Science.gov

Sample records for particle x-ray spectrometer

  1. Solar Intensity X-ray and particle Spectrometer (SIXS)

    NASA Astrophysics Data System (ADS)

    Huovelin, J.; Vainio, R.; Andersson, H.; Valtonen, E.; Alha, L.; Mälkki, A.; Grande, M.; Fraser, G. W.; Kato, M.; Koskinen, H.; Muinonen, K.; Näränen, J.; Schmidt, W.; Syrjäsuo, M.; Anttila, M.; Vihavainen, T.; Kiuru, E.; Roos, M.; Peltonen, J.; Lehti, J.; Talvioja, M.; Portin, P.; Prydderch, M.

    2010-01-01

    The Solar Intensity X-ray and particle Spectrometer (SIXS) on the BepiColombo Mercury Planetary Orbiter (MPO) will investigate the direct solar X-rays, and energetic protons and electrons which pass the Spacecraft on their way to the surface of Mercury. These measurements are vitally important for understanding quantitatively the processes that make Mercury's surface glow in X-rays, since all X-rays from Mercury are due to interactions of the surface with incoming highly energetic photons and space particles. The X-ray emission of Mercury's surface will be analysed to understand its structure and composition. SIXS data will also be utilised for studies of the solar X-ray corona, flares, solar energetic particles, and the magnetosphere of Mercury, and for providing information on solar eruptions to other BepiColombo instruments. SIXS consists of two detector subsystems. The X-ray detector system includes three identical GaAs PIN detectors which measure the solar spectrum at 1-20 keV energy range, and their combined field-of-view covers ˜1/4 of the whole sky. The particle detector system consists of an assembly including a cubic central CsI(Tl) scintillator detector with five of its six surfaces covered by a thin Si detector, which together perform low-resolution particle spectroscopy with a rough angular resolution over a field-of-view covering ˜1/4 of the whole sky. The energy range of detected particle spectra is 0.1-3 MeV for electrons and 1-30 MeV for protons. A major task for the SIXS instrument is the measurement of solar X-rays on the dayside of Mercury's surface to enable modeling of X-ray fluorescence and scattering on the planet's surface. Since highly energetic particles are expected to also induce a significant amount of X-ray emission via particle-induced X-ray emission (PIXE) and bremsstrahlung when they are absorbed by the solid surface of the planet Mercury, SIXS performs measurements of fluxes and spectra of protons and electrons. SIXS performs

  2. Alpha Particle X-Ray Spectrometer (APXS) on-board Chandrayaan-2 rover

    NASA Astrophysics Data System (ADS)

    Shanmugam, M.; Murty, S. V. S.; Acharya, Y. B.; Goyal, S. K.; Patel, Arpit R.; Shah, Bhumi; Hait, A. K.; Patinge, Aditya; Subrahmanyam, D.

    2014-11-01

    Alpha Particle X-ray Spectrometer (APXS) payload configuration for Chandrayaan-2 rover has been completed recently and fabrication of mechanical assembly, PCB layout design and fabrication are in progress. Here we present the design and performance evaluation of various subsystems developed for APXS payload. The low energy threshold of <1 keV and the energy resolution of ∼150 eV at 5.9 keV, for the Silicon Drift Detector (SDD), as measured from the developed APXS electronics is comparable to the standard spectrometers available off-the-shelf. We have also carried out experiments for measuring fluorescent X-ray spectrum from various standard samples from the USGS catalog irradiated by the laboratory X-ray source 241Am with 1 mCi activity. It is shown that intensities of various characteristic X-ray lines are well correlated with the respective elemental concentrations.

  3. X-ray Spectrometer

    NASA Technical Reports Server (NTRS)

    Porter, F. Scott

    2004-01-01

    The X-ray Spectrometer (XRS) instrument is a revolutionary non-dispersive spectrometer that will form the basis for the Astro-E2 observatory to be launched in 2005. We have recently installed a flight spare X R S microcalorimeter spectrometer at the EBIT-I facility at LLNL replacing the XRS from the earlier Astro-E mission and providing twice the resolution. The X R S microcalorimeter is an x-ray detector that senses the heat deposited by the incident photon. It achieves a high energy resolution by operating at 0.06K and by carefully controlling the heat capacity and thermal conductance. The XRS/EBIT instrument has 32 pixels in a square geometry and achieves an energy resolution of 6 eV at 6 keV, with a bandpass from 0.1 to 12 keV (or more at higher operating temperature). The instrument allows detailed studies of the x-ray line emission of laboratory plasmas. The XRS/EBIT also provides an extensive calibration "library" for the Astro-E2 observatory.

  4. Results of the Alpha-Particle-X-Ray Spectrometer on Board of the Mars Exploration Rovers

    NASA Technical Reports Server (NTRS)

    Geller, R.; Zipfel, J.; Brueckner, J.; Dreibus, G.; Lugmair, G.; Rieder, R.; Waenke, H.; Klingelhoefer, G.; Clark, B. C.; Ming, D. W.

    2005-01-01

    The Mars Exploration Rovers Spirit and Opportunity landed at Gusev crater and Meridiani Planum. The Alpha Particle X-ray Spectrometer (APXS) is part of the instrument suite on both rovers. It is equipped with six 244Cm sources which provide x-ray excitation with alpha-particles (PIXE) and x-ray radiation (XRF). This combination allows x-ray spectroscopy of elements from Na to Br in the energy range of 0.9 to 16 keV. X-ray detectors with a high energy resolution of 160 eV at Fe K allow us to separate even closely spaced energy peaks, such as Na, Mg, Al and Si. The APXS is attached to the rover s arm and provides in-situ measurements of the chemical composition of soils, surfaces of rocks and outcrops and their abraded surfaces. This abstract gives an overview of APXS results obtained during the first year of operation on both landing sites.

  5. Chemistry of Rocks and Soils in Gusev Crater from the Alpha Particle X-ray Spectrometer

    NASA Technical Reports Server (NTRS)

    Gellert, R.; Rieder, R.; Anderson, R. C.; Brueckner, J.; Clark, B. C.; Dreibus, G.; Economou, T.; Klingelhoefer, G.; Lugmair, G. W.; Ming, D. W.

    2005-01-01

    The alpha particle x-ray spectrometer on the Spirit rover determined major and minor elements of soils and rocks in Gusev crater in order to unravel the crustal evolution of planet Mars. The composition of soils is similar to those at previous landing sites, as a result of global mixing and distribution by dust storms. Rocks (fresh surfaces exposed by the rock abrasion tool) resemble volcanic rocks of primitive basaltic composition with low intrinsic potassium contents. High abundance of bromine (up to 170 parts per million) in rocks may indicate the alteration of surfaces formed during a past period of aqueous activity in Gusev crater.

  6. Mapping alpha-Particle X-Ray Fluorescence Spectrometer (Map-X)

    NASA Technical Reports Server (NTRS)

    Blake, D. F.; Sarrazin, P.; Bristow, T.

    2014-01-01

    Many planetary surface processes (like physical and chemical weathering, water activity, diagenesis, low-temperature or impact metamorphism, and biogenic activity) leave traces of their actions as features in the size range 10s to 100s of micron. The Mapping alpha-particle X-ray Spectrometer ("Map-X") is intended to provide chemical imaging at 2 orders of magnitude higher spatial resolution than previously flown instruments, yielding elemental chemistry at or below the scale length where many relict physical, chemical, and biological features can be imaged and interpreted in ancient rocks.

  7. Chemistry of rocks and soils in Gusev Crater from the alpha particle x-ray spectrometer.

    PubMed

    Gellert, R; Rieder, R; Anderson, R C; Brückner, J; Clark, B C; Dreibus, G; Economou, T; Klingelhöfer, G; Lugmair, G W; Ming, D W; Squyres, S W; D'Uston, C; Wänke, H; Yen, A; Zipfel, J

    2004-08-01

    The alpha particle x-ray spectrometer on the Spirit rover determined major and minor elements of soils and rocks in Gusev crater in order to unravel the crustal evolution of planet Mars. The composition of soils is similar to those at previous landing sites, as a result of global mixing and distribution by dust storms. Rocks (fresh surfaces exposed by the rock abrasion tool) resemble volcanic rocks of primitive basaltic composition with low intrinsic potassium contents. High abundance of bromine (up to 170 parts per million) in rocks may indicate the alteration of surfaces formed during a past period of aqueous activity in Gusev crater. PMID:15297665

  8. [Near infrared distance sensing method for Chang'e-3 alpha particle X-ray spectrometer].

    PubMed

    Liang, Xiao-Hua; Wu, Ming-Ye; Wang, Huan-Yu; Peng, Wen-Xi; Zhang, Cheng-Mo; Cui, Xing-Zhu; Wang, Jin-Zhou; Zhang, Jia-Yu; Yang, Jia-Wei; Fan, Rui-Rui; Gao, Min; Liu, Ya-Qing; Zhang, Fei; Dong, Yi-Fan; Guo, Dong-Ya

    2013-05-01

    Alpha particle X-ray spectrometer (APXS) is one of the payloads of Chang'E-3 lunar rover, the scientific objective of which is in-situ observation and off-line analysis of lunar regolith and rock. Distance measurement is one of the important functions for APXS to perform effective detection on the moon. The present paper will first give a brief introduction to APXS, and then analyze the specific requirements and constraints to realize distance measurement, at last present a new near infrared distance sensing algorithm by using the inflection point of response curve. The theoretical analysis and the experiment results verify the feasibility of this algorithm. Although the theoretical analysis shows that this method is not sensitive to the operating temperature and reflectance of the lunar surface, the solar infrared radiant intensity may make photosensor saturation. The solutions are reducing the gain of device and avoiding direct exposure to sun light. PMID:23905352

  9. The Alpha Particle X-Ray Spectrometer (APXS): Results from Gusev Crater and Calibration Report

    NASA Technical Reports Server (NTRS)

    Gellert, R.; Rieder, R.; Brueckner, J.; Clark, B.; Dreibus, G.; Klingelhoefer, G.; Lugmair, G.; Ming, D.; Waenke, H.; Yen, A.; Zipfel, J.; Squyres, S.

    2006-01-01

    The chemical composition of rocks and soils on Mars analyzed during the Mars Exploration Rover Spirit Mission was determined by X-ray analyses with the Alpha Particle X-Ray Spectrometer (APXS). Details of the data analysis method and the instrument calibration are presented. Measurements performed on Mars to address geometry effects and background contributions are shown. Cross calibration measurements among several instrument sensors and sources are discussed. An unintentional swap of the two flight instruments is evaluated. New concentration data acquired during the first 470 sols of rover Spirit in Gusev Crater are presented. There are two geological regions, the Gusev plains and the Columbia Hills. The plains contain soils that are very similar to previous landing sites on Mars. A meteoritic component in the soil is identified. Rocks in the plains revealed thin weathering rinds. The underlying abraded rock was classified as primitive basalt. One of these rocks contained significant Br that is probably associated with vein-filling material of different composition. One of the trenches showed large subsurface enrichments of Mg, S, and Br. Disturbed soils and rocks in the Columbia Hills revealed different elemental compositions. These rocks are significantly weathered and enriched in mobile elements, such as P, S, Cl, or Br. Even abraded rock surfaces have high Br concentrations. Thus, in contrast to the rocks and soils in the Gusev Plains, the Columbia Hills material shows more significant evidence of ancient aqueous alteration.

  10. Calibration of the Mars Science Laboratory Alpha Particle X-ray Spectrometer

    NASA Astrophysics Data System (ADS)

    Campbell, John L.; Perrett, Glynis M.; Gellert, Ralf; Andrushenko, Stefan M.; Boyd, Nicholas I.; Maxwell, John A.; King, Penelope L.; Schofield, Céleste D. M.

    2012-09-01

    The alpha-particle X-ray spectrometer (APXS) for the Mars Science Laboratory (MSL) mission was calibrated for routine analysis of: Na, Mg, Al, Si, P, S, Cl, K, Ca, Ti, Cr, Mn, Fe, Ni, Zn, Br, Rb, Sr, and Y. The following elements were also calibrated, but may be too low to be measured (10s-100s ppm) for their usual abundance on Mars: V, Cu, Ga, As, Se and W. An extensive suite of geological reference materials, supplemented by pure chemical elements and compounds was used. Special attention was paid to include phyllosilicates, sulfates and a broad selection of basalts as these are predicted minerals and rocks at the Gale Crater landing site. The calibration approach is from first principles, using fundamental physics parameters and an assumed homogeneous sample matrix to calculate expected elemental signals for a given instrument setup and sample composition. Resulting concentrations for most elements accord with expected values. Deviations in elements of lower atomic number (Na, Mg, Al) indicate significant influences of mineral phases, especially in basalts, ultramafic rocks and trachytes. The systematics of these deviations help us to derive empirical, iterative corrections for different rock groups, based on a preliminary APXS analysis which assumes a homogeneous sample. These corrections have the potential to significantly improve the accuracy of APXS analyses, especially when other MSL instrument results, such as the X-ray diffraction data from CheMin, are included in the overall analysis process.

  11. Imaging X-ray spectrometer

    NASA Astrophysics Data System (ADS)

    Grant, P. A.; Jackson, J. W., Jr.; Alcorn, G. E.; Marshall, F. E.

    1984-09-01

    An X-ray spectrometer for providing imaging and energy resolution of an X-ray source is described. This spectrometer is comprised of a thick silicon wafer having an embedded matrix or grid of aluminum completely through the wafer fabricated, for example, by thermal migration. The aluminum matrix defines the walls of a rectangular array of silicon X-ray detector cells or pixels. A thermally diffused aluminum electrode is also formed centrally through each of the silicon cells with biasing means being connected to the aluminum cell walls and causes lateral charge carrier depletion between the cell walls so that incident X-ray energy causes a photoelectric reaction within the silicon producing collectible charge carriers in the form of electrons which are collected and used for imaging.

  12. Imaging X-ray spectrometer

    NASA Technical Reports Server (NTRS)

    Grant, P. A.; Jackson, J. W., Jr.; Alcorn, G. E.; Marshall, F. E. (Inventor)

    1984-01-01

    An X-ray spectrometer for providing imaging and energy resolution of an X-ray source is described. This spectrometer is comprised of a thick silicon wafer having an embedded matrix or grid of aluminum completely through the wafer fabricated, for example, by thermal migration. The aluminum matrix defines the walls of a rectangular array of silicon X-ray detector cells or pixels. A thermally diffused aluminum electrode is also formed centrally through each of the silicon cells with biasing means being connected to the aluminum cell walls and causes lateral charge carrier depletion between the cell walls so that incident X-ray energy causes a photoelectric reaction within the silicon producing collectible charge carriers in the form of electrons which are collected and used for imaging.

  13. Alpha proton x ray spectrometer

    NASA Technical Reports Server (NTRS)

    Rieder, Rudi; Waeke, H.; Economou, T.

    1994-01-01

    Mars Pathfinder will carry an alpha-proton x ray spectrometer (APX) for the determination of the elemental chemical composition of Martian rocks and soils. The instrument will measure the concentration of all major and some minor elements, including C, N, and O at levels above typically 1 percent.

  14. Ground-based verification and data processing of Yutu rover Active Particle-induced X-ray Spectrometer

    NASA Astrophysics Data System (ADS)

    Guo, Dong-Ya; Wang, Huan-Yu; Peng, Wen-Xi; Cui, Xing-Zhu; Zhang, Cheng-Mo; Liu, Ya-Qing; Liang, Xiao-Hua; Dong, Yi-Fan; Wang, Jin-Zhou; Gao, Min; Yang, Jia-Wei; Zhang, Jia-Yu; Li, Chun-Lai; Zou, Yong-Liao; Zhang, Guang-Liang; Zhang, Li-Yan; Fu, Xiao-Hui

    2015-07-01

    The Active Particle-induced X-ray Spectrometer (APXS) is one of the payloads on board the Yutu rover of the Chang'E-3 mission. In order to assess the instrumental performance of APXS, a ground verification test was performed for two unknown samples (basaltic rock, mixed powder sample). In this paper, the details of the experiment configurations and data analysis method are presented. The results show that the elemental abundance of major elements can be well determined by the APXS with relative deviations <15 wt.% (detection distance=30 mm, acquisition time=30 min). The derived detection limit of each major element is inversely proportional to acquisition time and directly proportional to detection distance, suggesting that the appropriate distance should be <50 mm. Supported by National Science and Technology Major Project (Chang'E-3 Active Particle-induced X-ray Spectrometer)

  15. Advanced x-ray imaging spectrometer

    NASA Technical Reports Server (NTRS)

    Callas, John L. (Inventor); Soli, George A. (Inventor)

    1998-01-01

    An x-ray spectrometer that also provides images of an x-ray source. Coded aperture imaging techniques are used to provide high resolution images. Imaging position-sensitive x-ray sensors with good energy resolution are utilized to provide excellent spectroscopic performance. The system produces high resolution spectral images of the x-ray source which can be viewed in any one of a number of specific energy bands.

  16. Atmospheric electron x-ray spectrometer

    NASA Technical Reports Server (NTRS)

    Feldman, Jason E. (Inventor); George, Thomas (Inventor); Wilcox, Jaroslava Z. (Inventor)

    2002-01-01

    The present invention comprises an apparatus for performing in-situ elemental analyses of surfaces. The invention comprises an atmospheric electron x-ray spectrometer with an electron column which generates, accelerates, and focuses electrons in a column which is isolated from ambient pressure by a:thin, electron transparent membrane. After passing through the membrane, the electrons impinge on the sample in atmosphere to generate characteristic x-rays. An x-ray detector, shaping amplifier, and multi-channel analyzer are used for x-ray detection and signal analysis. By comparing the resultant data to known x-ray spectral signatures, the elemental composition of the surface can be determined.

  17. The Diffuse X-ray Spectrometer Experiment

    NASA Technical Reports Server (NTRS)

    Sanders, W. T.; Edgar, R. J.; Juda, M.; Kraushaar, W. L.; Mccammon, D.; Snowden, S. L.; Zhang, J.; Skinner, M. A.

    1992-01-01

    The Diffuse X-ray Spectrometer Experiment, or 'DXS', is designed to measure the spectrum of the low-energy diffuse X-ray background with about 10 eV energy resolution and 15-deg spatial resolution. During a 5-day Space Shuttle mission, DXS is to measure the spectrum of ten 15 x 15 deg regions lying along a single 150-deg-long great circle arc on the sky. DXS carries two large-area X-ray Bragg spectrometers for the 44-84 A wavelength range; these permit measurement of the wavelength spectrum of the cosmic low-energy diffuse X-ray background with good spectral resolution.

  18. A global Mars dust composition refined by the Alpha-Particle X-ray Spectrometer in Gale Crater

    NASA Astrophysics Data System (ADS)

    Berger, Jeff A.; Schmidt, Mariek E.; Gellert, Ralf; Campbell, John L.; King, Penelope L.; Flemming, Roberta L.; Ming, Douglas W.; Clark, Benton C.; Pradler, Irina; VanBommel, Scott J. V.; Minitti, Michelle E.; Fairén, Alberto G.; Boyd, Nicholas I.; Thompson, Lucy M.; Perrett, Glynis M.; Elliott, Beverley E.; Desouza, Elstan

    2016-01-01

    Modern Martian dust is similar in composition to the global soil unit and bulk basaltic Mars crust, but it is enriched in S and Cl. The Alpha Particle X-ray Spectrometer (APXS) on the Mars Science Laboratory Curiosity rover analyzed air fall dust on the science observation tray (o-tray) in Gale Crater to determine dust oxide compositions. The o-tray dust has the highest concentrations of SO3 and Cl measured in Mars dust (SO3 8.3%; Cl 1.1 wt %). The molar S/Cl in the dust (3.35 ± 0.34) is consistent with previous studies of Martian dust and soils (S/Cl = 3.7 ± 0.7). Fe is also elevated ~25% over average Mars soils and the bulk crust. These enrichments link air fall dust with the S-, Cl-, and Fe-rich X-ray amorphous component of Gale Crater soil. Dust and soil have the same S/Cl, constraining the surface concentrations of S and Cl on a global scale.

  19. Laboratory verification of the Active Particle-induced X-ray Spectrometer (APXS) on the Chang'e-3 mission

    NASA Astrophysics Data System (ADS)

    Zhang, Guang-Liang; Li, Chun-Lai; Fu, Xiao-Hui; Zhang, Li-Yan; Ban, Cao; Li, Han; Zou, Yong-Liao; Peng, Wen-Xi; Cui, Xing-Zhu; Zhang, Cheng-Mo; Wang, Huan-Yu

    2015-11-01

    In the Chang'e-3 mission, the Active Particle-induced X-ray Spectrometer (APXS) on the Yutu rover is used to analyze the chemical composition of lunar soil and rock samples. APXS data are only valid are only if the sensor head gets close to the target and integration time lasts long enough. Therefore, working distance and integration time are the dominant factors that affect APXS results. This study confirms the ability of APXS to detect elements and investigates the effects of distance and time on the measurements. We make use of a backup APXS instrument to determine the chemical composition of both powder and bulk samples under the conditions of different working distances and integration times. The results indicate that APXS can detect seven major elements, including Mg, Al, Si, K, Ca, Ti and Fe under the condition that the working distance is less than 30 mm and having an integration time of 30 min. The statistical deviation is smaller than 15%. This demonstrates the instrument's ability to detect major elements in the sample. Our measurements also indicate the increase of integration time could reduce the measurement error of peak area, which is useful for detecting the elements Mg, Al and Si. However, an increase in working distance can result in larger errors in measurement, which significantly affects the detection of the element Mg.

  20. CHANG'E-3 Active Particle-induced X-ray Spectrometer: first detection near the landing site and preliminary analysis result

    NASA Astrophysics Data System (ADS)

    Peng, Wenxi; Cui, XingZhu; Wang, Huanyu; Guo, Dongya

    Active Particle-induced X-ray Spectrometer (APXS) onboard CHANG'E-3 Yutu rover was the first high energy resolution instrument of X-ray spectrometry sent to the lunar surface. The scientific objective of APXS is to investigate the elemental compositions along the route of the lunar rover on the Moon.Here, the first lunar soil detection near the landing site made by APXS is presented. The initial analysis indicate that the lunar regolith in this area is rich in both TiO2 and FeO, which is consistent with the remote sensing results.

  1. X-Ray Background Survey Spectrometer (XBSS)

    NASA Technical Reports Server (NTRS)

    Sanders, W. T. (Principal Investigator); Paulos, R. J.

    1996-01-01

    The objective of this investigation was to perform a spectral survey of the low energy diffuse X-ray background using the X-ray Background Survey Spectrometer (XBSS) on board the Space Station Freedom (SSF). XBSS obtains spectra of the X-ray diffuse background in the 11-24 A and 44-84 A wavelength intervals over the entire sky with 15 deg spatial resolution. These X-rays are almost certainly from a very hot (10(exp 6) K) component of the interstellar medium that is contained in regions occupying a large fraction of the interstellar volume near the Sun. Astrophysical plasmas near 10(exp 6) K are rich in emission lines, and the relative strengths of these lines, besides providing information about the physical conditions of the emitting gas, also provide information about its history and heating mechanisms.

  2. Low Energy X-Ray Spectrometer

    NASA Astrophysics Data System (ADS)

    Woodruff, Wayne R.

    1981-10-01

    A subkilovolt spectrometer has been produced to permit high-energy-resolution, time-dependent x-ray intensity measurements. The diffracting element is a curved mica (d=9.95Å) crystal. To preclude higher order (n≳1) diffractions, a carbon x-ray mirror that reflects only photons with energies less than ˜1.1 keV is utilized ahead of the diffracting element. The nominal energy range of interest is 800 to 900 eV. The diffracted photons are detected by a gold-surfaced photoelectric diode designed to have a very good frequency response, and whose current is recorded on an oscilloscope. A thin, aluminum light barrier is placed between the diffracting crystal and the photoelectric diode detector to keep any UV generated on or scattered by the crystal from illuminating the detector. High spectral enegy resolution is provided by many photocathodes between 8- and 50-eV wide placed serially along the diffracted x-ray beam at the detector position. The spectrometer was calibrated for energy and energy dispersion using the Ni Lα1,2 lines produced in the LLNL IONAC accelerator and in third order using a molybdenum target x-ray tube. For the latter calibration the carbon mirror was replaced by one surfaced with rhodium to raise the cut-off energy to about 3 keV. The carbon mirror reflection dependence on energy was measured using one of our Henke x-ray sources. The curved mica crystal diffraction efficiency was measured on our Low-Energy X-ray (LEX) machine. The spectrometer performs well although some changes in the way the x-ray mirror is held are desirable.

  3. Low energy x-ray spectrometer

    SciTech Connect

    Woodruff, W.R.

    1981-06-05

    A subkilovolt spectrometer has been produced to permit high-energy-resolution, time-dependent x-ray intensity measurements. The diffracting element is a curved mica (d = 9.95A) crystal. To preclude higher order (n > 1) diffractions, a carbon x-ray mirror that reflects only photons with energies less than approx. 1.1 keV is utilized ahead of the diffracting element. The nominal energy range of interest is 800 to 900 eV. The diffracted photons are detected by a gold-surface photoelectric diode designed to have a very good frequency response, and whose current is recorded on an oscilloscope. A thin, aluminium light barrier is placed between the diffracting crystal and the photoelectric diode detector to keep any uv generated on or scattered by the crystal from illuminating the detector. High spectral energy resolution is provided by many photocathodes between 8- and 50-eV wide placed serially along the diffracted x-ray beam at the detector position. The spectrometer was calibrated for energy and energy dispersion using the Ni L..cap alpha../sub 1/ /sub 2/ lines produced in the LLNL IONAC accelerator and in third order using a molybdenum target x-ray tube. For the latter calibration the carbon mirror was replaced by one surfaced with rhodium to raise the cut-off energy to about 3 keV. The carbon mirror reflection dependence on energy was measured using one of our Henke x-ray sources. The curved mica crystal diffraction efficiency was measured on our Low-Energy x-ray (LEX) machine. The spectrometer performs well although some changes in the way the x-ray mirror is held are desirable. 16 figures.

  4. Major Elements Abundances in Chang'E-3 Landing Site from Active Particle-induced X-ray Spectrometer

    NASA Astrophysics Data System (ADS)

    Zhang, Xiaoping; Xie, Minggang; Zhu, Meng-Hua; Dong, Wudong; Tang, Zesheng; Xu, Aoao

    2015-04-01

    Chang'E-3, China's first Moon lander and rover mission, was launched at 17:30 on 1st December 2013 (UTC) and successfully landed on Moon surface at 13:11 on 14th December 2013 (UTC). About 8 hours later after the soft landing, the rover, named "Yutu' after a mythological rabbit that lives on the Moon as a pet of the Moon goddess, was successfully separated from the lander and started its adventure on the Moon. The success of this mission marks the first soft-landing on the Moon since 1976. The landing site is in northern Mare Imbrium (N44.12, W19.51), close to the boundary of two different geologic units and sits on 'young' Eratoshenian lava flows which spread several hundreds to thousands of kilometers. The mare basalts in the landing site are believed to be formed from the lava flows ~2.5 billion years ago, which are significantly younger than all of the returned lunar samples, dating from 3.1 to 3.8 billion years ago. This makes the landing site a very interesting place for exploring geochemical characteristics of the young lava flows and lunar evolution in a later stage. Active Particle-induced X-ray Spectrometer (APXS) is the only payload on the robotic arm of Yutu rover. It was designed to measure the intensities of characteristic fluorescent X-rays produced by interactions of lunar sample with incident X-rays. Major elements abundances of Mg, Al, Si, Ca, Ti, Fe on the lunar surface were expected to be detected after the exploration. On December 24th (UTC), 2013 and January 14th (UTC), 2014, APXS performed 4 successful measurements on lunar soils along Yutu's track. Characteristic peaks of Mg, Al, Si, K, Ca, Ti, Cr, Mn, Fe, Ni, Cu, Sr and Zr could be clearly seen from the measured spectra. A global fit based on minimum chi-square method has been performed to disentangle different components in the measured spectra. These components include Kα and/or Kβ peaks of each element, escape peaks, exponential and shelf tail of major peaks and electronic noises, etc

  5. Imaging slitless spectrometer for X-ray astronomy

    NASA Technical Reports Server (NTRS)

    Gursky, H.; Zehnpfennig, T.

    1968-01-01

    Imaging slitless spectrometer, a combination of an X ray transmission /or reflection/ grating and image-forming X ray telescope, is capable of obtaining simultaneous spatial and spectral information about celestial X ray sources.

  6. Elemental Analysis of the Surface of Comet 67p/Churyumov-Gerasimenko with the Alpha Particle X-Ray Spectrometer APXS on the Rosetta Lander Philae: Preliminary Results

    NASA Astrophysics Data System (ADS)

    Klingelhoefer, G.; Schmanke, D.; Girones-Lopez, J.; Brueckner, J.; d'Uston, C.; Economou, T.; Gellert, R.; Markovski, C.

    2014-12-01

    After a 10 years cruise the Rosetta probe has reached its final target, the comet 67P/Churyumov-Gerasimenko. The main objectives of the mission are to gain more knowledge of the composition, the origin and formation of comets and the solar system. After extensive remote exploration of the comet the lander Philae will be separated to land on the comet surface, starting immediately examining its landing site with its scientific payload. Part of this payload is the APXS (Alpha Particle X-Ray Spectrometer). It will measure in situ the chemical composition of the comet's surface and it's changes during the journey of the comet towards the sun. APXS is a combination of two spectrometers in one single instrument. It will irradiate the comet surface using Curium 244 sources, which are emitting alpha-particle and X-rays. In the alpha-mode the instrument uses alpha backscattering spectroscopy to detect lower Z elements like C, N and O and groups of elements with higher Z. In the X-ray mode alpha particle / X-ray induced X-ray spectroscopy (XRF) will allow the detection of most of the higher Z elements from Na up to Ni and above. Both modes will be always run in parallel allowing to determine lower and higher Z elements simultaneously. For 3 years the solar powered Rosetta probe had to pass a hibernation phase because of a long passage far away to the sun. After wakeup in January 2014 an extensive test phase of all instruments and subsystems has been performed, including the APXS. After landing on the comet an intense initial measurement phase of all instruments is planned, the First Science Sequence (FSS). It will be followed by a long term science phase (LTS). As long as possible APXS and the other instruments will continue to measure and monitor the changes and increasing activity of the comet during its journey towards the inner region of the solar system.The project is funded by the German Space Agency DLR under contracts 50 QP 0404 and 50 QP 0902. References: G

  7. Data processing for the Active Particle-induced X-ray Spectrometer and initial scientific results from Chang'e-3 mission

    NASA Astrophysics Data System (ADS)

    Fu, Xiao-Hui; Li, Chun-Lai; Zhang, Guang-Liang; Zou, Yong-Liao; Liu, Jian-Jun; Ren, Xin; Tan, Xu; Zhang, Xiao-Xia; Zuo, Wei; Wen, Wei-Bin; Peng, Wen-Xi; Cui, Xing-Zhu; Zhang, Cheng-Mo; Wang, Huan-Yu

    2014-12-01

    The Active Particle-induced X-ray Spectrometer (APXS) is an important payload mounted on the Yutu rover, which is part of the Chang'e-3 mission. The scientific objective of APXS is to perform in-situ analysis of the chemical composition of lunar soil and rock samples. The radioactive sources, 55Fe and 109Cd, decay and produce α-particles and X-rays. When X-rays and α-particles interact with atoms in the surface material, they knock electrons out of their orbits, which release energy by emitting X-rays that can be measured by a silicon drift detector (SDD). The elements and their concentrations can be determined by analyzing their peak energies and intensities. APXS has analyzed both the calibration target and lunar soil once during the first lunar day and again during the second lunar day. The total detection time lasted about 266 min and more than 2000 frames of data records have been acquired. APXS has three operating modes: calibration mode, distance sensing mode and detection mode. In detection mode, work distance can be calculated from the X-ray counting rate collected by SDD. Correction for the effect of temperature has been performed to convert the channel number for each spectrum to X-ray energy. Dead time correction is used to eliminate the systematic error in quantifying the activity of an X-ray pulse in a sample and derive the real count rate. We report APXS data and initial results during the first and second lunar days for the Yutu rover. In this study, we analyze the data from the calibration target and lunar soil on the first lunar day. Seven major elements, including Mg, Al, Si, K, Ca, Ti and Fe, have been identified. Comparing the peak areas and ratios of calibration basalt and lunar soil the landing site was found to be depleted in K, and have lower Mg and Al but higher Ca, Ti, and Fe. In the future, we will obtain the elemental concentrations of lunar soil at the Chang'e-3 landing site using APXS data.

  8. The Alpha Particle X-Ray Spectrometer APXS on the Rosetta lander Philae to explore the surface of comet 67P/Churyumov-Gerasimenko

    NASA Astrophysics Data System (ADS)

    Girones-Lopez, Jordi; Schmanke, Dirk; Klingelhoefer, Goestar; Maul, Jasmine; Brueckner, Johannes; Duston, Claude; Gellert, Ralf; Klingelhöfer, Göstar

    The Rosetta Mission was launched in 2004 with the main objectives to gain a better under-standing of the origin and formation of comets and the solar system. After 10 years of cruise the comet 67P/Churyumov-Gerasimenko will be reached in 2014 and the lander Philae will be deployed on the surface. As a part of the lander payload the APXS will measure in situ the chemical composition of the comet's surface and it's changes during the journey of the comet towards the sun. APXS combines an alpha mode for alpha backscattering spectroscopy and an x-ray mode for alpha particle/x-ray induced x-ray spectroscopy (XRF) in one single instrument, being low in mass and power consumption. The comet surface will be irradiated by a Curium 244 source exciting characteristic x-rays of the elements present in the surface material. The alpha mode will allow detection of elements like C and O and groups of elements with higher Z. The x-ray-SD-detector will allow the detection of most of the elements from Na up to Ni and above. During the long duration travel to the comet checkouts and software updates of the Rosetta probe and its payload are performed at regular intervals. These are used to opti-mise and improve the quality of the x-ray and alpha-spectra of the APXS. Soon the Rosetta probe will go into a 3 year long hibernation mode. It will awake when approaching it's target, providing us with new exiting data that will shed light on state, evolution and origin of comets and the solar system. Acknowledgements: This project is funded by the German Space Agency DLR under contracts 50 QP 0404 and 50 QP 0902. References: G. Klingelhüfer, J. Brückner, C. d'Uston, R. Gellert, and R. Rieder, The Rosetta Alpha Particle X-ray Spectrometer (APXS), Space Science Reviews, Vol.128 (2007) 383-396; doi:10.1007/s11214-006-9137-3

  9. Monolithic CMOS imaging x-ray spectrometers

    NASA Astrophysics Data System (ADS)

    Kenter, Almus; Kraft, Ralph; Gauron, Thomas; Murray, Stephen S.

    2014-07-01

    The Smithsonian Astrophysical Observatory (SAO) in collaboration with SRI/Sarnoff is developing monolithic CMOS detectors optimized for x-ray astronomy. The goal of this multi-year program is to produce CMOS x-ray imaging spectrometers that are Fano noise limited over the 0.1-10keV energy band while incorporating the many benefits of CMOS technology. These benefits include: low power consumption, radiation "hardness", high levels of integration, and very high read rates. Small format test devices from a previous wafer fabrication run (2011-2012) have recently been back-thinned and tested for response below 1keV. These devices perform as expected in regards to dark current, read noise, spectral response and Quantum Efficiency (QE). We demonstrate that running these devices at rates ~> 1Mpix/second eliminates the need for cooling as shot noise from any dark current is greatly mitigated. The test devices were fabricated on 15μm, high resistivity custom (~30kΩ-cm) epitaxial silicon and have a 16 by 192 pixel format. They incorporate 16μm pitch, 6 Transistor Pinned Photo Diode (6TPPD) pixels which have ~40μV/electron sensitivity and a highly parallel analog CDS signal chain. Newer, improved, lower noise detectors have just been fabricated (October 2013). These new detectors are fabricated on 9μm epitaxial silicon and have a 1k by 1k format. They incorporate similar 16μm pitch, 6TPPD pixels but have ~ 50% higher sensitivity and much (3×) lower read noise. These new detectors have undergone preliminary testing for functionality in Front Illuminated (FI) form and are presently being prepared for back thinning and packaging. Monolithic CMOS devices such as these, would be ideal candidate detectors for the focal planes of Solar, planetary and other space-borne x-ray astronomy missions. The high through-put, low noise and excellent low energy response, provide high dynamic range and good time resolution; bright, time varying x-ray features could be temporally and

  10. Refinement of the Compton-Rayleigh scatter ratio method for use on the Mars Science Laboratory alpha particle X-ray spectrometer: II - Extraction of invisible element content

    NASA Astrophysics Data System (ADS)

    Perrett, Glynis M.; Campbell, John L.; Gellert, Ralf; King, Penelope L.; Nield, Emily; O'Meara, Joanne M.; Pradler, Irina

    2016-02-01

    The intensity ratio C/R between Compton and Rayleigh scatter peaks of the exciting Pu L X-rays in the alpha particle X-ray spectrometer (APXS) is strongly affected by the presence of very light elements such as oxygen which cannot be detected directly by the APXS. C/R values are determined along with element concentrations by fitting APXS spectra of geochemical reference materials (GRMs) with the GUAPX code. A quantity K is defined as the ratio between the C/R value determined by Monte Carlo simulation based on the measured element concentrations and the fitted C/R value from the spectrum. To ensure optimally accurate K values, the choice of appropriate GRMs is explored in detail, with attention paid to Rb and Sr, whose characteristic Kα X-ray peaks overlap the Pu Lα scatter peaks. The resulting relationship between the ratio K and the overall oxygen fraction is linear. This provides a calibration from which the concentration of additional light invisible constituents (ALICs) such as water may be estimated in unknown rock and conglomerate samples. Several GRMs are used as 'unknowns' in order to evaluate the accuracy of ALIC concentrations derived in this manner.

  11. Two Years of Chemical Sampling on Meridiani Planum by the Alpha Particle X-Ray Spectrometer Onboard the Mars Exploration Rover Opportunity

    NASA Technical Reports Server (NTRS)

    Bruckner, J.; Gellert, R.; Clark, B.C.; Dreibus, G.; Rieder, R.; Wanke, H.; d'Uston, C.; Economou, T.; Klingelhofer, G.; Lugmair, G.; Ming, D.W.; Squyres, S.W.; Yen, A.; Zipfel, J.

    2006-01-01

    For over two terrestrial years, the Mars Exploration Rover Opportunity has been exploring the martian surface at Meridiani Planum using the Athena instrument payload [1], including the Alpha Particle X-Ray Spectrometer (APXS). The APXS has a small sensor head that is mounted on the robotic arm of the rover. The chemistry, mineralogy and morphology of selected samples were investigated by the APXS along with the Moessbauer Spectrometer (MB) and the Microscopic Imager (MI). The Rock Abrasion Tool (RAT) provided the possibility to dust and/or abrade rock surfaces down to several millimeters to expose fresh material for analysis. We report here on APXS data gathered along the nearly 6-kilometers long traverse in craters and plains of Meridiani.

  12. Elementary Analysis of a Cometary Surface - the Alpha Particle X-Ray Spectrometer APXS on the Rosetta Mission to Comet 67P/CHURYUMOV-GERASIMENKO

    NASA Astrophysics Data System (ADS)

    Schmanke, Dirk; Economou, Thanasis; Brueckner, Johannes; Gellert, Ralf; Rodionov, Daniel; Klingelhoefer, Goestar; Girones Lopez, Jordi; Uston, Lionel D.

    After a 10 years cruise the Rosetta probe will reach its final target in the middle of this year, the comet 67P/Churyumov-Gerasimenko. The main objectives of the mission are to gain more knowledge of the composition, the origin and formation of comets and the solar system. After extensive remote examination of the comet the lander Philae will be separated to land on the comet surface. It will start immediately examining the landing site with its scientific payload. A part of this payload is the APXS (Alpha Particle X-Ray Spectrometer), it will measure in situ the chemical composition of the comet's surface and its changes during the journey of the comet towards the sun. APXS is a combination of two spectrometers in one single instrument, being low in mass and power consumption. It will irradiate the cometary surface with Curium 244 sources, which are emitting alpha-particle and X-rays. In the alpha-mode the instrument uses alpha backscattering spectroscopy to detect lower Z elements like C, N and O and groups of elements with higher Z. In the X-ray mode alpha particle/X-ray induced X-ray spectroscopy (XRF) will allow the detection of most of the higher Z elements from Na up to Ni and above. Both modes will be always run in parallel allowing to determine lower and higher Z elements simultaneously. During the long duration travel to the comet checkouts and software updates of the Rosetta probe and its payload were performed at regular intervals. In recent 3 years the solar powered Rosetta probe had to pass a hibernation phase because of a long passage far away from the sun. After the successful wakeup in January 2014 an extensive test phase of all instruments and subsystems has to be performed, including the APXS. After the landing on the comet an intense long measurement phase of all instruments is planned, the First Science Sequence (FSS). It will be followed by a long term science phase (LTS), determined by periodical changes between measurements and forced breaks

  13. Non-linearity issues and multiple ionization satellites in the PIXE portion of spectra from the Mars alpha particle X-ray spectrometer

    NASA Astrophysics Data System (ADS)

    Campbell, John L.; Heirwegh, Christopher M.; Ganly, Brianna

    2016-09-01

    Spectra from the laboratory and flight versions of the Curiosity rover's alpha particle X-ray spectrometer were fitted with an in-house version of GUPIX, revealing departures from linear behavior of the energy-channel relationships in the low X-ray energy region where alpha particle PIXE is the dominant excitation mechanism. The apparent energy shifts for the lightest elements present were attributed in part to multiple ionization satellites and in part to issues within the detector and/or the pulse processing chain. No specific issue was identified, but the second of these options was considered to be the more probable. Approximate corrections were derived and then applied within the GUAPX code which is designed specifically for quantitative evaluation of APXS spectra. The quality of fit was significantly improved. The peak areas of the light elements Na, Mg, Al and Si were changed by only a few percent in most spectra. The changes for elements with higher atomic number were generally smaller, with a few exceptions. Overall, the percentage peak area changes are much smaller than the overall uncertainties in derived concentrations, which are largely attributable to the effects of rock heterogeneity. The magnitude of the satellite contributions suggests the need to incorporate these routinely in accelerator-based PIXE using helium beams.

  14. The Alpha Particle X-Ray Spectrometer APXS on the Rosetta lander Philae to explore the surface of comet 67P/Churyumov-Gerasimenko

    NASA Astrophysics Data System (ADS)

    Klingelhoefer, Goestar; Girones Lopez, Jordi; Schmanke, Dirk; Markovski, Cristina; Brückner, Johannes; d'Uston, Claude; Economu, Tom; Gellert, Ralf

    2015-04-01

    The Rosetta Mission was launched in 2004 with the main objectives to gain a better understanding of the origin and formation of comets and the solar system. After 10 years of cruise Rosetta rendevouded with the comet 67P/Churyumov-Gerasimenko in 2014 to study the nucleus of the comet and its environment. Rosetta consists of an orbiter and a lander (Philae) with 11 and 9 scientific experiments respectively. It did what has never been attempted before, orbiting and landing on a comet. After orbit insertion in August 2014, the main spacecraft will follow the comet for several months to investigate its surface. Subsequently, Philae has been deployed for a safe landing. As part of the lander payload the APXS will measure in situ the chemical composition of the comet's surface and it's changes during the journey of the comet around the sun. The data obtained with the APXS will be used to characterize the surface of the comet, to determine the chemical composition of the dust component, and to compare the dust with known meteorite types. APXS combines an alpha mode for alpha backscattering spectroscopy and an x-ray mode for alpha particle/x-ray induced x-ray spectroscopy (XRF) in one single instrument, being low in mass (640g) and power consumption (1.5 W in operating mode) [4]. The comet surface will be irradiated by a Curium 244 source exciting characteristic x-rays of the elements present in the surface material. The alpha mode will allow detection of elements like C and O and groups of elements with a higher Z. The x-ray-SD-detector will allow the detection of most of the elements from Na up to Ni and above. The design of the Rosetta APX spectrometer is based on the experience gained with the APXS built for Russian and American Mars missions: Mars 96 spacecraft and Mars Pathfinder, MPF [1]. Two APXS were also built for the Mars Exploration Rovers mission of the NASA, MER [2-3]. Acknowledgements This project is funded by the German Space Agency DLR under contracts 50

  15. Development of mercuric iodide uncooled x ray detectors and spectrometers

    NASA Technical Reports Server (NTRS)

    Iwanczyk, Jan S.

    1990-01-01

    The results obtained in the development of miniature, lowpower, light weight mercuric iodide, HgI2, x ray spectrometers for future space missions are summarized. It was demonstrated that HgI2 detectors can be employed in a high resolution x ray spectrometer, operating in a scanning electron microscope. Also, the development of HgI2 x ray detectors to augment alpha backscattering spectrometers is discussed. These combination instruments allow for the identification of all chemical elements, with the possible exception of hydrogen, and their respective concentrations. Additionally, further investigations of questions regarding radiation damage effects in the HgI2 x ray detectors are reported.

  16. X-ray spectrophotometer SphinX and particle spectrometer STEP-F of the satellite experiment CORONAS-PHOTON. Preliminary results of the joint data analysis

    NASA Astrophysics Data System (ADS)

    Dudnik, O. V.; Podgorski, P.; Sylwester, J.; Gburek, S.; Kowalinski, M.; Siarkowski, M.; Plocieniak, S.; Bakala, J.

    2012-04-01

    A joint analysis is carried out of data obtained with the help of the solar X-ray SphinX spectrophotometer and the electron and proton satellite telescope STEP-F in May 2009 in the course of the scientific space experiment CORONAS-PHOTON. In order to determine the energies and particle types, in the analysis of spectrophotometer records data are used on the intensities of electrons, protons, and secondary γ-radiation, obtained by the STEP-F telescope, which was located in close proximity to the SphinX spectrophotometer. The identical reaction of both instruments is noted at the intersection of regions of the Brazilian magnetic anomaly and the Earth's radiation belts. It is shown that large area photodiodes, serving as sensors of the X-ray spectrometer, reliably record electron fluxes of low and intermediate energies, as well as fluxes of the secondary gamma radiation from construction materials of detector modules, the TESIS instrument complex, and the spacecraft itself. The dynamics of electron fluxes, recorded by the SphinX spectrophotometer in the vicinity of a weak geomagnetic storm, supplements the information about the processes of radial diffusion of electrons, which was studied using the STEP-F telescope.

  17. The x-ray microcalorimeter spectrometer onboard of IXO

    NASA Astrophysics Data System (ADS)

    den Herder, J. W.; Kelley, R. L.; Mitsuda, K.; Piro, L.; Bandler, S. R.; Bastia, P.; Boyce, K. R.; Bruin, M.; Chervenak, J. A.; Colasanti, L.; Doriese, W. B.; Dipirro, M.; Eckart, M. E.; Ezoe, Y.; Figueroa-Feliciano, E.; Ferrari, L.; Fujimoto, R.; Gatti, F.; Gendreau, K. C.; Gottardi, L.; den Hartog, R.; Hilton, G. C.; Hoevers, H.; Irwin, K. D.; Ishisaki, Y.; Kashani, A.; Kilbourne, C. A.; de Korte, P.; van der Kuur, J.; Macculi, C.; Mineo, T.; Nieland, J. H.; Ohashi, T.; Paltani, S.; Perinati, E.; Porter, F. S.; Shirron, P. J.; Smith, S. J.; Takei, Y.; Tashiro, M.; Torrioli, G.; Tsujimoto, M.; van Weers, H.; Yamasaki, N. Y.

    2010-07-01

    One of the instruments on the International X-ray Observatory (IXO), under study with NASA, ESA and JAXA, is the X-ray Microcalorimeter Spectrometer (XMS). This instrument, which will provide high spectral resolution images, is based on X-ray micro-calorimeters with Transition Edge Sensor thermometers. The pixels have metallic X-ray absorbers and are read-out by multiplexed SQUID electronics. The requirements for this instrument are demanding. In the central array (40 x 40 pixels) an energy resolution of < 2.5 eV is required, whereas the energy resolution of the outer array is more relaxed (~ 10 eV) but the detection elements have to be a factor 16 larger in order to keep the number of read-out channels acceptable for a cryogenic instrument. Due to the large collection area of the IXO optics, the XMS instrument must be capable of processing high counting rates, while maintaining the spectral resolution and a low deadtime. In addition, an anti-coincidence detector is required to suppress the particle-induced background. In this paper we will summarize the instrument status and performance. We will describe the results of design studies for the focal plane assembly and the cooling systems. Also the system and its required spacecraft resources will be given.

  18. [The X-Ray Fluorescence Spectrometer Based on Pyroelectric Effect].

    PubMed

    Dong, Yi-fan; Fan, Rui-rui; Guo, Dong-ya; Zhang, Chun-lei; Gao, Min; Wang, Jin-zhou; Liu, Ya-qing; Zhou, Da-wei; Wang, Huan-yu

    2016-02-01

    Pyroelectric X-ray generator is implemented, and an X-ray fluorescence spectrometer is accomplished by combining the pyroelectric X-ray generator with a high energy resolution silicon drift detector. Firstly, the parameters of the X-ray generator are decided by analyzing and calculating the influence of the thickness of the pyroelectriccrystal and the thickness of the target on emitted X-ray. Secondly, the emitted X-ray is measured. The energy of emitted X-ray is from 1 to 27 keV, containing the characteristic X-ray of Cu and Ta, and the max counting rate is more than 3 000 per second. The measurement also proves that the detector of the spectrometer has a high energy resolution which the FWMH is 210 eV at 8. 05 keV. Lastly, samples of Fe, Ti, Cr and high-Ti basalt are analyzed using the spectrometer, and the results are agreed with the elements of the samples. It shows that the spectrometer consisting of a pyroelectric X-ray generator and a silicon drift detector is effective for element analysis. Additionally, because each part of the spectrometer has a small volume, it can be easily modified to a portable one which is suitable for non-destructive, on-site and quick element analysis. PMID:27209767

  19. Low intensity X-ray and gamma-ray spectrometer

    NASA Technical Reports Server (NTRS)

    Yin, L. I. (Inventor)

    1982-01-01

    A low intensity X-ray and gamma ray spectrometer for imaging, counting, and energy resolving of single invisible radiation particles is described. The spectrometer includes a converting device for converting single invisible radiation particles to visible light photons. Another converting device converts the visible light photons to photoelectrons. A fiber optics coupling device couples together the two converting devices. An intensifying device intensifies the photoelectrons by an average gain factor of between 10 to the 4th power and 10 to the 7th power. The tensifying device is an anti-ion feedback microchannel plate amplifier which is operated substantially below saturation. A displaying device displays the intensified photoelectrons. The displaying device 32 indicates the spatial position, number, and energy of the incoming single invisible radiation particles.

  20. The ITER core imaging x-ray spectrometer: x-ray calorimeter performance.

    PubMed

    Beiersdorfer, P; Brown, G V; Clementson, J; Dunn, J; Morris, K; Wang, E; Kelley, R L; Kilbourne, C A; Porter, F S; Bitter, M; Feder, R; Hill, K W; Johnson, D; Barnsley, R

    2010-10-01

    We describe the anticipated performance of an x-ray microcalorimeter instrument on ITER. As part of the core imaging x-ray spectrometer, the instrument will augment the imaging crystal spectrometers by providing a survey of the concentration of heavy ion plasma impurities in the core and possibly ion temperature values from the emission lines of different elemental ions located at various radial positions. PMID:21034021

  1. Atmospheric electron-induced x-ray spectrometer development

    NASA Technical Reports Server (NTRS)

    Wilcox, Jaroslava Z.; Urgiles, Eduardo; Toda, Risaku; Crisp, Joy

    2005-01-01

    This paper extends the work reported at the IEEE Aerospace conference in 2001 and 2003 where the concept and progress in the development of the so called atmospheric Electron X-ray Spectrometer (AEXS) has been described.

  2. Thermal detectors as X-ray spectrometers

    NASA Technical Reports Server (NTRS)

    Moseley, S. H.; Mather, J. C.; Mccammon, D.

    1984-01-01

    Sensitive thermal detectors should be useful for measuring very small energy pulses, such as those produced by the absorption of X-ray photons. The measurement uncertainty can be very small, making the technique promising for high resolution nondispersive X-ray spectroscopy. The limits to the energy resolution of such thermal detectors are derived and used to find the resolution to be expected for a detector suitable for X-ray spectroscopy in the 100 eV to 10,000 eV range. If there is no noise in the thermalization of the X-ray, resolution better than 1 eV full width at half maximum is possible for detectors operating at 0.1 K. Energy loss in the conversion of the photon energy to heat is a potential problem. The loss mechanisms may include emission of photons or electrons, or the trapping of energy in long lived metastable states. Fluctuations in the phonon spectrum could also limit the resolution if phonon relaxation times are very long. Conceptual solutions are given for each of these possible problems.

  3. High intensity line source for x-ray spectrometer calibration

    SciTech Connect

    Thoe, R.S.

    1986-06-01

    A high intensity electron-impact x-ray source using a one-dimensional Pierce lens has been built for the purpose of calibrating a bent crystal x-ray spectrometer. This source focuses up to 100 mA of 20-keV electrons to a line on a liquid-cooled anode. The line (which can serve as a virtual slit for the spectrometer) measures approximately 800 ..mu.. x 2 cm. The source is portable and therefore adaptable to numerous types of spectrometer applications. One particular application, the calibration of a high resolution (r = 10/sup 4/) time-resolved cyrstal spectrometer, will be discussed in detail.

  4. Geochemical properties of rocks and soils in Gusev Crater, Mars: Results of the Alpha Particle X-Ray Spectrometer from Cumberland Ridge to Home Plate

    NASA Astrophysics Data System (ADS)

    Ming, D. W.; Gellert, R.; Morris, R. V.; Arvidson, R. E.; Brückner, J.; Clark, B. C.; Cohen, B. A.; d'Uston, C.; Economou, T.; Fleischer, I.; Klingelhöfer, G.; McCoy, T. J.; Mittlefehldt, D. W.; Schmidt, M. E.; Schröder, C.; Squyres, S. W.; Tréguier, E.; Yen, A. S.; Zipfel, J.

    2008-12-01

    Geochemical diversity of rocks and soils has been discovered by the Alpha Particle X-Ray Spectrometer (APXS) during Spirit's journey over Husband Hill and down into the Inner Basin from sol 470 to 1368. The APXS continues to operate nominally with no changes in calibration or spectral degradation over the course of the mission. Germanium has been added to the Spirit APXS data set with the confirmation that it occurs at elevated levels in many rocks and soils around Home Plate. Twelve new rock classes and two new soil classes have been identified at the Spirit landing site since sol 470 on the basis of the diversity in APXS geochemistry. The new rock classes are Irvine (alkaline basalt), Independence (low Fe outcrop), Descartes (outcrop similar to Independence with higher Fe and Mn), Algonquin (mafic-ultramafic igneous sequence), Barnhill (volcaniclastic sediments enriched in Zn, Cl, and Ge), Fuzzy Smith (high Si and Ti rock), Elizabeth Mahon (high Si, Ni, and Zn outcrop and rock), Halley (hematite-rich outcrop and rock), Montalva (high K, hematite-rich rock), Everett (high Mg, magnetite-rich rock), Good Question (high Si, low Mn rock), and Torquas (high K, Zn, and Ni magnetite-rich rock). New soil classes are Gertrude Weise (very high Si soil) and Eileen Dean (high Mg, magnetite-rich soil). Aqueous processes have played a major role in the formation and alteration of rocks and soils on Husband Hill and in the Inner Basin.

  5. X-ray imaging crystal spectrometer for extended X-ray sources

    DOEpatents

    Bitter, Manfred L.; Fraenkel, Ben; Gorman, James L.; Hill, Kenneth W.; Roquemore, A. Lane; Stodiek, Wolfgang; von Goeler, Schweickhard E.

    2001-01-01

    Spherically or toroidally curved, double focusing crystals are used in a spectrometer for X-ray diagnostics of an extended X-ray source such as a hot plasma produced in a tokomak fusion experiment to provide spatially and temporally resolved data on plasma parameters using the imaging properties for Bragg angles near 45. For a Bragg angle of 45.degree., the spherical crystal focuses a bundle of near parallel X-rays (the cross section of which is determined by the cross section of the crystal) from the plasma to a point on a detector, with parallel rays inclined to the main plain of diffraction focused to different points on the detector. Thus, it is possible to radially image the plasma X-ray emission in different wavelengths simultaneously with a single crystal.

  6. X-Ray Imaging Crystal Spectrometer for Extended X-Ray Sources

    SciTech Connect

    Bitter, Manfred L.; Fraekel, Benjamin; Gorman, James L.; Hill, Kenneth W.; Roquemore, Lane A.; Stodiek, Wolfgang; Goeler, Schweickhard von

    1999-05-01

    Spherically or toroidally curved, double focusing crystals are used in a spectrometer for X-ray diagnostics of an extended X-ray source such as a hot plasma produced in a tokamak fusion experiment to provide spatially and temporally resolved data on plasma parameters such as ion temperature, toroidal and poloidal rotation, electron temperature, impurity ion charge-state distributions, and impurity transport. The imaging properties of these spherically or toroidally curved crystals provide both spectrally and spatially resolved X-ray data from the plasma using only one small spherically or toroidally curved crystal, thus eliminating the requirement for a large array of crystal spectrometers and the need to cross-calibrate the various crystals.

  7. Hard x-ray spectrometers for NIF (abstract)

    NASA Astrophysics Data System (ADS)

    Seely, John; Holland, Glenn; Brown, Charles; Deslattes, Richard; Hudson, Lawrence; Bell, Perry; Miller, Michael; Back, Christina

    2001-01-01

    A National Ignition Facility (NIF) core diagnostic instrument has been designed and will be fabricated to record x-ray spectra in the 1.2-20 keV energy range. The high-energy electronic x-ray instrument has four reflection crystals with overlapping coverage of 1.2-10.9 keV and one transmission crystal covering 8.6-20 keV. The spectral resolving power varies from approximately 1000 at low energies to 315 at 20 keV. The spectrum produced by each crystal is recorded by a modified commercial dental x-ray charge coupled device (CCD) detector. The scintillators on the CCD detectors are optimized for the energy ranges. A one-channel x-ray spectrometer, using one transmission crystal covering 12-60 keV, will be fabricated for the OMEGA laser facility. The transmission crystal spectrometers are based on instruments originally designed at National Institute for Standards and Technology for the purpose of characterizing the x-ray flux from medical radiography sources. Utilizing one of those instruments and a commercial dental x-ray CCD detector, x-ray images were recorded using a single pulse from a laboratory x-ray source with a peak charging voltage of 200 kV. A resolving power of 300 was demonstrated by recording on film the Kα1 and Kα2 characteristic x-ray lines near 17 keV from a molybdenum anode. The continuum radiation from a tungsten anode was recorded in the 20-50 keV energy range. The transmission crystal spectrometer has sufficient spectral resolution and sensitivity to record the line and continuum radiation from high-Z targets irradiated by the NIF laser and the OMEGA laser.

  8. A short working distance multiple crystal x-ray spectrometer

    USGS Publications Warehouse

    Dickinson, B.; Seidler, G.T.; Webb, Z.W.; Bradley, J.A.; Nagle, K.P.; Heald, S.M.; Gordon, R.A.; Chou, I.-Ming

    2008-01-01

    For x-ray spot sizes of a few tens of microns or smaller, a millimeter-sized flat analyzer crystal placed ???1 cm from the sample will exhibit high energy resolution while subtending a collection solid angle comparable to that of a typical spherically bent crystal analyzer (SBCA) at much larger working distances. Based on this observation and a nonfocusing geometry for the analyzer optic, we have constructed and tested a short working distance (SWD) multicrystal x-ray spectrometer. This prototype instrument has a maximum effective collection solid angle of 0.14 sr, comparable to that of 17 SBCA at 1 m working distance. We find good agreement with prior work for measurements of the Mn K?? x-ray emission and resonant inelastic x-ray scattering for MnO, and also for measurements of the x-ray absorption near-edge structure for Dy metal using L??2 partial-fluorescence yield detection. We discuss future applications at third- and fourth-generation light sources. For concentrated samples, the extremely large collection angle of SWD spectrometers will permit collection of high-resolution x-ray emission spectra with a single pulse of the Linac Coherent Light Source. The range of applications of SWD spectrometers and traditional multi-SBCA instruments has some overlap, but also is significantly complementary. ?? 2008 American Institute of Physics.

  9. The x-ray microcalorimeter spectrometer onboard Athena

    NASA Astrophysics Data System (ADS)

    den Herder, J. W.; Bagnali, D.; Bandler, S.; Barbera, M.; Barcons, X.; Barret, D.; Bastia, P.; Bisotti, M.; Boyce, K.; Cara, C.; Ceballos, M.; Corcione, L.; Cobo, B.; Colasanti, L.; de Plaa, J.; DiPirro, M.; Doriese, W. B.; Ezoe, Y.; Fujimoto, R.; Gatti, F.; Gottardi, L.; Guttridge, P.; den Hartog, R.; Hepburn, I.; Kelley, R.; Irwin, K.; Ishisaki, Y.; Kilbourne, C.; de Korte, P. A. J.; van der Kuur, J.; Lotti, S.; Macculi, C.; Mitsuda, K.; Mineo, T.; Natalucci, L.; Ohashi, T.; Page, M.; Paltani, S.; Perinati, E.; Piro, L.; Pigot, C.; Porter, F. S.; Rauw, G.; Ravera, L.; Renotte, E.; Sauvageot, J.-L.; Schmid, C.; Sciortino, S.; Shirron, P.; Takei, Y.; Torrioli, G.; Tsujimoto, M.; Valenziano, L.; Willingale, D.; de Vries, C.; van Weers, H.; Wilms, J.; Yamasaki, N. Y.

    2012-09-01

    One of the instruments on the Advanced Telescope for High-Energy Astrophysics (Athena) which was one of the three missions under study as one of the L-class missions of ESA, is the X-ray Microcalorimeter Spectrometer (XMS). This instrument, which will provide high-spectral resolution images, is based on X-ray micro-calorimeters with Transition Edge Sensor (TES) and absorbers that consist of metal and semi-metal layers and a multiplexed SQUID readout. The array (32 x 32 pixels) provides an energy resolution of < 3 eV. Due to the large collection area of the Athena optics, the XMS instrument must be capable of processing high counting rates, while maintaining the spectral resolution and a low deadtime. In addition, an anti-coincidence detector is required to suppress the particle-induced background. Compared to the requirements for the same instrument on IXO, the performance requirements have been relaxed to fit into the much more restricted boundary conditions of Athena. In this paper we illustrate some of the science achievable with the instrument. We describe the results of design studies for the focal plane assembly and the cooling systems. Also, the system and its required spacecraft resources will be given.

  10. Measuring Flash X-Ray Spectra with a Compton Spectrometer

    NASA Astrophysics Data System (ADS)

    Gehring, Amanda; Espy, Michelle; Haines, Todd; Hunter, James; King, Nick; Merrill, Frank; Sedillo, Robert; Urbaitis, Algis; Volegov, Petr

    2014-09-01

    The determination of the x-ray energy spectra of flash radiographic sources is difficult due to the short nature of the pulses (~50 ns). Recently, a Compton spectrometer has been refurbished and investigated as a potential device for conducting these measurements. The spectrometer was originally designed and characterized by Morgan et al.. The spectrometer consists of a 300 kg neodymium-iron magnet and measures spectra in the <1 MeV to 20 MeV energy range. In this apparatus, the incoming x-rays are collimated into a narrow beam before encountering a converter foil. Compton electrons are ejected and collimated so that the forward-directed electrons enter the magnetic field region of the device. The position of the electrons on the magnet focal plane is a function of their energy, allowing the x-ray spectrum to be reconstructed. Recent energy calibration measurements and the spectrum reconstruction of a Bremsstrahlung source will be presented. The determination of the x-ray energy spectra of flash radiographic sources is difficult due to the short nature of the pulses (~50 ns). Recently, a Compton spectrometer has been refurbished and investigated as a potential device for conducting these measurements. The spectrometer was originally designed and characterized by Morgan et al.. The spectrometer consists of a 300 kg neodymium-iron magnet and measures spectra in the <1 MeV to 20 MeV energy range. In this apparatus, the incoming x-rays are collimated into a narrow beam before encountering a converter foil. Compton electrons are ejected and collimated so that the forward-directed electrons enter the magnetic field region of the device. The position of the electrons on the magnet focal plane is a function of their energy, allowing the x-ray spectrum to be reconstructed. Recent energy calibration measurements and the spectrum reconstruction of a Bremsstrahlung source will be presented. LA-UR-14-23602.

  11. The NIF x-ray spectrometer calibration campaign at Omega

    SciTech Connect

    Pérez, F.; Kemp, G. E.; Barrios, M. A.; Pino, J.; Scott, H.; Ayers, S.; Chen, H.; Emig, J.; Colvin, J. D.; Fournier, K. B.; Regan, S. P.; Bedzyk, M.; Shoup, M. J.; Agliata, A.; Yaakobi, B.; Marshall, F. J.; Hamilton, R. A.; Jaquez, J.; Farrell, M.; Nikroo, A.

    2014-11-15

    The calibration campaign of the National Ignition Facility X-ray Spectrometer (NXS) was carried out at the OMEGA laser facility. Spherically symmetric, laser-driven, millimeter-scale x-ray sources of K-shell and L-shell emission from various mid-Z elements were designed for the 2–18 keV energy range of the NXS. The absolute spectral brightness was measured by two calibrated spectrometers. We compare the measured performance of the target design to radiation hydrodynamics simulations.

  12. Bragg x-ray survey spectrometer for ITER

    SciTech Connect

    Varshney, S. K.; Jakhar, S.; Barnsley, R.; O'Mullane, M. G.

    2012-10-15

    Several potential impurity ions in the ITER plasmas will lead to loss of confined energy through line and continuum emission. For real time monitoring of impurities, a seven channel Bragg x-ray spectrometer (XRCS survey) is considered. This paper presents design and analysis of the spectrometer, including x-ray tracing by the Shadow-XOP code, sensitivity calculations for reference H-mode plasma and neutronics assessment. The XRCS survey performance analysis shows that the ITER measurement requirements of impurity monitoring in 10 ms integration time at the minimum levels for low-Z to high-Z impurity ions can largely be met.

  13. Single Particle X-ray Diffractive Imaging

    SciTech Connect

    Bogan, M J; Benner, W H; Boutet, S; Rohner, U; Frank, M; Seibert, M; Maia, F; Barty, A; Bajt, S; Riot, V; Woods, B; Marchesini, S; Hau-Riege, S P; Svenda, M; Marklund, E; Spiller, E; Hajdu, J; Chapman, H N

    2007-10-01

    In nanotechnology, strategies for the creation and manipulation of nanoparticles in the gas phase are critically important for surface modification and substrate-free characterization. Recent coherent diffractive imaging with intense femtosecond X-ray pulses has verified the capability of single-shot imaging of nanoscale objects at sub-optical resolutions beyond the radiation-induced damage threshold. By intercepting electrospray-generated particles with a single 15 femtosecond soft-X-ray pulse, we demonstrate diffractive imaging of a nanoscale specimen in free flight for the first time, an important step toward imaging uncrystallized biomolecules.

  14. Thermal detectors as single photon X-ray spectrometers

    NASA Technical Reports Server (NTRS)

    Moseley, S. H.; Kelley, R. L.; Mather, J. C.; Mushotzky, R. F.; Szymkowiak, A. E.; Mccammon, D.

    1985-01-01

    In a thermal detector employed for X-ray spectroscopy applications, the energy of an X-ray is converted to heat in a small mass, and the energy of that X-ray inferred from the size of the temperature rise. The present investigation is concerned with the possibility to make an extremely low heat capacity calorimeter which can be employed as a thermal detector. Several types of calorimeters were fabricated and tested at temperatures as low as approximately 0.05 K. The obtained devices make use of thermistors constructed of melt-doped silicon, nuclear transmutation doped (NTD) germanium, and ion-implanted silicon with a variety of materials for the support and electrical leads. The utility of these microcalorimeters as X-ray spectrometers could be verified.

  15. The Bragg solar x-ray spectrometer SolpeX

    NASA Astrophysics Data System (ADS)

    Ścisłowski, D.; Sylwester, J.; Steślicki, M.; Płocieniak, S.; Bąkała, J.; Szaforz, Ż.; Kowaliński, M.; Podgórski, P.; Trzebiński, W.; Hernandez, J.; Barylak, J.; Barylak, A.; Kuzin, Sergey

    2015-09-01

    Detection of polarization and spectra measurement of X-ray solar flare emission are indispensable in improving our understanding of the processes releasing energy of these most energetic phenomena in the solar system. We shall present some details of the construction of SolpeX - an innovative Bragg soft X-ray flare polarimeter and spectrometer. The instrument is a part of KORTES - Russian instrument complex to be mounted aboard the science module to be attached to the International Space Station (2017/2018). The SolpeX will be composed of three individual measuring units: the soft X-ray polarimeter with 1-2% linear polarization detection threshold, a fast-rotating flat crystal X-ray spectrometer with a very high time resolution (0.1 s) and a simple pinhole soft X-ray imager-spectrometer with a moderate spatial (~20 arcsec), spectral (0.5 keV) and high time resolution (0.1 s). Having a fast rotating unit to be served with power, telemetry and "intelligence" poses a challenge for the designer. Some of the solutions to this will be provided and described.

  16. A multi-crystal wavelength dispersive x-ray spectrometer

    PubMed Central

    Alonso-Mori, Roberto; Kern, Jan; Sokaras, Dimosthenis; Weng, Tsu-Chien; Nordlund, Dennis; Tran, Rosalie; Montanez, Paul; Delor, James; Yachandra, Vittal K.; Yano, Junko; Bergmann, Uwe

    2012-01-01

    A multi-crystal wavelength dispersive hard x-ray spectrometer with high-energy resolution and large solid angle collection is described. The instrument is specifically designed for time-resolved applications of x-ray emission spectroscopy (XES) and x-ray Raman scattering (XRS) at X-ray Free Electron Lasers (XFEL) and synchrotron radiation facilities. It also simplifies resonant inelastic x-ray scattering (RIXS) studies of the whole 2d RIXS plane. The spectrometer is based on the Von Hamos geometry. This dispersive setup enables an XES or XRS spectrum to be measured in a single-shot mode, overcoming the scanning needs of the Rowland circle spectrometers. In conjunction with the XFEL temporal profile and high-flux, it is a powerful tool for studying the dynamics of time-dependent systems. Photo-induced processes and fast catalytic reaction kinetics, ranging from femtoseconds to milliseconds, will be resolvable in a wide array of systems circumventing radiation damage. PMID:22852678

  17. Accuracy evaluation of a Compton X-ray spectrometer with bremsstrahlung X-rays generated by a 6 MeV electron bunch

    SciTech Connect

    Kojima, Sadaoki Arikawa, Yasunobu; Zhang, Zhe; Ikenouchi, Takahito; Morace, Alessio; Nagai, Takahiro; Abe, Yuki; Sakata, Shouhei; Inoue, Hiroaki; Utsugi, Masaru; Nakai, Mitsuo; Nishimura, Hiroaki; Shiraga, Hiroyuki; Fujioka, Shinsuke; Azechi, Hiroshi; Nishimura, Yasuhiko; Togawa, Hiromi; Ozaki, Tetsuo; Kato, Ryukou

    2014-11-15

    A Compton-scattering-based X-ray spectrometer is developed to obtain the energy distribution of fast electrons produced by intense laser and matter interactions. Bremsstrahlung X-rays generated by fast electrons in a material are used to measure fast electrons’ energy distribution in matter. In the Compton X-ray spectrometer, X-rays are converted into recoil electrons by Compton scattering in a converter made from fused silica glass, and a magnet-based electron energy analyzer is used to measure the energy distribution of the electrons that recoil in the direction of the incident X-rays. The spectrum of the incident X-rays is reconstructed from the energy distribution of the recoil electrons. The accuracy of this spectrometer is evaluated using a quasi-monoenergetic 6 MeV electron bunch that emanates from a linear accelerator. An electron bunch is injected into a 1.5 mm thick tungsten plate to produce bremsstrahlung X-rays. The spectrum of these bremsstrahlung X-rays is obtained in the range from 1 to 9 MeV. The energy of the electrons in the bunch is estimated using a Monte Carlo simulation of particle-matter interactions. The result shows that the spectrometer's energy accuracy is ±0.5 MeV for 6.0 MeV electrons.

  18. Millimeter-Scale Chemistry of Observable Endmembers with the Mars Science Laboratory Alpha Particle X-Ray Spectrometer and Mars Hand Lens Imager

    NASA Astrophysics Data System (ADS)

    VanBommel, Scott; Gellert, Ralf; Thompson, Lucy; Berger, Jeff; Campbell, Iain; Edgett, Ken; McBride, Marie; Minitti, Michelle; Desouza, Elstan; Boyd, Nick

    2016-04-01

    The Alpha Particle X-ray Spectrometer (APXS) is a bulk chemistry instrument conducting high-precision in-situ measurements of Martian rocks and soils onboard both active NASA rovers [1]. Mounted at the end of the Curiosity rover arm, the APXS can conduct multi-spot (raster) investigations in a single morning or evening. Combining APXS raster spectra and Mars Hand Lens Imager (MAHLI) images, a modeled terrain is developed in which the positions of APXS field of views (FOV) can be localized, thereby mitigating arm placement uncertainty. An acquired APXS spectrum is the result of the weighted sum of the signals from within the FOV. The spatial sensitivity of the APXS consists of an off-nadir contribution in addition to a vertical separation (standoff with respect to the APXS detector) contribution [2, 3]. MAHLI images and focus merge (MFM) products facilitate a 3D surface model of the target [4] compensating for the effects of sample relief in an APXS spectrum. Employing a MFM relief map, APXS placement is modeled in three-dimensions, permitting variable APXS docking (standoff, deployment angle). Through minimization, we arrive at millimeter-scale chemistry of veins, diagenetic features and dust-free rock endmembers of Martian targets. Several rasters have been conducted with Curiosity's APXS on Mars including a study of the Garden City outcrop. The area is characterized by its contrasting light and dark veins of cm-scale surface relief. Three-dimensional localization and minimization indicated calcium sulfate as the major component of the light vein while the dark vein is enriched in CaO (without accompanying SO3), MnO, Ni and Zn, with respect to average Mars composition. References: [1] Gellert et al. (2014), LPSC XLV, #1876. [2] VanBommel et al. (2015), LPSC XLVI, #2049. [3] VanBommel et al. (2016), XRS #2681. [4] Edgett et al. (2015), MAHLI Tech Rept 0001. Acknowledgements: The MSL APXS is financed and managed by the Canadian Space Agency (CSA) with Mac

  19. The Astro-E High Resolution X-Ray Spectrometer

    NASA Technical Reports Server (NTRS)

    Kelley, Richard L.; Audley, Michael D.; Boyce, Kevin R.; Breon, Susan R.; Fujimoto, Ryuichi; Gendreau, Keith C.; Holt, Stephen S.; Ishisaki, Yoshitaka; McCammon, Dan; Mihara, Tatehiro

    1999-01-01

    The Astro-E High Resolution X-ray Spectrometer (XRS) was developed jointly by the NASA/Goddard Space Flight Center and the Institute of Space and Astronautical Science in Japan. The instrument is based on a new approach to spectroscopy, the X-ray microcalorimeter. This device senses the energies of individual X-ray photons as heat with extreme precision. A 32 channel array of microcalorimeters is being employed, each with an energy resolution of about 12 eV at 6 keV (the Fe-K region). This will provide spectral resolving power 10 times higher than any other non-dispersive X-ray spectrometer. The instrument incorporates a three stage cooling system capable of operating the array at 60 mK for about two years in orbit. The array sits at the focus of a grazing incidence conical mirror. The quantum efficiency of the microcalorimeters and the reflectivity of the X-ray mirror system combine to give high throughput over the 0.3-12 keV energy band. This new capability will enable the study of a wide range of high-energy astrophysical sources with unprecedented spectral sensitivity. This paper presents the basic design requirements and implementation of the XRS, and also describes the instrument parameters and performance.

  20. The SHEAL Diffuse X-ray Spectrometer experiment

    NASA Technical Reports Server (NTRS)

    Sanders, W. T.; Snowden, S. L.; Edgar, R. J.

    1990-01-01

    The paper describes the Diffuse X-ray Spectrometer (DXS) experiment which will be carried on board the NASA's SHEAL 2 mission, scheduled to be launched as an attached Shuttle payload in 1992. The SHEAL DXS is designed to measure the spectrum of the low-energy (0.15 to 0.28 keV) diffuse X-ray background with the energy resolution better than 0.01 keV. The results of calculations of the anticipated data are presented together with diagrams of the DXS assembly.

  1. Time-resolved doubly bent crystal x-ray spectrometer

    SciTech Connect

    Hockaday, M.P.; Wilke, M.D.; Blake, R.L.; Vaninetti, J.; Gray, N.T.; Nedrow, P.T.

    1988-08-01

    X-ray spectroscopy is an essential tool in high-temperature plasma research. We describe a time-resolved x-ray spectrometer suitable for measuring spectra in harsh environments common to many very high-energy density laboratory plasma sources. The spectrometer consisted of a doubly curved Si(111) crystal diffraction element, a WL-1201 (ZnO:Ga) phosphor, a coherent fiber-optic array, and two visible streak cameras. The spectrometer design described here has a minimum time resolution of 1.3 ns with 2.8-eV spectral resolution over a 200-eV-wide bandpass in the 6--7-keV region of the spectrum. Complete system spectral throughput calibrations were done at the Cornell High Energy Synchrotron (CHESS). Details of the design and calibration results are presented.

  2. Time-resolved doubly bent crystal x-ray spectrometer

    SciTech Connect

    Hockaday, M.P.; Wilke, M.D.; Blake, R.L.; Vaninetti, J.; Gray, N.T.; Nedrow, P.T.

    1988-01-01

    X-ray spectroscopy is an essential tool in high temperature plasma research. We describe a time-resolved x-ray spectrometer suitable for measuring spectra in harsh environments common to many very high energy density laboratory plasma sources. The spectrometer consisted of a doubly curved Si(111) crystal diffraction element, a WL-1201 (ZnO:Ga) phosphor, a coherent fiber optic array, and two visible streak cameras. The spectrometer design described here has a minimum time resolution of 1.3 ns with 2.8 eV spectral resolution over a 200 eV wide bandpass in the 6-7 keV region of the spectrum. Complete system spectral throughput calibrations were done at the Cornell High Energy Synchrotron (CHESS). Details of the design and calibration results are presented. 5 refs., 5 figs.

  3. Calibration of the MESSENGER X-Ray Spectrometer

    NASA Astrophysics Data System (ADS)

    Starr, Richard D.; Schlemm, Charles E., II; Ho, George C.; Nittler, Larry R.; Gold, Robert E.; Solomon, Sean C.

    2016-03-01

    The X-Ray Spectrometer (XRS) that flew on the MESSENGER spacecraft measured X-rays from the surface of Mercury in the energy range ~1-10 keV. Detection of characteristic Kα-line emissions from Mg, Al, Si, S, Ca, Ti, and Fe yielded the surface abundances of these geologically important elements. Spatial resolution as fine as ~40 km (across track) was possible at periapsis for those elements for which counting statistics were not a limiting factor. Four years of orbital observations have made it possible to generate from XRS spectra detailed elemental composition maps that cover a majority of Mercury's surface. Converting measurements to compositions requires a thorough understanding of the XRS instrument capabilities. The ground and flight calibration measurements presented here are necessary for the reduction and analysis of the X-ray data from the MESSENGER mission.

  4. Imaging X-ray Thomson Scattering Spectrometer Design and Demonstration

    SciTech Connect

    Gamboa, E.J.; Huntington, C.M.; Trantham, M.R.; Keiter, P.A; Drake, R.P.; Montgomery, David; Benage, John F.; Letzring, Samuel A.

    2012-05-04

    In many laboratory astrophysics experiments, intense laser irradiation creates novel material conditions with large, one-dimensional gradients in the temperature, density, and ionization state. X-ray Thomson scattering is a powerful technique for measuring these plasma parameters. However, the scattered signal has previously been measured with little or no spatial resolution, which limits the ability to diagnose inhomogeneous plasmas. We report on the development of a new imaging x-ray Thomson spectrometer (IXTS) for the Omega laser facility. The diffraction of x-rays from a toroidally-curved crystal creates high-resolution images that are spatially resolved along a one-dimensional profile while spectrally dispersing the radiation. This focusing geometry allows for high brightness while localizing noise sources and improving the linearity of the dispersion. Preliminary results are presented from a scattering experiment that used the IXTS to measure the temperature profile of a shocked carbon foam.

  5. Time-resolved hard x-ray spectrometer

    NASA Astrophysics Data System (ADS)

    Moy, Kenneth; Cuneo, Michael; McKenna, Ian; Keenan, Thomas; Sanford, Thomas; Mock, Ray

    2006-08-01

    Wired array studies are being conducted at the SNL Z accelerator to maximize the x-ray generation for inertial confinement fusion targets and high energy density physics experiments. An integral component of these studies is the characterization of the time-resolved spectral content of the x-rays. Due to potential spatial anisotropy in the emitted radiation, it is also critical to diagnose the time-evolved spectral content in a space-resolved manner. To accomplish these two measurement goals, we developed an x-ray spectrometer using a set of high-speed detectors (silicon PIN diodes) with a collimated field-of-view that converged on a 1-cm-diameter spot at the pinch axis. Spectral discrimination is achieved by placing high Z absorbers in front of these detectors. We built two spectrometers to permit simultaneous different angular views of the emitted radiation. Spectral data have been acquired from recent Z shots for the radial and axial (polar) views. UNSPEC 1 has been adapted to analyze and unfold the measured data to reconstruct the x-ray spectrum. The unfold operator code, UFO2, is being adapted for a more comprehensive spectral unfolding treatment.

  6. Time-Resolved Hard X-Ray Spectrometer

    SciTech Connect

    Kenneth Moya; Ian McKennaa; Thomas Keenana; Michael Cuneob

    2007-03-01

    Wired array studies are being conducted at the SNL Z accelerator to maximize the x-ray generation for inertial confinement fusion targets and high energy density physics experiments. An integral component of these studies is the characterization of the time-resolved spectral content of the x-rays. Due to potential spatial anisotropy in the emitted radiation, it is also critical to diagnose the time-evolved spectral content in a space-resolved manner. To accomplish these two measurement goals, we developed an x-ray spectrometer using a set of high-speed detectors (silicon PIN diodes) with a collimated field-of-view that converged on a 1-cm-diameter spot at the pinch axis. Spectral discrimination is achieved by placing high Z absorbers in front of these detectors. We built two spectrometers to permit simultaneous different angular views of the emitted radiation. Spectral data have been acquired from recent Z shots for the radial and polar views. UNSPEC1 has been adapted to analyze and unfold the measured data to reconstruct the x-ray spectrum. The unfold operator code, UFO2, is being adapted for a more comprehensive spectral unfolding treatment.

  7. The superconducting high-resolution soft X-ray spectrometer at the advanced biological and environmental X-ray facility

    NASA Astrophysics Data System (ADS)

    Friedrich, S.; Drury, O. B.; George, S. J.; Cramer, S. P.

    2007-11-01

    We have built a 36-pixel superconducting tunnel junction X-ray spectrometer for chemical analysis of dilute samples in the soft X-ray band. It offers an energy resolution of ˜10-20 eV FWHM below 1 keV, a solid angle coverage of ˜10 -3, and can be operated at total rates of up to ˜10 6 counts/s. Here, we describe the spectrometer performance in speciation measurements by fluorescence-detected X-ray absorption spectroscopy at the Advanced Biological and Environmental X-ray facility at the ALS synchrotron.

  8. Portable x-ray fluorescence spectrometer for coating thickness measurement

    SciTech Connect

    Carapelle, Alain; Fleury-Frenette, Karl; Collette, Jean-Paul; Garnir, Henri-Pierre; Harlet, Philippe

    2007-12-15

    A handheld x-ray spectrometer has been realized and tested. The purpose of the device is to measure the thickness of coated samples in the range of 1-1500 nm in an industrial environment. Accuracy of {approx}3% has been achieved in this range with a measurement time of 1 min. Automated software has been implemented to allow utilization by a nonspecialist operator. An automated calibration procedure, based on measurements of reference samples, is used.

  9. Elemental analysis using a handheld X-Ray fluorescence spectrometer

    USGS Publications Warehouse

    Groover, Krishangi; Izbicki, John

    2016-01-01

    The U.S. Geological Survey is collecting geologic samples from local stream channels, aquifer materials, and rock outcrops for studies of trace elements in the Mojave Desert, southern California. These samples are collected because geologic materials can release a variety of elements to the environment when exposed to water. The samples are to be analyzed with a handheld X-ray fluorescence (XRF) spectrometer to determine the concentrations of up to 27 elements, including chromium.

  10. The Mapping X-Ray Fluorescence Spectrometer (MAPX)

    NASA Technical Reports Server (NTRS)

    Blake, David; Sarrazin, Philippe; Bristow, Thomas; Downs, Robert; Gailhanou, Marc; Marchis, Franck; Ming, Douglas; Morris, Richard; Sole, Vincente Armando; Thompson, Kathleen; Walter, Philippe; Wilson, Michael; Yen, Albert; Webb, Samuel

    2016-01-01

    MapX will provide elemental imaging at =100 micron spatial resolution over 2.5 X 2.5 centimeter areas, yielding elemental chemistry at or below the scale length where many relict physical, chemical, and biological features can be imaged and interpreted in ancient rocks. MapX is a full-frame spectroscopic imager positioned on soil or regolith with touch sensors. During an analysis, an X-ray source (tube or radioisotope) bombards the sample surface with X-rays or alpha-particles / gamma rays, resulting in sample X-ray Fluorescence (XRF). Fluoresced X-rays pass through an X-ray lens (X-ray µ-Pore Optic, "MPO") that projects a spatially resolved image of the X-rays onto a CCD. The CCD is operated in single photon counting mode so that the positions and energies of individual photons are retained. In a single analysis, several thousand frames are stored and processed. A MapX experiment provides elemental maps having a spatial resolution of =100 micron and quantitative XRF spectra from Regions of Interest (ROI) 2 centimers = x = 100 micron. ROI are compared with known rock and mineral compositions to extrapolate the data to rock types and putative mineralogies. The MapX geometry is being refined with ray-tracing simulations and with synchrotron experiments at SLAC. Source requirements are being determined through Monte Carlo modeling and experiment using XMIMSIM [1], GEANT4 [2] and PyMca [3] and a dedicated XRF test fixture. A flow-down of requirements for both tube and radioisotope sources is being developed from these experiments. In addition to Mars lander and rover missions, MapX could be used for landed science on other airless bodies (Phobos/Deimos, Comet nucleus, asteroids, the Earth's moon, and the icy satellites of the outer planets, including Europa.

  11. Soft X-ray polarimeter-spectrometer SOLPEX

    NASA Astrophysics Data System (ADS)

    Steslicki, Marek; Sylwester, Janusz; Plocieniak, Stefan; Bakala, Jaroslaw; Szaforz, Zaneta Anna; Scislowski, Daniel; Kowalinski, Miroslaw; Hernandez, Jose; Vadimovich Kuzin, Sergey; Shestov, Sergey

    2015-08-01

    We present an innovative soft X-ray polarimeter and spectrometer SOLPEX. The instrument will be mounted aboard the ISS within the Russian science complex KORTES. The measurements to be made by SOLPEX are expected to be of unprecedented quality in terms of sensitivity to detect the soft-X- ray polarization of solar emission emanating from active regions and flares in particular. Simultaneous measurements of the polarization degree and the other characteristics (eg. evolution of the spectra) constitute the last, rather unexplored area of solar X-ray spectroscopy providing substantial diagnostic potential. Second important science task to be addressed are the measurements of Doppler shifts in selected X-ray spectral emission lines formed in hot flaring sources. The novel-type Dopplerometer (flat Bragg crystal drum unit) is planned to be a part of SOLPEX and will allow to measure line Doppler shifts in absolute terms with unprecedented time resolution (fraction of a second) during the impulsive flare phases. We shall present some details of the SolpeX instrument and discuss observing sequences in a view of science objectives to be reached.

  12. The X-Ray Microcalorimeter Spectrometer for the International X-Ray Observatory

    SciTech Connect

    Kelley, R. L.; Bandler, S. R.; Kilbourne, C. A.; Porter, F. S.; Shirron, P.; Smith, S. J.; Whitehouse, P.; Ezoe, Y.; Ishisaki, Y.; Ohashi, T.; Fujimoto, R.; Sato, K.; Gottardi, L.; Hartog, R. den; Herder, J.-W. den; Hoevers, H.; Korte, P. de; Kuur, J. van der

    2009-12-16

    The International X-Ray Observatory (IXO) is under formulation by NASA, ESA and JAXA for deployment in 2022. IXO emerged over the last 18 months as the NASA Constellation-X and ESA/JAXA X-Ray Evolving Universe Spectrometer (XEUS) missions were combined. The driving performance requirements for the X-Ray Microcalorimeter Spectrometer (XMS) are a spectral resolution of 2.5 eV over the central 2'x2' in the 0.3-7.0 keV band, and 10 eV to the edge of the 5'x5' field of view (FOV). The XMS is now based on a microcalorimeter array of Transition-Edge Sensor (TES) thermometers with Au/Bi absorbers and a SQUID MUX readout. One of the concepts studied as part of the mission formulation has a core 40x40 array corresponding to a 2'x2' FOV with 3'' pixels surrounded by an outer, annular 52x52 array of 6'' pixels that extends the field of view to 5.4'x5.4' with better than 10 eV resolution. There are several options for implementing the readout and cooling system of the XMS under study in the US, Europe and Japan. The ADR system will have from two to five stages depending on the performance of the cryocooler. Mechanical coolers with sufficient cooling power at 4K are available now, and {approx}2K coolers are under development. In this paper we give an overview of the XMS instrument, and some of the tradeoffs to be addressed for this observatory instrument.

  13. Estimation of lunar major elemental abundances in Chang'E-3 landing site based on Active Particle-induced X-ray Spectrometer (APXS)

    NASA Astrophysics Data System (ADS)

    Wang, Jian; Wang, Xianmin

    2015-09-01

    Elemental abundance provides an effective vehicle to understand lunar petrologic characteristics and evolutional history. The APXS mounted on the Yutu rover provides a valuable opportunity to determine the major elemental abundances in lunar soil within a short distance. In this study, we processed the APXS spectra including energy calibration, dead time correction and nonlinear least-squares fitting, and determined the abundances of the lunar major elements using the fundamental parameter method. In the calculation of X-ray fluorescence yield, a finite element method (FEM) was employed to improve the accuracy. The major elemental abundances derived from Chang'E-3 (CE-3) APXS possess a good consistency with the result of LP-GRS (Lunar Prospector gamma-ray spectrometer) data in the landing region. Compared with the chemical composition of the returned lunar rock samples, we draw the conclusion that the lunar soils in CE-3 landing site are fragments of mare basalts. Our conclusion is supported by the geological map of Mare Imbrium.

  14. Temporal Gain Correction for X-ray Calorimeter Spectrometers

    NASA Astrophysics Data System (ADS)

    Porter, F. S.; Chiao, M. P.; Eckart, M. E.; Fujimoto, R.; Ishisaki, Y.; Kelley, R. L.; Kilbourne, C. A.; Leutenegger, M. A.; McCammon, D.; Mitsuda, K.; Sawada, M.; Szymkowiak, A. E.; Takei, Y.; Tashiro, M.; Tsujimoto, M.; Watanabe, T.; Yamada, S.

    2016-07-01

    Calorimetric X-ray detectors are very sensitive to their environment. The boundary conditions can have a profound effect on the gain including heat sink temperature, the local radiation temperature, bias, and the temperature of the readout electronics. Any variation in the boundary conditions can cause temporal variations in the gain of the detector and compromise both the energy scale and the resolving power of the spectrometer. Most production X-ray calorimeter spectrometers, both on the ground and in space, have some means of tracking the gain as a function of time, often using a calibration spectral line. For small gain changes, a linear stretch correction is often sufficient. However, the detectors are intrinsically non-linear and often the event analysis, i.e., shaping, optimal filters etc., add additional non-linearity. Thus for large gain variations or when the best possible precision is required, a linear stretch correction is not sufficient. Here, we discuss a new correction technique based on non-linear interpolation of the energy-scale functions. Using Astro-H/SXS calibration data, we demonstrate that the correction can recover the X-ray energy to better than 1 part in 104 over the entire spectral band to above 12 keV even for large-scale gain variations. This method will be used to correct any temporal drift of the on-orbit per-pixel gain using on-board calibration sources for the SXS instrument on the Astro-H observatory.

  15. The Astro-H Soft X-ray Spectrometer (SXS)

    NASA Astrophysics Data System (ADS)

    Porter, F. Scott; Fujimoto, Ryuichi; Kelley, Richard L.; Kilbourne, Caroline A.; Mitsuda, Kazuhiasa; Ohashi, Takaya; Astro-H/SXS Collaboration

    2009-12-01

    The Soft-X-ray Spectrometer (SXS) is a high spectral resolution, cryogenic x-ray spectrometer that will fly on the Japan/U.S. Astro-H observatory in 2014. The SXS is composed of a 36 pixel, imaging, x-ray calorimeter array that will operate at 0.05 K utilizing a 2-stage adiabatic demagnetization refrigerator and a redundant pre-cooler design using both a 40 liter liquid helium tank and a 1.7 K Joule-Thomson (JT) cryocooler. Additional redundant Stirling cycle coolers provide pre-cooling for the (JT) and cool the outer thermal shields for the JT and the helium tank. The detector system, while similar to that flown on Suzaku, is composed of larger 0.81×0.81mm pixels, but has significantly better performance, currently predicted to be better than 4 eV FWHM at 6 keV with 95% quantum efficiency. This instrument is the result of a close collaboration between many institutions in the U.S. and Japan over the last 25 years. Here we will present an overview of the SXS instrument, the SXS cooling system, and recent laboratory improvements to the detector system.

  16. The Astro-H Soft X-ray Spectrometer (SXS)

    SciTech Connect

    Porter, F. Scott; Kelley, Richard L.; Kilbourne, Caroline A.; Fujimoto, Ryuichi; Mitsuda, Kazuhiasa; Ohashi, Takaya

    2009-12-16

    The Soft-X-ray Spectrometer (SXS) is a high spectral resolution, cryogenic x-ray spectrometer that will fly on the Japan/U.S. Astro-H observatory in 2014. The SXS is composed of a 36 pixel, imaging, x-ray calorimeter array that will operate at 0.05 K utilizing a 2-stage adiabatic demagnetization refrigerator and a redundant pre-cooler design using both a 40 liter liquid helium tank and a 1.7 K Joule-Thomson (JT) cryocooler. Additional redundant Stirling cycle coolers provide pre-cooling for the (JT) and cool the outer thermal shields for the JT and the helium tank. The detector system, while similar to that flown on Suzaku, is composed of larger 0.81x0.81mm pixels, but has significantly better performance, currently predicted to be better than 4 eV FWHM at 6 keV with 95% quantum efficiency. This instrument is the result of a close collaboration between many institutions in the U.S. and Japan over the last 25 years. Here we will present an overview of the SXS instrument, the SXS cooling system, and recent laboratory improvements to the detector system.0.

  17. Temporal Gain Correction for X-ray Calorimeter Spectrometers

    NASA Astrophysics Data System (ADS)

    Porter, F. S.; Chiao, M. P.; Eckart, M. E.; Fujimoto, R.; Ishisaki, Y.; Kelley, R. L.; Kilbourne, C. A.; Leutenegger, M. A.; McCammon, D.; Mitsuda, K.; Sawada, M.; Szymkowiak, A. E.; Takei, Y.; Tashiro, M.; Tsujimoto, M.; Watanabe, T.; Yamada, S.

    2016-01-01

    Calorimetric X-ray detectors are very sensitive to their environment. The boundary conditions can have a profound effect on the gain including heat sink temperature, the local radiation temperature, bias, and the temperature of the readout electronics. Any variation in the boundary conditions can cause temporal variations in the gain of the detector and compromise both the energy scale and the resolving power of the spectrometer. Most production X-ray calorimeter spectrometers, both on the ground and in space, have some means of tracking the gain as a function of time, often using a calibration spectral line. For small gain changes, a linear stretch correction is often sufficient. However, the detectors are intrinsically non-linear and often the event analysis, i.e., shaping, optimal filters etc., add additional non-linearity. Thus for large gain variations or when the best possible precision is required, a linear stretch correction is not sufficient. Here, we discuss a new correction technique based on non-linear interpolation of the energy-scale functions. Using Astro-H/SXS calibration data, we demonstrate that the correction can recover the X-ray energy to better than 1 part in 104 over the entire spectral band to above 12 keV even for large-scale gain variations. This method will be used to correct any temporal drift of the on-orbit per-pixel gain using on-board calibration sources for the SXS instrument on the Astro-H observatory.

  18. The Spectrometer Telescope for Imaging X-rays (STIX)

    NASA Astrophysics Data System (ADS)

    Krucker, Sam; STIX Team

    2013-07-01

    The Spectrometer Telescope for Imaging X-rays (STIX) is one of 10 instruments on board Solar Orbiter, a confirmed M-class mission of the European Space Agency (ESA) within the Cosmic Vision program scheduled to be launched in 2017. STIX applies a Fourier-imaging technique using a set of tungsten grids (at pitches from 0.038 to 1 mm) in front of 32 pixelized CdTe detectors to provide imaging spectroscopy of solar thermal and non-thermal hard X-ray emissions from 4 to 150 keV. The status of the instrument that will be presented at the Critical Design Review (CDR) later this year will be discussed in this poster.

  19. Portable x-ray fluorescence spectrometer for environmental monitoring of inorganic pollutants

    NASA Technical Reports Server (NTRS)

    Thornton, Michael G. (Inventor); Clark, III, Benton C. (Inventor)

    1991-01-01

    A portable x-ray fluorescence spectrometer has a portable sensor unit containing a battery, a high voltage power supply, an x-ray tube which produces a beam x-ray radiation directed toward a target sample, and a detector for fluorescent x-rays produced by the sample. If a silicon-lithium detector is used, the sensor unit also contains either a thermoelectric or thermochemical cooler, or a small dewar flask containing liquid nitrogen to cool the detector. A pulse height analyzer (PHA) generates a spectrum of data for each sample consisting of the number of fluorescent x-rays detected as a function of their energy level. The PHA can also store spectrum data for a number of samples in the field. A processing unit can be attached to the pulse height analyzer to upload and analyze the stored spectrum data for each sample. The processing unit provides a graphic display of the spectrum data for each sample, and provides qualitative and/or quantitative analysis of the elemental composition of the sample by comparing the peaks in the sample spectrum against known x-ray energies for various chemical elements. An optional filtration enclosure can be used to filter particles from a sample suspension, either in the form of a natural suspension or a chemically created precipitate. The sensor unit is then temporarily attached to the filtration unit to analyze the particles collected by the filter medium.

  20. Detecting X-ray Emission from Cometary Atmospheres Using the Suzaku X-ray Imaging Spectrometer

    SciTech Connect

    Brown, G V; Beiersdorfer, P; Bodewits, D; Porter, F S; Ezoe, Y; Hamaguchi, K; Hanya, M; Itoh, M; Kilbourne, C A; Kohmura, T; Maeda, Y; Negoro, H; Tsuboi, Y; Tsunemi, H; Urata, Y

    2009-11-16

    The Suzaku X-ray imaging spectrometer has been used to observe the X-ray emission from comets 73P/Schwassmann-Wachmann 3C and 8P/Tuttle. Comet 73P/Schwassmann-Wachmann 3C was observed during May and June of 2006, while it was near perihelion and passed within 0.1 AU of the Earth. Comet 8P/Tuttle was observed during January of 2008 when it was at its closest approach to the Earth at 0.25 AU, and again near perihelion at a distance of 0.5 Au from Earth. In the case of comet 73P/Schwassmann Wachmann 3C, the XIS spectra show line emission from highly charged oxygen and carbon ions as well as emission from what is most likely L-shell transitions from Mg, Si, and S ions. This line emission is caused by charge exchange recombination between solar wind ions and cometary neutrals, and can be used as a diagnostic of the solar wind. Here we present some of the results of the observation of the comet 73P/Schwassmann-Wachmann 3C.

  1. Results from the NSTX X-ray Crystal Spectrometer

    SciTech Connect

    M. Bitter; K. Hill; L. Roquemore; P. Beiersdorfer; D. Thorn; Ming Feng Gu

    2003-01-14

    A high-resolution X-ray crystal spectrometer has recently been installed at the National Spherical Torus Experiment to record the satellite spectra of helium-like argon, ArXVII, in the wavelength range from 3.94 to 4.00 {angstrom} for measurements of ion and electron temperatures, and measurements of the ionization equilibrium of argon, which is of interest for studies of ion transport. The instrument presently consists of a spherically bent quartz crystal and a conventional one-dimensional position-sensitive multi-wire proportional counter, but it will soon be upgraded to a new type of X-ray imaging crystal spectrometer by the installation of a large size (10 cm x 30 cm) two-dimensional position-sensitive detector that will allow us to obtain temporally and spatially resolved spectra from an 80 cm high cross-section of the plasma. In its present configuration, the spectrometer has been optimized for high throughput so that it is possible to record spectra with small statistical errors with a time resolution of 10 ms by adding only small, nonperturbing amounts of argon to the plasma. The spectrometer is most valuable for measurements of the ion temperature in the absence of a neutral beam in ohmically heated and radio-frequency heated discharges, when charge exchange recombination spectroscopy does not function. Electron temperature measurements from the satellite-to-resonance line ratios have been important for a quantitative comparison with (and verification of) the Thomson scattering data. The paper will describe the instrumental details of the present and future spectrometer configurations, and present recent experimental results.

  2. X-ray fluorescence spectrometer onboard Hayabusa: instrument, science and observation plan

    NASA Astrophysics Data System (ADS)

    Okada, T.; Shirai, K.; Yamamoto, Y.; Arai, T.; Ogawa, K.; Kato, M.; Hayabusa Xrs Team

    We have developed a CCD-based X-ray fluorescence spectrometer, XRS, onboard the HAYABUSA spacecraft, with heritage technology from the X-ray fluorescence and atmospheric detector onboard the S310-28 sounding rocket experiment. Its scientific objectives are (1) to determine surface major elemental composition of asteroid 25143 Itokawa (1998SF36), (2) to map longitudinal variation of elements, if it exists, by asteroid rotation, (3) to inform on surface microscopic roughness via measurement of surface regolith's particle size effect in X-ray fluorescence, and (4) to observe X-ray bodies and X-ray cosmic backgrounds. At the earth swing-by phase, we have a plan to observe X-rays from the earth and moon. In addition, thermal design of the XRS is suitable, and examined in the spacecraft thermal vacuum test, for thermal emission study of asteroid to observe during the asteroid touchdown phase for sample collection, because the XRS has a large radiator at the asteroid pointing direction and the chassis is thermally isolated from the structure of spacecraft. We will present details of the XRS instrumentation, scientific objectives, and future observation plans, together with some results of pre-flight laboratory experiments and preliminary results of in-flight observations.

  3. Basic studies on x-ray fluorescence analysis for active x-ray spectrometer on SELENE-2

    NASA Astrophysics Data System (ADS)

    Kusano, Hiroki; Hasebe, Nobuyuki; Nagaoka, Hiroshi; Kodama, Takuro; Oyama, Yuki; Tanaka, Reiko; Amano, Yoshiharu; Kim, Kyeong J.; Matias Lopes, Josè A.

    2013-09-01

    An active X-ray spectrometer (AXS) is now being developed as a payload candidate for the rover on SELENE-2, the next Japanese lunar exploration mission. The AXS will determine the chemical compositions of lunar rocks and regolith around the landing site. The surface of lunar rock samples will be ground using a rock abrasion tool. Thus, fundamental studies on the X-ray fluorescence analysis for lunar rocks and regolith are required to design and develop the AXS. In this study, we have investigated the X-ray fluorescence analysis in order to evaluate the effects of surface roughness of samples and the angle of incident and emergent X-rays. It was found that the fluorescent X-ray yield for low energy X-rays, i.e. the light elements, decreases at rough surface samples. This effect of surface roughness becomes small for smooth surface samples. It was also found that the fluorescent X-ray yield depends on the incident angle, which is attributed to the fact that the X-ray fluorescence occurs closer to the sample surface at larger incident angles. Since the emergent X-rays are affected by the detection geometry and surface roughness, the incident angle effect also depends on the above conditions.

  4. Evidence for beamed electrons in a limb X-ray flare observed by Hard X-Ray Imaging Spectrometer (HXIS)

    NASA Technical Reports Server (NTRS)

    Haug, Eberhard; Elwert, Gerhard

    1986-01-01

    The limb flare of November 18, 1980, 14:51 UT, was investigated on the basis of X-ray images taken by the Hard X-ray Imaging Spectrometer (HXIS) and of X-ray spectra from the Hard X-Ray Burst Spectrometer (HXRBS) aboard the Solar Maximum Mission (SMM). The impulsive burst was also recorded at microwave frequencies between 2 and 20 GHz whereas no optical flare and no radio event at frequencies below 1 GHz were reported. The flare occurred directly at the SW limb of the solar disk. Taking advantage of the spatial resolution of HXIS images, the time evolution of the X-radiation originating from relatively small source regions can be studied. Using Monte Carlo computations of the energy distribution of energetic electrons traversing the solar plasma, the bremsstrahlung spectra produced by the electrons were derived.

  5. SolpeX: the soft X-ray flare polarimeter-spectrometer for the ISS

    NASA Astrophysics Data System (ADS)

    Sylwester, Janusz; Płocieniak, Stefan; Bakała, Jarosław; Szaforz, Żaneta; Stȩślicki, Marek; Ścisłowski, