Science.gov

Sample records for near-surface non-destructive examination

  1. Non-destructive examination system of vitreous body

    NASA Astrophysics Data System (ADS)

    Shibata, Takuma; Gong, Jin; Watanabe, Yosuke; Kabir, M. Hasnat; Masato, Makino; Furukawa, Hidemitsu; Nishitsuka, Koichi

    2014-04-01

    Eyeball plays a quite important role in acquiring the vision. Vitreous body occupies the largest part of the eyeball and consists of biological, elastic, transparent, gel materials. In the present medical examination, the non-destructive examination method of the vitreous body has not been well established. Here, we focus on an application of dynamic light scattering to this topic. We tried to apply our lab-made apparatus, scanning microscopic light scattering (SMILS), which was specially designed for observing the nanometer-scale network structure in gel materials. In order to examine the vitreous body using SMILS method, a commercial apparatus, nano Partica (Horiba Co. Ltd.) was also customized. We analyzed vitreous body using both the SMILS and the customized nano Partica. We successfully examined the vitreous bodies of healthy pigs in non-destructive way.

  2. EVALUATION OF TRANSPORTATION OPTIONS FOR INTERMEDIATE NON DESTRUCTIVE EXAMINATIONS

    SciTech Connect

    Case, Susan; Hoggard, Gary

    2014-07-01

    Idaho National Laboratory (INL) shipments of irradiated experiments from the Advanced Test Reactor (ATR) to the Hot Fuels Examination Facility (HFEF) have historically been accomplished using the General Electric Model 2000 (GE 2000) Type B shipping container. Battelle Energy Alliance (BEA) concerns regarding the future availability and leasing and handling costs associated with the GE 2000 cask have warranted an evaluation of alternative shipping options. One or more of these shipping options may be utilized to perform non destructive examinations (NDE) such as neutron radiography and precision gamma scans of irradiated experiments at HFEF and then return the experiments to ATR for further irradiation, hereafter referred to as “intermediate NDE.”

  3. Non-destructive X-ray examination of weft knitted wire structures

    NASA Astrophysics Data System (ADS)

    Obermann, M.; Ellouz, M.; Aumann, S.; Martens, Y.; Bartelt, P.; Klöcker, M.; Kordisch, T.; Ehrmann, A.; Weber, M. O.

    2016-07-01

    Conductive yarns or wires are often integrated in smart textiles to enable data or energy transmission. In woven fabrics, these conductive parts are fixed at defined positions and thus protected from external loads. Knitted fabrics, however, have relatively loose structures, resulting in higher impacts of possible mechanical forces on the individual yarns. Hence, metallic wires with smaller diameters in particular are prone to break when integrated in knitted fabrics. In a recent project, wires of various materials including copper, silver and nickel with diameters varying between 0.05 mm and 0.23 mm were knitted in combination with textile yarns. Hand flat knitting machines of appropriate gauges were used to produce different structures. On these samples, non-destructive examinations, using an industrial X-ray system Seifert x|cube (225 kV) equipped with a minifocus X-ray tube, were carried out, directly after knitting as well as after different mechanical treatments (tensile, burst, and washing tests). In this way, structural changes of the stitch geometry could be visualized before failure. In this paper, the loop geometries in the knitted fabrics are depicted depending on knitted structures, wire properties and the applied mechanical load. Consequently, it is shown which metallic wires and yarns are most suitable to be integrated into knitted smart textiles.

  4. Near-surface structural examination of human tooth enamel subject to in vitro demineralization and remineralization

    NASA Astrophysics Data System (ADS)

    Gaines, Carmen Veronica

    The early stages of chemical tooth decay are governed by dynamic processes of demineralization and remineralization of dental enamel that initiates along the surface of the tooth. Conventional diagnostic techniques lack the spatial resolution required to analyze near-surface structural changes in enamel at the submicron level. In this study, slabs of highly-polished, decay-free human enamel were subjected to 0.12M EDTA and buffered lactic acid demineralizing agents and MI Paste(TM) and calcifying (0.1 ppm F) remineralizing treatments in vitro. Grazing incidence x-ray diffraction (GIXD), a technique typically used for thin film analysis, provided depth profiles of crystallinity changes in surface enamel with a resolution better than 100 nm. In conjunction with nanoindentation, a technique gaining acceptance as a means of examining the mechanical properties of sound enamel, these results were corroborated with well-established microscopy and Raman techniques to assess the nanohardness, morphologies and chemical nature of treated enamel. Interestingly, the average crystallite size of surface enamel along its c-axis dimension increased by nearly 40% after a 60 min EDTA treatment as detected by GIXD. This result was in direct contrast to the obvious surface degradation observed by microscopic and confocal Raman imaging. A decrease in nanohardness from 4.86 +/- 0.44 GPa to 0.28 +/- 0.10 GPa was observed. Collective results suggest that mineral dissolution characteristics evident on the micron scale may not be fully translated to the nanoscale in assessing the integrity of chemically-modified tooth enamel. While an intuitive decrease in enamel crystallinity was observed with buffered lactic acid-treated samples, demineralization was too slow to adequately quantify the enamel property changes seen. MI Paste(TM) treatment of EDTA-demineralized enamel showed preferential growth along the a-axis direction. Calcifying solution treatments of both demineralized sample types

  5. NON-DESTRUCTIVE BEAM MEASUREMENTS.

    SciTech Connect

    BAI,M.

    2004-07-05

    In high energy accelerators, especially storage rings, non-destructive beam measurements are highly desirable to minimize the impact on the beam quality. In principle, the non-destructive tools can be either passive detectors like Schottky, or active devices which excite either longitudinal or transverse beam motions for the corresponding measurements. An example of such a device is an ac dipole, a magnet with oscillating field, which can be used to achieve large coherent betatron oscillations. It has been demonstrated in the Brookhaven AGS that by adiabatically exciting the beam, the beam emittance growth due to the filamentation in the phase space can be avoided. This paper overviews both techniques in general. In particular, this paper also presents the beam tune measurement with a Schottky detector, phase advance measurements as well as nonlinear resonance measurements with the ac dipoles in the Brookhaven RHIC.

  6. Non-Destructive Testing Scanner

    NASA Technical Reports Server (NTRS)

    1990-01-01

    Bio-Imaging Research's technology that originated in an aerospace program has come full circle with a new aerospace adaptation called the Advanced Computed Tomography Inspection System, or ACTIS. The medical version of CT scans the human body for tumors or other abnormalities, the ACTIS system finds imperfections in aerospace structures and components, such as castings, assemblies, rocket motors and nozzles. ACTIS is described by its developer as the most versatile CT scanner available for non-destructive testing applications. ACTIS is a variable geometry system. ACTIS source and detectors can be moved closer together or farther apart to optimize the geometry for different sizes of test objects. The combination of variable geometry, three sources, and focusing detectors makes ACTIS cost effective for a broad range of applications. System can scan anything from very small turbine blades to large rocket assemblies.

  7. Non-destructive identification of twisted light.

    PubMed

    Li, Pengyun; Wang, Bo; Song, Xinbing; Zhang, Xiangdong

    2016-04-01

    The non-destructive identification of the orbital angular momentum (OAM) is essential to various applications in the optical information processing. Here, we propose and demonstrate experimentally an efficient method to identify non-destructively the OAM by using a modified Mach-Zehnder interferometer. Our schemes are applicable not only to the case with integer charges, but also to optical vortices with noninteger charges. Our Letter presents the first experimental demonstration of the non-destructive identification of twisted light with integer or noninteger topological charges, which has potential applications in the OAM-based data transmission for optical communications. PMID:27192290

  8. Method for non-destructive testing

    DOEpatents

    Akers, Douglas W.

    2011-08-30

    Non-destructive testing method may include providing a source material that emits positrons in response to bombardment of the source material with photons. The source material is exposed to photons. The source material is positioned adjacent the specimen, the specimen being exposed to at least some of the positrons emitted by the source material. Annihilation gamma rays emitted by the specimen are detected.

  9. Mathematical models applied in inductive non-destructive testing

    NASA Astrophysics Data System (ADS)

    Wac-Wlodarczyk, A.; Goleman, R.; Czerwinski, D.; Gizewski, T.

    Non-destructive testing are the wide group of investigative methods of non-homogenous material. Methods of computer tomography, ultrasonic, magnetic and inductive methods still developed are widely applied in industry. In apparatus used for non-destructive tests, the analysis of signals is made on the basis of complex system answers. The answer is linearized due to the model of research system. In this paper, the authors will discuss the applications of the mathematical models applied in investigations of inductive magnetic materials. The statistical models and other gathered in similarity classes will be taken into consideration. Investigation of mathematical models allows to choose the correct method, which in consequence leads to precise representation of the inner structure of examined object. Inductive research of conductive media, especially those with ferromagnetic properties, are run with high frequency magnetic field (eddy-currents method), which considerably decrease penetration depth.

  10. Hybrid holographic non-destructive test system

    NASA Technical Reports Server (NTRS)

    Kurtz, R. L. (Inventor)

    1978-01-01

    An automatic hybrid holographic non-destructive testing (HNDT) method and system capable of detecting flaws or debonds contained within certain materials are described. This system incorporates the techniques of optical holography, acoustical/optical holography and holographic correlation in determining the structural integrity of a test object. An automatic processing system including a detector and automatic data processor is used in conjunction with the three holographic techniques for correlating and interpreting the information supplied by the non-destructive systems. The automatic system also includes a sensor which directly translates an optical data format produced by the holographic techniques into electrical signals and then transmits this information to a digital computer for indicating the structural properties of the test object. The computer interprets the data gathered and determines whether further testing is necessary as well as the format of this new testing procedure.

  11. FIRST 100 T NON-DESTRUCTIVE MAGNET

    SciTech Connect

    J. R. SIMS; ET AL

    1999-10-01

    The first 100 T non-destructive (100 T ND) magnet and power supplies as currently designed are described. This magnet will be installed as part of the user facility research equipment at the National High Magnetic Field Laboratory (NHMFL) Pulsed Field Facility at Los Alamos National Laboratory. The 100 T ND magnet will provide a 100 T pulsed field of 5 ms duration (above 90% of full field) in a 15 mm diameter bore once per hour. Magnet operation will be non-destructive. The magnet will consist of a controlled power outer coil set which produces a 47 T platform field in a 225 mm diameter bore. Located within the outer coil set will be a 220 mm outer diameter capacitor powered insert coil. Using inertial energy storage a synchronous motor/generator will provide ac power to a set of seven ac-dc converters rated at 64 MW/80 MVA each. These converters will energize three independent coil circuits to create 170 MJ of field energy in the outer coil set at the platform field of 47 T. The insert will then be energized to produce the balance of the 100 T peak field using a 2.3 MJ, 18 kV (charged to 15 kV), 14.4 mF capacitor bank controlled with solid-state switches. The magnet will be the first of its kind and the first non-destructive, reusable 100 T pulsed magnet. The operation of the magnet will be described along with special features of its design and construction.

  12. Complementary Electromagnetic Non-Destructive Evaluation

    NASA Astrophysics Data System (ADS)

    Tian, Gui Yun; Wilson, John; Morozov, Maxim

    2011-06-01

    The use of non-destructive evaluation (NDE) for defect detection and failure prediction in structures and specimens is widespread in energy industries, aimed at ageing power plants and pipelines, material degradation, fatigue and radiation damage, etc. At present there are no suitable electromagnetic NDE methods for the measurement and characterization of material degradation, in irradiated samples in particular, which is very important and timely for the nuclear power industry in the UK. This paper reports recent developments in the field of electromagnetic (EM) NDE at Newcastle University, including pulsed eddy current (PEC), pulsed magnetic flux leakage (PMFL), magnetic Barkhausen emission (MBE) and magneto-acoustic emission (MAE). As different EM methods have different strengths, an integrative EM framework is introduced. Case studies through the second round robin tests organized by the Universal Network for Magnetic Non-Destructive Evaluation (UNMNDE), representing eighteen leading research groups worldwide in the area of electromagnetic NDE, are reported. Twelve samples with different ageing times and rolling reduction ratios were tested using different magnetic methods among the UNMNDE members. Based on the studies, the complementary characteristics of electromagnetic techniques for NDE are discussed.

  13. Non-destructive testing method and apparatus

    DOEpatents

    Akers, Douglas W.

    2011-10-04

    Non-destructive testing apparatus may comprise a photon source and a source material that emits positrons in response to bombardment of the source material with photons. The source material is positionable adjacent the photon source and a specimen so that when the source material is positioned adjacent the photon source it is exposed to photons produced thereby. When the source material is positioned adjacent the specimen, the specimen is exposed to at least some of the positrons emitted by the source material. A detector system positioned adjacent the specimen detects annihilation gamma rays emitted by the specimen. Another embodiment comprises a neutron source and a source material that emits positrons in response to neutron bombardment.

  14. Non-destructive evaluation of composites

    NASA Technical Reports Server (NTRS)

    Chu, Tsuchin Philip

    1996-01-01

    The composite materials have been used in aerospace industries for quite some time. Several non-destructive evaluation (NDE) methods have been developed to inspect composites in order to detect flaws, matrix cracking, and delamination. These methods include ultrasonics, acoustic emission, shearography, thermography, X-ray, and digital image correlation. The NDE Branch of Marshall Space Flight Center has recently acquired a thermal imaging NDE system. The same system has been used at NASA Langley Research Center for detecting disbonds. In order to compare different NDE methods, three carbon/carbon composite panels were used for experiment using ultrasonic C-scan, shearography, and thermography methods. These panels have teflon inserts to simulate the delamination between plies in a composite panel. All three methods have successfully located the insert. The experiment and results are presented in the following sections.

  15. NON-DESTRUCTIVE FLAW DETECTION APPARATUS

    DOEpatents

    Stateman, M.J.; Holloway, H.R.

    1957-12-17

    An apparatus is described for the non-destructive detection of flaws in electrical conducting articles. The particular feature of the detection apparatus is that a flaw in the front or back of the test article will not be masked by signals caused by the passage of the end and front of the article through the detection apparatus. The present invention alleviates the above problem by mounting detection coils on directly opposite sides of the test passageway so that the axes of the pickup coils are perpendicular to the axis of an energizing coil through which the article is passed. A flaw in the article will cause a change in the voltage induced in one pickup coil, but passage of the end or front of the article will not produce unequal signals. The signals are compared in appropriate electrical circuitry to actuate a recorder only when unequal signals are present, indicating the presence of a flaw.

  16. Cryogenic Storage Tank Non-Destructive Evaluation

    NASA Technical Reports Server (NTRS)

    Arens, Ellen

    2010-01-01

    This slide presentation reviews the work in non-destructive evaluation (NDE) of cryogenic storage tanks. Four large cryogenic tanks, constructed in 1965 with perlite insulation in the annular regions, are of concern. The construction of the tanks, two Liquid Oxygen (LOX) and two Liquid Hydrogen (LH2), are described. The loss rate for the LOX tank at Pad A is slightly higher than that for the one at Pad B. The concerns for the LH2 tank at Pad B are that there is a significantly higher boil-off rate than that at Pad A, that there is mold growth, indicative of increased heat flow, that there is a long down-time needed for repairs, and that 3 of 5 full thermal cycles have been used on the Pad B LH2 tank. The advantages and disadvantages of thermal imaging are given. A detailed description of what is visible of the structures in the infra-red is given and views of the thermal images are included. Missing Perlite is given as the probable cause of the cold spot on the Pad B LH2 tank. There is no indications of problematic cold regions on the Pad A LH2 tank, as shown by the thermal images given in the presentation. There is definite indication of a cold region on the Pad A LOX tank. There is however concerns with thermal imaging, as thermal images can be significantly effected by environmental conditions, image differences on similar days but with different wind speeds. Other effects that must be considered include ambient temperature, humidity levels/dew, and cloud reflections

  17. Non destructive testing of soft body armor

    NASA Astrophysics Data System (ADS)

    Bhise, Karan

    Pristine bullet proof vests are extremely effective at halting pre-determined projectile threats and have saved over 3000 lives. However, the effectiveness of these vests to halt a bullet is seen to decrease over time.Owing to the importance of bullet proof vests over a period of time, tests to determine their effectiveness have been carried out on every batch of vests at the time of inception and at certain time intervals by shooting a bullet through them. A few vests from every batch are picked up and shot at to check for bullet penetration during this process while these results are extrapolated onto the other vests from the batch.One of the main issues with this method is the fact that testing a few jackets among a large set of jackets does not guarantee the safety of every jacket in the entire batch.Further the jackets that are shot-at have the possibility of undergoing substantial damage during the process thus compromising its safety rendering them unsafe for future use.As the vest penetration phenomenon is extremely complex too, there arose a need for a better testing procedure that could not only help ensure more safety, but also save time and money.The new testing procedure proposed a non-destructive evaluation of the jackets that would solve the issues previous faced in testing the vests. This would lead to the building of a portable set up which could be carried to any location to test jackets in a matter of minutes thus saving time and money.

  18. Non-Destructive Testing A Developing Tool in Science and Engineering

    SciTech Connect

    Lin, Lianshan

    2013-01-01

    Non-destructive testing (NDT), sometimes also known as non-destructive inspection (NDI) or non-destructive examination (NDE), has been applied to solve a wide range of science and industry problems including construction, aerospace, nuclear engineering, manufacturing, space exploration, art objects, forensic studies, biological and medical fields, etc. Without any permanent changing or alteration of testing objects, NDT methods provide great advantages such as increased testing reliability, efficiency, and safety, as well as reduced time and cost. Since the second half of the 20th century, NDT technology has seen significant growth. Depending on the physical properties being measured, NDT techniques can be classified into several branches. This article will provide a brief overview of commonly used NDT methods and their up-to-date progresses including optical examination, radiography, acoustic emission, ultrasonic testing and eddy current testing. For extended reviews on many presently used NDT methods, please refer to articles by Mullins [1, 2].

  19. NON-DESTRUCTIVE SOIL CARBON ANALYZER.

    SciTech Connect

    Wielopolski, Lucian; Hendrey, G.; Orion, I.; Prior, S.; Rogers, H.; Runion, B.; Torbert, A.

    2004-02-01

    This report describes the feasibility, calibration, and safety considerations of a non-destructive, in situ, quantitative, volumetric soil carbon analytical method based on inelastic neutron scattering (INS). The method can quantify values as low as 0.018 gC/cc, or about 1.2% carbon by weight with high precision under the instrument's configuration and operating conditions reported here. INS is safe and easy to use, residual soil activation declines to background values in under an hour, and no radiological requirements are needed for transporting the instrument. The labor required to obtain soil-carbon data is about 10-fold less than with other methods, and the instrument offers a nearly instantaneous rate of output of carbon-content values. Furthermore, it has the potential to quantify other elements, particularly nitrogen. New instrumentation was developed in response to a research solicitation from the U.S. Department of Energy (DOE LAB 00-09 Carbon Sequestration Research Program) supporting the Terrestrial Carbon Processes (TCP) program of the Office of Science, Biological and Environmental Research (BER). The solicitation called for developing and demonstrating novel techniques for quantitatively measuring changes in soil carbon. The report includes raw data and analyses of a set of proof-of-concept, double-blind studies to evaluate the INS approach in the first phase of developing the instrument. Managing soils so that they sequester massive amounts of carbon was suggested as a means to mitigate the atmospheric buildup of anthropogenic CO{sub 2}. Quantifying changes in the soils' carbon stocks will be essential to evaluating such schemes and documenting their performance. Current methods for quantifying carbon in soil by excavation and core sampling are invasive, slow, labor-intensive and locally destroy the system being observed. Newly emerging technologies, such as Laser Induced Breakdown Spectroscopy and Near-Infrared Spectroscopy, offer soil

  20. Edward's sword? - A non-destructive study of a medieval king's sword

    SciTech Connect

    Segebade, Chr.

    2013-04-19

    Non-destructive and instrumental methods including photon activation analysis were applied in an examination of an ancient sword. It was tried to find indication of forgery or, if authentic, any later processing and alteration. Metal components of the hilt and the blade were analysed by instrumental photon activation. Non-destructive metallurgical studies (hardness measurements, microscopic microstructure analysis) are briefly described, too. The results of these investigations did not yield indication of non-authenticity. This stood in agreement with the results of stylistic and scientific studies by weapon experts.

  1. Edward's sword? - A non-destructive study of a medieval king's sword

    NASA Astrophysics Data System (ADS)

    Segebade, Chr.

    2013-04-01

    Non-destructive and instrumental methods including photon activation analysis were applied in an examination of an ancient sword. It was tried to find indication of forgery or, if authentic, any later processing and alteration. Metal components of the hilt and the blade were analysed by instrumental photon activation. Non-destructive metallurgical studies (hardness measurements, microscopic microstructure analysis) are briefly described, too. The results of these investigations did not yield indication of non-authenticity. This stood in agreement with the results of stylistic and scientific studies by weapon experts.

  2. Near surface analysis

    NASA Technical Reports Server (NTRS)

    Johnson, Gordon G.

    1993-01-01

    This is a study to assist in the understanding of earth near surface structure. Higher order moments are used to detect the density distribution as well as to seek patterns found in geological structures. It is shown how higher order moments at points outside a mass structure are determined as well as how to recover the mass distribution from the higher order moments. It is interesting to note that the first moment at a point P outside the mass structure, V(sub O)(P), is the entire mass and the second moment, V(sub 1)(P), is the potential at P due to the mass structure. Usually only the mass and the potential function are used to determine the density distribution in a body. An infinite function sequence (V(sub n)(P))(sub n=0)(sup infinity) is required to uniquely determine the density distribution.

  3. Near surface observations

    NASA Technical Reports Server (NTRS)

    1982-01-01

    Learning objectives include: (1) developing an understanding of the implications of the term "near surface observations"; (2) associating the appearance of large ground features as seen in satellite imagery with their appearance as seen from the ground; (3) grasping criteria and procedures for selecting training sites on the ground for use in supervised classification; (4) running through an example of training site selection; (5) becoming familiar with several methods of accuracy assessment; (6) becoming aware of the approach and value of making supporting measurements of the spectral and physical properties of materials on the ground and from aircraft; (7) taking note of the different types of instruments used in making specific ground measurements; and (8) appreciating the rationale underlying laboratory and field studies on or near the Earth's surface for the purpose of developing new sensor systems.

  4. Rapid, Non-Destructive Estimation of Leaf Area on Field-Grown Vitis labruscana Grapevines

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Three potential variables, shoot basal diameter, leaf count per shoot and shoot length, were examined as potential rapid, non-destructive methods for estimating leaf area per shoot, a frequent component of estimates of leaf area per vine. The metrics were recorded in large field-grown vines over fi...

  5. Non-Destructive Classification Approaches for Equilibrated Ordinary Chondrites

    NASA Astrophysics Data System (ADS)

    Righter, K.; Harrington, R.; Schroeder, C.; Morris, R. V.

    2013-09-01

    In order to compare a few non-destructive classification techniques with the standard approaches, we have characterized a group of chondrites from the Larkman Nunatak region using magnetic susceptibility and Mössbauer spectroscopy.

  6. NON-DESTRUCTIVE TESTING METHODS FOR GEOTHERMAL PIPING.

    SciTech Connect

    BERNDT,M.L.

    2001-03-23

    Non-destructive testing is a key component of optimized plant inspection and maintenance programs. Risk based inspection, condition based maintenance and reliability centered maintenance systems all require detection, location and sizing of defects or flaws by non-destructive methods. Internal damage of geothermal piping by corrosion and erosion-corrosion is an ongoing problem requiring inspection and subsequent maintenance decisions to ensure safe and reliable performance. Conventional manual ultrasonic testing to determine remaining wall thickness has major limitations, particularly when damage is of a random and localized nature. Therefore, it is necessary to explore alternative non-destructive methods that offer potential benefits in terms of accurate quantification of size, shape and location of damage, probability of detection, ability to use on-line over long ranges, and economics. A review of non-destructive methods and their applicability to geothermal piping was performed. Based on this, ongoing research will concentrate on long range guided wave and dynamic methods.

  7. Non-destructive testing and fracture mechanics: A short discussion

    NASA Astrophysics Data System (ADS)

    Zerbst, Uwe; Heckel, Thomas; Carboni, Michele

    2016-02-01

    A short discussion is provided on the relationship between non-destructive testing and fracture mechanics. The basic tasks behind this are to guarantee the safety of a component at a potential hazard loading event, to specify inspection intervals or, alternatively, of demands on non-destructive testing for a fixed inspection regime, to plan accompanying actions for cases of temporary continued operation of structures in which cracks have been detected, and, finally, fatigue strength considerations which take into account initial defects.

  8. Non destructive examination of immersed structures within liquid sodium

    SciTech Connect

    Baque, F.; Paumel, K.; Corneloup, G.; Ploix, M. A.; Augem, J. M.

    2011-07-01

    The In Service Inspection of internal structures of future liquid sodium cooled fast reactors implies, among different options, the use of ultrasounds from the outside of sodium circuit. In these conditions, ultrasounds have to propagate through the metallic envelope of main vessel, then other immersed plates. Thus the study aims at mastering ultrasonic propagation in these multilayered structures in order to determine the best conditions allowing NDT of a plate behind some screens. The necessity of propagating a maximum of energy through bounded media orientated the study towards Lamb waves. Those are often employed for singles plates or solid layers but they are less usual for liquid/solid alternations. Theoretical results are obtained using transfer matrix method. They are compared to in water experimental measurements. Cases with one, two and three parallel plates without then with an artificial defect are presented for identical and different thicknesses of plates. Results show that an artificial crack defect is obviously detected in a plate located behind one and two screens. Measured attenuation is compatible with industrial NDT conditions. Thus a promising potential is shown for this inspection technique. (authors)

  9. Non-destructive testing of the MEGAPIE target

    NASA Astrophysics Data System (ADS)

    Dai, Y.; Wohlmuther, M.; Boutellier, V.; Hahl, S.; Lagotzki, A.; Leu, H.; Linder, H. P.; Schwarz, R.; Spahr, A.; Zanini, L.; Kuster, D.; Gavillet, D.; Wagner, W.

    2016-01-01

    Non-destructive testing (NDT) is one important part of the post-irradiation examination (PIE) of the MEGAPIE target. It includes visual inspection and ultrasonic measurement of the beam window of the T91 LBE container and gamma mapping of the beam window of the AlMg3 safety-container. The visual inspection showed no visible failure in the proton beam window area of the T91 LBE container. The ultrasonic measurement demonstrated no detectable change in the wall thickness of the T91 beam window, which implies no severe corrosion effect induced by flowing LBE during the four-month irradiation period. The gamma mapping provided the distribution of 22Na, a spallation product, in the proton beam window area of the AlMg3 safety-container. The result was used to evaluate the accumulated proton fluence distribution profile, the input data for determining irradiation parameters. A maximum proton fluence of 1.9 × 1025 p/m2 was deduced. The corresponding displacement damage degree in the T91 beam window was 7.1 dpa.

  10. Non-destructive methods for food texture assessment

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Food texture is important to the successful marketing and profitability of food products. Non-destructive sensing would allow food producers and processors to inspect, sort, grade, or track individual product items, so that they can deliver consistent, superior food products to the marketplace. Over...

  11. Automated Non-Destructive Testing Array Evaluation System

    SciTech Connect

    Wei, T; Zavaljevski, N; Bakhtiari, S; Miron, A; Kupperman, D

    2004-12-24

    Automated Non-Destructive Testing Array Evaluation System (ANTARES) sofeware alogrithms were developed for use on X-probe(tm) data. Data used for algorithm development and preliminary perfomance determination was obtained for USNRC mock-up at Argone and data from EPRI.

  12. Non-Destructive Techniques Based on Eddy Current Testing

    PubMed Central

    García-Martín, Javier; Gómez-Gil, Jaime; Vázquez-Sánchez, Ernesto

    2011-01-01

    Non-destructive techniques are used widely in the metal industry in order to control the quality of materials. Eddy current testing is one of the most extensively used non-destructive techniques for inspecting electrically conductive materials at very high speeds that does not require any contact between the test piece and the sensor. This paper includes an overview of the fundamentals and main variables of eddy current testing. It also describes the state-of-the-art sensors and modern techniques such as multi-frequency and pulsed systems. Recent advances in complex models towards solving crack-sensor interaction, developments in instrumentation due to advances in electronic devices, and the evolution of data processing suggest that eddy current testing systems will be increasingly used in the future. PMID:22163754

  13. Infrared Thermography for Temperature Measurement and Non-Destructive Testing

    PubMed Central

    Usamentiaga, Rubèn; Venegas, Pablo; Guerediaga, Jon; Vega, Laura; Molleda, Julio; Bulnes, Francisco G.

    2014-01-01

    The intensity of the infrared radiation emitted by objects is mainly a function of their temperature. In infrared thermography, this feature is used for multiple purposes: as a health indicator in medical applications, as a sign of malfunction in mechanical and electrical maintenance or as an indicator of heat loss in buildings. This paper presents a review of infrared thermography especially focused on two applications: temperature measurement and non-destructive testing, two of the main fields where infrared thermography-based sensors are used. A general introduction to infrared thermography and the common procedures for temperature measurement and non-destructive testing are presented. Furthermore, developments in these fields and recent advances are reviewed. PMID:25014096

  14. Non-destructive NIR FT Raman analysis of plants

    NASA Astrophysics Data System (ADS)

    Schrader, B.; Klump, H. H.; Schenzel, K.; Schulz, H.

    1999-10-01

    Non-destructive analyses of animal and plant cells and tissues by 'classical' Raman spectroscopy with excitation in the visible range have not been possible since the samples are destroyed photochemically or their fluorescence conceals the Raman spectra completely. When excited with the Nd:YAG laser line at 1064 nm fluorescence-free Raman spectra of animal or plant cells and tissues can be recorded without special preparation. In this paper we concentrate on plants and its constituents: essential oils, natural dyes, flavors, spices, alkaloids and fibers can be characterized. The spectra allow the observation of biochemical processes, to observe the distribution of natural products, application to taxonomy, optimizing plant breeding, the harvesting time and control of food—everything non-destructively in living plants!

  15. Non-destructive techniques based on eddy current testing.

    PubMed

    García-Martín, Javier; Gómez-Gil, Jaime; Vázquez-Sánchez, Ernesto

    2011-01-01

    Non-destructive techniques are used widely in the metal industry in order to control the quality of materials. Eddy current testing is one of the most extensively used non-destructive techniques for inspecting electrically conductive materials at very high speeds that does not require any contact between the test piece and the sensor. This paper includes an overview of the fundamentals and main variables of eddy current testing. It also describes the state-of-the-art sensors and modern techniques such as multi-frequency and pulsed systems. Recent advances in complex models towards solving crack-sensor interaction, developments in instrumentation due to advances in electronic devices, and the evolution of data processing suggest that eddy current testing systems will be increasingly used in the future. PMID:22163754

  16. Non-destructive metallurgical analysis of astrolabes utilizing synchrotron radiation.

    SciTech Connect

    Newbury, B.; Stephenson, B.; Almer, J. D.; Notis, M.; Haeffner, D. R.; Slade Cargill, G., III

    2002-05-22

    From the experiments performed it is possible to determine a wide range of information about the metallurgy of the astrolabes studied. It was found that different brass alloys were used for components that were cast and those that were mechanically deformed. Chemical composition, forming history, and thickness measurements are all determined non-destructively, illustrating that this technique could be useful for many applications with metal artifact analysis where non-intrusive methods are required.

  17. Non-Destructive Testing for Control of Radioactive Waste Package

    NASA Astrophysics Data System (ADS)

    Plumeri, S.; Carrel, F.

    2015-10-01

    Characterization and control of radioactive waste packages are important issues in the management of a radioactive waste repository. Therefore, Andra performs quality control inspection on radwaste package before disposal to ensure the compliance of the radwast characteristics with Andra waste disposal specifications and to check the consistency between Andra measurements results and producer declared properties. Objectives of this quality control are: assessment and improvement of producer radwaste packages quality mastery, guarantee of the radwaste disposal safety, maintain of the public confidence. To control radiological characteristics of radwaste package, non-destructive passive methods (gamma spectrometry and neutrons counting) are commonly used. These passive methods may not be sufficient, for instance to control the mass of fissile material contained inside radwaste package. This is particularly true for large concrete hull of heterogeneous radwaste containing several actinides mixed with fission products like 137Cs. Non-destructive active methods, like measurement of photofission delayed neutrons, allow to quantify the global mass of actinides and is a promising method to quantify mass of fissile material. Andra has performed different non-destructive measurements on concrete intermediate-level short lived nuclear waste (ILW-SL) package to control its nuclear material content. These tests have allowed Andra to have a first evaluation of the performance of photofission delayed neutron measurement and to identify development needed to have a reliable method, especially for fissile material mass control in intermediate-level long lived waste package.

  18. Giant Magnetoresistance Sensors: A Review on Structures and Non-Destructive Eddy Current Testing Applications

    PubMed Central

    Rifai, Damhuji; Abdalla, Ahmed N.; Ali, Kharudin; Razali, Ramdan

    2016-01-01

    Non-destructive eddy current testing (ECT) is widely used to examine structural defects in ferromagnetic pipe in the oil and gas industry. Implementation of giant magnetoresistance (GMR) sensors as magnetic field sensors to detect the changes of magnetic field continuity have increased the sensitivity of eddy current techniques in detecting the material defect profile. However, not many researchers have described in detail the structure and issues of GMR sensors and their application in eddy current techniques for nondestructive testing. This paper will describe the implementation of GMR sensors in non-destructive testing eddy current testing. The first part of this paper will describe the structure and principles of GMR sensors. The second part outlines the principles and types of eddy current testing probe that have been studied and developed by previous researchers. The influence of various parameters on the GMR measurement and a factor affecting in eddy current testing will be described in detail in the third part of this paper. Finally, this paper will discuss the limitations of coil probe and compensation techniques that researchers have applied in eddy current testing probes. A comprehensive review of previous studies on the application of GMR sensors in non-destructive eddy current testing also be given at the end of this paper. PMID:26927123

  19. [Study on Non-Destructive Testing of Guqin Interior Structure Based on Computed Tomography].

    PubMed

    Zhao, De-da; Liu, Xing-e; Yang, Shu-min; Yu, Shenz; Tian, Gen-lin; Ma, Jian-feng; Wang, Qing-ping

    2015-12-01

    The wood property and production process affect quality of Guqin. At the same time, Guqin shape with cavity layout relations to the improvement of Guqin technology and inheritance, so it's very important to get the internal cavity characteristics and parameters on the condition of non-destructive the structure of Guqin. The image of interior structure in Guqin was investigated by overall scanning based on non-destructive testing technology of computed tomography, which texture of faceplate, connection method between faceplate and soleplate and interior defects were studied. The three-dimensional reconstruction of Guqin cavity was achieved through Mimics software of surface rendering method and put the two-dimensional CT tomography images convert into three-dimensional, which more complete show interior structural form in Guqin, and finally the parameter of cavity dimensions was obtained. Experimental research shows that there is significant difference in Guqin interior structure between Zhong-ni and Luo-xia type, in which the fluctuation of the interior surfacein Zhong-ni type's is larger than that in Luo-xia type; the interior volume of Zhong-ni typeis less than that of Luo-xia type, especially in Guqin neck. The accurate internal information of Guqin obtained through the computed tomography (CT) technology will provide technical support for the Guqin manufacture craft and the quality examination, as well as provide the reference in the aspect of non-destructive testing for other traditional precious internal structure research. PMID:26964242

  20. Giant Magnetoresistance Sensors: A Review on Structures and Non-Destructive Eddy Current Testing Applications.

    PubMed

    Rifai, Damhuji; Abdalla, Ahmed N; Ali, Kharudin; Razali, Ramdan

    2016-01-01

    Non-destructive eddy current testing (ECT) is widely used to examine structural defects in ferromagnetic pipe in the oil and gas industry. Implementation of giant magnetoresistance (GMR) sensors as magnetic field sensors to detect the changes of magnetic field continuity have increased the sensitivity of eddy current techniques in detecting the material defect profile. However, not many researchers have described in detail the structure and issues of GMR sensors and their application in eddy current techniques for nondestructive testing. This paper will describe the implementation of GMR sensors in non-destructive testing eddy current testing. The first part of this paper will describe the structure and principles of GMR sensors. The second part outlines the principles and types of eddy current testing probe that have been studied and developed by previous researchers. The influence of various parameters on the GMR measurement and a factor affecting in eddy current testing will be described in detail in the third part of this paper. Finally, this paper will discuss the limitations of coil probe and compensation techniques that researchers have applied in eddy current testing probes. A comprehensive review of previous studies on the application of GMR sensors in non-destructive eddy current testing also be given at the end of this paper. PMID:26927123

  1. Investigations and Non-destructive Testing in New Building Design

    NASA Astrophysics Data System (ADS)

    Klimenov, V.; Ovchinnikov, A.; Osipov, S.; Shtein, A.; Ustinov, A.; Danilson, A.

    2016-01-01

    Mechanical rebar couplers are preferable in the advanced building construction and structural design of antiseismic elements. The paper presents destructive inspection techniques used to investigate stress fields (tensile and compressive) and deformation curves for mechanical rebar splicing. The properties of mechanical rebar splicing are investigated by the non-destructive testing digital radiography. The behavior of real connections (column-to- column, beam-to-column) is studied under static and dynamic loads. Investigation results allow the elaboration of recommendations on their application in the universal prefabricated antiseismic structural system developed at Tomsk State University of Architecture and Building, Tomsk, Russia.

  2. Potential techniques for non-destructive evaluation of cable materials

    NASA Astrophysics Data System (ADS)

    Gillen, Kenneth T.; Clough, Roger L.; Mattson, Bengt; Stenberg, Bengt; Oestman, Erik

    This paper describes the connection between mechanical degradation of common cable materials, in radiation and elevated temperature environments, and density increases caused by the oxidation which leads to this degradation. Two techniques based on density changes are suggested as potential non-destructive evaluation (NDE) procedures which may be applicable to monitoring the mechanical condition of cable materials in power plant environments. The first technique is direct measurement of density changes, via a density gradient column, using small shavings removed from the surface of cable jackets at selected locations. The second technique is computed X-ray tomography, utilizing a portable scanning device.

  3. APPARATUS FOR NON-DESTRUCTIVE INSPECTION OF CANTILEVERED MEMBERS

    DOEpatents

    Taylor, E.R.; Mahoney, C.H.; Lay, C.R.

    1961-10-24

    An apparatus for non-destructive inspection of cantilevered members, such as compressor blades, is described. The member under inspection is vibrated with a regulated source of air under pressure. The amplitude of vibration of the member is maintained at its natural frequency. The frequency of vibration of the member is measured. An indication of an excessive decay or erratic shifting in the measured frequency above an allowable hysteretic decay is provided as an indication of a fault in the member. The member is vibrated for a selected test period. (AEC)

  4. Non-destructive characterization using pulsed fast-thermal neutrons

    NASA Astrophysics Data System (ADS)

    Womble, P. C.; Schultz, F. J.; Vourvopoulos, G.

    1995-05-01

    Explosives, illicit drugs, and other contraband materials contain various chemical elements in quantities and ratios that differentiate them from each other and from innocuous substances. Furthermore, the major chemical elements in coal can provide information about various parameters of importance to the coal industry. In both examples, the non-destructive identification of chemical elements can be performed using pulsed fast-thermal neutrons that, through nuclear reactions, excite the nuclei of the various elements. This technique is being currently developed for the dismantling of nuclear weapons classified as trainers, and for the on-line coal bulk analysis.

  5. Non-destructive estimation of foliar carotenoid content of tree species using merged vegetation indices.

    PubMed

    Fassnacht, Fabian E; Stenzel, Stefanie; Gitelson, Anatoly A

    2015-03-15

    Leaf pigment content is an important indicator of plant status and can serve to assess the vigor and photosynthetic activity of plants. The application of spectral information gathered from laboratory, field and remote sensing-based spectrometers to non-destructively assess total chlorophyll (Chl) content of higher plants has been demonstrated in earlier studies. However, the precise estimation of carotenoid (Car) content with non-destructive spectral measurements has so far not reached accuracies comparable to the results obtained for Chl content. Here, we examined the potential of a recently developed angular vegetation index (AVI) to estimate total foliar Car content of three tree species. Based on an iterative search of all possible band combinations, we identified a best candidate AVIcar. The identified index showed quite close but essentially not linear relation with Car contents of the examined species with increasing sensitivity to high Car content and a lack of sensitivity to low Car content for which earlier proposed vegetation indices (VI) performed better. To make use of the advantages of both VI types, we developed a simple merging procedure, which combined the AVIcar with two earlier proposed carotenoid indices. The merged indices had close linear relationship with total Car content and outperformed all other examined indices. The merged indices were able to accurately estimate total Car content with a percental root mean square error (%RMSE) of 8.12% and a coefficient of determination of 0.88. Our findings were confirmed by simulations using the radiative transfer model PROSPECT-5. For simulated data, the merged indices again showed a quasi linear relationship with Car content. This strengthens the assumption that the proposed merged indices have a general ability to accurately estimate foliar Car content. Further examination of the proposed merged indices to estimate foliar Car content of other plant species is desirable to prove the general

  6. Non destructive testing of works of art by terahertz analysis

    NASA Astrophysics Data System (ADS)

    Bodnar, Jean-Luc; Metayer, Jean-Jacques; Mouhoubi, Kamel; Detalle, Vincent

    2013-11-01

    Improvements in technologies and the growing security needs in airport terminals lead to the development of non destructive testing devices using terahertz waves. Indeed, these waves have the advantage of being, on one hand, relatively penetrating. They also have the asset of not being ionizing. It is thus potentially an interesting contribution in the non destructive testing field. With the help of the VISIOM Company, the possibilities of this new industrial analysis method in assisting the restoration of works of art were then approached. The results obtained within this framework are presented here and compared with those obtained by infrared thermography. The results obtained show first that the THZ method, like the stimulated infrared thermography allows the detection of delamination located in murals paintings or in marquetries. They show then that the THZ method seems to allow detecting defects located relatively deeply (10 mm) and defects potentially concealed by other defects. It is an advantage compared to the stimulated infra-red thermography which does not make it possible to obtain these results. Furthermore, they show that the method does not seem sensitive to the various pigments constituting the pictorial layer, to the presence of a layer of "Japan paper" and to the presence of a layer of whitewash. It is not the case of the stimulated infrared thermography. It is another advantage of the THZ method. Finally, they show that the THZ method is limited in the detection of low-size defects. It is a disadvantage compared to the stimulated infrared thermography.

  7. Local defect resonance for sensitive non-destructive testing

    NASA Astrophysics Data System (ADS)

    Adebahr, W.; Solodov, I.; Rahammer, M.; Gulnizkij, N.; Kreutzbruck, M.

    2016-02-01

    Ultrasonic wave-defect interaction is a background of ultrasound activated techniques for imaging and non-destructive testing (NDT) of materials and industrial components. The interaction, primarily, results in acoustic response of a defect which provides attenuation and scattering of ultrasound used as an indicator of defects in conventional ultrasonic NDT. The derivative ultrasonic-induced effects include e.g. nonlinear, thermal, acousto-optic, etc. responses also applied for NDT and defect imaging. These secondary effects are normally relatively inefficient so that the corresponding NDT techniques require an elevated acoustic power and stand out from conventional ultrasonic NDT counterparts for their specific instrumentation particularly adapted to high-power ultrasonic. In this paper, a consistent way to enhance ultrasonic, optical and thermal defect responses and thus to reduce an ultrasonic power required is suggested by using selective ultrasonic activation of defects based on the concept of local defect resonance (LDR). A strong increase in vibration amplitude at LDR enables to reliably detect and visualize the defect as soon as the driving ultrasonic frequency is matched to the LDR frequency. This also provides a high frequency selectivity of the LDR-based imaging, i.e. an opportunity of detecting a certain defect among a multitude of other defects in material. Some examples are shown how to use LDR in non-destructive testing techniques, like vibrometry, ultrasonic thermography and shearography in order to enhance the sensitivity of defect visualization.

  8. Research Performed within the Non-Destructive Evaluation Team at NASA Glenn Research Center

    NASA Technical Reports Server (NTRS)

    Burns, Erin A.

    2004-01-01

    Non-destructive testing is essential in many fields of manufacturing and research in order to perform reliable examination of potentially damaged materials and parts without destroying the inherent structure of the materials. Thus, the Non-Destructive Evaluation (NDE) Team at NASA Glenn Research Center partakes in various projects to improve materials testing equipment as well as analyze materials, material defects, and material deficiencies. Due to the array of projects within the NDE Team at this time, five research aims were supplemental to some current projects. A literature survey of "DE and testing methodologies as related to rocks was performed. Also, Mars Expedition Rover technology was assessed to understand the requirements for instrumentation in harsh space environments (e.g. temperature). Potential instrumentation and technologies were also considered and documented. The literature survey provided background and potential sources for a proposal to acquire funding for ultrasonic instrumentation on board a future Mars expedition. The laboratory uses a Santec Systems AcousticScope AS200 acoustography system. Labview code was written within the current program in order to improve the current performance of the acoustography system. A sample of Reinforced Carbon/Carbon (RCC) material from the leading edge of the space shuttle underwent various non-destructive tests (guided wave scanning, thermography, computed tomography, real time x-ray, etc.) in order to characterize its structure and examine possible defects. Guided wave scan data of a ceramic matrix composite (CMC) panel was reanalyzed utilizing image correlations and signal processing variables. Additional guided wave scans and thermography were also performed on the CMC panel. These reevaluated data and images will be used in future presentations and publications. An additional axis for the guided wave scanner was designed, constructed, and implemented. This additional axis allowed incremental spacing

  9. Non-destructive Raman analyses - polyacetylenes in plants

    NASA Astrophysics Data System (ADS)

    Schrader, Bernhard; Schulz, Hartwig; Baranska, Malgorzata; Andreev, George N.; Lehner, Caroline; Sawatzki, Juergen

    2005-05-01

    Ferdinand Bohlmann has described the isolation, the identification and the structure elucidation of acetylene compounds in many plants, and confirmed it by its synthesis. We have recorded the Raman spectra of most of these plants non-destructively by FT-Raman spectroscopy using radiation at 1064 nm. We could not observe any interfering fluorescence. We found acetylene compounds in some plants, even distinct compounds with different concentration in various parts of it. The distribution of the different compounds over the plant can be observed and their changes during the ontogenesis can be followed by a FT-Raman mapping technique. Of special help is a library of Raman and IR spectra and the structure of the compounds, synthesized by Bohlmann. Thus, the Raman technique allows analyses in a very short time replacing the usual time-consuming separation procedures and avoiding artefacts during clean-up procedures.

  10. Electromagnetic non-destructive technique for duplex stainless steel characterization

    NASA Astrophysics Data System (ADS)

    Rocha, João Vicente; Camerini, Cesar; Pereira, Gabriela

    2016-02-01

    Duplex stainless steel (DSS) is a two-phase (ferrite and austenite) material, which exhibits an attractive combination of mechanical properties and high corrosion resistance, being commonly employed for equipment of petrochemical plants, refining units and oil & gas platforms. The best properties of DSS are achieved when the phases are in equal proportions. However, exposition to high temperatures (e.g. welding process) may entail undesired consequences, such as deleterious phases precipitation (e.g. sigma, chi) and different proportion of the original phases, impairing dramatically the mechanical and corrosion properties of the material. A detailed study of the magnetic behavior of DSS microstructure with different ferrite austenite ratios and deleterious phases content was accomplished. The non destructive method evaluates the electromagnetic properties changes in the material and is capable to identify the presence of deleterious phases into DSS microstructure.

  11. Non-destructive evaluation method employing dielectric electrostatic ultrasonic transducers

    NASA Technical Reports Server (NTRS)

    Yost, William T. (Inventor); Cantrell, Jr., John H. (Inventor)

    2003-01-01

    An acoustic nonlinearity parameter (.beta.) measurement method and system for Non-Destructive Evaluation (NDE) of materials and structural members novelly employs a loosely mounted dielectric electrostatic ultrasonic transducer (DEUT) to receive and convert ultrasonic energy into an electrical signal which can be analyzed to determine the .beta. of the test material. The dielectric material is ferroelectric with a high dielectric constant .di-elect cons.. A computer-controlled measurement system coupled to the DEUT contains an excitation signal generator section and a measurement and analysis section. As a result, the DEUT measures the absolute particle displacement amplitudes in test material, leading to derivation of the nonlinearity parameter (.beta.) without the costly, low field reliability methods of the prior art.

  12. Non-Destructive Classification Approaches for Equilbrated Ordinary Chondrites

    NASA Technical Reports Server (NTRS)

    Righter, K.; Harrington, R.; Schroeder, C.; Morris, R. V.

    2013-01-01

    Classification of meteorites is most effectively carried out by petrographic and mineralogic studies of thin sections, but a rapid and accurate classification technique for the many samples collected in dense collection areas (hot and cold deserts) is of great interest. Oil immersion techniques have been used to classify a large proportion of the US Antarctic meteorite collections since the mid-1980s [1]. This approach has allowed rapid characterization of thousands of samples over time, but nonetheless utilizes a piece of the sample that has been ground to grains or a powder. In order to compare a few non-destructive techniques with the standard approaches, we have characterized a group of chondrites from the Larkman Nunatak region using magnetic susceptibility and Moessbauer spectroscopy.

  13. Non-destructive Faraday imaging of dynamically controlled ultracold atoms

    NASA Astrophysics Data System (ADS)

    Gajdacz, Miroslav; Pedersen, Poul L.; Mørch, Troels; Hilliard, Andrew J.; Arlt, Jan; Sherson, Jacob F.

    2013-08-01

    We describe an easily implementable method for non-destructive measurements of ultracold atomic clouds based on dark field imaging of spatially resolved Faraday rotation. The signal-to-noise ratio is analyzed theoretically and, in the absence of experimental imperfections, the sensitivity limit is found to be identical to other conventional dispersive imaging techniques. The dependence on laser detuning, atomic density, and temperature is characterized in a detailed comparison with theory. Due to low destructiveness, spatially resolved images of the same cloud can be acquired up to 2000 times. The technique is applied to avoid the effect of shot-to-shot fluctuations in atom number calibration, to demonstrate single-run vector magnetic field imaging and single-run spatial imaging of the system's dynamic behavior. This demonstrates that the method is a useful tool for the characterization of static and dynamically changing properties of ultracold atomic clouds.

  14. Non-destructive Faraday imaging of dynamically controlled ultracold atoms

    NASA Astrophysics Data System (ADS)

    Gajdacz, Miroslav; Pedersen, Poul; Mørch, Troels; Hilliard, Andrew; Arlt, Jan; Sherson, Jacob

    2013-05-01

    We investigate non-destructive measurements of ultra-cold atomic clouds based on dark field imaging of spatially resolved Faraday rotation. In particular, we pursue applications to dynamically controlled ultracold atoms. The dependence of the Faraday signal on laser detuning, atomic density and temperature is characterized in a detailed comparison with theory. In particular the destructivity per measurement is extremely low and we illustrate this by imaging the same cloud up to 2000 times. The technique is applied to avoid the effect of shot-to-shot fluctuations in atom number calibration. Adding dynamic changes to system parameters, we demonstrate single-run vector magnetic field imaging and single-run spatial imaging of the system's dynamic behavior. The method can be implemented particularly easily in standard imaging systems by the insertion of an extra polarizing beam splitter. These results are steps towards quantum state engineering using feedback control of ultracold atoms.

  15. Non-destructive Faraday imaging of dynamically controlled ultracold atoms.

    PubMed

    Gajdacz, Miroslav; Pedersen, Poul L; Mørch, Troels; Hilliard, Andrew J; Arlt, Jan; Sherson, Jacob F

    2013-08-01

    We describe an easily implementable method for non-destructive measurements of ultracold atomic clouds based on dark field imaging of spatially resolved Faraday rotation. The signal-to-noise ratio is analyzed theoretically and, in the absence of experimental imperfections, the sensitivity limit is found to be identical to other conventional dispersive imaging techniques. The dependence on laser detuning, atomic density, and temperature is characterized in a detailed comparison with theory. Due to low destructiveness, spatially resolved images of the same cloud can be acquired up to 2000 times. The technique is applied to avoid the effect of shot-to-shot fluctuations in atom number calibration, to demonstrate single-run vector magnetic field imaging and single-run spatial imaging of the system's dynamic behavior. This demonstrates that the method is a useful tool for the characterization of static and dynamically changing properties of ultracold atomic clouds. PMID:24007051

  16. Induction thermography for non-destructive evaluation of adhesive bonds

    NASA Astrophysics Data System (ADS)

    Balaji, L.; Balasubramaniam, Krishnan; Krishnamurthy, C. V.

    2013-01-01

    Adhesive bonding is widely used in automotive industry in the recent times. One of the major problems with adhesive bonds is the lack of a suitable non-destructive evaluation technique for assessing bonding. In this paper, an experimental study was carried out to apply induction thermography technique to evaluate adhesively bonded steel plates. Samples were fabricated with artificial defects such as air gap, foreign material, and improper adhesive filling. Induction thermography technique was found to detect defects and foreign inclusions. The sample specimen was also inspected using standard techniques such as Ultrasonic testing and Radiography testing. Defect detecting capabilities of the three techniques are compared. Induction thermography heating was FE modelled in 3D using COMSOL 3.5a. The simulated Induction thermography model was compared and validated with experimental results.

  17. Non-destructive analysis for the investigation of decomposition phenomena of historical manuscripts and prints

    NASA Astrophysics Data System (ADS)

    Faubel, Werner; Staub, Susanne; Simon, Rolf; Heissler, Stefan; Pataki, Andrea; Banik, Gerhard

    2007-07-01

    As a contribution to the increasing efforts to preserve cultural heritage, historical books as well as illuminated manuscripts endangered by corrosive writing and printing materials or destructive coloring matters, non-destructive analytical methods are highly desirable enabling an in-situ examination of the surface status of an object. The development and application of a novel combination of non-destructive analytic methods based on (a) synchrotron radiation induced micro-X-ray fluorescence (SR-μXRF) and (b) Fourier transform infrared (FTIR) microscope allows to investigate the state as well as the effectiveness of conservation procedures for historical manuscripts. Examples of measurements include (1) an iron gall ink manuscript of a historical memo on legal land description of the year 1769, (2) an original hand colored herbal of the years 1536/38 from the Senckenbergische Bibliothek, Frankfurt, and (3) the incunabula Johannes von Saaz: "Der Ackermann aus Boehmen" fated from 1463 and printed by Albrecht Pfister, Bamberg, owned by the Herzog August Bibliothek, Wolfenbuettel.

  18. Compressive strength evaluation of structural lightweight concrete by non-destructive ultrasonic pulse velocity method.

    PubMed

    Bogas, J Alexandre; Gomes, M Glória; Gomes, Augusto

    2013-07-01

    In this paper the compressive strength of a wide range of structural lightweight aggregate concrete mixes is evaluated by the non-destructive ultrasonic pulse velocity method. This study involves about 84 different compositions tested between 3 and 180 days for compressive strengths ranging from about 30 to 80 MPa. The influence of several factors on the relation between the ultrasonic pulse velocity and compressive strength is examined. These factors include the cement type and content, amount of water, type of admixture, initial wetting conditions, type and volume of aggregate and the partial replacement of normal weight coarse and fine aggregates by lightweight aggregates. It is found that lightweight and normal weight concretes are affected differently by mix design parameters. In addition, the prediction of the concrete's compressive strength by means of the non-destructive ultrasonic pulse velocity test is studied. Based on the dependence of the ultrasonic pulse velocity on the density and elasticity of concrete, a simplified expression is proposed to estimate the compressive strength, regardless the type of concrete and its composition. More than 200 results for different types of aggregates and concrete compositions were analyzed and high correlation coefficients were obtained. PMID:23351273

  19. Non-destructive Testing of Forged Metallic Materials by Active Infrared Thermography

    NASA Astrophysics Data System (ADS)

    Maillard, S.; Cadith, J.; Bouteille, P.; Legros, G.; Bodnar, J. L.; Detalle, V.

    2012-11-01

    Nowadays, infrared thermography is considered as the reference method in many applications such as safety, the inspection of electric installations, or the inspection of buildings' heat insulation. In recent years, the evolution of both material and data-processing tools also allows the development of thermography as a real non-destructive testing method. Thus, by subjecting the element to be inspected to an external excitation and by analyzing the propagation of heat in the examined zone, it is possible to highlight surface or subsurface defects such as cracks, delaminations, or corrosion. One speaks then about active infrared thermography. In this study, some results obtained during the collective studies carried out by CETIM and the University of Reims for the forging industry are presented. Various experimental possibilities offered by active thermography are presented and the interest in this method in comparison with the traditional non-destructive testing methods (penetrant testing and magnetic particle inspection) is discussed. For example, comparative results on a forged cracked hub, a steering joint, and a threaded rod are presented. They highlight the interest of infrared thermography stimulated by induction for forged parts.

  20. Scanning Acoustic Microscopy for Characterization of Coatings and Near-Surface Features of Ceramics

    SciTech Connect

    Qu, Jun; Blau, Peter Julian

    2006-01-01

    Scanning Acoustic Microscopy (SAcM) has been widely used for non-destructive evaluation (NDE) in various fields such as material characterization, electronics, and biomedicine. SAcM uses high-frequency acoustic waves (60 MHz to 2.0 GHz) providing much higher resolution (up to 0.5 {micro}m) compared to conventional ultrasonic NDE, which is typically about 500 {micro}m. SAcM offers the ability to non-destructively image subsurface features and visualize the variations in elastic properties. These attributes make SAcM a valuable tool for characterizing near-surface material properties and detecting fine-scale flaws. This paper presents some recent applications of SAcM in detecting subsurface damage, assessing coatings, and visualizing residual stress for ceramic and semiconductor materials.

  1. Method of non-destructively inspecting a curved wall portion

    DOEpatents

    Fong, James T.

    1996-01-01

    A method of non-destructively inspecting a curved wall portion of a large and thick walled vessel for a defect by computed tomography is provided. A collimated source of radiation is placed adjacent one side of the wall portion and an array of detectors for the radiation is placed on the other side adjacent the source. The radiation from the source passing through the wall portion is then detected with the detectors over a limited angle, dependent upon the curvature of the wall of the vessel, to obtain a dataset. The source and array are then coordinately moved relative to the wall portion in steps and a further dataset is obtained at each step. The plurality of datasets obtained over the limited angle is then processed to produce a tomogram of the wall portion to determine the presence of a defect therein. In a preferred embodiment, the curved wall portion has a center of curvature so that the source and the array are positioned at each step along a respective arc curved about the center. If desired, the detector array and source can be reoriented relative to a new wall portion and an inspection of the new wall portion can be easily obtained. Further, the source and detector array can be indexed in a direction perpendicular to a plane including the limited angle in a plurality of steps so that by repeating the detecting and moving steps at each index step, a three dimensional image can be created of the wall portion.

  2. Non-destructive investigation of thermoplastic reinforced composites

    DOE PAGESBeta

    Hassen, Ahmed; Taheri, Hossein; Vaidya, Uday

    2016-05-09

    This paper studies various manufacturing defects in glass fiber/Polypropylene (PP) composite parts and their methods of detection. Foreign Object Inclusion (FOI) of different shapes, sizes, and materials were placed in a glass fiber/PP panel made by compression molding. The paper aims to characterize the fiber orientation and fiber related defects such as fiber waviness in the composite specimen. Comprehensive investigation for different Non Destructive Evaluation (NDE) techniques, namely X-ray radiography and Ultrasonic Testing (UT) techniques to trace and characterize the embedded defects and the composite texture are presented. Conventional X-ray radiography successfully identified the fiber orientation in two dimension (2-D)more » plane; however, information for the sample depth was not captured. The radiography techniques showed low relative errors for the defect size measurements (maximum error was below 9.5%) when compared to the ultrasonic techniques. Ultrasonic techniques were able to map all the embedded artificial defects. Phase Array (PA) ultrasonic technique was able to precisely locate the FOI in the glass fiber/PP specimen. Nerveless, the shape and size of the defects were not accurately determined due to the high signal attenuation and distortion characteristics of the E-glass fiber.« less

  3. Non-Destructive Evaluation of Materials via Ultraviolet Spectroscopy

    NASA Technical Reports Server (NTRS)

    Pugel, Betsy

    2008-01-01

    A document discusses the use of ultraviolet spectroscopy and imaging for the non-destructive evaluation of the degree of cure, aging, and other properties of resin-based composite materials. This method can be used in air, and is portable for field use. This method operates in reflectance, absorbance, and luminescence modes. The ultraviolet source is used to illuminate a composite surface of interest. In reflectance mode, the reflected response is acquired via the imaging system or via the spectrometer. The spectra are analyzed for organic compounds (conjugated organics) and inorganic compounds (semiconducting band-edge states; luminescing defect states such as silicates, used as adhesives for composite aerospace applications; and metal oxides commonly used as thermal coating paints on a wide range of spacecraft). The spectra are compared with a database for variation in conjugation, substitution, or length of molecule (in the case of organics) or band edge position (in the case of inorganics). This approach is useful in the understanding of material quality. It lacks the precision in defining the exact chemical structure that is found in other materials analysis techniques, but it is advantageous over methods such as nuclear magnetic resonance, infrared spectroscopy, and chromatography in that it can be used in the field to assess significant changes in chemical structure that may be linked to concerns associated with weaknesses or variations in structural integrity, without disassembly of or destruction to the structure of interest.

  4. Non-destructive investigation of thermoplastic reinforced composites

    SciTech Connect

    Hassen, Ahmed; Vaidya, Uday

    2016-01-01

    This paper studies various manufacturing defects in glass fiber/Polypropylene (PP) composite parts and their methods of detection. Foreign Object Inclusion (FOI) of different shapes, sizes, and materials were placed in a glass fiber/PP panel made by compression molding. The paper aims to characterize the fiber orientation and fiber related defects such as fiber waviness in the composite specimen. Comprehensive investigation for different Non Destructive Evaluation (NDE) techniques, namely X-ray radiography and Ultrasonic Testing (UT) techniques to trace and characterize the embedded defects and the composite texture are presented. Conventional X-ray radiography successfully identified the fiber orientation in two dimension (2-D) plane; however, information for the sample depth was not captured. The radiography techniques showed low relative errors for the defect size measurements (maximum error was below 9.5%) when compared to the ultrasonic techniques. Ultrasonic techniques were able to map all the embedded artificial defects. Phase Array (PA) ultrasonic technique was able to precisely locate the FOI in the glass fiber/PP specimen. Nerveless, the shape and size of the defects were not accurately determined due to the high signal attenuation and distortion characteristics of the E-glass fiber.

  5. A non-destructive method for dating human remains

    USGS Publications Warehouse

    Lail, Warren K.; Sammeth, David; Mahan, Shannon; Nevins, Jason

    2013-01-01

    The skeletal remains of several Native Americans were recovered in an eroded state from a creek bank in northeastern New Mexico. Subsequently stored in a nearby museum, the remains became lost for almost 36 years. In a recent effort to repatriate the remains, it was necessary to fit them into a cultural chronology in order to determine the appropriate tribe(s) for consultation pursuant to the Native American Grave Protection and Repatriation Act (NAGPRA). Because the remains were found in an eroded context with no artifacts or funerary objects, their age was unknown. Having been asked to avoid destructive dating methods such as radiocarbon dating, the authors used Optically Stimulated Luminescence (OSL) to date the sediments embedded in the cranium. The OSL analyses yielded reliable dates between A.D. 1415 and A.D. 1495. Accordingly, we conclude that the remains were interred somewhat earlier than A.D. 1415, but no later than A.D. 1495. We believe the remains are from individuals ancestral to the Ute Mouache Band, which is now being contacted for repatriation efforts. Not only do our methods contribute to the immediate repatriation efforts, they provide archaeologists with a versatile, non-destructive, numerical dating method that can be used in many burial contexts.

  6. Non-destructive monitoring of curing process in precast concrete

    NASA Astrophysics Data System (ADS)

    Aparicio, S.; Ranz, J.; Fernández, R.; Albert, V.; Fuente, J. V.; Hernández, M. G.

    2012-12-01

    Currently, the use of precast concrete elements has gained importance because it offers many advantages over site-cast concrete. A disadvantage of site-cast concrete is that its properties vary according to the manufacturing method, the environment and even the operator who carried out the mixing, pouring and implementation of the concrete. Precast concrete elements are manufactured in a controlled environment (typically referred to as a precast plant) and this reduces the shrinkage and creep. One of the key properties of precast concrete is the capability to gain compressive strength rapidly under the appropriate conditions. The compressive strength determines if the precast can be stripped from the form or manipulated. This parameter is measured using destructive testing over cylindrical or cubic samples. The quality control of precast is derived from the fracture suffered by these elements, resulting in a "pass or fail" evaluation. In most cases, the solution to this problem is to allow the material to cure for a few hours until it acquires sufficient strength to handle the precast element. The focus of this paper is the description of the research project "CUREND". This project aims to design a non-destructive methodology to monitor the curing process in precast concrete. The monitoring will be performed using wireless sensor networks.

  7. Data fusion for automated non-destructive inspection

    PubMed Central

    Brierley, N.; Tippetts, T.; Cawley, P.

    2014-01-01

    In industrial non-destructive evaluation (NDE), it is increasingly common for data acquisition to be automated, driving a recent substantial increase in the availability of data. The collected data need to be analysed, typically necessitating the painstaking manual labour of a skilled operator. Moreover, in automated NDE a region of an inspected component is typically interrogated several times, be it within a single data channel due to multiple probe passes, across several channels acquired simultaneously or over the course of repeated inspections. The systematic combination of these diverse readings is recognized to offer an opportunity to improve the reliability of the inspection, but is not achievable in a manual analysis. This paper describes a data-fusion-based software framework providing a partial automation capability, allowing component regions to be declared defect-free to a very high probability while readily identifying defect indications, thereby optimizing the use of the operator's time. The system is designed to applicable to a wide range of automated NDE scenarios, but the processing is exemplified using the industrial ultrasonic immersion inspection of aerospace turbine discs. Results obtained for industrial datasets demonstrate an orders-of-magnitude reduction in false-call rates, for a given probability of detection, achievable using the developed software system. PMID:25002828

  8. FIRST 100 T NON-DESTRUCTIVE MAGNET OUTER COIL SET

    SciTech Connect

    J. BACON; A. BACA; ET AL

    1999-09-01

    The controlled power outer coil set of the first 100 T non-destructive (100 T ND) magnet is described. This magnet will be installed as part of the user facility research equipment at the National High Magnetic Field laboratory (NHMFL) Pulsed Field Facility at Los Alamos National Laboratory. The 100 T ND controlled power outer coil set consists of seven nested, mechanically independent externally reinforced coils. These coils, in combination, will produce a 47 T platform field in a 225-mm diameter bore. Using inertial energy storage a synchronous motor/generator provides ac power to a set of seven ac-dc converters rated at 64 MW/80 MVA each. These converters energize three independent coil circuits to create 170 MJ of field energy in the outer coil set at the platform field of 47 T. Each coil consists of a multi-layer winding of high strength conductor supported by an external high strength stainless steel shell. Coils with the highest magnetic loads will utilize a reinforcing shell fabricated from highly cold worked 301 stainless steel strip. The autofrettage conditioning method will be used to pre-stress the coils and thereby limit conductor and reinforcement strains to the elastic range. The purpose of pre-stressing the coils is to attain a design life of 10,000 full field pulses. The operation and conditioning of the coil set will be described along with special features of its design, magnetic and structural analyses and construction.

  9. Non-destructive evaluation of anchorage zones by ultrasonics techniques.

    PubMed

    Kharrat, M; Gaillet, L

    2015-08-01

    This work aims to evaluate the efficiency and reliability of two Non-Destructive Testing (NDT) methods for damage assessment in bridges' anchorages. The Acousto-Ultrasonic (AU) technique is compared to classical Ultrasonic Testing (UT) in terms of defect detection and structural health classification. The AU technique is firstly used on single seven-wire strands damaged by artificial defects. The effect of growing defects on the waves traveling through the strands is evaluated. Thereafter, three specimens of anchorages with unknown defects are inspected by the AU and UT techniques. Damage assessment results from both techniques are then compared. The structural health conditions of the specimens can be then classified by a damage severity criterion. Finally, a damaged anchorage socket with mastered defects is controlled by the same techniques. The UT allows the detection and localization of damaged wires. The AU technique is used to bring out the effect of defects on acoustic features by comparing a healthy and damaged anchorage sockets. It is concluded that the UT method is suitable for local and crack-like defects, whereas the AU technique enables the assessment of the global structural health of the anchorage zones. PMID:25824342

  10. Non-Destructive Evaluation (NDE) Applications of THz Radiation

    NASA Astrophysics Data System (ADS)

    Zimdars, David

    2005-03-01

    The technology and applications of time domain terahertz (THz) imaging to non-destructive evaluation (NDE) will be discussed. THz imaging has shown great promise in 2 and 3 dimensional non-contact inspection of non-conductive materials such as plastics, foam, composites, ceramics, paper, wood and glass. THz imaging employs safe low power non-ionizing electromagnetic pulses, with lateral resolution < 200 um, and depth resolution < 50 um. THz pulses can be analyzed spectroscopically to reveal chemical content. Recently, highly integrated turn-key THz imaging systems have been introduced commercially. We will demonstrate the detection of voids and disbonds intentionally incorporated within the sprayed on foam insulation of a space shuttle external tank mock-up segments. An industrially hardened THz scanning system which has been deployed to scan the space shuttle tank with small remote transceiver will be described. Additional terahertz security imaging applications for the detection of weapons and explosives will also be discussed, as well as the application of terahertz sensors for high speed industrial process monitoring and quality control.

  11. Complex Archaeological Prospection Using Combination of Non-destructive Techniques

    NASA Astrophysics Data System (ADS)

    Faltýnová, M.; Pavelka, K.; Nový, P.; Šedina, J.

    2015-08-01

    This article describes the use of a combination of non-destructive techniques for the complex documentation of a fabulous historical site called Devil's Furrow, an unusual linear formation lying in the landscape of central Bohemia. In spite of many efforts towards interpretation of the formation, its original form and purpose have not yet been explained in a satisfactory manner. The study focuses on the northern part of the furrow which appears to be a dissimilar element within the scope of the whole Devil's Furrow. This article presents detailed description of relics of the formation based on historical map searches and modern investigation methods including airborne laser scanning, aerial photogrammetry (based on airplane and RPAS) and ground-penetrating radar. Airborne laser scanning data and aerial orthoimages acquired by the Czech Office for Surveying, Mapping and Cadastre were used. Other measurements were conducted by our laboratory. Data acquired by various methods provide sufficient information to determine the probable original shape of the formation and proves explicitly the anthropological origin of the northern part of the formation (around village Lipany).

  12. Non-destructive compositional analysis of historic organ reed pipes

    NASA Astrophysics Data System (ADS)

    Manescu, A.; Fiori, F.; Giuliani, A.; Kardjilov, N.; Kasztovszky, Z.; Rustichelli, F.; Straumal, B.

    2008-03-01

    In order to be able to reproduce historic organ reed pipes, a bulk non-destructive chemical composition analysis was performed on the tongues and shallots, focusing mainly on the ratio between copper and zinc and on the presence of lead. Prompt gamma activation analysis results allowed us to observe for the first time that the ratio between the two main components of the brass alloy changed from Cu:Zn = 3:1 for the old tongues and shallots to Cu:Zn = 2:1 around the middle of the 18th century, which is typical also for the modern alloys offered to the organ builders nowadays. We also discovered that the Pb content in the old historic brass alloy diminished until the middle of 18th century when the brass alloy became mainly Pb free. The non-uniform lead distribution inside one of the shallots obtained from a prompt gamma activation analysis (PGAA) experiment was studied by neutron tomography. It gave us a three-dimensonal (3D) distribution of the lead inclusions inside the shallots. The lead particles are concentrated towards the base of the shallot.

  13. Lunar near-surface structure

    NASA Technical Reports Server (NTRS)

    Cooper, M. R.; Kovach, R. L.; Watkins, J. S.

    1974-01-01

    Seismic refraction data obtained at the Apollo 14, 16, and 17 landing sites permit a compressional wave velocity profile of the lunar near surface to be derived. Beneath the regolith at the Apollo 14 Fra Mauro site and the Apollo 16 Descartes site is material with a seismic velocity of about 300 m/sec, believed to be brecciated material or impact-derived debris. Considerable detail is known about the velocity structure at the Apollo 17 Taurus-Littrow site. Seismic velocities of 100, 327, 495, 960, and 4700 m/sec are observed. The depth to the top of the 4700-m/sec material is 1385 m, compatible with gravity estimates for the thickness of mare basaltic flows, which fill the Taurus-Littrow valley. The observed magnitude of the velocity change with depth and the implied steep velocity-depth gradient of more than 2 km/sec/km are much larger than have been observed on compaction experiments on granular materials and preclude simple cold compaction of a fine-grained rock powder to thicknesses of the order of kilometers.

  14. Near-Surface Engineered Environmental Barrier Integrity

    SciTech Connect

    Piet, S.J.; Breckenridge, R.P.

    2002-05-15

    The INEEL Environmental Systems Research and Analysis (ESRA) program has launched a new R and D project on Near-Surface Engineered Environmental Barrier Integrity to increase knowledge and capabilities for using engineering and ecological components to improve the integrity of near-surface barriers used to confine contaminants from the public and the environment. The knowledge gained and the capabilities built will help verify the adequacy of past remedial decisions and enable improved solutions for future cleanup decisions. The research is planned to (a) improve the knowledge of degradation mechanisms (weathering, biological, geological, chemical, radiological, and catastrophic) in times shorter than service life, (b) improve modeling of barrier degradation dynamics, (c) develop sensor systems to identify degradation prior to failure, and (d) provide a better basis for developing and testing of new barrier systems to increase reliability and reduce the risk of failure. Our project combine s selected exploratory studies (benchtop and field scale), coupled effects accelerated aging testing and the meso-scale, testing of new monitoring concepts, and modeling of dynamic systems. The performance of evapo-transpiration, capillary, and grout-based barriers will be examined.

  15. Near-Surface Engineered Environmental Barrier Integrity

    SciTech Connect

    Piet, Steven James; Breckenridge, Robert Paul; Beller, John Michael; Geesey, Gill Gregroy; Glenn, David Frankie; Jacobson, Jacob Jordan; Martian, Pete; Matthern, Gretchen Elise; Mattson, Earl Douglas; Porro, Indrek; Southworth, Finis Hio; Steffler, Eric Darwin; Stormberg, Angelica Isabel; Stormberg, Gregory John; Versteeg, Roelof Jan; White, Gregory J

    2002-08-01

    The INEEL Environmental Systems Research and Analysis (ESRA) program has launched a new R&D project on Near-Surface Engineered Environmental Barrier Integrity to increase knowledge and capabilities for using engineering and ecological components to improve the integrity of near-surface barriers used to confine contaminants from the public and the environment. The knowledge gained and the capabilities built will help verify the adequacy of past remedial decisions and enable improved solutions for future cleanup decisions. The research is planned to (a) improve the knowledge of degradation mechanisms (weathering, biological, geological, chemical, radiological, and catastrophic) in times shorter than service life, (b) improve modeling of barrier degradation dynamics, (c) develop sensor systems to identify degradation prior to failure, and (d) provide a better basis for developing and testing of new barrier systems to increase reliability and reduce the risk of failure. Our project combines selected exploratory studies (benchtop and field scale), coupled effects accelerated aging testing and the meso-scale, testing of new monitoring concepts, and modeling of dynamic systems. The performance of evapo- transpiration, capillary, and grout-based barriers will be examined.

  16. Geophysical Methods for Non-Destructive Testing in Civil Engineering

    NASA Astrophysics Data System (ADS)

    Niederleithinger, E.

    2013-12-01

    Many non-destructive testing (NDT) methods for civil engineering (e. g. ultrasonics, radar) are similar to geophysical techniques. They just differ in scale, material under investigation and vocabulary used. In spite of the fact that the same principles of physics and mathematics apply to both fields, exchange has been limited in the past. But since a few years more and more geophysical knowledge is used in civil engineering. One of the focal points in research is to improve ultrasonic testing of concrete to be able to image the inside even of large, complex structures and to detect any deterioration as early as possible. One of the main issues is the heterogeneity of concrete, including aggregates, reinforcement, cracks and many other features. Our current research focuses on three points. One is the application of state of the art geophysical migration techniques as Reverse Time Migration (RTM) to image vertical faces or the backside of voids and ducts in thick concrete structures, which isn't possible with conventional techniques used in NDT. Second, we have started to use seismic interferometric techniques to interpolate ultrasonic traces, which can't be measured directly for technical reasons. Third, we are using coda wave interferometry to detect concrete degradation due to load, fatigue, temperature or other influences as early as possible. Practical examples of the application of these techniques are given and potential future research directions will be discussed. It will be shown, how a subset of these techniques can be used for innovative monitoring systems for civil infrastructure. Imaging the interior of a concrete body by ultrasonics and reverse time migration(simulated data).

  17. Recent advances in the use of non-destructive near infrared spectroscopy on intact olive fruits

    Technology Transfer Automated Retrieval System (TEKTRAN)

    The objective of this review is to illustrate the state of the art in the use of non-destructive near infrared (NIR) spectroscopy for quality evaluation of intact fruit in the olive industry. First, the most recent studies regarding the application of non-destructive NIR spectroscopy methods to asse...

  18. Magnetic non-destructive evaluation of ruptures of tensile armor in oil risers

    NASA Astrophysics Data System (ADS)

    Pérez-Benitez, J. A.; Padovese, L. R.

    2012-04-01

    Risers are flexible multilayered pipes formed by an inner flexible metal structure surrounded by polymer layers and spiral wound steel ligaments, also known as armor wires. Since these risers are used to link subsea pipelines to floating oil and gas production installations, and their failure could produce catastrophic consequences, some methods have been proposed to monitor the armor integrity. However, until now there is no practical method that allows the automatic non-destructive detection of individual armor wire rupture. In this work we show a method using magnetic Barkhausen noise that has shown high efficiency in the detection of armor wire rupture. The results are examined under the cyclic and static load conditions of the riser. This work also analyzes the theory behind the singular dependence of the magnetic Barkhausen noise on the applied tension in riser armor wires.

  19. Evaluation and correction of readout artifacts from flat panel detectors for non-destructive testing purposes

    NASA Astrophysics Data System (ADS)

    Burtzlaff, S.; Voland, V.; Salamon, M.; Hofmann, Th.; Uhlmann, N.

    2009-08-01

    Flat panel detectors are commonly used for non-destructive testing purposes using X-ray technology. During a series of measurements with high absorbing objects, we observed an unknown kind of artifacts especially apparent with high contrast edges. These artifacts lead to unwanted results in radioscopic and computed tomography inspection. Given the object is fully occupying the lower part and half of the upper part of the detector. Looking at the image with high contrast visualization, it can be seen that the covered upper part of the detector is brighter than the covered lower half. The horizontal border of the detector tile is clearly recognizable. Furthermore, the uncovered area directly above the object is darker than next to the edge. In this area the vertical border of the edge below can be localized. We examined and evaluated the effect and developed a correction algorithm. The effect and its correction results are presented.

  20. Non-destructive evaluation of TBC by electrochemical impedance spectroscopy

    NASA Astrophysics Data System (ADS)

    Zhang, Jianqi

    suggested. An alternative electrolyte (trifluoroacetic acid) was investigated using EIS in order to be used as compatible or friendly solution to TBC. A similar characteristic EIS result was found using the alternative electrolyte compared with the commonly used electrolyte [Fe(CN)6]-3/[Fe(CN) 6]-4 in this work. It has indicated that a friendly electrolyte be viable for EIS technique to be used for non-destructive evaluation of TBC. Visualization of a flexible probe for EIS field detection has also been designed. (Abstract shortened by UMI.)

  1. Determining the Stability of Asphalt Concrete at Varying Temperatures and Exposure Times Using Destructive and Non-Destructive Methods

    NASA Astrophysics Data System (ADS)

    Ozgan, Ercan

    This study examined the effect of varying temperatures and varying exposure times on the stability of asphalt concrete using destructive and non-destructive methods. The study also looked at the relationship between destructive and non-destructive methods. In order to investigate the stability according to exposure time and environment temperature, exposure times of 1.5, 3, 4.5 and 6 h and temperatures of 30, 40 and 50°C were selected. The results showed that at the environment temperature of 17°C the stability of the asphalt core samples decreased by 40.16% at 30°C after 1.5 h and 62.39% after 6 h. At 40°C the decrease was 74.31% after 1.5 and 78.10% after 6 h. At 50°C the stability of the asphalt decreased by 83.22% after 1.5 h and 88.66% after 6 h. The results also pointed to a moderate negative relationship (R = -0.533) between second ultrasound and stability indicating that non-destructive ultrasound method can be used to predict stability.

  2. An accurate method for determining residual stresses with magnetic non-destructive techniques in welded ferromagnetic steels

    NASA Astrophysics Data System (ADS)

    Vourna, P.

    2016-03-01

    The scope of the present research work was to investigate the proper selection criteria for developing a suitable methodology for the accurate determination of residual stresses existing in welded parts. Magnetic non-destructive testing took place by the use of two magnetic non-destructive techniques: by the measurement of the magnetic Barkhausen noise and by the evaluation of the magnetic hysteresis loop parameters. The spatial distribution of residual stresses in welded metal parts by both non-destructive magnetic methods and two diffraction methods was determined. The conduction of magnetic measurements required an initial calibration of ferromagnetic steels. Based on the examined volume of the sample, all methods used were divided into two large categories: the first one was related to the determination of surface residual stress, whereas the second one was related to bulk residual stress determination. The first category included the magnetic Barkhausen noise and the X-ray diffraction measurements, while the second one included the magnetic permeability and the neutron diffraction data. The residual stresses determined by the magnetic techniques were in a good agreement with the diffraction ones.

  3. Non-destructive in situ mapping of macroholes, cracks and inhomogeneities of stalagmites in cave environments

    NASA Astrophysics Data System (ADS)

    Hegymegi, Erika; Gyöngy, Miklós; Bodolai, Tamás; Divós, Ferenc; Barta, Edit; Gribovszki, Katalin; Bokelmann, Götz; Hegymegi, Csaba; Lednická, Markéta; Kovács, Károly

    2016-04-01

    Intact and vulnerable, candle-stick type stalagmites can be used as prehistoric-earthquake indicators during seismic-hazard analysis of a given region, because they are old enough to survive several earthquakes. The continued intactness of the stalagmites indicates a lack of earthquakes that had the strength to destroy them. To make sure that the stalagmites are intact, we have to image their internal structure in order to estimate the steadiness more accurate and potential failure in the last few thousand years, during their evolution. These stalagmites play an important indicator role and carry fundamental information; however, legally they are strictly protected natural objects in Europe. Therefore it is impossible to examine them in the laboratory by conventional equipment such as computer tomography (CT) or X-ray, because this would require taking samples. With the presented non-destructive methods (ultrasound and acoustic tomography) we tried to detect macroholes, cracks and velocity anomalies inside the stalagmites on the mm scale in situ, in the cave. The acoustic tomography applied in the current work is an existing method in forest research. Forest researchers use it to non-destructively detect the size and location of decayed or hollow parts in the trunk and this technique is able to detect the velocity changing of wave propagation and anomalies in the stalagmites as well. The other method that we use is ultrasound imaging, which uses (and is able to calculate) the velocity of sound propagation. Here, the frequency used is much higher (typically 250 kHz to 5 MHz), which increases resolution but at the same time decreases penetration depth compared to acoustic tomography. In this latter work, through transmission and TOFD (time-of-flight-diffraction) ultrasound methods are using thickness-mode ultrasound transducers (Panametrics, Olympus). Such equipment is well-adapted to the cave environment and this is the first time that it has been used for these

  4. Portable 1,5 MeV X-Band Linac For Non-destructive Radiography

    NASA Astrophysics Data System (ADS)

    Saversky, A. J.; Rodionov, A. E.; Shaltyrev, A. P.; Shchedrin, I. S.

    1997-05-01

    Portable linear electron accelerator Y-34 developed in Small Accelerator Laboratory of MEPhI for non-destructive industrial radiography. This Linac is a fully self-contained device with the exception of external electric power 220Vx50Gz, 1 phase, 5 kVA. Full mass of Linac Y-34 - less than 300 kg. The Radiographic parameters: Nominal Energy - 1,5 MeV; Energy Range - 0,7...1,8 MeV; Maximum pulse current - 100 mA; Maximum Intensity - 15 R/min@m; Focal spot size - less than 2 mm. The Linac is comprised of 4 subassemblies. The X-ray head with weight less than 100 kg, dimensions: 0,7x0,7x1,0 m contains the traveling-wave accelerating structure with lens 0,4 m, electron gun, vacuum pump, tungsten target and RF-system with 500-kW magnetron. The permanent magnets focusing system provides focal spot less than 2 mm. The high voltage power unit consist of a line-type magnetron/electron gun modulator 2 kW power supply, the weight is equal 70 kg. The self-contained cooling water supply provides temperature controlled water for accelerator structure and magnetron. The control console allows convenient monitoring of critical system and Linac parameters by manual or remote computer. Portable X-band Linac Y-34 is the effective X - ray and/or electron beam source for such applications as non-destructive examination of nuclear reactor systems, solid rocket motors, technology research.

  5. Non-destructive hyperspectral imaging of quarantined Mars Returned Samples

    NASA Astrophysics Data System (ADS)

    Simionovici, Alexandre; Viso, Michel; Beck, Pierre; Lemelle, Laurence; Westphal, Andrew; Vincze, Laszlo; Schoonjans, Tom; Fihman, Francois; Chazalnoel, Pascale; Ferroir, Tristan; Solé, Vicente Armando; Tucoulou, R.

    Introduction: In preparation for the upcoming International Mars Sample Return mission (MSR), returning samples containing potential biohazards, we have implemented a hyperspec-tral method of in-situ analysis of grains performed in BSL4 quarantine conditions, by combining several non-destructive imaging diagnostics. This allows sample transportation on optimized experimental setups, while monitoring the sample quarantine conditions. Our hyperspectral methodology was tested during analyses of meteorites [1-2] and cometary and interstellar grains from the recent NASA Stardust mission [3-6]. Synchrotron Radiation protocols: X-ray analysis methods are widely accepted as the least destructive probes of fragile, unique samples. Diffraction, X-ray fluorescence and ab-sorption micro/nano-spectroscopies were performed on chondritic test samples using focused monochromatic beams at the ESRF synchrotron in Grenoble, France. 2D maps of grain com-position down to ppm concentrations and polycrystalline structure have simultaneously been acquired, followed by X-ray absorption performed on elements of Z 26. Ideally, absorption micro-tomography can later be performed in full-beam mode to record the 3D morphology of the grain followed by fluorescence-tomography in focus-beam mode which complements this picture with a 3D elemental image of the grain. Lab-based protocols: Raman and IR-based spectroscopies have been performed in reflection mode for mineralogical imaging of the grains in the laboratory using commercial microscopes. The spatial resolution varied in the 1-10 m range. Laser limited penetration of opaque samples permits only 2D imaging of the few nanometer-thick outer layers of the grains. Mineralogical maps are now routinely acquired using Raman spectroscopy at sub-micron scales through the 3 container walls of the Martian sample holder, followed by IR few-micrometer spot measurements recording C-based and potential aqueous alteration distributions. Sample Holder: A

  6. Non-destructive electrical characterization of controlled Waspaloy microstructures

    NASA Astrophysics Data System (ADS)

    G. Kelekanjeri, V. Siva Kumar

    In this research, controlled Waspaloy microstructures are produced with the objective of studying microstructural evolution in this alloy via non-destructive electrical measurements. Waspaloy is a precipitation-hardenable gamma-gamma' nickel-base superalloy that is used in turbine blade applications demanding superior strength retention capabilities at elevated temperatures. Overall, three different sets of microstructures were produced that varied systematically as a function of the matrix (gamma) grain size and gamma' precipitate size distribution or just the latter. Initial solutionizing treatments conducted at 1045°C, 1090°C and 1145°C resulted in average y grain size of 13, 52 and 89 mum respectively. A vacancy stabilization treatment at 1045°C followed the solutionizing treatments in Set I experiments, after which the specimens were aged at 800°C for durations ranging from 0.1 hrs to 100 hrs. In Sets 11 and III, the matrix grain size was kept unchanged by an initial solution-treatment at 1145°C. The stabilization treatment at 1045°C was only conducted in Set II after the solution-treatment. Aging experiments were then conducted at 700°C (or 725°C in Set III), 800°C and 875°C to study the growth kinetics of gamma' precipitate distribution. The specimens with controlled microstructures were investigated using scanning electron microscopy (SEM), atomic force microscopy (AFM), x-ray diffraction (XRD), ultra small-angle x-ray scattering (USAXS) and dc four-point probe resistivity. The applicability of two and four-probe ac impedance techniques was also investigated. Characterization of heat-treated specimens. Solution-treated SEM microstructures showed the presence of polygonal etch-pit shapes, which was proposed to be due to the condensation of excess quenched-in vacancies along crystallographically soft-directions in the gamma phase. The etch-pits evolved upon subsequent aging into progressively irregular shapes, concurrent with gamma' growth inside

  7. Ultrasonic characterization of near-surface material properties in shot peened Waspaloy

    NASA Astrophysics Data System (ADS)

    Lavrentyev, Anton I.; Veronesi, William A.

    2002-05-01

    When a stream of shot impinges a metal surface, a near-surface layer undergoes an intensive cold working resulting in material property changes. One of the effects induced by shot peening, a near-surface compressive stress, helps to slow down initiation and propagation of surface breaking cracks resulting in an extended fatigue life of a component. The capability to non-destructively evaluate near-surface residual stress would greatly aid the assurance of proper fatigue life in these components. This paper presents results from an ultrasonic characterization study of shot peened Waspaloy surfaces. Rayleigh wave velocity measurements by a V(z)-curve method were made on smooth and shot peened samples using line-focus ultrasonic transducers. Several factors are believed to influence measured surface wave velocity including surface roughness, near-surface grain reorientation (texture), and residual stress. In this study we estimate quantitatively the effect of these factors and discuss how these effects can be separated and accounted for in residual stress measurements.

  8. Mars water vapor, near-surface

    NASA Technical Reports Server (NTRS)

    Ryan, J. A.; Sharman, R. D.; Lucich, R. D.

    1982-01-01

    In a previous paper we concluded that the temperature sensors aboard the Viking landers (VL-1 and VL-2) were detecting the water vapor frost point. Analysis of one Mars year of data at both lander sites substantiates this conclusion. At VL-1 it is found that the water vapor mixing ratio is constant with height through the bulk of the atmosphere, most of the time. Exceptions are during the onset phases of the two major dust storms when temporary enhancement of near-surface vapor occurs (the same phenomenon is observed at VL-2), and some depletion of near-surface vapor during the decay phase of the first storm, possibly the second storm as well. The former suggests near-surface, northward transport of water vapor with the storms. The latter suggests adsorption of vapor on dust particles followed by surface deposition. At VL-2, severe near-surface depletion of water vapor occurs during northern autumn and winter. The residual vapor is in equilibrium with the surface condensate observed at the site during this period, indicating that the source region for the condensate must be aloft with downward transport by dust fall-out. Since the near-surface water vapor mixing ratio and concentration at VL-1 generally parallels the column abundance over VL-1 obtained by the orbiters, this suggests that VL-1 can be used to give a measure of column abundance for as long as the temperature sensors remain operational.

  9. Non-destructive quantification of alignment of nanorods embedded in uniaxially stretched polymer films

    SciTech Connect

    Stoenescu, Stefan Packirisamy, Muthukumaran; Truong, Vo-Van

    2014-03-21

    Among several methods developed for uniaxial alignment of metallic nanorods for optical applications, alignment by film stretching consists in embedding the rods in a transparent thin film of thermoplastic polymer, followed by simultaneous heating and uniaxial stretching of the composite film. As to the quantification of the resulting alignment, it has been limited to statistical calculations based on microscopic examination, which is incomplete, subject to errors due to geometric distortions of the scanning electron microscope images and destructive, since it involves cutting of samples. In contrast, we present in this paper a non-destructive quantification of the average orientation of the rods, based on a probabilistic approach combined with numerical simulations of absorbance spectra and spectrometric characterization of the composite film. Assuming electromagnetically non-interacting rods, we consider the longitudinal absorbance peak of their ensemble to consist of the superposition of their individual spectra that we obtain by numerical simulation using the size and shape adapted dielectric function of the metal and the finite difference time domain method. The accuracy of the solution depends on the number of discretization intervals, the accuracy of the numerical simulations, and the accurate knowledge of the polydispersity of the rods. For the sake of concreteness, we used nanorods to describe the quantification steps but the method is equally valid for any dichroic particles.

  10. Non-destructive quantification of alignment of nanorods embedded in uniaxially stretched polymer films

    NASA Astrophysics Data System (ADS)

    Stoenescu, Stefan; Truong, Vo-Van; Packirisamy, Muthukumaran

    2014-03-01

    Among several methods developed for uniaxial alignment of metallic nanorods for optical applications, alignment by film stretching consists in embedding the rods in a transparent thin film of thermoplastic polymer, followed by simultaneous heating and uniaxial stretching of the composite film. As to the quantification of the resulting alignment, it has been limited to statistical calculations based on microscopic examination, which is incomplete, subject to errors due to geometric distortions of the scanning electron microscope images and destructive, since it involves cutting of samples. In contrast, we present in this paper a non-destructive quantification of the average orientation of the rods, based on a probabilistic approach combined with numerical simulations of absorbance spectra and spectrometric characterization of the composite film. Assuming electromagnetically non-interacting rods, we consider the longitudinal absorbance peak of their ensemble to consist of the superposition of their individual spectra that we obtain by numerical simulation using the size and shape adapted dielectric function of the metal and the finite difference time domain method. The accuracy of the solution depends on the number of discretization intervals, the accuracy of the numerical simulations, and the accurate knowledge of the polydispersity of the rods. For the sake of concreteness, we used nanorods to describe the quantification steps but the method is equally valid for any dichroic particles.

  11. Non-Destructive Measurement of Vascular Tissue Development in Stems of Miniature Tomato Using Acoustic Method

    NASA Astrophysics Data System (ADS)

    Kageyama, Kensuke; Watanabe, Eiko; Kato, Hiroshi

    The guided wave effect resembling that of annual rings found in woods and the cortical region of bones is believed to be observable in vascular tissues of herbaceous plants. The properties of acoustic waves traveling through the vascular tissue in the stem of a miniature tomato were measured using a piezoelectric pulser and receiver. The thickness of the vascular tissues and the stem's water content were measured. The detected acoustic waves showed a guided wave effect. The apparent sound velocity, va, was related to the vascular tissue thickness, tv. These results reveal that the detected acoustic waves traveled along the vascular tissues in stems. The maximum peak intensity of the detected acoustic waves, Imax was also related to t. Furthermore, wilting of the examined plants decreased the Imax, although va was not changed. The decrease in Imax might result from cavitations and embolisms with a subsequent increase in air pores in xylem tissues. These results demonstrate that the measurement of acoustic waves traveling through vascular tissue is a useful tool for the non-destructive evaluation of vascular tissue development and embolism density in xylem tissues.

  12. Non-destructive Evaluation of Bonds Between Fiberglass Composite and Metal

    NASA Technical Reports Server (NTRS)

    Zhao, Selina; Sonta, Kestutis; Perey, Daniel F.; Cramer, K. E.; Berger, Libby

    2015-01-01

    To assess the integrity and reliability of an adhesive joint in an automotive composite component, several non-destructive evaluation (NDE) methodologies are correlated to lap shear bond strengths. A glass-fabric-reinforced composite structure was bonded to a metallic structure with a two-part epoxy adhesive. Samples were subsequently cut and tested in shear, and flaws were found in some areas. This study aims to develop a reliable and portable NDE system for service-level adhesive inspection in the automotive industry. The results of the experimental investigation using several NDE methods are presented and discussed. Fiberglass-to-metal bonding is the ideal configuration for NDE via thermography using excitation with induction heating, due to the conductive metal and non-conductive glass-fiber-reinforced composites. Excitation can be either by a research-grade induction heater of highly defined frequency and intensity, or by a service-level heater, such as would be used for sealing windshields in a body shop. The thermographs thus produced can be captured via a high-resolution infrared camera, with principal component analysis and 2D spatial Laplacian processing. Alternatively, the thermographs can be captured by low resolution thermochromic microencapsulated liquid crystal film imaging, which needs no post-processing and can be very inexpensive. These samples were also examined with phased-array ultrasound. The NDE methods are compared to the lap shear values and to each other for approximate cost, accuracy, and time and level of expertise needed.

  13. Feasibility for non-destructive discrimination of natural and beryllium-diffused sapphires using Raman spectroscopy.

    PubMed

    Chang, Kyeol; Lee, Sanguk; Park, Jimin; Chung, Hoeil

    2016-03-01

    Raman spectroscopy based non-destructive discrimination between natural and beryllium-diffused (Be-diffused) sapphires has been attempted. The initial examination of Raman image acquired on a sapphire revealed that microscopic structural and compositional heterogeneity was apparent in the sample, so acquisition of spectra able to represent a whole body of sapphire rather than a localized area was necessary for a reliable discrimination. For this purpose, a wide area illumination (WAI) scheme (illumination area: 28.3mm(2)) providing a large sampling volume was employed to collect representative Raman spectra of sapphires. Upon the diffusion of Be into a sapphire, the band shift originated from varied lattice structure by substitution of Be at cation sites was observed and utilized as a valuable spectral signature for the discrimination. In the domain of principal component (PC) scores, the groups of natural and Be-diffused sapphires were identifiable with minor overlapping and the cross-validated discrimination error was 7.3% when k-Nearest Neighbor (k-NN) was used as a classifier. PMID:26717849

  14. Near-surface Fun with Seismic Data

    NASA Astrophysics Data System (ADS)

    Clapp, M.

    2015-12-01

    What is happening in the near-surface often has a direct effect on human activity. Seismic exploration has routinely targeted geology at depths of kilometers to tens of kilometers. However, these techniques can be applied to answer questions about shallower targets. Several recent experiments demonstrate seismic applicability to near-surface problems. One example is passive seismic monitoring using ambient noise to identify shallow changes and potential hazards in a producing hydrocarbon field. Another example is the use of seismic reflection data from within the water column to determine layering caused by temperature and salinity differences in depth. A third example is identifying historical elevation changes along coast lines using seismic reflection data. These examples show that exploration seismic methods can be effectively used for a variety of near-surface applications.

  15. Non-destructive evaluation techniques for chemical weapons destruction

    SciTech Connect

    Hartwell, J.K.; Caffrey, A.J.

    1996-09-01

    fThe safe and verifiable disposition, either by incineration or chemical neutralization of chemical warfare (CW) agents requires correct {ital a priori} identification of each munition or container to be processed. A variety of NDE techniques have been used or tested for the examination and characterization of munitions. In the U.S., three widely used techniques are X-ray radiography, acoustic resonance spectroscopy (ARS), and prompt gamma ray neutron activation analysis (PINS). The technical bases, instrumental implementations, and applications of the U.S. versions of these methods are briefly discussed. 10 refs., 2 figs., 1 tab.

  16. Geophysical methods in drinkwater protection of near-surface reservoirs

    NASA Astrophysics Data System (ADS)

    Draskovits, Pál; Fejes, Imre

    1994-02-01

    Two case histories are presented in which near-surface water-bearing formations and their overburden are examined. This survey utilized a combination of traditional geoelectric methods (direct current resistivity and time domain induced polarization) and a special shallow-depth engineering geophysical sounding method. This latter method was developed in Hungary to investigate near-surface unconsolidated formations such as clay, silt, sand, gravel and other similarly "penetratable" formations. For a gravel terrace, in addition to the usual parameter maps (resistivity, thickness, polarizability), combined multiparametric characterization maps have been plotted. These maps illustrate the hydrogeologic value of the water-bearing formations and the protecting capacity of the overburden better than the conventional parameter maps. Surface measurement results together with filtration coefficient values show how an inexpensive geophysical survey can successfully be applied in estimating the dangerous or protected situation of near-surface reservoirs and how such a survey can be used for siting reservoirs. This work enabled the near-surface geological structure to be determined, hereby providing orientation for more expensive, highly detailed surveys.

  17. Non Destructive Defect Detection by Spectral Density Analysis

    PubMed Central

    Krejcar, Ondrej; Frischer, Robert

    2011-01-01

    The potential nondestructive diagnostics of solid objects is discussed in this article. The whole process is accomplished by consecutive steps involving software analysis of the vibration power spectrum (eventually acoustic emissions) created during the normal operation of the diagnosed device or under unexpected situations. Another option is to create an artificial pulse, which can help us to determine the actual state of the diagnosed device. The main idea of this method is based on the analysis of the current power spectrum density of the received signal and its postprocessing in the Matlab environment with a following sample comparison in the Statistica software environment. The last step, which is comparison of samples, is the most important, because it is possible to determine the status of the examined object at a given time. Nowadays samples are compared only visually, but this method can’t produce good results. Further the presented filter can choose relevant data from a huge group of data, which originate from applying FFT (Fast Fourier Transform). On the other hand, using this approach they can be subjected to analysis with the assistance of a neural network. If correct and high-quality starting data are provided to the initial network, we are able to analyze other samples and state in which condition a certain object is. The success rate of this approximation, based on our testing of the solution, is now 85.7%. With further improvement of the filter, it could be even greater. Finally it is possible to detect defective conditions or upcoming limiting states of examined objects/materials by using only one device which contains HW and SW parts. This kind of detection can provide significant financial savings in certain cases (such as continuous casting of iron where it could save hundreds of thousands of USD). PMID:22163742

  18. Non destructive evaluation of adhesively bonded carbon fiber reinforced composite lap joints with varied bond quality

    NASA Astrophysics Data System (ADS)

    Vijayakumar, R. L.; Bhat, M. R.; Murthy, C. R. L.

    2012-05-01

    Structural adhesive bonding is widely used to execute assemblies in automobile and aerospace structures. The quality and reliability of these bonded joints must be ensured during service. In this context non destructive evaluation of these bonded structures play an important role. Evaluation of adhesively bonded composite single lap shear joints has been attempted through experimental approach. Series of tests, non-destructive as well as destructive were performed on different sets of carbon fiber reinforced polymer (CFRP) composite lap joint specimens with varied bond quality. Details of the experimental investigations carried out and the outcome are presented in this paper.

  19. Development of non-destructive inspection method for the performance of thermal barrier coating.

    PubMed

    Morinaga, M; Takahashi, T

    2001-05-01

    This paper shows that our proprietary non-destructive inspection method can be used to effectively measure the thermal barrier performance of the thermal barrier coating used to coat gas turbine hot parts by the results of numerical analysis and laboratory experiments. PMID:11460665

  20. Time Domain Terahertz Non-Destructive Evaluation of Aeroturbine Blade Thermal Barrier Coatings

    NASA Astrophysics Data System (ADS)

    White, Jeffrey; Fichter, G.; Chernovsky, A.; Whitaker, John F.; Das, D.; Pollock, Tresa M.; Zimdars, David

    2009-03-01

    Time domain terahertz (TD-THz) non destructive evaluation (NDE) imaging is used to two-dimensionally map the thickness of yttria stabilized zirconia (YSZ) thermal barrier coatings (TBC) on aircraft engine turbine blades. Indications of thermal degradation can be seen. The method is non-contact, rapid, and requires no special preparation of the blade.

  1. The non-destructive identification of early Chinese porcelain by PIXE

    NASA Astrophysics Data System (ADS)

    Cheng, H. S.; Zhang, Z. Q.; Zhang, B.; Yang, F. J.

    2004-06-01

    PIXE is used for the non-destructive differentiation of early precious Chinese blue and white porcelain made in Yuan (AD 1206-1368), Ming (AD 1368-1644) Dynasty in Jingdezhen from imitations. Also, ancient celadon made in Song Dynasty (AD 960-1279) is identified by measuring the trace elements contained in the glazes.

  2. Using magnetic levitation for non-destructive quality control of plastic parts.

    PubMed

    Hennek, Jonathan W; Nemiroski, Alex; Subramaniam, Anand Bala; Bwambok, David K; Yang, Dian; Harburg, Daniel V; Tricard, Simon; Ellerbee, Audrey K; Whitesides, George M

    2015-03-01

    Magnetic levitation (MagLev) enables rapid and non-destructive quality control of plastic parts. The feasibility of MagLev as a method to: i) rapidly assess injection-molded plastic parts for defects during process optimization, ii) monitor the degradation of plastics after exposure to harsh environmental conditions, and iii) detect counterfeit polymers by density is demonstrated. PMID:25589230

  3. Research on non-destructive testing method of silkworm cocoons based on image processing technology

    NASA Astrophysics Data System (ADS)

    Gan, Yong; Kong, Qing-hua; Wei, Li-fu

    2008-03-01

    The major studied in this dissertation is the non-destructive testing method of silkworm cocoon's quality, based on the digital image processing and photoelectricity technology. Through the images collection and the data analysis, procession and calculation of the tested silkworm cocoons with the non-destructive testing technology, internet applications automatically reckon all items of the classification indexes. Finally we can conclude the classification result and the purchase price of the silkworm cocoons. According to the domestic classification standard of the silkworm cocoons, the author investigates various testing methods of silkworm cocoons which are used or have been explored at present, and devices a non-destructive testing scheme of the silkworm cocoons based on the digital image processing and photoelectricity technology. They are dissertated about the project design of the experiment. The precisions of all the implements are demonstrated. I establish Manifold mathematic models, compare them with each other and analyze the precision with technology of databank to get the best mathematic model to figure out the weight of the dried silkworm cocoon shells. The classification methods of all the complementary items are designed well and truly. The testing method has less error and reaches an advanced level of the present domestic non-destructive testing technology of the silkworm cocoons.

  4. Non-destructive freeze damage detection in oranges using machine vision and ultraviolet fluorescence

    Technology Transfer Automated Retrieval System (TEKTRAN)

    A non-contact, non-destructive, and rapid method of detecting freeze damaged oranges based on ultraviolet (UV) fluorescence of the peel oil constituents visible on the peel surface was investigated. The visual appearance is different from oleocellosis in that freeze damaged oranges exhibit a fine pa...

  5. Non-destructive method for inward leakage detection of a plate evaporator

    NASA Astrophysics Data System (ADS)

    Hribernik, Ales

    2007-05-01

    A new non-destructive method was developed for the detection of refrigerant leakage at an evaporator's inflow. Nitrogen and oxygen gas were successively blown through the evaporator. A gas analyser was applied at the outflow of the evaporator and the oxygen concentration measured. It was possible to detect any leakage by investigating the oxygen concentration-time history diagram.

  6. Non-Destructive Survey of Archaeological Sites Using Airborne Laser Scanning and Geophysical Applications

    NASA Astrophysics Data System (ADS)

    Poloprutský, Z.; Cejpová, M.; Němcová, J.

    2016-06-01

    This paper deals with the non-destructive documentation of the "Radkov" (Svitavy district, Czech Republic) archaeological site. ALS, GPR and land survey mapping will be used for the analysis. The fortified hilltop settlement "Radkov" is an immovable historical monument with preserved relics of anthropogenic origin in relief. Terrain reconnaissance can identify several accentuated objects on site. ALS enables identification of poorly recognizable archaeological objects and their contexture in the field. Geophysical survey enables defunct objects identification. These objects are hidden below the current ground surface and their layout is crucial. Land survey mapping provides technical support for ALS and GPR survey. It enables data georeferencing in geodetic reference systems. GIS can then be used for data analysis. M. Cejpová and J. Němcová have studied this site over a long period of time. In 2012 Radkov was surveyed using ALS in the project "The Research of Ancient Road in Southwest Moravia and East Bohemia". Since 2015 the authors have been examining this site. This paper summarises the existing results of the work of these authors. The digital elevation model in the form of a grid (GDEM) with a resolution 1 m of 2012 was the basis for this work. In 2015 the survey net, terrain reconnaissance and GPR survey of two archaeological objects were done at the site. GDEM was compared with these datasets. All datasets were processed individually and its results were compared in ArcGIS. This work was supported by the Grant Agency of the CTU in Prague, grant No. SGS16/063/OHK1/1T/11.

  7. A non-destructive synchrotron X-ray study of the metallurgy and manufacturing processes of Eastern and Western astrolabes in the Adler Planetarium collection

    NASA Astrophysics Data System (ADS)

    Newbury, Brian Dale

    The astrolabe collection of the Adler Planetarium and History of Astronomy Museum, Chicago, IL, was examined using non-destructive synchrotron based high-energy X-ray techniques including diffraction, fluorescence, and radiography to determine the metallurgy, microstructure, and metal forming processes used in astrolabe construction. All high-energy X-ray measurements were performed at the Advanced Photon Source (APS) synchrotron of Argonne National Laboratory, Argonne, IL. Astrolabes from the collection were selected to represent all major astrolabe production centers possible and time periods. It was found that all European astrolabes were manufactured of traditional cementation brass by hand worked metal forming processes consistent with technology in the literature. Of the Islamic astrolabes examined, all seven from Lahore in current-day Pakistan exhibited advanced brass alloys not typical of alloys discussed in the literature. It was found that these alloys were selected for their specific hot working properties, allowing the Lahore metalworkers to more efficiently make brass sheet from which to make astrolabe components. In addition, the alloy required a fundamental change in the brass foundry process, indicating advanced Zn metal production techniques. It was found that analysis by high energy X-rays from the APS was essential to produce data on the chemistry and microstructure from the interior of the astrolabe components in a non-destructive manner. Many astrolabe components had undergone surface dezincification due to heavy annealing during manufacturing, causing the Zn composition measured by the surface sensitive fluorescence technique to be lower than the true bulk alloy Zn composition. This would have been impossible to quantify non-destructively without the high-energy diffraction capability of the APS. The results of this study have proven the effectiveness of the synchrotron as a viable non-destructive analysis technique for examining cultural

  8. Full Elastic Waveform Search Engine for Near Surface Imaging

    NASA Astrophysics Data System (ADS)

    Zhang, J.; Zhang, X.

    2014-12-01

    For processing land seismic data, the near-surface problem is often very complex and may severely affect our capability to image the subsurface. The current state-of-the-art technology for near surface imaging is the early arrival waveform inversion that solves an acoustic wave-equation problem. However, fitting land seismic data with acoustic wavefield is sometimes invalid. On the other hand, performing elastic waveform inversion is very time-consuming. Similar to a web search engine, we develop a full elastic waveform search engine that includes a large database with synthetic elastic waveforms accounting for a wide range of interval velocity models in the CMP domain. With each CMP gather of real data as an entry, the search engine applies Multiple-Randomized K-Dimensional (MRKD) tree method to find approximate best matches to the entry in about a second. Interpolation of the velocity models at CMP positions creates 2D or 3D Vp, Vs, and density models for the near surface area. The method does not just return one solution; it gives a series of best matches in a solution space. Therefore, the results can help us to examine the resolution and nonuniqueness of the final solution. Further, this full waveform search method can avoid the issues of initial model and cycle skipping that the method of full waveform inversion is difficult to deal with.

  9. Non-destructive optical methods for the study of soft tissues

    NASA Astrophysics Data System (ADS)

    Santiago-Lona, Cynthia V.; Hernández-Montes, María. del Socorro; Mendoza Santoyo, F.; Muñoz, Silvino; Mendoza, Fernando

    2015-08-01

    In optical metrology, non-destructive methods allow studying some mechanical properties of the samples to investigate by using light, which leads to non-contact testing. This paper shows recent results of the application of non-destructive optical methods based on Digital Holographic Interferometry to the study biological tissues; particularly vocal folds and the tympanic membrane. The displacements data and its corresponding patterns found generates information on its characteristics that can be correlated with their physiological state. These methods prove to be an alternative viable and appropriate to characterize these soft tissues so important for the proper function of the human body. The result shows a potential impact on its possible uses in the field of otorhinolaryngology.

  10. Non-destructive imaging of buried electronic interfaces using a decelerated scanning electron beam.

    PubMed

    Hirohata, Atsufumi; Yamamoto, Yasuaki; Murphy, Benedict A; Vick, Andrew J

    2016-01-01

    Recent progress in nanotechnology enables the production of atomically abrupt interfaces in multilayered junctions, allowing for an increase in the number of transistors in a processor. However, uniform electron transport has not yet been achieved across the entire interfacial area in junctions due to the existence of local defects, causing local heating and reduction in transport efficiency. To date, junction uniformity has been predominantly assessed by cross-sectional transmission electron microscopy, which requires slicing and milling processes that can potentially introduce additional damage and deformation. It is therefore essential to develop an alternative non-destructive method. Here we show a non-destructive technique using scanning electron microscopy to map buried junction properties. By controlling the electron-beam energy, we demonstrate the contrast imaging of local junction resistances at a controlled depth. This technique can be applied to any buried junctions, from conventional semiconductor and metal devices to organic devices. PMID:27586090

  11. Inhomogeneous light shift effects on atomic quantum state evolution in non-destructive measurements

    NASA Astrophysics Data System (ADS)

    Windpassinger, Patrick J.; Oblak, Daniel; Busk Hoff, Ulrich; Appel, Jürgen; Kjærgaard, Niels; Polzik, Eugene S.

    2008-05-01

    Various parameters of a trapped collection of cold and ultracold atoms can be determined non-destructively by measuring the phase shift of an off-resonant probe beam, caused by the state-dependent index of refraction of the atoms. The dispersive light-atom interaction, however, gives rise to a differential light shift (ac Stark shift) between the atomic states which, for a non-uniform probe intensity distribution, causes an inhomogeneous dephasing between the atoms. In this paper, we investigate the effects of this inhomogeneous light shift in non-destructive measurement schemes in cold caesium. We interpret our experimental data on dispersively probed Rabi oscillations and Ramsey fringes in terms of a simple light shift model which is shown to describe the observed behavior well. Furthermore, we show that by using spin echo techniques, the inhomogeneous phase shift distribution between the two clock levels can be reversed.

  12. Quality parameters of mango and potential of non-destructive techniques for their measurement - a review.

    PubMed

    Jha, S N; Narsaiah, K; Sharma, A D; Singh, M; Bansal, S; Kumar, R

    2010-01-01

    The king of fruits "Mango" (Mangifera indica L.) is very nutritious and rich in carotenes. India produces about 50% of the total world's mango. Many researchers have reported the maturity indices and quality parameters for determination of harvesting time and eating quality. The methods currently used for determination of quality of mango are mostly based on the biochemical analysis, which leads to destruction of the fruits. Numerous works are being carried out to explore some non-destructive methods such as Near Infrared (NIR), Nuclear Magnetic Resonance (NMR), X-ray and Computed Tomography (CT), electronic nose, machine vision and ultrasound for quality determination of fruits. This paper deals with some recent work reported on quality parameters, harvesting and post-harvest treatments in relation to quality of mango fruits and reviews on some of the potential non-destructive techniques that can be explored for quality determination of mango cultivars. PMID:23572595

  13. Destructive and Non-Destructive Analysis Techniques for Failure Detection of QFN Packages

    NASA Astrophysics Data System (ADS)

    Adhila, M. N.; Wedianti, S.; Suhaimi, W. S. W. M.; Aishah, I.

    2010-03-01

    One of the latest developments in packaging technology is the QFN (Quad Flat Non-Lead) packages, which is both a chip scale package and plastic encapsulated package with lead pad at the bottom. In this paper, different type of commercial QFN single die packages were characterized by using destructive and non-destructive techniques. Non-destructive techniques such as Scanning Acoustic Microscope (SAM) and X-Ray analysis were used to observe package cracking, delamination and other failure mode. Application of SAM include detection of delaminations between lead frame, die face, paddle, heat sink, cracks and plastic encapsulant. In comparison to other techniques, SAM is sensitive to detect beneath the surface of devices which would be inaccessible otherwise by both conventional optical and electron microscopy inspection methods. Destructive technique such as Field Emission Electron Microscopy (FESEM) was implemented to address the failures of the QFN single die packages such as die cracking, lifted ball bonds and other failure mode.

  14. Non-destructive missile seeker flight testing: HWIL in the sky

    NASA Astrophysics Data System (ADS)

    Clements, Jim; Robinson, Joe; Robinson, Richard M.

    2010-04-01

    Surface to air missile development programs typically utilize hardware-in-the-loop (HWIL) simulations when available to provide a non-destructive high volume test environment for what are typically very expensive guidance sections. The HWIL, while invaluable, hasn't been able to obviate the need for missile flight tests. Because of the great expense of these missiles the designers are only allowed to perform a fraction of the desired tests. Missile Airframe Simulation Testbed (MAST) is a program conceived by US Army Aviation and Missile Research Development and Engineering Center (AMRDEC) that blends the non-destructive nature of HWIL with the confidence gained from flight tests to expand the knowledge gained while reducing the development schedule of new missile programs.

  15. The application of non-destructive techniques to the testing of a wind turbine blade

    SciTech Connect

    Sutherland, H.; Beattie, A.; Hansche, B.; Musial, W.; Allread, J.; Johnson, J.; Summers, M.

    1994-06-01

    NonDestructive Testing (NDT), also called NonDestructive Evaluation (NDE), is commonly used to monitor structures before, during, and after testing. This paper reports on the use of two NDT techniques to monitor the behavior of a typical wind turbine blade during a quasi-static test-to-failure. The two NDT techniques used were acoustic emission and coherent optical. The former monitors the acoustic energy produced by the blade as it is loaded. The latter uses electron shearography to measure the differences in surface displacements between two load states. Typical results are presented to demonstrate the ability of these two techniques to locate and monitor both high damage regions and flaws in the blade structure. Furthermore, this experiment highlights the limitations in the techniques that must be addressed before one or both can be transferred, with a high probability of success, to the inspection and monitoring of turbine blades during the manufacturing process and under normal operating conditions.

  16. Photoacoustic Spectroscopy as a Non-destructive Tool for Quantification of Pesticide Residue in Apple Cuticle

    NASA Astrophysics Data System (ADS)

    Liu, Lixian; Wang, Yafei; Gao, Chunming; Huan, Huiting; Zhao, Binxing; Yan, Laijun

    2015-06-01

    Photoacoustic spectroscopy (PAS), the non-destructive method to detect residue of dimethyl-dichloro-vinyl-phosphate (DDVP) pesticide in a cuticle of apple, is described. After constructing the PA experimental setup and identifying three characteristic peaks of DDVP in the near ultraviolet region, the PA spectra of an apple cuticle contaminated with DDVP were collected. The artificial neural network method was then applied to analyze data quantitatively. The results show a correlation coefficient exceeding 0.99 and a detection limit of 0.2 ppm, which is within the national food safety standard for maximum residue limits for pesticides in food (GB 2763-2012). This fact and the non-destructive character of PAS make the approach promising for detection of pesticide residue in fruits.

  17. Evaluation of Damage in Steels Subjected to Exploitation Loading - Destructive and Non-Destructive Methods

    NASA Astrophysics Data System (ADS)

    Kowalewski, Zbigniew L.; Mackiewicz, Sławomir; Szelążek, Jacek; Pietrzak, Krystyna; Augustyniak, Bolesław

    Damage due to creep and plastic flow is assessed using destructive and non-destructive methods in steels (40HNMA and P91). In the destructive methods the standard tension tests were carried out after prestraining and variations of the selected tension parameters were taken into account for damage identification. In order to assess a damage development during the creep and plastic deformation the tests for both steels were interrupted for a range of the selected strain magnitudes. The ultrasonic and magnetic techniques were used as the non-destructive methods for damage evaluation. The last step of the experimental programme contained microscopic observations. A very promising correlation between parameters of methods for damage development evaluation was achieved. It is well proved for the ultimate tensile stress and birefringence coefficient.

  18. Application of Non-destructive Methods of Stress-strain State at Hazardous Production Facilities

    NASA Astrophysics Data System (ADS)

    Shram, V.; Kravtsova, Ye; Selsky, A.; Bezborodov, Yu; Lysyannikova, N.; Lysyannikov, A.

    2016-06-01

    The paper deals with the sources of accidents in distillation columns, on the basis of which the most dangerous defects are detected. The analysis of the currently existing methods of non-destructive testing of the stress-strain state is performed. It is proposed to apply strain and acoustic emission techniques to continuously monitor dangerous objects, which helps prevent the possibility of accidents, as well as reduce the work.

  19. Non-destructive analysis in a study of the religious art objects

    NASA Astrophysics Data System (ADS)

    Vornicu, Nicoleta; Geba, Maria; Bibire, Cristina

    2009-08-01

    The icon Descending of the Saint Spirit from Bucium Church, dating in the year 1814 and was done in tempera on wood technology. The characterization of cultural heritage materials is essential for the comprehension of their degradation mechanisms. The present study aims at identifying the pigments in the various layers, establishing the possible existence of an organic binder and scientifically evaluating the state of preservation. To this end, were used non-destructive methods, as: microscopic (SEM), XRF and spectroscopic (FTIR).

  20. Rotational magnetic flux sensor with neural network for non-destructive testing

    SciTech Connect

    Enokizono, M.; Todaka, T.; Akita, M. . Faculty of Engineering); Nagata, S. . Faculty of Engineering)

    1993-11-01

    This paper presents a new non-destructive testing (NDT) method which utilizes rotational magnetic flux. In this system, the magnitude and phase value are measured and used to obtain information about defect. These values include the information about the shape or position of an unknown defect. The authors employ the neural network technique for estimation of a defect shape. The experimental results show the validity of the method.

  1. Non-destructive mapping of grain orientations in 3D by laboratory X-ray microscopy

    PubMed Central

    McDonald, S. A.; Reischig, P.; Holzner, C.; Lauridsen, E. M.; Withers, P. J.; Merkle, A. P.; Feser, M.

    2015-01-01

    The ability to characterise crystallographic microstructure, non-destructively and in three-dimensions, is a powerful tool for understanding many aspects related to damage and deformation mechanisms in polycrystalline materials. To this end, the technique of X-ray diffraction contrast tomography (DCT) using monochromatic synchrotron and polychromatic laboratory X-ray sources has been shown to be capable of mapping crystal grains and their orientations non-destructively in 3D. Here we describe a novel laboratory-based X-ray DCT modality (LabDCT), enabling the wider accessibility of the DCT technique for routine use and in-depth studies of, for example, temporal changes in crystallographic grain structure non-destructively over time through ‘4D’ in situ time-lapse studies. The capability of the technique is demonstrated by studying a titanium alloy (Ti-β21S) sample. In the current implementation the smallest grains that can be reliably detected are around 40 μm. The individual grain locations and orientations are reconstructed using the LabDCT method and the results are validated against independent measurements from phase contrast tomography and electron backscatter diffraction respectively. Application of the technique promises to provide important insights related to the roles of recrystallization and grain growth on materials properties as well as supporting 3D polycrystalline modelling of materials performance. PMID:26494523

  2. Non-destructively reading out information embedded inside real objects by using far-infrared light

    NASA Astrophysics Data System (ADS)

    Okada, Ayumi; Silapasuphakornwong, Piyarat; Suzuki, Masahiro; Torii, Hideyuki; Takashima, Youichi; Uehira, Kazutake

    2015-09-01

    This paper presents a technique that can non-destructively read out information embedded inside real objects by using far-infrared-light. We propose a technique that can protect the copyrights of digital content for homemade products using digital fabrication technologies such as those used in 3D printers. It embeds information on copyrights inside real objects produced by 3D printers by forming fine structures inside the objects as a watermark that cannot be observed from the outside. Fine structures are formed near the surface inside real objects when they are being fabricated. Information embedded inside real objects needs to be read out non-destructively. We used a technique that could non-destructively read out information from inside real objects by using far-infrared light. We conducted experiments where we structured fine cavities inside objects. The disposition of the fine domain contained valuable information. We used the flat and curved surfaces of the objects to identify them. The results obtained from the experiments demonstrated that the disposition patterns of the fine structures appeared on the surface of objects as a temperature profile when far-infrared light was irradiated on their surface. Embedded information could be read out successfully by analyzing the temperature profile images of the surface of the objects that were captured with thermography and these results demonstrated the feasibility of the technique we propose.

  3. Non-destructive single-pass low-noise detection of ions in a beamline.

    PubMed

    Schmidt, Stefan; Murböck, Tobias; Andelkovic, Zoran; Birkl, Gerhard; Nörtershäuser, Wilfried; Stahl, Stefan; Vogel, Manuel

    2015-11-01

    We have conceived, built, and operated a device for the non-destructive single-pass detection of charged particles in a beamline. The detector is based on the non-resonant pick-up and subsequent low-noise amplification of the image charges induced in a cylindrical electrode surrounding the particles' beam path. The first stage of the amplification electronics is designed to be operated from room temperature down to liquid helium temperature. The device represents a non-destructive charge counter as well as a sensitive timing circuit. We present the concept and design details of the device. We have characterized its performance and show measurements with low-energy highly charged ions (such as Ar(13+)) passing through one of the electrodes of a cylindrical Penning trap. This work demonstrates a novel approach of non-destructive, low noise detection of charged particles which is, depending on the bunch structure, suitable, e.g., for ion traps, low-energy beamlines or accelerator transfer sections. PMID:26628124

  4. Non-destructive single-pass low-noise detection of ions in a beamline

    SciTech Connect

    Schmidt, Stefan; Murböck, Tobias; Birkl, Gerhard; Andelkovic, Zoran; Vogel, Manuel; Nörtershäuser, Wilfried; Stahl, Stefan

    2015-11-15

    We have conceived, built, and operated a device for the non-destructive single-pass detection of charged particles in a beamline. The detector is based on the non-resonant pick-up and subsequent low-noise amplification of the image charges induced in a cylindrical electrode surrounding the particles’ beam path. The first stage of the amplification electronics is designed to be operated from room temperature down to liquid helium temperature. The device represents a non-destructive charge counter as well as a sensitive timing circuit. We present the concept and design details of the device. We have characterized its performance and show measurements with low-energy highly charged ions (such as Ar{sup 13+}) passing through one of the electrodes of a cylindrical Penning trap. This work demonstrates a novel approach of non-destructive, low noise detection of charged particles which is, depending on the bunch structure, suitable, e.g., for ion traps, low-energy beamlines or accelerator transfer sections.

  5. Non-destructive estimation of root pressure using sap flow, stem diameter measurements and mechanistic modelling

    PubMed Central

    De Swaef, Tom; Hanssens, Jochen; Cornelis, Annelies; Steppe, Kathy

    2013-01-01

    Background Upward water movement in plants via the xylem is generally attributed to the cohesion–tension theory, as a response to transpiration. Under certain environmental conditions, root pressure can also contribute to upward xylem water flow. Although the occurrence of root pressure is widely recognized, ambiguity exists about the exact mechanism behind root pressure, the main influencing factors and the consequences of root pressure. In horticultural crops, such as tomato (Solanum lycopersicum), root pressure is thought to cause cells to burst, and to have an important impact on the marketable yield. Despite the challenges of root pressure research, progress in this area is limited, probably because of difficulties with direct measurement of root pressure, prompting the need for indirect and non-destructive measurement techniques. Methods A new approach to allow non-destructive and non-invasive estimation of root pressure is presented, using continuous measurements of sap flow and stem diameter variation in tomato combined with a mechanistic flow and storage model, based on cohesion–tension principles. Key Results Transpiration-driven sap flow rates are typically inversely related to stem diameter changes; however, this inverse relationship was no longer valid under conditions of low transpiration. This decoupling between sap flow rates and stem diameter variations was mathematically related to root pressure. Conclusions Root pressure can be estimated in a non-destructive, repeatable manner, using only external plant sensors and a mechanistic model. PMID:23211757

  6. Non-destructive analysis of extracellular matrix development in cardiovascular tissue-engineered constructs.

    PubMed

    Tuemen, M; Nguyen, D V A; Raffius, J; Flanagan, T C; Dietrich, M; Frese, J; Schmitz-Rode, T; Jockenhoevel, S

    2013-05-01

    In the field of tissue engineering, there is an increasing demand for non-destructive methods to quantify the synthesis of extracellular matrix (ECM) components such as collagens, elastin or sulphated glycosaminoglycans (sGAGs) in vitro as a quality control before clinical use. In this study, procollagen I carboxyterminal peptide (PICP), procollagen III aminoterminal peptide (PIIINP), tropoelastin and sGAGs are investigated for their potential use as non-destructive markers in culture medium of statically cultivated cell-seeded fibrin gels. Measurement of PICP as marker for type I collagen synthesis, and PIIINP as marker of type III collagen turnover, correlated well with the hydroxyproline content of the fibrin gels, with a Pearson correlation coefficient of 0.98 and 0.97, respectively. The measurement of tropoelastin as marker of elastin synthesis correlated with the amount of elastin retained in fibrin gels with a Pearson correlation coefficient of 0.99. sGAGs were retained in fibrin gels, but were not detectable in culture medium at any time of measurement. In conclusion, this study demonstrates the potential of PICP and tropoelastin as non-destructive culture medium markers for collagen and elastin synthesis. To our knowledge, this is the first study in cardiovascular tissue engineering investigating the whole of here proposed biomarkers of ECM synthesis to monitor the maturation process of developing tissue non-invasively, but for comprehensive assessment of ECM development, these biomarkers need to be investigated in further studies, employing dynamic cultivation conditions and more complex tissue constructs. PMID:23307024

  7. The use of non destructive biomarkers in the study of marine mammals.

    PubMed

    M Cristina Fossi And Letizia Marsili

    1997-01-01

    Marine mammals have been subject to heavy anthropogenic pressure by direct killing and chemical pollution all over the world. Most studies of contamination and biomarker responses in marine mammals have been conducted using animals killed by hunting out of a total of 12 cetacean species studied, 45 of the specimens were obtained by sacrificing the animal; out of a total of eight pinniped species studied, 40 of the specimens were obtained by killing. The development of a series of non destructive techniques to evaluate biomarker responses and residue levels is recommended for the hazard assessment and conservation of endangered species of marine mammals. Here we review the current status of the non destructive biomarker approach in marine mammals, describing the biological materials available for non destructive tests in stranded brain, liver, blood, skin, subcutaneous blubber, muscle and fur and free ranging animals blood, skin biopsy, fur and faeces and the respective biomarker techniques mixed function oxidase activity and DNA damage in skin biopsy samples; porphyrins in faeces and fur; esterases, porphyrins, clinical biochemical parameter, vitamin A and micronuclei in blood samples. Residue analysis can be carried out in the various biological materials. We also report the results of applying this methodological approach to cetaceans minke whale Balaenoptera acutorostrata, fin whale-- Balaenoptera physalus, beluga whale-- Delphinapterus leucas, short finned pilot whale-- Globicephala macrorhynchus, harbour porpoise -- Phocoena phocoena, Rissos dolphin-- Risso s Grampus griseus, Dall s porpoise-- Phocoenoides dalli dalli, melon headed whale-- Peponocephala electra, bottlenose dolphin -- Tursiops truncatus, striped dolphin-- Stenella coeruleoalba, spinner dolphin-- Stenella longirostris, killer whale-- Orcinus orca and pinnipeds northern fur seal- Callorhinus ursinus, hooded seal-- Cystophora cristata, grey seal-- Halichoerus grypus, harbour seal-- Phoca vitulina

  8. Photothermal Analysis Applied To Non-Destructive Evaluation Of Paint On Polymer Substrates

    NASA Astrophysics Data System (ADS)

    Vergne, D.; Busse, G.

    1988-10-01

    The decoration and protection quality of coatings on polymers is of considerable interest for industrial applications. However, at present there is no non-destructive (NDE) method to monitor the quality of these coatings during the manufacturing process or while they are in use. As an approach for such a method we use photothermal analysis where the propagation and reflection of optically generated thermal waves is investigated. We found that one can monitor the drying process, the effect of surface temperature treatment, and coating thickness (accuracy + 2 μm in 50 μm thickness). The information obtained with this remote NDE method is adequate for most industrial applications, eg car manufacturing.

  9. Non-Destructive Testing with Atmospheric Pressure Radio-Frequency Plasma

    NASA Astrophysics Data System (ADS)

    May, A.; Andarawis, E.

    2007-03-01

    We summarize our recent work using radio-frequency (RF) atmospheric pressure plasma (APP) for non-destructive evaluation (NDE), specifically for: (1) Clearance sensing (0-5mm) on rotating components, and (2) Generation of broadband ultrasound in air at 900kHz. RF-APP showed potential in both of these common NDE requirements, but further work is required to better characterize and optimize the performance of the new techniques. Application of RF-APP to other NDE disciplines, such as plasma spectroscopy and gas flow measurement, is also likely to be advantageous, especially in harsh environments where existing approaches are prohibitively expensive or complex.

  10. A non-destructive metrology solution for detailed measurements of imprint templates and media

    NASA Astrophysics Data System (ADS)

    Roberts, Jeffrey; Hu, Linlin; Eriksson, Torbjörn; Thulin, Kristian; Heidari, Babak

    2009-10-01

    This study investigates a non-destructive optical metrology technique, that furnishes measurement solutions for hard drive discrete track recording (DTR) and bit patterned media (BPM) templates and imprints. From the measurement and analysis of polarized reflectance and transmittance, feature height and profile of DTR and BPM templates and imprints, as well as residual layer thickness of imprints, are accurately determined, and uniformity maps of these parameters are produced in a fraction of a minute. Simulations of theoretical polarized reflectance and transmittance, relating to next generation structures, demonstrate that the optical metrology solution has capability for future products.

  11. Non-destructive terahertz imaging of illicit drugs using spectral fingerprints

    NASA Astrophysics Data System (ADS)

    Kawase, Kodo; Ogawa, Yuichi; Watanabe, Yuuki; Inoue, Hiroyuki

    2003-10-01

    The absence of non-destructive inspection techniques for illicit drugs hidden in mail envelopes has resulted in such drugs being smuggled across international borders freely. We have developed a novel basic technology for terahertz imaging, which allows detection and identification of drugs concealed in envelopes, by introducing the component spatial pattern analysis. The spatial distributions of the targets are obtained from terahertz multispectral transillumination images, using absorption spectra measured with a tunable terahertz-wave source. The samples we used were methamphetamine and MDMA, two of the most widely consumed illegal drugs in Japan, and aspirin as a reference.

  12. Non-destructive Testing by Infrared Thermography Under Random Excitation and ARMA Analysis

    NASA Astrophysics Data System (ADS)

    Bodnar, J. L.; Nicolas, J. L.; Candoré, J. C.; Detalle, V.

    2012-11-01

    Photothermal thermography is a non-destructive testing (NDT) method, which has many applications in the field of control and characterization of thin materials. This technique is usually implemented under CW or flash excitation. Such excitations are not adapted for control of fragile materials or for multi-frequency analysis. To allow these analyses, in this article, the use of a new control mode is proposed: infrared thermography under random excitation and auto regressive moving average analysis. First, the principle of this NDT method is presented. Then, the method is shown to permit detection, with low energy constraints, of detachments situated in mural paintings.

  13. Non-destructive method for determining neutron exposure and constituent concentrations of a body

    DOEpatents

    Gold, Raymond; McElroy, William N.

    1986-01-01

    A non-destructive method for determination of neutron exposure and constituent concentrations in an object, such as reactor pressure vessel, is based on the observation of characteristic gamma-rays emitted by activation products in the object by using a unique continuous gamma-ray spectrometer. The spectrometer views the object through appropriate collimators to determine the absolute emission rate of these characteristic gamma-rays, thereby ascertaining the absolute activity of given activation products in the object. These data can then be used to deduce the spatial and angular dependence of neutron exposure or the spatial constituent concentration at regions of interest within the object.

  14. Non-Destructive Evaluation Method and Apparatus for Measuring Acoustic Material Nonlinearity

    NASA Technical Reports Server (NTRS)

    Yost, William T. (Inventor); Cantrell, John H. (Inventor)

    2002-01-01

    An acoustic non-linearity parameter (beta) measurement method and system for Non-Destructive Evaluation (NDE) of materials and structural members obviates the need for electronic calibration of the measuring equipment. Unlike known substitutional measuring techniques requiring elaborate calibration procedures, the electrical outputs of the capacitive detector of a sample with known beta and the test sample of unknown beta are compared to determine the unknown beta. In order to provide the necessary stability of the present-inventive reference-based approach, the bandpass filters of the measurement system are maintained in a temperature-controlled environment, and the line voltage supplied to said amplifiers is well-regulated.

  15. Computed tomography for non-destructive evaluation of composites: Applications and correlations

    NASA Technical Reports Server (NTRS)

    Goldberg, B.; Hediger, L.; Noel, E.

    1985-01-01

    The state-of-the-art fabrication techniques for composite materials are such that stringent species-specific acceptance criteria must be generated to insure product reliability. Non-destructive evaluation techniques including computed tomography (CT), X-ray radiography (RT), and ultrasonic scanning (UT) are investigated and compared to determine their applicability and limitations to graphite epoxy, carbon-carbon, and carbon-phenolic materials. While the techniques appear complementary, CT is shown to provide significant, heretofore unattainable data. Finally, a correlation of NDE techniques to destructive analysis is presented.

  16. Non-destructive high-resolution thermal imaging techniques to evaluate wildlife and delicate biological samples

    NASA Astrophysics Data System (ADS)

    Lavers, C.; Franklin, P.; Franklin, P.; Plowman, A.; Sayers, G.; Bol, J.; Shepard, D.; Fields, D.

    2009-07-01

    Thermal imaging cameras now allows routine monitoring of dangerous yet endangered wildlife in captivity. This study looks at the potential applications of radiometrically calibrated thermal data to wildlife, as well as providing parameters for future materials applications. We present a non-destructive active testing technique suitable for enhancing imagery contrast of thin or delicate biological specimens yielding improved thermal contrast at room temperature, for analysis of sample thermal properties. A broad spectrum of animals is studied with different textured surfaces, reflective and emissive properties in the infra red part of the electromagnetic spectrum. Some surface features offer biomimetic materials design opportunities.

  17. Non-destructive evaluation of metal-to-metal adhesive joints using vibration analysis: experimental results

    NASA Astrophysics Data System (ADS)

    Pandurangan, Pradeep; Buckner, Gregory D.

    2006-03-01

    Vibration based non-destructive evaluation shows promise for damage detection in metal-to-metal adhesive joints. This research investigates an experimental technique to diagnose damage in single-lap adhesive joints subject to cyclical tensile loading. Vibration analysis reveals that damage can be correlated with changes in identified modal damping ratios. Constant amplitude forcing functions are employed to eliminate amplitude-dependent nonlinearities in the dynamic response profiles. Damping estimates obtained from time-domain analyses correlate well with damage magnitudes. Finite element modal analysis of the lap joints supports the experimental results.

  18. Second harmonic generation for contactless non-destructive characterization of silicon on insulator wafers

    NASA Astrophysics Data System (ADS)

    Damianos, D.; Pirro, L.; Soylu, G.; Ionica, I.; Nguyen, V.; Vitrant, G.; Kaminski, A.; Blanc-Pelissier, D.; Onestas, L.; Changala, J.; Kryger, M.; Cristoloveanu, S.

    2016-01-01

    In this work we investigate a non-invasive, non-destructive characterization technique for monitoring the quality of film, oxide and interfaces in silicon-on-insulator (SOI) wafers. This technique is based on optical Second Harmonic Generation (SHG). The principles of SHG and the experimental setup will be thoroughly described. The experimental parameters best suited for testing SOI wafers with SHG are identified. SOI geometry, as well as the passivation of the top surface, both have an impact on the observed SHG signal. The back-gate bias applied on the substrate is shown to modulate the SHG signal.

  19. Non-destructive qualification tests for ITER cryogenic axial insulating breaks

    SciTech Connect

    Kosek, Jacek; Lopez, Roberto; Tommasini, Davide; Rodriguez-Mateos, Felix

    2014-01-29

    In the ITER superconducting magnets the dielectric separation between the CICC (Cable-In-Conduit Conductors) and the helium supply pipes is made through the so-called insulating breaks (IB). These devices shall provide the required dielectric insulation at a 30 kV level under different types of stresses and constraints: thermal, mechanical, dielectric and ionizing radiations. As part of the R and D program, the ITER Organization launched contracts with industrial companies aimed at the qualification of the manufacturing techniques. After reviewing the main functional aspects, this paper describes and discusses the protocol established for non-destructive qualification tests of the prototypes.

  20. Non-destructive evaluation of cylindrical composite structures using photothermal radiometry

    NASA Astrophysics Data System (ADS)

    Wang, C.; Mandelis, A.; Liu, Y.

    2005-06-01

    Thermal-wave diagnostics by means of infrared photothermal radiometry (PTR) has been used for quantitative non-destructive evaluation of cylindrical composite structures. To quantitatively evaluate the thermal-wave field of a cylindrical composite material, the Green function corresponding to the composite structure has been developed and subsequently the thermal-wave field has been derived. Furthermore, the characteristics of the thermal-wave field for a cylindrical material with a surface coating are discussed. Experimental results from a stainless steel (AISI 302) tube are used to validate the theoretical model.

  1. Application of magnetic resonance imaging to non-destructive void detection in watermelon

    NASA Astrophysics Data System (ADS)

    Saito, K.; Miki, T.; Hayashi, S.; Kajikawa, H.; Shimada, M.; Kawate, Y.; Nishizawa, T.; Ikegaya, D.; Kimura, N.; Takabatake, K.; Sugiura, N.; Suzuki, M.

    A novel application of magnetic resonance imaging (MRI) is described. The possibility of utilizing MRI for non-destructive quality evaluation of watermelons was studied. In this study, we applied MRI to the detection of internal voids in watermelons. In order to increase the measurement rate, we employed a one-dimensional projection profile method instead of observing a two-dimensional cross-sectional image. The void detection was carried out with this technique over 30 samples and 28 samples were correctly evaluated. The measurement rate was 900 ms per sample, which is an acceptable speed for a sorting machine in the agricultural field.

  2. A new facility for non-destructive assay using a 252Cf source.

    PubMed

    Stevanato, L; Caldogno, M; Dima, R; Fabris, D; Hao, Xin; Lunardon, M; Moretto, S; Nebbia, G; Pesente, S; Pino, F; Sajo-Bohus, L; Viesti, G

    2013-03-01

    A new laboratory facility for non-destructive analysis (NDA) using a time-tagged (252)Cf source is presented. The system is designed to analyze samples having maximum size of about 20 × 25 cm(2), the material recognition being obtained by measuring simultaneously total and energy dependent transmission of neutrons and gamma rays. The equipment technical characteristics and performances of the NDA system are presented, exploring also limits due to the sample thickness. Some recent applications in the field of cultural heritage are presented. PMID:23276691

  3. Improved Inversion Algorithms for Near Surface Characterization

    NASA Astrophysics Data System (ADS)

    Astaneh, Ali Vaziri; Guddati, Murthy N.

    2016-05-01

    Near-surface geophysical imaging is often performed by generating surface waves, and estimating the subsurface properties through inversion, i.e. iteratively matching experimentally observed dispersion curves with predicted curves from a layered half-space model of the subsurface. Key to the effectiveness of inversion is the efficiency and accuracy of computing the dispersion curves and their derivatives. This paper presents improved methodologies for both dispersion curve and derivative computation. First, it is shown that the dispersion curves can be computed more efficiently by combining an unconventional complex-length finite element method (CFEM) to model the finite depth layers, with perfectly matched discrete layers (PMDL) to model the unbounded half-space. Second, based on analytical derivatives for theoretical dispersion curves, an approximate derivative is derived for so-called effective dispersion curve for realistic geophysical surface response data. The new derivative computation has a smoothing effect on the computation of derivatives, in comparison with traditional finite difference (FD) approach, and results in faster convergence. In addition, while the computational cost of FD differentiation is proportional to the number of model parameters, the new differentiation formula has a computational cost that is almost independent of the number of model parameters. At the end, as confirmed by synthetic and real-life imaging examples, the combination of CFEM+PMDL for dispersion calculation and the new differentiation formula results in more accurate estimates of the subsurface characteristics than the traditional methods, at a small fraction of computational effort.

  4. Chain dynamics near surfaces: an unconventional approach

    NASA Astrophysics Data System (ADS)

    Masson, Jean-Loup; Green, Peter

    2001-03-01

    Chain dynamics near surfaces: an unconventional approach Jean-Loup Masson and Peter F. Green Graduate Program in Materials Science and Department of Chemical Engineering The University of Texas at Austin When the thickness of a polymer film is comparable to the radius of gyration, or a few radii of gyration, of the polymer chains, the properties of the film can differ appreciably from the bulk. Indeed, recent studies have documented the existence of changes of the glass transition, translational chain diffusion and the viscosity, with decreasing film thickness. For liquid films, a few tens of nanometers thick, on substrates, the disjoining pressure has a significant effect on the stability of the film. This can result on the formation of patterns reflecting fluctuations in the local film thickness. The structural, time-dependent, evolution of the film is a reflection of the effects of the disjoining pressure together with the translational dynamics of the chains. This presentation discusses the structural evolution of a thin polymer film in light of theoretical models to gain insight into the manner in which the diffusion and viscosity of the polymer changes with decreasing film thickness.

  5. PREFACE: III All-Russian Scientific and Practical Conference on Innovations in Non-Destructive Testing (SibTest 2015)

    NASA Astrophysics Data System (ADS)

    2016-01-01

    This issue of the journal is devoted to the research and studies presented at the III All-Russian Scientific and Practical Conference on Innovations in Non-Destructive Testing SibTest. The conference was held in Altai, Russia, on 27-31 July 2015. The conference brought together experts from different countries and organizations who had a great opportunity to share knowledge during oral and poster presentations and to initiate discussions on topics that are of interest to the conference attendees. The conference aimed to discuss innovative methods and the application of advanced technologies in non-destructive testing. The conference also attempted to bring together university, academic and industrial science, to expand the co-operation of scientists from different countries in research and development and the commercialization of innovative technologies in non-destructive testing. The key themes of the conference were: ultrasonic and acoustic testing; electromagnetic and thermal testing; various types of radiation non-destructive testing; passive and active testing techniques. The conference organizers are the Institute of Non-Destructive Testing, Tomsk Polytechnic University, with the assistance of the Russian Society for Non-Destructive Testing and Technical Diagnostics, Institute of Strength Physics and Materials Science, Siberian Branch of the Russian Academy of Sciences, National Research Tomsk State University, Moscow State Institute of Radio Engineering, Electronics and Automation.

  6. Surface preparation for non-destructive detection of surface cracks in stainless steel and carbon steel piping

    SciTech Connect

    Funderburg, I.M.

    1996-07-01

    Engineers within the chemical process industries are among other things, charged with the task of determining the reliability of piping and equipment. As part of this evaluation, the surfaces of process equipment and piping are often examined for evidence of stress corrosion cracking (SCC) or other tightly closed surface cracks. Presently there is no consensus as to which is the ``best`` technique for preparing and inspecting carbon steel and stainless steel vessels or piping for surface cracks. The specific concern within industry is that Stress Corrosion Cracking (SCC) might go undetected if the surface preparation closes over such tight cracks. This paper presents results of a study, MTI commissioned to collect additional data, examine the literature, and interview industrial materials engineers, independent inspection specialists, non-destructive examination consultants, and other representatives of industries that have equipment which must be inspected for surface cracks. Discussed are the differing surface preparation techniques used, the use of standards for evaluating the effectiveness of the techniques, and what is felt to be the ``Key Learnings`` from the investigation.

  7. Dust Levitation and Transport Near Surfaces

    NASA Astrophysics Data System (ADS)

    Sickafoose, A. A.; Colwell, J. E.; Horanyi, M.; Robertson, S.

    2002-12-01

    There are many examples of active dust transport near surfaces in the solar system: dust grains suspended above the lunar surface, spokes observed in Saturn's rings, and recent images of infilled craters from the NEAR spacecraft at Eros. Electrostatic dust levitation and transport have also been theorized to occur on Mercury, asteroids, and comets. Dusty regoliths are produced by the interplanetary micrometeoroid flux on nearly all airless bodies in the solar system. Therefore, understanding dust charging, levitation, and dynamics above surfaces is important for interpreting remote sensing data and analyzing the evolution of most planetary surfaces. Objects in a plasma, such as planetary bodies in the solar wind, charge to a floating potential determined by the balance between charging currents in the local plasma environment. The primary charging currents are due to collection of electrons and ions from the plasma, photoemission, and secondary electron emission. When photoemission is the dominant charging process, a photoelectron sheath forms near the surface of the object. Positively charged particles released from the surface can levitate above the surface at a height where the gravitational force is balanced by the electric force. In cases where secondary electron emission and photoemission are weak, objects will become negatively charged due to electron collection and will be surrounded by a plasma sheath. Negatively charged dust grains from these surfaces can levitate in the electric field created by the plasma sheath. Dust levitation and transport near surfaces in the solar system is thought to be primarily due to the interaction between charged dust particles and a photoelectron or plasma sheath on the surface. We report the results of experiments on the levitation and transport of dust particles in an argon plasma sheath above a flat, conducting surface. Levitation experiments are performed using monodisperse polystyrene DVB microbeads. Transport

  8. Non-destructive measurement of soil liquefaction density change by crosshole radar tomography, Treasure Island, California

    USGS Publications Warehouse

    Kayen, Robert E.; Barnhardt, Walter A.; Ashford, Scott; Rollins, Kyle

    2000-01-01

    A ground penetrating radar (GPR) experiment at the Treasure Island Test Site [TILT] was performed to non-destructively image the soil column for changes in density prior to, and following, a liquefaction event. The intervening liquefaction was achieved by controlled blasting. A geotechnical borehole radar technique was used to acquire high-resolution 2-D radar velocity data. This method of non-destructive site characterization uses radar trans-illumination surveys through the soil column and tomographic data manipulation techniques to construct radar velocity tomograms, from which averaged void ratios can be derived at 0.25 - 0.5m pixel footprints. Tomograms of void ratio were constructed through the relation between soil porosity and dielectric constant. Both pre- and post-blast tomograms were collected and indicate that liquefaction related densification occurred at the site. Volumetric strains estimated from the tomograms correlate well with the observed settlement at the site. The 2-D imagery of void ratio can serve as high-resolution data layers for numerical site response analysis.

  9. Non-invasive and non-destructive measurements of confluence in cultured adherent cell lines

    PubMed Central

    Busschots, Steven; O’Toole, Sharon; O’Leary, John J.; Stordal, Britta

    2014-01-01

    Many protocols used for measuring the growth of adherent monolayer cells in vitro are invasive, destructive and do not allow for the continued, undisturbed growth of cells within flasks. Protocols often use indirect methods for measuring proliferation. Microscopy techniques can analyse cell proliferation in a non-invasive or non-destructive manner but often use expensive equipment and software algorithms. In this method images of cells within flasks are captured by photographing under a standard inverted phase contract light microscope using a digital camera with a camera lens adaptor. Images are analysed for confluence using ImageJ freeware resulting in a measure of confluence known as an Area Fraction (AF) output. An example of the AF method in use on OVCAR8 and UPN251 cell lines is included. • Measurements of confluence from growing adherent cell lines in cell culture flasks is obtained in a non-invasive, non-destructive, label-free manner. • The technique is quick, affordable and eliminates sample manipulation. • The technique provides an objective, consistent measure of when cells reach confluence and is highly correlated to manual counting with a haemocytometer. The average correlation co-efficient from a Spearman correlation (n = 3) was 0.99 ± 0.008 for OVCAR8 (p = 0.01) and 0.99 ± 0.01 for UPN251 (p = 0.01) cell lines. PMID:26150966

  10. A semi-automatic non-destructive method to quantify grapevine downy mildew sporulation.

    PubMed

    Peressotti, Elisa; Duchêne, Eric; Merdinoglu, Didier; Mestre, Pere

    2011-02-01

    The availability of fast, reliable and non-destructive methods for the analysis of pathogen development contributes to a better understanding of plant-pathogen interactions. This is particularly true for the genetic analysis of quantitative resistance to plant pathogens, where the availability of a method allowing a precise quantification of pathogen development allows the reliable detection of different genomic regions involved in the resistance. Grapevine downy mildew, caused by the biotrophic Oomycete Plasmopara viticola, is one of the most important diseases affecting viticulture. Here we report the development of a simple image analysis-based semi-automatic method for the quantification of grapevine downy mildew sporulation, requiring just a compact digital camera and the open source software ImageJ. We confirm the suitability of the method for the analysis of the interaction between grapevine and downy mildew by performing QTL analysis of resistance to downy mildew as well as analysis of the kinetics of downy mildew infection. The non-destructive nature of the method will enable comparison between the phenotypic and molecular data obtained from the very same sample, resulting in a more accurate description of the interaction, while its simplicity makes it easily adaptable to other plant-pathogen interactions, in particular those involving downy mildews. PMID:21167874

  11. Non-invasive and non-destructive measurements of confluence in cultured adherent cell lines.

    PubMed

    Busschots, Steven; O'Toole, Sharon; O'Leary, John J; Stordal, Britta

    2015-01-01

    Many protocols used for measuring the growth of adherent monolayer cells in vitro are invasive, destructive and do not allow for the continued, undisturbed growth of cells within flasks. Protocols often use indirect methods for measuring proliferation. Microscopy techniques can analyse cell proliferation in a non-invasive or non-destructive manner but often use expensive equipment and software algorithms. In this method images of cells within flasks are captured by photographing under a standard inverted phase contract light microscope using a digital camera with a camera lens adaptor. Images are analysed for confluence using ImageJ freeware resulting in a measure of confluence known as an Area Fraction (AF) output. An example of the AF method in use on OVCAR8 and UPN251 cell lines is included. •Measurements of confluence from growing adherent cell lines in cell culture flasks is obtained in a non-invasive, non-destructive, label-free manner.•The technique is quick, affordable and eliminates sample manipulation.•The technique provides an objective, consistent measure of when cells reach confluence and is highly correlated to manual counting with a haemocytometer. The average correlation co-efficient from a Spearman correlation (n = 3) was 0.99 ± 0.008 for OVCAR8 (p = 0.01) and 0.99 ± 0.01 for UPN251 (p = 0.01) cell lines. PMID:26150966

  12. Non-destructive quantification of pharmaceutical tablet coatings using terahertz pulsed imaging and optical coherence tomography

    NASA Astrophysics Data System (ADS)

    Zhong, Shuncong; Shen, Yao-Chun; Ho, Louise; May, Robert K.; Zeitler, J. Axel; Evans, Mike; Taday, Philip F.; Pepper, Michael; Rades, Thomas; Gordon, Keith C.; Müller, Ronny; Kleinebudde, Peter

    2011-03-01

    Optical coherence tomography (OCT) and terahertz pulsed imaging (TPI) are two powerful techniques allowing high quality cross-sectional images from within scattering media to be obtained non-destructively. In this paper, we report experimental results of using OCT and TPI for quantitatively characterizing pharmaceutical tablet coatings in the thickness range of 10-140 μm. We found that the spectral OCT system developed in-house has an axial resolution of 0.9 μm, and is capable of quantifying very thin coatings in the range of 10-60 μm. The upper limit of 60 μm within the tablet coating and core is owed to the strong scattering of OCT light, which has relatively short wavelengths in the range of 0.5-1.0 μm. On the other hand, TPI utilizes terahertz radiation that has substantially long wavelengths in the range of hundreds of microns, and thus is less prone to the scattering problem. Consequently TPI has been demonstrated to be able to quantify thicker coatings in the range of 40-140 μm and beyond. We concluded that OCT and TPI are two complementary analytical techniques for non-destructive and quantitative characterization of pharmaceutical tablet coatings.

  13. Non-destructive Magnetic Evaluation of Laser Weld Quality in Hot Rolled Coils

    NASA Astrophysics Data System (ADS)

    Mohapatra, J. N.; Chakradhar, I.; Rao, K. R. C.; Rao, V. V. L.; Kaza, Marutiram

    2015-06-01

    Weld quality evaluation was conducted on laser welded thin sectsions (2 mm) of hot-rolled (HR) low-carbon steel coils during cold rolling process. The analysis revealed that the poor welds consisting of the weld defects like incomplete fusion, cluster of porosity, and large difference in hardness between the weld zone and base metal were responsible for the weld failures. Experiments were conducted by varying the welding parameters; laser power and welding speed to optimize the parameters for minimizing the weld defects. The optimized weld process parameters have helped elimination of weld defects and the results are verified with microscopy and microhardness measurements. As destructive evaluation techniques are time consuming and not always permitted in industrial applications, attempts have been made in the present investigation for the utilization of suitable non-destructive techniques for the evaluation of weld quality. Non-destructive magnetic techniques of magnetic hysteresis loop and magnetic Barkhausen emissions were used in the present investigation to establish possible correlations of magnetic properties across the weld seam with the mechanical property (microhardness) for evaluation of weld quality. It is inferred that the magnetic properties of coercivity and inverse of root mean square voltage can be effectively utilized to determine weld quality in HR steel coils.

  14. Application of non-destructive techniques to assess the state of Hagia Sophia's mosaics

    NASA Astrophysics Data System (ADS)

    Moropoulou, Antonia; Karoglou, Maria; Labropoulos, Kyriakos C.; Delegou, Ekaterini T.; Katsiotis, Nikolaos K.; Karagiannis-Bakolas, Asterios

    2012-04-01

    The church of Hagia Sophia in Istanbul is a world heritage monument that epitomizes the byzantine ecclesiastic architecture. The church is decorated with mosaics from various historic periods. The preservation state of the mosaics is of high importance. In this study, non-destructive techniques (ground penetrating radar, infra-red thermography, fibreoptics microscopy) were employed on south upper gallery mosaic areas. The main aim of this on-site investigation was the evaluation of the preservation state of the mosaics and the previous interventions (materials characterization and decay diagnosis) in order to assess the performance of previous conservation/restoration interventions, as well as to verify the presence of mosaics in layers below the external plaster surfaces. Results indicated that is indeed possible to locate the grid of rendered mosaics. Regarding the preservation state of the mosaics, it was indicated that the main environmental decay factors were the high relative humidity levels with co-action of salt damp as well as the air pollutants. Moreover, it was revealed that previous incompatible restoration/conservation interventions have often accelerated the mosaics' degradation processes. Using non-destructive techniques it was possible to identify areas where the mosaic materials (tesserae and mortars) presented decay problems and in addition identify sub-layers that pose risk of detachment or decay intensification. In this way, NDT can contribute to the development of a strategic planning for mosaics conservation, protection and revealing.

  15. Neural network and principal component regression in non-destructive soluble solids content assessment: a comparison.

    PubMed

    Chia, Kim-seng; Abdul Rahim, Herlina; Abdul Rahim, Ruzairi

    2012-02-01

    Visible and near infrared spectroscopy is a non-destructive, green, and rapid technology that can be utilized to estimate the components of interest without conditioning it, as compared with classical analytical methods. The objective of this paper is to compare the performance of artificial neural network (ANN) (a nonlinear model) and principal component regression (PCR) (a linear model) based on visible and shortwave near infrared (VIS-SWNIR) (400-1000 nm) spectra in the non-destructive soluble solids content measurement of an apple. First, we used multiplicative scattering correction to pre-process the spectral data. Second, PCR was applied to estimate the optimal number of input variables. Third, the input variables with an optimal amount were used as the inputs of both multiple linear regression and ANN models. The initial weights and the number of hidden neurons were adjusted to optimize the performance of ANN. Findings suggest that the predictive performance of ANN with two hidden neurons outperforms that of PCR. PMID:22302428

  16. Checking collagen preservation in archaeological bone by non-destructive studies (Micro-CT and IBA)

    NASA Astrophysics Data System (ADS)

    Beck, L.; Cuif, J.-P.; Pichon, L.; Vaubaillon, S.; Dambricourt Malassé, A.; Abel, R. L.

    2012-02-01

    The material to be studied is a piece of human skull discovered (1999) in Pleistocene sediments from the Orsang river (Gujarat state, India). From anatomical view point, this skull is highly composite: modern Homo sapiens characters are associated to undoubtedly more ancient features. Absolute dating by 14C is critical to understand this discovery. Prior to dating measurements, non-destructive studies have been carried out. Micro-CT reconstruction (X-ray microtomography) and Ion Beam Analysis (IBA) have been undertaken to check the structural preservation of the fossil and the collagen preservation. PIXE elemental map was used to select well-preserved bone area. RBS/EBS and NRA were used for light element quantification, in particular C, N and O contents. We also demonstrate that the PIXE-RBS/EBS combination is a effective tool for the whole characterization of archaeological and recent bones by analysing in one experiment both mineral and organic fractions. We have shown that the archaeological bone, a fragment of the potentially oldest modern Indian, is enough preserved for radiocarbon dating. We propose that Elastic Backscattering Spectrometry (EBS) using 3 MeV protons could be a good non destructive alternative to conventional CHN method using Carbon-Hydrogen-Nitrogen analyzer for measuring C and N before 14C dating.

  17. Non-Destructive Evaluation of Grain Structure Using Air-Coupled Ultrasonics

    SciTech Connect

    Belvin, A. D.; Burrell, R. K.; Cole, E.G.

    2009-08-01

    Cast material has a grain structure that is relatively non-uniform. There is a desire to evaluate the grain structure of this material non-destructively. Traditionally, grain size measurement is a destructive process involving the sectioning and metallographic imaging of the material. Generally, this is performed on a representative sample on a periodic basis. Sampling is inefficient and costly. Furthermore, the resulting data may not provide an accurate description of the entire part's average grain size or grain size variation. This project is designed to develop a non-destructive acoustic scanning technique, using Chirp waveforms, to quantify average grain size and grain size variation across the surface of a cast material. A Chirp is a signal in which the frequency increases or decreases over time (frequency modulation). As a Chirp passes through a material, the material's grains reduce the signal (attenuation) by absorbing the signal energy. Geophysics research has shown a direct correlation with Chirp wave attenuation and mean grain size in geological structures. The goal of this project is to demonstrate that Chirp waveform attenuation can be used to measure grain size and grain variation in cast metals (uranium and other materials of interest). An off-axis ultrasonic inspection technique using air-coupled ultrasonics has been developed to determine grain size in cast materials. The technique gives a uniform response across the volume of the component. This technique has been demonstrated to provide generalized trends of grain variation over the samples investigated.

  18. Non-destructive investigation of a time capsule using neutron radiography and X-ray fluorescence

    NASA Astrophysics Data System (ADS)

    MacDonald, B. L.; Vanderstelt, J.; O'Meara, J.; McNeill, F. E.

    2016-01-01

    Non-destructive analytical techniques are becoming increasingly important for the study of objects of cultural heritage interest. This study applied two techniques: X-ray fluorescence and neutron radiography, for the investigation of a capped, tubular metal object recovered from an urban construction site in Gore Park, Hamilton, Canada. The site is an urban park containing a World War I commemorative monument that underwent renovation and relocation. Historical documentation suggested that the object buried underneath the monument was a time capsule containing a paper document listing the names of 1800 Canadians who died during WWI. The purpose of this study was to assess the condition of the object, and to verify if it was what the historical records purported. XRF analysis was used to characterize the elemental composition of the metal artifact, while neutron radiography revealed that its contents were congruent with historical records and remained intact after being interred for 91 years. Results of this study demonstrate the value of non-destructive techniques for the analysis and preservation of cultural heritage.

  19. Early non-destructive biofouling detection and spatial distribution: Application of oxygen sensing optodes.

    PubMed

    Farhat, N M; Staal, M; Siddiqui, A; Borisov, S M; Bucs, Sz S; Vrouwenvelder, J S

    2015-10-15

    Biofouling is a serious problem in reverse osmosis/nanofiltration (RO/NF) applications, reducing membrane performance. Early detection of biofouling plays an essential role in an adequate anti-biofouling strategy. Presently, fouling of membrane filtration systems is mainly determined by measuring changes in pressure drop, which is not exclusively linked to biofouling. Non-destructive imaging of oxygen concentrations (i) is specific for biological activity of biofilms and (ii) may enable earlier detection of biofilm accumulation than pressure drop. The objective of this study was to test whether transparent luminescent planar O2 optodes, in combination with a simple imaging system, can be used for early non-destructive biofouling detection. This biofouling detection is done by mapping the two-dimensional distribution of O2 concentrations and O2 decrease rates inside a membrane fouling simulator (MFS). Results show that at an early stage, biofouling development was detected by the oxygen sensing optodes while no significant increase in pressure drop was yet observed. Additionally, optodes could detect spatial heterogeneities in biofouling distribution at a micro scale. Biofilm development started mainly at the feed spacer crossings. The spatial and quantitative information on biological activity will lead to better understanding of the biofouling processes, contributing to the development of more effective biofouling control strategies. PMID:26117369

  20. A Distributive, Non-Destructive, Real-Time Approach to Snowpack Monitoring

    NASA Technical Reports Server (NTRS)

    Frolik, Jeff; Skalka, Christian

    2012-01-01

    This invention is designed to ascertain the snow water equivalence (SWE) of snowpacks with better spatial and temporal resolutions than present techniques. The approach is ground-based, as opposed to some techniques that are air-based. In addition, the approach is compact, non-destructive, and can be communicated with remotely, and thus can be deployed in areas not possible with current methods. Presently there are two principal ground-based techniques for obtaining SWE measurements. The first is manual snow core measurements of the snowpack. This approach is labor-intensive, destructive, and has poor temporal resolution. The second approach is to deploy a large (e.g., 3x3 m) snowpillow, which requires significant infrastructure, is potentially hazardous [uses a approximately equal to 200-gallon (approximately equal to 760-L) antifreeze-filled bladder], and requires deployment in a large, flat area. High deployment costs necessitate few installations, thus yielding poor spatial resolution of data. Both approaches have limited usefulness in complex and/or avalanche-prone terrains. This approach is compact, non-destructive to the snowpack, provides high temporal resolution data, and due to potential low cost, can be deployed with high spatial resolution. The invention consists of three primary components: a robust wireless network and computing platform designed for harsh climates, new SWE sensing strategies, and algorithms for smart sampling, data logging, and SWE computation.

  1. Non-Destructive Techniques in the Tacis and Phare Nuclear Safety Programmes

    SciTech Connect

    Bieth, Michel

    2002-07-01

    Decisions regarding the verification of design plant lifetime and potential license renewal periods involve a determination of the component and circuit condition. In Service Inspection of key reactor components becomes a crucial consideration for continued safe plant operation. The determination of the equipment properties by Non Destructive Techniques during periodic intervals is an important aspect of the assessment of fitness-for-service and safe operation of nuclear power plants The Tacis and Phare were established since 1991 by the European Union as support mechanisms through which projects could be identified and addressed satisfactorily. In Nuclear Safety, the countries mainly concerned are Russia, Ukraine, Armenia, and Kazakhstan for the Tacis programme, and Bulgaria, Czech Republic, Hungary, Slovak Republic, Lithuania, Romania and Slovenia for the Phare programme. The Tacis and Phare programs concerning the Nuclear Power Plants consist of: - On Site Assistance and Operational Safety, - Design Safety, - Regulatory Authorities, - Waste management, and are focused on reactor safety issues, contributing to the improvement in the safety of East European reactors and providing technology and safety culture transfer. The main parts of these programmes are related to the On-Site Assistance and to the Design Safety of VVER and RBMK Nuclear power plants where Non Destructive Techniques for In Service Inspection of the primary circuit components are addressed. (authors)

  2. NON-DESTRUCTIVE THERMAL BARRIER COATING SPALLATION PREDICTION BY A LOADBASED MICRO-INDENTATION TECHNIQUE

    SciTech Connect

    J. M. Tannenbaum; K. Lee; B. S.-J. Kang; M.A. Alvin

    2010-11-18

    Currently, the durability and life cycle of thermal barrier coatings (TBC) applied to gas turbine blades and combustor components are limiting the maximum temperature and subsequent efficiency at which gas turbine engines operate. The development of new materials, coating technologies and evaluation techniques is required if enhanced efficiency is to be achieved. Of the current ceramic coating materials used in gas turbine engines, yttria stabilized zirconia (YSZ) is most prevalent, its low thermal conductivity, high thermal expansion coefficient and outstanding mechanical strength make it ideal for use in TBC systems. However, residual stresses caused by coefficients of thermal expansion mismatches within the TBC system and unstable thermally grown oxides are considered the primary causes for its premature and erratic spallation failure. Through finite element simulations, it is shown that the residual stresses generated within the thermally grown oxide (TGO), bond coat (BC), YSZ and their interfaces create slight variations in indentation unloading surface stiffness response prior to spallation failure. In this research, seven air plasma sprayed and one electron beam physical vapor deposition yttria partially stabilized zirconia TBCs were subjected to isothermal and cyclic loadings at 1100°C. The associated coating degradation was evaluated using a non-destructive multiple partial unloading micro-indentation procedure. The results show that the proposed non-destructive micro-indentation evaluation technique can be an effective and specimenindependent TBC failure prediction tool capable of determining the location of initial spallation failure prior to its actual occurrence.

  3. Non-destructive high-throughput DNA extraction and genotyping methods for cotton seeds and seedlings.

    PubMed

    Zheng, Xiuting; Hoegenauer, Kevin A; Maeda, Andrea B V; Wang, Fei; Stelly, David M; Nichols, Robert L; Jones, Don C

    2015-05-01

    Extensive use of targeted PCR-based genotyping is precluded for many plant research laboratories by the cost and time required for DNA extraction. Using cotton (Gossypium hirsutum) as a model for plants with medium-sized seeds, we report here manual procedures for inexpensive non-destructive high-throughput extraction of DNA suitable for PCR-based genotyping of large numbers of individual seeds and seedlings. By sampling only small amounts of cotyledon tissue of ungerminated seed or young seedlings, damage is minimized, and viability is not discernibly affected. The yield of DNA from each seed or seedling is typically sufficient for 1000 or 500 PCR reactions, respectively. For seeds, the tissue sampling procedure relies on a modified 96-well plate that is used subsequently for seed storage. For seeds and seedlings, the DNA is extracted in a strongly basic DNA buffer that is later neutralized and diluted. Extracts can be used directly for high-throughput PCR-based genotyping. Any laboratory can thus extract DNA from thousands of individual seeds/seedlings per person-day at a very modest cost for consumables (~$0.05 per sample). Being non-destructive, our approach enables a wide variety of time- and resource-saving applications, such as marker-assisted selection (MAS), before planting, transplanting, and flowering. PMID:25967902

  4. Non-destructive inspection in industrial equipment using robotic mobile manipulation

    NASA Astrophysics Data System (ADS)

    Maurtua, Iñaki; Susperregi, Loreto; Ansuategui, Ander; Fernández, Ane; Ibarguren, Aitor; Molina, Jorge; Tubio, Carlos; Villasante, Cristobal; Felsch, Torsten; Pérez, Carmen; Rodriguez, Jorge R.; Ghrissi, Meftah

    2016-05-01

    MAINBOT project has developed service robots based applications to autonomously execute inspection tasks in extensive industrial plants in equipment that is arranged horizontally (using ground robots) or vertically (climbing robots). The industrial objective has been to provide a means to help measuring several physical parameters in multiple points by autonomous robots, able to navigate and climb structures, handling non-destructive testing sensors. MAINBOT has validated the solutions in two solar thermal plants (cylindrical-parabolic collectors and central tower), that are very demanding from mobile manipulation point of view mainly due to the extension (e.g. a thermal solar plant of 50Mw, with 400 hectares, 400.000 mirrors, 180 km of absorber tubes, 140m height tower), the variability of conditions (outdoor, day-night), safety requirements, etc. Once the technology was validated in simulation, the system was deployed in real setups and different validation tests carried out. In this paper two of the achievements related with the ground mobile inspection system are presented: (1) Autonomous navigation localization and planning algorithms to manage navigation in huge extensions and (2) Non-Destructive Inspection operations: thermography based detection algorithms to provide automatic inspection abilities to the robots.

  5. Non-destructive detection of pesticide residues in cucumber using visible/near-infrared spectroscopy.

    PubMed

    Jamshidi, Bahareh; Mohajerani, Ezeddin; Jamshidi, Jamshid; Minaei, Saeid; Sharifi, Ahmad

    2015-01-01

    The feasibility of using visible/near-infrared (Vis/NIR) spectroscopy was assessed for non-destructive detection of diazinon residues in intact cucumbers. Vis/NIR spectra of diazinon solution and cucumber samples without and with different concentrations of diazinon residue were analysed at the range of 450-1000 nm. Partial least squares-discriminant analysis (PLS-DA) models were developed based on different spectral pre-processing techniques to classify cucumbers with contents of diazinon below and above the MRL as safe and unsafe samples, respectively. The best model was obtained using a first-derivative method with the lowest standard error of cross-validation (SECV = 0.366). Moreover, total percentages of correctly classified samples in calibration and prediction sets were 97.5% and 92.31%, respectively. It was concluded that Vis/NIR spectroscopy could be an appropriate, fast and non-destructive technology for safety control of intact cucumbers by the absence/presence of diazinon residues. PMID:25789964

  6. Rapid non-destructive assessment of pork edible quality by using VIS/NIR spectroscopic technique

    NASA Astrophysics Data System (ADS)

    Zhang, Leilei; Peng, Yankun; Dhakal, Sagar; Song, Yulin; Zhao, Juan; Zhao, Songwei

    2013-05-01

    The objectives of this research were to develop a rapid non-destructive method to evaluate the edible quality of chilled pork. A total of 42 samples were packed in seal plastic bags and stored at 4°C for 1 to 21 days. Reflectance spectra were collected from visible/near-infrared spectroscopy system in the range of 400nm to 1100nm. Microbiological, physicochemical and organoleptic characteristics such as the total viable counts (TVC), total volatile basic-nitrogen (TVB-N), pH value and color parameters L* were determined to appraise pork edible quality. Savitzky-Golay (SG) based on five and eleven smoothing points, Multiple Scattering Correlation (MSC) and first derivative pre-processing methods were employed to eliminate the spectra noise. The support vector machines (SVM) and partial least square regression (PLSR) were applied to establish prediction models using the de-noised spectra. A linear correlation was developed between the VIS/NIR spectroscopy and parameters such as TVC, TVB-N, pH and color parameter L* indexes, which could gain prediction results with Rv of 0.931, 0.844, 0.805 and 0.852, respectively. The results demonstrated that VIS/NIR spectroscopy technique combined with SVM possesses a powerful assessment capability. It can provide a potential tool for detecting pork edible quality rapidly and non-destructively.

  7. Non-Destructive Evaluation of Thermal Spray Coating Interface Quality by Eddy Current Method

    SciTech Connect

    B.Mi; X. Zhao; R. Bayles

    2006-05-26

    Thermal spray coating is usually applied through directing molten or softened particles at very high velocities onto a substrate. An eddy current non-destructive inspection technique is presented here for thermal spray coating interface quality characterization. Several high-velocity-oxy-fuel (HVOF) coated steel plates were produced with different surface preparation conditions before applying the coating, e.g., grit-blasted surface, wire-brush cleaned surface, and a dirty surface. A quad-frequency eddy current probe was used to manually scan over the coating surface to evaluate the bonding quality. Experimental results show that the three surface preparation conditions can be successfully differentiated by looking into the impedance difference observed from the eddy current probe. The measurement is fairly robust and consistent. More specimens are also prepared with variations of process parameters, such as spray angle, stand-off distance, and application of corrosion protective sealant, etc. They are blindly tested to evaluate the reliability of the eddy current system. Quantitative relations between the coating bond strength and the eddy current response are also established with the support of destructive testing. This non-contact, non-destructive, easy to use technique has the potential for evaluating the coating quality immediately after its application so that any defects can be corrected immediately.

  8. Non-destructive on-line monitoring of MIC (microbially influenced corrosion)

    SciTech Connect

    White, D.C. Tennessee Univ., Knoxville, TN ); Nivens, D.E.; Mittelman, M.W. . Inst. for Applied Microbiology); Chambers, J.Q. . Dept. of Chemistry); King, J.M.H. . Center for Environmental Biotechnology); Sayler, G.S. (Tennessee Univ., Knoxville, TN

    1990-01-01

    The formation of microbial biofilms on metal surfaces with the subsequent increase in heat transfer resistance and the induction of microbially influenced corrosion (MIC) is being increasingly recognized as an extremely important economic and safety problem for industrial water systems. The development of sufficiently rugged and accurate monitoring devices by which biofilm formation and activity of microbial biofilms can be monitored non-destructively, directly in water systems is the goal of this research. This on-line systems would allow the effective utilization of minimal levels of biocides and inhibitors as well as permit in situ testing of materials for MIC resistance. Several non-destructive technologies such as the quartz crystal microbalance (QCM), the attenuated total reflectance-Fourier transforming infrared spectrometer (ATR-FT/IR), and a genetically engineered bacterium containing the lux gene cassette in which its bioluminescence can be used to define its presence on coupons are on-line devices which accurately measure biofilm formation. Corrosion activity can be estimated by electrochemical impedance. 12 refs., 8 figs.

  9. Non-destructive forensic latent fingerprint acquisition with chromatic white light sensors

    NASA Astrophysics Data System (ADS)

    Leich, Marcus; Kiltz, Stefan; Dittmann, Jana; Vielhauer, Claus

    2011-02-01

    Non-destructive latent fingerprint acquisition is an emerging field of research, which, unlike traditional methods, makes latent fingerprints available for additional verification or further analysis like tests for substance abuse or age estimation. In this paper a series of tests is performed to investigate the overall suitability of a high resolution off-the-shelf chromatic white light sensor for the contact-less and non-destructive latent fingerprint acquisition. Our paper focuses on scanning previously determined regions with exemplary acquisition parameter settings. 3D height field and reflection data of five different latent fingerprints on six different types of surfaces (HDD platter, brushed metal, painted car body (metallic and non-metallic finish), blued metal, veneered plywood) are experimentally studied. Pre-processing is performed by removing low-frequency gradients. The quality of the results is assessed subjectively; no automated feature extraction is performed. Additionally, the degradation of the fingerprint during the acquisition period is observed. While the quality of the acquired data is highly dependent on surface structure, the sensor is capable of detecting the fingerprint on all sample surfaces. On blued metal the residual material is detected; however, the ridge line structure dissolves within minutes after fingerprint placement.

  10. Processes for non-destructive transfer of graphene: widening the bottleneck for industrial scale production

    NASA Astrophysics Data System (ADS)

    Zaretski, Aliaksandr V.; Lipomi, Darren J.

    2015-05-01

    The exceptional charge-transport, mechanical, and barrier properties of graphene are well known. High-quality films of single-layer graphene produced over large areas, however, are extremely expensive. The high cost of graphene precludes its use in industries--such as transparent electrodes and flexible packaging--that might take full advantage of its properties. This minireview presents several strategies for the transfer of graphene from the substrates used for growth to substrates used for the final application. Each strategy shares the characteristic of being non-destructive: that is, the growth substrate remains reusable for further synthesis of new graphene. These processes have the potential to lower significantly the costs of manufacturing graphene, to increase production yields, and to minimize environmental impact. This article is divided into sections on (i) the synthesis of high-quality single-layer graphene and (ii) its non-destructive transfer to a host substrate. Section (ii) is further divided according to the substrate from which graphene is transferred: single-crystalline wafers or flexible copper foils. We also comment, wherever possible, on defects produced as a result of the transfer, and potential strategies to mitigate these defects. We conclude that several methods for the green synthesis and transfer of graphene have several of the right characteristics to be useful in industrial scale production.

  11. Processes for non-destructive transfer of graphene: widening the bottleneck for industrial scale production.

    PubMed

    Zaretski, Aliaksandr V; Lipomi, Darren J

    2015-06-14

    The exceptional charge-transport, mechanical, and barrier properties of graphene are well known. High-quality films of single-layer graphene produced over large areas, however, are extremely expensive. The high cost of graphene precludes its use in industries-such as transparent electrodes and flexible packaging-that might take full advantage of its properties. This minireview presents several strategies for the transfer of graphene from the substrates used for growth to substrates used for the final application. Each strategy shares the characteristic of being non-destructive: that is, the growth substrate remains reusable for further synthesis of new graphene. These processes have the potential to lower significantly the costs of manufacturing graphene, to increase production yields, and to minimize environmental impact. This article is divided into sections on (i) the synthesis of high-quality single-layer graphene and (ii) its non-destructive transfer to a host substrate. Section (ii) is further divided according to the substrate from which graphene is transferred: single-crystalline wafers or flexible copper foils. We also comment, wherever possible, on defects produced as a result of the transfer, and potential strategies to mitigate these defects. We conclude that several methods for the green synthesis and transfer of graphene have several of the right characteristics to be useful in industrial scale production. PMID:25924926

  12. Non-destructive sampling of rock-dwelling microbial communities using sterile adhesive tape.

    PubMed

    Cutler, Nick A; Oliver, Anna E; Viles, Heather A; Whiteley, Andrew S

    2012-12-01

    Building stone provides a habitat for an array of microorganisms, many of which have been demonstrated to have a deleterious effect on the appearance and/or structural integrity of stone masonry. It is essential to understand the composition and structure of stone-dwelling (lithobiontic) microbial communities if successful stone conservation strategies are to be applied, particularly in the face of global environmental change. Ideally, the techniques used to sample such assemblages should be non-destructive due to the sensitive conservation status of many stone buildings. This paper quantitatively assesses the performance of sterile adhesive tape as a non-destructive sampling technique and compares the results of tape sampling with an alternative, destructive, sampling method. We used DNA fingerprinting (TRFLP) to characterise the algal, fungal and bacterial communities living on a stone slab. Our results demonstrate that tape sampling may be used to collect viable quantities of microbial DNA from environmental samples. This technique is ideally suited to the sampling of microbial biofilms, particularly when these communities are dominated by green algae. It provides a good approximation of total community diversity (i.e. the aggregate diversity of epilithic and endolithic communities). Tape sampling is straightforward, rapid and cost effective. When combined with molecular analytical techniques, this sampling method has the potential to make a major contribution to efforts to understand the structure of lithobiontic microbial communities and our ability to predict the response of such communities to future environmental change. PMID:23022426

  13. Assesment of uniaxial compressive strenght of repair mortars by using in situ non destructive techniques

    NASA Astrophysics Data System (ADS)

    Szemerey-Kiss, Balázs; Török, Ákos

    2014-05-01

    The present paper provides information on the strength assessment of restoration mortars by using ultrasonic pulse velocity. The aims of the tests were to determine the compressive strength of the mortars by using non destructive test methods. Four commercially available types of restoration mortars were tested. Besides the pure mortars, specimens with 30 and 50 wt% of limestone sand aggregate (from Sóskút quarry) were also made. The material properties of the tested mortars have been described in details previously (Szemerey-Kiss et al. 2013). Cubic test specimens of 3cm x 3cm x 3cm were prepared from the mortars and after casting and consolidation 10 cubes of each mortar type were tested. Ultrasonic pulse velocity was measured according to the guidelines given by EN 14579:2005. Uniaxial compressive strength of test specimens were measured following the instructions of EN 1015-11:2000. An exponential mathematical formula was outlined that describes the uniaxial compressive strength of mortars based on ultrasonic pulse velocity data. The best fit was found for two mortars while the formula with different constants could be also used for other mortars, too. These experiments have proved that non destructive tests can be used in the assessment of the strength of historic mortars. References: Szemerey-Kiss, B., Török, Á., Siegesmund S 2013. The influence of binder/aggregate ratio on the properties and strength of repair mortars. Environmental Earth Sciences, 69:1439-1449.

  14. Neural network and principal component regression in non-destructive soluble solids content assessment: a comparison*

    PubMed Central

    Chia, Kim-seng; Abdul Rahim, Herlina; Abdul Rahim, Ruzairi

    2012-01-01

    Visible and near infrared spectroscopy is a non-destructive, green, and rapid technology that can be utilized to estimate the components of interest without conditioning it, as compared with classical analytical methods. The objective of this paper is to compare the performance of artificial neural network (ANN) (a nonlinear model) and principal component regression (PCR) (a linear model) based on visible and shortwave near infrared (VIS-SWNIR) (400–1000 nm) spectra in the non-destructive soluble solids content measurement of an apple. First, we used multiplicative scattering correction to pre-process the spectral data. Second, PCR was applied to estimate the optimal number of input variables. Third, the input variables with an optimal amount were used as the inputs of both multiple linear regression and ANN models. The initial weights and the number of hidden neurons were adjusted to optimize the performance of ANN. Findings suggest that the predictive performance of ANN with two hidden neurons outperforms that of PCR. PMID:22302428

  15. Optimization of ISOCS Parameters for Quantitative Non-Destructive Analysis of Uranium in Bulk Form

    NASA Astrophysics Data System (ADS)

    Kutniy, D.; Vanzha, S.; Mikhaylov, V.; Belkin, F.

    2011-12-01

    Quantitative calculation of the isotopic masses of fissionable U and Pu is important for forensic analysis of nuclear materials. γ-spectrometry is the most commonly applied tool for qualitative detection and analysis of key radionuclides in nuclear materials. Relative isotopic measurement of U and Pu may be obtained from γ-spectra through application of special software such as MGAU (Multi-Group Analysis for Uranium, LLNL) or FRAM (Fixed-Energy Response Function Analysis with Multiple Efficiency, LANL). If the concentration of U/Pu in the matrix is unknown, however, isotopic masses cannot be calculated. At present, active neutron interrogation is the only practical alternative for non-destructive quantification of fissionable isotopes of U and Pu. An active well coincidence counter (AWCC), an alternative for analyses of uranium materials, has the following disadvantages: 1) The detection of small quantities (≤100 g) of 235U is not possible in many models; 2) Representative standards that capture the geometry, density and chemical composition of the analyzed unknown are required for precise analysis; and 3) Specimen size is severely restricted by the size of the measuring chamber. These problems may be addressed using modified γ-spectrometry techniques based on a coaxial HPGe-detector and ISOCS software (In Situ Object Counting System software, Canberra). We present data testing a new gamma-spectrometry method uniting actinide detection with commonly utilized software, modified for application in determining the masses of the fissionable isotopes in unknown samples of nuclear materials. The ISOCS software, widely used in radiation monitoring, calculates the detector efficiency curve in a specified geometry and range of photon energies. In describing the geometry of the source-detector, it is necessary to clearly describe the distance between the source and the detector, the material and the thickness of the walls of the container, as well as material, density

  16. Shearography for Non-destructive Inspection with applications to BAT Mask Tile Adhesive Bonding and Specular Surface Honeycomb Panels

    NASA Technical Reports Server (NTRS)

    Lysak, Daniel B.

    2003-01-01

    The applicability of shearography techniques for non-destructive evaluation in two unique application areas is examined. In the first application, shearography is used to evaluate the quality of adhesive bonds holding lead tiles to the B.4T gamma ray mask for the NASA Swift program. Using a vibration excitation, the more poorly bonded tiles are readily identifiable in the shearography image. A quantitative analysis is presented that compares the shearography results with a destructive pull test measuring the force at bond failure. The second application is to evaluate the bonding between the skin and core of a honeycomb structure with a specular (mirror-like) surface. In standard shearography techniques, the object under test must have a diffuse surface to generate the speckle patterns in laser light, which are then sheared. A novel configuration using the specular surface as a mirror to image speckles from a diffuser is presented, opening up the use of shearography to a new class of objects that could not have been examined with the traditional approach. This new technique readily identifies large scale bond failures in the panel, demonstrating the validity of this approach.

  17. Photonic non-destructive measurement methods for investigating the evolution of polar firn and ice

    NASA Astrophysics Data System (ADS)

    Breton, Daniel James

    When snow falls on glaciers or ice sheets, it persists for many tens, hundreds and sometimes thousands of years before becoming ice. The granular material in between fresh snow and glacial ice is known as firn and is generally 50 to 100 m thick over polar ice sheets. The compaction mechanism of firn into ice (called densification) has important glaciological ramifications in determination of ice sheet stability and related sea level rise effects via remote sensing altimetry. Firn densification is also important for correctly interpreting ice core paleoclimate records, especially those analyzing gases trapped in air bubbles within the glacial ice. Densification is thought to depend strongly on microstructure: the sizes, shapes, orientations and inter-particle bonds of the ice grains that make up polar firn. Microstructure-dependent densification is poorly understood and occurs in the region where two-thirds of the overall densification takes place. This work focuses on developing non-destructive methods for simultaneously evaluating changes in both the bulk density and microstructure of polar firn to better understand structure- dependent densification processes. The first method is an automated density gauge which uses gamma-ray transmission methods to non-destructively produce high resolution (3.3 mm) and high precision (+/-4 kg m-3) density profiles of firn and ice cores. This instrument was used to collect a density profile for the first 160 m of the West Antarctic Ice Sheet Divide WDCO6A deep ice core. The second method involves optical scattering measurements on firn and ice cores to determine the important microstructural parameters of ice grain and air bubble size and air-ice interface surface area. These measurements are modeled using both Monte Carlo radiative transfer and ray-tracing geometric optics methods, and are then tested against experiment using digital photography of the WDC06A core. Combining the results of both bulk density and optical

  18. Non-destructive infrared analyses: a method for provenance analyses of sandstones

    NASA Astrophysics Data System (ADS)

    Bowitz, Jörg; Ehling, Angela

    2008-12-01

    Infrared spectroscopy (IR spectroscopy) is commonly applied in the laboratory for mineral analyses in addition to XRD. Because such technical efforts are time and cost consuming, we present an infrared-based mobile method for non-destructive mineral and provenance analyses of sandstones. IR spectroscopy is based on activating chemical bonds. By irradiating a mineral mixture, special bonds are activated to vibrate depending on the bond energy (resonance vibration). Accordingly, the energy of the IR spectrum will be reduced thereby generating an absorption spectrum. The positions of the absorption maxima within the spectral region indicate the type of the bonds and in many cases identify minerals containing these bonds. The non-destructive reflection spectroscopy operates in the near infrared region (NIR) and can detect all common clay minerals as well as sulfates, hydroxides and carbonates. The spectra produced have been interpreted by computer using digital mineral libraries that have been especially collected for sandstones. The comparison of all results with XRD, RFA and interpretations of thin sections demonstrates impressively the accuracy and reliability of this method. Not only are different minerals detectable, but also differently ordered kaolinites and varieties of illites can be identified by the shape and size of the absorption bands. Especially clay minerals and their varieties in combination with their relative contents form the characteristic spectra of sandstones. Other components such as limonite, hematite and amorphous silica also influence the spectra. Sandstones, similar in colour and texture, often can be identified by their characteristic reflectance spectra. Reference libraries with more than 60 spectra of important German sandstones have been created to enable entirely computerized interpretations and identifications of these dimension stones. The analysis of infrared spectroscopy results is demonstrated with examples of different sandstones

  19. Non-destructive monitoring of creaming of oil-in-water emulsion-based formulations using magnetic resonance imaging.

    PubMed

    Onuki, Yoshinori; Horita, Akihiro; Kuribayashi, Hideto; Okuno, Yoshihide; Obata, Yasuko; Takayama, Kozo

    2014-07-01

    A non-destructive method for monitoring creaming of emulsion-based formulations is in great demand because it allows us to understand fully their instability mechanisms. This study was aimed at demonstrating the usefulness of magnetic resonance (MR) techniques, including MR imaging (MRI) and MR spectroscopy (MRS), for evaluating the physicochemical stability of emulsion-based formulations. Emulsions that are applicable as the base of practical skin creams were used as test samples. Substantial creaming was developed by centrifugation, which was then monitored by MRI. The creaming oil droplet layer and aqueous phase were clearly distinguished by quantitative MRI by measuring T1 and the apparent diffusion coefficient. Components in a selected volume in the emulsions could be analyzed using MRS. Then, model emulsions having different hydrophilic-lipophilic balance (HLB) values were tested, and the optimal HLB value for a stable dispersion was determined. In addition, the MRI examination enables the detection of creaming occurring in a polyethylene tube, which is commonly used for commercial products, without losing any image quality. These findings strongly indicate that MR techniques are powerful tools to evaluate the physicochemical stability of emulsion-based formulations. This study will make a great contribution to the development and quality control of emulsion-based formulations. PMID:23631538

  20. Characterization and source term assessments of radioactive particles from Marshall Islands using non-destructive analytical techniques

    NASA Astrophysics Data System (ADS)

    Jernström, J.; Eriksson, M.; Simon, R.; Tamborini, G.; Bildstein, O.; Marquez, R. Carlos; Kehl, S. R.; Hamilton, T. F.; Ranebo, Y.; Betti, M.

    2006-08-01

    Six plutonium-containing particles stemming from Runit Island soil (Marshall Islands) were characterized by non-destructive analytical and microanalytical methods. Composition and elemental distribution in the particles were studied with synchrotron radiation based micro X-ray fluorescence spectrometry. Scanning electron microscope equipped with energy dispersive X-ray detector and with wavelength dispersive system as well as a secondary ion mass spectrometer were used to examine particle surfaces. Based on the elemental composition the particles were divided into two groups: particles with pure Pu matrix, and particles where the plutonium is included in Si/O-rich matrix being more heterogenously distributed. All of the particles were identified as nuclear fuel fragments of exploded weapon components. As containing plutonium with low 240Pu/ 239Pu atomic ratio, less than 0.065, which corresponds to weapons-grade plutonium or a detonation with low fission yield, the particles were identified to originate from the safety test and low-yield tests conducted in the history of Runit Island. The Si/O-rich particles contained traces of 137Cs ( 239 + 240 Pu/ 137Cs activity ratio higher than 2500), which indicated that a minor fission process occurred during the explosion. The average 241Am/ 239Pu atomic ratio in the six particles was 3.7 × 10 - 3 ± 0.2 × 10 - 3 (February 2006), which indicated that plutonium in the different particles had similar age.

  1. Laser photothermal non-destructive metrology of cracks in un-sintered powder metallurgy manufactured automotive transmission sprockets

    NASA Astrophysics Data System (ADS)

    Tolev, J.; Mandelis, A.

    2010-03-01

    A non-contact and non-intrusive method of revealing crack presence in un-sintered (green) automotive transmission parts (sprockets), manufactured by means of a powder metallurgy technology based on analysis of photo-thermal radiometric (PTR) signals and their statistical analysis was developed. The inspection methodology relies on the interaction of a modulated laser generated thermal wave with the potential crack and the resulting change in amplitude and phase of the detected signal [1-5]. The crack existence at points in high stress regions of a group of green (unsintered) sprockets was evaluated through frequency scans. The results were validated by independent destructive cross-sectioning of the sprockets following sintering and polishing. Examination of the sectioned sprockets under a microscope at the locations where signal changes was used for correlation with the PTR signals. Statistical analysis confirmed the capabilities of the method to detect the presence of hairline cracks (~5 - 10 μm size) with excellent sensitivity (91%) and good accuracy (78%) and specificity (61%). This measurement technique and the associated statistical analysis can be used as a simple and reliable on-line inspection methodology of industrial powder metallurgy manufactured steel products for non-destructive quality and feedback control of the parts forming process.

  2. Monitoring of near surface CO2

    NASA Astrophysics Data System (ADS)

    Faber, E.; Möller, I.; Teschner, M.; Poggenburg, J.; Spickenbom, K.; Schulz, H. J.

    2009-04-01

    Monitoring of near surface CO2 ECKHARD FABER1, INGO MÖLLER1, MANFRED TESCHNER1, JÜRGEN POGGENBURG1, KAI SPICKENBOM1, HANS-MARTIN SCHULZ1,2 1Bundesanstalt für Geowissenschaften und Rohstoffe (BGR), Stilleweg 2, D-30655 Hannover, e.faber@bgr.de 2present adress: GeoForschungsZentrum Potsdam (GFZ), Telegrafenberg, D-14473 Potsdam Underground gas storage and sequestration of carbon dioxide is one of the methods to reduce the input of antropogenic CO2 into the atmosphere and its greenhouse effect. Storage of CO2 is planned in depleted reservoirs, in aquifers and in salt caverns. Storage sites must have very small leakage rates to safely store the CO2 for centuries. Thus, a careful investigation and site selection is crucial. However, any leakage of CO2 to the surface is potentially dangerous for humans and environment. Therefore, instruments and systems for the detection of any CO2 escaping the storage sites and reaching the atmosphere have to be developed. Systems to monitor gases in deep wells, groundwater and surface sediments for leaking CO2 are developed, tested and are contnuously improved. Our group is mainly analysing CO2 in shallow (down to 3 m) soil samples using automatically operating monitoring systems. The systems are equipped with sensors to measure CO2 (and other gases) concentrations and other environmental parameters (atmospheric pressure, ambient and soil temperatures, etc.). Data are measured in short intervals (minute to subminute), are stored locally and are transferred by telemetrical systems into the BGR laboratory (Weinlich et al., 2006). In addition to soil gases monitoring systems technical equipment is available for continuous underwater gas flow measurements. Several of those monitoring systems are installed in different areas like Czech Republic, Austria, Italy and Germany. To detect any leaking gas from a sequestration site after CO2 injection, the naturally existing CO2 concentration (before injection) must be known. Thus, the natural

  3. Template synthesis of test tube nanoparticles using non-destructive replication

    PubMed Central

    Wagner, Jonathan; Yao, Jingyuan; Rodgers, David; Hinds, Bruce

    2013-01-01

    Nano test tubes are a promising delivery vehicle for a range of therapeutics including small molecule drugs and biologics. However, current template synthesis methods of producing nano test tubes are prohibitively expensive and time consuming. Here, non-destructive template replication was used to increase nano test tube yield from porous alumina by more than a hundredfold. We demonstrate how to produce nano test tubes of several sizes and compositions including hybrid tubes with different inner and outer surfaces for targeted surface chemistry. Nano test tubes were readily suspended and stored in aqueous solutions without the need for chemical treatment. These nano test tubes should find application as delivery vehicles for therapeutics, particularly for processive “bionanoreactors” loaded with enzymes. PMID:23376956

  4. Prediction of Service Life of Cordierite-Mullite Refractory Materials by Non-Destructive Methods

    SciTech Connect

    Boccaccini, D. N.; Kamseu, Elie; Cannio, M.; Romagnoli, M.; Veronesi, P.; Leonelli, C.; Volkov-Husoviae, T. D.; Dlouhy, I.; Boccaccini, A. R.

    2008-02-15

    Ultrasonic pulse velocity testing was used to perform non-destructive quality control of refractory plates used as substrates in fast firing of porcelain whitewares. The measurement of the ultrasonic velocity was used to asses the presence of internal voids or cracks originated from the manufacturing procedure. Image analysis was used to predict thermal stability of the refractory materials. Two cordierite-mullite compositions were investigated that are characterized by different microstructure morphologies and crack propagation behaviour. A brief discussion about the correlation between microstructure, crack propagation behaviour and thermal shock resistance is presented. Moreover, empirical models were developed to predict the service life of refractory plates from measured values of ultrasonic velocities in plates in the as-received state.

  5. Portable generator-based XRF instrument for non-destructive analysis at crime scenes

    NASA Astrophysics Data System (ADS)

    Schweitzer, Jeffrey S.; Trombka, Jacob I.; Floyd, Samuel; Selavka, Carl; Zeosky, Gerald; Gahn, Norman; McClanahan, Timothy; Burbine, Thomas

    2005-12-01

    Unattended and remote detection systems find applications in space exploration, telemedicine, teleforensics, homeland security and nuclear non-proliferation programs. The National Institute of Justice (NIJ) and the National Aeronautics and Space Administration's (NASA) Goddard Space Flight Center (GSFC) have teamed up to explore the use of NASA developed technologies to help criminal justice agencies and professionals investigate crimes. The objective of the program is to produce instruments and communication networks that have application within both NASA's space program and NIJ, together with state and local forensic laboratories. A general-purpose X-ray fluorescence system has been built for non-destructive analyses of trace and invisible material at crime scenes. This portable instrument is based on a generator that can operate to 60 kV and a Schottky CdTe detector. The instrument has been shown to be successful for the analysis of gunshot residue and a number of bodily fluids at crime scenes.

  6. Three-dimensional non-destructive testing (NDT) in the infrared spectrum

    NASA Astrophysics Data System (ADS)

    Akhloufi, Moulay A.; Guyon, Yannis; Bendada, Abdelhakim; Castenado, Clemente-Ibarra

    2015-05-01

    Three-dimensional (3D) vision scanning for metrology and inspection applications is an area that knows an increasing interest in the industry. This interest is driven by the recent advances in 3D technologies, permitting to attain high precision measurements at an affordable cost. 3D vision allows for the modelling and inspection of the visible surface of objects. When it is necessary to detect subsurface defects, active infrared (IR) thermography is one of the most used tools today for non-destructive testing (NDT) of materials. Fusion of these two modalities allows the simultaneous detection of surface and subsurface defects and to visualize these defects overlaid on a 3D model of the scanned and modelled parts or their 3D computer-aided design (CAD) models. In this work, we present a framework for automatically fusing 3D data (scanned or CAD) with the infrared thermal images for an NDT process in 3D space.

  7. A modified positron lifetime spectrometer as method of non-destructive testing in materials

    NASA Astrophysics Data System (ADS)

    Chen, Z. Q.; Shi, J. J.; Jiang, J.; Liu, X. B.; Wang, R. S.; Wu, Y. C.

    2015-02-01

    This paper aims to develop a new non-destructive testing (NDT) method using positron annihilation spectroscopy, a powerful tool to detect vacancy-type defects and defect's chemical environment. A positron NDT system was designed and constructed by modifying the "sandwich" structure of sample-source-sample in the conventional positron lifetime spectrometer. The positron lifetime spectra of one single sample can be measured and analyzed by subtracting the contribution of a reference sample. The feasibility and reliability of the positron NDT system have been tested by analyzing nondestructively deformation damage caused by mechanical treatment in metals and steels. This system can be used for detecting defects and damage in thick or large-size samples without cutting off the sample materials, as well as for detecting two-dimensional distribution of defects.

