.K.

    1996-06-01

    Processing equipment for the infiltration of fiber-reinforced composite tubes is being designed that incorporates improvements over the equipment used to infiltrate disks. A computer-controlled machine-man interface is being developed to allow for total control of all processing variables. Additionally, several improvements are being made to the furnace that will reduce the complexity and cost of the process. These improvements include the incorporation of free standing preforms, cast mandrels, and simpler graphite heating elements.

  9. Wear of short carbon-fiber-reinforced PAI and PPS

    SciTech Connect

    Behrens, W.W.; Jerina, K.L.; Hahn, H.T.

    1988-07-01

    Wear of short carbon-fiber-reinforced polyamide-imide and polyphenylene sulfide is described. Comparative data from thrust washer wear tests for both polymers are presented. Fiber orientation is shown to have a significant effect on wear rates. The wear mechanisms in both polymers are illustrated with optical and scanning electron micrographs. Wear is shown to be a nonlinear function of time and stress for both PPS and PAI. 15 references, 14 figures.

  10. Modeling the thermal conductivity of fiber-reinforced ceramic composites

    SciTech Connect

    Beecher, S.C.; Dinwiddie, R.B.

    1993-06-01

    A review of models for the prediction of the thermal conductivity of uni-directional fiber-reinforced composites will be presented. The ability of these models to give an accurate prediction of the composite thermal conductivity depends on the amount of information known about the constituent phase properties under the assumption that these properties do not change as a result of processing. Also presented are models that take into account the effects of fiber coatings.

  11. On Healable Polymers and Fiber-Reinforced Composites

    NASA Astrophysics Data System (ADS)

    Nielsen, Christian Eric

    Polymeric materials capable of healing damage would be valuable in structural applications where access for repair is limited. Approaches to creating such materials are reviewed, with the present work focusing on polymers with thermally reversible covalent cross-links. These special cross-links are Diels-Alder (DA) adducts, which can be separated and re-formed, enabling healing of mechanical damage at the molecular level. Several DA-based polymers, including 2MEP4FS, are mechanically and thermally characterized. The polymerization reaction of 2MEP4FS is modeled and the number of established DA adducts is associated with the glass transition temperature of the polymer. The models are applied to concentric cylinder rotational measurements of 2MEP4FS prepolymer at room and elevated temperatures to describe the viscosity as a function of time, temperature, and conversion. Mechanical damage including cracks and scratches are imparted in cured polymer samples and subsequently healed. Damage due to high temperature thermal degradation is observed to not be reversible. The ability to repair damage without flowing polymer chains makes DA-based healable polymers particularly well-suited for crack healing. The double cleavage drilled compression (DCDC) fracture test is investigated as a useful method of creating and incrementally growing cracks in a sample. The effect of sample geometry on the fracture behavior is experimentally and computationally studied. Computational and empirical models are developed to estimate critical stress intensity factors from DCDC results. Glass and carbon fiber-reinforced composites are fabricated with 2MEP4FS as the matrix material. A prepreg process is developed that uses temperature to control the polymerization rate of the monomers and produce homogeneous prepolymer for integration with a layer of unidirectional fiber. Multiple prepreg layers are laminated to form multi-layered cross-ply healable composites, which are characterized in

  12. Fracture toughness of steel-fiber-reinforced bone cement.

    PubMed

    Kotha, S P; Li, C; Schmid, S R; Mason, J J

    2004-09-01

    Fractures in the bone-cement mantle (polymethyl methacrylate) have been linked to the failure of cemented total joint prostheses. The heat generated by the curing bone cement has also been implicated in the necrosis of surrounding bone tissue, leading to loosening of the implants. The addition of reinforcements may improve the fracture properties of bone cement and decrease the peak temperatures during curing. This study investigates the changes in the fracture properties and the temperatures generated in the ASTM F451 tests by the addition of 316L stainless steel fibers to bone cement. The influence of filler volume fraction (5-15% by volume) and aspect ratios (19, 46, 57) on the fracture toughness of the acrylic bone cement was assessed. Increasing the volume fraction of the steel fibers resulted in significant increases in the fracture toughness of the steel-fiber-reinforced composite. Fracture-toughness increases of up to 2.63 times the control values were obtained with the use of steel-fiber reinforcements. No clear trend in the fracture toughness was discerned for increasing aspect ratios of the reinforcements. There is a decrease in the peak temperatures reached during the curing of the steel-fiber-reinforced bone cement, though the decrease is too small to be clinically relevant. Large increases in the fatigue life of acrylic bone cement were also obtained by the addition of steel fibers. These results indicate that the use of steel fibers may enhance the durability of cemented joint prostheses. PMID:15293326

  13. Structure-property relationships of bismaleimides

    NASA Astrophysics Data System (ADS)

    Tenteris-Noebe, Anita Diane

    The purpose of this research was to control and systematically vary the network topology of bismaleimides through cure temperature and chemistry (addition of various coreactants) and subsequently attempt to determine structure-mechanical property relationships. Characterization of the bismaleimide structures by dielectric, rheological, and thermal analyses, and density measurements was subsequently correlated with mechanical properties such as modulus, yield strength, fracture energy, and stress relaxation. The model material used in this investigation was 4,4sp'-bismaleimidodiphenyl methane (BMI). BMI was coreacted with either 4,4sp'-methylene dianiline (MDA), o,osp'-diallyl bisphenol A (DABA) from Ciba Geigy, or diamino diphenyl sulfone (DDS). Three cure paths were employed: a low-temperature cure of 140sp°C where chain extension should predominate, a high-temperature cure of 220sp°C where both chain extension and crosslinking should occur simultaneously, and a low-temperature (140sp°C) cure followed immediately by a high-temperature (220sp°C) cure where the chain extension reaction or amine addition precedes BMI homopolymerization or crosslinking. Samples of cured and postcured PMR-15 were also tested to determine the effects of postcuring on the mechanical properties. The low-temperature cure condition of BMI/MDA exhibited the highest modulus values for a given mole fraction of BMI with the modulus decreasing with decreasing concentration of BMI. The higher elastic modulus is the result of steric hindrance by unreacted BMI molecules in the glassy state. The moduli values for the high- and low/high-temperature cure conditions of BMI/MDA decreased as the amount of diamine increased. All the moduli values mimic the yield strength and density trends. For the high-temperature cure condition, the room-temperature modulus remained constant with decreasing mole fraction of BMI for the BMI/DABA and BMI/DDS systems. Postcuring PMR-15 increases the modulus over that

  14. Structure-Property Relationships of Bismaleimides

    NASA Technical Reports Server (NTRS)

    Tenteris-Noebe, Anita D.

    1997-01-01

    The purpose of this research was to control and systematically vary the network topology of bismaleimides through cure temperature and chemistry (addition of various coreactants) and subsequently attempt to determine structure-mechanical property relationships. Characterization of the bismaleimide structures by dielectric, rheological, and thermal analyses, and density measurements was subsequently correlated with mechanical properties such as modulus, yield strength, fracture energy, and stress relaxation. The model material used in this investigation was 4,4'-BismaleiMidodIphenyl methane (BMI). BMI was coreacted with either 4,4'-Methylene Dianiline (MDA), o,o'-diallyl bisphenol A (DABA) from Ciba Geigy, or Diamino Diphenyl Sulfone (DDS). Three cure paths were employed: a low- temperature cure of 140 C where chain extension should predominate, a high-temperature cure of 220 C where both chain extension and crosslinking should occur simultaneously, and a low-temperature (140 C) cure followed immediately by a high-temperature (220 C) cure where the chain extension reaction or amine addition precedes BMI homopolymerization or crosslinking. Samples of cured and postcured PMR-15 were also tested to determine the effects of postcuring on the mechanical properties. The low-temperature cure condition of BMI/MDA exhibited the highest modulus values for a given mole fraction of BMI with the modulus decreasing with decreasing concentration of BMI. The higher elastic modulus is the result of steric hindrance by unreacted BMI molecules in the glassy state. The moduli values for the high- and low/high-temperature cure conditions of BMI/MDA decreased as the amount of diamine increased. All the moduli values mimic the yield strength and density trends. For the high-temperature cure condition, the room- temperature modulus remained constant with decreasing mole fraction of BMT for the BMI/DABA and BMI/DDS systems. Postcuring PMR-15 increases the modulus over that of the cured

  15. Teeth restored using fiber-reinforced posts: in vitro fracture tests and finite element analysis.

    PubMed

    Schmitter, M; Rammelsberg, P; Lenz, J; Scheuber, S; Schweizerhof, K; Rues, S

    2010-09-01

    In dentistry the restoration of decayed teeth is challenging and makes great demands on both the dentist and the materials. Hence, fiber-reinforced posts have been introduced. The effects of different variables on the ultimate load on teeth restored using fiber-reinforced posts is controversial, maybe because the results are mostly based on non-standardized in vitro tests and, therefore, give inhomogeneous results. This study combines the advantages of in vitro tests and finite element analysis (FEA) to clarify the effects of ferrule height, post length and cementation technique used for restoration. Sixty-four single rooted premolars were decoronated (ferrule height 1 or 2 mm), endodontically treated and restored using fiber posts (length 2 or 7 mm), composite fillings and metal crowns (resin bonded or cemented). After thermocycling and chewing simulation the samples were loaded until fracture, recording first damage events. Using UNIANOVA to analyze recorded fracture loads, ferrule height and cementation technique were found to be significant, i.e. increased ferrule height and resin bonding of the crown resulted in higher fracture loads. Post length had no significant effect. All conventionally cemented crowns with a 1-mm ferrule height failed during artificial ageing, in contrast to resin-bonded crowns (75% survival rate). FEA confirmed these results and provided information about stress and force distribution within the restoration. Based on the findings of in vitro tests and computations we concluded that crowns, especially those with a small ferrule height, should be resin bonded. Finally, centrally positioned fiber-reinforced posts did not contribute to load transfer as long as the bond between the tooth and composite core was intact. PMID:20227533

  16. ICCM - V; Proceedings of the fifth international conference on composite materials, San Diego, CA, July 29-August 1, 1985

    SciTech Connect

    Harrigan, W.C. Jr.; Strife, J.; Dhingra, A.K.

    1985-01-01

    The present conference considers such topics as residual stress effects on the strength of metal matrix composites, thermal cycling damage in SiC whisker-reinforced aluminum, the failure modes of laminates, biaxial fatigue damage of composites, the service life of aramid fibers under constant stress, fracture in particle dispersion composites, novel epoxy resin formulations, and a process for the metallization of carbon fibers. Also discussed are robotic processing of composites, ropes and cables as composite linear tensile materials, fiber-reinforced SiC, structural problems in ceramic matrix composites, the interface and matrix optimization of sintered ceramic composites, SiC fiber-reinforced glass-ceramic composites, the degradation of carbon fibers by molten aluminum, and the damage tolerance of thermoplastic-matrix graphite fiber-reinforced composites. Further topics encompass failure processes in carbon-reinforced aluminum composites, interlaminar fracture mechanisms in a thermoplastic matrix composite laminate, filament-winding process models, the effect of trigger geometry on the energy absorption of composite tubes, aeroelastic tailoring in aircraft design, the mechanical behavior of three-dimensional woven fiber composites, the postbuckling behavior of curved composite panels, moisture effects and damage in composites, the behavior of aramid fiber yarns under transverse impact, and the development status of bismaleimide resins for composites.

  17. Plastic matrix composites with continuous fiber reinforcement

    SciTech Connect

    1991-09-19

    Most plastic resins are not suitable for structural applications. Although many resins are extremely tough, most lack strength, stiffness, and deform under load with time. By mixing strong, stiff, fibrous materials into the plastic matrix, a variety of structural composite materials can be formed. The properties of these composites can be tailored by fiber selection, orientation, and other factors to suit specific applications. The advantages and disadvantages of fiberglass, carbon-graphite, aramid (Kevlar 49), and boron fibers are summarized.

  18. Simulated space environmental effects on a polyetherimide and its carbon fiber-reinforced composites

    NASA Technical Reports Server (NTRS)

    Kern, Kristen T.; Stancil, Phillip C.; Harries, Wynford L.; Long, Edward R., Jr.; Thibeault, Sheila A.

    1993-01-01

    The selection of materials for spacecraft construction requires identification of candidate materials which can perform reliably in the space environment. Understanding the effects of the space environment on the materials is an important step in the selection of candidate materials. This work examines the effects of energetic electrons, thermal cycling, electron radiation in conjunction with thermal cycling, and atomic oxygen on a thermoplastic polyetherimide and its carbon-fiber-reinforced composites. Composite materials made with non-sized fibers as well as materials made with fibers sized with an epoxy were evaluated. The mechanical and thermomechanical properties of the materials were studied and spectroscopic techniques were used to investigate the mechanisms for the observed effects. Considerations for future material development are suggested.

  19. Fiber-reinforced ceramic composites for Earth-to-orbit rocket engine turbines

    NASA Technical Reports Server (NTRS)

    Brockmeyer, Jerry W.; Schnittgrund, Gary D.

    1990-01-01

    Fiber reinforced ceramic matrix composites (FRCMC) are emerging materials systems that offer potential for use in liquid rocket engines. Advantages of these materials in rocket engine turbomachinery include performance gain due to higher turbine inlet temperature, reduced launch costs, reduced maintenance with associated cost benefits, and reduced weight. This program was initiated to assess the state of FRCMC development and to propose a plan for their implementation into liquid rocket engine turbomachinery. A complete range of FRCMC materials was investigated relative to their development status and feasibility for use in the hot gas path of earth-to-orbit rocket engine turbomachinery. Of the candidate systems, carbon fiber-reinforced silicon carbide (C/SiC) offers the greatest near-term potential. Critical hot gas path components were identified, and the first stage inlet nozzle and turbine rotor of the fuel turbopump for the liquid oxygen/hydrogen Space Transportation Main Engine (STME) were selected for conceptual design and analysis. The critical issues associated with the use of FRCMC were identified. Turbine blades were designed, analyzed and fabricated. The Technology Development Plan, completed as Task 5 of this program, provides a course of action for resolution of these issues.

  20. Novel surface modifications of carbon fiber-reinforced polyetheretherketone hip stem in an ovine model.

    PubMed

    Nakahara, Ichiro; Takao, Masaki; Bandoh, Shunichi; Bertollo, Nicky; Walsh, William R; Sugano, Nobuhiko

    2012-01-01

    A carbon fiber-reinforced polymer (CFRP) is theoretically a suitable material for use in an uncemented hip prosthesis considering it can provide isoelastic environment with the surrounding bone, adequate fatigue strength, and a metal-free radiographic evaluation. To date, the selection of polymer material and optimization of both design and surface finish of the prostheses for osseointegration has not been accomplished. This study examined radiographic and histologic results of an uncemented CFRP stem manufactured from carbon fiber-reinforced polyetheretherketone (CFR/PEEK) with a roughened surface and a bioactive treatment in an adult ovine model following a 12-month implantation period. A unilateral hemiarthroplasty of the hip was performed using the CFRP stem or a titanium stem as a control. Four cases with the CFRP stem and five cases with titanium stem were evaluated. Bone on-growth fixation was achieved in two cases with the CFRP stem and in all the cases with the titanium stem. The CFRP cases showed minimal stress shielding while three of five cases with the titanium stem demonstrated typical osteopenia associated with stiff metal stems. Bone on-growth to the uncemented CFRP stem was achieved by using the CFR/PEEK for the material and modifying the surface design and the bioactive surface finish. Bone resorption and osteopenia observed with the Ti stems was not found with the CFRP design. PMID:21819435

  1. [Tribological properties of carbon fiber-reinforced plastic. Experimental and clinical results].

    PubMed

    Früh, H J; Ascherl, R; Hipp, E

    1997-02-01

    Wear of the articulating components (especially PE-UHMW) of total hip endoprostheses is the most important technical factor limiting the functional lifetime. To minimize wear debris, ceramic heads, according to ISO 6474 (Al2O3), have been used, from 1969 paired with Al2O3 and since 1975 paired with PE-UHMW. Al2O3 balls articulating with cups made from CFRP have been in clinical use since 1988. Laboratory experiments and in-vivo testing showed minimized wear debris and mild biological response to wear products using CFRP (carbon fiber reinforced plastic) instead of PE-UHMW as the cup material. The articulating surfaces of retrieved ceramic heads (Al2O3-Biolox) and cementless CFRP cups (carbon fiber reinforced plastic, Caproman) were compared using sphericity measurement techniques, scanning electron microscopy (SEM) and roughness measurements (including advanced roughness parameters Rvk or Rpk according to ISO 4287). Altogether, the first results of the clinical study showed that the combination Al2O3-ball/CFRP-cup came up to the expected lower wear rates compared with the conventional combinations. The wear rates are comparable with the combination Al2O3/Al2O3 without the material-related problems of ceramic components in all ceramic combinations. PMID:9157355

  2. Enhancement of osteogenesis on micro/nano-topographical carbon fiber-reinforced polyetheretherketone-nanohydroxyapatite biocomposite.

    PubMed

    Xu, Anxiu; Liu, Xiaochen; Gao, Xiang; Deng, Feng; Deng, Yi; Wei, Shicheng

    2015-03-01

    As an FDA-approved implantable material, carbon fiber-reinforced polyetheretherketone (CFRPEEK) possesses excellent mechanical properties similar to those of human cortical bone and is a prime candidate to replace conventional metallic implants. The bioinertness and inferior osteogenic properties of CFRPEEK, however, limit its clinical application as orthopedic/dental implants. The present work aimed at developing a novel carbon fiber-reinforced polyetheretherketone-nanohydroxyapatite (PEEK/CF/n-HA) ternary biocomposite with micro/nano-topographical surface for the enhancement of the osteogenesis as a potential bioactive material for bone grafting and bone tissue-engineering applications. The combined modification of oxygen plasma and sand-blasting could improve the hydrophily and generate micro/nano-topographical structures on the surface of the CFRPEEK-based ternary biocomposite. The results clearly showcased that the micro-/nano-topographical PEEK/n-HA/CF ternary biocomposite demonstrated the outstanding ability to promote the proliferation and differentiation of MG-63 cells in vitro as well as to boost the osseointegration between implant and bone in vivo, thereby boding well application to bone tissue engineering. PMID:25579962

  3. Laser cutting of carbon fiber reinforced thermo-plastics (CFRTP) by single-mode fiber laser irradiation

    NASA Astrophysics Data System (ADS)

    Niino, Hiroyuki; Kawaguchi, Yoshizo; Sato, Tadatake; Narazaki, Aiko; Kurosaki, Ryozo; Muramatsu, Mayu; Harada, Yoshihisa; Anzai, Kenji; Aoyama, Mitsuaki; Matsushita, Masafumi; Furukawa, Koichi; Nishino, Michiteru; Fujisaki, Akira; Miyato, Taizo; Kayahara, Takashi

    2014-03-01

    We report on the laser cutting of carbon fiber reinforced thermo-plastics (CFRTP) with a cw IR fiber laser (single-mode fiber laser, average power: 350 W). CFRTP is a high strength composite material with a lightweight, and is increasingly being used various applications. A well-defined cutting of CFRTP which were free of debris and thermal-damages around the grooves, were performed by the laser irradiation with a fast beam galvanometer scanning on a multiple-scanpass method.

  4. Understanding the interdiffusion behavior and determining the long term stability of tungsten fiber reinforced niobium-base matrix composite systems

    NASA Technical Reports Server (NTRS)

    Tien, John K.

    1990-01-01

    The long term interdiffusional stability of tungsten fiber reinforced niobium alloy composites is addressed. The matrix alloy that is most promising for use as a high temperature structural material for reliable long-term space power generation is Nb1Zr. As an ancillary project to this program, efforts were made to assess the nature and kinetics of interphase reaction between selected beryllide intermetallics and nickel and iron aluminides.

  5. Continuous fiber-reinforced titanium aluminide composites

    NASA Technical Reports Server (NTRS)

    Mackay, R. A.; Brindley, P. K.; Froes, F. H.

    1991-01-01

    An account is given of the fabrication techniques, microstructural characteristics, and mechanical behavior of a lightweight, high service temperature SiC-reinforced alpha-2 Ti-14Al-21Nb intermetallic-matrix composite. Fabrication techniques under investigation to improve the low-temperature ductility and environmental resistance of this material system, while reducing manufacturing costs to competitive levels, encompass powder-cloth processing, foil-fiber-foil processing, and thermal-spray processing. Attention is given to composite microstructure problems associated with fiber distribution and fiber-matrix interfaces, as well as with mismatches of thermal-expansion coefficient; major improvements are noted to be required in tensile properties, thermal cycling effects, mechanical damage, creep, and environmental effects.

  6. Study on the laser irradiation effects on carbon fiber reinforced resin composite subjected to tangential gas flow loading

    NASA Astrophysics Data System (ADS)

    Chen, Minsun; Jiang, Houman; Jiao, Luguang; Li, Junshen; Liu, Zejin

    2013-05-01

    The irradiation effects of 976nm continuous-wave laser on carbon fiber reinforced E-51 resin composite is studied experimentally, with a 0.4Ma tangential airflow or 0.4Ma tangential nitrogen gas flow on the target surface. In order to simulate the thermal response of fiber reinforced resin composite materials subjected to combined laser and tangential gas flow loading, a three-dimensional thermal response model of resin composite materials is developed. In the model, the thermal decomposition of resin is described by a multi-step model. The motion of the decomposition gas is assumed to be one-dimensional, for the case that the laser spot is significantly larger than the thickness of the sample. According the above assumption, the flow of the decomposition gas is considered in the three-dimensional model without introducing any mechanical quantities. The influences of the tangential gas flow, the outflow of the thermal decomposition gas and the ablation-including phase change ablation or oxidative ablation-of the surface material on the laser irradiation effects are included in the surface boundary conditions. The three-dimensional thermal response model is calculated numerically by use of the modified smooth particle hydrodynamics (MSPH) method which is coded with FORTRAN. The model is tested by experimentally measuring the temperature profiles during carbon fiber reinforced E-51 resin composite subjected to combined laser and tangential gas flow. The predicted temperature profiles are in good agreement with experimental temperatures obtained using thermocouples.

  7. Low density bismaleimide-carbon microballoon composites

    NASA Technical Reports Server (NTRS)

    Kourtides, D. A.; Parker, J. A. (Inventor)

    1979-01-01

    A process is described for the preparation of composite laminate.structures of glass cloth preimpregnated with polybismaleimide resin and adhered to a polybismaleimide glass or aromatic polyamide paper honeycomb cell structure that is filled or partially filled with a syntactic foam consisting of a mixture of bismaleimide resin and carbon microballoons. The carbon microballoons are prepared by pyrolyzing phenolic microballoons and subsequently bonded using a 2% bismaleimide solution. The laminate structures are cured for two hours at 477 deg K and are adhered to the honeycomb bismaleimide adhesive using a pressure of 700 KN/sq m pressure at 450 deg K. The laminate composite is then post-cured for two hours at 527 deg K to produce a composite laminate having a density in the range from about 95 kilograms per cubic meter to 130 kilograms per cubic meter.

  8. Fiber reinforced thermoplastic resin matrix composites

    NASA Technical Reports Server (NTRS)

    Jones, Robert J. (Inventor); Chang, Glenn E. C. (Inventor)

    1989-01-01

    Polyimide polymer composites having a combination of enhanced thermal and mechanical properties even when subjected to service temperatures as high as 700.degree. F. are described. They comprise (a) from 10 to 50 parts by weight of a thermoplastic polyimide resin prepared from 2,2-bis[4-(4-aminophenoxy)phenyl]hexafluoropropane and (b) from 90 to 50 parts by weight of continuous reinforcing fibers, the total of (a) and (b) being 100 parts by weight. Composites based on polyimide resin formed from 2,2-bis[4-(4-aminophenoxy)phenyl]hexafluoropropane and pyromellitic dianhydride and continuous carbon fibers retained at least about 50% of their room temperature shear strength after exposure to 700.degree. F. for a period of 16 hours in flowing air. Preferably, the thermoplastic polyimide resin is formed in situ in the composite material by thermal imidization of a corresponding amide-acid polymer prepared from 2,2-bis[4-(4-aminophenoxy)phenyl]hexafluoropropane. It is also preferred to initially size the continuous reinforcing fibers with up to about one percent by weight of an amide-acid polymer prepared from 2,2-bis[4-(4-aminophenoxy)phenyl]hexafluoropropane. In this way imidization at a suitable elevated temperature results in the in-situ formation of a substantially homogeneous thermoplastic matrix of the polyimide resin tightly and intimately bonded to the continuous fibers. The resultant composites tend to have optimum thermo-mechanical properties.

  9. Nano-Aramid Fiber Reinforced Polyurethane Foam

    NASA Technical Reports Server (NTRS)

    Semmes, Edmund B.; Frances, Arnold

    2008-01-01

    Closed cell polyurethane and, particularly, polyisocyanurate foams are a large family of flexible and rigid products the result of a reactive two part process wherein a urethane based polyol is combined with a foaming or "blowing" agent to create a cellular solid at room temperature. The ratio of reactive components, the constituency of the base materials, temperature, humidity, molding, pouring, spraying and many other processing techniques vary greatly. However, there is no known process for incorporating reinforcing fibers small enough to be integrally dispersed within the cell walls resulting in superior final products. The key differentiating aspect from the current state of art resides in the many processing technologies to be fully developed from the novel concept of milled nano pulp aramid fibers and their enabling entanglement capability fully enclosed within the cell walls of these closed cell urethane foams. The authors present the results of research and development of reinforced foam processing, equipment development, strength characteristics and the evolution of its many applications.

  10. Strength and Durability of Fly Ash-Based Fiber-Reinforced Geopolymer Concrete in a Simulated Marine Environment

    NASA Astrophysics Data System (ADS)

    Martinez Rivera, Francisco Javier

    This research is aimed at investigating the corrosion durability of polyolefin fiberreinforced fly ash-based geopolymer structural concrete (hereafter referred to as GPC, in contradistinction to unreinforced geopolymer concrete referred to as simply geopolymer concrete), where cement is completely replaced by fly ash, that is activated by alkalis, sodium hydroxide and sodium silicate. The durability in a marine environment is tested through an electrochemical method for accelerated corrosion. The GPC achieved compressive strengths in excess of 6,000 psi. Fiber reinforced beams contained polyolefin fibers in the amounts of 0.1%, 0.3%, and 0.5% by volume. After being subjected to corrosion damage, the GPC beams were analyzed through a method of crack scoring, steel mass loss, and residual flexural strength testing. Fiber reinforced GPC beams showed greater resistance to corrosion damage with higher residual flexural strength. This makes GPC an attractive material for use in submerged marine structures.

  11. Anelastic relaxation in Al-4 wt pct Cu-Al{sub 2}O{sub 3} fiber-reinforced composites

    SciTech Connect

    Sgobba, S.; Parrini, L.; Kuenzi, H.U.; Ilschner, B.

    1995-10-01

    In many industrial applications, like high precision weighing and positioning, the elastic and dimensional stability of materials is required at a nanometric scale. High-resolution laser interferometry and mechanical spectroscopy have been employed to measure low-temperature anelastic creep of the short-fiber-reinforced composite Al-4 wt pct Cu-Al{sub 2}O{sub 3}. The typical strain resolution of the laser interferometer is 10{sup {minus}10}. Fiber reinforcement has been found to increase the dislocation density n the metal matrix; in parallel, damping and anelastic creep are enhanced. This behavior has been explained on the basis of the structure of interparticle dislocations and {theta}{prime} relaxation.

  12. Constitutive modeling of fiber-reinforced cement composites

    NASA Astrophysics Data System (ADS)

    Boulfiza, Mohamed

    The role of fibers in the enhancement of the inherently low tensile stress and strain capacities of fiber reinforced cementitious composites (FRC) has been addressed through both the phenomenological, using concepts of continuum damage mechanics, and micro-mechanical approaches leading to the development of a closing pressure that could be used in a cohesive crack analysis. The observed enhancements in the matrix behavior is assumed to be related to the ability of the material to transfer stress across cracks. In the micromechanics approach, this is modeled by the introduction of a nonlinear closing pressure at the crack lips. Due to the different nature of cracking in the pre-peak and post peak regimes, two different micro-mechanical models of the cohesive pressure have been proposed, one for the strain hardening stage and another for the strain softening regime. This cohesive pressure is subsequently incorporated into a finite element code so that a nonlinear fracture analysis can be carried out. On top of the fact that a direct fracture analysis has been performed to predict the response of some FRC structural elements, a numerical procedure for the homogenization of FRC materials has been proposed. In this latter approach, a link is established between the cracking taking place at the meso-scale and its mechanical characteristics as represented by the Young's modulus. A parametric study has been carried out to investigate the effect of crack patterning and fiber volume fractions on the overall Young's modulus and the thermodynamic force associated with the tensorial damage variable. After showing the usefulness and power of phenomenological continuum damage mechanics (PCDM) in the prediction of ERC materials' response to a stimuli (loading), a combined PCDM-NLFMsp1 approach is proposed to model (predict, forecast) the complete response of the composite up to failure. Based on experimental observations, this approach assumes that damage mechanics which predicts

  13. Bisphenyl-Polymer/Carbon-Fiber-Reinforced Composite Compared to Titanium Alloy Bone Implant

    PubMed Central

    Petersen, Richard C.

    2014-01-01

    Aerospace/aeronautical thermoset bisphenyl-polymer/carbon-fiber-reinforced composites are considered as new advanced materials to replace metal bone implants. In addition to well-recognized nonpolar chemistry with related bisphenol-polymer estrogenic factors, carbon-fiber-reinforced composites can offer densities and electrical conductivity/resistivity properties close to bone with strengths much higher than metals on a per-weight basis. In vivo bone-marrow tests with Sprague-Dawley rats revealed far-reaching significant osseoconductivity increases from bisphenyl-polymer/carbon-fiber composites when compared to state-of-the-art titanium-6-4 alloy controls. Midtibial percent bone area measured from the implant surface increased when comparing the titanium alloy to the polymer composite from 10.5% to 41.6% at 0.8 mm, P < 10−4, and 19.3% to 77.7% at 0.1 mm, P < 10−8. Carbon-fiber fragments planned to occur in the test designs, instead of producing an inflammation, stimulated bone formation and increased bone integration to the implant. In addition, low-thermal polymer processing allows incorporation of minerals and pharmaceuticals for future major tissue-engineering potential. PMID:25553057

  14. Smart damping of laminated fuzzy fiber reinforced composite shells using 1-3 piezoelectric composites

    NASA Astrophysics Data System (ADS)

    Kundalwal, S. I.; Kumar, R. Suresh; Ray, M. C.

    2013-10-01

    This paper deals with the investigation of active constrained layer damping (ACLD) of smart laminated continuous fuzzy fiber reinforced composite (FFRC) shells. The distinct constructional feature of a novel FFRC is that the uniformly spaced short carbon nanotubes (CNTs) are radially grown on the circumferential surfaces of the continuous carbon fiber reinforcements. The constraining layer of the ACLD treatment is considered to be made of vertically/obliquely reinforced 1-3 piezoelectric composite materials. A finite element (FE) model is developed for the laminated FFRC shells integrated with the two patches of the ACLD treatment to investigate the damping characteristics of the laminated FFRC shells. The effect of variation of the orientation angle of the piezoelectric fibers on the damping characteristics of the laminated FFRC shells has been studied when the piezoelectric fibers are coplanar with either of the two mutually orthogonal vertical planes of the piezoelectric composite layer. It is revealed that radial growth of CNTs on the circumferential surfaces of the carbon fibers enhances the attenuation of the amplitude of vibrations and the natural frequencies of the laminated FFRC shells over those of laminated base composite shells without CNTs.

  15. Analysis of pultrusion processing for long fiber reinforced thermoplastic composite system

    NASA Technical Reports Server (NTRS)

    Tso, W.; Hou, T. H.; Tiwari, S. N.

    1993-01-01

    Pultrusion is one of the composite processing technology, commonly recognized as a simple and cost-effective means for the manufacturing of fiber-reinforced, resin matrix composite parts with different regular geometries. Previously, because the majority of the pultruded composite parts were made of thermosetting resin matrix, emphasis of the analysis on the process has been on the conservation of energy from various sources, such as heat conduction and the curing kinetics of the resin system. Analysis on the flow aspect of the process was almost absent in the literature for thermosetting process. With the increasing uses of thermoplastic materials, it is desirable to obtain the detailed velocity and pressure profiles inside the pultrusion die. Using a modified Darcy's law for flow through porous media, closed form analytical solutions for the velocity and pressure distributions inside the pultrusion die are obtained for the first time. This enables us to estimate the magnitude of viscous dissipation and it's effects on the pultruded parts. Pulling forces refined in the pultrusion processing are also analyzed. The analytical model derived in this study can be used to advance our knowledge and control of the pultrusion process for fiber reinforced thermoplastic composite parts.

  16. Low Cost Fabrication of Silicon Carbide Based Ceramics and Fiber Reinforced Composites

    NASA Technical Reports Server (NTRS)

    Singh, M.; Levine, S. R.

    1995-01-01

    A low cost processing technique called reaction forming for the fabrication of near-net and complex shaped components of silicon carbide based ceramics and composites is presented. This process consists of the production of a microporous carbon preform and subsequent infiltration with liquid silicon or silicon-refractory metal alloys. The microporous preforms are made by the pyrolysis of a polymerized resin mixture with very good control of pore volume and pore size thereby yielding materials with tailorable microstructure and composition. Mechanical properties (elastic modulus, flexural strength, and fracture toughness) of reaction-formed silicon carbide ceramics are presented. This processing approach is suitable for various kinds of reinforcements such as whiskers, particulates, fibers (tows, weaves, and filaments), and 3-D architectures. This approach has also been used to fabricate continuous silicon carbide fiber reinforced ceramic composites (CFCC's) with silicon carbide based matrices. Strong and tough composites with tailorable matrix microstructure and composition have been obtained. Microstructure and thermomechanical properties of a silicon carbide (SCS-6) fiber reinforced reaction-formed silicon carbide matrix composites are discussed.

  17. A micromechanical approach to elastic and viscoelastic properties of fiber reinforced concrete

    SciTech Connect

    Pasa Dutra, V.F.; Maghous, S. Campos Filho, A.; Pacheco, A.R.

    2010-03-15

    Some aspects of the constitutive behavior of fiber reinforced concrete (FRC) are investigated within a micromechanical framework. Special emphasis is put on the prediction of creep of such materials. The linear elastic behavior is first examined by implementation of a Mori-Tanaka homogenization scheme. The micromechanical predictions for the overall stiffness prove to be very close to finite element solutions obtained from the numerical analysis of a representative elementary volume of FRC modeled as a randomly heterogeneous medium. The validation of the micromechanical concepts based on comparison with a set of experiments, shows remarkable predictive capabilities of the micromechanical representation. The second part of the paper is devoted to non-ageing viscoelasticity of FRC. Adopting a Zener model for the behavior of the concrete matrix and making use of the correspondence principle, the homogenized relaxation moduli are derived analytically. The validity of the model is established by mean of comparison with available experiment measurements of creep strain of steel fiber reinforced concrete under compressive load. Finally, the model predictions are compared to those derived from analytical models formulated within a one-dimensional setting.

  18. Processing and properties of multiscale cellular thermoplastic fiber reinforced composite (CellFRC)

    NASA Astrophysics Data System (ADS)

    Sorrentino, L.; Cafiero, L.; D'Auria, M.; Iannace, S.

    2015-12-01

    High performance fiber reinforced polymer composites are made by embedding high strength/modulus fibers in a polymeric matrix. They are a class of materials that owe its success to the impressive specific mechanical properties with respect to metals. In many weight-sensitive applications, where high mechanical properties and low mass are required, properties per unit of mass are more important than absolute properties and further weight reduction is desirable. A route to reach this goal could be the controlled induction of porosity into the polymeric matrix, while still ensuring load transfer to the reinforcing fibers and fiber protection from the environment. Cellular lightweight fiber reinforced composites (CellFRC) were prepared embedding gas bubbles of controlled size within a high performance thermoplastic matrix reinforced with continuous fibers. Pores were induced after the composite was first saturated with CO2 and then foamed by using an in situ foaming/shaping technology based on compression moulding with adjustable mould cavities. The presence of micro- or submicro-sized cells in the new CellFRC reduced the apparent density of the structure and led to significant improvements of its impact properties. Both structural and functional performances were further improved through the use of a platelet-like nanofiller (Expanded Graphite) dispersed into the matrix.

  19. Reconstruction of devital teeth using direct fiber-reinforced composite resins: a case report.

    PubMed

    Deliperi, Simone; Bardwell, David N; Coiana, Carlo

    2005-01-01

    Nonrestored devitalized teeth are structurally compromised and represent one of the greatest challenges for the clinician. Restoration of endodontically treated teeth has been associated with the use of posts. Various post materials and designs have been introduced over the years; however, motivated by the desire to conserve the remaining sound tooth structure and thanks to properties of modern adhesive systems, clinicians have re-evaluated the dogma of traditional restorative dentistry and seek alternative methods to build up devitalized teeth. The use of direct Ultra High Molecular Weight Polyethylene (UHMWPE) fiber-reinforced post systems is becoming popular among clinicians because enlargement of the root canal space is not required and the risk of root perforation eliminated. This article presents an experimental clinical technique to reconstruct severely damaged endodontically treated posterior teeth using direct fiber reinforced post systems. Particular attention is paid to the incremental and curing techniques adopted to build up the restoration. The problems that clinicians can encounter in bonding to teeth that have undergone endodontic treatment are also analyzed. Questions that have yet to be answered by scientific research are presented. PMID:16052766

  20. Low cost fabrication of silicon carbide based ceramics and fiber reinforced composites

    SciTech Connect

    Singh, M.; Levine, S.R.

    1995-07-01

    A low cost processing technique called reaction forming for the fabrication of near-net and complex shaped components of silicon carbide based ceramics and composites is presented. This process consists of the production of a microporous carbon preform and subsequent infiltration with liquid silicon or silicon-refractory metal alloys. The microporous preforms are made by the pyrolysis of a polymerized resin mixture with very good control of pore volume and pore size thereby yielding materials with tailorable microstructure and composition. Mechanical properties (elastic modulus, flexural strength, and fracture toughness) of reaction-formed silicon carbide ceramics are presented. This processing approach is suitable for various kinds of reinforcements such as whiskers, particulates, fibers (tows, weaves, and filaments), and 3-D architectures. This approach has also been used to fabricate continuous silicon carbide fiber reinforced ceramic composites (CFCC`s) with silicon carbide based matrices. Strong and tough composites with tailorable matrix microstructure and composition have been obtained. Microstructure and thermomechanical properties of a silicon carbide (SCS-6) fiber reinforced reaction-formed silicon carbide matrix composites are discussed.

  1. Design of Fiber Reinforced Foam Sandwich Panels for Large Ares V Structural Applications

    NASA Technical Reports Server (NTRS)

    Bednarcyk, Brett A.; Arnold, Steven M.; Hopkins, Dale A.

