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Sample records for horizontal-typed mocvd chamber

  1. Safety-Enclosure System For MOCVD Process Chamber

    NASA Technical Reports Server (NTRS)

    Singletery, James, Jr.; Velasquez, Hugo; Warner, Joseph

    1995-01-01

    Safety-enclosure system filled with nitrogen surrounds reaction chamber in which metallo-organic chemical vapor deposition (MOCVD) performed. Designed to protect against explosions and/or escaping toxic gases and particulates. Gas-purification subsystem ensures during loading and unloading of process materials, interior of MOCVD chamber exposed to less than 1 ppm of oxygen and less than 5 ppm of water in nitrogen atmosphere. Toxic byproducts of MOCVD process collected within inert atmosphere. Enclosure strong enough to contain any fragments in unlikely event of explosion.

  2. Solid source MOCVD system

    DOEpatents

    Hubert, Brian N.; Wu, Xin Di

    1998-01-01

    A system for MOCVD fabrication of superconducting and non-superconducting oxide films provides a delivery system for the feeding of metalorganic precursors for multi-component chemical vapor deposition. The delivery system can include multiple cartridges containing tightly packed precursor materials. The contents of each cartridge can be ground at a desired rate and fed together with precursor materials from other cartridges to a vaporization zone and then to a reaction zone within a deposition chamber for thin film deposition.

  3. Solid source MOCVD system

    DOEpatents

    Hubert, B.N.; Wu, X.D.

    1998-10-13

    A system for MOCVD fabrication of superconducting and non-superconducting oxide films provides a delivery system for the feeding of metallorganic precursors for multi-component chemical vapor deposition. The delivery system can include multiple cartridges containing tightly packed precursor materials. The contents of each cartridge can be ground at a desired rate and fed together with precursor materials from other cartridges to a vaporization zone and then to a reaction zone within a deposition chamber for thin film deposition. 13 figs.

  4. Vacuum MOCVD fabrication of high efficience cells

    NASA Technical Reports Server (NTRS)

    Partain, L. D.; Fraas, L. M.; Mcleod, P. S.; Cape, J. A.

    1985-01-01

    Vacuum metal-organic-chemical-vapor-deposition (MOCVD) is a new fabrication process with improved safety and easier scalability due to its metal rather than glass construction and its uniform multiport gas injection system. It uses source materials more efficiently than other methods because the vacuum molecular flow conditions allow the high sticking coefficient reactants to reach the substrates as undeflected molecular beams and the hot chamber walls cause the low sticking coefficient reactants to bounce off the walls and interact with the substrates many times. This high source utilization reduces the materials costs power device and substantially decreases the amounts of toxic materials that must be handled as process effluents. The molecular beams allow precise growth control. With improved source purifications, vacuum MOCVD has provided p GaAs layers with 10-micron minority carrier diffusion lengths and GaAs and GaAsSb solar cells with 20% AMO efficiencies at 59X and 99X sunlight concentration ratios. Mechanical stacking has been identified as the quickest, most direct and logical path to stacked multiple-junction solar cells that perform better than the best single-junction devices. The mechanical stack is configured for immediate use in solar arrays and allows interconnections that improve the system end-of-life performance in space.

  5. In-situ thin films by MOCVD

    SciTech Connect

    Norris, P.E.; Orlando, G.W. )

    1990-01-01

    This paper reports on the growth of high quality yttrium barium copper oxide (YBCO) thin films by MOCVD. Three MOCVD processes have been studied: a two-step (growth/post anneal) process requiring O{sub 2} anneal at 950--980 C, an in-situ (one step, no post growth anneal) process at 800--850 C and a plasma-enhanced, in-situ process (PE-MOCVD), which is operable at still lower substrate temperatures. The in-situ PE-MOCVD process is of great interest since, to a substantial degree, the growth temperature determines the degree of compatibility of a process with substrate materials and existing device technologies, such as VLSI-SilicoVLSI-Silicon.

  6. MOCVD OF YSZ COATINGS USING ?-DIKETONATE PRECURSORS

    SciTech Connect

    Varanasi, Venu G; Besmann, Theodore M; Hyde, Robin L.; Payzant, E Andrew; Anderson, Timothy J

    2009-01-01

    Metallorganic chemical vapor deposition (MOCVD) was used to fabricate yttria-stabilized zirconia as a thermal barrier coating. The MOCVD precursors were Y(tmhd)3 and Zr(tmhd)4 (tmhd = 2, 2, 6, 6-tetramethyl-3, 5-heptanedianato) and delivered via aerosol assisted liquid delivery (AALD). The maximum tetragonal YSZ coating rate was 14.2 1.3 m h -1 (at 845oC) yielding a layered coating microstructure. The growth was first-order with temperature (T < 827oC) with an apparent activation energy (Ea) of 50.9 4.3 kJ mol -1. Coating efficiency was a maximum of approximately 10% at the highest growth rate.

  7. MOCVD deposition of YSZ on stainless steels

    NASA Astrophysics Data System (ADS)

    Chevalier, S.; Kilo, M.; Borchardt, G.; Larpin, J. P.

    2003-01-01

    Yttria stabilized zirconia was deposited on stainless steel using the metal-organic chemical vapor deposition (MOCVD) technique, from β-diketonate precursors. The variation of the evaporation temperatures of yttrium and zirconium precursor allowed to control the level of Y within the film. Over the temperature range 125-150 °C, the Y content increased from 2.5 to 17.6 at.%. X-ray diffraction (XRD) analyses evidenced tetragonal phase of zirconia when the Y content was below 8 at.%, and cubic phase for higher concentration. Sputtered neutral mass spectrometry (SNMS) profiles confirmed that the control and stability of Y precursor temperature were of major importance to guarantee the homogeneity of the deposited films.

  8. Flow chamber

    DOEpatents

    Morozov, Victor

    2011-01-18

    A flow chamber having a vacuum chamber and a specimen chamber. The specimen chamber may have an opening through which a fluid may be introduced and an opening through which the fluid may exit. The vacuum chamber may have an opening through which contents of the vacuum chamber may be evacuated. A portion of the flow chamber may be flexible, and a vacuum may be used to hold the components of the flow chamber together.

  9. Transport phenomena and the effects of reactor geometry for epitaxial GaN growth in a vertical MOCVD reactor

    NASA Astrophysics Data System (ADS)

    Tseng, Chien-Fu; Tsai, Tsung-Yen; Huang, Yen-Hsiu; Lee, Ming-Tsang; Horng, Ray-Hua

    2015-12-01

    In this study a numerical simulation was carried out to analyze the transport phenomena in a vertical type metal organic chemical vapor deposition (MOCVD) reactor for Gallium Nitride (GaN) growth. The simulated results were compared and validated by experiment. The effects of showerhead design and chamber height are investigated and discussed. It was found that, by properly adjusting the height of the chamber, both the growth rate and film uniformity could be significantly improved. This is attributed to the suppression of the thermal and mass transfer boundary layers by the injection flow of reacting gas mixtures, as well as the confined vertical vortices caused by the geometry of the reduced space. However, inappropriate design of the distance between the showerhead and the susceptor can result in uneven distribution of the organic source in the vicinity of the substrate surface resulting in an uneven growth rate of the GaN film. Consequently, there exists an optimal chamber height that will give the best growth rate and uniformity to the GaN film as discussed in this study. This study provides comprehensive insight into the transport phenomena of GaN growth that includes coupled heat and mass transfer as well as chemical reactions. The results provide important information in a succinct format and enable decisions to be made about the showerhead and the geometrical design and size of a vertical MOCVD reactor.

  10. Radiative efficiency of MOCVD grown QD lasers

    NASA Astrophysics Data System (ADS)

    Mawst, Luke; Tsvid, Gene; Dudley, Peter; Kirch, Jeremy; Park, J. H.; Kim, N.

    2010-02-01

    The optical spectral gain characteristics and overall radiative efficiency of MOCVD grown InGaAs quantum dot lasers have been evaluated. Single-pass, multi-segmented amplified spontaneous emission measurements are used to obtain the gain, absorption, and spontaneous emission spectra in real units. Integration of the calibrated spontaneous emission spectra then allows for determining the overall radiative efficiency, which gives important insights into the role which nonradiative recombination plays in the active region under study. We use single pass, multi-segmented edge-emitting in which electrically isolated segments allow to vary the length of a pumped region. In this study we used 8 section devices (the size of a segment is 50x300 μm) with only the first 5 segments used for varying the pump length. The remaining unpumped segments and scribed back facet minimize round trip feedback. Measured gain spectra for different pump currents allow for extraction of the peak gain vs. current density, which is fitted to a logarithmic dependence and directly compared to conventional cavity length analysis, (CLA). The extracted spontaneous emission spectrum is calibrated and integrated over all frequencies and modes to obtain total spontaneous radiation current density and radiative efficiency, ηr. We find ηr values of approximately 17% at RT for 5 stack QD active regions. By contrast, high performance InGaAs QW lasers exhibit ηr ~50% at RT.

  11. Bakeout Chamber Within Vacuum Chamber

    NASA Technical Reports Server (NTRS)

    Taylor, Daniel M.; Soules, David M.; Barengoltz, Jack B.

    1995-01-01

    Vacuum-bakeout apparatus for decontaminating and measuring outgassing from pieces of equipment constructed by mounting bakeout chamber within conventional vacuum chamber. Upgrade cost effective: fabrication and installation of bakeout chamber simple, installation performed quickly and without major changes in older vacuum chamber, and provides quantitative data on outgassing from pieces of equipment placed in bakeout chamber.

  12. Exposure chamber

    DOEpatents

    Moss, Owen R.; Briant, James K.

    1983-01-01

    An exposure chamber includes an imperforate casing having a fluid inlet at the top and an outlet at the bottom. A single vertical series of imperforate trays is provided. Each tray is spaced on all sides from the chamber walls. Baffles adjacent some of the trays restrict and direct the flow to give partial flow back and forth across the chambers and downward flow past the lowermost pan adjacent a central plane of the chamber.

  13. In-situ deposition of YBCO high-Tc superconducting thin films by MOCVD and PE-MOCVD

    NASA Technical Reports Server (NTRS)

    Zhao, J.; Noh, D. W.; Chern, C.; Li, Y. Q.; Norris, P. E.; Kear, B.; Gallois, B.

    1991-01-01

    Metal-Organic Chemical Vapor Deposition (MOCVD) offers the advantages of a high degree of compositional control, adaptability for large scale production, and the potential for low temperature fabrication. The capability of operating at high oxygen partial pressure is particularly suitable for in situ formation of high temperature superconducting (HTSC) films. Yttrium barium copper oxide (YBCO) thin films having a sharp zero-resistance transition with T(sub c) greater than 90 K and J(sub c) of approximately 10(exp 4) A on YSZ have been prepared, in situ, at a substrate temperature of about 800 C. Moreover, the ability to form oxide films at low temperature is very desirable for device applications of HTSC materials. Such a process would permit the deposition of high quality HTSC films with a smooth surface on a variety of substrates. Highly c-axis oriented, dense, scratch resistant, superconducting YBCO thin films with mirror-like surfaces have been prepared, in situ, at a reduced substrate temperature as low as 570 C by a remote microwave-plasma enhanced metal-organic chemical vapor deposition (PE-MOCVD) process. Nitrous oxide was used as a reactant gas to generate active oxidizing species. This process, for the first time, allows the formation of YBCO thin films with the orthorhombic superconducting phase in the as-deposited state. The as-deposited films grown by PE-MOCVD show attainment of zero resistance at 72 K with a transition width of about 5 K. MOCVD was carried out in a commercial production scale reactor with the capability of uniform deposition over 100 sq cm per growth run. Preliminary results indicate that PE-MOCVD is a very attractive thin film deposition process for superconducting device technology.

  14. In Situ deposition of YBCO high-T(sub c) superconducting thin films by MOCVD and PE-MOCVD

    NASA Technical Reports Server (NTRS)

    Zhao, J.; Noh, D. W.; Chern, C.; Li, Y. Q.; Norris, P.; Gallois, B.; Kear, B.

    1990-01-01

    Metalorganic Chemical Vapor Deposition (MOCVD) offers the advantages of a high degree of compositional control, adaptability for large scale production, and the potential for low temperature fabrication. The capability of operating at high oxygen partial pressure is particularly suitable for in situ formation of high temperature superconducting (HTSC) films. Yttrium barium copper oxide (YBCO) thin films having a sharp zero-resistance transition with T( sub c) greater than 90 K and Jc approx. 10 to the 4th power A on YSZ have been prepared, in situ, at a substrate temperature of about 800 C. Moreover, the ability to form oxide films at low temperature is very desirable for device applications of HTSC materials. Such a process would permit the deposition of high quality HTSC films with a smooth surface on a variety of substrates. Highly c-axis oriented, dense, scratch resistant, superconducting YBCO thin films with mirror-like surfaces have been prepared, in situ, at a reduced substrate temperature as low as 570 C by a remote microwave-plasma enhanced metalorganic chemical vapor deposition (PE-MOCVD) process. Nitrous oxide was used as a reactant gas to generate active oxidizing species. This process, for the first time, allows the formation of YBCO thin films with the orthorhombic superconducting phase in the as-deposited state. The as-deposited films grown by PE-MOCVD show attainment of zero resistance at 72 K with a transition width of about 5 K. MOCVD was carried out in a commercial production scale reactor with the capability of uniform deposition over 100 sq cm per growth run. Preliminary results indicate that PE-MOCVD is a very attractive thin film deposition process for superconducting device technology.

  15. A synergistic approach to environmental concerns in large scale MOCVD processes

    SciTech Connect

    Thompson, A.G.; Tompa, G.S.; Zawadzki, P.A.; McKee, M.; Beckham, C.; Powers, A.; Gurary, A.; Moy, K.; Schumaker, N.E.

    1994-12-31

    Processes used in the production of epitaxial III-V semiconducting materials employ a wide variety of materials that are environmentally hazardous. As production volumes increase, the need to manage these materials becomes a serious concern. As the leading supplier of production scale single and multi-wafer MOCVD systems, EMCORE has taken the approach of minimizing the generation of waste by designing a reactor for high reactant utilization efficiency, and then trapping the remainder so that the exhaust stream is clean. They have paid particular attention to both operational efficiency and operator safety. The trapped materials are reduced to an inert state for subsequent commercial disposal; this is particularly important for phosphorus, which can be highly flammable if improperly handled. The reactor chamber deposits occur below the wafer level and typically are cleaned only after several hundred deposition cycles. These factors contribute to a quick cycle time and high uptime, both of which increase throughput. These issues become more important as the reactor size is increased and when multiple shifts are utilized. These points are exemplified by the operational experience with the new Enterprise series, which holds four 100 mm wafers (or seventeen 50mm wafers) per run. The authors will discuss the progressive trapping of solid As and P compounds and those hydride gases which are not completely decomposed in the reaction chamber. The use of computer modeling to scale the process to larger dimensions and to optimize the deposition conditions will also be discussed.

  16. From research to manufacture—The evolution of MOCVD

    NASA Astrophysics Data System (ADS)

    Grodzinski, Piotr; Denbaars, Steven P.; Lee, H. C.

    1995-12-01

    The article provides an overview of the manufacturing capabilities of metalorganic chemical vapor deposition (MOCVD) technology and describes its application to the growth and fabrication of devices in three different material groups: AlGaAs/GaAs, AlInGaP, and AlGaN/GaN. Discussed are GaN blue light-emitting diodes (LEDs), AlInGaP red and yellow LEDs, and AlGaAs/GaAs vertical cavity surface-emitting lasers and high-electron-mobility transistors. Based on these examples, the evolution of MOCVD technology from fundamental materials studies and advanced materials development through the early stages of pilot manufacturing and large-volume manufacturing capabilities is demonstrated.

  17. Surface Stoichiometry, Structure, and Kinetics of GaAs MOCVD

    SciTech Connect

    Baucom, K.C.; Creighton, J.R.; Moffat, H.K.

    1999-01-29

    We have used reflectance-difference spectroscopy (RDS) to examine the surface phases of GaAs(100) during metalorganic chemical vapor deposition (MOCVD). Since the identities of two important surface phases were unknown, we determined their structure and stoichiometry using a variety of surface science techniques. The Type III phase is a newly characterized As-rich (1 X 2)-CH{sub 3} reconstruction. The Type II phase is a metastable derivative of the Type I phase. RDS also indicates that the surface during MOCVD has a considerable degree of heterogeneity. Deposition rates were measured over a similar range of conditions and the kinetically-limited regime was found to correlate with the Type III phase. A simple kinetic model was found to quantitatively describe the deposition rates.

  18. Study of high [Tc] superconducting thin films grown by MOCVD

    SciTech Connect

    Erbil, A.

    1990-01-01

    Work is described briefly, which was carried out on development of techniques to grow metal-semiconductor superlattices (artificially layered materials) and on the copper oxide based susperconductors (naturally layered materials). The current growth technique utilized is metalorganic chemical vapor deposition (MOCVD). CdTe, PbTe, La, LaTe, and Bi[sub 2]Te[sub 3] were deposited, mostly on GaAs. Several YBa[sub 2]Cu[sub 3]O[sub 7] compounds were obtained with possible superconductivity at temperatures up to 550 K (1 part in 10[sup 4]). YBa[sub 2]Cu[sub 3]O[sub 7[minus]x] and Tl[sub 2]CaBa[sub 2]Cu[sub 2]O[sub y] thin films were deposited by MOCVD on common substrates such as glass.

  19. Equilibrium composition in II?VI telluride MOCVD systems

    NASA Astrophysics Data System (ADS)

    Ben-Dor, L.; Greenberg, J. H.

    1999-03-01

    Thermodynamic calculations, or computer simulation of the equilibrium composition, offer an excellent possibility to reduce drastically the elaborate trial-and-error experimental efforts of finding the optimal preparation conditions for MOCVD processes (temperature T, pressure P, initial composition of the vapors X), to limit them only to the P- T- X field of existence of the solid to be prepared and an acceptable yield of the product. In this communication equilibrium composition was investigated for MOCVD processes of CdTe, ZnTe, HgTe and solid solutions Cd xZn 1- xTe and Hg xCd 1- xTe. A number of volatile organometallic compounds have been used as precursors for MOCVD growth. These are dimethylcadmium (CH 3) 2Cd, DMCd; diethylzinc (C 2H 5) 2Zn, DEZn; diisopropylzinc [CH(CH 3) 2] 2Zn, DiPZn; diethyltellurium (C 2H 5) 2Te, DETe; diisopropyltellurium [CH(CH 3) 2] 2Te, DiPTe; methylallyltellurium CH 3TeCH 2CHCH 2, MATe. A choice of the particular combination of the precursors largely depends on the desired composition of the film to be prepared, especially in cases of solid solutions Cd xZn 1- xTe and Hg xCd 1- xTe where the vapor pressure of the precursors is instrumental for the composition of the vapor in the reaction zone and, ultimately, for the composition x of the solid solution. Equilibrium composition for II-VI telluride MOCVD systems was investigated at temperatures up to 873 K in hydrogen and inert gas atmospheres at pressures up to 1 atm. P- T- X regions of existence were outlined for each of the five materials.

  20. Exposure chamber

    DOEpatents

    Moss, Owen R.

    1980-01-01

    A chamber for exposing animals, plants, or materials to air containing gases or aerosols is so constructed that catch pans for animal excrement, for example, serve to aid the uniform distribution of air throughout the chamber instead of constituting obstacles as has been the case in prior animal exposure chambers. The chamber comprises the usual imperforate top, bottom and side walls. Within the chamber, cages and their associated pans are arranged in two columns. The pans are spaced horizontally from the walls of the chamber in all directions. Corresponding pans of the two columns are also spaced horizontally from each other. Preferably the pans of one column are also spaced vertically from corresponding pans of the other column. Air is introduced into the top of the chamber and withdrawn from the bottom. The general flow of air is therefore vertical. The effect of the horizontal pans is based on the fact that a gas flowing past the edge of a flat plate that is perpendicular to the flow forms a wave on the upstream side of the plate. Air flows downwardly between the chamber walls and the outer edges of the pan. It also flows downwardly between the inner edges of the pans of the two columns. It has been found that when the air carries aerosol particles, these particles are substantially uniformly distributed throughout the chamber.

  1. Wire chamber

    DOEpatents

    Atac, Muzaffer

    1989-01-01

    A wire chamber or proportional counter device, such as Geiger-Mueller tube or drift chamber, improved with a gas mixture providing a stable drift velocity while eliminating wire aging caused by prior art gas mixtures. The new gas mixture is comprised of equal parts argon and ethane gas and having approximately 0.25% isopropyl alcohol vapor.

  2. IONIZATION CHAMBER

    DOEpatents

    Redman, W.C.; Shonka, F.R.

    1958-02-18

    This patent describes a novel ionization chamber which is well suited to measuring the radioactivity of the various portions of a wire as the wire is moved at a uniform speed, in order to produce the neutron flux traverse pattern of a reactor in which the wire was previously exposed to neutron radiation. The ionization chamber of the present invention is characterized by the construction wherein the wire is passed through a tubular, straight electrode and radiation shielding material is disposed along the wire except at an intermediate, narrow area where the second electrode of the chamber is located.

  3. MOCVD of multimetal and noble metal films

    NASA Astrophysics Data System (ADS)

    Endle, James Patrick

    2000-11-01

    Carbon content in TiN films produced with tetrakis(dimethylamino)titanium (TDMAT) and methylhydrazine or dimethylhydrazine can be controlled at or below 10% with a N/Ti ratio of ˜1.3 at growth temperatures between 573 and 723 K. Post-dosing either hydrazine on a CVD TiN film results in additional N-Ti bonds, indicating a surface reaction between the two precursors occurs. Co-dosing hydrazine-like compounds with larger alkyl ligands than methyl resulted in additional carbon incorporation in the TiN film. A growth system, consisting of a load lock and growth chamber, and a precursor pyrolysis system were designed and built to study metalorganic chemical vapor deposition. Addition of a bubbler and a direct liquid injection system allowed for the vaporization of solid and liquid precursors and solutions of multiple precursors. A precursor pyrolysis system was designed for high and low vapor pressure precursors and high carrier gas flow rates. The systems were used to study (Al,Ti)N and Ir film growth. (Al,Ti)N was used as a template to study the incorporation of elements into a multimetal chemical vapor deposited film using NH3 and a DLI solution of TDMAT and the tris(dimethylarnino)alane dimer (TDMAA) in toluene-NH 3 significantly decreases the decomposition temperature of both precursors. Carbon was reduced by increasing the NH3 partial pressure, and the Al incorporation was increased by increasing the TDMAA/TDMAT ratio in the DLI solution. Exposure to ambient resulted in significant oxygen incorporation and the removal of carbon and nitrogen from the (AI,Ti)N film. Conformal (AI,Ti)N films were produced at 450 K in the presence of NH3 and at 550 K without NH3. The role of O2 in Ir film growth was studied with the newly designed equipment. O2 significantly decreases the decomposition temperature of (MeCp)Ir(COD) below 425 K by preventing a carbonaceous build-up on the iridium film. By decreasing the oxygen partial pressure, the island nucleation and coalescence

  4. MOCVD growth of vertically aligned InGaN nanowires

    NASA Astrophysics Data System (ADS)

    Kuo, H. C.; Su Oh, Tae; Ku, P.-C.

    2013-05-01

    In this work, we report the growth of vertically aligned bulk InGaN nanowires (NWs) on r-plane sapphire substrate by metal organic chemical vapor deposition (MOCVD). Through the optimization process of growth conditions, such as growth temperature and pressure, we obtained high density InGaN NWs consisting of one (0001) polar- and two equivalent {1101} semi-polar planes. We have shown the highest InGaN NWs wire density of 8×108 cm-2,with an average diameter of 300 nm and a length of 2 μm. From results of photoluminescence (PL) at 30 K and 300 K, we observed the intense and broad emission peak from InGaN NWs at around 595 nm, and confirmed that the luminescence could be tuned from 580 nm to 660 nm by controlling the indium flow (TMIn) rate. Our results indicate that MOCVD-grown InGaN NWs can be effective absorbers of the blue-green range of solar spectrum and may be one of the good candidates for high efficiency photovoltaic devices targeting at blue-green photons.

  5. Real-time physico-neural solutions for MOCVD

    SciTech Connect

    Kelkar, A.S.; Mahajan, R.L.; Sani, R.L.

    1995-12-31

    This paper presents an integrated physical neural network approach for the modeling and optimization of a vertical MOCVD reactor. A first-principles physical model for the reactor was solved numerically using the Fluid Dynamics Analysis Package (FIDAP). This transient model included property variation and thermodiffusion effects. Artificial Neural Network (ANN) models were then trained to predict the growth rate profiles within the reactor. The data used to train the network was obtained from FIDAP simulations for combinations of process parameters determined by statistical Design of Experiments (DOE) methodology. It is shown that the trained ANN predicts the behavior of the reactor accurately. Optimum process conditions to obtain a uniform thickness of the deposited film were determined and tested using the ANN model. The results demonstrate the power and robustness of ANNs for obtaining fast on-line responses to changing input conditions. This capability of ANNs is particularly important for implementing run-to-run and on-line control of the MOCVD process.

  6. Ionization chamber

    DOEpatents

    Walenta, Albert H.

    1981-01-01

    An ionization chamber has separate drift and detection regions electrically isolated from each other by a fine wire grid. A relatively weak electric field can be maintained in the drift region when the grid and another electrode in the chamber are connected to a high voltage source. A much stronger electric field can be provided in the detection region by connecting wire electrodes therein to another high voltage source. The detection region can thus be operated in a proportional mode when a suitable gas is contained in the chamber. High resolution output pulse waveforms are provided across a resistor connected to the detection region anode, after ionizing radiation enters the drift region and ionize the gas.

  7. Ionization chamber

    DOEpatents

    Walenta, A.H.

    An ionization chamber is described which has separate drift and detection regions electrically isolated from each other by a fine wire grid. A relatively weak electric field can be maintained in the drift region when the grid and another electrode in the chamber are connected to a high voltage source. A much stronger electric field can be provided in the detection region by connecting wire electrodes therein to another high voltage source. The detection region can thus be operated in a proportional mode when a suitable gas is contained in the chamber. High resolution output pulse waveforms are provided across a resistor connected to the detection region anode, after ionizing radiation enters the drift region and ionizes the gas.

  8. MOCVD growth of AlGaN UV LEDs

    SciTech Connect

    Han, J.; Crawford, M.H.

    1998-09-01

    Issues related to the MOCVD growth of AlGaN, specifically the gas-phase parasitic reactions among TMG, TMA, and NH{sub 3}, are studied using an in-situ optical reflectometer. It is observed that the presence of the well-known gas phase adduct (TMA: NH{sub 3}) could seriously hinder the incorporation behavior of TMGa. Relatively low reactor pressures (30--50 Torr) are employed to grow an AlGaN/GaN SCH QW p-n diode structure. The UV emission at 360 nm (FWHM {approximately} 10 nm) represents the first report of LED operation from an indium-free GaN QW diode.

  9. MOCVD manifold switching effects on growth and characterization

    NASA Astrophysics Data System (ADS)

    Clark, Ivan O.; Fripp, Archibald L.; Jesser, William A.

    1991-02-01

    A combined modeling and experimental approach is used to quantify the effects of various manifold components on the switching speed in metalorganic chemical vapor deposition (MOCVD). In particular, two alternative vent-run high-speed switching manifold designs suitable for either continuous or interrupted growth have been investigated. Both designs are incorporated in a common manifold, instrumented with a mass spectrometer. The experiments have been performed using nitrogen as the transport gas and argon as the simulated source gas. The advantages and limitations of two designs are discussed. It is found that while constant flow manifold switching systems may have fluid dynamic advantages, care must be taken to minimize sections of the supply manifold with low flow rates if rapid changes in alloy composition are required.

  10. Magma chambers

    NASA Technical Reports Server (NTRS)

    Marsh, Bruce D.

    1989-01-01

    Recent observational and theoretical investigations of terrestrial magma chambers (MCs) are reviewed. Consideration is given to the evidence for MCs with active convection and crystal sorting, problems of direct MC detection, theoretical models of MC cooling, the rheology and dynamics of solidification fronts, crystal capture and differentiation, convection with solidification, MC wall flows, and MC roof melting. Diagrams, graphs, and a list of problems requiring further research are provided.

  11. Effect of crystal orientation on anisotropic etching and MOCVD growth of grooves on GaAs

    NASA Technical Reports Server (NTRS)

    Bailey, Sheila G.; Landis, Geoffrey A.; Wilt, David M.

    1989-01-01

    Grooves can be formed on GaAs by wet-chemical anisotropic etching of surfaces masked by photoresist stripes. The effect of crystal orientation on the shape of the grooves etched and on subsequent epitaxial growth by MOCVD is presented. The polar lattice increases the complexity of the etching and growth processes. The slow-etch planes defined by anisotropic etching are not always the same as the growth facets produced during MOCVD deposition, especially for deposition on higher order planes.

  12. Study of TiO2 nanomembranes obtained by an induction heated MOCVD reactor

    NASA Astrophysics Data System (ADS)

    Crisbasan, A.; Chaumont, D.; Sacilotti, M.; Crisan, A.; Lazar, A. M.; Ciobanu, I.; Lacroute, Y.; Chassagnon, R.

    2015-12-01

    Nanostructures of TiO2 were grown using the metal oxide chemical vapor deposition (MOCVD) technique. The procedure used induction heating on a graphite susceptor. This specific feature and the use of cobalt and ferrocene catalysts resulted in nanomembranes never obtained by common MOCVD reactors. The present study discusses the preparation of TiO2 nanomembranes and the dependence of nanomembrane structure and morphology on growth parameters.

  13. MOCVD of very thin films of lead lanthanum titanate

    SciTech Connect

    Beach, D.B.; Vallet, C.E.

    1995-12-31

    Films of lead lanthanum titanate were deposited using metal-organic chemical vapor deposition (MOCVD) at temperatures between 500 and 550{degrees}C in a hot-wall reactor. The precursors used were Pb(THD){sub 2}, La(THD){sub 3}, and Ti(THD){sub 2}(I-OPr){sub 2} where THD = 2,2,6,6-tetramethyl-3,5-heptanedionate, O{sub 2}C{sub 11}H{sub 19}, and I-OPr = isopropoxide, OC{sub 3}H{sub 7}. The three precursors were delivered to the reactor using a single solution containing all three precursors dissolved in tetraglyme and the precursor solution was volatilized at 225{degrees}C. Films were deposited on Si and Si/Ti/Pt substrates, and characterized using Rutherford Backscattering Spectroscopy (RPS) and X-ray diffraction(XRD). Films deposited at 550{degrees}C had a composition which was close to that of the precursor solution while films deposited at 500{degrees}C were deficient in lanthanum. Even at 500{degrees}C, the desired perovskite phase showed an increase in the intensity of the X-ray lines, but did not change the width of these lines, implying the grain sizes had remained unchanged.

  14. MOCVD process technology for affordable, high-yield, high-performance MESFET structures. Phase 3: MIMIC

    NASA Astrophysics Data System (ADS)

    1993-01-01

    Under the MIMIC Program, Spire has pursued improvements in the manufacturing of low cost, high quality gallium arsenide MOCVD wafers for advanced MIMIC FET applications. As a demonstration of such improvements, Spire was tasked to supply MOCVD wafers for comparison to MBE wafers in the fabrication of millimeter and microwave integrated circuits. In this, the final technical report for Spire's two-year MIMIC contract, we report the results of our work. The main objectives of Spire's MIMIC Phase 3 Program, as outlined in the Statement of Work, were as follows: Optimize the MOCVD growth conditions for the best possible electrical and morphological gallium arsenide. Optimization should include substrate and source qualification as well as determination of the optimum reactor growth conditions; Perform all work on 75 millimeter diameter wafers, using a reactor capable of at least three wafers per run; and Evaluate epitaxial layers using electrical, optical, and morphological tests to obtain thickness, carrier concentration, and mobility data across wafers.

  15. Deposition studies and coordinated characterization of MOCVD YBCO films on IBAD-MgO templates.

    SciTech Connect

    Aytug, Tolga; Paranthaman, Mariappan Parans; Heatherly Jr, Lee; Zhang, Yifei; Kim, Kyunghoon; Goyal, Amit; Maroni, V. A.; List III, Frederick Alyious

    2009-01-01

    A recently installed research metal organic chemical vapor deposition (MOCVD) system at Oak Ridge National Laboratory, provided by SuperPower, Inc., has been used to investigate the processing variables of MOCVD YBCO precursors and trends in the resulting properties. Systematic studies of film growth were carried out by optimizing deposition temperature and oxygen flow rate. Structural and superconducting properties of the YBCO films were analyzed by extensive X-ray diffraction, scanning electron microspcopy and transport measurements. The identification of intermediate phase formations after the YBCO precursor transformation was investigated with coordinated reel-to-reel Raman microprobe analysis. With the combination of these characterization techniques, an improved understanding of the growth characteristics of MOCVD YBCO films was established. Finally, critical current densities greater than 2 MA/cm2 for film thicknesses of 0.8 m have been demonstrated.

  16. Influence of Natural Convection and Thermal Radiation Multi-Component Transport in MOCVD Reactors

    NASA Technical Reports Server (NTRS)

    Lowry, S.; Krishnan, A.; Clark, I.

    1999-01-01

    The influence of Grashof and Reynolds number in Metal Organic Chemical Vapor (MOCVD) reactors is being investigated under a combined empirical/numerical study. As part of that research, the deposition of Indium Phosphide in an MOCVD reactor is modeled using the computational code CFD-ACE. The model includes the effects of convection, conduction, and radiation as well as multi-component diffusion and multi-step surface/gas phase chemistry. The results of the prediction are compared with experimental data for a commercial reactor and analyzed with respect to the model accuracy.

  17. Synchrotron radiation assistant MOCVD deposition of ZnO films on Si substrate

    NASA Astrophysics Data System (ADS)

    Guangtao, Yang; Guobin, Zhang; Hongjun, Zhou; Zeming, Qi

    2009-06-01

    The growth of ZnO film on Si(1 0 0) substrate has been studied with synchrotron radiation (SR) assisted MOCVD method. The diethylzinc (DEZn) and CO 2 are used as source materials, while Nitrogen is employed as a carrier gas for DEZn. With the assistance of SR the ZnO film can be deposited even at room temperature. XRD, SEM and photoluminescence (PL) studies show that the crystal quality of ZnO films grown with the assistance of SR is higher than that of those without SR assistance. The growth mechanism of ZnO film with the SR assistant MOCVD system is primarily discussed.

  18. Method for Improving Mg Doping During Group-III Nitride MOCVD

    DOEpatents

    Creighton, J. Randall; Wang, George T.

    2008-11-11

    A method for improving Mg doping of Group III-N materials grown by MOCVD preventing condensation in the gas phase or on reactor surfaces of adducts of magnesocene and ammonia by suitably heating reactor surfaces between the location of mixing of the magnesocene and ammonia reactants and the Group III-nitride surface whereon growth is to occur.

  19. Photoluminescence of Nitrogen-Doped Zinc Selenide by Photo-Assisted Mocvd.

    NASA Astrophysics Data System (ADS)

    Gillespie, Paul Matthew

    Zinc selenide is a wide band-gap (2.67 eV) II -VI compound semiconductor with potential use as a blue electro-optic device material. Problems with obtaining suitable p-type conductivity have limited device development. Zinc selenide epitaxial films, doped with nitrogen from NH _3, have been grown on gallium arsenide substrates by laser-assisted metal organic chemical vapor deposition (MOCVD). The effect of nitrogen doping was investigated with and without direct surface irradiation incident on the surface from a broad-band light source. Low temperature (8 K) photoluminescence spectroscopy has confirmed the incorporation of nitrogen as a shallow acceptor by the presence of acceptor-bound-excitons and associated donor -acceptor-pair recombination emissions. The MOCVD growth parameters have been optimized based on the presence of characteristic features in the photoluminescence spectra. Growth rate mechanisms have been proposed for both laser-assisted MOCVD and direct-irradiation MOCVD. Simultaneous interaction of the two photo-assisted techniques show that direct irradiation of the surface does not enhance the growth rate under the laser-assisted condition. This confirms that direct surface irradiation growth mechanisms involve the interaction of photo-generated carriers with alkyl groups from the precursors.

  20. RF plasma enhanced MOCVD of yttria stabilized zirconia thin films using octanedionate precursors and their characterization

    NASA Astrophysics Data System (ADS)

    Chopade, S. S.; Nayak, C.; Bhattacharyya, D.; Jha, S. N.; Tokas, R. B.; Sahoo, N. K.; Deo, M. N.; Biswas, A.; Rai, Sanjay; Thulasi Raman, K. H.; Rao, G. M.; Kumar, Niranjan; Patil, D. S.

    2015-11-01

    Yttria stabilized zirconia thin films have been deposited by RF plasma enhanced MOCVD technique on silicon substrates at substrate temperature of 400 °C. Plasma of precursor vapors of (2,7,7-trimethyl-3,5-octanedionate) yttrium (known as Y(tod)3), (2,7,7-trimethyl-3,5-octanedionate) zirconium (known as Zr(tod)4), oxygen and argon gases is used for deposition. To the best of our knowledge, plasma assisted MOCVD of YSZ films using octanediaonate precursors have not been reported in the literature so far. The deposited films have been characterized by GIXRD, FTIR, XPS, FESEM, AFM, XANES, EXAFS, EDAX and spectroscopic ellipsometry. Thickness of the films has been measured by stylus profilometer while tribological property measurement has been done to study mechanical behavior of the coatings. Characterization by different techniques indicates that properties of the films are dependent on the yttria content as well as on the structure of the films.

  1. Structural and optical characterization of MOCVD-grown ZnO thin films

    NASA Astrophysics Data System (ADS)

    Pagni, O.; James, G. R.; Leitch, A. W. R.

    2004-03-01

    We report on the characterization of ZnO thin films grown by metal organic chemical vapor deposition (MOCVD) using diethyl zinc (DEZ) and tert-butanol (TBOH) as precursors. Substrate temperature proved to be a crucial factor in the crystallization process, as it vastly impacted the structural properties of the samples studied. Highly c-axis oriented films with large grain size (52 nm), low tensile strain (0.6%), uniform substrate coverage and a columnar structure devoid of hexagonal needles were successfully deposited on n-Si (100) substrates. The temperature-dependent luminescence spectra recorded confirmed the excellent quality of the material obtained in this work. Our results so far set TBOH apart as an outstanding oxygen source for the MOCVD growth of ZnO.

  2. A novel MOCVD reactor for growth of high-quality GaN-related LED layers

    NASA Astrophysics Data System (ADS)

    Hu, Shaolin; Liu, Sheng; Zhang, Zhi; Yan, Han; Gan, Zhiyin; Fang, Haisheng

    2015-04-01

    Gallium nitride (GaN), a direct bandgap semiconductor widely used in bright light-emitting diodes (LEDs), is mostly grown by metal-organic chemical vapor deposition (MOCVD) method. A good reactor design is critical for the production of high-quality GaN thin films. In this paper, we presented a novel buffered distributed spray (BDS) MOCVD reactor with vertical gas sprayers and horizontal gas inlets. Experiments based on a 36×2″ BDS reactor were conducted to examine influence of the process parameters, such as the operating pressure and the gas flow rate, on the growth efficiency and on the layer thickness uniformity. Transmission electron microscopy (TEM) and photoluminescence (PL) are further conducted to evaluate quality of the epitaxial layers and to check performance of the reactor. Results show that the proposed novel reactor is of high performance in growing high-quality thin films, including InGaN/GaN multiquantum wells (MQWs) structures.

  3. Photoreflectance for in-situ characterization of MOCVD growth of semiconductors under micro-gravity conditions

    NASA Technical Reports Server (NTRS)

    Pollak, Fred H.

    1990-01-01

    A contactless electromodulation technique of photoreflectance (PR) was developed for in-situ monitoring of metal-organic chemical vapor deposition (MOCVD) semiconductor growth for micro-gravity applications. PR can be employed in a real MOCVD reactor including rotating substrate (approximately 500 rev/min) in flowing gases and through a diffuser plate. Measurements on GaAs and Ga(0.82)Al(0.18)As were made up to 690 C. The direct band gaps of In(x)Ga(1-x)As (x = 0.07 and 0.16) were evaluated up to 600 C. In order to address the question of real time measurement, the spectra of the direct gap of GaAs at 650 C was obtained in 30 seconds and 15 seconds seems feasible.

  4. Two chamber reaction furnace

    DOEpatents

    Blaugher, R.D.

    1998-05-05

    A vertical two chamber reaction furnace is described. The furnace comprises a lower chamber having an independently operable first heating means for heating the lower chamber and a gas inlet means for admitting a gas to create an ambient atmosphere, and an upper chamber disposed above the lower chamber and having an independently operable second heating means for heating the upper chamber. Disposed between the lower chamber and the upper chamber is a vapor permeable diffusion partition. The upper chamber has a conveyor means for conveying a reactant there through. Of particular importance is the thallinating of long-length thallium-barium-calcium-copper oxide (TBCCO) or barium-calcium-copper oxide (BCCO) precursor tapes or wires conveyed through the upper chamber to thereby effectuate the deposition of vaporized thallium (being so vaporized as the first reactant in the lower chamber at a temperature between about 700 C and 800 C) on TBCCO or BCCO tape or wire (the second reactant) at its simultaneous annealing temperature in the upper chamber of about 800 to 950 C to thereby replace thallium oxide lost from TBCCO tape or wire because of the high annealing temperature or to deposit thallium on BCCO tape or wire. Continuously moving the tape or wire provides a single-step process that effectuates production of long-length TBCCO superconducting product. 2 figs.

  5. Two chamber reaction furnace

    DOEpatents

    Blaugher, Richard D.

    1998-05-05

    A vertical two chamber reaction furnace. The furnace comprises a lower chamber having an independently operable first heating means for heating the lower chamber and a gas inlet means for admitting a gas to create an ambient atmosphere, and an upper chamber disposed above the lower chamber and having an independently operable second heating means for heating the upper chamber. Disposed between the lower chamber and the upper chamber is a vapor permeable diffusion partition. The upper chamber has a conveyor means for conveying a reactant there through. Of particular importance is the thallinating of long-length thallium-barium-calcium-copper oxide (TBCCO) or barium-calcium-copper oxide (BCCO) precursor tapes or wires conveyed through the upper chamber to thereby effectuate the deposition of vaporized thallium (being so vaporized as the first reactant in the lower chamber at a temperature between about 700.degree. and 800.degree. C.) on TBCCO or BCCO tape or wire (the second reactant) at its simultaneous annealing temperature in the upper chamber of about 800.degree. to 950.degree. C. to thereby replace thallium oxide lost from TBCCO tape or wire because of the high annealing temperature or to deposit thallium on BCCO tape or wire. Continuously moving the tape or wire provides a single-step process that effectuates production of long-length TBCCO superconducting product.

  6. Characteristics of CoxTi1-xO2 thin films deposited by MOCVD

    SciTech Connect

    McClure, A.; Kayani, A.; Idzerda, Y.U.; Arenholz, E.; Cruz, E.

    2008-05-09

    This paper deals with the growth and characterization of ferromagnetic cobalt doped TiO{sub 2} thin films deposited by liquid precursor metal organic chemical vapor deposition (MOCVD) using a new combination of the source materials Co(TMHD){sub 3}, tetrahydrofuran (THF), and titanium isopropoxide (TIP). An array of experiments reveals the intrinsic ferromagnetic nature of the grown films, and suggests that the magnetism is not generated by oxygen vacancies.

  7. Final report on LDRD project : outstanding challenges for AlGaInN MOCVD.

    SciTech Connect

    Mitchell, Christine Charlotte; Follstaedt, David Martin; Russell, Michael J.; Cross, Karen Charlene; Wang, George T.; Creighton, James Randall; Allerman, Andrew Alan; Koleske, Daniel David; Lee, Stephen Roger; Coltrin, Michael Elliott

    2005-03-01

    The AlGaInN material system is used for virtually all advanced solid state lighting and short wavelength optoelectronic devices. Although metal-organic chemical vapor deposition (MOCVD) has proven to be the workhorse deposition technique, several outstanding scientific and technical challenges remain, which hinder progress and keep RD&A costs high. The three most significant MOCVD challenges are: (1) Accurate temperature measurement; (2) Reliable and reproducible p-doping (Mg); and (3) Low dislocation density GaN material. To address challenge (1) we designed and tested (on reactor mockup) a multiwafer, dual wavelength, emissivity-correcting pyrometer (ECP) for AlGaInN MOCVD. This system simultaneously measures the reflectance (at 405 and 550 nm) and emissivity-corrected temperature for each individual wafer, with the platen signal entirely rejected. To address challenge (2) we measured the MgCp{sub 2} + NH{sub 3} adduct condensation phase diagram from 65-115 C, at typical MOCVD concentrations. Results indicate that it requires temperatures of 80-100 C in order to prevent MgCp{sub 2} + NH{sub 3} adduct condensation. Modification and testing of our research reactor will not be complete until FY2005. A new commercial Veeco reactor was installed in early FY2004, and after qualification growth experiments were conducted to improve the GaN quality using a delayed recovery technique, which addresses challenge (3). Using a delayed recovery technique, the dislocation densities determined from x-ray diffraction were reduced from 2 x 10{sup 9} cm{sup -2} to 4 x 10{sup 8} cm{sup -2}. We have also developed a model to simulate reflectance waveforms for GaN growth on sapphire.

  8. Radiation effects on p+n InP junctions grown by MOCVD

    NASA Technical Reports Server (NTRS)

    Messenger, Scott R.; Walters, Robert J.; Panunto, M. J.; Summers, Geoffrey P.

    1994-01-01

    The superior radiation resistance of InP over other solar cell materials such as Si or GaAs has prompted the development of InP cells for space applications. The early research on radiation effects in InP was performed by Yamaguchi and co-workers who showed that, in diffused p-InP junctions, radiation-induced defects were readily annealed both thermally and by injection, which was accompanied by significant cell recovery. More recent research efforts have been made using p-InP grown by metalorganic chemical vapor deposition (MOCVD). While similar deep level transient spectroscopy (DLTS) results were found for radiation induced defects in these cells and in diffused junctions, significant differences existed in the annealing characteristics. After injection annealing at room temperature, Yamaguchi noticed an almost complete recovery of the photovoltaic parameters, while the MOCVD samples showed only minimal annealing. In searching for an explanation of the different annealing behavior of diffused junctions and those grown by MOCVD, several possibilities have been considered. One possibility is the difference in the emitter structure. The diffused junctions have S-doped graded emitters with widths of approximately 0.3 micrometers, while the MOCVD emitters are often doped with Si and have widths of approximately 300A (0.03 micrometers). The difference in the emitter thickness can have important effects, e.g. a larger fraction of the total photocurrent is generated in the n-type material for thicker emitters. Therefore the properties of the n-InP material may explain the difference in the observed overall annealing behavior of the cells.

  9. MOCVD growth of gallium nitride with indium surfactant

    NASA Astrophysics Data System (ADS)

    Won, Dong Jin

    In this thesis research, the effect of indium surfactant on Ga-polar and N-polar GaN films grown at 950 °C by MOCVD on various substrates such as Si-face SiC, bulk GaN, Si(111), and C-face SiC was studied to investigate the stress relaxation mechanism, structural, and optical properties of GaN films which were modified by the indium surfactant. The effect of indium surfactant on GaN films grown on SiC was studied first. In the 1.8 microm thick Ga-polar GaN films grown on lattice-mismatched Si-face SiC substrates utilizing indium surfactant at 950 °C, inverted hexagonal pyramid surface defects, so-called V-defects which consist of six (1011) planes, formed at threading dislocations on the GaN surface, which gave rise to the relaxation of compressive misfit stress in an elastic way. Simultaneously, enhanced surface mobility of Ga and N adatoms with indium surfactant lead to improved 2D growth, which may be contradictory to the formation of surface defects like V-defects. In order to find the driving force for V-defect formation in the presence of indium, a nucleation and growth model was developed, taking into consideration the strain, surface, and dislocation energies modified by indium surfactant. This model found that the V-defect formation can be energetically preferred since indium reduces the surface energy of the (1011) plane, which gives rise to the V-defect formation and growth that can overcome the energy barrier at the critical radius of the V-defect. These Ga-polar GaN films were found to be unintentionally doped with Si. Thus, an investigation into the effect of intentional Si doping at a constant TMIn flow rate on GaN films was also performed. Si turned out to be another important factor in the generation of V-defects because Si may be captured at the threading dislocation cores by forming Si -- N bonds, acting as a mask to locally prevent GaN growth. This behavior appeared to assist the initiation of the V-defect which enables V-defects to easily

  10. Progress in MOCVD growth of HgCdTe epilayers for HOT infrared detectors

    NASA Astrophysics Data System (ADS)

    Kebłowski, A.; Gawron, W.; Martyniuk, P.; Stepień, D.; Kolwas, K.; Piotrowski, J.; Madejczyk, P.; Kopytko, M.; Piotrowski, A.; Rogalski, A.

    2016-05-01

    In this paper we present progress in MOCVD growth of (100) HgCdTe epilayers achieved recently at the Institute of Applied Physics, Military University of Technology and Vigo System S.A. It is shown that MOCVD technology is an excellent tool in fabrication of different HgCdTe detector structures with a wide range of composition, donor/acceptor doping and without post grown annealing. Particular progress has been achieved in the growth of (100) HgCdTe epilayers for long wavelength infrared photoconductors operated in HOT conditions. The (100) HgCdTe photoconductor optimized for 13-μm attain detectivity equal to 6.5x109 Jones and therefore outperform its (111) counterpart. The paper also presents technological progress in fabrication of MOCVD-grown (111) HgCdTe barrier detectors. The barrier device performance is comparable with state-of-the-art of HgCdTe photodiodes. The detectivity of HgCdTe detectors is close to the value marked HgCdTe photodiodes. Dark current densities are close to the values given by "Rule 07".

  11. Recent progress in MOCVD growth for thermoelectrically cooled HgCdTe medium wavelength infrared photodetectors

    NASA Astrophysics Data System (ADS)

    Gawron, W.; Martyniuk, P.; Kębłowski, A.; Kolwas, K.; Stępień, D.; Piotrowski, J.; Madejczyk, P.; Pędzińska, M.; Rogalski, A.

    2016-04-01

    The authors report on advanced metalorganic chemical vapour deposition (MOCVD) of Hg1-xCdxTe (HgCdTe) structures for high operating temperature, medium wavelength infrared (MWIR) detector application. MOCVD technology with wide range of composition and donor/acceptor doping and without post grown annealing was proved to be an excellent tool for HgCdTe heterostructure epitaxial growth used for uncooled photodetector design. The interdiffused multilayer process (IMP) technique was applied for the HgCdTe deposition. HgCdTe epilayers were grown at 350 °C with Hg source kept at 210 °C. The II/VI mole ratio was assumed in the range from 1.5 to 3 during CdTe/HgTe cycles of the IMP process. The MWIR detectors grown by MOCVD exhibit detectivity ∼7.3 × 1011 Jones at λPEAK = 3.5 μm and T = 230 K being determined by background limited photodetector (BLIP) condition.

  12. MOCVD for solar cells, a transition towards a chamberless inline process

    NASA Astrophysics Data System (ADS)

    Barrioz, V.; Monir, S.; Kartopu, G.; Lamb, D. A.; Brooks, W.; Siderfin, P.; Jones, S.; Clayton, A. J.; Irvine, S. J. C.

    2015-03-01

    MOCVD has been associated with batch processing of III-V opto-electronic devices for decades, with epitaxial structures deposited on up to 200 mm diameter wafers. Recent development in thin film PV has seen the gap in conversion efficiencies closing in on that of the commonly found multicrystalline Si wafer based PV. To further improve the conversion efficiency of thin film PV towards the theoretical limits of single junction solar cells requires a technique such as MOCVD with scalability potential. Preliminary results on the development of a chamberless inline process are reported for up to 15 cm wide float glass, progressively coating each layer in the CdTe solar cell as the heated substrate passes under each coating head in turn and entirely at atmospheric pressure. Emphasis is made on ensuring that the chamberless coating heads can be operated safely using a combination of nitrogen curtain flows and a balanced exhaust pressure system. Results are also presented on the exclusion of oxygen and moisture from the coating area, achieved using the same gas flow isolation process. This paper also reviews the achievements made to-date in the transfer of the high efficiency batch MOCVD produced CdTe solar cell to the chamberless inline process demonstrating device quality thin films deposition.

  13. Synthesis of (Hg,Pb)(Sr,Ba) 2Ca 2Cu 3O z superconducting films via MOCVD and PLD

    NASA Astrophysics Data System (ADS)

    Klimonsky, S. O.; Samoilenkov, S. V.; Gorbenko, O. Yu.; Emelianov, D. A.; Lyashenko, A. V.; Lee, S. R.; Kaul, A. R.; Tretyakov, Yu. D.; Andrianov, D. G.; Kalinov, A. V.; Voloshin, I. F.

    2002-12-01

    (0 0 1)-oriented Sr-containing (Hg,Pb)-1223 films have been synthesised for the first time using the two-step procedure. Hg-free precursor films with the thickness up to 1 μm have been deposited by metalorganic chemical vapor deposition (MOCVD) or pulsed infra-red laser ablation (PLD) and then the films were annealed in a mercury-containing atmosphere in sealed quartz ampoules. No post-annealing in oxygen was used. The phase composition of the PLD-derived films depended crucially on the deposition temperature of the precursor films. MOCVD-derived films contained only very small amounts of non-superconducting phases according to XRD. The Tc=118 K and j c(77 K,0.01 T)=2.5×10 6A/cm 2 have been measured for the MOCVD-derived samples.

  14. The Mobile Chamber

    NASA Technical Reports Server (NTRS)

    Scharfstein, Gregory; Cox, Russell

    2012-01-01

    A document discusses a simulation chamber that represents a shift from the thermal-vacuum chamber stereotype. This innovation, currently in development, combines the capabilities of space simulation chambers, the user-friendliness of modern-day electronics, and the modularity of plug-and-play computing. The Mobile Chamber is a customized test chamber that can be deployed with great ease, and is capable of bringing payloads at temperatures down to 20 K, in high vacuum, and with the desired metrology instruments integrated to the systems control. Flexure plans to lease Mobile Chambers, making them affordable for smaller budgets and available to a larger customer base. A key feature of this design will be an Apple iPad-like user interface that allows someone with minimal training to control the environment inside the chamber, and to simulate the required extreme environments. The feedback of thermal, pressure, and other measurements is delivered in a 3D CAD model of the chamber's payload and support hardware. This GUI will provide the user with a better understanding of the payload than any existing thermal-vacuum system.

  15. Target chambers for gammashpere

    SciTech Connect

    Carpenter, M.P.; Falout, J.W.; Nardi, B.G.

    1995-08-01

    One of our responsibilities for Gammasphere, was designing and constructing two target chambers and associated beamlines to be used with the spectrometer. The first chamber was used with the early implementation phase of Gammasphere, and consisted of two spun-Al hemispheres welded together giving a wall thickness of 0.063 inches and a diameter of 12 inches.

  16. Static diffusion cloud chambers

    NASA Technical Reports Server (NTRS)

    Ayers, G.

    1981-01-01

    The chamber geometry and optical arrangement are described. The supersaturation range is given and consists of readings taken at five fixed points: 0.25%, 0.5%, 0.75%, 1.0%, and 1.25%. The detection system is described including light source, cameras, and photocell detectors. The temperature control and the calibration of the chamber are discussed.

  17. High resolution drift chambers

    SciTech Connect

    Va'vra, J.

    1985-07-01

    High precision drift chambers capable of achieving less than or equal to 50 ..mu..m resolutions are discussed. In particular, we compare so called cool and hot gases, various charge collection geometries, several timing techniques and we also discuss some systematic problems. We also present what we would consider an ''ultimate'' design of the vertex chamber. 50 refs., 36 figs., 6 tabs.

  18. Morphology of ZnO grown by MOCVD on sapphire substrates

    NASA Astrophysics Data System (ADS)

    Munuera, C.; Zúñiga-Pérez, J.; Rommeluere, J. F.; Sallet, V.; Triboulet, R.; Soria, F.; Muñoz-Sanjosé, V.; Ocal, C.

    2004-03-01

    A quantitative roughness and microstructural analysis of ZnO grown on sapphire by atmospheric metalorganic chemical vapor deposition (MOCVD) is presented. In order to investigate the influence of the substrate on the morphology, different sapphire orientations have been employed. Scanning force microscopy data have been analyzed for a variety of thicknesses to elucidate, if possible, the growth mechanisms involved in the growth process. Our study reveals significant differences between morphologies depending on whether the substrate surface exhibits steps (misoriented a-, c- and r-planes) or not ( m-plane); however, no major differences on the calculated roughness coefficients have been found.

  19. Investigation of GaP/Si Heteroepitaxy on MOCVD Prepared Si(100) Surfaces

    SciTech Connect

    Warren, Emily L.; Kibbler, Alan E.; France, Ryan M.; Norman, Andrew G.; Olson, Jerry M.; McMahon, William E.

    2015-06-14

    Antiphase-domain (APD) free growth of GaP on Si has been achieved on Si surfaces prepared in situ by etching with AsH3. The pre-nucleation AsH3 etching removes O and C contaminants at a relatively low temperature, and creates a single-domain arsenic-terminated Si surface. The As-As dimer rows are all parallel to the step edges, and subsequent GaP growth by MOCVD retains this dimerization orientation. Both LEED and TEM indicate that the resulting epilayer is APD-free, and could thereby serve as a template for III-V/Si multijunction solar cells.

  20. Significance of microstructure for a MOCVD-grown YSZ thin film gas sensor

    SciTech Connect

    Vetrone, J.; Foster, C.; Bai, G.

    1996-11-01

    The authors report the fabrication and characterization of a low temperature (200--400 C) thin film gas sensor constructed from a MOCVD-grown yttria-stabilized zirconia (YSZ) layer sandwiched between two platinum thin film electrodes. A reproducible gas-sensing response is produced by applying a cyclic voltage which generates voltammograms with gas-specific current peaks and shapes. Growth conditions are optimized for preparing YSZ films having dense microstructures, low leakage currents, and maximum ion conductivities. In particular, the effect of growth temperature on film morphology and texture is discussed and related to the electrical and gas-sensing properties of the thin film sensor device.

  1. High quality GaN-based LED epitaxial layers grown in a homemade MOCVD system

    NASA Astrophysics Data System (ADS)

    Haibo, Yin; Xiaoliang, Wang; Junxue, Ran; Guoxin, Hu; Lu, Zhang; Hongling, Xiao; Jing, Li; Jinmin, Li

    2011-03-01

    A homemade 7 × 2 inch MOCVD system is presented. With this system, high quality GaN epitaxial layers, InGaN/GaN multi-quantum wells and blue LED structural epitaxial layers have been successfully grown. The non-uniformity of undoped GaN epitaxial layers is as low as 2.86%. Using the LED structural epitaxial layers, blue LED chips with area of 350 × 350 μm2 were fabricated. Under 20 mA injection current, the optical output power of the blue LED is 8.62 mW.

  2. 45. AUXILIARY CHAMBER BETWEEN CHAMBER AND CONCRETE ENCLOSURE (LOCATION DDD), ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    45. AUXILIARY CHAMBER BETWEEN CHAMBER AND CONCRETE ENCLOSURE (LOCATION DDD), VIEW LOOKING EAST. LEAD ENCLOSED PIPING IS DRAIN FROM BOILER CHAMBER No. 1 - Shippingport Atomic Power Station, On Ohio River, 25 miles Northwest of Pittsburgh, Shippingport, Beaver County, PA

  3. Fabrication of GaN nanotubular material using MOCVD with aluminum oxide membrane

    NASA Astrophysics Data System (ADS)

    Jung, Woo-Gwang; Jung, Se-Hyuck; Kung, Patrick; Razeghi, Manijeh

    2006-02-01

    GaN nanotubular material is fabricated with aluminum oxide membrane in MOCVD. SEM, XRD, TEM and PL are employed to characterize the fabricated GaN nanotubular material. An aluminum oxide membrane with ordered nano holes is used as template. Gallium nitride is deposited at the inner wall of the nano holes in aluminum oxide template, and the nanotubular material with high aspect ratio is synthesized using the precursors of TMG and ammonia gas. Optimal synthesis condition in MOCVD is obtained successfully for the gallium nitride nanotubular material in this research. The diameter of GaN nanotube fabricated is approximately 200 ~ 250 nm and the wall thickness is about 40 ~ 50 nm. GaN nanotubular material consists of numerous fine GaN particulates with sizes ranging 15 to 30 nm. The composition of gallium nitride is confirmed to be stoichiometrically 1:1 for Ga and N by EDS. XRD and TEM analyses indicate that grains in GaN nanotubular material have nano-crystalline structure. No blue shift is found in the PL spectrum on the GaN nanotubular material fabricated in aluminum oxide template.

  4. Fabrication of GaN nanotubular material using MOCVD with an aluminium oxide membrane

    NASA Astrophysics Data System (ADS)

    Jung, Woo-Gwang; Jung, Se-Hyuck; Kung, Patrick; Razeghi, Manijeh

    2006-01-01

    GaN nanotubular material is fabricated with an aluminium oxide membrane in MOCVD. SEM, XRD, TEM and PL are employed to characterize the fabricated GaN nanotubular material. An aluminium oxide membrane with ordered nanoholes is used as a template. Gallium nitride is deposited at the inner wall of the nanoholes in the aluminium oxide template, and the nanotubular material with high aspect ratio is synthesized using the precursors of TMG and ammonia gas. Optimal synthesis conditions in MOCVD are obtained successfully for the gallium nitride nanotubular material in this research. The diameter of the GaN nanotube fabricated is approximately 200-250 nm and the wall thickness is about 40-50 nm. GaN nanotubular material consists of numerous fine GaN particulates with size range 15-30 nm. The composition of gallium nitride is confirmed to be stoichiometrically 1:1 for Ga and N by EDS. XRD and TEM analyses indicate that the grains in GaN nanotubular material have a nano-crystalline structure. No blue shift is found in the PL spectrum on the GaN nanotubular material fabricated in an aluminium oxide template.

  5. The Mars Chamber

    NASA Video Gallery

    The Mars chamber is a box about the size of a refrigerator that re-creates the temperatures, pressures, and atmosphere of the Martian surface, essentially creating a Mars environment on Earth! Scie...

  6. Sleeve reaction chamber system

    SciTech Connect

    Northrup, M. Allen; Beeman, Barton V.; Benett, William J.; Hadley, Dean R.; Landre, Phoebe; Lehew, Stacy L.; Krulevitch, Peter A.

    2009-08-25

    A chemical reaction chamber system that combines devices such as doped polysilicon for heating, bulk silicon for convective cooling, and thermoelectric (TE) coolers to augment the heating and cooling rates of the reaction chamber or chambers. In addition the system includes non-silicon-based reaction chambers such as any high thermal conductivity material used in combination with a thermoelectric cooling mechanism (i.e., Peltier device). The heat contained in the thermally conductive part of the system can be used/reused to heat the device, thereby conserving energy and expediting the heating/cooling rates. The system combines a micromachined silicon reaction chamber, for example, with an additional module/device for augmented heating/cooling using the Peltier effect. This additional module is particularly useful in extreme environments (very hot or extremely cold) where augmented heating/cooling would be useful to speed up the thermal cycling rates. The chemical reaction chamber system has various applications for synthesis or processing of organic, inorganic, or biochemical reactions, including the polymerase chain reaction (PCR) and/or other DNA reactions, such as the ligase chain reaction.

  7. Improved Rhenium Thrust Chambers

    NASA Technical Reports Server (NTRS)

    O'Dell, John Scott

    2015-01-01

    Radiation-cooled bipropellant thrust chambers are being considered for ascent/ descent engines and reaction control systems on various NASA missions and spacecraft, such as the Mars Sample Return and Orion Multi-Purpose Crew Vehicle (MPCV). Currently, iridium (Ir)-lined rhenium (Re) combustion chambers are the state of the art for in-space engines. NASA's Advanced Materials Bipropellant Rocket (AMBR) engine, a 150-lbf Ir-Re chamber produced by Plasma Processes and Aerojet Rocketdyne, recently set a hydrazine specific impulse record of 333.5 seconds. To withstand the high loads during terrestrial launch, Re chambers with improved mechanical properties are needed. Recent electrochemical forming (EL-Form"TM") results have shown considerable promise for improving Re's mechanical properties by producing a multilayered deposit composed of a tailored microstructure (i.e., Engineered Re). The Engineered Re processing techniques were optimized, and detailed characterization and mechanical properties tests were performed. The most promising techniques were selected and used to produce an Engineered Re AMBR-sized combustion chamber for testing at Aerojet Rocketdyne.

  8. Automated Electrostatics Environmental Chamber

    NASA Technical Reports Server (NTRS)

    Calle, Carlos; Lewis, Dean C.; Buchanan, Randy K.; Buchanan, Aubri

    2005-01-01

    The Mars Electrostatics Chamber (MEC) is an environmental chamber designed primarily to create atmospheric conditions like those at the surface of Mars to support experiments on electrostatic effects in the Martian environment. The chamber is equipped with a vacuum system, a cryogenic cooling system, an atmospheric-gas replenishing and analysis system, and a computerized control system that can be programmed by the user and that provides both automation and options for manual control. The control system can be set to maintain steady Mars-like conditions or to impose temperature and pressure variations of a Mars diurnal cycle at any given season and latitude. In addition, the MEC can be used in other areas of research because it can create steady or varying atmospheric conditions anywhere within the wide temperature, pressure, and composition ranges between the extremes of Mars-like and Earth-like conditions.

  9. Filament wound rocket motor chambers

    NASA Technical Reports Server (NTRS)

    1976-01-01

    The design, analysis, fabrication and testing of a Kevlar-49/HBRF-55A filament wound chamber is reported. The chamber was fabricated and successfully tested to 80% of the design burst pressure. Results of the data reduction and analysis from the hydrotest indicate that the chamber design and fabrication techniques used for the chamber were adequate and the chamber should perform adequately in a static test.

  10. Automated soil gas monitoring chamber

    DOEpatents

    Edwards, Nelson T.; Riggs, Jeffery S.

    2003-07-29

    A chamber for trapping soil gases as they evolve from the soil without disturbance to the soil and to the natural microclimate within the chamber has been invented. The chamber opens between measurements and therefore does not alter the metabolic processes that influence soil gas efflux rates. A multiple chamber system provides for repetitive multi-point sampling, undisturbed metabolic soil processes between sampling, and an essentially airtight sampling chamber operating at ambient pressure.

  11. The role of impurities in LP-MOCVD grown gallium nitride

    SciTech Connect

    Hwang, C.Y.; Li, Y.; Schurman, M.J.; Mayo, W.E.; Lu, Y.; Stall, R.A.

    1996-11-01

    The authors have investigated the relationship of the Hall electron mobility to the background carrier concentration in low pressure MOCVD grown GaN. The highest electron mobility (400 cm{sup 2}/V{center_dot}s) of the unintentionally doped GaN was obtained at a carrier concentration of 1 {times} 10{sup 17} cm{sup {minus}3} and samples with carrier concentrations lower than this exhibited lower mobilities. SIMS analysis shows C and O concentrations in the range of 2--3 {times} 10{sup 16} cm{sup {minus}3} and H in the 2--3 {times} 10{sup 17} cm{sup {minus}3} range. Structural defects, stoichiometry and impurities in the GaN films grown under different conditions are investigated to understand their relationship to the electron Hall mobilities. In particular, different growth temperatures and pressures were used to grow undoped GaN and modify the background doping effect of the impurities.

  12. Three-dimensional modelling of horizontal chemical vapor deposition. I - MOCVD at atmospheric pressure

    NASA Technical Reports Server (NTRS)

    Ouazzani, Jalil; Rosenberger, Franz

    1990-01-01

    A systematic numerical study of the MOCVD of GaAs from trimethylgallium and arsine in hydrogen or nitrogen carrier gas at atmospheric pressure is reported. Three-dimensional effects are explored for CVD reactors with large and small cross-sectional aspect ratios, and the effects on growth rate uniformity of tilting the susceptor are investigated for various input flow rates. It is found that, for light carrier gases, thermal diffusion must be included in the model. Buoyancy-driven three-dimensional flow effects can greatly influence the growth rate distribution through the reactor. The importance of the proper design of the lateral thermal boundary conditions for obtaining layers of uniform thickness is emphasized.

  13. Free-standing GaAs nanowires growth on ITO glass by MOCVD

    NASA Astrophysics Data System (ADS)

    Wu, D.; Tang, X. H.; Olivier, A.; Li, X. Q.

    2015-04-01

    GaAs nanowires (NWs) are directly grown on indium tin oxide (ITO) glass substrate by metalorganic chemical vapour deposition (MOCVD), using Au nanoparticles (NPs) as catalyst. By functionalization of the ITO glass and optimization of the Au NPs deposition time, the Au NPs area density deposited on the ITO glass reaches 92 NP μm-2. Uniform and free-standing GaAs NWs without kinking or worm-shape defects have been grown at 430 °C. More than 96% of the NWs have tilt angles larger than 45° with respect of the substrate. The effects of the growth temperature and the Au NPs size on the GaAs NWs growth rate, the NW diameter, and tapering effect are investigated. These results of GaAs NWs growth are the essential step for understanding III-V NWs integration on transparent conductive oxide coated low cost substrate and developing high efficiencyhybrid solar cells.

  14. Monitoring and Controlling of Strain During MOCVD of AlGaN for UV Optoelectronics

    SciTech Connect

    Han, J.; Crawford, M.H.; Shul, R.J.; Hearne, S.J.; Chason, E.; Figiel, J.J.; Banas, M.

    1999-01-14

    The grown-in tensile strain, due to a lattice mismatch between AlGaN and GaN, is responsible for the observed cracking that seriously limits the feasibility of nitride-based ultraviolet (UV) emitters. We report in-situ monitoring of strain/stress during MOCVD of AlGaN based on a wafer-curvature measurement technique. The strain/stress measurement confirms the presence of tensile strain during growth of AlGaN pseudomorphically on a thick GaN layer. Further growth leads to the onset of stress relief through crack generation. We find that the growth of AlGaN directly on low-temperature (LT) GaN or AlN buffer layers results in a reduced and possibly controllable strain.

  15. Low ohmic contact AlN/GaN HEMTs grown by MOCVD

    NASA Astrophysics Data System (ADS)

    Guodong, Gu; Shaobo, Dun; Yuanjie, Lü; Tingting, Han; Peng, Xu; Jiayun, Yin; Zhihong, Feng

    2013-11-01

    AlN/GaN high-electron-mobility transistors (HEMTs) on SiC substrates were fabricated by metal-organic chemical vapor deposition (MOCVD) and then characterized. An Si/Ti/Al/Ni/Au stack was used to reduce ohmic contact resistance (0.33 Ω·mm) at a low annealing temperature. The fabricated devices exhibited a maximum drain current density of 1.07 A/mm (VGS = 1 V) and a maximum peak extrinsic transconductance of 340 mS/mm. The off-state breakdown voltage of the device was 64 V with a gate—drain distance of 1.9 μm. The current gain extrinsic cutoff frequency fT and the maximum oscillation frequency fmax were 36 and 80 GHz with a 0.25 μm gate length, respectively.

  16. Raman spectra of MOCVD-grown ferroelectric PbTiO{sub 3} thin films

    SciTech Connect

    Feng, Z.C.; Kwak, B.S. |; Erbil, A.; Boatner, L.A.

    1993-12-31

    Lead titanate (PbTiO{sub 3}) has been grown on a variety of substrates by using the metalorganic chemical vapor deposition (MOCVD) technique. The substrates employed included Si, GaAs, MgO, fused-quartz, sapphire, and KTaO{sub 3}. Raman spectra from these heterostructures are presented. All of the films exhibited the strong, narrow spectral features characteristic of PbTiO{sub 3} perovskite-oxide crystals and indicative of high crystalline quality. The temperature behavior of the Raman modes, including the so-called ``soft-mode,`` was studied. A ``difference-Raman`` technique was used to distinguish the contributions of the PbTiO{sub 3} film and the KTaO{sub 3} single-crystal substrate.

  17. Microstructure of GaN Grown on (111) Si by MOCVD

    SciTech Connect

    Fleming, J.G.; Follstaedt, D.M.; Han, J.; Provencio, P.

    1998-12-17

    Gallium nitride was grown on (111) Si by MOCVD by depositing an AIN buffer at 108O"C and then GaN at 1060 {degrees}C. The 2.2pm layer cracked along {1-100} planes upon cooling to room temperature, but remained adherent. We were able to examine the microstructure of material between cracks with TEM. The character and arrangement of dislocation are much like those of GaN grown on Al{sub 2}O{sub 3}: -2/3 pure edge and - 1/3 mixed (edge + screw), arranged in boundaries around domains of GaN that are slightly disoriented with respect to neighboring material. The 30 nm AIN buffer is continuous, indicating that AIN wets the Si, in contrast to GaN on Al{sub 2}O{sub 3}.

  18. A mathematical representation of a modified stagnation flow reactor for MOCVD applications

    NASA Astrophysics Data System (ADS)

    Dilawari, A. H.; Szekely, J.

    1991-02-01

    Computed results are presented describing the behavior of a modified stagnation point reactor for an MOCVD system, employing a showerhead type gas distributor. The principal findings of the work are the following: (a) By this arrangement, it is possible to obtain a very high spatial uniformity in the deposition rate, in cases better than 0.35% for a five inch diameter wafer. (b) Both the absolute values of the gas velocity and the standoff distance were found to play a critical role in affecting the uniformity of the deposition rate. Indeed a small standoff distance was found to be an essential ingredient in obtaining a good spatial uniformity of the deposit. (c) "An upside down" orientation was found to be helpful in minimizing thermal natural convection and a further refinement was found to be possible by imposing a desired radial distribution on the gas inlet velocity profile.

  19. Growth of AlN nanostructure on GaN using MOCVD

    SciTech Connect

    Loganathan, R.; Ramesh, R.; Jayasakthi, M.; Prabakaran, K.; Kuppulingam, B.; Sankaranarayanan, M.; Balaji, M.; Arivazhagan, P.; Singh, Subra; Baskar, K.

    2015-06-24

    Aluminum nitride (AlN) nanowalls have been epitaxially grown on dislocation assisted GaN/Al{sub 2}O{sub 3} template by metal organic chemical vapor deposition (MOCVD) without any help of metal catalysts. A large number of nanowalls with thicknesses of 1.5-2.0 µm and height 400 nm have been deposited. The AlN nanowalls were found to have a preferred c-axis oriented with a hexagonal crystal structure. The AlN nanowalls and GaN/Al{sub 2}O{sub 3} template have been characterize at room temperature photoluminescence (PL) and high resolution X-ray diffraction (HRXRD)

  20. Enhanced flux pinning in MOCVD-YBCO films through Zr-additions:Systematic feasibility studies

    SciTech Connect

    Aytug, Tolga; Paranthaman, Mariappan Parans; Specht, Eliot D; Kim, Kyunghoon; Zhang, Yifei; Cantoni, Claudia; Zuev, Yuri L; Goyal, Amit; Christen, David K; Maroni, Victor A.

    2009-01-01

    Systematic effects of Zr additions on the structural and flux pinning properties of YBa{sub 2}Cu{sub 3}O{sub 7-{delta}} (YBCO) films deposited by metal-organic chemical vapor deposition (MOCVD) have been investigated. Detailed characterization, conducted by coordinated transport, x-ray diffraction, scanning and transmission electron microscopy analyses, and imaging Raman microscopy have revealed trends in the resulting property/performance correlations of these films with respect to varying mole percentages (mol%) of added Zr. For compositions {le} 7.5 mol%, Zr additions lead to improved in-field critical current density, as well as extra correlated pinning along the c-axis direction of the YBCO films via the formation of columnar, self-assembled stacks of BaZrO{sub 3} nanodots.

  1. Enhanced flux pinning in MOCVD-YBCO films through Zr additions : systematic feasibility studies.

    SciTech Connect

    Aytug, T.; Paranthaman, M.; Specht, E. D.; Zhang, Y.; Kim, K.; Zuev, Y. L.; Cantoni, C.; Goyal, A.; Christen, D. K.; Maroni, V. A.; Chen, Y.; Selvamanickam, V.; ORNL; SuperPower, Inc.

    2010-01-01

    Systematic effects of Zr additions on the structural and flux pinning properties of YBa{sub 2}Cu{sub 3}O{sub 7-{delta}} (YBCO) films deposited by metal-organic chemical vapor deposition (MOCVD) have been investigated. Detailed characterization, conducted by coordinated transport, x-ray diffraction, scanning and transmission electron microscopy analyses, and imaging Raman microscopy have revealed trends in the resulting property/performance correlations of these films with respect to varying mole percentages (mol%) of added Zr. For compositions {le} 7.5 mol%, Zr additions lead to improved in-field critical current density, as well as extra correlated pinning along the c-axis direction of the YBCO films via the formation of columnar, self-assembled stacks of BaZrO{sub 3} nanodots.

  2. MOCVD capacitors

    SciTech Connect

    Lanagan, M.T.; Foster, C.

    1997-09-01

    A significant effort within the Department of Energy`s Office of Transportation Technologies and the U.S. Navy`s Power Electronic Building Block (PEBB) project has focused on reducing the size and weight of power electronic devices for electric and hybrid vehicles. Power electronic circuits, which are composed of active switching elements and passive components such as capacitors and inductors, provide motor control, power distribution, and DC/AC conversion functions in electric vehicles. Progress has been made on reducing the size and weight of power electronic components such as MOS-controlled thristors and insulated-gate bipolar transistors. Additional effort on high-power capacitors will be needed for load leveling and filter functions. The objective of this work is to fabricate a new class of high-power capacitors with reduced size and weight. Capacitors will be integrated with semiconductor components of electric motor and actuator control subsystems.

  3. Study of GaP single crystal layers grown on GaN by MOCVD

    SciTech Connect

    Li, Shuti; Liu, Chao; Ye, Guoguang; Xiao, Guowei; Zhou, Yugang; Su, Jun; Fan, Guanghan; Zhang, Yong; Liang, Fubo; Zheng, Shuwen

    2011-11-15

    Highlights: {yields} We investigated the growth of GaP layers on GaN by MOCVD. {yields} A single crystal GaP layer could be grown on GaN. {yields} The V/III ratio played an important role to improve GaP layer quality. {yields} The GaP:Mg layer with hole concentration of 4.2 x 10{sup 18} cm{sup -3} was obtained. -- Abstract: The performance of GaN based devices could possibly be improved by utilizing the good p-type properties of GaP layer and it provides the possibility of the integration of InAlGaN and AlGaInP materials to produce new devices, if high quality GaP compounds can be grown on III-nitride compounds. In this paper, the growth of GaP layers on GaN by metalorganic chemical vapor deposition (MOCVD) has been investigated. The results show that the GaP low temperature buffer layer can provide a high density of nucleation sites for high temperature GaP growth. Using a 40 nm thick GaP buffer layer, a single crystal GaP layer, whose full-width at half-maximum of the (1 1 1) plane measured by double crystal X-ray diffraction is 580'', can be grown on GaN. The V/III ratio plays an important role in the GaP layer growth and an appropriate V/III ratio can improve the quality of GaP layer. The GaP:Mg layer with hole carrier concentration of 4.2 x 10{sup 18} cm{sup -3} has been obtained.

  4. Ultrasonic Drying Processing Chamber

    NASA Astrophysics Data System (ADS)

    Acosta, V.; Bon, J.; Riera, E.; Pinto, A.

    The design of a high intensity ultrasonic chamber for drying process was investigated. The acoustic pressure distribution in the ultrasonic drying chamber was simulated solving linear elastic models with attenuation for the acoustic-structure interaction. Together with the government equations, the selection of appropriate boundary conditions, mesh refinement, and configuration parameters of the calculation methods, which is of great importance to simulate adequately the process, were considered. Numerical solution, applying the finite element method (FEM), of acoustic-structure interactions involves to couple structural and fluid elements (with different degrees of freedom), whose solution implies several problems of hardware requirements and software configuration, which were solved. To design the drying chamber, the influence of the directivity of the drying open camera and the staggered reflectors over the acoustic pressure distribution was analyzed. Furthermore, to optimize the influence of the acoustic energy on the drying process, the average value of the acoustic energy distribution in the drying chamber was studied. This would determine the adequate position of the food samples to be dried. For this purpose, the acoustic power absorbed by the samples will be analyzed in later studies.

  5. Improved wire chamber

    DOEpatents

    Atac, M.

    1987-05-12

    An improved gas mixture for use with proportional counter devices, such as Geiger-Mueller tubes and drift chambers. The improved gas mixture provides a stable drift velocity while eliminating wire aging caused by prior art gas mixtures. The new gas mixture is comprised of equal parts argon and ethane gas and having approximately 0.25% isopropyl alcohol vapor. 2 figs.

  6. Liquid Wall Chambers

    SciTech Connect

    Meier, W R

    2011-02-24

    The key feature of liquid wall chambers is the use of a renewable liquid layer to protect chamber structures from target emissions. Two primary options have been proposed and studied: wetted wall chambers and thick liquid wall (TLW) chambers. With wetted wall designs, a thin layer of liquid shields the structural first wall from short ranged target emissions (x-rays, ions and debris) but not neutrons. Various schemes have been proposed to establish and renew the liquid layer between shots including flow-guiding porous fabrics (e.g., Osiris, HIBALL), porous rigid structures (Prometheus) and thin film flows (KOYO). The thin liquid layer can be the tritium breeding material (e.g., flibe, PbLi, or Li) or another liquid metal such as Pb. TLWs use liquid jets injected by stationary or oscillating nozzles to form a neutronically thick layer (typically with an effective thickness of {approx}50 cm) of liquid between the target and first structural wall. In addition to absorbing short ranged emissions, the thick liquid layer degrades the neutron flux and energy reaching the first wall, typically by {approx}10 x x, so that steel walls can survive for the life of the plant ({approx}30-60 yrs). The thick liquid serves as the primary coolant and tritium breeding material (most recent designs use flibe, but the earliest concepts used Li). In essence, the TLW places the fusion blanket inside the first wall instead of behind the first wall.

  7. Comparison of the strain of GaN films grown on MOCVD-GaN/Al2O3 and MOCVD-GaN/SiC samples by HVPE growth

    NASA Astrophysics Data System (ADS)

    Zhang, Lei; Shao, Yongliang; Hao, Xiaopeng; Wu, Yongzhong; Qu, Shuang; Chen, Xiufang; Xu, Xiangang

    2011-11-01

    In this paper, GaN films were successfully grown on the samples of MOCVD-GaN/Al2O3 (MGA) and MOCVD-GaN/6H-SiC (MGS) by HVPE method. We compare the strain of GaN films grown on the two samples by employing various characterization techniques. The surface morphology of GaN films were characterized by field emission scanning electron microscopy (FE-SEM) and atomic force microscopy (AFM). The variations of strain characteristic were also microscopically identified using the Z scan of Raman spectroscopy. The Raman peak (E2) shift indicates that the stress enhanced gradually as a function of increasing the measurement depth. The strain of GaN grown on MGA sample is compressive strain, while on MGS is tensile strain. The stress of GaN films grown on MGA and MGS sample are calculated. The difference in the value of stress between calculation and measurement was interpreted.

  8. Multi-chamber deposition system

    DOEpatents

    Jacobson, Richard L.; Jeffrey, Frank R.; Westerberg, Roger K.

    1989-10-17

    A system for the simultaneous deposition of different coatings onto a thin web within a large volume vacuum chamber is disclosed which chamber is provided with a plurality of deposition chambers in which the different layers are deposited onto the film as its moves from a supply roll to a finished take-up roll of coated web. The deposition chambers provided within the large vacuum chamber are provided with separate seals which minimize back diffusion of any dopant gas from adjacent deposition chambers.

  9. Multi-chamber deposition system

    DOEpatents

    Jacobson, Richard L.; Jeffrey, Frank R.; Westerberg, Roger K.

    1989-06-27

    A system for the simultaneous deposition of different coatings onto a thin web within a large volume vacuum chamber is disclosed which chamber is provided with a plurality of deposition chambers in which the different layers are deposited onto the film as its moves from a supply roll to a finished take-up roll of coated web. The deposition chambers provided within the large vacuum chamber are provided with separate seals which minimize back diffusion of any dopant gas from adjacent deposition chambers.

  10. Combustor with fuel preparation chambers

    NASA Technical Reports Server (NTRS)

    Zelina, Joseph (Inventor); Myers, Geoffrey D. (Inventor); Srinivasan, Ram (Inventor); Reynolds, Robert S. (Inventor)

    2001-01-01

    An annular combustor having fuel preparation chambers mounted in the dome of the combustor. The fuel preparation chamber comprises an annular wall extending axially from an inlet to an exit that defines a mixing chamber. Mounted to the inlet are an air swirler and a fuel atomizer. The air swirler provides swirled air to the mixing chamber while the atomizer provides a fuel spray. On the downstream side of the exit, the fuel preparation chamber has an inwardly extending conical wall that compresses the swirling mixture of fuel and air exiting the mixing chamber.

  11. 50. BOILER CHAMBER No. 1, LOOKING SOUTHEAST BETWEEN CHAMBER AND ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    50. BOILER CHAMBER No. 1, LOOKING SOUTHEAST BETWEEN CHAMBER AND ENCLOSURE (LOCATION III) - Shippingport Atomic Power Station, On Ohio River, 25 miles Northwest of Pittsburgh, Shippingport, Beaver County, PA

  12. 61. BOILER CHAMBER No. 2, LOOKING SOUTHWEST BETWEEN CHAMBER AND ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    61. BOILER CHAMBER No. 2, LOOKING SOUTHWEST BETWEEN CHAMBER AND CONCRETE ENCLOSURE (LOCATION PPP) - Shippingport Atomic Power Station, On Ohio River, 25 miles Northwest of Pittsburgh, Shippingport, Beaver County, PA

  13. 44. AUXILIARY CHAMBER BETWEEN CHAMBER AND CONCRETE ENCLOSURE (LOCATION CCC), ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    44. AUXILIARY CHAMBER BETWEEN CHAMBER AND CONCRETE ENCLOSURE (LOCATION CCC), LOOKING NORTHEAST SHOWING DRAIN PIPE FROM SUMP - Shippingport Atomic Power Station, On Ohio River, 25 miles Northwest of Pittsburgh, Shippingport, Beaver County, PA

  14. 41. AUXILIARY CHAMBER, CONCRETE ENCLOSURE CHAMBER AIR LOCK (EXTERIOR), LOOKING ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    41. AUXILIARY CHAMBER, CONCRETE ENCLOSURE CHAMBER AIR LOCK (EXTERIOR), LOOKING NORTHEAST FROM SOUTHWEST CORNER (LOCATION AAA) - Shippingport Atomic Power Station, On Ohio River, 25 miles Northwest of Pittsburgh, Shippingport, Beaver County, PA

  15. 72. VISITOR'S CENTER, MODEL OF BOILER CHAMBER, AUXILIARY CHAMBER, REACTOR ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    72. VISITOR'S CENTER, MODEL OF BOILER CHAMBER, AUXILIARY CHAMBER, REACTOR AND CANAL (LOCATION T) - Shippingport Atomic Power Station, On Ohio River, 25 miles Northwest of Pittsburgh, Shippingport, Beaver County, PA

  16. Temperature coefficients and radiation induced DLTS spectra of MOCVD grown n(+)p InP solar cells

    NASA Technical Reports Server (NTRS)

    Walters, Robert J.; Statler, Richard L.; Summers, Geoffrey P.

    1991-01-01

    The effects of temperature and radiation on n(+)p InP solar cells and mesa diodes grown by metallorganic chemical vapor deposition (MOCVD) were studied. It was shown that MOCVD is capable of consistently producing good quality InP solar cells with Eff greater than 19 percent which display excellent radiation resistance due to minority carrier injection and thermal annealing. It was also shown that universal predictions of InP device performance based on measurements of a small group of test samples can be expected to be quite accurate, and that the degradation of an InP device due to any incident particle spectrum should be predictable from a measurement following a single low energy proton irradiation.

  17. Study of high {Tc} superconducting thin films grown by MOCVD. Final report, July 1, 1986--April 30, 1990

    SciTech Connect

    Erbil, A.

    1990-12-31

    Work is described briefly, which was carried out on development of techniques to grow metal-semiconductor superlattices (artificially layered materials) and on the copper oxide based susperconductors (naturally layered materials). The current growth technique utilized is metalorganic chemical vapor deposition (MOCVD). CdTe, PbTe, La, LaTe, and Bi{sub 2}Te{sub 3} were deposited, mostly on GaAs. Several YBa{sub 2}Cu{sub 3}O{sub 7} compounds were obtained with possible superconductivity at temperatures up to 550 K (1 part in 10{sup 4}). YBa{sub 2}Cu{sub 3}O{sub 7{minus}x} and Tl{sub 2}CaBa{sub 2}Cu{sub 2}O{sub y} thin films were deposited by MOCVD on common substrates such as glass.

  18. Three chamber negative ion source

    DOEpatents

    Leung, Ka-Ngo; Ehlers, Kenneth W.; Hiskes, John R.

    1985-01-01

    A negative ion vessel is divided into an excitation chamber, a negative ionization chamber and an extraction chamber by two magnetic filters. Input means introduces neutral molecules into a first chamber where a first electron discharge means vibrationally excites the molecules which migrate to a second chamber. In the second chamber a second electron discharge means ionizes the molecules, producing negative ions which are extracted into or by a third chamber. A first magnetic filter prevents high energy electrons from entering the negative ionization chamber from the excitation chamber. A second magnetic filter prevents high energy electrons from entering the extraction chamber from the negative ionizing chamber. An extraction grid at the end of the negative ion vessel attracts negative ions into the third chamber and accelerates them. Another grid, located adjacent to the extraction grid, carries a small positive voltage in order to inhibit positive ions from migrating into the extraction chamber and contour the plasma potential. Additional electrons can be suppressed from the output flux using ExB forces provided by magnetic field means and the extractor grid electric potential.

  19. One-step preparation of highly dispersed metal-supported catalysts by fluidized-bed MOCVD for carbon nanotube synthesis

    NASA Astrophysics Data System (ADS)

    Xu, Chunbao; Zhu, Jesse

    2004-11-01

    A new technique of fluidized-bed metal-organic chemical vapour deposition (FB-MOCVD) is developed as a one-step method to prepare highly dispersed metal-supported catalysts for carbon nanotube synthesis. By using ultrafine powder of gamma-alumina (70 nm Sauter mean in size) as the support with Fe(CO)5 and Mo(CO)6 as the metal precursors, Fe/Al2O3, Mo/Al2O3 and Fe-Mo/Al2O3 catalysts have been prepared in an FB-MOCVD reactor. Compared with the conventional catalyst-preparation methods such as impregnation, ion exchange, co-precipitation and co-crystallization, the one-step FB-MOCVD technique is advantageous in many aspects. These include eliminating the solid-liquid separation and the subsequent operations of drying and high-temperature calcination/reduction, thus minimizing the aggregation or the crystalline size-growing problem for the supported metal particles caused by these operations. The metal-supported catalysts obtained by FB-MOCVD are characterized with various techniques including ICP-AES, SEM-EDX, XRD and nitrogen isothermal adsorption. Some catalysts are selected and used for carbon nanotube synthesis by CVD from acetylene (C2H2) in a fluidized bed at 650 or 850 °C. The formation of the entangled multi-walled carbon nanotubes (MWNTs), around 50 nm in outer diameter and 10 nm in inner diameter, and several to tens of microns in length, has been confirmed by the TEM and SEM analyses. High CNT selectivity ({\\ge }95{%} ) with the carbon yield ranging widely from about 10% to over 60%, depending on the type of catalyst used and the CNT deposition temperature, has been demonstrated with TGA tests.

  20. Multiwire proportional chamber development

    NASA Technical Reports Server (NTRS)

    Doolittle, R. F.; Pollvogt, U.; Eskovitz, A. J.

    1973-01-01

    The development of large area multiwire proportional chambers, to be used as high resolution spatial detectors in cosmic ray experiments is described. A readout system was developed which uses a directly coupled, lumped element delay-line whose characteristics are independent of the MWPC design. A complete analysis of the delay-line and the readout electronic system shows that a spatial resolution of about 0.1 mm can be reached with the MWPC operating in the strictly proportional region. This was confirmed by measurements with a small MWPC and Fe-55 X-rays. A simplified analysis was carried out to estimate the theoretical limit of spatial resolution due to delta-rays, spread of the discharge along the anode wire, and inclined trajectories. To calculate the gas gain of MWPC's of different geometrical configurations a method was developed which is based on the knowledge of the first Townsend coefficient of the chamber gas.

  1. CONTINUOUSLY SENSITIVE BUBBLE CHAMBER

    DOEpatents

    Good, R.H.

    1959-08-18

    A radiation detector of the bubble chamber class is described which is continuously sensitive and which does not require the complex pressure cycling equipment characteristic of prior forms of the chamber. The radiation sensitive element is a gas-saturated liquid and means are provided for establishing a thermal gradient across a region of the liquid. The gradient has a temperature range including both the saturation temperature of the liquid and more elevated temperatures. Thus a supersaturated zone is created in which ionizing radiations may give rise to visible gas bubbles indicative of the passage of the radiation through the liquid. Additional means are provided for replenishing the supply of gas-saturated liquid to maintaincontinuous sensitivity.

  2. Advanced thrust chamber designs

    NASA Technical Reports Server (NTRS)

    Dietrich, F. J.; Leach, A. E.

    1971-01-01

    A regeneratively cooled thrust chamber has been designed and fabricated, consisting of an inner TD nickel liner which was spin formed, welded, and machined and an outer shell of electroformed nickel. Coolant channels were produced in the outer surface of the inner liner by the electric discharge machining process before electroforming the shell. Accessory manifolds and piping were attached by welding. Manufacturing processes employed are described.

  3. Digital optical spark chambers

    NASA Technical Reports Server (NTRS)

    Evenson, Paul; Tuska, Evelyn

    1989-01-01

    The authors constructed and tested a prototype digital readout system for optical spark chambers using a linear, solid-state charge-coupled-device detector array. Position resolution of 0.013 mm (sigma) over a 25-cm field of view has been demonstrated. It is concluded that this technique should permit the construction of economical, lightweight and low-power trajectory hodoscopes for use in cosmic-ray instrumentation on balloons and in spacecraft.

  4. Vertical two chamber reaction furnace

    DOEpatents

    Blaugher, R.D.

    1999-03-16

    A vertical two chamber reaction furnace is disclosed. The furnace comprises a lower chamber having an independently operable first heating means for heating the lower chamber and a gas inlet means for admitting a gas to create an ambient atmosphere, and an upper chamber disposed above the lower chamber and having an independently operable second heating means for heating the upper chamber. Disposed between the lower chamber and the upper chamber is a vapor permeable diffusion partition. The upper chamber has a conveyor means for conveying a reactant there through. Of particular importance is the thallinating of long-length thallium-barium-calcium copper oxide (TBCCO) or barium-calcium-copper oxide (BCCO) precursor tapes or wires conveyed through the upper chamber to thereby effectuate the deposition of vaporized thallium (being so vaporized as the first reactant in the lower chamber at a temperature between about 700 and 800 C) on TBCCO or BCCO tape or wire (the second reactant) at its simultaneous annealing temperature in the upper chamber of about 800 to 950 C to thereby replace thallium oxide lost from TBCCO tape or wire because of the high annealing temperature or to deposit thallium on BCCO tape or wire. Continuously moving the tape or wire provides a single-step process that effectuates production of long-length TBCCO superconducting product. 2 figs.

  5. Vertical two chamber reaction furnace

    DOEpatents

    Blaugher, Richard D.

    1999-03-16

    A vertical two chamber reaction furnace. The furnace comprises a lower chamber having an independently operable first heating means for heating the lower chamber and a gas inlet means for admitting a gas to create an ambient atmosphere, and an upper chamber disposed above the lower chamber and having an independently operable second heating means for heating the upper chamber. Disposed between the lower chamber and the upper chamber is a vapor permeable diffusion partition. The upper chamber has a conveyor means for conveying a reactant there through. Of particular importance is the thallinating of long-length thallium-barium-calcium-copper oxide (TBCCO) or barium-calcium-copper oxide (BCCO) precursor tapes or wires conveyed through the upper chamber to thereby effectuate the deposition of vaporized thallium (being so vaporized as the first reactant in the lower chamber at a temperature between about 700.degree. and 800.degree. C.) on TBCCO or BCCO tape or wire (the second reactant) at its simultaneous annealing temperature in the upper chamber of about 800.degree. to 950.degree. C. to thereby replace thallium oxide lost from TBCCO tape or wire because of the high annealing temperature or to deposit thallium on BCCO tape or wire. Continuously moving the tape or wire provides a single-step process that effectuates production of long-length TBCCO superconducting product.

  6. Multi-anode ionization chamber

    DOEpatents

    Bolotnikov, Aleksey E.; Smith, Graham; Mahler, George J.; Vanier, Peter E.

    2010-12-28

    The present invention includes a high-energy detector having a cathode chamber, a support member, and anode segments. The cathode chamber extends along a longitudinal axis. The support member is fixed within the cathode chamber and extends from the first end of the cathode chamber to the second end of the cathode chamber. The anode segments are supported by the support member and are spaced along the longitudinal surface of the support member. The anode segments are configured to generate at least a first electrical signal in response to electrons impinging thereon.

  7. Wire chambers revisited.

    PubMed

    Ott, R J

    1993-04-01

    Detectors used for radioisotope imaging have, historically, been based on scintillating crystal/photomultiplier combinations in various forms. From the rectilinear scanner through to modern gamma cameras and positron cameras, the basic technology has remained much the same. Efforts to overcome the limitations of this form of technology have foundered on the inability to reproduce the required sensitivity, spatial resolution and sensitive area at acceptable cost. Multiwire proportional chambers (MWPCs) have long been used as position-sensitive charged particle detectors in nuclear and high-energy physics. MWPCs are large-area gas-filled ionisation chambers in which large arrays of fine wires are used to measure the position of ionisation produced in the gas by the passage of charged particles. The important properties of MWPCs are high-spatial-resolution, large-area, high-count-rate performance at low cost. For research applications, detectors several metres square have been built and small-area detectors have a charged particle resolution of 0.4 mm at a count rate of several million per second. Modification is required to MWPCs for nuclear medicine imaging. As gamma rays or X-rays cannot be detected directly, they must be converted into photo- or Compton scatter electrons. Photon-electron conversion requires the use of high atomic number materials in the body of the chamber. Pressurised xenon is the most useful form of "gas only" photon-electron convertor and has been used successfully in a gamma camera for the detection of gamma rays at energies below 100 keV. This camera has been developed specifically for high-count-rate first-pass cardiac imaging. This high-pressure xenon gas MWPC is the key to a highly competitive system which can outperform scintillator-based systems. The count rate performance is close to a million counts per second and the intrinsic spatial resolution is better than the best scintillator-based camera. The MWPC camera produces quantitative

  8. Review of wire chamber aging

    SciTech Connect

    Va'Vra, J.

    1986-02-01

    This paper makes an overview of the wire chamber aging problems as a function of various chamber design parameters. It emphasizes the chemistry point of view and many examples are drawn from the plasma chemistry field as a guidance for a possible effort in the wire chamber field. The paper emphasizes the necessity of variable tuning, the importance of purity of the wire chamber environment, as well as it provides a practical list of presently known recommendations. In addition, several models of the wire chamber aging are qualitatively discussed. The paper is based on a summary talk given at the Wire Chamber Aging Workshop held at LBL, Berkeley on January 16-17, 1986. Presented also at Wire Chamber Conference, Vienna, February 25-28, 1986. 74 refs., 18 figs., 11 tabs.

  9. MOCVD growth and structure of PbTiO{sub 3} thin films

    SciTech Connect

    Gao, Y.; Bai, G.; Merkle, K.L.; Chang, H.L.M.; Lam, D.J.

    1993-08-01

    PbTiO{sub 3} thin films grown on (001)MgO and (110)MgO by MOCVD have been characterized by x-ray diffraction and transmission electron microscopy. The PbTiO{sub 3} films deposited on (001)MgO under the optimum conditions always show a bi-layer structure. The top layer of the films near the free surface is c-axis oriented with the orientation relationship (001)[100]PbTiO{sub 3}{parallel}(001)[100]MgO. The bottom layer of the films near the substrate is a-axis oriented with (100)[001]PbTiO{sub 3}{parallel}(001)[100]MgO. 90{degrees} domains were observed, but only in the c-axis oriented layers. The thickness of the a-axis oriented layers near the substrate decreases with decreasing the cooling rate. PbTiO{sub 3} films deposited on (110) MgO, however, are single-layer, epitaxial films with (101)[001]PbTiO{sub 3}{parallel}(110)[001]MgO.

  10. P-type Ge epitaxy on GaAs (100) substrate grown by MOCVD

    NASA Astrophysics Data System (ADS)

    Jin, Y. J.; Chia, C. K.; Liu, H. F.; Wong, L. M.; Chai, J. W.; Chi, D. Z.; Wang, S. J.

    2016-07-01

    In this work, Ga-doped Geranium (Ge) films have been grown on GaAs (100) substrates by metal-organic chemical vapor deposition (MOCVD). Undesired pillar structures have been observed on the epilayers prepared at relatively lower temperatures. Energy dispersive X-ray spectroscopy (EDX) indicated that the pillars are mainly consisted of Ga atoms, which is totally different from that of the Ge film. It was demonstrated that the pillar structures could be reduced by simply raising the growth temperature while keeping the other growth conditions unchanged. In this regard, the growth mechanism of the pillars was related to the Ge-Ga dimers formed during the growth of p-Ge films. By further studying the influence of a GaAs or Ge buffer layer on the growth of p-Ge layers, we found that the GaAs substrate with lower density of Ga or Ge dangling bonds was helpful in suppressing the formation of the undesired pillar structures.

  11. Wurtzite InP nanowire arrays grown by selective area MOCVD

    SciTech Connect

    Chu, Hyung-Joon; Yeh, Ting-Wei; Stewart, Lawrence; Dapkus, P. Daniel

    2010-06-22

    InP nanowires are a unique material phase because this normally zincblende material forms in the wurtzite crystal structure below a critical diameter owing to the contribution of sidewalls to the total formation energy. This may allow control of the carrier transport and optical properties of InP nanowires for applications such as nano scale transistors, lasers and detectors. In this work, we describe the fabrication of InP nanowire arrays by selective area growth using MOCVD in the diameter range where the wurtzite structure is formed. The spatial growth rate in selective area growth is modeled by a diffusion model for the precursors. The proposed model achieves an average error of 9%. Electron microscopy shows that the grown InP nanowires are in the wurtzite crystal phase with many stacking faults. The threshold diameter of the crystal phase transition of InP nanowires is larger than the thermodynamic estimation. In order to explain this tendency, we propose a surface kinetics model based on a 2×2 reconstruction. This model can explain the increased tendency for wurtzite nanowire formation on InP (111)A substrates and the preferred growth direction of binary III-V compound semiconductor nanowires.

  12. MOCVD synthesis of group III-nitride heterostructure nanowires for solid-state lighting.

    SciTech Connect

    Wang, George T.; Creighton, James Randall; Talin, Albert Alec

    2006-11-01

    Solid-state lighting (SSL) technologies, based on semiconductor light emitting devices, have the potential to reduce worldwide electricity consumption by more than 10%, which could significantly reduce U.S. dependence on imported energy and improve energy security. The III-nitride (AlGaInN) materials system forms the foundation for white SSL and could cover a wide spectral range from the deep UV to the infrared. For this LDRD program, we have investigated the synthesis of single-crystalline III-nitride nanowires and heterostructure nanowires, which may possess unique optoelectronic properties. These novel structures could ultimately lead to the development of novel and highly efficient SSL nanodevice applications. GaN and III-nitride core-shell heterostructure nanowires were successfully synthesized by metal organic chemical vapor deposition (MOCVD) on two-inch wafer substrates. The effect of process conditions on nanowire growth was investigated, and characterization of the structural, optical, and electrical properties of the nanowires was also performed.

  13. The annealing effects of V-doped GaN thin films grown by MOCVD

    NASA Astrophysics Data System (ADS)

    Souissi, M.; Bouzidi, M.; El Jani, B.

    2012-02-01

    We have investigated the annealing effect of V-doped GaN (GaN:V) epitaxial layers grown on sapphire by metal organic chemical vapor deposition (MOCVD). The film was annealed at a temperature of 1075 °C for 30 min in N 2 ambient after growth. The structural, surface morphology and optical properties of GaN:V films were studied by high resolution X-ray diffraction (HRXRD), atomic force microscope (AFM) and photoluminescence (PL). The results show that the annealing makes for the destruction in the crystal quality and surface morphology. After thermal annealing, the photoluminescence (PL) measurement showed a reduction of the blue luminescence (BL) band observed in GaN:V at room temperature (RT). The phenomenon is attributed to vanadium diffusion or to the V-related complex dissociation. Near-band-edge (NBE) peak exhibited a red shift after 1075 °C anneal. This is due to the decrease in the level of strain. In the infrared region, we observed the emergence of the line 0.93 eV accompanied by a decrease in the intensity of the 0.82 eV emission. Their possible origins are discussed.

  14. Hetero-epitaxy of ε-Ga2O3 layers by MOCVD and ALD

    NASA Astrophysics Data System (ADS)

    Boschi, F.; Bosi, M.; Berzina, T.; Buffagni, E.; Ferrari, C.; Fornari, R.

    2016-06-01

    Growth of gallium oxide thin films was carried out by Metalorganic Chemical Vapor Deposition (MOCVD) at different temperatures. Pure ε-phase epilayers of Ga2O3, with good morphology and structural properties, were obtained, for the first time with this technique, on sapphire at the temperature of 650 °C. XRD analysis performed by high-resolution diffractometry confirmed the good crystallographic quality of the grown layers. At temperatures higher than 700 °C the usual stable β-Ga2O3 phase was obtained. The ε-films were successfully deposited also on (0001)-oriented GaN and (111)- and (001)-oriented 3C-SiC templates, provided that the appropriate temperature was chosen. This indicates that the temperature, rather than substrate structure, is the growth parameter which decides what phase actually forms. The growth proceeds via coalescence of hexagonal islands and is favored when a substrate with an in-plane hexagonal arrangement of the atoms is employed. By applying Atomic Layer Deposition (ALD), epitaxial growth of the ε-phase was achieved at lower temperature, while the overall uniformity resulted improved, even on large sapphire substrates.

  15. Process control of MOCVD growth for LEDs by in-situ photoluminescence

    NASA Astrophysics Data System (ADS)

    Prall, C.; Haberland, K.; Kaspari, C.; Brunner, F.; Weyers, M.; Rueter, D.

    2016-03-01

    Development and manufacturing of LED structures is still driven by production cost reduction and performance improvements. Therefore, in-situ monitoring during the epitaxial process plays a key role in view of further yield improvement and process optimization. With the continuing trend towards larger wafers, stronger bow and increased aspherical curvature are additional challenges the growers have to face, leading to non-uniform LED-emission. Compared to traditional in-situ metrology like curvature measurement and near UV pyrometry, in-situ photoluminescence measurements can provide a more direct access to the quantum well emission already during growth. In this paper we show how in-situ photoluminescence measurements can be used in a production type multi-wafer MOCVD system to characterize the quantum well emission already during growth. We also demonstrate how deviations from the desired wavelength can be detected and corrected in the same growth run. Since the method is providing spatially resolved line-scans across the wafer, also the uniformity of the emission wavelength can be characterized already during growth. Comparison of in-situ and ex-situ photoluminescence data show excellent agreement with respect to wavelength uniformity on 4 inch wafers.

  16. Effect of Deposition Temperature on the Properties of TIO2 Thin Films Deposited by Mocvd

    NASA Astrophysics Data System (ADS)

    Khalifa, Zaki S.

    2016-02-01

    Crystal structure, microstructure, and optical properties of TiO2 thin films deposited on quartz substrates by metal-organic chemical vapor deposition (MOCVD) in the temperature range from 250∘C to 450∘C have been studied. The crystal structure, thickness, microstructure, and optical properties have been carried out using X-ray diffraction (XRD), field emission scanning electron microscope (FESEM), atomic force microscope (AFM), and UV-visible transmittance spectroscopy, respectively. XRD patterns show that the obtained films are pure anatase. Simultaneously, the crystal size calculated using XRD peaks, and the grain size measured by AFM decrease with the increase in deposition temperature. Moreover, the texture of the films change and roughness decrease with the increase in deposition temperature. The spectrophotometric transmittance spectra have been used to calculate the refractive index, extinction coefficient, dielectric constant, optical energy gap, and porosity of the deposited films. While the refractive index and dielectric constant decrease with the increase of deposition temperature, the porosity shows the opposite.

  17. High Growth Rate YSZ Thermal Barrier Coatings Deposited by MOCVD Demonstrate High Thermal Cycling Lifetime

    SciTech Connect

    Varanasi, Venu G; Besmann, Theodore M; Payzant, E Andrew; Pint, Bruce A; Lothian, Janet L; Anderson, Timothy J

    2011-01-01

    Yttria-stabilized zirconia (YSZ) thermal barrier coatings (TBC) were prepared by metalorganic chemical vapor deposition (MOCVD) using Y(OBut{sup n}){sub 3}, Zr(OBut{sup n}){sub 4} precursors and O{sub 2} carrier gas. A thermodynamic analysis guided experiments by optimizing elemental molar (n) stoichiometric ratios for the (Zr-Y-O-C-H system). This analysis showed single-phase YSZ was favored at 950 C, 1 kPa, n{sub O}/(n{sub Y} + n{sub Zr}) > 30, n{sub Y}/(n{sub Y} + n{sub Zr}) = 0.06-0.10 (fixed n{sub C}, n{sub H}). Experimental YSZ growth had multiple phases (fcc, monoclinic), had a relatively high growth rate (43 {micro}m/h, 1005 C), had an Arrhenius dependence (845-950 C, E{sub a} = 53.8 {+-} 7.9 kJ/mol), had columnar grains (SEM analysis), and had a coating through-thickness n{sub Y}/(n{sub Y} + n{sub Zr}) = 0.04 (EPMA analysis). Doubling the inlet yttrium precursor mole fraction resulted in fcc YSZ growth with a coating through-thickness n{sub Y}/(n{sub Y} + n{sub Zr}) = 0.07. Hot-insertion thermal cycling of YSZ coatings on FeCrAlY bond coats showed >1000 h lifetime, matching current standards for EB-PVD YSZ coatings.

  18. MOCVD growth of AlGaInP at atmospheric pressure using triethylmetals and phosphine

    NASA Astrophysics Data System (ADS)

    Ikeda, M.; Nakano, K.; Mori, Y.; Kaneko, K.; Watanabe, N.

    1986-09-01

    (Al xGa 1- x) 0.5In 0.5P quaternary alloy has been successfully grown by conventional atmospheric-pressure MOCVD using triethylaluminum, triethylgallium, triethylindium and phosphine as source materials. The relationship between photoluminescence (PL) line width and lattice mismatch ( {δa}/{a}) was examined. PL spectra at 4 K showed a line width narrower than 12 meV for layers with x less than 0.3 ( {δa}/{a ⩽ 1×10 -3}. Very narrow, down to 10 Å thick (A1 0.5Ga 0.50.5In 0.5P/Ga 0.5In 0.50.5Ga 0.5) 0.5In 0.5P quantum wells have been grown with no growth interruption at the heterojunction. 4 K PL spectra from 30 Å thick GaInP double quantum wells separated by 5, 10 and 20 Å thick A1GaInP barrier layers had a single peak, suggesting that no cluster on any significant size was formed in the A1GaInP alloy. An A1GaInP/GaInP double heterostructure laser operated continuously at room temperature with an emission wavelength from 670 to 680 nm.

  19. Effects of Au on the Growth of ZnO Nanostructures on Si by MOCVD

    NASA Astrophysics Data System (ADS)

    Cong, Chen; Fan, Lu Yang; Ping, He Hai; Wei, Wu Ke; Zhen, Ye Zhi

    2013-08-01

    The effects of Au on the growth of ZnO nanostructures on Si by metal organic chemical vapor deposition (MOCVD) at a relatively low temperature (450°C) were investigated. The experimental results showed that Au nanoparticles played a critical role during the growth of the ZnO nanostructures and affected their morphology and optical properties. It was found that Au nanoparticles particularly affected the nucleation of ZnO nanostructures during the growth process and the Au-assisted growth mechanism of ZnO nanostructures should be ascribed to the vapor-solid (VS) mechanism. The formation of a nanoneedle may be attributed to a more reactive interface between Au and ZnO, which leads to more zinc gaseous species absorbed near the interface. Different nucleation sites on ZnO nuclei resulted in the disorder of ZnO nanoneedles. Moreover, the crystalline quality of nano-ZnO was improved due to the presence of Au, according to the smaller full width at half maximum (FWHM) of the low-temperature exciton emission. We confirmed that ZnO nanoneedles showed better crystalline quality than ZnO nanorods through the HRTEM images and the SAED patterns. The reason for the improvement of the crystalline quality of nano-ZnO may be due to the less lattice mismatch.

  20. Microstructure Characteristics of High Lift Factor MOCVD REBCO Coated Conductors With High Zr Content

    SciTech Connect

    Galstyan, E; Gharahcheshmeh, MH; Delgado, L; Xu, AX; Majkic, G; Selvamanickam, V

    2015-06-01

    We report the microstructural characteristics of high levels of Zr-added REBa2Cu3O7-x (RE = Gd, Y rare earth) coated conductors fabricated by Metal Organic Chemical Vapor Deposition (MOCVD). The enhancements of the lift factor defined as a ratio of the in-field (3 T, B parallel to c-axis) critical current density (J(c)) at 30 K and self-field J(c) at 77 K have been achieved for Zr addition levels of 20 and 25 mol% via optimization of deposition parameters. The presence of strong flux pinning is attributed to the aligned nanocolumns of BaZrO3 and nanoprecipitates embedded in REBa2Cu3O7-x matrix with good crystal quality. A high density of BZO nanorods with a typical size 6-8 nm and spacing of 20 nm has been observed. Moreover, the high Zr content was found to induce a high density of intrinsic defects, including stacking faults and dislocations. The correlation between in-field performance along the c-axis and microstructure of (Gd, Y) BCO film with a high level of Zr addition is discussed.

  1. Diogene pictorial drift chamber

    SciTech Connect

    Gosset, J.

    1984-01-01

    A pictorial drift chamber, called DIOGENE, has been installed at Saturne in order to study central collisions of high energy heavy ions. It has been adapted from the JADE internal detector, with two major differences to be taken into account. First, the center-of-mass of these collisions is not identical to the laboratory reference frame. Second, the energy loss and the momentum ranges of the particles to be detected are different from the ones in JADE. It was also tried to keep the cost as small as possible, hence the choice of minimum size and minimum number of sensitive wires. Moreover the wire planes are shifted from the beam axis: this trick helps very much to quickly reject the bad tracks caused by the ambiguity of measuring drift distances (positive or negative) through times (always positive).

  2. Mush Column Magma Chambers

    NASA Astrophysics Data System (ADS)

    Marsh, B. D.

    2002-12-01

    Magma chambers are a necessary concept in understanding the chemical and physical evolution of magma. The concept may well be similar to a transfer function in circuit or time series analysis. It does what needs to be done to transform source magma into eruptible magma. In gravity and geodetic interpretations the causative body is (usually of necessity) geometrically simple and of limited vertical extent; it is clearly difficult to `see' through the uppermost manifestation of the concentrated magma. The presence of plutons in the upper crust has reinforced the view that magma chambers are large pots of magma, but as in the physical representation of a transfer function, actual magma chambers are clearly distinct from virtual magma chambers. Two key features to understanding magmatic systems are that they are vertically integrated over large distances (e.g., 30-100 km), and that all local magmatic processes are controlled by solidification fronts. Heat transfer considerations show that any viable volcanic system must be supported by a vertically extensive plumbing system. Field and geophysical studies point to a common theme of an interconnected stack of sill-like structures extending to great depth. This is a magmatic Mush Column. The large-scale (10s of km) structure resembles the vertical structure inferred at large volcanic centers like Hawaii (e.g., Ryan et al.), and the fine scale (10s to 100s of m) structure is exemplified by ophiolites and deeply eroded sill complexes like the Ferrar dolerites of the McMurdo Dry Valleys, Antarctica. The local length scales of the sill reservoirs and interconnecting conduits produce a rich spectrum of crystallization environments with distinct solidification time scales. Extensive horizontal and vertical mushy walls provide conditions conducive to specific processes of differentiation from solidification front instability to sidewall porous flow and wall rock slumping. The size, strength, and time series of eruptive behavior

  3. HATCH CONNECTING TEMPERED AIR CHAMBER AND HOT AIR CHAMBER OF ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    HATCH CONNECTING TEMPERED AIR CHAMBER AND HOT AIR CHAMBER OF PLENUM WITH ATTACHED DRAFT REGULATOR. - Hot Springs National Park, Bathhouse Row, Superior Bathhouse: Mechanical & Piping Systems, State Highway 7, 1 mile north of U.S. Highway 70, Hot Springs, Garland County, AR

  4. Optical properties of InGaN grown by MOCVD on sapphire and on bulk GaN

    NASA Astrophysics Data System (ADS)

    Osinski, Marek; Eliseev, Petr G.; Lee, Jinhyun; Smagley, Vladimir A.; Sugahara, Tamoya; Sakai, Shiro

    1999-11-01

    Experimental data on photoluminescence of various bulk and quantum-well epitaxial InGaN/GaN structures grown by MOCVD are interpreted in terms of a band-tail model of inhomogeneously broadened radiative recombination. The anomalous temperature-induced blue spectral is shown to result from band-tail recombination under non-degenerate conditions. Significant differences are observed between epilayers grown on sapphire substrates and on GaN substrates prepared by the sublimination method, with no apparent evidence of band tails in homoepitaxial structures, indicating their higher crystalline quality.

  5. Fabrication of low-density GaN/AlN quantum dots via GaN thermal decomposition in MOCVD

    PubMed Central

    2014-01-01

    With an appropriate high anneal temperature under H2 atmosphere, GaN quantum dots (QDs) have been fabricated via GaN thermal decomposition in metal organic chemical vapor deposition (MOCVD). Based on the characterization of atomic force microscopy (AFM), the obtained GaN QDs show good size distribution and have a low density of 2.4 × 108 cm-2. X-ray photoelectron spectroscopy (XPS) analysis demonstrates that the GaN QDs were formed without Ga droplets by thermal decomposition of GaN. PMID:25136276

  6. Optoelectronic and structural properties of InGaN nanostructures grown by plasma-assisted MOCVD

    NASA Astrophysics Data System (ADS)

    Seidlitz, Daniel; Senevirathna, M. K. I.; Abate, Y.; Hoffmann, A.; Dietz, N.

    2015-09-01

    This paper presents optoelectronic and structural layer properties of InN and InGaN epilayers grown on sapphire templates by Migration-Enhanced Plasma Assisted Metal Organic Chemical Vapor Deposition (MEPA-MOCVD). Real-time characterization techniques have been applied during the growth process to gain insight of the plasma-assisted decomposition of the nitrogen precursor and associated growth surface processes. Analyzed Plasma Emission Spectroscopy (PES) and UV Absorption Spectroscopy (UVAS) provide detection and concentrations of plasma generated active species (N*/NH*/NHx*). Various precursors have been used to assess the nitrogen-active fragments that are directed from the hollow cathode plasma tube to the growth surface. The in-situ diagnostics results are supplemented with ex-situ materials structures investigation results of nanoscale structures using Scanning Near-field Optical Microscopy (SNOM). The structural properties have been analyzed by Raman spectroscopy and Fourier transform infrared (FTIR) reflectance. The Optoelectronic and optical properties were extracted by modeling the FTIR reflectance (e.g. free carrier concentration, high frequency dielectric constant, mobility) and optical absorption spectroscopy. The correlation and comparison between the in-situ metrology results with the ex-situ nano-structural and optoelectronic layer properties provides insides into the growth mechanism on how plasma-activated nitrogen-fragments can be utilized as nitrogen precursor for group III-nitride growth. The here assessed growth process parameter focus on the temporal precursor exposure of the growth surface, the reactor pressure, substrate temperature and their effects of the properties of the InN and InGaN epilayers.

  7. Characterization of high-purity arsine and gallium arsenide epilayers grown by MOCVD

    NASA Astrophysics Data System (ADS)

    Feng, Jun; Clement, Ryan; Raynor, Mark

    2008-11-01

    Impurities present in the metal organic chemical vapor deposition (MOCVD) process gases and precursors can have a significant effect on the performance of III-V compound semiconductor devices. High-purity arsine purified using chemical, adsorption and distillation techniques, has been characterized for impurities by using high sensitivity gas analysis methods and low temperature photoluminescence (PL) of GaAs epilayers. Permanent gas, hydrocarbon and dopant impurities can all be removed using these purification methods to below the detection limit of instrumentation (low nmol mol -1-pmol mol -1, depending on method). Capability to remove water vapor to single digit nmol mol -1 levels is also demonstrated and cylinder depletion studies show that gas-phase arsine, with consistently low H 2O, can be delivered from the cylinder, even well after phase break. Low temperature PL measurements are made on 10 μm GaAs/GaAs grown with three different arsine sources. Well-resolved near-band emission characteristics of high-purity n-type GaAs is obtained with high-purity distilled arsine. PL of epilayers grown with less pure arsine show the presence of Ge as well as elevated levels of Mg and Zn, incorporated from the trimethylgallium. The incorporation of O from an arsine cylinder containing H 2O at 200 nmol mol -1 results in reduced full width at half maximum (FWHM) of the near-band emission and decreased ( D0, X) and ( F, X) intensity, highlighting the importance of minimizing H 2O impurity.

  8. Study of carrier recombination transient characteristics in MOCVD grown GaN dependent on layer thickness

    SciTech Connect

    Gaubas, E. Čeponis, T.; Jasiunas, A.; Jelmakas, E.; Juršėnas, S.; Kadys, A.; Malinauskas, T.; Tekorius, A.; Vitta, P.

    2013-11-15

    The MOCVD grown GaN epi-layers of different thickness have been examined in order to clarify a role of surface recombination, to separate an impact of radiative and non-radiative recombination and disorder factors. The microwave probed –photoconductivity (MW-PC) and spectrally resolved photo-luminescence (PL) transients were simultaneously recorded under ultraviolet (UV) light 354 nm pulsed 500 ps excitation. The MW-PC transients exhibited the carrier decay components associated with carrier decay within micro-crystals and the disordered structure on the periphery areas surrounding crystalline columns. Three PL bands were resolved within PL spectrum, namely, the exciton ascribed UV-PL band edge for hν>3.3 eV, blue B-PL band for 2.5 < hν < 3.0 eV and yellow Y-PL band with hν < 2.4 eV. It has been obtained that intensity of UV-PL band increases with excitation density, while intensity of B-PL band is nearly invariant. However, intensity of the Y-PL increases with reduction of the excitation density. The Y-PL can be associated with trapping centers. A reduction of UV excitation density leads to a decrease of the relative amplitude of the asymptotic component within the MW-PC transients and to an increase of the amplitude as well as duration of the yellow spectral band (Y-PL) asymptotic component. Fractional index α with values 0.5 < α < 0.8 was evaluated for the stretched-exponent component which fits the experimental transients determined by the disordered structure ascribed to the periphery areas surrounding the crystalline columns.

  9. Small rocket flowfield diagnostic chambers

    NASA Technical Reports Server (NTRS)

    Morren, Sybil; Reed, Brian

    1993-01-01

    Instrumented and optically-accessible rocket chambers are being developed to be used for diagnostics of small rocket (less than 440 N thrust level) flowfields. These chambers are being tested to gather local fluid dynamic and thermodynamic flowfield data over a range of test conditions. This flowfield database is being used to better understand mixing and heat transfer phenomena in small rockets, influence the numerical modeling of small rocket flowfields, and characterize small rocket components. The diagnostic chamber designs include: a chamber design for gathering wall temperature profiles to be used as boundary conditions in a finite element heat flux model; a chamber design for gathering inner wall temperature and static pressure profiles; and optically-accessible chamber designs, to be used with a suite of laser-based diagnostics for gathering local species concentration, temperature, density, and velocity profiles. These chambers were run with gaseous hydrogen/gaseous oxygen (GH2/GO2) propellants, while subsequent versions will be run on liquid oxygen/hydrocarbon (LOX/HC) propellants. The purpose, design, and initial test results of these small rocket flowfield diagnostic chambers are summarized.

  10. Fast-response cloud chamber

    NASA Technical Reports Server (NTRS)

    Fogal, G. L.

    1977-01-01

    Wall structure keeps chambers at constant, uniform temperature, yet allows them to be cooled rapidly if necessary. Wall structure, used in fast-response cloud chamber, has surface heater and coolant shell separated by foam insulation. It is lightweight and requires relatively little power.

  11. Beam Window for Pressure Chambers

    NASA Technical Reports Server (NTRS)

    Bransford, J. W.; Austin, J. G., Jr.

    1985-01-01

    Window resists products of combustion experiments. Sodium chloride window seals over chamber pressures from 0.1 to 13.8 MPa while absorbing minimal energy from CO2 laser beam that passes through it into chamber. Window inexpensive and easily replacable.

  12. Chamber Music: Skills and Teamwork.

    ERIC Educational Resources Information Center

    Villarrubia, Charles

    2000-01-01

    Focuses on the benefits of participating in chamber music ensembles, such as the development of a heightened level of awareness, and considers the role of the music educator/conductor. Provides tools and exercises that teachers can introduce to chamber music players to improve their rehearsals and performances. (CMK)

  13. LRL 25-inch Bubble Chamber

    DOE R&D Accomplishments Database

    Alvarez, L. W.; Gow, J. D.; Barrera, F.; Eckman, G.; Shand, J.; Watt, R.; Norgren, D.; Hernandez, H. P.

    1964-07-08

    The recently completed 25-inch hydrogen bubble chamber combines excellent picture quality with a fast operating cycle. The chamber has a unique optical system and is designed to take several pictures each Bevatron pulse, in conjunction with the Bevatron rapid beam ejection system.

  14. National Ignition Facility Target Chamber

    SciTech Connect

    Wavrik, R W; Cox, J R; Fleming, P J

    2000-10-05

    On June 11, 1999 the Department of Energy dedicated the single largest piece of the National Ignition Facility (NIF) at Lawrence Livermore National Laboratory (LLNL) in Livermore, California. The ten (10) meter diameter aluminum target high vacuum chamber will serve as the working end of the largest laser in the world. The output of 192 laser beams will converge at the precise center of the chamber. The laser beams will enter the chamber in two by two arrays to illuminate 10 millimeter long gold cylinders called hohlraums enclosing 2 millimeter capsule containing deuterium, tritium and isotopes of hydrogen. The two isotopes will fuse, thereby creating temperatures and pressures resembling those found only inside stars and in detonated nuclear weapons, but on a minute scale. The NIF Project will serve as an essential facility to insure safety and reliability of our nation's nuclear arsenal as well as demonstrating inertial fusion's contribution to creating electrical power. The paper will discuss the requirements that had to be addressed during the design, fabrication and testing of the target chamber. A team from Sandia National Laboratories (SNL) and LLNL with input from industry performed the configuration and basic design of the target chamber. The method of fabrication and construction of the aluminum target chamber was devised by Pitt-Des Moines, Inc. (PDM). PDM also participated in the design of the chamber in areas such as the Target Chamber Realignment and Adjustment System, which would allow realignment of the sphere laser beams in the event of earth settlement or movement from a seismic event. During the fabrication of the target chamber the sphericity tolerances had to be addressed for the individual plates. Procedures were developed for forming, edge preparation and welding of individual plates. Construction plans were developed to allow the field construction of the target chamber to occur parallel to other NIF construction activities. This was

  15. Ion chamber based neutron detectors

    DOEpatents

    Derzon, Mark S; Galambos, Paul C; Renzi, Ronald F

    2014-12-16

    A neutron detector with monolithically integrated readout circuitry, including: a bonded semiconductor die; an ion chamber formed in the bonded semiconductor die; a first electrode and a second electrode formed in the ion chamber; a neutron absorbing material filling the ion chamber; and the readout circuitry which is electrically coupled to the first and second electrodes. The bonded semiconductor die includes an etched semiconductor substrate bonded to an active semiconductor substrate. The readout circuitry is formed in a portion of the active semiconductor substrate. The ion chamber has a substantially planar first surface on which the first electrode is formed and a substantially planar second surface, parallel to the first surface, on which the second electrode is formed. The distance between the first electrode and the second electrode may be equal to or less than the 50% attenuation length for neutrons in the neutron absorbing material filling the ion chamber.

  16. Proton beam monitor chamber calibration.

    PubMed

    Gomà, C; Lorentini, S; Meer, D; Safai, S

    2014-09-01

    The first goal of this paper is to clarify the reference conditions for the reference dosimetry of clinical proton beams. A clear distinction is made between proton beam delivery systems which should be calibrated with a spread-out Bragg peak field and those that should be calibrated with a (pseudo-)monoenergetic proton beam. For the latter, this paper also compares two independent dosimetry techniques to calibrate the beam monitor chambers: absolute dosimetry (of the number of protons exiting the nozzle) with a Faraday cup and reference dosimetry (i.e. determination of the absorbed dose to water under IAEA TRS-398 reference conditions) with an ionization chamber. To compare the two techniques, Monte Carlo simulations were performed to convert dose-to-water to proton fluence. A good agreement was found between the Faraday cup technique and the reference dosimetry with a plane-parallel ionization chamber. The differences-of the order of 3%-were found to be within the uncertainty of the comparison. For cylindrical ionization chambers, however, the agreement was only possible when positioning the effective point of measurement of the chamber at the reference measurement depth-i.e. not complying with IAEA TRS-398 recommendations. In conclusion, for cylindrical ionization chambers, IAEA TRS-398 reference conditions for monoenergetic proton beams led to a systematic error in the determination of the absorbed dose to water, especially relevant for low-energy proton beams. To overcome this problem, the effective point of measurement of cylindrical ionization chambers should be taken into account when positioning the reference point of the chamber. Within the current IAEA TRS-398 recommendations, it seems advisable to use plane-parallel ionization chambers-rather than cylindrical chambers-for the reference dosimetry of pseudo-monoenergetic proton beams. PMID:25109620

  17. Electrical properties of ferroelectric-gate FETs with SrBi2Ta2O9 formed using MOCVD technique

    NASA Astrophysics Data System (ADS)

    Yan, Kang; Takahashi, Mitsue; Sakai, Shigeki

    2012-09-01

    Ferroelectric-gate field-effect transistors (FeFETs) with a Pt/SrBi2Ta2O9/Hf-Al-O/Si gate stack were fabricated using the metal-organic chemical vapor deposition (MOCVD) technique to prepare the SrBi2Ta2O9 (SBT) ferroelectric layer. A good threshold voltage ( V th) distribution was found for more than 90 n-channel FeFETs in one chip with a 170 nm SBT layer owing to the good film uniformity of the SBT layer deposited by MOCVD. The average memory window (Vw^{av}) and the standard deviations ( σ thl, σ thr) of the left- and right-side branches of the drain-gate voltage curves of the FeFETs yielded a Vw^{av}/(σ_{thl} + σ_{thr}) value of 5.45, indicating that the FeFETs can be adapted for large-scale-integration. The electric field, the energy band profile in the gate stack, and the gate leakage current were also investigated at high gate voltages. We found that the effect of Fowler-Nordheim tunneling appeared under these conditions. Because of the tunneling injection and trapping of electrons into the gate insulators, the operation voltage ranges of the FeFETs were limited by this tunneling.

  18. The finite size effect on the metal-insulator transition of MOCVD grown VO{sub 2} films

    SciTech Connect

    Kim, Hyung Kook; Chiarello, R.P.; You, Hoydoo; Chang, M.H.L.; Zhang, T.J.; Lam, D.J.

    1991-11-01

    We studied the finite size effect on the metal-insulator phase transition and the accompanying tetragonal to monoclinic structural phase transition of VO{sub 2} films grown by MOCVD. X-ray diffraction measurements and electrical conductivity measurements were done as a function of temperature for VO{sub 2} films with out-of-plane particle size ranging from 60--310 {Angstrom}. Each Vo{sub 2} film was grown on a thin TiO{sub 2} buffer layer, which in turn was grown by MOCVD on a polished sapphire (112) substrate. The transition was found to be first order. As the out-of-plane particle size becomes larger, the transition temperature shifts and the transition width narrows. For the 60{Angstrom} film the transition was observed at {approximately}61{degrees}C with a transition width if {approximately}10{degrees}C, while for the 310{Angstrom} film the transition temperature was {approximately}59{degrees}C and the transition width {approximately} 2{degree}C. We also observed thermal hysteresis for each film, which became smaller with increasing particle size.

  19. The finite size effect on the metal-insulator transition of MOCVD grown VO sub 2 films

    SciTech Connect

    Kim, Hyung Kook; Chiarello, R.P.; You, Hoydoo; Chang, M.H.L.; Zhang, T.J.; Lam, D.J.

    1991-11-01

    We studied the finite size effect on the metal-insulator phase transition and the accompanying tetragonal to monoclinic structural phase transition of VO{sub 2} films grown by MOCVD. X-ray diffraction measurements and electrical conductivity measurements were done as a function of temperature for VO{sub 2} films with out-of-plane particle size ranging from 60--310 {Angstrom}. Each Vo{sub 2} film was grown on a thin TiO{sub 2} buffer layer, which in turn was grown by MOCVD on a polished sapphire (112) substrate. The transition was found to be first order. As the out-of-plane particle size becomes larger, the transition temperature shifts and the transition width narrows. For the 60{Angstrom} film the transition was observed at {approximately}61{degrees}C with a transition width if {approximately}10{degrees}C, while for the 310{Angstrom} film the transition temperature was {approximately}59{degrees}C and the transition width {approximately} 2{degree}C. We also observed thermal hysteresis for each film, which became smaller with increasing particle size.

  20. Influence of Mg and In on defect formation in GaN; bulk and MOCVD grown samples

    SciTech Connect

    Liliental-Weber, Z.; Benamara, M.; Jasinski, J.; Swider, W.; Washburn, J.; Grzegory, I.; Porowski, S.; Bak-Misiuk, J.; Domagala, J.; Bedair, S.; Eiting, C.J.; Dupuis, R.D.

    2000-11-22

    Transmission electron microscopy studies were applied to study GaN crystals doped with Mg. Both: bulk GaN:Mg crystals grown by a high pressure and high temperature process and those grown by metal-organic chemical-vapor deposition (MOCVD) have been studied. Structural dependence on growth polarity was observed in the bulk crystals. Spontaneous ordering (formation of polytypoids) was observed for growth in the N to Ga polar direction (N polarity). On the opposite site of the crystal (growth in the Ga to N polar direction) Mg-rich pyramidal defects with base on the basal planes and with walls inclined about 45O to these planes, empty inside (pinholes) were observed. A high concentration of these pyramidal defects was also observed in the MOCVD grown crystals. For samples grown with Mg delta doping planar defects were also observed especially at the early stages of growth followed by formation of pyramidal defects. TEM and x-ray studies of InxGa{sub 1{minus}x}N crystals for the range of 28-45% nominal In concentration shows formation of two sub-layers: strained and relaxed, with a much lower In concentration in the strained layer. Layers with the highest In concentration were fully relaxed.

  1. Fabrication of GdBa2Cu3O7-δ films by photo-assisted-MOCVD process

    NASA Astrophysics Data System (ADS)

    Li, Wei; Li, Guoxing; Zhang, Baolin; Chou, Penchu; Liu, Suping; Ma, Xiaoyu

    2014-06-01

    Pure GdBa2Cu3O7-δ (GdBCO) films were deposited on (1 0 0)-oriented LaAlO3 (LAO) substrates by photo-assisted metal organic chemical vapor deposition (PhA-MOCVD) technique. The effects of substrate temperature (Ts) and oxygen partial pressure (Po2) on microstructure, growth rate and superconducting critical current density (Jc) were investigated. A dense and no grain boundary visible, single-crystal-like cross-sectional morphology was observed. For the GdBCO film sample obtained at Ts of 810 °C and Po2 of 4 Torr, the full width at half-maximum were 0.08° and 0.41° for out-of-plane and in-plane orientations, respectively. Such low values were similar to that of single crystal GdBCO. Optimally processed GdBCO samples exhibited Jc of 2.5 MA/cm2 at 77 K in self-field. A relatively high growth rate of 0.104 μm/min for the GdBCO film is realized by the PhA-MOCVD technique.

  2. Status of HgCdTe Barrier Infrared Detectors Grown by MOCVD in Military University of Technology

    NASA Astrophysics Data System (ADS)

    Kopytko, M.; Jóźwikowski, K.; Martyniuk, P.; Gawron, W.; Madejczyk, P.; Kowalewski, A.; Markowska, O.; Rogalski, A.; Rutkowski, J.

    2016-06-01

    In this paper we present the status of HgCdTe barrier detectors with an emphasis on technological progress in metalorganic chemical vapor deposition (MOCVD) growth achieved recently at the Institute of Applied Physics, Military University of Technology. It is shown that MOCVD technology is an excellent tool for HgCdTe barrier architecture growth with a wide range of composition, donor/acceptor doping, and without post-grown annealing. The device concept of a specific barrier bandgap architecture integrated with Auger-suppression is as a good solution for high-operating temperature infrared detectors. Analyzed devices show a high performance comparable with the state-of-the-art of HgCdTe photodiodes. Dark current densities are close to the values given by "Rule 07" and detectivities of non-immersed detectors are close to the value marked for HgCdTe photodiodes. Experimental data of long-wavelength infrared detector structures were confirmed by numerical simulations obtained by a commercially available software APSYS platform. A detailed analysis applied to explain dark current plots was made, taking into account Shockley-Read-Hall, Auger, and tunneling currents.

  3. The domain structure features of epitaxial PbTiO{sub 3} thin films prepared by MOCVD

    SciTech Connect

    Bai, G.R.; Chang, H.L.M.; Foster, C.M.; Lam, D.J.

    1992-03-01

    Ferroelectric oxide thin films have attracted great interest in recent years because of their potential applications in numerous electro-optic, pyroelectric, acousto-optical, and nonvolatile memory devices, and a variety of methods such as sputtering, laser ablation, and MOCVD has been used for preparation of the films. Among these ferroelectric materials, the PbTiO{sub 3} thin film has been extensively studied because of its small dielectric constant, large spontaneous polarization, small coercive field, and high Curie temperature of {approximately}500{degrees}C. However, very little work has dealt with the detailed structural properties of the films. In this work, we have prepared epitaxial PbTiO{sub 3} thin films by MOCVD and performed some detailed studies on the structure of the films, particularly those related to the twin domain structure, using X-ray diffraction technique. Based on the comparison of the domain structure features of the films grown at above Curie temperature with those of the films grown at below Curie temperature as well as of bulk PbTiO{sub 3} single crystal, a model is proposed to explain our experimental results.

  4. The domain structure features of epitaxial PbTiO sub 3 thin films prepared by MOCVD

    SciTech Connect

    Bai, G.R.; Chang, H.L.M.; Foster, C.M.; Lam, D.J.

    1992-03-01

    Ferroelectric oxide thin films have attracted great interest in recent years because of their potential applications in numerous electro-optic, pyroelectric, acousto-optical, and nonvolatile memory devices, and a variety of methods such as sputtering, laser ablation, and MOCVD has been used for preparation of the films. Among these ferroelectric materials, the PbTiO{sub 3} thin film has been extensively studied because of its small dielectric constant, large spontaneous polarization, small coercive field, and high Curie temperature of {approximately}500{degrees}C. However, very little work has dealt with the detailed structural properties of the films. In this work, we have prepared epitaxial PbTiO{sub 3} thin films by MOCVD and performed some detailed studies on the structure of the films, particularly those related to the twin domain structure, using X-ray diffraction technique. Based on the comparison of the domain structure features of the films grown at above Curie temperature with those of the films grown at below Curie temperature as well as of bulk PbTiO{sub 3} single crystal, a model is proposed to explain our experimental results.

  5. Growth and conduction mechanism of As-doped p-type ZnO thin films deposited by MOCVD

    SciTech Connect

    Ma, Y.; Gao, Q.; Wu, G.G.; Li, W.C.; Gao, F.B.; Yin, J.Z.; Zhang, B.L.; Du, G.T.

    2013-03-15

    Highlight: ► P-type As-doped ZnO thin films was fabricated by MOCVD after post-growth annealing. ► The formation mechanism of p-ZnO with high hole concentration above 10{sup 19} cm{sup −3} was elucidated. ► Besides As{sub Zn}–2V{sub Zn} complex, C impurities also played an important role in realizing p-ZnO. ► The formations of As{sub O} and O-C-O complex were partially contributed to the p-type ZnO: As films. - Abstract: As-doped p-type ZnO thin films were fabricated by metal organic chemical vapor deposition (MOCVD) after in situ annealing in a vacuum. The p-type conduction mechanism was suggested by the analysis of X-ray photoelectron spectroscopy and ultraviolet photoemission spectroscopy. It was found that most of the As dopants in p-ZnO thin films formed As{sub Zn}–2V{sub Zn} shallow acceptor complex, simultaneously, carbon impurities also played an important role in realizing p-type conductivity in ZnO. Substitutional carbon on oxygen site created passivated defect bands by combining with Ga atoms due to the donor-acceptor pair Coulomb binding, which shifted the valence-band maximum upwards for ZnO and thus increased the hole concentration.

  6. Status of HgCdTe Barrier Infrared Detectors Grown by MOCVD in Military University of Technology

    NASA Astrophysics Data System (ADS)

    Kopytko, M.; Jóźwikowski, K.; Martyniuk, P.; Gawron, W.; Madejczyk, P.; Kowalewski, A.; Markowska, O.; Rogalski, A.; Rutkowski, J.

    2016-09-01

    In this paper we present the status of HgCdTe barrier detectors with an emphasis on technological progress in metalorganic chemical vapor deposition (MOCVD) growth achieved recently at the Institute of Applied Physics, Military University of Technology. It is shown that MOCVD technology is an excellent tool for HgCdTe barrier architecture growth with a wide range of composition, donor /acceptor doping, and without post-grown annealing. The device concept of a specific barrier bandgap architecture integrated with Auger-suppression is as a good solution for high-operating temperature infrared detectors. Analyzed devices show a high performance comparable with the state-of-the-art of HgCdTe photodiodes. Dark current densities are close to the values given by "Rule 07" and detectivities of non-immersed detectors are close to the value marked for HgCdTe photodiodes. Experimental data of long-wavelength infrared detector structures were confirmed by numerical simulations obtained by a commercially available software APSYS platform. A detailed analysis applied to explain dark current plots was made, taking into account Shockley-Read-Hall, Auger, and tunneling currents.

  7. Starting a High School Chamber Music Group.

    ERIC Educational Resources Information Center

    Rutkowski, Joseph

    2000-01-01

    Presents ideas on how to begin a chamber music ensemble. Discusses how to find time to accomplish chamber music playing in and around the school day. Presents short descriptions of chamber music that can be used with ensembles. Includes chamber music resources and additional chamber works. (CMK)

  8. Neutron detection via bubble chambers.

    PubMed

    Jordan, D V; Ely, J H; Peurrung, A J; Bond, L J; Collar, J I; Flake, M; Knopf, M A; Pitts, W K; Shaver, M; Sonnenschein, A; Smart, J E; Todd, L C

    2005-01-01

    Research investigating the application of pressure-cycled bubble chambers to fast neutron detection is described. Experiments with a Halon-filled chamber showed clear sensitivity to an AmBe neutron source and insensitivity to a (137)Cs gamma source. Bubble formation was documented using high-speed photography, and a ceramic piezo-electric transducer element registered the acoustic signature of bubble formation. In a second set of experiments, the bubble nucleation response of a Freon-134a chamber to an AmBe neutron source was documented with high-speed photography. PMID:16005238

  9. Energy band engineering using polarization induced interface charges in MOCVD grown III-nitride heterojunction devices

    NASA Astrophysics Data System (ADS)

    Tripathi, Neeraj

    2011-12-01

    Characteristics of III-nitride based heterojunction devices are greatly influenced by the presence of high density of polarization induced interface charges. Research undertaken in the current doctoral thesis demonstrates the effect of presence of one, three and six sheets of polarization induced charges in three different III-nitride based devices, namely in a photocathode, a high electron mobility transistor (HEMT) and a hyperspectral detector structure. Through a systematic set of experiments and theoretical modeling an in-depth study of the interaction between multiple sheets of polarization induced charges and their impact on energy band profile was undertaken. Various device designs were studied and optimized using device simulations. Subsequently device structures were grown using metallorganic chemical vapor deposition (MOCVD). Growth conditions for III-nitride epilayers were optimized for pressure, temperature and V/III ratio. Devices were fabricated using photolithography and e-beam evaporation. Novel GaN and GaN/AlGaN photocathode structures were developed. First demonstration of effective negative electron affinity (ENEA) in a GaN photocathode without the use of Cs was made. Effect of polarization induced surface charges on photoemission characteristics was successfully explained using simulated energy band diagrams. AlGaN/GaN/AlGaN/SiO2 based back barrier HEMT structures were developed in which bandgap, thin film thicknesses and polarization induced charge density were engineered to demonstrate Normally OFF operation along with the ability to engineer turn ON voltage of the device. Further, AlGaN based tunable hyperspectral detector pixel with 6-heterojunctions, for application in wavelength spectrometry from UV to IR part of the spectrum, was developed. The novel device design used in the hyperspectral detector utilized voltage tunable internal photoemission (IPE) barriers to measure the energy of the incident photon. Detailed IPE measurements were

  10. High-efficiency solar cells fabricated by vacuum MO-CVD

    NASA Technical Reports Server (NTRS)

    Fraas, L. M.; Cape, J. A.; Partain, L. D.; Mcleod, P. S.

    1984-01-01

    High-efficiency, monolithic, two-color, three-terminal solar cells were fabricated by a novel growth technique, vacuum metal-organic chemical vapor deposition. The technique uses the expensive metal alkyls efficiently and toxic gases sparingly. The fact that the outer chamber is constructed of nonbreakable stainless steel is an attractive safety feature associated with this deposition system.

  11. The multigap resistive plate chamber

    SciTech Connect

    Zeballos, E. Cerron; Crotty, I.; Hatzifotiadou, D.; Valverde, J. Lamas; Neupane, S.; Williams, M. C. S.; Zichichi, A.

    2015-02-03

    The paper describes the multigap resistive plate chamber (RPC). This is a variant of the wide gap RPC. However it has much improved time resolution, while keeping all the other advantages of the wide gap RPC design.

  12. Perspectives on anechoic chamber qualification

    NASA Astrophysics Data System (ADS)

    Cunefare, Kenneth A.; Biesel, Van B.

    2002-11-01

    The qualification of a new anechoic chamber requires demonstration that the chamber produces a free-field environment within some tolerance bounds and over some acceptable volume. At the most basic level, qualification requires measurement of sound levels at increasing distances from a test source, and then comparing the levels to a theoretical free-field decay. While simple in concept, the actual performance of a qualification test is problematic in implementation, with troublesome issues relevant to the nature of the sound source, test signal (broadband or pure tone), spatial resolution of measurements (e.g., measurements at discrete locations or spatially continuous), and comparison of the data to a theoretical decay. This presentation will provide a brief historical perspective on chamber qualification and review current practice. It will demonstrate the inadequacy of broadband noise and widely spaced discrete measurements for qualification purposes. It will demonstrate that pure tone signals and spatially continuous measurements provide a rigorous test of a chambers performance.

  13. Drift and proportional tracking chambers

    NASA Astrophysics Data System (ADS)

    Jaros, J. A.

    1980-11-01

    The many techniques exploited in constructing tracking chambers, particle detectors which measure the trajectories and momenta of charged particles, are discussed. In high energy interactions, the final states are dominated by closely collimated jets of high multiplicity, requiring good track-pair resolution in the tracking chamber. High energy particles deflect very little in limited magnetic field volumes, necessitating good spatial resolution for accurate momentum measurements. The colliding beam technique requires a device easily adapted to full solid angle coverage, and the high event rates expected in some of these machines put a premium on good time resolution. Finally, the production and subsequent decays of the tau, charmed and beautiful mesons provide multiple vertex topologies. To reconstruct these vertices reliably requires improvements in spatial resolution and track pair resolution. The proportional counter and its descendant, the drift chamber, are considered as tracking chambers. The physics of this device are discussed in order to understand its performance limitations and promises.

  14. IRIS Leaves Thermal Vacuum Chamber

    NASA Video Gallery

    This video shows the transportation of the IRIS observatory from the thermal vacuum chamber back to the clean tent for final testing and preparations for delivery to the launch site at Vandenberg A...

  15. Cyclically controlled welding purge chamber

    NASA Technical Reports Server (NTRS)

    Gallagher, Robert L. (Inventor)

    1996-01-01

    An arrangement for butt-welding cylindrical sections of large, thin-wall tanks includes a rotatable mandrel with side-by-side sets of radial position adjusters. Each set of adjusters bears on one of the tank sections adjacent the seam, to prevent the sections from sagging out-of-round. The mandrel rotates relative to the welder, so that a continuous seam is formed. A purge chamber is fixed in position behind the seam at the weld head, and is flushed with inert gas. The purge chamber includes a two-sided structure which is contiguous with the cylindrical sections and a circumferential vane to form an open-ended tube-like structure, through which the radial position adjusters pass as the mandrel and cylindrical workpiece sections rotate. The tube-like structure is formed into a chamber by a plurality of movable gates which are controlled to maintain a seal while allowing adjusters to progress through the purge chamber.

  16. Light diffusing fiber optic chamber

    DOEpatents

    Maitland, Duncan J.

    2002-01-01

    A light diffusion system for transmitting light to a target area. The light is transmitted in a direction from a proximal end to a distal end by an optical fiber. A diffusing chamber is operatively connected to the optical fiber for transmitting the light from the proximal end to the distal end and transmitting said light to said target area. A plug is operatively connected to the diffusing chamber for increasing the light that is transmitted to the target area.

  17. 63. Interior view, kitchen chamber, north elevation. The kitchen chamber ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    63. Interior view, kitchen chamber, north elevation. The kitchen chamber was completed in the first stages of phase III construction. The paneled wall to the fireplace's right displays a phase III molding profile. The mark between the cabinet doors and on the large lower panel indicates the former position of a partition wall. The chimney-breast paneling bears a phase I profile and might have been moved to the room when the fireplace mass in the hall was reduced. - John Bartram House & Garden, House, 54th Street & Lindbergh Boulevard, Philadelphia, Philadelphia County, PA

  18. Initial stages of TiO 2 thin films MOCVD growth studied by in situ surface analyses

    NASA Astrophysics Data System (ADS)

    Brevet, A.; Peterlé, P. M.; Imhoff, L.; Marco de Lucas, M. C.; Bourgeois, S.

    2005-02-01

    In situ chemical surface analyses using X-ray photoelectron spectroscopy (XPS) were performed to understand the initial stages of TiO 2 thin-film MOCVD growth. Deposits on Si (1 0 0), a few nanometres thick, were obtained at a fixed temperature of 650 °C and for two different pressures, 2.9 and 0.05 mbar, using titanium tetraisopropoxide (TTIP) as precursor. Pressure lowering led to a higher deposit growth rate. Reduction of titanium with respect to stoichiometric titanium dioxide and oxidation of the wet-cleaned silicon substrate are observed from decomposition of the Ti 2p and Si 2p peaks. The formation of a TiSi xO y mixed oxide is also pointed out and confirmed by the presence of a characteristic component in the O 1 s peak.

  19. Heavy p-type carbon doping of MOCVD GaAsP using CBrCl3

    NASA Astrophysics Data System (ADS)

    Heidelberger, Christopher; Fitzgerald, Eugene A.

    2016-07-01

    CBrCl3 is shown to be a useful precursor for heavy p-type carbon doping of GaAsxP1-x grown via metalorganic chemical vapor deposition (MOCVD) across a range of compositions. Structural and electrical properties of the GaAsP films were measured for various processing conditions. Use of CBrCl3 decreased the growth rate of GaAsP by up to 32% and decreases x by up to 0.025. The dependence of these effects on precursor inputs is investigated, allowing C-doped GaAsP films to be grown with good thickness and compositional control. Hole concentrations of greater than 2×1019 cm-3 were measured for values of x from 0.76 to 0.90.

  20. MOCVD of YBa 2Cu 3O 7-x thin films using a Ba fluorocarbon-based precursor

    NASA Astrophysics Data System (ADS)

    Fröhlich, K.; Šouc, J.; Chromik, S.; Machajdik, D.; Kliment, V.

    1992-11-01

    We have prepared superconducting YBa 2Cu 3O 7- x films by MOCVD using fluorocarbon based Ba(hfa) 2 precursor. The films were deposited at 500°C and annealed in low pressure ( pO2=10 -2Pa) dry oxygen atmosphere as well as in argon/oxygen mixture in the presence of water vapour. The samples on a MgO single crystal substrate had Tc( R=0)=79 K and Jc=10 4 A/cm 2 at T=30 K in zero magnetic field while the film on SrTiO 3, annealed under the same conditions had Tc( R=0)=86 K and Jc reached a value of 10 5 A/cm 2 at T=78 K.

  1. Analysis of HgTe/CdTe MOCVD grown superlattice epitaxial structures on GaAs by ion beam techniques

    NASA Astrophysics Data System (ADS)

    Wielunski, L. S.; Kenny, M. J.; Pain, G. N.

    1992-02-01

    Heteroepitaxial MOCVD grown HgTe/CdTe superlattice structures have been examined by Rutherford backscattering spectrometry (RBS) to monitor Hg, Cd and Te concentrations as a function of depth. Individual sublayers thicknesses have been measured at the same time. Crystal quality has been assessed using ion channeling. In addition the nuclear reaction 12C(d,p) 13C was used to detect carbon impurities and proton induced X-ray emision (PIXE) analysis used to detect In and Sb introduced during growth. The results show that the as-grown HgTe/CdTe superlattice has good crystal quality and reasonable lateral uniformity. Mercury concentration is difficult to control during growth and variation between sub-layers is observed. Hg-Cd interdiffusion is observed in heat treated samples. Carbon concentration varies; in a good quality samples ⩽ 20 ppm is present.

  2. The anti-surfactant effect of silane on the facets-controlled growth of GaN nanorods by MOCVD

    NASA Astrophysics Data System (ADS)

    Li, J. Z.; Chen, Z. Z.; Li, S. F.; Jiao, Q. Q.; Feng, Y. L.; Jiang, S. X.; Chen, Y. F.; Yu, T. J.; Shen, B.; Zhang, G. Y.

    2016-08-01

    N-polar GaN nanorods were selective area grown by continuous mode metalorganic chemical vapor deposition (MOCVD) under a Ga-rich and high silane flow condition. The interruption comparing with continuous supply of silane flow was performed to study the role of silane flux. High resolution scanning electron microscopy (SEM), x-ray diffraction (XRD), cathodoluminescence (CL) and x-ray photoelectron spectroscopy (XPS) measurements were performed. The enhanced vertical growth rate was achieved as 42 μm/h and sharp smooth m-plane, r-plane and c-plane facets were obtained for the nanorods with high silane flux. Sisbnd N bonds were clarified to be formed on the surface of the nanorod by XPS spectra. The silane acting as anti-surfactant was suggested to explain the diffusion and incorporation of the species on the facets of GaN nanorods.

  3. Multi-staged, InAsSb mid-infrared lasers and light-emitting diodes, grown by MOCVD

    SciTech Connect

    Kurtz, S.R.; Allerman, A.A.; Biefeld, R.M.; Baucom, K.C.

    1997-09-01

    Due to lower nonradiative rates, mid-infrared (2-6 micron) lasers with strained, narrow bandgap, Sb-based active regions have the potential to operate at lower current density and higher temperature than competing devices. Superior performance may be achieved through the {open_quotes}band structure engineered{close_quotes} reduction of Auger recombination and the implementation of multi-stage (or {open_quotes}cascaded{close_quotes}) active regions. We describe the first lasers and LEDs utilizing strained InAsSb, multi-stage active regions. An (n)InAs / (p)GaAsSb semimetal layer is incorporated into each stage as an internal electron-hole source. To date, 2-stage LEDs and 2-stage lasers have been demonstrated. Our multi-stage devices were grown by MOCVD.

  4. Driving Down HB-LED Costs. Implementation of Process Simulation Tools and Temperature Control Methods of High Yield MOCVD Growth

    SciTech Connect

    Quinn, William

    2012-04-30

    The overall objective of this multi-faceted program is to develop epitaxial growth systems that meet a goal of 75% (4X) cost reduction in the epitaxy phase of HB-LED manufacture. A 75% reduction in yielded epitaxy cost is necessary in order to achieve the cost goals for widespread penetration of HB-LED's into back-lighting units (BLU) for LCD panels and ultimately for solid-state lighting (SSL). To do this, the program will address significant improvements in overall equipment Cost of Ownership, or CoO. CoO is a model that includes all costs associated with the epitaxy portion of production. These aspects include cost of yield, capital cost, operational costs, and maintenance costs. We divide the program into three phases where later phases will incorporate the gains of prior phases. Phase one activities are enabling technologies. In collaboration with Sandia National Laboratories we develop a Fluent-compatible chemistry predictive model and a set of mid-infrared and near-ultraviolet pyrometer monitoring tools. Where previously the modeling of the reactor dynamics were studied within FLUENT alone, here, FLUENT and Chemkin are integrated into a comprehensive model of fluid dynamics and the most advanced transport equations developed for Chemkin. Specifically, the Chemkin model offered the key reaction terms for gas-phase nucleation, a key consideration in the optimization of the MOCVD process. This new predictive model is used to design new MOCVD reactors with optimized growth conditions and the newly developed pyrometers are used monitor and control the MOCVD process temperature to within 0.5°C run-to-run and within each wafer. This portion of the grant is in collaboration with partners at Sandia National Laboratories. Phase two activities are continuous improvement projects which extend the current reactor platform along the lines of improved operational efficiency, improved systems control for throughput, and carrier modifications for increased yield

  5. Plant growth chamber M design

    NASA Technical Reports Server (NTRS)

    Prince, R. P.; Knott, W. M.

    1986-01-01

    Crop production is just one of the many processes involved in establishing long term survival of man in space. The benefits of integrating higher plants into the overall plan was recognized early by NASA through the Closed Ecological Life Support System (CELSS) program. The first step is to design, construct, and operate a sealed (gas, liquid, and solid) plant growth chamber. A 3.6 m diameter by 6.7 m high closed cylinder (previously used as a hypobaric vessel during the Mercury program) is being modified for this purpose. The chamber is mounted on legs with the central axis vertical. Entrance to the chamber is through an airlock. This chamber will be devoted entirely to higher plant experimentation. Any waste treatment, food processing or product storage studies will be carried on outside of this chamber. Its primary purpose is to provide input and output data on solids, liquids, and gases for single crop species and multiple species production using different nutrient delivery systems.

  6. Emulsion Chamber Technology Experiment (ECT)

    NASA Technical Reports Server (NTRS)

    Gregory, John C.; Takahashi, Yoshiyuki

    1996-01-01

    The experimental objective of Emulsion Chamber Technology (ECT) was to develop space-borne emulsion chamber technology so that cosmic rays and nuclear interactions may subsequently be studied at extremely high energies with long exposures in space. A small emulsion chamber was built and flown on flight STS-62 of the Columbia in March 1994. Analysis of the several hundred layers of radiation-sensitive material has shown excellent post-flight condition and suitability for cosmic ray physics analysis at much longer exposures. Temperature control of the stack was 20 +/-1 C throughout the active control period and no significant deviations of temperature or pressure in the chamber were observed over the entire mission operations period. The unfortunate flight attitude of the orbiter (almost 90% Earth viewing) prevented any significant number of heavy particles (Z greater than or equal to 10) reaching the stack and the inverted flow of shower particles in the calorimeter has not allowed evaluation of absolute primary cosmic ray-detection efficiency nor of the practical time limits of useful exposure of these calorimeters in space to the level of detail originally planned. Nevertheless, analysis of the observed backgrounds and quality of the processed photographic and plastic materials after the flight show that productive exposures of emulsion chambers are feasible in low orbit for periods of up to one year or longer. The engineering approaches taken in the ECT program were proven effective and no major environmental obstacles to prolonged flight are evident.

  7. Neutron Detection via Bubble Chambers

    SciTech Connect

    Jordan, David V.; Ely, James H.; Peurrung, Anthony J.; Bond, Leonard J.; Collar, J. I.; Flake, Matthew; Knopf, Michael A.; Pitts, W. K.; Shaver, Mark W.; Sonnenschein, Andrew; Smart, John E.; Todd, Lindsay C.

    2005-10-06

    The results of a Pacific Northwest National Laboratory (PNNL) exploratory research project investigating the feasibility of fast neutron detection using a suitably prepared and operated, pressure-cycled bubble chamber are described. The research was conducted along two parallel paths. Experiments with a slow pressure-release Halon chamber at the Enrico Fermi Institute at the University of Chicago showed clear bubble nucleation sensitivity to an AmBe neutron source and insensitivity to the 662 keV gammas from a 137Cs source. Bubble formation was documented via high-speed (1000 frames/sec) photography, and the acoustic signature of bubble formation was detected using a piezo-electric transducer element mounted on the base of the chamber. The chamber’s neutron sensitivity as a function of working fluid temperature was mapped out. The second research path consisted of the design, fabrication, and testing of a fast pressure-release Freon-134a chamber at PNNL. The project concluded with successful demonstrations of the PNNL chamber’s AmBe neutron source sensitivity and 137Cs gamma insensitivity. The source response tests of the PNNL chamber were documented with high-speed photography.

  8. Plasma chemistry in wire chambers

    SciTech Connect

    Wise, J.

    1990-05-01

    The phenomenology of wire chamber aging is discussed and fundamentals of proportional counters are presented. Free-radical polymerization and plasma polymerization are discussed. The chemistry of wire aging is reviewed. Similarities between wire chamber plasma (>1 atm dc-discharge) and low-pressure rf-discharge plasmas, which have been more widely studied, are suggested. Construction and use of a system to allow study of the plasma reactions occurring in wire chambers is reported. A proportional tube irradiated by an {sup 55}Fe source is used as a model wire chamber. Condensable species in the proportional tube effluent are concentrated in a cryotrap and analyzed by gas chromatography/mass spectrometry. Several different wire chamber gases (methane, argon/methane, ethane, argon/ethane, propane, argon/isobutane) are tested and their reaction products qualitatively identified. For all gases tested except those containing methane, use of hygroscopic filters to remove trace water and oxygen contaminants from the gas resulted in an increase in the average molecular weight of the products, consistent with results from low-pressure rf-discharge plasmas. It is suggested that because water and oxygen inhibit polymer growth in the gas phase that they may also reduce polymer deposition in proportional tubes and therefore retard wire aging processes. Mechanistic implications of the plasma reactions of hydrocarbons with oxygen are suggested. Unresolved issues in this work and proposals for further study are discussed.

  9. MOCVD growth of magnesium zinc oxide films and nanostructures for photovoltaics

    NASA Astrophysics Data System (ADS)

    Duan, Ziqing

    MgxZn1-xO, which is formed by alloying ZnO with MgO, has been developed as a promising window layer in chalcopyrite thin film solar cells and hybrid polymer solar cells for enhanced open-circuit voltage and solar conversion efficiency because of its bandgap tunability. The surface morphology of MgxZn1-xO layers in those photovoltaic applications plays important roles on the performances of solar cells. Two-dimensional (2-D) dense and smooth film is preferred in the inorganic p-n junction solar cells while one-dimensional (1-D) nanostructures are favorable for the hybrid polymer solar cells. In this dissertation, metal-organic chemical vapor deposition (MOCVD) is used to grow both of MgxZn1-xO polycrystalline 2-D films and single crystalline 1-D nanostructures for solar cells. A low-temperature (~250°C) ZnO buffer layer, followed by the high-temperature (~500°C) growth of MgxZn1-xO, is found to be beneficial for the formation of a 2-D dense and smooth film. On the other hand, a high-temperature (~520°C) ZnO buffer layer followed by a high temperature (530°C-560°C) growth of MgxZn1-xO is needed to grow the 1-D Mg xZn1-xO (0≤x≤0.15) nanostructures on Si. For the first time, 1-D MgxZn1-xO nanostructures (0≤x≤0.1) are sequentially grown on a Ga-doped ZnO (GZO) 2-D film to form the 3-D photoelectrode, which is used to fabricate the P3HT-MgxZn1-xO hybride solar cells. The preliminary testing results of solar cells show that Mg xZn1-xO is promising to be used in hybrid polymer solar cells for the enhancement of open circuit voltage (VOC). MgxZn1-xO (0≤x≤0.1) polycrystalline films are used in Cu2O-MgxZn1-x O heterojunction solar cells. The current density-voltage (J-V) measurements of solar cells under illumination show that VOC, shunt resistance Rsh and the solar conversion efficiency η are improved with increasing of Mg% until 10%. A relatively high solar conversion efficiency, η AM1.5 = 0.71 % with a short circuit current JSC = 3.0 mA/cm 2 and VOC

  10. Heteroepitaxy of nitrogen-polar, nonpolar, and semipolar gallium nitride by MOCVD

    NASA Astrophysics Data System (ADS)

    Sun, Qian

    Since the early breakthroughs of two-step GaN growth and Mg-acceptor activation by Prof. Akasaki in the 1980s and Dr. Nakamura in the 1990s, nearly all the works related to GaN-based materials and devices were performed on Ga-polar (0001) c-plane. In spite of its popularity and technological dominance, Ga-polar c-plane orientation has fundamental limitations, including the well-known quantum confined Stark effect (QCSE) and the difficulty in micro-fabrication due to its chemical inertness. In the recent years, there has been increasing interest in exploring other crystallographic orientations for high brightness light-emitting diodes, enhancement mode transistors, and novel bio/chemical sensors, to name a few possibilities. This dissertation presents our investigations on the heteroepitaxy of N-polar c-plane (0001&barbelow;), nonpolar a-plane (112&barbelow;0) and m-plane (101&barbelow;0), as well as semipolar (112&barbelow;2) GaN by metalorganic chemical vapor deposition (MOCVD). To bypass the conventional knob-turning exercise for optimizing GaN heteroepitaxy process for each orientation, we constructed the first kinetic Wulff plots (growth rate polar plots) through differential selective area growth. Insights from the kinetic Wulff plots were used to explain complex phenomena in nonpolar GaN growth, including island formation, surface pits, and surface striations. Based on the kinetic Wulff plots, we designed and carried out a two-step growth of nonpolar a-plane (112&barbelow;0) GaN on r-plane sapphire. By correlating the morphological evolution with the microstructure of a-plane GaN, we proposed a model for the reduction of basal-plane stacking faults (BSFs) and associated partial dislocations (PDs). For the growth of nonpolar m-plane (101&barbelow;0) GaN on m-plane SiC, we demonstrated an effective way (Al composition graded AlGaN layers) for reducing the BSF density. The possible mechanisms for the formation of BSFs in nonpolar and semipolar GaN were

  11. Iridium-Coated Rhenium Combustion Chamber

    NASA Technical Reports Server (NTRS)

    Schneider, Steven J.; Tuffias, Robert H.; Rosenberg, Sanders D.

    1994-01-01

    Iridium-coated rhenium combustion chamber withstands operating temperatures up to 2,200 degrees C. Chamber designed to replace older silicide-coated combustion chamber in small rocket engine. Modified versions of newer chamber could be designed for use on Earth in gas turbines, ramjets, and scramjets.

  12. The CLAS drift chamber system

    SciTech Connect

    Mestayer, M.D.; Carman, D.S.; Asavaphibhop, B.

    1999-04-01

    Experimental Hall B at Jefferson Laboratory houses the CEBAF Large Acceptance Spectrometer, the magnetic field of which is produced by a superconducting toroid. The six coils of this toroid divide the detector azimuthally into six sectors, each of which contains three large multi-layer drift chambers for tracking charged particles produced from a fixed target on a toroidal axis. Within the 18 drift chambers are a total of 35,148 individually instrumented hexagonal drift cells. The novel geometry of these chambers provides for good tracking resolution and efficiency, along with large acceptance. The design and construction challenges posed by these large-scale detectors are described, and detailed results are presented from in-beam measurements.

  13. Impedances of Laminated Vacuum Chambers

    SciTech Connect

    Burov, A.; Lebedev, V.; /Fermilab

    2011-06-22

    First publications on impedance of laminated vacuum chambers are related to early 70s: those are of S. C. Snowdon [1] and of A. G. Ruggiero [2]; fifteen years later, a revision paper of R. Gluckstern appeared [3]. All the publications were presented as Fermilab preprints, and there is no surprise in that: the Fermilab Booster has its laminated magnets open to the beam. Being in a reasonable mutual agreement, these publications were all devoted to the longitudinal impedance of round vacuum chambers. The transverse impedance and the flat geometry case were addressed in more recent paper of K. Y. Ng [4]. The latest calculations of A. Macridin et al. [5] revealed some disagreement with Ref. [4]; this fact stimulated us to get our own results on that matter. Longitudinal and transverse impendances are derived for round and flat laminated vacuum chambers. Results of this paper agree with Ref. [5].

  14. Hydrostatic Hyperbaric Chamber Ventilation System

    NASA Technical Reports Server (NTRS)

    Sargusingh, Miriam M.

    2011-01-01

    The hydrostatic hyperbaric chamber (HHC) represents the merger of several technologies in development for NASA aerospace applications, harnessed to directly benefit global health. NASA has significant experience developing composite hyperbaric chambers for a variety of applications, including the treatment of medical conditions. NASA also has researched the application of water-filled vessels to increase tolerance of acceleration forces. The combination of these two applications has resulted in the hydrostatic chamber, which has been conceived as a safe, affordable means of making hyperbaric oxygen therapy available in the developing world for the treatment of a variety of medical conditions. Specifically, hyperbaric oxygen therapy is highly-desired as a possibly curative treatment for Buruli Ulcer, an infectious condition that afflicts children in sub-Saharan Africa. Hyperbaric oxygen therapy is simply too expensive and too dangerous to implement in the developing world using standard equipment. The hydrostatic hyperbaric chamber technology changes the paradigm. The HHC differs from standard hyperbaric chambers in that the majority of its volume is filled with water which is pressurized by oxygen being supplied in the portion of the chamber containing the patient s head. This greatly reduces the amount of oxygen required to sustain a hyperbaric atmosphere, thereby making the system more safe and economical to operate. An effort was taken to develop an HHC system to apply HBOT to children that is simple and robust enough to support transport, assembly, maintenance and operation in developing countries. This paper details the concept for an HHC ventilation and pressurization system that will provide controlled pressurization of the system, and provide adequate washout of carbon dioxide while the subject is enclosed in the confined space during the administration of the medical treatment. The concept took into consideration operational complexity, safety to the

  15. The Mark III vertex chamber

    SciTech Connect

    Adler, J.; Bolton, T.; Bunnell, K.; Cassell, R.; Cheu, E.; Freese, T.; Grab, C.; Mazaheri, G.; Mir, R.; Odian, A.

    1987-07-01

    The design and construction of the new Mark III vertex chamber is described. Initial tests with cosmic rays prove the ability of track reconstruction and yield triplet resolutions below 50 ..mu..m at 3 atm using argon/ethane (50:50). Also performed are studies using a prototype of a pressurized wire vertex chamber with 8 mm diameter straw geometry. Spatial resolution of 35mm was obtained using dimethyl ether (DME) at 1 atm and 30 ..mu..m using argon/ethane (50/50 mixture) at 4 atm. Preliminary studies indicate the DME to adversely affect such materials as aluminized Mylar and Delrin.

  16. CHAMBERS FERRY ROADLESS AREA, TEXAS.

    USGS Publications Warehouse

    Houser, B.B.; Ryan, George S.

    1984-01-01

    A geologic and geochemical investigation of the Chambers Ferry Roadless Area, Texas was conducted. The area has probable mineral-resource potential for oil and gas and for lignite. No metallic or additional energy resources were identified in the investigation. Detailed analyses of well logs from the vicinity of the Chambers Ferry Roadless Area, in conjunction with seismic data, are necessary to determine if the subsurface stratigraphy and structure are favorable for the accumulation of oil and gas. A shallow drilling program involving coring on a close-space grid is necessary for determination of the rank and continuity of seams of lignitic sediments in the area.

  17. Test chamber for alpha spectrometry

    DOEpatents

    Larsen, Robert P.

    1977-01-01

    Alpha emitters for low-level radiochemical analysis by measurement of alpha spectra are positioned precisely with respect to the location of a surface-barrier detector by means of a chamber having a removable threaded planchet holder. A pedestal on the planchet holder holds a specimen in fixed engagement close to the detector. Insertion of the planchet holder establishes an O-ring seal that permits the chamber to be pumped to a desired vacuum. The detector is protected against accidental contact and resulting damage.

  18. Double window viewing chamber assembly

    NASA Technical Reports Server (NTRS)

    Keller, V. W. (Inventor); Owen, R. B. (Inventor); Elkins, B. R. (Inventor); White, W. T. (Inventor)

    1986-01-01

    A viewing chamber which permits observation of a sample retained therein includes a pair of double window assemblies mounted in opposed openings in the walls thereof so that a light beam can directly enter and exit from the chamber. A flexible mounting arrangement for the outer windows of the window assemblies enables the windows to be brought into proper alignment. An electrical heating arrangement prevents fogging of the outer windows whereas desiccated air in the volume between the outer and inner windows prevents fogging of the latter.

  19. Laboratory Course on Drift Chambers

    NASA Astrophysics Data System (ADS)

    García-Ferreira, Ix-B.; García-Herrera, J.; Villaseñor, L.

    2006-09-01

    Drift chambers play an important role in particle physics experiments as tracking detectors. We started this laboratory course with a brief review of the theoretical background and then moved on to the the experimental setup which consisted of a single-sided, single-cell drift chamber. We also used a plastic scintillator paddle, standard P-10 gas mixture (90% Ar, 10% CH4) and a collimated 90Sr source. During the laboratory session the students performend measurements of the following quantities: a) drift velocities and their variations as function of the drift field; b) gas gains and c) diffusion of electrons as they drifted in the gas.

  20. Annular-Cross-Section CFE Chamber

    NASA Technical Reports Server (NTRS)

    Sharnez, Rizwan; Sammons, David W.

    1994-01-01

    Proposed continuous-flow-electrophoresis (CFE) chamber of annular cross section offers advantages over conventional CFE chamber, and wedge-cross-section chamber described in "Increasing Sensitivity in Continuous-Flow Electrophoresis" (MFS-26176). In comparison with wedge-shaped chamber, chamber of annular cross section virtually eliminates such wall effects as electro-osmosis and transverse gradients of velocity. Sensitivity enhanced by incorporating gradient maker and radial (collateral) flow.

  1. Nondestructive test of regenerative chambers

    NASA Technical Reports Server (NTRS)

    Malone, G. A.; Stauffis, R.; Wood, R.

    1972-01-01

    Flat panels simulating internally cooled regenerative thrust chamber walls were fabricated by electroforming, brazing and diffusion bonding to evaluate the feasibility of nondestructive evaluation techniques to detect bonds of various strength integrities. Ultrasonics, holography, and acoustic emission were investigated and found to yield useful and informative data regarding the presence of bond defects in these structures.

  2. Simulation of Layered Magma Chambers.

    ERIC Educational Resources Information Center

    Cawthorn, Richard Grant

    1991-01-01

    The principles of magma addition and liquid layering in magma chambers can be demonstrated by dissolving colored crystals. The concepts of density stratification and apparent lack of mixing of miscible liquids is convincingly illustrated with hydrous solutions at room temperature. The behavior of interstitial liquids in "cumulus" piles can be…

  3. Chamber Music for Every Instrumentalist.

    ERIC Educational Resources Information Center

    Latten, James E.

    2001-01-01

    Discusses why students who play musical instruments should participate in a chamber music ensemble. Provides rationale for using small ensembles in the high school band curriculum. Focuses on the topic of scheduling, illustrating how to insert small ensembles into the lesson schedule, and how to set up a new schedule. (CMK)

  4. Chamber Music for Better Bands.

    ERIC Educational Resources Information Center

    Brown, Michael R.

    1998-01-01

    Considers why students should participate in a chamber music ensemble: (1) students develop a sense of collegiality and self-worth; (2) ensembles encourage practice time; and (3) ensembles provide flexible performance opportunities. Highlights the different aspects of creating an ensemble from the availability of faculty to selecting challenging…

  5. Chamber Clearing First Principles Modeling

    SciTech Connect

    Loosmore, G

    2009-06-09

    LIFE fusion is designed to generate 37.5 MJ of energy per shot, at 13.3 Hz, for a total average fusion power of 500 MW. The energy from each shot is partitioned among neutrons ({approx}78%), x-rays ({approx}12%), and ions ({approx}10%). First wall heating is dominated by x-rays and debris because the neutron mean free path is much longer than the wall thickness. Ion implantation in the first wall also causes damage such as blistering if not prevented. To moderate the peak-pulse heating, the LIFE fusion chamber is filled with a gas (such as xenon) to reduce the peak-pulse heat load. The debris ions and majority of the x-rays stop in the gas, which re-radiates this energy over a longer timescale (allowing time for heat conduction to cool the first wall sufficiently to avoid damage). After a shot, because of the x-ray and ion deposition, the chamber fill gas is hot and turbulent and contains debris ions. The debris needs to be removed. The ions increase the gas density, may cluster or form aerosols, and can interfere with the propagation of the laser beams to the target for the next shot. Moreover, the tritium and high-Z hohlraum debris needs to be recovered for reuse. Additionally, the cryogenic target needs to survive transport through the gas mixture to the chamber center. Hence, it will be necessary to clear the chamber of the hot contaminated gas mixture and refill it with a cool, clean gas between shots. The refilling process may create density gradients that could interfere with beam propagation, so the fluid dynamics must be studied carefully. This paper describes an analytic modeling effort to study the clearing and refilling process for the LIFE fusion chamber. The models used here are derived from first principles and balances of mass and energy, with the intent of providing a first estimate of clearing rates, clearing times, fractional removal of ions, equilibrated chamber temperatures, and equilibrated ion concentrations for the chamber. These can be used

  6. Comparative study of deep levels in HVPE and MOCVD GaN by combining O-DLTS and pulsed photo-ionization spectroscopy

    NASA Astrophysics Data System (ADS)

    Pavlov, J.; Čeponis, T.; Gaubas, E.; Meskauskaite, D.; Reklaitis, I.; Vaitkus, J.; Grigonis, R.; Sirutkaitis, V.

    2015-12-01

    Operational characteristics of sensors made of GaN significantly depend on technologically introduced defects acting as rapid traps of excess carriers which reduce charge collection efficiency of detectors. In order to reveal the prevailing defects in HVPE and MOCVD grown GaN, the carrier lifetime and photo-ionization spectra have been simultaneously measured by using microwave probed photo-conductivity transient technique. Several traps ascribed to impurities as well as vacancy and anti-site type defects have been identified in HVPE GaN material samples by combining photo-ionization and electron spin resonance spectroscopy. The optical deep level transient spectroscopy technique has been applied for spectroscopy of the parameters of thermal emission from the traps ascribed to technological defects in the Schottky barrier terrace structures fabricated on MOCVD GaN.

  7. Hydrostatic Hyperbaric Chamber Ventilation System

    NASA Technical Reports Server (NTRS)

    Sarguisingh, Miriam J.

    2012-01-01

    The hydrostatic hyperbaric chamber (HHC) represents the merger of several technologies in development for NASA aerospace applications, harnessed to directly benefit global health. NASA has significant experience developing composite hyperbaric chambers for a variety of applications. NASA also has researched the application of water-filled vessels to increase tolerance of acceleration forces. The combination of these two applications has resulted in the hydrostatic chamber, which has been conceived as a safe, affordable means of making hyperbaric oxygen therapy (HBOT) available in the developing world for the treatment of a variety of medical conditions. Specifically, HBOT is highly-desired as a possibly curative treatment for Buruli Ulcer, an infectious condition that afflicts children in sub-Saharan Africa. HBOT is simply too expensive and too dangerous to implement in the developing world using standard equipment. The HHC technology changes the paradigm. The HHC differs from standard hyperbaric chambers in that the majority of its volume is filled with water which is pressurized by oxygen being supplied in the portion of the chamber containing the patient s head. This greatly reduces the amount of oxygen required to sustain a hyperbaric atmosphere, thereby making the system more safe and economical to operate. An effort was taken to develop an HHC system to apply HBOT to children that is simple and robust enough to support transport, assembly, maintenance and operation in developing countries. This paper details the concept for an HHC ventilation and pressurization system to provide controlled pressurization and adequate washout of carbon dioxide while the subject is enclosed in the confined space during the administration of the medical treatment. The concept took into consideration operational complexity, safety to the patient and operating personnel, and physiological considerations. The simple schematic, comprised of easily acquired commercial hardware

  8. Anomalous current-voltage characteristics along the c-axis in YBaCuO thin films prepared by MOCVD and AFM lithography

    NASA Astrophysics Data System (ADS)

    Yamamoto, Shuu'ichirou; Kawaguchi, Atsushi; Oda, Shunri

    1997-12-01

    We have proposed a fabrication process of intrinsic Josephson junctions (IJJs) using AFM lithography and successfully obtained IJJs in YBaCuO thin films deposited by MOCVD. A sample shows clear hysteresis and 23 voltage steps related to IJJs in the I- V curve. The maximum width of a step is about 2 mV at 5 K. We discuss the I- V characteristics and estimate the order of the parameters for the IJJ.

  9. Multi-wafer growth of GaInAs photodetectors on 4" InP by MOCVD for SWIR imaging applications

    NASA Astrophysics Data System (ADS)

    Furlong, Mark J.; Mattingley, Mark; Lim, Sung Wook; Geen, Matthew; Jones, Wynne

    2013-12-01

    Photodiodes based on the GaInAs/InP material system responding in the 1.3-1.7 μm wavelength range are of interest in a wide range of applications, from optical power and channel monitors in telecommunication systems through to advanced night vision imaging using large format focal plane type detectors for defense and security applications. Here we report on our results of GaInAs PIN photo detector structures grown on 2", 3" and 4" InP substrates by low pressure Metalorganic Chemical Vapor Deposition (MOCVD) in both standard and new larger volume format reactor configurations. High quality, lattice matched InP/GaInAs epitaxial layers were grown and we demonstrate that when moving to larger platen configurations, high degree of thickness uniformity (<3%, FTIR), lattice mismatch (<0.1%, XRD) and compositional uniformity (<2 nm, PL) can be maintained. The surface quality of epitaxial wafers will be assessed by various surface analytical techniques. We also make comparisons with the performance of 2", 3" and 4" photodetector structures grown, this demonstrating that MOCVD production processes have been successfully scaled. We conclude by discussing the material requirements for large area infrared focal plane array photodetectors and describe how MOCVD growth technology will address industry's requirements for increasing device sizes with improved performance.

  10. Multi-wafer growth of GaInAs photodetectors on 4" InP by MOCVD for SWIR imaging applications

    NASA Astrophysics Data System (ADS)

    Furlong, Mark J.; Mattingley, Mark; Lim, Sung Wook; Geen, Matthew; Jones, Wynne

    2014-06-01

    Photodiodes based on the GaInAs/InP material system responding in the 1.3-1.7 μm wavelength range are of interest in a wide range of applications, from optical power and channel monitors in telecommunication systems through to advanced night vision imaging using large format focal plane type detectors for defense and security applications. Here we report on our results of GaInAs PIN photo detector structures grown on 2", 3" and 4" InP substrates by low pressure Metalorganic Chemical Vapor Deposition (MOCVD) in both standard and new larger volume format reactor configurations. High quality, lattice matched InP/GaInAs epitaxial layers were grown and we demonstrate that when moving to larger platen configurations, high degree of thickness uniformity (<3%, FTIR), lattice mismatch (<0.1%, XRD) and compositional uniformity (<2 nm, PL) can be maintained. The surface quality of epitaxial wafers will be assessed by various surface analytical techniques. We also make comparisons with the performance of 2", 3" and 4" photodetector structures grown, this demonstrating that MOCVD production processes have been successfully scaled. We conclude by discussing the material requirements for large area infrared focal plane array photodetectors and describe how MOCVD growth technology will address industry's requirements for increasing device sizes with improved performance.

  11. Growth mechanism of GaAs1-xSbx ternary alloy thin film on MOCVD reactor using TMGa, TDMAAs and TDMASb

    NASA Astrophysics Data System (ADS)

    Suhandi, A.; Tayubi, Y. R.; Arifin, P.

    2016-04-01

    Metal Organic Chemical Vapor Deposition (MOCVD) is a method for growing a solid material (in the form of thin films, especially for semiconductor materials) using vapor phase metal organic sources. Studies on the growth mechanism of GaAs1-xSbx ternary alloy thin solid film in the range of miscibility-gap using metal organic sources trimethylgallium (TMGa), trisdimethylaminoarsenic (TDMAAs), and trisdimethylaminoantimony (TDMASb) on MOCVD reactor has been done to understand the physical and chemical processes involved. Knowledge of the processes that occur during alloy formation is very important to determine the couple of growth condition and growth parameters are appropriate for yield high quality GaAs1-xSbx alloy. The mechanism has been studied include decomposition of metal organic sources and chemical reactions that may occur, the incorporation of the alloy elements forming and the contaminants element that are formed in the gown thin film. In this paper presented the results of experimental data on the growth of GaAs1-xSbx alloy using Vertical-MOCVD reactor to demonstrate its potential in growing GaAs1-xSbx alloy in the range of its miscibility gap.

  12. Chamber dynamic research with pulsed power

    SciTech Connect

    PETERSON,ROBERT R.; OLSON,CRAIG L.; RENK,TIMOTHY J.; ROCHAU,GARY E.; SWEENEY,MARY ANN

    2000-05-15

    In Inertial Fusion Energy (IFE), Target Chamber Dynamics (TCD) is an integral part of the target chamber design and performance. TCD includes target output deposition of target x-rays, ions and neutrons in target chamber gases and structures, vaporization and melting of target chamber materials, radiation-hydrodynamics in target chamber vapors and gases, and chamber conditions at the time of target and beam injections. Pulsed power provides a unique environment for IFE-TCD validation experiments in two important ways: they do not require the very clean conditions which lasers need and they currently provide large x-ray and ion energies.

  13. Rocket Engine Thrust Chamber Assembly

    NASA Technical Reports Server (NTRS)

    Cornelius, Charles S. (Inventor); Counts, Richard H. (Inventor); Myers, W. Neill (Inventor); Lackey, Jeffrey D. (Inventor); Peters, Warren (Inventor); Shadoan, Michael D. (Inventor); Sparks, David L. (Inventor); Lawrence, Timothy W. (Inventor)

    2001-01-01

    A thrust chamber assembly for liquid fueled rocket engines and the method of making it wherein a two-piece mandrel wrapped with a silica tape saturated with a phenolic resin, the tape extending along the mandrel and covering the combustion chamber portion of the mandrel to the throat portion. The phenolic in the tape is cured and the end of the wrap is machined. The remainder of the mandrel is wrapped with a third silica tape. The resin in the third tape is cured and the assembly is machined. The entire assembly is then wrapped with a tow of graphite fibers wetted with an epoxy resin and, after the epoxy resin is cured, the graphite is machined to final dimensions.

  14. MPS II drift chamber system

    SciTech Connect

    Platner, E.D.

    1982-01-01

    The MPS II detectors are narrow drift space chambers designed for high position resolution in a magnetic field and in a very high particle flux environment. Central to this implementation was the development of 3 multi-channel custom IC's and one multi-channel hybrid. The system is deadtimeless and requires no corrections on an anode-to-anode basis. Operational experience and relevance to ISABELLE detectors is discussed.

  15. Space Chambers for Crop Treatment

    NASA Technical Reports Server (NTRS)

    1985-01-01

    Vacuum chambers, operated by McDonnell Douglas Corporation to test spacecraft, can also be used to dry water-soaked records. The drying temperature is low enough to allow paper to dry without curling or charging. Agricultural crops may also be dried using a spinoff system called MIVAC, which has proven effective in drying rice, wheat, soybeans, corn, etc. The system is energy efficient and can incorporate a sanitation process for destroying insects without contamination.

  16. Rocket Engine Thrust Chamber Assembly

    NASA Technical Reports Server (NTRS)

    Cornelius, Charles S. (Inventor); Counts, Richard H. (Inventor); Myers, W. Neill (Inventor); Lackey, Jeffrey D. (Inventor); Peters, Warren (Inventor); Shadoan, Michael (Inventor); Sparks, David L. (Inventor); Lawrence, Timothy W. (Inventor)

    2001-01-01

    A thrust chamber assembly for liquid fueled rocket engines and the method of making it wherein a two-piece mandrel having the configuration of an assembly having a combustion chamber portion connected to a nozzle portion through a throat portion is wrapped with a silica tape saturated with a phenolic resin, the tape extending along the mandrel and covering the combustion chamber portion of the mandrel to the throat portion. The width of the tape is positioned at an angle of 30 to 50 deg. to the axis of the mandrel such that one edge of the tape contacts the mandrel while the other edge is spaced from the mandrel. The phenolic in the tape is cured and the end of the wrap is machined to provide a frusto-conical surface extending at an angle of 15 to 30 deg. with respect to the axis of the mandrel for starting a second wrap on the mandrel to cover the throat portion. The remainder of the mandrel is wrapped with a third silica tape having its width positioned at a angle of 5 to 20 deg. from the axis of the mandrel. The resin in the third tape is cured and the assembly is machined to provide a smooth outer surface. The entire assembly is then wrapped with a tow of graphite fibers wetted with an epoxy resin and, after the epoxy resin is cured, the graphite is machined to final dimensions.

  17. The crop growth research chamber

    NASA Technical Reports Server (NTRS)

    Wagenbach, Kimberly

    1993-01-01

    The Crop Growth Research Chamber (CGRC) has been defined by CELSS principle investigators and science advisory panels as a necessary ground-based tool in the development of a regenerative life support system. The focus of CGRC research will be on the biomass production component of the CELSS system. The ground-based Crop Growth Research Chamber is for the study of plant growth and development under stringently controlled environments isolated from the external environment. The chamber has importance in three areas of CELSS activities: (1) crop research; (2) system control and integration, and (3) flight hardware design and experimentation. The laboratory size of the CGRC will be small enough to allow duplication of the unit, the conducting of controlled experiments, and replication of experiments, but large enough to provide information representative of larger plant communities. Experiments will focus on plant growth in a wide variety of environments and the effects of those environments on plant production of food, water, oxygen, toxins, and microbes. To study these effects in a closed system, tight control of the environment is necessary.

  18. 21 CFR 868.5470 - Hyperbaric chamber.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... than atmospheric pressure. This device does not include topical oxygen chambers for extremities (§ 878... hyperbaric chamber is a device that is intended to increase the environmental oxygen pressure to promote...

  19. 21 CFR 868.5470 - Hyperbaric chamber.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... than atmospheric pressure. This device does not include topical oxygen chambers for extremities (§ 878... hyperbaric chamber is a device that is intended to increase the environmental oxygen pressure to promote...

  20. 21 CFR 868.5470 - Hyperbaric chamber.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... than atmospheric pressure. This device does not include topical oxygen chambers for extremities (§ 878... hyperbaric chamber is a device that is intended to increase the environmental oxygen pressure to promote...

  1. 21 CFR 868.5470 - Hyperbaric chamber.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... than atmospheric pressure. This device does not include topical oxygen chambers for extremities (§ 878... hyperbaric chamber is a device that is intended to increase the environmental oxygen pressure to promote...

  2. SMOG CHAMBER VALIDATION USING LAGRANGIAN ATMOSPHERIC DATA

    EPA Science Inventory

    A method was developed for validating outdoor smog chamber experiments as a means of determining the relationships between oxidant concentrations and its precursors - hydrocarbons and nitrogen oxides. When chamber experiments were performed in a manner that simulated relevant met...

  3. Gas turbine combustion chamber with air scoops

    SciTech Connect

    Mumford, S.E.; Smed, J.P.

    1989-12-19

    This patent describes a gas turbine combustion chamber. It comprises: means for admission of fuel to the upstream end thereof and discharge of hot gases from the downstream end thereof, and a combustion chamber wall, having an outer surface, with apertures therethrough, and air scoops provided through the apertures to direct air into the combustion chamber.

  4. Making a Fish Tank Cloud Chamber

    ERIC Educational Resources Information Center

    Green, Frances

    2012-01-01

    The cloud chambers described here are large, made from readily available parts, simple to set up and always work. With no source in the chamber, background radiation can be observed. A large chamber means that a long rod containing a weakly radioactive material can be introduced, increasing the chance of seeing decays. Details of equipment and…

  5. A Sensitive Cloud Chamber without Radioactive Sources

    ERIC Educational Resources Information Center

    Zeze, Syoji; Itoh, Akio; Oyama, Ayu; Takahashi, Haruka

    2012-01-01

    We present a sensitive diffusion cloud chamber which does not require any radioactive sources. A major difference from commonly used chambers is the use of a heat sink as its bottom plate. The result of a performance test of the chamber is given. (Contains 8 figures.)

  6. Simple Cloud Chambers Using Gel Ice Packs

    ERIC Educational Resources Information Center

    Kamata, Masahiro; Kubota, Miki

    2012-01-01

    Although cloud chambers are highly regarded as teaching aids for radiation education, school teachers have difficulty in using cloud chambers because they have to prepare dry ice or liquid nitrogen before the experiment. We developed a very simple and inexpensive cloud chamber that uses the contents of gel ice packs which can substitute for dry…

  7. Uniform-Temperature Walls for Cloud Chambers

    NASA Technical Reports Server (NTRS)

    Fleischman, G.

    1985-01-01

    Flat heat pipes rapidly transfer heat to and from experimental volumes. Heat pipe vapor chamber carries heat to and from thermo electric modules. Critical surface acts as evaporator or condenser in cloud physics experiments. Used as walls of spaceborne atmospheric cloud chambers. On Earth, used as isothermal floors for environmental test chambers.

  8. EPA GAS PHASE CHEMISTRY CHAMBER STUDIES

    EPA Science Inventory

    Gas-phase smog chamber experiments are being performed at EPA in order to evaluate a number of current chemical mechanisms for inclusion in EPA regulatory and research models. The smog chambers are 9000 L in volume and constructed of 2-mil teflon film. One of the chambers is co...

  9. Vacuum chamber for an undulator straight section

    SciTech Connect

    Kim, S.; Wehrle, R.; Genens, L.

    1987-01-01

    A prototype aluminum extruded vacuum chamber for an undulator straight section of the Advanced Photon Source is described. The 52.-m long vacuum system is designed so that the undulator gap variation does not interfere with it. The chamber is gripped in a stiff close toleranced mounting structure to insure dimensional tolerance of the chamber height.

  10. Making a fish tank cloud chamber

    NASA Astrophysics Data System (ADS)

    Green, Frances

    2012-05-01

    The cloud chambers described here are large, made from readily available parts, simple to set up and always work. With no source in the chamber, background radiation can be observed. A large chamber means that a long rod containing a weakly radioactive material can be introduced, increasing the chance of seeing decays. Details of equipment and construction are given.

  11. Fluidized wall for protecting fusion chamber walls

    SciTech Connect

    Maniscalco, J.A.; Meier, W.R.

    1982-08-17

    Apparatus for protecting the inner wall of a fusion chamber from microexplosion debris, x-rays, neutrons, etc. Produced by deuterium-tritium (DT) targets imploded within the fusion chamber. The apparatus utilizes a fluidized wall similar to a waterfall comprising liquid lithium or solid pellets of lithiumceramic, the waterfall forming a blanket to prevent damage of the structural materials of the chamber.

  12. TSNIIMASH's U-22 gasdynamic vacuum chamber

    NASA Astrophysics Data System (ADS)

    Anfimov, N. A.; Prochukhaev, M. V.

    1993-06-01

    The description of operating principles of the TSNIIMASH's U-22 large-scale gasdynamic vacuum chamber is presented. The chamber's key systems and their performances are described. Examples of using the gasdynamic vacuum chamber for conducting experimental research and ground testing of rockets, launch vehicles and spacecraft are given.

  13. Chamber B Thermal/Vacuum Chamber: User Test Planning Guide

    NASA Technical Reports Server (NTRS)

    Montz, Mike E.

    2012-01-01

    Test process, milestones and inputs are unknowns to first-time users of Chamber B. The User Test Planning Guide aids in establishing expectations for both NASA and non-NASA facility customers. The potential audience for this guide includes both internal and commercial spaceflight hardware/software developers. It is intended to assist their test engineering personnel in test planning and execution. Material covered includes a roadmap of the test process, roles and responsibilities of facility and user, major milestones, facility capabilities, and inputs required by the facility. Samples of deliverables, test article interfaces, and inputs necessary to define test scope, cost, and schedule are included as an appendix to the guide.

  14. Investigation on structural, optical and electrical properties of Cp2Mg flow varied p-GaN grown by MOCVD

    NASA Astrophysics Data System (ADS)

    Surender, S.; Pradeep, S.; Ramesh, R.; Baskar, K.

    2016-05-01

    In this work the effect of different concentration of Magnesium doped GaN (p-GaN) were systematically studied. The p-GaN epilayers were grown on c-plane sapphire substrate by horizontal flow Metal Organic Chemical Vapor Deposition (MOCVD) with various flow rates of 100 sccm to 300 sccm using bis-(cyclopentadienyl) - magnesium (Cp2Mg) precursor. The samples were subjected to structural, optical, morphological and electrical studies using High Resolution X-ray diffraction (HRXRD), room temperature photoluminescence (PL), Atomic Force Microscopy (AFM) and Hall measurement respectively. Results indicated that the Mg doped GaN of 200 sccm Cp2Mg has the root mean square (rms) roughness of about 0.3 nm for a scan area of 5×5 µm2 which has good two dimensional growth. Moreover, Hall measurements results shows that (200 sccm Cp2Mg) Mg-doped GaN possess the highest hole concentration of 5.4×1017cm-3 and resistivity of 1.7 Ωcm at room temperature.

  15. Effect of Ge on SiC film morphology in SiC/Si films grown by MOCVD

    SciTech Connect

    Sarney, W.L.; Salamanca-Riba, L.; Zhou, P.; Spencer, M.G.; Taylor, C.; Sharma, R.P.; Jones, K.A.

    1999-07-01

    SiC/Si films generally contain stacking faults and amorphous regions near the interface. High quality SiC/Si films are especially difficult to obtain since the temperatures usually required to grow high quality SiC are above the Si melting point. The authors added Ge in the form of GeH{sub 2} to the reactant gases to promote two-dimensional CVD growth of SiC films on (111) Si substrates at 1,000 C. The films grown with no Ge are essentially amorphous with very small crystalline regions, whereas those films grown with GeH{sub 2} flow rates of 10 and 15 sccm are polycrystalline with the 3C structure. Increasing the flow rate to 20 sccm improves the crystallinity and induces growth of 6H SiC over an initial 3C layer. This study presents the first observation of spontaneous polytype transformation in SiC grown on Si by MOCVD.

  16. Broad Temperature Pinning Study of 15 mol.% Zr-Added (Gd, Y)-Ba-Cu-O MOCVD Coated Conductors

    SciTech Connect

    Xu, AX; Khatri, N; Liu, YH; Majkic, G; Galstyan, E; Selvamanickam, V; Chen, YM; Lei, CH; Abraimov, D; Hu, XB; Jaroszynski, J; Larbalestier, D

    2015-06-01

    BaZrO3 (BZO) nanocolumns have long been shown to be very effective for raising the pinning force F-p of REBa2Cu3Ox (REBCO, where RE = rare earth) films at high temperatures and recently at low temperatures too. We have successfully incorporated a high density of BZO nanorods into metal organic chemical vapor deposited (MOCVD) REBCO coated conductors via Zr addition. We found that, compared to the 7.5% Zr-added coated conductor, dense BZO nanorod arrays in the 15% Zr-added conductor are effective over the whole temperature range from 77 K down to 4.2 K. We attribute the substantially enhanced J(c) at 30 K to the weak uncorrelated pinning as well as the strong correlated pinning. Meanwhile, by tripling the REBCO layer thickness to similar to 2.8 mu m, the engineering critical current density J(e) at 30 K exceeds J(e) of optimized Nb-Ti wires at 4.2 K.

  17. MOCVD of high quality YBa 2Cu 3O 7-δ thin films using a fluorinated barium precursor

    NASA Astrophysics Data System (ADS)

    Richards, B. C.; Cook, S. L.; Pinch, D. L.; Andrews, G. W.; Lengeling, G.; Schulte, B.; Jürgensen, H.; Shen, Y. Q.; Vase, P.; Freltoft, T.; Spee, C. I. M. A.; Linden, J. L.; Hitchman, M. L.; Shamlian, S. H.; Brown, A.

    1995-02-01

    MOCVD of superconducting YBa 2Cu 3O 7δ thin films using the novel fluorinated barium β-diketonate complex [Ba(TDFND) 2·tetraglyme] 1 in combination with [Y(TMHD) 3] 2 and [Cu(TMHD) 2] is reported. The Ba complex has a low melting point (72°C), is thermally stable to 200°C and allows reproducible and reliable film deposition even when maintained at 145°C for several weeks. Conversion of the fluoride to the oxide is achieved by in situ hydrolysis. Films deposited on SrTiO 3 (100) were characterised by scanning electron microscopy, energy dispersive X-ray spectroscopy, X-ray diffraction, rocking curve, ac susceptibility and secondary ion mass spectrometry. Homogeneous layers of YBa 2Cu 3O 7-δ, ≈ 0.25 μm thick, were grown at ≈ 0.13 μm h -1. The films are epitaxial with good c axis orientation. Critical temperatures Tc are typically 91 K and critical current densities c (at 77 K) of ≈ 5 MA cm -2 are reported. SIMS results showing levels of residual fluorine do not exceed 250 ppm.

  18. GaAs nanowires and GaAs/AlGaAs core/shell nanowires synthesized by MOCVD

    NASA Astrophysics Data System (ADS)

    Peters, Brian; Minutillo, Nicholas; Carlin, John; Yang, Fengyuan

    2011-03-01

    Nanowires made by the ``bottom-up'' approach can be used in a variety of electrical and optoelectronic devices as well as in the study of low dimensional transport physics. We have grown GaAs nanowires using Au catalysts in a closed couple showerhead MOCVD system. A number of growth parameters, including the substrate temperature, growth rate, and Arsine/TMGa ratio, are explored to identify optimal conditions for growth of GaAs nanowires with large aspect ratio and minimal tapering. Higher substrate temperatures result in larger tapering and lower temperature leads to ``kinks.'' Meanwhile, large V/III source ratio gives large tapering as well. We have found that our optimal conditions are at a substrate temperature of 420°C and V/III ratio of ~ 25 , which gives a tapering of less than 1 nm increase in diameter per micron in length. In addition, GaAs/AlGaAs core/shell structured nanowires were also grown to minimize the surface states. Characterizations by SEM and photoluminescence will be presented. This work is supported by Department of Energy (DE-SC0001304).

  19. Growth parameters effect on the electric and thermoelectric characteristics of Bi 2Se 3 thin films grown by MOCVD system

    NASA Astrophysics Data System (ADS)

    Al Bayaz, A.; Giani, A.; Artaud, M. C.; Foucaran, A.; Pascal-Delannoy, F.; Boyer, A.

    2002-06-01

    Bi 2Se 3 thin films were grown by metal organic chemical vapour deposition (MOCVD) on pyrex substrate in an horizontal reactor using Trimethylbismuth (TMBi) and Diethylselinium (DESe) as metal-organic sources. The effect of the growth parameters such as substrate temperature, Tg, and TMBi partial pressure, PTMBi, on the structural, electrical and thermoelectrical properties of Bi 2Se 3 films, has been investigated. We noticed that a high growth temperature is very important for a good orientation of crystallites, which can be directly related to the best values of Hall mobility and Seebeck coefficient found. Therefore, a large stability of the reactions over the substrates with following growth conditions: 455°C⩽ Tg⩽485°C,0.5×10 -4⩽ PTMBi⩽1×10 -4 atm and a total hydrogen flow rate DT=3 slm, is achieved. In these optimal growth conditions, we found a better crystalline structure of Bi 2Se 3 thin films using X-ray diffraction. Thus, these layers always displayed n-type conduction using Hall effect, with carrier concentration close to 2×10 19 cm -3 and maximum values of Hall mobility and Seebeck coefficient of μ=247 cm 2/V s and | α|=120 μV/K respectively. Then, these films appear to be very promising for thermoelectric applications.

  20. Advanced light-scattering materials: Double-textured ZnO:B films grown by LP-MOCVD

    NASA Astrophysics Data System (ADS)

    Addonizio, M. L.; Spadoni, A.; Antonaia, A.

    2013-12-01

    Double-textured ZnO:B layers with enhanced optical scattering in both short and long wavelength regions have been successfully fabricated using MOCVD technique through a three step process. Growth of double-textured structures has been induced by wet etching on polycrystalline ZnO surface. Our double-layer structure consists of a first ZnO:B layer wet etched and subsequently used as substrate for a second ZnO:B layer deposition. Polycrystalline ZnO:B layers were etched by utilizing diluted solutions of fluoridic acid (HF), chloridric acid (HCl) and phosphoric acid (H3PO4) and their effect on surface morphology modification was systematically investigated. The morphology of the second deposited ZnO layer strongly depended on the surface properties of the etched ZnO first layer. Growth of cauliflower-like texture was induced by protrusions presence on the HCl etched surface. Optimized double-layer structure shows a cauliflower-like double texture with higher RMS roughness and increased spectral haze values in both short and long wavelength regions, compared to conventional pyramidal-like single texture. Furthermore, this highly scattering structure preserves excellent optical and electrical properties.

  1. Au-catalyzed synthesis and characterisation of phase change Ge-doped Sb-Te nanowires by MOCVD

    NASA Astrophysics Data System (ADS)

    Longo, M.; Stoycheva, T.; Fallica, R.; Wiemer, C.; Lazzarini, L.; Rotunno, E.

    2013-05-01

    The interest in the Ge doped Sb-Te chalcogenide alloy is mainly related to phase change memory applications. In view of phase change device scaling and reduction of programming energy, Sb-Te nanowires (NWs) become an attractive option. In this work, in order to investigate their potential transferability to industrial implementation, the self-assembly of Sb2Te3 NWs and Ge-Sb-Te NWs with Ge content in the range of 1-13% (Ge doping) was studied by coupling the advantages of MOCVD and the Vapour-Liquid-Solid (VLS) mechanism. The results show the structural and compositional gradual changes occurring from pure Sb2Te3 NWs to the previously reported, stoichiometric Ge1Sb2Te4 NWs [[12] M. Longo et al., Nano Lett., 12 (2012) 1509]. The typical diameter of the obtained NWs resulted to be 50 nm, with lengths up to 3 μm. The typology of Au catalyst nanoislands influenced both the NW morphology and the Ge incorporation during the VLS self-assembly; the Ge metalorganic precursor partial pressure affected the NW morphology and their structure. Finally, TEM observations revealed that defect-free, monocrystalline Sb2Te3 and Ge-doped Sb-Te phase change NWs could be obtained.

  2. Effects of oxygen pressure in preparation of insulating Sr 2AlTaO 6 thin films by MOCVD

    NASA Astrophysics Data System (ADS)

    Takahashi, Yoshihiro; Nakajima, Yuuichi; Morishita, Tadataka; Tanabe, Keiichi

    2002-10-01

    Approximately 300-nm-thick insulating Sr 2AlTaO 6 (SAT) films were prepared on 10-μm-thick YBa 2Cu 3O 7- δ (YBCO) films by metalorganic chemical vapor deposition (MOCVD) in the range of oxygen partial pressure from 13 Pa (0.1 Torr) to 667 Pa (5 Torr) for total deposition pressure of 13 hPa (10 Torr). Stoichiometric SAT films with good crystallinity and square-like grains originating from the cubic structure of SAT were obtained for all the oxygen partial pressure conditions. However, extraordinary areas were partially observed on the sample prepared in the low oxygen partial pressure below 67 Pa (0.5 Torr), which are supposed to be caused by unstableness of YBCO surface. Under the highest oxygen partial pressure condition of 667 Pa, the lower tetragonal YBCO film exhibited a Tc of 80 K, indicating a possibility of in situ oxygenation during cooling. It was also confirmed that the SAT film fabricated under this condition has good dielectric properties such as the dielectric constant of approximately 24 and the conductance below 10 -8 S.

  3. Oxygen ion irradiation on AlGaN/GaN heterostructure grown on silicon substrate by MOCVD method

    SciTech Connect

    Ramesh, R.; Arivazhagan, P.; Balaji, M.; Baskar, K.; Asokan, K.

    2015-06-24

    In the present work, we have reported 100 MeV O{sup 7+} ion irradiation with 1×10{sup 12} and 5×10{sup 12} ions/cm{sup 2} fluence on AlGaN/GaN heterostructures grown on silicon substrate by Metal Organic Chemical Vapour Deposition (MOCVD). The Irradiated samples were characterized by High Resolution X-Ray Diffraction (HRXRD), Atomic Force Microscope (AFM) and Photoluminescence (PL). Crystalline quality has been analysed before and after irradiation using HRXRD. Different kinds of morphology are attributed to specific type of dislocations using the existing models available in the literature. A sharp band-edge emission in the as grown samples was observed at ∼3.4 eV in GaN and 3.82 for AlGaN. The band-edge absorption intensity reduced due to irradiation and these results have been discussed in view of the damage created by the incident ions. In general the effect of irradiation induced-damages were analysed as a function of material properties. A possible mechanism responsible for the observations has been discussed.

  4. Normally-off metamorphic AlInAs/AlInAs HEMTs on Si substrates grown by MOCVD

    NASA Astrophysics Data System (ADS)

    Huang, Jie; Li, Ming; Lau, Kei-May

    2015-07-01

    A combination of self-aligned fluoride-based plasma treatment and post-gate rapid thermal annealing was developed to fabricate a novel 120-nm T-shaped gate normally-off metamorphic Al0.49In0.51As/Ga0.47In0.53As HEMT device on a Si substrate grown by metal-organic chemical vapor deposition (MOCVD). A shift of the threshold voltage, from -0.42 V to 0.11 V was obtained and the shift can be effectively adjusted by the process parameter of CF4 plasma treatment. Furthermore, a side benefit of reducing the leakage current of the device up to two orders of magnitude was also observed. E-mode transistors with 120 nm gate length own fT up to 160 GHz and fmax of 140 GHz. These characteristics imply the potential of the fluoride-based plasma treatment technology for the fabrication of monolithic enhancement/depletion-mode mHEMTs, which also encourage the massive production with this low-cost technology. Project supported by the Young Scientists Fund of the National Natural Science Foundation, China (Grant No. 61401373), the Fundamental Research Funds for Central University, China (Grant No. XDJK2013B004 and 2362014XK13), and the Research Fund for the Doctoral Program of Southwest University, China (Grant No. SWU111030).

  5. Liquid argon Time Projection Chamber

    SciTech Connect

    Doe, P.J.; Mahler, H.J.; Chen, H.H.

    1984-01-01

    The principal features of the liquid argon TPC are outlined and the status of development efforts, particularly at UCI, are discussed. Technical problems associated with liquid TPC's are: the liquid must be maintained at a high level of purity to enable long distance drifting of ionization electrons, and the signal size is small due to the absence of practical charge multiplication as found in gas chambers. These problems have been largely resolved in studies using small (1 to 100 l) detectors, thus allowing a realistic consideration of the physics potential of such devices.

  6. The DELPHI time projection chamber

    SciTech Connect

    Brand, C.; Cairanti, G.; Charpentier, P.; Clara, M.P.; Delikaris, D.; Foeth, H.; Heck, B.W.; Hilke, H.J.; Sulkowski, K.; Aubret, C.

    1989-02-01

    The central tracking device of the DELPHI Experiment at LEP is a Time Projection Chamber (TPC) with an active volume of 2 x 1.34m in length and 2.22m in diameter. Since spring 1988 the TPC has undergone extensive tests in a cosmic ray set-up. It will be installed in the LEP tunnel by early 1989. This report covers the construction, the read-out electronics and the contribution of the TPC to the DELPHI trigger. Emphasis is given to novelties which are not used in similar detectors.

  7. TRU waste characterization chamber gloveboxes.

    SciTech Connect

    Duncan, D. S.

    1998-07-02

    Argonne National Laboratory-West (ANL-W) is participating in the Department of Energy's (DOE) National Transuranic Waste Program in support of the Waste Isolation Pilot Plant (WIPP). The Laboratory's support currently consists of intrusive characterization of a selected population of drums containing transuranic waste. This characterization is performed in a complex of alpha containment gloveboxes termed the Waste Characterization Gloveboxes. Made up of the Waste Characterization Chamber, Sample Preparation Glovebox, and the Equipment Repair Glovebox, they were designed as a small production characterization facility for support of the Idaho National Engineering and Environmental Laboratory (INEEL). This paper presents salient features of these gloveboxes.

  8. Portable Ethylene Oxide Sterilization Chamber

    PubMed Central

    Songer, J. R.; Mathis, R. G.

    1969-01-01

    A portable ethylene oxide sterilization chamber was designed, constructed, and tested for use in the sterilization of embolectomy catheters. The unit can accommodate catheters up to 40 inches (101.6 cm) in length and can be operated for less than 4 cents per cycle. A constant concentration of 500 mg of ethylene oxide per liter of space and holding periods of 4 and 6 hr at 43 and 22 C, respectively, were adequate when tested with B. subtilis spores. The estimated cost of construction was $165.00. If temperature control is unnecessary, the cost is approximately $80.00. Images PMID:4977644

  9. Studies with the Arapahoe smoke chamber

    NASA Technical Reports Server (NTRS)

    Hilado, C. J.; Cumming, H. J.

    1977-01-01

    Samples of polymethyl methacrylate, polyvinyl chloride, polyester, and polystyrene were evaluated using the Arapahoe smoke chamber. These same materials had been previously evaluated using the National Bureau of Standards (NBS) smoke chamber. The percent smoke based on initial weight as determined using the Arapahoe smoke chamber appeared to correlate with the maximum specific optical density under flaming conditions as determined using the NBS smoke chamber. In addition, the percent smoke based on weight loss as determined using the Arapahoe smoke chamber appeared to correlate with the maximum specific optical density under nonflaming conditions as determined using the NBS smoke chamber. The Arapahoe smoke chamber also offers the advantage of high sample throughput and the possibility of related studies of smoke particulates.

  10. Thrust chamber material technology program

    NASA Technical Reports Server (NTRS)

    Andrus, J. S.; Bordeau, R. G.

    1989-01-01

    This report covers work performed at Pratt & Whitney on development of copper-based materials for long-life, reusable, regeneratively cooled rocket engine thrust chambers. The program approached the goal of enhanced cyclic life through the application of rapid solidification to alloy development, to introduce fine dispersions to strengthen and stabilize the alloys at elevated temperatures. After screening of alloy systems, copper-based alloys containing Cr, Co, Hf, Ag, Ti, and Zr were processed by rapid-solidification atomization in bulk quantities. Those bulk alloys showing the most promise were characterized by tensile testing, thermal conductivity testing, and elevated-temperature, low-cycle fatigue (LFC) testing. Characterization indicated that Cu- 1.1 percent Hf exhibited the greatest potential as an improved-life thrust chamber material, exhibiting LCF life about four times that of NASA-Z. Other alloys (Cu- 0.6 percent Zr, and Cu- 0.6 percent Zr- 1.0 percent Cr) exhibited promise for use in this application, but needed more development work to balance properties.

  11. Tubular copper thrust chamber design study

    NASA Technical Reports Server (NTRS)

    Masters, A. I.; Galler, D. E.

    1992-01-01

    The use of copper tubular thrust chambers is particularly important in high performance expander cycle space engines. Tubular chambers have more surface area than flat wall chambers, and this extra surface area provides enhanced heat transfer for additional energy to power the cycle. This paper was divided into two sections: (1) a thermal analysis and sensitivity study; and (2) a preliminary design of a selected thrust chamber configuration. The thermal analysis consisted of a statistical optimization to determine the optimum tube geometry, tube booking, thrust chamber geometry, and cooling routing to achieve the maximum upper limit chamber pressure for a 25,000 pound thrust engine. The preliminary design effort produced a layout drawing of a tubular thrust chamber that is three inches shorter than the Advanced Expander Test Bed (AETB) milled channel chamber but is predicted to provide a five percent increase in heat transfer. Testing this chamber in the AETB would confirm the inherent advantages of tubular chamber construction and heat transfer.

  12. Rocket thrust chamber thermal barrier coatings

    NASA Technical Reports Server (NTRS)

    Quentmeyer, R. J.

    1985-01-01

    Subscale rocket thrust chamber tests were conducted to evaluate the effectiveness and durability of thin yttria stabilized zirconium oxide coatings applied to the thrust chamber hot-gas side wall. The fabrication consisted of arc plasma spraying the ceramic coating and bond coat onto a mandrell and then electrodepositing the copper thrust chamber wall around the coating. Chambers were fabricated with coatings .008, and .005 and .003 inches thick. The chambers were thermally cycled at a chamber pressure of 600 psia using oxygen-hydrogen as propellants and liquid hydrogen as the coolant. The thicker coatings tended to delaminate, early in the cyclic testing, down to a uniform sublayer which remained well adhered during the remaining cycles. Two chambers with .003 inch coatings were subjected to 1500 thermal cycles with no coating loss in the throat region, which represents a tenfold increase in life over identical chambers having no coatings. An analysis is presented which shows that the heat lost to the coolant due to the coating, in a rocket thrust chamber design having a coating only in the throat region, can be recovered by adding only one inch to the combustion chamber length.

  13. Composite fermions in 2 {times} 10{sup 6} cm{sup 2}/Vs mobility AlGaAs/GaAs heterostructures grown by MOCVD

    SciTech Connect

    Simmons, J.A.; Chui, H.C.; Harff, N.E.; Hammons, B.E.; Du, R.R.; Zudov, M.A.

    1996-08-01

    The authors report on the recent growth by MOCVD of 2.0 {times} 106 cm2/Vs mobility heterostructures. These mobilities, the highest reported to date, are attributed to the use of tertiarybutylarsine as the arsenic precursor. Measurements in tilted magnetic fields of the fractional quantum Hall effect (FQHE) states near filling factor 3/2 are consistent with a spin-split composite fermion (CF) model proposed earlier. The extracted values of the product of the CF g-factor and CF effective mass agree with values previously obtained for MBE samples.

  14. Composite fermions in 2 x 10{sup 6} cm{sup 2}/Vs mobility A1GaAs/GaAs heterostructures grown by MOCVD

    SciTech Connect

    Simmons, J.A., Chui, H.C., Harff, N.E., Hammons, B.E.; Du, R.R., Zudov, M.A.

    1996-12-31

    Recent growth by MOCVD (metalorganic chemical vapor deposition) of 2.0x10{sup 6} cm{sup 2}/Vs mobility heterostructures are reported. These mobilities, the highest reported to date, are attributed to use of tertiarybutylarsine as the arsenic precursor. Measurements in tilted magnetic fields of the fractional quantum Hall effect states near filling factor 3/2 are consistent with a spin-split composite fermion (CF) model proposed earlier. Extracted values of the product of the CF g-factor and CF effective mass agree with values previously obtained for MBE samples.

  15. Quantum cascade laser based on GaAs/Al0.45Ga0.55As heteropair grown by MOCVD

    NASA Astrophysics Data System (ADS)

    Zasavitskii, I. I.; Zubov, A. N.; Andreev, A. Yu; Bagaev, T. A.; Gorlachuk, P. V.; Ladugin, M. A.; Padalitsa, A. A.; Lobintsov, A. V.; Sapozhnikov, S. M.; Marmalyuk, A. A.

    2016-05-01

    A pulsed quantum cascade laser emitting in the wavelength range 9.5–9.7 μm at 77.4 K is developed based on the GaAs/Al0.45Ga0.55As heteropair. The laser heterostructure was grown by MOCVD. The threshold current density was 1.8 kA cm-2. The maximum output power of the laser with dimensions of 30 μm × 3 mm and with cleaved mirrors exceeded 200 mW.

  16. Influence of stress in GaN crystals grown by HVPE on MOCVD-GaN/6H-SiC substrate.

    PubMed

    Zhang, Lei; Yu, Jiaoxian; Hao, Xiaopeng; Wu, Yongzhong; Dai, Yuanbin; Shao, Yongliang; Zhang, Haodong; Tian, Yuan

    2014-01-01

    GaN crystals without cracks were successfully grown on a MOCVD-GaN/6H-SiC (MGS) substrate with a low V/III ratio of 20 at initial growth. With a high V/III ratio of 80 at initial growth, opaque GaN polycrystals were obtained. The structural analysis and optical characterization reveal that stress has a great influence on the growth of the epitaxial films. An atomic level model is used to explain these phenomena during crystal growth. It is found that atomic mobility is retarded by compressive stress and enhanced by tensile stress. PMID:24569601

  17. Growth and characterization of In{sub X}Ga{sub 1-X}N/GaN single quantum well prepared by MOCVD

    SciTech Connect

    Prabakaran, K.; Ramesh, R.; Jayasakthi, M.; Loganathan, R.; Arivazhagan, P.; Baskar, K.

    2015-06-24

    The InGaN/GaN SQW structures were grown on c-plane sapphire substrate using metal-organic chemical vapor deposition (MOCVD). The thickness and indium composition of the InGaN was determined by HRXRD. From simulation fit the composition of indium was found to be 10% and thickness was around 5nm and 10nm. The Photoluminescence emission was found to be shifited towards lower wavelength as 479nm, 440nm on increasing the thickness. The photoluminescence intensity was degrades with increases of InGaN thickness. Atomic force microscopy studies were also carried out and the results are discussed in detail.

  18. Influence of stress in GaN crystals grown by HVPE on MOCVD-GaN/6H-SiC substrate

    PubMed Central

    Zhang, Lei; Yu, Jiaoxian; Hao, Xiaopeng; Wu, Yongzhong; Dai, Yuanbin; Shao, Yongliang; Zhang, Haodong; Tian, Yuan

    2014-01-01

    GaN crystals without cracks were successfully grown on a MOCVD-GaN/6H-SiC (MGS) substrate with a low V/III ratio of 20 at initial growth. With a high V/III ratio of 80 at initial growth, opaque GaN polycrystals were obtained. The structural analysis and optical characterization reveal that stress has a great influence on the growth of the epitaxial films. An atomic level model is used to explain these phenomena during crystal growth. It is found that atomic mobility is retarded by compressive stress and enhanced by tensile stress. PMID:24569601

  19. An airborne isothermal haze chamber

    NASA Technical Reports Server (NTRS)

    Hindman, E. E.

    1981-01-01

    Thermal gradient diffusion cloud chambers (TGDCC) are used to determine the concentrations of cloud condensation nuclei (CCN) with critical supersaturations greater than or equal to about 0.2%. The CCN concentrations measured with the airborne IHC were lower than theoretically predicted by factors ranging between 7.9 and 9.0. The CCN concentrations measured with the airborne IHC were lower than the concentrations measured with the larger laboratory IHC's by factors ranging between 3.9 and 7.5. The bounds of the supersaturation ranges of the airborne IHC and the CSU-Mee TGDCC do not overlap. Nevertheless, the slopes of the interpolated data between the bounds agree favorably with the theoretical slopes.

  20. Formation of crustal magma chambers in Iceland

    SciTech Connect

    Gudmundsson, A.

    1986-02-01

    Formation of crustal magma chambers in Iceland may be facilitated by the occurrence of stress barriers that lead to formation of thick sills. Such sills absorb the magma of all dikes that enter them and may evolve into magma chambers. Ideal sites for stress barriers, and hence for magma chambers, are rock formations where individual layers have different elastic properties. The rocks formed during the Pleistocene have notably different elastic properties, and when buried in the volcanic zones, they form more promising sites for magma chambers than the Tertiary rocks. This may explain why the number of magma chambers, indicated by the number of corresponding central volcanoes, during the late Pleistocene (i.e., during the past 0.7 m.y.) appears to be proportionally greater than the number of chambers (i.e., central volcanoes) active during Tertiary time.

