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Sample records for niobium 110

  1. TEM and SIMS Analysis of (100), (110), and (111) Single Crystal Niobium

    SciTech Connect

    Batchelor, A. D.; Stevie, F. A.; Leonard, D. N.; Russell, P. E.; Griffis, D. P.; Myneni, G. R.

    2007-08-09

    Single crystal niobium specimens of (100), (110) and (111) crystal orientations have been analyzed using TEM and SIMS. The TEM specimens were prepared using Focused Ion Beam (FIB) and show niobium oxide thicknesses ranging from 4.9 to 8.3 nm for the three specimens after buffer chemical polishing. The oxide layers appear uniform and no significant sub-oxide region was noted. SIMS analysis was made for all three orientations on hydrogen, carbon, and oxygen before and after heat treatments at 90, 600, and 1250 deg. C. Hydrogen is at a high level between the oxide layer and niobium, but at a relatively low level in the oxide. No high oxygen concentration region was noted in the niobium below the oxide. C contamination on the surface is detected mainly at the surface. Analysis after heat treatments showed some decrease in hydrogen after the 600 deg. C heat treatment, and significant oxidation of the niobium after the 1250 deg. C heat treatment.

  2. Response to Comment on '#28;Twin Symmetry Texture of Energetically Condensed 2 Niobium Thin Films on Sapphire Substrate' #29; [J. Appl. Phys. 110, 033523(2011)

    SciTech Connect

    Xin Zhao, Charles Reece, Phillips Larry, Mahadevan Krishnan, Kang Seo

    2012-07-01

    Welander commented that in our article [J. Appl. Phys. 110, 033523(2011)] , Zhao et al claim to have found a new three-dimensional (3D) relationship for niobium-on-sapphire epitaxy”. Welander might have misunderstood the purpose of our article, which was to show that energetic condensation of Nb on sapphire drives crystal growth that is quite distinct from the type of epitaxy encountered in lower energy deposition. Welander is correct about the misidentified crystal-directions in the top-view sapphire lattice (Fig.4[ref.1]). He is also correct about the misorientation of the pole figures in Fig4[ref.1]. In Fig.1 of this response, we have corrected these errors. Perhaps because of these errors, Welander misconstrued our discussion of the Nb crystal growth as claiming a new 3D registry. That was not our intention. Rather, we wished to highlight the role of energetic condensation that drives low-defect crystal growth by a combination of non-equilibrium sub-plantation that disturbs the substrate lattice and thermal annealing that annihilates defects and promotes large-grain crystal growth.

  3. Process for recovering niobium from uranium-niobium alloys

    DOEpatents

    Wallace, Steven A.; Creech, Edward T.; Northcutt, Walter G.

    1983-01-01

    Niobium is recovered from scrap uranium-niobium alloy by melting the scrap with tin, solidifying the billet thus formed, heating the billet to combine niobium with tin therein, placing the billet in hydrochloric acid to dissolve the uranium and leave an insoluble residue of niobium stannide, then separating the niobium stannide from the acid.

  4. Process for recovering niobium from uranium-niobium alloys

    SciTech Connect

    Wallace, S.A.; Creech, E.T.; Northcutt, W.G.

    1983-11-01

    Niobium is recovered from scrap uranium-niobium alloy by melting the scrap with tin, solidifying the billet thus formed, heating the billet to combine niobium with tin therein, placing the billet in hydrochloric acid to dissolve the uranium and leave an insoluble residue of niobium stannide, then separating the niobium stannide from the acid.

  5. Passivated niobium cavities

    DOEpatents

    Myneni, Ganapati Rao; Hjorvarsson, Bjorgvin; Ciovati, Gianluigi

    2006-12-19

    A niobium cavity exhibiting high quality factors at high gradients is provided by treating a niobium cavity through a process comprising: 1) removing surface oxides by plasma etching or a similar process; 2) removing hydrogen or other gases absorbed in the bulk niobium by high temperature treatment of the cavity under ultra high vacuum to achieve hydrogen outgassing; and 3) assuring the long term chemical stability of the niobium cavity by applying a passivating layer of a superconducting material having a superconducting transition temperature higher than niobium thereby reducing losses from electron (cooper pair) scattering in the near surface region of the interior of the niobium cavity. According to a preferred embodiment, the passivating layer comprises niobium nitride (NbN) applied by reactive sputtering.

  6. Process for recovering niobium from uranium-niobium alloys

    DOEpatents

    Wallace, S.A.; Creech, E.T.; Northcutt, W.G.

    1982-09-27

    Niobium is recovered from scrap uranium-niobium alloy by melting the scrap with tin, solidifying the billet thus formed, heating the billet to combine niobium with tin therein, placing the billet in hydrochloric acid to dissolve the uranium and form a precipitate of niobium stannide, then separating the precipitate from the acid.

  7. Melting And Purification Of Niobium

    SciTech Connect

    Salles Moura, Hernane R.; Moura, Lourenco de

    2007-08-09

    The aspects involved in the purification of niobium in Electron Beam Furnaces will be outlined and correlated with practical experience accumulated over 17 years of continuously producing high purity niobium metal and niobium-zirconium ingots at CBMM, meeting the needs for a wide range of uses. This paper also reports some comments regarding raw material requirements, the experience on cold hearth operation melting niobium and the production of large grains niobium ingots by CBMM with some comments of their main characteristics.

  8. Melting And Purification Of Niobium

    NASA Astrophysics Data System (ADS)

    Moura, Hernane R. Salles; de Moura, Lourenço

    2007-08-01

    The aspects involved in the purification of niobium in Electron Beam Furnaces will be outlined and correlated with practical experience accumulated over 17 years of continuously producing high purity niobium metal and niobium-zirconium ingots at CBMM, meeting the needs for a wide range of uses. This paper also reports some comments regarding raw material requirements, the experience on cold hearth operation melting niobium and the production of large grains niobium ingots by CBMM with some comments of their main characteristics.

  9. Corrosion behavior of niobium coated 304 stainless steel in acid solution

    NASA Astrophysics Data System (ADS)

    Pan, T. J.; Chen, Y.; Zhang, B.; Hu, J.; Li, C.

    2016-04-01

    The niobium coating is fabricated on the surface of AISI Type 304 stainless steel (304SS) by using a high energy micro arc alloying technique in order to improvecorrosion resistance of the steel against acidic environments. The electrochemical corrosion resistance of the niobium coating in 0.7 M sulfuric acid solutions is evaluated by electrochemical impedance spectroscopy, potentiodynamic polarization and the open circuit potential versus time. Electrochemical measurements indicate that the niobium coating increases the free corrosion potential of the substrate by 110 mV and a reduction in the corrosion rate by two orders of magnitude compared to the substrate alone. The niobium coating maintains large impedance and effectively offers good protection for the substrate during the long-term exposure tests, which is mainly ascribed to the niobium coating acting inhibiting permeation of corrosive species. Finally, the corresponding electrochemical impedance models are proposed to elucidate the corrosion resistance behavior of the niobium coating in acid solutions.

  10. Introduction to Ingot Niobium

    SciTech Connect

    Ganapati Rao Mynen, Andrew Hutton

    2011-03-01

    Superconducting radiofrequency (SRF) technology using niobium accelerating cavities was first applied at large scale in the recirculating electron linear accelerator CEBAF—the Continuous Electron Beam Accelerator Facility in Newport News, Virginia, USA, at what is now called Thomas Jefferson National Accelerator Facility, or Jefferson Lab. Building on the high quality factors and peak magnetic fields found in low residual resistivity ratio (low-RRR) solid niobium in the 1970s, Jefferson Lab has reintroduced ingot niobium technology. High tantalum content in ingot niobium is not expected to negatively impact cavity performance, but will reduce the cost of accelerator structures considerably. Optimized low-cost CW linear accelerators built with ingot niobium will show the way for future R&D and industrial applications. This paper portrays the Jefferson Lab SRF context, reviews the early history of ingot niobium technology from over a third of a century ago, explains the technical advantages of that technology's recent reintroduction, and presents the outlook for further development.

  11. Introduction to Ingot Niobium

    SciTech Connect

    Myneni, Ganapati Rao; Hutton, Andrew

    2011-03-31

    Superconducting radiofrequency (SRF) technology using niobium accelerating cavities was first applied at large scale in the recirculating electron linear accelerator CEBAF--the Continuous Electron Beam Accelerator Facility in Newport News, Virginia, USA, at what is now called Thomas Jefferson National Accelerator Facility, or Jefferson Lab. Building on the high quality factors and peak magnetic fields found in low residual resistivity ratio (low-RRR) solid niobium in the 1970s, Jefferson Lab has reintroduced ingot niobium technology. High tantalum content in ingot niobium is not expected to negatively impact cavity performance, but will reduce the cost of accelerator structures considerably. Optimized low-cost CW linear accelerators built with ingot niobium will show the way for future R and D and industrial applications. This paper portrays the Jefferson Lab SRF context, reviews the early history of ingot niobium technology from over a third of a century ago, explains the technical advantages of that technology's recent reintroduction, and presents the outlook for further development.

  12. Proton in SRF Niobium

    NASA Astrophysics Data System (ADS)

    Wallace, John Paul

    2011-03-01

    Hydrogen is a difficult impurity to physically deal with in superconducting radio frequency (SRF) niobium, therefore, its properties in the metals should be well understood to allow the metal's superconducting properties to be optimized for minimum loss in the construction of resonant accelerator cavities. It is known that hydrogen is a paramagnetic impurity in niobium from NMR studies. This paramagnetism and its effect on superconducting properties are important to understand. To that end analytical induction measurements aimed at isolating the magnetic properties of hydrogen in SRF niobium are introduced along with optical reflection spectroscopy which is also sensitive to the presence of hydrogen. From the variety, magnitude and rapid kinetics found in the optical and magnetic properties of niobium contaminated with hydrogen forced a search for an atomic model. This yielded quantum mechanical description that correctly generates the activation energy for diffusion of the proton and its isotopes not only in niobium but the remaining metals for which data is available. This interpretation provides a frame work for understanding the individual and collective behavior of protons in metals.

  13. Proton in SRF Niobium

    SciTech Connect

    Wallace, John Paul

    2011-03-31

    Hydrogen is a difficult impurity to physically deal with in superconducting radio frequency (SRF) niobium, therefore, its properties in the metals should be well understood to allow the metal's superconducting properties to be optimized for minimum loss in the construction of resonant accelerator cavities. It is known that hydrogen is a paramagnetic impurity in niobium from NMR studies. This paramagnetism and its effect on superconducting properties are important to understand. To that end analytical induction measurements aimed at isolating the magnetic properties of hydrogen in SRF niobium are introduced along with optical reflection spectroscopy which is also sensitive to the presence of hydrogen. From the variety, magnitude and rapid kinetics found in the optical and magnetic properties of niobium contaminated with hydrogen forced a search for an atomic model. This yielded quantum mechanical description that correctly generates the activation energy for diffusion of the proton and its isotopes not only in niobium but the remaining metals for which data is available. This interpretation provides a frame work for understanding the individual and collective behavior of protons in metals.

  14. METHOD OF PRODUCING NIOBIUM METAL

    DOEpatents

    Wilhelm, H.A.; Stevens, E.R.

    1960-05-24

    A process is given for preparing ductile niobium metal by the reduction of niobium pentoxide with carbon. The invention resides in the addition, to the reaction mass, of from 0.05 to 0.4 atom of titanium (in the form of metallic titanium, titanium carbide, and/or titanium oxide) per one mole of niobium pentoxide. The mixture is heated under subatmospheric pressure to above 1300 deg C but below the melting point of niobium, and the carbon- and oxygen-free niobium sponge obtained is cooled under reduced pressure.

  15. Method of surface preparation of niobium

    SciTech Connect

    Srinivasan-Rao, Triveni; Schill, John F.

    2003-01-01

    The present invention is for a method of preparing a surface of niobium. The preparation method includes polishing, cleaning, baking and irradiating the niobium surface whereby the resulting niobium surface has a high quantum efficiency.

  16. Vapor deposition of hardened niobium

    DOEpatents

    Blocher, Jr., John M.; Veigel, Neil D.; Landrigan, Richard B.

    1983-04-19

    A method of coating ceramic nuclear fuel particles containing a major amount of an actinide ceramic in which the particles are placed in a fluidized bed maintained at ca. 800.degree. to ca. 900.degree. C., and niobium pentachloride vapor and carbon tetrachloride vapor are led into the bed, whereby niobium metal is deposited on the particles and carbon is deposited interstitially within the niobium. Coating apparatus used in the method is also disclosed.

  17. Large grain cavities from pure niobium ingot

    DOEpatents

    Myneni, Ganapati Rao; Kneisel, Peter; Cameiro, Tadeu

    2012-03-06

    Niobium cavities are fabricated by the drawing and ironing of as cast niobium ingot slices rather than from cold rolled niobium sheet. This method results in the production of niobium cavities having a minimum of grain boundaries at a significantly reduced cost as compared to the production of such structures from cold rolled sheet.

  18. NIOBIUM-TANTALUM SEPARATION

    DOEpatents

    Wilhelm, H.A.; Foos, R.A.

    1959-01-27

    The usual method for the separation of tantalum and niobium consists of a selective solvent extraction from an aqueous hydrofluoric acid solution of the metals. A difficulty encountered in this process is the fact that the corrosion problems associated with hydrofluoric acid are serious. It has been found that the corrosion caused by the hydrofluoric acid may be substantially reduced by adding to the acidic solution an amine, such as phenyl diethanolamine or aniline, and adjusting pH value to between 4 and 6.

  19. Niobium Production at Tokyo Denkai

    SciTech Connect

    Umezawa, Hiroaki

    2011-03-31

    In recent years, single-crystal/large-grain niobium has received much attention. It has the following advantages: rolling-annealing is unnecessary, and superconducting cavities made from large-grain niobium discs may not require electropolishing. However, to obtain a large-grain disc, an ingot must be sliced using a saw and finished smooth by using a lathe. Slicing a disc takes several hours and produces niobium shavings. KEK, Tokyo Denkai, and TKX Corporation have developed a new niobium ingot slicing technique, and Tokyo Denkai has installed the slicing machine. This study describes the new ingot slicing technology, which ensures state-of-the-art productivity for the superconducting radio frequency (SRF) cavity material industry.

  20. Niobium and tantalum: indispensable twins

    USGS Publications Warehouse

    Schulz, Klaus; Papp, John

    2014-01-01

    Niobium and tantalum are transition metals almost always paired together in nature. These “twins” are difficult to separate because of their shared physical and chemical properties. In 1801, English chemist Charles Hatchett uncovered an unknown element in a mineral sample of columbite; John Winthrop found the sample in a Massachusetts mine and sent it to the British Museum in London in 1734. The name columbium, which Hatchet named the new element, came from the poetic name for North America—Columbia—and was used interchangeably for niobium until 1949, when the name niobium became official. Swedish scientist Anders Ekberg discovered tantalum in 1802, but it was confused with niobium, because of their twinned properties, until 1864, when it was recognized as a separate element. Niobium is a lustrous, gray, ductile metal with a high melting point, relatively low density, and superconductor properties. Tantalum is a dark blue-gray, dense, ductile, very hard, and easily fabricated metal. It is highly conductive to heat and electricity and renowned for its resistance to acidic corrosion. These special properties determine their primary uses and make niobium and tantalum indispensable.

  1. METHOD FOR COATING GRAPHITE WITH NIOBIUM CARBIDE

    DOEpatents

    Kane, J.S.; Carpenter, J.H.; Krikorian, O.H.

    1962-01-16

    A method is given for coating graphite with a hard, tenacious layer of niobium carbide up to 30 mils or more thick. The method makes use of the discovery that niobium metal, if degassed and heated rapidly below the carburization temperature in contact with graphite, spreads, wets, and penetrates the graphite without carburization. The method includes the obvious steps of physically contacting niobium powders or other physical forms of niobium with graphite, degassing the assembly below the niobium melting point, e.g., 1400 deg C, heating to about 2200 to 2400 deg C within about 15 minutes while outgassing at a high volume throughput, and thereafter carburizing the niobium. (AEC)

  2. A Single Crystal Niobium RF Cavity of the TESLA Shape

    SciTech Connect

    Singer, W.; Singer, X.; Kneisel, P.

    2007-08-09

    A fabrication method for single crystal niobium cavities of the TESLA shape was proposed on the basis of metallographic investigations and electron beam welding tests on niobium single crystals. These tests showed that a cavity can be produced without grain boundaries even in the welding area. An appropriate annealing allows the outgassing of hydrogen and stress relaxation of the material without destruction of the single crystal. A prototype single crystal single cell cavity was build. An accelerating gradient of 37.5 MV/m was reached after approximately 110 {mu}m of Buffered Chemical Polishing (BCP) and in situ baking at 120 deg. C for 6 hrs with a quality factor exceeding 2x1010 at 1.8 K. The developed fabrication method can be extended to fabrication of multi cell cavities.

  3. A Single Crystal Niobium RF Cavity of the TESLA Shape

    SciTech Connect

    W. Singer; X. Singer; P. Kneisel

    2007-09-01

    A fabrication method for single crystal niobium cavities of the TESLA shape was proposed on the basis of metallographic investigations and electron beam welding tests on niobium single crystals. These tests showed that a cavity can be produced without grain boundaries even in the welding area. An appropriate annealing allows the outgassing of hydrogen and stress relaxation of the material without destruction of the single crystal. A prototype single crystal single cell cavity was built. An accelerating gradient of 37.5 MV/m was reached after approximately 110 mu-m of Buffered Chanical Polishing (BCP) and in situ baking at 120°C for 6 hrs with a quality factor exceeding 2x1010 at 1.8 K. The developed fabrication method can be extended to fabrication of multi cell cavities.

  4. Direct Flotation of Niobium Oxide Minerals from Carbonatite Niobium Ores

    NASA Astrophysics Data System (ADS)

    Ni, Xiao

    Currently the recovery of niobium oxide minerals from carbonatite niobium ores relies on the use of non-selective cationic collectors. This leads to complicated process flowsheets involving multiple desliming and multiple reverse flotation stages, and low niobium recovery. In this research, anionic collectors that are capable of strong chemisorption on the niobium minerals were studied with the objective of directly floating the niobium oxide minerals from the carbonatite ores. In the flotation of both high purity minerals and Niobec ores, it was shown that the combination of hydroxamic acid and sodium metaphosphate was an effective reagent scheme for the direct flotation of niobium oxide from its ores. Batch flotation on the Niobec Mill Feed showed that over 95% of niobium oxide was recovered into a rougher concentrate that was less than 47% of the original feed mass. Preliminary cleaning tests showed that the reagent scheme could also be used to upgrade the rougher concentrate, although the depression of iron oxide minerals required further study. X-ray photoelectron spectroscopic (XPS) measurement results confirm that OHA (octyl hydroxamic acid) could chemisorb on pyrochlore surface while only physically adsorb on calcite, judging by the chemical shifts of electron binding energies in the elements in both OHA and the mineral surfaces. When hydroxamic acid was adsorbed on calcite surface, the binding energies of the N 1s electrons, at 400.3 eV, did not shift. However, after adsorption on pyrochlore, the N 1s binding energy peak split into two peaks, one at a binding energy of around 399 eV, representing chemically adsorbed OHA, the other at between 400 and 401 eV. The experimental data suggested a strong chemisorption of the OHA on pyrochlore surface in the form of a vertical head-on orientation of the OHA molecules so that the pyrochlore was strongly hydrophobized even at low OHA concentrations, followed by possibly randomly oriented physisorbed OHA molecules

  5. Niobium - Proceedings of the international symposium

    SciTech Connect

    Stuart, H.

    1984-01-01

    This book presents the papers given at a symposium on niobium. Topics considered at the symposium included niobium mining, ore processing, uses, fabrication, microstructure, mechanical properties, physical properties, corrosion, physical radiation effects, and marketing.

  6. Spectrophotometric determination of niobium and its application to niobium-stabilized stainless steel.

    PubMed

    Dutta, R K; Banerjee, S

    1974-10-01

    A spectrophotometric method is described for the determination of niobium by means of its reaction with tannin and thioglycollic acid. The yellow-orange colour developed with the reagent mixture at pH 4 is measured at 410-420 nm and obeys Beer's law between 0.5 and 10 ppm niobium. The method is suitable for the determination of niobium in niobium-stabilized stainless steel and other types of steels containing niobium, but a prior separation of niobium is necessary. Titanium interferes even in traces. PMID:18961571

  7. 10 CFR 110.110 - Default.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Default. 110.110 Section 110.110 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Hearings § 110.110 Default. When a participant fails to act within a specified time, the presiding officer may consider him in default, issue...

  8. Superconductive niobium films coating carbon nanotube fibers

    NASA Astrophysics Data System (ADS)

    Salvato, M.; Lucci, M.; Ottaviani, I.; Cirillo, M.; Behabtu, N.; Young, C. C.; Pasquali, M.; Vecchione, A.; Fittipaldi, R.; Corato, V.

    2014-11-01

    Superconducting niobium (Nb) has been successfully obtained by sputter deposition on carbon nanotube fibers. The transport properties of the niobium coating the fibers are compared to those of niobium thin films deposited on oxidized Si substrates during the same deposition run. For niobium films with thicknesses above 300 nm, the niobium coating the fibers and the thin films show similar normal state and superconducting properties with critical current density, measured at T = 4.2 K, of the order of 105 A cm-2. Thinner niobium layers coating the fibers also show the onset of the superconducting transition in the resistivity versus temperature dependence, but zero resistance is not observed down to T = 1 K. We evidence by scanning electron microscopy (SEM) and current-voltage measurements that the granular structure of the samples is the main reason for the lack of true global superconductivity for thicknesses below 300 nm.

  9. Investigation of active slip systems in high purity single crystal niobium

    NASA Astrophysics Data System (ADS)

    Baars, Derek

    The superconducting radio-frequency (SRF) community uses high purity niobium to manufacture SRF cavities for a variety of accelerator applications. Cavities are either made from large-grain sheets cut directly from the ingot and formed, or the ingot microstructure is broken down to form polycrystalline sheets or tubes. Reducing the number of costly electron beam welds to assemble the cavities is also desired. A greater understanding of the active slip systems and their relation to subsequent dislocation substructure would be of use in all these areas, to better understand how large grain niobium deforms and to develop more accurate computational models that will aid in the design and use of more cost-effective forming methods. Studies of slip in high-purity niobium suggest that temperature, material purity, and crystal orientation affect which slip systems are active during deformation, though have not examined the somewhat lesser purity niobium used for SRF cavities. As a step toward these goals, two sets of SRF-purity single crystal niobium samples were deformed to 40% strain in tension at room temperature. The first set was cut and welded back together. The second set consisted of deliberately orientated samples that resolved shear stress onto desired slip systems to evaluate different combinations of slip. Determining likely active slip systems was complex, though the evidence suggests that {112} slip may be dominant at yield at room temperature as suggested by theory, though {110} slip could not be ruled out.

  10. Dissipative hydride precipitates in superconducting niobium cavities

    SciTech Connect

    Romanenko, A.; Cooley, L.D.; Ciovati, G.; Wu, G.; /Argonne

    2011-10-01

    We report the first direct observation of the microstructural features exhibiting RF losses at high surface magnetic fields of above 100 mT in field emission free superconducting niobium cavities. The lossy areas were identified by advanced thermometry. Surface investigations using different techniques were carried out on cutout samples from lossy areas and showed the presence of dendritic niobium hydrides. This finding has possible implications to the mechanisms of RF losses in superconducting niobium at all field levels.

  11. Process for alloying uranium and niobium

    DOEpatents

    Holcombe, Cressie E.; Northcutt, Jr., Walter G.; Masters, David R.; Chapman, Lloyd R.

    1991-01-01

    Alloys such as U-6Nb are prepared by forming a stacked sandwich array of uraniun sheets and niobium powder disposed in layers between the sheets, heating the array in a vacuum induction melting furnace to a temperature such as to melt the uranium, holding the resulting mixture at a temperature above the melting point of uranium until the niobium dissolves in the uranium, and casting the uranium-niobium solution. Compositional uniformity in the alloy product is enabled by use of the sandwich structure of uranium sheets and niobium powder.

  12. Niobium content of soils from West Africa

    USGS Publications Warehouse

    Grimaldi, F.S.; Berger, I.A.

    1961-01-01

    Analysis of twenty lateritic soil samples from West Africa has shown them to contain an average 24 p.p.m. of niobium; four similar samples taken from within a few miles from a niobium deposit contain from 79 to 87 p.p.m. niobium. It has been shown that as the aluminum content of the soils increases, the following depletion sequence is obtained: Si > Nb > Al = Fe The data indicate that, in general, high enrichments of niobium are not to be expected in lateritic soils. ?? 1961.

  13. Process for alloying uranium and niobium

    SciTech Connect

    Holcombe, C.E.; Northcutt, W.G.; Masters, D.R.; Chapman, L.R.

    1990-12-31

    Alloys such as U-6Nb are prepared by forming a stacked sandwich array of uranium sheets and niobium powder disposed in layers between the sheets, heating the array in a vacuum induction melting furnace to a temperature such as to melt the uranium, holding the resulting mixture at a temperature above the melting point of uranium until the niobium dissolves in the uranium, and casting the uranium-niobium solution. Compositional uniformity in the alloy product is enabled by use of the sandwich structure of uranium sheets and niobium powder.

  14. Seamless/bonded niobium cavities

    NASA Astrophysics Data System (ADS)

    Singer, W.

    2006-07-01

    Technological aspects and performance of seamless cavities produced by hydroforming are presented. Problems related to the fabrication of seamless cavities from bulk niobium are mainly solved thanks to the progress of the last years. The highest achieved accelerating gradients are comparable for both seamless and welded versions (ca. 40 MV/m) Nevertheless further development of seamless cavities is desirable in order to avoid the careful preparation of parts for welding and get reliable statistic. Fabrication of NbCu clad cavities from bimetallic tubes is an interesting option that gives new opportunity to the seamless technique. On the one hand it allows reducing the niobium costs contribution; on the other hand it increases the thermal stability of the cavity. The highest accelerating gradient achieved on seamless NbCu clad single cell cavities (ca. 40 MV/m) is comparable to the one reached on bulk Nb cavities. Fabrication of multi-cell NbCu cavities by hydroforming was recently proven.

  15. SRF MATERIALS OTHER THAN NIOBIUM

    SciTech Connect

    Valente, Anne-Marie

    2008-02-12

    For the past three decades, bulk niobium has been the material of choice for SRF cavity applications. Alternative materials, mainly Nb compounds and A15 compounds have been investigated with moderate effort in the past. In the recent years, RF cavity performance has approached the theoretical limit for bulk niobium. For further improvement of RF cavity performance for future accelerator projects, research interest is renewed towards alternative materials to niobium. A few laboratories around the world are now investigating superconductors with higher transition temperature Tc for application to SRF cavities. This paper gives an overview of the results obtained and challenges encountered for Nb compounds and A15 compounds, as well as for MgB2, for SRF cavity applications. An interesting alternative has been recently proposed by Alex Gurevich with the Superconductor-Insulator-Superconductor multilayer approach. This could potentially lead to further improvement in RF cavity performance using the benefit of the higher critical field Hc of higher-Tc superconductors without being limited with their lower Hc1.

  16. Purification of Niobium by Electron Beam Melting

    NASA Astrophysics Data System (ADS)

    Sankar, M.; Mirji, K. V.; Prasad, V. V. Satya; Baligidad, R. G.; Gokhale, A. A.

    2016-06-01

    Pure niobium metal, produced by alumino-thermic reduction of niobium oxide, contains various impurities which need to be reduced to acceptable levels to obtain aerospace grade purity. In the present work, an attempt has been made to refine niobium metals by electron beam drip melting technique to achieve purity confirming to the ASTM standard. Input power to the electron gun and melt rate were varied to observe their combined effect on extend of refining and loss of niobium. Electron beam (EB) melting is shown to reduce alkali metals, trace elements and interstitial impurities well below the specified limits. The reduction in the impurities during EB melting is attributed to evaporation and degassing due to the combined effect of high vacuum and high melt surface temperature. The % removal of interstitial impurities is essentially a function of melt rate and input power. As the melt rate decreases or input power increases, the impurity levels in the solidified niobium ingot decrease. The EB refining process is also accompanied by considerable amount of niobium loss, which is attributed to evaporation of pure niobium and niobium sub-oxide. Like other impurities, Nb loss increases with decreasing melt rate or increase in input power.

  17. Method of nitriding niobium to form a superconducting surface

    DOEpatents

    Kelley, Michael J.; Klopf, John Michael; Singaravelu, Senthilaraja

    2014-08-19

    A method of forming a delta niobium nitride .delta.-NbN layer on the surface of a niobium object including cleaning the surface of the niobium object; providing a treatment chamber; placing the niobium object in the treatment chamber; evacuating the chamber; passing pure nitrogen into the treatment chamber; focusing a laser spot on the niobium object; delivering laser fluences at the laser spot until the surface of the niobium object reaches above its boiling temperature; and rastering the laser spot over the surface of the niobium object.

  18. Buffered Electrochemical Polishing of Niobium

    SciTech Connect

    Gianluigi Ciovati; Tian, Hui; Corcoran, Sean

    2011-03-01

    The standard preparation of superconducting radio-frequency (SRF) cavities made of pure niobium include the removal of a 'damaged' surface layer, by buffered chemical polishing (BCP) or electropolishing (EP), after the cavities are formed. The performance of the cavities is characterized by a sharp degradation of the quality factor when the surface magnetic field exceeds about 90 mT, a phenomenon referred to as 'Q-drop.' In cavities made of polycrystalline fine grain (ASTM 5) niobium, the Q-drop can be significantly reduced by a low-temperature (? 120 °C) 'in-situ' baking of the cavity if the chemical treatment was EP rather than BCP. As part of the effort to understand this phenomenon, we investigated the effect of introducing a polarization potential during buffered chemical polishing, creating a process which is between the standard BCP and EP. While preliminary results on the application of this process to Nb cavities have been previously reported, in this contribution we focus on the characterization of this novel electrochemical process by measuring polarization curves, etching rates, surface finish, electrochemical impedance and the effects of temperature and electrolyte composition. In particular, it is shown that the anodic potential of Nb during BCP reduces the etching rate and improves the surface finish.

  19. A Terminally Bound Niobium Methylidyne.

    PubMed

    Kurogi, Takashi; Carroll, Patrick J; Mindiola, Daniel J

    2016-04-01

    Complex (PNP)Nb(CH3)2(OAr) (PNP = N[2-P(i)Pr2-4-methylphenyl]2(-), Ar = 2,6-(i)Pr2C6H3), prepared from treatment of (PNP)NbCl3 with NaOAr followed by 2 equiv of H3CMgCl, can be oxidized with [FeCp2][OTf] to afford (PNP)Nb(CH3)2(OAr)(OTf). While photolysis of the latter resulted in formation of a rare example of a niobium methylidene, (PNP)Nb═CH2(OAr)(OTf), treatment of the dimethyl triflate precursor with the ylide H2CPPh3 produced the mononuclear group 5 methylidyne complex, (PNP)Nb≡CH(OAr). Adding a Brønsted base to (PNP)Nb═CH2(OAr)(OTf) also resulted in formation of the methylidyne. Solid-state structural analysis confirms both methylidene and methylidyne moieties to be terminal, having very short Nb-C distances of 1.963(2) and 1.820(2) Å, respectively. It is also shown that methylidyne for nitride cross-metathesis between (PNP)Nb≡CH(OAr) and NCR (R = tert-butyl or 1-adamantyl) results in formation of a neutral and mononuclear niobium nitride, (PNP)Nb≡N(OAr), along with the terminal alkyne HC≡CR. PMID:26977892

  20. Method for etching thin films of niobium and niobium-containing compounds for preparing superconductive circuits

    DOEpatents

    Kampwirth, Robert T.; Schuller, Ivan K.; Falco, Charles M.

    1981-01-01

    An improved method of preparing thin film superconducting electrical circuits of niobium or niobium compounds in which a thin film of the niobium or niobium compound is applied to a nonconductive substrate, and covered with a layer of photosensitive material. The sensitive material is in turn covered with a circuit pattern exposed and developed to form a mask of the circuit in photoresistive material on the surface of the film. The unmasked excess niobium film is removed by contacting the substrate with an aqueous etching solution of nitric acid, sulfuric acid and hydrogen fluoride, which will rapidly etch the niobium compound without undercutting the photoresist. A modification of the etching solution will permit thin films to be lifted from the substrate without further etching.

  1. The oxidation behavior and protection of niobium

    NASA Astrophysics Data System (ADS)

    Perkins, Roger A.; Meier, Gerald H.

    1990-08-01

    Despite years of effort, researchers have been unable to develop a high-temperature niobium-base alloy with the ability to form a protective oxide scale. Although some of the alloys tested have potentially useful properties, the alloying elements usually act to the detriment of at least one property. Currently, niobium-base alloys are protected from high-temperature oxidation with a highly reliable silicide coating. This article reviews the efforts to develop oxidation-resistant alloys and summarizes the results of recent research on oxidation-resistant niobium-base intermetallics.

  2. Effect of hydrogen on surface of niobium

    SciTech Connect

    Gadgil, V.J.; Keim, E.G.

    1998-12-31

    Niobium single crystals are used as substrate material for constructing superconducting quantum interference device of SQUID. The use of niobium is prompted by the fact that it is a low {Tc} metallic superconductor. In order to fabricate the device the surface of the crystal has to be polished flat. This is achieved by combination of mechanical polishing and electrochemical polishing. It has been reported that during electrochemical polishing hydrogen can enter the material forming Niobium hydrides. These can result in surface roughening of a magnitude greater than the thickness of the films subsequently deposited. This leads to failure of the films. The problem can be solved by annealing the material at 300 C to remove any hydrogen that might be present. However it is phenomenologically interesting to study the effect of electrochemical hydrogen charging on the surface of Niobium.

  3. Degreasing and cleaning superconducting RF Niobium cavities

    SciTech Connect

    Rauchmiller, Michael; Kellett, Ron; /Fermilab

    2011-09-01

    The purpose and scope of this report is to detail the steps necessary for degreasing and cleaning of superconducting RF Niobium cavities in the A0 clean room. It lists the required equipment and the cleaning procedure.

  4. Recovery of niobium from irradiated targets

    SciTech Connect

    Phillips, D.R.; Jamriska, D.J. Sr.; Hamilton, V.T.

    1994-03-22

    A process for selective separation of niobium from proton irradiated molybdenum targets is provided and includes dissolving the molybdenum target in a hydrogen peroxide solution to form a first ion-containing solution, contacting the first ion-containing solution with a cationic resin whereby ions selected form the group consisting of molybdenum, niobium, technetium, selenium, vanadium, arsenic, germanium, zirconium and rubidium remain in a second ion-containing solution while ions selected from the group consisting of rubidium, zinc, beryllium, cobalt, iron, manganese, chromium, strontium, yttrium and zirconium are selectively adsorbed by the cationic resin; adjusting the pH of the second ion-containing solution to within a range of from about 5.0 to about 6.0; contacting the pH adjusting second ion-containing solution with a dextran-based material for a time to selectively separate niobium from the solution and recovering the niobium from the dextran-based material.

  5. Mineral Resource of the Month: Niobium

    USGS Publications Warehouse

    Papp, John F.

    2014-01-01

    Niobium, also called columbium, is a transition metal with a very high melting point. It is in greatest demand in industrialized countries, like the United States, because of its defense-related uses in the aerospace, energy and transportation industries. Niobium is used mostly to make high-strength, low-alloy (HSLA) steel and stainless steel. HSLA steels are used in large-diameter pipes for oil and natural gas pipelines and automobile wheels.

  6. Mineral resource of the month: niobium (columbium)

    USGS Publications Warehouse

    Papp, John F.

    2007-01-01

    It’s not just diamonds associated with conflict in Africa. Coltan, short for columbite-tantalite (a blend of niobium — also called columbium — and tantalum minerals), is linked with the recent conflicts in the Congo that involved several African countries. The metallic ore, which is processed to separate out niobium and the very valuable tantalum (see Geotimes, August 2004), is believed to be smuggled out and sold to help finance the armed conflicts.

  7. Niobium based coatings for dental implants

    NASA Astrophysics Data System (ADS)

    Ramírez, G.; Rodil, S. E.; Arzate, H.; Muhl, S.; Olaya, J. J.

    2011-01-01

    Niobium based thin films were deposited on stainless steel (SS) substrates to evaluate them as possible biocompatible surfaces that might improve the biocompatibility and extend the life time of stainless steel dental implants. Niobium nitride and niobium oxide thin films were deposited by reactive unbalanced magnetron sputtering under standard deposition conditions without substrate bias or heating. The biocompatibility of the surfaces was evaluated by testing the cellular adhesion and viability/proliferation of human cementoblasts during different culture times, up to 7 days. The response of the films was compared to the bare substrate and pieces of Ti6Al4V; the most commonly used implant material for orthopedics and osteo-synthesis applications. The physicochemical properties of the films were evaluated by different means; X-ray diffraction, Rutherford backscattering spectroscopy and contact angle measurements. The results suggested that the niobium oxide films were amorphous and of stoichiometric Nb2O5 (a-Nb2O5), while the niobium nitride films were crystalline in the FCC phase (c-NbN) and were also stoichiometric with an Nb to N ratio of one. The biological evaluation showed that the biocompatibility of the SS could be improved by any of the two films, but neither was better than the Ti6Al4V alloy. On the other hand, comparing the two films, the c-NbN seemed to be a better surface than the oxide in terms of the adhesion and proliferation of human cemetoblasts.

  8. 40 CFR 721.10602 - Lead niobium titanium zirconium oxide.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 32 2013-07-01 2013-07-01 false Lead niobium titanium zirconium oxide... Specific Chemical Substances § 721.10602 Lead niobium titanium zirconium oxide. (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified as lead niobium...

  9. 40 CFR 721.10602 - Lead niobium titanium zirconium oxide.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Lead niobium titanium zirconium oxide... Specific Chemical Substances § 721.10602 Lead niobium titanium zirconium oxide. (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified as lead niobium...

  10. Oxygen Atom Adsorption on and Diffusion into Nb(110) and Nb(100) from First Principles

    SciTech Connect

    Tafen, De Nyago; Gao, Michael C

    2013-11-01

    In order to understand the dynamics of oxidation of Nb, we examine the adsorption, absorption, and diffusion of an oxygen atom on, in, and into Nb(110) and Nb(100) surfaces, respectively, using density functional theory. Our calculations predict that the oxygen atom adsorbs on the threefold site on Nb(110) and the fourfold hollow site on Nb(100), and the adsorption energy is -5.08 and -5.18 eV respectively. We find the long and short bridge sites to be transition states for O diffusion on Nb(110), while the on top site is a rank-2 saddle point. In the subsurface region, the oxygen atom prefers the octahedral site, as in bulk niobium. Our results also show that the O atom is more stable on Nb(110) subsurface than on Nb(100) subsurface. The diffusion of oxygen atoms into niobium surfaces passes through transition states where the oxygen atom is coordinated to four niobium atoms. The diffusion barriers of the oxygen atom into Nb(110) and Nb(100) are 1.81 and 2.05 eV, respectively. Analysis of the electronic density of states reveals the emergence of well localized electronic states below the lowest states of clean Nb surfaces due to d-p orbital hybridization.

  11. Recovery of niobium from irradiated targets

    DOEpatents

    Phillips, Dennis R.; Jamriska, Sr., David J.; Hamilton, Virginia T.

    1994-01-01

    A process for selective separation of niobium from proton irradiated molybdenum targets is provided and includes dissolving the molybdenum target in a hydrogen peroxide solution to form a first ion-containing solution, contacting the first ion-containing solution with a cationic resin whereby ions selected form the group consisting of molybdenum, biobium, technetium, selenium, vanadium, arsenic, germanium, zirconium and rubidium remain in a second ion-containing solution while ions selected from the group consisting of rubidium, zinc, beryllium, cobalt, iron, manganese, chromium, strontium, yttrium and zirconium are selectively adsorbed by the cationic resin; adjusting the pH of the second ion-containing solution to within a range of from about 5.0 to about 6.0; contacting the pH adjusting second ion-containing solution with a dextran-based material for a time to selectively separate niobium from the solution and recovering the niobium from the dextran-based material.

  12. Production of High Purity Niobium Ingots at CBMM

    SciTech Connect

    Moura, Lourenco de; Faria Sousa, Clovis Antonio de; Burgos Cruz, Edmundo

    2011-03-31

    CBMM is a fully integrated company, from the mine to the end line of the production chain, supplying different niobium products to the world market: ferroniobium, nickelniobium, niobium pentoxide and high purity metallic niobium. This high purity metallic niobium has long been known to exhibit superconductivity below 9.25 Kelvin. This characteristic has the potential to bring technological benefits for many different areas such as medicine, computing and environment. This paper presents the raw material requirements as well as CBMM experience on producing high purity niobium ingots. The results prove that CBMM material can be the best solution for special applications such as low cost superconductive radiofrequency cavities.

  13. New two-dimensional niobium and vanadium carbides as promising materials for Li-ion batteries.

    PubMed

    Naguib, Michael; Halim, Joseph; Lu, Jun; Cook, Kevin M; Hultman, Lars; Gogotsi, Yury; Barsoum, Michel W

    2013-10-30

    New two-dimensional niobium and vanadium carbides have been synthesized by selective etching, at room temperature, of Al from Nb2AlC and V2AlC, respectively. These new matrials are promising electrode materials for Li-ion batteries, demonstrating good capability to handle high charge-discharge rates. Reversible capacities of 170 and 260 mA·h·g(-1) at 1 C, and 110 and 125 mA·h·g(-1) at 10 C were obtained for Nb2C and V2C-based electrodes, respectively. PMID:24144164

  14. PURE NIOBIUM AS A PRESSURE VESSEL MATERIAL

    SciTech Connect

    Peterson, T. J.; Carter, H. F.; Foley, M. H.; Klebaner, A. L.; Nicol, T. H.; Page, T. M.; Theilacker, J. C.; Wands, R. H.; Wong-Squires, M. L.; Wu, G.

    2010-04-09

    Physics laboratories around the world are developing niobium superconducting radio frequency (SRF) cavities for use in particle accelerators. These SRF cavities are typically cooled to low temperatures by direct contact with a liquid helium bath, resulting in at least part of the helium container being made from pure niobium. In the U.S., the Code of Federal Regulations allows national laboratories to follow national consensus pressure vessel rules or use of alternative rules which provide a level of safety greater than or equal to that afforded by ASME Boiler and Pressure Vessel Code. Thus, while used for its superconducting properties, niobium ends up also being treated as a material for pressure vessels. This report summarizes what we have learned about the use of niobium as a pressure vessel material, with a focus on issues for compliance with pressure vessel codes. We present results of a literature search for mechanical properties and tests results, as well as a review of ASME pressure vessel code requirements and issues.

  15. Developing of superconducting niobium cavities for accelerators

    NASA Astrophysics Data System (ADS)

    Pobol, I. L.; Yurevich, S. V.

    2015-11-01

    The results of a study of structure and mechanical properties of welding joints, superconducting characteristics of the material after joining of welded components of superconducting radio frequency cavities are presented. The paper also describes the results of testing of the RF 1.3 GHz single-cell niobium cavity manufactured in the PTI NAS Belarus.

  16. RF Sputtering of Gold Contacts On Niobium

    NASA Technical Reports Server (NTRS)

    Barr, D. W.

    1983-01-01

    Reliable gold contacts are deposited on niobium by combination of RF sputtering and photolithography. Process results in structures having gold only where desired for electrical contact. Contacts are stable under repeated cycling from room temperature to 4.2 K and show room-temperature contact resistance as much as 40 percent below indium contacts made by thermalcompression bonding.

  17. A spiraled niobium tin superconductive ribbon

    NASA Technical Reports Server (NTRS)

    Coles, W. D.

    1973-01-01

    Copper film is vapor-deposited on clean ribbon and sprayed with photosensitive etch-resistant material. Photographic film masks are placed on ribbon and exposed to ultraviolet light. Etchant removes copper and exposure to oxidizing atmosphere forms niobium oxide. Photosensitive material is removed and ribbon is immersed in molten temperatures.

  18. Pure Niobium as a Pressure Vessel Material

    NASA Astrophysics Data System (ADS)

    Peterson, T. J.; Carter, H. F.; Foley, M. H.; Klebaner, A. L.; Nicol, T. H.; Page, T. M.; Theilacker, J. C.; Wands, R. H.; Wong-Squires, M. L.; Wu, G.

    2010-04-01

    Physics laboratories around the world are developing niobium superconducting radio frequency (SRF) cavities for use in particle accelerators. These SRF cavities are typically cooled to low temperatures by direct contact with a liquid helium bath, resulting in at least part of the helium container being made from pure niobium. In the U.S., the Code of Federal Regulations allows national laboratories to follow national consensus pressure vessel rules or use of alternative rules which provide a level of safety greater than or equal to that afforded by ASME Boiler and Pressure Vessel Code. Thus, while used for its superconducting properties, niobium ends up also being treated as a material for pressure vessels. This report summarizes what we have learned about the use of niobium as a pressure vessel material, with a focus on issues for compliance with pressure vessel codes. We present results of a literature search for mechanical properties and tests results, as well as a review of ASME pressure vessel code requirements and issues.

  19. Ingot Niobium RF Cavity Design and Development at BARC

    SciTech Connect

    Mittal, K. C.; Mondal, J.; Ghatak, S.; Dhavale, A. S.; Ghodke, S. R.; Vohra, R. S.; Jawale, S. B.; Dutta, D.; Pujari, P. K.; Saha, T. K.; Bapat, A. V.

    2011-03-31

    This article presents the different activity of Ingot niobium in BARC. BARC is developing a technology for the accelerator driven subcritical system (ADSS) that will be mainly utilized for the transmutation of nuclear waste and enrichment of U{sup 233}. Design and development of superconducting medium velocity cavity has been taken up as a part of the ADSS project. The design and fabrication of f = 1050 MHz, {beta} = 0.49 with Ingot niobium will be presented. Positron annihilation studies are conducted on small samples of ingot niobium to understand the defect depth profile of the niobium surface. The results are presented here.

  20. PROCESS OF COATING GRAPHITE WITH NIOBIUM-TITANIUM CARBIDE

    DOEpatents

    Halden, F.A.; Smiley, W.D.; Hruz, F.M.

    1961-07-01

    A process of coating graphite with niobium - titanium carbide is described. It is found that the addition of more than ten percent by weight of titanium to niobium results in much greater wetting of the graphite by the niobium and a much more adherent coating. The preferred embodiment comprises contacting the graphite with a powdered alloy or mixture, degassing simultaneously the powder and the graphite, and then heating them to a high temperature to cause melting, wetting, spreading, and carburization of the niobium-titanium powder.

  1. Field Emission Measurements from Niobium Electrodes

    SciTech Connect

    M. BastaniNejad, P.A. Adderley, J. Clark, S. Covert, J. Hansknecht, C. Hernandez-Garcia, R. Mammei, M. Poelker

    2011-03-01

    Increasing the operating voltage of a DC high voltage photogun serves to minimize space charge induced emittance growth and thereby preserve electron beam brightness, however, field emission from the photogun cathode electrode can pose significant problems: constant low level field emission degrades vacuum via electron stimulated desorption which in turn reduces photocathode yield through chemical poisoning and/or ion bombardment and high levels of field emission can damage the ceramic insulator. Niobium electrodes (single crystal, large grain and fine grain) were characterized using a DC high voltage field emission test stand at maximum voltage -225kV and electric field gradient > 10MV/m. Niobium electrodes appear to be superior to diamond-paste polished stainless steel electrodes.

  2. Nitrogen doping study in ingot niobium cavities

    SciTech Connect

    Dhakal, Pashupati; Ciovati, Gianluigi; Kneisel, Peter; Myneni, Ganapati Rao; Makita, Junki

    2015-09-01

    Thermal diffusion of nitrogen in niobium superconducting radio frequency cavities at temperature ~800 °C has resulted in the increase in quality factor with a low-field Q-rise extending to Bp > 90 mT. However, the maximum accelerating gradient of these doped cavities often deteriorates below the values achieved by standard treatments prior to doping. Here, we present the results of the measurements on ingot niobium cavities doped with nitrogen at 800 °C. The rf measurements were carried out after the successive electropolishing to remove small amount of material from the inner surface layer. The result showed higher breakdown field with lower quality factor as material removal increases.

  3. Microstructures in rapidly solidified niobium aluminides

    NASA Technical Reports Server (NTRS)

    Hebsur, Mohan G.; Locci, Ivan E.

    1988-01-01

    The microstructures of niobium aluminides produced by chill block melt spinning were compared to those of niobium aluminides produced by conventional casting. The rapidly solidified alloys were rapidly solidified by melt spinning in an argon atmosphere, and the melt-spun ribbons were examined by optical, X-ray, and TEM techniques. Microstructures were found to range from single-phase for Nb-75 at. pct Al (NbAl3) to two phase for Nb-46 at. pct Al (NbAl3 + Nb2Al). It was found that the melt spinning of Nb-aluminides produced finer grained microstructures than those produced in induction-melted ingots or in powders produced by the rotating electrode process. Ternary additions such as Cr, Ti, and Si tended to form intermetallic phases along the grain boundaries.

  4. Microwave mixing with niobium variable thickness bridges

    NASA Technical Reports Server (NTRS)

    Wang, L.-K.; Callegari, A.; Deaver, B. S., Jr.

    1977-01-01

    Niobium thin-film bridges 300-A thick, 1-micron wide, and 0.5-micron long joining two bulk films 5000-A thick and having normal resistance of the order of 1 ohm have been fabricated and used for microwave mixing at 10 GHz. They exhibit Josephson, bolometric, and multiple-flux-flow mixing and have useful response at 100-200 GHz. The data show in a direct way limitations imposed by flux flow and heating.

  5. Creep behavior of tungsten/niobium and tungsten/niobium-1 percent zirconium composites

    NASA Technical Reports Server (NTRS)

    Petrasek, D. W.; Titran, R. H.

    1988-01-01

    A study was conducted to determine the feasibility of using tungsten fiber reinforced niobium or niobium-1 percent zirconium matrix composites to meet the anticipated increased temperature and creep resistance requirements imposed by advanced space power systems. The results obtained on the short time tensile properties indicated that W/Nb composites showed significant improvements in high temperature strength and offer significant mass reductions for high temperature space power systems. The prime material requirement for space power systems applications is long time creep resistance. A study was conducted to determine the effect of high temperature exposure on the properties of these composites, with emphasis upon their creep behavior at elevated temperatures.

  6. Liquid-film assisted formation of alumina/niobium interfaces

    SciTech Connect

    Sugar, Joshua D.; McKeown, Joseph T.; Marks, Robert A.; Glaeser, Andreas M.

    2002-06-16

    Alumina has been joined at 1400 degrees C using niobium-based interlayers. Two different joining approaches were compared: solid-state diffusion bonding using a niobium foil as an interlayer, and liquid-film assisted bonding using a multilayer copper/niobium/copper interlayer. In both cases, a 127-(mu)m thick niobium foil was used; =1.4-(mu)m or =3-(mu)m thick copper films flanked the niobium. Room-temperature four-point bend tests showed that the introduction of a copper film had a significant beneficial effect on the average strength and the strength distribution. Experiments using sapphire substrates indicated that during bonding the initially continuous copper film evolved into isolated copper-rich droplets/particles at the sapphire/interlayer interface, and extensive regions of direct bonding between sapphire and niobium. Film breakup appeared to initiate at either niobium grain boundary ridges, or at asperities or irregularities on the niobium surface that caused localized contact with the sapphire.

  7. Extraction spectrophotometric determination of niobium in rocks with sulfochlorophenol S

    USGS Publications Warehouse

    Childress, A.E.; Greenland, L.P.

    1980-01-01

    After acid decomposition and potassium pyrosulfate fusion, niobium (1-26 ppm) is separated from interfering elements by extraction into methyl isobutyl ketone from 6 M H2SO4-2 M HF and back-extracted into water. The niobium-sulfochloro-phenol S complex is extracted into amyl alcohol. ?? 1980.

  8. Niobium oxide compositions and methods for using same

    DOEpatents

    Goodenough, John B; Han, Jian-Tao

    2014-02-11

    The disclosure relates a niobium oxide useful in anodes of secondary lithium ion batteries. Such niobium oxide has formula Li.sub.xM.sub.1-yNb.sub.yNb.sub.2O.sub.7, wherein 0.ltoreq.x.ltoreq.3, 0.ltoreq.y.ltoreq.1, and M represents Ti or Zr. The niobium oxide may be in the form of particles, which may be carbon coated. The disclosure also relates to an electrode composition containing at least one or more niobium oxides of formula Li.sub.xM.sub.1-yNb.sub.yNb.sub.2O.sub.7. The disclosure further relates to electrodes, such as anodes, and batteries containing at least one or more niobium oxides of formula Li.sub.xM.sub.1-yNb.sub.yNb.sub.2O.sub.7. Furthermore, the disclosure relates to methods of forming the above.

  9. Superconducting structure with layers of niobium nitride and aluminum nitride

    DOEpatents

    Murduck, James M.; Lepetre, Yves J.; Schuller, Ivan K.; Ketterson, John B.

    1989-01-01

    A superconducting structure is formed by depositing alternate layers of aluminum nitride and niobium nitride on a substrate. Deposition methods include dc magnetron reactive sputtering, rf magnetron reactive sputtering, thin-film diffusion, chemical vapor deposition, and ion-beam deposition. Structures have been built with layers of niobium nitride and aluminum nitride having thicknesses in a range of 20 to 350 Angstroms. Best results have been achieved with films of niobium nitride deposited to a thickness of approximately 70 Angstroms and aluminum nitride deposited to a thickness of approximately 20 Angstroms. Such films of niobium nitride separated by a single layer of aluminum nitride are useful in forming Josephson junctions. Structures of 30 or more alternating layers of niobium nitride and aluminum nitride are useful when deposited on fixed substrates or flexible strips to form bulk superconductors for carrying electric current. They are also adaptable as voltage-controlled microwave energy sources.

  10. Superconducting structure with layers of niobium nitride and aluminum nitride

    DOEpatents

    Murduck, J.M.; Lepetre, Y.J.; Schuller, I.K.; Ketterson, J.B.

    1989-07-04

    A superconducting structure is formed by depositing alternate layers of aluminum nitride and niobium nitride on a substrate. Deposition methods include dc magnetron reactive sputtering, rf magnetron reactive sputtering, thin-film diffusion, chemical vapor deposition, and ion-beam deposition. Structures have been built with layers of niobium nitride and aluminum nitride having thicknesses in a range of 20 to 350 Angstroms. Best results have been achieved with films of niobium nitride deposited to a thickness of approximately 70 Angstroms and aluminum nitride deposited to a thickness of approximately 20 Angstroms. Such films of niobium nitride separated by a single layer of aluminum nitride are useful in forming Josephson junctions. Structures of 30 or more alternating layers of niobium nitride and aluminum nitride are useful when deposited on fixed substrates or flexible strips to form bulk superconductors for carrying electric current. They are also adaptable as voltage-controlled microwave energy sources. 8 figs.

  11. Niobium matrix composites for high temperature turbine blades, phase 2

    NASA Technical Reports Server (NTRS)

    Heng, Sangvavann; Laferla, Raffaele; Tuffias, Robert H.

    1991-01-01

    This program demonstrated the feasibility of fabricating fiber-reinforced MMC (niobium matrix) turbine blades to net shape by chemical vapor infiltration (CVI). A controllable, repeatable niobium infiltration process was developed, and the kinetics of both deposition and infiltration were studied. Several continuous refractory fibers (Nicalon, Nextel 440, FP-Al2O3, HPZ, and tungsten mesh) were investigated as potential reinforcements for strengthening niobium. Thermodynamic and experimental evaluation indicated FP-Al2O3 and tungsten to be the most chemically compatible with niobium, while Nicalon, FP-Al2O3, and tungsten were found to be best with regard to reinforcing capability. Finally, a protective coating for iridium was found to provide substantial oxidation protection to the niobium blade matrix.

  12. The Manufacturing of Niobium Powder by Hunter Process

    NASA Astrophysics Data System (ADS)

    Yoon, Jae-Sik

    Niobium powder was fabricated by metallothermic reduction process using K2NbF7 as the raw material, KCl and KF as the diluents and Na as the reducing agent. The apparatus for the experiment was designed and built specifically for the present study. Varying properties of niobium powder depending on reaction temperature and excess of reducing agent were analyzed. The niobium particle size increased significantly as the reduction temperature increased from 993 to 1093 K. The particle size was fairly uniform at a given reaction temperature, varying from 0.2 μ m to 50 nm depending on the reaction temperature. The yield of niobium powder increased from 58 to 83% with an increase in reaction temperature. The average particle size of niobium powder was improved from 70 nm to 0.2 μ m with the increase in the amount of Na excess. In addition, the yield rate of Nb powder was 82% in the 5% excess sodium.

  13. Laser polishing of niobium for SRF applications

    SciTech Connect

    Zhao, Liang; Klopf, J. Michael; Reece, Charles E.; Kelley, Michael

    2013-09-01

    Smooth interior surfaces are desired for niobium SRF cavities, now obtained by buffered chemical polish (BCP) and/or electropolish (EP). Laser polishing is a potential alternative, having advantages of speed, freedom from chemistry and in-process inspection. Here we show that laser polishing can produce smooth topography with Power Spectral Density (PSD) measurements similar to that obtained by EP. We studied the influence of the laser power density and laser beam raster rate on the surface topography. These two factors need to be combined carefully to smooth the surface without damaging it. Computational modeling was used to simulate the surface temperature and explain the mechanism of laser polishing.

  14. Germanium-overcoated niobium Dayem bridges

    NASA Technical Reports Server (NTRS)

    Holdeman, L. B.; Peters, P. N.

    1976-01-01

    Overcoating constriction microbridges with semiconducting germanium provides additional thermal conductivity at liquid-helium temperatures to reduce the effects of self-heating in these Josephson junctions. Microwave-induced steps were observed in the I-V characteristics of an overcoated Dayem bridge fabricated in a 15-nm-thick niobium film; at least 20 steps could be counted at 4.2 K. No steps were observed in the I-V characteristics of the bridge prior to overcoating. In addition, the germanium overcoat can protect against electrical disturbances at room temperature.

  15. Design of a 10-T superconducting dipole magnet using niobium-tin conductor

    SciTech Connect

    Taylor, C.; Meuser, R.; Caspi, S.; Gilbert, W.; Hassenzahl, W.; Peters, C.; Schafer, R.; Wolgast, R.

    1982-11-01

    In order to minimize the size and cost of conventional facilities - land, tunneling, shielding, cryogenic and vacuum system - the dipole magnets for the next generation of particle accelerators must produce as strong a magnetic field as possible. Ten tesla seems to be a reasonable goal, and can be attained by using either niobium-tin conductor at 4.2 K or niobium-titanium at 1.8 K. The beam diameter in a multi-TeV accelerator, can in principle, be quite small, say 20 mm, depending on the design of the injection and extraction systems, and on beam-cooling technology. Magnet cost is strongly dependent on bore diameter, so there is a strong incentive to minimize that. We believe that a 40-mm bore diameter - about 60-mm winding inside diameter is feasible and is a reasonable goal for initial research and development. For such a high field and small bore, there is an incentive to achieve a high overall current density in order to minimize the amount of superconductor. Our design is based on an overall current density of 400 A/sq mm. LBL has undertaken the development of a magnet using niobium-tin conductor intended to meet the above specifications. The conductor is a Rutherford-type cable consisting of twelve strands of 1.71-mm-dia wire. Dimensions of the uninsulated cable are 11.0 x 3.0 mm. The configuration chosen consists of flat race-track layers - four per pole - with the ends bent up and down to clear the bore. Two coils are wound from a single piece of cable with a cross-over at the inside: the familiar double pancake arrangement.

  16. SEPARATION OF URANIUM FROM ZIRCONIUM AND NIOBIUM BY SOLVENT EXTRACTION

    DOEpatents

    Voiland, E.E.

    1958-05-01

    A process for separation of the uranium from zirconium and/or niobium values contained in 3 to 7M aqueous nitric acid solutions is described. This is accomplished by adding phosphoric acid anions to the nitric acid solution containing the uranium, zirconium, and/or niobium in an amount sufficient to make the solution 0.05 to 0.2M in phosphate ion and contacting the solution with an organic water-immiscible solvent such as MEK, whereby the uranyl values are taken up by the extract phase while the zirconium and niobium preferentially remain in the aqueous raffinate.

  17. Niobium alloy heat pipes for use in oxidizing environments

    NASA Astrophysics Data System (ADS)

    Craig Wojcik, C.

    1991-01-01

    Niobium alloys have been used for many years in rocket propulsion systems and afterburner sections of gas turbine engines. In these applications, adequate oxidation resistance is provided by protective silicide coatings. By utilizing these coatings and niobium powder metallurgy to produce porous wicks, it has been demonstrated that niobium alloy heat pipes can comfortably operate in flame temperatures exceeding 3000 K. Results of lithium corrosion tests on C-103 (Nb-10%Hf-1%Ti) up to 1477 K will be presented along with thermal performance data for specific heat pipe designs.

  18. Research & Development on Superconducting Niobium Materials via Magnetic Measurements

    SciTech Connect

    S. B. Roy, V. C. Sahni, and G. R. Myneni

    2011-03-01

    We present a study of superconducting properties of both large grain (1 mm average grain size) and small grain (50 micron average grain size) Niobium materials containing varying amounts of Tantalum impurities that have been used in the fabrication of high accelerating gradient superconducting radio frequency cavities. We found that a buffered chemical polishing of these Niobium samples causes a distinct reduction in the superconducting parameters like TC, wt- ppm to 1300 wt-ppm. Implications of these results on the performance of niobium superconducting radio frequency cavities are discussed, especially the anomalous high field RF losses that have been reported in the literature.

  19. Creep behavior of tungsten/niobium and tungsten/niobium-1 percent zirconium composites

    NASA Technical Reports Server (NTRS)

    Petrasek, Donald W.; Titran, Robert H.

    1988-01-01

    The creep behavior and microstructural stability of tungsten fiber reinforced niobium and niobium 1 percent zirconium was determined at 1400 and 1500 K in order to assess the potential of this material for use in advanced space power systems. The creep behavior of the composite materials could be described by a power law creep equation. A linear relationship was found to exist between the minimum creep rate of the composite and the inverse of the composite creep rupture life. The composite materials had an order of magnitude increase in stress to achieve 1 percent creep strain and in rupture strength at test temperatures of 1400 and 1500 K compared to unreinforced material. The composite materials were also stronger than the unreinforced materials by an order of magnitude when density was taken into consideration. Results obtained on the creep behavior and microstructural stability of the composites show significant potential improvement in high temperature properties and mass reduction for space power system components.

  20. Crystallography and Morphology of Niobium Carbide in As-Cast HP-Niobium Reformer Tubes

    NASA Astrophysics Data System (ADS)

    Buchanan, Karl G.; Kral, Milo V.

    2012-06-01

    The microstructures of two as-cast heats of niobium-modified HP stainless steels were characterized. Particular attention was paid to the interdendritic niobium-rich carbides formed during solidification of these alloys. At low magnifications, these precipitates are grouped in colonies of similar lamellae. Higher magnifications revealed that the lamellae actually obtain two distinct morphologies. The type I morphology exhibits broad planar interfaces with a smooth platelike shape. Type II lamellae have undulating interfaces and an overall reticulated shape. To provide further insight into the origin of these two different morphologies, the microstructure and crystallography of each have been studied in detail using high resolution scanning electron microscopy, transmission electron microscopy, various electron diffraction methods (electron backscatter diffraction (EBSD), selected area diffraction (SAD), and convergent beam electron diffraction (CBED)), and energy dispersive X-ray spectroscopy.

  1. Synthesis of piezoelectric and bioactive NaNbO3 from metallic niobium and niobium oxide.

    PubMed

    Prado da Silva, Marcelo Henrique; da Rocha, Daniel Navarro; de Andrade Gobbo, Luciano; Dos Santos Azevedo, Luciana Maria; Louro, Luís Henrique Leme; Machado Costa, Andréa; Brant de Campos, José

    2016-07-01

    NaNbO3 was synthesized by two different routes, one using metallic niobium powder, and another using niobium oxide (Nb2 O5 ) powder. In both routes an aqueous sodium hydroxide solution was used to hydrothermally treating the powders. In the first approach, the solution concentrations were 3M, 1M, and 0.5M. The second route used solution concentrations of 10M and 12.5M. After the hydrothermal treatments, the powders were heat treated in order to synthesize NaNbO3 . The products were characterized by scanning electron microscopy (SEM) with energy dispersive spectrometry (EDS), and X-ray diffraction (XRD) with Rietveld refinement. The phases were identified by means of X-ray diffraction (XRD) with Rietveld refinement. It was observed that the molar concentrations of the solutions had opposing effects for each route. An antiferroelectric phase was found in both routes. In the niobium metallic route, a ferroelectric phase was also synthesized. This study proves that piezoelectric NaNbO3 can be obtained after alkali treatment of both Nb and Nb2 O5. © 2015 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater, 104B: 979-985, 2016. PMID:25980635

  2. Manufacture of superconducting niobium cavity parts by hydropercussion punching

    NASA Astrophysics Data System (ADS)

    Azaryan, N. S.; Shirkov, G. D.; Zhurauski, A. Yu.; Petrakovski, V. S.; Batouritski, M. A.

    2016-03-01

    A complete cycle of manufacturing all parts of superconducting niobium cavities which comprise two half-cells, two drift tubes, and two flanges each has been developed. The cavity half-cells are manufactured by hydropercussion punching, which has a number of advantages over the instrumental stamping technique. For the first time, the diagram of formability of ultrapure niobium has been experimentally obtained for hydropercussion punching and the key parameters of the process have been determined that ensure complete deep-drawing of workpieces, viz., the value of the limit drawing ratio of ultrapure niobium that is 1.92 at a specific impact energy of 0.42 MJ/m2. The deviations of the half-cell dimensions from the rated values do not exceed 0.1 mm. Production tools required for all manufacturing steps have been created. The parameters of machining of the niobium cavity parts prior to welding have been experimentally established.

  3. Studies of Niobium Thin Film Produced by Energetic Vacuum Deposition

    SciTech Connect

    Genfa Wu; Anne-Marie Valente; H. Phillips; Haipeng Wang; Andy Wu; T. J. Renk; P Provencio

    2004-05-01

    An energetic vacuum deposition system has been used to study deposition energy effects on the properties of niobium thin films on copper and sapphire substrates. The absence of working gas avoids the gaseous inclusions commonly seen with sputtering deposition. A biased substrate holder controls the deposition energy. Transition temperature and residual resistivity ratio of the niobium thin films at several deposition energies are obtained together with surface morphology and crystal orientation measurements by AFM inspection, XRD and TEM analysis. The results show that niobium thin films on sapphire substrate exhibit the best cryogenic properties at deposition energy around 123 eV. The TEM analysis revealed that epitaxial growth of film was evident when deposition energy reaches 163 eV for sapphire substrate. Similarly, niobium thin film on copper substrate shows that film grows more oriented with higher deposition energy and grain size reaches the scale of the film thickness at the deposition energy around 153 eV.

  4. Electrochemical Synthesis of Niobium-Hafnium Coatings in Molten Salts

    NASA Astrophysics Data System (ADS)

    Kuznetsov, Sergey A.; Kuznetsova, Svetlana V.

    2007-08-01

    Graphite is widely used in technology because of its unique properties. A drawback of graphite is its low heat resistance in oxidizing atmospheres. To increase its heat resistance, Nb-Hf protective coatings were synthesized. Electrodeposition of niobium coatings on graphite with subsequent precise surface alloying of niobium with hafnium was studied. Electrochemical synthesis of Nb-Hf coatings from molten salt systems containing compounds of niobium and hafnium was used too. It was shown that Nb-Hf coatings with a planar growing front can be obtained if the concentration and therefore the limiting current density of the more electropositive component Nb is kept low. Nb-Hf coatings with a thickness of 20 - 30 μm have been obtained in this way from an NaCl-KCl-K2NbF7 (1 wt%)-K2HfF6 (10 wt%)-NaF (5 wt%) melt, above the limiting current density of niobium deposition.

  5. Effects of Impurities on Alumina-Niobium InterfacialMicrostructures

    SciTech Connect

    McKeown, Joseph T.; Sugar, Joshua D.; Gronsky, Ronald; Glaeser,Andreas M.

    2005-06-20

    Optical microscopy, scanning electron microscopy, and transmission electron microscopy were employed to examine the interfacial microstructural effects of impurities in alumina substrates used to fabricate alumina-niobium interfaces via liquid-film-assisted joining. Three types of alumina were used: undoped high-purity single-crystal sapphire; a high-purity, high-strength polycrystalline alumina; and a lower-purity, lower-strength polycrystalline alumina. Interfaces formed between niobium and both the sapphire and high-purity polycrystalline alumina were free of detectable levels of impurities. In the lower-purity alumina, niobium silicides were observed at the alumina-niobium interface and on alumina grain boundaries near the interface. These silicides formed in small-grained regions of the alumina and were found to grow from the interface into the alumina along grain boundaries. Smaller silicide precipitates found on grain boundaries are believed to form upon cooling from the bonding temperature.

  6. Electroplating and stripping copper on molybdenum and niobium

    NASA Technical Reports Server (NTRS)

    Power, J. L.

    1978-01-01

    Molybdenum and niobium are often electroplated and subsequently stripped of copper. Since general standard plating techniques produce poor quality coatings, general procedures have been optimized and specified to give good results.

  7. STS-110 Crew Portrait

    NASA Technical Reports Server (NTRS)

    2001-01-01

    This is the official STS-110 crew portrait. In front, from the left, are astronauts Stephen N. Frick, pilot; Ellen Ochoa, flight engineer; and Michael J. Bloomfield, mission commander; In the back, from left, are astronauts Steven L. Smith, Rex J. Walheim, Jerry L. Ross and Lee M.E. Morin, all mission specialists. Launched aboard the Space Shuttle Orbiter Atlantis on April 8, 2002, the STS-110 mission crew prepared the International Space Station (ISS) for future space walks by installing and outfitting a 43-foot-long Starboard side S0 truss and preparing the Mobile Transporter. The mission served as the 8th ISS assembly flight.

  8. STS-110 Crew Insignia

    NASA Technical Reports Server (NTRS)

    2001-01-01

    The STS-110 mission began the third and final phase of construction for the International Space Station (ISS) by delivering and installing the Starboard side S0 (S-zero) truss segment that was carried into orbit in the payload bay of the Space Shuttle Atlantis. The STS-110 crew patch is patterned after the cross section of the S0 truss, and encases the launch of the Shuttle Atlantis and a silhouette of the ISS as it will look following mission completion. The successfully installed S0 segment is highlighted in gold. The three prominent flames blasting from the shuttle emphasizes the first shuttle flight to use three Block II Main Engines.

  9. A bulk niobium superconducting quarter wave resonator

    SciTech Connect

    Ben-Zvi, I. ); Chiaveri, E. ); Elkonin, B.V. ); Facco, A.; Sokolowski, J.S. . Lab. Nazionale di Legnaro)

    1990-01-01

    A bath-cooled all-niobium 160 MHz quarter wave resonator prototype was constructed and tested. The objective of this research has been the development of a high performance accelerating element with {beta}{sub opt} {approx equal} 0.11 for the ALPI linac at the Laboratori Nazionali di Legnaro. The design of this resonator was based upon a previous 150 MHz model, with minor changes due to the different frequency and to modified welding procedure. An accelerating field of 5 MV/m was achieved at a power dissipation of 10 W and the low power Q was 2.4 {times} 10{sup 8}. The resonator could dissipate 70 W of power without thermal breakdown. 16 refs., 2 figs., 1 tab.

  10. Niobium Silicon Alloys for Kinetic Inductance Detectors

    NASA Astrophysics Data System (ADS)

    Calvo, M.; D'Addabbo, A.; Monfardini, A.; Benoit, A.; Boudou, N.; Bourrion, O.; Catalano, A.; Dumoulin, L.; Goupy, J.; Le Sueur, H.; Marnieros, S.

    2014-08-01

    We are studying the properties of Niobium Silicon amorphous alloys as a candidate material for the fabrication of highly sensitive kinetic inductance detectors (KID), optimized for very low optical loads. As in the case of other composite materials, the NbSi properties can be changed by varying the relative amounts of its components. Using a NbSi film with T = 1 K we have been able to obtain the first NbSi resonators, observe an optical response and acquire a spectrum in the band 50-300 GHz. The data taken show that this material has very high kinetic inductance and normal state surface resistivity . These properties are ideal for the development of KID. More measurements are planned to further characterize the NbSi alloy and fully investigate its potential.

  11. Vacuum plasma spraying of tantalum and niobium

    SciTech Connect

    Lugscheider, E.; Eschnauer, H.; Haeuser, B.; Jaeger, D.

    1985-11-01

    Vacuum plasma spraying is a suitable process for producing high quality coatings of reactive metals such as tantalum and niobium. Ta and Nb coatings used for corrosion protection must be extremely dense, homogeneous, and of high purity and adhesion. Hence, the process parameters have to be carefully optimized even with regard to the spraying powder, its grain size and morphology. Spraying equipment with vacuum systems which allow for a final pressure of 10/sup -3/ mbar, which have heated and evacuated powder feeder units, and heated substrates, as well as the use of powders with high purity and low gas content, are required for producing high quality Ta and Nb coatings. Corrosion tests in sulfuric acid and aqua regia at different concentrations show that Ta and Nb coatings sprayed under optimized conditions have high resistance to both general and localized corrosion.

  12. Enhanced characterization of niobium surface topography

    NASA Astrophysics Data System (ADS)

    Xu, Chen; Tian, Hui; Reece, Charles E.; Kelley, Michael J.

    2011-12-01

    Surface topography characterization is a continuing issue for the superconducting radio frequency (SRF) particle accelerator community. Efforts are under way to both improve surface topography and its characterization and analysis using various techniques. In measurement of topography, power spectral density (PSD) is a promising method to quantify typical surface parameters and develop scale-specific interpretations. PSD can also be used to indicate how the process modifies topography at different scales. However, generating an accurate and meaningful topographic PSD of an SRF surface requires careful analysis and optimization. In this report, niobium surfaces with different process histories are sampled with atomic force microscopy and stylus profilometry and analyzed to trace topography evolution at different scales. An optimized PSD analysis protocol to serve SRF needs is presented.

  13. Parameter Optimization for Laser Polishing of Niobium for SRF Applications

    SciTech Connect

    Zhao, Liang; Klopf, John Michael; Reece, Charles E.; Kelley, Michael J.

    2013-06-01

    Surface smoothness is critical to the performance of SRF cavities. As laser technology has been widely applied to metal machining and surface treatment, we are encouraged to use it on niobium as an alternative to the traditional wet polishing process where aggressive chemicals are involved. In this study, we describe progress toward smoothing by optimizing laser parameters on BCP treated niobium surfaces. Results shows that microsmoothing of the surface without ablation is achievable.

  14. Characterization of electron beam melted uranium - 6% niobium ingots

    SciTech Connect

    McKoon, R.H.

    1997-10-31

    A study was undertaken at Lawrence Livermore National Laboratory to characterize uranium, 6{percent} niobium ingots produced via electron beam melting,hearth refining and continuous casting and to compare this material with conventional VIM/skull melt /VAR material. Samples of both the ingot and feed material were analyzed for niobium, trace metallic elements, carbon, oxygen and nitrogen. Ingot samples were also inspected metallographically and via microprobe analysis.

  15. International strategic minerals inventory summary report; niobium (columbium) and tantalum

    USGS Publications Warehouse

    Crockett, R.N.; Sutphin, D.M.

    1993-01-01

    Major world resources of niobium and tantalum are described in this summary report of information in the International Strategic Minerals Inventory (ISMI). ISMI is a cooperative data-collection effort of earth-science and mineral-resource agencies in Australia, Canada, the Federal Republic of Germany, the Republic of South Africa, the United Kingdom, and the United States of America. Part I of this report presents an overview of the resources and potential supply of niobium and tantalum based on inventory information; Part II contains tables of both geologic and mineral-resource information and includes production data collected by ISMI participants. Niobium is used principally as an alloying element in special steels and superalloys, and tantalum is used mainly in electronics. Minerals in the columbite-tantalite series are principal ore minerals of niobium and tantalum. Pyrochlore is a principal source of niobium. These minerals are found in carbonatite, certain rocks in alkaline igneous complexes, pegmatite, and placer deposits. ISMI estimates show that there are over 7 million metric tons of niobium and almost 0.5 million metric tons of tantalum in known deposits, outside of China and the former Soviet Union, for which reliable estimates have been made. Brazilian deposits, followed by Canadian deposits, contain by far the largest source of niobium. Tantalum production is spread widely among several countries, and Brazil and Canada are the most significant of these producers. Brazil's position is further strengthened by potential byproduct columbite from tin mining. Present economically exploitable resources of niobium appear to be sufficient for the near future, but Brazil will continue to be the predominant world supplier of ferrocolumbium. Tantalum, a byproduct of tin production, has been captive to the fluctuations of that market, but resources in pegmatite in Canada and Australia make it likely that future increases in the present modest demand will be met.

  16. Grain boundary niobium carbides in Inconel 718

    SciTech Connect

    Gao, M.; Wei, R.P.

    1997-12-15

    A coordinated, multidisciplinary investigation was conducted to determine the mechanisms and rate controlling processes for environmentally assisted crack growth under sustained (static) loading in Inconel 718 at elevated temperatures. The results showed that oxygen had a significant influence on crack growth, increasing the crack growth rate, for example, by nearly four orders of magnitude at 973 K. Based on results from the companion surface chemical and metallurgical studies, it was suggested that the mechanism for crack growth enhancement by oxygen was the formation and fracture of a brittle niobium oxide (Nb{sub 2}O{sub 5}-type) film on the grain boundary surfaces. The Nb came principally from the oxidation and decomposition of NbC (or Nb-rich carbides) at the grain boundaries, and crack growth was controlled by the rate of oxidation and decomposition of these carbides. Because there was extensive oxidation of the primary NbC, these carbides were implicitly considered to be the primary source of Nb. Although these carbides were large and contained substantial amounts of Nb, they were too few and spaced too far apart to be of concern (averaging one NbC for two grain boundary facets and spaced about 25 {micro}m apart). To wit, whether the freed Nb could diffuse over such a large distance and be oxidized to support the postulated mechanism for crack growth? The presence of other Nb-rich carbides elsewhere on the grain boundaries, or other sources for Nb, therefore, needs to be re-examined and is the focus of this study. In this paper, the results of a study of grain boundary niobium carbides and their distribution in Inconel 718 are reported, and are discussed in terms of their contribution to crack growth.

  17. Niobium (columbium) and tantalum resources of Brazil

    USGS Publications Warehouse

    White, Max Gregg

    1975-01-01

    Most of the niobium resources of Brazil occur as pyrochlore in carbonatites within syenitic intrusives of Late Cretaceous to early Tertiary age in western Minas Gerais and southeastern Goils. Minor amounts of it are produced together with tantalum from columbite-tantalite concentrates from pegmatites and placers adjacent to them, in the Sao Joao del Rei district in south-central Minas Gerais. All the niobium and tantalum produced in Brazil is exported. The only pyrochlore mined is from the Barreiro carbonatite deposit near Araxa in Minas Gerais where concentrates and ferroniobium are produced. Exploration work for pyrochlore and other mineral resources are being undertaken on other carbonatites, particularly at Catalao I in southeast Goias and at Tapira and Serra Negra in western Minas Gerais. Annual production and export from the Barreiro deposit are about 8,000 metric tons of pyrochlore concentrate containing about 60 percent Nb205 and about 2,700 metric tons of ferroniobium with 63 percent Nb2O5. The annual production capacity of the Barreiro plant is 18,000 tons of concentrate and 4,000 tons of ferroniobium. Ore reserves of the Barreiro deposit in all categories are 380 million tons with percent Nb2O5. Annual production of tantalite-columbite from the Sao Joao del Rei district, most of which is exported to the United States, is about 290 tons, of which about 79 percent is tantalite and about percent is columbite. Reserves of tantalite-columbite in the Sao Joao del Rei district are about 43,000 tons of proved and 73,000 tons of probable ore.

  18. Titanium-niobium, a new finishing wire alloy.

    PubMed

    Dalstra, M; Denes, G; Melsen, B

    2000-02-01

    The mechanical properties of the newly introduced titanium-niobium finishing wires were investigated. Both in bending and torsional loading mode, the stiffness, yield point, post-yield behavior, and springback of titanium-niobium wires were experimentally determined and compared to those of equally sized stainless steel wires. The experimentally obtained values were also validated with theoretical values from engineering formulas of cantilever deformations. The ratios for these parameters for the two materials proved to be different in bending and torsion. The stiffness of titanium-niobium in bending is roughly half of that of stainless steel, whereas in torsion it is roughly one-third. These characteristics enable the clinician to use titanium-niobium for creative bends without the excessive force levels of steel wires. The springback of titanium-niobium in bending is 14% lower than that of steel, whereas in torsion it is about the same or even slightly higher than that of steel, thus making it possible to utilize the wire for even major third-order corrections. Finally, the weldability of titanium-niobium wires was found to be good, so it is possible to weld wires of different dimensions together for the generation of differentiated force systems. PMID:11168279

  19. Recent developments in high purity niobium metal production at CBMM

    SciTech Connect

    Abdo, Gustavo Giovanni Ribeiro Sousa, Clovis Antonio de Faria Guimarães, Rogério Contato Ribas, Rogério Marques Vieira, Alaércio Salvador Martins Menezes, Andréia Duarte Fridman, Daniel Pallos Cruz, Edmundo Burgos

    2015-12-04

    CBMM is a global supplier of high quality niobium products including pure niobium, the focus of this paper. CBMM’s position has been consolidated over three decades of producing high purity niobium metal ingots. The company supplies, among other products, commercial and reactor grade niobium ingots. One of the main uses of CBMM’s ingots is for the manufacture of particle accelerators (superconducting radio frequency – SRF – cavities), where the purity and homogeneity of niobium metal is essentially important for good performance. CBMM constantly strives to improve process controls and product quality, and is currently implementing innovations in production, research and development to further improve ingot quality. The main aim is to reduce the content of interstitial elements, such as nitrogen (N), oxygen (O), carbon (C), and hydrogen (H), starting with the raw materials through the final step of ingot production. CBMM held the first trial to produce the world’s largest-diameter niobium ingot (as cast 535 mm). The results of this initial trial presented very low levels of interstitial impurities (N, O, C, H), allowing the achievement of residual resistivity ratio (RRR) values very close to 300 in a six-melt process in an electron beam furnace. These values were reached with 850 ppm of tantalum. SRF cavities will be produced with this material in order to study the effect of low impurities and high RRR on the Q factor and accelerating gradient.

  20. Field determination of microgram quantities of niobium in rocks

    USGS Publications Warehouse

    Ward, F.N.; Marranzino, A.P.

    1955-01-01

    A rapid, simple, and moderately accurate method was needed for the determination of traces of niobium in rocks. The method developed is based on the reaction of niobium(V) with thiocyanate ion in a 4M hydrochloric acid and 0.5M tartaric acid medium, after which the complex is extracted with ethyl ether. The proposed procedure is applicable to rocks containing from 50 to 2000 p.p.m. of niobium, and, with modifications, can be used on rocks containing larger amounts. Five determinations on two rocks containing 100 p.p.m. or less of niobium agree within 5 p.p.m. of the mean, and the confidence limits at the 95% level are, respectively, ??6 and ??4 p.p.m. The addition of acetone to the ether extract of the niobium thiocyanate inhibits the polymerization of the thiocyanate ion and stabilizes the solution for at least 20 hours. The proposed procedure permits the determination of 20 ?? of niobium in the presence of 1000 ?? of iron, titanium, or uranium; 500 ?? of vanadium; or 100 ?? of tungsten or molybdenum or both.

  1. Recent developments in high purity niobium metal production at CBMM

    NASA Astrophysics Data System (ADS)

    Abdo, Gustavo Giovanni Ribeiro; Sousa, Clovis Antonio de Faria; Guimarães, Rogério Contato; Ribas, Rogério Marques; Vieira, Alaércio Salvador Martins; Menezes, Andréia Duarte; Fridman, Daniel Pallos; Cruz, Edmundo Burgos

    2015-12-01

    CBMM is a global supplier of high quality niobium products including pure niobium, the focus of this paper. CBMM's position has been consolidated over three decades of producing high purity niobium metal ingots. The company supplies, among other products, commercial and reactor grade niobium ingots. One of the main uses of CBMM's ingots is for the manufacture of particle accelerators (superconducting radio frequency - SRF - cavities), where the purity and homogeneity of niobium metal is essentially important for good performance. CBMM constantly strives to improve process controls and product quality, and is currently implementing innovations in production, research and development to further improve ingot quality. The main aim is to reduce the content of interstitial elements, such as nitrogen (N), oxygen (O), carbon (C), and hydrogen (H), starting with the raw materials through the final step of ingot production. CBMM held the first trial to produce the world's largest-diameter niobium ingot (as cast 535 mm). The results of this initial trial presented very low levels of interstitial impurities (N, O, C, H), allowing the achievement of residual resistivity ratio (RRR) values very close to 300 in a six-melt process in an electron beam furnace. These values were reached with 850 ppm of tantalum. SRF cavities will be produced with this material in order to study the effect of low impurities and high RRR on the Q factor and accelerating gradient.

  2. Determination of niobium in the parts per million range in rocks

    USGS Publications Warehouse

    Grimaldi, F.S.

    1960-01-01

    A modified niobium thiocyanate spectrophotometric procedure relatively insensitive to titanium interference is presented. Elements such as tungsten, molybdenum, vanadium, and rhenium, which seriously interfere in the spectrophotometric determination of niobium, are separated by simple sodium hydroxide fusion and leach; iron and magnesium are used as carriers for the niobium. Tolerance limits are given for 28 elements in the spectrophotometric method. Specific application is made to the determination of niobium in the parts per million range in rocks. The granite G-1 contains 0.0022% niobium and the diabase W-1 0.00096% niobium.

  3. Thermal transport properties of niobium and some niobium base alloys from 80 to 1600/sup 0/K

    SciTech Connect

    Moore, J.P.; Graves, R.S.; Williams, R.K.

    1980-01-01

    The electrical resistivities and absolute Seebeck coefficients of 99.8 at. % niobium with a RRR of 36, Nb-4.8 at. % W, Nb-5 at. % Mo, Nb-10 at. % Mo, and Nb-2.4 at. % Mo-2.4 at. % Zr were measured from 80 to 1600/sup 0/K, and the thermal conductivities of the niobium and Nb-5 at. % W were measured from 80 to 1300/sup 0/K. A technique is described for measuring the electrical resistivity and Seebeck coefficient of a specimen during radial heat flow measurements of the thermal conductivity. The transport property results, which had uncertainties of +-0.4%for electrical resistivity and +-1.4% for thermal conductivity, showed the influence of tungsten and molybdenum solutes on the transport properties of niobium and were used to obtain the electronic Lorenz function of pure niobium, which was found to approach the Sommerfeld value at high temperatures.

  4. Physical and Mechanical Properties of Niobium for SRF Science and Technology

    SciTech Connect

    Ganapati Rao Myneni

    2006-10-31

    Optimized mechanical and physical properties of high purity niobium are crucial for obtaining high performance SRF particle beam accelerator structures consistently. This paper summarizes these important material properties for both high purity polycrystalline and single crystal niobium.

  5. Niobium-based superconducting nano-device fabrication using all-metal suspended masks

    NASA Astrophysics Data System (ADS)

    Samaddar, S.; van Zanten, D.; Fay, A.; Sacépé, B.; Courtois, H.; Winkelmann, C. B.

    2013-09-01

    We report a novel method for the fabrication of superconducting nano-devices based on niobium. The well-known difficulties of lithographic patterning of high-quality niobium are overcome by replacing the usual organic resist mask by a metallic one. The quality of the fabrication procedure is demonstrated by the realization and characterization of long and narrow superconducting lines and niobium-gold-niobium proximity SQUIDs.

  6. Single crystal niobium tubes for particle colliders accelerator cavities

    SciTech Connect

    Murphy, James E

    2013-02-28

    The objective of this research project is to produce single crystal niobium (Nb) tubes for use as particle accelerator cavities for the Fermi laboratory’s International Linear Collider project. Single crystal Nb tubes may have superior performance compared to a polycrystalline tubes because the absence of grain boundaries may permit the use of higher accelerating voltages. In addition, Nb tubes that are subjected to the high temperature, high vacuum crystallization process are very pure and well annealed. Any impurity with a significantly higher vapor pressure than Nb should be decreased by the relatively long exposure at high temperature to the high vacuum environment. After application of the single crystal process, the surfaces of the Nb tubes are bright and shiny, and the tube resembles an electro polished Nb tube. For these reasons, there is interest in single crystal Nb tubes and in a process that will produce single crystal tubes. To convert a polycrystalline niobium tube into a single crystal, the tube is heated to within a few hundred °C of the melting temperature of niobium, which is 2477 °C. RF heating is used to rapidly heat the tube in a narrow zone and after reaching the operating temperature, the hot zone is slowly passed along the length of the tube. For crystallization tests with Nb tubes, the traverse rate was in the range of 1-10 cm per hour. All the crystallization tests in this study were performed in a water-cooled, stainless steel chamber under a vacuum of 5 x10-6 torr or better. In earliest tests of the single crystal growth process, the Nb tubes had an OD of 1.9 cm and a wall thickness of 0.15 mm. With these relatively small Nb tubes, the single crystal process was always successful in producing single crystal tubes. In these early tests, the operating temperature was normally maintained at 2200 °C, and the traverse rate was 5 cm per hour. In the next test series, the Nb tube size was increased to 3.8 cm OD and the wall thickness was

  7. Structure and texture of electrolytic superconducting coatings of high-purity niobium

    NASA Astrophysics Data System (ADS)

    Kolosov, V. N.; Shevyrev, A. A.

    2014-08-01

    Modes of epitaxial growth of electrolytic superconducting coatings of high-purity niobium on substrates of niobium, molybdenum, and tungsten have been investigated. The dynamics of changes in the structure and texture of the coatings depending on the method of treatment of substrates, cathode current density, and thickness of the deposited niobium layer has been studied.

  8. Elucidating the Band Gap of Niobium Dioxide

    NASA Astrophysics Data System (ADS)

    O'Hara, Andrew; Vigil-Fowler, Derek; Louie, Steven G.; Demkov, Alexander A.

    2015-03-01

    Like VO2, niobium dioxide (NbO2) belongs to the family of transition metal oxides with a temperature-driven metal-to-insulator transition. However, NbO2 has received considerably less attention, and several open questions about the material remain. One such question, of both practical and fundamental importance, is the nature and size of the band gap in the low-temperature, distorted rutile phase with a range reported for the gap of 0.5 eV to 1.2 eV. In this work, we investigate the low-temperature phase, utilizing several methodologies - density functional theory within the standard local density approximation (LDA), LDA +U, hybrid functional, and the GW approximation, to better understand the physics of the band gap in NbO2. Comparisons of the calculations are made to recent experimental work on NbO2 utilizing photoemission spectroscopy and ellipsometry. This work is supported by DOE under the SciDAC program, the NSF, and SRC.

  9. SRF niobium characterization using SIMS and FIB-TEM

    NASA Astrophysics Data System (ADS)

    Stevie, F. A.

    2015-12-01

    Our understanding of superconducting radio frequency (SRF) accelerator cavities has been improved by elemental analysis at high depth resolution and by high magnification microscopy. This paper summarizes the technique development and the results obtained on poly-crystalline, large grain, and single crystal SRF niobium. Focused ion beam made possible sample preparation using transmission electron microscopy and the images obtained showed a very uniform oxide layer for all samples analyzed. Secondary ion mass spectrometry indicated the presence of a high concentration of hydrogen and the hydrogen content exhibited a relationship with improvement in performance. Depth profiles of carbon, nitrogen, and oxygen did not show major differences with heat treatment. Niobium oxide less than 10 nm thick was shown to be an effective hydrogen barrier. Niobium with titanium contamination showed unexpected performance improvement.

  10. Precipitation of hydrides in high purity niobium after different treatments

    SciTech Connect

    Barkov, F.; Romanenko, A.; Trenikhina, Y.; Grassellino, A.

    2013-01-01

    Precipitation of lossy non-superconducting niobium hydrides represents a known problem for high purity niobium in superconducting applications. Using cryogenic optical and laser confocal scanning microscopy we have directly observed surface precipitation and evolution of niobium hydrides in samples after different treatments used for superconducting RF cavities for particle acceleration. Precipitation is shown to occur throughout the sample volume, and the growth of hydrides is well described by the fast diffusion-controlled process in which almost all hydrogen is precipitated at $T=140$~K within $\\sim30$~min. 120$^{\\circ}$C baking and mechanical deformation are found to affect hydride precipitation through their influence on the number of nucleation and trapping centers.

  11. Superconducting DC and RF Properties of Ingot Niobium

    SciTech Connect

    Pashupati Dhakal, Gianluigi Ciovati, Peter Kneisel, Ganapati Rao Myneni

    2011-07-01

    The thermal conductivity, DC magnetization and penetration depth of large-grain niobium hollow cylindrical rods fabricated from ingots, manufactured by CBMM subjected to chemical and heat treatment were measured. The results confirm the influence of chemical and heat-treatment processes on the superconducting properties, with no significant dependence on the impurity concentrations in the original ingots. Furthermore, RF properties, such as the surface resistance and quench field of the niobium rods were measured using a TE{sub 011} cavity. The hollow niobium rod is the center conductor of this cavity, converting it to a coaxial cavity. The quench field is limited by the critical heat flux through the rods' cooling channel.

  12. SRF niobium characterization using SIMS and FIB-TEM

    SciTech Connect

    Stevie, F. A.

    2015-12-04

    Our understanding of superconducting radio frequency (SRF) accelerator cavities has been improved by elemental analysis at high depth resolution and by high magnification microscopy. This paper summarizes the technique development and the results obtained on poly-crystalline, large grain, and single crystal SRF niobium. Focused ion beam made possible sample preparation using transmission electron microscopy and the images obtained showed a very uniform oxide layer for all samples analyzed. Secondary ion mass spectrometry indicated the presence of a high concentration of hydrogen and the hydrogen content exhibited a relationship with improvement in performance. Depth profiles of carbon, nitrogen, and oxygen did not show major differences with heat treatment. Niobium oxide less than 10 nm thick was shown to be an effective hydrogen barrier. Niobium with titanium contamination showed unexpected performance improvement.

  13. Interfacial fracture toughness of alumina/niobium systems

    SciTech Connect

    Stout, M.G. ); O'Dowd, N.P.; Shih, C.F. . Div. of Engineering)

    1991-01-01

    The interfacial fracture toughness of an alumina/niobium composite has been measured as a function of phase angle. The interface was formed by solid-state bonding bulk Coor's AD-999 fine-grain alumina with a commercial purity niobium at 1600{degrees}C for 0.5 hr under a pressure of 10.5 MPa. The alumina/niobium system has a number of features which makes it ideal for an investigation of interfacial fracture toughness. From HREM data we estimate that the width of the interface is no more than 10 atomic planes. Furthermore the thermal expansion coefficients of the two materials differ by less than 5% so residual stresses due to the bonding process are small. Using symmetric and asymmetric four point bend specimens we have measured the fracture toughness of homogenous alumina and that of the alumina/niobium bimaterial in combinations of in-plane shear and tension. The fracture toughness of the homogenous alumina is relatively insensitive to the loading phase. The measured fracture toughness K{sub c} of the interface, however, depended strongly on phase angle. We were unable to obtain valid alumina/niobium interfacial toughness data at negative phase angles as the fracture initiates in the alumina and not at the interface. In symmetric bending at a phase angle {approx}5{degrees}, we measured a nominal interface toughness of 4.0 MPa{radical}m, comparable to the homogeneous alumina. We found that the toughness increased with loading phase angle to a value of K{sub c} {approx} 9 MPa{radical}m at a phase between 25{degrees} and 40{degrees}. Preliminary calculations and experiments suggest that this effect is due to an asymmetric stress distribution, with respect to the interface, and plastic deformation in the niobium. 12 refs., 9 figs., 1 tab.

  14. Effect of Surface Flow on Topography in Niobium Electropolishing

    SciTech Connect

    M.J. Kelley, C.E. Reece, L. Zhao

    2011-03-01

    Electropolishing (EP) is reliably delivering improved performance of multi-celled niobium SRF accelerator cavities, attributed to the smoother surface obtained. This superior leveling is a consequence of an etchant concentration gradient layer that arises in the HF-H2SO4 electrolyte adjacent to the niobium surface during polishing. Electrolyte circulation raises the prospect that fluid flow adjacent to the surface might affect the diffusion layer and impair EP performance. In this study, preliminary bench-top experiments with a moving electrode apparatus were conducted. We find that flow conditions approximating cavity EP show no effects attributable to depletion layer disruption.

  15. Study of AC/RF properties of SRF ingot niobium

    SciTech Connect

    Dhakal, Pashupati; Tsindlekht, Menachem I; Genkin, Valery M; Ciovati, Gianluigi; Myneni, Ganapati Rao

    2013-09-01

    In an attempt to correlate the performance of superconducting radiofrequency cavities made of niobium with the superconducting properties, we present the results of the magnetization and ac susceptibility of the niobium used in the superconducting radiofrequency cavity fabrication. The samples were subjected to buffer chemical polishing (BCP) surface and high temperature heat treatments, typically applied to the cavities fabrications. The analysis of the results show the different surface and bulk ac conductivity for the samples subjected to BCP and heat treatment. Furthermore, the RF surface impedance is measured on the sample using a TE011 microwave cavity for a comparison to the low frequency measurements.

  16. PROCESS OF PRODUCING A NIOBIUM-TIN COMPOUND

    DOEpatents

    Zegler, S.T.; Darby, J.B. Jr.

    1963-04-01

    This patent deals with a process of preparing pure Nb/sub 3/Sn. The process comprises heating powders of niobium and excess tin to 900 to 1000 deg C, whereby niobium reacts with the molten tin under the formation of Nb/sub 3/Sn; cooling and powdering the product and immersing the powder in concentrated hydrochloric acid for removal of excessive tin; separating the Nb/sub 3/Sn, rinsing and drying it and sintering it in an inert atmosphere at 900 to 1300 deg C. (AEC)

  17. America's Overview of Superconducting Science and Technology of Ingot Niobium

    SciTech Connect

    Gianluigi Ciovati, Peter Kneisel, Ganapati Myneni

    2011-03-01

    This contribution will present an overview of the results from R&D programs in the USA over the past four years towards the development of ingot Niobium as a viable alternative material to fabricate SRF cavities for particle accelerators. Activities at several laboratories and universities include fabrication, surface treatment and RF testing of single- and multi-cell cavities and studies of the thermal, mechanical and superconducting properties of samples from ingots of different purity. Possible advantages of ingot niobium over standard fine-grain (ASTM 6) are discussed and a streamlined treatment procedure to fully exploit those advantages is proposed.

  18. Niobium-Matrix-Composite High-Temperature Turbine Blades

    NASA Technical Reports Server (NTRS)

    Kaplan, Richard B.; Tuffias, Robert H.; La Ferla, Raffaele; Heng, Sangvavann; Harding, John T.

    1995-01-01

    High-temperture composite-material turbine blades comprising mainly niobium matrices reinforced with refractory-material fibers being developed. Of refractory fibrous materials investigated, FP-AL(2)0(3), tungsten, and polymer-based SiC fibers most promising. Blade of this type hollow and formed in nearly net shape by wrapping mesh of reinforcing refractory fibers around molybdenum mandrel, then using thermal-gradient chemical-vapor infiltration (CVI) to fill interstices with niobium. CVI process controllable and repeatable, and kinetics of both deposition and infiltration well understood.

  19. Niobium enrichment and environmental enhancement of creep crack growth in nickel-base superalloys

    SciTech Connect

    Gao, M.; Wei, R.P.; Dwyer, D.J.

    1995-04-15

    In this paper, the possible role of niobium in the environmental enhancement of creep crack growth in nickel-base superalloys is further examined. The examination included (1) surface enrichment of Nb in a commercial Inconel 718; (2) a source of niobium and its interaction with oxygen; (3) preferential oxidation of Nb at the crack tip, and (4) correlations between environmental sensitivity and niobium concentration of nickel-base superalloys from the literature. The role of niobium was suggested by recent X-ray photoelectron spectroscopic (XPS) studies. The XPS studies show a significant increase in the concentration of niobium on the (001) surface of an Inconel 718 single crystal after heating at temperatures above 775 K. Considerable segregation of niobium was also found on the grain boundaries of a thermally aged commercial (polycrystalline) Inconel 718. The CCGR data showed significant enhancement by oxygen and water vapor at temperatures of 800--975 K where niobium enrichment occurred.

  20. Variation of Mechanical Properties of High RRR And Reactor Grade Niobium With Heat Treatments

    SciTech Connect

    Ganapati Myneni; H. Umezawa

    2003-06-01

    Superconducting rf cavities used as accelerating structures in particle accelerators are made from high purity niobium with residual resistance ratios greater than 250. Reactor grade niobium is also used to make wave-guide and/or end group components for these accelerating structures. The major impurities in this type of niobium are interstitially dissolved gases such as hydrogen, nitrogen, and oxygen in addition to carbon. After fabricating the niobium accelerating structures, they are subjected to heat treatments for several hours in vacuum at temperatures of up to 900 C for degassing hydrogen or up to 1400 C for improving the thermal conductivity of niobium considerably. These heat treatments are affecting the mechanical properties of niobium drastically. In this paper the variation of the mechanical properties of high purity and reactor grade niobium with heat treatments in a vacuum of {approx} 10{sup -6} Torr and temperatures from 600 C to 1250 C for periods of 10 to 6 hours are presented.

  1. Mechanical properties of niobium radio-frequency cavities

    SciTech Connect

    Ciovati, Gianluigi; Dhakal, Pashupati; Matalevich, Joseph R.; Myneni, Ganapati Rao; Schmidt, A.; Iversen, J.; Matheisen, A.; Singer, W.

    2015-07-02

    Radio-frequency cavities made of bulk niobium are one of the components used in modern particle accelerators. The mechanical stability is an important aspect of cavity design, which typically relies on finite-element analysis simulations using material properties from tensile tests on sample. This contribution presents the results of strain and resonant frequency measurements as a function of a uniform pressure up to 722 kPa, applied to single-cell niobium cavities with different crystallographic structure, purity and treatments. In addition, burst tests of high-purity multi-cell cavities with different crystallographic structure have been conducted up to the tensile strength of the material. Finite-element analysis of the single-cell cavity geometry is in good agreement with the observed behavior in the elastic regime assuming a Young's modulus value of 88.5 GPa and a Poisson's ratio of 0.4, regardless of crystallographic structure, purity or treatment. However, the measured yield strength and tensile strength depend on crystallographic structure, material purity and treatment. In particular, the results from this study show that the mechanical properties of niobium cavities with large crystals are comparable to those of cavities made of fine-grain niobium.

  2. High-Q superconducting niobium cavities for gravitational wave detectors

    NASA Astrophysics Data System (ADS)

    de Paula, L. A. N.; Furtado, S. R.; Aguiar, O. D.; Oliveira, N. F., Jr.; Castro, P. J.; Barroso, J. J.

    2014-10-01

    The main purpose of this work is to optimize the electric Q-factor of superconducting niobium klystron cavities to be used in parametric transducers of the Mario Schenberg gravitational wave detector. Many cavities were manufactured from niobium with relatively high tantalum impurities (1420 ppm) and they were cryogenically tested to determine their resonance frequencies, unloaded electrical quality factors (Q0) and electromagnetic couplings. These cavities were closed with a flat niobium plate with tantalum impurities below 1000 ppm and an unloaded electrical quality factors of the order of 105 have been obtained. AC conductivity of the order of 1012 S/m has been found for niobium cavities when matching experimental results with computational simulations. These values for the Q-factor would allow the detector to reach the quantum limit of sensitivity of ~ 10-22 Hz-1/2 in the near future, making it possible to search for gravitational waves around 3.2 kHz. The experimental tests were performed at the laboratories of the National Institute for Space Research (INPE) and at the Institute for Advanced Studies (IEAv - CTA).

  3. Stress dependent oxidation of sputtered niobium and effects on superconductivity

    SciTech Connect

    David Henry, M. Wolfley, Steve; Monson, Todd; Clark, Blythe G.; Shaner, Eric; Jarecki, Robert

    2014-02-28

    We report on the suppression of room temperature oxidation of DC sputtered niobium films and the effects upon the superconductive transition temperature, T{sub c}. Niobium was sputter-deposited on silicon dioxide coated 150 mm wafers and permitted to oxidize at room temperature and pressure for up to two years. Resistivity and stress measurements indicate that tensile films greater than 400 MPa resist bulk oxidation with measurements using transmission electron microscope, electron dispersive X-ray spectroscopy, x-ray photoelectric spectroscopy, and secondary ion mass spectrometry confirming this result. Although a surface oxide, Nb{sub 2}O{sub 5}, consumed the top 6–10 nm, we measure less than 1 at. % oxygen and nitrogen in the bulk of the films after the oxidation period. T{sub c} measurements using a SQUID magnetometer indicate that the tensile films maintained a T{sub c} approaching the dirty superconductive limit of 8.4 K after two years of oxidation while maintaining room temperature sheet resistance. This work demonstrates that control over niobium film stress during deposition can prevent bulk oxidation by limiting the vertical grain boundaries ability to oxidize, prolonging the superconductive properties of sputtered niobium when exposed to atmosphere.

  4. Cu-Nb-Si (Copper-Niobium-Silicon)

    NASA Astrophysics Data System (ADS)

    Materials Science International Team MSIT

    This document is part of Subvolume C2 'Non-Ferrous Metal Systems. Part 2: Selected Copper Systems' of Volume 11 'Ternary Alloy Systems - Phase Diagrams, Crystallographic and Thermodynamic Data critically evaluated by MSIT®' of Landolt-Börnstein - Group IV 'Physical Chemistry'. It provides data of the ternary system Copper-Niobium-Silicon.

  5. Ordering in non-stoichiometric carbides of niobium and tantalum

    SciTech Connect

    Markhasev, B.I.; Pilipovskii, Yu. L.; Shamatov, Yu. M.; Svintsova, S.E.

    1986-03-01

    Ordering processes were studied in the nonstoichiometric carbides of Nb and Ta. A mechanism of slip transition was proposed for the ordering of NbC/sub 2/, accompanied by precipitation of niobium metal. A diagram of the restructuring of the fcc lattice of NbC to the bcc lattice of Nb is presented.

  6. Carbon-supported and alumina-supported niobium sulfide catalysts

    SciTech Connect

    Allali, N.; Marie, A.M.; Danot, M.

    1995-10-01

    Few studies deal with the properties of niobium sulfide as a hydrodesulfurization catalyst. In this paper, the preparation of carbon-supported niobium sulfide catalysts was optimized concerning (i) the nature of the soluble precursor, (ii) the drying process, and (iii) the sulfurizing treatment, which was always performed under atmospheric pressure but for different H{sub 2}S-based flows and reaction temperatures. The activities of the best samples prepared with niobium oxalate as the impregnation salt, drying at room temperature, and presulfurization with N{sub 2}/H{sub 2}S at 400{degrees}C are superior to that of a supported MoS{sub 2} reference catalyst. Alumina-supported systems can be sulfurized only under more severe conditions (CS{sub 2} under pressure). After optimization of the sulfurization treatment (400{degrees}C, 10 h) the maximum activity obtained is significantly higher than that of a molybdenum sulfide reference catalyst. The catalytic activities of the various catalysts studied are related to their morphological and chemical characteristics using TPR and EXAFS measurements. The work illustrates the importance of the support and the sulfurization method on the genesis of a niobium sulfide active phase. 37 refs., 7 figs., 4 tabs.

  7. Mechanical properties of niobium radio-frequency cavities

    DOE PAGESBeta

    Ciovati, Gianluigi; Dhakal, Pashupati; Matalevich, Joseph R.; Myneni, Ganapati Rao; Schmidt, A.; Iversen, J.; Matheisen, A.; Singer, W.

    2015-07-02

    Radio-frequency cavities made of bulk niobium are one of the components used in modern particle accelerators. The mechanical stability is an important aspect of cavity design, which typically relies on finite-element analysis simulations using material properties from tensile tests on sample. This contribution presents the results of strain and resonant frequency measurements as a function of a uniform pressure up to 722 kPa, applied to single-cell niobium cavities with different crystallographic structure, purity and treatments. In addition, burst tests of high-purity multi-cell cavities with different crystallographic structure have been conducted up to the tensile strength of the material. Finite-element analysismore » of the single-cell cavity geometry is in good agreement with the observed behavior in the elastic regime assuming a Young's modulus value of 88.5 GPa and a Poisson's ratio of 0.4, regardless of crystallographic structure, purity or treatment. However, the measured yield strength and tensile strength depend on crystallographic structure, material purity and treatment. In particular, the results from this study show that the mechanical properties of niobium cavities with large crystals are comparable to those of cavities made of fine-grain niobium.« less

  8. Stress dependent oxidation of sputtered niobium and effects on superconductivity

    NASA Astrophysics Data System (ADS)

    David Henry, M.; Wolfley, Steve; Monson, Todd; Clark, Blythe G.; Shaner, Eric; Jarecki, Robert

    2014-02-01

    We report on the suppression of room temperature oxidation of DC sputtered niobium films and the effects upon the superconductive transition temperature, Tc. Niobium was sputter-deposited on silicon dioxide coated 150 mm wafers and permitted to oxidize at room temperature and pressure for up to two years. Resistivity and stress measurements indicate that tensile films greater than 400 MPa resist bulk oxidation with measurements using transmission electron microscope, electron dispersive X-ray spectroscopy, x-ray photoelectric spectroscopy, and secondary ion mass spectrometry confirming this result. Although a surface oxide, Nb2O5, consumed the top 6-10 nm, we measure less than 1 at. % oxygen and nitrogen in the bulk of the films after the oxidation period. Tc measurements using a SQUID magnetometer indicate that the tensile films maintained a Tc approaching the dirty superconductive limit of 8.4 K after two years of oxidation while maintaining room temperature sheet resistance. This work demonstrates that control over niobium film stress during deposition can prevent bulk oxidation by limiting the vertical grain boundaries ability to oxidize, prolonging the superconductive properties of sputtered niobium when exposed to atmosphere.

  9. High-Temperature Creep Behavior Of Fiber-Reinforced Niobium

    NASA Technical Reports Server (NTRS)

    Petrasek, Donald W.; Titran, Robert H.

    1990-01-01

    Study conducted to determine feasibility of using composite materials in advanced space power systems, described in 22-page report. Tungsten fibers reduce creep and mass in advanced power systems. Reinforcing niobium alloys with tungsten fibers increases their resistances to creep by factors of as much as 10.

  10. Superconducting niobium thin film slow-wave structures

    NASA Technical Reports Server (NTRS)

    Bautista, J. J.; Petty, S. M.; Allen, L. H.; Beasley, M. R.; Hammond, R. H.

    1983-01-01

    A superconducting comb structure as a slow-wave element in a traveling-wave maser will significantly improve maser noise temperature and gain by reducing the insertion loss. The results of the insertion loss measurements of superconducting niobium slow-wave structures subjected to maser operating conditions at X-Band frequencies are presented.

  11. Oxidation Behavior of Binary Niobium Alloys

    NASA Technical Reports Server (NTRS)

    Barrett, Charles A.; Corey, James L.

    1960-01-01

    This investigation concludes a study to determine the effects of up to 25 atomic percent of 55 alloying additions on the oxidation characteristics of niobium. The alloys were evaluated by oxidizing in an air atmosphere for 4 hours at 1000 C and 2 hours at 1200 C. Titanium and chromium improved oxidation resistance at both evaluation conditions. Vanadium and aluminum improved oxidation resistance at 1000 C, even though the V scale tended to liquefy and the Al specimens became brittle and the scale powdery. Copper, cobalt, iron, and iridium improved oxidation resistance at 1200 C. Other investigations report tungsten and molybdenum are protective up to about 1000 C, and tantalum at 1100 C. The most important factor influencing the rate of oxidation was the ion size of the alloy additions. Ions slightly smaller than the Nb(5+) ion are soluble in the oxide lattice and tend to lower the compressive stresses in the bulk scale that lead to cracking. The solubility of the alloying addition also depends on the valence to some extent. All of the elements mentioned that improve the oxidation resistance of Nb fit this size criterion with the possible exception of Al, whose extremely small size in large concentrations would probably lead to the formation of a powdery scale. Maintenance of a crack-free bulk scale for as long as possible may contribute to the formation of a dark subscale that ultimately is rate- controlling in the oxidation process. The platinum-group metals, especially Ir, appear to protect by entrapment of the finely dispersed alloying element by the incoming Nb2O5 metal-oxide interface. This inert metallic Ir when alloyed in a sufficient amount with Yb appears to give a ductile phase dispersed in the brittle oxide. This scale would then flow more easily to relieve the large compressive stresses to delay cracking. Complex oxide formation (which both Ti and Zr tend to initiate) and valence effects, which probably change the vacancy concentration in the scale

  12. Equilibrium properties of the fluxoid lattice in single-crystal niobium. II. Small-angle neutron-diffraction measurements

    SciTech Connect

    Christen, D.K.; Kerchner, H.R.; Sekula, S.T.; Thorel, P.

    1980-01-01

    A small-angle neutron-diffraction technique has been used to measure several properties of the flux-line lattice (FLL) in a single-crystal sphere of pure niobium. For applied fields parallel to several crystallographic directions in the (100) and (110) planes, the low-field mixed state and intermediate mixed state were investigated. From these results, the orientation dependence of the low-field critical parameters H/sub c/1 and B/sub 0/ are deduced. The consistency of these results is verified by comparison with direct measurements of the equilibrium misalignment angle between the applied-field direction and the fluxoid axes. In addition, results are reported which extend the available information concerning correlations between the FLL and crystal lattice (CL) symmetry properties.

  13. Twin symmetry texture of energetically condensed niobium thin films on sapphire substrate (a-plane Al2O3)

    NASA Astrophysics Data System (ADS)

    Zhao, X.; Phillips, L.; Reece, C. E.; Seo, Kang; Krishnan, M.; Valderrama, E.

    2011-08-01

    An energetic condensation technique, cathodic arc discharge deposition, is used to grow epitaxial Niobium (Nb) thin films on a-plane sapphire (hexagonal-closed-packed Al2O3) at moderate substrate heating temperature (<400 °C). The epitaxial Nb(110)/Al2O3(1,1,-2,0) thin films reached a maximum residual resistance ratio (RRR) value 214, despite using a reactor-grade Nb cathode source whose RRR was only 30. The measurements suggest that the film's density of impurities and structural defects are lower when compared to Nb films produced by other techniques, such as magnetron sputtering, e-beam evaporation or molecular-beam-epitaxy. At lower substrate temperature, textured polycrystalline Nb thin films were created, and the films might have twin symmetry grains with {110} orientations in-plane. The texture was revealed by x-ray diffraction pole figures. The twin symmetry might be caused by a combination effect of the Nb/Al2O3 three-dimensional epitaxial relationship ("3D-Registry" Claassen's nomenclature) and the "Volmer-Weber" (Island) growth model. However, pole figures obtained by electron backscattering diffraction (EBSD) found no twin symmetry on the thin films' topmost surface (˜50 nm in depth). The EBSD pole figures showed only one Nb{110} crystal plane orientation. A possible mechanism is suggested to explain the differences between the bulk (XRD) and surface (EBSD) pole figures.

  14. First-principles calculations of niobium hydride formation in superconducting radio-frequency cavities

    SciTech Connect

    Ford, Denise C.; Cooley, Lance D.; Seidman, David N.

    2013-09-01

    Niobium hydride is suspected to be a major contributor to degradation of the quality factor of niobium superconducting radio-frequency (SRF) cavities. In this study, we connect the fundamental properties of hydrogen in niobium to SRF cavity performance and processing. We modeled several of the niobium hydride phases relevant to SRF cavities and present their thermodynamic, electronic, and geometric properties determined from calculations based on density-functional theory. We find that the absorption of hydrogen from the gas phase into niobium is exothermic and hydrogen becomes somewhat anionic. The absorption of hydrogen by niobium lattice vacancies is strongly preferred over absorption into interstitial sites. A single vacancy can accommodate six hydrogen atoms in the symmetrically equivalent lowest-energy sites and additional hydrogen in the nearby interstitial sites affected by the strain field: this indicates that a vacancy can serve as a nucleation center for hydride phase formation. Small hydride precipitates may then occur near lattice vacancies upon cooling. Vacancy clusters and extended defects should also be enriched in hydrogen, potentially resulting in extended hydride phase regions upon cooling. We also assess the phase changes in the niobium-hydrogen system based on charge transfer between niobium and hydrogen, the strain field associated with interstitial hydrogen, and the geometry of the hydride phases. The results of this study stress the importance of not only the hydrogen content in niobium, but also the recovery state of niobium for the performance of SRF cavities.

  15. Nuclear data sheets for A = 110

    NASA Astrophysics Data System (ADS)

    Gelder, P. De; Jacobs, E.; De Frenne, D.

    1983-04-01

    The 1977 evaluation on mass A=110 has been reviewed, considering all data available before October 1982. Experimental information is presented from the neutron-rich 110Tc to the neutron-deficient 110Xe. At the neutron-rich side, new information on the β-decay of 110Ru and 110Rh (3.16 s) is presented. From (n,ψ) studies, very elaborate level and ψ information in 110Ag were obtained. Also the β-decay. of 110Ag (249.76 d) was studied extensively. For 110Sn, a lot of new information is presented, resulting from decay and reaction studies. For the first time, experimental information is shown for 110Te, 110I, and 110Xe. For 110Rh and 110In, however, the relative positions of, the two isomers remain unknown in each. Theoretical studies on different properties of A=110 nuclei are reported in the adopted l evels tables.

  16. Niobium tetrahalide complexes with neutral diphosphine ligands.

    PubMed

    Benjamin, Sophie L; Chang, Yao-Pang; Hector, Andrew L; Jura, Marek; Levason, William; Reid, Gillian; Stenning, Gavin

    2016-05-10

    The reactions of NbCl4 with diphosphine ligands o-C6H4(PMe2)2, Me2PCH2CH2PMe2 or Et2PCH2CH2PEt2 in a 1 : 2 molar ratio in MeCN solution produced eight-coordinate [NbCl4(diphosphine)2]. [NbBr4(diphosphine)2] (diphosphine = o-C6H4(PMe2)2 or Me2PCH2CH2PMe2) were made similarly from NbBr4. X-ray crystal structures show that [NbCl4{o-C6H4(PMe2)2}2] has a dodecahedral geometry, but the complexes with dimethylene-backboned diphosphines are distorted square antiprisms. The Nb-P distances and niobium tetrabromide, conveniently made from NbCl4 and BBr3, is a chain polymer with edge-linked NbBr6 octahedra and alternating long and short Nb-Nb distances, the latter ascribed to Nb-Nb bonds. PMID:27094082

  17. Method for etching thin films of niboium and niobium-containing compounds for preparing superconductive circuits

    DOEpatents

    Kampwirth, R.T.; Schuller, I.K.; Falco, C.M.

    1979-11-23

    An improved method of preparing thin film superconducting electrical circuits of niobium or niobium compounds is provided in which a thin film of the niobium or niobium compound is applied to a nonconductive substrate and covered with a layer of photosensitive material. The sensitive material is in turn covered with a circuit pattern exposed and developed to form a mask of the circuit in photoresistive material on the surface of the film. The unmasked excess niobium film is removed by contacting the substrate with an aqueous etching solution of nitric acid, sulfuric acid, and hydrogen fluoride, which will rapidly etch the niobium compound without undercutting the photoresist. A modification of the etching solution will permit thin films to be lifted from the substrate without further etching.

  18. Microstructure, oxidation behavior and mechanical behavior of lens deposited niobium-titanium-silicon and niobium-titanium-silicon based alloys

    NASA Astrophysics Data System (ADS)

    Dehoff, Ryan Richard

    With current high temperature structural materials such as nickel based superalloys being pushed to the limits of suitable operating conditions, there comes a need for replacement materials with even higher temperature capabilities. Niobium silicon based systems have been shown to have superior density normalized strength at elevated temperatures when compared to currently used alloys. The drawbacks associated with the niobium silicon system are due to catastrophic oxidation behavior at elevated temperatures. Alloying addition have been shown to increase the oxidation resistance near suitable levels, but also decrease the high temperature strength and increases creep rates when compared to the binary alloy system. The microstructure of the material is similar to metal matrix composites in which high melting temperature silicides are dispersed in a niobium based matrix phase. The silicides produce high temperature strength while the niobium based matrix increases the room temperature properties such as fracture toughness. The bulk of the research has been conducted on directionally solidified material which has a coarse microstructure due to the slow cooling rates associated with the processing condition. The current research uses a powder metallurgy process termed Laser Engineered Net Shaping, or LENS, to produce material with a significantly refined microstructure due to fast cooling rates associated with the laser process. Several compositions of alloys were examined and the ideal processing parameters were determined for each alloy. The resulting microstructures show a refinement of the microstructure as expected with a fine scale distribution of Nb5Si3 and Nb3Si dispersed in a niobium based matrix phase. The high temperature oxidation behavior of the LENS deposited alloys was comparable to alloys produced using other techniques. A non protective oxide scale formed on samples exposed for only 0.5 hours but was not protective and showed large amounts of

  19. Thermotransport of hydrogen and deuterium in vanadium, niobium and tantalum alloys

    SciTech Connect

    Smith, M.F.

    1981-10-01

    Heats of transport have been determined for thermotransport of hydrogen and deuterium in pure vanadium, niobium and tantalum; in vanadium alloyed with either niobium, titanium or chromium; and in niobium-tantalum alloys. In all cases, thermotransport was toward colder regions and was significantly greater for deuterium than for hydrogen. A mass spectrometric technique was used to simultaneously measure heats of transport for hydrogen and deuterium in a single specimen containing both isotopes. This technique greatly increased the precision with which isotope effects in the heat of transport could be measured. The predominant effect of alloying was to dramatically increase thermotransport; however, thermotransport decreased as niobium was added to tantalum.

  20. Determination of niobium in rocks by an isotope dilution spectrophotometric method

    USGS Publications Warehouse

    Greenland, L.P.; Campbell, E.Y.

    1970-01-01

    Rocks and minerals are fused with sodium peroxide in the presence of carrierfree 95Nb. The fusion cake is leached with water and the precipitate dissolved in hydrofluoric-sulfuric acid mixture. Niobium is extracted into methyl isobutyl ketone and further purified by ion exchange. The amount of niobium is determined spectrophotometrically with 4-(2-pyridylazo)-resorcinol, and the chemical yield of the separations determined by counting 95Nb. This procedure is faster and less sensitive to interferences than previously proposed methods for determining niobium in rocks.The high purity of the separated niobium makes the method applicable to nearly all matrices. ?? 1970.

  1. Magnetic Property in Large Array Niobium Antidot Thin Films

    NASA Astrophysics Data System (ADS)

    Tinghui, Chen; Hsiang-Hsi, Kung; Wei-Li, Lee; Institute of Physics, Academia Sinica, Taipei, Taiwan Team

    2014-03-01

    In a superconducting ring, the total flux inside the ring is required to be an integer number of the flux quanta. Therefore, a supercurrent current can appear within the ring in order to satisfy this quantization rule, which gives rise to certain magnetic response. By using a special monolayer polymer/nanosphere hybrid we developed previously, we fabricated a series of superconducting niobium antidot thin films with different antidot diameters. The antidots form well-ordered triangular lattice with a lattice spacing about 200 nm and extend over an area larger than 1 cm2, which enables magnetic detections simply by a SQUID magnetometer. We observed magnetization oscillation with external magnetic field due to the supercurrent screening effect, where different features for large and small antidot thin films were found. Detailed size and temperature dependencies of the magnetization in niobium antidot nanostructures will be presented.

  2. Creep behavior of tungsten fiber reinforced niobium metal matrix composites

    NASA Technical Reports Server (NTRS)

    Grobstein, T. L.

    1989-01-01

    Tungsten fiber reinforced niobium metal matrix composites were evaluated for use in space nuclear power conversion systems. The composite panels were fabricated using the arc-spray monotape technique at the NASA Lewis Research Center. The creep behavior of W/Nb composite material was determined at 1400 and 1500 K in vacuum over a wide range of applied loads. The time to reach 1 percent strain, the time to rupture, and the minimum creep rate were measured. The W/Nb composites exceeded the properties of monolithic niobium alloys significantly even when compared on a strength to density basis. The effect of fiber orientation on the creep strength also was evaluated. Kirkendall void formation was observed at the fiber/matrix interface; the void distribution differed depending on the fiber orientation relative to the stress axis. A relationship was found between the fiber orientation and the creep strength.

  3. Creep behavior of tungsten fiber reinforced niobium metal matrix composites

    NASA Technical Reports Server (NTRS)

    Grobstein, Toni L.

    1992-01-01

    Tungsten fiber reinforced niobium metal matrix composites were evaluated for use in space nuclear power conversion systems. The composite panels were fabricated using the arc-spray monotape technique at the NASA Lewis Research Center. The creep behavior of W/Nb composite material was determined at 1400 and 1500 K in vacuum over a wide range of applied loads. The time to reach 1 percent strain, the time to rupture, and the minimum creep rate were measured. The W/Nb composites exceeded the properties of monolithic niobium alloys significantly even when compared creep strength also was evaluated. Kirkendall void formation was observed at the fiber/matrix interface; the void distribution differed depending the fiber orientation relative to the stress axis. A relationship was found between the fiber orientation and the creep strength.

  4. Niobium Uptake and Release by Bacterial Ferric Ion Binding Protein

    PubMed Central

    Shi, Yanbo; Harvey, Ian; Campopiano, Dominic; Sadler, Peter J.

    2010-01-01

    Ferric ion binding proteins (Fbps) transport FeIII across the periplasm and are vital for the virulence of many Gram negative bacteria. Iron(III) is tightly bound in a hinged binding cleft with octahedral coordination geometry involving binding to protein side chains (including tyrosinate residues) together with a synergistic anion such as phosphate. Niobium compounds are of interest for their potential biological activity, which has been little explored. We have studied the binding of cyclopentadienyl and nitrilotriacetato NbV complexes to the Fbp from Neisseria gonorrhoeae by UV-vis spectroscopy, chromatography, ICP-OES, mass spectrometry, and Nb K-edge X-ray absorption spectroscopy. These data suggest that NbV binds strongly to Fbp and that a dinuclear NbV centre can be readily accommodated in the interdomain binding cleft. The possibility of designing niobium-based antibiotics which block iron uptake by pathogenic bacteria is discussed. PMID:20445753

  5. Decomposition of Niobium Ore by Sodium Hydroxide Fusion Method

    NASA Astrophysics Data System (ADS)

    Yang, Xiu-Li; Wang, Xiao-Hui; Wei, Chang; Zheng, Shi-Li; Sun, Qing

    2013-02-01

    The decomposition kinetics of niobium ore in the NaOH system was studied experimentally. The results show that the reaction products are sodium metaniobate and sodium niobate formed by the reaction of pyrochlore with sodium hydroxide under roasting. The effects of temperature, particle size, and mass ratio of alkali-to-ore were studied. The conversion rate of niobium exceeded 99 pct after 20 minutes at 923 K (650 °C) with a mass ratio of alkali-to-ore 1.2:1 and with initial particle size 75 to 106 μm. The kinetic study indicates that the shrinking core model is applicable and the process is controlled by a chemical reaction. The activation energy was calculated to be 78.82 kJ mol-1.

  6. Tensile tests of niobium material for SRF cavities

    SciTech Connect

    Wu, G.; Dhanaraj, N.; Cooley, L.; Hicks, D.; Hahn, E.; Burk, D.; Muranyi, W.; Foley, N.; Edwards, H.; Harms, E.; Champion, M.; /Fermilab /Michigan State U.

    2009-06-01

    Mechanical tests of cavity-grade niobium samples were conducted to provide engineering information for the certification of 3rd-harmonic superconducting radio-frequency cavities and cryomodules. Large changes of mechanical properties occur throughout the cavity fabrication process due to the cold work introduced by forming, the heating introduced by electron beam welding, and the recovery of cold work during the anneal used to degas hydrogen after chemical processing. Data is provided here to show the different properties at various stages of fabrication, including both weld regions and samples from the bulk niobium far away from the weld. Measurements of RRR were used to assure that any contamination during annealing was negligible.

  7. Formation and Redox Interconversion of Niobium Methylidene and Methylidyne Complexes.

    PubMed

    Searles, Keith; Smith, Kyle T; Kurogi, Takashi; Chen, Chun-Hsing; Carroll, Patrick J; Mindiola, Daniel J

    2016-06-01

    The niobium methylidene [{(Ar'O)2 Nb}2 (μ2 -Cl)2 (μ2 -CH2 )] (2) can be cleanly prepared via thermolysis or photolysis of [(Ar'O)2 Nb(CH3 )2 Cl] (1) (OAr'=2,6-bis(diphenylmethyl)-4-tert-butylphenoxide). Reduction of 2 with two equivalents of KC8 results in formation of the first niobium methylidyne [K][{(Ar'O)2 Nb}2 (μ2 -CH)(μ2 -H)(μ2 -Cl)] (3) via a binuclear α-hydrogen elimination. Oxidation of 3 with two equiv of ClCPh3 reforms 2. In addition to solid state X-ray analysis, all these complexes were elucidated via multinuclear NMR experiments and isotopic labelling studies, including a crossover experiment, support the notion for a radical mechanism as well as a binuclear α-hydrogen abstraction pathway being operative in the formation of 2 from 1. PMID:27110689

  8. Temperature dependence of penetration depth in thin film niobium

    NASA Technical Reports Server (NTRS)

    More, N.; Muhlfelder, B.; Lockhart, J.

    1989-01-01

    A novel technique is presented which should allow precise determination of the temperature dependence of the inductance, and hence of the penetration depth, of superconducting niobium thin-film structures. Four niobium thin-film stripline inductors are arranged in a bridge configuration, and inductance differences are measured using a potentiometric technique with a SQUID (superconducting quantum interference device) as the null detector. Numerical simulations of the stripline inductances are presented which allow the performance of the measurement technique to be evaluated. The prediction of the two-fluid model for the penetration-depth temperature dependence is given for reduced temperatures of 0.3 to 0.9. The experimental apparatus and its resolution and accuracy are discussed.

  9. Producing titanium-niobium alloy by high energy beam

    NASA Astrophysics Data System (ADS)

    Sharkeev, Yu. P.; Golkovski, M. G.; Glukhov, I. A.; Eroshenko, A. Yu.; Bataev, V. A.; Fortuna, S. V.

    2016-01-01

    The research is involved in producing a Ti-Nb alloy surface layer on titanium substrate by high energy beam method, as well as in examining their structures and mechanical properties. Applying electron-beam cladding it was possible to produce a Ti-Nb alloy surface layer of several millimeters, where the niobium concentration was up to 40% at. and the structure itself could be related to martensite quenching structure. At the same time, a significant microhardness increase of 3200-3400 MPa was observed, which, in its turn, is connected with the formation of martensite structure. Cladding material of Ti-Nb composition could be the source in producing alloys of homogeneous microhardness and desired concentration of alloying niobium element.

  10. Development of high purity niobium used in SRF accelerating cavity

    NASA Astrophysics Data System (ADS)

    Chen, Lin; Xie, Wei-Ping; Li, Ming-Yang; He, Ji-Lin; Fan, Hui-Ru; Zhang, Bao-Cheng; He, Fei-Si; Zhao, Kui; Chen, Jia-Er; Liu, Ke-Xin

    2008-12-01

    Niobium is widely used in SRF (Superconducting Radio Frequency) cavities due to its excellent superconductivity and workability. With the continuous development of technology, higher demands of material are raised. One of the key issues is that RRR (Residual Resistance Ratio) of the Nb material should be more than 300, which requires that the Nb ingot have even higher RRR. This article introduces the development and the experimental results of high purity niobium in OTIC in Ningxia (Ningxia Orient Tantalum Industry Co. Ltd.), and the test results of the single cell TESLA (Tera Electron volt energy Superconducting Linear Accelerator) shaped cavity manufactured by Peking University using Nb material from OTIC. Supported by National Basic Research Program of China (2002CB713600)

  11. Tensile Tests of Niobium Material for Srf Cavities

    NASA Astrophysics Data System (ADS)

    Wu, G.; Dhanaraj, N.; Cooley, L.; Hicks, D.; Hahn, E.; Burk, D.; Muranyi, W.; Foley, M.; Edwards, H.; Harms, E.; Champion, M.; Baars, D.; Compton, C.

    2010-04-01

    Mechanical tests of cavity-grade niobium samples were conducted to provide engineering information for the certification of 3rd-harmonic superconducting radio-frequency cavities and cryomodules. Large changes of mechanical properties occur throughout the cavity fabrication process due to the cold work introduced by forming, the heating introduced by electron beam welding, and the recovery of cold work during the anneal used to degas hydrogen after chemical processing. Data is provided here to show the different properties at various stages of fabrication, including both weld regions and samples from the bulk niobium far away from the weld. Measurements of RRR were used to assure that any contamination during annealing was negligible.

  12. 40 CFR 1039.110 - [Reserved

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 33 2011-07-01 2011-07-01 false 1039.110 Section 1039.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR POLLUTION CONTROLS CONTROL OF... Requirements § 1039.110...

  13. Structural behaviour of niobium oxynitride under high pressure

    SciTech Connect

    Sharma, Bharat Bhooshan Poswal, H. K. Pandey, K. K. Sharma, Surinder M.; Yakhmi, J. V.; Ohashi, Y.; Kikkawa, S.

    2014-04-24

    High pressure investigation of niobium oxynitrides (NbN{sub 0.98}O{sub 0.02}) employing synchrotron based angle dispersive x-ray diffraction experiments was carried out in very fine pressure steps using membrane driven diamond anvil cell. Ambient cubic phase was found to be stable up to ∼18 GPa. At further high pressure cubic phase showed rhombohedral distortion.

  14. Synthesis and photocatalytic activity of electrospun niobium oxide nanofibers

    SciTech Connect

    Qi, Shishun; Zuo, Ruzhong; Liu, Yi; Wang, Yu

    2013-03-15

    Graphical abstract: Different morphologies are obtained for the electrospun niobium oxide nanofibers with different phase structures. The nanofibers of the two phase structures present different band gap value and the light absorption. Hexagonal phase nanofibers show better photocatalytic activity compared with the orthorhombic nanofibers. Highlights: ► Niobium oxide nanofibers of two phase structures were fabricated by electrospinning. ► Photocatalytic properties of the niobium oxide nanofibers were first explored. ► Nanofibers of different phase structures showed different photocatalytic activities. ► Reasons for the differences in the photocatalysis were carefully discussed. - Abstract: Niobium oxide (Nb{sub 2}O{sub 5}) nanofibers have been synthesized by sol–gel based electrospinning technique. Pure hexagonal phase (H-Nb{sub 2}O{sub 5}) and orthorhombic phase (O-Nb{sub 2}O{sub 5}) nanofibers were obtained by thermally annealing the electrospun Nb{sub 2}O{sub 5}/polyvinylpyrrolidone composite fibers in air at 500 °C and 700 °C, respectively. The fibers were characterized using the X-ray diffraction, scanning electron microscopy, specific surface area analyzer and UV–vis diffuse reflectance spectroscopy. Photocatalytic activities of the obtained nanofibers were evaluated depending on the degradation of methyl orange. The results indicate that the heat-treatment temperature, the crystalline structure and the morphology affected the physical and chemical properties of the as-prepared Nb{sub 2}O{sub 5} nanofibers. The H-Nb{sub 2}O{sub 5} nanofibers obtained at lower temperature showed better potential for the application as a promising photocatalyst.

  15. Development of a Niobium Bellow for Beamline Connections

    SciTech Connect

    Larry Turlington; John Brawley; Robert Manus; Stephen Manning; Samuel Morgan; Gary Slack; Peter Kneisel

    2003-09-01

    Superconducting cavities in an accelerator assembly are usually connected at the beampipes by stainless steel bellows. They operate at an intermediate temperature, compensating for alignment tolerances on the cavity beamlines and for thermal contraction during cooldown to cryogenic temperatures. This transition from one cavity to the next in a cavity string is typically of the order of 3/2 wavelength along with approximately half a wavelength taken up by the bellows. If one could incorporate a niobium bellows in the beam pipe, this distance could be reduced by half a wave length. In the case of a big accelerator such as TESLA the overall cavity length for the accelerator could be reduced by roughly 10% or 2000 m. In terms of cost savings this would amount to several million dollars. Based on this estimate we have begun to develop a niobium bellows to be used on a 2.75 inch diameter beamline. It is made from 0.3 mm thick niobium sheet, rolled into a tube and secured by a longitudinal full penetration electron beam weld; the weld is made with a high speed a narrow, focused beam reducing the heat affected zone, thus limiting the grain growth, which could affect the formability. Subsequently, two convolutions have been pressed into this tube in a 2-stage process, using an external die and a polyurethane internal expander. Niobium cuffs and flanges were electron beam welded to the formed bellows, which facilitated leak testing and allowed some measurements of compression/expansion and bending. In this contribution the fabrication process and the subsequent mechanical and vacuum tests with the bellows will be described.

  16. Surface fractal dimension of sintered porous solid niobium

    NASA Astrophysics Data System (ADS)

    Skatkov, L. I.; Konotop, V. V.; Cheremskoy, P. G.; Gomozov, V. P.; Bayrachny, B. I.

    1994-12-01

    The surface fractal dimension of porous solid niobium obtained by vacuum sintering Nb powder is experimentally investigated. The surface fractal dimension D is the main object of our study. Results of small-angle X-ray scattering (SAXS) agree very closely with those of Hg porosimetry. The surface dimensions are stated to be of the order of 2.8 which is a stipulation of a highly developed porous structure. Our results provide experimental support to the SAXS theory developed earlier.

  17. Prototype 350 MHz niobium spoke-loaded cavities.

    SciTech Connect

    Delayen, J. R.; Kedzie, M.; Mammosser, J.; Piller, C.; Shepard, K. W.

    1999-05-10

    This paper reports the development of 350 MHz superconducting cavities of a spoke-loaded geometry, intended for the velocity range 0.2 < v/c < 0.6. Two prototype single-cell cavities have been designed, one optimized for velocity v/c = 0.4, and the other for v/c = 0.29. Construction of the prototype niobium cavities is nearly complete. Details of the design and construction are discussed, along with the results of cold tests.

  18. Mechanical Properties of High Purity Niobium - Novel Measurements

    SciTech Connect

    Ganapati Myneni

    2003-09-01

    One of the procedures to improve the performance of superconducting niobium cavities is a heat treatment for several hours in an ultrahigh vacuum at temperatures between 800C and 1400C for hydrogen degassing or post-purification, respectively. However, it was recently observed with Spallation Neutron Source Project (SNS) prototype cavities, that a heat treatment at 800 C for even 1 hour degraded the mechanical properties of RRR niobium, in particular the yield strength. This lower strength resulted in cavity deformations during handling thus affecting both their resonant frequency and field profile. In addition to lowering the yield strength, it was observed in some lots of material that the Young's modulus was also apparently reduced by a factor of 2 as a result of the hydrogen outgassing at 800 C. Surprisingly, material received at other national laboratories exhibited similar anomalous behavior even without any heat treatments in vacuum. Based on these observations a multi-institutional collaborative basic research activity on high RRR niobium (determination of Nb yield strength as a function of grain size, work hardening, chemical composition, and heat treatment temperature) has been initiated by JLAB to gain a better understanding of the material properties affecting the mechanical behavior In this contribution, a brief review of the measurements at JLAB, at the Materials Science and Engineering Department of the University of Virginia, at the Analytical Chemistry and Metallurgy Divisions of the National Institute of Standard and Technology, Gaithersburg and in the Department of Physics, SUNY, Albany are presented. The measurements include yield strength, hardness, ultrasonic velocity, crystallographic structure, microstructure, determination of interstitial contents using internal friction; particular emphasis is placed on determining the hydrogen concentration in the niobium via Cold Neutron Prompt Gamma-Ray Activation Analysis and Neutron Incoherent

  19. Fabrication of Niobium Nanobridge Josephson Junctions

    NASA Astrophysics Data System (ADS)

    Tachiki, T.; Horiguchi, K.; Uchida, T.

    2014-05-01

    To realize antenna-coupled Josephson detectors for microwave and millimeter-wave radiation, planar-type Nb nanobridge Josephson junctions were fabricated. Nb thin films whose thickness, the root mean square roughness and the critical temperature were 20.0 nm, 0.109 nm and 8.4 K, respectively were deposited using a DC magnetron sputtering at a substrate temperature of 700°C. Nanobridges were obtained from the film using 80-kV electron beam lithography and reactive ion-beam etching in CF4 (90%) + O2 (10%) gases. The minimum bridge area was 65 nm wide and 60 nm long. For the nanobridge whose width and length were less than 110 nm, an I-V characteristic showed resistively-shunted-junction behaviour near the critical temperature. Moreover, Shapiro steps were observed in the nanobridge with microwave irradiation at a frequency of 6 - 30 GHz. The Nb nanobridges can be used as detectors in the antenna-coupled devices.

  20. Effect of low temperature baking on niobium cavities

    SciTech Connect

    Peter Kneisel; Ganapati Myneni; William Lanford; Gianluigi Ciovati

    2003-09-01

    A low temperature (100 C-150 C) ''in situ'' baking under ultra-high vacuum has been successfully applied as final preparation of niobium RF cavities by several laboratories over the last few years. The benefits reported consist mainly of an improvement of the cavity quality factor and a recovery from the so-called ''Q-drop'' without field emission at high field. A series of experiments with a CEBAF single cell cavity have been carried out at Jefferson Lab to carefully investigate the effect of baking at progressively higher temperatures for a fixed time on all the relevant material parameters. Measurements of the cavity quality factor in the temperature range 1.37K-280K and resonant frequency shift between 6K-9.3K provide information about the surface resistance, energy gap, penetration depth and mean free path. The experimental data have been analyzed with the complete BCS theory of superconductivity using a modified version of the computer code originally written by J. Halbritter [1] . Small niobium samples inserted in the cavity during its surface preparation were analyzed with respect to their hydrogen content with a Nuclear Reaction Analysis (NRA). The single cell cavity has been tested at three different temperatures before and after baking to gain some insight on thermal conductivity and Kapitza resistance and the data are compared with different models. This paper describes the results from these experiments and comments on the existing models to explain the effect of baking on the performance of niobium RF cavities.

  1. Field dependent surface resistance of niobium on copper cavities

    NASA Astrophysics Data System (ADS)

    Junginger, T.

    2015-07-01

    The surface resistance RS of superconducting cavities prepared by sputter coating a niobium film on a copper substrate increases significantly stronger with the applied rf field compared to cavities of bulk material. A possible cause is that the thermal boundary resistance between the copper substrate and the niobium film induces heating of the inner cavity wall, resulting in a higher RS. Introducing helium gas in the cavity, and measuring its pressure as a function of applied field allowed to conclude that the inner surface of the cavity is heated up by less than 120 mK when RS increases with Eacc by 100 n Ω . This is more than one order of magnitude less than what one would expect from global heating. Additionally, the effects of cooldown speed and low temperature baking have been investigated in the framework of these experiments. It is shown that for the current state of the art niobium on copper cavities there is only a detrimental effect of low temperature baking. A fast cooldown results in a lowered RS.

  2. Semimicrodetermination of combined tantalum and niobium with selenous acid

    USGS Publications Warehouse

    Grimaldi, F.S.; Schnepfe, M.

    1959-01-01

    Tantalum and niobium are separated and determined gravimetrically by precipitation with selenous acid from highly acidic solutions in the absence of complexing agents. Hydrogen peroxide is used in the preparation of the solution and later catalytically destroyed during digestion of the precipitate. From 0.2 to 30 mg., separately or in mixtures, of niobium or tantalum pentoxide can be separated from mixtures containing 100 mg. each of the oxides of scandium, yttrium, cerium, vanadium, molybdenum, iron, aluminum, tin, lead, and bismuth with a single precipitation; and from 30 mg. of titanium dioxide, and 50 mg. each of the oxides of antimony and thorium, when present separately, with three precipitations. At least 50 mg. of uranium(VI) oxide can be separated with a single precipitation when present alone; otherwise, three precipitations may be needed. Zirconium does not interfere when the tantalum and niobium contents of the sample are small, but in general, zirconium as well as tungsten interfere. The method is applied to the determination of the earth acids in tantaloniobate ores.

  3. Catalytically active single-atom niobium in graphitic layers.

    PubMed

    Zhang, Xuefeng; Guo, Junjie; Guan, Pengfei; Liu, Chunjing; Huang, Hao; Xue, Fanghong; Dong, Xinglong; Pennycook, Stephen J; Chisholm, Matthew F

    2013-01-01

    Carbides of groups IV through VI (Ti, V and Cr groups) have long been proposed as substitutes for noble metal-based electrocatalysts in polymer electrolyte fuel cells. However, their catalytic activity has been extremely limited because of the low density and stability of catalytically active sites. Here we report the excellent performance of a niobium-carbon structure for catalysing the cathodic oxygen reduction reaction. A large number of single niobium atoms and ultra small clusters trapped in graphitic layers are directly identified using state-of-the-art aberration-corrected scanning transmission electron microscopy. This structure not only enhances the overall conductivity for accelerating the exchange of ions and electrons, but it suppresses the chemical/thermal coarsening of the active particles. Experimental results coupled with theory calculations reveal that the single niobium atoms incorporated within the graphitic layers produce a redistribution of d-band electrons and become surprisingly active for O2 adsorption and dissociation, and also exhibit high stability. PMID:23715283

  4. Deposition of aluminide and silicide based protective coatings on niobium

    NASA Astrophysics Data System (ADS)

    Majumdar, S.; Arya, A.; Sharma, I. G.; Suri, A. K.; Banerjee, S.

    2010-11-01

    We compare aluminide and alumino-silicide composite coatings on niobium using halide activated pack cementation (HAPC) technique for improving its oxidation resistance. The coated samples are characterized by SEM, EDS, EPMA and hardness measurements. We observe formation of NbAl3 in aluminide coating of Nb, though the alumino-silicide coating leads to formation primarily of NbSi2 in the inner layer and a ternary compound of Nb-Si-Al in the outer layer, as reported earlier (Majumdar et al. [11]). Formation of niobium silicide is preferred over niobium aluminide during alumino-silicide coating experiments, indicating Si is more strongly bonded to Nb than Al, although equivalent quantities of aluminium and silicon powders were used in the pack chemistry. We also employ first-principles density functional pseudopotential-based calculations to calculate the relative stability of these intermediate phases and the adhesion strength of the Al/Nb and Si/Nb interfaces. NbSi2 exhibits much stronger covalent character as compared to NbAl3. The ideal work of adhesion for the relaxed Al/Nb and Si/Nb interfaces are calculated to be 3226 mJ/m2 and 3545 mJ/m2, respectively, indicating stronger Nb-Si bonding across the interface.

  5. Measuring and modeling oxygen diffusion in niobium-vanadium and niobium-palladium alloys

    NASA Astrophysics Data System (ADS)

    Hennessey, Theresa P.

    Niobium alloys are under consideration for high-temperature aerospace applications, but they have poor oxidation resistance and need high-temperature coatings for protection in severe environments. Our approach to creating an oxidation-resistant Nb alloy is to identify substitutional solute elements that lower the diffusivity of oxygen in Nb. In theory, this will induce a transition from internal to external oxidation and promote the formation of a desirable, protective oxide scale. The objective of this particular project is to compare the oxygen diffusivity in Nb alloys that contain either trap or repulsive sites. In Nb, oxygen atoms diffuse via an interstitial mechanism, and they can interact with substitutional solute atoms in different ways. The interstitial sites adjacent to a substitutional atom constitute a "zone of influence". If the sites in this zone have a lower energy than the normal sites, they are called "trap" sites. If these sites have a higher energy, they are called "repulsive" sites. Oxygen diffusion is inhibited in both cases: trap sites hold the oxygen and keep it from diffusing further, while repulsive sites block the path of the oxygen. Two new mathematical models for interstitial diffusion in these systems were derived from probability and statistical thermodynamic theory. The models were verified using a new random-walk computer simulation of oxygen diffusion through Nb alloys. These models were also tested experimentally by measuring oxygen diffusivity in Nb-V and Nb-Pd alloys. These results showed that V atoms create trap sites for oxygen atoms, confirming previous work. However, there was not enough data to prove definitively that Pd atoms create repulsive sites, as expected by theory.

  6. Process for the generation of .alpha., .beta.-unsaturated carboxylic acids and esters using niobium catalyst

    DOEpatents

    Gogate, Makarand Ratnakav; Spivey, James Jerome; Zoeller, Joseph Robert

    1999-01-01

    A process using a niobium catalyst includes the step of reacting an ester or carboxylic acid with oxygen and an alcohol in the presence a niobium catalyst to respectively produce an .alpha.,.beta.-unsaturated ester or carboxylic acid. Methanol may be used as the alcohol, and the ester or carboxylic acid may be passed over the niobium catalyst in a vapor stream containing oxygen and methanol. Alternatively, the process using a niobium catalyst may involve the step of reacting an ester and oxygen in the presence the niobium catalyst to produce an .alpha.,.beta.-unsaturated carboxylic acid. In this case the ester may be a methyl ester. In either case, niobium oxide may be used as the niobium catalyst with the niobium oxide being present on a support. The support may be an oxide selected from the group consisting of silicon oxide, aluminum oxide, titanium oxide and mixtures thereof. The catalyst may be formed by reacting niobium fluoride with the oxide serving as the support. The niobium catalyst may contain elemental niobium within the range of 1 wt % to 70 wt %, and more preferably within the range of 10 wt % to 30 wt %. The process may be operated at a temperature from 150 to 450.degree. C. and preferably from 250 to 350.degree. C. The process may be operated at a pressure from 0.1 to 15 atm. absolute and preferably from 0.5-5 atm. absolute. The flow rate of reactants may be from 10 to 10,000 L/kg.sub.(cat) /h, and preferably from 100 to 1,000 L/kg.sub.(cat) /h.

  7. Niobium thin films are superconductive in strong magnetic fields at low temperatures

    NASA Technical Reports Server (NTRS)

    Clough, P. J.; Fowler, P.

    1966-01-01

    Niobium film superconductor carries high currents in strong magnetic fields. The thin niobium film is formed on an inert substrate through evaporation in a vacuum environment. Control of temperature and vacuum results in rejection of gaseous impurities so that the film is of a very high purity.

  8. 10 CFR 110.67 - Criminal penalties.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... regulations in 10 CFR part 110 are issued under one or more of sections 161b, 161i, or 161o, except for the... 10 Energy 2 2014-01-01 2014-01-01 false Criminal penalties. 110.67 Section 110.67 Energy NUCLEAR... Enforcement § 110.67 Criminal penalties. (a) Section 223 of the Atomic Energy Act provides for...

  9. 10 CFR 110.67 - Criminal penalties.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... regulations in 10 CFR part 110 are issued under one or more of sections 161b, 161i, or 161o, except for the... 10 Energy 2 2013-01-01 2013-01-01 false Criminal penalties. 110.67 Section 110.67 Energy NUCLEAR... Enforcement § 110.67 Criminal penalties. (a) Section 223 of the Atomic Energy Act provides for...

  10. Influence of Niobium on the Beginning of the Plastic Flow of Material during Cold Deformation

    PubMed Central

    2013-01-01

    Investigations were conducted on low-carbon steel and the steel with same chemical composition with addition of microalloying element niobium. While tensile testing was carried out, the thermographic measurement was tacking place simultaneously. A specific behavior of niobium microalloyed steel was noticed. Test results have shown that, in the elastic deformation region, thermoelastic effect occurs, which is more pronounced in niobium microalloyed steel. Start of plastic flow in steel which is not microalloyed with niobium begins later in comparison to the microalloyed steel, and it is conducted so that, at the point of maximum stress, deformation zone is formed within which stresses grow. In steel microalloyed with niobium after proportionality limit, comes the occurrence of the localized increase in temperature and the occurrence of Lüders band, which propagate along the sample forming a deformation zone. PMID:24453896

  11. Qualification of niobium materials for superconducting radio frequency cavity applications: View of a condensed matter physicist

    SciTech Connect

    Roy, S. B.; Myneni, G. R.