    2010-01-01

    The preliminary design of three major structural components within NASA's Ares V heavy lift vehicle using a novel fiber reinforced foam composite sandwich panel concept is presented. The Ares V payload shroud, interstage, and core intertank are designed for minimum mass using this panel concept, which consists of integral composite webs separated by structural foam between two composite facesheets. The HyperSizer structural sizing software, in conjunction with NASTRAN finite element analyses, is used. However, since HyperSizer does not currently include a panel concept for fiber reinforced foam, the sizing was performed using two separate approaches. In the first, the panel core is treated as an effective (homogenized) material, whose properties are provided by the vendor. In the second approach, the panel is treated as a blade stiffened sandwich panel, with the mass of the foam added after completion of the panel sizing. Details of the sizing for each of the three Ares V components are given, and it is demonstrated that the two panel sizing approaches are in reasonable agreement for thinner panel designs, but as the panel thickness increases, the blade stiffened sandwich panel approach yields heavier panel designs. This is due to the effects of local buckling, which are not considered in the effective core property approach.

  2. Characterizing the self-sensing performance of carbon nanotube-enhanced fiber-reinforced polymers

    NASA Astrophysics Data System (ADS)

    Loyola, Bryan R.; La Saponara, Valeria; Loh, Kenneth J.

    2010-04-01

    The increased usage of fiber-reinforced polymers (FRP) in recent decades has created a need to monitor the unique response of these materials to impact and fatigue damage. As most traditional nondestructive evaluation methods are illsuited to detecting damage in FRPs, new methods must be created without compromising the high strength-to-weight aspects of FRPs. This paper describes the characterization of carbon nanotube-polyelectrolyte thin films applied to glass fiber substrates as a means for in situ strain sensing in glass fiber-reinforced polymers (GFRP). The layer-by-layer deposition process employed is capable of depositing individual and small bundles of carbon nanotubes within a polyelectrolyte matrix and directly onto glass fiber matrices. Upon film fabrication, the nanocomposite-coated GFRP specimens are mounted in a load frame for characterizing their electromechanical performance. This preliminary results obtained from this study has shown that these thin films exhibit bilinear piezoresistivity. Time- and frequency-domain techniques are utilized to characterize the nanocomposite strain sensing response. An equivalent circuit is also derived from electrical impedance spectroscopic analysis of thin film specimens.

  3. Arrangement for connecting a fiber-reinforced plastic pipe to a stainless steel flange

    DOEpatents

    Allais, Arnaud; Hoffmann, Ernst

    2008-02-05

    Arrangement for connecting a fiber-reinforced plastic pipe (18) to a stainless steel flange (12, 16), in which the end of the fiber-reinforced plastic pipe (18) is accommodated in a ring-shaped groove (12a, 16a) in the flange (12, 16), the groove conforming to the dimensions of the fiber-reinforced plastic pipe (18), where the gap remaining between the end of the fiber-reinforced plastic pipe (18) and the ring-shaped groove (12a, 16a) is filled with a sealant (19).

  4. Fiber-Reinforced-Foam (FRF) Core Composite Sandwich Panel Concept for Advanced Composites Technologi

    NASA Technical Reports Server (NTRS)

    2010-01-01

    Fiber-Reinforced-Foam (FRF) Core Composite Sandwich Panel Concept for Advanced Composites Technologies Project - Preliminary Manufacturing Demonstration Articles for Ares V Payload Shroud Barrel Acreage Structure

  5. Graphite fiber reinforced structure for supporting machine tools

    DOEpatents

    Knight, Jr., Charles E.; Kovach, Louis; Hurst, John S.

    1978-01-01

    Machine tools utilized in precision machine operations require tool support structures which exhibit minimal deflection, thermal expansion and vibration characteristics. The tool support structure of the present invention is a graphite fiber reinforced composite in which layers of the graphite fibers or yarn are disposed in a 0/90.degree. pattern and bonded together with an epoxy resin. The finished composite possesses a low coefficient of thermal expansion and a substantially greater elastic modulus, stiffness-to-weight ratio, and damping factor than a conventional steel tool support utilized in similar machining operations.

  6. Microbiologically influenced degradation of fiber-reinforced polymeric composites

    SciTech Connect

    Wagner, P.A.; Ray, R.I.; Little, B.J. ); Tucker, W.C. )

    1994-04-01

    Two fiber-reinforced polymer composites were examined for susceptibility to microbiologically influenced degradation. Composites, resins, and fibers were exposed to sulfur/iron-oxidizing, calcareous-depositing, ammonium-producing, hydrogen-producing, and sulfate-reducing bacteria (SRB) in batch culture. Surfaces were uniformly colonized by all physiological types of bacteria. Epoxy and vinyl ester neat resins, carbon fibers, and epoxy composites were not adversely affected by microbiological species. SRB degraded the organic surfactant on glass fibers and preferentially colonized fiber-vinyl ester interfaces. Hydrogen-producing bacteria appeared to disrupt bonding between fibers and vinyl ester resin and to penetrate the resin at the interface.

  7. Microbiologically influenced degradation of fiber reinforced polymeric composites

    SciTech Connect

    Wagner, P.A.; Ray, R.I.; Little, B.J.; Tucker, W.C.

    1994-12-31

    Two fiber reinforced polymer composites were examined for susceptibility to microbiologically influenced degradation. Composites, resins, and fibers were exposed to sulfur/iron-oxidizing, calcareous-depositing, ammonium-producing, hydrogen-producing and sulfate-reducing bacteria (SRB) in batch culture. Surfaces were uniformly colonized by all physiological types of bacteria. Epoxy and vinyl ester neat resins, carbon fibers, and epoxy composites were not adversely affected by microbial species. SRB degraded the organic surfactant on glass fibers and preferentially colonized fiber-vinyl ester interfaces. Hydrogen-producing bacteria appeared to disrupt bonding between fibers and vinyl ester resin and to penetrate the resin at the interface.

  8. Fabrication Routes for Continuous Fiber-Reinforced Ceramic Composites (CFCC)

    NASA Technical Reports Server (NTRS)

    DiCarlo, James A.; Bansal, Narottam P.

    1998-01-01

    The primary approaches used for fabrication of continuous fiber-reinforced ceramic composite (CFCC) components have been reviewed. The CFCC fabrication issues related to fiber, interface, and matrix have been analyzed. The capabilities. advantages and limitations of the five matrix-infiltration routes have been compared and discussed. Today. the best fabrication route for the CFCC end-user is not clear and compromises need to be made depending on the details of the CFCC application. However, with time, this problem should be reduced as research continues to develop advanced CFCC constituents and fabrication routes.

  9. Fabrication Routes for Continuous Fiber-Reinforced Ceramic Composites (CFCC)

    NASA Technical Reports Server (NTRS)

    DiCarlo, James A.; Bansal, Narottam P.

    1998-01-01

    The primary approaches used for fabrication of continuous fiber-reinforced ceramic composite (CFCC) components have been reviewed. The CFCC fabrication issues related to fiber, interface, and matrix have been analyzed. The capabilities, advantages and limitations of the five matrix-infiltration routes have been compared and discussed. Today, the best fabrication route for the CFCC end-user is not clear and compromises need to be made depending on the details of the CFCC application. However, with time, this problem should be reduced as research continues to develop advanced CFCC constituents and fabrication routes.

  10. Postcrack creep of polymeric fiber-reinforced concrete in flexure

    SciTech Connect

    Kurtz, S.; Balaguru, P.

    2000-02-01

    Results of an experimental investigation of the creep-time behavior of polypropylene and nylon fiber-reinforced concrete (FRC) are presented. Gravity loads were applied in flexure to precracked low volume fraction (0.1%) polypropylene and nylon FRC beams. Beams were tested at a range of stress levels to produce three outcomes: load sustained indefinitely (low stress), creep failure (intermediate stress), and rapid failure (high stress). Emphasis was placed on determining the maximum flexural stress that is sustainable indefinitely. The results indicate that polypropylene FRC has higher initial strength but nylon FRC can sustain a higher stress level. For both groups the sustainable stress is much lower than the postcrack strength.

  11. Physicochemical characterization of three fiber-reinforced epoxide-based composites for dental applications.

    PubMed

    Bonon, Anderson J; Weck, Marcus; Bonfante, Estevam A; Coelho, Paulo G

    2016-12-01

    Fiber-reinforced composite (FRC) biomedical materials are in contact with living tissues arising biocompatibility questions regarding their chemical composition. The hazards of materials such as Bisphenol A (BPA), phthalate and other monomers and composites present in FRC have been rationalized due to its potential toxicity since its detection in food, blood, and saliva. This study characterized the physicochemical properties and degradation profiles of three different epoxide-based materials intended for restorative dental applications. Characterization was accomplished by several methods including FTIR, Raman, Brunauer-Emmett-Teller (BET) Analysis, X-ray fluorescence spectroscopy, and degradation experiments. Physicochemical characterization revealed that although materials presented similar chemical composition, variations between them were more largely accounted by the different phase distribution than chemical composition. PMID:27612785

  12. Mechanical characterization and structural analysis of recycled fiber-reinforced-polymer resin-transfer-molded beams

    NASA Astrophysics Data System (ADS)

    Tan, Eugene Wie Loon

    1999-09-01

    The present investigation was focussed on the mechanical characterization and structural analysis of resin-transfer-molded beams containing recycled fiber-reinforced polymers. The beams were structurally reinforced with continuous unidirectional glass fibers. The reinforcing filler materials consisted entirely of recycled fiber-reinforced polymer wastes (trim and overspray). The principal resin was a 100-percent dicyclo-pentadiene unsaturated polyester specially formulated with very low viscosity for resin transfer molding. Variations of the resin transfer molding technique were employed to produce specimens for material characterization. The basic materials that constituted the structural beams, continuous-glass-fiber-reinforced, recycled-trim-filled and recycled-overspray-filled unsaturated polyesters, were fully characterized in axial and transverse compression and tension, and inplane and interlaminar shear, to ascertain their strengths, ultimate strains, elastic moduli and Poisson's ratios. Experimentally determined mechanical properties of the recycled-trim-filled and recycled-overspray-filled materials from the present investigation were superior to those of unsaturated polyester polymer concretes and Portland cement concretes. Mechanical testing and finite element analyses of flexure (1 x 1 x 20 in) and beam (2 x 4 x 40 in) specimens were conducted. These structurally-reinforced specimens were tested and analyzed in four-point, third-point flexure to determine their ultimate loads, maximum fiber stresses and mid-span deflections. The experimentally determined load capacities of these specimens were compared to those of equivalent steel-reinforced Portland cement concrete beams computed using reinforced concrete theory. Mechanics of materials beam theory was utilized to predict the ultimate loads and mid-span deflections of the flexure and beam specimens. However, these predictions proved to be severely inadequate. Finite element (fracture propagation

  13. Matrix free fiber reinforced polymeric composites via high-temperature high-pressure sintering

    NASA Astrophysics Data System (ADS)

    Xu, Tao

    2004-11-01

    A novel manufacturing process called high-temperature high-pressure sintering was studied and explored. Solid fiber reinforced composites are produced by consolidating and compacting layers of polymeric fabrics near their melting temperature under high pressure. There is no need to use an additional matrix as a bonding material. Partial melting and recrystallization of the fibers effectively fuse the material together. The product is called a "matrix free" fiber reinforced composite and essentially a one-polymer composite in which the fiber and the matrix have the same chemical composition. Since the matrix is eliminated in the process, it is possible to achieve a high fiber volume fraction and light weight composite. Interfacial adhesion between fibers and matrix is very good due to the molecular continuity throughout the system and the material is thermally shapeable. Plain woven Spectra RTM cloth made of SpectraRTM fiber was used to comprehensively study the process. The intrinsic properties of the material demonstrate that matrix free SpectraRTM fiber reinforced composites have the potential to make ballistic shields such as body armor and helmets. The properties and structure of the original fiber and the cloth were carefully examined. Optimization of the processing conditions started with the probing of sintering temperatures by Differential Scanning Calorimetry. Coupled with the information from structural, morphological and mechanical investigations on the samples sintered at different processing conditions, the optimal processing windows were determined to ensure that the outstanding original properties of the fibers translate into high ballistic performance of the composites. Matrix free SpectraRTM composites exhibit excellent ballistic resistance in the V50 tests conducted by the US Army. In the research, process-structure-property relationship is established and correlations between various properties and structures are understood. Thorough knowledge is

  14. Effects of interphase regions on performance of carbon fiber reinforced thermoset composites

    SciTech Connect

    Lesko, J.J.; Case, S.W.; Reifsnider, K.L.

    1995-12-31

    The effects of systematically varied interphase materials on carbon fiber reinforced epoxy and vinyl ester matrix composites are under continuing investigation. Substantial differences in composite strength and fatigue durability have been observed between two composite material systems with epoxy matrices and contrasting interphases. The improvements were directly attributed to the application of a thermoplastic sizing miscible with the matrix resin, poly(vinylpyrrolidone), as opposed to a conventional epoxy sizing. In some cases, fiber dominated composite strength was improved by 50% and fatigue lives were increased by two orders of magnitude using the polyamide sizing. Distinct morphological differences resulted in the interphase regions using the different sizings, and thus, it was assumed that the local mechanical properties of the composites in this region were dissimilar. This work has now been extended to carbon fabric reinforced, vinyl ester/styrene matrix composites. Analogously, dramatically increased fatigue durability of these materials using poly(vinylpyrrolidone) sizings has also been observed.

  15. Processing and Characterization of Basalt Fiber Reinforced Ceramic Composites for High Temperature Applications Using Polymer Precursors

    NASA Technical Reports Server (NTRS)

    Cox, Sarah B.; Lui, Donovan; Gou, Jihua

    2014-01-01

    The development of high temperature structural composite materials has been very limited due to the high cost of the materials and the processing needed. Polymer Derived Ceramics (PDCs) begin as a polymer matrix, which allows a shape to be formed prior to the cure, and is then pyrolized in order to obtain a ceramic with the associated thermal and mechanical properties. The two PDCs used in this development are polysiloxane and polycarbosilane. Basalt fibers are used for the reinforcement in the composite system. The use of basalt in structural and high temperature applications has been under development for over 50 years, yet there has been little published research on the incorporation of basalt fibers as a reinforcement in composites. Continuous basalt fiber reinforced PDCs have been fabricated and tested for the applicability of this composite system as a high temperature structural composite material.

  16. PERFORMANCE EVALUATION OF AN INNOVATIVE FIBER REINFORCED GEOPOLYMER SPRAY-APPLIED MORTAR FOR LARGE DIAMETER WASTEWATER MAIN REHABILITATION IN HOUSTON, TX

    EPA Science Inventory

    This report describes the performance evaluation of a fiber reinforced geopolymer spray-applied mortar, which has potential as a structural alternative to traditional open cut techniques used in large-diameter sewer pipes. Geopolymer is a sustainable green material that incorpor...

  17. The assessment of metal fiber reinforced polymeric composites

    NASA Technical Reports Server (NTRS)

    Chung, Wenchiang R.

    1990-01-01

    Because of their low cost, excellent electrical conductivity, high specific strength (strength/density), and high specific modulus (modulus/density) short metal fiber reinforced composites have enjoyed a widespread use in many critical applications such as automotive industry, aircraft manufacturing, national defense, and space technology. However, little data has been found in the study of short metal fibrous composites. Optimum fiber concentration in a resin matrix and fiber aspect ratio (length-to-diameter ratio) are often not available to a user. Stress concentration at short fiber ends is the other concern when the composite is applied to a load-bearing application. Fracture in such composites where the damage will be initiated or accumulated is usually difficult to be determined. An experimental investigation is therefore carefully designed and undertaken to systematically evaluate the mechanical properties as well as electrical properties. Inconel 601 (nickel based) metal fiber with a diameter of eight microns is used to reinforce commercially available thermoset polyester resin. Mechanical testing such as tensile, impact, and flexure tests along with electrical conductivity measurements is conducted to study the feasibility of using such composites. The advantages and limitations of applying chopped metal fiber reinforced polymeric composites are also discussed.

  18. Fabrication of Fiber-Reinforced Celsian Matrix Composites

    NASA Technical Reports Server (NTRS)

    Bansal, Narottam P.; Setlock, John A.

    2000-01-01

    A method has been developed for the fabrication of small diameter, multifilament tow fiber reinforced ceramic matrix composites. Its application has been successfully demonstrated for the Hi-Nicalon/celsian system. Strong and tough celsian matrix composites, reinforced with BN/SiC-coated Hi-Nicalon fibers, have been fabricated by infiltrating the fiber tows with the matrix slurry, winding the tows on a drum, cutting and stacking of the prepreg tapes in the desired orientation, and hot pressing. The monoclinic celsian phase in the matrix was produced in situ, during hot pressing, from the 0.75BaO-0.25SrO-Al2O3-2SiO2 mixed precursor synthesized by solid state reaction from metal oxides. Hot pressing resulted in almost fully dense fiber-reinforced composites. The unidirectional composites having approx. 42 vol% of fibers exhibited graceful failure with extensive fiber pullout in three-point bend tests at room temperature. Values of yield stress and strain were 435 +/- 35 MPa and 0.27 +/- 0.01 percent, respectively, and ultimate strengths of 900 +/- 60 MPa were observed. The Young's modulus of the composites was measured to be 165 +/- 5 GPa.

  19. A synthetic fiber-reinforced stentless heart valve.

    PubMed

    Cacciola, G; Peters, G W; Baaijens, F P

    2000-06-01

    There is strong evidence that failure of bioprosthetic and synthetic valves occurs as a consequence of high tensile and bending stresses, acting on the leaflets during opening and closing. In stented prostheses, whether synthetic or biological, the absence of contraction of the aortic base causes the leaflets to be subjected to an unphysiological degree of flexure, which is also related to calcification. However, a stentless synthetic valve, which has a flexible aorta base, can be a good alternative for stented synthetic valves. Moreover, fiber-reinforcement is assumed to lead to a decrease of tears and perforation as a result of reduced stresses in the weaker parts of the leaflets in their closed configuration. The manufacturing method for a stentless, fiber-reinforced, synthetic valve is presented. Prototypes are tested in a pulse duplicator system. The results show that the mean systolic pressure difference is very low, while the high regurgitation (up to 26%) is probably caused by a too small coaptation area of the leaflets. PMID:10807985

  20. Mechanism of interface formation in a silicon carbide fiber-reinforced magnesuium aluminosilicate

    SciTech Connect

    Kumar, A.; Knowles, K.M.

    1995-12-01

    The formation of sliding interfacial layers is a major key to the success of fiber-reinforced glass-ceramics. This paper reports the mechanism of formation of fiber-matrix interfaces during oxidizing heat treatments in a SiC fiber-reinforced magnesium aluminosilicate.

  1. Segmenting delaminations in carbon fiber reinforced polymer composite CT using convolutional neural networks

    NASA Astrophysics Data System (ADS)

    Sammons, Daniel; Winfree, William P.; Burke, Eric; Ji, Shuiwang

    2016-02-01

    Nondestructive evaluation (NDE) utilizes a variety of techniques to inspect various materials for defects without causing changes to the material. X-ray computed tomography (CT) produces large volumes of three dimensional image data. Using the task of identifying delaminations in carbon fiber reinforced polymer (CFRP) composite CT, this work shows that it is possible to automate the analysis of these large volumes of CT data using a machine learning model known as a convolutional neural network (CNN). Further, tests on simulated data sets show that with a robust set of experimental data, it may be possible to go beyond just identification and instead accurately characterize the size and shape of the delaminations with CNNs.

  2. Performance of integrated active fiber composites in fiber reinforced epoxy laminates

    NASA Astrophysics Data System (ADS)

    Melnykowycz, M.; Kornmann, X.; Huber, C.; Barbezat, M.; Brunner, A. J.

    2006-02-01

    Active fiber composite (AFC) composed of lead zirconate titanate (PZT) fibers with interdigitated electrodes (IDEs) has been integrated into orthotropic glass fiber reinforced plastic (GFRP) laminates to characterize the performance of AFC as a smart material component in laminated materials. Monotonic cyclic tensile loading was performed on integrated specimens at different strain levels. The AFC output was monitored to determine the effect of applied strain level on the AFC performance. It was found that the AFC sensitivity degraded beyond strains of 0.20% and approached a minimum at 0.50% strain. The degradation in the AFC performance appears to be attributed to the dominating effect of PZT fiber fragmentation during testing, as opposed to depolarization. Acoustic emission (AE) monitoring was used to detect damage in laminates during testing and was correlated with crack evidence from microscopy observations during testing to characterize damage evolution in response to strain levels.

  3. First light with a carbon fiber reinforced polymer 0.4 meter telescope

    NASA Astrophysics Data System (ADS)

    Wilcox, Christopher C.; Santiago, Freddie; Jungwirth, Matthew E.; Martinez, Ty; Restaino, Sergio R.; Bagwell, Brett; Romeo, Robert

    2014-03-01

    For the passed several years, the Naval Research Laboratory (NRL) has been investigating the use of Carbon Fiber Reinforced Polymer (CFRP) material in the construction of a telescope assembly including the optical components. The NRL, Sandia National Laboratories (SNL), and Composite Mirror Applications, Inc. (CMA) have jointly assembled a prototype telescope and achieved "first light" images with a CFRP 0.4 m aperture telescope. CFRP offers several advantages over traditional materials such as creating structures that are lightweight and low coefficient of thermal expansion and conductivity. The telescope's primary and secondary mirrors are not made from glass, but CFRP, as well. The entire telescope weighs approximately 10 kg while a typical telescope of this size would weigh quite a bit more. We present the achievement of "first light" with this telescope demonstrating the imaging capabilities of this prototype and the optical surface quality of the mirrors with images taken during a day's quiescent periods.

  4. Ultrasonic inspection of carbon fiber reinforced plastic by means of sample-recognition methods

    NASA Technical Reports Server (NTRS)

    Bilgram, R.

    1985-01-01

    In the case of carbon fiber reinforced plastic (CFRP), it has not yet been possible to detect nonlocal defects and material degradation related to aging with the aid of nondestructive inspection method. An approach for overcoming difficulties regarding such an inspection involves an extension of the ultrasonic inspection procedure on the basis of a use of signal processing and sample recognition methods. The basic concept involved in this approach is related to the realization that the ultrasonic signal contains information regarding the medium which is not utilized in conventional ultrasonic inspection. However, the analytical study of the phyiscal processes involved is very complex. For this reason, an empirical approach is employed to make use of the information which has not been utilized before. This approach uses reference signals which can be obtained with material specimens of different quality. The implementation of these concepts for the supersonic inspection of CFRP laminates is discussed.

  5. Graphite Sheet Coating for Improved Thermal Oxidative Stability of Carbon Fiber Reinforced/PMR-15 Composites

    NASA Technical Reports Server (NTRS)

    Campbell, Sandi; Papadopoulos, Demetrios; Heimann, Paula; Inghram, Linda; McCorkle, Linda

    2005-01-01

    Expanded graphite was compressed into graphite sheets and used as a coating for carbon fiber reinforced PMR-15 composites. BET analysis of the graphite indicated an increase in graphite pore size on compression, however the material was proven to be an effective barrier to oxygen when prepegged with PMR-15 resin. Oxygen permeability of the PMR-15/graphite was an order of magnitude lower than the compressed graphite sheet. By providing a barrier to oxygen permeation, the rate of oxidative degradation of PMR-15 was decreased. As a result, the composite thermo-oxidative stability increased by up to 25%. The addition of a graphite sheet as a top ply on the composites yielded little change in the material's flexural strength or interlaminar shear strength.

  6. Design and realization a skiff racing boat hull made of natural fibers reinforced composite

    NASA Astrophysics Data System (ADS)

    Collotta, M.; Solazzi, L.; Pandini, S.; Tomasoni, G.; Alberti, M.; Donzella, G.

    2016-05-01

    This paper discusses the development of a racing boat with an hull made of a composite material reinforced by natural fibers. In particular, we report here the design and realization of the boat hull, the assessment of its mechanical performance by means of a computer assisted simulation, and the cost analysis to assess the economic sustainability of the new composite developed. The results have shown that the new composite has a performance comparable with conventional glass fiber reinforced composites employed for the realization of this type of boat, accordingly to the technology employed and the lamination sequence adopted. Moreover, the FEM analysis performed over the skiff of the designed and constructed boat has demonstrated a successful choice of the material for real application, as it was later confirmed by the good performance of the boat in water. Finally, the cost analysis highlighted the economic sustainability of the new composite, allowing a cost saving of over 28% with respect to carbon fiber composites.

  7. Corrosion of steel members strengthenened with carbon fiber reinforced polymer sheets

    NASA Astrophysics Data System (ADS)

    Bumadian, Ibrahim

    Due to many years of service at several cases of exposure at various environments there are many of steel bridges which are in need of rehabilitation. The infrastructure needs upgrading, repair or maintenance, and also strengthening, but by using an alternative as retrofits methods. The alternative retrofit method, which used fiber reinforced polymer (FRP) composite materials which their strength materials comes largely from the fiber such as carbon, glass, and aramid fiber. Of the most important materials used in the rehabilitation of infrastructure is a composite material newly developed in bonded externally carbon fiber and polymer (CFRP) sheets, which has achieved remarkable success in the rehabilitation and upgrading of structural members. This technique has many disadvantages one of them is galvanic corrosion. This study presents the effect of galvanic corrosion on the interfacial strength between carbon fiber reinforced polymer (CFRP) sheets and a steel substrate. A total of 35 double-lap joint specimens and 19 beams specimens are prepared and exposed to an aggressive service environment in conjunction with an electrical potential method accelerating corrosion damage. Six test categories are planned at a typical exposure interval of 12 hours, including five specimens per category for double-lap joint specimens. And six test categories are planned at a typical exposure interval of 12 hours, including three specimens per category for Beam section specimens. In addition one beam section specimen is control. The degree of corrosion is measured. Fourier transform infrared (FTIR) reflectance spectroscopy has been used to monitor and confirm the proposed corrosion mechanisms on the surface of CFRP. In this study we are using FTIR-spectroscopic measurement systems in the mid infrared (MIR) wavelength region (4000 - 400) cm-1 to monitor characteristic spectral features. Upon completion of corrosion processes, all specimens are monotonically loaded until failure

  8. On Complexities of Impact Simulation of Fiber Reinforced Polymer Composites: A Simplified Modeling Framework

    PubMed Central

    Alemi-Ardakani, M.; Milani, A. S.; Yannacopoulos, S.

    2014-01-01

    Impact modeling of fiber reinforced polymer composites is a complex and challenging task, in particular for practitioners with less experience in advanced coding and user-defined subroutines. Different numerical algorithms have been developed over the past decades for impact modeling of composites, yet a considerable gap often exists between predicted and experimental observations. In this paper, after a review of reported sources of complexities in impact modeling of fiber reinforced polymer composites, two simplified approaches are presented for fast simulation of out-of-plane impact response of these materials considering four main effects: (a) strain rate dependency of the mechanical properties, (b) difference between tensile and flexural bending responses, (c) delamination, and (d) the geometry of fixture (clamping conditions). In the first approach, it is shown that by applying correction factors to the quasistatic material properties, which are often readily available from material datasheets, the role of these four sources in modeling impact response of a given composite may be accounted for. As a result a rough estimation of the dynamic force response of the composite can be attained. To show the application of the approach, a twill woven polypropylene/glass reinforced thermoplastic composite laminate has been tested under 200 J impact energy and was modeled in Abaqus/Explicit via the built-in Hashin damage criteria. X-ray microtomography was used to investigate the presence of delamination inside the impacted sample. Finally, as a second and much simpler modeling approach it is shown that applying only a single correction factor over all material properties at once can still yield a reasonable prediction. Both advantages and limitations of the simplified modeling framework are addressed in the performed case study. PMID:25431787

  9. On complexities of impact simulation of fiber reinforced polymer composites: a simplified modeling framework.

    PubMed

    Alemi-Ardakani, M; Milani, A S; Yannacopoulos, S

    2014-01-01

    Impact modeling of fiber reinforced polymer composites is a complex and challenging task, in particular for practitioners with less experience in advanced coding and user-defined subroutines. Different numerical algorithms have been developed over the past decades for impact modeling of composites, yet a considerable gap often exists between predicted and experimental observations. In this paper, after a review of reported sources of complexities in impact modeling of fiber reinforced polymer composites, two simplified approaches are presented for fast simulation of out-of-plane impact response of these materials considering four main effects: (a) strain rate dependency of the mechanical properties, (b) difference between tensile and flexural bending responses, (c) delamination, and (d) the geometry of fixture (clamping conditions). In the first approach, it is shown that by applying correction factors to the quasistatic material properties, which are often readily available from material datasheets, the role of these four sources in modeling impact response of a given composite may be accounted for. As a result a rough estimation of the dynamic force response of the composite can be attained. To show the application of the approach, a twill woven polypropylene/glass reinforced thermoplastic composite laminate has been tested under 200 J impact energy and was modeled in Abaqus/Explicit via the built-in Hashin damage criteria. X-ray microtomography was used to investigate the presence of delamination inside the impacted sample. Finally, as a second and much simpler modeling approach it is shown that applying only a single correction factor over all material properties at once can still yield a reasonable prediction. Both advantages and limitations of the simplified modeling framework are addressed in the performed case study. PMID:25431787

  10. Comparison of mechanical properties of a new fiber reinforced composite and bulk filling composites

    PubMed Central

    Pradelle, Nelly; Villat, Cyril; Attik, Nina; Colon, Pierre; Grosgogeat, Brigitte

    2015-01-01

    Objectives The aim of this study was to evaluate the mechanical and physical properties of a newly developed fiber reinforced dental composite. Materials and Methods Fiber reinforced composite EverX Posterior (EXP, GC EUROPE), and other commercially available bulk fill composites, including Filtek Bulk Fill (FB, 3M ESPE), SonicFill (SF, Kerr Corp.), SureFil (SDR, Dentsply), Venus Bulk Fill (VB, HerausKultzer), Tetric evoceram bulk fill (TECB, Ivoclar Vivadent), and Xtra Base (XB, Voco) were characterized. Composite samples light-cured with a LED device were evaluated in terms of flexural strength, flexural modulus (ISO 4049, n = 6), fracture toughness (n = 6), and Vickers hardness (0, 2, and 4 mm in depth at 24 hr, n = 5). The EXP samples and the fracture surface were observed under a scanning electron microscopy. Data were statistically analyzed using one-way ANOVA and unpaired t-test. Results EXP, FB, and VB had significantly higher fracture toughness value compared to all the other bulk composite types. SF, EXP, and XB were not statistically different, and had significantly higher flexural strength values compared to other tested composite materials. EXP had the highest flexural modulus, VB had the lowest values. Vickers hardness values revealed SF, EXP, TECB, and XB were not statistically different, and had significantly higher values compared to other tested composite materials. SEM observations show well dispersed fibers working as a reinforcing phase. Conclusions The addition of fibers to methacrylate-based matrix results in composites with either comparable or superior mechanical properties compared to the other bulk fill materials tested. PMID:26587411

  11. Integration of long-gage fiber optic sensor into a fiber-reinforced composite sensing tape

    NASA Astrophysics Data System (ADS)

    Glisic, Branko; Inaudi, Daniele

    2003-07-01

    Thermoplastic and thermoset fiber-reinforced composite materials are well established in aerospace engineering, but also more and more used in the oil and gas industry as well as in civil engineering. In these applications they are mainly used to reinfoce, repair or straighten existing structures, but recently full-composite structures have also been built. Independently from the domain of the use, there is a need for these composite structures to be monitored. Since the composite materials are usually applied in the form of thin tapes or sheets, sensors have to be embedded within the structure, depending on structural layer that has to be monitored. Embedding the sensors may have as a consequence a significant decrease of the mechanical properties of the composite material due to the dimensions of the sensor. The solution presented in this paper is integration of a fiber optic sensor directly into the main composite component, i.e. into the composite tape. In this paper we present the development of a thermoplastic fiber-reinforced composite tape with integrated long-gage fiber-optic sensors. The fiber-optic sensors are selected due to small transversal dimension and good compatibility with the plastic materials. The tape with integrated optical fiber can be used for tape winding of a structural element, embedded between different layers, but also as a separate sensor - a sensing tape. The optical and mechanical properties of the tapes with sensor are tested. The sensing tape is then installed onto the rail along with standard long-gage fiber optic sensor, additional tests are performed and performance of both sensor compared. The integration of optical fiber into the composite tape, the results of the tests as well as the performances of the tape with integrated optical fiber are presented in this paper.

  12. Friction and Wear of Monolithic and Fiber Reinforced Silicon-Ceramics Sliding Against IN-718 Alloy at 25 to 800 C in Atmospheric Air at Ambient Pressure

    NASA Technical Reports Server (NTRS)

    Deadmore, Daniel L.; Sliney, Harold E.

    1988-01-01

    The friction and wear of monolithic and fiber reinforced Si-ceramics sliding against the nickel base alloy IN-718 at 25 to 800 C was measured. The monolithic materials tested were silicon carbide (SiC), fused silica (SiO2), syalon, silicon nitride (Si3N4) with W and Mg additives, and Si3N4 with Y2O3 additive. At 25 C fused silica had the lowest friction while Si3N4 (W,Mg type) had the lowest wear. At 800 C syalon had the lowest friction while Si3N4 (W,Mg type) and syalon had the lowest wear. The SiC/IN-718 couple had the lowest total wear at 25 C. At 800 C the fused silica/IN-718 couple exhibited the least total wear. SiC fiber reinforced reaction bonded silicon nitride (RBSN) composite material with a porosity of 32 percent and a fiber content of 23 vol percent had a lower coefficient of friction and wear when sliding parallel to the fiber direction than in the perpendicular at 25 C. The coefficient of friction for the carbon fiber reinforced borosilicate composite was 0.18 at 25 C. This is the lowest of all the couples tested. Wear of this material was about two decades smaller than that of the monolithic fused silica. This illustrates the large improvement in tribological properties which can be achieved in ceramic materials by fiber reinforcement. At higher temperatures the oxidation products formed on the IN-718 alloy are transferred to the ceramic by sliding action and forms a thin, solid lubricant layer which decreases friction and wear for both the monolithic and fiber reinforced composites.

  13. The effect of glass and polyethylene fiber reinforcement on flexural strength of provisional restorative resins: an in vitro study.

    PubMed

    Natarajan, Parthasarathy; Thulasingam, C

    2013-12-01

    The aim is to evaluate and compare the flexural strength of different provisional restorative materials reinforced with glass and polyethylene fibers. A total of 90 samples were prepared and divided into three groups based on the type of fiber reinforcement, unidirectional S-glass (Splint-It) and ultra-molecular weight polyethylene (Ribbond). Unreinforced samples served as control group. Again each group was subdivided into three subgroups based on type of provisional restorative resins, heats cure polymethyl methacrylate, self-cure poly methyl methacrylate and self-cure bis-acryl composite. Samples were loaded in a universal testing machine until fracture occurs. The mean flexural strengths (MPa) were subjected to the one-way ANOVA, followed by the Tukey-HSD test at a significance level of 0.001. The result shows all the fiber reinforced samples possessed greater strength than the control samples. In control samples, the heat cure poly methyl methacrylate resin (72.74 ± 2.28 MPa) had the greatest flexural strength, followed by self-cure bis-acryl composite (67.05 ± 2.35 MPa) and self-cure poly methyl methacrylate resin (52.88 ± 1.90 MPa). In both heat and self-cure poly methyl methacrylate resin, the polyethylene fiber reinforcement (96.00 ± 2.63 MPa, 86.17 ± 1.92 MPa) provides the greatest strength than glass fiber reinforcement (92.68 ± 1.58 MPa, 76.40 ± 2.11 MPa). In self-cure bis-acryl composite, the glass fiber (105.95 ± 3.07 MPa) shows better reinforcement than polyethylene fiber (99.41 ± 1.74 MPa).The fibers reinforcement increases the flexural strength of provisional restorative resins. PMID:24431771

  14. Suitability of carbon fiber-reinforced polyetheretherketone cages for use as anterior struts following corpectomy.

    PubMed

    Heary, Robert F; Parvathreddy, Naresh K; Qayumi, Zainab S; Ali, Naiim S; Agarwal, Nitin

    2016-08-01

    OBJECTIVE Fibular allograft remains a widely used strut for corpectomy surgeries. The amount of graft material that can be packed into an allograft strut has not been quantified. Cages are an alternative to fibular allograft for fusion surgeries. The authors of this study assessed the suitability of carbon fiber-reinforced polyetheretherketone (CFRP) cages for anterior corpectomy surgeries. They further explored the parameters known to affect fusion rates in clinical practice. METHODS Six fibular allografts were tested at standard lengths. Three sets of carbon fiber cages (Bengal, DePuy Spine), each with a different footprint size but the same lengths, were tested. The allografts and cages were wrapped in adhesive, fluid-tight transparent barriers and filled with oil. The volume and weight of the oil instilled as well as the implant footprints were measured. The fibular allografts and cages were tested at 20-, 40-, and 50-mm lengths. Two investigators independently performed all measurements 5 times. Five CFRP cubes (1 × 1 × 1 cm) were tested under pure compression, and load versus displacement curves were plotted to determine the modulus of elasticity. RESULTS Significantly more oil fit in the CFRP cages than in the fibular allografts (p < 0.0001). The weight and volume of oil was 4-6 times greater in the cages. Interobserver (r = 0.991) and intraobserver (r = 0.993) reliability was excellent. The modulus of elasticity for CFRP was 16.44 ± 2.07 GPa. CONCLUSIONS Carbon fiber-reinforced polyetheretherketone cages can accommodate much more graft material than can fibular allografts. In clinical practice, the ability to deliver greater amounts of graft material following a corpectomy may improve fusion rates. PMID:27058498

  15. Process for the preparation of fiber-reinforced ceramic composites by chemical vapor deposition

    DOEpatents

    Lackey, Jr., Walter J.; Caputo, Anthony J.

    1986-01-01

    A chemical vapor deposition (CVD) process for preparing fiber-reinforced ceramic composites. A specially designed apparatus provides a steep thermal gradient across the thickness of a fibrous preform. A flow of gaseous ceramic matrix material is directed into the fibrous preform at the cold surface. The deposition of the matrix occurs progressively from the hot surface of the fibrous preform toward the cold surface. Such deposition prevents the surface of the fibrous preform from becoming plugged. As a result thereof, the flow of reactant matrix gases into the uninfiltrated (undeposited) portion of the fibrous preform occurs throughout the deposition process. The progressive and continuous deposition of ceramic matrix within the fibrous preform provides for a significant reduction in process time over known chemical vapor deposition processes.

  16. Oxidation kinetics of coated silicon carbide fiber-reinforced silicon carbide (SiC/SiC)

    SciTech Connect

    Fox, D.S.

    1994-12-31

    Silicon carbide fiber-reinforced silicon carbide (SiC/SiC) was exposed for 100 hours to dry, flowing oxygen. Oxidation kinetics were determined via thermogravimetric analysis at 981{degrees}, 1204{degrees} and 1316{degrees}C (1800{degrees}, 2200{degrees} and 2400{degrees}F). The effectiveness of three external coating systems applied for oxidation protection is discussed. In all cases, weight gains were observed, and the pyrolytic carbon interface layer remained intact. A CVD SiC external coating is the most promising due to low oxidation kinetics resulting from solid silica formation. A borosilicate glass was observed on the surface of two of the materials that have boron-containing coatings.

  17. Economical processing of fiber-reinforced components with thermal expansion molding

    NASA Technical Reports Server (NTRS)

    Schneider, K.

    1979-01-01

    The concept of economical fabrication of fiber-reinforced structural components is illustrated with an example of a typical control surface (aileron). The concept provides for fabricating struts, ribs, and a cover plate as an integral structure in a hardening device and then joining the closure cover plate mechanically. Fabrication of the integral structure is achieved by the 'thermal expansion molding' technique. The hardening pressure is produced by silicone rubber cores which expand under the influence of temperature. Test results are presented for several rubber materials as well as for various structural pieces. The technique is demonstrated extensively for an aileron, consisting of five ribs, struts, and a cover plate. Economically, for a large scale technical production of an aileron, cost savings of twenty-five percent can be realized compared to those for a sheet metal structure.

  18. Fabrication and properties of SiNO continuous fiber reinforced BN wave-transparent composites

    NASA Astrophysics Data System (ADS)

    Cao, F.; Fang, Z.; Chen, F.; Shen, Q.; Zhang, C.

    2012-06-01

    SiNO continuous fiber reinforced boron nitride (BN) wave-transparent composites (SiNO f /BN) have been fabricated by a precursor infiltration pyrolysis (PIP) method using borazine as the precursor. The densification behavior, microstructures, mechanical properties, and dielectric properties of the composites have been investigated. After four PIP cycles, the density of the composites had increased from 1.1 g·cm-3 to 1.81 g·cm-3. A flexural strength of 128.9 MPa and an elastic modulus of 23.5 GPa were achieved. The obtained composites have relatively high density and the fracture faces show distinct fiber pull-out and interface de-bonding features. The dielectric properties of the SiNO f /BN composites, including the dielectric constant of 3.61 and the dielectric loss angle tangent of 5.7×10-3, are excellent for application as wave-transparent materials.

  19. Mechanisms controlling fatigue damage development in continuous fiber reinforced metal matrix composites

    NASA Technical Reports Server (NTRS)

    Johnson, W. S.

    1989-01-01

    Damage in continuous fiber reinforced metal matrix composite materials can be quite complex since there are a number of different constituents (fiber, matrix, and the fiber/matrix interface) that can fail. Multidirectional lay-ups have an even greater number of possible damage orientations and mechanisms. Based on the simplifying assumption of equivalent constituent strain states in the absence of damage, a strain based failure criteria may be applied to determine when and where initial damage will occur. Based on the relative strain to fatigue failure of the fiber and matrix, the possible damage mechanisms of an MMC can be grouped into three categories: (1) matrix dominated, (2) fiber dominated, and (3) self-similar damage growth. A fourth type of damage development, fiber/matrix interface failure, is dependent on the relative strength of the fiber/matrix interface and the matrix yield strength. These four types of damage are discussed and illustrated by examples.

  20. Dynamic tensile response of a carbon-fiber-reinforced LCP composite and its temperature sensitivity

    NASA Astrophysics Data System (ADS)

    Shim, Victor P. W.; Yuan, J.; Lim, C. T.

    2001-06-01

    The tensile mechanical behavior of a short carbon fiber filled liquid crystalline polymer (LCP) composite, Vectra A230, was examined under static extension and dynamic loading at three temperatures. Dynamic tension was applied using a pendulum-type tensile spilt Hopkinson bar device. Specimens fabricated according to both the mould flow and transverse directions were tested. The stress-strain curves at various strain rates and temperatures were determined and found to be sensitive to strain rate as well as temperature for both types of specimens. With reference to the properties of pure LCP, mechanical anisotropy and fiber reinforcement effects were characterized and are discussed. Failed specimens were observed suing an optical microscope. Deformation and failure mechanisms in the microstructure of the LCP composite were studied to understand the effects of strain rate and temperature on material strength and failure strain.

  1. Nondestructive Evaluation of Carbon Fiber Reinforced Polymer Composites Using Reflective Terahertz Imaging

    PubMed Central

    Zhang, Jin; Li, Wei; Cui, Hong-Liang; Shi, Changcheng; Han, Xiaohui; Ma, Yuting; Chen, Jiandong; Chang, Tianying; Wei, Dongshan; Zhang, Yumin; Zhou, Yufeng

    2016-01-01

    Terahertz (THz) time-domain spectroscopy (TDS) imaging is considered a nondestructive evaluation method for composite materials used for examining various defects of carbon fiber reinforced polymer (CFRP) composites and fire-retardant coatings in the reflective imaging modality. We demonstrate that hidden defects simulated by Teflon artificial inserts are imaged clearly in the perpendicular polarization mode. The THz TDS technique is also used to measure the thickness of thin fire-retardant coatings on CFRP composites with a typical accuracy of about 10 micrometers. In addition, coating debonding is successfully imaged based on the time-delay difference of the time-domain waveforms between closely adhered and debonded sample locations. PMID:27314352

  2. Mid IR pulsed light source for laser ultrasonic testing of carbon-fiber-reinforced plastic

    NASA Astrophysics Data System (ADS)

    Hatano, H.; Watanabe, M.; Kitamura, K.; Naito, M.; Yamawaki, H.; Slater, R.

    2015-09-01

    A quasi-phase-matched (QPM) optical parametric oscillator (OPO) was developed using a periodically poled Mg-doped stoichiometric LiTaO3 crystal to generate mid-IR light for excitation of laser ultrasound in carbon fiber reinforced plastic (CFRP). The ultrasound generation efficiency was measured at the three different wavelengths that emanate from the OPO: 1.064 μm, 1.59/1.57 μm, and 3.23/3.30 μm. The measurements indicate that mid-IR 3.2-3.3 μm light generates the most efficient ultrasonic waves in CFRP with the least laser damage. We used mid-IR light in conjunction with a laser interferometer to demonstrate the detection of flaws/defects in CFRP such as the existence of air gaps that mimic delamination and voids in CFRP, and the inhomogeneous adhesion of CFRP material to a metal plate was also clearly detected.

  3. Finite element analysis of drilling in carbon fiber reinforced polymer composites

    NASA Astrophysics Data System (ADS)

    Phadnis, V. A.; Roy, A.; Silberschmidt, V. V.

    2012-08-01

    Carbon fiber reinforced polymer composite (CFRP) laminates are attractive for many applications in the aerospace industry especially as aircraft structural components due to their superior properties. Usually drilling is an important final machining process for components made of composite laminates. In drilling of CFRP, it is an imperative task to determine the maximum critical thrust forces that trigger inter-laminar and intra-laminar damage modes owing to highly anisotropic fibrous media; and negotiate integrity of composite structures. In this paper, a 3D finite element (FE) model of drilling in CFRP composite laminate is developed, which accurately takes into account the dynamic characteristics involved in the process along with the accurate geometrical considerations. A user defined material model is developed to account for accurate though thickness response of composite laminates. The average critical thrust forces and torques obtained using FE analysis, for a set of machining parameters are found to be in good agreement with the experimental results from literature.

  4. Fundamental analysis of the failure of polymer-based fiber reinforced composites

    NASA Technical Reports Server (NTRS)

    Kanninen, M. F.; Rybicki, E. F.; Griffith, W. I.; Broek, D.

    1975-01-01

    A mathematical model predicting the strength of unidirectional fiber reinforced composites containing known flaws and with linear elastic-brittle material behavior was developed. The approach was to imbed a local heterogeneous region surrounding the crack tip into an anisotropic elastic continuum. This (1) permits an explicit analysis of the micromechanical processes involved in the fracture, and (2) remains simple enough to be useful in practical computations. Computations for arbitrary flaw size and orientation under arbitrary applied loads were performed. The mechanical properties were those of graphite epoxy. With the rupture properties arbitrarily varied to test the capabilities of the model to reflect real fracture modes, it was shown that fiber breakage, matrix crazing, crack bridging, matrix-fiber debonding, and axial splitting can all occur during a period of (gradually) increasing load prior to catastrophic failure. The calculations also reveal the sequential nature of the stable crack growth process proceding fracture.

  5. Nondestructive Evaluation of Carbon Fiber Reinforced Polymer Composites Using Reflective Terahertz Imaging.

    PubMed

    Zhang, Jin; Li, Wei; Cui, Hong-Liang; Shi, Changcheng; Han, Xiaohui; Ma, Yuting; Chen, Jiandong; Chang, Tianying; Wei, Dongshan; Zhang, Yumin; Zhou, Yufeng

    2016-01-01

    Terahertz (THz) time-domain spectroscopy (TDS) imaging is considered a nondestructive evaluation method for composite materials used for examining various defects of carbon fiber reinforced polymer (CFRP) composites and fire-retardant coatings in the reflective imaging modality. We demonstrate that hidden defects simulated by Teflon artificial inserts are imaged clearly in the perpendicular polarization mode. The THz TDS technique is also used to measure the thickness of thin fire-retardant coatings on CFRP composites with a typical accuracy of about 10 micrometers. In addition, coating debonding is successfully imaged based on the time-delay difference of the time-domain waveforms between closely adhered and debonded sample locations. PMID:27314352

  6. SiC fiber reinforced reaction-bonded Si3N4 composites

    NASA Technical Reports Server (NTRS)

    Bhatt, Ramakrishna T.

    1986-01-01

    A technique for fabricating strong and tough SiC fiber reinforced reaction bonded Si3N4 matrix composites (SiC/RBSN) was developed. Using this technique, composites containing approximately 23, 30, and 40 volume fractions of aligned 140 micron diameter, chemically vapor deposited SiC fibers were fabricated. The room temperature physical and mechanical properties were evaluated. The results for composite tensile strength, bend strength, and fracture strain indicate that the composite displays excellent properties when compared with the unreinforced matrix of comparable porosity. The composite stress at which the matrix first cracks and the ultimate composite fracture strength increase with increasing volume fraction of fibers, and the composite fails gracefully. The mechanical property data of this ceramic composite are compared with similar data for unreinforced commercially available Si3N4 materials and for SEP SiC/SiC composites.

  7. Flexural strengthening of Reinforced Concrete (RC) Beams Retrofitted with Corrugated Glass Fiber Reinforced Polymer (GFRP) Laminates

    NASA Astrophysics Data System (ADS)

    Aravind, N.; Samanta, Amiya K.; Roy, Dilip Kr. Singha; Thanikal, Joseph V.

    2015-01-01

    Strengthening the structural members of old buildings using advanced materials is a contemporary research in the field of repairs and rehabilitation. Many researchers used plain Glass Fiber Reinforced Polymer (GFRP) sheets for strengthening Reinforced Concrete (RC) beams. In this research work, rectangular corrugated GFRP laminates were used for strengthening RC beams to achieve higher flexural strength and load carrying capacity. Type and dimensions of corrugated profile were selected based on preliminary study using ANSYS software. A total of twenty one beams were tested to study the load carrying capacity of control specimens and beams strengthened with plain sheets and corrugated laminates using epoxy resin. This paper presents the experimental and theoretical study on flexural strengthening of Reinforced Concrete (RC) beams using corrugated GFRP laminates and the results are compared. Mathematical models were developed based on the experimental data and then the models were validated.

  8. A method for measuring residual strains in fiber-reinforced titanium matrix composites

    SciTech Connect

    Ramamurty, U.; Dary, F.C.; Zok, F.W.

    1996-08-01

    A new method for measuring the residual fiber strains in fiber-reinforced titanium matrix composites has been developed. The method involves selectively etching the matrix over a prescribed length of composite and subsequently measuring the extension of the relaxed fibers relative to neighboring fibers that are still embedded within the matrix material. The extensions are measured using confocal microscopy. The method is demonstrated on three unidirectionally reinforced composites with varying fiber volume fractions. The effects of specimen tilt and fiber splaying following dissolution on the measured fiber extensions are analyzed. The residual fiber strains are rationalized on the basis of the thermoelastic properties of the constituents through a concentric cylinder model. The current method can be applied to other metal matrix composites reinforced with large diameter (monofilament) fibers, provided the matrix can be selectively etched.

  9. Utilization of power plant bottom ash as aggregates in fiber-reinforced cellular concrete.

    PubMed

    Lee, H K; Kim, H K; Hwang, E A

    2010-02-01

    Recently, millions tons of bottom ash wastes from thermoelectric power plants have been disposed of in landfills and coastal areas, regardless of its recycling possibility in construction fields. Fiber-reinforced cellular concrete (FRCC) of low density and of high strength may be attainable through the addition of bottom ash due to its relatively high strength. This paper focuses on evaluating the feasibility of utilizing bottom ash of thermoelectric power plant wastes as aggregates in FRCC. The flow characteristics of cement mortar with bottom ash aggregates and the effect of aggregate type and size on concrete density and compressive strength were investigated. In addition, the effects of adding steel and polypropylene fibers for improving the strength of concrete were also investigated. The results from this study suggest that bottom ash can be applied as a construction material which may not only improve the compressive strength of FRCC significantly but also reduce problems related to bottom ash waste. PMID:19910181

  10. Influence of attenuation on acoustic emission signals in carbon fiber reinforced polymer panels.

    PubMed

    Asamene, Kassahun; Hudson, Larry; Sundaresan, Mannur

    2015-05-01

    Influence of attenuation on acoustic emission (AE) signals in Carbon Fiber Reinforced Polymer (CFRP) crossply and quasi-isotropic panels is examined in this paper. Attenuation coefficients of the fundamental antisymmetric (A0) and symmetric (S0) wave modes were determined experimentally along different directions for the two types of CFRP panels. In the frequency range from 100 kHz to 500 kHz, the A0 mode undergoes significantly greater changes due to material related attenuation compared to the S0 mode. Moderate to strong changes in the attenuation levels were noted with propagation directions. Such mode and frequency dependent attenuation introduces major changes in the characteristics of AE signals depending on the position of the AE sensor relative to the source. Results from finite element simulations of a microscopic damage event in the composite laminates are used to illustrate attenuation related changes in modal and frequency components of AE signals. PMID:25682294

  11. Application of glass-fiber reinforced plastic (GRP) mud-mats for Daria-A platform

    SciTech Connect

    Bertorelli, D.; Spessa, A.

    1994-12-31

    A review of the experience gained with glass-fiber reinforced plastic (GRP) mud-mat materials used for the Garibaldi-C jacket, in the Adriatic sea, has shown that this solution can result in substantial cost savings. Therefore, Agip has investigated a further use of GRP mud-mats for the Daria-A platform as a means of reducing the lifting weight of the jacket and, moreover, to negate the requirement for additional buoyancy tanks during the free flotation and upending phases. Two possible solutions, the ``pultrusion`` and the ``lamination`` techniques, have been investigated to fabricate sandwich panels for the mud-mats. In this paper these two technologies are discussed with respect to their application to the construction and they are compared on a performance and cost basis.

  12. [Recent development of research on the biotribology of carbon fiber reinforced poly ether ether ketone composites].

    PubMed

    Chen, Yan; Pan, Yusong

    2014-12-01

    Carbon fiber reinforced poly ether ether ketone (CF/PEEK) composite possesses excellent biocompatible, biomechanical and bioribological properties. It is one of the most promising implant materials for artificial joint. Many factors influence the bioribological properties of CF/PEEK composites. In this paper, the authors reviewed on the biotribology research progress of CF/PEEK composites. The influences of various factors such as lubricant, reinforcement surface modification, functional particles, friction counterpart and friction motion modes on the bio-tribological properties of CF/PEEK composites are discussed. Based on the recent research, the authors suggest that the further research should be focused on the synergistic effect of multiple factors on the wear and lubrication mechanism of CF/PEEK. PMID:25868268

  13. Fatigue damage monitoring for basalt fiber reinforced polymer composites using acoustic emission technique

    NASA Astrophysics Data System (ADS)

    Wang, Wentao; Li, Hui; Qu, Zhi

    2012-04-01

    Basalt fiber reinforced polymer (BFRP) is a structural material with superior mechanical properties. In this study, unidirectional BFRP laminates with 14 layers are made with the hand lay-up method. Then, the acoustic emission technique (AE) combined with the scanning electronic microscope (SEM) technique is employed to monitor the fatigue damage evolution of the BFRP plates in the fatigue loading tests. Time-frequency analysis using the wavelet transform technique is proposed to analyze the received AE signal instead of the peak frequency method. A comparison between AE signals and SEM images indicates that the multi-frequency peaks picked from the time-frequency curves of AE signals reflect the accumulated fatigue damage evolution and fatigue damage patterns. Furthermore, seven damage patterns, that is, matrix cracking, delamination, fiber fracture and their combinations, are identified from the time-frequency curves of the AE signals.

  14. The failure of notched specimens of boron-fiber reinforced 6061 aluminum alloy

    NASA Technical Reports Server (NTRS)

    Wright, M. A.; Iannuzzi, F. A.

    1974-01-01

    The effect of notches on the strength of boron fiber reinforced 6061 aluminum alloy was determined at room temperature, 300 F, and 600 F. Both unidirectional and cross-plied specimens were tested. The strengths of individual fibers were measured, and upper and lower bounds of composite strength were calculated using bundle theory. Fracture tests were performed on specimens containing center slots of various lengths, and the values of the critical stress intensity factor for initial crack propagation or final failure were calculated. For unidirectional specimens, these parameters depended on thickness; for cross-plied specimens, fairly constant values were obtained at room temperature. The cross-plied material invariably failed at a lower stress as the environmental temperature was raised.

  15. Metal-bonded, carbon fiber-reinforced composites

    DOEpatents

    Sastri, S.A.; Pemsler, J.P.; Cooke, R.A.; Litchfield, J.K.; Smith, M.B.

    1996-03-05

    Metal bonded carbon fiber-reinforced composites are disclosed in which the metal and the composite are strongly bound by (1) providing a matrix-depleted zone in the composite of sufficient depth to provide a binding site for the metal to be bonded and then (2) infiltrating the metal into the matrix-free zone to fill a substantial portion of the zone and also provide a surface layer of metal, thereby forming a strong bond between the composite and the metal. The invention also includes the metal-bound composite itself, as well as the provision of a coating over the metal for high-temperature performance or for joining to other such composites or to other substrates. 2 figs.

  16. Metal-bonded, carbon fiber-reinforced composites

    DOEpatents

    Sastri, Suri A.; Pemsler, J. Paul; Cooke, Richard A.; Litchfield, John K.; Smith, Mark B.

    1996-01-01

    Metal bonded carbon fiber-reinforced composites are disclosed in which the metal and the composite are strongly bound by (1) providing a matrix-depleted zone in the composite of sufficient depth to provide a binding site for the metal to be bonded and then (2) infiltrating the metal into the matrix-free zone to fill a substantial portion of the zone and also provide a surface layer of metal, thereby forming a strong bond between the composite and the metal. The invention also includes the metal-bound composite itself, as well as the provision of a coating over the metal for high-temperature performance or for joining to other such composites or to other substrates.

  17. Fatigue strength of woven kenaf fiber reinforced composites

    NASA Astrophysics Data System (ADS)

    Ismail, A. E.; Aziz, M. A. Che Abdul

    2015-12-01

    Nowadays, green composites provide alternative to synthetic fibers for non-bearing and load-bearing applications. According to literature review, lack of information is available on the fatigue performances especially when the woven fiber is used instead of randomly oriented fibers. In order to overcome this problem, this paper investigates the fatigue strength of different fiber orientations and number of layers of woven kenaf fiber reinforced composites. Four types of fiber orientations are used namely 0°, 15°, 30° and 45°. Additionally, two numbers of layers are also considered. It is revealed that the fatigue life has no strong relationship with the fiber orientations. For identical fiber orientations, the fatigue life can be predicted considerably using the normalized stress. However as expected, the fatigue life enhancement occur when the number of layer is increased.

  18. Polymer microcapsules with a fiber-reinforced nanocomposite shell.

    PubMed

    Sagis, Leonard M C; Ruiter, Riëlle de; Miranda, Francisco J Rossier; Ruiter, Jolet de; Schroën, Karin; Aelst, Adriaan C van; Kieft, Henk; Boom, Remko; Linden, Erik van der

    2008-03-01

    Polymer microcapsules can be used as controlled release systems in drugs or in foods. Using layer-by-layer adsorption of common food proteins and polysaccharides, we produced a new type of microcapsule with tunable strength and permeability. The shell consists of alternating layers of pectin and whey protein fibrils, yielding a fiber-reinforced nanocomposite shell. The strength can be tightly controlled by varying the number of layers or the density and length of the fibrils in the protein layers. The mechanical stability of these microcapsules appears to be superior to that of currently available multilayer capsules. The method involves only standard unit operations and has the potential for scaling up to industrial production volumes. PMID:18237217

  19. Anomalous rheological behavior of long glass fiber reinforced polypropylene

    NASA Astrophysics Data System (ADS)

    Kim, Dong Hak; Lee, Young Sil; Son, Younggon

    2012-12-01

    Dynamic rheological properties of PP-based long glass fiber-reinforced thermoplastics (LFT) were investigated. Weight fractions of the glass fibers investigated in the present study ranged from 0.15 to 0.5, which are higher than those of previous studies. We observed very abnormal rheological behavior. Complex viscosity (η*) of the LFT increased with the glass fiber content up to 40 wt. %. However, the η* with a weight fraction of 0.5 is observed to be lower than that of LFT with a weight fraction of 0.4 in spite of higher glass fiber content. From various experiments, we found that this abnormal behavior is analogous to the rheological behavior of a lyotropic liquid crystalline polymer solution and concluded that the abnormal rheological behavior for the LFT is attributed to the formation of a liquid crystal- like structure at high concentrations of long glass fibers.

  20. Durability Studies on Confined Concrete using Fiber Reinforced Polymer

    NASA Astrophysics Data System (ADS)

    Ponmalar, V.; Gettu, R.

    2014-06-01

    In this study, 24 concrete cylinders with a notch at the centre were prepared. Among them six cylinders were wrapped using single and double layers of fiber reinforced polymer; six cylinders were coated with epoxy resin; the remaining cylinders were used as a control. The cylinders were exposed to wet and dry cycling and acid (3 % H2SO4) solution for the period of 120 days. Two different concrete strengths M30 and M50 were considered for the study. It is found that the strength, ductility and failure mode of wrapped cylinders depend on number of layers and the nature of exposure conditions. It was noticed that the damage due to wet and dry cycling and acid attack was severe in control specimen than the epoxy coated and wrapped cylinders.

  1. Thermal shock behavior of fiber-reinforced ceramic composites

    SciTech Connect

    Singh, R.N.; Wang, H.

    1995-10-01

    The influence of fiber type and method of composite fabrication on the thermal shock behavior of 2-D fiber-reinforced ceramic composites is studied. Thermal shock tests are performed using a water quench technique, and thermal shock damage is characterized by both destructive and nondestructive techniques. It is shown that the composites possessed superior resistance to thermal shock damage than the monolithic ceramics. Catastrophic failure due to severe thermal stresses is prevented in composites and a significant portion of their original strength is retained at a quench temperature difference up to 1,000 C. These results along with an analysis of the thermal shock damage mechanism based on the destructive and nondestructive tests is described.

  2. Robotic inspection of fiber reinforced composites using phased array UT

    NASA Astrophysics Data System (ADS)

    Stetson, Jeffrey T.; De Odorico, Walter

    2014-02-01

    Ultrasound is the current NDE method of choice to inspect large fiber reinforced airframe structures. Over the last 15 years Cartesian based scanning machines using conventional ultrasound techniques have been employed by all airframe OEMs and their top tier suppliers to perform these inspections. Technical advances in both computing power and commercially available, multi-axis robots now facilitate a new generation of scanning machines. These machines use multiple end effector tools taking full advantage of phased array ultrasound technologies yielding substantial improvements in inspection quality and productivity. This paper outlines the general architecture for these new robotic scanning systems as well as details the variety of ultrasonic techniques available for use with them including advances such as wide area phased array scanning and sound field adaptation for non-flat, non-parallel surfaces.

  3. Process of Making Boron-Fiber Reinforced Composite Tape

    NASA Technical Reports Server (NTRS)

    Belvin, Harry L. (Inventor); Cano, Roberto J. (Inventor); Johnston, Norman J. (Inventor); Marchello, Joseph M. (Inventor)

    2002-01-01

    The invention is an apparatus and method for producing a hybrid boron reinforced polymer matrix composition from powder pre-impregnated fiber tow bundles and a linear array of boron fibers. The boron fibers are applied onto the powder pre-impregnated fiber tow bundles and then are processed within a processing component having an impregnation bar assembly. After passing through variable-dimension forming nip-rollers, the powder pre-impregnated fiber tow bundles with the boron fibers become a hybrid boron reinforced polymer matrix composite tape. A driving mechanism pulls the powder pre-impregnated fiber tow bundles with boron fibers through the processing line of the apparatus and a take-up spool collects the formed hybrid boron-fiber reinforced polymer matrix composite tape.

  4. Fiber breakage phenomena in long fiber reinforced plastic preparation

    NASA Astrophysics Data System (ADS)

    Huang, Chao-Tsai; Tseng, Huan-Chang; Vlcek, Jiri; Chang, Rong-Yeu

    2015-07-01

    Due to the high demand of smart green, the lightweight technologies have become the driving force for the development of automotives and other industries in recent years. Among those technologies, using short and long fiber-reinforced plastics (FRP) to replace some metal components can reduce the weight of an automotive significantly. However, the microstructures of fibers inside plastic matrix are too complicated to manage and control during the injection molding through the screw, the runner, the gate, and then into the cavity. This study focuses on the fiber breakage phenomena during the screw plastification. Results show that fiber breakage is strongly dependent on screw design and operation. When the screw geometry changes, the fiber breakage could be larger even with lower compression ratio.

  5. Fracture behavior of glass fiber reinforced polymer composite

    SciTech Connect

    Avci, A.; Arikan, H.; Akdemir, A

    2004-03-01

    Chopped strand glass fiber reinforced particle-filled polymer composite beams with varying notch-to-depth ratios and different volume fractions of glass fibers were investigated in Mode I fracture using three-point bending tests. Effects of polyester resin content and glass fiber content on fracture behavior was also studied. Polyester resin contents were used 13.00%%, 14.75%, 16.50%, 18.00% and 19.50%, and glass fiber contents were 1% and 1.5% of the total weight of the polymer composite system. Flexural strength of the polymer composite increases with increase in polyester and fiber content. The critical stress intensity factor was determined by using several methods such as initial notch depth method, compliance method and J-integral method. The values of K{sub IC} obtained from these methods were compared.

  6. Objective Surface Evaluation of Fiber Reinforced Polymer Composites

    NASA Astrophysics Data System (ADS)

    Palmer, Stuart; Hall, Wayne

    2013-08-01

    The mechanical properties of advanced composites are essential for their structural performance, but the surface finish on exterior composite panels is of critical importance for customer satisfaction. This paper describes the application of wavelet texture analysis (WTA) to the task of automatically classifying the surface finish properties of two fiber reinforced polymer (FRP) composite construction types (clear resin and gel-coat) into three quality grades. Samples were imaged and wavelet multi-scale decomposition was used to create a visual texture representation of the sample, capturing image features at different scales and orientations. Principal components analysis was used to reduce the dimensionality of the texture feature vector, permitting successful classification of the samples using only the first principal component. This work extends and further validates the feasibility of this approach as the basis for automated non-contact classification of composite surface finish using image analysis.

  7. Glass Fiber Reinforced Metal Pressure Vessel Design Guide

    NASA Technical Reports Server (NTRS)

    Landes, R. E.

    1972-01-01

    The Engineering Guide presents curves and general equations for safelife design of lightweight glass fiber reinforced (GFR) metal pressure vessels operating under anticipated Space Shuttle service conditions. The high composite vessel weight efficiency is shown to be relatively insensitive to shape, providing increased flexibility to designers establishing spacecraft configurations. Spheres, oblate speroids, and cylinders constructed of GFR Inconel X-750, 2219-T62 aluminum, and cryoformed 301 stainless steel are covered; design parameters and performance efficiencies for each configuration are compared at ambient and cryogenic temperature for an operating pressure range of 690 to 2760 N/sq cm (1000 to 4000 psi). Design variables are presented as a function of metal shell operating to sizing (proof) stress ratios for use with fracture mechanics data generated under a separate task of this program.

  8. Glass fiber reinforced concrete for terrestrial photovoltaic arrays

    NASA Technical Reports Server (NTRS)

    Maxwell, H.

    1979-01-01

    The use of glass-fiber-reinforced concrete (GRC) as a low-cost structural substrate for terrestrial solar cell arrays is discussed. The properties and fabrication of glass-reinforced concrete structures are considered, and a preliminary design for a laminated solar cell assembly built on a GRC substrate is presented. A total cost for such a photovoltaic module, composed of a Korad acrylic plastic film front cover, an aluminum foil back cover, an ethylene/vinyl acetate pottant/adhesive and a cotton fabric electrical isolator in addition to the GRC substrate, of $9.42/sq m is projected, which is less than the $11.00/sq m cost goal set by the Department of Energy. Preliminary evaluations are concluded to have shown the design capabilities and cost effectiveness of GRC; however, its potential for automated mass production has yet to be evaluated.

  9. Toughened Matrix SiC Fiber Reinforced Composites

    NASA Technical Reports Server (NTRS)

    Levine, Stanley R.; Bhatt, Ramakrishna T.; Morscher, Gregory N.; Kiser, James D.

    2005-01-01

    First matrix cracking stress is a critical parameter for application of Sic fiber reinforced composites in highly stressed, environmentally demanding applications such as turbine blades. High matrix fracture toughness is a key property that contributes to high composite fracture stress. Silicon nitride offers reduced matrix elastic modulus, lower coefficient of thermal expansion, and potentially high fracture toughness compared to Sic matrices. All of these factors can be used to advantage to increase matrix fracture stress. As a first model system we are pursuing toughened silicon nitride matrix composites reinforced with SCS-9 fibers. Fabrication is by tape casting the matrix plies and tape lay-up with fiber plies followed by hot pressing at 1800 C. Progress toward this end will be reported.

  10. Interfacial optimization of fiber-reinforced hydrogel composites for soft fibrous tissue applications.

    PubMed

    Holloway, Julianne L; Lowman, Anthony M; VanLandingham, Mark R; Palmese, Giuseppe R

    2014-08-01

    Meniscal tears are the most common orthopedic injuries to the human body, yet the current treatment of choice is a partial meniscectomy, which is known to lead to joint degeneration and osteoarthritis. As a result, there is a significant clinical need to develop materials capable of restoring function to the meniscus following an injury. Fiber-reinforced hydrogel composites are particularly suited for replicating the mechanical function of native fibrous tissues due to their ability to mimic the native anisotropic property distribution present. A critical issue with these materials, however, is the potential for the fiber-matrix interfacial properties to severely limit composite performance. In this work, the interfacial properties of an ultra-high-molecular-weight polyethylene (UHMWPE) fiber-reinforced poly(vinyl alcohol) (PVA) hydrogel are studied. A novel chemical grafting technique, confirmed using X-ray photoelectron spectroscopy, is used to improve UHMWPE-PVA interfacial adhesion. Interfacial shear strength is quantified using fiber pull-out tests. Results indicate significantly improved fiber-hydrogel interfacial adhesion after chemical grafting, where chemically grafted samples have an interfacial shear strength of 256.4±64.3kPa compared to 11.5±2.9kPa for untreated samples. Additionally, scanning electron microscopy of fiber surfaces after fiber pull-out reveal cohesive failure within the hydrogel matrix for treated fiber samples, indicating that the UHMWPE-PVA interface has been successfully optimized. Lastly, inter-fiber spacing is observed to have a significant effect on interfacial adhesion. Fibers spaced further apart have significantly higher interfacial shear strengths, which is critical to consider when optimizing composite design. The results in this study are applicable in developing similar chemical grafting techniques and optimizing fiber-matrix interfacial properties for other hydrogel-based composite systems. PMID:24814880

  11. Titanium Implant Osseointegration Problems with Alternate Solutions Using Epoxy/Carbon-Fiber-Reinforced Composite

    PubMed Central

    Petersen, Richard C.

    2014-01-01

    The aim of the article is to present recent developments in material research with bisphenyl-polymer/carbon-fiber-reinforced composite that have produced highly influential results toward improving upon current titanium bone implant clinical osseointegration success. Titanium is now the standard intra-oral tooth root/bone implant material with biocompatible interface relationships that confer potential osseointegration. Titanium produces a TiO2 oxide surface layer reactively that can provide chemical bonding through various electron interactions as a possible explanation for biocompatibility. Nevertheless, titanium alloy implants produce corrosion particles and fail by mechanisms generally related to surface interaction on bone to promote an inflammation with fibrous aseptic loosening or infection that can require implant removal. Further, lowered oxygen concentrations from poor vasculature at a foreign metal surface interface promote a build-up of host-cell-related electrons as free radicals and proton acid that can encourage infection and inflammation to greatly influence implant failure. To provide improved osseointegration many different coating processes and alternate polymer matrix composite (PMC) solutions have been considered that supply new designing potential to possibly overcome problems with titanium bone implants. Now for important consideration, PMCs have decisive biofunctional fabrication possibilities while maintaining mechanical properties from addition of high-strengthening varied fiber-reinforcement and complex fillers/additives to include hydroxyapatite or antimicrobial incorporation through thermoset polymers that cure at low temperatures. Topics/issues reviewed in this manuscript include titanium corrosion, implant infection, coatings and the new epoxy/carbon-fiber implant results discussing osseointegration with biocompatibility related to nonpolar molecular attractions with secondary bonding, carbon fiber in vivo properties, electrical

  12. Resin characterization in cured graphite fiber reinforced composites using diffuse reflectance-FTIR. [Fourier transform infrared spectroscopy

    NASA Technical Reports Server (NTRS)

    Young, P. R.; Stein, B. A.; Chang, A. C.

    1983-01-01

    The feasibility of using diffuse reflectance in combination with Fourier transform infrared spectroscopy to obtain information on cured graphite fiber reinforced polymeric matrix resin composites was investigated. Several graphite/epoxy, polysulfone, and polyimide composites exposed to thermal or radiation environments were examined. An experimental polyimide-sulfone adhesive tape was also studied during processing. In each case, significant changes in resin molecular structure was observed due to environmental exposure. These changes in molecular structure were correlated with previously observed changes in material properties providing new insights into material behavior.

  13. Investigation of electrical and impact properties of carbon fiber reinforced polymer matrix composites with carbon nanotube buckypaper layers

    NASA Astrophysics Data System (ADS)

    Hill, Christopher Brandon

    Carbon fiber reinforced composite materials have become commonplace in many industries including aerospace, automotive, and sporting goods. Previous research has determined a coupling relationship between the mechanical and electrical properties of these materials where the application of electrical current has been shown to improve their mechanical strengths. The next generations of these composites have started to be produced with the addition of nanocarbon buckypaper layers which provide even greater strength and electrical conductivity potentials. The focus of this current research was to characterize these new composites and compare their electro-mechanical coupling capabilities to those composites which do not contain any nonocarbons.

  14. High temperature resistant composites from bismaleimide resin.

    NASA Technical Reports Server (NTRS)

    Gilwee, W. J.; Rosser, R. W.; Parker, J. A.

    1973-01-01

    It is shown that bismaleimide/woven fiberglass composites molded at moderate pressures (100 psi) yield void-free laminates of good integrity. The strength of the laminates at room temperature compares favorably with epoxy/glass laminates; at 260 C, the laminates are far superior in oxidative aging to epoxy and silicon laminates. The synthesis, processing, and fabrication of a bismaleide polymer are discussed.

  15. Affordable Fiber-Reinforced Ceramic Composites Win 1995 R and D 100 Award

    NASA Technical Reports Server (NTRS)

    1995-01-01

    Affordable fiber-reinforced ceramic matrix composites (AFReCC) with high strength and toughness, good thermal conductivity, thermal shock resistance, and oxidation resistance are needed for high-temperature structural applications. AFReCC materials will have various applications in advanced high-efficiency and high-performance engines: that is, the High Speed Civil Transport (HSCT), space propulsion components, and land-based systems. For example, silicon-carbide-fiber-reinforced silicon carbide matrix composites show promise for meeting the criteria of high strength, thermal conductivity, and toughness required for the HSCT combustor liner. AFReCC received R&D Magazine's prestigious R&D 100 Award in 1995. The fabrication process for these composites has three steps. In the first step, fiber preforms are made and chemical vapor infiltration is used to apply the desired interface coating on the fibers. This step also rigidizes the preform. The second step consists of resin infiltration, which after pyrolysis, yields an interconnected network of porous carbon as the matrix. In the final step of the process, the carbon-containing preform is infiltrated with molten silicon or silicon alloys in a furnace. This converts the carbon to silicon carbide leaving as little as 5 percent residual free silicon or refractory disilicide phase. This process is suitable for any type of small-diameter fiber (e.g., carbon, alumina, or silicon carbide) woven into a two- or three-dimensional architecture. This processing approach leads to dense composites where matrix microstructure and composition can be tailored for optimum properties. It has much lower processing cost (less than 50 percent) in comparison to other approaches to fabricating silicon-carbide-based composites. The photograph shows the various AFReCC components. Thermomechanical and thermochemical characterization of these composites under the hostile environments that will be encountered in engine applications is underway.

  16. Development of Rapid Pipe Moulding Process for Carbon Fiber Reinforced Thermoplastics by Direct Resistance Heating

    NASA Astrophysics Data System (ADS)

    Tanaka, Kazuto; Harada, Ryuki; Uemura, Toshiki; Katayama, Tsutao; Kuwahara, Hideyuki

    To deal with environmental issues, the gasoline mileage of passenger cars can be improved by reduction of the car weight. The use of car components made of Carbon Fiber Reinforced Plastics (CFRP) is increasing because of its superior mechanical properties and relatively low density. Many vehicle structural parts are pipe-shaped, such as suspension arms, torsion beams, door guard bars and impact beams. A reduction of the car weight is expected by using CFRP for these parts. Especially, when considering the recyclability and ease of production, Carbon Fiber Reinforced Thermoplastics are a prime candidate. On the other hand, the moulding process of CFRTP pipes for mass production has not been well established yet. For this pipe moulding process an induction heating method has been investigated already, however, this method requires a complicated coil system. To reduce the production cost, another system without such complicated equipment is to be developed. In this study, the pipe moulding process of CFRTP using direct resistance heating was developed. This heating method heats up the mould by Joule heating using skin effect of high-frequency current. The direct resistance heating method is desirable from a cost perspective, because this method can heat the mould directly without using any coils. Formerly developed Non-woven Stitched Multi-axial Cloth (NSMC) was used as semi-product material. NSMC is very suitable for the lamination process due to the fact that non-crimp stitched carbon fiber of [0°/+45°/90°/-45°] and polyamide 6 non-woven fabric are stitched to one sheet, resulting in a short production cycle time. The use of the pipe moulding process with the direct resistance heating method in combination with the NSMC, has resulted in the successful moulding of a CFRTP pipe of 300 mm in length, 40 mm in diameter and 2 mm in thickness.

  17. Evaluation of the Load-bearing Capacity of Fractured Incisal Edge of Maxillary Permanent Central Incisors restored with a Glass Fiber-reinforced Nanocomposite: An in vitro Study

    PubMed Central

    Srilatha, KT; Nandlal, B; Dhull, Kanika Singh

    2015-01-01

    ABSTRACT Objectives: The aim of this study was to evaluate and compare the load-bearing capacity of fractured incisal edge of maxillary permanent central incisors restored with a nanocomposite and a glass fiber-reinforced nanocomposite. Materials and methods: Thirty-six extracted sound maxillary central incisors randomly divided in three groups were used for the present study. Group I (control) contained untreated teeth. Samples in experimental groups II and III were prepared by cutting the incisal (one-third) part of the crown horizontally and subjected to enamel preparations and restored with a nanocomposite and a glass fiber-reinforced nanocomposite respectively. All restored teeth were stored in distilled water at room temperature for 24 hours. Fracture resistance was evaluated as peak load at failure (Newton) for samples tested in a cantilever-bending test using Hounsfield universal testing machine. Failure modes were microscopically examined. Results: Highest mean peak failure load (Newton) among experimental groups was observed in glass fiber-reinforced nano composite group (863.50 ± 76.12 N) followed by nanocomposite group (633.67 ± 40.14 N). One-way analysis of variance (ANOVA) revealed that the restoration technique significantly affected the load-bearing capacity (p < 0.001). Scheffe’s post-hoc comparison test (subset for α = 0.05) revealed that there was significant difference in the mean peak failure load values of nanocomposite and glass fiber-reinforced nanocomposite groups when considered together (p < 0.001). Experimental groups showed similar types of failure modes with majority occurring ascohesive and mixed type. Fifty-eight percent of the teeth in glass fiber-reinforced nanocomposite group fractured below the cementoenamel junction. Conclusion: By using fiber-reinforced composite substructure under conventional composites in the repair of fractured incisors, the load-bearing capacity of the restored incisal edge could be substantially

  18. The effect of joint surface contours and glass fiber reinforcement on the transverse strength of repaired acrylic resin: An in vitro study

    PubMed Central

    Anasane, Nayana; Ahirrao, Yogesh; Chitnis, Deepa; Meshram, Suresh

    2013-01-01

    Background: Denture fracture is an unresolved problem in complete denture prosthodontics. However, the repaired denture often experiences a refracture at the repaired site due to poor transverse strength. Hence, this study was conducted to evaluate the effect of joint surface contours and glass fiber reinforcement on the transverse strength of repaired acrylic resins. Materials and Methods: A total of 135 specimens of heat polymerized polymethyl methacrylate resin of dimensions 64 × 10 × 2.5 mm were fabricated. Fifteen intact specimens served as the control and 120 test specimens were divided into four groups (30 specimens each), depending upon the joint surface contour (butt, bevel, rabbet and round), with two subgroups based on type of the repair. Half of the specimens were repaired with plain repair resin and the other half with glass fibers reinforced repair resin. Transverse strength of the specimens was determined using three-point bending test. The results were analyzed using one-way ANOVA and Tukey post-hoc test (α= 0.05). Results: Transverse strength values for all repaired groups were significantly lower than those for the control group (P < 0.001) (88.77 MPa), with exception of round surface design repaired with glass fiber reinforced repair resin (89.92 MPa) which was significantly superior to the other joint surface contours (P < 0.001). Glass fiber reinforced resin significantly improved the repaired denture base resins as compared to the plain repair resin (P < 0.001). Conclusion: Specimens repaired with glass fiber reinforced resin and round surface design exhibited highest transverse strength; hence, it can be advocated for repair of denture base resins. PMID:23946739

  19. Diaphragm forming of carbon-fiber-reinforced thermoplastic composite materials

    SciTech Connect

    Smiley, A.J.

    1988-01-01

    The experimental work consisted of fabricating composite components and identifying the effects of the forming parameters on the resulting thickness profiles and fiber orientation. The transverse fiber flow produced thickness variations and fiber-orientation fields peculiar to the tool-surface geometry, diaphragm deformation behavior, and laminate configuration. The transverse flow in the surface-ply layers was dominated by the stretching diaphragms. In the interior ply layers the flow appeared to be driven by the pressure gradients produced at the contact points. The analytical work consisted of the development of a diaphragm-forming process model which employed engineering mechanics and fiber kinematics to predict post-formed thickness variations and fiber orientation fields of axisymmetric composite components. The flow analysis determined the thickness variation and flow velocities in the transverse fiber direction. The flow velocities were employed to determine the relative fiber realignment. The realignment of the fibers was then utilized in a geometric mapping procedure to determine the fiber-orientation field. Overall, the predictions on interior-ply and surface-ply layer orientations matched reasonably well with the experimental observations.

  20. Modelling of dimensional stability of fiber reinforced composite materials

    NASA Technical Reports Server (NTRS)

    Hahn, H. T.; Hosangadi, A.

    1982-01-01

    Various methods of predicting the expansion and diffusion properties of composite laminates are reviewed. The prediction equations for continuous fiber composites can be applied to SMC composites as the effective fiber aspect ratio in the latter is large enough. The effect of hygrothermal expansion on the dimensional stability of composite laminates was demonstrated through the warping of unsymmetric graphite/epoxy laminates. The warping is very sensitive to the size of the panel, and to the moisture content which is in turn sensitive to the relative humidity in the environment. Thus, any long term creep test must be carried out in a humidity-controlled environment. Environmental effects in SMC composites and bulk polyester were studied under seven different environments. The SMC composites chosen are SMC-R25, SMC-R40, and SMC-R65.

  1. Laser drilling of carbon fiber reinforced plastics (CFRP) by picosecond laser pulses: comparative study of different drilling tools

    NASA Astrophysics Data System (ADS)

    Herrmann, T.; Stolze, M.; L'huillier, J.

    2014-03-01

    Carbon fiber reinforced plastic (CFRP) as a lightweight material with superior properties is increasingly being used in industrial manufacturing. Using ultrashort laser pulses can improve the quality in cutting or drilling applications, but at high power levels it is more complicated to maintain the accuracy and precision in CFRP drilling. According to the application requirements for the extent of the heat affected zone, the geometric precision and the productivity different drilling tools can be used. Therefore we report on the application of three different beam delivery systems to drilling processes of CFRP: Galvanometer scanner, trepanning head and diffractive optical elements.

  2. Experimental Study on Tensile Behavior of Carbon Fiber and Carbon Fiber Reinforced Aluminum at Different Strain Rate

    NASA Astrophysics Data System (ADS)

    Zhou, Yuanxin; Wang, Ying; Jeelani, Shaik; Xia, Yuanming

    2007-01-01

    In this study, dynamic and quasi-static tensile behaviors of carbon fiber and unidirectional carbon fiber reinforced aluminum composite have been investigated. The complete stress strain curves of fiber bundles and the composite at different strain rates were obtained. The experimental results show that carbon fiber is a strain rate insensitive material, but the tensile strength and critical strain of the Cf/Al composite increased with increasing of strain rate because of the strain rate strengthening effect of aluminum matrix. Based on experimental results, a fiber bundles model has been combined with Weibull strength distribution function to establish a one-dimensional damage constitutive equation for the Cf/Al composite.

  3. Inductive wireless sensor-actuator node for structural health monitoring of fiber reinforced polymers by means of Lamb-waves

    NASA Astrophysics Data System (ADS)

    Focke, Oliver; Salas, Mariugenia; Herrmann, Axel S.; Lang, Walter

    2015-03-01

    Wireless excitation of Piezo-Wafer-Active-Sensors (PWAS) was achieved using Low-frequency coils produced via Tailored-Fiber-Placement. Carbon Fiber Reinforced Polymer behaves as conductor and depending on the frequency it shields radio waves; this effect is rising at high-frequency. A high permeability material was placed under the highfrequency antenna and re-tuning was performed to improve the quality of transmission. In this manner sensor responses were successfully transmitted wirelessly by analog amplitude modulation. The signals were evaluated to verify the functionality in presence of defects like delamination or holes. Generated power was confirmed to be enough to excite the actuator.

  4. Solid Free-Form Fabrication of Continuous Fiber Reinforced Composites for Propulsion Application

    NASA Technical Reports Server (NTRS)

    Vaidyanathan, R.; Walish, J.; Fox, M.; Rigali, M.; Sutaria, M.; Gillespie, John W., Jr.; Yarlagadda, Shridhar; Effinger, Mike; Munafo, Paul M. (Technical Monitor)

    2001-01-01

    For propulsion related applications, materials must be able to demonstrate excellent ablation and oxidation resistance at temperature approaching 3500 C, adequate load bearing capabilities, non-catastrophic failure modes, and ability to withstand transient thermal shock. A potential list of propulsion-material property requirements includes, low density, high elastic modulus, low thermal-expansion coefficient, high thermal conductivity, excellent erosion and oxidation/corrosion resistance, and flaw-insensitivity. In many cases, they will also need to be able to be joined, survive thermal cycling and multi-axial stress states, and for reusable applications, the materials must maintain the above attributes after prolonged exposure to extremely harsh chemical environments. The final and possibly most important attribute for these materials are the need to be lower cost and readily available in large quantities. Recently, Advanced Ceramics Research, Inc. (ACR) has developed low cost, flexible-manufacturing processes for Zr & Hf-based carbon fiber reinforced composites, materials with good oxidation and ablation resistance up to 3500 C. This process, called Continuous Composite Co-extrusion (C(sup 3)), incorporates carbon fibers to fabricate 'in-situ' carbide and boride-matrix/carbon fiber composites. M is a variation of ACR's manufacturing process for low-cost structural ceramic materials called Fibrous Monoliths with carbon fiber reinforcements. Fibrous Monolithic materials have a distinct fibrous texture, consist of intertwined cells of a primary phase, separated by cell boundaries of a tailored secondary phase and show very high fracture energies, damage tolerance, and graceful failure. Since they are monolithic powder based composites; they can be manufactured by conventional powder processing techniques using inexpensive raw materials. This combination of high performance and low cost is a breakthrough that could enable wider application of ceramics in high

  5. Solid Freeform Fabrication of Continuous Fiber Reinforced Composites for Propulsion Applications

    NASA Technical Reports Server (NTRS)

    Vaidyanathan, R.; Walish, J.; Fox, M.; Rigali, M.; Sutaria, M.; Gillespie, John W., Jr.; Yarlagadda, Shridhar; Effinger, Mike

    2000-01-01

    For propulsion related applications, materials must be able to demonstrate excellent ablation and oxidation resistance at temperature approaching 3500'C, adequate load bearing capabilities, non-catastrophic failure modes, and ability to withstand transient thermal shock. A potential list of propulsion-material property requirements includes, low density, high elastic modulus, low thermal-expansion coefficient, high thermal conductivity, excellent erosion and oxidation/corrosion resistance, and flaw-insensitivity. In many cases, they will also need to be able to be joined, survive thermal cycling and multi-axial stress states, and for reusable applications, the materials must maintain the above attributes after prolonged exposure to extremely harsh chemical environments. The final and possibly most important attribute for these materials are the need to be lower cost and readily available in large quantities. Recently, Advanced Ceramics Research, Inc. (ACR) has developed low cost, flexible- manufacturing processes for Zr & Hf-based carbon fiber reinforced composites, materials with good oxidation and ablation resistance up to 3500 C. This process, called Continuous Composite Co-extrusion (C(sup 3)), incorporates carbon fibers to fabricate 'in-situ' carbide and boride-matrix/carbon fiber composites. This is a variation of ACR's manufacturing process for low-cost structural ceramic materials called Fibrous Monoliths With carbon fiber reinforcements. Fibrous Monolithic materials have a distinct fibrous texture, consist of intertwined cells of a primary phase, separated by cell boundaries of a tailored secondary phase and show very high fracture energies, damage tolerance, and graceful failure. Since they are monolithic powder based composites-, they can be manufactured by conventional powder processing techniques using inexpensive raw materials. This combination of high performance and low cost is a breakthrough that could enable wider application of ceramics in high

  6. Intermediate-temperature environmental effects on boron nitride-coated silicon carbide-fiber-reinforced glass-ceramic composites

    SciTech Connect

    Sun, E.Y.; Lin, H.T.; Brennan, J.J.

    1997-03-01

    The environmental effects on the mechanical properties of fiber-reinforced composites at intermediate temperatures were investigated by conducting flexural static-fatigue experiments in air at 600 and 950 C. The material that was studied was a silicon carbide/boron nitride (SiC/BN) dual-coated Nicalon-fiber-reinforced barium magnesium aluminosilicate glass-ceramic. Comparable time-dependent failure responses were found at 600 and 950 C when the maximum tensile stress applied in the bend bar was >60% of the room-temperature ultimate flexural strength of as-received materials. At both temperatures, the materials survived 500 h fatigue tests at lower stress levels. Among the samples that survived the 500 h fatigue tests, a 20% degradation in the room temperature flexural strength was measured in samples that were fatigued at 600 C. The growth rate of the Si-C-O fiber oxidation product at 600 C was not sufficient to seal the stress-induced cracks, so that the interior of the material was oxidized and resulted in a strength degradation and less fibrous fracture. In contrast, the interior of the material remained intact at 950 C because of crack sealing by rapid silicate formation, and strength/toughness of the composite was maintained. Also, at 600 C, BN oxidized via volatilization, because no borosilicate was formed.

  7. FIBER LENGTH DISTRIBUTION MEASUREMENT FOR LONG GLASS AND CARBON FIBER REINFORCED INJECTION MOLDED THERMOPLASTICS

    SciTech Connect

    Kunc, Vlastimil; Frame, Barbara J; Nguyen, Ba N.; TuckerIII, Charles L.; Velez-Garcia, Gregorio

    2007-01-01

    Procedures for fiber length distribution (FLD) measurement of long fiber reinforced injection molded thermoplastics were refined for glass and carbon fibers. Techniques for sample selection, fiber separation, digitization and length measurement for both fiber types are described in detail. Quantitative FLD results are provided for glass and carbon reinforced polypropylene samples molded with a nominal original fiber length of 12.7 mm (1/2 in.) using equipment optimized for molding short fiber reinforced thermoplastics.

  8. Nondestructive Evaluation of Advanced Fiber Reinforced Polymer Matrix Composites: A Technology Assessment

    NASA Technical Reports Server (NTRS)

    Yolken, H. Thomas; Matzkanin, George A.

    2009-01-01

    Because of their increasing utilization in structural applications, the nondestructive evaluation (NDE) of advanced fiber reinforced polymer composites continues to receive considerable research and development attention. Due to the heterogeneous nature of composites, the form of defects is often very different from a metal and fracture mechanisms are more complex. The purpose of this report is to provide an overview and technology assessment of the current state-of-the-art with respect to NDE of advanced fiber reinforced polymer composites.

  9. Feasibility research report of villa constructed of glass fiber reinforced concrete

    NASA Astrophysics Data System (ADS)

    Li, Shengli; Lu, Yu; Wang, Dongwei

    2011-04-01

    With the development of economy and improvement degree of modernization, the villa project design program tend to focus on the green, high-tech, humanities, and more emphasis on the integrity of space, noble and elegant feeling. Therefore, based on the study of literatures, this paper discussed the present situation and issue and features of Glass Fiber Reinforced Concrete and the feature of assembly house, and confirmed that the villa of assemble house is feasible by built of Glass Fiber Reinforced Concrete.

  10. Discontinuous Fiber-reinforced Composites above Critical Length

    PubMed Central

    Petersen, R.C.

    2014-01-01

    Micromechanical physics of critical fiber length, describing a minimum filament distance for resin impregnation and stress transfer, has not yet been applied in dental science. As a test of the hypothesis that 9-micron-diameter, 3-mm-long quartz fibers would increase mechanical strength over particulate-filled composites, photocure-resin-pre-impregnated discontinuous reinforcement was incorporated at 35 wt% into 3M Corporation Z100, Kerr Corporation HerculiteXRV, and an experimental photocure paste with increased radiopaque particulate. Fully articulated four-point bend testing per ASTM C 1161-94 for advanced ceramics and Izod impact testing according to a modified unnotched ASTM D 256-00 specification were then performed. All photocure-fiber-reinforced composites demonstrated significant improvements over particulate-filled compounds (p < 0.001) for flexural strength, modulus, work of fracture, strain at maximum load, and Izod toughness, with one exception for the moduli of Z100 and the experimental reinforced paste. The results indicate that inclusion of pre-impregnated fibers above the critical aspect ratio yields major advancements regarding the mechanical properties tested. PMID:15790745

  11. Natural Curaua Fiber-Reinforced Composites in Multilayered Ballistic Armor

    NASA Astrophysics Data System (ADS)

    Monteiro, Sergio Neves; Louro, Luis Henrique Leme; Trindade, Willian; Elias, Carlos Nelson; Ferreira, Carlos Luiz; de Sousa Lima, Eduardo; Weber, Ricardo Pondé; Miguez Suarez, João Carlos; da Silva Figueiredo, André Ben-Hur; Pinheiro, Wagner Anacleto; da Silva, Luis Carlos; Lima, Édio Pereira

    2015-10-01

    The performance of a novel multilayered armor in which the commonly used plies of aramid fabric layer were replaced by an equal thickness layer of distinct curaua fiber-reinforced composites with epoxy or polyester matrices was assessed. The investigated armor, in addition to its polymeric layer (aramid fabric or curaua composite), was also composed of a front Al2O3 ceramic tile and backed by an aluminum alloy sheet. Ballistic impact tests were performed with actual 7.62 caliber ammunitions. Indentation in a clay witness, simulating human body behind the back layer, attested the efficacy of the curaua-reinforced composite as an armor component. The conventional aramid fabric display a similar indentation as the curaua/polyester composite but was less efficient (deeper indentation) than the curaua/epoxy composite. This advantage is shown to be significant, especially in favor of the lighter and cheaper epoxy composite reinforced with 30 vol pct of curaua fiber, as possible substitute for aramid fabric in multilayered ballistic armor for individual protection. Scanning electron microscopy revealed the mechanism associated with the curaua composite ballistic performance.

  12. Evaluation of a new fiber-reinforced resin composite.

    PubMed

    Suzuki, S; Saimi, Y; Ono, T

    2006-01-01

    Efficacy of the usage of an experimental fiber-reinforced composite (FRC) on mechanical properties of an indirect composite was investigated by means of three-point bending and Charpy impact tests. Bond strength between the FRC and the indirect composite was also evaluated by tensile testing. The FRC consisted of a matrix resin with 25% silanized milled glass fiber (11-microm diameter, 150-microm length) and 5% colloidal silica. The values of strain of proportional limit, total strain, and fracture energy of the FRC during the bending test (1.2%, 10.4%, and 41.6 x 10(-3) J) were significantly higher than those of the indirect composite (0.1%, 2.5%, and 11.9 x 10(-3) J). The impact strengths of the 1-mm specimens with FRC ranged from 15.2 to 15.9 kJ/m(2), and were significantly higher than that of the control (3.1 kJ/m(2)). The 2-mm specimens showed significant difference from the control when the FRC thickness was equal or greater than 0.5 mm. The bond strength after the thermocycling was 15.2 MPa, and all of the specimens exhibited cohesive fracture inside the indirect composite. Based upon the results, it was concluded that the FRC tested in this study improved toughness and impact resistance of the indirect composite. The interfacial bonding between the FRC and the indirect composite was strong enough to prevent delamination. PMID:16161120

  13. Micromechanical model of crack growth in fiber reinforced ceramics

    NASA Technical Reports Server (NTRS)

    Rubinstein, Asher A.; Xu, Kang

    1990-01-01

    A model based on the micromechanical mechanism of crack growth resistance in fiber reinforced ceramics is presented. The formulation of the model is based on a small scale geometry of a macrocrack with a bridging zone, the process zone, which governs the resistance mechanism. The effect of high toughness of the fibers in retardation of the crack advance, and the significance of the fiber pullout mechanism on the crack growth resistance, are reflected in this model. The model allows one to address issues such as influence of fiber spacing, fiber flexibility, and fiber matrix friction. Two approaches were used. One represents the fracture initiation and concentrated on the development of the first microcracks between fibers. An exact closed form solution was obtained for this case. The second case deals with the development of an array of microcracks between fibers forming the bridging zone. An implicit exact solution is formed for this case. In both cases, a discrete fiber distribution is incorporated into the solution.

  14. Oxidation Behavior of Carbon Fiber Reinforced Silicon Carbide Composites

    NASA Technical Reports Server (NTRS)

    Valentin, Victor M.

    1995-01-01

    Carbon fiber reinforced Silicon Carbide (C-SiC) composites offer high strength at high temperatures and good oxidation resistance. However, these composites present some matrix microcracks which allow the path of oxygen to the fiber. The aim of this research was to study the effectiveness of a new Silicon Carbide (SiC) coating developed by DUPONT-LANXIDE to enhance the oxidation resistance of C-SiC composites. A thermogravimetric analysis was used to determine the oxidation rate of the samples at different temperatures and pressures. The Dupont coat proved to be a good protection for the SiC matrix at temperatures lower than 1240 C at low and high pressures. On the other hand, at temperatures above 1340 C the Dupont coat did not seem to give good protection to the composite fiber and matrix. Even though some results of the tests have been discussed, because of time restraints, only a small portion of the desired tests could be completed. Therefore, no major conclusions or results about the effectiveness of the coat are available at this time.

  15. Creep of experimental short fiber-reinforced composite resin.

    PubMed

    Garoushi, Sufyan; Kaleem, Muhammad; Shinya, Akikazu; Vallittu, Pekka K; Satterthwaite, Julian D; Watts, David C; Lassila, Lippo V J

    2012-01-01

    The purpose of this study was to investigate the reinforcing effect of short E-glass fiber fillers oriented in different directions on composite resin under static and dynamic loading. Experimental short fiber-reinforced composite resin (FC) was prepared by mixing 22.5 wt% of short E-glass fibers, 22.5 wt% of resin, and 55 wt% of silane-treated silica fillers. Three groups of specimens (n=5) were tested: FC with isotropic fiber orientation, FC with anisotropic fiber orientation, and particulate-filled composite resin (PFC) as a control. Time-dependent creep and recovery were recorded. ANOVA revealed that after secondary curing in a vacuum oven and after storage in dry condition for 30 days, FC with isotropic fiber orientation (1.73%) exhibited significantly lower static creep value (p<0.05) than PFC (2.54%). For the different curing methods and storage conditions evaluated in this study, FC achieved acceptable static and dynamic creep values when compared to PFC. PMID:23037835

  16. Unsaturated and Saturated Permeabilities of Fiber Reinforcement: Critics and Suggestions

    NASA Astrophysics Data System (ADS)

    Park, Chung Hae; Krawczak, Patricia

    2015-04-01

    In general, permeability measurement results show a strong scattering according to the measurement method, the type of test fluid and the fluid injection condition, even though permeability is regarded as a unique property of porous medium. In particular, the discrepancy between the unsaturated and saturated permeabilities for the same fabric has been widely reported. In the literature, relative permeability has been adopted to model the unsaturated flow. This approach has some limits in the modeling of double-scale porosity medium. We address this issue of permeability measurement by rigorously examining the mass conservation condition. Finally, we identify that the pressure gradient is non-linear with positive curvature in the unsaturated flow and a misinterpretation of pressure gradient is the main reason for the difference between the saturated and unsaturated permeabilities of the same fiber reinforcement. We propose to use a fixed value of permeability and to modify the mass conservation equation if there are air voids which are entrapped inside the fiber tow. Finally, we also suggest some guidelines and future perspectives to obtain more consistent permeability measurement results.

  17. Novel hybrid columns made of ultra-high performance concrete and fiber reinforced polymers

    NASA Astrophysics Data System (ADS)

    Zohrevand, Pedram

    The application of advanced materials in infrastructure has grown rapidly in recent years mainly because of their potential to ease the construction, extend the service life, and improve the performance of structures. Ultra-high performance concrete (UHPC) is one such material considered as a novel alternative to conventional concrete. The material microstructure in UHPC is optimized to significantly improve its material properties including compressive and tensile strength, modulus of elasticity, durability, and damage tolerance. Fiber-reinforced polymer (FRP) composite is another novel construction material with excellent properties such as high strength-to-weight and stiffness-to-weight ratios and good corrosion resistance. Considering the exceptional properties of UHPC and FRP, many advantages can result from the combined application of these two advanced materials, which is the subject of this research. The confinement behavior of UHPC was studied for the first time in this research. The stress-strain behavior of a series of UHPC-filled fiber-reinforced polymer (FRP) tubes with different fiber types and thicknesses were tested under uniaxial compression. The FRP confinement was shown to significantly enhance both the ultimate strength and strain of UHPC. It was also shown that existing confinement models are incapable of predicting the behavior of FRP-confined UHPC. Therefore, new stress-strain models for FRP-confined UHPC were developed through an analytical study. In the other part of this research, a novel steel-free UHPC-filled FRP tube (UHPCFFT) column system was developed and its cyclic behavior was studied. The proposed steel-free UHPCFFT column showed much higher strength and stiffness, with a reasonable ductility, as compared to its conventional reinforced concrete (RC) counterpart. Using the results of the first phase of column tests, a second series of UHPCFFT columns were made and studied under pseudo-static loading to study the effect of column

  18. Modeling continuous-fiber reinforced polymer composites for exploration of damage tolerant concepts

    NASA Astrophysics Data System (ADS)

    Matthews, Peter J.

    This work aims to improve the predictive capability for fiber-reinforced polymer matrix composite laminates using the finite element method. A new tool for modeling composite damage was developed which considers important modes of failure. Well-known micromechanical models were implemented to predict material values for material systems of interest to aerospace applications. These generated material values served as input to intralaminar and interlaminar damage models. A three-dimensional in-plane damage material model was implemented and behavior verified. Deficiencies in current state-of-the-art interlaminar capabilities were explored using the virtual crack closure technique and the cohesive zone model. A user-defined cohesive element was implemented to discover the importance of traction-separation material constitutive behavior. A novel method for correlation of traction-separation parameters was created. This new damage modeling tool was used for evaluation of novel material systems to improve damage tolerance. Classical laminate plate theory was used in a full-factorial study of layerwise-hybrid laminates. Filament-wound laminated composite cylindrical shells were subjected to quasi-static loading to validate the finite element computational composite damage model. The new tool for modeling provides sufficient accuracy and generality for use on a wide-range of problems.

  19. Strain monitoring of bismaleimide composites using embedded microcavity sensor

    NASA Astrophysics Data System (ADS)

    Kaur, Amardeep; Anandan, Sudharshan; Yuan, Lei; Watkins, Steve E.; Chandrashekhara, K.; Xiao, Hai; Phan, Nam

    2016-03-01

    A type of extrinsic Fabry-Perot interferometer (EFPI) fiber optic sensor, i.e., the microcavity strain sensor, is demonstrated for embedded, high-temperature applications. The sensor is fabricated using a femtosecond (fs) laser. The fs-laser-based fabrication makes the sensor thermally stable to sustain operating temperatures as high as 800°C. The sensor has low sensitivity toward the temperature as compared to its response toward the applied strain. The performance of the EFPI sensor is tested in an embedded application. The host material is carbon fiber/bismaleimide (BMI) composite laminate that offer thermally stable characteristics at high ambient temperatures. The sensor exhibits highly linear response toward the temperature and strain. Analytical work done with embedded optical-fiber sensors using the out-of-autoclave BMI laminate was limited until now. The work presented in this paper offers an insight into the strain and temperature interactions of the embedded sensors with the BMI composites.

  20. Bismaleimide resins for flame resistant honeycomb sandwich panels

    NASA Technical Reports Server (NTRS)

    Stenzenberger, H. D.

    1978-01-01

    Bismaleimide resins are prime candidates for nonflammable aircraft interior panels. Three resin types with different structures and processing characteristics were formulated. Resin M 751 was used to fabricate 100 kg of glass fabric prepregs which were used for the preparation of face sheets for honeycomb sandwich panels. Prepreg characteristics and curing cycles for laminate fabrication are provided. In order to advance beyond the current solvent resin technology for fibre and fabric impregnation, a hot melt solvent-less resin system was prepared and characterized. Preliminary tests were performed to develop a wet bonding process for the fabrication of advanced sandwich honeycomb panels by use of polybismaleimide glass fabric face sheets and polybismaleimide Nomex honeycomb core. B-stage material was used for both the core and the face sheet, providing flatwise tensile properties equivalent to those obtained by the state-of-the-art 3-step process which includes an epoxy adhesive resin.

  1. Solvent-based self-healing approaches for fiber-reinforced composites

    NASA Astrophysics Data System (ADS)

    Jones, Amanda R.

    Damage in composite materials spans many length scales and is often difficult to detect or costly to repair. The incorporation of self-healing functionality in composite materials has the potential to greatly extend material lifetime and reliability. Although there has been remarkable progress in self-healing polymers over the past decade, self-repair in fiber-reinforced composite materials presents significant technical challenges due to stringent manufacturing and performance requirements. For high performance, fiber-reinforced composites, the self-healing components need to survive high temperature processing, reside in matrix interstitial regions to retain a high fiber volume fraction, and have minimal impact on the mechanical properties of the host material. This dissertation explores several microencapsulated solvent-based self-healing approaches for fiber-reinforced composites at the fiber/ matrix interface size scale as well as matrix cracking. Systems are initially developed for room temperature cured epoxies/ glass fiber interfaces and successfully transitioned to carbon fibers and high temperature-cured, thermoplastic-toughened matrices. Full recovery of interfacial bond strength after complete fiber/matrix debonding is achieved with a microencapsulated solvent-based healing chemistry. The surface of a glass fiber is functionalized with microcapsules containing varying concentrations of reactive epoxy resin and ethyl phenyl acetate (EPA) solvent. Microbond specimens consisting of a single fiber and a microdroplet of epoxy are cured at 35°C, tested, and the interfacial shear strengths (IFSS) during the initial (virgin) debonding and subsequent healing events are measured. Debonding of the fiber/matrix interface ruptures the capsules, releasing resin and solvent into the crack plane. The solvent swells the matrix, initiating transport of residual amine functionality for further curing with the epoxy resin delivered to the crack plane. Using a resin

  2. An overview of self-consistent methods for fiber-reinforced composites

    NASA Technical Reports Server (NTRS)

    Gramoll, Kurt C.; Freed, Alan D.; Walker, Kevin P.

    1991-01-01

    The Walker et al. (1989) self-consistent method to predict both the elastic and the inelastic effective material properties of composites is examined and compared with the results of other self-consistent and elastically based solutions. The elastic part of their method is shown to be identical to other self-consistent methods for non-dilute reinforced composite materials; they are the Hill (1965), Budiansky (1965), and Nemat-Nasser et al. (1982) derivations. A simplified form of the non-dilute self-consistent method is also derived. The predicted, elastic, effective material properties for fiber reinforced material using the Walker method was found to deviate from the elasticity solution for the v sub 31, K sub 12, and mu sub 31 material properties (fiber is in the 3 direction) especially at the larger volume fractions. Also, the prediction for the transverse shear modulus, mu sub 12, exceeds one of the accepted Hashin bounds. Only the longitudinal elastic modulus E sub 33 agrees with the elasticity solution. The differences between the Walker and the elasticity solutions are primarily due to the assumption used in the derivation of the self-consistent method, i.e., the strain fields in the inclusions and the matrix are assumed to remain constant, which is not a correct assumption for a high concentration of inclusions.

  3. Enhancing the mechanical properties of cement paste by growing in-situ fiber reinforcement during hydration

    NASA Astrophysics Data System (ADS)

    Constantinides, Margarita

    Efforts to improve the mechanical properties of concrete by modifying the cement paste matrix have focused entirely on strength enhancement. But the intrinsic brittleness of the cement paste matrix limits the possible improvement in the mechanical properties of concrete, and in particular the toughness of the material. Increasing the toughness of the cement paste matrix could lead to a reduction in flaw sensitivity by delaying unstable crack propagation. Consequently, the resistance of the material to cracking due to drying shrinkage, thermal shrinkage, expansive deterioration processes, and applied loads could increase considerably. The goal of this study was to grow in-situ fiber reinforcement in cement paste, a technique never before applied to cement-based materials, to enhance the toughness of the material. Ettringite, an existing, fiber-like hydration product was selected as the fiber reinforcement. Ettringite met all the necessary criteria to act as reinforcement in cement paste: adequate distribution in the matrix; adjustable volume fraction, aspect ratio and size; high stiffness along the fiber length; and finally compatibility with existing hydration products. Alkali-free accelerators were selected as the admixtures used to grow the ettringite in the cement paste. X-ray diffraction and scanning electron microscopy experiments were performed to study the volume fraction, distribution, size, and morphology of the ettringite crystals in the cement paste matrix (both plain and accelerator-containing). Mechanical tests (compression, splitting tension, flexural, compact tension) were used to evaluate the effect of the accelerators on the strength and toughness of cement paste. Microindentations on the surface of the cement paste matrix were performed to study the morphology of the cracks and the toughening mechanisms taking place. Through the characterization tests we identified that while more ettringite forms with the addition of the alkali-free accelerators

  4. Method for Forming Fiber Reinforced Composite Bodies with Graded Composition and Stress Zones

    NASA Technical Reports Server (NTRS)

    Singh, Mrityunjay (Inventor); Levine, Stanley R. (Inventor); Smialek, James A. (Inventor)

    1999-01-01

    A near-net, complex shaped ceramic fiber reinforced silicon carbide based composite bodies with graded compositions and stress zones is disclosed. To provide the composite a fiber preform is first fabricated and an interphase is applied by chemical vapor infiltration, sol-gel or polymer processes. This first body is further infiltrated with a polymer mixture containing carbon, and/or silicon carbide, and additional oxide, carbide, or nitride phases forming a second body. One side of the second body is spray coated or infiltrated with slurries containing high thermal expansion and oxidation resistant. crack sealant phases and the other side of this second body is coated with low expansion phase materials to form a third body. This third body consisting of porous carbonaceous matrix surrounding the previously applied interphase materials, is then infiltrated with molten silicon or molten silicon-refractory metal alloys to form a fourth body. The resulting fourth body comprises dense composites consisting of fibers with the desired interphase which are surrounded by silicon carbide and other second phases materials at the outer and inner surfaces comprising material of silicon, germanium, refractory metal suicides, borides, carbides, oxides, and combinations thereof The resulting composite fourth body has different compositional patterns from one side to the other.

  5. Tensile properties of nicalon fiber-reinforced carbon following aerospace turbine engine testing

    NASA Astrophysics Data System (ADS)

    Pierce, J. L.; Zawada, L. P.; Srinivasan, R.

    2003-06-01

    The durability of coated Nicalon silicon carbide fiber-reinforced carbon (SiC/C) as the flap and seal exhaust nozzle components in a military aerospace turbine engine was studied. Test specimens machined from both a flap and a seal component were tested for residual strength following extended ground engine testing on a General Electric F414 afterburning turbofan engine. Although small amounts of damage to the protective exterior coating were identified on each component following engine testing, the tensile strengths were equal to the as-fabricated tensile strength of the material. Differences in strength between the two components and variability within the data sets could be traced back to the fabrication process using witness coupon test data from the manufacturer. It was also observed that test specimens machined transversely across the flap and seal components were stronger than those machined along the length. The excellent retained strength of the coated SiC/C material after extended exposure to the severe environment in the afterburner exhaust section of an aerospace turbofan engine has resulted in this material being selected as the baseline material for the F414 exhaust nozzle system.

  6. Intrinsic signatures of polymer based fiber reinforced composite structures: An ultrasonic approach

    SciTech Connect

    Good, M.S.; Hansen, N.H.; Heasler, P.G.; Undem, H.A.; Fuller, J.L.; Skorpik, J.R.

    1993-09-01

    Combination of ultrasound, image comparison, and statistical analysis provide a method for acquiring a subsurface, intrinsic signature from polymer based, fiber-reinforced composites. Although materials properties are carefully controlled, localized fluctuations in the macrostructure and microstructure permit a basis for ultrasound and other NDE methods to read intrinsic signatures from a material. Under ideal conditions where a material signature is stable and has sufficient spatial features as a signature, an error rate on the order of one-out-of-a-million is feasible. A conclusion of an independent functional test performed on the laboratory prototype as it existed in June 1991 is that the system proved effective as a proof-of-concept system. An issue raised by the independent evaluation is that system performance is still at risk of factors relating to signature stability, particularly moisture absorption and material creep. System improvements made to mitigate noise sources identified by the independent evaluation include (1) implementation of a 3.0 {minus} 4.5 {mu}S software gate, (2) use of a RMS amplitude instead of the gated peak amplitude, and (3) optional use of a suction cup holder to facilitate reader alignment and scan consistency.

  7. Processing and Characterization of Basalt Fiber Reinforced Ceramic Composites for High Temperature Applications Using Polymer Precursors

    NASA Technical Reports Server (NTRS)

    Cox, Sarah; Lui, Donovan; Gou, Jihua

    2014-01-01

    The development of high temperature structural composite materials has been very limited due to the high cost of the materials and the processing needed. Ceramics can take much higher temperatures, but they are difficult to produce and form in bulk volumes. Polymer Derived Ceramics (PDCs) begin as a polymer matrix, allowing a shape to be formed, to be cured, and be pyrolized in order to obtain a ceramic with the associated thermal and mechanical properties. The two PDCs used in this development are polysiloxane and polycarbosilane. Polysiloxanes contain a silicon oxycarbide backbone when pyrolized up to 1000degC. Polycarbosilane, an organosilicon polymer, contain a silicon-carbon backbone; around 1200degC, -SiC begins to crystallize. The use of basalt in structural and high temperature applications has been under development for over 50 years, yet there has been little published research on the incorporation of basalt fibers as a reinforcement in composites. Basalt is a naturally occurring material found in volcanic rock. Continuous basalt fiber reinforced PDCs have been fabricated and tested for the applicability of this composite system as a high temperature structural composite material. Testing for this included thermal and mechanical testing per ASTM standard tests.

  8. Processing and Characterization of Basalt Fiber Reinforced Ceramic Composites for High Temperature Applications Using Polymer Precursors

    NASA Technical Reports Server (NTRS)

    Cox, Sarah B.; Lui, Donovan; Gou, Jihua

    2014-01-01

    The development of high temperature structural composite materials has been very limited due to the high cost of the materials and the processing needed. Ceramics can take much higher temperatures, but they are difficult to produce and form in bulk volumes. Polymer Derived Ceramics (PDCs) begin as a polymer matrix, allowing a shape to be formed and cured and then to be pyrolized in order to obtain a ceramic with the associated thermal and mechanical properties. The two PDCs used in this development are polysiloxane and polycarbosilane. Polysiloxanes contain a silicon oxycarbide backbone when pyrolized up to 1000C. Polycarbosilane, an organosilicon polymer, contain a silicon-carbon backbone; around 1200C, beta-SiC begins to crystallize. The use of basalt in structural and high temperature applications has been under development for over 50 years, yet there has been little published research on the incorporation of basalt fibers as a reinforcement in composites. Basalt is a naturally occurring material found in volcanic rock. Continuous basalt fiber reinforced PDCs have been fabricated and tested for the applicability of this composite system as a high temperature structural composite material. Thermal and mechanical testing includes oxyacetylene torch testing and three point bend testing.

  9. Processing and Characterization of Basalt Fiber Reinforced Ceramic Composites for High Temperature Applications Using Polymer Precursors

    NASA Technical Reports Server (NTRS)

    Cox, Sarah B.; Lui, Donovan; Wang, Xin; Gou, Jihua

    2014-01-01

    The development of high temperature structural composite materials has been very limited due to the high cost of the materials and the processing needed. Ceramics can take much higher temperatures, but they are difficult to produce and form in bulk volumes. Polymer Derived Ceramics (PDCs) begin as a polymer matrix, allowing a shape to be formed and cured and then to be pyrolized in order to obtain a ceramic with the associated thermal and mechanical properties. The two PDCs used in this development are polysiloxane and polycarbosilane. Polysiloxanes contain a silicon oxycarbide backbone when pyrolized up to 1000 deg C. Polycarbosilane, an organosilicon polymer, contain a silicon-carbon backbone; around 1200 deg C, Beta-SiC begins to crystallize. The use of basalt in structural and high temperature applications has been under development for over 50 years, yet there has been little published research on the incorporation of basalt fibers as a reinforcement in composites. Basalt is a naturally occurring material found in volcanic rock. Continuous basalt fiber reinforced PDCs have been fabricated and tested for the applicability of this composite system as a high temperature structural composite material. Thermal and mechanical testing includes oxyacetylene torch testing and three point bend testing.

  10. Process Optimization of Bismaleimide (BMI) Resin Infused Carbon Fiber Composite

    NASA Technical Reports Server (NTRS)

    Ehrlich, Joshua W.; Tate, LaNetra C.; Cox, Sarah B.; Taylor, Brian J.; Wright, M. Clara; Caraccio, Anne J.; Sampson, Jeffery W.

    2013-01-01

    Bismaleimide (BMI) resins are an attractive new addition to world-wide composite applications. This type of thermosetting polyimide provides several unique characteristics such as excellent physical property retention at elevated temperatures and in wet environments, constant electrical properties over a vast array of temperature settings, and nonflammability properties as well. This makes BMI a popular choice in advance composites and electronics applications [I]. Bismaleimide-2 (BMI-2) resin was used to infuse intermediate modulus 7 (IM7) based carbon fiber. Two panel configurations consisting of 4 plies with [+45deg, 90deg]2 and [0deg]4 orientations were fabricated. For tensile testing, a [90deg]4 configuration was tested by rotating the [0deg]4 configirration to lie orthogonal with the load direction of the test fixture. Curing of the BMI-2/IM7 system utilized an optimal infusion process which focused on the integration of the manufacturer-recommended ramp rates,. hold times, and cure temperatures. Completion of the cure cycle for the BMI-2/IM7 composite yielded a product with multiple surface voids determined through visual and metallographic observation. Although the curing cycle was the same for the three panellayups, the surface voids that remained within the material post-cure were different in abundance, shape, and size. For tensile testing, the [0deg]4 layup had a 19.9% and 21.7% greater average tensile strain performance compared to the [90deg]4 and [+45deg, 90deg, 90deg,-45degg] layups, respectively, at failure. For tensile stress performance, the [0deg]4 layup had a 5.8% and 34.0% greater average performance% than the [90deg]4 and [+45deg, 90deg, 90deg,-45deg] layups.

  11. Interfacial studies in fiber-reinforced thermoplastic-matrix composites

    SciTech Connect

    Brady, R.L.

    1989-01-01

    The major theme of this dissertation is structure/property relationships in fiber-reinforced thermoplastic-matrix composites. Effort has been focused on the interface: interfacial crystallization and fiber/matrix adhesion. Included are investigations on interfacial nucleation and morphology, measurement of fiber/matrix adhesion, effects of interfacial adsorption and crystallization on fiber/matrix adhesion, and composites reinforced with thermotropic liquid crystal copolyester fibers. Crystallization of a copolyester and polybutylene terephthalate with glass, carbon, or aramid fibers has been studied with regard to interfacial morphology. Techniques employed included hot-stage optical microscopy and differential scanning calorimetry. Nucleation by the fibers was found to be a general phenomenon. Morphology could be varied by changing the cooling rate. In order to better monitor fiber /matrix adhesion, a buckled plate test has been developed. The test measures transverse toughness as the parameter characterizing interfacial adhesion in unidirectional, continuous-fiber composites. The test is simple to perform yet has advantages over other interfacial evaluation techniques. The buckled plate test was found to be a sensitive measure of fiber/matrix adhesion. The buckled plate test has been used along with the transverse tensile test to examine how interfacial adsorption and crystallization affect fiber/matrix adhesion in polycarbonate/carbon fiber composites. Adsorption was found to be of primary importance in developing adhesion, while crystallization is a secondary effect. The toughness data have been fit successfully for annealing time and temperature dependence. The dependence of adsorption and transverse toughness on matrix molecular weight was found to be large, with higher molecular weights adsorbing more effectively.

  12. Fiber-Reinforced Epoxy Composites and Methods of Making Same Without the Use of Oven or Autoclave

    NASA Technical Reports Server (NTRS)

    Barnell, Thomas J. (Inventor); Rauscher, Michael D. (Inventor); Stienecker, Rick D. (Inventor); Nickerson, David M. (Inventor); Tong, Tat H. (Inventor)

    2016-01-01

    Method embodiments for producing a fiber-reinforced epoxy composite comprise providing a mold defining a shape for a composite, applying a fiber reinforcement over the mold, covering the mold and fiber reinforcement thereon in a vacuum enclosure, performing a vacuum on the vacuum enclosure to produce a pressure gradient, insulating at least a portion of the vacuum enclosure with thermal insulation, infusing the fiber reinforcement with a reactive mixture of uncured epoxy resin and curing agent under vacuum conditions, wherein the reactive mixture of uncured epoxy resin and curing agent generates exothermic heat, and producing the fiber-reinforced epoxy composite having a glass transition temperature of at least about 100.degree. C. by curing the fiber reinforcement infused with the reactive mixture of uncured epoxy resin and curing agent by utilizing the exothermically generated heat, wherein the curing is conducted inside the thermally insulated vacuum enclosure without utilization of an external heat source or an external radiation source.

  13. Characterization of interphase environmental degradation at elevated temperature of fiber-reinforced TMCs

    NASA Astrophysics Data System (ADS)

    Matikas, Theodore E.

    2009-03-01

    Fiber reinforced metallic composite materials are being considered for a number of applications because of their attractive mechanical properties as compared to monolithic metallic alloys. An engineered interphase, including the bond strength between the composite's constituents, contributes to a large extent to the improvement of strength and stiffness properties of this class of materials. However, in high temperature applications, where combination of cyclic loading with environmental effects is expected, consideration should be given to interphase degradation, especially in the vicinity of stress risers, such as notches and holes. The applicability of damage tolerance analysis in structural components made of titanium matrix composite materials designed to operate under high temperature environments would depend on the availability of adequate characterization methods for the evaluation of interfacial degradation. The objective of this work is to provide a basic understanding of interfacial degradation mechanisms due to oxidation in environmentally exposed titanium-based composites subjected to cyclic stresses. A nondestructive method has been developed enabling highresolution monitoring of interfacial damage initiation and accumulation as well as surface/subsurface cracking behavior during interrupted fatigue tests. This nondestructive technique is based on surface acoustic wave propagation in the composites and can detect minute changes in elastic properties of the interfacial region due to elevated temperatures as well as oxygen effects.

  14. Mechanical properties of resin glass fiber-reinforced abutment in comparison to titanium abutment

    PubMed Central

    Andreasi Bassi, Mirko; Bedini, Rossella; Pecci, Raffella; Ioppolo, Pietro; Lauritano, Dorina; Carinci, Francesco

    2015-01-01

    Purpose: So far, definitive implant abutments have been performed with high elastic modulus materials, which prevented any type of shock absorption of the chewing loads and as a consequence, the protection of the bone-fixture interface. This is particularly the case when the esthetic restorative material chosen is ceramic rather than composite resin. The adoption of an anisotropic abutment, characterized by an elastic deformability, could allow decreasing the impulse of chewing forces transmitted to the crestal bone. Materials and Methods: According to research protocol, the mechanical resistance to cyclical load was evaluated in a tooth-colored fiber-reinforced abutment (TCFRA) prototype and compared to that of a titanium abutment (TA), thus eight TCFRAs and eight TAs were adhesively cemented on as many titanium implants. The swinging that the two types of abutments showed during the application of sinusoidal load was also analyzed. Results: In the TA group, both fracture and deformation occurred in 12.5% of samples while debonding 62.5%. In the TCFRA group, only debonding was present in 37.5% of samples. In comparison to the TAs, the TCFRAs exhibited a greater swinging during the application of sinusoidal load. In the TA group, the extrusion prevailed, whereas in the TCFRA group, the intrusion was more frequent. Conclusion: The greater elasticity of TCFRA to the flexural load allows absorbing part of the transversal load applied on the fixture during the chewing function, thus reducing the stress on the bone-implant interface. PMID:26229266

  15. Effect of fiber reinforcement on thermo-oxidative stability and mechanical properties of polymer matrix composites

    NASA Technical Reports Server (NTRS)

    Bowles, K. J.

    1992-01-01

    A number of studies have investigated the thermooxidative behavior of polymer matrix composites. Two significant observations have been made from these research efforts: (1) fiber reinforcement has a significant effect on composite thermal stability; and (2) geometric effects must be considered when evaluating thermal aging data. The polyimide PMR-15 was the matrix material used in these studies. The control composite material was reinforced with Celion 6000 graphite fiber. T-4OR graphite fibers, along with some very stable ceramic fibers were selected as reinforcing fibers because of their high thermal stability. The ceramic fibers were Nicalon (silicon carbide) and Nextel 312 (alumina-silica-boron oxide). The mechanical properties of the two graphite fiber composites were significantly different, probably owing to variations in interfacial bonding between the fibers and the polyimide matrix. Three oxidation mechanisms were observed: (1) the preferential oxidation of the Celion 6000 fiber ends at cut surfaces, leaving a surface of matrix material with holes where the fiber ends were originally situated; (2) preferential oxidation of the composite matrix; and (3) interfacial degradation by oxidation. The latter two mechanisms were also observed on fiber end cut surfaces. The fiber and interface attacks appeared to initiate interfiber cracking along these surfaces.

  16. Effect of γ irradiation on the properties of basalt fiber reinforced epoxy resin matrix composite

    NASA Astrophysics Data System (ADS)

    Li, Ran; Gu, Yizhuo; Yang, Zhongjia; Li, Min; Wang, Shaokai; Zhang, Zuoguang

    2015-11-01

    Gamma-ray (γ-ray) irradiation is a crucial reason for the aging in materials used for nuclear industry. Due to high specific strength and stiffness, light weight and good corrosion resistance, fiber reinforced composites are regarded as an alternative of traditional materials used on nuclear facilities. In this study, basalt fiber (BF)/AG80 epoxy composite laminates were fabricated by autoclave process and treated with 60Co gamma irradiation dose up to 2.0 MGy. Irradiation induced polymer chain scission and oxidation of AG80 resin were detected from physical and chemical analysis. The experimental results show that the tensile and flexural performances of irradiated BF/AG80 composite maintain stable and have a low amplitude attenuation respectively, and the interlaminar shear strength has increased from irradiation dose of 0-1.5 MGy. Furthermore, the comparison between the studied BF composite and reported polymer and composite materials was done for evaluating the γ resistance property of BF composite.

  17. Effect of fiber reinforcements on thermo-oxidative stability and mechanical properties of polymer matrix composites

    NASA Technical Reports Server (NTRS)

    Bowles, Kenneth J.

    1991-01-01

    A number of studies have investigated the thermo-oxidative behavior of polymer matrix composites. Two significant observations have been made from these research efforts: (1) fiber reinforcement has a significant effect on composite thermal stability; and (2) geometric effects must be considered when evaluating thermal aging data. A compilation of some results from these studies is presented, and this information shows the influence of the reinforcement fibers on the oxidative degradation of various polymer matrix composites. The polyimide PMR-15 was the matrix material that was used in these studies. The control composite material was reinforced with Celion 6000 graphite fiber. T-40R graphite fibers, along with some very stable ceramic fibers were selected as reinforcing fibers because of their high thermal stability. The ceramic fibers were Nicalon (silicon carbide) and Nextel 312 (alumina-silica-boron oxide). The mechanical properties of the two graphite fiber composites were significantly different, probably owing to variations in interfacial bonding between the fibers and the polyimide matrix. The Celion 6000/PMR-15 bond is very tight but the T-40/PMR-15 bond is less tight. Three oxidation mechanisms were observed: (1) the preferential oxidation of the Celion 6000 fiber ends at cut surfaces, leaving a surface of matrix material with holes where the fiber ends were originally situated; (2) preferential oxidation of the composite matrix; and (3) interfacial degradation by oxidation. The latter two mechanisms were also observed on fiber end cut surfaces. The fiber and interface attacks appeared to initiate interfiber cracking along these surfaces.

  18. Stress and strength analysis of fiber reinforced plastic pipe tees with reinforcement

    SciTech Connect

    Wei, Z.; Widera, G.E.O.; Xue, M.

    1996-12-01

    In this paper, a stress and strength analysis of fiber reinforced plastic (FRP) pipe tees with reinforcement by use of 3-D finite element method is presented. Wilson`s incompatible elements and the 16-node 3-D element with relative degrees of freedom have been employed to carry out the analysis. The reliability of the program is also investigated. Two reinforcing methods, pad and compact reinforcement, are investigated. The fact that the properties and principal directions of the materials of the two intersecting pipes and the reinforcement are different has been taken into account in the analysis. The continuity of stress and strain fields at the intersecting surface of two different materials is considered in the post processing of the FEM results. The results show that the stress concentration in a FRP pipe intersection without reinforcement (r/R = 0.4--0.7) is significant. A reasonable design can be obtained by considering both stress fields and the orthotropic strength parameters of the materials. The in-plane shear stress may be the controlling factor because of the relatively low shear strength of most composites. Use of either reinforcing method does not change the location of the maximum tensile stress and the maximum shear stress, and both alleviate the stress concentration at the intersection. It is shown that the compact reinforcing method is more effective than the pad one. The larger the reinforcing area of the compact reinforcing method, the smaller the stress concentration factor, but the lower the rate of reduction.

  19. Glass fiber reinforced plastics within the fringe and flexure tracker of LINC-NIRVANA

    NASA Astrophysics Data System (ADS)

    Smajic, Semir; Eckart, A.; Horrobin, M.; Lindhorst, B.; Pott, J.-U.; Rauch, C.; Rost, S.; Straubmeier, C.; Tremou, E.; Wank, I.; Zuther, J.

    2012-07-01

    The Fringe and Flexure Tracking System (FFTS) is meant to monitor and correct atmospheric piston varia­ tion and instrumental vibrations and flexure during near-infrared interferometric image acquisition of LING­ NIRVANA. In close work with the adaptive optics system the FFTS enables homothetic imaging for the Large Binocular Telescope. One of the main problems we had to face is the connection between the cryogenic upper part of the instrument, e.g. detector head, and the lower ambient temperature part. In this ambient temperature part the moving stages are situated that move the detector head in the given field of view (FOV). We show how we solved this problem using the versatile material glass fiber reinforced plastics (GFRP's) and report in what way this material can be worked. We discuss in detail the exquisite characteristics of this material which we use to combine the cryogenic and ambient environments to a fully working system. The main characteristics that we focus on are the low temperature conduction and the tensile strength of the GFRP's. The low temperature conduction is needed to allow for a low heat-exchange between the cryogenic and ambient part whereas the tensile strength is needed to support heavy structures like the baffle motor and to allow for a minimum of flexure for the detector head. Additionally, we discuss the way we attached the GFRP to the remaining parts of the FFTS using a two component encapsulant.

  20. Simulation of crack propagation in fiber-reinforced concrete by fracture mechanics

    SciTech Connect

    Zhang Jun; Li, Victor C

    2004-02-01

    Mode I crack propagation in fiber-reinforced concrete (FRC) is simulated by a fracture mechanics approach. A superposition method is applied to calculate the crack tip stress intensity factor. The model relies on the fracture toughness of hardened cement paste (K{sub IC}) and the crack bridging law, so-called stress-crack width ({sigma}-{delta}) relationship of the material, as the fundamental material parameters for model input. As two examples, experimental data from steel FRC beams under three-point bending load are analyzed with the present fracture mechanics model. A good agreement has been found between model predictions and experimental results in terms of flexural stress-crack mouth opening displacement (CMOD) diagrams. These analyses and comparisons confirm that the structural performance of concrete and FRC elements, such as beams in bending, can be predicted by the simple fracture mechanics model as long as the related material properties, K{sub IC} and ({sigma}-{delta}) relationship, are known.

  1. Analysis of surface damage in retrieved carbon fiber-reinforced and plain polyethylene tibial components from posterior stabilized total knee replacements.

    PubMed

    Wright, T M; Rimnac, C M; Faris, P M; Bansal, M

    1988-10-01

    The performance of carbon fiber-reinforced ultra-high molecular weight polyethylene was compared with that of plain (non-reinforced) polyethylene on the basis of the damage that was observed on the articulating surfaces of retrieved tibial components of total knee prostheses. Established microscopy techniques for subjectively grading the presence and extent of surface damage and the histological structure of the surrounding tissues were used to evaluate twenty-six carbon fiber-reinforced and twenty plain polyethylene components that had been retrieved after an average of twenty-one months of implantation. All of the tibial components were from the same design of total knee replacement. The two groups of patients from whom the components were retrieved did not differ with regard to weight, the length of time that the component had been implanted, the radiographic position and angular alignment of the component, the original diagnosis, or the reason for removal of the component. The amounts and types of damage that were observed did not differ for the two materials. For both materials, the amount of damage was directly related to the length of time that the component had been implanted. The histological appearance of tissues from the area around the component did not differ for the two materials, except for the presence of fragments of carbon fiber in many of the samples from the areas around carbon fiber-reinforced components. PMID:3053722

  2. Role of the matrix precipitation and interface dislocations on the nanostability of an Al-4w%Cu-Al{sub 2}O{sub 3} fiber-reinforced composite

    SciTech Connect

    Sgobba, S.; Parrini, L.; Kuenzi, H.U.; Ilschner, B.

    1994-12-31

    In many industrial applications the elastic and dimensional stability of materials is required at a nanometric scale. High resolution laser interferometry and mechanical spectroscopy have been employed to measure low temperature creep of the short-fiber reinforced composite Al-4w%Cu-Al{sub 2}O{sub 3}. The typical strain resolution of the laser interferometer is 10{sup {minus}10}. Fiber reinforcement generally increases the dislocation density in the metal matrix; in parallel, damping is enhanced. The models relating the dislocation structures at the precipitate-matrix and fiber-matrix interfaces to the damping behavior are discussed.

  3. Strain-rate dependence of the compressive properties of normal and carbon-fiber-reinforced bone cement.

    PubMed

    Saha, S; Pal, S

    1983-11-01

    Normal and carbon-fiber-reinforced (1 wt. %) bone cement samples were tested in compression at various strain rates. Both the compressive strength and proportional limit increased in general with increasing strain rate. Similar strain-rate sensitivity was also shown by the carbon-fiber-reinforced bone cement. The mechanical properties, namely the modulus of elasticity, the proportional limit, and the compressive strength of the carbon-fiber-reinforced bone cement showed highly significant positive correlations with the strain rate. PMID:6654926

  4. Preliminary investigation on the suitablity of using fiber reinforced concrete in the construction of a hazardous waste disposal vessel

    SciTech Connect

    Ramey, M.R.; Daie-e, G.

    1988-07-01

    There are certain hazardous wastes that must be contained in an extremely secure vessel for transportation and disposal. The vessel, among other things, must be able to withstand relatively large impacts without rupturing. Such containment vessels therefore must be able to absorb substantial amounts of energy during an impact and still perform their function. One of the impacts that the vessel must withstand is a 30-foot fall onto an unyielding surface. For some disposal scenarios it is proposed to encase the waste in a steel enclosure which is to be surrounded by a thick layer of concrete which, in turn, is encased by a relatively thin steel shell. Tests on concrete in compression and flexure, including static, dynamic and impact tests, have shown that low modulus concretes tend to behave in a less brittle manner than higher modulus concretes. Tests also show that fiber reinforced concretes have significantly greater ductility, crack propagation resistance and toughness than conventional concretes. Since it is known that concrete is a reasonably brittle material, it is necessary to do impact tests on sample containment structures consisting of thin-walled metal containers having closed ends which are filled with concrete, grout, or fiber reinforced concrete. This report presents the results of simple tests aimed at observing the behavior of sample containment structures subjected to impacts due to a fall from 30 feet. 8 figs., 4 tabs.

  5. Application of headed studs in steel fiber reinforced cementitious composite slab of steel beam-column connection

    NASA Astrophysics Data System (ADS)

    Yao, Cui; Nakashima, Masayoshi

    2012-03-01

    Steel fiber reinforced cementitous composites (SFRCC) is a promising material with high strength in both compression and tension compared with normal concrete. The ductility is also greatly improved because of 6% volume portion of straight steel fibers. A steel beam-column connection with Steel fiber reinforced cementitous composites (SFRCC) slab diaphragms is proposed to overcome the damage caused by the weld. The push-out test results suggested that the application of SFRCC promises larger shear forces transferred through headed studs allocated in a small area in the slab. Finite element models were developed to simulate the behavior of headed studs. The failure mechanism of the grouped arrangement is further discussed based on a series of parametric analysis. In the proposed connection, the SFRCC slab is designed as an exterior diaphragm to transfer the beam flange load to the column face. The headed studs are densely arranged on the beam flange to connect the SFRCC slab diaphragms and steel beams. The seismic performance and failure mechanism of the SFRCC slab diaphragm beam-column connection were investigated based on the cyclic loading test. Beam hinge mechanism was achieved at the end of the SFRCC slab diaphragm by using sufficient studs and appropriate rebars in the SFRCC slab.

  6. Influence of laminate sequence and fabric type on the inherent acoustic nonlinearity in carbon fiber reinforced composites.

    PubMed

    Chakrapani, Sunil Kishore; Barnard, Daniel J; Dayal, Vinay

    2016-05-01

    This paper presents the study of influence of laminate sequence and fabric type on the baseline acoustic nonlinearity of fiber-reinforced composites. Nonlinear elastic wave techniques are increasingly becoming popular in detecting damage in composite materials. It was earlier observed by the authors that the non-classical nonlinear response of fiber-reinforced composite is influenced by the fiber orientation [Chakrapani, Barnard, and Dayal, J. Acoust. Soc. Am. 137(2), 617-624 (2015)]. The current study expands this effort to investigate the effect of laminate sequence and fabric type on the non-classical nonlinear response. Two hypotheses were developed using the previous results, and the theory of interlaminar stresses to investigate the influence of laminate sequence and fabric type. Each hypothesis was tested by capturing the nonlinear response by performing nonlinear resonance spectroscopy and measuring frequency shifts, loss factors, and higher harmonics. It was observed that the laminate sequence can either increase or decrease the nonlinear response based on the stacking sequence. Similarly, tests were performed to compare unidirectional fabric and woven fabric and it was observed that woven fabric exhibited a lower nonlinear response compared to the unidirectional fabric. Conjectures based on the matrix properties and interlaminar stresses were used in an attempt to explain the observed nonlinear responses for different configurations. PMID:27250126

  7. Numerical simulation of combustion effects during laser processing of carbon fiber reinforced plastics

    NASA Astrophysics Data System (ADS)

    Ohkubo, Tomomasa; Tsukamoto, Masahiro; Sato, Yuji

    2016-03-01

    We applied the finite difference method to a numerical simulation of material removal in the laser ablation of a carbon fiber reinforced plastic (CFRP). Although a few theoretical and numerical studies of heat-affected zone (HAZ) formation have been reported, there has been no report describing heat generation due to oxidization of the materials. It is important to consider combustion effects when discussing the generation of a HAZ in order to improve the quality of CFRP cutting by laser. To develop a new calculation model that includes the effects of the combustion of each element of the CFRP, thermogravimetric analysis (TGA) and differential thermal analysis (DTA) were performed for CFRP in air. We succeeded in qualitatively simulating the generation of a HAZ, including the effects of combustion, using data obtained by TGA and DTA. Therefore, not only thermal conductivity, but also combustion effects, should be considered when discussing how a HAZ is generated and in order to improve the cutting quality of CFRPs in laser processing.

  8. Feature guided waves (FGW) in fiber reinforced composite plates with 90° transverse bends

    NASA Astrophysics Data System (ADS)

    Yu, Xudong; Ratassepp, Madis; Fan, Zheng; Manogharan, Prabhakaran; Rajagopal, Prabhu

    2016-02-01

    Fiber reinforced composite materials have been increasingly used in high performance structures such as aircraft and large wind turbine blades. 90◦ composite bends are common in reinforcing structural elements, which are prone to defects such as delamination, crack, fatigue, etc. Current techniques are based on local inspection which makes the whole bend area scanning time consuming and tedious. This paper explores the feasibility of using feature guided waves (FGW) for rapid screening of 90◦ composite laminated bends. In this study, the behavior of the bend-guided wave in the anisotropic composite material is investigated through modal studies by applying the Semi-Analytical Finite Element (SAFE) method, also 3D Finite Element (FE) simulations are performed to visualize the results and to obtain cross validation. To understand the influence of the anisotropy, three-dimensional dispersion surfaces of the guided modes in flat laminated plates are obtained, showing the dependence of the phase velocity with the frequency and the fiber orientation. S H0-like and S 0-like bend-guided modes are identified with energy concentrated in the bend region, limiting energy radiation into adjacent plates and thus achieving increased inspection length. Finally, parametric studies are carried out to further investigate the properties of these two bend-guided modes, demonstrating the variation of the group velocity, the energy concentration, and the attenuation with the frequency.

  9. Fiber-reinforced composite analysis using optical coherence tomography after mechanical and thermal cycling

    NASA Astrophysics Data System (ADS)

    Kyotoku, B. B. C.; Braz, A. K. S.; Braz, R.; Gomes, A. S. L.

    2007-02-01

    Fiber-reinforced composites are new materials which have been used for a variety of dental applications, including tooth splinting, replacement of missing teeth, treatment of dental emergencies, reinforcement of resin provisional fixed prosthodontic restorations, orthodontic retention, and other clinical applications. Different fiber types are available, but little clinical information has been disseminated. The traditional microscopy investigation, most commonly used to study this material, is a destructive technique, which requires specimen sectioning and are essentially surface measurements. On the basis of these considerations, the aim of this research is to analyze the interior of a dental sample reinforced with fiber after a mechanical and thermal cycling to emulate oral conditions using optical coherence tomography (OCT). The device we are using is a home built Fourier domain OCT working at 800 nm with 6 μm resolution. The results are compared with microscopy images to validate OCT as a working method. In long term, fractures allow bacterial invasion provoking plaque and calculus formation that can cause caries and periodontal disease. Therefore, non invasive imaging of the bridge fiber enables the possibility of periodic clinical evaluation to ensure the patient health. Furthermore, OCT images can provide a powerful method for quantitative analysis of crack propagation, and can potentially be used for in vivo assessment.

  10. Microstructure and Mechanical Properties of Warm-Sprayed Titanium Coating on Carbon Fiber-Reinforced Plastic

    NASA Astrophysics Data System (ADS)

    Ganesan, Amirthan; Takuma, Okada; Yamada, Motohiro; Fukumoto, Masahiro

    2016-04-01

    Polymer materials are increasingly dominating various engineering fields. Recently, polymer-based composite materials' surface performances—in particular, surface in relative motion—have been improved markedly by thermal spray coating. Despite this recent progress, the deposition of high-strength materials—producing a coating thickness of the order of more than 500 μm—remains highly challenging. In the present work, a highly dense and thick titanium coating was successfully deposited onto the carbon fiber-reinforced plastic (CFRP) substrate using a newly developed high-pressure warm spray (WS) system. The coating properties, such as hardness (300 ± 20 HV) and adhesion strength (8.1 ± 0.5 MPa), were evaluated and correlated with the microstructures of the coating. In addition, a wipe-test and in situ particle velocity and temperature measurement were performed to validate the particle deposition behavior as a function of the nitrogen flow rate in the WS system. It was found that the microstructures, deposition efficiency, and mechanical properties of the coatings were highly sensitive to nitrogen flow rates. The coating porosity increased with increasing nitrogen flow rates; however, the highest density was observed for nitrogen flow rate of 1000 standard liters per minute (SLM) samples due to the high fraction of semi-molten particles in the spray stream.

  11. Self-monitoring fiber reinforced polymer strengthening system for civil engineering infrastructures

    NASA Astrophysics Data System (ADS)

    Jiang, Guoliang; Dawood, Mina; Peters, Kara; Rizkalla, Sami

    2008-03-01

    Fiber reinforced polymer (FRP) materials are currently used for strengthening civil engineering infrastructures. The strengthening system is dependant on the bond characteristics of the FRP to the external surface of the structure to be effective in resisting the applied loads. This paper presents an innovative self-monitoring FRP strengthening system. The system consists of two components which can be embedded in FRP materials to monitor the global and local behavior of the strengthened structure respectively. The first component of the system is designed to evaluate the applied load acting on a structure based on elongation of the FRP layer along the entire span of the structure. Success of the global system has been demonstrated using a full-scale prestressed concrete bridge girder which was loaded up to failure. The test results indicate that this type of sensor can be used to accurately determine the load prior to failure within 15 percent of the measured value. The second sensor component consists of fiber Bragg grating sensors. The sensors were used to monitor the behavior of steel double-lap shear splices tested under tensile loading up to failure. The measurements were used to identify abnormal structural behavior such as epoxy cracking and FRP debonding. Test results were also compared to numerical values obtained from a three dimensional shear-lag model which was developed to predict the sensor response.

  12. Mechanical properties and shape memory effect of short fiber reinforced SMP composite

    NASA Astrophysics Data System (ADS)

    Yu, Kai; Lv, Haibao; Yi, Guo; Liu, Yanju; Leng, Jinsong

    2010-04-01

    By adding randomly distributed short fiber into a shape memory polymer (SMP) matrix, both the mechanical properties and the shape memory behavior are improved significantly, overcoming some traditional defects of SMP composite reinforced by long fiber and particles. In this paper, the short fiber reinforced SMP composite are developed for the improvement of the mechanical and thermal properties of styrene-based SMP bulk. The specimens with different chopped fiber weight fractions are prepared, and then their mechanical behavior and electrical properties are investigated. As a result, the resistance against mechanical and thermal mechanical loads in the developed materials increases due to the role of reinforcement fiber. For the conducting composite filled with short carbon fiber, not only the actuation of SMP composite can be driven by low voltage, but also its tensile, bending strength, glass transition temperature, storage modulus and thermal conductivity increase by a factor of filler content of carbon fiber increasing. The results show meaningful guidance for further design and the performance evaluation of such composite materials.

  13. Erosive wear characteristics of multi-fiber reinforced polyester under different operating conditions

    NASA Astrophysics Data System (ADS)

    Debnath, U. K.; Chowdhury, M. A.; Nuruzzaman, D. M.

    2016-02-01

    Composite materials are used in a wide range of applications. The erosion properties of combination of glass, jute and carbon fiber-reinforced polyester were analyzed in this study. Randomly-shaped silica (SiO2) particles of various sizes (300-355μm, 355-500μm, and 500- 600μm) were selected as the erosive element. Impingement angles between 15-90°, impingement velocities between 30-50 m/sec, and stand-off distances of 15-25 mm at ambient temperature were selected. During experiment, the maximum erosion of the tested composite occurred at 60° impingement angle, indicating a semi-ductile nature of the test material. Erosion increased with impact velocity and decreased with stand-off distance. In a dimensional analysis, erosion efficiency (η) and the relationship between friction and erosion were established. Test results were evaluated using Taguchi's concept to minimize the observations needed, and ANOVA was used to identify interactions between tested parameters and to identify the most significant parameters. The S/N ratio indicates that there is only percentage of deviation between the predicted and experimental results. In further, sophisticated analyses and GMDH methods were employed, and surface damage was examined using scanning electron microscopy (SEM) to examine the nature of the wear behaviour.

  14. Experimental Study of the Flexural and Compression Performance of an Innovative Pultruded Glass-Fiber-Reinforced Polymer-Wood Composite Profile

    PubMed Central

    Qi, Yujun; Xiong, Wei; Liu, Weiqing; Fang, Hai; Lu, Weidong

    2015-01-01

    The plate of a pultruded fiber-reinforced polymer or fiber-reinforced plastic (FRP) profile produced via a pultrusion process is likely to undergo local buckling and cracking along the fiber direction under an external load. In this study, we constructed a pultruded glass-fiber-reinforced polymer-light wood composite (PGWC) profile to explore its mechanical performance. A rectangular cross-sectional PGWC profile was fabricated with a paulownia wood core, alkali-free glass fiber filaments, and unsaturated phthalate resin. Three-point bending and short column axial compression tests were conducted. Then, the stress calculation for the PGWC profile in the bending and axial compression tests was performed using the Timoshenko beam theory and the composite component analysis method to derive the flexural and axial compression rigidity of the profile during the elastic stress stage. The flexural capacity for this type of PGWC profile is 3.3-fold the sum of the flexural capacities of the wood core and the glass-fiber-reinforced polymer (GFRP) shell. The equivalent flexural rigidity is 1.5-fold the summed flexural rigidity of the wood core and GFRP shell. The maximum axial compressive bearing capacity for this type of PGWC profile can reach 1.79-fold the sum of those of the wood core and GFRP shell, and its elastic flexural rigidity is 1.2-fold the sum of their rigidities. These results indicate that in PGWC profiles, GFRP and wood materials have a positive combined effect. This study produced a pultruded composite material product with excellent mechanical performance for application in structures that require a large bearing capacity. PMID:26485431

  15. Experimental Study of the Flexural and Compression Performance of an Innovative Pultruded Glass-Fiber-Reinforced Polymer-Wood Composite Profile.

    PubMed

    Qi, Yujun; Xiong, Wei; Liu, Weiqing; Fang, Hai; Lu, Weidong

    2015-01-01

    The plate of a pultruded fiber-reinforced polymer or fiber-reinforced plastic (FRP) profile produced via a pultrusion process is likely to undergo local buckling and cracking along the fiber direction under an external load. In this study, we constructed a pultruded glass-fiber-reinforced polymer-light wood composite (PGWC) profile to explore its mechanical performance. A rectangular cross-sectional PGWC profile was fabricated with a paulownia wood core, alkali-free glass fiber filaments, and unsaturated phthalate resin. Three-point bending and short column axial compression tests were conducted. Then, the stress calculation for the PGWC profile in the bending and axial compression tests was performed using the Timoshenko beam theory and the composite component analysis method to derive the flexural and axial compression rigidity of the profile during the elastic stress stage. The flexural capacity for this type of PGWC profile is 3.3-fold the sum of the flexural capacities of the wood core and the glass-fiber-reinforced polymer (GFRP) shell. The equivalent flexural rigidity is 1.5-fold the summed flexural rigidity of the wood core and GFRP shell. The maximum axial compressive bearing capacity for this type of PGWC profile can reach 1.79-fold the sum of those of the wood core and GFRP shell, and its elastic flexural rigidity is 1.2-fold the sum of their rigidities. These results indicate that in PGWC profiles, GFRP and wood materials have a positive combined effect. This study produced a pultruded composite material product with excellent mechanical performance for application in structures that require a large bearing capacity. PMID:26485431

  16. Design criteria for pultruded fiber-reinforced polymer composite columns

    NASA Astrophysics Data System (ADS)

    Choi, Yeol

    This dissertation investigated the behavior of pultruded fiber-reinforced polymer (FRP) composite columns under extensive time-independent short-term and time-dependent long-term experiments. Based on the experimental results, analytical studies were performed to propose a design approach for pultruded FRP composite columns. In the time-independent short-term tests, a total of 100 tests on wide flange, I-shape and box section columns were selected to develop the empirical column strength equation. All column tests were performed with pinned-pinned end conditions using either a 30 feet reaction frame or a MTS machine depending on the column length. The experimental results from short-term column tests provided valuable realistic information, such as the ultimate column capacity, failure mode, and column strength equation for pultruded FRP composite columns subjected to axial compression. To develop empirical column strength equation, ultimate column capacity at failure may be examined by plotting of the ultimate compressive stress versus effective slenderness ratio, and then nondimensionalize the ultimate compressive stress and slenderness ratio to compare columns having different cross sections. Finally, a set of empirical column strength equations of FRP composite column was developed from the column strength curves using curve-fitting technique. In the time-dependent long-term creep tests, a total of 4 box and 4 wide flange section columns were tested to investigate time-dependent deformation of pultruded FRP composite columns. The cross-section used in the investigation is 4 in. x 4 in. x 1/4 in. (100 mm x 100 mm x 6.4 mm) and length is 4 feet (1.2 m) with box and wide flange sections. Creep tests were carried out at four different loading levels; 20, 30, 40 and 50 percents of the ultimate column strength from the short-term column tests. The axial time-dependent deformation under sustained loading was monitored for time duration up to 2,500 hours. The

  17. Development of wind turbine towers using fiber reinforced polymers

    NASA Astrophysics Data System (ADS)

    Ungkurapinan, Nibong

    With an ongoing trend in the wind turbine market, the size of wind turbines has been increasing continuously. Larger wind turbines imply an increase in size, weight, and loads acting on the wind turbine tower. This requires towers to be stronger and stiffer, and consequently leads to bigger tower diameters. Because of their size and weight, transportation and erection require heavy equipment that makes the use of such towers prohibitive in remote communities. To tackle this problem, a research program was initiated at the University of Manitoba to develop the technology required for the fabrication of wind turbine towers constructed of fiber reinforced polymers (FRP) for use in remote communities in Canada. The research program was carried out in stages. During the first stage, a feasibility study and an analytical investigation on various shapes of FRP towers were conducted. The concept of a multi-cellular composite tower was examined in great detail and the finite element results showed that such a tower could result in almost 45 percent reduction in weight. In the second stage of this research program, a robotic filament winding machine was designed and constructed in the Composites Laboratory of the University of Manitoba. It was used to fabricate the multi-cell tower specimens for testing. The third stage of the research program involved the experimental investigation, which was carried out in three phases. In the first phase, two single cell specimens were tested to failure under lateral loading. The specimens were 8 ft (2.44 m) long. The second phase involved the testing of two single cells loaded in compression. The third phase of the experimental investigation involved the testing of two eight-cell jointed tower specimens. The specimens were octagonal and tapered, with a diameter of 21.4 in (543 mm) at the base and 17.4 in (441 mm) at the top. They were 16 ft (4.88 m) in height and tested as cantilever under static loading. Local buckling was the dominant

  18. The effect of stress on ultrasonic pulses in fiber reinforced composites

    NASA Technical Reports Server (NTRS)

    Hemann, J. H.; Baaklini, G. Y.

    1983-01-01

    An acoustical-ultrasonic technique was used to demonstrate relationships existing between changes in attenuation of stress waves and tensile stress for an eight ply 0 degree graphite-epoxy fiber reinforced composite. All tests were conducted in the linear range of the material for which no mechanical or macroscopic damage was evident. Changes in attenuation were measured as a function of tensile stress in the frequency domain and in the time domain. Stress wave propagation in these specimens was dispersive, i.e., the wave speed depends on frequency. Wave speeds varied from 267 400 cm/sec to 680 000 cm/sec as the frequency of the signal was varied from 150 kHz to 1.9 MHz which strongly suggests that flexural/lamb wave modes of propagation exist. The magnitude of the attenuation changes depended strongly on tensile stress. It was further observed that the wave speeds increased slightly for all tested frequencies as the stress was increased.

  19. Micromechanical modeling of short glass-fiber reinforced thermoplastics-Isotropic damage of pseudograins

    SciTech Connect

    Kammoun, S.; Brassart, L.; Doghri, I.; Delannay, L.; Robert, G.