  1. Sequential Notch activation regulates ventricular chamber development

    PubMed Central

    D'Amato, Gaetano; Luxán, Guillermo; del Monte-Nieto, Gonzalo; Martínez-Poveda, Beatriz; Torroja, Carlos; Walter, Wencke; Bochter, Matthew S.; Benedito, Rui; Cole, Susan; Martinez, Fernando; Hadjantonakis, Anna-Katerina; Uemura, Akiyoshi; Jiménez-Borreguero, Luis J.; de la Pompa, José Luis

    2016-01-01

    Ventricular chambers are essential for the rhythmic contraction and relaxation occurring in every heartbeat throughout life. Congenital abnormalities in ventricular chamber formation cause severe human heart defects. How the early trabecular meshwork of myocardial fibres forms and subsequently develops into mature chambers is poorly understood. We show that Notch signalling first connects chamber endocardium and myocardium to sustain trabeculation, and later coordinates ventricular patterning and compaction with coronary vessel development to generate the mature chamber, through a temporal sequence of ligand signalling determined by the glycosyltransferase manic fringe (MFng). Early endocardial expression of MFng promotes Dll4–Notch1 signalling, which induces trabeculation in the developing ventricle. Ventricular maturation and compaction require MFng and Dll4 downregulation in the endocardium, which allows myocardial Jag1 and Jag2 signalling to Notch1 in this tissue. Perturbation of this signalling equilibrium severely disrupts heart chamber formation. Our results open a new research avenue into the pathogenesis of cardiomyopathies. PMID:26641715

  2. X-ray diffraction study of A- plane non-polar InN epilayer grown by MOCVD

    NASA Astrophysics Data System (ADS)

    Moret, Matthieu; Briot, Olivier; Gil, Bernard

    2015-03-01

    Strong polarisation-induced electric fields in C-plane oriented nitrides semiconductor layers reduce the performance of devices. Eliminating the polarization fields can be achieved by growing nitrides along non polar direction. We have grown non polar A-plane oriented InN on R-plane (1‾102) nitridated sapphire substrate by MOCVD. We have studied the structural anisotropy observed in these layers by analyzing High Resolution XRay Diffraction rocking curve (RC) experiments as a function of the in-plane beam orientation. A-plane InN epilayer have a unique epitaxial relationship on R-Plane sapphire and show a strong structural anisotropy. Full width at half maximum (FWHM) of the InN(11‾20) XRD RC values are contained between 44 and 81 Arcmin. FWHM is smaller when the diffraction occurs along the [0001] and the largest FWHM values, of the (11‾20) RC, are obtained when the diffraction occurs along the [1‾100] in-plane direction. Atomic Force Microscopy imaging revealed morphologies with well organized crystallites. The grains are structured along a unique crystallographic orientation of InN, leading to larger domains in this direction. This structural anisotropy can be, in first approximation, attributed to the difference in the domain sizes observed. XRD reciprocal space mappings (RSM) were performed in asymmetrical configuration on (13‾40) and (2‾202) diffraction plane. RSM are measured with a beam orientation corresponding to a maximal and a minimal width of the (11‾20) Rocking curves, respectively. A simple theoretical model is exposed to interpret the RSM. We concluded that the dominant contribution to the anisotropy is due to the scattering coherence length anisotropy present in our samples.

  3. High and low energy proton radiation damage in p/n InP MOCVD solar cells

    NASA Technical Reports Server (NTRS)

    Rybicki, George; Weinberg, Irving; Scheiman, Dave; Vargas-Aburto, Carlos

    1995-01-01

    InP p(+)nn(+) MOCVD solar cells were irradiated with 0.2 MeV and 10 MeV protons to a fluence of 10(exp 13)/sq cm. The degradation of power output, IV behavior, carrier concentration and defect concentration were observed at intermediate points throughout the irradiations. The 0.2 MeV proton irradiated solar cells suffered much greater and more rapid degradation in power output than those irradiated with 10 meV protons. The efficiency losses were accompanied by larger increases in the recombination currents in the 0.2 MeV proton irradiated solar cells. The low energy proton irradiations also had a larger impact on the series resistance of the solar cells. Despite the radiation induced damage, the carrier concentration in the base of the solar cells showed no reduction after 10 MeV or 0.2 MeV proton irradiations and even increased during irradiation with 0.2 MeV protons. In a DLTS study of the irradiated samples, the minority carrier defects H4 and H5 at E(v) + 0.33 and E(v) + 0.52 eV and the majority carrier defects E7 and E10 at E(c)- 0.39 and E(c)-0.74 eV, were observed. The defect introduction rates for the 0.2 MeV proton irradiations were about 20 times higher than for the 10 MeV proton irradiations. The defect E10, observed here after irradiation, has been shown to act as a donor in irradiated n-type InP and may be responsible for obscuring carrier removal. The results of this study are consistent with the much greater damage produced by low energy protons whose limited range causes them to stop in the active region of the solar cell.

  4. Vertically p-n-junctioned GaN nano-wire array diode fabricated on Si(111) using MOCVD.

    PubMed

    Park, Ji-Hyeon; Kim, Min-Hee; Kissinger, Suthan; Lee, Cheul-Ro

    2013-04-01

    We demonstrate the fabrication of n-GaN:Si/p-GaN:Mg nanowire arrays on (111) silicon substrate by metal organic chemical vapor deposition (MOCVD) method .The nanowires were grown by a newly developed two-step growth process. The diameter of as-grown nanowires ranges from 300-400 nm with a density of 6-7 × 10(7) cm(-2). The p- and n-type doping of the nanowires is achieved with Mg and Si dopant species. Structural characterization by X-ray diffraction (XRD) and high-resolution transmission electron microscopy (HRTEM) indicates that the nanowires are relatively defect-free. The room-temperature photoluminescence emission with a strong peak at 370 nm indicates that the n-GaN:Si/p-GaN:Mg nanowire arrays have potential application in light-emitting nanodevices. The cathodoluminscence (CL) spectrum clearly shows a distinct optical transition of GaN nanodiodes. The nano-n-GaN:Si/p-GaN:Mg diodes were further completed using a sputter coating approach to deposit Au/Ni metal contacts. The polysilazane filler has been etched by a wet chemical etching process. The n-GaN:Si/p-GaN:Mg nanowire diode was fabricated for different Mg source flow rates. The current-voltage (I-V) measurements reveal excellent rectifying properties with an obvious turn-on voltage at 1.6 V for a Mg flow rate of 5 sccm (standard cubic centimeters per minute). PMID:23455517

  5. Effects of TMSb/TEGa ratios on epilayer properties of gallium antimonide grown by low-pressure MOCVD

    NASA Astrophysics Data System (ADS)

    Wu, Tong S.; Su, Yan-Kuin; Juang, Fuh S.; Li, N. Y.; Gan, K. J.

    1991-03-01

    Undoped GaSb epitaxial layers have been grown on (100) GaSb and GaAs substrates by low pressure MOCVD. It was found that the layer morphologies were strongly dependent on TMSb/TEGa (V/Ill) ratios. The mirrorlike surface can be easily obtained under V/Ill ratio in the range of 68 at growth temperature 600 C and growth pressure 100 torr. Beyond this range the surface deteriorated seriously. The epilayers were characterized by electron diffraction patterns and photoluminescent measurements. The boundexciton (BE) peaks and strong acceptor band peak in PL spectra were observed from the sample grown under V/Ill ratio of 6. 84 on GaSb substrates. PL peak intensity was found to be a function of the V/Ill ratios. When V/Ill ratios increased beyond the range of 68 the BE peaks disappeared and PL spectra became roughened. The full width at half maximum (FWHM) of acceptor-band peaks in PL spectra was dependent on V/Ill ratios ensuring that obtained from the analysis of surface morphology. IV characteristics of the pn diodes fabricated on the sample of undoped-GaSb/GaSb:Te was measured. The electrical properties of undoped GaSb were studied from the epilayers grown on GaAs semiinsulating substrates. The hole concentration increased and mobility decreased with growth temperature between 520 and 635C under V/1116. 84. For 550 C grown epilayers: as V/Ill ratio increased above 6. 64 or decreased below 6. 64 the hole concentration increased and hole mobility decreased. .

  6. Drift chamber tracking with neural networks

    SciTech Connect

    Lindsey, C.S.; Denby, B.; Haggerty, H.

    1992-10-01

    We discuss drift chamber tracking with a commercial log VLSI neural network chip. Voltages proportional to the drift times in a 4-layer drift chamber were presented to the Intel ETANN chip. The network was trained to provide the intercept and slope of straight tracks traversing the chamber. The outputs were recorded and later compared off line to conventional track fits. Two types of network architectures were studied. Applications of neural network tracking to high energy physics detector triggers is discussed.

  7. Experimental investigation of a lightweight rocket chamber

    NASA Technical Reports Server (NTRS)

    Dalgleish, John E; Tischler, Adelbert O

    1953-01-01

    Experiments have been conducted with a jacketed rocket combustion chamber that was fabricated by hydraulic-forming from sheet metal. Rocket combustion chambers made by this method have been used successfully. Runs with these combustion chambers have been made at over-all heat-transfer rates 1.7 Btu per square inch per second with water cooling and also ammonia as a regenerative coolant.

  8. Fluidized wall for protecting fusion chamber walls

    SciTech Connect

    Maniscalco, James A.; Meier, Wayne R.

    1982-01-01

    Apparatus for protecting the inner wall of a fusion chamber from microexplosion debris, x-rays, neutrons, etc. produced by deuterium-tritium (DT) targets imploded within the fusion chamber. The apparatus utilizes a fluidized wall similar to a waterfall comprising liquid lithium or solid pellets of lithium-ceramic, the waterfall forming a blanket to prevent damage of the structural materials of the chamber.

  9. IFE Chamber Technology - Status and Future Challenges

    SciTech Connect

    Meier, W R; Raffrary, A R; Abdel-Khalik, S; Kulcinski, G; Latkowski, J F; Najmabadi, F; Olson, C L; Peterson, P F; Ying, A; Yoda, M

    2002-11-15

    Significant progress has been made on addressing critical issues for inertial fusion energy (IFE) chambers for heavy-ion, laser and Z-pinch drivers. A variety of chamber concepts are being investigated including dry-wall (currently favored for laser IFE), wetted-wall (applicable to both laser and ion drivers), and thick-liquid-wall favored by heavy ion and z-pinch drivers. Recent progress and remaining challenges in developing IFE chambers are reviewed.

  10. D0 central tracking chamber performance studies

    SciTech Connect

    Pizzuto, D.

    1991-12-01

    The performance of the completed DO central tracking chamber was studied using cosmic rays at the State University of New York at Stony Brook. Also studied was a prototype tracking chamber identical in design to the completed DO tracking chamber. The prototype chamber was exposed to a collimated beam of 150 GeV pions at the Fermilab NWA test facility. Results indicate an R{Phi} tracking resolution compatible with the limitations imposed by physical considerations, excellent 2 track resolution, and a high track reconstruction efficiency along with a good rejection power against {gamma} {yields} e {sup +} e{sup {minus}} events.

  11. Engineering verification of the biomass production chamber

    NASA Technical Reports Server (NTRS)

    Prince, R. P.; Knott, W. M., III; Sager, J. C.; Jones, J. D.

    1992-01-01

    The requirements for life support systems, both biological and physical-chemical, for long-term human attended space missions are under serious study throughout NASA. The KSC 'breadboard' project has focused on biomass production using higher plants for atmospheric regeneration and food production in a special biomass production chamber. This chamber is designed to provide information on food crop growth rate, contaminants in the chamber that alter plant growth requirements for atmospheric regeneration, carbon dioxide consumption, oxygen production, and water utilization. The shape and size, mass, and energy requirements in relation to the overall integrity of the biomass production chamber are under constant study.

  12. Optical and crystal quality improvement in green emitting InxGa1-xN multi-quantum wells through optimization of MOCVD growth

    NASA Astrophysics Data System (ADS)

    Berkman, Erkan A.; Lee, Soo Min; Ramos, Frank; Tucker, Eric; Arif, Ronald A.; Armour, Eric A.; Papasouliotis, George D.

    2016-02-01

    We report on green-emitting In0.18Ga0.82N/GaN multi-quantum well (MQW) structures over a variety of metalorganic chemical vapor deposition (MOCVD) growth conditions to examine the morphology, optical quality, and micron-scale emission properties. The MOCVD growth parameter space was analyzed utilizing two orthogonal metrics which allows comparing and optimizing growth conditions over a wide range of process parameters: effective gas speed, S*, and effective V/III ratio, V/III*. Optimized growth conditions with high V/III, low gas speed, and slow growth rates resulted in improved crystal quality, PL emission efficiency, and micron-scale wavelength uniformity. One of the main challenges in green MQWs with high Indium content is the formation of Indium inclusion type defects due to the large lattice mismatch combined with the miscibility gap between GaN and InN. An effective way of eliminating Indium inclusions was demonstrated by introducing a small fraction of H2 (2.7%) in the gas composition during the growth of high temperature GaN quantum barriers. In addition, the positive effects of employing an InGaN/GaN superlattice (SL) underlayer to crystal quality and micron-scale emission uniformity was demonstrated, which is of special interest for applications such as micro-LEDs.

  13. Growth parameters effect on the thermoelectric characteristics of Bi 2Se 3 thin films grown by MOCVD system using Ditertiarybutylselenide as a precursor

    NASA Astrophysics Data System (ADS)

    Bayaz, A. Al; Giani, A.; Khalfioui, M. Al; Foucaran, A.; Pascal-Delannoy, F.; Boyer, A.

    2003-10-01

    The growth of Bi 2Se 3 thin films by metalorganic chemical vapour deposition (MOCVD) using Trimethylbismuth (TMBi) and a novel Se-precursor: Ditertiarybutylselenide (DTBSe) as bismuth and selenium sources, respectively, is investigated on pyrex substrates. The effect of the growth parameters such as substrate temperature, Tg, and TMBi partial pressure, PTMBi, on the structural, electrical and thermoelectrical properties for the following growth conditions: 440°C⩽ Tg⩽475°C, 0.5×10 -4 atm⩽ PTMBi⩽1×10 -4 atm and a total hydrogen flow rate DT=3 l/mn, of Bi 2Se 3 films has been investigated. The crystallinity versus growth condition ( Tg, PTMBi) using X-ray diffraction was studied and a typical preferential c-orientation was observed. Thus, these layers always displayed n-type conduction using Hall effect measurement. The best electric and thermoelectric characteristics under the optimal growth conditions have been found; μ>250 cm 2/V s, ρ⩽11.8 μΩ m and α=-163.7 μV/K Then, These initial results suggest a significant potential for the MOCVD method to produce good thermoelectrical materials using DTBSe as Se-precursor.

  14. A Comparative Study of a Series of Dimethylgold(III) Complexes with S,S Chelating Ligands Used as MOCVD Precursors

    NASA Astrophysics Data System (ADS)

    Turgambaeva, Asiya; Parkhomenko, Roman; Aniskin, Vladimir; Krisyuk, Vladislav; Igumenov, Igor

    Dimethylgold(III) complexes with S,S donor ligands having AuC2S2 coordination core are compared as precursors for gold MOCVD. Three of them are liquids, the fourth one is low-melting compound. They are non-sensitive to air and light, stable under storage, do not require special handling conditions, and show a good volatility and sufficient vaporization stability. Based on monitoring of the gas phase during the programmed heating of the compound vapor in vacuum, in hydrogen and in oxygen presence, the information concerning stability of the precursor in the gas phase and gaseous products of thermolysis was obtained. It was established that decomposition mechanism in the presence of the studied gas- reactants changed in comparison with vacuum only for diethyldithiocarbamate complex. MOCVD experiments have been performed within the temperature range 210-300 oC with and without hydrogen or oxygen. The films obtained in hydrogen presence were more thick indicating higher growth rate. Effect of gas-reactant on the morphology of the films deposited is discussed.

  15. Trade-offs of the opto-electrical properties of a-Si:H solar cells based on MOCVD BZO films.

    PubMed

    Chen, Ze; Zhang, Xiao-dan; Liang, Jun-hui; Fang, Jia; Liang, Xue-jiao; Sun, Jian; Zhang, De-kun; Chen, Xin-liang; Huang, Qian; Zhao, Ying

    2015-01-01

    Boron-doped zinc oxide (BZO) films, deposited by metal-organic chemical vapor deposition (MOCVD), have been widely used as front electrodes in thin-film solar cells due to their native pyramidal surface structure, which results in efficient light trapping. This light trapping effect can enhance the short-circuit current density (Jsc) of solar cells. However, nanocracks or voids in the silicon active layer may form when the surface morphology of the BZO is too sharp; this usually leads to degraded electrical properties of the cells, such as open-circuit voltage (Voc) and the fill factor (FF), which in turn decreases efficiency (Eff) [Bailat et al., Photovoltaic Energy Conversion, Conference Record of the 2006 IEEE 4th World Conference on. IEEE, 2006, vol. 2, pp. 1533-1536]. In this paper, an etching and coating method was proposed to modify the sharp "pyramids" on the surface of the BZO films. As a result, an evident enhancement was achieved for these modified, BZO-based cells' Voc, FF, and Eff, although the Jsc exhibited a small decrease. In order to increase the Jsc and maintain the improved electrical properties (Voc, FF) of the cell, a thin BZO coating, deposited by MOCVD, was introduced to coat the sputtering-treated BZO film. Finally, we optimized the trade-off among the Voc, FF, and Jsc, that is, we identified a regime with an increase of the Jsc as well as a further improvement of the other electrical properties. PMID:25407724

  16. Dual-purpose chamber-cooling system

    NASA Technical Reports Server (NTRS)

    Fraze, R. E.

    1968-01-01

    Inexpensive, portable system was designed for cooling small environmental test chambers with a temperature-controlled gas stream evaporated from a cryogenic liquid. The system reduces the temperature of a chamber to any desired point in a fraction of the time required by previous systems.

  17. Studying Phototropism Using a Small Growth Chamber.

    ERIC Educational Resources Information Center

    Fisher, Maryanna, F.; Llewellyn, Gerald C.

    1978-01-01

    Describes a simple and inexpensive way to construct two small growth chambers for studying phototropism in the science classroom. One chamber is designed to illustrate how plants grow around obstacles to reach light and the other to illustrate directional light responses. (HM)

  18. 21 CFR 868.5470 - Hyperbaric chamber.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... hyperbaric chamber is a device that is intended to increase the environmental oxygen pressure to promote the movement of oxygen from the environment to a patient's tissue by means of pressurization that is greater than atmospheric pressure. This device does not include topical oxygen chambers for extremities (§...

  19. Results from the MAC Vertex chamber

    SciTech Connect

    Nelson, H.N.

    1987-05-01

    The design, construction, and performance characteristics of a high precision gaseous drift chamber made of thin walled proportional tubes are described. The device achieved an average spatial resolution of 45 ..mu..m in use for physics analysis with the MAC detector. The B-lifetime result obtained with this chamber is discussed.

  20. Space Simulation Chamber Rescues Water Damaged Books.

    ERIC Educational Resources Information Center

    American School and University, 1981

    1981-01-01

    More than 4,000 valuable water-damaged books were restored by using a space-simulation chamber at the Lockheed Missile and Space Company. It was the fifth time that the chamber has been used for the restoration of valuable books and documents. (Author/MLF)

  1. Space Power Facility Reverberation Chamber Calibration Report

    NASA Technical Reports Server (NTRS)

    Lewis, Catherine C.; Dolesh, Robert J.; Garrett, Michael J.

    2014-01-01

    This document describes the process and results of calibrating the Space Environmental Test EMI Test facility at NASA Plum Brook Space Power Facility according to the specifications of IEC61000-4-21 for susceptibility testing from 100 MHz to 40 GHz. The chamber passed the field uniformity test, in both the empty and loaded conditions, making it the world's largest Reverberation Chamber.

  2. Chamber Music's Lesson in Performing Confidence.

    ERIC Educational Resources Information Center

    Stubbs, Darrel W.

    1983-01-01

    Chamber music has the advantage of offering the student maximum exposure as an individual performer. The absence of a conductor means that the student assumes the role of interpreter, thereby gaining musical maturity. For these reasons, curriculum hours should be more evenly divided between chamber music and larger ensembles. (CS)

  3. Creating Chamber Music Enthusiasts in High School.

    ERIC Educational Resources Information Center

    Cummiskey, Cynthia

    1999-01-01

    Describes the Fairfield High School Chamber Music Honors Program for students in grades nine through twelve in Fairfield (Connecticut). Explains that the program's goal is to provide students with a positive experience in chamber music. Highlights the creation and the first two years of the program. (CMK)

  4. Promoting "Minds-on" Chamber Music Rehearsals

    ERIC Educational Resources Information Center

    Berg, Margaret H.

    2008-01-01

    Chamber music provides myriad opportunities to develop students' ability to think like professional musicians while engaged in the authentic task of working closely with and learning from peers. However, the potential for musical growth inherent in chamber music participation is often unrealized due to either a lack of teacher guidance and support…

  5. 21 CFR 866.2120 - Anaerobic chamber.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Anaerobic chamber. 866.2120 Section 866.2120 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES IMMUNOLOGY AND MICROBIOLOGY DEVICES Microbiology Devices § 866.2120 Anaerobic chamber....

  6. 21 CFR 866.2120 - Anaerobic chamber.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Anaerobic chamber. 866.2120 Section 866.2120 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES IMMUNOLOGY AND MICROBIOLOGY DEVICES Microbiology Devices § 866.2120 Anaerobic chamber....

  7. 21 CFR 866.2120 - Anaerobic chamber.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Anaerobic chamber. 866.2120 Section 866.2120 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES IMMUNOLOGY AND MICROBIOLOGY DEVICES Microbiology Devices § 866.2120 Anaerobic chamber....

  8. 21 CFR 866.2120 - Anaerobic chamber.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Anaerobic chamber. 866.2120 Section 866.2120 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES IMMUNOLOGY AND MICROBIOLOGY DEVICES Microbiology Devices § 866.2120 Anaerobic chamber....

  9. 21 CFR 866.2120 - Anaerobic chamber.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Anaerobic chamber. 866.2120 Section 866.2120 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES IMMUNOLOGY AND MICROBIOLOGY DEVICES Microbiology Devices § 866.2120 Anaerobic chamber....

  10. Aging in large CDF tracking chambers

    SciTech Connect

    M. Binkley et al.

    2001-03-19

    The experience of the Collider Detector at Fermilab (CDF) with aging in the large axial drift chamber responsible for tracking in the central region is presented. Premature aging in the Run 1 chamber was observed after only 0.02 C/cm. After cleaning much of the gas system and making modifications to reduce aerosols from the alcohol bubbler, the observed aging rate fell dramatically in test chambers. Considerable effort has been made to better understand the factors that affect aging since the replacement chamber for Run 2 will accumulate about 1.0 C/cm. Current test chambers using the full CDF gas system show aging rates of less than 5%/C/cm.

  11. Note: Small anaerobic chamber for optical spectroscopy.

    PubMed

    Chauvet, Adrien A P; Agarwal, Rachna; Cramer, William A; Chergui, Majed

    2015-10-01

    The study of oxygen-sensitive biological samples requires an effective control of the atmosphere in which they are housed. In this aim however, no commercial anaerobic chamber is adequate to solely enclose the sample and small enough to fit in a compact spectroscopic system with which analysis can be performed. Furthermore, spectroscopic analysis requires the probe beam to pass through the whole chamber, introducing a requirement for adequate windows. In response to these challenges, we present a 1 l anaerobic chamber that is suitable for broad-band spectroscopic analysis. This chamber has the advantage of (1) providing access, via a septum, to the sample and (2) allows the sample position to be adjusted while keeping the chamber fixed and hermetic during the experiment. PMID:26520998

  12. Note: Small anaerobic chamber for optical spectroscopy

    NASA Astrophysics Data System (ADS)

    Chauvet, Adrien A. P.; Agarwal, Rachna; Cramer, William A.; Chergui, Majed

    2015-10-01

    The study of oxygen-sensitive biological samples requires an effective control of the atmosphere in which they are housed. In this aim however, no commercial anaerobic chamber is adequate to solely enclose the sample and small enough to fit in a compact spectroscopic system with which analysis can be performed. Furthermore, spectroscopic analysis requires the probe beam to pass through the whole chamber, introducing a requirement for adequate windows. In response to these challenges, we present a 1 l anaerobic chamber that is suitable for broad-band spectroscopic analysis. This chamber has the advantage of (1) providing access, via a septum, to the sample and (2) allows the sample position to be adjusted while keeping the chamber fixed and hermetic during the experiment.

  13. Ionization-chamber smoke detector system

    DOEpatents

    Roe, Robert F.

    1976-10-19

    This invention relates to an improved smoke-detection system of the ionization-chamber type. In the preferred embodiment, the system utilizes a conventional detector head comprising a measuring ionization chamber, a reference ionization chamber, and a normally non-conductive gas triode for discharging when a threshold concentration of airborne particulates is present in the measuring chamber. The improved system is designed to reduce false alarms caused by fluctuations in ambient temperature. Means are provided for periodically firing the gas discharge triode and each time recording the triggering voltage required. A computer compares each triggering voltage with its predecessor. The computer is programmed to energize an alarm if the difference between the two compared voltages is a relatively large value indicative of particulates in the measuring chamber and to disregard smaller differences typically resulting from changes in ambient temperature.

  14. Compact ion chamber based neutron detector

    SciTech Connect

    Derzon, Mark S.; Galambos, Paul C.; Renzi, Ronald F.

    2015-10-27

    A directional neutron detector has an ion chamber formed in a dielectric material; a signal electrode and a ground electrode formed in the ion chamber; a neutron absorbing material filling the ion chamber; readout circuitry which is electrically coupled to the signal and ground electrodes; and a signal processor electrically coupled to the readout circuitry. The ion chamber has a pair of substantially planar electrode surfaces. The chamber pressure of the neutron absorbing material is selected such that the reaction particle ion trail length for neutrons absorbed by the neutron absorbing material is equal to or less than the distance between the electrode surfaces. The signal processor is adapted to determine a path angle for each absorbed neutron based on the rise time of the corresponding pulse in a time-varying detector signal.

  15. Advanced tube-bundle rocket thrust chamber

    NASA Technical Reports Server (NTRS)

    Kazaroff, John M.; Pavli, Albert J.

    1990-01-01

    An advanced rocket thrust chamber for future space application is described along with an improved method of fabrication. Potential benefits of the concept are improved cyclic life, reusability, and performance. Performance improvements are anticipated because of the enhanced heat transfer into the coolant which will enable higher chamber pressure in expander cycle engines. Cyclic life, reusability and reliability improvements are anticipated because of the enhanced structural compliance inherent in the construction. The method of construction involves the forming of the combustion chamber with a tube-bundle of high conductivity copper or copper alloy tubes, and the bonding of these tubes by an electroforming operation. Further, the method of fabrication reduces chamber complexity by incorporating manifolds, jackets, and structural stiffeners while having the potential for thrust chamber cost and weight reduction.

  16. Note: Small anaerobic chamber for optical spectroscopy

    SciTech Connect

    Chauvet, Adrien A. P. Chergui, Majed; Agarwal, Rachna; Cramer, William A.

    2015-10-15

    The study of oxygen-sensitive biological samples requires an effective control of the atmosphere in which they are housed. In this aim however, no commercial anaerobic chamber is adequate to solely enclose the sample and small enough to fit in a compact spectroscopic system with which analysis can be performed. Furthermore, spectroscopic analysis requires the probe beam to pass through the whole chamber, introducing a requirement for adequate windows. In response to these challenges, we present a 1 l anaerobic chamber that is suitable for broad-band spectroscopic analysis. This chamber has the advantage of (1) providing access, via a septum, to the sample and (2) allows the sample position to be adjusted while keeping the chamber fixed and hermetic during the experiment.

  17. An atmospheric exposure chamber for small animals

    NASA Technical Reports Server (NTRS)

    Glaser, R. M.; Weiss, H. S.; Pitt, J. F.; Grimard, M.

    1982-01-01

    The purpose of this project was to design a long-term environmental exposure chamber for small animals. This chamber is capable of producing hypoxic, normoxic and hyperoxic atmospheres which are closely regulated. The chamber, which is of the recycling type, is fashioned after clear plastic germ-free isolators. Oxygen concentration is set and controlled by a paramagnetic O2 analyzer and a 3-way solenoid valve. In this way either O2 or N2 may be provided to the system by way of negative O2 feedback. Relative humidity is maintained at 40-50 percent by a refrigeration type dryer. Carbon dioxide is absorbed by indicating soda lime. A diaphragm pump continuously circulates chamber gas at a high enough flow rate to prevent buildup of CO2 and humidity. This chamber has been used for numerous studies which involve prolonged exposure of small animals to various O2 concentrations.

  18. RADIATION MONITOR CONTAINING TWO CONCENTRIC IONIZATION CHAMBERS AND MEANS FOR INSULATING THE SEPARATE CHAMBERS

    DOEpatents

    Braestrup, C.B.; Mooney, R.T.

    1964-01-21

    This invention relates to a portable radiation monitor containing two concentric ionization chambers which permit the use of standard charging and reading devices. It is particularly adapted as a personnel x-ray dosimeter and to this end comprises a small thin walled, cylindrical conductor forming an inner energy dependent chamber, a small thin walled, cylindrical conductor forming an outer energy independent chamber, and polymeric insulation means which insulates said chambers from each other and holds the chambers together with exposed connections in a simple, trouble-free, and compact assembly substantially without variation in directional response. (AEC)

  19. High and Low Energy Proton Radiation Damage in p/n InP MOCVD Solar Cells

    NASA Technical Reports Server (NTRS)

    Rybicki, George; Weinberg, Irv; Scheiman, Dave; Vargas-Aburto, Carlos; Uribe, Roberto

    1995-01-01

    InP p(+)/n/n(+) solar cells, fabricated by metal organic chemical vapor deposition, (MOCVD) were irradiated with 0.2 MeV and 10 MeV protons to a fluence of 10(exp 13)/sq cm. The power output degradation, IV behavior, carrier concentration and defect concentration were observed at intermediate points throughout the irradiations. The 0.2 MeV proton-irradiated solar cells suffered much greater and more rapid degradation in power output than those irradiated with 10 MeV protons. The efficiency losses were accompanied by larger increases in the recombination currents in the 0.2 MeV proton-irradiated solar cells. The low energy proton irradiations also had a larger impact on the series resistance of the solar cells. Despite the radiation induced damage, the carrier concentration in the base of the solar cells showed no reduction after 10 MeV or 0.2 MeV proton irradiations and even increased during irradiation with 0.2 MeV protons. In a deep level transient spectroscopy (DLTS) study of the irradiated samples, the minority carrier defects H4 and H5 at E(sub v) + 0.33 and E(sub v) + 0.52 eV and the majority carrier defects E7 and El0 at E(sub c) - 0.39 and E(sub c) - 0.74 eV, were observed. The defect introduction rates for the 0.2 MeV proton irradiations were about 20 times higher than for the 10 MeV proton irradiations. The defect El0, observed here after irradiation, has been shown to act as a donor in irradiated n-type InP and may be responsible for obscuring carrier removal. The results of this study are consistent with the much greater damage produced by low energy protons whose limited range causes them to stop in the active region of the solar cell.

  20. Preparation of ZnO:CeO{sub 2-x} thin films by AP-MOCVD: Structural and optical properties

    SciTech Connect

    Torres-Huerta, A.M.; Dominguez-Crespo, M.A.; Brachetti-Sibaja, S.B.; Dorantes-Rosales, H.; Hernandez-Perez, M.A.; Lois-Correa, J.A.

    2010-09-15

    The growth of columnar CeO{sub 2}, ZnO and ZnO:CeO{sub 2-x} films on quartz and AA6066 aluminum alloy substrates by economic atmospheric pressure metal-organic chemical vapor deposition (AP-MOCVD) is reported. A novel and efficient combination of metal acetylacetonate precursors as well as mild operating conditions were used in the deposition process. The correlation among crystallinity, surface morphology and optical properties of the as-prepared films was analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM), atomic force microscopy (AFM), transmission electron microscopy (TEM) and UV-vis spectroscopy. The synthesized films showed different crystallographic orientations depending on the ZnO and CeO{sub 2} lattice mismatch, cerium content and growth rate. The CeO{sub 2} films synthesized in this work showed plate-like compact structures as a result of the growth process typical of CVD. Both pure and ZnO:CeO{sub 2-x} films were obtained with a hexagonal structure and highly preferred orientation with the c-axis perpendicular to both substrates under the optimal deposition conditions. The microstructure was modified from dense, short round columns to round structures with cavities ('rose-flower-like' structures) and the typical ZnO morphology by controlling the cerium doping the film and substrate nature. High optical transmittance (>87%) was observed in the pure ZnO films. As for the ZnO:CeO{sub 2-x} films, the optical transmission was decreased and the UV absorption increased, which subsequently was affected by an increase in cerium content. This paper assesses the feasibility of using ZnO:CeO{sub 2-x} thin films as UV-absorbers in industrial applications. - Graphical abstract: TEM micrographs and their corresponding SAED pattern obtained for the as-deposited ZnO-CeO{sub 2-x} thin films for a Zn/Ce metallic ratio 16:9.

  1. Compound semiconductor native oxide-based technologies for optical and electrical devices grown on gallium arsenide substrates using MOCVD

    NASA Astrophysics Data System (ADS)

    Holmes, Adrian Lawrence

    1999-11-01

    The beginning of the modern microelectronics industry can be traced back to an invention made in 1947 when Bardeen and Brattain created the first semiconductor switch, called a transistor. Several other important discoveries followed; however, two of the more significant were (i) the development of the first planar process using silicon dioxide (SiO2) as a mask for diffusions into silicon by Frosch in 1955, and (ii) the subsequent integration of several transistors in tiny circuits by Kilby in 1958. Due to the superior quality of the SiO2-silicon interface, Si-based metal-oxide-semiconductor (MOS) transistors have primarily been used in integrated circuits. Until recently, compound semiconductors did not have a native oxide of sufficient quality to create similar MOS transistors. In 1990, research performed by Professor Holonyak and his group at the University of Illinois at Urbana-Champaign has led to a high-quality, stable, and insulating native oxide created from aluminum-containing compound semiconductor alloys. This study investigates native oxide films that are formed by the thermal oxidation of AlAs and InAlP epitaxial layers grown lattice-matched on GaAs substrates using metalorganic chemical vapor deposition (MOCVD). The primary goal is to evaluate how these native oxides can help form novel device structures and transistors. To qualify the material properties of these native oxide films, we have used several characterization techniques including photoluminescence, cross-sectional scanning electron microscopy (SEM), X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS). Additionally, we have performed leakage current and capacitance-voltage measurements to evaluate the electrical characteristics of the native oxide-semiconductor interface. The kinetics of the thermal oxidation process for both the surface oxidation of InAlP and lateral oxidation of AlAs are studied and contrasted. Aided by this knowledge, we have created a sealed

  2. The emulsion chamber technology experiment

    NASA Technical Reports Server (NTRS)

    Gregory, John C.

    1992-01-01

    Photographic emulsion has the unique property of recording tracks of ionizing particles with a spatial precision of 1 micron, while also being capable of deployment over detector areas of square meters or 10's of square meters. Detectors are passive, their cost to fly in Space is a fraction of that of instruments of similar collecting. A major problem in their continued use has been the labor intensiveness of data retrieval by traditional microscope methods. Two factors changing the acceptability of emulsion technology in space are the astronomical costs of flying large electronic instruments such as ionization calorimeters in Space, and the power and low cost of computers, a small revolution in the laboratory microscope data-taking. Our group at UAH made measurements of the high energy composition and spectra of cosmic rays. The Marshall group has also specialized in space radiation dosimetry. Ionization calorimeters, using alternating layers of lead and photographic emulsion, to measure particle energies up to 10(exp 15) eV were developed. Ten balloon flights were performed with them. No such calorimeters have ever flown in orbit. In the ECT program, a small emulsion chamber was developed and will be flown on the Shuttle mission OAST-2 to resolve the principal technological questions concerning space exposures. These include assessments of: (1) pre-flight and orbital exposure to background radiation, including both self-shielding and secondary particle generation; the practical limit to exposure time in space can then be determined; (2) dynamics of stack to optimize design for launch and weightlessness; and (3) thermal and vacuum constraints on emulsion performance. All these effects are cumulative and affect our ability to perform scientific measurements but cannot be adequately predicted by available methods.

  3. Gas Electron Multiplier (GEM) Chamber Characteristics Test

    SciTech Connect

    Yu, Jaehoon; White, Andy; Park, Seongtae; Hahn, Changhie; Baldeloma, Edwin; Tran, Nam; McIntire, Austin; Soha, Aria; /Fermilab

    2011-01-11

    Gas Electron Multipliers (GEMs) have been used in many HEP experiments as tracking detectors. They are sensitive to X-rays which allows use beyond that of HEP. The UTA High Energy group has been working on using GEMs as the sensitive gap detector in a DHCAL for the ILC. The physics goals at the ILC put a stringent requirement on detector performance. Especially the precision required for jet mass and positions demands an unprecedented jet energy resolution to hadronic calorimeters. A solution to meet this requirement is using the Particle Flow Algorithm (PFA). In order for PFA to work well, high calorimeter granularity is necessary. Previous studies based on GEANT simulations using GEM DHCAL gave confidence on the performance of GEM in the sensitive gap in a sampling calorimeter and its use as a DHCAL in PFA. The UTA HEP team has built several GEM prototype chambers, including the current 30cm x 30cm chamber integrated with the SLAC-developed 64 channel kPiX analog readout chip. This chamber has been tested on the bench using radioactive sources and cosmic ray muons. In order to have fuller understanding of various chamber characteristics, the experiments plan to expose 1-3 GEM chambers of dimension 35cm x 35cm x 5cm with 1cm x 1cm pad granularity with 64 channel 2-D simultaneous readout using the kPiX chip. In this experiment the experiments pan to measure MiP signal height, chamber absolute efficiencies, chamber gain versus high voltage across the GEM gap, the uniformity of the chamber across the 8cm x 8cm area, cross talk and its distance dependence to the triggered pad, chamber rate capabilities, and the maximum pad occupancy rate.

  4. Making MUSIC: A multiple sampling ionization chamber

    NASA Astrophysics Data System (ADS)

    Shumard, B.; Henderson, D. J.; Rehm, K. E.; Tang, X. D.

    2007-08-01

    A multiple sampling ionization chamber (MUSIC) was developed for use in conjunction with the Atlas scattering chamber (ATSCAT). This chamber was developed to study the (α, p) reaction in stable and radioactive beams. The gas filled ionization chamber is used as a target and detector for both particles in the outgoing channel (p + beam particles for elastic scattering or p + residual nucleus for (α, p) reactions). The MUSIC detector is followed by a Si array to provide a trigger for anode events. The anode events are gated by a gating grid so that only (α, p) reactions where the proton reaches the Si detector result in an anode event. The MUSIC detector is a segmented ionization chamber. The active length of the chamber is 11.95 in. and is divided into 16 equal anode segments (3.5 in. × 0.70 in. with 0.3 in. spacing between pads). The dead area of the chamber was reduced by the addition of a Delrin snout that extends 0.875 in. into the chamber from the front face, to which a mylar window is affixed. 0.5 in. above the anode is a Frisch grid that is held at ground potential. 0.5 in. above the Frisch grid is a gating grid. The gating grid functions as a drift electron barrier, effectively halting the gathering of signals. Setting two sets of alternating wires at differing potentials creates a lateral electric field which traps the drift electrons, stopping the collection of anode signals. The chamber also has a reinforced mylar exit window separating the Si array from the target gas. This allows protons from the (α, p) reaction to be detected. The detection of these protons opens the gating grid to allow the drift electrons released from the ionizing gas during the (α, p) reaction to reach the anode segment below the reaction.

  5. Multisegmented ion chamber for CT scanner dosimetry

    SciTech Connect

    Moore, M.M.; Cacak, R.K.; Hendee, W.R.

    1981-01-01

    A multisegmented, ionization chamber capable of determining dosimetric profiles from a CT scanner has been developed and tested. The chamber consists of a number of 2 mm wide electrically isolated segments from which ionization currents may be measured. Presented here are the performance characteristics of the chamber including energy response, dose linearity, and corrections for ''cross talk'' between segments. Sample dosimetric profiles are depicted for 3 and 6 mm nominal beam widths at two locations in a dosimetric phantom positioned in the x-ray beam of a fourth generation CT scanner. The results agree well with the conventional method of obtaining dosimetry measurements with TLD chips.

  6. The Japanese Radon and Thoron Reference Chambers

    SciTech Connect

    Tokonami, Shinji; Ishikawa, Tetsuo; Sorimachi, Atsuyuki; Takahashi, Hiroyuki; Miyahara, Nobuyuki

    2008-08-07

    Passive detectors used for large-scale and long-term surveys are generally calibrated in a well-controlled environment such as a radon chamber. It has been also pointed out that some of them are sensitive to thoron. Thus it is necessary to check the thoron contribution to the detector response with the proposed or similar test before practical use. The NIRS accommodates radon/aerosol and thoron chambers for quality assurance and quality control of radon measurements. Thus both chambers work so well that they can supply us with the calibration technique and consequently, a good level of knowledge of the radon and thoron issue.

  7. Sample chambers with mother-daughter mode

    SciTech Connect

    Wilk, P.A.; Gregorich, K.E.; Hoffman, D.C.

    2001-07-12

    A set of eight stand-alone sample chambers with a common interface were constructed at LBNL for improved detection of alpha and fission decay chains over currently used designs. The stainless steel chambers (see Figure 1 for a schematic and Figure 2 for a photograph of a completed chamber) were constructed to allow for low background detection of a daughter event by removal of the sample following the detection of a parent event. This mother-daughter mode of operation has been utilized successfully with our Merry-go-Round (MG) detection system [Gregorich 1994].

  8. Test stand system for vacuum chambers

    NASA Technical Reports Server (NTRS)

    Newman, D. F. (Inventor)

    1973-01-01

    A test stand system for supporting test items in a vacuum chamber is described. The system consists of a frame adapted to conform to the inside of the vacuum chamber and supporting a central vertical shaft. The shaft rotates on bearings located at each end of the shaft. Several vertically spaced plates which fixed to the vertical shaft may be adjusted for height to support the test equipment as required. The test equipment may be rotated during tests without disturbing the vacuum by a manually actuated drive external to the vacuum chamber.

  9. Simple cloud chambers using gel ice packs

    NASA Astrophysics Data System (ADS)

    Kamata, Masahiro; Kubota, Miki

    2012-07-01

    Although cloud chambers are highly regarded as teaching aids for radiation education, school teachers have difficulty in using cloud chambers because they have to prepare dry ice or liquid nitrogen before the experiment. We developed a very simple and inexpensive cloud chamber that uses the contents of gel ice packs which can substitute for dry ice or liquid nitrogen. The gel can be frozen in normal domestic freezers, and can be used repeatedly by re-freezing. The tracks of alpha-ray particles can be observed continuously for about 20 min, and the operation is simple and easy.

  10. 30 CFR 77.305 - Access to drying chambers, hot gas inlet chambers and ductwork; installation and maintenance.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 30 Mineral Resources 1 2010-07-01 2010-07-01 false Access to drying chambers, hot gas inlet chambers and ductwork; installation and maintenance. 77.305 Section 77.305 Mineral Resources MINE SAFETY... drying chambers, hot gas inlet chambers and ductwork; installation and maintenance. Drying chambers,...

  11. 30 CFR 77.305 - Access to drying chambers, hot gas inlet chambers and ductwork; installation and maintenance.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 30 Mineral Resources 1 2012-07-01 2012-07-01 false Access to drying chambers, hot gas inlet chambers and ductwork; installation and maintenance. 77.305 Section 77.305 Mineral Resources MINE SAFETY... drying chambers, hot gas inlet chambers and ductwork; installation and maintenance. Drying chambers,...

  12. 30 CFR 77.305 - Access to drying chambers, hot gas inlet chambers and ductwork; installation and maintenance.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 30 Mineral Resources 1 2014-07-01 2014-07-01 false Access to drying chambers, hot gas inlet chambers and ductwork; installation and maintenance. 77.305 Section 77.305 Mineral Resources MINE SAFETY... drying chambers, hot gas inlet chambers and ductwork; installation and maintenance. Drying chambers,...

  13. 30 CFR 77.305 - Access to drying chambers, hot gas inlet chambers and ductwork; installation and maintenance.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 30 Mineral Resources 1 2011-07-01 2011-07-01 false Access to drying chambers, hot gas inlet chambers and ductwork; installation and maintenance. 77.305 Section 77.305 Mineral Resources MINE SAFETY... drying chambers, hot gas inlet chambers and ductwork; installation and maintenance. Drying chambers,...

  14. 30 CFR 77.305 - Access to drying chambers, hot gas inlet chambers and ductwork; installation and maintenance.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 30 Mineral Resources 1 2013-07-01 2013-07-01 false Access to drying chambers, hot gas inlet chambers and ductwork; installation and maintenance. 77.305 Section 77.305 Mineral Resources MINE SAFETY... drying chambers, hot gas inlet chambers and ductwork; installation and maintenance. Drying chambers,...

  15. 11. Detail view west from airlock chamber of typical refrigerator ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    11. Detail view west from airlock chamber of typical refrigerator door into Trophic Chamber. - Natick Research & Development Laboratories, Climatic Chambers Building, U.S. Army Natick Research, Development & Engineering Center (NRDEC), Natick, Middlesex County, MA

  16. Developing Cloud Chambers with High School Students

    NASA Astrophysics Data System (ADS)

    Ishizuka, Ryo; Tan, Nobuaki; Sato, Shoma; Zeze, Syoji

    The result and outcome of the cloud chamber project, which aims to develop a cloud chamber useful for science education is reported in detail. A project includes both three high school students and a teacher as a part of Super Science High School (SSH) program in our school. We develop a dry-ice-free cloud chamber using salt and ice (or snow). Technical details of the chamber are described. We also argue how the project have affected student's cognition, motivation, academic skills and behavior. The research project has taken steps of professional researchers, i.e., in planning research, applying fund, writing a paper and giving a talk in conferences. From interviews with students, we have learnt that such style of scientific activity is very effective in promoting student's motivation for learning science.

  17. Internal combustion engine with multiple combustion chambers

    SciTech Connect

    Gruenwald, D.J.

    1992-05-26

    This patent describes a two-cycle compression ignition engine. It comprises one cylinder, a reciprocable piston moveable in the cylinder, a piston connecting rod, a crankshaft for operation of the piston connecting rod, a cylinder head enclosing the cylinder, the upper surface of the piston and the enclosing surface of the cylinder head defining a cylinder clearance volume, a first combustion chamber and a second combustion chamber located in the cylinder head. This patent describes improvement in means for isolating the combustion process for one full 360{degrees} rotation of the crankshaft; wherein the combustion chambers alternatively provide for expansion of combustion products in the respective chambers into the cylinder volume near top dead center upon each revolution of the crankshaft.

  18. ORGANIC EMISSION MEASUREMENTS VIA SMALL CHAMBER TESTING

    EPA Science Inventory

    The paper discusses the measurement of organic emissions from a variety of indoor materials, using small (166 liter) environmental test chambers. The following materials were tested: adhesives, caulks, pressed wood products, floor waxes, paints, solid insecticides. For each mater...

  19. LDCM TIRS: Cracking open the chamber

    NASA Video Gallery

    Engineers at Goddard Space Flight Center inspect and move the Thermal Infrared Sensor (TIRS) after two months of testing in the thermal vacuum chamber. TIRS completed its first round of thermal vac...

  20. Effectiveness of Chamber Music Ensemble Experience

    ERIC Educational Resources Information Center

    Zorn, Jay D.

    1973-01-01

    This investigation was concerned with the effectiveness of chamber music ensemble experience for certain members of a ninth grade band and the evaluation of the effectiveness in terms of performing abilities, cognitive learnings, and attitude changes. (Author)

  1. Three dimensional thrust chamber life prediction

    NASA Technical Reports Server (NTRS)

    Armstrong, W. H.; Brogren, E. W.

    1976-01-01

    A study was performed to analytically determine the cyclic thermomechanical behavior and fatigue life of three configurations of a Plug Nozzle Thrust Chamber. This thrust chamber is a test model which represents the current trend in nozzle design calling for high performance coupled with weight and volume limitations as well as extended life for reusability. The study involved the use of different materials and material combinations to evaluate their application to the problem of low-cycle fatigue in the thrust chamber. The thermal and structural analyses were carried out on a three-dimensional basis. Results are presented which show plots of continuous temperature histories and temperature distributions at selected times during the operating cycle of the thrust chamber. Computed structural data show critical regions for low-cycle fatigue and the histories of strain within the regions for each operation cycle.

  2. How does a bubble chamber work?

    SciTech Connect

    Konstantinov, D.; Homsi, W.; Luzuriaga, J.; Su, C.K.; Weilert, M.A.; Maris, H.J.

    1998-11-01

    A charged particle passing through a bubble chamber produces a track of bubbles. The way in which these bubbles are produced has been a matter of some controversy. The authors consider the possibility that in helium and hydrogen bubble chambers the production of bubbles is primarily a mechanical process, rather than a thermal process as has often been assumed. The model the authors propose gives results which are in excellent agreement with experiment.

  3. Robust Acoustic Transducers for Bubble Chambers

    NASA Astrophysics Data System (ADS)

    Wells, Jonathan

    2015-04-01

    The PICO collaboration utilizes bubble chambers filled with various superheated liquids as targets for dark matter. Acoustic sensors have proved able to distinguish nuclear recoils from radioactive background on an event-by-event basis. We have recently produced a more robust transducer which should be able to operate for years, rather than months, in the challenging environment of a heated high pressure hydraulic fluid outside these chambers. Indiana University South Bend.

  4. Numerical simulation of magma chamber dynamics.

    NASA Astrophysics Data System (ADS)

    Longo, Antonella; Papale, Paolo; Montagna, Chiara Paola; Vassalli, Melissa; Giudice, Salvatore; Cassioli, Andrea

    2010-05-01

    Magma chambers are characterized by periodic arrivals of deep magma batches that give origin to complex patterns of magma convection and mixing, and modify the distribution of physical quantities inside the chamber. We simulate the transient, 2D, multi-component homogeneous dynamics in geometrically complex dyke+chamber systems, by means of GALES, a finite element parallel C++ code solving mass, momentum and energy equations for multi-component homogeneous gas-liquid (± crystals) mixtures in compressible-to-incompressible flow conditions. Code validation analysis includes several cases from the classical engineering literature, corresponding to a variety of subsonic to supersonic gas-liquid flow regimes (see http://www.pi.ingv.it/~longo/gales/gales.html). The model allows specification of the composition of the different magmas in the domain, in terms of ten major oxides plus the two volatile species H2O and CO2. Gas-liquid thermodynamics are modeled by using the compositional dependent, non-ideal model in Papale et al. (Chem.. Geol., 2006). Magma properties are defined in terms of local pressure, temperature, and composition including volatiles. Several applications are performed within domains characterized by the presence of one or more magma chambers and one or more dykes, with different geometries and characteristic size from hundreds of m to several km. In most simulations an initial compositional interface is placed at the top of a feeding dyke, or at larger depth, with the deeper magma having a lower density as a consequence of larger volatile content. The numerical results show complex patterns of magma refilling in the chamber, with alternating phases of magma ingression and magma sinking from the chamber into the feeding dyke. Intense mixing takes place in feeding dykes, so that the new magma entering the chamber is always a mixture of the deep and the initially resident magma. Buoyant plume rise occurs through the formation of complex convective

  5. Cloud chamber visualization of primary cosmic rays

    SciTech Connect

    Earl, James A.

    2013-02-07

    From 1948 until 1963, cloud chambers were carried to the top of the atmosphere by balloons. From these flights, which were begun by Edward P. Ney at the University of Minnesota, came the following results: discovery of heavy cosmic ray nuclei, development of scintillation and cherenkov detectors, discovery of cosmic ray electrons, and studies of solar proton events. The history of that era is illustrated here by cloud chamber photographs of primary cosmic rays.

  6. Engine Knock and Combustion Chamber Form

    NASA Technical Reports Server (NTRS)

    Zinner, Karl

    1939-01-01

    The present report is confined to the effect of the combustion chamber shape on engine knock from three angles, namely: 1) The uniformity of flame-front movement as affected by chamber design and position of the spark plug; 2) The speed of advance of the flame as affected by turbulence and vibrations; 3) The reaction processes in the residual charge as affected by the walls.

  7. High-pressure promoted combustion chamber

    NASA Technical Reports Server (NTRS)

    Rucker, Michelle A. (Inventor); Stoltzfus, Joel M. (Inventor)

    1991-01-01

    In the preferred embodiment of the promoted combusiton chamber disclosed herein, a thick-walled tubular body that is capable of withstanding extreme pressures is arranged with removable upper and lower end closures to provide access to the chamber for dependently supporting a test sample of a material being evaluated in the chamber. To facilitate the real-time analysis of a test sample, several pressure-tight viewing ports capable of withstanding the simulated environmental conditions are arranged in the walls of the tubular body for observing the test sample during the course of the test. A replaceable heat-resistant tubular member and replaceable flame-resistant internal liners are arranged to be fitted inside of the chamber for protecting the interior wall surfaces of the combustion chamber during the evaluation tests. Inlet and outlet ports are provided for admitting high-pressure gases into the chamber as needed for performing dynamic analyses of the test sample during the course of an evaluation test.

  8. The GODDESS ionization chamber: developing robust windows

    NASA Astrophysics Data System (ADS)

    Blanchard, Rose; Baugher, Travis; Cizewski, Jolie; Pain, Steven; Ratkiewicz, Andrew; Goddess Collaboration

    2015-10-01

    Reaction studies of nuclei far from stability require high-efficiency arrays of detectors and the ability to identify beam-like particles, especially when the beam is a cocktail beam. The Gammasphere ORRUBA Dual Detectors for Experimental Structure Studies (GODDESS) is made up of the Oak Ridge-Rutgers University Barrel Array (ORRUBA) of silicon detectors for charged particles inside of the gamma-ray detector array Gammasphere. A high-rate ionization chamber is being developed to identify beam-like particles. Consisting of twenty-one alternating anode and cathode grids, the ionization chamber sits downstream of the target chamber and is used to measure the energy loss of recoiling ions. A critical component of the system is a thin and robust mylar window which serves to separate the gas-filled ionization chamber from the vacuum of the target chamber with minimal energy loss. After construction, windows were tested to assure that they would not break below the required pressure, causing harm to the wire grids. This presentation will summarize the status of the ionization chamber and the results of the first tests with beams. This work is supported in part by the U.S. Department of Energy and National Science Foundation.

  9. Development of sputtered techniques for thrust chambers

    NASA Technical Reports Server (NTRS)

    Mullaly, J. R.; Hecht, R. J.; Schmid, T. E.; Torrey, C. T.

    1975-01-01

    Techniques and materials were developed and evaluated for the fabrication and coating of advanced, long life, regeneratively cooled thrust chambers. Materials were analyzed as fillers for sputter application of OFHC copper as a closeout layer to channeled inner structures; of the materials evaluated, aluminum was found to provide the highest bond strength and to be the most desirable for chamber fabrication. The structures and properties were investigated of thick sputtered OFHC copper, 0.15 Zr-Cu, Al2O3,-Cu, and SiC-Cu. Layered structures of OFHC copper and 0.15 Zr-Cu were investigated as means of improving chamber inner wall fatigue life. The evaluation of sputtered Ti-5Al-2.5Sn, NASA IIb-11, aluminum and Al2O3-Al alloys as high strength chamber outer jackets was performed. Techniques for refurbishing degraded thrust chambers with OFHC copper and coating thrust chambers with protective ZrO2 and graded ZrO2-copper thermal barrier coatings were developed.

  10. Expandable Purge Chambers Would Protect Cryogenic Fittings

    NASA Technical Reports Server (NTRS)

    Townsend, Ivan I., III

    2004-01-01

    Expandable ice-prevention and cleanliness-preservation (EIP-CP) chambers have been proposed to prevent the accumulation of ice or airborne particles on quick-disconnect (QD) fittings, or on ducts or tubes that contain cryogenic fluids. In the original application for which the EIP-CP chambers were conceived, there is a requirement to be able to disconnect and reconnect the QD fittings in rapid succession. If ice were to form on the fittings by condensation and freezing of airborne water vapor on the cold fitting surfaces, the ice could interfere with proper mating of the fittings, making it necessary to wait an unacceptably long time for the ice to thaw before attempting reconnection. By keeping water vapor away from the cold fitting surfaces, the EIP-CP chambers would prevent accumulation of ice, preserving the ability to reconnect as soon as required. Basically, the role of an EIP-CP chamber would be to serve as an enclosure for a flow of dry nitrogen gas that would keep ambient air away from QD cryogenic fittings. An EIP-CP chamber would be an inflatable device made of a fabriclike material. The chamber would be attached to an umbilical plate holding a cryogenic QD fitting.

  11. Designing an Active Target Test Projection Chamber

    NASA Astrophysics Data System (ADS)

    Koci, James; Tan Ahn Collaboration, Dr.; Nicolas Dixneuf Collaboration

    2015-10-01

    The development of instrumentation in nuclear physics is crucial for advancing our ability to measure the properties of exotic nuclei. One limitation of the use of exotic nuclei in experiment is their very low production intensities. Recently, detectors, called active-target dectectors, have been developed to address this issue. Active-target detectors use a gas medium to image charged-particle tracks that are emitted in nuclear reactions. Last semester, I designed a vacuum chamber to be used in developing Micro-Pattern Gas detectors that will upgrade the capabilities of an active-target detector called the Prototype AT-TPC. With the exterior of the chamber complete, I have now been using an electric field modeling program, Garfield, developed by CERN to design a field cage to be placed within the vacuum chamber. The field cage will be a box-like apparatus consisting of two parallel metal plates connected with a resistor chain and attached to wires wrapped between them. The cage will provide a uniform electric field within the chamber to drift electrons from nuclear reactions down to the detector in the bottom of the chamber. These signals are then amplified by a proportional counter, and the data is sent to a computer. For the long term, we would like to incorporate a Micro-Pattern Gas Detectors in the interior of the chamber and eventually use the AT-TPC to examine various nuclei. Dr. Ahn is my advising professor.