    2015-12-04

    We address the issue of qualifications of the niobium materials to be used for superconducting radio frequency (SCRF) cavity fabrications, from the point of view of a condensed matter physicist/materials scientist. We focus on the particular materials properties of niobium required for the functioning a SCRF cavity, and how to optimize the same properties for the best SCRF cavity performance in a reproducible manner. In this way the niobium materials will not necessarily be characterized by their purity alone, but in terms of those materials properties, which will define the limit of the SCRF cavity performance and also other related material properties, which will help to sustain this best SCRF cavity performance. Furthermore we point out the need of standardization of the post fabrication processing of the niobium-SCRF cavities, which does not impair the optimized superconducting and thermal properties of the starting niobium-materials required for the reproducible performance of the SCRF cavities according to the design values.

  12. Influence of niobium on the beginning of the plastic flow of material during cold deformation.

    PubMed

    Rešković, Stoja; Jandrlić, Ivan

    2013-01-01

    Investigations were conducted on low-carbon steel and the steel with same chemical composition with addition of microalloying element niobium. While tensile testing was carried out, the thermographic measurement was tacking place simultaneously. A specific behavior of niobium microalloyed steel was noticed. Test results have shown that, in the elastic deformation region, thermoelastic effect occurs, which is more pronounced in niobium microalloyed steel. Start of plastic flow in steel which is not microalloyed with niobium begins later in comparison to the microalloyed steel, and it is conducted so that, at the point of maximum stress, deformation zone is formed within which stresses grow. In steel microalloyed with niobium after proportionality limit, comes the occurrence of the localized increase in temperature and the occurrence of Lüders band, which propagate along the sample forming a deformation zone. PMID:24453896

  13. HRLEED study of the roughening transitions in Cu(110), Ni(110) and Ag(110) surfaces

    SciTech Connect

    Wang, K.; Montano, P.A. |

    1996-12-01

    The authors present the results of High Resolution Low Energy Electron Diffraction (HRLEED) measurements of the thermal roughening transition on Cu(110), Ag(110) and Ni(110) surfaces. They performed careful spot profile intensity measurements as a function of temperature. They observed a proliferation of steps along the (110) and (001) directions. In addition a strong deviation from a Debye model was observed in the scattered intensity of the Bragg reflections. This deviation from the harmonic approximation occurs well below the roughening transition temperature. The behavior of the three metal surfaces is qualitatively similar except for the transition temperatures. Ni shows the highest transition temperature (1,300 K), Cu is intermediate (1,000 K) and Ag has the lowest temperature (730 K). Analyzing the behavior of the (00) reflection intensity, and the evolution of the line shape as a function of the temperature, they found clear evidence of a roughening transition at the (110) surface. A lineshape analysis of the (00) reflection shows the transition from a Lorentzian lineshape to a power law. They also proved, based on the experimental data and a recent theoretical model, that there is a tremendous increase in step density and a decrease in the average terrace size as the temperature increases. They used STM to corroborate the HRLEED results at room temperature. They found excellent agreement.

  14. Ferroelectric properties of niobium-doped strontium bismuth tantalate films

    NASA Astrophysics Data System (ADS)

    Golosov, D. A.; Zavadski, S. M.; Kolos, V. V.; Turtsevich, A. S.

    2016-01-01

    The characteristics of ferroelectric thin films of strontium bismuth tantalate (SBT) and niobium-doped strontium bismuth tantalate (SBTN) deposited by radio-frequency (RF) magnetron sputtering on Pt/TiO2/SiO2/Si substrates were investigated. For the formation of the structure of the ferroelectric material, the deposited films were subjected to a subsequent annealing at temperatures of 970-1070 K in an O2 atmosphere. The results of the X-ray diffraction analysis demonstrated that, in contrast to SBT films, in which the Aurivillius phase is formed only at annealing temperatures of 1050-1070 K, the formation of this phase in SBTN films is observed already at a temperature of 970 K. The dependences of the dielectric permittivity, remanent polarization, and coercive force of the SBT and SBTN films on the subsequent annealing conditions were determined. It was found that, upon doping of the SBT films with niobium, the remanent polarization increases by a factor of approximately three, the Curie temperature increases by 50 K, and the dielectric permittivity also increases. It was revealed that, in contrast to the SBT films, the polarization of the SBTN films is observed already at an annealing temperature of approximately 970 K. It was shown that the replacement of SBT films by SBTN films in the manufacture of high-density nonvolatile ferroelectric randomaccess memory (FeRAM) capacitor modules makes it possible to decrease the synthesis temperature from 1070 to 990-1000 K, which improves the compatibility with the planar technology of semiconductor devices. However, it turned out that an increase in the coercive field makes niobium-doped SBT films less attractive for the use in FeRAM.

  15. Monolithic Gyroidal Mesoporous Mixed Titanium–Niobium Nitrides

    PubMed Central

    2015-01-01

    Mesoporous transition metal nitrides are interesting materials for energy conversion and storage applications due to their conductivity and durability. We present ordered mixed titanium–niobium (8:2, 1:1) nitrides with gyroidal network structures synthesized from triblock terpolymer structure-directed mixed oxides. The materials retain both macroscopic integrity and mesoscale ordering despite heat treatment up to 600 °C, without a rigid carbon framework as a support. Furthermore, the gyroidal lattice parameters were varied by changing polymer molar mass. This synthesis strategy may prove useful in generating a variety of monolithic ordered mesoporous mixed oxides and nitrides for electrode and catalyst materials. PMID:25122534

  16. Cathodic arc grown niobium films for RF superconducting cavity applications

    NASA Astrophysics Data System (ADS)

    Catani, L.; Cianchi, A.; Lorkiewicz, J.; Tazzari, S.; Langner, J.; Strzyzewski, P.; Sadowski, M.; Andreone, A.; Cifariello, G.; Di Gennaro, E.; Lamura, G.; Russo, R.

    2006-07-01

    Experimental results on the characterization of the linear and non-linear microwave properties of niobium film produced by UHV cathodic arc deposition are presented. Surface impedance Zs as a function of RF field and intermodulation distortion (IMD) measurement have been carried out by using a dielectrically loaded resonant cavity operating at 7 GHz. The experimental data show that these samples have a lower level of intrinsic non-linearities at low temperature and low circulating power in comparison with Nb samples grown by sputtering. These results make UHV cathodic arc deposition a promising technique for the improvement of RF superconducting cavities for particle accelerators.

  17. Columbium (niobium) recycling in the United States in 1998

    USGS Publications Warehouse

    Cunningham, Larry D.

    2001-01-01

    This report describes the flow of columbium in the United States in 1998 with emphasis on the extent to which columbium (niobium) was recycled/reused. Columbium was mostly recycled from products of columbium-bearing steels and superalloys; little was recovered from products specifically for their columbium content. In 1998, about 1,800 metric tons of columbium was recycled/reused, with about 55% derived from old scrap. The columbium recycling rate was calculated to be 22%, and columbium scrap recycling efficiency, 50%.

  18. Niobium direct detectors for fast and sensitive terahertz spectroscopy.

    PubMed

    Reese, M O; Santavicca, D F; Prober, D E; True, A B; Schmuttenmaer, C A

    2007-08-01

    We report the performance of a niobium hot-electron bolometer designed for laboratory terahertz spectroscopy. The antenna-coupled detector can operate above 4.2 K and has fast (subnanosecond) response. Detailed microwave measurements of performance over a wide range of operating conditions were correlated with quantitative terahertz measurements. The maximum responsivity is 4 x 10(4) VW with a noise equivalent power at the detector of 2 x 10(-14) W/Hz(12), approaching the intrinsic thermal fluctuation limit for the device. This detector enables a variety of novel laboratory spectroscopy measurements. PMID:17764371

  19. Electrochemical behavior of niobium triselenide cathode in lithium secondary cells

    NASA Technical Reports Server (NTRS)

    Ratnakumar, B. V.; Di Stefano, S.; Bankston, C. P.

    1988-01-01

    Niobium triselenide cathodes in Li ambient-temperature rechargeable batteries for space applications undergo a topotactic reaction, with three equivalents of Li at high positive potential furnishing high energy density. It also yields good electronic conductivity, a long life cycle, and high diffusivity for Li. An attempt is presently made to characterize the intercalation mechanism between Li and NbSe3 by means of an ac impedance study conducted at various charge stages in the process of SbSe3 reduction. An effort is also made to predict the charge state of NbSe3 nondestructively, on the basis of the impedance parameters.

  20. PBXN-110 Burn Rate Estimate

    SciTech Connect

    Glascoe, E

    2008-08-11

    It is estimated that PBXN-110 will burn laminarly with a burn function of B = (0.6-1.3)*P{sup 1.0} (B is the burn rate in mm/s and P is pressure in MPa). This paper provides a brief discussion of how this burn behavior was estimated.

  1. STS-110 Extravehicular Activity (EVA)

    NASA Technical Reports Server (NTRS)

    2002-01-01

    STS-110 Mission Specialists Jerry L. Ross and Lee M.E. Morin work in tandem on the fourth scheduled EVA session for the STS-110 mission aboard the Space Shuttle Orbiter Atlantis. Ross is anchored on the mobile foot restraint on the International Space Station's (ISS) Canadarm2, while Morin works inside the S0 (S-zero) truss. The STS-110 mission prepared the Station for future spacewalks by installing and outfitting a 43-foot-long S0 truss and preparing the Mobile Transporter. The 27,000 pound S0 Truss was the first of 9 segments that will make up the Station's external framework that will eventually stretch 356 feet (109 meters), or approximately the length of a football field. This central truss segment also includes a flatcar called the Mobile Transporter and rails that will become the first 'space railroad,' which will allow the Station's robotic arm to travel up and down the finished truss for future assembly and maintenance. The completed truss structure will hold solar arrays and radiators to provide power and cooling for additional international research laboratories from Japan and Europe that will be attached to the Station. Milestones of the S-110 mission included the first time the ISS robotic arm was used to maneuver spacewalkers around the Station and marked the first time all spacewalks were based out of the Station's Quest Airlock. It was also the first Shuttle to use three Block II Main Engines. The Space Shuttle Orbiter Atlantis, STS-110 mission, was launched April 8, 2002 and returned to Earth April 19, 2002.

  2. Structure and Manufacturing Process of MnO2 Counter Electrode in Niobium Suboxide Capacitors

    NASA Astrophysics Data System (ADS)

    Chen, Liqin; Li, Bo; Qi, Zhaoxiong; Guo, Hai; Zhou, Ji; Li, Longtu

    2013-10-01

    The influence of iterative heat treatment of impregnated aqueous Mn(NO3)2 solution on the microstructure of the produced MnO2 has been investigated in the fabrication process for niobium suboxide capacitors. We separate the whole process into two stages: At the early stage of impregnations in Mn(NO3)2 solution (with specific density less than 1.35 g/cm3), the produced MnO2 grains with equiaxed nanocrystalline morphology are mainly located in the inner space and pores, avoiding the performance deterioration due to the electrical conductivity anisotropy of columnar texture in NbO capacitors. For impregnation in Mn(NO3)2 solutions with specific density greater than 1.35 g/cm3, MnO2 grains in the inner space and pores continue to grow and present a hexagonal pyramid shape. At this stage, MnO2 starts to be produced on the outer surface of pellets and exhibits a cluster morphology that consists of MnO2 grains with size between 30 nm and 80 nm. The electrical performance of NbO capacitors has been optimized by adjusting the impregnation times and sequence. By alternately impregnating in Mn(NO3)2 solutions with specific densities of 1.23 g/cm3 and 1.35 g/cm3, MnO2 grains are better combined and the internal space of the pellets is fully filled. Impregnation in Mn(NO3)2 solutions with low specific densities (1.10 g/cm3 and 1.23 g/cm3) in dry atmosphere produces a denser MnO2 layer in the internal space, leading to improved capacitor performance.

  3. A vacuum window for a 1 MW CW 110 GHz gyrotron

    SciTech Connect

    Moeller, C.P.; Doane, J.L.; DiMartino, M.

    1994-07-01

    Development of high power microwave sources for fusion applications is limited by the availability of suitable vacuum windows in the 100 to 200 GHz frequency range. A novel vacuum window is described which uses water cooled sapphire as the dielectric. Heat removal is achieved by using thin slats of sapphire interleaved and brazed to niobium hexagonal tubes in which the cooling water flows. Analysis indicates a window 100 cm{sup 2} in area can readily pass 1 MW in the HE{sub 11} mode at 110 GHz for current experimental applications and 1 MW with a HE{sub 11}{sup 0}-HE{sub 12}{sup 0} mixture at 170 GHz, the projected ITER frequency.

  4. An evolutionary yield function based on Barlat 2000 yield function for the superconducting niobium sheet

    SciTech Connect

    Darbandi, Payam; Pourboghrat, Farhang

    2011-08-22

    Superconducting radio frequency (SRF) niobium cavities are widely used in high-energy physics to accelerate particle beams in particle accelerators. The performance of SRF cavities is affected by the microstructure and purity of the niobium sheet, surface quality, geometry, etc. Following optimum strain paths in the forming of these cavities can significantly control these parameters. To select these strain paths, however, information about the mechanical behavior, microstructure, and formability of the niobium sheet is required. In this study the Barlat 2000 yield function has been used as a yield function for high purity niobium. Results from this study showed that, due to intrinsic behavior, it is necessary to evolve the anisotropic coefficients of Barlat's yield function in order to properly model the plastic behavior of the niobium sheet. The accuracy of the newly developed evolutionary yield function was verified by applying it to the modeling of the hydrostatic bulging of the niobium sheet. Also, in a separate attempt crystal plasticity finite element method was use to model the behavior of the polycrystalline niobium sheet with a particular initial texture.

  5. Localized magnetism on the surface of niobium: experiments and theory

    NASA Astrophysics Data System (ADS)

    Proslier, Thomas; Zasadzinski, John; Ciovati, Gianluigi; Pellin, Mike

    2011-03-01

    The presence of magnetic impurities in native niobium oxides have been confirmed by Point contact spectroscopy (PCT), SQUID magnetometry and Electron paramagnetic resonance (EPR). All niobium (Nb) samples displayed a small impurity contribution to the magnetic susceptibility at low temperatures which exhibited Curie-Weiss behavior, indicative of weakly coupled localized paramagnetic moments. By examining Nb samples with widely varying surface-to-volume ratios it was found that the impurity contribution is correlated with surface area. Tunneling measurements which use the native oxide layers as barriers exhibit a zero-bias conductance peak which splits in a magnetic field > 4 T , consistentwiththeAppelbaummodelforspinfliptunneling . ViewedtogethertheexperimentsstronglysuggestthatthenativeoxidesofNbareintrinsicallydefective , andconsistentlyexhibitlocalizedparamagneticmomentscausedbyoxygenvacanciesinNb 2 O 5 . Thecomputationofthesurfaceimpedance (R S) in presence of magnetic impurities in the Shiba approximation reveals the saturation at low temperature of Rs, suggesting that magnetic impurities are responsible for the so-called residual resistance. Work supported by DOE-HEP office, under contract No. DE-AC02-06CH11357.

  6. Preliminary Experience with ''In-Site'' Baking of Niobium Cavities

    SciTech Connect

    P. Kneisel

    2000-01-01

    In a series of experiments several single cell and multi-cell niobium cavities made from reactor grade and high RRR niobium (frequencies were 700 MHz, 1300 MHz and 1497 MHz) have been baked--after initial testing--in-situ around 145 C for up to 90 hours prior to being recooled. Surprisingly, all cavities showed significant improvements in Q-values between 4.2 and 1.6K. The BCS surface resistance was lowered by nearly a factor of two. This cannot be explained by solely a reduction of dielectric losses caused by adsorbates at the surface or by a decrease of the mean free path due to possibly diffusion of oxygen into the surface layer. In several experiments also the high field behavior of the cavity improved after the in-situ baking procedure. The observed effect opens the possibility for the CEBAF upgrade cavities, which in turn will permit to run the cavities at higher gradients if field emission loading can be prevented. Utilizing this effect can possibly translate into sizeable cost savings since fewer modules are needed for the upgrade program.

  7. Alkali oxide-tantalum, niobium and antimony oxide ionic conductors

    NASA Technical Reports Server (NTRS)

    Roth, R. S.; Brower, W. S.; Parker, H. S.; Minor, D. B.; Waring, J. L.

    1975-01-01

    The phase equilibrium relations of four systems were investigated in detail. These consisted of sodium and potassium antimonates with antimony oxide and tantalum and niobium oxide with rubidium oxide as far as the ratio 4Rb2O:llB2O5 (B=Nb, Ta). The ternary system NaSbO3-Sb2O4-NaF was investigated extensively to determine the actual composition of the body centered cubic sodium antimonate. Various other binary and ternary oxide systems involving alkali oxides were examined in lesser detail. The phases synthesized were screened by ion exchange methods to determine mobility of the mobility of the alkali ion within the niobium, tantalum or antimony oxide (fluoride) structural framework. Five structure types warranted further investigation; these structure types are (1) hexagonal tungsten bronze (HTB), (2) pyrochlore, (3) the hybrid HTB-pyrochlore hexagonal ordered phases, (4) body centered cubic antimonates and (5) 2K2O:3Nb2O5. Although all of these phases exhibit good ion exchange properties only the pyrochlore was prepared with Na(+) ions as an equilibrium phase and as a low porosity ceramic. Sb(+3) in the channel interferes with ionic conductivity in this case, although relatively good ionic conductivity was found for the metastable Na(+) ion exchanged analogs of RbTa2O5F and KTaWO6 pyrochlore phases.

  8. Development of a superconducting connection for niobium cavities

    SciTech Connect

    Peter Kneisel; Gianluigi Ciovati; Jacek Sekutowicz; Waldemar Singer; Xenia Singer; Axel Matheisen

    2007-06-18

    Several, partially successful attempts have been made in the past to develop a superconducting connection between adjacent niobium cavities with the capability to carry up to 30 mT of the magnetic flux. Such a connection would be particularly of great benefit to layouts of long accelerators like ILC because it would shorten the distances between structures and therefore the total length of an accelerator with the associated cost reductions. In addition the superconducting connection would be ideal for a super-structure – two multi-cell cavities connected through a half wavelength long beam pipe providing the coupling. Two welded prototypes of super-structure have been successfully tested with the beam at DESY. The chemical treatment and water rinsing was rather complicated for these prototypes because of the length of the assembly. We have engaged in a program to develop such a connection, initially based on the Nb55Ti material. Several options are pursued such as e.g. a two-cell cavity is being used to explore the reachable magnetic flux for the TESLA like connection with a squeezed niobium gasket between the flanges. Other materials, such as NbZr or NbN are also being considered. In this contribution, we will report about the progress of our investigations.

  9. Development of a superconducting connection for niobium cavities

    SciTech Connect

    Peter Kneisel; Gianluigi Ciovati; Jacek Sekutowicz; Waldemar Singer; Xenia Singer; Axel Matheisen

    2007-06-22

    Several, partially successful attempts have been made in the past to develop a superconducting connection between adjacent niobium cavities with the capability to carry up to 30 mT of the magnetic flux. Such a connection would be particularly of great benefit to layouts of long accelerators like ILC because it would shorten the distances between structures and therefore the total length of an accelerator with the associated cost reductions. In addition the superconducting connection would be ideal for a super-structure – two multi-cell cavities connected through a half wavelength long beam pipe providing the coupling. Two welded prototypes of super-structure have been successfully tested with the beam at DESY. The chemical treatment and water rinsing was rather complicated for these prototypes because of the length of the assembly. We have engaged in a program to develop such a connection, initially based on the Nb55Ti material. Several options are pursued such as e.g. a two-cell cavity is being used to explore the reachable magnetic flux for the TESLA like connection with a squeezed niobium gasket between the flanges. Other materials, such as NbZr or NbN are also being considered. In this contribution, we will report about the progress of our investigations.

  10. Silicidation of Niobium Deposited on Silicon by Physical Vapor Deposition

    SciTech Connect

    Coumba Ndoye, Kandabara Tapily, Marius Orlowski, Helmut Baumgart, Diefeng Gu

    2011-07-01

    Niobium was deposited by physical vapor deposition (PVD) using e-beam evaporation on bare (100) silicon substrates and SiO2 surfaces. The formation of niobium silicide was investigated by annealing PVD Nb films in the temperatures range 400–1000°C. At all elevated annealing temperatures the resistivity of Nb silicide is substantially higher than that of Nb. The Nb silicidation as a function of temperature has been investigated and different NbXSiy compounds have been characterized. It has been observed that the annealing of the Nb film on Si is accompanied by a strong volume expansion of about 2.5 of the resulting reacted film. The films' structural properties were studied using X-Ray diffraction (XRD), energy dispersive X-ray spectroscopy (EDS), and atomic force microscopy (AFM), which was not previously presented in the context of the extant NbSi literature. The X-Ray diffraction characterization of the Nb on Si sample annealed at 1000°C, showed the presence of hexagonal Nb5Si3 phases, with a dominant peak at the (200) plane, and NbSi2 phases. Fractal dimension calculations indicate a distinct transition from Stranski-Krastanov to Volmer-Weber film growth for NbSi formation at the annealing temperature of 600°C and above.

  11. Plasma Treatment of Single-Cell Niobium SRF Cavities

    SciTech Connect

    J. Upadhyay, M. Nikolić, S. Popović, L. Vušković, H.L. Phillips, A-M. Valente-Feliciano

    2011-03-01

    Superconducting radio frequency cavities of bulk Niobium are integral components of particle accelerators based on superconducting technology. Wet chemical processing is the commonly used procedure for impurities and surface defects removal and surface roughness improvement , both required to improve the RF performance of the cavity. We are studying plasma etching as an alternate technique to process these cavities. The uniformity of the plasma sheath at the inner wall of the cavity is one prerequisite for its uniform etching. We are developing electro-optic diagnostic techniques to assess the plasma uniformity. Multiple electro-optical probes are placed at different locations of the single cell cavity to diagnose the electrical and optical properties of the plasma. The electrical parameters are required to understand the kinetic nature of the plasma and the optical emission spectroscopy provides the spatial distribution of radicals in the plasma. The spatial variation of the plasma parameters inside the cavity and their effect on the etching of niobium samples placed at different locations in the cavity will be presented.

  12. Eddy current scanning of niobium for SRF cavities at Fermilab

    SciTech Connect

    Boffo, C.; Bauer, P.; Foley, M.; Antoine, C.; Cooper, C.; Brinkmann, A.; /DESY

    2006-08-01

    In the framework of SRF cavity development, Fermilab is creating the infrastructure needed for the characterization of the material used in the cavity fabrication. An important step in the characterization of ''as received'' niobium sheets is eddy current scanning. Eddy current scanning is a non-destructive technique first adopted and further developed by DESY with the purpose of checking the cavity material for subsurface defects and inclusions. Fermilab has received and further upgraded a commercial eddy current scanner previously used for the SNS project. This scanner is now used daily to scan the niobium sheets for the Fermilab third harmonic, the ILC, and the Proton Driver cavities. After optical inspection, more than 400 squares and disks have been scanned and when necessary checked at the optical and electron microscopes, anodized, or measured with profilometers looking for surface imperfections that might limit the performance of the cavities. This paper gives a status report on the scanning results obtained so far, including a discussion of the classification of signals being detected.

  13. Ultrasonic Velocity and Texture of High RRR Niobium

    SciTech Connect

    S. R. Agnew; F. Zeng; G.R. Myneni

    2003-06-01

    Conventional assessments of the mechanical properties of rolled high RRR niobium plate material via tensile testing have revealed an unusually low apparent Young's moduli and yield strength in some annealed samples. These observations motivated a series of measurements of ultrasonic velocity, a dynamic assessment of the elastic moduli. In fact, the dynamic modulus is within the range of normal for all samples tested. However, there is a trend of increasing shear velocities for shear waves propagating through the sheet thickness and polarized in the sheet transverse direction. Careful analyses of the crystallographic texture using SEM-based electron backscattered diffraction (EBSD) have revealed a subtle, but systematic change in the texture, which can explain the trend. It is further important to note that the change in texture is not observable from surface measurements using x-ray diffraction, but requires sectioning of the samples. Thus, measurements of ultrasonic velocity represent a non-destructive evaluation tool which is extremely sensitive to subtle changes in the texture of high RRR niobium. Finally, there are material lot variations, which are currently attributed to the effects of impurities, such as Ta and H.

  14. Joining of alumina via copper/niobium/copper interlayers

    SciTech Connect

    Marks, Robert A.; Chapman, Daniel R.; Danielson, David T.; Glaeser, Andreas M.

    2000-03-15

    Alumina has been joined at 1150 degrees C and 1400 degrees C using multilayer copper/niobium/copper interlayers. Four-point bend strengths are sensitive to processing temperature, bonding pressure, and furnace environment (ambient oxygen partial pressure). Under optimum conditions, joints with reproducibly high room temperature strengths (approximately equal 240 plus/minus 20 MPa) can be produced; most failures occur within the ceramic. Joints made with sapphire show that during bonding an initially continuous copper film undergoes a morphological instability, resulting in the formation of isolated copper-rich droplets/particles at the sapphire/interlayer interface, and extensive regions of direct bonding between sapphire and niobium. For optimized alumina bonds, bend tests at 800 degrees C-1100 degrees C indicate significant strength is retained; even at the highest test temperature, ceramic failure is observed. Post-bonding anneals at 1000 degrees C in vacuum or in gettered argon were used to assess joint stability and to probe the effect of ambient oxygen partial pressure on joint characteristics. Annealing in vacuum for up to 200 h causes no significant decrease in room temperature bend strength or change in fracture path. With increasing anneal time in a lower oxygen partial pressure environment, the fracture strength decreases only slightly, but the fracture path shifts from the ceramic to the interface.

  15. Materials for Accelerator Technologies Beyond the Niobium Family

    SciTech Connect

    Cooley, Lance; Larbalestier, David; Ghosh, Arup; Tollestrup, Alvin; /Fermilab

    2009-01-01

    Three niobium-based materials make up the entire present portfolio of superconducting technology for accelerators: Nb-Ti and Nb{sub 3}Sn magnet wires and pure niobium for RF cavities. Because these materials are at a high level of maturity, limits imposed by the boundaries of their superconductivity constrain the energy reach of accelerators to several TeV. We sketch here a plan for targeted development of emerging higher field and higher temperature superconductors that could enable accelerators at significantly higher energies. Niobium-based superconductors are the crucial enablers of present accelerators. The Nb-Ti LHC dipole and quadrupole wires, with transition temperature T{sub c} of 9 K and upper critical field H{sub c2} of 15 T, represent the highest form of superconductor strand art: massive, quarter-ton conductor billets are drawn from 300 mm diameter to {approx}1 mm as a single, multi-kilometer-long piece, while retaining uniformity of the several thousand Nb-Ti filaments to within 5% at the scale of a few micrometers. Strands are twisted into fully transposed cables with virtually no loss, preserving a carefully tuned nanostructure that generates the high flux-pinning forces and high current densities to enable high magnetic fields. Nb{sub 3}Sn, with twice the T{sub c} and H{sub c2}, is now approaching this level of conductor art, where over the last 5 years the LHC Accelerator Research Program (LARP) and the Next European Dipole (NED) program have demonstrated that Nb{sub 3}Sn can be made into 4 meter long quadrupoles with 12 T fields and 250 T/m gradients. Linear accelerators at TJNAF, ORNL (SNS), and under construction for the European XFEL exploit niobium superconducting radio-frequency (SRF) technology, with gradients at {approx}20 MV/m. Tremendous research and development is underway to realize high-power goals for Project X at FNAL and for a possible ILC at 35 MV/m gradients. Despite these impressive achievements, the very maturity of these

  16. Influence of electropolishing and anodic oxidation on morphology, chemical composition and corrosion resistance of niobium.

    PubMed

    Sowa, Maciej; Greń, Katarzyna; Kukharenko, Andrey I; Korotin, Danila M; Michalska, Joanna; Szyk-Warszyńska, Lilianna; Mosiałek, Michał; Zak, Jerzy; Pamuła, Elżbieta; Kurmaev, Ernst Z; Cholakh, Seif O; Simka, Wojciech

    2014-09-01

    The work presents results of the studies performed on electropolishing of pure niobium in a bath that contained: sulphuric acid, hydrofluoric acid, ethylene glycol and acetanilide. After the electropolishing, the specimens were subjected to anodic passivation in a 1moldm(-3) phosphoric acid solution at various voltages. The surface morphology, thickness, roughness and chemical composition of the resulting oxide layers were analysed. Thusly prepared niobium samples were additionally investigated in terms of their corrosion resistance in Ringer's solution. The electropolished niobium surface was determined to be smooth and lustrous. The anodisation led to the growth of barrier-like oxide layers, which were enriched in phosphorus species. PMID:25063150

  17. Acidic properties of supported niobium oxide catalysts: An infrared spectroscopy investigation

    SciTech Connect

    Datka, J.; Turek, A.M.; Jehng, J.M.; Wachs, I.E. )

    1992-05-01

    Chemisorption of pyridine was applied as a method for studying the acidic properties of niobium pentoxide supported on silica, magnesia, alumina, titania, and zirconia. The infrared spectra of adsorbed pyridine were used to evaluate the concentration and the relative strength of Broensted and Lewis acid sites. Lewis acidity was found in all the supported niobium oxide systems, while Broensted acid sites were only detected for niobia supported on the alumina and silica supports. The origin and characteristics of the surface acid sites present in supported niobium oxide catalysts are discussed in the present study.

  18. Redistribution of components in the niobium-silicon system under high-temperature proton irradiation

    SciTech Connect

    Afonin, N. N.; Logacheva, V. A. Khoviv, A. M.

    2011-12-15

    The redistribution of components in the niobium-silicon system during magnetron-assisted sputtering of niobium, vacuum annealing, and high-temperature proton irradiation is studied. It is established that, during magnetron-assisted sputtering followed by vacuum annealing, silicon penetrates through the metal film to the outer boundary of the film. Under high-temperature proton irradiation, the suppression of the diffusion of niobium into silicon is observed. This effect is attributed to the high concentration of radiation vacancies in the region of the Nb/Si interphase boundary.

  19. STS-110 Extravehicular Activity (EVA)

    NASA Technical Reports Server (NTRS)

    2002-01-01

    STS-110 Mission astronauts Steven L. Smith (right) and Rex J. Walheim work in tandem on the third scheduled EVA session in which they released the locking bolts on the Mobile Transporter and rewired the Station's robotic arm (out of frame). Part of the Destiny laboratory and a glimpse of the Earth's horizon are seen in the lower portion of this digital image. The STS-110 mission prepared the International Space Station (ISS) for future spacewalks by installing and outfitting the S0 (S-zero) Truss and the Mobile Transporter. The 43-foot-long S0 truss weighing in at 27,000 pounds was the first of 9 segments that will make up the Station's external framework that will eventually stretch 356 feet (109 meters), or approximately the length of a football field. This central truss segment also includes a flatcar called the Mobile Transporter and rails that will become the first 'space railroad,' which will allow the Station's robotic arm to travel up and down the finished truss for future assembly and maintenance. The completed truss structure will hold solar arrays and radiators to provide power and cooling for additional international research laboratories from Japan and Europe that will be attached to the Station. Milestones of the S-110 mission included the first time the ISS robotic arm was used to maneuver spacewalkers around the Station and marked the first time all spacewalks were based out of the Station's Quest Airlock. It was also the first Shuttle to use three Block II Main Engines. The Space Shuttle Orbiter Atlantis, STS-110 mission, was launched April 8, 2002 and returned to Earth April 19, 2002.

  20. STS-110 Extravehicular Activity (EVA)

    NASA Technical Reports Server (NTRS)

    2002-01-01

    STS-110 Mission astronaut Rex J. Walheim, accompanied by astronaut Steven L. Smith (out of frame) translates along the Destiny laboratory on the International Space Station (ISS) during the third scheduled EVA session. The duo released the locking bolts on the Mobile Transporter and rewired the Station's robotic arm. The STS-110 mission prepared the ISS for future space walks by installing and outfitting the S0 (S-Zero) Truss and the Mobile Transporter. The 43-foot-long S0 truss weighing in at 27,000 pounds was the first of 9 segments that will make up the Station's external framework that will eventually stretch 356 feet (109 meters), or approximately the length of a football field. This central truss segment also includes a flatcar called the Mobile Transporter and rails that will become the first 'space railroad,' which will allow the Station's robotic arm to travel up and down the finished truss for future assembly and maintenance. The completed truss structure will hold solar arrays and radiators to provide power and cooling for additional international research laboratories from Japan and Europe that will be attached to the Station. Milestones of the S-110 mission included the first time the ISS robotic arm was used to maneuver space walkers around the Station and marked the first time all space walks were based out of the Station's Quest Airlock. It was also the first Shuttle to use three Block II Main Engines. The Space Shuttle Orbiter Atlantis, STS-110 mission, was launched April 8, 2002 and returned to Earth April 19, 2002.

  1. STS-110 Extravehicular Activity (EVA)

    NASA Technical Reports Server (NTRS)

    2002-01-01

    STS-110 mission specialist Lee M.E. Morin carries an affixed 35 mm camera to record work which is being performed on the International Space Station (ISS). Working with astronaut Jerry L. Ross (out of frame), the duo completed the structural attachment of the S0 (s-zero) truss, mating two large tripod legs of the 13 1/2 ton structure to the station's main laboratory during a 7-hour, 30-minute space walk. The STS-110 mission prepared the Station for future space walks by installing and outfitting the 43-foot-long S0 truss and preparing the Mobile Transporter. The S0 Truss was the first of 9 segments that will make up the Station's external framework that will eventually stretch 356 feet (109 meters), or approximately the length of a football field. This central truss segment also includes a flatcar called the Mobile Transporter and rails that will become the first 'space railroad,' which will allow the Station's robotic arm to travel up and down the finished truss for future assembly and maintenance. The completed truss structure will hold solar arrays and radiators to provide power and cooling for additional international research laboratories from Japan and Europe that will be attached to the Station. Milestones of the S-110 mission included the first time the ISS robotic arm was used to maneuver space walkers around the Station and marked the first time all space walks were based out of the Station's Quest Airlock. It was also the first Shuttle to use three Block II Main Engines. The Space Shuttle Orbiter Atlantis, STS-110 mission, was launched April 8, 2002 and returned to Earth April 19, 2002.

  2. 40 CFR 141.110 - General requirements.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 141.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS (CONTINUED) NATIONAL PRIMARY DRINKING WATER REGULATIONS Treatment Techniques § 141.110 General requirements. The requirements of subpart K of this part constitute national primary drinking water...

  3. 40 CFR 141.110 - General requirements.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 141.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS (CONTINUED) NATIONAL PRIMARY DRINKING WATER REGULATIONS Treatment Techniques § 141.110 General requirements. The requirements of subpart K of this part constitute national primary drinking water...

  4. 40 CFR 47.110 - Eligible applicants.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ....110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY GRANTS AND OTHER FEDERAL ASSISTANCE NATIONAL ENVIRONMENTAL EDUCATION ACT GRANTS § 47.110 Eligible applicants. Any local education agency (including any tribal education agency), college or university, State education agency or...

  5. 40 CFR 141.110 - General requirements.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 141.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS (CONTINUED) NATIONAL PRIMARY DRINKING WATER REGULATIONS Treatment Techniques § 141.110 General requirements. The requirements of subpart K of this part constitute national primary drinking water...

  6. 40 CFR 141.110 - General requirements.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 141.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS (CONTINUED) NATIONAL PRIMARY DRINKING WATER REGULATIONS Treatment Techniques § 141.110 General requirements. The requirements of subpart K of this part constitute national primary drinking water...

  7. 40 CFR 141.110 - General requirements.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 141.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS (CONTINUED) NATIONAL PRIMARY DRINKING WATER REGULATIONS Treatment Techniques § 141.110 General requirements. The requirements of subpart K of this part constitute national primary drinking water...

  8. 49 CFR 110.80 - Procurement.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... CFR 18.36. ... 49 Transportation 2 2010-10-01 2010-10-01 false Procurement. 110.80 Section 110.80 Transportation..., DEPARTMENT OF TRANSPORTATION HAZARDOUS MATERIALS AND OIL TRANSPORTATION HAZARDOUS MATERIALS PUBLIC...

  9. 7 CFR 917.110 - Communications.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 8 2011-01-01 2011-01-01 false Communications. 917.110 Section 917.110 Agriculture... CALIFORNIA Rules and Regulations General § 917.110 Communications. Unless otherwise prescribed in this... commodity committee, all reports, applications, submittals, requests, and communications in connection...

  10. 7 CFR 917.110 - Communications.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 8 2010-01-01 2010-01-01 false Communications. 917.110 Section 917.110 Agriculture... CALIFORNIA Rules and Regulations General § 917.110 Communications. Unless otherwise prescribed in this... commodity committee, all reports, applications, submittals, requests, and communications in connection...

  11. 10 CFR 110.4 - Communications.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Communications. 110.4 Section 110.4 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL General Provisions § 110.4 Communications. Except where otherwise specified in this part, all communications and...

  12. 32 CFR 110.3 - Policy.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 32 National Defense 1 2010-07-01 2010-07-01 false Policy. 110.3 Section 110.3 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE PERSONNEL, MILITARY AND CIVILIAN STANDARDIZED RATES OF SUBSISTENCE ALLOWANCE AND COMMUTATION INSTEAD OF UNIFORMS FOR MEMBERS OF THE SENIOR RESERVE OFFICERS' TRAINING CORPS § 110.3 Policy. It...

  13. 7 CFR 718.110 - Adjustments.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 7 2010-01-01 2010-01-01 false Adjustments. 718.110 Section 718.110 Agriculture Regulations of the Department of Agriculture (Continued) FARM SERVICE AGENCY, DEPARTMENT OF AGRICULTURE FARM... Determination of Acreage and Compliance § 718.110 Adjustments. (a) The farm operator or other...

  14. 7 CFR 718.110 - Adjustments.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 7 2012-01-01 2012-01-01 false Adjustments. 718.110 Section 718.110 Agriculture Regulations of the Department of Agriculture (Continued) FARM SERVICE AGENCY, DEPARTMENT OF AGRICULTURE FARM... Determination of Acreage and Compliance § 718.110 Adjustments. (a) The farm operator or other...

  15. 7 CFR 718.110 - Adjustments.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 7 Agriculture 7 2014-01-01 2014-01-01 false Adjustments. 718.110 Section 718.110 Agriculture Regulations of the Department of Agriculture (Continued) FARM SERVICE AGENCY, DEPARTMENT OF AGRICULTURE FARM... Determination of Acreage and Compliance § 718.110 Adjustments. (a) The farm operator or other...

  16. 21 CFR 556.110 - Carbomycin.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 21 Food and Drugs 6 2014-04-01 2014-04-01 false Carbomycin. 556.110 Section 556.110 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) ANIMAL DRUGS, FEEDS... Residues of New Animal Drugs § 556.110 Carbomycin. A tolerance of zero is established for residues...

  17. 21 CFR 556.110 - Carbomycin.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 21 Food and Drugs 6 2012-04-01 2012-04-01 false Carbomycin. 556.110 Section 556.110 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) ANIMAL DRUGS, FEEDS... Residues of New Animal Drugs § 556.110 Carbomycin. A tolerance of zero is established for residues...

  18. 21 CFR 556.110 - Carbomycin.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 21 Food and Drugs 6 2013-04-01 2013-04-01 false Carbomycin. 556.110 Section 556.110 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) ANIMAL DRUGS, FEEDS... Residues of New Animal Drugs § 556.110 Carbomycin. A tolerance of zero is established for residues...

  19. 24 CFR 91.110 - Consultation; states.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 24 Housing and Urban Development 1 2010-04-01 2010-04-01 false Consultation; states. 91.110 Section 91.110 Housing and Urban Development Office of the Secretary, Department of Housing and Urban Development CONSOLIDATED SUBMISSIONS FOR COMMUNITY PLANNING AND DEVELOPMENT PROGRAMS Citizen Participation and Consultation § 91.110 Consultation;...

  20. 45 CFR 235.110 - Fraud.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 45 Public Welfare 2 2012-10-01 2012-10-01 false Fraud. 235.110 Section 235.110 Public Welfare... PROGRAMS § 235.110 Fraud. State plan requirements: A State plan under title I, IV-A, X, XIV, or XVI of the... criteria for identifying situations in which a question of fraud in the program may exist, and...

  1. 45 CFR 235.110 - Fraud.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 45 Public Welfare 2 2013-10-01 2012-10-01 true Fraud. 235.110 Section 235.110 Public Welfare... PROGRAMS § 235.110 Fraud. State plan requirements: A State plan under title I, IV-A, X, XIV, or XVI of the... criteria for identifying situations in which a question of fraud in the program may exist, and...

  2. 45 CFR 235.110 - Fraud.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 45 Public Welfare 2 2014-10-01 2012-10-01 true Fraud. 235.110 Section 235.110 Public Welfare... PROGRAMS § 235.110 Fraud. State plan requirements: A State plan under title I, IV-A, X, XIV, or XVI of the... criteria for identifying situations in which a question of fraud in the program may exist, and...

  3. 10 CFR 110.28 - Embargoed destinations.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 10 Energy 2 2014-01-01 2014-01-01 false Embargoed destinations. 110.28 Section 110.28 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Licenses § 110.28 Embargoed destinations. Cuba Iran Iraq North Korea Syria Sudan...

  4. 10 CFR 110.28 - Embargoed destinations.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 10 Energy 2 2013-01-01 2013-01-01 false Embargoed destinations. 110.28 Section 110.28 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Licenses § 110.28 Embargoed destinations. Cuba Iran Iraq North Korea Syria Sudan...

  5. 34 CFR 110.22 - Information requirements.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false Information requirements. 110.22 Section 110.22... ASSISTANCE Duties of ED Recipients § 110.22 Information requirements. Each recipient shall— (a) Provide ED with information that ED determines is necessary to ascertain whether the recipient is in...

  6. 10 CFR 110.29 - Restricted destinations.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 2 2012-01-01 2012-01-01 false Restricted destinations. 110.29 Section 110.29 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Licenses § 110.29 Restricted destinations. Afghanistan Andorra Angola Burma (Myanmar) Djibouti India Israel...

  7. 10 CFR 110.29 - Restricted destinations.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 10 Energy 2 2013-01-01 2013-01-01 false Restricted destinations. 110.29 Section 110.29 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Licenses § 110.29 Restricted destinations. Afghanistan Andorra Angola Burma (Myanmar) Djibouti India Israel...

  8. 10 CFR 110.29 - Restricted destinations.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 10 Energy 2 2014-01-01 2014-01-01 false Restricted destinations. 110.29 Section 110.29 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Licenses § 110.29 Restricted destinations. Afghanistan Andorra Angola Burma (Myanmar) Djibouti India Israel...

  9. 10 CFR 110.29 - Restricted destinations.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 10 Energy 2 2011-01-01 2011-01-01 false Restricted destinations. 110.29 Section 110.29 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Licenses § 110.29 Restricted destinations. Afghanistan Andorra Angola Burma (Myanmar) Djibouti India Israel...

  10. 10 CFR 110.29 - Restricted destinations.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Restricted destinations. 110.29 Section 110.29 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Licenses § 110.29 Restricted destinations. Afghanistan Andorra Angola Burma (Myanmar) Djibouti India Israel...

  11. 46 CFR 110.01-1 - General.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false General. 110.01-1 Section 110.01-1 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING GENERAL PROVISIONS Applicability § 110.01-1 General. (a) This subchapter applies to all electrical installations on vessels subject...

  12. 46 CFR 110.01-1 - General.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false General. 110.01-1 Section 110.01-1 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING GENERAL PROVISIONS Applicability § 110.01-1 General. (a) This subchapter applies to all electrical installations on vessels subject...

  13. 38 CFR 4.110 - Ulcers.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 38 Pensions, Bonuses, and Veterans' Relief 1 2010-07-01 2010-07-01 false Ulcers. 4.110 Section 4.110 Pensions, Bonuses, and Veterans' Relief DEPARTMENT OF VETERANS AFFAIRS SCHEDULE FOR RATING DISABILITIES Disability Ratings The Digestive System § 4.110 Ulcers. Experience has shown that the term “peptic ulcer” is not sufficiently specific...

  14. 45 CFR 1386.110 - Posthearing briefs.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 45 Public Welfare 4 2011-10-01 2011-10-01 false Posthearing briefs. 1386.110 Section 1386.110... Posthearing Procedures, Decisions § 1386.110 Posthearing briefs. The presiding officer must fix the time for filing posthearing briefs. This time may not exceed 30 days after termination of the hearing and...

  15. 45 CFR 1386.110 - Posthearing briefs.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 45 Public Welfare 4 2010-10-01 2010-10-01 false Posthearing briefs. 1386.110 Section 1386.110... Posthearing Procedures, Decisions § 1386.110 Posthearing briefs. The presiding officer must fix the time for filing posthearing briefs. This time may not exceed 30 days after termination of the hearing and...

  16. 10 CFR 110.91 - Commission consultations.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Commission consultations. 110.91 Section 110.91 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Public Participation Procedures Concerning License Applications § 110.91 Commission consultations. The Commission...

  17. 10 CFR 110.100 - Public hearings.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Public hearings. 110.100 Section 110.100 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Hearings § 110.100 Public hearings. Hearings under this part will be public unless the Commission directs otherwise....

  18. 10 CFR 110.102 - Hearing docket.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Hearing docket. 110.102 Section 110.102 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Hearings § 110.102 Hearing docket. For each hearing, the Secretary will maintain a docket which will include the...

  19. 46 CFR 176.110 - Routes permitted.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 7 2012-10-01 2012-10-01 false Routes permitted. 176.110 Section 176.110 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) SMALL PASSENGER VESSELS (UNDER 100 GROSS TONS) INSPECTION AND CERTIFICATION General Provisions; Certificate of Inspection § 176.110 Routes permitted....

  20. 46 CFR 176.110 - Routes permitted.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 7 2010-10-01 2010-10-01 false Routes permitted. 176.110 Section 176.110 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) SMALL PASSENGER VESSELS (UNDER 100 GROSS TONS) INSPECTION AND CERTIFICATION Certificate of Inspection § 176.110 Routes permitted. (a) The area of...

  1. 46 CFR 176.110 - Routes permitted.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 7 2014-10-01 2014-10-01 false Routes permitted. 176.110 Section 176.110 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) SMALL PASSENGER VESSELS (UNDER 100 GROSS TONS) INSPECTION AND CERTIFICATION General Provisions; Certificate of Inspection § 176.110 Routes permitted....

  2. 46 CFR 176.110 - Routes permitted.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 7 2013-10-01 2013-10-01 false Routes permitted. 176.110 Section 176.110 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) SMALL PASSENGER VESSELS (UNDER 100 GROSS TONS) INSPECTION AND CERTIFICATION General Provisions; Certificate of Inspection § 176.110 Routes permitted....

  3. 46 CFR 176.110 - Routes permitted.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 7 2011-10-01 2011-10-01 false Routes permitted. 176.110 Section 176.110 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) SMALL PASSENGER VESSELS (UNDER 100 GROSS TONS) INSPECTION AND CERTIFICATION Certificate of Inspection § 176.110 Routes permitted. (a) The area of...

  4. 18 CFR 401.110 - Fees.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 18 Conservation of Power and Water Resources 2 2012-04-01 2012-04-01 false Fees. 401.110 Section 401.110 Conservation of Power and Water Resources DELAWARE RIVER BASIN COMMISSION ADMINISTRATIVE MANUAL RULES OF PRACTICE AND PROCEDURE Public Access to Records and Information § 401.110 Fees. (a) Unless waived in accordance with the provisions of...

  5. 45 CFR 2541.110 - State plans.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... CFR, 1982 Comp., p. 197), “Intergovernmental Review of Federal Programs,” States are allowed to... 45 Public Welfare 4 2012-10-01 2012-10-01 false State plans. 2541.110 Section 2541.110 Public... Pre-Award Requirements § 2541.110 State plans. (a) Scope. The statutes for some programs...

  6. 49 CFR 174.110 - Car magazine.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 49 Transportation 2 2014-10-01 2014-10-01 false Car magazine. 174.110 Section 174.110...) Materials § 174.110 Car magazine. When specially authorized by the carrier, Division 1.1 or 1.2 (explosive) materials in quantity not exceeding 68 kg (150 pounds) may be carried in construction or repair cars if...

  7. 49 CFR 174.110 - Car magazine.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 49 Transportation 2 2013-10-01 2013-10-01 false Car magazine. 174.110 Section 174.110...) Materials § 174.110 Car magazine. When specially authorized by the carrier, Division 1.1 or 1.2 (explosive) materials in quantity not exceeding 68 kg (150 pounds) may be carried in construction or repair cars if...

  8. 49 CFR 174.110 - Car magazine.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 49 Transportation 2 2012-10-01 2012-10-01 false Car magazine. 174.110 Section 174.110...) Materials § 174.110 Car magazine. When specially authorized by the carrier, Division 1.1 or 1.2 (explosive) materials in quantity not exceeding 68 kg (150 pounds) may be carried in construction or repair cars if...

  9. 40 CFR 110.4 - Dispersants.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 21 2010-07-01 2010-07-01 false Dispersants. 110.4 Section 110.4 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS DISCHARGE OF OIL § 110.4 Dispersants. Addition of dispersants or emulsifiers to oil to be discharged that would circumvent...

  10. 40 CFR 110.2 - Applicability.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 21 2010-07-01 2010-07-01 false Applicability. 110.2 Section 110.2 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS DISCHARGE OF OIL § 110.2 Applicability. The regulations of this part apply to the discharge of oil prohibited by section 311(b)(3) of...

  11. 32 CFR 110.5 - Procedures.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 32 National Defense 1 2011-07-01 2011-07-01 false Procedures. 110.5 Section 110.5 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE PERSONNEL, MILITARY AND CIVILIAN STANDARDIZED RATES OF SUBSISTENCE ALLOWANCE AND COMMUTATION INSTEAD OF UNIFORMS FOR MEMBERS OF THE SENIOR RESERVE OFFICERS' TRAINING CORPS § 110.5...

  12. 33 CFR 106.110 - Compliance dates.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 33 Navigation and Navigable Waters 1 2014-07-01 2014-07-01 false Compliance dates. 106.110 Section 106.110 Navigation and Navigable Waters COAST GUARD, DEPARTMENT OF HOMELAND SECURITY MARITIME SECURITY MARINE SECURITY: OUTER CONTINENTAL SHELF (OCS) FACILITIES General § 106.110 Compliance dates. (a) On...

  13. 33 CFR 106.110 - Compliance dates.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 33 Navigation and Navigable Waters 1 2012-07-01 2012-07-01 false Compliance dates. 106.110 Section 106.110 Navigation and Navigable Waters COAST GUARD, DEPARTMENT OF HOMELAND SECURITY MARITIME SECURITY MARINE SECURITY: OUTER CONTINENTAL SHELF (OCS) FACILITIES General § 106.110 Compliance dates. (a) On...

  14. 21 CFR 131.110 - Milk.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 21 Food and Drugs 2 2010-04-01 2010-04-01 false Milk. 131.110 Section 131.110 Food and Drugs FOOD... CONSUMPTION MILK AND CREAM Requirements for Specific Standardized Milk and Cream § 131.110 Milk. (a) Description. Milk is the lacteal secretion, practically free from colostrum, obtained by the complete...

  15. 33 CFR 183.110 - Definitions.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 33 Navigation and Navigable Waters 2 2011-07-01 2011-07-01 false Definitions. 183.110 Section 183.110 Navigation and Navigable Waters COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) BOATING SAFETY BOATS AND ASSOCIATED EQUIPMENT Flotation Requirements for Inboard Boats, Inboard/Outdrive Boats, and Airboats § 183.110 Definitions. For...

  16. 22 CFR 513.110 - Coverage.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 22 Foreign Relations 2 2012-04-01 2009-04-01 true Coverage. 513.110 Section 513.110 Foreign Relations BROADCASTING BOARD OF GOVERNORS GOVERNMENT DEBARMENT AND SUSPENSION (NONPROCUREMENT) AND GOVERNMENTWIDE REQUIREMENTS FOR DRUG-FREE WORKPLACE (GRANTS) General § 513.110 Coverage. (a) These...

  17. 22 CFR 513.110 - Coverage.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 22 Foreign Relations 2 2011-04-01 2009-04-01 true Coverage. 513.110 Section 513.110 Foreign Relations BROADCASTING BOARD OF GOVERNORS GOVERNMENT DEBARMENT AND SUSPENSION (NONPROCUREMENT) AND GOVERNMENTWIDE REQUIREMENTS FOR DRUG-FREE WORKPLACE (GRANTS) General § 513.110 Coverage. (a) These...

  18. 22 CFR 513.110 - Coverage.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 22 Foreign Relations 2 2014-04-01 2014-04-01 false Coverage. 513.110 Section 513.110 Foreign Relations BROADCASTING BOARD OF GOVERNORS GOVERNMENT DEBARMENT AND SUSPENSION (NONPROCUREMENT) AND GOVERNMENTWIDE REQUIREMENTS FOR DRUG-FREE WORKPLACE (GRANTS) General § 513.110 Coverage. (a) These...

  19. 22 CFR 513.110 - Coverage.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 22 Foreign Relations 2 2010-04-01 2010-04-01 true Coverage. 513.110 Section 513.110 Foreign Relations BROADCASTING BOARD OF GOVERNORS GOVERNMENT DEBARMENT AND SUSPENSION (NONPROCUREMENT) AND GOVERNMENTWIDE REQUIREMENTS FOR DRUG-FREE WORKPLACE (GRANTS) General § 513.110 Coverage. (a) These...

  20. 22 CFR 513.110 - Coverage.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 22 Foreign Relations 2 2013-04-01 2009-04-01 true Coverage. 513.110 Section 513.110 Foreign Relations BROADCASTING BOARD OF GOVERNORS GOVERNMENT DEBARMENT AND SUSPENSION (NONPROCUREMENT) AND GOVERNMENTWIDE REQUIREMENTS FOR DRUG-FREE WORKPLACE (GRANTS) General § 513.110 Coverage. (a) These...

  1. 46 CFR 170.110 - Stability booklet.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 7 2012-10-01 2012-10-01 false Stability booklet. 170.110 Section 170.110 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) SUBDIVISION AND STABILITY STABILITY REQUIREMENTS FOR ALL INSPECTED VESSELS Stability Instructions for Operating Personnel § 170.110 Stability booklet. (a) Except as provided in paragraph (e)...

  2. 11 CFR 110.13 - Candidate debates.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 11 Federal Elections 1 2010-01-01 2010-01-01 false Candidate debates. 110.13 Section 110.13 Federal Elections FEDERAL ELECTION COMMISSION GENERAL CONTRIBUTION AND EXPENDITURE LIMITATIONS AND PROHIBITIONS § 110.13 Candidate debates. (a) Staging organizations. (1) Nonprofit organizations described in 26 U.S.C. 501 (c)(3) or (c)(4) and which do...

  3. 10 CFR 110.50 - Terms.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 10 Energy 2 2014-01-01 2014-01-01 false Terms. 110.50 Section 110.50 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL License Terms and Related Provisions § 110.50 Terms. (a) General and specific licenses. (1) Each license is subject to all applicable provisions of the Atomic Energy Act...

  4. 10 CFR 110.81 - Written comments.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Written comments. 110.81 Section 110.81 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Public Participation Procedures Concerning License Applications § 110.81 Written comments. (a) The Commission encourages written comments from the public...

  5. 21 CFR 225.110 - Distribution records.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 21 Food and Drugs 4 2011-04-01 2011-04-01 false Distribution records. 225.110 Section 225.110 Food...: GENERAL CURRENT GOOD MANUFACTURING PRACTICE FOR MEDICATED FEEDS Records and Reports § 225.110 Distribution records. (a) Distribution records permit the manufacturer to relate complaints to specific batches...

  6. 14 CFR 1250.110 - Judicial review.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 14 Aeronautics and Space 5 2010-01-01 2010-01-01 false Judicial review. 1250.110 Section 1250.110... PROGRAMS OF NASA-EFFECTUATION OF TITLE VI OF THE CIVIL RIGHTS ACT OF 1964 § 1250.110 Judicial review. Action taken pursuant to section 602 of the Act is subject to judicial review as provided in section...

  7. 34 CFR 110.30 - Compliance reviews.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 34 Education 1 2012-07-01 2012-07-01 false Compliance reviews. 110.30 Section 110.30 Education..., Conciliation, and Enforcement Procedures § 110.30 Compliance reviews. (a) ED may conduct compliance reviews, pre-award reviews, and other similar procedures that permit ED to investigate and correct...

  8. 10 CFR 110.40 - Commission review.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 2 2012-01-01 2012-01-01 false Commission review. 110.40 Section 110.40 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Review of License Applications § 110.40 Commission review. (a) Immediately after receipt of a license application for an...

  9. 40 CFR 211.110 - Exemptions.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 25 2011-07-01 2011-07-01 false Exemptions. 211.110 Section 211.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) NOISE ABATEMENT PROGRAMS PRODUCT NOISE LABELING General Provisions § 211.110 Exemptions....

  10. 40 CFR 211.110 - Exemptions.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 26 2013-07-01 2013-07-01 false Exemptions. 211.110 Section 211.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) NOISE ABATEMENT PROGRAMS PRODUCT NOISE LABELING General Provisions § 211.110 Exemptions....

  11. 40 CFR 211.110 - Exemptions.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 25 2014-07-01 2014-07-01 false Exemptions. 211.110 Section 211.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) NOISE ABATEMENT PROGRAMS PRODUCT NOISE LABELING General Provisions § 211.110 Exemptions....

  12. 40 CFR 211.110 - Exemptions.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 26 2012-07-01 2011-07-01 true Exemptions. 211.110 Section 211.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) NOISE ABATEMENT PROGRAMS PRODUCT NOISE LABELING General Provisions § 211.110 Exemptions....

  13. 40 CFR 211.110 - Exemptions.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 24 2010-07-01 2010-07-01 false Exemptions. 211.110 Section 211.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) NOISE ABATEMENT PROGRAMS PRODUCT NOISE LABELING General Provisions § 211.110 Exemptions....

  14. 46 CFR 134.110 - Initial inspection.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false Initial inspection. 134.110 Section 134.110 Shipping... LIFTBOATS § 134.110 Initial inspection. Liftboat jacking systems, liftboat legs, liftboat leg pads, and arrangements for supply of water to fire mains, as well as the items listed by § 126.340 of this...

  15. 46 CFR 134.110 - Initial inspection.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Initial inspection. 134.110 Section 134.110 Shipping... LIFTBOATS § 134.110 Initial inspection. Liftboat jacking systems, liftboat legs, liftboat leg pads, and arrangements for supply of water to fire mains, as well as the items listed by § 126.340 of this...

  16. 46 CFR 134.110 - Initial inspection.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false Initial inspection. 134.110 Section 134.110 Shipping... LIFTBOATS § 134.110 Initial inspection. Liftboat jacking systems, liftboat legs, liftboat leg pads, and arrangements for supply of water to fire mains, as well as the items listed by § 126.340 of this...

  17. 46 CFR 134.110 - Initial inspection.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false Initial inspection. 134.110 Section 134.110 Shipping... LIFTBOATS § 134.110 Initial inspection. Liftboat jacking systems, liftboat legs, liftboat leg pads, and arrangements for supply of water to fire mains, as well as the items listed by § 126.340 of this...

  18. 46 CFR 134.110 - Initial inspection.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Initial inspection. 134.110 Section 134.110 Shipping... LIFTBOATS § 134.110 Initial inspection. Liftboat jacking systems, liftboat legs, liftboat leg pads, and arrangements for supply of water to fire mains, as well as the items listed by § 126.340 of this...

  19. 40 CFR 46.110 - Objectives.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 1 2011-07-01 2011-07-01 false Objectives. 46.110 Section 46.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY GRANTS AND OTHER FEDERAL ASSISTANCE FELLOWSHIPS General § 46.110 Objectives. EPA awards fellowships to help individuals participate in academic...

  20. 15 CFR 930.110 - Objectives.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 3 2010-01-01 2010-01-01 false Objectives. 930.110 Section 930.110 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) NATIONAL OCEANIC... CONSISTENCY WITH APPROVED COASTAL MANAGEMENT PROGRAMS Secretarial Mediation § 930.110 Objectives. The...

  1. 40 CFR 45.110 - Objectives.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 1 2010-07-01 2010-07-01 false Objectives. 45.110 Section 45.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY GRANTS AND OTHER FEDERAL ASSISTANCE TRAINING ASSISTANCE § 45.110 Objectives. Assistance agreements are awarded under this part to support students...

  2. 40 CFR 46.110 - Objectives.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 1 2010-07-01 2010-07-01 false Objectives. 46.110 Section 46.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY GRANTS AND OTHER FEDERAL ASSISTANCE FELLOWSHIPS General § 46.110 Objectives. EPA awards fellowships to help individuals participate in academic...

  3. 40 CFR 45.110 - Objectives.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 1 2011-07-01 2011-07-01 false Objectives. 45.110 Section 45.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY GRANTS AND OTHER FEDERAL ASSISTANCE TRAINING ASSISTANCE § 45.110 Objectives. Assistance agreements are awarded under this part to support students...

  4. 15 CFR 930.110 - Objectives.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 3 2011-01-01 2011-01-01 false Objectives. 930.110 Section 930.110 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) NATIONAL OCEANIC... CONSISTENCY WITH APPROVED COASTAL MANAGEMENT PROGRAMS Secretarial Mediation § 930.110 Objectives. The...

  5. 7 CFR 766.110 - Conservation Contract.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 7 2010-01-01 2010-01-01 false Conservation Contract. 766.110 Section 766.110 Agriculture Regulations of the Department of Agriculture (Continued) FARM SERVICE AGENCY, DEPARTMENT OF AGRICULTURE SPECIAL PROGRAMS DIRECT LOAN SERVICING-SPECIAL Loan Servicing Programs § 766.110 Conservation Contract. (a) General. (1) A debtor with...

  6. 7 CFR 766.110 - Conservation Contract.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 7 2012-01-01 2012-01-01 false Conservation Contract. 766.110 Section 766.110 Agriculture Regulations of the Department of Agriculture (Continued) FARM SERVICE AGENCY, DEPARTMENT OF AGRICULTURE SPECIAL PROGRAMS DIRECT LOAN SERVICING-SPECIAL Loan Servicing Programs § 766.110 Conservation Contract. (a) General. (1) A debtor with...

  7. 21 CFR 172.110 - BHA.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 21 Food and Drugs 3 2014-04-01 2014-04-01 false BHA. 172.110 Section 172.110 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) FOOD ADDITIVES PERMITTED FOR DIRECT ADDITION TO FOOD FOR HUMAN CONSUMPTION Food Preservatives § 172.110 BHA. The food additive BHA (butylated hydroxyanisole) alone or...

  8. 32 CFR 110.6 - Information requirement.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 32 National Defense 1 2010-07-01 2010-07-01 false Information requirement. 110.6 Section 110.6 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE PERSONNEL, MILITARY AND CIVILIAN... RESERVE OFFICERS' TRAINING CORPS § 110.6 Information requirement. The reporting requirement for...

  9. 32 CFR 110.6 - Information requirement.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 32 National Defense 1 2013-07-01 2013-07-01 false Information requirement. 110.6 Section 110.6 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE PERSONNEL, MILITARY AND CIVILIAN... RESERVE OFFICERS' TRAINING CORPS § 110.6 Information requirement. The reporting requirement for...

  10. 31 CFR 1.10 - Oral information.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 31 Money and Finance: Treasury 1 2013-07-01 2013-07-01 false Oral information. 1.10 Section 1.10... Disclosure Provisions § 1.10 Oral information. (a) Officers and employees of the Department may, in response to requests, orally provide information contained in records of the Department that are determined...

  11. 21 CFR 160.110 - Frozen eggs.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 21 Food and Drugs 2 2011-04-01 2011-04-01 false Frozen eggs. 160.110 Section 160.110 Food and... CONSUMPTION EGGS AND EGG PRODUCTS Requirements for Specific Standardized Eggs and Egg Products § 160.110 Frozen eggs. (a) Frozen eggs, frozen whole eggs, frozen mixed eggs is the food prepared by...

  12. 21 CFR 160.110 - Frozen eggs.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 21 Food and Drugs 2 2013-04-01 2013-04-01 false Frozen eggs. 160.110 Section 160.110 Food and... CONSUMPTION EGGS AND EGG PRODUCTS Requirements for Specific Standardized Eggs and Egg Products § 160.110 Frozen eggs. (a) Frozen eggs, frozen whole eggs, frozen mixed eggs is the food prepared by...

  13. 21 CFR 160.110 - Frozen eggs.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 21 Food and Drugs 2 2012-04-01 2012-04-01 false Frozen eggs. 160.110 Section 160.110 Food and... CONSUMPTION EGGS AND EGG PRODUCTS Requirements for Specific Standardized Eggs and Egg Products § 160.110 Frozen eggs. (a) Frozen eggs, frozen whole eggs, frozen mixed eggs is the food prepared by...

  14. 21 CFR 160.110 - Frozen eggs.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 21 Food and Drugs 2 2014-04-01 2014-04-01 false Frozen eggs. 160.110 Section 160.110 Food and... CONSUMPTION EGGS AND EGG PRODUCTS Requirements for Specific Standardized Eggs and Egg Products § 160.110 Frozen eggs. (a) Frozen eggs, frozen whole eggs, frozen mixed eggs is the food prepared by...

  15. 21 CFR 160.110 - Frozen eggs.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 21 Food and Drugs 2 2010-04-01 2010-04-01 false Frozen eggs. 160.110 Section 160.110 Food and... CONSUMPTION EGGS AND EGG PRODUCTS Requirements for Specific Standardized Eggs and Egg Products § 160.110 Frozen eggs. (a) Frozen eggs, frozen whole eggs, frozen mixed eggs is the food prepared by...

  16. 40 CFR 110.4 - Dispersants.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 22 2011-07-01 2011-07-01 false Dispersants. 110.4 Section 110.4 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS DISCHARGE OF OIL § 110.4 Dispersants. Addition of dispersants or emulsifiers to oil to be discharged that would circumvent...

  17. 40 CFR 110.2 - Applicability.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 22 2011-07-01 2011-07-01 false Applicability. 110.2 Section 110.2 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS DISCHARGE OF OIL § 110.2 Applicability. The regulations of this part apply to the discharge of oil prohibited by section 311(b)(3) of...

  18. 46 CFR 110.15-1 - Definitions.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... electronic terms are defined in IEEE 100 or IEC 60092-101 (both incorporated by reference; see 46 CFR 110.10... the testing requirements of ASTM B 117 (incorporated by reference; see 46 CFR 110.10-1) or test Kb in... equipment meets at least a NEMA 250 (incorporated by reference; see 46 CFR 110.10-1) Type 1 with...

  19. 46 CFR 110.15-1 - Definitions.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... electronic terms are defined in IEEE 100 or IEC 60092-101 (both incorporated by reference; see 46 CFR 110.10... the testing requirements of ASTM B 117 (incorporated by reference; see 46 CFR 110.10-1) or test Kb in... equipment meets at least a NEMA 250 (incorporated by reference; see 46 CFR 110.10-1) Type 1 with...

  20. 33 CFR 106.110 - Compliance dates.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 33 Navigation and Navigable Waters 1 2013-07-01 2013-07-01 false Compliance dates. 106.110 Section 106.110 Navigation and Navigable Waters COAST GUARD, DEPARTMENT OF HOMELAND SECURITY MARITIME SECURITY MARINE SECURITY: OUTER CONTINENTAL SHELF (OCS) FACILITIES General § 106.110 Compliance dates. (a) On...

  1. 7 CFR 4280.110 - Grant funding.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ...-kind contributions are acceptable in accordance with 7 CFR part 3015 of this title. (2) Passive third... 7 Agriculture 15 2010-01-01 2010-01-01 false Grant funding. 4280.110 Section 4280.110 Agriculture... Improvements Program Section A. Grants § 4280.110 Grant funding. (a) The amount of grant funds that will...

  2. 7 CFR 4280.110 - Grant funding.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ...-kind contributions are acceptable in accordance with 7 CFR part 3015 of this title. (2) Passive third... 7 Agriculture 15 2011-01-01 2011-01-01 false Grant funding. 4280.110 Section 4280.110 Agriculture... Improvements Program Section A. Grants § 4280.110 Grant funding. (a) The amount of grant funds that will...

  3. 42 CFR 488.110 - Procedural guidelines.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 42 Public Health 5 2011-10-01 2011-10-01 false Procedural guidelines. 488.110 Section 488.110 Public Health CENTERS FOR MEDICARE & MEDICAID SERVICES, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) STANDARDS AND CERTIFICATION SURVEY, CERTIFICATION, AND ENFORCEMENT PROCEDURES SURVEY FORMS AND PROCEDURES § 488.110 Procedural guidelines....

  4. 11 CFR 6.110 - Evaluation.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 11 Federal Elections 1 2010-01-01 2010-01-01 false Evaluation. 6.110 Section 6.110 Federal... OR ACTIVITIES CONDUCTED BY THE FEDERAL ELECTION COMMISSION § 6.110 Evaluation. (a) Within one year of... persons, including handicapped persons and organizations representing handicapped persons, and...

  5. 10 CFR 110.28 - Embargoed destinations.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 2 2012-01-01 2012-01-01 false Embargoed destinations. 110.28 Section 110.28 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Licenses § 110.28 Embargoed destinations. Cuba Iran Iraq North Korea Syria Sudan...

  6. 21 CFR 556.110 - Carbomycin.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 21 Food and Drugs 6 2011-04-01 2011-04-01 false Carbomycin. 556.110 Section 556.110 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) ANIMAL DRUGS, FEEDS... Residues of New Animal Drugs § 556.110 Carbomycin. A tolerance of zero is established for residues...

  7. 21 CFR 556.110 - Carbomycin.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 21 Food and Drugs 6 2010-04-01 2010-04-01 false Carbomycin. 556.110 Section 556.110 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) ANIMAL DRUGS, FEEDS, AND RELATED PRODUCTS TOLERANCES FOR RESIDUES OF NEW ANIMAL DRUGS IN FOOD Specific Tolerances for Residues of New Animal Drugs § 556.110...

  8. 34 CFR 110.22 - Information requirements.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false Information requirements. 110.22 Section 110.22... EDUCATION NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Duties of ED Recipients § 110.22 Information requirements. Each recipient shall— (a) Provide...

  9. 34 CFR 110.22 - Information requirements.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 34 Education 1 2012-07-01 2012-07-01 false Information requirements. 110.22 Section 110.22... EDUCATION NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Duties of ED Recipients § 110.22 Information requirements. Each recipient shall— (a) Provide...

  10. 34 CFR 110.22 - Information requirements.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false Information requirements. 110.22 Section 110.22... EDUCATION NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Duties of ED Recipients § 110.22 Information requirements. Each recipient shall— (a) Provide...

  11. 7 CFR 4290.110 - Qualified management.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 15 2011-01-01 2011-01-01 false Qualified management. 4290.110 Section 4290.110... Qualifications for the RBIC Program Organizing A Rbic § 4290.110 Qualified management. An Applicant must show, to the satisfaction of the Secretary, that its current or proposed management team is qualified and...

  12. 7 CFR 4290.110 - Qualified management.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 7 Agriculture 15 2014-01-01 2014-01-01 false Qualified management. 4290.110 Section 4290.110... Qualifications for the RBIC Program Organizing A Rbic § 4290.110 Qualified management. An Applicant must show, to the satisfaction of the Secretary, that its current or proposed management team is qualified and...

  13. 49 CFR 174.110 - Car magazine.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 49 Transportation 2 2010-10-01 2010-10-01 false Car magazine. 174.110 Section 174.110 Transportation Other Regulations Relating to Transportation PIPELINE AND HAZARDOUS MATERIALS SAFETY ADMINISTRATION, DEPARTMENT OF TRANSPORTATION HAZARDOUS MATERIALS REGULATIONS CARRIAGE BY RAIL Class I (Explosive) Materials § 174.110 Car magazine. When...

  14. 42 CFR 110.33 - Death benefits.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 42 Public Health 1 2012-10-01 2012-10-01 false Death benefits. 110.33 Section 110.33 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES VACCINES COUNTERMEASURES INJURY COMPENSATION PROGRAM Available Benefits § 110.33 Death benefits. (a) Eligible survivors may be able to...

  15. 42 CFR 110.1 - Purpose.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 42 Public Health 1 2013-10-01 2013-10-01 false Purpose. 110.1 Section 110.1 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES VACCINES COUNTERMEASURES INJURY COMPENSATION PROGRAM General Provisions § 110.1 Purpose. This part implements the Public Readiness and...

  16. 42 CFR 110.33 - Death benefits.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 42 Public Health 1 2011-10-01 2011-10-01 false Death benefits. 110.33 Section 110.33 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES VACCINES COUNTERMEASURES INJURY COMPENSATION PROGRAM Available Benefits § 110.33 Death benefits. (a) Eligible survivors may be able to...

  17. 42 CFR 110.1 - Purpose.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 42 Public Health 1 2012-10-01 2012-10-01 false Purpose. 110.1 Section 110.1 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES VACCINES COUNTERMEASURES INJURY COMPENSATION PROGRAM General Provisions § 110.1 Purpose. This part implements the Public Readiness and...

  18. 42 CFR 110.33 - Death benefits.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 42 Public Health 1 2014-10-01 2014-10-01 false Death benefits. 110.33 Section 110.33 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES VACCINES COUNTERMEASURES INJURY COMPENSATION PROGRAM Available Benefits § 110.33 Death benefits. (a) Eligible survivors may be able to...

  19. 42 CFR 110.33 - Death benefits.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 42 Public Health 1 2013-10-01 2013-10-01 false Death benefits. 110.33 Section 110.33 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES VACCINES COUNTERMEASURES INJURY COMPENSATION PROGRAM Available Benefits § 110.33 Death benefits. (a) Eligible survivors may be able to...

  20. 42 CFR 110.31 - Medical benefits.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 42 Public Health 1 2014-10-01 2014-10-01 false Medical benefits. 110.31 Section 110.31 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES VACCINES COUNTERMEASURES INJURY COMPENSATION PROGRAM Available Benefits § 110.31 Medical benefits. (a) Injured countermeasure recipients...

  1. 42 CFR 110.31 - Medical benefits.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 42 Public Health 1 2013-10-01 2013-10-01 false Medical benefits. 110.31 Section 110.31 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES VACCINES COUNTERMEASURES INJURY COMPENSATION PROGRAM Available Benefits § 110.31 Medical benefits. (a) Injured countermeasure recipients...

  2. 42 CFR 110.31 - Medical benefits.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 42 Public Health 1 2012-10-01 2012-10-01 false Medical benefits. 110.31 Section 110.31 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES VACCINES COUNTERMEASURES INJURY COMPENSATION PROGRAM Available Benefits § 110.31 Medical benefits. (a) Injured countermeasure recipients...

  3. 42 CFR 110.1 - Purpose.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 42 Public Health 1 2014-10-01 2014-10-01 false Purpose. 110.1 Section 110.1 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES VACCINES COUNTERMEASURES INJURY COMPENSATION PROGRAM General Provisions § 110.1 Purpose. This part implements the Public Readiness and...

  4. 42 CFR 110.31 - Medical benefits.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 42 Public Health 1 2011-10-01 2011-10-01 false Medical benefits. 110.31 Section 110.31 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES VACCINES COUNTERMEASURES INJURY COMPENSATION PROGRAM Available Benefits § 110.31 Medical benefits. (a) Injured countermeasure recipients...

  5. 42 CFR 110.1 - Purpose.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 42 Public Health 1 2011-10-01 2011-10-01 false Purpose. 110.1 Section 110.1 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES VACCINES COUNTERMEASURES INJURY COMPENSATION PROGRAM General Provisions § 110.1 Purpose. This part implements the Public Readiness and...

  6. 38 CFR 4.110 - Ulcers.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 38 Pensions, Bonuses, and Veterans' Relief 1 2012-07-01 2012-07-01 false Ulcers. 4.110 Section 4.110 Pensions, Bonuses, and Veterans' Relief DEPARTMENT OF VETERANS AFFAIRS SCHEDULE FOR RATING DISABILITIES Disability Ratings The Digestive System § 4.110 Ulcers. Experience has shown that the term...