    2011-05-04

    A micromechanical damage modeling approach is presented to predict the overall elasto-plastic behavior and damage evolution in short fiber reinforced composite materials. The practical use of the approach is for injection molded thermoplastic parts reinforced with short glass fibers. The modeling is proceeded as follows. The representative volume element is decomposed into a set of pseudograins, the damage of which affects progressively the overall stiffness and strength up to total failure. Each pseudograin is a two-phase composite with aligned inclusions having same aspect ratio. A two-step mean-field homogenization procedure is adopted. In the first step, the pseudograins are homogenized individually according to the Mori-Tanaka scheme. The second step consists in a self-consistent homogenization of homogenized pseudograins. An isotropic damage model is applied at the pseudograin level. The model is implemented as a UMAT in the finite element code ABAQUS. Model is shown to reproduce the strength and the anisotropy (Lankford coefficient) during uniaxial tensile tests on samples cut under different directions relative to the injection flow direction.

  20. The effect of silica nanoparticles on the mechanical properties of fiber-reinforced composite resins.

    PubMed

    Rezvani, Mohammad Bagher; Atai, Mohammad; Hamze, Faeze; Hajrezai, Reihane

    2016-01-01

    Background. Nanotechnology has introduced many nanoparticles in recent years, which can be incorporated for mechanical improvement of dental materials. However, the existing data are widely sparse. This study investigated the reinforcing effect of silica nanoparticles when incorporated into the matrix phase of an experimental dental fiber-reinforced compositeresin (FRC) through evaluation of its flexural properties. Methods. In this experimental study FRC samples were divided into two main groups (containing two or three bundles),either of whic consisted of five subgroups with 0, 0.2, 0.5, 2 and 5 wt% of silica nanoparticles in the matrix resin (n=10 in each subgroup); a commercial FRC (Angelus, Brazil) was used as the control group (n=10). Three-point bending test was performed to evaluate the flexural strength and modulus. Thereafter, the microstructure of the fractured samples was evalu-ated using scanning electron microscopy (SEM). The results were analyzed with one-way ANOVA and HSD Tukey tests (α = 0.05). Results. The results revealed that the silica nanoparticles had a significant and positive effect on the flexural strength and modulus of FRCs (P<0.05), with no significant differences from 0.2 to 5 wt% of nanoparticles (P > 0.05) in either group with two or three bundles of fibers. Conclusion. Incorporating silica nanoparticles into the FRC resin phase resulted in improved flexural strength and modulus of the final product. PMID:27429728

  1. Effect of Home Bleaching on Microleakage of Fiber-reinforced and Particle-filled Composite Resins.

    PubMed

    Sharafeddin, Farahnaz; Zare, Samira; Javnmardi, Zahra

    2013-01-01

    Background and aims. Bleaching may exert some negative effects on existing composite resin restorations. The aim of this study was to evaluate the effect of home bleaching on microleakage of fiber-reinforced and particle-filled composite resins. Materials and methods. Ninety class V cavities (1.5×2×3 mm) were prepared on the buccal surfaces of 90 bovine teeth. The teeth were randomly divided into 6 groups (n=15) and restored as follows: Groups 1 and 2 with Z100, groups 3 and 4 with Z250, and groups 5 and 6 with Nulite F composite resins. All the specimens were thermocycled. Groups 1, 3 and 5 were selected as control groups (without bleaching) and the experimental groups 2, 4 and 6 were bleached with 22% carbamide peroxide gel. All the samples were immersed in 2% basic fuchsin dye for 24 hours and then sectioned longitudinally. Dye penetration was evaluated under a stereomicroscope (×25), at both the gingival and incisal margins. Data were analyzed using Kruskal-Wallis, Mann-Whitney and Wilcoxon tests (a=0.05). Results. Statistical analyses revealed that bleaching gel increased microleakage only at gingival margins with Z250 (P=0.007). Moreover, the control groups showed a statistically significant difference in microleakage at their gingival margins. Nulite F had the maximum microleakage while Z250 showed the minimum (P=0.006). Conclusion. Microleakage of home-bleached restorations might be related to the type of composite resin used. PMID:24578819

  2. Effect of Home Bleaching on Microleakage of Fiber-reinforced and Particle-filled Composite Resins

    PubMed Central

    Sharafeddin, Farahnaz; Zare, Samira; Javnmardi, Zahra

    2013-01-01

    Background and aims. Bleaching may exert some negative effects on existing composite resin restorations. The aim of this study was to evaluate the effect of home bleaching on microleakage of fiber-reinforced and particle-filled composite resins. Materials and methods. Ninety class V cavities (1.5×2×3 mm) were prepared on the buccal surfaces of 90 bovine teeth. The teeth were randomly divided into 6 groups (n=15) and restored as follows: Groups 1 and 2 with Z100, groups 3 and 4 with Z250, and groups 5 and 6 with Nulite F composite resins. All the specimens were thermocycled. Groups 1, 3 and 5 were selected as control groups (without bleaching) and the experimental groups 2, 4 and 6 were bleached with 22% carbamide peroxide gel. All the samples were immersed in 2% basic fuchsin dye for 24 hours and then sectioned longitudinally. Dye penetration was evaluated under a stereomicroscope (×25), at both the gingival and incisal margins. Data were analyzed using Kruskal-Wallis, Mann-Whitney and Wilcoxon tests (a=0.05). Results. Statistical analyses revealed that bleaching gel increased microleakage only at gingival margins with Z250 (P=0.007). Moreover, the control groups showed a statistically significant difference in microleakage at their gingival margins. Nulite F had the maximum microleakage while Z250 showed the minimum (P=0.006). Conclusion. Microleakage of home-bleached restorations might be related to the type of composite resin used. PMID:24578819

  3. Use of fiber-reinforced composites to improve the durability of bridge elements

    NASA Astrophysics Data System (ADS)

    Garon, Ronald; Balaguru, P. N.; Cao, Yong; Lee, K. Wayne

    2000-04-01

    Fiber composites made of carbon fibers and organic polymers are being used to strengthen plain, reinforced, and prestressed concrete structures. The composites are becoming more popular as compared to traditional strengthening with steel plates and jackets because they do not corrode and also have a very high strength to weight ratio. Organic polymers have been used as protective coatings for more than thirty years. The impermeable membrane of the polymer seals the concrete surface of the structures preventing the ingress of salts. Their main drawback is their inability to release vapor pressure buildup that causes damage in the concrete and delamination of the bonded fiber reinforced plastic. As a result of this and other weaknesses in the organic polymers, a new generation of breathable coating materials is being developed. These compositions range from epoxy modified portland cement coatings to completely inorganic silicate systems. The durability of five of the most promising compositions was evaluated under freeze-thaw, wet-dry, and scaling conditions. The silicate matrix was also used to bond carbon tows and fabrics to unreinforced concrete members. These beams were tested after exposure to wet-dry and scaling conditions. The results indicate that the inorganic matrix can be effectively used for repairs. The carbon tows can be used to replace the existing corroded reinforcing bars. The possibility of embedding optical fibers with the carbon fibers to monitor the field performance is being studied.

  4. Stiffness, thermal expansion, and thermal bending formulation of stiffened, fiber-reinforced composite panels

    NASA Technical Reports Server (NTRS)

    Collier, Craig S.

    1993-01-01

    A method is presented for formulating stiffness terms and thermal coefficients of stiffened, fiber-reinforced composite panels. The method is robust enough to handle panels with general cross sectional shapes, including those which are unsymmetric and/or unbalanced. Nonlinear, temperature and load dependent constitutive material data of each laminate are used to 'build-up' the stiffened panel membrane, bending, and membrane-bending coupling stiffness terms and thermal coefficients. New thermal coefficients are introduced to quantify panel response from through-the-thickness temperature gradients. A technique of implementing this capability with a single plane of shell finite elements using the MSC/NASTRAN analysis program (FEA) is revealed that provides accurate solutions of entire airframes or engines with coarsely meshed models. An example of a composite, hat-stiffened panel is included to demonstrate errors that occur when an unsymmetric panel is symmetrically formulated as traditionally done. The erroneous results and the correct ones produced from this method are compared to analysis from discretely meshed three-dimensional FEA.

  5. Modeling of stress/strain behavior of fiber-reinforced ceramic matrix composites including stress redistribution

    NASA Technical Reports Server (NTRS)

    Mital, Subodh K.; Murthy, Pappu L. N.; Chamis, Christos C.

    1994-01-01

    A computational simulation procedure is presented for nonlinear analyses which incorporates microstress redistribution due to progressive fracture in ceramic matrix composites. This procedure facilitates an accurate simulation of the stress-strain behavior of ceramic matrix composites up to failure. The nonlinearity in the material behavior is accounted for at the constituent (fiber/matrix/interphase) level. This computational procedure is a part of recent upgrades to CEMCAN (Ceramic Matrix Composite Analyzer) computer code. The fiber substructuring technique in CEMCAN is used to monitor the damage initiation and progression as the load increases. The room-temperature tensile stress-strain curves for SiC fiber reinforced reaction-bonded silicon nitride (RBSN) matrix unidirectional and angle-ply laminates are simulated and compared with experimentally observed stress-strain behavior. Comparison between the predicted stress/strain behavior and experimental stress/strain curves is good. Collectively the results demonstrate that CEMCAN computer code provides the user with an effective computational tool to simulate the behavior of ceramic matrix composites.

  6. Double layer oxidation resistant coating for carbon fiber reinforced silicon carbide matrix composites

    NASA Astrophysics Data System (ADS)

    Zheng, X. H.; Du, Y. G.; Xiao, J. Y.; Zhang, W. J.; Zhang, L. C.

    2009-01-01

    Double layer coatings, with celsian-Y 2SiO 5 as inner layer and Y 2Si 2O 7 as outer layer, were prepared by microwave sintering on the surface of carbon fiber reinforced silicon carbide matrix composite. Both celsian, Y 2SiO 5 and Y 2Si 2O 7 were synthesized by in situ method using BAS glass, Y 2O 3 and SiO 2 as staring materials. The sintering temperature was 1500 °C, and little damage was induced to the composite. The composition and micrograph of the fired coating were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The oxidation and thermal shock resistance of samples with doubled-layered coating were characterized at 1400 °C in air. After 150 min oxidation and thermal cycling between 1400 °C and room temperature for 15 times, the weight loss of double layer-coated sample was 1.22% and there were no cracks in the coating.

  7. Stiffness, thermal expansion, and thermal bending formulation of stiffened, fiber-reinforced composite panels

    NASA Astrophysics Data System (ADS)

    Collier, Craig S.

    1993-04-01

    A method is presented for formulating stiffness terms and thermal coefficients of stiffened, fiber-reinforced composite panels. The method is robust enough to handle panels with general cross sectional shapes, including those which are unsymmetric and/or unbalanced. Nonlinear, temperature and load dependent constitutive material data of each laminate are used to 'build-up' the stiffened panel membrane, bending, and membrane-bending coupling stiffness terms and thermal coefficients. New thermal coefficients are introduced to quantify panel response from through-the-thickness temperature gradients. A technique of implementing this capability with a single plane of shell finite elements using the MSC/NASTRAN analysis program (FEA) is revealed that provides accurate solutions of entire airframes or engines with coarsely meshed models. An example of a composite, hat-stiffened panel is included to demonstrate errors that occur when an unsymmetric panel is symmetrically formulated as traditionally done. The erroneous results and the correct ones produced from this method are compared to analysis from discretely meshed three-dimensional FEA.

  8. Development of multifunctional fiber reinforced polymer composites through ZnO nanowire arrays

    NASA Astrophysics Data System (ADS)

    Malakooti, Mohammad H.; Patterson, Brendan A.; Hwang, Hyun-Sik; Sodano, Henry A.

    2016-04-01

    Piezoelectric nanowires, in particular zinc oxide (ZnO) nanowires, have been vastly used in the fabrication of electromechanical devices to convert wasted mechanical energy into useful electrical energy. Over recent years, the growth of vertically aligned ZnO nanowires on various structural fibers has led to the development of fiber-based nanostructured energy harvesting devices. However, the development of more realistic energy harvesters that are capable of continuous power generation requires a sufficient mechanical strength to withstand typical structural loading conditions. Yet, a durable, multifunctional material system has not been developed thoroughly enough to generate electrical power without deteriorating the mechanical performance. Here, a hybrid composite energy harvester is fabricated in a hierarchical design that provides both efficient power generating capabilities while enhancing the structural properties of the fiber reinforced polymer composite. Through a simple and low-cost process, a modified aramid fabric with vertically aligned ZnO nanowires grown on the fiber surface is embedded between woven carbon fabrics, which serve as the structural reinforcement as well as the top and the bottom electrodes of the nanowire arrays. The performance of the developed multifunctional composite is characterized through direct vibration excitation and tensile strength examination.

  9. High Power Laser Cutting of Fiber Reinforced Thermoplastic Polymers with cw- and Pulsed Lasers

    NASA Astrophysics Data System (ADS)

    Schneider, F.; Wolf, N.; Petring, D.

    Glass fiber and carbon fiber reinforced polymers with thermoplastic matrix enable high volume production with short cycle times. Cutting and trimming operations in these production chains require the use of high average laser power for an efficient cutting speed, but employment of high laser power runs the risk to induce a wide heat affected zone (HAZ). This paper deals with investigations with cw and ns-pulsed CO2-laser radiation in the kilowatt range in single-pass and multiple-pass processes. Using multi-pass processing at high processing speeds of 100 m/min and above a reduced heat affected zone in the range of 100 μm to 200 μm could be achieved by the ns-pulsed radiation. With cw radiation at the same average power of 1 kW however, the HAZ was 300-400 μm. Also employing ns-pulses in the kW-range average power leads to heat accumulation in the material. Small HAZ were obtained with sufficient break times between subsequent passes.

  10. Graphite-fiber-reinforced polyimide liners of various compositions in plain spherical bearings

    NASA Technical Reports Server (NTRS)

    Sliney, H. E.; Jacobson, T. P.

    1978-01-01

    A plain spherical bearing design with a ball diameter of 28.6 mm, a race length of 12.7 mm, and a 1.7-mm-thick, molded composite liner was evaluated. The liner material is a self-lubricating composite of graphite-fiber-reinforced polyimide resin (GFRPI). The liner is prepared by transfer molding a mixture of one part chopped graphite fiber and one part partially polymerized resin into the space between the bearing ball and the outer race and then completing the polymerization under heat and pressure. Several liner compositions were evaluated: two types of polyimide, condensation and addition; two types of graphite fiber, low and high modulus; and four powder additives - cadmium oxide, cadmium iodide, graphite fluoride, and molybdenum disulfide. The bearings were oscillated + or - 15 deg at 1 Hz for 20 kilocycles under a radial unit load of 29 MN sq m (4200 psi) in dry air at 25, 200, or 315 C. Both types of fiber and polyimide gave low friction and wear. A simple equation was developed to fit the wear-time data and adequately predicted wear to 100 kilocycles.

  11. The effect of silica nanoparticles on the mechanical properties of fiber-reinforced composite resins

    PubMed Central

    Rezvani, Mohammad Bagher; Atai, Mohammad; Hamze, Faeze; Hajrezai, Reihane

    2016-01-01

    Background. Nanotechnology has introduced many nanoparticles in recent years, which can be incorporated for mechanical improvement of dental materials. However, the existing data are widely sparse. This study investigated the reinforcing effect of silica nanoparticles when incorporated into the matrix phase of an experimental dental fiber-reinforced compositeresin (FRC) through evaluation of its flexural properties. Methods. In this experimental study FRC samples were divided into two main groups (containing two or three bundles),either of whic consisted of five subgroups with 0, 0.2, 0.5, 2 and 5 wt% of silica nanoparticles in the matrix resin (n=10 in each subgroup); a commercial FRC (Angelus, Brazil) was used as the control group (n=10). Three-point bending test was performed to evaluate the flexural strength and modulus. Thereafter, the microstructure of the fractured samples was evalu-ated using scanning electron microscopy (SEM). The results were analyzed with one-way ANOVA and HSD Tukey tests (α = 0.05). Results. The results revealed that the silica nanoparticles had a significant and positive effect on the flexural strength and modulus of FRCs (P<0.05), with no significant differences from 0.2 to 5 wt% of nanoparticles (P > 0.05) in either group with two or three bundles of fibers. Conclusion. Incorporating silica nanoparticles into the FRC resin phase resulted in improved flexural strength and modulus of the final product. PMID:27429728

  12. Prediction of cutting forces in machining of unidirectional glass fiber reinforced plastics composite

    NASA Astrophysics Data System (ADS)

    Gill, Surinder Kumar; Gupta, Meenu; Satsangi, P. S.

    2013-06-01

    Machining of plastic materials has become increasingly important in any engineering industry subsequently the prediction of cutting forces. Forces quality has greater influence on components, which are coming in contact with each other. So it becomes necessary to measure and study machined forces and its behavior. In this research work, experimental investigations are conducted to determine the effects of cutting conditions and tool geometry on the cutting forces in the turning of the unidirectional glass fiber reinforced plastics (UD-GFRP) composites. In this experimental study, carbide tool (K10) having different tool nose radius and tool rake angle is used. Experiments are conducted based on the established Taguchi's technique L18 orthogonal array on a lathe machine. It is found that the depth of cut is the cutting parameter, which has greater influence on cutting forces. The effect of the tool nose radius and tool rake angles on the cutting forces are also considerably significant. Based on statistical analysis, multiple regression model for cutting forces is derived with satisfactory coefficient ( R 2). This model proved to be highly preferment for predicting cutting forces.

  13. Analysis of cracks emanating from a circular hole in unidirectional fiber reinforced composites, part 2

    NASA Technical Reports Server (NTRS)

    Wang, S. S.; Yau, J. F.

    1981-01-01

    An analytical method is developed for cracks emanating from a circular hole in an off-axis unidirectional fiber-reinforced composite. The method which is formulated by using conservation laws of elasticity and fundamental relationships in anisotropic fracture mechanics, provides a convenient and accurate means to examine the complicated crack behavior, when used in conjunction with a suitable numerical scheme such as the finite element method. The formulation is eventually reduced to a system of linear algebraic equations of mixed-mode stress intensity factors. Fracture parameters, describing crack-tip deformation and fracture in the composite, are obtained explicitly. Effects of material anisotropy and crack/hole geometry are examined also. Of particular interest are the energy release rates associated with crack extension; their values are evaluated for various cases. Results show that mixed-mode stress intensity factors and energy release rates associated with the cracks emanating from a hole change very appreciably with fiber orientation in the composite. K sub 1 and G increase monotonically with increasing theta; but K sub 2 reaches its maximum at theta = 45 deg, and then decreases gradually as theta increases further.

  14. Active vibration control of a smart pultruded fiber-reinforced polymer I-beam

    NASA Astrophysics Data System (ADS)

    Song, Gangbing; Qiao, Pizhong; Sethi, Vineet; Prasad, A.

    2002-06-01

    Advanced and innovative materials and structures are increasingly used in civil infrastructure applications. By combining the advantages of composites and smart sensors and actuators, active or smart composite structures can be created and be efficiently adopted in practical structural applications. This paper presents results of active vibration control of a pultruded fiber-reinforced polymer (FRP) composites thin-walled I-beams using smart sensors and actuators. The FRP I-beams are made of E-glass fibers and polyester resins. The FRP I-beam is in a cantilevered configuration. PZT (Lead zirconate titanate) type of piezoelectric ceramic patches are used as smart sensors and actuators. These patches are surface-bonded near the cantilevered end of the I-beam. Utilizing results from modal analyses and experimental modal testing, several active vibration control methods, such as position feedback control, strain rate feedback control and lead compensator, are investigated. Experimental results demonstrate that the proposed methods achieve effective vibration control of FRP I-beams. For instance, the modal damping ratio of the strong direction first bending mode increases by more than 1000 percent with a positive position feedback control.

  15. Active vibration control of a smart pultruded fiber-reinforced polymer I-beam

    NASA Astrophysics Data System (ADS)

    Song, G.; Qiao, P.; Sethi, V.; Prasad, A.

    2004-08-01

    Advanced and innovative materials and structures are increasingly used in civil infrastructure applications. By combining the advantages of composites and smart sensors and actuators, active or smart composite structures can be created and be efficiently adopted in practical structural applications. This paper presents results on active vibration control of pultruded fiber-reinforced polymer (FRP) composite thin-walled I-beams using smart sensors and actuators. The FRP I-beams are made of E-glass fibers and polyester resins. The FRP I-beam is in a cantilevered configuration. The PZT (lead zirconate titanate) type of piezoelectric ceramic patches are used as smart sensors and actuators. These patches are surface bonded near the cantilevered end of the I-beam. Utilizing results from modal analyses and experimental modal testing, several active vibration control methods, such as position feedback control, strain rate feedback control and lead compensation, are investigated. Experimental results demonstrate that the proposed methods achieve effective vibration control of FRP I-beams. For instance, the modal damping ratio of the strong direction first bending mode increases by more than 1000% with positive position feedback control.

  16. Nondestructive testing of externally reinforced structures for seismic retrofitting using flax fiber reinforced polymer (FFRP) composites

    NASA Astrophysics Data System (ADS)

    Ibarra-Castanedo, C.; Sfarra, S.; Paoletti, D.; Bendada, A.; Maldague, X.

    2013-05-01

    Natural fibers constitute an interesting alternative to synthetic fibers, e.g. glass and carbon, for the production of composites due to their environmental and economic advantages. The strength of natural fiber composites is on average lower compared to their synthetic counterparts. Nevertheless, natural fibers such as flax, among other bast fibers (jute, kenaf, ramie and hemp), are serious candidates for seismic retrofitting applications given that their mechanical properties are more suitable for dynamic loads. Strengthening of structures is performed by impregnating flax fiber reinforced polymers (FFRP) fabrics with epoxy resin and applying them to the component of interest, increasing in this way the load and deformation capacities of the building, while preserving its stiffness and dynamic properties. The reinforced areas are however prompt to debonding if the fabrics are not mounted properly. Nondestructive testing is therefore required to verify that the fabric is uniformly installed and that there are no air gaps or foreign materials that could instigate debonding. In this work, the use of active infrared thermography was investigated for the assessment of (1) a laboratory specimen reinforced with FFRP and containing several artificial defects; and (2) an actual FFRP retrofitted masonry wall in the Faculty of Engineering of the University of L'Aquila (Italy) that was seriously affected by the 2009 earthquake. Thermographic data was processed by advanced signal processing techniques, and post-processed by computing the watershed lines to locate suspected areas. Results coming from the academic specimen were compared to digital speckle photography and holographic interferometry images.

  17. Natural Weathering and Sea Water Effects on the Durability of Glass Fiber Reinforced Vinylester: Fractographic Analysis

    NASA Astrophysics Data System (ADS)

    Merah, Nesar; Nizamuddin, Seyed; Khan, Zafarullah; Al-Sulaiman, Faleh; Mehdi, Moeid

    2010-10-01

    This paper presents a study of the effects of harsh outdoor weather and warm sea water on the tensile behavior of Glass-Fiber Reinforced Vinylester (GFRV) pipe materials destined for sea water handling and transportation. The effect of Dhahran’s outdoor weather for exposure periods ranging from 3 to 36 months revealed an improvement in tensile strength when compared with the as received GFRV sample. A significant increasing trend of tensile strength from 3 to 12 months was noted. This is attributed mainly to the post curing effects resulting in higher cross linking density. After 12 months of exposure the tensile strength showed a decreasing trend, but remaining still higher than the average tensile strength of as received (baseline) GFRV sample. Similar results of enhanced tensile strength were noted after immersion of GFRV pipes in warm Gulf sea water for 12 months. Fractographic analysis was performed on the tensile tested GFRV samples using optical microscope followed by scanning electron microscope (SEM). The characterization of the controlling failure mechanisms involved from fracture initiation to fracture propagation through the gage section of the specimen were predicted and were justified by correlating the optical and SEM pictures.

  18. Mechanical Properties of Carbon Fiber-Reinforced Aluminum Manufactured by High-Pressure Die Casting

    NASA Astrophysics Data System (ADS)

    Kachold, Franziska; Singer, Robert

    2016-03-01

    Carbon fiber reinforced aluminum was produced by a specially adapted high-pressure die casting process. The MMC has a fiber volume fraction of 27%. Complete infiltration was achieved by preheating the bidirectional, PAN-based carbon fiber body with IR-emitters to temperatures of around 750 °C. The degradation of the fibers, due to attack of atmospheric oxygen at temperatures above 600 °C, was limited by heating them in argon-rich atmosphere. Additionally, the optimization of heating time and temperature prevented fiber degradation. Only the strength of the outer fibers is reduced by 40% at the most. The fibers in core of fiber body are nearly undamaged. In spite of successful manufacturing, the tensile strength of the MMC is below strength of the matrix material. Also unidirectional MMCs with a fiber volume fraction of 8% produced under the same conditions, lack of the reinforcing effect. Two main reasons for the unsatisfactory mechanical properties were identified: First, the fiber-free matrix, which covers the reinforced core, prevents effective load transfer from the matrix to the fibers. And second, the residual stresses in the fiber-free zones are as high as 100 MPa. This causes premature failure in the matrix. From this, it follows that the local reinforcement of an actual part is limited. The stress distribution caused by residual stresses and by loading needs to be known. In this way, the reinforcing phase can be placed and aligned accordingly. Otherwise delamination and premature failure might occur.

  19. Marginal Adaptation and Microleakeage of Directly and Indirectly Made Fiber Reinforced Composite Inlays

    PubMed Central

    Ovul, Kumbuloglu; Arzu, Tezvergil-Mutluay; Ahmet, Saracoglu; Lippo VJ, Lassila; Pekka K, Vallittu

    2011-01-01

    Aim: This study evaluated in vitro microleakage of inlays made by direct or indirect techique with or without fiber reinforced composite (FRC) substructure. Materials and Methods: Standardized mesio-occlusal cavities were prepared and restored using direct-technique with composite resin only or FRC-composite resin, and indirect technique with laboratory composite only or FRC-laboratory composite resin. After thermocycling, teeth were immersed in basic fuchsin dye, sectioned and examined under a stereo-microscope (x40). Results: No differences of cement thickness and dye penetration were found in gingival area (p>0.05), whereas microleakage revealed statistical differences between groups (p=0.02) in occlusal area, where FRC-groups had lower microleakage than composite restorations. Thickness of cement layer did not show significant difference between groups with indirect technique (p>0.05). Conclusion: The present study suggests that insertion of FRC substructure to the inlay cavity by direct composite filling technique does not increase the marginal leakage compared to that of cementing indirectly made restotorations by composite resin luting cement. Clinical Significance: On the basis of the results of this in vitro study, the use of direct FRC technique might be an effective way to decrease the marginal leakage. PMID:21566717

  20. Comparative evaluation of fracture resistance of glass fiber reinforced, carbon, and quartz post in endodontically treated teeth: An in-vitro study

    PubMed Central

    Sharma, Shweta; Attokaran, George; Singh, Kunwar S.; Jerry, Jeethu J.; Ahmed, Naima; Mitra, Nirban

    2016-01-01

    Aim and Objectives: Use of posts improves the physical properties of endodontically-treated teeth. Different post types are developed such as metal, custom-made, carbon, and quartz. The present study was conducted to evaluate the fracture resistance of glass fiber-reinforced, carbon, and quartz post in endodontically-treated teeth. Materials and Methods: Forty extracted human maxillary incisor teeth were decoronated and endodontically treated and equally divided into 4 groups; control, glass fiber-reinforced, carbon, and quartz posts. No post was used in the control group. Post space was prepared and cemented with different posts and subjected to universal testing machine to check fracture resistance. The data were statistically analyzed using t-test and analysis of variance to compare the mean difference between groups (SPSS version 20, IBM). Results: Quartz type of endodontic post showed good fracture resistance compared to carbon and resin-reinforced post. Least resistance was observed in the control group without post. Conclusion: Quartz, carbon, and glass fiber-reinforced posts show good resistance to fracture, and hence can be used in endodontically-treated teeth to enhance their strength. PMID:27583227

  1. An In Vitro Comparative Evaluation of Fracture Resistance of Custom Made, Metal, Glass Fiber Reinforced and Carbon Reinforced Posts in Endodontically Treated Teeth

    PubMed Central

    Sonkesriya, Subhash; Olekar, Santosh T; Saravanan, V; Somasunderam, P; Chauhan, Rashmi Singh; Chaurasia, Vishwajit Rampratap

    2015-01-01

    Background: Posts are used to enhance crown buildup in pulpless teeth with destructed crown portion. Different types of post are used in endodontically treated teeth. The aim of the present in vitro study was to evaluate fracture resistance of custom made, metal, glass fiber reinforced and carbon reinforced posts in endodontically treated teeth. Materials and Methods: An in vitro study was carried out on extracted 40 human maxillary central incisor teeth, which was divided into four groups with 10 samples in each group with custom made, metal post, glass fiber reinforced, and carbon reinforced posts. The samples were decoronated at cemento-enamel junction and endodontically treated. Post space was prepared and selected posts were cemented. The composite cores were prepared at the height of 5 mm and samples mounted on acrylic blocks. Later fracture resistance to the compressive force of samples was measured using Universal Testing Machine. Results: The maximum resistance to the compressive force was observed in carbon reinforced and glass fiber reinforced posts compared others which is statistically significant (P > 0.001) and least was seen in custom fabricated post. Conclusion: It is concluded that carbon reinforced fiber post and glass fiber posts showed good fracture resistance compared to custom made and metal posts. PMID:26028904

  2. Improvement of mechanical properties of acrylic bone cement by fiber reinforcement.

    PubMed

    Saha, S; Pal, S

    1984-01-01

    Acrylic bone cement is significantly weaker and less stiff than compact bone. Bone cement is also weaker in tension than in compression. This limits its use in orthopaedics to areas where tensile stresses are minimum. We have attempted to improve the mechanical properties of PMMA by reinforcing it with metal wires, and graphite and aramid fibers. Normal, carbon fiber reinforced and aramid fiber reinforced bone cement specimens were tested in compression. Addition of a small percentage (1-2% by weight for carbon and up to 6% for aramid) of these fibers improved the mechanical properties significantly. Due to the improved mechanical properties of fiber reinforced bone cement, its clinical use may reduce the incidence of cement fracture and thus loosening of the prosthesis. PMID:6480622

  3. Direct and indirect fiber-reinforced fixed partial dentures: case reports.

    PubMed

    Ahlstrand, Wisua M; Finger, Werner J

    2002-05-01

    Direct and indirect fiber-reinforced resin composite fixed partial dentures are a new way to produce minimally invasive, esthetic, and cost-effective metal-free tooth replacements. These treatment alternatives have a number of indications, for example, chairside tooth replacements, long-term provisional fixed partial dentures, economically feasible tooth replacements for patients who cannot afford more traditional treatment regimens, and tooth replacements for medically compromised patients who are unable to withstand the physical stress associated with fabrication of traditional fixed prostheses. This article presents four typical cases in which fiber-reinforced fixed partial dentures seemed to be the preferable treatment modality. PMID:12014165

  4. Research on the melt impregnation of continuous carbon fiber reinforced nylon 66 composites

    NASA Astrophysics Data System (ADS)

    Jia, M. Y.; Li, C. X.; Xue, P.; Chen, K.; Chen, T. H.

    2016-07-01

    Impregnation mold of continuous carbon fiber reinforced thermoplastic composites was designed and built in the article. Based on the theory of fluid mechanics and Darcy's law, a model of the melt impregnation was also established. The influences of fiber bundle width and impregnation pins’ diameter on the impregnation degree were studied by numerical simulation. Continuous carbon fiber reinforced nylon 66 composites were prepared. The effects of coated angle and impregnation mold temperature on the mechanical properties of the composites were also described.The agreement between the experimental data and prediction by the model was found to be satisfactory.

  5. Analytical, Numerical and Experimental Examination of Reinforced Composites Beams Covered with Carbon Fiber Reinforced Plastic

    NASA Astrophysics Data System (ADS)

    Kasimzade, A. A.; Tuhta, S.

    2012-03-01

    In the article, analytical, numerical (Finite Element Method) and experimental investigation results of beam that was strengthened with fiber reinforced plastic-FRP composite has been given as comparative, the effect of FRP wrapping number to the maximum load and moment capacity has been evaluated depending on this results. Carbon FRP qualitative dependences have been occurred between wrapping number and beam load and moment capacity for repair-strengthen the reinforced concrete beams with carbon fiber. Shown possibilities of application traditional known analysis programs, for the analysis of Carbon Fiber Reinforced Plastic (CFRP) strengthened structures.

  6. The Effect of Mechanical Force on Generalized Thermoelasticity in a Fiber-Reinforcement Under Three Theories

    NASA Astrophysics Data System (ADS)

    Othman, Mohamed I. A.; Said, Samia M.

    2012-06-01

    The present paper is concerned with effect of mechanical force on generalized thermoelasticity in a fiber-reinforcement. The formulation is applied to generalized thermoelasticity based on the coupled theory, Lord-Shulman theory, and Green-Lindsay theory. The analytical expression of the displacement components, stresses, and temperature are obtained in the physical domain and illustrated graphically using normal mode analysis. Comparisons are made among the three theories for the field quantities in the absence and in the presence of a fiber-reinforcement as well as for different values of mechanical force.

  7. A nonlinear biphasic fiber-reinforced porohyperviscoelastic model of articular cartilage incorporating fiber reorientation and dispersion.

    PubMed

    Seifzadeh, A; Wang, J; Oguamanam, D C D; Papini, M

    2011-08-01

    A nonlinear biphasic fiber-reinforced porohyperviscoelastic (BFPHVE) model of articular cartilage incorporating fiber reorientation effects during applied load was used to predict the response of ovine articular cartilage at relatively high strains (20%). The constitutive material parameters were determined using a coupled finite element-optimization algorithm that utilized stress relaxation indentation tests at relatively high strains. The proposed model incorporates the strain-hardening, tension-compression, permeability, and finite deformation nonlinearities that inherently exist in cartilage, and accounts for effects associated with fiber dispersion and reorientation and intrinsic viscoelasticity at relatively high strains. A new optimization cost function was used to overcome problems associated with large peak-to-peak differences between the predicted finite element and experimental loads that were due to the large strain levels utilized in the experiments. The optimized material parameters were found to be insensitive to the initial guesses. Using experimental data from the literature, the model was also able to predict both the lateral displacement and reaction force in unconfined compression, and the reaction force in an indentation test with a single set of material parameters. Finally, it was demonstrated that neglecting the effects of fiber reorientation and dispersion resulted in poorer agreement with experiments than when they were considered. There was an indication that the proposed BFPHVE model, which includes the intrinsic viscoelasticity of the nonfibrillar matrix (proteoglycan), might be used to model the behavior of cartilage up to relatively high strains (20%). The maximum percentage error between the indentation force predicted by the FE model using the optimized material parameters and that measured experimentally was 3%. PMID:21950897

  8. Design aid for shear strengthening of reinforced concrete T-joints using carbon fiber reinforced plastic composites

    NASA Astrophysics Data System (ADS)

    Gergely, Ioan

    The research presented in the present work focuses on the shear strengthening of beam column joints using carbon fiber composites, a material considered in seismic retrofit in recent years more than any other new material. These composites, or fiber reinforced polymers, offer huge advantages over structural steel reinforced concrete or timber. A few of these advantages are the superior resistance to corrosion, high stiffness to weight and strength to weight ratios, and the ability to control the material's behavior by selecting the orientation of the fibers. The design and field application research on reinforced concrete cap beam-column joints includes analytical investigations using pushover analysis; design of carbon fiber layout, experimental tests and field applications. Several beam column joints have been tested recently with design variables as the type of composite system, fiber orientation and the width of carbon fiber sheets. The surface preparation has been found to be critical for the bond between concrete and composite material, which is the most important factor in joint shear strengthening. The final goal of this thesis is to develop design aids for retrofitting reinforced concrete beam column joints. Two bridge bents were tested on the Interstate-15 corridor. One bent was tested in the as-is condition. Carbon fiber reinforced plastic composite sheets were used to externally reinforce the second bridge bent. By applying the composite, the displacement ductility has been doubled, and the bent overall lateral load capacity has been increased as well. The finite element model (using DRAIN-2DX) was calibrated to model the actual stiffness of the supports. The results were similar to the experimental findings.

  9. Development and fabrication of bismaleimide-graphite composites

    NASA Technical Reports Server (NTRS)

    Stenzenberger, H.; Herzog, M.; Roemer, W.; Scheiblich, R.

    1979-01-01

    The successful fabrication of high temperature resistant composites depends mainly on the processability of the resin binder matrix. For two new bismaleimide type resins the processing of graphite fabric prepregs to composites is described. One resin coded M 751 has to be processed from N-Methylpyrrolidone, the other resin evaluated is a so-called hot melt solvent-less system. Commercial T300/3000 Graphite fabrics were used as reinforcement. The M 751 - Resin is a press grade material and laminates are therefore moulded in high pressure conditions (400 N/sq cm). The solvent-less resin system H 795 is an autoclave grade material and can be cured at 40 N/sq cm. The cure cycles for both the press grade and the autoclave grade material (Fiberite W 143 fabric prepregs) are provided and the mechanical properties of laminates at low (23 C) and high (232 C) temperatures were measured. For comparison, the neat resin flexural properties are also presented. The water absorption for the neat resins and the graphite fabric laminates after a 1000 hour period was evaluated.

  10. Bioactive Glass Fiber Reinforced Starch-Polycaprolactone Composite for Bone Applications

    SciTech Connect

    Jukola, H.; Nikkola, L.; Tukiainen, M.; Kellomaeki, M.; Ashammakhi, N.; Gomes, M. E.; Reis, R. L.; Chiellini, F.; Chiellini, E.

    2008-02-15

    For bone regeneration and repair, combinations of different materials are often needed. Biodegradable polymers are often combined with osteoconductive materials, such as bioactive glass (BaG), which can also improve the mechanical properties of the composite. The aim of this study was to develop and characterize BaG fiber-reinforced starch-poly-{epsilon}-caprolactone (SPCL) composite. Sheets of SPCL (30/70 wt%) were produced using single-screw extrusion. They were then cut and compression molded in layers with BaG fibers to form composite structures of different combinations. Thermal, mechanical, and degradation properties of the composites were studied. The actual amount of BaG in the composites was determined using combustion tests. A strong endothermic peak indicating melting at about 56 deg. C was observed by differential scanning calorimetry (DSC) analysis. Thermal gravimetry analysis (TGA) showed that thermal decomposition of SPCL started at 325 deg. C with the decomposition of starch and continued at 400 deg. C with the degradation of polycaprolactone (PCL). Initial mechanical properties of the reinforced composites were at least 50% better than the properties of the non-reinforced composites. However, the mechanical properties of the composites after two weeks of hydrolysis were comparable to those of the non-reinforced samples. During the six weeks' hydrolysis the mass of the composites had decreased only by about 5%. The amount of glass in the composites remained the same for the six-week period of hydrolysis. In conclusion, it is possible to enhance the initial mechanical properties of SPCL by reinforcing it with BaG fibers. However, the mechanical properties of the composites are only sufficient for use as filler material and they need to be further improved to allow long-lasting bone applications.