  8. Non-Destructive Evaluation of Depth of Surface Cracks Using Ultrasonic Frequency Analysis

    PubMed Central

    Her, Shiuh-Chuan; Lin, Sheng-Tung

    2014-01-01

    Ultrasonic is one of the most common uses of a non-destructive evaluation method for crack detection and characterization. The effectiveness of the acoustic-ultrasound Structural Health Monitoring (SHM) technique for the determination of the depth of the surface crack was presented. A method for ultrasonic sizing of surface cracks combined with the time domain and frequency spectrum was adopted. The ultrasonic frequency spectrum was obtained by Fourier transform technique. A series of test specimens with various depths of surface crack ranging from 1 mm to 8 mm was fabricated. The depth of the surface crack was evaluated using the pulse-echo technique. In this work, three different longitudinal waves with frequencies of 2.25 MHz, 5 MHz and 10 MHz were employed to investigate the effect of frequency on the sizing detection of surface cracks. Reasonable accuracies were achieved with measurement errors less than 7%. PMID:25225875

  9. System and method for non-destructive evaluation of surface characteristics of a magnetic material

    DOEpatents

    Jiles, David C.; Sipahi, Levent B.

    1994-05-17

    A system and a related method for non-destructive evaluation of the surface characteristics of a magnetic material. The sample is excited by an alternating magnetic field. The field frequency, amplitude and offset are controlled according to a predetermined protocol. The Barkhausen response of the sample is detected for the various fields and offsets and is analyzed. The system produces information relating to the frequency content, the amplitude content, the average or RMS energy content, as well as count rate information, for each of the Barkhausen responses at each of the excitation levels applied during the protocol. That information provides a contiguous body of data, heretofore unavailable, which can be analyzed to deduce information about the surface characteristics of the material at various depths below the surface.

  10. Interferometric system for non-destructive testing based on large diameter bacteriorhodopsin films

    NASA Astrophysics Data System (ADS)

    Juchem, Thorsten; Hampp, Norbert

    2000-08-01

    A system for holographic interferometry using bacteriorhodopsin films as an erasable optical recording medium is presented. Bacteriorhodopsin is a photochromic protein found in archaebacteria. Bacteriorhodopsin films with an aperture of 90×90 mm are used for high-resolution lensless recording (5000 lines/mm). The holograms are recorded in reflection-type geometry in order to achieve a compact design. A frequency-doubled Nd : YVO 4 laser, emitting at 532 nm, is used for recording and incoherent blue light is employed for photochemical erasure. The system is suitable for a variety of different interferometric techniques like double-exposure, time-averaging and real-time interferometry. As an example for the application of the BR-based non-destructive testing system the inspection of ceramic motor valves, made from silicone nitride (Si 3N 4), under mechanical load is reported.

  11. Non-destructive testing of an original XVI century painting on wood by ESPI system

    NASA Astrophysics Data System (ADS)

    Arena, G.; Paturzo, M.; Fatigati, G.; Grilli, M.; Pezzati, L.; Ferraro, P.

    2015-03-01

    Electronic Speckle Pattern Interferometry (ESPI), a non-contact and non-destructive optical techniques, was employed for assessing the conservation state of a XVI Century painting on wood (72x88x1,9 cm). By a long term analysis, the whole structure alterations, induced by the room temperature and relative humidity variations, were evaluated. Measurement of the whole painting structural bends was achieved. Local flaws and hidden detachments of pictorial layers from the support, which cannot be recognized by traditional art-restorer methods, were also revealed. This work was prevalently aimed at achieving a simple approach, in the laboratory practice, to get an intuitively user-friendly method for art conservators, not accustomed to high-tech or math based methods. The results demonstrate that ESPI can largely improve the traditional art conservation survey techniques.

  12. Could non-destructive methodologies enhance the microbiologically influenced corrosion (MIC) in pipeline systems?

    NASA Astrophysics Data System (ADS)

    Al-Abbas, F.; Kakpovbia, A.; Mishra, B.; Olson, D.; Spear, J.

    2013-01-01

    Stringent corrosion management programs are being deployed by oil and gas industry to ensure the integrity of pipeline systems. Parts of this program are the corrosion protection systems and inspection detection methods included non-destructive techniques. Those measures induce remnant magnetic field (RMF) in the pipeline steel. Potentially the RMF could affect the corrosion process in the pipeline including microbiologically influenced corrosion (MIC). Microorganisms in pipelines have surface charges and produce a wide variety of metabolic products. Consequently, when they are exposed to RMF generated at the linepipe steel surface by the aforementioned sources there will be potential effects. This sequentially will increase the likelihood of biofilm formation and hence enhance/promote MIC. This study investigates the potential effects of RFM on the MIC by sulfate reducing bacteria (SRB).

  13. Design of ERL Spoke Cavity For Non-Destructive Assay Research

    NASA Astrophysics Data System (ADS)

    Sawamura, M.; Nagai, R.; Nishimori, N.; Hajima, R.

    2015-10-01

    We are proposing non-destructive assay system of nuclear materials with laser Compton scattering combined with an energy-recovery linac (ERL) and a laser. Since constructing accelerator system for nuclear safe guard and security requires small cavities, spoke cavities have many advantages such as shortening the distance between cavities, small frequency detune due to micro-phonics and easy adjustment of field distribution for strong cell coupling. Calculations of optimized cavity shape and HOM coupler shape have been performed and rf properties with aluminum spoke cavity model have been also measured. Considering refrigerator system required for superconducting accelerator, we are planning to develop 325MHz spoke cavity which can be practically operated with 4K liquid helium. We have started to fabricate the niobium one-spoke cavity.

  14. Template synthesis of test tube nanoparticles using non-destructive replication.

    PubMed

    Wagner, Jonathan; Yao, Jingyuan; Rodgers, David; Hinds, Bruce

    2013-03-01

    Nano test tubes are a promising delivery vehicle for a range of therapeutics, including small molecule drugs and biologics. However, current template synthesis methods of producing nano test tubes are prohibitively expensive and time consuming. Here, non-destructive template replication was used to increase nano test tube yield from porous alumina by more than a hundredfold. We demonstrate how to produce nano test tubes of several sizes and compositions, including hybrid tubes with different inner and outer surfaces for targeted surface chemistry. Nano test tubes were readily suspended and stored in aqueous solutions without the need for chemical treatment. These nano test tubes should find application as delivery vehicles for therapeutics, particularly for processive 'bionanoreactors' loaded with enzymes. PMID:23376956

  15. Non-destructive testing of mid-IR optical fiber using infrared imaging

    NASA Astrophysics Data System (ADS)

    Gagnon, Marc-André; Fortin, Vincent; Vallée, Réal; Farley, Vincent; Lagueux, Philippe; Guyot, Éric; Marcotte, Frédérick

    2016-05-01

    Optical fiber lasers offers the advantage of being relatively compact and efficient. However, the materials such as fluoride and chalcogenide glasses used for their fabrication must be exempt of defects in order to make efficient laser systems. However, most existing quality control techniques are not compatible with chalcogenide fibers because of their limited transparency in the visible spectral range. For this reason, the Université Laval's Centre d'optique, photonique et laser (COPL), in Quebec City, Canada, has developed a novel non-destructive testing (NDT) methodology based on infrared imaging to address this problem. The results show how this simple screening technique eases the selection of high-quality fibers for the design of high-power mid-IR lasers.

  16. Evaluation of thermal cameras for non-destructive thermal testing applications

    NASA Astrophysics Data System (ADS)

    Chrzanowski, K.; Park, S. N.

    2001-04-01

    Thermal cameras are nowadays often used in industry and science for non-destructive thermal testing (NDTT). There have been published, by the American Society for Testing of Materials, two standards that present detailed measurement procedures of the minimum resolvable temperature difference (MRTD) and the minimum detectable temperature difference (MDTD) of commercial thermal cameras for NDTT applications. However, the standards provide only very general guidelines about the use of the measured MRTD and MDTD values for evaluation of thermal cameras for NDTT applications. Precise methods that enable evaluation of a thermal imager for NDTT application on the basis of measurement results of the MRTD and the MDTD are presented in this paper. The methods enable estimation of probabilities of detection, orientation, recognition and identification of thermal anomalies generated by flaws in the materials imaged.

  17. Prediction of Service Life of Cordierite-Mullite Refractory Materials by Non-Destructive Methods

    NASA Astrophysics Data System (ADS)

    Boccaccini, D. N.; Kamseu, Elie; Volkov-Husoviæ, T. D.; Cannio, M.; Romagnoli, M.; Veronesi, P.; Dlouhy, I.; Boccaccini, A. R.; Leonelli, C.

    2008-02-01

    Ultrasonic pulse velocity testing was used to perform non-destructive quality control of refractory plates used as substrates in fast firing of porcelain whitewares. The measurement of the ultrasonic velocity was used to asses the presence of internal voids or cracks originated from the manufacturing procedure. Image analysis was used to predict thermal stability of the refractory materials. Two cordierite-mullite compositions were investigated that are characterized by different microstructure morphologies and crack propagation behaviour. A brief discussion about the correlation between microstructure, crack propagation behaviour and thermal shock resistance is presented. Moreover, empirical models were developed to predict the service life of refractory plates from measured values of ultrasonic velocities in plates in the as-received state.

  18. Non-destructive fraud detection in rosehip oil by MIR spectroscopy and chemometrics.

    PubMed

    Santana, Felipe Bachion de; Gontijo, Lucas Caixeta; Mitsutake, Hery; Mazivila, Sarmento Júnior; Souza, Leticia Maria de; Borges Neto, Waldomiro

    2016-10-15

    Rosehip oil (Rosa eglanteria L.) is an important oil in the food, pharmaceutical and cosmetic industries. However, due to its high added value, it is liable to adulteration with other cheaper or lower quality oils. With this perspective, this work provides a new simple, fast and accurate methodology using mid-infrared (MIR) spectroscopy and partial least squares discriminant analysis (PLS-DA) as a means to discriminate authentic rosehip oil from adulterated rosehip oil containing soybean, corn and sunflower oils in different proportions. The model showed excellent sensitivity and specificity with 100% correct classification. Therefore, the developed methodology is a viable alternative for use in the laboratory and industry for standard quality analysis of rosehip oil since it is fast, accurate and non-destructive. PMID:27173556

  19. PREDICTION OF DISSOLVER LIFETIMES THROUGH NON-DESTRUCTIVE EVALUATION AND LABORATORY TESTING

    SciTech Connect

    Mickalonis, J.; Woodsmall, T.; Hinz, W.; Edwards, T.

    2011-10-03

    Non-destructive evaluation was used as the primary method of monitoring the corrosion degradation of nuclear material dissolvers and assessing the remaining lifetimes. Materials were typically processed in nitric acid based (4-14M) solutions containing fluoride concentrations less than 0.2 M. The primary corrosion issue for the stainless steel dissolvers is the occurrence of localized corrosion near the tank bottom and the heat affected zones of the welds. Laboratory data for a range of operational conditions, including solution chemistry and temperature, was used to assess the impact of processing changes on the dissolver corrosion rate. Experimental and NDE-based general corrosion rates were found to be in reasonable agreement for standard dissolution chemistries consisting of nitric acid with fluorides and at temperatures less than 95 C. Greater differences were observed when chloride was present as an impurity and temperatures exceeded 100 C.

  20. Rapid, non-destructive evaluation of ultrathin WSe{sub 2} using spectroscopic ellipsometry

    SciTech Connect

    Eichfeld, Sarah M.; Lin, Yu-Chuan; Hossain, Lorraine; Eichfeld, Chad M.; Robinson, Joshua A.

    2014-09-01

    The utilization of tungsten diselenide (WSe{sub 2}) in electronic and optoelectronic devices depends on the ability to understand and control the process-property relationship during synthesis. We demonstrate that spectroscopic ellipsometry is an excellent technique for accurate, non-destructive determination of ultra-thin (<30 nm) WSe{sub 2} properties. The refractive index (n) and extinction coefficient (k) were found to be independent of thickness down to 1.3 nm, and were used to determine film thickness, which was confirmed to be within 9% of values found via atomic force microscopy. Finally, the optical bandgap was found to closely correlate with thickness, ranging from 1.2 to 1.55 eV as the WSe{sub 2} is thinned to the equivalent of 2 atomic layers.

  1. Monitoring ground anchor using non-destructive ground anchor integrity test (NDT-GRANIT)

    NASA Astrophysics Data System (ADS)

    Robbany, Z.; Handayani, G.

    2015-09-01

    Monitoring at ground anchor commonly uses a pull out test method, therefor we developing a non-destructive ground anchor integrity testing (NDT-GRANIT). NDT-GRANIT using the principle of seismic waves that have been modified into form of sweep signal, the signal will be demodulated, filtered, and Fourier transformation (inverse discrete Fourier transform) so the data can be interpreted reflected wave from the ground anchor. The method was applied to determine whether the ground anchor still gripped in the subsurface by looking the attenuation of the wave generated sources. From the result we can see that ground anchor does not grip. To validate the results of the comparison method of measurement used pile integrity test.

  2. MCNP ESTIMATE OF THE SAMPLED VOLUME IN A NON-DESTRUCTIVE IN SITU SOIL CARBON ANALYSIS.

    SciTech Connect

    WIELOPOLSKI, L.; DIOSZEGI, I.; MITRA, S.

    2004-05-03

    Global warming, promoted by anthropogenic CO{sub 2} emission into the atmosphere, is partially mitigated by the photosynthesis processes of the terrestrial echo systems that act as atmospheric CO{sub 2} scrubbers and sequester carbon in soil. Switching from till to no till soils management practices in agriculture further augments this process. Carbon sequestration is also advanced by putting forward a carbon ''credit'' system whereby these can be traded between CO{sub 2} producers and sequesters. Implementation of carbon ''credit'' trade will be further promulgated by recent development of a non-destructive in situ carbon monitoring system based on inelastic neutron scattering (INS). Volumes and depth distributions defined by the 0.1, 1.0, 10, 50, and 90 percent neutron isofluxes, from a point source located at either 5 or 30 cm above the surface, were estimated using Monte Carlo calculations.

  3. Non-destructive evaluation of depth of surface cracks using ultrasonic frequency analysis.

    PubMed

    Her, Shiuh-Chuan; Lin, Sheng-Tung

    2014-01-01

    Ultrasonic is one of the most common uses of a non-destructive evaluation method for crack detection and characterization. The effectiveness of the acoustic-ultrasound Structural Health Monitoring (SHM) technique for the determination of the depth of the surface crack was presented. A method for ultrasonic sizing of surface cracks combined with the time domain and frequency spectrum was adopted. The ultrasonic frequency spectrum was obtained by Fourier transform technique. A series of test specimens with various depths of surface crack ranging from 1 mm to 8 mm was fabricated. The depth of the surface crack was evaluated using the pulse-echo technique. In this work, three different longitudinal waves with frequencies of 2.25 MHz, 5 MHz and 10 MHz were employed to investigate the effect of frequency on the sizing detection of surface cracks. Reasonable accuracies were achieved with measurement errors less than 7%. PMID:25225875

  4. In-situ and non-destructive focus determination device for high-precision laser applications

    NASA Astrophysics Data System (ADS)

    Armbruster, Oskar; Naghilou, Aida; Pöhl, Hannes; Kautek, Wolfgang

    2016-09-01

    A non-destructive, in-line, and low-cost focusing device based on an image sensor has been developed and demonstrated. It allows an in situ focus determination for a broad variety of laser types (e.g. cw and pulsed lasers). It provides stringent focusing conditions with high numerical apertures. This approach does not require sub-picosecond and/or auxiliary lasers, or high fluences above damage thresholds. Applications of this system include, but are not limited to the laser-illumination of micro-electrodes, pump-probe microscopy on thin films, and laser ablation of small samples without sufficient surface area for focus determination by ablation. An uncertainty of the focus position by an order of magnitude less than the respective Rayleigh length could be demonstrated.

  5. High-resolution thermal imaging methodology for non-destructive evaluation of historic structures

    NASA Astrophysics Data System (ADS)

    Hess, Michael; Vanoni, David; Petrovic, Vid; Kuester, Falko

    2015-11-01

    This paper presents a methodology for automated, portable thermography, for the acquisition of high-resolution thermal image mosaics supporting the non-destructive evaluation of historic structures. The presented approach increases the spatial resolution of thermal surveys to a level of detail needed for building scale analysis. The integration of a robotic camera platform enables automated alignment of multiple images into a high-resolution thermal image mosaic giving a holistic view of the structure while maintaining a level of detail equaling or exceeding that of traditional spot surveys using existing cameras. Providing a digital workflow for automated data and metadata recording increases the consistency and accuracy of surveys regardless of the location or operator. An imaging workflow and instrumentation are shown for a case-study on buildings in Florence, Italy demonstrating the effectiveness of this methodology for structural diagnostics.

  6. Non-destructive research methods applied on materials for the new generation of nuclear reactors

    NASA Astrophysics Data System (ADS)

    Bartošová, I.; Slugeň, V.; Veterníková, J.; Sojak, S.; Petriska, M.; Bouhaddane, A.

    2014-06-01

    The paper is aimed on non-destructive experimental techniques applied on materials for the new generation of nuclear reactors (GEN IV). With the development of these reactors, also materials have to be developed in order to guarantee high standard properties needed for construction. These properties are high temperature resistance, radiation resistance and resistance to other negative effects. Nevertheless the changes in their mechanical properties should be only minimal. Materials, that fulfil these requirements, are analysed in this work. The ferritic-martensitic (FM) steels and ODS steels are studied in details. Microstructural defects, which can occur in structural materials and can be also accumulated during irradiation due to neutron flux or alpha, beta and gamma radiation, were analysed using different spectroscopic methods as positron annihilation spectroscopy and Barkhausen noise, which were applied for measurements of three different FM steels (T91, P91 and E97) as well as one ODS steel (ODS Eurofer).

  7. Transient elastodynamic model for beam defect interaction: application to non-destructive testing

    PubMed

    Raillon; Lecoeur-Taibi

    2000-03-01

    Modeling tools have been developed at the French Atomic Energy Commission (CEA) for the simulation of ultrasonic non-destructive testing inspections. In this paper the model for the prediction of echoes arising from defects within a piece (Mephisto) is presented and some examples are given and compared with experimental results. The model for computing wave defect interaction is based on Kirchhoff's approximation, and uses the principle of reciprocity and a mode-by-mode (between the transducer and the defect) calculation of the echoes. It accounts for possible mode conversions. These approximations and other approximations for the radiated field incident on the defect allow us to obtain a formulation of the echo received at the transducer, which is able to be computed rapidly. PMID:10829719

  8. Non-destructive quantitative analysis of risperidone in film-coated tablets.

    PubMed

    Orkoula, M G; Kontoyannis, C G

    2008-07-15

    A simple, non-destructive, methodology based on FT-Raman spectroscopy was developed for the quantitative analysis of risperidone in commercially available film-coated tablets. A simple linear regression model was constructed based on standard tablets, prepared using the same manufacturing process as the commercially available. The tablets contained 0.27, 0.54, 1.08, 1.62, 2.16, 3.24 and 4.32 wt% risperidone. The most prominent Raman vibration of the active pharmaceutical ingredient at 1533 cm(-1), recorded using a home-made rotating system, was plotted against concentration. The model was tested on commercial film-coated tablets. The results were compared against those obtained by application of HPLC on the same samples. PMID:18359600

  9. Non-Destructive Evaluation of Thermal Spray Coating Interface Quality By Eddy Current Method

    SciTech Connect

    B. Mi; G. Zhao; R. Bayles

    2006-08-10

    Thermal spray coating is usually applied through directing molten or softened particles at very high velocities onto a substrate. An eddy current non-destructive inspection technique is presented here for thermal spray coating interface quality characterization. Several high-velocity-oxy-fuel (HVOF) coated steel plates were produced with various surface preparation conditions or spray process parameters. A quad-frequency eddy current probe was used to manually scan over the coating surface to evaluate the bonding quality. Experimental results show that different surface preparation conditions and varied process parameters can be successfully differentiated by the impedance value observed from the eddy current probe. The measurement is fairly robust and consistent. This non-contact, nondestructive, easy-to-use technique has the potential for evaluating the coating quality immediately after its application so that any defects can be corrected immediately.

  10. Contribution to the improvement of heritage mural painting non-destructive testing by stimulated infrared thermography

    NASA Astrophysics Data System (ADS)

    Bodnar, Jean-Luc; Mouhoubi, Kamel; Di Pallo, Luigi; Detalle, Vincent; Vallet, Jean-Marc; Duvaut, Thierry

    2013-10-01

    Non-destructive testing of heritage mural paintings by means of stimulated infrared thermography has now become rather efficient [1-14]. However, pigments, which form a pictorial layer, have contrasting radiative properties possibly leading to artifact detection. In this paper, attempts to alleviate this difficulty are presented. Based on the spectroscopic study of different paint layers, one can argue that, in the medium infrared field, this radiative disparity decreases significantly. Then, with similar settings, it can be shown that ceramic radiative sources allow reaching this wavelength band. Finally, on the basis of a study carried out on an academic sample and a partial copy of a fresco from the cathedral of Angers, combining ceramic heat sources with a laboratory SAMMTHIR experimental setup enables to make real headway in terms of defects' detection.

  11. Monitoring ground anchor using non-destructive ground anchor integrity test (NDT-GRANIT)

    SciTech Connect

    Robbany, Z. Handayani, G.

    2015-09-30

    Monitoring at ground anchor commonly uses a pull out test method, therefor we developing a non-destructive ground anchor integrity testing (NDT-GRANIT). NDT-GRANIT using the principle of seismic waves that have been modified into form of sweep signal, the signal will be demodulated, filtered, and Fourier transformation (inverse discrete Fourier transform) so the data can be interpreted reflected wave from the ground anchor. The method was applied to determine whether the ground anchor still gripped in the subsurface by looking the attenuation of the wave generated sources. From the result we can see that ground anchor does not grip. To validate the results of the comparison method of measurement used pile integrity test.

  12. Wavelet Processing of Continuous Scanning Laser Doppler Vibrometry data in Non-Destructive Testing

    NASA Astrophysics Data System (ADS)

    Chiariotti, P.; Revel, G. M.; Martarelli, M.

    2015-11-01

    The present paper proposes a novel non-destructive testing procedure based on the exploitation of the simultaneous time and spatial sampling provided by Continuous Scanning Laser Doppler Vibrometry (CSLDV) and the feature extraction capabilities of wavelet-based processing. Two criteria for selecting in an objective way the mother-wavelet to be used in the decomposition procedure, the Relative Wavelet Energy and Energy to Shannon Entropy Ratio, are compared in terms of capability of best locating the damage. The paper demonstrates the applicability of the procedure for the identification of superficial and in-depth defects in simulated and real test cases when an area scan is performed over the test sample. The method shows promising results, since defects are identified in different severity conditions.

  13. Extracting Entanglement Entropy Via Non-Destructive Imaging of an Ultracold Atomic Gas

    NASA Astrophysics Data System (ADS)

    Price, Craig; Liu, Qi; Gemelke, Nathan

    2015-03-01

    Entanglement plays an important role in determining the thermodynamic ground state of many many-body quantum systems, and recent theoretical studies have provided evidence that broad classes of quantum critical and topologically ordered states may be characterized by the scaling properties of their entanglement entropy (EE). We describe how EE can be extracted in a QND imaging process, in which information is transferred from one quantum gas to another using pairwise entangling schemes, and how the subsequent non-local thermal back-action of detection may be used to probe pre-existing entanglement in the sample. We discuss related applications of quantum collisional microscopy, including minimally destructive imaging of non-equilibrium quantum gases, and the algorithmic cooling of a Mott-insulator by non-destructive detection and removal of thermal defects.

  14. Gigahertz time-domain spectroscopy and imaging for non-destructive materials research and evaluation

    PubMed Central

    Bulgarevich, Dmitry S.; Shiwa, Mitsuharu; Furuya, Takashi; Tani, Masahiko

    2016-01-01

    By using optical sampling with repetition frequency modulation of pump/probe laser pulses on photoconductive emitter/detector antennas, the high-speed time/frequency domain gigahertz imaging is reported due to the absence of opto-mechanical delay line in this optical scheme. The clear contrast for a 3-cm wide metal plate, which was placed behind a 5-cm thick concrete block, was observed with a 1 × 1 mm image pixilation. On average, it took only ~0.75 s per pixel/waveform acquisition/assignment with a 675 ps time-domain window. This could become a valuable non-destructive evaluation technique in gigahertz spectral range with all benefits of time-domain spectroscopy. PMID:27302877

  15. In situ non-destructive measurement of biofilm thickness and topology in an interferometric optical microscope.

    PubMed

    Larimer, Curtis; Suter, Jonathan D; Bonheyo, George; Addleman, Raymond Shane

    2016-06-01

    Biofilms are ubiquitous and impact the environment, human health, dental hygiene, and a wide range of industrial processes. Biofilms are difficult to characterize when fully hydrated, especially in a non-destructive manner, because of their soft structure and water-like bulk properties. Herein a method of measuring and monitoring the thickness and topology of live biofilms of using white light interferometry is described. Using this technique, surface morphology, surface roughness, and biofilm thickness were measured over time without while the biofilm continued to grow. The thickness and surface topology of a P. putida biofilm were monitored growing from initial colonization to a mature biofilm. Measured thickness followed expected trends for bacterial growth. Surface roughness also increased over time and was a leading indicator of biofilm growth. PMID:26992071

  16. Gigahertz time-domain spectroscopy and imaging for non-destructive materials research and evaluation

    NASA Astrophysics Data System (ADS)

    Bulgarevich, Dmitry S.; Shiwa, Mitsuharu; Furuya, Takashi; Tani, Masahiko

    2016-06-01

    By using optical sampling with repetition frequency modulation of pump/probe laser pulses on photoconductive emitter/detector antennas, the high-speed time/frequency domain gigahertz imaging is reported due to the absence of opto-mechanical delay line in this optical scheme. The clear contrast for a 3-cm wide metal plate, which was placed behind a 5-cm thick concrete block, was observed with a 1 × 1 mm image pixilation. On average, it took only ~0.75 s per pixel/waveform acquisition/assignment with a 675 ps time-domain window. This could become a valuable non-destructive evaluation technique in gigahertz spectral range with all benefits of time-domain spectroscopy.

  17. Gigahertz time-domain spectroscopy and imaging for non-destructive materials research and evaluation.

    PubMed

    Bulgarevich, Dmitry S; Shiwa, Mitsuharu; Furuya, Takashi; Tani, Masahiko

    2016-01-01

    By using optical sampling with repetition frequency modulation of pump/probe laser pulses on photoconductive emitter/detector antennas, the high-speed time/frequency domain gigahertz imaging is reported due to the absence of opto-mechanical delay line in this optical scheme. The clear contrast for a 3-cm wide metal plate, which was placed behind a 5-cm thick concrete block, was observed with a 1 × 1 mm image pixilation. On average, it took only ~0.75 s per pixel/waveform acquisition/assignment with a 675 ps time-domain window. This could become a valuable non-destructive evaluation technique in gigahertz spectral range with all benefits of time-domain spectroscopy. PMID:27302877

  18. Yucca Mountain project container fabrication, closure and non-destructive evaluation development activities; Summary and viewgraphs

    SciTech Connect

    Russell, E.W.; Nelson, T.A.

    1989-06-01

    In this presentation, container fabrication, closure, and non-destructive evaluation (NDE) process development activities are described. All of these activities are interrelated, and will contribute to the metal barrier selection activity. The plan is to use a corrosion-resistant material in the form of a cylinder with a wall thickness of {approximately}1cm (2cm for pure copper.) The materials under consideration include the three austenitic alloys: stainless steel-304L, stainless steel-316L and alloy 825, as well as the three copper alloys: CDA 102, CDA 613, and CDA 715. This document reviews the recommended procedures and processes for fabricating, closing and evaluating each of the candidate materials. (KGD)

  19. Monitoring fungal growth on brown rice grains using rapid and non-destructive hyperspectral imaging.

    PubMed

    Siripatrawan, U; Makino, Y

    2015-04-16

    This research aimed to develop a rapid, non-destructive, and accurate method based on hyperspectral imaging (HSI) for monitoring spoilage fungal growth on stored brown rice. Brown rice was inoculated with a non-pathogenic strain of Aspergillus oryzae and stored at 30 °C and 85% RH. Growth of A. oryzae on rice was monitored using viable colony counts, expressed as colony forming units per gram (CFU/g). The fungal development was observed using scanning electron microscopy. The HSI system was used to acquire reflectance images of the samples covering the visible and near-infrared (NIR) wavelength range of 400-1000 nm. Unsupervised self-organizing map (SOM) was used to visualize data classification of different levels of fungal infection. Partial least squares (PLS) regression was used to predict fungal growth on rice grains from the HSI reflectance spectra. The HSI spectral signals decreased with increasing colony counts, while conserving similar spectral pattern during the fungal growth. When integrated with SOM, the proposed HSI method could be used to classify rice samples with different levels of fungal infection without sample manipulation. Moreover, HSI was able to rapidly identify infected rice although the samples showed no symptoms of fungal infection. Based on PLS regression, the coefficient of determination was 0.97 and root mean square error of prediction was 0.39 log (CFU/g), demonstrating that the HSI technique was effective for prediction of fungal infection in rice grains. The ability of HSI to detect fungal infection at early stage would help to prevent contaminated rice grains from entering the food chain. This research provides scientific information on the rapid, non-destructive, and effective fungal detection system for rice grains. PMID:25662486

  20. Non-destructive ripeness sensing by using proton NMR (Nuclear Magnetic Resonance)

    SciTech Connect

    Cho, Seong In; Krutz, G.W.; Stroshine, R.L. . Dept. of Agricultural Engineering); Bellon, V. , 34 - Montpellier )

    1990-01-01

    More than 80 kinds of fruits and vegetables are available in the United States. But only about 6 of them have their quality standards (Dull, 1986). In the 1990 Fresh Trends survey (Zind, 1990), consumers were asked to rate 16 characteristics important to their decision to purchase fresh produce. The four top ranking factors were ripeness/freshness, taste/flavor, appearance/condition and nutritional value. Of these surveyed, 96% rated ripeness/freshness as extremely important or very important. Therefore, the development of reliable grading or sorting techniques for fresh commodities is essential. Determination of fruit quality often involves cutting and tasting. Non-destructive quality control in fruit and vegetables is a goal of growers and distributors, as well as the food processing industry. Many nondestructive techniques have been evaluated including soft x-ray, optical transmission, near infrared radiation, and machine vision. However, there are few reports of successful non-destructive measurement of sugar content directly in fruit. Higher quality fruit could be harvested and available to consumers if a nondestructive sensor that detects ripeness level directly by measuring sugar content were available. Using proton Nuclear Magnetic Resonance (NMR) principle is the possibility. A nondestructive ripeness (or sweetness) sensor for fruit quality control can be developed with the proton NMR principle (Cho, 1989). Several feasibility studies were necessary for the ripeness sensor development. Main objectives in this paper was to investigate the feasibilities (1) to detect ripeness (or sweetness level) of raw fruit tissue with an high resolution proton NMR spectroscopy (200 MHz) and (2) to measure sugar content of intact fruit with a low resolution proton NMR spectroscopy (10 MHz). 7 refs., 4 figs.

  1. NON-DESTRUCTIVE TBC SPALLATION DETECTION BY A MICRO-INDENTATION METHOD

    SciTech Connect

    J. M. Tannenbaum; B.S.-J. Kang; M.A. Alvin

    2010-06-18

    In this research, a load-based depth-sensing micro-indentation method for spallation detection and damage assessment of thermal barrier coating (TBC) materials is presented. A non-destructive multiple loading/partial unloading testing methodology was developed where in stiffness responses of TBC coupons subjected to various thermal cyclic loading conditions were analyzed to predict the spallation site and assess TBC degradation state. The measured stiffness responses at various thermal loading cycles were used to generate time-series color maps for correlation with accumulation of TBC residual stress states. The regions with higher stiffness responses can be linked to a rise in out-of-plane residual stress located near or at the yttria stabilized zirconia (YSZ)/thermally grown oxide (TGO) interface, which is ultimately responsible for initiating TBC spallation failure. A TBC thermal exposure testing plan was carried out where time-series cross-sectional microstructural analyses of damage accumulation and spallation failure associated with the evolution of bond coat/TGO/top coat composite (e.g. thickness, ratcheting, localized oxidations, etc.) of air plasma sprayed (APS) TBCs were evaluated and correlated to the measured stiffness responses at various thermal cycles. The results show that the load-based micro-indentation test methodology is capable of identifying the spallation site(s) before actual occurrence. This micro-indentation technique can be viewed as a viable non-destructive evaluation (NDE) technique for determining as-manufactured and process-exposed TBCs. This technique also shows promise for the development of a portable instrument for on-line, in-situ spallation detection/prediction of industrial-size TBC turbine components.

  2. Non-destructive Ripeness Sensing by Using Proton NMR [Nuclear Magnetic Resonance

    DOE R&D Accomplishments Database

    Cho, Seong In; Krutz, G. W.; Stroshine, R. L.; Bellon, V.