  7. 38 CFR 4.110 - Ulcers.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 38 Pensions, Bonuses, and Veterans' Relief 1 2011-07-01 2011-07-01 false Ulcers. 4.110 Section 4.110 Pensions, Bonuses, and Veterans' Relief DEPARTMENT OF VETERANS AFFAIRS SCHEDULE FOR RATING DISABILITIES Disability Ratings The Digestive System § 4.110 Ulcers. Experience has shown that the term...

  8. 49 CFR 174.110 - Car magazine.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 49 Transportation 2 2011-10-01 2011-10-01 false Car magazine. 174.110 Section 174.110...) Materials § 174.110 Car magazine. When specially authorized by the carrier, Division 1.1 or 1.2 (explosive) materials in quantity not exceeding 68 kg (150 pounds) may be carried in construction or repair cars if...

  9. 14 CFR 1214.110 - Reflight.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 14 Aeronautics and Space 5 2012-01-01 2012-01-01 false Reflight. 1214.110 Section 1214.110 Aeronautics and Space NATIONAL AERONAUTICS AND SPACE ADMINISTRATION SPACE FLIGHT General Provisions Regarding Space Shuttle Flights of Payloads for Non-U.S. Government, Reimbursable Customers § 1214.110...

  10. 14 CFR 1214.110 - Reflight.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 14 Aeronautics and Space 5 2010-01-01 2010-01-01 false Reflight. 1214.110 Section 1214.110 Aeronautics and Space NATIONAL AERONAUTICS AND SPACE ADMINISTRATION SPACE FLIGHT General Provisions Regarding Space Shuttle Flights of Payloads for Non-U.S. Government, Reimbursable Customers § 1214.110...

  11. 14 CFR 1214.110 - Reflight.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 14 Aeronautics and Space 5 2013-01-01 2013-01-01 false Reflight. 1214.110 Section 1214.110 Aeronautics and Space NATIONAL AERONAUTICS AND SPACE ADMINISTRATION SPACE FLIGHT General Provisions Regarding Space Shuttle Flights of Payloads for Non-U.S. Government, Reimbursable Customers § 1214.110...

  12. 14 CFR 1214.110 - Reflight.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 14 Aeronautics and Space 5 2011-01-01 2010-01-01 true Reflight. 1214.110 Section 1214.110 Aeronautics and Space NATIONAL AERONAUTICS AND SPACE ADMINISTRATION SPACE FLIGHT General Provisions Regarding Space Shuttle Flights of Payloads for Non-U.S. Government, Reimbursable Customers § 1214.110...

  13. 14 CFR § 1214.110 - Reflight.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 14 Aeronautics and Space 5 2014-01-01 2014-01-01 false Reflight. § 1214.110 Section § 1214.110 Aeronautics and Space NATIONAL AERONAUTICS AND SPACE ADMINISTRATION SPACE FLIGHT General Provisions Regarding Space Shuttle Flights of Payloads for Non-U.S. Government, Reimbursable Customers § 1214.110...

  14. 21 CFR 110.10 - Personnel.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 21 Food and Drugs 2 2013-04-01 2013-04-01 false Personnel. 110.10 Section 110.10 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) FOOD FOR HUMAN CONSUMPTION CURRENT GOOD MANUFACTURING PRACTICE IN MANUFACTURING, PACKING, OR HOLDING HUMAN FOOD General Provisions § 110.10 Personnel. The...

  15. 10 CFR 110.122 - Classification assistance.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Classification assistance. 110.122 Section 110.122 Energy... Procedures for Classified Information in Hearings § 110.122 Classification assistance. On the request of any... security classification of information and the protective requirements to be observed....

  16. 32 CFR 110.4 - Responsibilities.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 32 National Defense 1 2011-07-01 2011-07-01 false Responsibilities. 110.4 Section 110.4 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE PERSONNEL, MILITARY AND CIVILIAN... RESERVE OFFICERS' TRAINING CORPS § 110.4 Responsibilities. (a) The Assistant Secretary of Defense...

  17. 32 CFR 110.4 - Responsibilities.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 32 National Defense 1 2013-07-01 2013-07-01 false Responsibilities. 110.4 Section 110.4 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE PERSONNEL, MILITARY AND CIVILIAN... RESERVE OFFICERS' TRAINING CORPS § 110.4 Responsibilities. (a) The Assistant Secretary of Defense...

  18. Grob aircraft construction: The G 110 flies

    NASA Technical Reports Server (NTRS)

    Malzbender, B.

    1982-01-01

    Description, specifications and test flight performance of the G 110 are provided. The G 110 completely incorporates modern GfK construction techniques which heretofore have been developed and perfected for the construction of sailplanes. The G 110 is a prototype of a GfK constructed motorized aircraft and shows much promise for the future of German aviation.

  19. 10 CFR 110.28 - Embargoed destinations.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Embargoed destinations. 110.28 Section 110.28 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Licenses § 110.28 Embargoed destinations. Cuba Iran Iraq North Korea Syria Sudan...

  20. 10 CFR 110.28 - Embargoed destinations.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 10 Energy 2 2011-01-01 2011-01-01 false Embargoed destinations. 110.28 Section 110.28 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Licenses § 110.28 Embargoed destinations. Cuba Iran Iraq North Korea Syria Sudan...

  1. 34 CFR 110.23 - Assurances required.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false Assurances required. 110.23 Section 110.23 Education... Recipients § 110.23 Assurances required. (a) Assurances. An applicant for Federal financial assistance to which these regulations apply shall sign a written assurance, on a form specified by ED, that...

  2. 12 CFR 347.110 - Affiliate holdings.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 12 Banks and Banking 4 2011-01-01 2011-01-01 false Affiliate holdings. 347.110 Section 347.110 Banks and Banking FEDERAL DEPOSIT INSURANCE CORPORATION REGULATIONS AND STATEMENTS OF GENERAL POLICY INTERNATIONAL BANKING § 347.110 Affiliate holdings. References in §§ 347.107, 347.108, and 347.109 to...

  3. 12 CFR 347.110 - Affiliate holdings.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 12 Banks and Banking 5 2014-01-01 2014-01-01 false Affiliate holdings. 347.110 Section 347.110 Banks and Banking FEDERAL DEPOSIT INSURANCE CORPORATION REGULATIONS AND STATEMENTS OF GENERAL POLICY INTERNATIONAL BANKING § 347.110 Affiliate holdings. References in §§ 347.107, 347.108, and 347.109 to...

  4. 12 CFR 347.110 - Affiliate holdings.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 12 Banks and Banking 5 2013-01-01 2013-01-01 false Affiliate holdings. 347.110 Section 347.110 Banks and Banking FEDERAL DEPOSIT INSURANCE CORPORATION REGULATIONS AND STATEMENTS OF GENERAL POLICY INTERNATIONAL BANKING § 347.110 Affiliate holdings. References in §§ 347.107, 347.108, and 347.109 to...

  5. 12 CFR 347.110 - Affiliate holdings.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 12 Banks and Banking 5 2012-01-01 2012-01-01 false Affiliate holdings. 347.110 Section 347.110 Banks and Banking FEDERAL DEPOSIT INSURANCE CORPORATION REGULATIONS AND STATEMENTS OF GENERAL POLICY INTERNATIONAL BANKING § 347.110 Affiliate holdings. References in §§ 347.107, 347.108, and 347.109 to...

  6. 12 CFR 347.110 - Affiliate holdings.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 12 Banks and Banking 4 2010-01-01 2010-01-01 false Affiliate holdings. 347.110 Section 347.110 Banks and Banking FEDERAL DEPOSIT INSURANCE CORPORATION REGULATIONS AND STATEMENTS OF GENERAL POLICY INTERNATIONAL BANKING § 347.110 Affiliate holdings. References in §§ 347.107, 347.108, and 347.109 to...

  7. 33 CFR 120.110 - Definitions.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 33 Navigation and Navigable Waters 1 2012-07-01 2012-07-01 false Definitions. 120.110 Section 120.110 Navigation and Navigable Waters COAST GUARD, DEPARTMENT OF HOMELAND SECURITY SECURITY OF VESSELS SECURITY OF PASSENGER VESSELS General § 120.110 Definitions. As used in this part: Captain of the Port (COTP) means the Coast Guard...

  8. 33 CFR 120.110 - Definitions.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 33 Navigation and Navigable Waters 1 2014-07-01 2014-07-01 false Definitions. 120.110 Section 120.110 Navigation and Navigable Waters COAST GUARD, DEPARTMENT OF HOMELAND SECURITY SECURITY OF VESSELS SECURITY OF PASSENGER VESSELS General § 120.110 Definitions. As used in this part: Captain of the Port (COTP) means the Coast Guard...

  9. 10 CFR 110.50 - Terms.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 10 Energy 2 2011-01-01 2011-01-01 false Terms. 110.50 Section 110.50 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL License Terms and Related Provisions § 110.50 Terms. (a) General and specific licenses. (1) Each license is subject to all applicable provisions of the Atomic Energy Act...

  10. 24 CFR 1710.110 - Roads.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 24 Housing and Urban Development 5 2010-04-01 2010-04-01 false Roads. 1710.110 Section 1710.110... (INTERSTATE LAND SALES REGISTRATION PROGRAM) LAND REGISTRATION Reporting Requirements § 1710.110 Roads. (a) Access to the subdivision. (1) Is access to the subdivision provided by public or private roads?...

  11. 12 CFR 1010.110 - Roads.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 12 Banks and Banking 8 2012-01-01 2012-01-01 false Roads. 1010.110 Section 1010.110 Banks and... § 1010.110 Roads. (a) Access to the subdivision. (1) Is access to the subdivision provided by public or private roads? What type of surface do they have? How many lanes? What is the width of the wearing...

  12. 12 CFR 1010.110 - Roads.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 12 Banks and Banking 8 2014-01-01 2014-01-01 false Roads. 1010.110 Section 1010.110 Banks and... § 1010.110 Roads. (a) Access to the subdivision. (1) Is access to the subdivision provided by public or private roads? What type of surface do they have? How many lanes? What is the width of the wearing...

  13. 24 CFR 1710.110 - Roads.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 24 Housing and Urban Development 5 2012-04-01 2012-04-01 false Roads. 1710.110 Section 1710.110... (INTERSTATE LAND SALES REGISTRATION PROGRAM) LAND REGISTRATION Reporting Requirements § 1710.110 Roads. (a) Access to the subdivision. (1) Is access to the subdivision provided by public or private roads?...

  14. 24 CFR 1710.110 - Roads.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 24 Housing and Urban Development 5 2014-04-01 2014-04-01 false Roads. 1710.110 Section 1710.110... (INTERSTATE LAND SALES REGISTRATION PROGRAM) LAND REGISTRATION Reporting Requirements § 1710.110 Roads. (a) Access to the subdivision. (1) Is access to the subdivision provided by public or private roads?...

  15. 12 CFR 1010.110 - Roads.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 12 Banks and Banking 8 2013-01-01 2013-01-01 false Roads. 1010.110 Section 1010.110 Banks and... § 1010.110 Roads. (a) Access to the subdivision. (1) Is access to the subdivision provided by public or private roads? What type of surface do they have? How many lanes? What is the width of the wearing...

  16. 24 CFR 1710.110 - Roads.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 24 Housing and Urban Development 5 2013-04-01 2013-04-01 false Roads. 1710.110 Section 1710.110... (INTERSTATE LAND SALES REGISTRATION PROGRAM) LAND REGISTRATION Reporting Requirements § 1710.110 Roads. (a) Access to the subdivision. (1) Is access to the subdivision provided by public or private roads?...

  17. 24 CFR 1710.110 - Roads.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 24 Housing and Urban Development 5 2011-04-01 2011-04-01 false Roads. 1710.110 Section 1710.110... (INTERSTATE LAND SALES REGISTRATION PROGRAM) LAND REGISTRATION Reporting Requirements § 1710.110 Roads. (a) Access to the subdivision. (1) Is access to the subdivision provided by public or private roads?...

  18. 10 CFR 110.67 - Criminal penalties.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Criminal penalties. 110.67 Section 110.67 Energy NUCLEAR... Enforcement § 110.67 Criminal penalties. (a) Section 223 of the Atomic Energy Act of 1954, as amended, provides for criminal sanctions for willful violation of, attempted violation of, or conspiracy to...

  19. 7 CFR 1.10 - Search services.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 1 2010-01-01 2010-01-01 false Search services. 1.10 Section 1.10 Agriculture Office of the Secretary of Agriculture ADMINISTRATIVE REGULATIONS Official Records § 1.10 Search services. Search services are services of agency personnel—clerical or professional—used in trying to find...

  20. 7 CFR 1.10 - Search services.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 7 Agriculture 1 2013-01-01 2013-01-01 false Search services. 1.10 Section 1.10 Agriculture Office of the Secretary of Agriculture ADMINISTRATIVE REGULATIONS Official Records § 1.10 Search services. Search services are services of agency personnel—clerical or professional—used in trying to find...

  1. 9 CFR 3.110 - Veterinary care.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 9 Animals and Animal Products 1 2011-01-01 2011-01-01 false Veterinary care. 3.110 Section 3.110 Animals and Animal Products ANIMAL AND PLANT HEALTH INSPECTION SERVICE, DEPARTMENT OF AGRICULTURE ANIMAL... Mammals Animal Health and Husbandry Standards § 3.110 Veterinary care. (a) Newly acquired marine...

  2. 9 CFR 3.110 - Veterinary care.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 9 Animals and Animal Products 1 2012-01-01 2012-01-01 false Veterinary care. 3.110 Section 3.110 Animals and Animal Products ANIMAL AND PLANT HEALTH INSPECTION SERVICE, DEPARTMENT OF AGRICULTURE ANIMAL... Mammals Animal Health and Husbandry Standards § 3.110 Veterinary care. (a) Newly acquired marine...

  3. 9 CFR 3.110 - Veterinary care.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 9 Animals and Animal Products 1 2014-01-01 2014-01-01 false Veterinary care. 3.110 Section 3.110 Animals and Animal Products ANIMAL AND PLANT HEALTH INSPECTION SERVICE, DEPARTMENT OF AGRICULTURE ANIMAL... Mammals Animal Health and Husbandry Standards § 3.110 Veterinary care. (a) Newly acquired marine...

  4. 9 CFR 3.110 - Veterinary care.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 9 Animals and Animal Products 1 2010-01-01 2010-01-01 false Veterinary care. 3.110 Section 3.110 Animals and Animal Products ANIMAL AND PLANT HEALTH INSPECTION SERVICE, DEPARTMENT OF AGRICULTURE ANIMAL... Mammals Animal Health and Husbandry Standards § 3.110 Veterinary care. (a) Newly acquired marine...

  5. 9 CFR 3.110 - Veterinary care.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 9 Animals and Animal Products 1 2013-01-01 2013-01-01 false Veterinary care. 3.110 Section 3.110 Animals and Animal Products ANIMAL AND PLANT HEALTH INSPECTION SERVICE, DEPARTMENT OF AGRICULTURE ANIMAL... Mammals Animal Health and Husbandry Standards § 3.110 Veterinary care. (a) Newly acquired marine...

  6. 21 CFR 139.110 - Macaroni products.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 21 Food and Drugs 2 2010-04-01 2010-04-01 false Macaroni products. 139.110 Section 139.110 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) FOOD FOR... Noodle Products § 139.110 Macaroni products. (a) Macaroni products are the class of food each of which...

  7. 21 CFR 139.110 - Macaroni products.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 21 Food and Drugs 2 2014-04-01 2014-04-01 false Macaroni products. 139.110 Section 139.110 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) FOOD FOR... Noodle Products § 139.110 Macaroni products. (a) Macaroni products are the class of food each of which...

  8. 21 CFR 139.110 - Macaroni products.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 21 Food and Drugs 2 2012-04-01 2012-04-01 false Macaroni products. 139.110 Section 139.110 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) FOOD FOR... Noodle Products § 139.110 Macaroni products. (a) Macaroni products are the class of food each of which...

  9. 21 CFR 139.110 - Macaroni products.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 21 Food and Drugs 2 2013-04-01 2013-04-01 false Macaroni products. 139.110 Section 139.110 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) FOOD FOR... Noodle Products § 139.110 Macaroni products. (a) Macaroni products are the class of food each of which...

  10. 21 CFR 139.110 - Macaroni products.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 21 Food and Drugs 2 2011-04-01 2011-04-01 false Macaroni products. 139.110 Section 139.110 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) FOOD FOR... Noodle Products § 139.110 Macaroni products. (a) Macaroni products are the class of food each of which...

  11. 7 CFR 1.10 - Search services.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 1 2012-01-01 2012-01-01 false Search services. 1.10 Section 1.10 Agriculture Office of the Secretary of Agriculture ADMINISTRATIVE REGULATIONS Official Records § 1.10 Search services. Search services are services of agency personnel—clerical or professional—used in trying to find...

  12. 7 CFR 1.10 - Search services.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 7 Agriculture 1 2014-01-01 2014-01-01 false Search services. 1.10 Section 1.10 Agriculture Office of the Secretary of Agriculture ADMINISTRATIVE REGULATIONS Official Records § 1.10 Search services. Search services are services of agency personnel—clerical or professional—used in trying to find...

  13. 7 CFR 1.10 - Search services.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 1 2011-01-01 2011-01-01 false Search services. 1.10 Section 1.10 Agriculture Office of the Secretary of Agriculture ADMINISTRATIVE REGULATIONS Official Records § 1.10 Search services. Search services are services of agency personnel—clerical or professional—used in trying to find...

  14. 40 CFR 110.4 - Dispersants.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 23 2012-07-01 2012-07-01 false Dispersants. 110.4 Section 110.4 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS DISCHARGE OF OIL § 110.4 Dispersants. Addition of dispersants or emulsifiers to oil to be discharged that would circumvent...

  15. 40 CFR 110.2 - Applicability.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 23 2012-07-01 2012-07-01 false Applicability. 110.2 Section 110.2 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS DISCHARGE OF OIL § 110.2 Applicability. The regulations of this part apply to the discharge of oil prohibited by section 311(b)(3) of...

  16. 32 CFR 865.110 - Decision process.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... and 32 CFR part 70: available official military records, documentary evidence submitted by or on... 32 National Defense 6 2014-07-01 2014-07-01 false Decision process. 865.110 Section 865.110...-GENERAL PERSONNEL REVIEW BOARDS Air Force Discharge Review Board § 865.110 Decision process. (a) The...

  17. 32 CFR 865.110 - Decision process.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... and 32 CFR part 70: available official military records, documentary evidence submitted by or on... 32 National Defense 6 2010-07-01 2010-07-01 false Decision process. 865.110 Section 865.110...-GENERAL PERSONNEL REVIEW BOARDS Air Force Discharge Review Board § 865.110 Decision process. (a) The...

  18. 32 CFR 865.110 - Decision process.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... and 32 CFR part 70: available official military records, documentary evidence submitted by or on... 32 National Defense 6 2011-07-01 2011-07-01 false Decision process. 865.110 Section 865.110...-GENERAL PERSONNEL REVIEW BOARDS Air Force Discharge Review Board § 865.110 Decision process. (a) The...

  19. 32 CFR 865.110 - Decision process.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... and 32 CFR part 70: available official military records, documentary evidence submitted by or on... 32 National Defense 6 2013-07-01 2013-07-01 false Decision process. 865.110 Section 865.110...-GENERAL PERSONNEL REVIEW BOARDS Air Force Discharge Review Board § 865.110 Decision process. (a) The...

  20. 32 CFR 865.110 - Decision process.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... and 32 CFR part 70: available official military records, documentary evidence submitted by or on... 32 National Defense 6 2012-07-01 2012-07-01 false Decision process. 865.110 Section 865.110...-GENERAL PERSONNEL REVIEW BOARDS Air Force Discharge Review Board § 865.110 Decision process. (a) The...

  1. 12 CFR 269b.110 - Charges.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 12 Banks and Banking 3 2011-01-01 2011-01-01 false Charges. 269b.110 Section 269b.110 Banks and Banking FEDERAL RESERVE SYSTEM (CONTINUED) BOARD OF GOVERNORS OF THE FEDERAL RESERVE SYSTEM CHARGES OF UNFAIR LABOR PRACTICES Charges of Violations of § 269.6 (of the Policy) § 269b.110 Charges. A...

  2. 12 CFR 269b.110 - Charges.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 12 Banks and Banking 3 2010-01-01 2010-01-01 false Charges. 269b.110 Section 269b.110 Banks and Banking FEDERAL RESERVE SYSTEM (CONTINUED) BOARD OF GOVERNORS OF THE FEDERAL RESERVE SYSTEM CHARGES OF UNFAIR LABOR PRACTICES Charges of Violations of § 269.6 (of the Policy) § 269b.110 Charges. A...

  3. 7 CFR 1956.110 - Joint debtors.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 14 2010-01-01 2009-01-01 true Joint debtors. 1956.110 Section 1956.110 Agriculture... REGULATIONS (CONTINUED) DEBT SETTLEMENT Debt Settlement-Community and Business Programs § 1956.110 Joint debtors. Settlements may not be approved for one joint debtor unless approved for all debtors....

  4. 7 CFR 1956.110 - Joint debtors.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 14 2012-01-01 2012-01-01 false Joint debtors. 1956.110 Section 1956.110 Agriculture... REGULATIONS (CONTINUED) DEBT SETTLEMENT Debt Settlement-Community and Business Programs § 1956.110 Joint debtors. Settlements may not be approved for one joint debtor unless approved for all debtors....

  5. 7 CFR 1956.110 - Joint debtors.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 7 Agriculture 14 2013-01-01 2013-01-01 false Joint debtors. 1956.110 Section 1956.110 Agriculture... REGULATIONS (CONTINUED) DEBT SETTLEMENT Debt Settlement-Community and Business Programs § 1956.110 Joint debtors. Settlements may not be approved for one joint debtor unless approved for all debtors....

  6. 7 CFR 1956.110 - Joint debtors.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 14 2011-01-01 2011-01-01 false Joint debtors. 1956.110 Section 1956.110 Agriculture... REGULATIONS (CONTINUED) DEBT SETTLEMENT Debt Settlement-Community and Business Programs § 1956.110 Joint debtors. Settlements may not be approved for one joint debtor unless approved for all debtors....

  7. 7 CFR 1956.110 - Joint debtors.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 7 Agriculture 14 2014-01-01 2014-01-01 false Joint debtors. 1956.110 Section 1956.110 Agriculture... REGULATIONS (CONTINUED) DEBT SETTLEMENT Debt Settlement-Community and Business Programs § 1956.110 Joint debtors. Settlements may not be approved for one joint debtor unless approved for all debtors....

  8. 34 CFR 110.33 - Investigation.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false Investigation. 110.33 Section 110.33 Education... NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 110.33 Investigation. (a) Initial investigation. ED...

  9. 34 CFR 110.33 - Investigation.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false Investigation. 110.33 Section 110.33 Education... NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 110.33 Investigation. (a) Initial investigation. ED...

  10. 7 CFR 760.110 - Appeals.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 7 2010-01-01 2010-01-01 false Appeals. 760.110 Section 760.110 Agriculture Regulations of the Department of Agriculture (Continued) FARM SERVICE AGENCY, DEPARTMENT OF AGRICULTURE SPECIAL PROGRAMS INDEMNITY PAYMENT PROGRAMS General Provisions for Supplemental Agricultural Disaster Assistance Programs § 760.110 Appeals. (a)...

  11. 46 CFR 132.110 - Piping.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Piping. 132.110 Section 132.110 Shipping COAST GUARD....110 Piping. (a) Except as provided for liftboats by § 134.180 of this subchapter, each fitting, flange, valve, and run of piping must meet the applicable requirements of part 128 of this subchapter....

  12. 46 CFR 132.110 - Piping.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Piping. 132.110 Section 132.110 Shipping COAST GUARD....110 Piping. (a) Except as provided for liftboats by § 134.180 of this subchapter, each fitting, flange, valve, and run of piping must meet the applicable requirements of part 128 of this subchapter....

  13. 6 CFR 27.110 - Applicability.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 6 Domestic Security 1 2011-01-01 2011-01-01 false Applicability. 27.110 Section 27.110 Domestic Security DEPARTMENT OF HOMELAND SECURITY, OFFICE OF THE SECRETARY CHEMICAL FACILITY ANTI-TERRORISM STANDARDS General § 27.110 Applicability. (a) This part applies to chemical facilities and to...

  14. 6 CFR 27.110 - Applicability.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 6 Domestic Security 1 2013-01-01 2013-01-01 false Applicability. 27.110 Section 27.110 Domestic Security DEPARTMENT OF HOMELAND SECURITY, OFFICE OF THE SECRETARY CHEMICAL FACILITY ANTI-TERRORISM STANDARDS General § 27.110 Applicability. (a) This part applies to chemical facilities and to...

  15. 6 CFR 27.110 - Applicability.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 6 Domestic Security 1 2012-01-01 2012-01-01 false Applicability. 27.110 Section 27.110 Domestic Security DEPARTMENT OF HOMELAND SECURITY, OFFICE OF THE SECRETARY CHEMICAL FACILITY ANTI-TERRORISM STANDARDS General § 27.110 Applicability. (a) This part applies to chemical facilities and to...

  16. 6 CFR 27.110 - Applicability.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 6 Domestic Security 1 2014-01-01 2014-01-01 false Applicability. 27.110 Section 27.110 Domestic Security DEPARTMENT OF HOMELAND SECURITY, OFFICE OF THE SECRETARY CHEMICAL FACILITY ANTI-TERRORISM STANDARDS General § 27.110 Applicability. (a) This part applies to chemical facilities and to...

  17. 36 CFR 228.110 - Indemnification.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 36 Parks, Forests, and Public Property 2 2010-07-01 2010-07-01 false Indemnification. 228.110 Section 228.110 Parks, Forests, and Public Property FOREST SERVICE, DEPARTMENT OF AGRICULTURE MINERALS Oil and Gas Resources Authorization of Occupancy within A Leasehold § 228.110 Indemnification....

  18. 36 CFR 228.110 - Indemnification.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 36 Parks, Forests, and Public Property 2 2013-07-01 2013-07-01 false Indemnification. 228.110 Section 228.110 Parks, Forests, and Public Property FOREST SERVICE, DEPARTMENT OF AGRICULTURE MINERALS Oil and Gas Resources Authorization of Occupancy within A Leasehold § 228.110 Indemnification....

  19. 46 CFR 170.110 - Stability booklet.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 7 2011-10-01 2011-10-01 false Stability booklet. 170.110 Section 170.110 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) SUBDIVISION AND STABILITY STABILITY REQUIREMENTS FOR ALL INSPECTED VESSELS Stability Instructions for Operating Personnel § 170.110...

  20. 45 CFR 235.110 - Fraud.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 45 Public Welfare 2 2011-10-01 2011-10-01 false Fraud. 235.110 Section 235.110 Public Welfare... PROGRAMS § 235.110 Fraud. State plan requirements: A State plan under title I, IV-A, X, XIV, or XVI of the... criteria for identifying situations in which a question of fraud in the program may exist, and...

  1. 45 CFR 235.110 - Fraud.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 45 Public Welfare 2 2010-10-01 2010-10-01 false Fraud. 235.110 Section 235.110 Public Welfare... PROGRAMS § 235.110 Fraud. State plan requirements: A State plan under title I, IV-A, X, XIV, or XVI of the... criteria for identifying situations in which a question of fraud in the program may exist, and...

  2. 46 CFR 403.110 - Accounting entities.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 8 2010-10-01 2010-10-01 false Accounting entities. 403.110 Section 403.110 Shipping COAST GUARD (GREAT LAKES PILOTAGE), DEPARTMENT OF HOMELAND SECURITY GREAT LAKES PILOTAGE UNIFORM ACCOUNTING SYSTEM General § 403.110 Accounting entities. Each Association shall be a separate...

  3. 46 CFR 403.110 - Accounting entities.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 8 2012-10-01 2012-10-01 false Accounting entities. 403.110 Section 403.110 Shipping COAST GUARD (GREAT LAKES PILOTAGE), DEPARTMENT OF HOMELAND SECURITY GREAT LAKES PILOTAGE UNIFORM ACCOUNTING SYSTEM General § 403.110 Accounting entities. Each Association shall be a separate...

  4. 46 CFR 403.110 - Accounting entities.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 8 2014-10-01 2014-10-01 false Accounting entities. 403.110 Section 403.110 Shipping COAST GUARD (GREAT LAKES PILOTAGE), DEPARTMENT OF HOMELAND SECURITY GREAT LAKES PILOTAGE UNIFORM ACCOUNTING SYSTEM General § 403.110 Accounting entities. Each Association shall be a separate...

  5. 46 CFR 403.110 - Accounting entities.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 8 2013-10-01 2013-10-01 false Accounting entities. 403.110 Section 403.110 Shipping COAST GUARD (GREAT LAKES PILOTAGE), DEPARTMENT OF HOMELAND SECURITY GREAT LAKES PILOTAGE UNIFORM ACCOUNTING SYSTEM General § 403.110 Accounting entities. Each Association shall be a separate...

  6. 46 CFR 403.110 - Accounting entities.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 8 2011-10-01 2011-10-01 false Accounting entities. 403.110 Section 403.110 Shipping COAST GUARD (GREAT LAKES PILOTAGE), DEPARTMENT OF HOMELAND SECURITY GREAT LAKES PILOTAGE UNIFORM ACCOUNTING SYSTEM General § 403.110 Accounting entities. Each Association shall be a separate...

  7. 5 CFR 950.110 - Prohibited discrimination.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 5 Administrative Personnel 2 2012-01-01 2012-01-01 false Prohibited discrimination. 950.110 Section 950.110 Administrative Personnel OFFICE OF PERSONNEL MANAGEMENT (CONTINUED) CIVIL SERVICE... PRIVATE VOLUNTARY ORGANIZATIONS General Provisions § 950.110 Prohibited discrimination. Discrimination...

  8. 5 CFR 950.110 - Prohibited discrimination.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 5 Administrative Personnel 2 2011-01-01 2011-01-01 false Prohibited discrimination. 950.110 Section 950.110 Administrative Personnel OFFICE OF PERSONNEL MANAGEMENT (CONTINUED) CIVIL SERVICE... PRIVATE VOLUNTARY ORGANIZATIONS General Provisions § 950.110 Prohibited discrimination. Discrimination...

  9. 21 CFR 163.110 - Cacao nibs.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 21 Food and Drugs 2 2012-04-01 2012-04-01 false Cacao nibs. 163.110 Section 163.110 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) FOOD FOR HUMAN CONSUMPTION CACAO PRODUCTS Requirements for Specific Standardized Cacao Products § 163.110 Cacao nibs. (a) Description. (1) Cacao nibs is the...

  10. 6 CFR 27.110 - Applicability.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 6 Domestic Security 1 2010-01-01 2010-01-01 false Applicability. 27.110 Section 27.110 Domestic Security DEPARTMENT OF HOMELAND SECURITY, OFFICE OF THE SECRETARY CHEMICAL FACILITY ANTI-TERRORISM STANDARDS General § 27.110 Applicability. (a) This Part applies to chemical facilities and to...

  11. 41 CFR 101-1.110 - Deviation.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 41 Public Contracts and Property Management 2 2011-07-01 2007-07-01 true Deviation. 101-1.110 Section 101-1.110 Public Contracts and Property Management Federal Property Management Regulations System FEDERAL PROPERTY MANAGEMENT REGULATIONS GENERAL 1-INTRODUCTION 1.1-Regulation System § 101-1.110...

  12. 41 CFR 101-1.110 - Deviation.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 41 Public Contracts and Property Management 2 2012-07-01 2012-07-01 false Deviation. 101-1.110 Section 101-1.110 Public Contracts and Property Management Federal Property Management Regulations System FEDERAL PROPERTY MANAGEMENT REGULATIONS GENERAL 1-INTRODUCTION 1.1-Regulation System § 101-1.110...

  13. 41 CFR 101-1.110 - Deviation.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 41 Public Contracts and Property Management 2 2010-07-01 2010-07-01 true Deviation. 101-1.110 Section 101-1.110 Public Contracts and Property Management Federal Property Management Regulations System FEDERAL PROPERTY MANAGEMENT REGULATIONS GENERAL 1-INTRODUCTION 1.1-Regulation System § 101-1.110...

  14. 41 CFR 101-1.110 - Deviation.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 41 Public Contracts and Property Management 2 2014-07-01 2012-07-01 true Deviation. 101-1.110 Section 101-1.110 Public Contracts and Property Management Federal Property Management Regulations System FEDERAL PROPERTY MANAGEMENT REGULATIONS GENERAL 1-INTRODUCTION 1.1-Regulation System § 101-1.110...

  15. 40 CFR 40.110 - Authority.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 1 2012-07-01 2012-07-01 false Authority. 40.110 Section 40.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY GRANTS AND OTHER FEDERAL ASSISTANCE RESEARCH AND DEMONSTRATION GRANTS § 40.110 Authority. EPA research and demonstration grants are authorized under the following statutes: (a) The Clean Air Act,...

  16. 40 CFR 40.110 - Authority.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 1 2013-07-01 2013-07-01 false Authority. 40.110 Section 40.110 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY GRANTS AND OTHER FEDERAL ASSISTANCE RESEARCH AND DEMONSTRATION GRANTS § 40.110 Authority. EPA research and demonstration grants are authorized under the following statutes: (a) The Clean Air Act,...

  17. 10 CFR 110.134 - Public participation.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 10 Energy 2 2011-01-01 2011-01-01 false Public participation. 110.134 Section 110.134 Energy... § 110.134 Public participation. (a) The Commission may hold an oral hearing on a proposed rule or permit...) When it is in the public interest and is authorized by law, public rule-making procedures may...

  18. 10 CFR 110.100 - Public hearings.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 10 Energy 2 2011-01-01 2011-01-01 false Public hearings. 110.100 Section 110.100 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL Hearings § 110.100 Public hearings. Hearings under this part will be public unless the Commission directs otherwise....

  19. 41 CFR 105-1.110 - Deviation.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 41 Public Contracts and Property Management 3 2010-07-01 2010-07-01 false Deviation. 105-1.110 Section 105-1.110 Public Contracts and Property Management Federal Property Management Regulations System (Continued) GENERAL SERVICES ADMINISTRATION 1-INTRODUCTION 1.1-Regulations System § 105-1.110 Deviation....

  20. 7 CFR 762.110 - Loan application.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 7 2010-01-01 2010-01-01 false Loan application. 762.110 Section 762.110 Agriculture Regulations of the Department of Agriculture (Continued) FARM SERVICE AGENCY, DEPARTMENT OF AGRICULTURE SPECIAL PROGRAMS GUARANTEED FARM LOANS § 762.110 Loan application. (a) Loans for $125,000 or less. All lenders except PLP lenders will submit...

  1. 49 CFR 230.110 - Pilots.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 49 Transportation 4 2010-10-01 2010-10-01 false Pilots. 230.110 Section 230.110 Transportation... and Equalizing System § 230.110 Pilots. (a) General provisions. Pilots shall be securely attached... clearance. The minimum clearance of pilot above the rail shall be 3 inches and the maximum clearance...

  2. 49 CFR 230.110 - Pilots.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 49 Transportation 4 2011-10-01 2011-10-01 false Pilots. 230.110 Section 230.110 Transportation... and Equalizing System § 230.110 Pilots. (a) General provisions. Pilots shall be securely attached... clearance. The minimum clearance of pilot above the rail shall be 3 inches and the maximum clearance...

  3. 10 CFR 110.4 - Communications.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 10 Energy 2 2014-01-01 2014-01-01 false Communications. 110.4 Section 110.4 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL General Provisions § 110.4 Communications. Except where otherwise specified in this part, all communications and...

  4. 10 CFR 110.4 - Communications.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 2 2012-01-01 2012-01-01 false Communications. 110.4 Section 110.4 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL General Provisions § 110.4 Communications. Except where otherwise specified in this part, all communications and...

  5. 10 CFR 110.4 - Communications.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 10 Energy 2 2013-01-01 2013-01-01 false Communications. 110.4 Section 110.4 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL General Provisions § 110.4 Communications. Except where otherwise specified in this part, all communications and...

  6. 34 CFR 110.32 - Mediation.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false Mediation. 110.32 Section 110.32 Education Regulations..., Conciliation, and Enforcement Procedures § 110.32 Mediation. (a) ED promptly refers to the Federal Mediation and Conciliation Service or to the mediation agency designated by the Secretary of Health and...

  7. 34 CFR 110.30 - Compliance reviews.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false Compliance reviews. 110.30 Section 110.30 Education... NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 110.30 Compliance reviews. (a) ED may conduct compliance...

  8. 34 CFR 110.35 - Compliance procedure.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false Compliance procedure. 110.35 Section 110.35 Education... NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 110.35 Compliance procedure. (a) ED may enforce the Act and...

  9. 34 CFR 110.35 - Compliance procedure.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false Compliance procedure. 110.35 Section 110.35 Education... NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 110.35 Compliance procedure. (a) ED may enforce the Act and...

  10. 34 CFR 110.30 - Compliance reviews.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false Compliance reviews. 110.30 Section 110.30 Education... NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 110.30 Compliance reviews. (a) ED may conduct compliance...

  11. 34 CFR 110.35 - Compliance procedure.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false Compliance procedure. 110.35 Section 110.35 Education... NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 110.35 Compliance procedure. (a) ED may enforce the Act and...

  12. 34 CFR 110.30 - Compliance reviews.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false Compliance reviews. 110.30 Section 110.30 Education... NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 110.30 Compliance reviews. (a) ED may conduct compliance...

  13. 34 CFR 110.35 - Compliance procedure.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 34 Education 1 2012-07-01 2012-07-01 false Compliance procedure. 110.35 Section 110.35 Education... NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 110.35 Compliance procedure. (a) ED may enforce the Act and...

  14. 34 CFR 110.35 - Compliance procedure.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false Compliance procedure. 110.35 Section 110.35 Education... NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 110.35 Compliance procedure. (a) ED may enforce the Act and...

  15. 34 CFR 110.30 - Compliance reviews.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false Compliance reviews. 110.30 Section 110.30 Education... NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 110.30 Compliance reviews. (a) ED may conduct compliance...

  16. 10 CFR 110.50 - Terms.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Terms. 110.50 Section 110.50 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) EXPORT AND IMPORT OF NUCLEAR EQUIPMENT AND MATERIAL License Terms and Related Provisions § 110.50 Terms. (a) General and specific licenses. (1) Each license is subject to all applicable provisions of the Atomic Energy Act and...

  17. 47 CFR 5.110 - Power limitations.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 1 2013-10-01 2013-10-01 false Power limitations. 5.110 Section 5.110... Operating Requirements § 5.110 Power limitations. (a) The transmitting radiated power for stations authorized under the Experimental Radio Service shall be limited to the minimum practical radiated...

  18. 47 CFR 5.110 - Power limitations.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 1 2014-10-01 2014-10-01 false Power limitations. 5.110 Section 5.110... Operating Requirements § 5.110 Power limitations. (a) The transmitting radiated power for stations authorized under the Experimental Radio Service shall be limited to the minimum practical radiated...

  19. 7 CFR 4290.110 - Qualified management.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 7 Agriculture 15 2013-01-01 2013-01-01 false Qualified management. 4290.110 Section 4290.110... Qualifications for the RBIC Program Organizing A Rbic § 4290.110 Qualified management. An Applicant must show, to the satisfaction of the Secretary, that its current or proposed management team is qualified and...

  20. 7 CFR 4290.110 - Qualified management.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 15 2012-01-01 2012-01-01 false Qualified management. 4290.110 Section 4290.110... Qualifications for the RBIC Program Organizing A Rbic § 4290.110 Qualified management. Link to an amendment..., that its current or proposed management team is qualified and has the knowledge, experience,...

  1. 34 CFR 110.22 - Information requirements.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false Information requirements. 110.22 Section 110.22... EDUCATION NONDISCRIMINATION ON THE BASIS OF AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Duties of ED Recipients § 110.22 Information requirements. Each recipient shall— (a) Provide...

  2. 29 CFR 452.110 - Adequate safeguards.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 29 Labor 2 2010-07-01 2010-07-01 false Adequate safeguards. 452.110 Section 452.110 Labor... DISCLOSURE ACT OF 1959 Election Procedures; Rights of Members § 452.110 Adequate safeguards. (a) In addition to the election safeguards discussed in this part, the Act contains a general mandate in section...

  3. 29 CFR 452.110 - Adequate safeguards.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 29 Labor 2 2011-07-01 2011-07-01 false Adequate safeguards. 452.110 Section 452.110 Labor... DISCLOSURE ACT OF 1959 Election Procedures; Rights of Members § 452.110 Adequate safeguards. (a) In addition to the election safeguards discussed in this part, the Act contains a general mandate in section...

  4. 29 CFR 1928.110 - Field sanitation.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 29 Labor 9 2012-07-01 2012-07-01 false Field sanitation. 1928.110 Section 1928.110 Labor Regulations Relating to Labor (Continued) OCCUPATIONAL SAFETY AND HEALTH ADMINISTRATION, DEPARTMENT OF LABOR (CONTINUED) OCCUPATIONAL SAFETY AND HEALTH STANDARDS FOR AGRICULTURE General Environmental Controls § 1928.110 Field sanitation. (a) Scope....

  5. 10 CFR 110.64 - Civil penalty.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 2 2012-01-01 2012-01-01 false Civil penalty. 110.64 Section 110.64 Energy NUCLEAR... Enforcement § 110.64 Civil penalty. (a) In response to a violation, the Commission may institute a proceeding to impose a civil penalty under section 234 of the Atomic Energy Act by issuing a notice to...

  6. 10 CFR 110.64 - Civil penalty.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 10 Energy 2 2011-01-01 2011-01-01 false Civil penalty. 110.64 Section 110.64 Energy NUCLEAR... Enforcement § 110.64 Civil penalty. (a) In response to a violation, the Commission may institute a proceeding to impose a civil penalty under section 234 of the Atomic Energy Act by issuing a notice to...

  7. 10 CFR 110.64 - Civil penalty.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 10 Energy 2 2013-01-01 2013-01-01 false Civil penalty. 110.64 Section 110.64 Energy NUCLEAR... Enforcement § 110.64 Civil penalty. (a) In response to a violation, the Commission may institute a proceeding to impose a civil penalty under section 234 of the Atomic Energy Act by issuing a notice to...

  8. 10 CFR 110.64 - Civil penalty.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 10 Energy 2 2014-01-01 2014-01-01 false Civil penalty. 110.64 Section 110.64 Energy NUCLEAR... Enforcement § 110.64 Civil penalty. (a) In response to a violation, the Commission may institute a proceeding to impose a civil penalty under section 234 of the Atomic Energy Act by issuing a notice to...

  9. 14 CFR 1250.110 - Judicial review.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 14 Aeronautics and Space 5 2011-01-01 2010-01-01 true Judicial review. 1250.110 Section 1250.110... PROGRAMS OF NASA-EFFECTUATION OF TITLE VI OF THE CIVIL RIGHTS ACT OF 1964 § 1250.110 Judicial review. Action taken pursuant to section 602 of the Act is subject to judicial review as provided in section...

  10. 14 CFR 1250.110 - Judicial review.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 14 Aeronautics and Space 5 2013-01-01 2013-01-01 false Judicial review. 1250.110 Section 1250.110... PROGRAMS OF NASA-EFFECTUATION OF TITLE VI OF THE CIVIL RIGHTS ACT OF 1964 § 1250.110 Judicial review. Action taken pursuant to section 602 of the Act is subject to judicial review as provided in section...

  11. 10 CFR 110.64 - Civil penalty.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Civil penalty. 110.64 Section 110.64 Energy NUCLEAR... Enforcement § 110.64 Civil penalty. (a) In response to a violation, the Commission may institute a proceeding to impose a civil penalty under section 234 of the Atomic Energy Act by issuing a notice to...

  12. 23 CFR 500.110 - PTMS.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 23 Highways 1 2010-04-01 2010-04-01 false PTMS. 500.110 Section 500.110 Highways FEDERAL HIGHWAY ADMINISTRATION, DEPARTMENT OF TRANSPORTATION TRANSPORTATION INFRASTRUCTURE MANAGEMENT MANAGEMENT AND MONITORING SYSTEMS Management Systems § 500.110 PTMS. An effective PTMS for public transportation facilities...

  13. 7 CFR 966.110 - Order.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 8 2012-01-01 2012-01-01 false Order. 966.110 Section 966.110 Agriculture Regulations... Orders; Fruits, Vegetables, Nuts), DEPARTMENT OF AGRICULTURE TOMATOES GROWN IN FLORIDA Rules and Regulations Definitions § 966.110 Order. Order means Order No. 966 (§§ 966.1 to 966.92) regulating...

  14. 7 CFR 966.110 - Order.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 8 2011-01-01 2011-01-01 false Order. 966.110 Section 966.110 Agriculture Regulations... Orders; Fruits, Vegetables, Nuts), DEPARTMENT OF AGRICULTURE TOMATOES GROWN IN FLORIDA Rules and Regulations Definitions § 966.110 Order. Order means Order No. 966 (§§ 966.1 to 966.92) regulating...

  15. 7 CFR 966.110 - Order.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 7 Agriculture 8 2013-01-01 2013-01-01 false Order. 966.110 Section 966.110 Agriculture Regulations... ORDERS; FRUITS, VEGETABLES, NUTS), DEPARTMENT OF AGRICULTURE TOMATOES GROWN IN FLORIDA Rules and Regulations Definitions § 966.110 Order. Order means Order No. 966 (§§ 966.1 to 966.92) regulating...

  16. 7 CFR 945.110 - Order.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 8 2012-01-01 2012-01-01 false Order. 945.110 Section 945.110 Agriculture Regulations... Orders; Fruits, Vegetables, Nuts), DEPARTMENT OF AGRICULTURE IRISH POTATOES GROWN IN CERTAIN DESIGNATED COUNTIES IN IDAHO, AND MALHEUR COUNTY, OREGON Rules and Regulations Definitions § 945.110 Order....

  17. 7 CFR 945.110 - Order.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 7 Agriculture 8 2014-01-01 2014-01-01 false Order. 945.110 Section 945.110 Agriculture Regulations... ORDERS; FRUITS, VEGETABLES, NUTS), DEPARTMENT OF AGRICULTURE IRISH POTATOES GROWN IN CERTAIN DESIGNATED COUNTIES IN IDAHO, AND MALHEUR COUNTY, OREGON Rules and Regulations Definitions § 945.110 Order....

  18. 7 CFR 966.110 - Order.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 7 Agriculture 8 2014-01-01 2014-01-01 false Order. 966.110 Section 966.110 Agriculture Regulations... ORDERS; FRUITS, VEGETABLES, NUTS), DEPARTMENT OF AGRICULTURE TOMATOES GROWN IN FLORIDA Rules and Regulations Definitions § 966.110 Order. Order means Order No. 966 (§§ 966.1 to 966.92) regulating...

  19. 7 CFR 945.110 - Order.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 8 2010-01-01 2010-01-01 false Order. 945.110 Section 945.110 Agriculture Regulations... Orders; Fruits, Vegetables, Nuts), DEPARTMENT OF AGRICULTURE IRISH POTATOES GROWN IN CERTAIN DESIGNATED COUNTIES IN IDAHO, AND MALHEUR COUNTY, OREGON Rules and Regulations Definitions § 945.110 Order....

  20. 7 CFR 945.110 - Order.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 8 2011-01-01 2011-01-01 false Order. 945.110 Section 945.110 Agriculture Regulations... Orders; Fruits, Vegetables, Nuts), DEPARTMENT OF AGRICULTURE IRISH POTATOES GROWN IN CERTAIN DESIGNATED COUNTIES IN IDAHO, AND MALHEUR COUNTY, OREGON Rules and Regulations Definitions § 945.110 Order....

  1. 7 CFR 966.110 - Order.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 8 2010-01-01 2010-01-01 false Order. 966.110 Section 966.110 Agriculture Regulations... Orders; Fruits, Vegetables, Nuts), DEPARTMENT OF AGRICULTURE TOMATOES GROWN IN FLORIDA Rules and Regulations Definitions § 966.110 Order. Order means Order No. 966 (§§ 966.1 to 966.92) regulating...

  2. 7 CFR 945.110 - Order.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 7 Agriculture 8 2013-01-01 2013-01-01 false Order. 945.110 Section 945.110 Agriculture Regulations... ORDERS; FRUITS, VEGETABLES, NUTS), DEPARTMENT OF AGRICULTURE IRISH POTATOES GROWN IN CERTAIN DESIGNATED COUNTIES IN IDAHO, AND MALHEUR COUNTY, OREGON Rules and Regulations Definitions § 945.110 Order....

  3. 21 CFR 110.3 - Definitions.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 21 Food and Drugs 2 2011-04-01 2011-04-01 false Definitions. 110.3 Section 110.3 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) FOOD FOR HUMAN CONSUMPTION CURRENT GOOD MANUFACTURING PRACTICE IN MANUFACTURING, PACKING, OR HOLDING HUMAN FOOD General Provisions § 110.3 Definitions. The...

  4. 45 CFR 96.110 - Scope.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 45 Public Welfare 1 2012-10-01 2012-10-01 false Scope. 96.110 Section 96.110 Public Welfare DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL ADMINISTRATION BLOCK GRANTS Transition Provisions § 96.110 Scope. Except as otherwise stated, this subpart applies to the community services, preventive health and health services, alcohol and drug abuse...

  5. 48 CFR 2137.110 - Contract clause.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 48 Federal Acquisition Regulations System 6 2010-10-01 2010-10-01 true Contract clause. 2137.110 Section 2137.110 Federal Acquisition Regulations System OFFICE OF PERSONNEL MANAGEMENT, FEDERAL EMPLOYEES... CONTRACTING Service Contracts-General 2137.110 Contract clause. The clause at 2152.237-70 shall be inserted...

  6. 46 CFR 110.30-1 - General.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false General. 110.30-1 Section 110.30-1 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING GENERAL PROVISIONS Testing and Inspection § 110.30-1 General. (a) This section supplements the general requirements for testing and...

  7. 46 CFR 110.30-1 - General.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false General. 110.30-1 Section 110.30-1 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING GENERAL PROVISIONS Testing and Inspection § 110.30-1 General. (a) This section supplements the general requirements for testing and...

  8. 46 CFR 110.01-1 - General.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false General. 110.01-1 Section 110.01-1 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING GENERAL PROVISIONS Applicability § 110.01-1 General. (a) This subchapter applies to all electrical installations on vessels subject...

  9. 46 CFR 110.01-1 - General.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false General. 110.01-1 Section 110.01-1 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING GENERAL PROVISIONS Applicability § 110.01-1 General. (a) This subchapter applies to all electrical installations on vessels subject...

  10. High-Performance Supercapacitors from Niobium Nanowire Yarns.

    PubMed

    Mirvakili, Seyed M; Mirvakili, Mehr Negar; Englezos, Peter; Madden, John D W; Hunter, Ian W

    2015-07-01

    The large-ion-accessible surface area of carbon nanotubes (CNTs) and graphene sheets formed as yarns, forests, and films enables miniature high-performance supercapacitors with power densities exceeding those of electrolytics while achieving energy densities equaling those of batteries. Capacitance and energy density can be enhanced by depositing highly pseudocapacitive materials such as conductive polymers on them. Yarns formed from carbon nanotubes are proposed for use in wearable supercapacitors. In this work, we show that high power, energy density, and capacitance in yarn form are not unique to carbon materials, and we introduce niobium nanowires as an alternative. These yarns show higher capacitance and energy per volume and are stronger and 100 times more conductive than similarly spun carbon multiwalled nanotube (MWNT) and graphene yarns. The long niobium nanowires, formed by repeated extrusion and drawing, achieve device volumetric peak power and energy densities of 55 MW·m(-3) (55 W·cm(-3)) and 25 MJ·m(-3) (7 mWh·cm(-3)), 2 and 5 times higher than that for state-of-the-art CNT yarns, respectively. The capacitance per volume of Nb nanowire yarn is lower than the 158 MF·m(-3) (158 F·cm(-3)) reported for carbon-based materials such as reduced graphene oxide (RGO) and CNT wet-spun yarns, but the peak power and energy densities are 200 and 2 times higher, respectively. Achieving high power in long yarns is made possible by the high conductivity of the metal, and achievement of high energy density is possible thanks to the high internal surface area. No additional metal backing is needed, unlike for CNT yarns and supercapacitors in general, saving substantial space. As the yarn is infiltrated with pseudocapacitive materials such as poly(3,4-ethylenedioxythiophene) (PEDOT), the energy density is further increased to 10 MJ·m(-3) (2.8 mWh·cm(-3)). Similar to CNT yarns, niobium nanowire yarns are highly flexible and show potential for weaving into textiles

  11. Grain boundary {gamma}{double_prime} precipitation and niobium segregation in Inconel 718

    SciTech Connect

    Gao, M.; Wei, R.P.

    1995-04-01

    In a previous study, the surface enrichment and grain boundary segregation of niobium in the Inconel 718 single crystal and polycrystals were studied by x-ray photoelectron spectroscopy (XPS). Considerable segregation of niobium, about three to four times higher than that in bulk, was observed at the grain boundaries of the polycrystalline alloy. The observed niobium segregation was thought to be associated with the preferential formation of {gamma}{double_prime}-Ni{sub 3}Nb precipitates at the boundaries during aging. In this paper, the results of a transmission electron microscopic (TEM) study of grain boundary {gamma}{double_prime} precipitates and their relation to niobium segregation in the Inconel 718 are reported.

  12. Review of R&D at DESY on ingot niobium for accelerators

    NASA Astrophysics Data System (ADS)

    Navitski, Aliaksandr; Sekutowicz, Jacek; Singer, Waldemar; Singer, Xenia

    2015-12-01

    An R&D program at DESY exploring the potential of the production of 1.3 GHz TESLA shape cavities from large grain or ingot niobium material has been carried out as a feasibility study for using ingot niobium material for the European X-ray Free-Electron Laser project. The most important issues like feasibility of the fabrication of niobium discs from ingots, material properties, cavity fabrication, treatment, and finally the cryogenic radiofrequency (RF) performance of the cavity in the accelerator modules are presented and discussed. At least 25% higher intrinsic quality factor comparing to conventional fine-grain niobium and high accelerating gradient of up to 45 MV/m have been demonstrated during the cryogenic RF tests both in the vertical cryostats and in a completely assembled accelerating cryo-module.

  13. Niobium Thin Film Properties Affected by Deposition Energy during Vacuum Deposition

    SciTech Connect

    Genfa Wu; H. Phillips; Ronald Sundelin; Anne-Marie Valente

    2003-05-01

    In order to understand and improve the super-conducting performance of niobium thin films at cryogenic temperatures, an energetic vacuum deposition system has been developed to study deposition energy effects on the properties of niobium thin films on various substrates. Ultra high vacuum avoids the gaseous inclusions in thin films commonly seen in sputtering deposition. A retarding field energy analyzer is used to measure the kinetic energy of niobium ions at the substrate location. A biased substrate holder controls the deposition energy. Transition temperature and residual resistivity ratio (RRR) of the niobium thin films at several deposition energies are obtained together with crystal orientation measurements and atomic force microscope (AFM) inspection, and the results show that there exists a preferred deposition energy around 115eV (the average deposition energy 64 eV plus the 51 V bias voltage).

  14. Iron-niobium-aluminum alloy having high-temperature corrosion resistance

    DOEpatents

    Hsu, Huey S.

    1988-04-14

    An alloy for use in high temperature sulfur and oxygen containing environments, having aluminum for oxygen resistance, niobium for sulfur resistance and the balance iron, is discussed. 4 figs., 2 tabs.

  15. Improving the oxidation protection of niobium and tantalum by the use of multilayer coatings

    NASA Astrophysics Data System (ADS)

    Dzyadykevich, Y. V.; Kytskay, L. I.

    1997-01-01

    This article examines how the applicability of the refractory metals niobium and tantalum in high-temperature applications can be improved through the use of high-temperature, multilayer coatings based on molybdenum disilicide for oxidation resistance.

  16. Reclamation of niobium compounds from ionic liquid electrochemical polishing of superconducting radio frequency cavities

    SciTech Connect

    Wixtrom, Alex I.; Buhler, Jessica E.; Reece, Charles E.; Abdel-Fattah, Tarek M.

    2013-06-01

    Recent research has shown that choline chloride (vitamin B4)-based solutions can be used as a greener alternative to acid-based electrochemical polishing solutions. This study demonstrated a successful method for electrochemical deposition of niobium compounds onto the surface of copper substrates using a novel choline chloride-based ionic liquid. Niobium ions present in the ionic liquid solution were dissolved into the solution prior to deposition via electrochemical polishing of solid niobium. A black coating was clearly visible on the surface of the Cu following deposition. This coating was analyzed using scanning electron microscopy (SEM), electron dispersive X-ray spectroscopy (EDX), atomic force microscopy (AFM), and X-ray fluorescence spectroscopy (XRF). This ionic liquid-based electrochemical deposition method effectively recycles previously dissolved niobium from electrochemical polishing of superconducting radio frequency (SRF) cavities.

  17. Review of R&D at DESY on ingot niobium for accelerators

    SciTech Connect

    Navitski, Aliaksandr Sekutowicz, Jacek Singer, Waldemar Singer, Xenia

    2015-12-04

    An R&D program at DESY exploring the potential of the production of 1.3 GHz TESLA shape cavities from large grain or ingot niobium material has been carried out as a feasibility study for using ingot niobium material for the European X-ray Free-Electron Laser project. The most important issues like feasibility of the fabrication of niobium discs from ingots, material properties, cavity fabrication, treatment, and finally the cryogenic radiofrequency (RF) performance of the cavity in the accelerator modules are presented and discussed. At least 25% higher intrinsic quality factor comparing to conventional fine-grain niobium and high accelerating gradient of up to 45 MV/m have been demonstrated during the cryogenic RF tests both in the vertical cryostats and in a completely assembled accelerating cryo-module.

  18. Physical and mechanical properties of single and large crystal high-RRR niobium

    SciTech Connect

    Ganapati Myneni

    2005-07-10

    High RRR bulk niobium SRF cavities are the building blocks of the latest and future particle accelerators, free electron lasers (FEL's) and energy recovery linacs (ERL's.). These cavities are fabricated from high purity (RRR) poly crystalline niobium sheets via deep drawing, e-beam welding and surface treatment to obtain high accelerating gradients and quality factors. However, the starting bulk RRR niobium properties are not yet optimized with respect to both cost reduction and achievement of ultimate performance. A major limitation in achieving the highest performance can possibly be attributed to imperfections at or near the grain boundaries. Recently, at Jefferson Lab single/large grain RRR niobium cavities are developed using customized RRR ingots with optimized amounts of impurities such as Tantalum and minimizing the interstitial contents (O, C, N and H).

  19. SIMS analysis of high-performance accelerator niobium

    SciTech Connect

    Maheshwari, P.; Stevie, F. A.; Myneni, Ganapati Rao; Rigsbee, J, M.; Dhakal, Pashupati; Ciovati, Gianluigi; Griffis, D. P.

    2014-11-01

    Niobium is used to fabricate superconducting radio frequency accelerator modules because of its high critical temperature, high critical magnetic field, and easy formability. Recent experiments have shown a very significant improvement in performance (over 100%) after a high-temperature bake at 1400 degrees C for 3h. SIMS analysis of this material showed the oxygen profile was significantly deeper than the native oxide with a shape that is indicative of diffusion. Positive secondary ion mass spectra showed the presence of Ti with a depth profile similar to that of O. It is suspected that Ti is associated with the performance improvement. The source of Ti contamination in the anneal furnace has been identified, and a new furnace was constructed without Ti. Initial results from the new furnace do not show the yield improvement. Further analyses should determine the relationship of Ti to cavity performance.

  20. Thermodynamic Evaluation of Hydrogen Absorption by Niobium During SRF Fabrication

    SciTech Connect

    Ricker, R. E.; Myneni, G. R.

    2011-03-31

    The properties and performance of the ultra high purity Nb used to fabricate superconducting radio frequency (SRF) particle accelerator cavities have been found to vary with processing conditions. One hypothesis for these variations is that hydrogen, absorbed during processing, is responsible for this behavior. The key assumption behind this hypothesis is that niobium can absorb hydrogen from one or more of the processing environments. This paper reviews work examining the validity of this assumption. It was determined that Nb will spontaneously react with water producing adsorbed atomic hydrogen that is readily absorbed into the metal. The passivating oxide film normally prevents this reaction, but this film is frequently removed during processing and it is attacked by the fluoride ion used in the polishing solutions for SRF cavities. However, during electropolishing that cathodic reduction of hydrogen is transferred to the auxiliary electrode and this should suppress hydrogen absorption.

  1. Thermodynamic Evaluation of Hydrogen Absorption by Niobium During SRF Fabrication

    SciTech Connect

    R.E. Ricker, G.R. Myneni

    2011-03-01

    The properties and performance of the ultra high purity Nb used to fabricate superconducting radio frequency (SRF) particle accelerator cavities have been found to vary with processing conditions. One hypothesis for these variations is that hydrogen, absorbed during processing, is responsible for this behavior. The key assumption behind this hypothesis is that niobium can absorb hydrogen from one or more of the processing environments. This paper reviews work examining the validity of this assumption. It was determined that Nb will spontaneously react with water producing adsorbed atomic hydrogen that is readily absorbed into the metal. The passivating oxide film normally prevents this reaction, but this film is frequently removed during processing and it is attacked by the fluoride ion used in the polishing solutions for SRF cavities. However, during electropolishing that cathodic reduction of hydrogen is transferred to the auxiliary electrode and this should suppress hydrogen absorption.

  2. Surface Participation Effects in Titanium Nitride and Niobium Resonators

    NASA Astrophysics Data System (ADS)

    Dove, Allison; Kreikebaum, John Mark; Livingston, William; Delva, Remy; Qiu, Yanjie; Lolowang, Reinhard; Ramasesh, Vinay; O'Brien, Kevin; Siddiqi, Irfan

    Improving the coherence time of superconducting qubits requires a precise understanding of the location and density of surface defects. Superconducting microwave resonators are commonly used for quantum state readout and are a versatile testbed to systematically characterize materials properties as a function of device geometry and fabrication method. We report on sputter deposited titanium nitride and niobium on silicon coplanar waveguide resonators patterned using reactive ion etches to define the device geometry. We discuss the impact of different growth conditions (temperature and electrical bias) and processing techniques on the internal quality factor (Q) of these devices. In particular, to investigate the effect of surface participation, we use a Bosch process to etch many-micron-deep trenches in the silicon substrate and quantify the impact of etch depth and profile on the internal Q. This research was supported by the ARO.

  3. Metastable structures in drop tube processed niobium based alloys

    NASA Astrophysics Data System (ADS)

    Evans, N. D.; Bayuzick, R. J.; Kenik, E. A.

    Analytical electron microscopy has been employed to reveal metastable structures in near eutectic niobium-germanium alloys which were processed in a 100 meter drop tube. Drop masses were generally 300 to 400-mg, with undercooling as much as 0.14-Tm prior to recalescence. Specimens which were slightly hypoeutectic and undercooled 0.10 below the liquidus prior to recalescence contain β cells which grew with solute rejection, and an intercellular metastable α + Nb5Ge3 eutectic. When deep undercooling was followed by Rapid Solidification Processing (RSP) via splatting onto a copper block, cellular β formed with solute entrapment, though the high cooling rate of RSP did not prevent the formation of Nb5Ge3 precipitates from the Ge enriched β. In one specimen, an amorphous Nb-Ge phase has been identified.

  4. Temperature Mapping of Nitrogen-doped Niobium Superconducting Radiofrequency Cavities

    SciTech Connect

    Makita, Junki; Ciovati, Gianluigi; Dhakal, Pashupati

    2015-09-01

    It was recently shown that diffusing nitrogen on the inner surface of superconducting radiofrequency (SRF) cavities at high temperature can improve the quality factor of the niobium cavity. However, a reduction of the quench field is also typically found. To better understand the location of rf losses and quench, we used a thermometry system to map the temperature of the outer surface of ingot Nb cavities after nitrogen doping and electropolishing. Surface temperature of the cavities was recorded while increasing the rf power and also during the quenching. The results of thermal mapping showed no precursor heating on the cavities and quenching to be ignited near the equator where the surface magnetic field is maximum. Hot-spots at the equator area during multipacting were also detected by thermal mapping.

  5. Performance of Large grain and Single Crystal Niobium Cavities

    SciTech Connect

    Kneisel, Peter; Ciovati, Gianluigi; Sekutowicz, Jacek

    2006-07-01

    We have fabricated and tested several single and one multi-cell cavity made from large grain niobium of four different ingots. Two cavities at a frequency of ~ 2.2 GHz were made from single crystal sheets. Large grain material was used for four single cell cavities of the HG â and OC shapes, a 7-cell cavity of the HG â shape â all resonating at 1500 MHz â and an ILC_LL single cell cavity at 1300 MHz. We began to explore also different chemical polishing baths such as a 1:1:1 and a 1:1:2 buffered solution and explored the change of cavity performance as a function of material removal. The results from these preliminary investigations are reported in this contribution.

  6. Synthesis and characterization of superconducting nanocrystalline niobium nitride.

    PubMed

    Shi, Liang; Gu, Yunle; Chen, Luyang; Yang, Zeheng; Ma, Jianhua; Qian, Yitai

    2005-02-01

    Nanocrystalline niobium nitride (NbN0.9) was successfully synthesized at 600 degrees C through a solid-state reaction. The synthesis was carried out in an autoclave by using NbCl5 and NaN3 as the reactants. The X-ray powder diffraction pattern indicates the formation of cubic NbN0.9. Transmission electron microscopy images show that typical NbN0.9 crystallites are composed of uniform particles with an average size of about 30 nm and nanorod crystallites with a typical size of about 40 x 2500 nm. Magnetic measurements exhibited that a superconducting transition occurred at 15.4 K for the NbN0.9 product. PMID:15853151

  7. EXAFS structure and electrical properties of lithium niobium phosphate

    SciTech Connect

    Bruque, S.; Martinez Lara, M.; Moreno, L.

    1995-02-01

    The acidic character of the hydration water in NbOPO{sub 4} {center_dot} 2H{sub 2}O permits the exchange of protons for Li{sup +} ions. The lithium phase annealed at 773 K presents a slightly distorted lattice with respect to the niobium phosphate network, allowing high mobility of the lithium ion. The structural modifications due to Li insertion have been studied by extended X-ray absorption spectroscopy (EXAFS) at the Nb K-edge. The analysis of the EXAFS spectra indicates the presence of an additional oxygen atom close to Nb which is probably not bonded to the framework. The ionic conductivity of the LiNb(OH)OPO{sub 4} phase is high and increases up to 880 K. At higher temperatures, the Li{sup +} ion migrates to a permanent position in the network and the ionic conductivity is then stopped.

  8. Springback in Deep Drawn High Purity Niobium for Superconductor Cavities

    SciTech Connect

    Ganapati Rao Myneni; Peter Kneisel

    2005-09-01

    Superconducting radio frequency (SRF) cavities made from deep drawn high-purity niobium have become a popular approach for the design of particle accelerators. A number of current accelerators use this technology and it is a leading candidate for future designs. The development of this technology has required significant advances in many scientific fields including metallurgy, high vacuum physics, surface science, and forming. Recently proposed modifications to the current process for fabrication of these cavities has resulted in increased concern about the distribution of deformation, residual stress patterns, and springback. This presentation will report on the findings of a recently initiated program to study plastic flow and springback in the fabrication of these cavities and the influence of metallurgical variables including grain size and impurity content.

  9. Characterization on RF magnetron sputtered niobium pentoxide thin films

    SciTech Connect

    Usha, N.; Sivakumar, R.; Sanjeeviraja, C.

    2014-10-15

    Niobium pentoxide (Nb{sub 2}O{sub 5}) thin films with amorphous nature were deposited on microscopic glass substrates at 100°C by rf magnetron sputtering technique. The effect of rf power on the structural, morphological, optical, and vibrational properties of Nb{sub 2}O{sub 5} films have been investigated. Optical study shows the maximum average transmittance of about 87% and the optical energy band gap (indirect allowed) changes between 3.70 eV and 3.47 eV. AFM result indicates the smooth surface nature of the samples. Photoluminescence measurement showed the better optical quality of the deposited films. Raman spectra show the LO-TO splitting of Nb-O stretching of Nb{sub 2}O{sub 5} films.

  10. Secondary electron emission from plasma processed accelerating cavity grade niobium

    NASA Astrophysics Data System (ADS)

    Basovic, Milos

    by different techniques. Specifically, this work provides the results of SEY from the plasma cleaned cavity grade niobium (Nb) samples. Pure niobium is currently the material of choice for the fabrication of Superconducting Radio Frequency (SRF) cavities. The effect of plasma processing with two different gases will be examined in two groups of samples. The first group of samples is made from cavity grade niobium. The second group of samples is made from the same material, but include a welded joint made by electron beam welding, since in niobium SRF cavities the peak electric and magnetic field are seen in close proximity to the welded joints. Both groups of samples will be exposed to nitrogen (N2) and a mixture of argon with oxygen (Ar/O2) plasma. It is the goal of this research to determine the SEY on these two groups of samples before and after plasma processing as a function of the energy of primary electrons. The SEY as a function of the angle of incidence of the primary electrons is tested on the samples treated with Ar/O2 plasma.

  11. Quantum Phase Slips in 6 mm Long Niobium Nanowire.

    PubMed

    Zhao, Weiwei; Liu, Xin; Chan, M H W

    2016-02-10

    Transport measurements were made to study the superconducting transition of four 6 mm long niobium nanowires with different cross-sectional dimensions. A low-temperature residual resistance tail measured with an excitation current of 5 nA is found in the thinnest wire down to 50 mK or 7.7% of Tc of Nb. The functional form of the residual resistance is consistent with quantum phase slip (QPS) processes. Resistance measured at high bias excitation current switches among many discrete values that are well below the normal state resistance. These discrete resistance values as a function of temperature fall into several parallel curves all showing QPS-like decay in the low temperature limit similar to that found at low current. The coexistence of QPS-like resistance tails and resistance jumps found in the same wire unifies results from previous experiments where these two distinct sets of evidence for QPS are exclusive of each other. PMID:26788964

  12. Fabricating niobium test loops for the SP-100 space reactor

    NASA Technical Reports Server (NTRS)

    Bryhan, Anthony J.; Chan, Ricky C.

    1993-01-01

    This article describes the successful fabrication, operation, and evaluation of a series of niobium-alloy (Nb-1 Zr and PWC-11) thermal convection loops designed to contain and circulate molten lithium at 1,350 K. These loops were used to establish the fabrication variables of significance for a nuclear power supply for space. Approximately 200 weldments were evaluated for their tendency to be attacked by lithium as a function of varying atmospheric contamination. No attack occurred for any weldment free of contamination, with or without heat treatment, and no welds accidentally deviated from purity. The threshold oxygen content for weldment attack was determined to be 170-200 ppm. Attack varied directly with weldment oxygen and nitrogen contents.

  13. High-gradient, pulsed operation of superconducting niobium cavities

    SciTech Connect

    Campisi, I.E.; Farkas, Z.D.

    1984-02-01

    Tests performed on several Niobium TM/sub 010/ cavities at frequencies of about 2856 MHz using a high-power, pulsed method indicate that, at the end of the charging pulse, peak surface magnetic fields of up to approx. 1300 Oe, corresponding to a peak surface electric field of approx. 68 MV/m, can be reached at 4.2/sup 0/K without appreciable average losses. Further studies of the properties of superconductors under pulsed operation might shed light on fundamental properties of rf superconductivity, as well as lead to the possibility of applying the pulse method to the operation of high-gradient linear colliders. 7 references, 30 figures, 2 tables.

  14. Properties and potential of high-temperature niobium beryllides

    SciTech Connect

    Bruemmer, S.M.; Brimhall, J.L.; Henager, C.H. Jr.; Hirth, J.P.

    1992-12-01

    Recent research on the low- and high-temperature properties of two beryllium-niobium intermetallic compounds, Be{sub l2}Nb and Be{sub l7}Nb{sub 2}, is reviewed and discussed. Strength (bend and compression), hardness and fracture toughness has been mapped as a function of test temperature up to 1200C. Results for hot-isostatically-pressed Be{sub 12}Nb and Be{sub l7}Nb{sub 2} are highlighted illustrating the potential for reasonable strength at both low and high temperatures. Limitations for structural use of the beryllides are identified and discussed including low-temperature toughness, intermediate-temperature embrittlement, high-temperature creep strength and composite compatability.

  15. Method of manufacturing a niobium-aluminum-germanium superconductive material

    DOEpatents

    Wang, John L.; Pickus, Milton R.; Douglas, Kent E.

    1980-01-01

    A method for manufacturing flexible Nb.sub.3 (Al,Ge) multifilamentary superconductive material in which a sintered porous niobium compact is infiltrated with an aluminum-germanium alloy and thereafter deformed and heat treated in a series of steps at different successively higher temperatures preferably below 1000.degree. C. to produce filaments composed of Nb.sub.3 (Al,G3) within the compact. By avoiding temperatures in excess of 1000.degree. C. during the heat treatment, cladding material such as copper can be applied to facilitate a deformation step preceding the heat treatment and can remain in place through the heat treatment to also serve as a temperature stabilizer for supeconductive material produced. Further, these lower heat treatment temperatures favor formation of filaments with reduced grain size and, hence with more grain boundaries which in turn increase the current-carrying capacity of the superconductive material.

  16. Room-temperature dislocation climb in copper-niobium interfaces

    SciTech Connect

    Wang, Jian; Hoagland, Richard G; Hirth, John P; Misra, Amit

    2008-01-01

    Using atomistic simulations, we show that dislocations climb efficiently in metallic copper-niobium interfaces through absorption and emission of vacancies in the dislocation core, as well as an associated counter diffusion of Cu atoms in the interfacial plane. The high efficiency of dislocation climb in the interface is ascribed to the high vacancy concentration of 0.05 in the interfacial plane, the low formation energy of 0.12 e V with respect to removal or insertion of Cu atoms, as well as the low kinetic barrier of 0.10 eV for vacancy migration in the interfacial Cu plane. Dislocation climb in the interface facilitates reactions of interfacial dislocations, and enables interfaces to be in the equilibrium state with respect to concentrations ofpoint defects.

  17. Hardness behavior of binary and ternary niobium alloys at 77 and 300 K

    NASA Technical Reports Server (NTRS)

    Stephens, J. R.; Witzke, W. R.

    1974-01-01

    The effects of alloy additions of zirconium, hafnium, molybdenum, tungsten, rhenium, ruthenium, osmium, rhodium, and iridium on the hardness of niobium was determined. Both binary and ternary alloys were investigated by means of hardness tests at 77 K and 300 K. Results showed that atomic size misfit plays a dominant role in controlling hardness of binary niobium alloys. Alloy softening, which occurred at dilute solute additions, is most likely due to an extrinsic mechanism involving interaction between solute elements and interstitial impurities.

  18. Quench-age method for the fabrication of niobium-aluminum superconductors

    DOEpatents

    Pickus, Milton R.; Ciardella, Robert L.

    1978-01-01

    A flexible Nb.sub.3 Al superconducting wire is fabricated from a niobium-aluminum composite wire by heating to form a solid solution which is retained at room temperature as a metastable solid solution by quenching. The metastable solid solution is then transformed to the stable superconducting A-15 phase by low temperature aging. The transformation induced by aging can be controlled to yield either a multifilamentary or a solid A-15 core surrounded by ductile niobium.

  19. Niobium quarter-wave cavity for the New Delhi booster linac

    SciTech Connect

    Shepard, K.W.; Roy, A.; Potukuchi, P.N.

    1997-09-01

    This paper reports the completion of development of a 97 Mhz niobium coaxial quarter-wave cavity to be used in a booster linac for the New Delhi 16UD pellatron electrostatic accelerator. A prototype cavity, which incorporates a niobium-bellows tuning device, has been completed and operated at 4.2 K at accelerating gradients above 4 MV/m for extended periods of time.

  20. High performance superconducting radio frequency ingot niobium technology for continuous wave applications

    SciTech Connect

    Dhakal, Pashupati Ciovati, Gianluigi Myneni, Ganapati R.

    2015-12-04

    Future continuous wave (CW) accelerators require the superconducting radio frequency cavities with high quality factor and medium accelerating gradients (≤20 MV/m). Ingot niobium cavities with medium purity fulfill the specifications of both accelerating gradient and high quality factor with simple processing techniques and potential reduction in cost. This contribution reviews the current superconducting radiofrequency research and development and outlines the potential benefits of using ingot niobium technology for CW applications.