  11. Bioactive Glass Fiber Reinforced Starch-Polycaprolactone Composite for Bone Applications

    NASA Astrophysics Data System (ADS)

    Jukola, H.; Nikkola, L.; Gomes, M. E.; Chiellini, F.; Tukiainen, M.; Kellomäki, M.; Chiellini, E.; Reis, R. L.; Ashammakhi, N.

    2008-02-01

    For bone regeneration and repair, combinations of different materials are often needed. Biodegradable polymers are often combined with osteoconductive materials, such as bioactive glass (BaG), which can also improve the mechanical properties of the composite. The aim of this study was to develop and characterize BaG fiber-reinforced starch-poly-ɛ-caprolactone (SPCL) composite. Sheets of SPCL (30/70 wt%) were produced using single-screw extrusion. They were then cut and compression molded in layers with BaG fibers to form composite structures of different combinations. Thermal, mechanical, and degradation properties of the composites were studied. The actual amount of BaG in the composites was determined using combustion tests. A strong endothermic peak indicating melting at about 56 °C was observed by differential scanning calorimetry (DSC) analysis. Thermal gravimetry analysis (TGA) showed that thermal decomposition of SPCL started at 325 °C with the decomposition of starch and continued at 400 °C with the degradation of polycaprolactone (PCL). Initial mechanical properties of the reinforced composites were at least 50% better than the properties of the non-reinforced composites. However, the mechanical properties of the composites after two weeks of hydrolysis were comparable to those of the non-reinforced samples. During the six weeks' hydrolysis the mass of the composites had decreased only by about 5%. The amount of glass in the composites remained the same for the six-week period of hydrolysis. In conclusion, it is possible to enhance the initial mechanical properties of SPCL by reinforcing it with BaG fibers. However, the mechanical properties of the composites are only sufficient for use as filler material and they need to be further improved to allow long-lasting bone applications.

  12. The effect of interphase and interfacial cracks on the elastic and elastoplastic behavior of fiber-reinforced composites

    NASA Astrophysics Data System (ADS)

    Zheng, Shanfu

    In order to provide a better understanding on the mechanical properties of composite materials, a dual homogenization and finite-element study is carried out in this thesis to examine the elastic stiffness and elastoplastic behavior of a fiber-reinforced composite containing either ductile interphase or interfacial cracks. In the case of interphase, circular fibers are examined. In the other case of interfacial cracks, the fibers are taken to be with elliptic cross-section to demonstrate the influence of the fiber shape. The influence of interphase is studied by the generalized self-consistent model and by finite element method (FEM) with NASTRAN. Both the traction specified boundary and displacement specified boundary conditions are carried out to determine their influence on the elastoplastic behaviors of the fiber-reinforced composite. The propagation of plastic zone in both the interphase and the ductile matrix, and stress distribution in the interphase are also vividly demonstrated. A fictitious fiber model is adopted to mimic the effect of double debonding on composites. Based on this model, the elastic stiffness of elliptic fiber-reinforced composites is obtained directly by the homogenization method, and its elastoplastic behavior is further studied by use of the concept of secant moduli and an energy-based effective stress which is evaluated by a field fluctuation method. The finite element method is carried out by ANSYS to check the accuracy of the homogenization theory and to find out its associated debonding range in practice. The local stress and deformation behavior of the composite are also given by FEM as the complementary to the homogenization theory. The single debonding is performed also by FEM to compare its influence with that of the double debonding. A new model to investigate the effect of single debonding on the effective elastic moduli is developed based on the elasticity solution of a circular cylinder with an interface crack. The solution

  13. Crystallization processes in poly(ethylene terephthalate) as modified by polymer additives and fiber reinforcement

    SciTech Connect

    Reinsch, V.E.; Rebenfeld, L.

    1993-12-31

    The effect of fiber reinforcement on the crystallization of poly(ethylene terephthalate) (PET) was investigated using differential scanning calorimetry. The objective of the study was to determine how the effects of fiber reinforcement on PET crystallization are modified by the presence of polymer additives. The interaction of fiber effects and nucleating and plasticizing agents was studied. Unidirectional fiber composites were prepared using aramid and glass fibers in PET. The rate of crystallization of PET, as reflected by crystallization half-time, it seem to depend on reinforcing fiber type, crystallization temperature, and presence of nucleant or plasticizer. However, degree of crytallinity of PET is largely unaffected by the presence of additives and reinforcing fibers. Crystallization kinetics are analyzed using a series Avrami model for PET volume crystallized as a function of time. The using a series Arami model for PET volume crystallized as a function of time. The crystalline morphology of fiber reinforced PET was studied using polarized light microscopy. Results concerning nucleation density, chain mobility, and growth morphology are used in explaining differences seen in crystallization kinetics in fiber reinforced systems.

  14. Fracture resistance of abutment screws made of titanium, polyetheretherketone, and carbon fiber-reinforced polyetheretherketone.

    PubMed

    Neumann, Eduardo Aloisio Fleck; Villar, Cristina Cunha; França, Fabiana Mantovani Gomes

    2014-01-01

    Fractured abutment screws may be replaced; however, sometimes, the screw cannot be removed and the entire implant must be surgically removed and replaced. The aim of this study was to compare the fracture resistance of abutment retention screws made of titanium, polyetheretherketone (PEEK) and 30% carbon fiber-reinforced PEEK, using an external hexagonal implant/UCLA-type abutment interface assembly. UCLA-type abutments were fixed to implants using titanium screws (Group 1), polyetheretherketone (PEEK) screws (Group 2), and 30% carbon fiber-reinforced PEEK screws (Group 3). The assemblies were placed on a stainless steel holding apparatus to allow for loading at 45o off-axis, in a universal testing machine. A 200 N load (static load) was applied at the central point of the abutment extremity, at a crosshead speed of 5 mm/minute, until failure. Data was analyzed by ANOVA and Tukey's range test. The titanium screws had higher fracture resistance, compared with PEEK and 30% carbon fiber-reinforced PEEK screws (p < 0.05). In contrast, no statistically significant difference was observed between the fracture resistance of the PEEK and the 30% carbon fiber-reinforced PEEK screws (p> 0.05). Finally, visual analysis of the fractions revealed that 100% of them occurred at the neck of the abutment screw, suggesting that this is the weakest point of this unit. PEEK abutment screws have lower fracture resistance, in comparison with titanium abutment screws. PMID:25098826

  15. AN EMPIRICAL MODEL TO PREDICT STYRENE EMISSIONS FROM FIBER-REINFORCED PLASTICS FABRICATION PROCESSES

    EPA Science Inventory

    Styrene is a designated hazardous air pollutant, per the 1990 Clean Air Act Amendments. It is also a tropospheric ozone precursor. Fiber-reinforced plastics (FRP) fabrication is the primary source of anthropogenic styrene emissions in the United States. This paper describes an em...

  16. Practical experience of steel fiber reinforced wet shotcrete in large underground construction projects

    SciTech Connect

    Garshol, K.

    1995-12-31

    The paper discusses advantages of SFRS (steel fiber reinforced shotcrete) in underground construction projects, including trends in rock support design; quality and durability of wet mix shotcrete; advantages in safety and working environment and the technical properties of SFRS. Key data from cases illustrate the above. Cost and time factors are highlighted.

  17. A constitutive function for the heat flux in short-fiber-reinforced composites

    NASA Astrophysics Data System (ADS)

    Herrmann, Heiko

    2015-12-01

    A constitutive function for heat flux in short-fiber-reinforced composites is developed. The fiber orientation distribution is considered using second-order orientation tensor; therefore, the constitutive function for the heat flux will depend on the orientation tensor. The resulting orthotropic equation is discussed also in the context of energy efficiency of buildings.

  18. PILOT-SCALE EVALUATION OF NEW RESIN APPLICATION EQUIPMENT FOR FIBER- REINFORCED PLASTICS

    EPA Science Inventory

    The article gives results of a pilot-scale evaluation of new resin application equipment for fiber- reinforced plastics. The study, an evaluation and comparison of styrene emissions, utilized Magnum's FIT(TM) nozzle with conventional spray guns and flow coaters (operated at both ...

  19. Characterization of mode II fracture behavior in fiber-reinforced ceramic composite utilizing laser interferometry

    SciTech Connect

    Mall, S.; Truskowski, J.W. USAF, Wright-Patterson AFB, OH )

    1992-09-01

    A test technique to characterize the mode II fracture behavior in fiber-reinforced ceramic composites utilizing laser interferometry was developed. This was demonstrated by measuring the mode II critical strain energy release rate at room temperature. The present study used the silicon-carbide-fiber/glass-ceramic matrix composite system. 13 refs.

  20. The effects of hot corrosion on the microstructure of a silicon carbide fiber-reinforced calcium aluminosilicate

    SciTech Connect

    Kumar, A.; Oppici, M.A.; Fox, A.G.; Wang, S.W.

    1995-12-01

    This work, funded by the navy exploratory development program, aircraft materials section, studied the effects of sodium sulfate hot corrosion on the microstructure of a SiC fiber-reinforced calcium aluminosilicate by x-ray diffraction and scanning electron microscopy. The corrosion of the composite by liquid sodium sulfate at 900{degrees}C for 50 hours gave an approximately 50-75 {mu}m thick reaction zone. Several phases, including wollastonite, nepheline and albite were identified within this reaction zone. The mechanisms by which these phases are developed are explained in terms of the kinetics of the dissociation of the sodium sulfate and its reaction with both the oxidized silicon carbide fibers and the anorthite matrix.

  1. In-plane and Interlaminar Shear Strength of a Unidirectional Hi-nicalon Fiber-reinforced Celsian Matrix Composite

    NASA Technical Reports Server (NTRS)

    Uenal, O.; Bansal, N. P.

    2000-01-01

    In-plane and interlaminar shear strength of a unidirectional SiC fiber-reinforced (BaSr)Al2Si2O8 celsian composite were measured by the double-notch shear test method between room temperature and 1200 C. The interlaminar shear strength was lower than the in-plane shear strength at all temperatures. Stress analysis, using finite element modeling, indicated that shear stress concentration was not responsible for the observed difference in strength. Instead, the difference in layer architecture and thus, the favorable alignment of fiber-rich layers with the shear plane in the interlaminar specimens appears to be the reason for the low strength of this composite. A rapid decrease in strength was observed with temperature due to softening of the glassy phase in the material.

  2. The influence of porosity on ultrasound attenuation in carbon fiber reinforced plastic composites using the laser-ultrasound spectroscopy

    NASA Astrophysics Data System (ADS)

    Karabutov, A. A.; Podymova, N. B.; Belyaev, I. O.

    2013-11-01

    Wideband acoustic spectroscopy with a laser ultrasound source for quantitative analysis of the effect of porosity on the attenuation coefficient of longitudinal acoustic waves in carbon fiber reinforced plastic (CFRP) composite materials was experimentally implemented. The samples under study had different bulk-porosity levels (up to 10%), which were determined using X-ray computer tomography. A resonance ultrasound attenuation peak associated with the one-dimensional periodicity of the layered composite structure was observed for all samples. The absolute value of the resonance-peak maximum and its width depend on the local concentration of microscopic isolated pores and extended delaminations in the sample structure. The obtained empirical relationships between these parameters of the frequency dependence of the ultrasound attenuation coefficient and the type of inhomogeneities and their volume concentration can be used for rapid evaluation of the structural quality of CFRP composites.

  3. On the Theory and Numerical Simulation of Cohesive Crack Propagation with Application to Fiber-Reinforced Composites

    NASA Technical Reports Server (NTRS)

    Rudraraju, Siva Shankar; Garikipati, Krishna; Waas, Anthony M.; Bednarcyk, Brett A.

    2013-01-01

    The phenomenon of crack propagation is among the predominant modes of failure in many natural and engineering structures, often leading to severe loss of structural integrity and catastrophic failure. Thus, the ability to understand and a priori simulate the evolution of this failure mode has been one of the cornerstones of applied mechanics and structural engineering and is broadly referred to as "fracture mechanics." The work reported herein focuses on extending this understanding, in the context of through-thickness crack propagation in cohesive materials, through the development of a continuum-level multiscale numerical framework, which represents cracks as displacement discontinuities across a surface of zero measure. This report presents the relevant theory, mathematical framework, numerical modeling, and experimental investigations of through-thickness crack propagation in fiber-reinforced composites using the Variational Multiscale Cohesive Method (VMCM) developed by the authors.

  4. Carbon-fiber-reinforced polymer variable-curvature mirror used for optical zoom imaging: prototype design and experimental demonstration

    NASA Astrophysics Data System (ADS)

    Zhao, Hui; Fan, Xuewu; Pang, Zhihai; Ren, Guorui; Wang, Wei; Xie, Yongjie; Ma, Zhen; Du, Yunfei; Su, Yu; Wei, Jingxuan

    2015-02-01

    In recent years, optical zoom imaging without moving elements has received much attention. The key to realizing this technique lies in the design of the variable-curvature mirror (VCM). To obtain enough optical magnification, the VCM should be able to change its radius of curvature over a wide range. In other words, the VCM must be able to provide a large sagittal variation, which requires the mirror material to be robust during curvature variation, require little force to deform, and have high ultimate strength. Carbon-fiber-reinforced polymer (CFRP) satisfies all these requirements and is suitable for fabricating such a VCM. Therefore, in this research, a CFRP prototype VCM has been designed, fabricated, and tested. With a diameter of 100 mm, a thickness of 2 mm, and an initial radius of curvature of 1740 mm, this VCM can provide a maximum 23-μm sagittal variation and a minimum and maximum radius of curvature of 1705 and 1760 mm.

  5. Anisotropy of conductivity in carbon fiber-reinforced plastics with continuous fibers

    NASA Astrophysics Data System (ADS)

    Ponomarenko, Anatoliy T.; Shevchenko, Vitaliy G.; Letyagin, Sergey V.; Klason, Carl

    1995-05-01

    Carbon fiber-reinforced plastics (CFRP), as high strength advanced materials are often used as media for embedding sensors and actuators. Due to the properties of components and processing conditions they are electrically anisotropic, with coefficient of anisotropy sometimes exceeding several thousands. This may prevent elimination of static electricity and cause erosion of material due to micro discharges at contacts with fastenings and embedded sensors and actuators, causing their malfunction. For this reason, the investigation of electrical properties of CFRP may provide the solution to this problem. Distribution of electric current field in CFRP and related with it possible errors in measurements of longitudinal conductivity and anisotropy are analyzed. CFRP have been prepared from PAN or cellulose fibers with different heat treatment temperatures and conductivity anisotropy was measured as a function of filler volume fraction and processing conditions. With increasing loading coefficient of anisotropy (alpha) decreases. Lower values of (alpha) were observed when curing agents containing ionic complexes of metals were used. Modifications of fiber surface with hydrophobic agents results in increased anisotropy. Composites prepared with carbon fabrics are isotropic in the fabric plane. Coefficient of anisotropy decreases with increasing molding pressure and depends on the type of weaving of fabric. In hybrid composites with alternating layers of carbon fabric and complex fiber fabric anisotropy is higher due to partial decomposition of conducting layer on top of complex fibers. A method for reducing anisotropy by introducing conducting `jumpers', shorting individual fibers or layers of fabric is proposed. The change of anisotropy in the process of fabrication of carbon-carbon composite by passing electric current through fibers has been investigated. In conclusion, alternative uses of CFRP with reduced anisotropy for contact elements of electric current through

  6. Post-cracking characteristics of high performance fiber reinforced cementitious composites

    NASA Astrophysics Data System (ADS)

    Suwannakarn, Supat W.

    The application of high performance fiber reinforced cement composites (HPFRCC) in structural systems depends primarily on the material's tensile response, which is a direct function of fiber and matrix characteristics, the bond between them, and the fiber content or volume fraction. The objective of this dissertation is to evaluate and model the post-cracking behavior of HPFRCC. In particular, it focused on the influential parameters controlling tensile behavior and the variability associated with them. The key parameters considered include: the stress and strain at first cracking, the stress and strain at maximum post-cracking, the shape of the stress-strain or stress-elongation response, the multiple cracking process, the shape of the resistance curve after crack localization, the energy associated with the multiple cracking process, and the stress versus crack opening response of a single crack. Both steel fibers and polymeric fibers, perceived to have the greatest potential for current commercial applications, are considered. The main variables covered include fiber type (Torex, Hooked, PVA, and Spectra) and fiber volume fraction (ranging from 0.75% to 2.0%). An extensive experimental program is carried out using direct tensile tests and stress-versus crack opening displacement tests on notched tensile prisms. The key experimental results were analysed and modeled using simple prediction equations which, combined with a composite mechanics approach, allowed for predicting schematic simplified stress-strain and stress-displacement response curves for use in structural modeling. The experimental data show that specimens reinforced with Torex fibers performs best, follows by Hooked and Spectra fibers, then PVA fibers. Significant variability in key parameters was observed througout suggesting that variability must be studied further. The new information obtained can be used as input for material models for finite element analysis and can provide greater

  7. Wet-laid soy fiber reinforced hydrogel scaffold: Fabrication, mechano-morphological and cell studies.

    PubMed

    Wood, Andrew T; Everett, Dominique; Budhwani, Karim I; Dickinson, Brenna; Thomas, Vinoy

    2016-06-01

    Among materials used in biomedical applications, hydrogels have received consistent linear growth in interest over the past decade due to their large water volume and saliency to the natural extracellular matrix. These materials are often limited due to their sub-optimal mechanical properties which are typically improved via chemical or physical crosslinking. Chemical crosslinking forms strong inter-polymer bonds but typically uses reagents that are cytotoxic while physical crosslinking is more temperamental to environmental changes but can be formed without these toxic reagents. In this study, we added a fiber-reinforcement phase to a poly(vinyl alcohol) (PVA) hydrogel formed through successive freezing-thawing cycles by incorporating a non-woven microfiber mat formed by the wet-lay process. By reinforcing the hydrogel with a wet-laid fibrous mat, the ultimate tensile strength and modulus increased from 0.11±0.01MPa and 0.17±0.02kPa to 0.24±0.02MPa and 5.76±1.12kPa, respectively. An increase in toughness and elongation was also found increasing from 2.52±0.37MPa to 25.6±3.84 and 51.89±5.16% to 111.16±9.68%, respectively. The soy fibers were also found to induce minimal cytotoxicity with endothelial cell viability showing 96.51%±1.91 living cells after a 48h incubation. This approach to hydrogel-reinforcement presents a rapid, tunable method by which hydrogels can attain increased mechanical properties without sacrificing their inherent biologically favorable properties. PMID:27040224

  8. The effect of nanoclay filler loading on the flexural strength of fiber-reinforced composites

    PubMed Central

    Mortazavi, Vajihesadat; Atai, Mohammad; Fathi, Mohammadhossein; Keshavarzi, Solmaz; Khalighinejad, Navid; Badrian, Hamid

    2012-01-01

    Background: Flexural strength of prosthesis made with dental composite resin materials plays an important role in their survival. The aim of this study was investigating the effect of nanoclay fillers and Poly (methyl methacrylate)-grafted (PMMA-grafted) nanoclay fillers loading on the flexural strength of fiber-reinforced composites (FRCs). Materials and Methods: Standard FRC bars (2 × 2 × 25 mm) for flexural strength testing were prepared with E-glass fibers and a synthetic resin loaded with different quantities of unmodified nanoclay and PMMA-grafted nanoclay filler particles (0% as control group, 0.2%, 0.5%, 1%, 2%, 5%). Flexural strength and flexural modulus were determined. The data were analyzed using 2-way, 1-way ANOVA and post hoc Tukey's test (α = 0.05). The fracture surfaces were evaluated by Scanning Electron Microscopy. Results: For groups with the same concentration of nanoparticles, PMMA-grafted filler-loaded group showed significantly higher flexural strength, except for 0.2% wt. For groups that contain PMMA-grafted nanoclay fillers, the 2% wt had the highest flexural strength value with significant difference to other subgroups. 1% wt and 2% wt showed significantly higher values compared to control (P < 0.05). None of the unmodified nanoclay particles loaded group represented statistically higher values of flexural strength compared to control group (P > 0.05). Flexural modulus of 2%, 5% wt PMMA-grafted and 0.5%, 1%, 2%, 5% wt unmodified nanoclay particles-loaded subgroups decreased significantly compared to control group (P < 0.05). Conclusions: PMMA-grafted nanoclay filler loading may enhance the flexural strength of FRCs. Addition of unmodified nanoparticles cannot significantly improve the flexural strength of FRCs. Addition of both unmodified and PMMA-grafted nanoclay particles in some concentrations decreased the flexural modulus. PMID:23087731

  9. CO2-laser-assisted processing of glass fiber-reinforced thermoplastic composites

    NASA Astrophysics Data System (ADS)

    Brecher, Christian; Emonts, Michael; Schares, Richard Ludwig; Stimpfl, Joffrey

    2013-02-01

    To fully exploit the potential of fiber-reinforced thermoplastic composites (FRTC) and to achieve a broad industrial application, automated manufacturing systems are crucial. Investigations at Fraunhofer IPT have proven that the use of laser system technology in processing FRTC allows to achieve high throughput, quality, flexibility, reproducibility and out-of-autoclave processing simultaneously. As 90% of the FRP in Europe1 are glass fiber-reinforced a high impact can be achieved by introducing laser-assisted processing with all its benefits to glass fiber-reinforced thermoplastics (GFRTC). Fraunhofer IPT has developed the diode laser-assisted tape placement (laying and winding) to process carbon fiber-reinforced thermoplastic composites (CFRTC) for years. However, this technology cannot be transferred unchanged to process milky transparent GFRTC prepregs (preimpregnated fibers). Due to the short wavelength (approx. 980 nm) and therefore high transmission less than 20% of the diode laser energy is absorbed as heat into non-colored GFRTC prepregs. Hence, the use of a different wave length, e.g. CO2-laser (10.6 μm) with more than 90% laser absorption, is required to allow the full potential of laser-assisted processing of GFRTC. Also the absorption of CO2-laser radiation at the surface compared to volume absorption of diode laser radiation is beneficial for the interlaminar joining of GFRTC. Fraunhofer IPT is currently developing and investigating the CO2-laser-assisted tape placement including new system, beam guiding, process and monitoring technology to enable a resource and energy efficient mass production of GFRP composites, e.g. pipes, tanks, masts. The successful processing of non-colored glass fiber-reinforced Polypropylene (PP) and Polyphenylene Sulfide (PPS) has already been proven.

  10. Study of noise reduction characteristics of composite fiber-reinforced panels, interior panel configurations, and the application of the tuned damper concept

    NASA Technical Reports Server (NTRS)

    Lameris, J.; Stevenson, S.; Streeter, B.

    1982-01-01

    The application of fiber reinforced composite materials, such as graphite epoxy and Kevlar, for secondary or primary structures developing in the commercial airplane industry was investigated. A composite panel program was initiated to study the effects of some of the parameters that affect noise reduction of these panels. The fiber materials and the ply orientation were chosen to be variables in the test program. It was found that increasing the damping characteristics of a structural panel will reduce the vibration amplitudes at resonant frequencies with attendant reductions in sound reduction. Test results for a dynamic absorber, a tuned damper, are presented and evaluated.

  11. Matrix Dominated Failure of Fiber-Reinforced Composite Laminates Under Static and Dynamic Loading

    NASA Astrophysics Data System (ADS)

    Schaefer, Joseph Daniel

    Hierarchical material systems provide the unique opportunity to connect material knowledge to solving specific design challenges. Representing the quickest growing class of hierarchical materials in use, fiber-reinforced polymer composites (FRPCs) offer superior strength and stiffness-to-weight ratios, damage tolerance, and decreasing production costs compared to metals and alloys. However, the implementation of FRPCs has historically been fraught with inadequate knowledge of the material failure behavior due to incomplete verification of recent computational constitutive models and improper (or non-existent) experimental validation, which has severely slowed creation and development. Noted by the recent Materials Genome Initiative and the Worldwide Failure Exercise, current state of the art qualification programs endure a 20 year gap between material conceptualization and implementation due to the lack of effective partnership between computational coding (simulation) and experimental characterization. Qualification processes are primarily experiment driven; the anisotropic nature of composites predisposes matrix-dominant properties to be sensitive to strain rate, which necessitates extensive testing. To decrease the qualification time, a framework that practically combines theoretical prediction of material failure with limited experimental validation is required. In this work, the Northwestern Failure Theory (NU Theory) for composite lamina is presented as the theoretical basis from which the failure of unidirectional and multidirectional composite laminates is investigated. From an initial experimental characterization of basic lamina properties, the NU Theory is employed to predict the matrix-dependent failure of composites under any state of biaxial stress from quasi-static to 1000 s-1 strain rates. It was found that the number of experiments required to characterize the strain-rate-dependent failure of a new composite material was reduced by an order of

  12. Computational modeling of high performance steel fiber reinforced concrete using a micromorphic approach

    NASA Astrophysics Data System (ADS)

    Huespe, A. E.; Oliver, J.; Mora, D. F.

    2013-12-01

    A finite element methodology for simulating the failure of high performance fiber reinforced concrete composites (HPFRC), with arbitrarily oriented short fibers, is presented. The composite material model is based on a micromorphic approach. Using the framework provided by this theory, the body configuration space is described through two kinematical descriptors. At the structural level, the displacement field represents the standard kinematical descriptor. Additionally, a morphological kinematical descriptor, the micromorphic field, is introduced. It describes the fiber-matrix relative displacement, or slipping mechanism of the bond, observed at the mesoscale level. In the first part of this paper, we summarize the model formulation of the micromorphic approach presented in a previous work by the authors. In the second part, and as the main contribution of the paper, we address specific issues related to the numerical aspects involved in the computational implementation of the model. The developed numerical procedure is based on a mixed finite element technique. The number of dofs per node changes according with the number of fiber bundles simulated in the composite. Then, a specific solution scheme is proposed to solve the variable number of unknowns in the discrete model. The HPFRC composite model takes into account the important effects produced by concrete fracture. A procedure for simulating quasi-brittle fracture is introduced into the model and is described in the paper. The present numerical methodology is assessed by simulating a selected set of experimental tests which proves its viability and accuracy to capture a number of mechanical phenomenon interacting at the macro- and mesoscale and leading to failure of HPFRC composites.

  13. Development and Evaluation of Novel Coupling Agents for Kenaf-Fiber-Reinforced Unsaturated Polyester Composites

    NASA Astrophysics Data System (ADS)

    Ren, Xiaofeng

    Natural fibers are gaining popularity as reinforcement materials for thermoset resins over the last two decades. Natural fibers are inexpensive, abundant, renewable and environmentally friendly. Kenaf fibers are one of the natural fibers that can potentially be used for reinforcing unsaturated polyester (UPE). As a polymer matrix, UPE enjoys a 40% market share of all the thermoset composites. This widespread application is due to many favorable characteristics including low cost, ease of cure at room temperature, ease of molding, a good balance of mechanical, electrical and chemical properties. One of the barriers for the full utilization of the kenaf fiber reinforced UPE composites, however, is the poor interfacial adhesion between the natural fibers and the UPE resins. The good interfacial adhesion between kenaf fibers and UPE matrix is essential for generating the desired properties of kenaf-UPE composites for most of the end applications. Use of a coupling agent is one of the most effective ways of improving the interfacial adhesion. In this study, six novel effective coupling agents were developed and investigated for kenaf-UPE composites: DIH-HEA, MFA, NMA, AESO-DIH, AESO-MDI, and AESO-PMDI. All the coupling agents were able to improve the interfacial adhesion between kanaf and UPE resins. The coupling agents were found to significantly enhance the flexural properties and water resistance of the kenaf-UPE composites. Fourier transform infrared spectroscopy (FTIR) confirmed all the coupling agents were covalently bonded onto kenaf fibers. Scanning electron microscopy (SEM) images of the composites revealed the improved interfacial adhesion between kanaf fibers and UPE resins.

  14. Mechanical effect of static loading on endodontically treated teeth restored with fiber-reinforced posts.

    PubMed

    Chieruzzi, Manila; Rallini, Marco; Pagano, Stefano; Eramo, Stefano; D'Errico, Potito; Torre, Luigi; Kenny, José M

    2014-02-01

    The aim of this study was to investigate the mechanical behavior of a dental system built up with fiber-reinforced composite (FRC) endodontic posts with different types of fibers and two cements (the first one used with a primer, the second one without it). Six FRC posts were used. Each system was characterized in terms of structural efficiency under external applied loads similar to masticatory forces. An oblique force was applied and stiffness and maximum load data were obtained. The same test was used for the dentine. The systems were analyzed by scanning electron microscope (SEM) to investigate the surface of the post and inner surface of root canal after failure. The mechanical tests showed that load values in dental systems depend on the post material and used cement. The highest load (281 ± 59 N) was observed for the conical glass fiber posts in the cement without primer. There was a 50 and 85% increase in the maximum load for two of the conical posts with glass fibers and a 229% increase for the carbon fiber posts in the cement without primer as compared with the cement with primer. Moreover, almost all the studied systems showed fracture resistances higher than the typical masticatory loads. The microscopic analysis underlined the good adhesion of the second cement at the interfaces between dentine and post. The mechanical tests confirmed that the strength of the dental systems subjected to masticatory loads was strictly related to the bond at the interface post/cement and cement/dentine. PMID:24000235

  15. New environmental barrier coating system on carbon-fiber reinforced silicon carbide composites

    NASA Astrophysics Data System (ADS)

    Latzel, S.; Vaßen, R.; Stöver, D.

    2005-06-01

    Carbon-fiber-reinforced silicon carbide composites (C/SiC) are promising materials for high-temperature, light weight structural components. However, a protective coating and environmental barrier coating (EBC) are necessary to prevent the oxidation of the carbon and the reaction of the formed silica scale with water vapor. Current EBC systems use multiple layers, each serving unique requirements. However, any mismatch in the coefficients of thermal expansion (CTE) creates internal stresses and might lead to crack formation. In this case, oxygen and water vapor penetrate through the EBC, reducing the lifetime of the component. Mullite (Al6Si2O13) is used in many known EBC systems on silicon-based ceramics either as an EBC itself or as a bondcoat. Due to its low CTE and its sufficient thermal cycling behavior, mullite was chosen in this investigation as a first layer. As mullite suffers loss of SiO2 when exposed to water vapor at high temperatures, an additional protective top coat is needed to complete the EBC system. Different oxides were evaluated to serve as top coat, especially high-temperature oxides with low coefficients of thermal expansion (LCTE). An EBC containing mullite as bondcoat and the LCTE oxide La2Hf2O7 as a top coat is proposed. Both layers were applied via atmospheric plasma spraying. In this paper, results of the influence of processing conditions on the microstructure of single mullite and LCTE oxide layers as well as mullite/LCTE oxide systems are presented. Special emphasis was directed toward the crystallinity of the mullite layer and, in the top layer, toward low porosity and reduced crack density.

  16. Composites of vinyl polystyrylpyridine/bismaleimide-aliphatic ether copolymers

    NASA Technical Reports Server (NTRS)

    Heimbuch, Alvin H.; Rosser, Robert W.; Hsu, Ming-Ta S.

    1989-01-01

    An aliphatic ether bismaleimide was prepared and coreacted with a polyvinylstyrylpyridine (VPSP) oligomer. Studies showed that a controlled ratio of aliphatic to aromatic units in the polymer backbone improved both processibility and interlaminar shear properties for the carbon-fiber composite system. This modified resin was readily soluble in tetrahydrofuran, allowing for better fiber impregnation and thus enhancing adhesive properties and reproducibility. DSC studies have shown a lower cure temperature for the copolymer than for the neat aliphatic bismaleimide, and a glass transition temperature of 260 C, which is more than adequate for most applications. Limited measurements indicated an improvement in toughness (impact resistance).

  17. Effect of Resin Viscosity in Fiber Reinforcement Compaction in Resin Injection Pultrusion Process

    NASA Astrophysics Data System (ADS)

    Shakya, N.; Roux, J. A.; Jeswani, A. L.

    2013-12-01

    In resin injection pultrusion, the liquid resin is injected through the injection slots into the fiber reinforcement; the liquid resin penetrates through the fibers as well as pushes the fibers towards the centerplane causing fiber compaction. The compacted fibers are more difficult to penetrate, thus higher resin injection pressure becomes necessary to achieve complete reinforcement wetout. Lower injection pressures below a certain range (depending upon the fiber volume fraction and resin viscosity) cannot effectively penetrate through the fiber bed and thus cannot achieve complete wetout. Also, if the degree of compaction is very high the fibers might become essentially impenetrable. The more viscous the resin is, the harder it is to penetrate through the fibers and vice versa. The effect of resin viscosity on complete wetout achievement with reference to fiber-reinforcement compaction is presented in this study.

  18. Tensile creep and creep fracture of a fiber-reinforced SiC/SiC composite

    SciTech Connect

    Wilshire, B.; Carreno, F.; Percival, M.J.L.

    1998-08-11

    Several studies have been completed on silicon carbide fiber-reinforced silicon carbide (SiC{sub f}/SiC) composites produced with carbon-coated fibres having a 0/90{degree} architecture. Yet, while mechanical property measurements have been made at temperatures up to 1,473K in air and argon high-temperature creep tests have been carried out only under protective atmospheres. To clarify the creep behavior patterns displayed by continuous-fiber-reinforced CMCs, while simultaneously providing information relevant to aeroengine turbine design, the tensile creep and creep fracture properties of a 0/90{degree} SiC{sub f}/SiC composite have been determined over a stress range giving creep rupture lives up to approximately 2,000 hours in air at 1,573K.

  19. Network model for thermal conductivities of unidirectional fiber-reinforced composites

    NASA Astrophysics Data System (ADS)

    Wang, Yang; Peng, Chaoyi; Zhang, Weihua

    2014-12-01

    An empirical network model has been developed to predict the in-plane thermal conductivities along arbitrary directions for unidirectional fiber-reinforced composites lamina. Measurements of thermal conductivities along different orientations were carried out. Good agreement was observed between values predicted by the network model and the experimental data; compared with the established analytical models, the newly proposed network model could give values with higher precision. Therefore, this network model is helpful to get a wider and more comprehensive understanding of heat transmission characteristics of fiber-reinforced composites and can be utilized as guidance to design and fabricate laminated composites with specific directional or specific locational thermal conductivities for structures that simultaneously perform mechanical and thermal functions, i.e. multifunctional structures (MFS).

  20. Effect of hot-dry environment on fiber-reinforced self-compacting concrete

    NASA Astrophysics Data System (ADS)

    Tioua, Tahar; Kriker, Abdelouahed; Salhi, Aimad; Barluenga, Gonzalo

    2016-07-01

    Drying shrinkage can be a major reason for the deterioration of concrete structures. Variation in ambient temperature and relative humidity cause changes in the properties of hardened concrete which can affect their mechanical and drying shrinkage characteristics. The present study investigated mechanical strength and particularly drying shrinkage properties of self-compacting concretes (SCC) reinforced with date palm fiber exposed to hot and dry environment. In this study a total of nine different fibers reinforced self compacting concrete (FRSCC) mixtures and one mixture without fiber were prepared. The volume fraction and the length of fibers reinforcement were 0.1-0.2-0.3% and 10-20-30 mm. It was observed that drying shrinkage lessened with adding low volumetric fraction and short length of fibers in curing condition (T = 20 °C and RH = 50 ± 5 %), but increased in hot and dry environment.

  1. Fiber-reinforced Composite for Chairside Replacement of Anterior Teeth: A Case Report.

    PubMed

    Garoushi, S; Vallittu, Pk; Lassila, Lvj

    2008-01-01

    A variety of therapeutic modalities, from implant to conventional Maryland prosthesis, can be used for the replacement of a missing anterior tooth. Whenever a minimal tooth reduction is preferred, a fiber reinforced composite (FRC) prosthesis could be a good alternative to conventional prosthetic techniques, chiefly as temporary restoration before making a final decision on the treatment. The purpose of this case report is to describe the clinical procedure of fabricating anterior chairside FRC prosthesis with pre-impregnated unidirectional E-glass fibers and veneered particulate filler composite. Fiber-reinforced composite in combination with adhesive technology appears to be a promising treatment option for replacing missing teeth. However, further and long-term clinical investigation will be required to provide additional information on the survival of directly-bonded anterior fixed prosthesis made with FRC systems. PMID:21499473

  2. Generalized Magneto-thermoelasticity in a Fiber-Reinforced Anisotropic Half-Space with Energy Dissipation

    NASA Astrophysics Data System (ADS)

    Othman, Mohamed I. A.; Atwa, Sarhan Y.

    2012-06-01

    The propagation of plane waves in a fiber-reinforced, anisotropic thermoelastic half-space proposed by Green and Naghdi theory under the effect of magnetic field is discussed. The problem has been solved analytically using normal mode analysis to obtain the exact solution of the temperature, the displacement components, and the thermal stress. Numerical results for the temperature distribution, the displacement components, and the thermal stress are given and illustrated graphically. Comparisons are made with the results predicted by types II and III in the presence and in the absence of the effect of a magnetic field and fiber reinforcement. It is found that the reinforcement and magnetic field have great effects on the distribution of the field quantities.

  3. Adsorption of parotid saliva proteins and adhesion of Streptococcus mutans ATCC 21752 to dental fiber-reinforced composites.

    PubMed

    Tanner, Johanna; Carlén, Anette; Söderling, Eva; Vallittu, Pekka K

    2003-07-15

    The use of fiber-reinforced composites (FRC) in dentistry has increased during recent years. In marginal areas of crowns and removable partial dentures the fibers may become exposed and come into contact with oral tissues, saliva, and microbes. To date, few articles have been published on oral microbial adhesion to FRCs. The aim of this study was to compare different FRCs, their components, and conventional restorative materials with respect to S. mutans ATCC 21752 adhesion and adsorption of specific S. mutans binding proteins. Surface roughness of the materials was also determined. Four different FRCs, a restorative composite, and a high-leucite ceramic material were studied. Polyethylene FRC was found to be significantly rougher than all other materials. Aramid FRC also showed higher surface roughness in comparison with all materials but polyethylene FRC. Without a saliva pellicle, adhesion of S. mutans coincided with surface roughness and polyethylene and aramid FRC promoted S. mutans adhesion better than the other smoother materials. In the presence of salivary pellicle, ceramic and polyethylene FRC bound more bacteria than the other materials studied. Higher quantities of S. mutans binding proteins in the pellicles may in part account for the higher S. mutans adhesion to saliva-coated ceramic and polyethylene FRC. PMID:12808599

  4. Effects of high energy radiation on the mechanical properties of epoxy graphite fiber reinforced composites

    NASA Technical Reports Server (NTRS)

    Gilbert, R. D.; Fornes, R. E.; Memory, J. D.

    1983-01-01

    The effects of high energy radiation on mechanical properties and on the molecular and structural properties of graphite fiber reinforced composites are assessed so that durability in space applications can be predicted. A listing of composite systems irradiated along with the maximum radiation dose applied and type of mechanical tests performed is shown. These samples were exposed to 1/2 MeV electrons.