  12. Chamber for Growing and Observing Fungi

    NASA Technical Reports Server (NTRS)

    Pierson, Duane L.; Molina, Thomas C.

    2005-01-01

    A chamber has been designed to enable growth and observation of microcolonies of fungi in isolation from the external environment. Unlike prior fungus-growing apparatuses, this chamber makes it possible to examine a fungus culture without disrupting it. Partly resembling a small picture frame, the chamber includes a metal plate having a rectangular through-thethickness opening with recesses for a top and a bottom cover glass, an inlet for air, and an inlet for water. The bottom cover glass is put in place and held there by clips, then a block of nutrient medium and a moisture pad are placed in the opening. The block is inoculated, then the top cover glass is put in place and held there by clips. Once growth is evident, the chamber can be sealed with tape. Little (if any) water evaporates past the edges of the cover glasses, and, hence there is little (if any) need to add water. A microscope can be used to observe the culture through either cover glass. Because the culture is sealed in the chamber, it is safe to examine the culture without risking contamination. The chamber can be sterilized and reused.

  13. Magma chamber paradox: decompression upon replenishment

    NASA Astrophysics Data System (ADS)

    Papale, Paolo; Longo, Antonella; Montagna, Chiara Paola

    2013-04-01

    The invasion of active magma chambers by fresh magma of deeper provenance is invariably assumed to cause chamber pressurization. Pressure increase thus stands as an intuitive consequence of magma chamber replenishment. However, new numerical simulations demonstrate that pressure evolution is highly non-linear, and that decompression dominates when large density contrasts exist between injected and resident magmas. This apparent paradox originates from the compressible nature of volatile-rich magma and the dynamics of convection associated with injections of buoyant magma. While decompression can dominate in a shallow chamber, pressure increase develops in the connected deep regions of magma provenance. These results contradict classical views adopted to interpret observations at active as well as fossil magma chambers, and demonstrate that a simple reliance on intuition is insufficient: what may be perceived as a paradox - magma chamber decompression upon replenishment - is instead likely, and rooted in the complex physics that governs the multiphase, multi-component dynamics of magma transport in geometrically composite, spatially extended magmatic systems.

  14. Cyclic fatigue analysis of rocket thrust chambers. Volume 1: OFHC copper chamber low cycle fatigue

    NASA Technical Reports Server (NTRS)

    Miller, R. W.

    1974-01-01

    A three-dimensional finite element elasto-plastic strain analysis was performed for the throat section of a regeneratively cooled rocket combustion chamber. The analysis employed the RETSCP finite element computer program. The analysis included thermal and pressure loads, and the effects of temperature dependent material properties, to determine the strain range corresponding to the chamber operating cycle. The analysis was performed for chamber configuration and operating conditions corresponding to a hydrogen-oxygen combustion chamber which was fatigue tested to failure. The computed strain range at typical chamber operating conditions was used in conjunction with oxygen-free, high-conductivity (OHFC) copper isothermal fatigue test data to predict chamber low-cycle fatigue life.

  15. 12. View north of Tropic Chamber. Natick Research & ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    12. View north of Tropic Chamber. - Natick Research & Development Laboratories, Climatic Chambers Building, U.S. Army Natick Research, Development & Engineering Center (NRDEC), Natick, Middlesex County, MA

  16. 13. View south of Arctic Chamber. Natick Research & ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    13. View south of Arctic Chamber. - Natick Research & Development Laboratories, Climatic Chambers Building, U.S. Army Natick Research, Development & Engineering Center (NRDEC), Natick, Middlesex County, MA

  17. Effect of Al-mole fraction in Al{sub x}Ga{sub 1−x}N grown by MOCVD

    SciTech Connect

    Jayasakthi, M. Ramesh, R. Prabakaran, K. Loganathan, R. Kuppulingam, B. Balaji, M. Arivazhagan, P. Sankaranarayanan, S. Singh, Shubra Baskar, K.

    2014-04-24

    AlGaN/AlN layers were grown by metalorganic chemical vapor deposition (MOCVD) on sapphire substrates. The Al{sub x}Ga{sub 1−x}N layer composition was varied from 15% to 25%. The crystalline quality, thickness and aluminum (Al) composition of AlGaN were determined using high resolution X-ray diffraction (HRXRD). The growth rate decreases on increasing Al composition. Reciprocal space mapping (RSM) was used to estimate the strain and relaxation between AlGaN and AlN. The optical properties of AlGaN layers were investigated by room temperature Photoluminescence (PL). The AlGaN peak shifts towards lower wavelength with Al composition. The surface morphology of AlGaN was studied by atomic force microscopy (AFM). Root mean square (RMS) roughness values were found to be increased in AlGaN layers with composition.

  18. Modified pulse growth and misfit strain release of an AlN heteroepilayer with a Mg-Si codoping pair by MOCVD

    NASA Astrophysics Data System (ADS)

    Majid Soomro, Abdul; Wu, Chenping; Lin, Na; Zheng, Tongchang; Wang, Huachun; Chen, Hangyang; Li, Jinchai; Li, Shuping; Cai, Duanjun; Kang, Junyong

    2016-03-01

    We report the modified pulse growth method together with an alternating introduction of larger-radius impurity (Mg) for the quality improvement and misfit strain release of an AlN epitaxial layer by the metal-organic chemical vapour deposition (MOCVD) method. Various pulse growth methods were employed to control the migration of Al atoms on the substrate surface. The results showed that the pulse time and overlapping of V/III flux is closely related with the enhancement of the 2D and 3D growth mode. In order to reduce the misfit strain between AlN and sapphire, an impurity of larger atomic radius (e.g. Mg) was doped into the AlN lattice to minimize the rigidity of the AlN epilayer. It was found that the codoping of Mg-Si ultrathin layers could significantly minimize the residual strain as well as the density of threading dislocations.

  19. Pressure dependence of the photoluminescence from γ-In2Se3 thin films prepared using MOCVD with a single-source precursor

    NASA Astrophysics Data System (ADS)

    Choi, In Hwan; Park, Hyeon Jeong

    2014-05-01

    Single γ-phase In2Se3 films were prepared by using metal-organic chemical-vapor deposition(MOCVD) with a single-source precursor [(Me)2In( μ-SeMe)]2. The basic physical properties of the grown films were examined by using X-ray diffraction, Raman spectroscopy, and photoluminescence spectroscopy at room temperature. The pressure dependence of the photoluminescence spectrum of the In2Se3 films was measured at room temperature. At 1 atm, 2 PL peaks were observed, one at 1.88 eV due to a bound exciton transition and the other at 1.50 eV due to a bound-to-free transition. While the pressure coefficients, at pressures below 1.4 GPa were nearly zero, the pressure coefficients of both PL peaks at pressures above 1.4 GPa were -25 meV/GPa.

  20. The use of metalorganics in the preparation of semiconductor materials. VIII - Feasibility studies of the growth of Group III-Group V compounds of boron by MOCVD

    NASA Technical Reports Server (NTRS)

    Manasevit, H. M.; Hewitt, W. B.; Nelson, A. J.; Mason, A. R.

    1989-01-01

    The MOCVD growth of B-As and B-P films on Si, sapphire, and Si-on-sapphire substrates is described; in this process, trimethylborane (TMB) or triethylborane (TEB) is pyrolyzed in the presence of AsH3 or PH3 in an H2 atmosphere. The procedures employed are outlined, and the results are presented in graphs, tables, and micrographs. It is found that the growth rate of the primarily amorphous films is dependent on the TMB or TEB concentration but approximately constant for TEB and AsH3 at 550-900 C. The nominal compositions of films grown using TMB are given as B(12-16)As2 and B(1-1.3)P. Carbon impurities and significant stress, bowing, and crazing are observed in the films grown on Si substrates, with the highest carbon content in the films grown from TMB and PH3.

  1. High-speed growth of YBa2Cu3O7-δ superconducting films on multilayer-coated Hastelloy C276 tape by laser-assisted MOCVD

    NASA Astrophysics Data System (ADS)

    Zhao, Pei; Ito, Akihiko; Kato, Takeharu; Yokoe, Daisaku; Hirayama, Tsukasa; Goto, Takashi

    2013-05-01

    The high-speed epitaxial growth of YBa2Cu3O7-δ (YBCO) superconducting films on multilayer (CeO2/LaMnO3/MgO/Gd2Zr2O7)-coated Hastelloy C276 tape was demonstrated using laser-assisted metal-organic chemical vapour deposition (laser-assisted MOCVD). The preferred orientation of the YBCO films changed from a-axis to c-axis as the deposition temperature was increased from 769 to 913 K. The c-axis-oriented YBCO film exhibited a high critical temperature of 90 K and a high critical current density of 0.5 MA cm-2 even at a high deposition rate of 55 μm h-1.

  2. Growth condition dependence of Mg-doped GaN film grown by horizontal atmospheric MOCVD system with three layered laminar flow gas injection

    NASA Astrophysics Data System (ADS)

    Tokunaga, H.; Waki, I.; Yamaguchi, A.; Akutsu, N.; Matsumoto, K.

    1998-06-01

    We developed a novel atmospheric pressure horizontal MOCVD system (SR2000) for the growth of III-nitride film. This system was designed for high-speed gas flow in order to suppress thermal convection and undesirable reactant gas reaction. We have grown Mg-doped GaN films using SR2000. We studied the bis-cyclopentadienyl magnesium (Cp 2Mg) flow rate dependence and growth temperature ( Tg) dependence of Mg-doped GaN. As a result, we have obtained p-type GaN film with hole carrier density of 8×10 17 cm -3 with a mobility of 7.5 cm 2/(V s) at the growth condition with Cp 2Mg flow rate of 0.1 μmol/min at Tg of 1025°C.

  3. Control of carbon content in amorphous GeTe films deposited by plasma enhanced chemical vapor deposition (PE-MOCVD) for phase-change random access memory applications

    NASA Astrophysics Data System (ADS)

    Aoukar, M.; Szkutnik, P. D.; Jourde, D.; Pelissier, B.; Michallon, P.; Noé, P.; Vallée, C.

    2015-07-01

    Amorphous and smooth GeTe thin films are deposited on 200 mm silicon substrates by plasma enhanced—metal organic chemical vapor deposition (PE-MOCVD) using the commercial organometallic precursors TDMAGe and DIPTe as Ge and Te precursors, respectively. X-ray photoelectron spectroscopy (XPS) measurements show a stoichiometric composition of the deposited GeTe films but with high carbon contamination. Using information collected by Optical Emission Spectroscopy (OES) and XPS, the origin of carbon contamination is determined and the dissociation mechanisms of Ge and Te precursors in H2 + Ar plasma are proposed. As a result, carbon level is properly controlled by varying operating parameters such as plasma radio frequency power, pressure and H2 rate. Finally, GeTe films with carbon level as low as 5 at. % are obtained.

  4. CuPt-type ordering of MOCVD In{sub 0.49}Al{sub 0.51}P.

    SciTech Connect

    Kosel, T. H.; Hall, D. C.; Dupuis, R. D.; Heller, R. D.; Cook, R. E.

    2002-03-14

    CuPt-type ordering in In{sub 0.49}Al{sub 0.51}P is studied by TEM. The lattice-matched film was grown by MOCVD on a GaAs substrate oriented 10{sup o} off (001) towards [110], at 650 C and 25 nm/min. TEM [110] and [1{bar 1}0] cross-sections (XS) were made by wedge polishing and 2 kV Ar ion milling. In CuPt-type ordering of In{sub 0.52}Ga{sub 0.48}P, alternating In-Ga-In-Ga {l_brace}111{r_brace} planes of group III atoms produce 1/2 {bar 1}11 and 1/2 1{bar 1}1 order spots in the 110 SADP, while the [1{bar 1}0] SADP shows no order spots [1-3]. A few studies have reported this type of order in In{sub 0.49}Al{sub 0.51}P [4]. The 004 BF image of the [1{bar 1}0] XS in Fig. 1 shows uneven light/dark contrast modulation due to phase separation often observed in In{sub 0.52}Ga{sub 0.48}P. There are also light/dark layers marked ML parallel to the film growth plane; such unintentional multilayers have also been observed [5] but their origin is not understood. Order lamellae {approx}1.5 nm thick inclined at a shallow angle to the growth plane overlap the multilayer to produce Moire fringe contrast. Fig. 2 is a DF image showing the thin ordered domains in the [1{bar 1}0] XS, which are inclined at 12{sup o} to the growth plane and 2{sup o} to (001). Fig. 3a shows the absence of order spots in the [1{bar 1}0] SADP, while tilting 26.6{sup o} to [3{bar 1}0] reveals rows of order spots characteristic of CuPt ordering (Fig. 3b). The fact that the domains lie within {approx}2{sup o} of (001) shows that their orientation is crystallographically determined, while the fact that the ''multilayer'' is parallel to the growth plane rather than to (001) shows that it is not crystallographically determined. Most work does not describe domains in the [1{bar 1}0] XS, but Bellon et al. [1] commented that in a [1{bar 1}0] XS their In{sub 0.52}Ga{sub 0.48}P domains were exactly on (001) in a wafer 6{sup o} off (001) towards [110], consistent with our results. The domains and streaked order spots in

  5. Final report for NIF chamber dynamics studies

    SciTech Connect

    Burnham, A; Peterson, P F; Scott, J M

    1998-09-01

    The National Ignition Facility (NIF), a 1.8 MJ, 192 laser beam facility, will have anticipated fusion yields of up to 20 MJ from D-T pellets encased in a gold hohlraum target. The energy emitted from the target in the form of x rays, neutrons, target debris kinetic energy, and target shrapnel will be contained in a 5 m. radius spherical target chamber. various diagnostics will be stationed around the target at varying distances from the target. During each shot, the target will emit x rays that will vaporize nearby target facing surfaces including those of the diagnostics, the target positioner, and other chamber structures. This ablated vapor will be transported throughout the chamber, and will eventually condense and deposit on surfaces in the chamber, including the final optics debris shields. The research at the University of California at Berkeley relates primarily to the NIF chamber dynamics. The key design issues are the ablation of the chamber structures, transport of the vapor through the chamber and the condensation or deposition processes of those vaporized materials. An understanding of these processes is essential in developing a concept for protecting the fina optics debris shields from an excessive coating (> 10 A) of target debris and ablated material, thereby prolonging their lifetime between change-outs. At Berkeley, we have studied the physical issues of the ablation process and the effects of varying materials, the condensation process of the vaporized material, and design schemes that can lower the threat posed to the debris shields by these processes. The work or portions of the work completed this year have been published in several papers and a dissertation [l-5].

  6. Aging effect in the BESIII drift chamber

    NASA Astrophysics Data System (ADS)

    Ming-Yi, Dong; Qing-Lei, Xiu; Ling-Hui, Wu; Zhi, Wu; Zhong-Hua, Qin; Pin, Shen; Fen-Fen, An; Xu-Dong, Ju; Yi, Liu; Kai, Zhu; Qun, Ou-Yang; Yuan-Bo, Chen

    2016-01-01

    As the main tracking detector of BESIII, the drift chamber provides accurate measurements of the position and the momentum of the charged particles produced in e+e- collisions at BEPCII. After six years of operation, the drift chamber is suffering from aging problems due to huge beam-related background. The gains of the cells in the first ten layers show an obvious decrease, reaching a maximum decrease of about 29% for the first layer cells. Two calculation methods for the gain change (Bhabha events and accumulated charges with 0.3% aging ratio for inner chamber cells) give almost the same results. For the Malter effect encountered by the inner drift chamber in January 2012, about 0.2% water vapor was added to the MDC gas mixture to solve this cathode aging problem. These results provide an important reference for MDC operating high voltage settings and the upgrade of the inner drift chamber. Supported by the CAS Center for Excellence in Particle Physics (CCEPP)

  7. Chamber, Target and Final Focus Integrated Design

    SciTech Connect

    Moir, R.W.

    2000-03-03

    Liquid wall protection, which challenges chamber clearing, has such advantages it's Heavy Ion Fusion's (HIF) main line chamber design. Thin liquid protection from x rays is necessary to avoid erosion of structural surfaces and thick liquid makes structures behind 0.5 m of Flibe (7 mean free paths for 14 MeV neutrons), last the life of the plant. Liquid wall protection holds the promise of greatly increased economic competitiveness. Driver designers require {approx}200 beams to illuminate recent target designs from two sides. The illumination must be compatible with liquid wall protection. The ''best'' values for driver energy, gain, yield and pulse rate comes out of well-known trade-off studies. The chamber design is based on several key assumptions, which are to be proven before HIF can be shown to be feasible. The chamber R&D needed to reduce the unknowns and risks depend on resolving a few technical issues such as jet surface smoothness and rapid chamber clearing.

  8. Chamber, Target and Final Focus Integrated Design

    SciTech Connect

    Moir, R.W

    2000-03-22

    Liquid wall protection, which challenges chamber clearing, has such advantages it's Heavy Ion Fusion's (HIF) main line chamber design. Thin liquid protection from x rays is necessary to avoid erosion of structural surfaces and thick liquid makes structures behind 0.5 m of Flibe (7 mean free paths for 14 MeV neutrons), last the life of the plant. Liquid wall protection holds the promise of greatly increased economic competitiveness. Driver designers require {approx}200 beams to illuminate recent target designs from two sides. The illumination must be compatible with liquid wall protection. The ''best'' values for driver energy, gain, yield and pulse rate comes out of well-known trade-off studies. An integrated chamber design, yet to be made, depends on several key assumptions, which are to be proven before HIF can be shown to be feasible. The chamber R&D needed to reduce the unknowns and risks depend on resolving a few technical issues such as jet surface smoothness and rapid chamber clearing.

  9. Thermal Vacuum Chamber Repressurization with Instrument Purging

    NASA Technical Reports Server (NTRS)

    Woronowicz, Michael S.

    2014-01-01

    At the conclusion of cryogenic vacuum testing of the James Webb Space Telescope Optical Telescope Element Integrated Science Instrument Module (JWST-OTIS) in NASA Johnson Space Center’s (JSCs) thermal vacuum (TV) Chamber A, contamination control (CC) engineers are postulating that chamber particulate material stirred up by the repressurization process may be kept from falling into the Integrated Science Instrument Module (ISIM) interior to some degree by activating instrument purge flows over some initial period before opening the chamber valves. This manuscript describes development of a series of models designed to describe this process. The models are strung together in tandem with a fictitious set of conditions to estimate overpressure evolution from which net outflow velocity behavior may be obtained. Creeping flow assumptions are then used to determine the maximum particle size that may be kept suspended above the ISIM aperture, keeping smaller particles from settling within the instrument module.

  10. Chamber LIDAR measurements of aerosolized biological simulants

    NASA Astrophysics Data System (ADS)

    Brown, David M.; Thrush, Evan P.; Thomas, Michael E.; Siegrist, Karen M.; Baldwin, Kevin; Quizon, Jason; Carter, Christopher C.

    2009-05-01

    A chamber aerosol LIDAR is being developed to perform well-controlled tests of optical scattering characteristics of biological aerosols, including Bacillus atrophaeus (BG) and Bacillus thuringiensis (BT), for validation of optical scattering models. The 1.064 μm, sub-nanosecond pulse LIDAR allows sub-meter measurement resolution of particle depolarization ratio or backscattering cross-section at a 1 kHz repetition rate. Automated data acquisition provides the capability for real-time analysis or recording. Tests administered within the refereed 1 cubic meter chamber can provide high quality near-field backscatter measurements devoid of interference from entrance and exit window reflections. Initial chamber measurements of BG depolarization ratio are presented.

  11. Thermal Vacuum Chamber Repressurization with Instrument Purging

    NASA Technical Reports Server (NTRS)

    Woronowicz, Michael

    2016-01-01

    At the end of James Webb Space Telescope (JWST) OTIS (Optical Telescope Element-OTE-Integrated Science Instrument Module-ISIM) cryogenic vacuum testing in NASA Johnson Space Centers (JSCs) thermal vacuum (TV) Chamber A, contamination control (CC) engineers are mooting the idea that chamber particulate material stirred up by the repressurization process may be kept from falling into the ISIM interior to some degree by activating instrument purge flows over some initial period before opening the chamber valves. This memo describes development of a series of models designed to describe this process. These are strung together in tandem to estimate overpressure evolution from which net outflow velocity behavior may be obtained. Creeping flow assumptions are then used to determine the maximum particle size that may be kept suspended above the ISIM aperture, keeping smaller particles from settling within the instrument module.

  12. High temperature thrust chamber for spacecraft

    NASA Technical Reports Server (NTRS)

    Chazen, Melvin L. (Inventor); Mueller, Thomas J. (Inventor); Kruse, William D. (Inventor)

    1998-01-01

    A high temperature thrust chamber for spacecraft (20) is provided herein. The high temperature thrust chamber comprises a hollow body member (12) having an outer surface and an internal surface (16) defining the high temperature chamber (10). The body member (12) is made substantially of rhenium. An alloy (18) consisting of iridium and at least alloying metal selected of the group consisting of rhodium, platinum and palladium is deposited on at least a portion of the internal surface (16) of the body member (12). The iridium and the alloying metal are electrodeposited onto the body member (12). A HIP cycle is performed upon the body member (12) to cause the coating of iridium and the alloying metal to form the alloy (18) which protects the body member (12) from oxidation.

  13. Lightweight Chambers for Thrust Cell Applications

    NASA Technical Reports Server (NTRS)

    Elam, S.; Effinger, M.; Holmes, R.; Lee, J.; Jaskowiak, M.

    2000-01-01

    Traditional metals like steel and copper alloys have been used for many years to fabricate injector and chamber components of thruster assemblies. While the materials perform well, reducing engine weights would help existing and future vehicles gain performance and payload capability. It may now be possible to reduce current thruster weights up to 50% by applying composite materials. In this task, these materials are being applied to an existing thrust cell design to demonstrate new fabrication processes and potential weight savings. Two ceramic matrix composite (CMC) designs, three polymer matrix composite (PMC) designs, and two metal matrix composite (MMC) designs are being fabricated as small chamber demonstration units. In addition, a new alloy of copper, chrome, and niobium (Cu-8Cr-4Nb) is being investigated for thrust chamber liners since it offers higher strength and increased cycle life over traditional alloys. This new alloy is being used for the liner in each MMC and PMC demonstration unit. During June-August of 2000, hot-fire testing of each unit is planned to validate designs in an oxygen/hydrogen environment at chamber pressures around 850 psi. Although the weight savings using CMC materials is expected to be high, they have proven to be much harder to incorporate into chamber designs based on current fabrication efforts. However, the PMC & MMC concepts using the Cu-8Cr-4Nb liner are nearly complete and ready for testing. Additional efforts intend to use the PMC & MMC materials to fabricate a full size thrust chamber (60K lb(sub f) thrust class). The fabrication of this full size unit is expected to be complete by October 2000, followed by hot-fire testing in November-December 2000.

  14. Advanced technology application for combustion chamber concepts

    NASA Technical Reports Server (NTRS)

    Tygielski, Kathy S.

    1992-01-01

    NASA-Marshall is engaged in the development of an Advanced Main Combustion Chamber under the aegis of the Earth-to-Orbit Propulsion Technology Program. AMCC is to be a robust and highly reliable combustion-chamber prototype costing one-third as much as current designs of comparable performance; it will be associated with a reduction of fabrication time by one-half. Attention is presently given to the three component-manufacturing processes used: single-piece investment casting for the structural jacket and manifolds; vacuum plasma spraying, for the combustion liner, and an alternative, platelet-compounded liner.

  15. Cosmic muon detector using proportional chambers

    NASA Astrophysics Data System (ADS)

    Varga, Dezső; Gál, Zoltán; Hamar, Gergő; Sára Molnár, Janka; Oláh, Éva; Pázmándi, Péter

    2015-11-01

    A set of classical multi-wire proportional chambers was designed and constructed with the main purpose of efficient cosmic muon detection. These detectors are relatively simple to construct, and at the same time are low cost, making them ideal for educational purposes. The detector layers have efficiencies above 99% for minimum ionizing cosmic muons, and their position resolution is about 1 cm, that is, particle trajectories are clearly observable. Visualization of straight tracks is possible using an LED array, with the discriminated and latched signal driving the display. Due to the exceptional operating stability of the chambers, the design can also be used for cosmic muon telescopes.

  16. Almond test body. [for microwave anechoic chambers

    NASA Technical Reports Server (NTRS)

    Dominek, Allen K. (Inventor); Wood, Richard M. (Inventor); Gilreath, Melvin C. (Inventor)

    1989-01-01

    The invention is an almond shaped test body for use in measuring the performance characteristics of microwave anechoic chambers and for use as a support for components undergoing radar cross-section measurements. The novel aspect of this invention is its shape, which produces a large dynamic scattered field over large angular regions making the almond valuable for verifying the performance of microwave anechoic chambers. As a component mount, the almond exhibits a low return that does not perturb the measurement of the component and it simulates the backscatter characteristics of the component as if over an infinite ground plane.

  17. Sealed Plant-Growth Chamber For Clinostat

    NASA Technical Reports Server (NTRS)

    Brown, Christopher S.; Dreschel, Thomas W.

    1993-01-01

    Laboratory chamber for growing plants used to measure photosynthesis and respiration in simulated microgravity. Holds plant specimens while rotated on clinostat, see article, "Clinostat Delivers Power To Plant-Growth Cabinets" (KSC-11537). Provides way of comparing gas-exchange rates of plants rotated horizontally on clinostat with those of stationary or vertically rotated plants. Gas extracted for analysis without stopping clinostat. Chamber includes potlike base and cylindrical cover, both made of transparent acrylic pipe. Gasket forms seal between cover and bottom plate of base. Cover bolted to pot baseplate, which in turn bolted to clinostat.

  18. Quasi-Porous Plug With Vortex Chamber

    NASA Technical Reports Server (NTRS)

    Walsh, J. V.

    1985-01-01

    Pressure-letdown valve combines quasi-porous-plug and vortex-chamber in one controllable unit. Valve useful in fossil-energy plants for reducing pressures in such erosive two-phase process streams as steam/water, coal slurries, or combustion gases with entrained particles. Quasi-Porous Plug consists of plenums separated by perforated plates. Number or size of perforations increases with each succeeding stage to compensate for expansion. In Vortex Chamber, control flow varies to control swirl and therefore difference between inlet and outlet pressures.

  19. Space shuttle orbit maneuvering engine reusable thrust chamber program

    NASA Technical Reports Server (NTRS)

    Pauckert, R. P.; Yost, M. C.; Tobin, R. D.

    1973-01-01

    Tests were conducted on the regenerative cooled thrust chamber of the space shuttle orbit maneuvering engine. The conditions for the tests and the durations obtained are presented. The tests demonstrated thrust chamber operation over the nominal ranges of chamber pressure mixture ratio. Variations in auxiliary film coolant flowrate were also demonstrated. High pressure tests were conducted to demonstrate the thrust chamber operation at conditions approaching the design chamber pressure for the derivative space tug application.

  20. Detecting dark matter with scintillating bubble chambers

    NASA Astrophysics Data System (ADS)

    Zhang, Jianjie; Dahl, C. Eric; Jin, Miaotianzi; Baxter, Daniel

    2016-03-01

    Threshold based direct WIMP dark matter detectors such as the superheated bubble chambers developed by the PICO experiment have demonstrated excellent electron-recoil and alpha discrimination, excellent scalability, ease of change of target fluid, and low cost. However, the nuclear-recoil like backgrounds have been a limiting factor in their dark matter sensitivity. We present a new type of detector, the scintillating bubble chamber, which reads out the scintillation pulse of the scattering events as well as the pressure, temperature, acoustic traces, and bubble images as a conventional bubble chamber does. The event energy provides additional handle to discriminate against the nuclear-recoil like backgrounds. Liquid xenon is chosen as the target fluid in our prototyping detector for its high scintillation yield and suitable vapor pressure which simplifies detector complexity. The detector can be used as an R&D tool to study the backgrounds present in the current PICO bubble chambers or as a prototype for standalone dark matter detectors in the future. Supported by DOE Grant DE-SC0012161.

  1. Lifetime tests for MAC vertex chamber

    SciTech Connect

    Nelson, H.N.

    1986-07-01

    A vertex chamber for MAC was proposed to increase precision in the measurement of the B hadron and tau lepton lifetimes. Thin-walled aluminized mylar drift tubes were used for detector elements. A study of radiation hardness was conducted under the conditions of the proposed design using different gases and different operating conditions. (LEW)

  2. Isotopic zonations in silicic magma chambers

    SciTech Connect

    Johnson, C.M. )

    1989-12-01

    Many ash-flow tuffs are zoned in radiogenic isotope ratios, indicating that roofward assimilation of crust occurs in ash-flow magma chambers prior to eruption. Cases where relatively well constrained calculations may be made regarding the percentage of assimilation in the roof zone indicate that the percentage of assimilation often exceeds the percentage of phenocrysts in the tuffs. This relation, in addition to the fact that assimilation gradients are opposite to that of the percentage of phenocrysts, suggests that assimilation and crystallization in the silicic roof zones of crustal magma chambers are separated in time and space, and that these processes are best modeled as two-component mixing; true assimilation-fractional crystallization is probably restricted to the lower mafic parts. Most phenocrysts in the silicic upper parts of magma chambers crystallized after assimilation, providing minimum estimates of time between assimilation and eruption (1-100 yr). Preservation of monotonic isotopic gradients suggests that convection is minor in the upper parts of silicic magma chambers during the late stages of evolution.

  3. Miniature reaction chamber and devices incorporating same

    DOEpatents

    Mathies, Richard A.; Woolley, Adam T.

    2000-10-17

    The present invention generally relates to miniaturized devices for carrying out and controlling chemical reactions and analyses. In particular, the present invention provides devices which have miniature temperature controlled reaction chambers for carrying out a variety of synthetic and diagnostic applications, such as PCR amplification, nucleic acid hybridization, chemical labeling, nucleic acid fragmentation and the like.

  4. Multiphysics Nuclear Thermal Rocket Thrust Chamber Analysis

    NASA Technical Reports Server (NTRS)

    Wang, Ten-See

    2005-01-01

    The objective of this effort is t o develop an efficient and accurate thermo-fluid computational methodology to predict environments for hypothetical thrust chamber design and analysis. The current task scope is to perform multidimensional, multiphysics analysis of thrust performance and heat transfer analysis for a hypothetical solid-core, nuclear thermal engine including thrust chamber and nozzle. The multiphysics aspects of the model include: real fluid dynamics, chemical reactivity, turbulent flow, and conjugate heat transfer. The model will be designed to identify thermal, fluid, and hydrogen environments in all flow paths and materials. This model would then be used to perform non- nuclear reproduction of the flow element failures demonstrated in the Rover/NERVA testing, investigate performance of specific configurations and assess potential issues and enhancements. A two-pronged approach will be employed in this effort: a detailed analysis of a multi-channel, flow-element, and global modeling of the entire thrust chamber assembly with a porosity modeling technique. It is expected that the detailed analysis of a single flow element would provide detailed fluid, thermal, and hydrogen environments for stress analysis, while the global thrust chamber assembly analysis would promote understanding of the effects of hydrogen dissociation and heat transfer on thrust performance. These modeling activities will be validated as much as possible by testing performed by other related efforts.

  5. Simple chamber facilitates chemiluminescent detection of bacteria

    NASA Technical Reports Server (NTRS)

    Marts, E. C.; Wilkins, J. R.

    1970-01-01

    Test chamber enables rapid estimation of bacteria in a test sample through the reaction of luminol and an oxidant with the cytochrome C portion of certain species of bacteria. Intensity of the light emitted in the reaction is a function of the specific bacteria in the test sample.

  6. Wave Phenomena in an Acoustic Resonant Chamber

    ERIC Educational Resources Information Center

    Smith, Mary E.; And Others

    1974-01-01

    Discusses the design and operation of a high Q acoustical resonant chamber which can be used to demonstrate wave phenomena such as three-dimensional normal modes, Q values, densities of states, changes in the speed of sound, Fourier decomposition, damped harmonic oscillations, sound-absorbing properties, and perturbation and scattering problems.…

  7. Acoustical-Levitation Chamber for Metallurgy

    NASA Technical Reports Server (NTRS)

    Barmatz, M. B.; Trinh, E.; Wang, T. G.; Elleman, D. D.; Jacobi, N.

    1983-01-01

    Sample moved to different positions for heating and quenching. Acoustical levitation chamber selectively excited in fundamental and second-harmonic longitudinal modes to hold sample at one of three stable postions: A, B, or C. Levitated object quickly moved from one of these positions to another by changing modes. Object rapidly quenched at A or C after heating in furnace region at B.

  8. OUTDOOR SMOG CHAMBER EXPERIMENTS USING AUTOMOBILE EXHAUST

    EPA Science Inventory

    Outdoor smog chamber experiments using automobile exhaust were performed in this study. The purpose of the study was to provide a data base that modelers could use to develop new, improved mechanisms for use in the Empirical Kinetics Modeling Approach (EKMA). Thirty-three dual sm...

  9. Anterior Chamber Live Loa loa: Case Report.

    PubMed

    Kagmeni, G; Cheuteu, R; Bilong, Y; Wiedemann, P

    2016-01-01

    We reported a case of unusual intraocular Loa loa in a 27-year-old patient who presented with painful red eye. Biomicroscopy revealed a living and active adult worm in the anterior chamber of the right eye. After surgical extraction under local anesthesia, parasitological identification confirmed L. loa filariasis. PMID:27441005

  10. A reusable prepositioned ATP reaction chamber

    NASA Technical Reports Server (NTRS)

    Hoffman, D. G.

    1972-01-01

    Luminescence biometer detects presence of life by means of light-emitting chemical reaction of luciferin and luciferase with adenosine triphosphate (ATP) that occurs in all living cells. Amount of light in reaction chamber is measured to determine presence and extent of life.

  11. PAINT COATINGS: CONTROLLED FIELD AND CHAMBER EXPERIMENTS

    EPA Science Inventory

    To determine the impact of pollution levels on the weathering rates of coatings, laboratory chamber experiments and controlled field exposures at North Carolina and Ohio sites were conducted in such a manner to separate the contributions due to dry deposition, wet deposition, pre...

  12. Presenting Chamber Music to Young Children

    ERIC Educational Resources Information Center

    Smith, Terry Fonda

    2011-01-01

    The number of professional ensembles and organizations with dedicated outreach concerts has been steadily increasing over the past decade. More recently, educational concerts pairing chamber music with young children have been documented. The work presented in this article is a study in the efficacy and feasibility of this format. Various music…

  13. Try Chamber Music--Here's How.

    ERIC Educational Resources Information Center

    Rudaitis, Cheryl

    1995-01-01

    Profiles four middle school teachers maintaining early chamber music programs. The teachers advise varying degrees of musical competency before students begin the program, but all of them caution against starting too soon. They also stress the importance of purchasing early music scores and establishing rehearsal times. (MJP)

  14. Anterior Chamber Live Loa loa: Case Report

    PubMed Central

    Kagmeni, G.; Cheuteu, R.; Bilong, Y.; Wiedemann, P.

    2016-01-01

    We reported a case of unusual intraocular Loa loa in a 27-year-old patient who presented with painful red eye. Biomicroscopy revealed a living and active adult worm in the anterior chamber of the right eye. After surgical extraction under local anesthesia, parasitological identification confirmed L. loa filariasis. PMID:27441005

  15. Chamber for Aerosol Deposition of Bioparticles

    NASA Technical Reports Server (NTRS)

    Kern, Roger; Kirschner, Larry

    2008-01-01

    Laboratory apparatus is depicted that is a chamber for aerosol deposition of bioparticles on surfaces of test coupons. It is designed for primary use in inoculating both flat and three-dimensional objects with approximately reproducible, uniform dispersions of bacterial spores of the genus Bacillus so that the objects could be used as standards for removal of the spores by quantitative surface sampling and/or cleaning processes. The apparatus is also designed for deposition of particles other than bacterial spores, including fungal spores, viruses, bacteriophages, and standard micron-sized beads. The novelty of the apparatus lies in the combination of a controllable nebulization system with a settling chamber large enough to contain a significant number of test coupons. Several companies market other nebulizer systems, but none are known to include chambers for deposition of bioparticles to mimic the natural fallout of bioparticles. The nebulization system is an expanded and improved version of commercially available aerosol generators that include nebulizers and drying columns. In comparison with a typical commercial aerosol generator, this system includes additional, higher-resolution flowmeters and an additional pressure regulator. Also, unlike a typical commercial aerosol generator, it includes stopcocks for separately controlling flows of gases to the nebulizer and drying column. To maximize the degree of uniformity of dispersion of bioaerosol, the chamber is shaped as an axisymmetrical cylinder and the aerosol generator is positioned centrally within the chamber and aimed upward like a fountain. In order to minimize electric charge associated with the aerosol particles, the drying column is made of aluminum, the drying column is in direct contact with an aluminum base plate, and three equally spaced Po-210 antistatic strips are located at the exit end of the drying column. The sides and top of the chamber are made of an acrylic polymer; to prevent

  16. Four chamber pacing in dilated cardiomyopathy.

    PubMed

    Cazeau, S; Ritter, P; Bakdach, S; Lazarus, A; Limousin, M; Henao, L; Mundler, O; Daubert, J C; Mugica, J

    1994-11-01

    A 54-year-old man received a four chamber pacing system for severe congestive heart failure (NYHA functional Class IV). His ECG showed a left bundle branch block (200-msec QRS duration) with 200-msec PR interval, normal QRS axis, and 90-msec interatrial interval. An acute hemodynamic study with insertion of four temporary leads was performed prior to the implant, which demonstrated a significant increase in cardiac output and decrease of pulmonary capillary wedge pressure. A permanent pacemaker was implanted based on the encouraging results of the acute study. The right chamber leads were introduced by cephalic and subclavian approaches. The left atrium was paced with a coronary sinus lead, Medtronic SP 2188-58 model. An epicardial Medtronic 5071 lead was placed on the LV free wall. The four leads were connected to a standard bipolar DDD pacemaker, Chorus 6234. The two atrial leads were connected via a Y-connector to the atrial channel of the pacemaker with a bipolar pacing configuration. The two ventricular leads were connected in a similar fashion to the ventricular channel of the device. The right chamber leads were connected to the distal poles. The left chamber leads were connected to the proximal poles of the pacemaker. Six weeks later, the patient's clinical status improved markedly with a weight loss of 17 kg and disappearance of peripheral edema. His functional class was reduced to NYHA II. Four chamber pacing is technically feasible. In patients with evidence of interventricular dyssynchrony, this original pacing mode probably provides a mechanical activation sequence closer to the natural one.(ABSTRACT TRUNCATED AT 250 WORDS) PMID:7845801

  17. Test plan pressure fed thrust chamber technology

    NASA Technical Reports Server (NTRS)

    Dunn, Glenn

    1990-01-01

    Aerojet is developing the technology for the design of a reliable, low cost, efficient, and lightweight LOX/RP-1 pressure fed engine. This technology program is a direct result of Aerojet's liquid rocket booster (LRB) study and previous NASA studies that identified liquid engines using high bulk density hydrocarbon fuels as very attractive for a space transportation system (STS). Previous large thrust LOX/RP-1 engine development programs were characterized by costly development problems due to combustion instability damage. The combustion stability solution was typically obtained through trial and error methods of minimizing instability damage by degrading engine performance. The approach to this program was to utilize existing and newly developed combustion analysis models and design methodology to create a thrust chamber design with features having the potential of producing reliable and efficient operation. This process resulted in an engine design with a unique high thrust-per-element OFO triplet injector utilizing a low cost modular approach. Cost efficient ablative materials are baselined for the injector face and chamber. Technology demonstration will be accomplished through a hot fire test program using appropriately sized subscale hardware. This subscale testing will provide a data base to supplement the current industry data bank and to anchor and validate the applied analysis models and design methodology. Once anchored and validated, these analysis models and design methodology can be applied with greatly increased confidence to design and characterize a large scale pressure fed LOX/RP-1 thrust chamber. The objective of this test program is to generate a data base that can be used to anchor and validate existing analysis models and design methodologies and to provide early concept demonstration of a low cost, efficient LOX/RP-1 thrust chamber. Test conditions and hardware instrumentation were defined to provide data sufficient to characterize combustion

  18. Achievable field strength in reverberation chambers

    NASA Astrophysics Data System (ADS)

    Eulig, N.; Enders, A.; Krauthäuser, H. G.; Nitsch, J.

    2003-05-01

    Feldvariable Kammern (FVK, engl.: modestirred- chamber) werden unter anderem für EMV-Störfestigkeitsprüfungen verwendet. Ein häufig genanntes Argument, das die Einführung dieser Kammern als normgerechte Prüfumgebung vorantreiben soll, ist eine hohe Feldstärke, die im Vergleich zu anderen Testumgebungen mit relativ moderaten HF-Leistungen erreicht werden kann. Besonders für sicherheitskritische Geräte, wie Komponenten aus der Avionik- oder KFZ-Industrie, sind heutzutage Testfeldstärken von mehreren 100 V/m notwendig. Derart hohe Feldstärken können in Umgebungen, die ein ebenes Wellenfeld erzeugen oder nachbilden, nur mit großen HFLeistungen generiert werden. Durch die Resonanzeigenschaften einer FVK können demgegenüber mit sehr viel weniger Leistung und damit Verstärkeraufwand vergleichbare Werte der Feldstärke erzeugt werden. Allerdings sinkt mit zunehmendem Volumen die erreichbare Feldstärke bei gleicher Speiseleistung. Idealerweise sollen Feldvariable Kammern bei möglichst niedrigen Frequenzen für EMVTests nutzbar sein, was jedoch ein großes Kammervolumen erfordert. Das Problem, bei niedrigen Frequenzen hohe Feldstärken erzeugen zu können, relativiert deshalb den Vorteil von FVKn gegenüber bekannten Testumgebungen bei niedrigen Testfrequenzen. Der Posterbeitrag erläutert, welche Feldstärken in verschieden großen Feldvariablen Kammern beim Einspeisen einer bestimmten hochfrequenten Leistung erreicht werden können. Anhand dieser Ergebnisse wird aufgezeigt, oberhalb welcher Grenzfrequenz eine Anwendung von FVKn nur sinnvoll erscheint. Mode-stirred chambers (MSCs) can be used for radiated immunity tests in EMC testing. Advantageous compared to conventional test methods is the high field strength which can here be generated with less RF-Power. This point is often the main argument for pushing the standardization of MSCs as an other EMC testing environment. Especially for safety-critical electronic equipment like

  19. Metallic spherical anechoic chamber for antenna pattern measurement

    NASA Astrophysics Data System (ADS)

    Farahbakhsh, Ali; Khalaj-Amirhosseini, Mohammad

    2016-08-01

    Anechoic chambers are used for indoor antenna measurements. The common method of constructing an anechoic chamber is to cover all inside walls by the electromagnetic absorbers. In this paper, a fully metallic spherical chamber structure is presented in which the propagation of the electromagnetic waves inside the chamber is controlled and they are guided to an absorber. In the proposed method, an appropriate quiet zone is obtained, and unlike ordinary anechoic chambers, the absorber usage amount is reduced greatly. The performance of the chamber is evaluated by simulation. The results show that the proposed method could provide a useful technique for the indoor antenna measurements.

  20. Modelling new particle formation from Jülich plant atmosphere chamber and CERN CLOUD chamber measurements

    NASA Astrophysics Data System (ADS)

    Liao, Li; Boy, Michael; Mogensen, Ditte; Schobesberger, Siegfried; Franchin, Alessandro; Mentel, Thomas F.; Kleist, Einhard; Kiendler-Scharr, Astrid; Kulmala, Markku; dal Maso, Miikka

    2013-05-01

    An MALTE-BOX model is used to study the effects of oxidation of SO2 and BVOCs to new particle formation from Jülich Plant Atmosphere Chamber and CERN CLOUD chamber measurements. Several days of continuously measurements were chosen for the simulation. Our preliminary results show that H2SO4 is one of the critical compounds in nucleation process. Nucleation involving the oxidation of BVOCs shows better agreements with measurements.

  1. A new plant chamber facility PLUS coupled to the atmospheric simulation chamber SAPHIR

    NASA Astrophysics Data System (ADS)

    Hohaus, T.; Kuhn, U.; Andres, S.; Kaminski, M.; Rohrer, F.; Tillmann, R.; Wahner, A.; Wegener, R.; Yu, Z.; Kiendler-Scharr, A.

    2015-11-01

    A new PLant chamber Unit for Simulation (PLUS) for use with the atmosphere simulation chamber SAPHIR (Simulation of Atmospheric PHotochemistry In a large Reaction Chamber) has been build and characterized at the Forschungszentrum Jülich GmbH, Germany. The PLUS chamber is an environmentally controlled flow through plant chamber. Inside PLUS the natural blend of biogenic emissions of trees are mixed with synthetic air and are transferred to the SAPHIR chamber where the atmospheric chemistry and the impact of biogenic volatile organic compounds (BVOC) can be studied in detail. In PLUS all important enviromental parameters (e.g. temperature, PAR, soil RH etc.) are well-controlled. The gas exchange volume of 9.32 m3 which encloses the stem and the leafes of the plants is constructed such that gases are exposed to FEP Teflon film and other Teflon surfaces only to minimize any potential losses of BVOCs in the chamber. Solar radiation is simulated using 15 LED panels which have an emission strength up to 800 μmol m-2 s-1. Results of the initial characterization experiments are presented in detail. Background concentrations, mixing inside the gas exchange volume, and transfer rate of volatile organic compounds (VOC) through PLUS under different humidity conditions are explored. Typical plant characteristics such as light and temperature dependent BVOC emissions are studied using six Quercus Ilex trees and compared to previous studies. Results of an initial ozonolysis experiment of BVOC emissions from Quercus Ilex at typical atmospheric concentrations inside SAPHIR are presented to demonstrate a typical experimental set up and the utility of the newly added plant chamber.

  2. A new plant chamber facility, PLUS, coupled to the atmosphere simulation chamber SAPHIR

    NASA Astrophysics Data System (ADS)

    Hohaus, T.; Kuhn, U.; Andres, S.; Kaminski, M.; Rohrer, F.; Tillmann, R.; Wahner, A.; Wegener, R.; Yu, Z.; Kiendler-Scharr, A.

    2016-03-01

    A new PLant chamber Unit for Simulation (PLUS) for use with the atmosphere simulation chamber SAPHIR (Simulation of Atmospheric PHotochemistry In a large Reaction Chamber) has been built and characterized at the Forschungszentrum Jülich GmbH, Germany. The PLUS chamber is an environmentally controlled flow-through plant chamber. Inside PLUS the natural blend of biogenic emissions of trees is mixed with synthetic air and transferred to the SAPHIR chamber, where the atmospheric chemistry and the impact of biogenic volatile organic compounds (BVOCs) can be studied in detail. In PLUS all important environmental parameters (e.g., temperature, photosynthetically active radiation (PAR), soil relative humidity (RH)) are well controlled. The gas exchange volume of 9.32 m3 which encloses the stem and the leaves of the plants is constructed such that gases are exposed to only fluorinated ethylene propylene (FEP) Teflon film and other Teflon surfaces to minimize any potential losses of BVOCs in the chamber. Solar radiation is simulated using 15 light-emitting diode (LED) panels, which have an emission strength up to 800 µmol m-2 s-1. Results of the initial characterization experiments are presented in detail. Background concentrations, mixing inside the gas exchange volume, and transfer rate of volatile organic compounds (VOCs) through PLUS under different humidity conditions are explored. Typical plant characteristics such as light- and temperature- dependent BVOC emissions are studied using six Quercus ilex trees and compared to previous studies. Results of an initial ozonolysis experiment of BVOC emissions from Quercus ilex at typical atmospheric concentrations inside SAPHIR are presented to demonstrate a typical experimental setup and the utility of the newly added plant chamber.

  3. Convective Regimes in Crystallizing Basaltic Magma Chambers

    NASA Astrophysics Data System (ADS)

    Gilbert, A. J.; Neufeld, J. A.; Holness, M. B.

    2015-12-01

    Cooling through the chamber walls drives crystallisation in crustal magma chambers, resulting in a cumulate pile on the floor and mushy regions at the walls and roof. The liquid in many magma chambers, either the bulk magma or the interstitial liquid in the mushy regions, may convect, driven either thermally, due to cooling, or compositionally, due to fractional crystallization. We have constructed a regime diagram of the possible convective modes in a system containing a basal mushy layer. These modes depend on the large-scale buoyancy forcing characterised by a global Rayleigh number and the proportion of the chamber height constituting the basal mushy region. We have tested this regime diagram using an analogue experimental system composed of a fluid layer overlying a pile of almost neutrally buoyant inert particles. Convection in this system is driven thermally, simulating magma convection above and within a porous cumulate pile. We observe a range of possible convective regimes, enabling us to produce a regime diagram. In addition to modes characterised by convection of the bulk and interstitial fluid, we also observe a series of regimes where the crystal pile is mobilised by fluid motions. These regimes feature saltation and scouring of the crystal pile by convection in the bulk fluid at moderate Rayleigh numbers, and large crystal-rich fountains at high Rayleigh numbers. For even larger Rayleigh numbers the entire crystal pile is mobilised in what we call the snowglobe regime. The observed mobilisation regimes may be applicable to basaltic magma chambers. Plagioclase in basal cumulates crystallised from a dense magma may be a result of crystal mobilisation from a plagioclase-rich roof mush. Compositional convection within such a mush could result in disaggregation, enabling the buoyant plagioclase to be entrained in relatively dense descending liquid plumes and brought to the floor. The phenocryst load in porphyritic lavas is often interpreted as a

  4. Soil Flux Chamber Measurements with Five Species CRDS and New Realtime Chamber Flux Processor

    NASA Astrophysics Data System (ADS)

    Saad, N.; Alstad, K. P.; Arata, C.; Franz, P.

    2014-12-01

    Continuous soil flux chamber measurements remains a key tool for determining production and sequestration of direct and indirect greenhouse gases. The Picarro G2508 Cavity Ring-down Spectrometer has radically simplified soil flux studies by providing simultaneous measurements of five gases: CO2, CH4, N2O, NH3, and H2O, and by lending itself to field deployment. Successful use of the Picarro G2508 for continuous soil flux measurements in a variety of ecosystem types has already been demonstrated. Most recently, Picarro is developing a real-time processing software to simplify chamber measurements of soil flux with the G2508 CRDS. The new Realtime Chamber Flux Processor is designed to work with all chamber types and sizes, and provides real-time flux values of N2O, CO2 & CH4. The software features include chamber sequence table, flexible data tagging feature, ceiling concentration measurement shut-off parameter, user-defined run-time interval, temperature/pressure input for field monitoring and volumetric conversion, and manual flux measurement start/stop override. Realtime Chamber Flux Processor GUI interface is presented, and results from a variety of sampling designs are demonstrated to emphasize program flexibility and field capability.

  5. Diesel exhaust cleaner with burner vortex chamber

    SciTech Connect

    Riddel, J.W.

    1983-05-17

    A diesel engine exhaust cleaner and burner system includes at least one exhaust cleaner member with a filter positioned therein to effect removal of particulates from a stream of exhaust gas delivered thereto via an inlet manifold. A fuel burner supplied with fuel by a fuel nozzle is operatively associated with the inlet manifold to supply the necessary heat to effect incineration of particulates collected on the filter. A cyclone duct providing a vortex chamber therein is operatively positioned downstream of the fuel nozzle and is supplied with sufficient air so as to effect both the complete combustion of the fuel and the controlled incineration of the particulates by increasing the residence time of the fuel in the reaction region within the vortex chamber and also effecting a more uniform distribution of the heat of combustion across the inlet face of the filter for the uniform heating of the particulates thereon to their combustion temperature.

  6. Bubble chamber as a trace chemical detector

    SciTech Connect

    Luo, X.; McCreary, E.I.; Atencio, J.H.; McCown, A.W.; Sander, R.K.

    1998-08-01

    A novel concept for trace chemical analysis in liquid has been demonstrated. The technique utilizes light absorption in a superheated liquid. Although a superheated liquid is thermodynamically unstable, a high degree of superheating can be dynamically achieved for a short period of time. During this time the superheated liquid is extremely sensitive to boiling at nucleation sites produced by energy deposition. Observation of bubbles in the superheated liquid in some sense provides amplification of the initial energy deposition. Bubble chambers containing superheated liquids have been used to detect energetic particles; now a bubble chamber is used to detect a trace chemical in superheated liquid propane by observing bubble formation initiated by optical absorption. Crystal violet is used as a test case and can be detected at the subpart-per-10{sup 12} level by using a Nd:YAG laser. The mechanism for bubble formation and ideas for further improvement are discussed. {copyright} 1998 Optical Society of America

  7. Space station auxiliary thrust chamber technology

    NASA Technical Reports Server (NTRS)

    Senneff, J. M.

    1987-01-01

    A program to design, fabricate, and test a 50 lb sub f (222 N) thruster was undertaken to demonstrate the applicability of the reverse flow concept as an item of auxillary propulsion for the Space Station. The thruster was to operate at a mixture ratio (O/F) of 4, be capable of operating for 2 million lb sub f-seconds (8.896 million N-seconds) impulse with a chamber pressure of 75 psia (52N/sq cm) and a nozzle area ratio of 40. A successful demonstration of an (0/F) of 4 thruster, was followed by the design objective of operating at (O/F) of 8. The demonstration of this thruster resulted in the order of and additional (O/F) of 8 thruster chamber under the present NAS 3-24883 contract. The effort to fabricate and test the second (0/F) of 8 thruster is documented.

  8. Combustion interaction with radiation-cooled chambers

    NASA Technical Reports Server (NTRS)

    Rosenberg, S. D.; Jassowski, D. M.; Barlow, R.; Lucht, R.; Mccarty, K.

    1990-01-01

    Over 15 hours of thruster operation at temperatures between 1916 and 2246 C without failure or erosion has been demonstrated using iridium-coated rhenium chamber materials with nitrogen tetroxide/monomethylhydrazine propellants operating over a mixture ratio range of 1.60-2.05. Research is now under way to provide a basic understanding of the mechanisms which make high-temperature operation possible and to extend the capability to a wider range of conditions, including other propellant combinations and chamber materials. Techniques have been demonstrated for studying surface fracture phenomena. These include surface Raman and Auger for study of oxide formation, surface Raman and X-ray diffraction to determine the oxide phase, Auger to study oxide stoichiometry, and sputter Auger to study interdiffusion of alloy species.

  9. Miniature microwave powered steam sterilization chamber

    NASA Astrophysics Data System (ADS)

    Atwater, James E.; Dahl, Roger W.; Garmon, Frank C.; Lunsford, Teddie D.; Michalek, William F.; Wheeler, Richard R., Jr.; Sauer, Richard L.

    1997-10-01

    A small device for the rapid ultrahigh temperature sterilization of surfaces is described. Microwave power generated by a 2.45 GHz magnetron is delivered via coaxial cable to a silicon carbide block housed within the chamber. Small quantities of water or aqueous hydrogen peroxide are introduced into the chamber. Upon application of power, the liquid flashes to vapor and superheats producing temperatures to 300 °C. The hot vapor permeates the enclosed space and contacts all exposed surfaces. Complete microbial kill of >10 6 colony forming units of the spore forming thermophile, Bacillus stearothermophilus, has been demonstrated using a variety of temperatures and exposure times in both steady state and thermal pulse modes of operation.

  10. Compact Vapor Chamber Cools Critical Components

    NASA Technical Reports Server (NTRS)

    2015-01-01

    Advancements in the production of proton exchange membrane fuel cells have NASA considering their use as a power source for spacecraft and robots in future space missions. With SBIR funding from Glenn Research Center, Lancaster, Pennsylvania-based Thermacore Inc. developed strong, lightweight titanium vapor chambers to keep the fuel cells operating at optimum temperatures. The company is now selling the technology for cooling electronic components.

  11. High pressure hydrogen time projection chamber

    SciTech Connect

    Goulianos, K.

    1983-01-01

    We describe a high pressure hydrogen gas time projection chamber which consists of two cylindrical drift regions each 45 cm in diameter and 75 cm long. Typically, at 15 atm of H/sub 2/ with 2 kV/cm drift field and 7 kV on the 35..mu.. sense wires, the drift velocity is about 0.5 cm/..mu..sec and the spatial resolution +-200..mu...

  12. Comment on 'Proton beam monitor chamber calibration'.

    PubMed

    Palmans, Hugo; Vatnitsky, Stanislav M

    2016-09-01

    We comment on a recent article (Gomà et al 2014 Phys. Med. Biol. 59 4961-71) which compares different routes of reference dosimetry for the energy dependent beam monitor calibration in scanned proton beams. In this article, a 3% discrepancy is reported between a Faraday cup and a plane-parallel ionization chamber in the experimental determination of the number of protons per monitor unit. It is further claimed that similar discrepancies between calorimetry and ionization chamber based dosimetry indicate that [Formula: see text]-values tabulated for proton beams in IAEA TRS-398 might be overestimated. In this commentary we show, however, that this supporting argument misrepresents the evidence in the literature and that the results presented, together with published data, rather confirm that there exist unresolved problems with Faraday cup dosimetry. We also show that the comparison in terms of the number of protons gives a biased view on the uncertainty estimates for both detectors while the quantity of interest is absorbed dose to water or dose-area-product to water, even if a beam monitor is calibrated in terms of the number of protons. Gomà et al (2014 Phys. Med. Biol. 59 4961-71) also report on the discrepancy between cylindrical and plane-parallel ionization chambers and confirm experimentally that in the presence of a depth dose gradient, theoretical values of the effective point of measurement, or alternatively a gradient correction factor, account for the discrepancy. We believe this does not point to an error or shortcoming of IAEA TRS-398, which prescribes taking the centre of cylindrical ionization chambers as reference point, since it recommends reference dosimetry to be performed in the absence of a depth dose gradient. But these observations reveal that important aspects of beam monitor calibration in scanned proton beams are not addressed in IAEA TRS-398 given that those types of beams were not widely implemented at the time of its publication

  13. The fast Ice Nucleus chamber FINCH

    NASA Astrophysics Data System (ADS)

    Bundke, U.; Nillius, B.; Jaenicke, R.; Wetter, T.; Klein, H.; Bingemer, H.

    2008-11-01

    We present first results of our new developed Ice Nucleus (IN) counter FINCH from the sixth Cloud and Aerosol Characterization Experiment (CLACE 6) campaign at Jungfraujoch station, 3571 m asl. Measurements were made at the total and the ICE CVI inlet. Laboratory measurements of ice onset temperatures by FINCH are compared to those of the static diffusion chamber FRIDGE (FRankfurt Ice Deposition Freezing Experiment). Within the errors of both new instruments the results compare well to published data.

  14. Multi-chamber controllable heat pipe

    NASA Technical Reports Server (NTRS)

    Shlosinger, A. P. (Inventor)

    1970-01-01

    A temperature controllable heat pipe switching device is reported. It includes separate evaporating and condensing chambers interconnected by separate vapor flow and liquid return conduits. The vapor flow conduit can be opened or closed to the flow of vapor, whereas the liquid return conduit blocks vapor flow at all times. When the vapor flow path is open, the device has high thermal conductivity, and when the vapor flow path is blocked the device has low thermal conductivity.

  15. CFD Code Survey for Thrust Chamber Application

    NASA Technical Reports Server (NTRS)

    Gross, Klaus W.

    1990-01-01

    In the quest fo find analytical reference codes, responses from a questionnaire are presented which portray the current computational fluid dynamics (CFD) program status and capability at various organizations, characterizing liquid rocket thrust chamber flow fields. Sample cases are identified to examine the ability, operational condition, and accuracy of the codes. To select the best suited programs for accelerated improvements, evaluation criteria are being proposed.

  16. Visual-Inspection Probe For Cryogenic Chamber

    NASA Technical Reports Server (NTRS)

    Friend, Steve; Valenzuela, James; Yoshinaga, Jay

    1990-01-01

    Visual-inspection probe that resembles borescope enables observer at ambient temperature to view objects immersed in turbulent flow of liquid oxygen, liquid nitrogen, or other cryogenic fluid. Design of probe fairly conventional, except special consideration given to selection of materials and to thermal expansion to provide for expected range of operating temperatures. Penetrates wall of cryogenic chamber to provide view of interior. Similar probe illuminates scene. View displayed on video monitor.

  17. Image digitizer system for bubble chamber laser

    SciTech Connect

    Haggerty, H

    1986-12-08

    An IBM PC-based image digitizer system has been assembled to monitor the laser flash used for holography at the 15 foot bubble chamber. The hardware and the operating software are outlined. For an operational test of the system, an array of LEDs was flashed with a 10 microsecond pulse and the image was grabbed by one of the operating programs and processed. (LEW)

  18. Systematic approach to MOCVD processing chemistry for epitaxial Pb(Zr{sub x}Ti{sub 1-x})O{sub 3} thin films

    SciTech Connect

    Foster, C.M.; Jammy, R.; Bai, G.R.

    1996-12-31

    We have developed a simplified and systematic strategy to the MOCVD synthesis of single crystal thin films of Pb(Ti{sub x}Zr{sub 1-x})O{sub 3} for 0.1 {le}x{le}1. The films were prepared on epitaxial SrRuO{sub 3} buffered on SrTiO{sub 3} substrates by using tetraethyl lead, Pb(C{sub 2}H{sub 5}){sub 4}, zirconium t-butoxide, Zr(OC(CH{sub 3}){sub 3}){sub 4} and titanium isopropoxide, Ti(OCH(CH{sub 3}){sub 2}){sub 4} as metal-organic precursors. The synthesis of these single-crystalline films provided excellent model films to study the systematic variations in the optical, dielectric, polarization, and transport properties as a function of composition and the epitaxy induced modifications in the solid solution phase diagram of this system. High values of remnant polarization (30-55 {mu}C/cm{sup 2}) were observed at all ferroelectric compositions. The remnant polarization, coercive fields, and dielectric constant exhibited a clear dependence on composition. These films exhibited both high resistivity and dielectric strength ({approximately} 10{sup 13} {Omega}-cm at 100 kV/cm and >300 kV/cm, respectively).

  19. Properties variation with composition of single-crystal Pb(Zr{sub x}Ti{sub 1-x})O{sub 3} thin films prepared by MOCVD

    SciTech Connect

    Foster, C.M.; Bai, G.R.; Li, Z.; Jammy, R.; Wills, L.A.; Hiskes, R.

    1995-12-01

    Single-crystal thin films covering the full range of PZT 0{le}x{le}1 have been deposited by metal-organic chemical vapor deposition (MOCVD). The films were grown on epitaxial, RF-sputter-deposited SrRuO{sub 3} thin film electrodes on (001) SrTiO{sub 3} substrates. X-ray diffraction, energy-dispersive electron spectroscopy and optical waveguiding were used to characterize the crystalline structure, composition, refractive index, and film thickness. We found that the PZT films were single-crystalline for all compositions exhibiting cube-on-cube epitaxy with the substrate with very high degrees of crystallinity and orientation. We report the systematic variations in the optical, dielectric, polarization, and transport properties as a function of composition and the epitaxy-induced modifications in the solid-solution phase diagram of this system. These films exhibited electronic properties which showed clear systematic variations with composition. High values of remnant polarization (30--55 {mu}C/cm{sup 2}) were observed at all ferroelectric compositions. Unlike previous studies, the dielectric constant exhibited a clear dependence on composition with values ranging from 225--650. Coercive fields decreased with increasing Zr concentration to a minimum of 20 kV/cm at the (70/30) composition. In addition, these films exhibited both high resistivity and dielectric-breakdown strength ({approximately}10{sup 13} {Omega}-cm at 100 kV/cm and >300 kV/cm, respectively) without any compensative doping.

  20. MOCVD Growth of High-Quality and Density-Tunable GaAs Nanowires on ITO Catalyzed by Au Nanoparticles Deposited by Centrifugation.

    PubMed

    Wu, Dan; Tang, Xiaohong; Yoon, Ho Sup; Wang, Kai; Olivier, Aurelien; Li, Xianqiang

    2015-12-01

    High-quality and density-tunable GaAs nanowires (NWs) are directly grown on indium tin oxide (ITO) using Au nanoparticles (NPs) as catalysts by metal organic chemical vapor deposition (MOCVD). Au catalysts were deposited on ITO glass substrate using a centrifugal method. Compared with the droplet-only method, high-area density Au NPs were uniformly distributed on ITO. Tunable area density was realized through variation of the centrifugation time, and the highest area densities were obtained as high as 490 and 120 NP/μm(2) for 10- and 20-nm diameters of Au NPs, respectively. Based on the vapor-liquid-solid growth mechanism, the growth rates of GaAs NWs at 430 °C were 18.2 and 21.5 nm/s for the highest area density obtained of 10- and 20-nm Au NP-catalyzed NWs. The growth rate of the GaAs NWs was reduced with the increase of the NW density due to the competition of precursor materials. High crystal quality of the NWs was also obtained with no observable planar defects. 10-nm Au NP-induced NWs exhibit wurtzite structure whereas zinc-blende is observed for 20-nm NW samples. Controllable density and high crystal quality of the GaAs NWs on ITO demonstrate their potential application in hybrid a solar cell. PMID:26487507

  1. Electron microscopy study of MOCVD-grown TiO sub 2 thin films and TiO sub 2 /Al sub 2 O sub 3 interfaces

    SciTech Connect

    Gao, Y.; Merkle, K.L.; Chang, H.L.M.; Zhang, T.J.; Lam, D. J.

    1990-11-01

    TiO{sub 2} thin films grown on (11{bar 2}0) sapphire at 800{degree}C by the MOCVD technique have been characterized by transmission electron microscopy. The TiO{sub 2} thin films are single crystalline and have the rutile structure. The epitaxial orientation relationship between the TiO{sub 2} thin films (R) and the substrate (S) has been found to be: (101)(0{bar 1}0){sub R}{parallel}(11{bar 2}0)(0001){sub S}. Growth twins in the films are commonly observed with the twin plane {l brace}101{r brace} and twinning direction {l angle}011{r angle}. Detailed atomic structures of the twin boundaries and TiO{sub 2}/{alpha}-Al{sub 2}O{sub 3} interfaces have been investigated by high-resolution electron microscopy (HREM). When the interfaces are viewed in the direction of (0{bar 1}0){sub R}/(0001){sub S}, the interfaces are found to be structurally coherent in the direction of ({bar 1}01){sub R}/(1{bar 1}00){sub S}, in which the lattice mismatch at the interfaces is about 0.5%. 8 refs., 4 figs.

  2. Power recovery of radiation damaged MOCVD grown indium phosphide on silicon solar cells through argon-ion laser annealing. Master`s thesis

    SciTech Connect

    Boyer, L.L.

    1996-06-01

    This thesis reports the results of a laser annealing technique used to remove defect sites from radiation damaged indium phosphide on silicon MOCVD grown solar cells. This involves the illumination of damaged solar cells with a continuous wave laser to produce a large forward-biased current. The InP/Si cells were irradiated with 1 MeV electrons to a given fluence, and tested for degradation. Light from an argon laser was used to illuminate four cells with an irradiance of 2.5 W/sq cm, producing a current density 3 to 5 times larger than AMO conditions. Cells were annealed at 19 deg C with the laser and at 25 deg C under AMO conditions. Annealing under laser illumination of n/p-type cells resulted in recovery of 48%. P/n type cells lost 4 to 12% of the assumed degradaton. Annealing under AMO conditions resulted in power recovery of 70% in n/p type cells. P/n-type cells recovered approximately 16% of lost power. Results indicate that significant power recovery results from the annealing of defects within n/p type InP/Si solar cells.

  3. Self-assembling of strain-induced Y2O3 nanostructures grown on LaAlO3 by photo-assisted MOCVD

    NASA Astrophysics Data System (ADS)

    Li, Wei; Li, Shanwen; Li, Guoxing; Zhang, Baolin; Chou, Penchu

    2013-01-01

    Y2O3 nanodots were fabricated on vicinal substrate (1 0 0)-oriented LaAlO3 (LAO) by photo-assisted metalorganic chemical vapor deposition (PhA-MOCVD). Nucleation and growth processes of Y2O3 nanodots self-assembled as rows along the terraces of LAO were investigated with various growth parameters. It is found that density and size of Y2O3 nanodots can be tuned and well controlled by varying substrate temperature (Ts), oxygen partial pressure and growth time. At lower Ts, the morphologies of Y2O3 nanodots are characterized by small and dense solid cones. With elevating Ts, the dots gradually grow larger and sparser. This phenomenon could be illustrated by two competitive kinetic processes, i.e. surface diffusion of adatoms and yttrium desorption. Morphologies of these nanodots were also influenced by variation of oxygen partial pressure. To further discuss the growth kinetics, a more clearly quasi-linear distribution was obtained and the coarsening effect is modified by varying growth time.

  4. Growth study of Ge xSb yTe z deposited by MOCVD under nitrogen for non-volatile memory applications

    NASA Astrophysics Data System (ADS)

    Longo, M.; Salicio, O.; Wiemer, C.; Fallica, R.; Molle, A.; Fanciulli, M.; Giesen, C.; Seitzinger, B.; Baumann, P. K.; Heuken, M.; Rushworth, S.

    2008-11-01

    We report on the bubbler-type MOCVD growth of Ge xSb yTe z (GST) on SiO 2/Si substrates, potentially transferable to phase change memory (PCM) devices. Pure nitrogen was used as the process gas in order to reduce toxicity whilst increasing the simplicity of the process. This systematic study allowed the modification of the growth parameters on SiO 2 to move through initial sub-micrometric crystalline grain deposition on to lateral island growth. Temperature was observed to play a critical role in film quality with strong morphology and island shape/size changes for small thermal variations. Eventually, continuous layers of GST in the hcp phase and composition close to the 2:2:5 were studied. The deposition on different substrates was also investigated. Although crystal nucleation is still far from achieving the target step coverage required for uniform coating of patterned substrates, the electrical sheet resistance of GST films exhibited values corresponding to those expected for chalcogenide materials suitable to be integrated into PCM devices.

  5. Novel Neo-Pentoxide Precursors for MOCVD Thin Films of TiO(2) and ZrO(2).[1

    SciTech Connect

    Boyle, Timothy J.; Francisco, Laila P.; Gallegos, Jesus J.; Rodriguez, Mark A.; Ward, Timothy L.

    1999-07-14

    Two novel Group IV precursors, titanium (IV) neo-pentoxide, [Ti({mu}-ONep)(ONep){sub 3}]{sub 2} (l), and zirconium (IV) neo-pentoxide, [Zr({mu}-ONep)(ONep){sub 3}]{sub 2} (2), were reported to possess relatively high volatility at low temperatures. These compounds were therefore investigated as MOCVD precursors using a lamp-heated cold-wall CVD reactor and direct sublimation without carrier gas. The ONep derivatives proved to be competitive precursors for the production of thin films of the appropriate MO{sub 2} (M = Ti or Zr) materials in comparison to other metallo-organic precursors. Compound 1 was found to sublime at 120 C with a deposition rate of {approximately}0.350 {mu}m/min onto a substrate at 330 C forming the anatase phase with < 1% residual C found in the final film. Compound 2 was found to sublime at 160 C and deposited as crystalline material at 300 C with < 1% residual C found in the final film. A comparison to standard alkoxide and {beta}-diketonates is presented where appropriate.

  6. Optical properties of m-plane GaN grown on patterned Si(112) substrates by MOCVD using a two-step approach

    NASA Astrophysics Data System (ADS)

    Izyumskaya, N.; Okur, S.; Zhang, F.; Monavarian, M.; Avrutin, V.; Özgür, Ü.; Metzner, S.; Karbaum, C.; Bertram, F.; Christen, J.; Morkoç, H.

    2014-03-01

    Nonpolar m-plane GaN layers were grown on patterned Si (112) substrates by metal-organic chemical vapor deposition (MOCVD). A two-step growth procedure involving a low-pressure (30 Torr) first step to ensure formation of the m-plane facet and a high-pressure step (200 Torr) for improvement of optical quality was employed. The layers grown in two steps show improvement of the optical quality: the near-bandedge photoluminescence (PL) intensity is about 3 times higher than that for the layers grown at low pressure, and deep emission is considerably weaker. However, emission intensity from m-GaN is still lower than that of polar and semipolar (1 100 ) reference samples grown under the same conditions. To shed light on this problem, spatial distribution of optical emission over the c+ and c- wings of the nonpolar GaN/Si was studied by spatially resolved cathodoluminescence and near-field scanning optical microscopy.

  7. High-resolution X-ray diffraction study of laser lift-off AlGaN/GaN HEMTs grown by MOCVD method

    NASA Astrophysics Data System (ADS)

    Leung, K. K.; Chan, C. P.; Fong, W. K.; Pilkuhn, M.; Schweizer, H.; Surya, C.

    2007-01-01

    High-resolution X-ray diffraction (HRXRD) study of laser debonded AlGaN/GaN high electron mobility transistors (HEMTs), grown by metal-organic chemical vapor deposition (MOCVD), is performed. The lattice parameters as well as the in-plane and out-of-plane strains of the transistors before and after laser lift-off are determined from θ-2 θ X-ray diffraction spectra. The biaxial strains of the laser debonded HEMTs in a- and c-directions compared with the non-debonded HEMTs are extracted from the measured strain. The results clearly indicate stress relaxation in the device after laser debonding. Additionally, the full-width at half-maximum (FWHM) of the X-ray rocking curves are compared before and after laser debonding. The results do not indicate any increase in the dislocation densities in the heterojunction after laser debonding. This corroborates with the studies on the I-V characteristics of the devices, which also indicate no degradation in the electronic properties after laser debonding.

  8. Ring cusp discharge chamber performance optimization

    NASA Technical Reports Server (NTRS)

    Hiatt, J. M.; Wilbur, P. J.

    1985-01-01

    An experimental study of the effects of discharge chamber length and the locations of the anode, cathode and ring cusp within the chamber on the performance of an 8 cm dia. ring cusp thruster is described. As these lengths and positions are varied the changes induced in plasma ion energy costs, extracted ion fractions and ion beam profiles are measured. Results show that the anode may be positioned at any location along an 'optimum virtual anode' magnetic field line and minimum plasma ion energy costs will result. The actual location of this field line is related to a 'virtual cathode' magnetic field line that is defined by the cathode position. The magnetic field has to be such that the virtual anode field line intersects the grids at the outermost ring of grid holes to maximize the extracted ion fraction and flatten the ion beam profile. Discharge chamber lengths that were as small as possible in the test apparatus yielded the lowest extracted ion fractions.

  9. Basaltic injections into floored silicic magma chambers

    NASA Astrophysics Data System (ADS)

    Wiebe, R. A.

    Recent studies have provided compelling evidence that many large accumulations of silicic volcanic rocks erupted from long-lasting, floored chambers of silicic magma that were repeatedly injected by basaltic magma. These basaltic infusions are commonly thought to play an important role in the evolution of the silicic systems: they have been proposed as a cause for explosive silicic eruptions [Sparks and Sigurdsson, 1977], compositional variation in ash-flow sheets [Smith, 1979], mafic magmatic inclusions in silicic volcanic rocks [Bacon, 1986], and mixing of mafic and silicic magmas [Anderson, 1976; Eichelberger, 1978]. If, as seems likely, floored silicic magma chambers have frequently been invaded by basalt, then plutonic bodies should provide records of these events. Although plutonic evidence for mixing and commingling of mafic and silicic magmas has been recognized for many years, it has been established only recently that some intrusive complex originated through multiple basaltic injections into floored chambers of silicic magma [e.g., Wiebe, 1974; Michael, 1991; Chapman and Rhodes, 1992].

  10. SONTRAC: A solar neutron track chamber detector

    NASA Technical Reports Server (NTRS)

    Frye, G. M., Jr.; Jenkins, T. L.; Owens, A.

    1985-01-01

    The recent detection on the solar maximum mission (SMM) satellite of high energy neutrons emitted during large solar flares has provided renewed incentive to design a neutron detector which has the sensitivity, energy resolution, and time resolution to measure the neutron time and energy spectra with sufficient precision to improve our understanding of the basic flare processes. Over the past two decades a variety of neutron detectors has been flown to measure the atmospheric neutron intensity above 10 MeV and to search for solar neutrons. The SONTRAC (Solar Neutron Track Chamber) detector, a new type of neutron detector which utilizes n-p scattering and has a sensitivity 1-3 orders of magnitude greater than previous instruments in the 20-200 MeV range is described. The energy resolution is 1% for neutron kinetic energy, T sub n 50 MeV. When used with a coded aperture mask at 50 m (as would be possible on the space station) an angular resolution of approx. 4 arc sec could be achieved, thereby locating the sites of high energy nuclear interactions with an angular precision comparable to the existing x-ray experiments on SMM. The scintillation chamber is investigated as a track chamber for high energy physics, either by using arrays of scintillating optical fibers or by optical imaging of particle trajectories in a block of scintillator.

  11. Sperm Cell Dynamics in Shallow Chambers

    NASA Astrophysics Data System (ADS)

    Condat, Carlos; Marconi, Veronica; Guidobaldi, Alejandro; Giojalas, Laura; Silhanek, Alejandro; Jeyaram, Yogesh; Moshchalkov, Victor

    2015-03-01

    Self-propelled microorganisms are attracted to surfaces. This makes their dynamic behavior in restricted geometries very different from that observed in the bulk. Here we analyze the motion of spermatozoids confined to shallow chambers, investigating the nature of the cell trajectories and their accumulation near the side boundaries. Observed cell trajectories are composed of a succession of quasi-circular and quasi-linear segments. This suggests that the cells follow a path of intermittent trappings near the top and down surfaces separated by stretches of quasi-free motion near the center of the gap. Use of microstructured petal-shaped edges limits accumulation near the borders and contributes to increase the concentration in the chamber interior. System stabilization occurs over times of the order of minutes, which agrees well with a theoretical estimate that assumes that the cell mean-square displacement is largely due to the quasi-linear segments. Pure quasi-circular trajectories would require several hours to stabilize. Our estimates also indicate that stabilization proceeds 2.5 times faster in the rosette geometries than in the smooth-edged chambers, which is another practical reason to prefer the former.

  12. 11. Second floor, northwest chamber, south wall. Former passage to ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    11. Second floor, northwest chamber, south wall. Former passage to southwest chamber (door blocked off on far side) on left; closet on right. - Conner Homestead, House, Epping Road (State Route 101), Exeter, Rockingham County, NH

  13. INTERIOR VIEW, NORTH WALL OF THE SOUTHEAST BED CHAMBER. THE ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    INTERIOR VIEW, NORTH WALL OF THE SOUTHEAST BED CHAMBER. THE DOOR TO THE RIGHT OF THE FIREPLACE OPENS ONTO THE NORTHEAST BED CHAMBER - The Woodlands, 4000 Woodlands Avenue, Philadelphia, Philadelphia County, PA

  14. 17. View northwest of Tropic Chamber refrigeration equipment, in machine ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    17. View northwest of Tropic Chamber refrigeration equipment, in machine area. - Natick Research & Development Laboratories, Climatic Chambers Building, U.S. Army Natick Research, Development & Engineering Center (NRDEC), Natick, Middlesex County, MA

  15. 23. PHOTOCOPY OF PHOTOGRAPH. View west of Tropic Chamber refrigeration ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    23. PHOTOCOPY OF PHOTOGRAPH. View west of Tropic Chamber refrigeration equipment, ca. 1955. (Source: NRDEC). - Natick Research & Development Laboratories, Climatic Chambers Building, U.S. Army Natick Research, Development & Engineering Center (NRDEC), Natick, Middlesex County, MA

  16. Quartz crystals detect gas contaminants during vacuum chamber evacuation

    NASA Technical Reports Server (NTRS)

    Stephens, J. B.

    1967-01-01

    Piezoelectric quartz crystals detect condensable gas contaminants backstreaming into a vacuum chamber when a pump is evacuating the chamber. One crystal acts as a thermometer, the other detects mass change. They are energized by electronic equipment which records frequency changes.

  17. 16. View northwest of Arctic Chamber Worthington centrifugal compressor and ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    16. View northwest of Arctic Chamber Worthington centrifugal compressor and control panel, in machine area. - Natick Research & Development Laboratories, Climatic Chambers Building, U.S. Army Natick Research, Development & Engineering Center (NRDEC), Natick, Middlesex County, MA

  18. 18. View north of Tropic Chamber Worthington centrifugal compressor and ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    18. View north of Tropic Chamber Worthington centrifugal compressor and control panel, in machine area. - Natick Research & Development Laboratories, Climatic Chambers Building, U.S. Army Natick Research, Development & Engineering Center (NRDEC), Natick, Middlesex County, MA

  19. DESIGN, CONSTRUCTION, AND EVALUATION OF A CHAMBER FOR AEROBIOLOGY

    EPA Science Inventory

    A chamber was designed and constructed for aeromicrobiology applications. An ultraviolet (UV) radiation source was incorporated to sterilize the chamber between trials. Twelve bacterial species originally isolated from air samples and obtained from the American Type Culture Colle...

  20. DETAIL OF VACUUM PIPE OPENING WITHIN ALTITUDE CHAMBER R, FACING ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    DETAIL OF VACUUM PIPE OPENING WITHIN ALTITUDE CHAMBER R, FACING SOUTHEAST - Cape Canaveral Air Force Station, Launch Complex 39, Altitude Chambers, First Street, between Avenue D and Avenue E, Cape Canaveral, Brevard County, FL

  1. Andy Chambers Homestead, Chicken Coop, Saddle Shop, and Granary, looking ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    Andy Chambers Homestead, Chicken Coop, Saddle Shop, and Granary, looking northeast - Andy Chambers Homestead, 0.4 mile south of Antelope Flats Road on the east side of Mormon Row Road, Kelly, Teton County, WY

  2. Chamber Design For Slow Nucleation Protein Crystal Growth

    NASA Technical Reports Server (NTRS)

    Pusey, Marc Lee

    1995-01-01

    Multiple-chamber dialysis apparatus grows protein crystals on Earth or in microgravity with minimum of intervention by technician. Use of multiple chambers provides gradation of nucleation and growth rates.

  3. 7. Detail view west of Arctic Chamber wind tunnel shell ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    7. Detail view west of Arctic Chamber wind tunnel shell (typical) in east elevation. - Natick Research & Development Laboratories, Climatic Chambers Building, U.S. Army Natick Research, Development & Engineering Center (NRDEC), Natick, Middlesex County, MA

  4. 19. View northwest of Tropic Chamber reciprocal compressors (typical), in ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    19. View northwest of Tropic Chamber reciprocal compressors (typical), in machine area. - Natick Research & Development Laboratories, Climatic Chambers Building, U.S. Army Natick Research, Development & Engineering Center (NRDEC), Natick, Middlesex County, MA

  5. 1. View southeast of Climatic Chambers Building from roof of ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    1. View southeast of Climatic Chambers Building from roof of Research Building. - Natick Research & Development Laboratories, Climatic Chambers Building, U.S. Army Natick Research, Development & Engineering Center (NRDEC), Natick, Middlesex County, MA

  6. 21. PHOTOCOPY OF PHOTOGRAPH. view north of Tropic Chamber, ca. ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    21. PHOTOCOPY OF PHOTOGRAPH. view north of Tropic Chamber, ca. 1955. (Source: NRDEC). - Natick Research & Development Laboratories, Climatic Chambers Building, U.S. Army Natick Research, Development & Engineering Center (NRDEC), Natick, Middlesex County, MA

  7. Space Station Live: Historic Vacuum Chamber to Test Webb Telescope

    NASA Video Gallery

    NASA Public Affairs Officer Dan Huot recently visited Johnson Space Center’s 400,000 cubic foot vacuum chamber, Chamber A, and spoke with Mary Cerimele, the lab manager for this historic facility.

  8. Utilizing Chamber Data for Developing and Validating Climate Change Models

    NASA Technical Reports Server (NTRS)

    Monje, Oscar

    2012-01-01

    Controlled environment chambers (e.g. growth chambers, SPAR chambers, or open-top chambers) are useful for measuring plant ecosystem responses to climatic variables and CO2 that affect plant water relations. However, data from chambers was found to overestimate responses of C fluxes to CO2 enrichment. Chamber data may be confounded by numerous artifacts (e.g. sidelighting, edge effects, increased temperature and VPD, etc) and this limits what can be measured accurately. Chambers can be used to measure canopy level energy balance under controlled conditions and plant transpiration responses to CO2 concentration can be elucidated. However, these measurements cannot be used directly in model development or validation. The response of stomatal conductance to CO2 will be the same as in the field, but the measured response must be recalculated in such a manner to account for differences in aerodynamic conductance, temperature and VPD between the chamber and the field.

  9. 51. UPPER CHAMBER OF BISCUIT KILN No. 4, FROM THE ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    51. UPPER CHAMBER OF BISCUIT KILN No. 4, FROM THE SECOND FLOOR. ALL BRICK KILNS AT THE MORAVIAN POTTERY AND TILE WORKS HAD TWO CHAMBERS. WARE WAS STACKED IN THE LOWER CHAMBERS FOR FIRING AND THE UPPER CHAMBERS PROVIDED ACCESS TO FLUES AND DAMPERS FROM THE SECOND FLOOR. - Moravian Pottery & Tile Works, Southwest side of State Route 313 (Swamp Road), Northwest of East Court Street, Doylestown, Bucks County, PA

  10. Replenishment of magma chambers by light inputs

    NASA Astrophysics Data System (ADS)

    Huppert, Herbert E.; Sparks, R. Stephen J.; Whitehead, John A.; Hallworth, Mark A.

    1986-05-01

    Magma chambers, particularly those of basaltic composition, are often replenished by an influx of magma whose density is less than that of the resident magma. This paper describes the fundamental fluid mechanics involved in the replenishment by light inputs. If ρ denotes the uniform density of the resident magma and ρ — Δρ that of the input, the situation is described by the reduced gravity g' = gΔρ/ρ, the volume flux Q, and the viscosities of the resident and input magmas νe and νi, respectively. The (nondimensional) Reynolds numbers, Ree = (g'Q3)1/5/νe and Rei = (g'Q3)1/5/νi and chamber geometry then completely specify the system. For sufficiently low values of the two Reynolds numbers (each less than approximately 10), the input rises as a laminar conduit. For larger values of the Reynolds numbers, the conduit may break down and exhibit either a varicose or a meander instability and entrain some resident magma. At still larger Reynolds numbers, the flow will become quite unsteady and finally turbulent. The values of the Reynolds numbers at which these transitions occur have been documented by a series of experiments with water, glycerine, and corn syrup. If the input rises as a turbulent plume, significant entrainment of the resident magma can take place. The final spatial distribution of the mixed magma depends on the geometry of the chamber. If the chamber is much wider than it is high, the mixed magma forms a compositionally stratified region between the roof and a sharp front above uncontaminated magma. In the other geometrical extreme, the input magma is mixed with almost all of the resident magma. If the density of the resident magma is already stratified, the input plume may penetrate only part way into the chamber, even though its initial density is less than that of the lowest density resident magma. The plume will then intrude horizontally and form a hybrid layer at an intermediate depth. This provides a mechanism for preventing even

  11. Herds of methane chambers grazing bubbles

    NASA Astrophysics Data System (ADS)

    Grinham, Alistair; Dunbabin, Matthew

    2014-05-01

    Water to air methane emissions from freshwater reservoirs can be dominated by sediment bubbling (ebullitive) events. Previous work to quantify methane bubbling from a number of Australian sub-tropical reservoirs has shown that this can contribute as much as 95% of total emissions. These bubbling events are controlled by a variety of different factors including water depth, surface and internal waves, wind seiching, atmospheric pressure changes and water levels changes. Key to quantifying the magnitude of this emission pathway is estimating both the bubbling rate as well as the areal extent of bubbling. Both bubbling rate and areal extent are seldom constant and require persistent monitoring over extended time periods before true estimates can be generated. In this paper we present a novel system for persistent monitoring of both bubbling rate and areal extent using multiple robotic surface chambers and adaptive sampling (grazing) algorithms to automate the quantification process. Individual chambers are self-propelled and guided and communicate between each other without the need for supervised control. They can maintain station at a sampling site for a desired incubation period and continuously monitor, record and report fluxes during the incubation. To exploit the methane sensor detection capabilities, the chamber can be automatically lowered to decrease the head-space and increase concentration. The grazing algorithms assign a hierarchical order to chambers within a preselected zone. Chambers then converge on the individual recording the highest 15 minute bubbling rate. Individuals maintain a specified distance apart from each other during each sampling period before all individuals are then required to move to different locations based on a sampling algorithm (systematic or adaptive) exploiting prior measurements. This system has been field tested on a large-scale subtropical reservoir, Little Nerang Dam, and over monthly timescales. Using this technique

  12. MEASUREMENT OF SOIL RESPIRATION IN SITU: CHAMBER TECHNIQUES

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Chambers temporarily sealed to the soil surface are important and often the only means of measuring trace gas emissions to the atmosphere. However, such chamber measurements are not exempt from methodological problems. This review article identifies known sources of chamber-induced errors encounte...

  13. 30 CFR 57.7807 - Flushing the combustion chamber.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 30 Mineral Resources 1 2010-07-01 2010-07-01 false Flushing the combustion chamber. 57.7807... and Rotary Jet Piercing Rotary Jet Piercing-Surface Only § 57.7807 Flushing the combustion chamber. The combustion chamber of a jet drill stem which has been sitting unoperated in a drill hole shall...

  14. 21 CFR 878.5650 - Topical oxygen chamber for extremities.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Topical oxygen chamber for extremities. 878.5650... (CONTINUED) MEDICAL DEVICES GENERAL AND PLASTIC SURGERY DEVICES Therapeutic Devices § 878.5650 Topical oxygen chamber for extremities. (a) Identification. A topical oxygen chamber for extremities is a device that...

  15. 21 CFR 878.5650 - Topical oxygen chamber for extremities.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Topical oxygen chamber for extremities. 878.5650... (CONTINUED) MEDICAL DEVICES GENERAL AND PLASTIC SURGERY DEVICES Therapeutic Devices § 878.5650 Topical oxygen chamber for extremities. (a) Identification. A topical oxygen chamber for extremities is a device that...

  16. 21 CFR 878.5650 - Topical oxygen chamber for extremities.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Topical oxygen chamber for extremities. 878.5650... (CONTINUED) MEDICAL DEVICES GENERAL AND PLASTIC SURGERY DEVICES Therapeutic Devices § 878.5650 Topical oxygen chamber for extremities. (a) Identification. A topical oxygen chamber for extremities is a device...

  17. 21 CFR 878.5650 - Topical oxygen chamber for extremities.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Topical oxygen chamber for extremities. 878.5650... (CONTINUED) MEDICAL DEVICES GENERAL AND PLASTIC SURGERY DEVICES Therapeutic Devices § 878.5650 Topical oxygen chamber for extremities. (a) Identification. A topical oxygen chamber for extremities is a device that...

  18. 21 CFR 878.5650 - Topical oxygen chamber for extremities.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Topical oxygen chamber for extremities. 878.5650... (CONTINUED) MEDICAL DEVICES GENERAL AND PLASTIC SURGERY DEVICES Therapeutic Devices § 878.5650 Topical oxygen chamber for extremities. (a) Identification. A topical oxygen chamber for extremities is a device...

  19. Engineering analyses of large precision cathode strip chambers for GEM

    SciTech Connect

    Horvath, J.A.; Belser, F.C.; Pratuch, S.M.; Wuest, C.R.; Mitselmakher, G.; Gordeev, A.; Johnson, C.V. |; Polychronakos, V.A.; Golutvin, I.A.

    1993-10-21

    Structural analyses of large precision cathode strip chambers performed up to the date of this publication are documented. Mechanical property data for typical chamber materials are included. This information, originally intended to be an appendix to the {open_quotes}CSC Structural Design Bible,{close_quotes} is presented as a guide for future designers of large chambers.

  20. 30 CFR 57.7807 - Flushing the combustion chamber.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 30 Mineral Resources 1 2011-07-01 2011-07-01 false Flushing the combustion chamber. 57.7807... and Rotary Jet Piercing Rotary Jet Piercing-Surface Only § 57.7807 Flushing the combustion chamber. The combustion chamber of a jet drill stem which has been sitting unoperated in a drill hole shall...

  1. 7 CFR 58.423 - Cheese vacuumizing chamber.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 3 2012-01-01 2012-01-01 false Cheese vacuumizing chamber. 58.423 Section 58.423 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards....423 Cheese vacuumizing chamber. The vacuum chamber shall be satisfactorily constructed and...

  2. 7 CFR 58.423 - Cheese vacuumizing chamber.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 3 2011-01-01 2011-01-01 false Cheese vacuumizing chamber. 58.423 Section 58.423 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards....423 Cheese vacuumizing chamber. The vacuum chamber shall be satisfactorily constructed and...

  3. 7 CFR 58.423 - Cheese vacuumizing chamber.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 7 Agriculture 3 2014-01-01 2014-01-01 false Cheese vacuumizing chamber. 58.423 Section 58.423 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards....423 Cheese vacuumizing chamber. The vacuum chamber shall be satisfactorily constructed and...

  4. Anechoic chamber in industrial plants. [construction materials and structural design

    NASA Technical Reports Server (NTRS)

    Halpert, E.; Juncu, O.; Lorian, R.; Marfievici, D.; Mararu, I.

    1974-01-01

    A light anechoic chamber for routine acoustical measurements in the machine building industry is reported. The outer housing of the chamber consists of modules cast in glass fiber reinforced polyester resin; the inner housing consists of pyramidal modules cut out of sound absorbing slates. The parameters of this anechoic chamber facilitate acoustical measurements according to ISO and CAEM recommendations.

  5. An improved nutrient delivery system for SPAR chambers

    Technology Transfer Automated Retrieval System (TEKTRAN)

    The USDA-ARS Crop Systems and Global Change Laboratory (CSGCL), located at Beltsville, MD, maintains and operates 18 outdoor, natural sunlit plant growth chambers referred to as soil-plant-atmosphere research (SPAR) growth chambers. Each state-of-the-art SPAR chamber provides precise control over a...

  6. Cloud Chamber Activities for the High School Classroom.

    ERIC Educational Resources Information Center

    Perry, John Timothy; Sankey, Mary Ann

    1995-01-01

    Presents the idea that cloud chambers can be used by students as an experimental tool enabling them to conduct their own investigations on radiation. Provides detail regarding the construction of a cloud chamber and suggestions for student assignments that involve the cloud chamber. (DDR)

  7. Semiclosed-circuit atmosphere control in a portable recompression chamber

    NASA Technical Reports Server (NTRS)

    Riegel, P. S.; Caudy, D. W.

    1972-01-01

    A small portable recompression chamber is described that can be used both to treat a diver for decompression sickness or to transport him to a larger chamber complex. The device can be operated in either open circuit or semiclosed circuit atmospheres, permits two way conversation between patient and attendant, and uses an air injector for circulation of the chamber atmosphere.

  8. Characterization of a homemade ionization chamber for radiotherapy beams.

    PubMed

    Neves, Lucio P; Perini, Ana P; dos Santos, Gelson P; Xavier, Marcos; Khoury, Helen J; Caldas, Linda V E

    2012-07-01

    A homemade cylindrical ionization chamber was studied for routine use in therapy beams of (60)Co and X-rays. Several characterization tests were performed: leakage current, saturation, ion collection efficiency, polarity effect, stability, stabilization time, chamber orientation and energy dependence. All results obtained were within international recommendations. Therefore the homemade ionization chamber presents usefulness for routine dosimetric procedures in radiotherapy beams. PMID:22153889

  9. Theoretical Performance of Hydrogen-Oxygen Rocket Thrust Chambers

    NASA Technical Reports Server (NTRS)

    Sievers, Gilbert K.; Tomazic, William A.; Kinney, George R.

    1961-01-01

    Data are presented for liquid-hydrogen-liquid-oxygen thrust chambers at chamber pressures from 15 to 1200 pounds per square inch absolute, area ratios to approximately 300, and percent fuel from about 8 to 34 for both equilibrium and frozen composition during expansion. Specific impulse in vacuum, specific impulse, combustion-chamber temperature, nozzle-exit temperature, characteristic velocity, and the ratio of chamber-to-nozzle-exit pressure are included. The data are presented in convenient graphical forms to allow quick calculation of theoretical nozzle performance with over- or underexpansion, flow separation, and introduction of the propellants at various initial conditions or heat loss from the combustion chamber.

  10. New drift chamber for the Mark II at SLC

    SciTech Connect

    Hanson, G.G.

    1984-04-01

    A new cylindrical drift chamber is being constructed for the Mark II detector for use at the new SLAC Linear Collider. The design of the new chamber is based on a multi-sense-wire cell of the jet-chamber type. In addition to drift-time measurements, pulse height measurements from the sense wires will provide electron-hadron separation by dE/dx. The design and construction of the chamber, tests of prototypes, and chamber electronics are discussed. 7 references, 12 figures.

  11. Advanced Modified High Performance Synthetic Jet Actuator with Curved Chamber

    NASA Technical Reports Server (NTRS)

    Xu, Tian-Bing (Inventor); Su, Ji (Inventor); Jiang, Xiaoning (Inventor)

    2014-01-01

    The advanced modified high performance synthetic jet actuator with optimized curvature shape chamber (ASJA-M) is a synthetic jet actuator (SJA) with a lower volume reservoir or chamber. A curved chamber is used, instead of the conventional cylinder chamber, to reduce the dead volume of the jet chamber and increase the efficiency of the synthetic jet actuator. The shape of the curvature corresponds to the maximum displacement (deformation) profile of the electroactive diaphragm. The jet velocity and mass flow rate for the ASJA-M will be several times higher than conventional piezoelectric actuators.

  12. Outgassing measurement of the aluminum alloy UHV chamber

    NASA Technical Reports Server (NTRS)

    Miyamoto, M.; Itoh, T.; Komaki, S.; Narushima, K.; Ishimaru, H.

    1986-01-01

    A large vacuum chamber (580 mm diameter) was fabricated from an aluminum alloy surface treated by a special process normally used on small chambers. The chamber was tested unbaked and baked at various temperatures, pressures, and holding periods. The chamber was filled with N2 gas, and the outgassing rate was measured after one hour. Then the ultimate pressure was measured. Outgassing rates for baked and unbaked groups were compared. It is concluded that the same surface treatment technique can be used on both large and small chambers produced by the same special extrusion process.

  13. Advanced photon source experience with vacuum chambers for insertion devices

    SciTech Connect

    Hartog, P.D.; Grimmer, J.; Xu, S.; Trakhtenberg, E.; Wiemerslage, G.

    1997-08-01

    During the last five years, a new approach to the design and fabrication of extruded aluminum vacuum chambers for insertion devices was developed at the Advanced Photon Source (APS). With this approach, three different versions of the vacuum chamber, with vertical apertures of 12 mm, 8 mm, and 5 mm, were manufactured and tested. Twenty chambers were installed into the APS vacuum system. All have operated with beam, and 16 have been coupled with insertion devices. Two different vacuum chambers with vertical apertures of 16 mm and 11 mm were developed for the BESSY-II storage ring and 3 of 16 mm chambers were manufactured.

  14. New central drift chamber for the MARK II at SLC

    SciTech Connect

    Bartelt, J.E.

    1986-09-01

    A new central drift chamber has been constructed for the Mark II detector for use at the new SLAC Linear Collider (SLC). The design of the chamber is based on a multi-sense-wire cell of the jet chamber type. In addition to drift-time measurements, pulse-height measurements from the sense wires provide electron-hadron separation by dE/dx. The chamber has been tested in operation at PEP before its move to the SLC. The design and construction are described, and measurements from the new chamber are presented.

  15. Finite Element Analysis of Reverberation Chambers

    NASA Technical Reports Server (NTRS)

    Bunting, Charles F.; Nguyen, Duc T.

    2000-01-01

    The primary motivating factor behind the initiation of this work was to provide a deterministic means of establishing the validity of the statistical methods that are recommended for the determination of fields that interact in -an avionics system. The application of finite element analysis to reverberation chambers is the initial step required to establish a reasonable course of inquiry in this particularly data-intensive study. The use of computational electromagnetics provides a high degree of control of the "experimental" parameters that can be utilized in a simulation of reverberating structures. As the work evolved there were four primary focus areas they are: 1. The eigenvalue problem for the source free problem. 2. The development of a complex efficient eigensolver. 3. The application of a source for the TE and TM fields for statistical characterization. 4. The examination of shielding effectiveness in a reverberating environment. One early purpose of this work was to establish the utility of finite element techniques in the development of an extended low frequency statistical model for reverberation phenomena. By employing finite element techniques, structures of arbitrary complexity can be analyzed due to the use of triangular shape functions in the spatial discretization. The effects of both frequency stirring and mechanical stirring are presented. It is suggested that for the low frequency operation the typical tuner size is inadequate to provide a sufficiently random field and that frequency stirring should be used. The results of the finite element analysis of the reverberation chamber illustrate io-W the potential utility of a 2D representation for enhancing the basic statistical characteristics of the chamber when operating in a low frequency regime. The basic field statistics are verified for frequency stirring over a wide range of frequencies. Mechanical stirring is shown to provide an effective frequency deviation.

  16. Streamer studies in Resistive Plate Chambers

    NASA Astrophysics Data System (ADS)

    Denni, U.; Felici, G.; Frani, M. A.; Mengucci, A.; Papalino, G.; Spinetti, M.; Paoloni, A.

    2011-06-01

    Resistive Plate Chambers (RPCs) are widely used in high energy physics. While avalanche mode operation is mandatory in high rate environments (ATLAS and CMS experiments at LHC), streamer mode operation is often preferred in low rate applications because of the high signal amplitude. Typical mixtures for streamer operation are composed of Argon, Tetrafluoroethane and Isobutane, with additions of SF 6 below 1% to reduce the charge delivered in the gas. In this paper, results about the streamer properties observed with different mixtures are presented.

  17. Indian LSSC (Large Space Simulation Chamber) facility

    NASA Technical Reports Server (NTRS)

    Brar, A. S.; Prasadarao, V. S.; Gambhir, R. D.; Chandramouli, M.

    1988-01-01

    The Indian Space Agency has undertaken a major project to acquire in-house capability for thermal and vacuum testing of large satellites. This Large Space Simulation Chamber (LSSC) facility will be located in Bangalore and is to be operational in 1989. The facility is capable of providing 4 meter diameter solar simulation with provision to expand to 4.5 meter diameter at a later date. With such provisions as controlled variations of shroud temperatures and availability of infrared equipment as alternative sources of thermal radiation, this facility will be amongst the finest anywhere. The major design concept and major aspects of the LSSC facility are presented here.

  18. Carbon copy deaths: carbon monoxide gas chamber.

    PubMed

    Patel, F

    2008-08-01

    The news media can exert a powerful influence over suicidal behaviour. It has been observed that like-minded individuals are able to preplan a group suicide method using modern communication technology in the form of websites and online chatrooms and mobile phone texting. A case of carbon monoxide (CO) poisoning is presented to illustrate the recent phenomenon of cyber suicides by suffocation from a burning barbecue (charcoal burner) in 'gas chamber' conversions. Although barbecues (BBQ) are very popular in Britain and widely available, there have been relatively few reported cases of copycat deaths from CO gas suffocation. PMID:18586213

  19. Vacuum chamber for containing particle beams

    DOEpatents

    Harvey, A.

    1985-11-26

    A vacuum chamber for containing a charged particle beam in a rapidly changing magnetic environment comprises a ceramic pipe with conducting strips oriented along the longitudinal axis of the pipe and with circumferential conducting bands oriented perpendicular to the longitudinal axis but joined with a single longitudinal electrical connection. When both strips and bands are on the outside of the ceramic pipe, insulated from each other, a high-resistance conductive layer such as nickel can be coated on the inside of the pipe.

  20. Vacuum chamber for containing particle beams

    DOEpatents

    Harvey, Alexander

    1987-01-01

    A vacuum chamber for containing a charged particle beam in a rapidly changing magnetic environment comprises a ceramic pipe with conducting strips oriented along the longitudinal axis of the pipe and with circumferential conducting bands oriented perpendicular to the longitudinal axis but joined with a single longitudinal electrical connection. When both strips and bands are on the outside of the ceramic pipe, insulated from each other, a high-resistance conductive layer, such as nickel can be coated on the inside of the pipe.

  1. Sensing circuits for multiwire proportional chambers

    NASA Technical Reports Server (NTRS)

    Peterson, H. T.; Worley, E. R.

    1977-01-01

    Integrated sensing circuits were designed, fabricated, and packaged for use in determining the direction and fluence of ionizing radiation passing through a multiwire proportional chamber. CMOS on sapphire was selected because of its high speed and low power capabilities. The design of the proposed circuits is described and the results of computer simulations are presented. The fabrication processes for the CMOS on sapphire sensing circuits and hybrid substrates are outlined. Several design options are described and the cost implications of each discussed. To be most effective, each chip should handle not more than 32 inputs, and should be mounted on its own hybrid substrate.

  2. Condensate Recycling in Closed Plant Growth Chambers

    NASA Technical Reports Server (NTRS)

    Bledsoe, J. O.; Sager, J. C.; Fortson, R. E.

    1994-01-01

    Water used in the the Controlled Ecological Life Support System (CELSS) Breadboard Project at the Kennedy Space Center is being recycled. Condensation is collected in the air ducts, filtered and deionized, and resupplied to the system for nutrient solutions, supplemental humidification, solvents and diluents. While the system functions well from a process control standpoint, precise and accurate tracking of water movement through the system to answer plant physiological questions is not consistent. Possible causes include hardware errors, undetected vapor loss from chamber leakage, and unmeasured changes in water volume in the plant growth trays.

  3. Review of isothermal haze chamber performance

    NASA Technical Reports Server (NTRS)

    Fitzgerald, J. W.; Rogers, C. F.; Hudson, J. G.

    1981-01-01

    The theory of this method of characterizing cloud condensation nuclei (CCN) over the critical supersaturation range of about 0.01% to 0.2% was reviewed, and guidelines for the design and operation of IHC's are given. IHC data are presented and critically analyzed. Two of the four IHC's agree to about 40% over the entire range of critical. a third chamber shows similar agreement with the first two over the lower part of the critical supersaturation range but only a factor of two agreement at higher supersaturation. Some reasons for the discrepancies are given.

  4. Drift Chamber Alignment using Cosmic Rays

    SciTech Connect

    Kotwal, Ashutosh V.; Hays, Christopher P.

    2014-05-07

    The Collider Detector at Fermilab (CDF) is a general-purpose experimental apparatus with an inner tracking detector for measuring charged particles, surrounded by a calorimeter for measurements of electromagnetic and hadronic showers, and a muon detector system. We present a technique for, and results of, a precise relative alignment of the drift chamber wires of the CDF tracker. This alignment has been an important component of the track momentum calibration, which is the basis for the charged-lepton calibration for the measurement of the W boson mass at CDF.

  5. A 'breadboard' biomass production chamber for CELSS

    NASA Technical Reports Server (NTRS)

    Prince, Ralph P.; Knott, William M., III; Hilding, Suzanne E.; Mack, Tommy L.

    1987-01-01

    The Breadboard Project of the Controlled Ecological Life Support System (CELSS) Program is the first attempt by NASA to integrate the primary components of a bioregenerative life support system into a functioning system. The central component of this project is a Biomass Production Chamber (BPC). The BPC is under construction, and when finished will be sealed for the study of the flux of gases, liquids, and solids through the production module of a CELSS. Features of the CELSS breadboard facility will be covered as will design requirements for the BPC. Cultural practices developed for wheat for the BPC wil be discussed.

  6. Liquid Engine Design: Effect of Chamber Dimensions on Specific Impulse

    NASA Technical Reports Server (NTRS)

    Hoggard, Lindsay; Leahy, Joe

    2009-01-01

    Which assumption of combustion chemistry - frozen or equilibrium - should be used in the prediction of liquid rocket engine performance calculations? Can a correlation be developed for this? A literature search using the LaSSe tool, an online repository of old rocket data and reports, was completed. Test results of NTO/Aerozine-50 and Lox/LH2 subscale and full-scale injector and combustion chamber test results were found and studied for this task. NASA code, Chemical Equilibrium with Applications (CEA) was used to predict engine performance using both chemistry assumptions, defined here. Frozen- composition remains frozen during expansion through the nozzle. Equilibrium- instantaneous chemical equilibrium during nozzle expansion. Chamber parameters were varied to understand what dimensions drive chamber C* and Isp. Contraction Ratio is the ratio of the nozzle throat area to the area of the chamber. L is the length of the chamber. Characteristic chamber length, L*, is the length that the chamber would be if it were a straight tube and had no converging nozzle. Goal: Develop a qualitative and quantitative correlation for performance parameters - Specific Impulse (Isp) and Characteristic Velocity (C*) - as a function of one or more chamber dimensions - Contraction Ratio (CR), Chamber Length (L ) and/or Characteristic Chamber Length (L*). Determine if chamber dimensions can be correlated to frozen or equilibrium chemistry.

  7. Liquid rocket engine self-cooled combustion chambers

    NASA Technical Reports Server (NTRS)

    1977-01-01

    Self-cooled combustion chambers are chambers in which the chamber wall temperature is controlled by methods other than fluid flow within the chamber wall supplied from an external source. In such chambers, adiabatic wall temperature may be controlled by use of upstream fluid components such as the injector or a film-coolant ring, or by internal flow of self-contained materials; e.g. pyrolysis gas flow in charring ablators, and the flow of infiltrated liquid metals in porous matrices. Five types of self-cooled chambers are considered in this monograph. The name identifying the chamber is indicative of the method (mechanism) by which the chamber is cooled, as follows: ablative; radiation cooled; internally regenerative (Interegen); heat sink; adiabatic wall. Except for the Interegen and heat sink concepts, each chamber type is discussed separately. A separate and final section of the monograph deals with heat transfer to the chamber wall and treats Stanton number evaluation, film cooling, and film-coolant injection techniques, since these subjects are common to all chamber types. Techniques for analysis of gas film cooling and liquid film cooling are presented.

  8. Right/left assignment in drift chambers and proportional multiwire chambers (PWC's) using induced signals

    DOEpatents

    Walenta, Albert H.

    1979-01-01

    Improved multiwire chamber having means for resolving the left/right ambiguity in the location of an ionizing event. The chamber includes a plurality of spaced parallel anode wires positioned between spaced planar cathodes. Associated with each of the anode wires are a pair of localizing wires, one positioned on either side of the anode wire. The localizing wires are connected to a differential amplifier whose output polarity is determined by whether the ionizing event occurs to the right or left of the anode wire.

  9. A new ring-shaped graphite monitor ionization chamber

    NASA Astrophysics Data System (ADS)

    Yoshizumi, M. T.; Caldas, L. V. E.

    2010-07-01

    A ring-shaped monitor ionization chamber was developed at the Instituto de Pesquisas Energéticas e Nucleares. This ionization chamber presents an entrance window of aluminized polyester foil. The guard ring and collecting electrode are made of graphite coated Lucite plates. The main difference between this new ionization chamber and commercial monitor chambers is its ring-shaped design. The new monitor chamber has a central hole, allowing the passage of the direct radiation beam without attenuation; only the penumbra radiation is measured by the sensitive volume. This kind of ionization chamber design has already been tested, but using aluminium electrodes. By changing the electrode material from aluminium to a graphite coating, an improvement in the chamber response stability was expected. The pre-operational tests, as saturation curve, recombination loss and polarity effect showed satisfactory results. The repeatability and the long-term stability tests were also evaluated, showing good agreement with international recommendations.

  10. Vacuum chamber with a supersonic-flow aerodynamic window

    DOEpatents

    Hanson, C.L.

    1980-10-14

    A supersonic flow aerodynamic window is disclosed whereby a steam ejector situated in a primary chamber at vacuum exhausts superheated steam toward an orifice to a region of higher pressure, creating a barrier to the gas in the region of higher pressure which attempts to enter through the orifice. In a mixing chamber outside and in fluid communication with the primary chamber, superheated steam and gas are combined into a mixture which then enters the primary chamber through the orifice. At the point of impact of the ejector/superheated steam and the incoming gas/superheated steam mixture, a barrier is created to the gas attempting to enter the ejector chamber. This barrier, coupled with suitable vacuum pumping means and cooling means, serves to keep the steam ejector and primary chamber at a negative pressure, even though the primary chamber has an orifice to a region of higher pressure.

  11. Vacuum chamber with a supersonic flow aerodynamic window

    DOEpatents

    Hanson, Clark L.

    1982-01-01

    A supersonic flow aerodynamic window, whereby a steam ejector situated in a primary chamber at vacuum exhausts superheated steam toward an orifice to a region of higher pressure, creating a barrier to the gas in the region of higher pressure which attempts to enter through the orifice. In a mixing chamber outside and in fluid communication with the primary chamber, superheated steam and gas are combined into a mixture which then enters the primary chamber through the orifice. At the point of impact of the ejector/superheated steam and the incoming gas/superheated steam mixture, a barrier is created to the gas attempting to enter the ejector chamber. This barrier, coupled with suitable vacuum pumping means and cooling means, serves to keep the steam ejector and primary chamber at a negative pressure, even though the primary chamber has an orifice to a region of higher pressure.

  12. Investigation on temperature separation and flow behaviour in vortex chamber

    NASA Astrophysics Data System (ADS)

    Matsuno, Yuhi; Fukushima, Yusuke; Matsuo, Shigeru; Hashimoto, Tokitada; Setoguchi, Toshiaki; Kim, Heuy Dong

    2015-04-01

    In the previous researches, it is known that the swirl flow in circular pipe causes the temperature separation. Recently, it is shown that the temperature separation occurs in a vortex chamber when compressed air are pumped into this device from the periphery. Especially, in a cavity installed in the periphery of the chamber, the highest temperature was observed. Therefore, it is expected that this device can be used as a heat source in the engineering field. In recent researches, the mechanism of temperature separation in vortex chamber has been investigated by some researchers. However, there are few researches for the effect of diameter and volume of vortex chamber, height of central rod and position of cavity on the temperature separation. Further, no detailed physical explanation has been made for the temperature separation phenomena in the vortex chamber. In the present study, the effects of chamber configuration and position of the cavity on temperature separation in the vortex chamber were investigated experimentally.

  13. Wire chamber radiation detector with discharge control

    DOEpatents

    Perez-Mendez, Victor; Mulera, Terrence A.

    1984-01-01

    A wire chamber radiation detector (11) has spaced apart parallel electrodes (16) and grids (17, 18, 19) defining an ignition region (21) in which charged particles (12) or other ionizing radiations initiate brief localized avalanche discharges (93) and defining an adjacent memory region (22) in which sustained glow discharges (94) are initiated by the primary discharges (93). Conductors (29, 32) of the grids (18, 19) at each side of the memory section (22) extend in orthogonal directions enabling readout of the X-Y coordinates of locations at which charged particles (12) were detected by sequentially transmitting pulses to the conductors (29) of one grid (18) while detecting transmissions of the pulses to the orthogonal conductors (36) of the other grid (19) through glow discharges (94). One of the grids (19) bounding the memory region (22) is defined by an array of conductive elements (32) each of which is connected to the associated readout conductor (36) through a separate resistance (37). The wire chamber (11) avoids ambiguities and imprecisions in the readout of coordinates when large numbers of simultaneous or near simultaneous charged particles (12) have been detected. Down time between detection periods and the generation of radio frequency noise are also reduced.

  14. Bubble chambers for experiments in nuclear astrophysics

    NASA Astrophysics Data System (ADS)

    DiGiovine, B.; Henderson, D.; Holt, R. J.; Raut, R.; Rehm, K. E.; Robinson, A.; Sonnenschein, A.; Rusev, G.; Tonchev, A. P.; Ugalde, C.

    2015-05-01

    A bubble chamber has been developed to be used as an active target system for low energy nuclear astrophysics experiments. Adopting ideas from dark matter detection with superheated liquids, a detector system compatible with γ-ray beams has been developed. This detector alleviates some of the limitations encountered in standard measurements of the minute cross-sections of interest to stellar environments. While the astrophysically relevant nuclear reaction processes at hydrostatic burning temperatures are dominated by radiative captures, in this experimental scheme we measure the time-reversed processes. Such photodisintegrations allow us to compute the radiative capture cross-sections when transitions to excited states of the reaction products are negligible. Due to the transformation of phase space, the photodisintegration cross-sections are up to two orders of magnitude higher. The main advantage of the new target-detector system is a density several orders of magnitude higher than conventional gas targets. Also, the detector is virtually insensitive to the γ-ray beam itself, thus allowing us to detect only the products of the nuclear reaction of interest. The development and the operation as well as the advantages and disadvantages of the bubble chamber are discussed.

  15. Vapor Wall Deposition in Chambers: Theoretical Considerations

    NASA Astrophysics Data System (ADS)

    McVay, R.; Cappa, C. D.; Seinfeld, J.

    2014-12-01

    In order to constrain the effects of vapor wall deposition on measured secondary organic aerosol (SOA) yields in laboratory chambers, Zhang et al. (2014) varied the seed aerosol surface area in toluene oxidation and observed a clear increase in the SOA yield with increasing seed surface area. Using a coupled vapor-particle dynamics model, we examine the extent to which this increase is the result of vapor wall deposition versus kinetic limitations arising from imperfect accommodation of organic species into the particle phase. We show that a seed surface area dependence of the SOA yield is present only when condensation of vapors onto particles is kinetically limited. The existence of kinetic limitation can be predicted by comparing the characteristic timescales of gas-phase reaction, vapor wall deposition, and gas-particle equilibration. The gas-particle equilibration timescale depends on the gas-particle accommodation coefficient αp. Regardless of the extent of kinetic limitation, vapor wall deposition depresses the SOA yield from that in its absence since vapor molecules that might otherwise condense on particles deposit on the walls. To accurately extrapolate chamber-derived yields to atmospheric conditions, both vapor wall deposition and kinetic limitations must be taken into account.

  16. A rare case of anterior chamber dirofilariasis

    PubMed Central

    Das, Dipankar; Das, Kalyan; Islam, Saidul; Bhattacharjee, Kasturi; Bhattacharjee, Harsha; Das, Shrutanjoy Mohan; Deka, Apurba

    2015-01-01

    We report a rare case of anterior chamber live dirofilariasis presenting as anterior uveitis. A 60-year-old man presented with dimness of vision in the right eye for 1 month. Vision recorded was 6/18 P, N 18 in the right eye. Slit lamp examination of the right eye revealed anterior uveitis with a moving nemathelminthes. The worm was removed live from the anterior chamber under local anesthesia with assisted methyl cellulose delivery and post-operatively, the worm was examined directly under light microscope. Morphometric measurement showed length of the worm was 6.061 mm. A thin, pale, slender worm was diagnosed as immature female Dirofilaria repens and was documented completely. Patient had made an excellent recovery of vision and intraocular inflammation after the surgical removal of the worm. Intraocular infection of dirofilaria is a rare presentation and successful surgical removal of the worm resulted in complete recovery of uveitis and visual status in the affected eye. PMID:25709276

  17. Rocket thrust chamber thermal barrier coatings

    NASA Technical Reports Server (NTRS)

    Batakis, A. P.; Vogan, J. W.

    1985-01-01

    A research program was conducted to generate data and develop analytical techniques to predict the performance and reliability of ceramic thermal barrier coatings in high heat flux environments. A finite element model was used to analyze the thermomechanical behavior of coating systems in rocket thrust chambers. Candidate coating systems (using a copper substrate, NiCrAlY bond coat and ZrO2.8Y2O3 ceramic overcoat) were selected for detailed study based on photomicrographic evaluations of experimental test specimens. The effects of plasma spray application parameters on the material properties of these coatings were measured and the effects on coating performance evaluated using the finite element model. Coating design curves which define acceptable operating envelopes for seleted coating systems were constructed based on temperature and strain limitations. Spray gun power levels was found to have the most significant effect on coating structure. Three coating systems were selected for study using different power levels. Thermal conductivity, strain tolerance, density, and residual stress were measured for these coatings. Analyses indicated that extremely thin coatings ( 0.02 mm) are required to accommodate the high heat flux of a rocket thrust chamber and ensure structural integrity.

  18. Space station auxiliary thrust chamber technology

    NASA Technical Reports Server (NTRS)

    Senneff, J. M.

    1986-01-01

    A program to design, fabricate and test a 50 lb sub f (222 N) thruster was undertaken (Contract NAS 3-24656) to demonstrate the applicability of the reverse flow concept as an item of auxiliary propulsion for the space station. The thruster was to operate at a mixture ratio (O/F) of 4, be capable of operating for 2 million lb sub f- seconds (8.896 million N-seconds) impulse with a chamber pressure of 75 psia (52 N/square cm) and a nozzle area ratio of 40. Superimposed was also the objective of operating with a strainless steel spherical combustion chamber, which limited the wall temperature to 1700 F (1200 K), an objective specific impulse of 400 lb sub f sec/lbm (3923 N-seconds/Kg), and a demonstration of 500,000 lb sub f-seconds (2,224,000 N-seconds) of impulse. The demonstration of these objectives required a number of design iterations which eventually culminated in a very successful 1000 second demonstration, almost immediately followed by a changed program objective imposed to redesign and demonstrate at a mixture ratio (O/F) of 8. This change was made and more then 250,000 lb sub f seconds (1,112,000 N-seconds) of impulse was successfully demonstrated at a mixture ratio of 8. This document contains a description of the effort conducted during the program to design and demonstrate the thrusters involved.

  19. Vacuum-cleaning System for Isolation Chambers

    PubMed Central

    Yale, Charles E.

    1969-01-01

    To encourage the utilization of the isolation chamber as a research tool, the cost of its use should be lowered. Methods and devices must be developed which make more efficient use of the space within the isolator and allow the operator to work more effectively in this confined area. A simple vacuum-cleaning system is described; it consists of a nozzle and flexible hose which connect through the isolator wall to an externally placed waste tank, attached by way of its outlet filter to a source of vacuum. The cylindrical waste tank [48 inches (1.219 m) high and 36 inches (0.914 m) in diameter] was sterilized in a large autoclave. During a 9-month test period, the system was used to remove soiled corncob bedding from a large isolator containing 90 adult monocontaminated rats. During this period, the microbial flora of the isolator was unchanged, and the time required to clean the cages was reduced by 50%. This vacuum-cleaning system is a safe, convenient, and economical means of increasing the efficiency of an isolation chamber. Images PMID:5775913

  20. Structural and optical properties of Ga{sub 2}O{sub 3}:In films deposited on MgO (1 0 0) substrates by MOCVD

    SciTech Connect

    Kong Lingyi; Ma Jin; Luan Caina; Zhu Zhen

    2011-08-15

    Ga{sub 2}O{sub 3}:In films with different indium (In) content x [x=In/(Ga+In) atomic ratio] have been deposited on MgO (1 0 0) substrates by metalorganic chemical vapor deposition (MOCVD). Structural analyses revealed that the film deposited with actual In content (x') of 0.09 was an epitaxial film and the films with x'=0.18 and 0.37 had mixed-phase structures of monoclinic Ga{sub 2}O{sub 3} and bixbyite In{sub 2}O{sub 3}. The absolute average transmittance of the obtained films in the visible region exceeded 95%, and the band gap was in the range of 4.74-4.87 eV. Photoluminescence (PL) measurements were performed at room temperature, in which the visible luminescences were strong and could be seen by the naked eye. The strong emissions in the visible light region were proposed to originate from the gallium vacancies, oxygen deficiencies and other defects in these films. - Graphical abstract: Low magnification XTEM (a), HRTEM (b) and SAED (c) micrographs of the interface area between Ga{sub 1.82}In{sub 0.18}O{sub 3} film and MgO substrate have showed the Ga{sub 1.82}In{sub 0.18}O{sub 3} is an epitaxial film. Highlights: > Ga{sub 1.82}In{sub 0.18}O{sub 3} epitaxial film was deposited on MgO(1 0 0) substrate. > The transmittance of the Ga{sub 2}O{sub 3}:In films in the visible region exceeded 95%. > Strong emissions were observed in the photoluminescence measurements of the films.

  1. On the reliability of heteronuclear precursors-ligand effects in the Li-MOCVD synthesis of SrTiO3 films.

    PubMed

    Seisenbaeva, Gulaim A; Gohil, Suresh; Kessler, Vadim G; Andrieux, Michel; Legros, Corinne; Ribot, Patrick; Brunet, Magali

    2011-09-01

    Strontium titanate SrTiO3 thin films are highly perspective as gate dielectric material. Difference in volatility of the common homometallic precursors-strontium beta-diketonates and titanium alkoxides remains major hinder for preparation of high quality coatings based on this phase. An attractive alternative in its synthesis by MOCVD is provided by application of heterometallic mixed-ligand complexes, Sr2Ti2(beta-diket)4(OR)8(ROH)x. Mass-spectrometric study reveals, however, that none of these species can be considered a true single-source precursor. The relative stability of the molecules in solution and the congruence of in-situ release of homometallic species on evaporation are, on the other hand, crucial for the quality of the produced films and are strongly influenced by the nature of alkoxide ligands, OR. The historically first discovered representative of this heterometallic family, a sec-alkoxide derivative Sr2Ti2(thd)4(O(i)Pr)8, is in fact unexpectedly unstable, transforming in solution into Sr2Ti(thd)4(O(i)Pr)4((i)PrOH), which explains difficulties in keeping the correct stoichiometry using isopropoxide precursor. The primary alkoxide complexes, Sr2Ti2(thd)4(OR)8(ROH)2, R = Et, (n)Pr are also unstable yielding Sr4Ti2(thd)4(OR)8(ROH)2 on decomposition. The best solution stability and most uniform evaporation was observed for the iso-derivative, Sr2Ti2(thd)4(O(i)Bu)8, permitting to apply it in long term experiments under industrial process conditions. Present contribution provides detailed experimental comparison between and sec-and iso-alkoxide derivatives and sheds light on the influence of the ligand on molecular stability of a precursor and how it influences the quality of the derived oxide film, especially in relation to its electrophysical properties. PMID:22097573

  2. The management of stress in MOCVD-grown InGaN/GaN LED multilayer structures on Si(1 1 1) substrates

    NASA Astrophysics Data System (ADS)

    Jiang, Quanzhong; Allsopp, Duncan W. E.; Bowen, Chris R.; Wang, Wang N.

    2013-09-01

    The tensile stress in light-emitting diode (LED)-on-Si(1 1 1) multilayer structures must be reduced so that it does not compromise the multiple quantum well emission wavelength uniformity and structural stability. In this paper it is shown for non-optimized LED structures grown on Si(1 1 1) substrates that both emission wavelength uniformity and structural stability can be achieved within the same growth process. In order to gain a deeper understanding of the stress distribution within such a structure, cross-sectional Raman and photo-luminescence spectroscopy techniques were developed. It is observed that for a Si:GaN layer grown on a low-temperature (LT) AlN intermediate layer there is a decrease in compressive stress with increasing Si:GaN layer thickness during MOCVD growth which leads to a high level of tensile stress in the upper part of the layer. This may lead to the development of cracks during cooling to room temperature. Such a phenomenon may be associated with annihilation of defects such as dislocations. Therefore, a reduction of dislocation intensity should take place at the early stage of GaN growth on an AlN or AlGaN layer in order to reduce a build up of tensile stress with thickness. Furthermore, it is also shown that a prolonged three dimensional GaN island growth on a LT AlN interlayer for the reduction of dislocations may result in a reduction in the compressive stress in the resulting GaN layer.

  3. Photodetectors of slit and sandwich types based on CdS and CdS1-xSex films obtained using MOCVD method from dithiocarbamates

    NASA Astrophysics Data System (ADS)

    Zavyalova, Ludmila V.; Svechnikov, Sergey V.; Tchoni, Vladimir G.

    1997-04-01

    Here we report the results of working out an original, simple in control and not requiring expensive equipment MOCVD-method for depositing films of semiconductor compounds A2B6. Dithiocarbamates (DTC) are used as starting materials. The compounds are stable, easily synthesized, cheap and low toxic. Atoms of metal and sulfur in the DTC are strongly bonded. The DTC could be easily dissolved in various organic solvents. The experimental unit for film deposition comprises a spraying apparatus, a substrate heater, and a quartz cylinder for separation of a reaction zone from ambience. The process of film deposition is carried out in air conditions. Films of CdS, bright-yellow, transparent, having mirror smooth surface at thickness less than 2 mkm and rough surface at thickness 8-12 mkm, were deposited by spraying cadmium dithiocarbamate, that is DTC with radical C2H5, solution in pyridine on substrates heated to 240-280 degrees C. Deposition rate was 60-90 nm/min. Films obtained were of hexagonal modification, polycrystalline, textured, with low, at the level of centipercents content of oxygen and carbon. Slit type photodetectors based on CdS and CdS1-xSex of 1.0 mkm thickness have dark conductivity (sigma) d equals 10-9 divided by 10-8 Ohm-1cm-1 and photoconductivity (sigma) ph equals 10-2 divided by 10-1 Ohm-1cm-1 at 200 lux. Industrially suitable technology for production of photopotentiometer on the base of these films was developed. Sandwich-type photodetectors In2S3 - CdS: Cu, Cl - In with 8-12 mkm thickness have the same value of photoconductivity and the light-to-dark ratio is 106 divided by 107. Based on sandwich-type photodetectors, a hybrid structure of pyroelectric-photodetector as a resonant-type coordinate-sensitive detector was developed.

  4. Characterization of CdTe substrates and MOCVD Cd 1- xZn xTe epilayers by Raman, photoluminescence and X-ray diffraction techniques

    NASA Astrophysics Data System (ADS)

    Levy, M.; Amir, N.; Khanin, E.; Muranevich, A.; Nemirovsky, Y.; Beserman, R.

    1998-05-01

    CdTe substrates and the quality of the Cd 1- xZn xTe ( x⩽0.1) epilayers grown by metalorganic chemical vapor deposition (MOCVD) on CdTe substrates, are characterized by Raman scattering and photoluminescence (PL) as well as by X-ray double-crystal rocking curve (DCRC). At a low temperature the intensity of LO phonon is enhanced wherever there is a structural defect. The defect-induced enhancement is due to a large momentum transfer which enhances the intraband Frolich interaction. In addition, the bound exciton peak intensity measured by PL decreases wherever the LO phonon scattering efficiency increases confirming that the defect is the origin of the above Raman enhancement. The quantitative measure of the structural perfection is related to the ratio between the defect band and excitonic peaks in the PL spectra, and correlates with the X-ray full-width at half-maximum (FWHM) of the layer peak. It is shown that in addition to these parameters, the FWHM of the PL defect band is a useful parameter to determine the quality of the epilayer, and a good correlation is obtained between the different parameters. The effect of growth parameters such as zinc partial pressure in the reactor during growth and the reactor design are studied. The results indicate that crystalline imperfection is caused by lattice mismatch between the CdTe substrate and the CdZnTe epilayer and by the nonuniformity of the zinc composition throughout the layers. The quality of the layers is independent of the reactor volume.

  5. EXAFS study on yttrium oxide thin films deposited by RF plasma enhanced MOCVD under the influence of varying RF self-bias

    NASA Astrophysics Data System (ADS)

    Chopade, S. S.; Nayak, C.; Bhattacharyya, D.; Jha, S. N.; Tokas, R. B.; Sahoo, N. K.; Patil, D. S.

    2014-09-01

    Extended X-ray absorption fine structure (EXAFS) and atomic force microscopy (AFM) studies are carried out on yttrium oxide (Y2O3) thin films deposited by radio frequency plasma assisted metalorganic chemical vapor deposition (MOCVD) process at different RF self-bias (-50 V to -175 V with a step of -25 V) on silicon substrates. A (2,2,6,6-tetramethyl-3,5-heptanedionate) yttrium (commonly known as Y(thd)3) precursor is used in a plasma of argon and oxygen gases at a substrate temperature of 350 °C for deposition. To gain profound understanding about influence of RF self-bias on the properties of the deposited Y2O3 thin films, the films are characterized by EXAFS and AFM measurements. From the EXAFS measurements it is observed that oxygen co-ordination is high for the film deposited at the lowest self bias (-50 V) which is due to presence of higher amount of hydroxyl group in the sample. Oxygen coordination however decrease to lower values for the films deposited at self bias of -75 V. Ysbnd O bond length decreases gradually with increase in self bias indicating reduction in hydroxyl content. However there is reduction in bond length for the film deposited at -100 V as compared to other films resulting from structural changes. The disorder factor obtained from EXAFS measurement increases for films deposited at voltages beyond -125 V due to degradation in crystallinity of the films caused by increased bombardment by incident ions. From AFM measurements, it is observed that the surface morphology of the films also change with self bias. The root mean square roughness value and the entropy factor are found to be low for films deposited at lower bias values and increase for films deposited at bias voltages above -100 V.

  6. Advanced hydrogen/oxygen thrust chamber design analysis

    NASA Technical Reports Server (NTRS)

    Shoji, J. M.

    1973-01-01

    The results are reported of the advanced hydrogen/oxygen thrust chamber design analysis program. The primary objectives of this program were to: (1) provide an in-depth analytical investigation to develop thrust chamber cooling and fatigue life limitations of an advanced, high pressure, high performance H2/O2 engine design of 20,000-pounds (88960.0 N) thrust; and (2) integrate the existing heat transfer analysis, thermal fatigue and stress aspects for advanced chambers into a comprehensive computer program. Thrust chamber designs and analyses were performed to evaluate various combustor materials, coolant passage configurations (tubes and channels), and cooling circuits to define the nominal 1900 psia (1.31 x 10 to the 7th power N/sq m) chamber pressure, 300-cycle life thrust chamber. The cycle life capability of the selected configuration was then determined for three duty cycles. Also the influence of cycle life and chamber pressure on thrust chamber design was investigated by varying in cycle life requirements at the nominal chamber pressure and by varying the chamber pressure at the nominal cycle life requirement.

  7. Magma chambers: Formation, local stresses, excess pressures, and compartments

    NASA Astrophysics Data System (ADS)

    Gudmundsson, Agust

    2012-09-01

    An existing magma chamber is normally a necessary condition for the generation of a large volcanic edifice. Most magma chambers form through repeated magma injections, commonly sills, and gradually expand and change their shapes. Highly irregular magma-chamber shapes are thermo-mechanically unstable; common long-term equilibrium shapes are comparatively smooth and approximate those of ellipsoids of revolution. Some chambers, particularly small and sill-like, may be totally molten. Most chambers, however, are only partially molten, the main part of the chamber being crystal mush, a porous material. During an eruption, magma is drawn from the crystal mush towards a molten zone beneath the lower end of the feeder dyke. Magma transport to the feeder dyke, however, depends on the chamber's internal structure; in particular on whether the chamber contains pressure compartments that are, to a degree, isolated from other compartments. It is only during large drops in the hydraulic potential beneath the feeder dyke that other compartments become likely to supply magma to the erupting compartment, thereby contributing to its excess pressure (the pressure needed to rupture a magma chamber) and the duration of the eruption. Simple analytical models suggest that during a typical eruption, the excess-pressure in the chamber decreases exponentially. This result applies to a magma chamber that (a) is homogeneous and totally fluid (contains no compartments), (b) is not subject to significant replenishment (inflow of new magma into the chamber) during the eruption, and (c) contains magma where exsolution of gas has no significant effect on the excess pressure. For a chamber consisting of pressure compartments, the exponential excess-pressure decline applies primarily to a single erupting compartment. When more than one compartment contributes magma to the eruption, the excess pressure may decline much more slowly and irregularly. Excess pressure is normally similar to the in

  8. Plasma arc heated secondary combustion chamber

    SciTech Connect

    Haun, R.; Paulson, B.; Schlienger, M.; Goerz, D.; Kerns, J.; Vernazza, J.

    1995-02-01

    This paper describes a secondary combustion chamber (SCC) for hazardous waste treatment systems that uses a plasma arc torch as the heat source. Developed under a cooperative research and development agreement (CRADA) between Retech, Inc. and Lawrence Livermore National Laboratory (LLNL), the unit is intended primarily to handle the off-gas from a Plasma Arc Centrifugal Treatment (PACT) system. ft is designed to heat the effluent gas which may contain volatile organic compounds, and maintain the gas temperature above 1000 C for two seconds or more. The benefits of using a plasma arc gas heater are described in comparison to a conventional fossil fuel heated SCC. Thermal design considerations are discussed. Analysis and experimental results are presented to show the effectiveness in destroying hazardous compounds and reducing the total volume of gaseous emissions.

  9. The coated cathode conductive layer chamber

    NASA Astrophysics Data System (ADS)

    Bouclier, R.; Gaudaen, J.; Sauli, F.

    1991-12-01

    We describe a gaseous detector consisting of thin anode strips vacuum-evaporated on one side of a 100 μm thick plastic layer, alternating on the back side of the same foil with wider parallel cathode strips. Ionization released in a drift space on the anode side is amplified and detected much in the same way as in the microstrip gas chamber; in our detector however spontaneous breakdown due to surface currents is completely avoided by the presence of the insulating layer between anodes and cathodes. To reduce surface and volume charging up, we have used polymer foils with a moderate volume resistivity. The first results show good efficiency, good plateaux and time resolution in detecting low-rate minimum ionizing electrons. Although not suited for high rate or good energy resolution applications, this kind of detector seems rather promising for realizing cheaply large active surfaces.

  10. Fabrication of GRCop-84 Rocket Thrust Chambers

    NASA Technical Reports Server (NTRS)

    Loewenthal, William; Ellis, David

    2006-01-01

    GRCop-84, a copper alloy, Cu-8 at% Cr-4 at% Nb developed at NASA Glenn Research Center for regenerative1y cooled rocket engine liners has excellent combinations of elevated temperature strength, creep resistance, thermal conductivity and low cycle fatigue. GRCop-84 is produced from pre-alloyed atomized powder and has been fabricated into plate, sheet and tube forms as well as near net shapes. Fabrication processes to produce demonstration rocket combustion chambers will be presented and includes powder production, extruding, rolling, forming, friction stir welding, and metal spinning. GRCop-84 has excellent workability and can be readily fabricated into complex components using conventional powder and wrought metallurgy processes. Rolling was examined in detail for process sensitivity at various levels of total reduction, rolling speed and rolling temperature representing extremes of commercial processing conditions. Results indicate that process conditions can range over reasonable levels without any negative impact to properties.

  11. Emulsion chamber observations and interpretation (HE 3)

    NASA Technical Reports Server (NTRS)

    Shibata, M.

    1986-01-01

    Experimental results from Emulsion Chamber (EC) experiments at mountain altitudes or at higher levels using flying carriers are examined. The physical interest in this field is concentrated on the strong interaction at the very high energy region exceeding the accelerator energy, also on the primary cosmic ray intensity and its chemical composition. Those experiments which observed cosmic ray secondaries gave information on high energy interaction characteristics through the analyses of secondary spectra, gamma-hadron families and C-jets (direct observation of the particle production occuring at the carbon target). Problems of scaling violation in fragmentation region, interaction cross section, transverse momentum of produced secondaries, and some peculiar features of exotic events are discussed.

  12. A nonuniform electrical field electroporation chamber design.

    PubMed

    Hollon, T; Yoshimura, F K

    1989-11-01

    We show an inexpensive design for an electroporation chamber which subjects electroporated cells to a nonuniform electrical field. Our design, which we call an electroporation cylinder, improved transfection efficiency over that of a uniform field design (electroporation cuvettes) by about sixfold when tested in five mouse cell lines with a transient gene expression assay. Electroporation cylinders subjected cells to electrical field strengths at least as powerful as those of electroporation cuvettes, as judged by comparing the percentages of cells killed by electroporation. Cylinder and cuvette designs were similar in their effect on the variability of transfection efficiency. Electroporation cylinders may be particularly useful when the optimal electrical field strength for a cell line is not known or is unattainable with a given power supply. PMID:2610341

  13. Isothermally heatsunk diffusion cloud chamber refrigerator

    SciTech Connect

    Menocal, S.G.

    1987-05-05

    This patent describes a diffusion cloud chamber isothermally heatsunk refrigerator which comprises: a heatsink consisting of two phases of a saturated substance existing in thermodynamic equilibrium at constant pressure and therefore at constant temperature, contained in a reservoir; a means of pressure damping to maintain constant pressure, as the ratio of the two phases present changes and introduces volumetric changes in the substance; a cooling member which transfer heat from vapor in contact with the cooling member surface to the ''cold side'' of a Peltier thermoelectric element with which the cooling member is in thermal contact; a Peltier thermoelectric element which removes the heat supplied by the cooling member from its ''cold side'' and pumps it to the ''hot side'' when driven by an electric current; and a means of transferring heat from the ''hot side'' of the Peltier thermoelectric element to the two-phase isothermal substance in the reservoir.

  14. Foreign body embedded in anterior chamber angle.

    PubMed

    Graffi, Shmuel; Tiosano, Beatrice; Ben Cnaan, Ran; Bahir, Jonathan; Naftali, Modi

    2012-01-01

    Introduction. We present a case of a metallic foreign body embedded in the anterior chamber angle. After standing in close proximity to a construction worker breaking a tile, a 26-year-old woman using soft contact lens for the correction of mild myopia presented to emergency department for evaluation of a foreign body sensation of her right eye. Methods and Results. Diagnosis was confirmed by gonioscopic examination and a noncontrast CT scan of head and orbits. The foreign body was removed by an external approach without utilizing a magnet. The patient's final outcome was favorable. Discussion. The above is a rare clinical situation, which is impossible to detect on slit-lamp examination without a gonioscopic view. Proper imaging and a specific management are mandatory in order to achieve favorable outcome. PMID:23091762

  15. Nuclear Fission Investigation with Twin Ionization Chamber

    SciTech Connect

    Zeynalova, O.; Zeynalov, Sh.; Nazarenko, M.; Hambsch, F.-J.; Oberstedt, S.

    2011-11-29

    The purpose of the present paper was to report the recent results, obtained in development of digital pulse processing mathematics for prompt fission neutron (PFN) investigation using twin ionization chamber (TIC) along with fast neutron time-of-flight detector (ND). Due to well known ambiguities in literature (see refs. [4, 6, 9 and 11]), concerning a pulse induction on TIC electrodes by FF ionization, we first presented detailed mathematical analysis of fission fragment (FF) signal formation on TIC anode. The analysis was done using Ramo-Shockley theorem, which gives relation between charged particle motion between TIC electrodes and so called weighting potential. Weighting potential was calculated by direct numerical solution of Laplace equation (neglecting space charge) for the TIC geometry and ionization, caused by FF. Formulae for grid inefficiency (GI) correction and digital pulse processing algorithms for PFN time-of-flight measurements and pulse shape analysis are presented and discussed.

  16. Development of an optical digital ionization chamber

    SciTech Connect

    Turner, J.E.; Hunter, S.R.; Hamm, R.N.; Wright, H.A.; Hurst, G.S.; Gibson, W.A.

    1988-01-01

    We are developing a new device for optically detecting and imaging the track of a charged particle in a gas. The electrons in the particle track are made to oscillate rapidly by the application of an external, short-duration, high-voltage, RF electric field. The excited electrons produce additional ionization and electronic excitation of the gas molecules in their immediate vicinity, leading to copious light emission (fluorescence) from the selected gas, allowing the location of the electrons along the track to be determined. Two digital cameras simultaneously scan the emitted light across two perpendicular planes outside the chamber containing gas. The information thus obtained for a given track can be used to infer relevant quantities for microdosimetry and dosimetry, e.g., energy deposited, LET, and track structure in the gas. The design of such a device now being constructed and methods of obtaining the dosimetric data from the digital output will be described. 4 refs., 4 figs.

  17. Water vapor recovery from plant growth chambers

    NASA Technical Reports Server (NTRS)

    Ray, R. J.; Newbold, D. D.; Colton, R. H.; Mccray, S. B.

    1991-01-01

    NASA is investigating the use of plant growth chambers (PGCs) for space missions and for bases on the moon and Mars. Key to successful development of PGCs is a system to recover and reuse the water vapor that is transpired from the leaves of the plants. A design is presented for a simple, reliable, membrane-based system that allows the recovery, purification, and reuse of the transpired water vapor through control of temperature and humidity levels in PGCs. The system is based on two membrane technologies: (1) dehumidification membrane modules to remove water vapor from the air, and (2) membrane contactors to return water vapor to the PGC (and, in doing so, to control the humidity and temperature within the PGC). The membrane-based system promises to provide an ideal, stable growth environment for a variety of plants, through a design that minimizes energy usage, volume, and mass, while maximizing simplicity and reliability.

  18. Phoenix Lowered into Thermal Vacuum Chamber

    NASA Technical Reports Server (NTRS)

    2007-01-01

    NASA's Phoenix Mars Lander was lowered into a thermal vacuum chamber at Lockheed Martin Space Systems, Denver, in December 2006.

    The spacecraft was folded in its aeroshell and underwent environmental testing that simulated the extreme conditions the spacecraft will see during its nine-and-a-half-month cruse to Mars.

    The Phoenix mission is led by Principal Investigator Peter H. Smith of the University of Arizona, Tucson, with project management at NASA's Jet Propulsion Laboratory and development partnership with Lockheed Martin Space Systems. International contributions for Phoenix are provided by the Canadian Space Agency, the University of Neuchatel (Switzerland), the University of Copenhagen, and the Max Planck Institute in Germany. JPL is a division of the California Institute of Technology in Pasadena.

  19. Performance of the TOPAZ time projection chamber

    SciTech Connect

    Shirahashi, A.; Aihara, H.; Itoh, R.; Kamae, T.; Kusuki, N.; Tanaka, M.; Fujii, H.; Fujii, K.; Ikeda, H.; Iwasaki, H.

    1988-02-01

    The TOPAZ detector has began taking data at the TRISTAN e/sup +/e/sup -/ colliding beam ring in May 1987. The major detector elements including the time projection chamber (TPC) have been working quite satisfactorily. The authors report here the performance of TPC based on real e/sup +/e/sup -/ events and cosmic ray events. They measure spatial resolution of sigma/sub xy/ = 185..mu..m and sigma/sub z/ = 335..mu..m, momentum resolution of sigma/sub PT//P/sub T/ = ..sqrt..(1.5P/sub T/)/sup 2/ + (1.6)/sup 2%/ and dE/dx resolution of 4.6%.

  20. Fabrication of GRCop-84 Rocket Thrust Chambers

    NASA Technical Reports Server (NTRS)

    Loewenthal, William S.; Ellis, David L.

    2005-01-01

    GRCop-84, a copper alloy, Cu-8 at% Cr-4 at% Nb developed at NASA Glenn Research Center for regeneratively cooled rocket engine liners has excellent combinations of elevated temperature strength, creep resistance, thermal conductivity and low cycle fatigue. GRCop-84 is produced from prealloyed atomized powder and has been fabricated into plate, sheet and tube forms as well as near net shapes. Fabrication processes to produce demonstration rocket combustion chambers will be presented and includes powder production, extruding, rolling, forming, friction stir welding, and metal spinning. GRCop-84 has excellent workability and can be readily fabricated into complex components using conventional powder and wrought metallurgy processes. Rolling was examined in detail for process sensitivity at various levels of total reduction, rolling speed and rolling temperature representing extremes of commercial processing conditions. Results indicate that process conditions can range over reasonable levels without any negative impact to properties.

  1. Plant exposure laboratory and chambers. Volume 1

    SciTech Connect

    McFarlane, C.; Pfleeger, T.

    1986-01-01

    The research is to learn the factors that control plant uptake, translocation, and metabolism of anthropogenic organic chemicals. Understanding these processes is essential to predict food contamination and environmental damage from various agricultural and industrial pollutants. Contamination of plants is only one component, but since plants are the fulcrum upon which all nourishment systems depend, understanding the ways they become contaminated is critical to prudent production, transportation, and use of organic chemicals. These efforts to identify the controlling mechanisms of these phenomena require an understanding of the physiological parameters of the plants during uptake and translocation of the extraneous chemicals. Since the chemicals of interest are toxic and studies generally include /sup 14/C as a label for monitoring chemical kinetics, containment is an important criterion. The paper describes the laboratory and support system, the exposure chambers, the computer system, and the plant hydroponic nursery built to accomplish this research.

  2. Main Chamber and Preburner Injector Technology

    NASA Technical Reports Server (NTRS)

    Santoro, Robert J.; Merkle, Charles L.

    1999-01-01

    This document reports the experimental and analytical research carried out at the Penn State Propulsion Engineering Research Center in support of NASA's plan to develop advanced technologies for future single stage to orbit (SSTO) propulsion systems. The focus of the work is on understanding specific technical issues related to bi-propellant and tri-propellant thrusters. The experiments concentrate on both cold flow demonstrations and hot-fire uni-element tests to demonstrate concepts that can be incorporated into hardware design and development. The analysis is CFD-based and is intended to support the design and interpretation of the experiments and to extrapolate findings to full-scale designs. The research is divided into five main categories that impact various SSTO development scenarios. The first category focuses on RP-1/gaseous hydrogen (GH2)/gaseous oxygen (GO2) tri-propellant combustion with specific emphasis on understanding the benefits of hydrogen addition to RP-1/oxygen combustion and in developing innovative injector technology. The second category investigates liquid oxygen (LOX)/GH2 combustion at main chamber near stoichiometric conditions to improve understanding of existing LOX/GH2 rocket systems. The third and fourth categories investigate the technical issues related with oxidizer-rich and fuel-rich propulsive concepts, issues that are necessary for developing the full-flow engine cycle. Here, injector technology issues for both LOX/GH2 and LOX/RP-1 propellants are examined. The last category, also related to the full-flow engine cycle, examines injector technology needs for GO2/GH2 propellant combustion at near-stoichiometric conditions for main chamber application.

  3. Electromagnetic Imaging of Crustal Magma Chambers

    NASA Astrophysics Data System (ADS)

    Constable, S.; Li, Y.; Key, K.

    2006-12-01

    In February/March 2004 we carried out a combined magnetotelluric (MT) and controlled source electromagnetic (CSEM) study of the mid-ocean ridge in the Pacific Ocean at 9°--10° North latitude. A 40-kilometer line of 22 seafloor electromagnetic recorders at 9°30' collected data from 27 kilometers of deep-towed CSEM transmission at 2~Hz, with a source dipole moment of 22~kAm. In order to obtain a first-order image of the information contained in the CSEM data we computed an apparent resistivity psuedosection based on signal amplitudes. This generates a spectacular image of a 10-kilometer wide, 20~Ømegam magma chamber embedded in a 500~Ømegam crust, along with pockets of melt or brine offset to the east of the ridge. We used the pseudosection to guide trial-and-error forward modeling using a newly developed 2D unstructured finite element code which allows seafloor bathymetry to be accurately meshed. The more rigorous modeling results in a good fit to the data from a much narrower 20~Ømegam `mush' zone only 2.5~km wide, capped by a 600-m thick 5~Ømegam melt lens. Unlike the pseudosection, the forward model requires a conductive (5~Ømegam) tent which extends from the melt lens to within about 100~m of the seafloor, probably corresponding to a zone of hydrothermal circulation. This is in contrast to earlier results from the slow-spreading, deeper magma chamber at the Valu Fa Ridge in the Lau Basin, where a large, asymmetric conductivity anomaly in the upper crust suggests that hydrothermal fluids extend 10~km west of the ridge axis.

  4. Effects of open-top chambers on 'Valencia' orange trees

    SciTech Connect

    Olszyk, D.M.; Takemoto, B.K.; Kats, G.; Dawson, P.J.; Morrison, C.L.

    1992-01-01

    Young 'Valencia' orange trees (Citrus sinensis(L) Osbeck) were grown for four years in large open-top chambers with ambient (nonfiltered) air or in outside air to determine any effects of the chambers on the air pollutant susceptibility of the trees. Long-term ozone average concentrations (12 hours, growing season) were 8% lower, and cumulative ozone dose (hourly values >0.1 microL/L) was 29% lower in ambient chambers compared to outside air. Fruit yields were much higher (>39%) for ambient chamber trees than for outside trees over three harvests, due at least partly to less fruit drop during the growing season for ambient chamber trees. Ambient chamber trees were much larger than outside trees and produced over twice as much leaf material over four years of study. Leaves on ambient chamber trees were larger and less dense than on outside trees. Leaves on ambient chamber trees were under more stress than leaves on outside trees during summer months; with lower stomatal conductances (14% average) and transpiration rates (12%), and more negative leaf water pressure potentials (28%). In contrast, leaves on ambient chamber trees had higher net photosynthetic rates (13%) and higher leaf starch concentrations prior to tree flowering (31%), than leaves on outside trees. While these results indicated large long-term impacts on tree growth which must be considered when using open-top chambers, they did not indicate any net effect of chambers on the air pollutant susceptibility of trees which would limit the usefulness of chamber tree data for air quality impact assessment purposes.

  5. BOREAS TGB-1 NSA SF6 Chamber Flux Data

    NASA Technical Reports Server (NTRS)

    Crill, Patrick; Varner, Ruth K.; Hall, Forrest G. (Editor); Conrad, Sara K. (Editor)

    2000-01-01

    The BOREAS TGB-1 team made several chamber and tower measurements of trace gases at sites in the BOREAS NSA. This data set contains sulfur hexafluoride (SF6) dark chamber flux measurements at the NSA-OJP and NSA-YJP sites from 16-May through 13-Sep-1994. Gas samples were extracted approximately every 7 days from dark chambers and analyzed at the NSA lab facility. The data are provided in tabular ASCII files.

  6. Target area chamber system design for the National Ignition Facility

    SciTech Connect

    Wavrik, R.; Boyes, J.; Olson, C.; Dempsey, F.; Garcia, R.; Karpenko, V.; Anderson, A.; Tobin, M.; Latkowski, J.

    1994-06-01

    The National Ignition Facility (NIF) is a proposed Department of Energy facility which will contribute to the resolution of important Defense Program and inertial fusion energy issues for energy production in the future. The NIF will consist of a laser system with 192 independent beamlets transported to a target chamber. The target chamber is a multi-purpose structure that provides the interface between the target and the laser optics. The chamber must be capable of achieving moderate vacuum levels in reasonable times; it must remain dimensionally stable within micron tolerances, provide support for the optics, diagnostics, and target positioner; it must minimize the debris from the x-ray and laser light environments; and it must be capable of supporting external neutron shielding. The chamber must also be fabricated from a low activation material. The fusion reaction in the target gives off neutrons, x-ray and gamma rays. The x-rays and gamma rays interact with the interior of the target chamber wall while neutrons penetrate the wall. In order to minimize the neutron activation of components outside the target chamber and to absorb gammas emitted from the activated chamber, shielding will be placed immediately outside the chamber. The target chamber contains the target positioner. The target positioner moves the target from outside the chamber to the center of the chamber and positions the target at the focal spot of the laser beams. The target positioner must be survivable in a harsh radioactive environment. The materials used must be low activation and have a high stiffness to weight ratio to maintain target stability. This paper describes the conceptual design of the target chamber, target postioner, and shielding for the NIF.

  7. Experience with the jet chamber of the JADE-experiment

    SciTech Connect

    Heuer, R.D.

    1984-01-01

    The jet chamber, a pictorial drift chamber used as the central track detector of the JADE experiment at PETRA, is briefly described. The present status of the spatial and dE/dx resolutions and the experience during 4 years of operation is reported. Improvement plans for the readout electronics are described and a short review of the jet chamber designed for the proposed LEP experiment OPAL is given.

  8. MOCVD-derived highly transparent, conductive zinc- and tin-doped indium oxide thin films: precursor synthesis, metastable phase film growth and characterization, and application as anodes in polymer light-emitting diodes.

    PubMed

    Ni, Jun; Yan, He; Wang, Anchuang; Yang, Yu; Stern, Charlotte L; Metz, Andrew W; Jin, Shu; Wang, Lian; Marks, Tobin J; Ireland, John R; Kannewurf, Carl R

    2005-04-20

    Four diamine adducts of bis(hexafluoroacetylacetonato)zinc [Zn(hfa)(2).(diamine)] can be synthesized in a single-step reaction. Single crystal X-ray diffraction studies reveal monomeric, six-coordinate structures. The thermal stabilities and vapor phase transport properties of these new complexes are considerably greater than those of conventional solid zinc metal-organic chemical vapor deposition (MOCVD) precursors. One of the complexes in the series, bis(1,1,1,5,5,5-hexafluoro-2,4-pentadionato)(N,N'-diethylethylenediamine)zinc, is particularly effective in the growth of thin films of the transparent conducting oxide Zn-In-Sn-O (ZITO) because of its superior volatility and low melting point of 64 degrees C. ZITO thin films with In contents ranging from 40 to 70 cation % (a metastable phase) were grown by low-pressure MOCVD. These films exhibit conductivity as high as 2900 S/cm and optical transparency comparable to or greater than that of commercial Sn-doped indium oxide (ITO) films. ZITO films with the nominal composition of ZnIn(2.0)Sn(1.5)O(z)() were used in fabrication of polymer light-emitting diodes. These devices exhibit light outputs and current efficiencies almost 70% greater than those of ITO-based control devices. PMID:15826201

  9. Metal-Organic Chemical Vapor Deposition (MOCVD) Synthesis of Heteroepitaxial Pr0.7Ca0.3MnO3 Films: Effects of Processing Conditions on Structural/Morphological and Functional Properties.

    PubMed

    Catalano, Maria R; Cucinotta, Giuseppe; Schilirò, Emanuela; Mannini, Matteo; Caneschi, Andrea; Lo Nigro, Raffaella; Smecca, Emanuele; Condorelli, Guglielmo G; Malandrino, Graziella

    2015-08-01

    Calcium-doped praseodymium manganite films (Pr0.7Ca0.3MnO3, PCMO) were prepared by metal-organic chemical vapor deposition (MOCVD) on SrTiO3 (001) and SrTiO3 (110) single-crystal substrates. Structural characterization through X-ray diffraction (XRD) measurements and transmission electron microscopy (TEM) analyses confirmed the formation of epitaxial PCMO phase films. Energy dispersive X-ray (EDX) and X-ray photoelectron spectroscopy (XPS) characterization was used to confirm lateral and vertical composition and the purity of the deposited films. Magnetic measurements, obtained in zero-field-cooling (ZFC) and field-cooling (FC) modes, provided evidence of the presence of a ferromagnetic (FM) transition temperature, which was correlated to the transport properties of the film. The functional properties of the deposited films, combined with the structural and chemical characterization collected data, indicate that the MOCVD approach represents a suitable route for the growth of pure, good quality PCMO for the fabrication of novel spintronic devices. PMID:26478849

  10. Metal-Organic Chemical Vapor Deposition (MOCVD) Synthesis of Heteroepitaxial Pr0.7Ca0.3MnO3 Films: Effects of Processing Conditions on Structural/Morphological and Functional Properties

    PubMed Central

    Catalano, Maria R; Cucinotta, Giuseppe; Schilirò, Emanuela; Mannini, Matteo; Caneschi, Andrea; Lo Nigro, Raffaella; Smecca, Emanuele; Condorelli, Guglielmo G; Malandrino, Graziella

    2015-01-01

    Calcium-doped praseodymium manganite films (Pr0.7Ca0.3MnO3, PCMO) were prepared by metal-organic chemical vapor deposition (MOCVD) on SrTiO3 (001) and SrTiO3 (110) single-crystal substrates. Structural characterization through X-ray diffraction (XRD) measurements and transmission electron microscopy (TEM) analyses confirmed the formation of epitaxial PCMO phase films. Energy dispersive X-ray (EDX) and X-ray photoelectron spectroscopy (XPS) characterization was used to confirm lateral and vertical composition and the purity of the deposited films. Magnetic measurements, obtained in zero-field-cooling (ZFC) and field-cooling (FC) modes, provided evidence of the presence of a ferromagnetic (FM) transition temperature, which was correlated to the transport properties of the film. The functional properties of the deposited films, combined with the structural and chemical characterization collected data, indicate that the MOCVD approach represents a suitable route for the growth of pure, good quality PCMO for the fabrication of novel spintronic devices. PMID:26478849

  11. Vacuum Chamber for the Measurement System of the Beam Energy

    NASA Astrophysics Data System (ADS)

    Abakumova, E.; Achasov, M.; Dong, HaiYi; Qu, HuaMin; Krasnov, A.; Kosarev, A.; Muchnoi, N.; Pyata, E.; Xiao, Qiong; Mo, XiaoHu; Wang, YiFang; Zhukov, A.

    Vacuum chamber for the beam energy measurement system based on the Compton backscattering method is presented. The main elements of the chamber are GaAs entrance viewport and a copper mirror. The viewport design provides baking out of the vacuum chamber up to 250 °C. To produce the viewport, an original technology based on brazing GaAs plate by lead has been developed. The vacuum chambers were installed at the BEPC-II and VEPP-4 M colliders. After installation the residual gas pressure is about 10-10 Torr.

  12. Determination of molecular contamination performance for space chamber tests

    NASA Technical Reports Server (NTRS)

    Scialdone, J. J.

    1973-01-01

    The limitations of chamber tests with regard to the molecular contamination of a spacecraft undergoing vacuum test were examined. The molecular flow conditions existing in the chamber and the parameters dictating the degree of contamination were analyzed. Equations and graphs were developed to show the fraction of molecules returning to the spacecraft out of those emitted and to show other chamber flow parameters as a function of chamber and spacecraft surface molecular pumping and geometric configuration. Type and location of instruments required to measure the outgassing, the degree of contamination, and the returning flows are also discussed.

  13. Space shuttle orbit maneuvering engine reusable thrust chamber program

    NASA Technical Reports Server (NTRS)

    Senneff, J. M.

    1975-01-01

    The feasibility of potential reusable thrust chamber concepts is studied. Propellant condidates were examined and analytically combined with potential cooling schemes. A data base of engine data which would assist in a configuration selection was produced. The data base verification was performed by the demonstration of a thrust chamber of a selected coolant scheme design. A full scale insulated columbium thrust chamber was used for propellant coolant configurations. Combustion stability of the injectors and a reduced size thrust chamber were experimentally verified as proof of concept demonstrations of the design and study results.

  14. Comsol Simulations as a Tool in Validating a Measurement Chamber

    NASA Astrophysics Data System (ADS)

    Lakka, Antti; Sairanen, Hannu; Heinonen, Martti; Högström, Richard

    2015-12-01

    The Centre for Metrology and Accreditation (MIKES) is developing a temperature-humidity calibration system for radiosondes. The target minimum air temperature and dew-point temperature are -80° C and -90° C, respectively. When operating in this range, a major limiting factor is the time of stabilization which is mainly affected by the design of the measurement chamber. To find an optimal geometry for the chamber, we developed a numerical simulation method taking into account heat and mass transfer in the chamber. This paper describes the method and its experimental validation using two stainless steel chambers with different geometries. The numerical simulation was carried out using Comsol Multiphysics simulation software. Equilibrium states of dry air flow at -70° C with different inlet air flow rates were used to determine the geometry of the chamber. It was revealed that the flow is very unstable despite having relatively small Reynolds number values. Humidity saturation abilities of the new chamber were studied by simulating water vapor diffusion in the chamber in time-dependent mode. The differences in time of humidity stabilization after a step change were determined for both the new chamber model and the MIKES Relative Humidity Generator III (MRHG) model. These simulations were used as a validation of the simulation method along with experimental measurements using a spectroscopic hygrometer. Humidity saturation stabilization simulations proved the new chamber to be the faster of the two, which was confirmed by experimental measurements.

  15. Discharge Chamber Primary Electron Modeling Activities in Three-Dimensions

    NASA Technical Reports Server (NTRS)

    Steuber, Thomas J.

    2004-01-01

    Designing discharge chambers for ion thrusters involves many geometric configuration decisions. Various decisions will impact discharge chamber performance with respect to propellant utilization efficiency, ion production costs, and grid lifetime. These hardware design decisions can benefit from the assistance of computational modeling. Computational modeling for discharge chambers has been limited to two-dimensional codes that leveraged symmetry for interpretation into three-dimensional analysis. This paper presents model development activities towards a three-dimensional discharge chamber simulation to aid discharge chamber design decisions. Specifically, of the many geometric configuration decisions toward attainment of a worthy discharge chamber, this paper focuses on addressing magnetic circuit considerations with a three-dimensional discharge chamber simulation as a tool. With this tool, candidate discharge chamber magnetic circuit designs can be analyzed computationally to gain insight into factors that may influence discharge chamber performance such as: primary electron loss width in magnetic cusps, cathode tip position with respect to the low magnetic field volume, definition of a low magnetic field region, and maintenance of a low magnetic field region across the grid span. Corroborating experimental data will be obtained from mockup hardware tests. Initially, simulated candidate magnetic circuit designs will resemble previous successful thruster designs. To provide opportunity to improve beyond previous performance benchmarks, off-design modifications will be simulated and experimentally tested.

  16. The Other Shoe: An Early Operant Conditioning Chamber for Pigeons.

    PubMed

    Sakagami, Takayuki; Lattal, Kennon A

    2016-05-01

    We describe an early operant conditioning chamber fabricated by Harvard University instrument maker Ralph Gerbrands and shipped to Japan in 1952 in response to a request of Professor B. F. Skinner by Japanese psychologists. It is a rare example, perhaps the earliest still physically existing, of such a chamber for use with pigeons. Although the overall structure and many of the components are similar to contemporary pigeon chambers, several differences are noted and contrasted to evolutionary changes in this most important laboratory tool in the experimental analysis of behavior. The chamber also is testimony to the early internationalization of behavior analysis. PMID:27606188

  17. A Regeneratively-Cooled Thrust Chamber for the Fastrac Engine

    NASA Technical Reports Server (NTRS)

    Brown, Kendall; Sparks, Dave; Woodcock, Gordon; Jim Turner (Technical Monitor)

    2000-01-01

    This document consists of presentation slides about the development of the regeneratively cooled thrust chamber for the Fastrac engine. The Fastrac engine was originally developed to demonstrate low cost design and fabrication methods. It was intended to be used in an expendable booster. The regen thrust chamber enables a more cost efficient test program. Using the low cost design and fabrication methodology designed for the 12K regeneratively cooled chamber, the contractor designed, developed and fabricated a regeneratively cooled thrust chamber for the Fastrac engine.

  18. Formed platelets for low cost regeneratively cooled rocket combustion chambers

    NASA Astrophysics Data System (ADS)

    Burkhardt, Wendel M.

    1992-02-01

    The ongoing work performed to demonstrate the fabrication feasibility of a formed platelet regeneratively cooled combustion chamber liner is described. The combustion chambers are fabricated in three or four axial sections from formed platelet stacks joined together. The platelets are etched, stacked, and bonded into flat panels that contain the regen passages. The flat panels are formed into the final contour with a die. The formed platelet approach takes advantage of the inherent low cost, high accuracy, and thin wall capability of photoetched platelet technology to fabricate long life, low cost rocket combustion chambers. Combustion chamber liner sections were fabricated with extremely thin (tw = 0.20 mm (0.008-in.)) hot gas side walls and very high aspect ratio coolant channels (aspect ratio greater than 10:1). Combustion chamber liner sections were formed of both Zr-Cu and stainless steel. The results of both the forming of individual panels and the joining of panels together are discussed. Work performed demonstrating the feasibility of rocket combustion chamber liners from formed platelets is described. A discussion of the benefits of chamber liners so constructed and of a chamber producing 176,000 N (40 Klbf) of thrust currently fabricated is presented. The results of a study examining the forming of large scale platelet panels for an Space Shuttle Main Engine (SSME) Main Combustion Chamber (MCC) liner are included.

  19. Evaluation of Vortex Chamber Concepts for Liquid Rocket Engine Applications

    NASA Technical Reports Server (NTRS)

    Trinh, Huu Phuoc; Knuth, Williams; Michaels, Scott; Turner, James E. (Technical Monitor)

    2000-01-01

    Rocket-based combined-cycle engines (RBBC) being considered at NASA for future generation launch vehicles feature clusters of small rocket thrusters as part of the engine components. Depending on specific RBBC concepts, these thrusters may be operated at various operating conditions including power level and/or propellant mixture ratio variations. To pursue technology developments for future launch vehicles, NASA/Marshall Space Flight Center (MSFC) is examining vortex chamber concepts for the subject cycle engine application. Past studies indicated that the vortex chamber schemes potentially have a number of advantages over conventional chamber methods. Due to the nature of the vortex flow, relatively cooler propellant streams tend to flow along the chamber wall. Hence, the thruster chamber can be operated without the need of any cooling techniques. This vortex flow also creates strong turbulence, which promotes the propellant mixing process. Consequently, the subject chamber concepts not only offer the system simplicity but they also would enhance the combustion performance. The test results showed that the chamber performance was markedly high even at a low chamber length-to- diameter ratio (L/D). This incentive can be translated to a convenience in the thrust chamber packaging.

  20. Hot fire fatigue testing results for the compliant combustion chamber

    NASA Technical Reports Server (NTRS)

    Pavli, Albert J.; Kazaroff, John M.; Jankovsky, Robert S.

    1992-01-01

    A hydrogen-oxygen subscale rocket combustion chamber was designed incorporating an advanced design concept to reduce strain and increase life. The design permits unrestrained thermal expansion of a circumferential direction and, thereby, provides structural compliance during the thermal cycling of hot-fire testing. The chamber was built and test fired at a chamber pressure of 4137 kN/sq m (600 psia) and a hydrogen-oxygen mixture ratio of 6.0. Compared with a conventional milled-channel configuration, the new structurally compliant chamber had a 134 or 287 percent increase in fatigue life, depending on the life predicted for the conventional configuration.