    1990-01-01

    More than 80 kinds of fruits and vegetables are available in the United States. But only about 6 of them have their quality standards (Dull, 1986). In the 1990 Fresh Trends survey (Zind, 1990), consumers were asked to rate 16 characteristics important to their decision to purchase fresh produce. The four top ranking factors were ripeness/freshness, taste/flavor, appearance/condition and nutritional value. Of these surveyed, 96% rated ripeness/freshness as extremely important or very important. Therefore, the development of reliable grading or sorting techniques for fresh commodities is essential. Determination of fruit quality often involves cutting and tasting. Non-destructive quality control in fruit and vegetables is a goal of growers and distributors, as well as the food processing industry. Many nondestructive techniques have been evaluated including soft x-ray, optical transmission, near infrared radiation, and machine vision. However, there are few reports of successful non-destructive measurement of sugar content directly in fruit. Higher quality fruit could be harvested and available to consumers if a nondestructive sensor that detects ripeness level directly by measuring sugar content were available. Using proton Nuclear Magnetic Resonance (NMR) principle is the possibility. A nondestructive ripeness (or sweetness) sensor for fruit quality control can be developed with the proton NMR principle (Cho, 1989). Several feasibility studies were necessary for the ripeness sensor development. Main objectives in this paper was to investigate the feasibilities (1) to detect ripeness (or sweetness level) of raw fruit tissue with an high resolution proton NMR spectroscopy (200 MHz) and (2) to measure sugar content of intact fruit with a low resolution proton NMR spectroscopy (10 MHz).

  3. μ-XRF analysis of glasses: a non-destructive utility for Cultural Heritage applications.

    PubMed

    Vaggelli, G; Cossio, R

    2012-02-01

    This paper presents a μ-XRF analytical approach for a non-destructive study of Cultural Heritage glass finds. This technique can be used for quantitative analysis of small volumes of solid samples, with a sensitivity that is superior to the electron microprobe but inferior to an ICP-MS system. An experimental set-up with natural and synthetic glass standards is proposed here for the quantitative analyses of major and trace elements on glass objects which cannot be sampled such as small archaeological or historical artefacts from Cultural Heritage. The described method, performed by means of the commercial μ-XRF Eagle III-XPL, was applied to Islamic glass specimens of Sasanian production (III-VII century A.D.) previously analyzed by ICP-MS and SEM-EDS techniques (P. Mirti, M. Pace, M. Negro Ponzi and M. Aceto, Archaeometry, 2008, 50(3), 429-450; P. Mirti, M. Pace, M. Malandrino and M. Negro Ponzi, J. Archaeol. Sci., 36, 1061-1069; and M. Gulmini, M. Pace, G. Ivaldi, M. Negro Ponzi and P. Mirti, J. Non-Cryst. Solids, 2009, 355, 1613-1621) and coming from the archaeological site of Veh Ardasir in modern Iraq. Major elements (Na, Mg, Al, Si, K, Ca, Fe) of glass specimens show an accuracy better than 5%. Trace elements (Cr, Mn, Sr and Zr) display an accuracy better than 5% when the checked elements have a concentration >100 ppm by weight, whereas it is around 10% with a concentration <100 ppm by weight. μ-XRF is, therefore, a suitable elemental analysis technique for the non-destructive study of small glass finds due to its relatively good accuracy, reproducibility and low detection limits (∼tens ppm). PMID:22163367

  4. EMAT and Eddy Current Dual Probe for Detecting Surface and Near-Surface Defects

    SciTech Connect

    Edwards, R. S.; Dixon, S.; Sophian, A.; Tian, G. Y.

    2006-03-06

    In non-destructive testing (NDT) it is often preferable to test samples using several different techniques, in order to gain a higher probability of detection and a more reliable characterisation of each defect. However, this can lead to an increase in testing time and cost. A probe containing several NDT devices will give this accuracy and reliability, with the testing speed of using only one technique. We present initial results using a dual-probe containing a pulsed eddy current probe and a pair of electro-magnetic acoustic transducers generating ultrasonic surface waves in a pitch-catch manner. These two techniques are complimentary and are sensitive to surface and near surface defects, and no detrimental interference between the two techniques is observed. As both techniques are non-contact there is the possibility of use in hot or moving environments. The results from both can be combined using data fusion to give a higher probability of detection and more reliable sizing. Measurements of aluminium and steel samples containing manufactured and real defects are presented.

  5. Accuracy of Non-Destructive Testing of PBRs to Estimate Fragilities

    NASA Astrophysics Data System (ADS)

    Brune, J. N.; Brune, R.; Biasi, G. P.; Anooshehpoor, R.; Purvance, M.

    2011-12-01

    Prior studies of Precariously Balanced Rocks (PBRs) have involved various methods of documenting rock shapes and fragilities. These have included non-destructive testing (NDT) methods such as photomodeling, and potentially destructive testing (PDT) such as forced tilt tests. PDT methods usually have the potential of damaging or disturbing the rock or its pedestal so that the PBR usefulness for future generations is compromised. To date we have force-tilt tested approximately 28 PBRs, and of these we believe 7 have been compromised. We suggest here that given other inherent uncertainties in the current methodologies, NDT methods are now sufficiently advanced as to be adequate for the current state of the art use for comparison with Ground Motion Prediction Equations (GMPEs) and seismic hazard maps (SHMs). Here we compare tilt-test static toppling estimates to three non-destructive methods: (1) 3-D photographic modeling (2) profile analysis assuming the rock is 2-D, and (3) expert judgments from photographs. 3-D modeling uses the commercial Photomodeler program and photographs in the field taken from numerous directions around the rock. The output polyhedral shape is analyzed in Matlab determine the center of mass and in Autocad to estimate the static overturning angle alpha. For the 2-D method we chose the photograph in profile looking perpendicular to the estimated direction of toppling. The rock is outlined as a 2-D object in Matlab. Rock dimensions, rocking points, and a vertical reference are supplied by the photo analyst to estimate the center of gravity and static force overturning angles. For the expert opinion method we used additional photographs taken from different directions to improve the estimates of the center of mass and the rocking points. We used 7 rocks for comparisons. The error in estimating tan alpha from 3-D modeling is about 0.05. For 2-D estimates an average error is about 0.1 (?). For expert opinion estimates the error is about 0.06. For

  6. Non-destructive testing for the structures and civil infrastructures characterization

    NASA Astrophysics Data System (ADS)

    Capozzoli, L.; Rizzo, E.

    2012-04-01

    infrared thermography and sonic testing. Finally, we investigated a radiant floor by GPR (900 MHz to 2000 MHz antennas) and long-wave infrared camera. Non-destructive diagnostic techniques allow to investigate a building structure in reinforced concrete or masonry without altering the characteristics of the element investigated. For this reason, geo-electrical and electromagnetic surveys of masonry are a suitable non-destructive tool for the diagnosis of a deteriorated concrete structure. Moreover, the integration of different NDT techniques (conventional and no-conventional) is a very powerful to maximize the capabilities and to compensate for the limitations of each method.

  7. Fast solver for large scale eddy current non-destructive evaluation problems

    NASA Astrophysics Data System (ADS)

    Lei, Naiguang

    Eddy current testing plays a very important role in non-destructive evaluations of conducting test samples. Based on Faraday's law, an alternating magnetic field source generates induced currents, called eddy currents, in an electrically conducting test specimen. The eddy currents generate induced magnetic fields that oppose the direction of the inducing magnetic field in accordance with Lenz's law. In the presence of discontinuities in material property or defects in the test specimen, the induced eddy current paths are perturbed and the associated magnetic fields can be detected by coils or magnetic field sensors, such as Hall elements or magneto-resistance sensors. Due to the complexity of the test specimen and the inspection environments, the availability of theoretical simulation models is extremely valuable for studying the basic field/flaw interactions in order to obtain a fuller understanding of non-destructive testing phenomena. Theoretical models of the forward problem are also useful for training and validation of automated defect detection systems. Theoretical models generate defect signatures that are expensive to replicate experimentally. In general, modelling methods can be classified into two categories: analytical and numerical. Although analytical approaches offer closed form solution, it is generally not possible to obtain largely due to the complex sample and defect geometries, especially in three-dimensional space. Numerical modelling has become popular with advances in computer technology and computational methods. However, due to the huge time consumption in the case of large scale problems, accelerations/fast solvers are needed to enhance numerical models. This dissertation describes a numerical simulation model for eddy current problems using finite element analysis. Validation of the accuracy of this model is demonstrated via comparison with experimental measurements of steam generator tube wall defects. These simulations generating two

  8. Future Chances and Challenges for Near Surface Geophysics

    NASA Astrophysics Data System (ADS)

    Noell, U.; Meyer, U.

    2011-12-01

    Near surface geophysics provides information from global to local scale: a) Standardized geophysical observations are utilized e.g. in risk management frameworks beyond the national level a) Specific tasks in local or regional frameworks as mine flooding or ground water recharge monitoring are required. Either way, near surface geophysics is connected more than ever to technical problems and thus is vastly adopted by engineering. This is a chance and challenge at the same time. The chance is to make near surface geophysics more useful in applied and practical issues, the challenge is to develop new profiles and research directions. Recent satellite earth observation missions have much enhanced capabilities to observe near surface features and changes but generally very limited penetration. Near surface geophysics can bridge the gap between surface characterization and subsurface structures. Subsurface structures as aquifer systems, layering, deposits and mineralization can be determined by non-invasive near surface geophysics. A special challenge here is the enhanced interpretation of the physical data combined with an improved understanding of complex subsurface processes. Moreover, the limits of the interpretation and the measurements need to be quantified. Another future challenge is to gain a better and reliable understanding of soil - water cycles and gaseous flows via near surface geophysics. New methods and techniques that did not seem feasible in the past must reviewed whilst technology developed. This includes squids for magnetics and electromagnetics applications, nuclear magnetic resonance methods etc.

  9. Direct, non-destructive, and rapid evaluation of developmental cotton fibers by ATR FT-IR spectroscopy

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Chemical, compositional, and structural differences within the fibers at different growth stages have been investigated considerably through a number of methodologies. Due to its direct, non-destructive, and rapid attribute, this study reports the utilization of attenuated total reflection Fourier t...

  10. Development of non-destructive quality measurement technique for cabbage seed (Brassica campestris L) using hyperspectral reflectance imaging

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Cabbage (Brassica campestris L) is an important crop for Asian countries especially in Korea, Japan and China. In order to achieve uniform and high-yield rate of cabbage product, the seed lot quality needs to be controlled. Non-destructive evaluation of seed viability is an important technique for i...

  11. A new facility for Non-Destructive Assay with a time-tagged {sup 252}Cf source

    SciTech Connect

    Stevanato, L.; Caldogno, M.; Hao Xin; Dima, R.; Fabris, D.; Nebbia, G.; Lunardon, M.; Moretto, S.; Pesente, S.; Viesti, G.; Sajo-Bohus, L.

    2010-08-04

    A new facility for non-destructive assay using a time-tagged {sup 252}Cf source is presented. The system is designed to analyze samples having maximum size of about 15x20 cm{sup 2}, the material recognition being obtained by measuring simultaneously transmission of neutrons and gamma rays.

  12. Development of vibrational spectroscopic methods to rapidly and non-destructively assess quality of chicken breast meat

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Development of Vibrational Spectroscopic Methods to Rapidly and Non-Destructively Assess Quality of Chicken Breast Meat H. Zhuang1, M. Sohn2, S. Trabelsi1 and K. Lawrence1 1Quality and Safety Assessment Research Unit, ARS-USDA, 950 College Station Road, Athens, GA 30605 2University of Georgia, De...

  13. A multi-inspection non-destructive testing method for quality evaluation of composite riveted structure

    NASA Astrophysics Data System (ADS)

    Wang, Weihan; He, Jingjing; Yang, Jingsong; Liu, Shengwang; Zhang, Weifang

    2015-03-01

    Carbon fiber composites have excellent mechanical properties, which are widely used in aerospace industry. However, 60% to 80% damages in composite occur in riveted structures. This research focuses on the quality evaluation of three major riveted structures used in mechanical connection: pressure riveted connection, hammer riveted connection and pull riveted connection. The non-destructive testing results show that the pull riveting technology introduces minimal damage to the composite, but the hammer riveted structure can be seriously damaged by the riveting technology. The pull riveted structure is an interference fit, which makes the composite plate firmly fixed. However, the fix is weak in the pressure riveted structure and the hammer riveted structure, due to the small gap between the rivets and plate. The results show that the pull riveted structure has a higher tensile strength compared with the pressure riveted structure and hammer riveted structure. The hammer riveted structure has a large dispersion in mechanical properties caused by the impact loading used in the hammer riveting technology.

  14. Imaging air volume fraction in sea ice using non-destructive X-ray tomography

    NASA Astrophysics Data System (ADS)

    Crabeck, Odile; Galley, Ryan; Delille, Bruno; Else, Brent; Geilfus, Nicolas-Xavier; Lemes, Marcos; Des Roches, Mathieu; Francus, Pierre; Tison, Jean-Louis; Rysgaard, Søren

    2016-05-01

    Although the presence of a gas phase in sea ice creates the potential for gas exchange with the atmosphere, the distribution of gas bubbles and transport of gases within the sea ice are still poorly understood. Currently no straightforward technique exists to measure the vertical distribution of air volume fraction in sea ice. Here, we present a new fast and non-destructive X-ray computed tomography technique to quantify the air volume fraction and produce separate images of air volume inclusions in sea ice. The technique was performed on relatively thin (4-22 cm) sea ice collected from an experimental ice tank. While most of the internal layers showed air volume fractions < 2 %, the ice-air interface (top 2 cm) systematically showed values up to 5 %. We suggest that the air volume fraction is a function of both the bulk ice gas saturation factor and the brine volume fraction. We differentiate micro bubbles (Ø < 1 mm), large bubbles (1 mm < Ø < 5 mm) and macro bubbles (Ø > 5 mm). While micro bubbles were the most abundant type of gas bubbles, most of the air porosity observed resulted from the presence of large and macro bubbles. The ice texture (granular and columnar) as well as the permeability state of ice are important factors controlling the air volume fraction. The technique developed is suited for studies related to gas transport and bubble migration.

  15. Non-destructive measurement of the steel cable stress based on magneto-mechanical effect

    NASA Astrophysics Data System (ADS)

    Chen, Weimin; Liu, Lin; Zhang, Peng; Hu, Shunren

    2010-03-01

    Since steel cables are widely used to be crucial components in cable-stayed bridges and architectural structures, stress measurement of the steel cables has been given serious attentions. Among the current stress measurement methods, magnetic method seems to be the most potential one, but its application is limited because of the complex theoretical mechanism. According to the magneto-mechanical effect, which demonstrates that magnetization in the ferromagnetic material varies with applied stress, a theoretical model of magnetic method is proposed to perfect the theoretical mechanism. Thus, an equation is derived about the relation between magnetization in steel cables and cable stress. In this model, a magnetic stress sensor is designed, with a smart steel cable as a part of it, and then a cable stress measurement system based on LabVIEW is developed. This method allows new application in non-destructive testing, such as monitoring the conditions of stayed-cable. Considering the impact of the magnetic hysteresis, positive and negative pulsed current excitation was used to demagnetize and decrease the output of heat. This method is applied to the stress measurement of prestressed steel cable in Jiangsu Fasten Nippon Steel Cable Company, the experimental results agree with theoretical assumptions, which indicates that the method is feasible and can improve the mechanical stress measurement.

  16. Spatial distribution pattern analysis of subtidal macroalgae assemblages by a non-destructive rapid assessment method

    NASA Astrophysics Data System (ADS)

    Guinda, Xabier; Juanes, José Antonio; Puente, Araceli; Echavarri-Erasun, Beatriz

    2012-01-01

    The extensive field work carried out over the last century has allowed the worldwide description of general distribution patterns and specific composition of rocky intertidal communities. However, the information concerning subtidal communities on hard substrates is more recent and scarce due to the difficulties associated with working in such environments. In this work, a non-destructive method is applied to the study and mapping of subtidal rocky bottom macroalgae assemblages on the coast of Cantabria (N Spain) which is quick, easy and economical. Gelidium corneum and Cystoseira baccata were the dominant species, however, the composition and coverage of macroalgae assemblages varied significantly at different locations and depth ranges. The high presence of Laminaria ochroleuca and Saccorhiza polyschides, characteristic of colder waters, shows the transitional character of this coastal area. The results obtained throughout this study have been very useful to the application of the European Water Framework Directive (WFD 2000/60/EC) and could be of great interest for the future conservation and management of these ecosystems (e.g. Habitats Directive 92/43/EEC).

  17. Rapid and non-destructive identification of water-injected beef samples using multispectral imaging analysis.

    PubMed

    Liu, Jinxia; Cao, Yue; Wang, Qiu; Pan, Wenjuan; Ma, Fei; Liu, Changhong; Chen, Wei; Yang, Jianbo; Zheng, Lei

    2016-01-01

    Water-injected beef has aroused public concern as a major food-safety issue in meat products. In the study, the potential of multispectral imaging analysis in the visible and near-infrared (405-970 nm) regions was evaluated for identifying water-injected beef. A multispectral vision system was used to acquire images of beef injected with up to 21% content of water, and partial least squares regression (PLSR) algorithm was employed to establish prediction model, leading to quantitative estimations of actual water increase with a correlation coefficient (r) of 0.923. Subsequently, an optimized model was achieved by integrating spectral data with feature information extracted from ordinary RGB data, yielding better predictions (r = 0.946). Moreover, the prediction equation was transferred to each pixel within the images for visualizing the distribution of actual water increase. These results demonstrate the capability of multispectral imaging technology as a rapid and non-destructive tool for the identification of water-injected beef. PMID:26213059

  18. Image pixel guided tours: a software platform for non-destructive x-ray imaging

    NASA Astrophysics Data System (ADS)

    Lam, K. P.; Emery, R.

    2009-02-01

    Multivariate analysis seeks to describe the relationship between an arbitrary number of variables. To explore highdimensional data sets, projections are often used for data visualisation to aid discovering structure or patterns that lead to the formation of statistical hypothesis. The basic concept necessitates a systematic search for lower-dimensional representations of the data that might show interesting structure(s). Motivated by the recent research on the Image Grand Tour (IGT), which can be adapted to view guided projections by using objective indexes that are capable of revealing latent structures of the data, this paper presents a signal processing perspective on constructing such indexes under the unifying exploratory frameworks of Independent Component Analysis (ICA) and Projection Pursuit (PP). Our investigation begins with an overview of dimension reduction techniques by means of orthogonal transforms, including the classical procedure of Principal Component Analysis (PCA), and extends to an application of the more powerful techniques of ICA in the context of our recent work on non-destructive testing technology by element specific x-ray imaging.

  19. Non-destructive testing techniques for the forensic engineering investigation of reinforced concrete buildings.

    PubMed

    Hobbs, Brian; Tchoketch Kebir, Mohamed

    2007-04-11

    This study describes in detail the results of a laboratory investigation where the compressive strength of 150mm side-length cubes was evaluated. Non-destructive testing (NDT) was carried out using ultrasonic pulse velocity (UPV) and impact rebound hammer (IRH) techniques to establish a correlation with the compressive strengths of compression tests. To adapt the Schmidt hammer apparatus and the ultrasonic pulse velocity tester to the type of concrete used in Algeria, concrete mix proportions that are recommended by the Algerian code were chosen. The resulting correlation curve for each test is obtained by changing the level of compaction, water/cement ratio and concrete age of specimens. Unlike other works, the research highlights the significant effect of formwork material on surface hardness of concrete where two different mould materials for specimens were used (plastic and wood). A combined method for the above two tests, reveals an improvement in the strength estimation of concrete. The latter shows more improvement by including the concrete density. The resulting calibration curves for strength estimation were compared with others from previous published literature. PMID:16904854

  20. Nitrogen Concentration Estimation in Tomato Leaves by VIS-NIR Non-Destructive Spectroscopy

    PubMed Central

    Ulissi, Valentina; Antonucci, Francesca; Benincasa, Paolo; Farneselli, Michela; Tosti, Giacomo; Guiducci, Marcello; Tei, Francesco; Costa, Corrado; Pallottino, Federico; Pari, Luigi; Menesatti, Paolo

    2011-01-01

    Nitrogen concentration in plants is normally determined by expensive and time consuming chemical analyses. As an alternative, chlorophyll meter readings and N-NO3 concentration determination in petiole sap were proposed, but these assays are not always satisfactory. Spectral reflectance values of tomato leaves obtained by visible-near infrared spectrophotometry are reported to be a powerful tool for the diagnosis of plant nutritional status. The aim of the study was to evaluate the possibility and the accuracy of the estimation of tomato leaf nitrogen concentration performed through a rapid, portable and non-destructive system, in comparison with chemical standard analyses, chlorophyll meter readings and N-NO3 concentration in petiole sap. Mean reflectance leaf values were compared to each reference chemical value by partial least squares chemometric multivariate methods. The correlation between predicted values from spectral reflectance analysis and the observed chemical values showed in the independent test highly significant correlation coefficient (r = 0.94). The utilization of the proposed system, increasing efficiency, allows better knowledge of nutritional status of tomato plants, with more detailed and sharp information and on wider areas. More detailed information both in space and time is an essential tool to increase and stabilize crop quality levels and to optimize the nutrient use efficiency. PMID:22163962

  1. Research Based on Optical Non-Destructive Testing of Pigment Identification.

    PubMed

    Wang, Jigang; Hao, Shengcai; Zhou, Wenhua; Qi, Xiaokun; Shi, Jilong

    2016-04-01

    Optical Non-Destructive Testing (ONDT) can be applied as penetrating elemental and structure analysis technology in the Pigments identification field. Three-dimensional video microscopy, Raman microscopy and energy dispersive X-ray fluorescence spectroscopy are employed to measure the materials based on a Qing Dynasty meticulous painting. The results revealed that the dark yellow area within the decorative patterns was presented due to the interaction of Emerald green and hematite, and the bright yellow edge area was delineated by Cu-Zn-Pb composition. The interesting thing is that an artificial synthetic ultramarine blue was checked in the painting. According to the first synthesized time of ultramarine blue and Paris green, the time limit of the painting completion can be identified. The principle of Pigment subtractive colorant and nitikaset method were employed to interpreting the results. Optical testing combined with the area of cultural relic identification can be a potential method to build an expert identification system successfully. This work also help lay the optical method groundwork for further cultural relic identification, sterilization, and preservation. PMID:27451669

  2. Nitrogen concentration estimation in tomato leaves by VIS-NIR non-destructive spectroscopy.

    PubMed

    Ulissi, Valentina; Antonucci, Francesca; Benincasa, Paolo; Farneselli, Michela; Tosti, Giacomo; Guiducci, Marcello; Tei, Francesco; Costa, Corrado; Pallottino, Federico; Pari, Luigi; Menesatti, Paolo

    2011-01-01

    Nitrogen concentration in plants is normally determined by expensive and time consuming chemical analyses. As an alternative, chlorophyll meter readings and N-NO(3) concentration determination in petiole sap were proposed, but these assays are not always satisfactory. Spectral reflectance values of tomato leaves obtained by visible-near infrared spectrophotometry are reported to be a powerful tool for the diagnosis of plant nutritional status. The aim of the study was to evaluate the possibility and the accuracy of the estimation of tomato leaf nitrogen concentration performed through a rapid, portable and non-destructive system, in comparison with chemical standard analyses, chlorophyll meter readings and N-NO(3) concentration in petiole sap. Mean reflectance leaf values were compared to each reference chemical value by partial least squares chemometric multivariate methods. The correlation between predicted values from spectral reflectance analysis and the observed chemical values showed in the independent test highly significant correlation coefficient (r = 0.94). The utilization of the proposed system, increasing efficiency, allows better knowledge of nutritional status of tomato plants, with more detailed and sharp information and on wider areas. More detailed information both in space and time is an essential tool to increase and stabilize crop quality levels and to optimize the nutrient use efficiency. PMID:22163962

  3. Non-destructive inspection of drilled holes in reinforced honeycomb sandwich panels using active thermography

    NASA Astrophysics Data System (ADS)

    Usamentiaga, R.; Venegas, P.; Guerediaga, J.; Vega, L.; López, I.

    2012-11-01

    The aerospace industry is in constant need of ever-more efficient inspection methods for quality control. Product inspection is also essential to maintain the safe operation of aircraft components designed to perform for decades. This paper proposes a method for non-destructive inspection of drilled holes in reinforced honeycomb sandwich panels. Honeycomb sandwich panels are extensively employed in the aerospace industry due to their high strength and stiffness to weight ratios. In order to attach additional structures to them, panels are reinforced by filling honeycomb cells and drilling holes into the reinforced areas. The proposed procedure is designed to detect the position of the holes within the reinforced area and to provide a robust measurement of the distance between each hole and the boundary of the reinforced area. The result is a fast, safe and clean inspection method for drilled holes in reinforced honeycomb sandwich panels that can be used to robustly assess a possible displacement of the hole from the center of the reinforced area, which could have serious consequences. The proposed method is based on active infrared thermography, and uses state of the art methods for infrared image processing, including signal-to-nose ratio enhancement, hole detection and segmentation. Tests and comparison with X-ray inspections indicate that the proposed system meets production needs.

  4. Non-destructive testing of ceramic balls using high frequency ultrasonic resonance spectroscopy.

    PubMed

    Petit, S; Duquennoy, M; Ouaftouh, M; Deneuville, F; Ourak, M; Desvaux, S

    2005-12-01

    Although ceramic balls are used more and more for bearings in the aerospace and space industries, defects in this type of ceramic material could be dangerous, particularly if such defects are located close to the surface. In this paper, we propose a non-destructive testing method for silicon nitride balls, based on ultrasonic resonance spectroscopy. Through the theoretical study of their elastic vibrations, it is possible to characterize the balls using a vibration mode that is similar to surface wave propagation. The proposed methodology can both excite spheroidal vibrations in the ceramic balls and detect such vibrations over a large frequency range. Studying their resonance spectrums allows the balls' elastic parameters be characterized. Ours is an original method that can quickly estimate the velocity of surface waves using high frequency resonances, which permits surface and sub-surface areas to be tested specifically. Two applications are described in this paper. Both use velocity measurements to achieve their different goals, the first to differentiate between flawless balls from different manufacturing processes, and the second to detect small defects, such as cracks. Our method is rapid and permits the entire ceramic ball to be tested in an industrial context. PMID:16083931

  5. Non-destructive state detection for quantum logic spectroscopy of molecular ions.

    PubMed

    Wolf, Fabian; Wan, Yong; Heip, Jan C; Gebert, Florian; Shi, Chunyan; Schmidt, Piet O

    2016-02-25

    Precision laser spectroscopy of cold and trapped molecular ions is a powerful tool in fundamental physics--used, for example, in determining fundamental constants, testing for their possible variation in the laboratory, and searching for a possible electric dipole moment of the electron. However, the absence of cycling transitions in molecules poses a challenge for direct laser cooling of the ions, and for controlling and detecting their quantum states. Previously used state-detection techniques based on photodissociation or chemical reactions are destructive and therefore inefficient, restricting the achievable resolution in laser spectroscopy. Here, we experimentally demonstrate non-destructive detection of the quantum state of a single trapped molecular ion through its strong Coulomb coupling to a well controlled, co-trapped atomic ion. An algorithm based on a state-dependent optical dipole force changes the internal state of the atom according to the internal state of the molecule. We show that individual quantum states in the molecular ion can be distinguished by the strength of their coupling to the optical dipole force. We also observe quantum jumps (induced by black-body radiation) between rotational states of a single molecular ion. Using the detuning dependence of the state-detection signal, we implement a variant of quantum logic spectroscopy of a molecular resonance. Our state-detection technique is relevant to a wide range of molecular ions, and could be applied to state-controlled quantum chemistry and to spectroscopic investigations of molecules that serve as probes for interstellar clouds. PMID:26855427

  6. Non-destructive mobile monitoring of microbial contaminations on meat surfaces using porphyrin fluorescence intensities.

    PubMed

    Durek, J; Fröhling, A; Bolling, J; Thomasius, R; Durek, P; Schlüter, O K

    2016-05-01

    A non-destructive mobile system for meat quality monitoring was developed and investigated for the possible application along the whole production chain of fresh meat. Pork and lamb meat was stored at 5 °C for up to 20 days post mortem and measured with a fluorescence spectrometer. Additionally, the bacterial influence on the fluorescence signals was evaluated by different experimental procedures. Fluorescence of NADH and different porphyrins could be correlated to the growth of diverse bacteria and hence used for contamination monitoring. The increase of porphyrin fluorescence started after 9 days p.m. for pork and after 2 days p.m. for lamb meat. Based on the results, a mobile fluorescence system was built and compared with the laboratory system. The corrected function of the meat slices showed a root mean square error of 1156.97 r.u. and a mean absolute percentage error of 12.59%; for lamb the values were 470.81 r.u. and 15.55%, respectively. A mobile and non-invasive measurement system would improve the microbial security of fresh meat. PMID:26773794

  7. Non-destructive Assay Measurements Using the RPI Lead Slowing Down Spectrometer

    SciTech Connect

    Becker, Bjorn; Weltz, Adam; Kulisek, Jonathan A.; Thompson, J. T.; Thompson, N.; Danon, Yaron

    2013-10-01

    The use of a Lead Slowing-Down Spectrometer (LSDS) is consid- ered as a possible option for non-destructive assay of fissile material of used nuclear fuel. The primary objective is to quantify the 239Pu and 235U fissile content via a direct measurement, distinguishing them through their characteristic fission spectra in the LSDS. In this pa- per, we present several assay measurements performed at the Rensse- laer Polytechnic Institute (RPI) to demonstrate the feasibility of such a method and to provide benchmark experiments for Monte Carlo cal- culations of the assay system. A fresh UOX fuel rod from the RPI Criticality Research Facility, a 239PuBe source and several highly en- riched 235U discs were assayed in the LSDS. The characteristic fission spectra were measured with 238U and 232Th threshold fission cham- bers, which are only sensitive to fission neutron with energy above the threshold. Despite the constant neutron and gamma background from the PuBe source and the intense interrogation neutron flux, the LSDS system was able to measure the characteristic 235U and 239Pu responses. All measurements were compared to Monte Carlo simula- tions. It was shown that the available simulation tools and models are well suited to simulate the assay, and that it is possible to calculate the absolute count rate in all investigated cases.

  8. Non-destructive inspection using HTS SQUID on aluminum liner covered by CFRP

    NASA Astrophysics Data System (ADS)

    Hatsukade, Y.; Yotsugi, K.; Sakaguchi, Y.; Tanaka, S.

    2007-10-01

    An eddy-current-based SQUID non-destructive inspection (NDI) system to detect deep-lying cracks in multi-layer composite-Al vessels was developed taking advantage of the uncontested sensitivity of HTS-SQUID in low-frequency range. An HTS-SQUID gradiometer was mounted in a pulse tube cryocooler. A pair of differential coils with C-shaped ferrite cores was employed to induce an enhanced eddy current in an Al vessel wrapped in a carbon fiber reinforced plastic (CFRP) cover. Ellipsoidal dome-shaped Al liners containing through cracks, which were made by pressure cycle tests, in the CFRP covers with total thickness of 6 mm (CFPR 3 mm, and Al 3 mm) were inspected by the system. While inducing eddy currents in the vessels with excitation fields at 100 Hz or 7 kHz, the vessels were rotated under the HTS-SQUID. Above the cracks, anomalous signals due to the cracks were clearly detected at both frequencies. These results suggested the SQUID-NDI technique would be a possible candidate for inspection of high-pressure multi-layer composite-Al vessels.

  9. Non-destructive characterization of microdamage in cortical bone using low field pulsed NMR.

    PubMed

    Nicolella, Daniel P; Ni, Qingwen; Chan, Kwai S

    2011-04-01

    The microcracking and damage accumulation process in human cortical bone was characterized by performing cyclic loading under four-point bending at ambient temperature. A non-destructive nuclear magnetic resonance (NMR) spin-spin (T(2)) relaxation technique was applied to quantify the apparent changes in bone porosity as a function of cyclic loading and prior damage accumulation, first to unloaded cortical bone to quantify the initial porosity and then to fatigued cortical bone that was subjected to cyclic loading to various levels of modulus degradation and microdamage in the form of microcracks. The NMR T(2) relaxation time and amplitude data of the fatigued bone were compared against the undamaged state. The difference in the T(2) relaxation time data was taken as a measure of the increase in pore size, bone porosity or microcrack density due to microdamage induced by cyclic loading. A procedure was developed to deduce the number and size distributions of microcracks formed in cortical bone. Serial sectioning of the fatigued bone showed the formation of microcracks along the cement lines or within the interstitial tissue. The results on the evolution of microdamage derived from NMR measurements were verified by independent experimental measurements of microcrack density using histological characterization techniques. The size distribution and population of the microcracks were then utilized in conjunction with an analytical model to predict the degradation of the elastic modulus of cortical bone as a function of damage accumulation. PMID:21316626

  10. NON-DESTRUCTIVE RADIOCARBON DATING: NATURALLY MUMMIFIED INFANT BUNDLE FROM SW TEXAS

    SciTech Connect

    Steelman, K L; Rowe, M W; Turpin, S A; Guilderson, T P; Nightengale, L

    2004-09-07

    Plasma oxidation was used to obtain radiocarbon dates on six different materials from a naturally mummified baby bundle from the Lower Pecos River region of southwest Texas. This bundle was selected because it was thought to represent a single event and would illustrate the accuracy and precision of the plasma oxidation method. Five of the materials were clearly components of the original bundle with 13 dates combined to yield a weighted average of 2135 {+-} 11 B.P. Six dates from a wooden stick of Desert Ash averaged 939 {+-} 14 B.P., indicating that this artifact was not part of the original burial. Plasma oxidation is shown to be a virtually non-destructive alternative to combustion. Because only sub-milligram amounts of material are removed from an artifact over its exposed surface, no visible change in fragile materials has been observed, even under magnification. The method is best applied when natural organic contamination is unlikely and serious consideration of this issue is needed in all cases. If organic contamination is present, it will have to be removed before plasma oxidation to obtain accurate radiocarbon dates.