  5. Replacement of missing teeth with fiber-reinforced composite FPDs: clinical protocol.

    PubMed

    Bouillaguet, Serge; Schütt, Andrea; Marin, Isabelle; Etechami, Leila; Di Salvo, Giancarlo; Krejci, Ivo

    2003-04-01

    The concept of minimally invasive preparation protocols has resulted in reduced loss of critical tooth structures and maintenance of optimal strength, form, and aesthetics. While various treatment options have been described for single-tooth replacement, fiber-reinforced composite (FRC) fixed partial dentures (FPDs) provide a viable treatment alternative with proven mechanical properties, aesthetics, and function. This article presents several clinical scenarios in which minimally invasive adhesive FRC FPDs are provided to deliver enhanced predictability, strength, and durability. PMID:12956045

  6. μ-COMPUTED Tomography for Micro-Structure Characterization of Carbon Fiber Reinforced Plastic (cfrp)

    NASA Astrophysics Data System (ADS)

    Stoessel, R.; Guenther, T.; Dierig, T.; Schladitz, K.; Godehardt, M.; Kessling, P.-M.; Fuchs, T.

    2011-06-01

    Non-destructive testing is of major importance for quality assurance of carbon fiber reinforced plastic (CFRP) in aerospace industry. It is of interest to obtain information of the 3D inner micro-structure of CFRP. A promising option is the usage of μ-CT inspection. State-of-the art software tools are used to characterize the 3D inner micro-structure and to gather knowledge about porosity, cracks, and fiber orientation.

  7. Thermal characterization and tomography of carbon fiber reinforced plastics using individual identification technique

    SciTech Connect

    Vavilov, V.P.; Grinzato, E.; Bison, P.G.; Marinetti, S.; Bressan, C.

    1996-05-01

    A method for thermal characterization of defect depth and thickness using individual inversion functions is described. Experimental results are obtained with standard carbon fiber reinforced plastic specimens which contained Teflon inserts and impact damage. Accuracy in determining defect dimensions was about 10 percent for defect depth and 33 percent for defect thickness. A technique to synthesize images of defect parameters is proposed. Thermal tomography advantages in analyzing defect in-depth propagation are illustrated.

  8. Graphite fiber reinforced thermoplastic glass matrix composites for use at 1000 F

    NASA Technical Reports Server (NTRS)

    Prewo, K. M.; Minford, E. J.

    1985-01-01

    The fabrication and properties of the graphite fiber reinforced glass matrix composite system are described. By reinforcing borosilicate glass with graphite fibers it has been possible to develop a composite whose properties can be compared favorably with resin matrix counterparts. Both high elastic modulus and strength can be obtained and maintained to temperatures of approximately 600 C. In addition, composite dimensional stability is superior to resin or metal matrix systems due to the low thermal expansion behavior of the glass matrix.

  9. Ultrasonic velocity technique for monitoring property changes in fiber-reinforced ceramic matrix composites

    NASA Technical Reports Server (NTRS)

    Kautz, Harold E.; Bhatt, Ramakrishna T.

    1991-01-01

    A technique for measuring ultrasonic velocity was used to monitor changes that occur during processing and heat treatment of a SiC/RBSM composite. Results indicated that correlations exist between the ultrasonic velocity data and elastic modulus and interfacial shear strength data determined from mechanical tests. The ultrasonic velocity data can differentiate strength. The advantages and potential of this nondestructive evaluation method for fiber reinforced ceramic matrix composite applications are discussed.

  10. A fiber-reinforced composite prosthesis restoring a lateral midfacial defect: a clinical report.

    PubMed

    Kurunmäki, Hemmo; Kantola, Rosita; Hatamleh, Muhanad M; Watts, David C; Vallittu, Pekka K

    2008-11-01

    This clinical report describes the use of a glass fiber-reinforced composite (FRC) substructure to reinforce the silicone elastomer of a large facial prosthesis. The FRC substructure was shaped into a framework and embedded into the silicone elastomer to form a reinforced facial prosthesis. The prosthesis is designed to overcome the disadvantages associated with traditionally fabricated prostheses; namely, delamination of the silicone of the acrylic base, poor marginal adaptation over time, and poor simulation of facial expressions. PMID:18992568

  11. On the structure of nonlinear constitutive equations for fiber reinforced composites

    NASA Technical Reports Server (NTRS)

    Jansson, Stefan

    1992-01-01

    The structure of constitutive equations for nonlinear multiaxial behavior of transversely isotropic fiber reinforced metal matrix composites subject to proportional loading was investigated. Results from an experimental program were combined with numerical simulations of the composite behavior for complex stress to reveal the full structure of the equations. It was found that the nonlinear response can be described by a quadratic flow-potential, based on the polynomial stress invariants, together with a hardening rule that is dominated by two different hardening mechanisms.

  12. Fiber-reinforced composite anterior bridge in pediatric traumatology: clinical considerations.

    PubMed

    Chafaie, Amir; Dahan, Serge; Le Gall, Michel

    2013-12-01

    This article describes the protocol for creation of a fiber-reinforced composite bridge for temporary treatment of traumatic tooth loss affecting young adult dentition. This non-invasive solution is justified by the time lapse between the end of orthodontic treatment and the moment when the state of maturity of the various tissues makes it possible to install a conventional or implant-based prosthesis. PMID:24144520

  13. Use of carbon-fiber-reinforced composite implants in orthopedic surgery.

    PubMed

    Hak, David J; Mauffrey, Cyril; Seligson, David; Lindeque, Bennie

    2014-12-01

    Carbon-fiber-reinforced polyetheretherketone implants offer several benefits over traditional metal implants. Their radiolucent property permits improved, artifact-free radiographic imaging. Their lower modulus of elasticity better matches that of bone. Their fatigue strength is greater than most metal implants. This article reviews the use of these implants in orthopedic surgery, including treatment of conditions involving the spine, trauma, tumor, and infection. PMID:25437074

  14. Plane Waves of a Fiber-Reinforcement Magneto-thermoelastic Comparison of Three Different Theories

    NASA Astrophysics Data System (ADS)

    Othman, Mohamed I. A.; Said, Samia M.

    2013-02-01

    In this article, the coupled theory, Lord-Shulman theory, and Green-Lindsay (GL) theory are used to study the influence of a magnetic field on a fiber-reinforced thermoelastic half-space. Normal mode analysis is used to solve a thermal shock problem. Numerical results for the temperature, displacement components, and stress components are given and illustrated graphically. A comparison is made between the coupled and GL theories in the absence and presence of a magnetic field and reinforcement.

  15. Investigation of rectangular concrete columns reinforced or prestressed with fiber reinforced polymer (FRP) bars or tendons

    NASA Astrophysics Data System (ADS)

    Choo, Ching Chiaw

    Fiber reinforced polymer (FRP) composites have been increasingly used in concrete construction. This research focused on the behavior of concrete columns reinforced with FRP bars, or prestressed with FRP tendons. The methodology was based the ultimate strength approach where stress and strain compatibility conditions and material constitutive laws were applied. Axial strength-moment (P-M) interaction relations of reinforced or prestressed concrete columns with FRP, a linearly-elastic material, were examined. The analytical results identified the possibility of premature compression and/or brittle-tension failure occurring in FRP reinforced and prestressed concrete columns where sudden and explosive type failures were expected. These failures were related to the rupture of FRP rebars or tendons in compression and/or in tension prior to concrete reaching its ultimate strain and strength. The study also concluded that brittle-tension failure was more likely to occur due to the low ultimate tensile strain of FRP bars or tendons as compared to steel. In addition, the failures were more prevalent when long term effects such as creep and shrinkage of concrete, and creep rupture of FRP were considered. Barring FRP failure, concrete columns reinforced with FRP, in some instances, gained significant moment resistance. As expected the strength interaction of slender steel or FRP reinforced concrete columns were dependent more on column length rather than material differences between steel and FRP. Current ACI minimum reinforcement ratio for steel (rhomin) reinforced concrete columns may not be adequate for use in FRP reinforced concrete columns. Design aids were developed in this study to determine the minimum reinforcement ratio (rhof,min) required for rectangular reinforced concrete columns by averting brittle-tension failure to a failure controlled by concrete crushing which in nature was a less catastrophic and more gradual type failure. The proposed method using rhof

  16. Enhanced Schapery Theory Software Development for Modeling Failure of Fiber-Reinforced Laminates

    NASA Technical Reports Server (NTRS)

    Pineda, Evan J.; Waas, Anthony M.

    2013-01-01

    Progressive damage and failure analysis (PDFA) tools are needed to predict the nonlinear response of advanced fiber-reinforced composite structures. Predictive tools should incorporate the underlying physics of the damage and failure mechanisms observed in the composite, and should utilize as few input parameters as possible. The purpose of the Enhanced Schapery Theory (EST) was to create a PDFA tool that operates in conjunction with a commercially available finite element (FE) code (Abaqus). The tool captures the physics of the damage and failure mechanisms that result in the nonlinear behavior of the material, and the failure methodology employed yields numerical results that are relatively insensitive to changes in the FE mesh. The EST code is written in Fortran and compiled into a static library that is linked to Abaqus. A Fortran Abaqus UMAT material subroutine is used to facilitate the communication between Abaqus and EST. A clear distinction between damage and failure is imposed. Damage mechanisms result in pre-peak nonlinearity in the stress strain curve. Four internal state variables (ISVs) are utilized to control the damage and failure degradation. All damage is said to result from matrix microdamage, and a single ISV marks the micro-damage evolution as it is used to degrade the transverse and shear moduli of the lamina using a set of experimentally obtainable matrix microdamage functions. Three separate failure ISVs are used to incorporate failure due to fiber breakage, mode I matrix cracking, and mode II matrix cracking. Failure initiation is determined using a failure criterion, and the evolution of these ISVs is controlled by a set of traction-separation laws. The traction separation laws are postulated such that the area under the curves is equal to the fracture toughness of the material associated with the corresponding failure mechanism. A characteristic finite element length is used to transform the traction-separation laws into stress-strain laws

  17. Development of ductile hybrid fiber reinforced polymer (D-H-FRP) reinforcement for concrete structures

    NASA Astrophysics Data System (ADS)

    Somboonsong, Win

    The corrosion of steel rebars has been the major cause of the reinforced concrete deterioration in transportation structures and port facilities. Currently, the Federal Highway Administration (FHWA) spends annually $31 billion for maintaining and repairing highways and highway bridges. The study reported herein represents the work done in developing a new type of reinforcement called Ductile Hybrid Fiber Reinforced Polymer or D-H-FRP using non-corrosive fiber materials. Unlike the previous FRP reinforcements that fail in a brittle manner, the D-H-FRP bars exhibit the stress-strain curves that are suitable for concrete reinforcement. The D-H-FRP stress-strain curves are linearly elastic with a definite yield point followed by plastic deformation and strain hardening resembling that of mild steel. In addition, the D-H-FRP reinforcement has integrated ribs required for concrete bond. The desirable mechanical properties of D-H-FRP reinforcement are obtained from the integrated design based on the material hybrid and geometric hybrid concepts. Using these concepts, the properties can be tailored to meet the specific design requirements. An analytical model was developed to predict the D-H-FRP stress-strain curves with different combination of fiber materials and geometric configuration. This model was used to optimize the design of D-H-FRP bars. An in-line braiding-pultrusion manufacturing process was developed at Drexel University to produce high quality D-H-FRP reinforcement in diameters that can be used in concrete structures. A series of experiments were carried out to test D-H-FRP reinforcement as well as their individual components in monotonic and cyclic tensile tests. Using the results from the tensile tests and fracture analysis, the stress-strain behavior of the D-H-FRP reinforcement was fully characterized and explained. Two series of concrete beams reinforced with D-H-FRP bars were studied. The D-H-FRP beam test results were then compared with companion

  18. Low Frequency Guided Plate Waves Propagation in Fiber Reinforced Composites

    NASA Technical Reports Server (NTRS)

    Lih, S-S.; Bar-Cohen, Y.

    1995-01-01

    Conventional destructive techniques for the determination of the elastic stiffness constants of composite materials can be costly and often inaccurate. Reliable nondestructive evaluation methods for monitoring the integrity of composite materials and structures are needed. Guided wave propagation in isotropic plate have been studied. Studies on the low frequency symmetric guide waves are presented.

  19. Microstructure of AI2O3 fiber-reinforced superalloy (INCONEL 718) composites

    NASA Astrophysics Data System (ADS)

    Nourbakhsh, S.; Sahin, O.; Rhee, W. H.; Margolin, H.

    1996-02-01

    Composites of INCONEL 718 alloy reinforced with either single-crystal (SAPHIKON) or polycrys-talline (Du Pont's FP) A12O3 fiber were fabricated by pressure casting. Optical and transmission electron microscopy were used to characterize the microstructure of the composites and to determine the nature of the fiber/matrix reaction. The widely dispersed fibers in the SAPHIKON-fiber-reinforced composite had no influence on the solidification of the matrix. Six phases, γ-Ni3Al, γ'-Ni3Nb, δ-Ni3Nb, TiC, NbC, and Laves, were present in the matrix of the composite. The last three phases were formed during solidification and the others precipitated during subsequent cooling. The high density of fibers in the FP-fiber-reinforced composite led to a more uniform microstructure within the matrix. Only three phases, γ″-Ni3Nb, NbC, and Laves, were identified. Diffusion of Ti into the A12O3 fiber resulted in preferential grain growth in the FP fiber in areas adjacent to the fiber/matrix interface. The fiber/matrix bond strength in shear in the SAPHIKON-fiber-reinforced composite was in excess of 150 MPa.

  20. Hi-Nicalon Fiber-Reinforced Celsian Matrix Composites: Influence of Interface Modification

    NASA Technical Reports Server (NTRS)

    Bansal, Narottam P.; Eldridge, Jeffrey I.

    1998-01-01

    Unidirectional celsian matrix composites having 42-45 vol % of uncoated or BN-SIC coated Hi-Nicalon fibers were tested in three-point bend at room temperature. The uncoated fiber-reinforced composites showed catastrophic failure with strength of 210 35 MPa and a flat fracture surface. In contrast, composites reinforced with coated fibers exhibited graceful failure with extensive fiber pullout. Values of first matrix cracking stress and strain were 435 +/- 35 MPa and 0.27 +/- 0.01%, respectively, with ultimate strength as high as 960 MPa. The elastic Young modulus of the uncoated and coated fiber-reinforced composites were 184 +/- 4 GPa and 165 +/- 5 GPa, respectively. Fiber push-through tests and microscopic examination indicated no chemical reaction at the uncoated or coated fiber-matrix interface. The low strength of composite with uncoated fibers is due to degradation of the fiber strength from mechanical damage during processing. Because both the coated- and uncoated-fiber-reinforced composites exhibited weak interfaces, the beneficial effect of the BN-SIC dual layer is primarily the protection of fibers from mechanical damage during processing.

  1. Application of fiber-reinforced plastic rods as prestressing tendons in concrete structures. Final report

    SciTech Connect

    Mattock, A.H.; Babaei, K.

    1989-08-01

    The study is concerned with the possibility of utilizing fiber-reinforced plastic rods as prestressing tendons, in place of traditional steel tendons, in elements of prestressed-concrete bridges exposed to corrosive environments. A survey was made of available information on the behavior characteristics of fiber-reinforced plastic tension elements and, in particular, those of glass-fiber-reinforced (GFR) tension elements. Also, an analytical study was made of the flexural behavior of concrete elements prestressed by GFR tendons. Based on the analytical study and on the survey of available information, an assessment is made of the impact on the design of prestressed-concrete members if GFR tendons are used. Some preliminary design recommendations are made, together with proposals for research needed before GFR prestressing tendons should be used in practice. Four GFR tendons with Con-Tech Systems anchorages were tested, the primary variable being the embedded length of the GFR rods in the anchorages. All the tendons failed by the rods pulling out of the anchorages. For embedded lengths of 15.2 in or greater, the failure loads were 90% of the advertised tendon strength of 220 ksi, or about 100% of the guaranteed tensile strength of 197 ksi (60 kN/rod).

  2. Sensing uniaxial tensile damage in fiber-reinforced polymer composites using electrical resistance tomography

    NASA Astrophysics Data System (ADS)

    Lestari, Wahyu; Pinto, Brian; La Saponara, Valeria; Yasui, Jennifer; Loh, Kenneth J.

    2016-08-01

    This work describes the application of electrical resistance tomography (ERT) in sensing damage in fiber-reinforced polymer composites under uniaxial quasi-static tension. Damage is manifested as numerous matrix cracks which are distributed across the composite volume and which eventually coalesce into intralayer cracks. Hence, tensile damage is distributed throughout the volume, and could be more significant outside the sensor area. In this work, tensile damage of unidirectional glass fiber-reinforced polymer composites (GFRP) and plain weave carbon fiber-reinforced polymer composites (CFRP) is sensed by utilizing a spray-on nanocomposite sensor, which is then instrumented by boundary electrodes. The resistance change distribution within the sensor area is reconstructed from a series of boundary voltage measurements, and ERT is implemented using a maximum a posteriori approach and assumptions on the type of noise in the reconstruction. Results show that this technique has promise in tracking uniaxial damage in composites. The different fiber architectures (unidirectional GFRP, plain weave CFRP) give distinct features in the ERT, which are consistent with the physical behavior of the tested samples.

  3. Effects of manufacturing techniques on the flexural behavior of steel fiber-reinforced concrete

    SciTech Connect

    Toutanji, H.; Bayasi, Z.

    1998-01-01

    This paper presents experimental research investigating the effects of manufacturing techniques on the mechanical properties of steel fiber-reinforced concrete. Both the effects of curing environments and that of testing direction relative to casting direction on the mechanical properties of fiber-reinforced concrete are reported. Specimens were cured in three different environmental conditions: steam, moisture, and air. Results show that steam curing, as compared to moisture curing, does not enhance the flexural strength of steel fibrous concrete but does reduce flexural toughness. As expected, air curing shows detrimental effects on all aspects of the test results, as compared to steam and moisture curing. The flexural behavior of steel fiber-reinforced concrete is strongly affected by testing direction. When testing direction is perpendicular to casting direction, specimens exhibit reductions in both flexural strength and toughness compared to the case when testing and casting directions are parallel. The effect of testing direction relative to casting direction on flexural strength and toughness increases with increasing the flowability (workability) of the fibrous mixture, which encourages fiber settlement during placement.

  4. Putty Index: An Important Aid for the Direct Fabrication of Fiber Reinforced Composite Resin FPD.

    PubMed

    Gupta, Nidhi; Singh, Kunwarjeet

    2014-12-01

    Fiber reinforced composite resin fixed partial dentures (FRCFPD) with composite resin, PFM or all ceramic pontic can be used as a short term or long term alternative to conventional fixed partial dentures or implant supported crown in young patients where conventional FPD is contraindicated (large pulp chambers) or in patient's unwilling to invasive implant placement surgical procedure and those who do not want to allow preparation of natural sound abutments for placement of retainers for FPD. FRCFPD can be successfully used for replacing missing anterior tooth (Turker and Sener, J Prosthet Dent 100:254-258, 2008), in conditions which allows minimum occlusal loading of pontic, over jet and overbite not greater than 3 mm (Ricketts, Provocations and perceptions in craniofacial orthopedics: dental science and facial art/parts 1 and 2. Rocky Mountain Orthodontics, Denver, p 7023, 1990) and structurally sound and intact abutments for the fiber reinforced matrix (Rose et al., Quintessence Int 33:579-583, 2002). The successful esthetic and functional rehabilitation of missing tooth with fiber reinforced composite resin FPD depends on accurate positioning of pontic in patient's mouth. It is difficult to hold the pontic in proper position with instrument or fingers while direct fabrication in mouth. For accurate positioning, stabilization of pontic is very important which can be achieved with putty index. Putty index maintain pontic in accurate mesiodistal, labiolingual and cervicoincisal position while fabricating FRCFPD directly. PMID:26199513

  5. Fatigue Hysteresis of Carbon Fiber-Reinforced Ceramic-Matrix Composites at Room and Elevated Temperatures

    NASA Astrophysics Data System (ADS)

    Li, Longbiao

    2016-02-01

    When the fiber-reinforced ceramic-matrix composites (CMCs) are first loading to fatigue peak stress, matrix multicracking and fiber/matrix interface debonding occur. Under fatigue loading, the stress-strain hysteresis loops appear as fiber slipping relative to matrix in the interface debonded region upon unloading/reloading. Due to interface wear at room temperature or interface oxidation at elevated temperature, the interface shear stress degredes with increase of the number of applied cycles, leading to the evolution of the shape, location and area of stress-strain hysteresis loops. The evolution characteristics of fatigue hysteresis loss energy in different types of fiber-reinforced CMCs, i.e., unidirectional, cross-ply, 2D and 2.5D woven, have been investigated. The relationships between the fatigue hysteresis loss energy, stress-strain hysteresis loops, interface frictional slip, interface shear stress and interface radial thermal residual stress, matrix stochastic cracking and fatigue peak stress of fiber-reinforced CMCs have been established.

  6. Effect of diameter of glass fibers on flexural properties of fiber-reinforced composites.

    PubMed

    Obukuro, Motofumi; Takahashi, Yutaka; Shimizu, Hiroshi

    2008-07-01

    This study investigated the effect of the diameter of glass fibers on the flexural properties of fiber-reinforced composites. Bar-shaped test specimens of highly filled fiber-reinforced composites (FRCs) and FRC of 30 vol% fiber content were made from a light-cured dimethacrylate monomer liquid (mixture of urethane dimethacrylate and triethylene glycol dimethacrylate) with silanized E-glass fibers (7, 10, 13, 16, 20, 25, 30, and 45 microm in diameter). Flexural strength and elastic modulus were measured. The flexural strength of the highly filled FRCs increased with increasing fiber diameter. In particular, the strengths of highly filled FRCs with 20-, 25-, 30-, and 45-microm-diameter fibers was significantly higher than the others (p<0.05). The flexural strength of FRC of 30 vol% fiber content increased with increasing fiber diameter, except for the FRC with 45-microm-diameter fibers; FRCs with 20-, 25-, and 30-microm-diameter fibers were significantly stronger than the others (p<0.05). Therefore, it was revealed that the diameter of glass fibers significantly affected the flexural properties of fiber-reinforced composites. PMID:18833767

  7. Acousto-ultrasonic characterization of fiber reinforced composites

    NASA Technical Reports Server (NTRS)

    Vary, A.

    1981-01-01

    The acousto-ultrasonic technique combines advantageous aspects of acoustic emission and ultrasonic methodologies. Acousto-ultrasonics operates by introducing a repeating series of ultrasonic pulses into a material. The waves introduced simulate the spontaneous stress waves that would arise if the material were put under stress as in the case of acoustic emission measurements. These benign stress waves are detected by an acoustic emission sensor. The physical arrangement of the ultrasonic (input) transducer and acoustic emission (output) sensor is such that the resultant waveform carries an imprint of morphological factors that govern or contribute to material performance. The output waveform is complex, but it can be quantitized in terms of a 'stress wave factor.' The stress wave factor, which can be defined in a number of ways, is a relative measure of the efficiency of energy dissipation in a material. If flaws or other material anomalies exist in the volume being examined, their combined effect appears in the stress wave factor.

  8. Development and Characterization of UHMWPE Fiber-Reinforced Hydrogels For Meniscal Replacement

    NASA Astrophysics Data System (ADS)

    Holloway, Julianne Leigh

    Meniscal tears are the most common orthopedic injuries to the human body. The current treatment of choice, however, is a partial meniscectomy that leads to osteoarthritis proportional to the amount of tissue removed. As a result, there is a significant clinical need to develop materials capable of restoring the biomechanical contact stress distribution to the knee after meniscectomy and preventing the onset of osteoarthritis. In this work, a fiber-reinforced hydrogel-based synthetic meniscus was developed that allows for tailoring of the mechanical properties and molding of the implant to match the size, shape, and property distribution of the native tissue. Physically cross-linked poly(vinyl alcohol) (PVA) hydrogels were reinforced with ultrahigh molecular weight polyethylene (UHMWPE) fibers and characterized in compression (0.1-0.8 MPa) and tension (0.1-250 MPa) showing fine control over mechanical properties within the range of the human meniscus. Morphology and crystallinity analysis of PVA hydrogels showed increases in crystallinity and PVA densification, or phase separation, with freeze-thaw cycles. A comparison of freeze-thawed and aged, physically cross-linked hydrogels provided insight on both crystallinity and phase separation as mechanisms for PVA gelation. Results indicated both mechanisms independently contributed to hydrogel modulus for freeze-thawed hydrogels. In vitro swelling studies were performed using osmotic solutions to replicate the swelling pressure present in the knee. Minimal swelling was observed for hydrogels with a PVA concentration of 30-35 wt%, independently of hydrogel freeze-thaw cycles. This allows for independent tailoring of hydrogel modulus and pore structure using freeze-thaw cycles and swelling behavior using polymer concentration to match a wide range of properties needed for various soft tissue applications. The UHMWPE-PVA interface was identified as a significant weakness. To improve interfacial adhesion, a novel

  9. Modeling and numerical simulation of the progressive failure of pultruded fiber-reinforced plastic structures

    NASA Astrophysics Data System (ADS)

    Yin, Jianshen

    Fiber reinforced plastic pultruded (FRP) materials generally fail in a brittle manner. After first failure, a small increment of applied load can cause the failure to propagate to neighboring regions in the material and seriously reduce the load carrying capacity of the FRP structure. Two methods are being developed to model progressive failure of solid structures by the finite element method. One method is based on reduction of the stiffness components of failed elements. The other is based on node/element separation so that the failure configuration of the structure can be simulated. The latter one is more appropriate to large scales of failures. This method has been applied mainly in explicit finite element codes. In an explicit code, which is appropriate to transient dynamic problems, the solution is at element level at each time step. No global stiffness matrix is needed. In an implicit code, which is appropriate for static or quasi-static problems, the global stiffness matrix must be assembled at each time step. The geometrical configuration of the finite element model at failure changes the global stiffness matrix. Therefore, implementing the node separation method in an implicit code is more difficult than in an explicit code. Although efforts have been made to model static failure problems with explicit codes using dynamic relaxation, the results of these tests have been disappointing. The computational methods for progressive failures of statics problems will need to rely on implicit codes. This thesis presents a methodology for implementing the node/element separation method in an implicit code. Numerical strategies such as constrained node pairs with failure, releasing constraints and regenerating node-variable relations, are proposed to accomplish this task. The modifications to the general implicit time procedure due to the inclusion of this method are investigated in detail. NIKE3D, a 3-D implicit finite element code, was employed to test this method

  10. Creep deformation characteristics of ductile discontinuous fiber reinforced composites

    SciTech Connect

    Biner, S.B.

    1993-10-01

    Role of material parameters and geometric parameters of ductile reinforcing phase on the creep deformation behavior of 20% discontinuously reinforced composite was numerically investigated including debonding and pull-out mechanisms. Results indicate that for rigidly bonded interfaces, the creep rate of the composite is not significantly influenced by the material properties and geometric parameters of the ductile reinforcing phase due to development of large hydrostatic stress and constrained deformation in the reinforcement. For debonding interfaces, the geometric parameters of the reinforcing phase are important; however, event with very weak interfacial behavior low composite creep rates can be achieved by suitable selection of the geometric parameters of the ductile reinforcing phase.

  11. Fatigue of continuous fiber reinforced titanium matrix composites

    NASA Technical Reports Server (NTRS)

    Johnson, W. S.

    1991-01-01

    Several lay-ups of SCS-6/Ti-15-3 composites were investigated. Static and fatigue tests were conducted for both notched and unnotched specimens at room and elevated temperatures. Test results indicated that the stress in the 0 fibers is the controlling factor in fatigue life. The static and fatigue strength of these materials is shown to be dependent on the level of residual stresses and the fiber/ matrix interfacial strength. Fatigue tests of notched specimens showed that cracks can initiate and grow many fiber spacings in the matrix material without breaking fibers. These matrix cracks can significantly reduce the residual strength of notched composite.

  12. Properties of fiber reinforced plastics about static and dynamic loadings

    NASA Astrophysics Data System (ADS)

    Kudinov, Vladimir V.; Korneeva, Natalia V.

    2016-05-01

    A method for investigation of impact toughness of anisotropic polymer composite materials (reinforced plastics) with the help of CM model sample in the configuration of microplastic (micro plastic) and impact pendulum-type testing machine under static and dynamic loadings has been developed. The method is called "Break by Impact" (Impact Break IB). The estimation of impact resistance CFRP by this method showed that an increase in loading velocity ~104 times the largest changes occurs in impact toughness and deformation ability of a material.

  13. High-Temperature Creep Behavior Of Fiber-Reinforced Niobium

    NASA Technical Reports Server (NTRS)

    Petrasek, Donald W.; Titran, Robert H.

    1990-01-01

    Study conducted to determine feasibility of using composite materials in advanced space power systems, described in 22-page report. Tungsten fibers reduce creep and mass in advanced power systems. Reinforcing niobium alloys with tungsten fibers increases their resistances to creep by factors of as much as 10.

  14. Health monitoring of precast bridge deck panels reinforced with glass fiber reinforced polymer bars

    NASA Astrophysics Data System (ADS)

    Ries, James Mcdaniel

    The Beaver Creek Bridge on US highway 6 is the pilot project for Glass Fiber Reinforced Polymer (GFRP) bridge decks and posttensioned bridge decks in the state of Utah. The bridge was built in 2009, using accelerated bridge construction practices, including the use of precast prestressed girders, as well as precast decking. The westbound bridge decking was composed of 12 precast panels each measuring 41'-5" long, 6'-10" wide, and 9¼" thick, and weighing approximately 33 kips. At the time, these panels were the longest GFRP panels in the United States. The Utah Department of Transportation has decided to evaluate GFRP reinforcing bars as an alternative to steel rebar in this bridge deck. The hope is to increase the lifespan of bridge decks to match the service life of the entire bridge. Due to the nature of the GFRP bars, the panels were lifted at four points using straps instead of imbedded anchors. During the four-point lifting, the panels exhibited small deflections and strains; furthermore, no cracks larger than hairline cracks were found in the panels after lifting. The Beaver Creek Bridge deck is the first precast deck in the state of Utah to be posttensioned in the direction of traffic. Posttensioning bridge decks is expected to become the norm in the state of Utah. The posttensioning resulted in increased continuity between panels. In order to quantify the expected performance of the bridge during its service life, a truck load test was performed. The truck load test was comprised of a static and dynamic test. During the truck load test, the bridge experienced deflections in the panels which were 93% below design values. Girder deflections were also small. The use of GFRP bars has the potential to extend the life of bridge decks exposed to deicing salts from 45 years to 100 years, while only requiring an increased capital cost in the bridge of 8%. Furthermore, the use of GFRP bars in conjunction with accelerated building practices has the potential to

  15. Characterization of a carbon fiber reinforced polymer repair system for structurally deficient steel piping

    NASA Astrophysics Data System (ADS)

    Wilson, Jeffrey M.

    This Dissertation investigates a carbon fiber reinforced polymer repair system for structurally deficient steel piping. Numerous techniques exist for the repair of high-pressure steel piping. One repair technology that is widely gaining acceptance is composite over-wraps. Thermal analytical evaluations of the epoxy matrix material produced glass transition temperature results, a cure kinetic model, and a workability chart. These results indicate a maximum glass transition temperature of 80°C (176°F) when cured in ambient conditions. Post-curing the epoxy, however, resulted in higher glass-transition temperatures. The accuracy of cure kinetic model presented is temperature dependent; its accuracy improves with increased cure temperatures. Cathodic disbondment evaluations of the composite over-wrap show the epoxy does not breakdown when subjected to a constant voltage of -1.5V and the epoxy does not allow corrosion to form under the wrap from permeation. Combustion analysis of the composite over-wrap system revealed the epoxy is flammable when in direct contact with fire. To prevent combustion, an intumescent coating was developed to be applied on the composite over-wrap. Results indicate that damaged pipes repaired with the carbon fiber composite over-wrap withstand substantially higher static pressures and exhibit better fatigue characteristics than pipes lacking repair. For loss up to 80 percent of the original pipe wall thickness, the composite over-wrap achieved failure pressures above the pipe's specified minimum yield stress during monotonic evaluations and reached the pipe's practical fatigue limit during cyclical pressure testing. Numerous repairs were made to circular, thru-wall defects and monotonic pressure tests revealed containment up to the pipe's specified minimum yield strength for small diameter defects. The energy release rate of the composite over-wrap/steel interface was obtained from these full-scale, leaking pipe evaluations and results

  16. Optimal design of variable-stiffness fiber-reinforced composites using cellular automata

    NASA Astrophysics Data System (ADS)

    Setoodeh, Shahriar

    The growing number of applications of composite materials in aerospace and naval structures along with advancements in manufacturing technologies demand continuous innovations in the design of composite structures. In the traditional design of composite laminates, fiber orientation angles are constant for each layer and are usually limited to 0, 90, and +/-45 degrees. To fully benefit from the directional properties of composite laminates, such limitations have to be removed. The concept of variable-stiffness laminates allows the stiffness properties to vary spatially over the laminate. Through tailoring of fiber orientations and laminate thickness spatially in an optimal fashion, mechanical properties of a part can be improved. In this thesis, the optimal design of variable-stiffness fiber-reinforced composite laminates is studied using an emerging numerical engineering optimization scheme based on the cellular automata paradigm. A cellular automaton (CA) based design scheme uses local update rule for both field variables (displacements) and design variables (lay-up configuration and laminate density measure) in an iterative fashion to convergence to an optimal design. In the present work, the displacements are updated based on the principle of local equilibrium and the design variables are updated according to the optimality criteria for minimum compliance design. A closed form displacement update rule for constant thickness isotropic continua is derived, while for the general anisotropic continua with variable thickness a numeric update rule is used. Combined lay-up and topology design of variable-stiffness flat laminates is performed under the action of in-plane loads and bending loads. An optimality criteria based formulation is used to obtain local design rules for minimum compliance design subject to a volume constraint. It is shown that the design rule splits into a two step application. In the first step an optimal lay-up configuration is computed and in

  17. Effects of Fiber-reinforced Composite Bases on Microleakage of Composite Restorations in Proximal Locations

    PubMed Central

    A, Tezvergil-Mutluay; P.K, Vallittu

    2014-01-01

    Objectives: The aim of this study was to evaluate the microleakage of direct restorative composite resin upon the addition of an intermediate glass fiber-reinforced composite (GFRC) layer of various fiber orientations between tooth and particulate filler composite resin (PFRC). Materials and Methods: Cavities were prepared both on the mesial and distal surfaces of sixty extracted human molars with one margin placed below and the other above the cementoenamel junction (CEJ). Teeth were assigned to five different groups. Four of the groups received a layer of semi-interpenetrating polymer network (semi-IPN) resin system impregnated E-glass GFRC at the bottom of the cavity: Group 1; unidirectional continuous GFRC (EVS) in buccolingual direction (EVS-BL), Group 2; EVS in mesiodistal direction (EVS-MD), Group 3; bidirectional woven GFRC (EVN), Group 4; multidirectional short GFRC (EXP-MLT), Group 5; PRFC only (control). After acid etching and priming of the cavities and insertion of GFRC layer with the adhesive resin (Scotchbond Multipurpose 3M-ESPE), the cavities were filled incrementally with PRFC (Filtek Z250, 3M-ESPE) and each layer was light cured for 20 s. After finishing and polishing, the restored teeth were water-stored for 24 h at 37 °C and then thermocycled for 6000 cycles between 5-55 °C, before immersion in 0.5 % basic fuchsin dye for 24 h. After sectioning by 3-5 sagittal cuts, each sequential section was imaged and digitally analyzed to determine the stain depth. Results: All GFRC groups in dentin revealed significantly lower microleakage compared to control (p<0.05). The orientation of FRC intermediate layer did not reveal significant differences in microleakage (p>0.05). The microleakeage in enamel was not different between the groups (p>0.05). Conclusion: Use of intermediate GFRC layer between tooth and PFRC could provide alternative method to minimize microleakage. Clinical Relevance: Use of GFRC intermediate layer underneath the particulate filler

  18. Damage evolution in uniaxial silicon carbide fiber-reinforced titanium matrix composites

    NASA Astrophysics Data System (ADS)

    Hanan, Jay Clarke

    Fiber fractures initiate damage zones ultimately determining the strength and lifetime of metal matrix composites (MMCs). The evolution of damage in a MMC comprising a row of unidirectional SiC fibers (32 vol.%) surrounded by a Ti matrix was examined using X-ray microdiffraction (gym beam size) and macrodiffraction (mm beam size). A comparison of high-energy X-ray diffraction (XRD) techniques including a powerful two-dimensional XRD method capable of obtaining powder averaged strains from a small number of grains is presented (HEmuXRD2). Using macrodiffraction, the bulk residual strain in the composite was determined against a true strain-free reference. In addition, the bulk in situ response of both the fiber reinforcement and the matrix to tensile stress was observed and compared to a three-dimensional finite element model. Using microdiffraction, multiple strain maps including both phases were collected in situ before, during, and after the application of tensile stress, providing an unprecedented detailed picture of the micromechanical behavior in the laminate metal matrix composite. Finally, the elastic axial strains were compared to predictions from a modified shear lag model, which unlike other shear lag models, considers the elastic response of both constituents. The strains showed excellent correlation with the model. The results confirmed, for the first time, both the need and validity of this new model specifically developed for large scale multifracture and damage evolution simulations of metal matrix composites. The results also provided unprecedented insight for the model, revealing the necessity of incorporating such factors as plasticity of the matrix, residual stress in the composite, and selection of the load sharing parameter. The irradiation of a small number of grains provided strain measurements comparable to a continuum mechanical state in the material. Along the fiber axes, thermal residual stresses of 740 MPa (fibers) and +350 MPa (matrix

  19. Surface analysis of grapite fiber reinforced polyimide composites. I

    NASA Technical Reports Server (NTRS)

    Messick, D. L.; Wightman, J. P.; Progar, D. J.

    1983-01-01

    The results of experimental analyses of the effects of pretreatment on bonding between composite materials are reported. The materials comprised graphite fibers in a polyimide matrix. The surfaces were bonded as-received or subjected to grit blasting, bead blasting, hand sanding, washes with ethanolic KOH, NH2NH2-H2O or H2SO4 + 0.30 H2O2 or flashblasting. SEM and X-ray photoelectron spectroscopy revealed fluorine contents in the as-received samples. Contact angles were determined by means of five different liquids with various surface tensions. The flashblast technique removed all fluorine from the samples. Low critical surface tensions were found in the composite surfaces with high fluorine concentrations. The surface scanning techniques are concluded to be useful for studying factors influencing the strength and durability of adhesively bonded composites.

  20. Flexural analysis of palm fiber reinforced hybrid polymer matrix composite

    NASA Astrophysics Data System (ADS)

    Venkatachalam, G.; Gautham Shankar, A.; Raghav, Dasarath; Santhosh Kiran, R.; Mahesh, Bhargav; Kumar, Krishna

    2015-07-01

    Uncertainty in availability of fossil fuels in the future and global warming increased the need for more environment friendly materials. In this work, an attempt is made to fabricate a hybrid polymer matrix composite. The blend is a mixture of General Purpose Resin and Cashew Nut Shell Liquid, a natural resin extracted from cashew plant. Palm fiber, which has high strength, is used as reinforcement material. The fiber is treated with alkali (NaOH) solution to increase its strength and adhesiveness. Parametric study of flexure strength is carried out by varying alkali concentration, duration of alkali treatment and fiber volume. Taguchi L9 Orthogonal array is followed in the design of experiments procedure for simplification. With the help of ANOVA technique, regression equations are obtained which gives the level of influence of each parameter on the flexure strength of the composite.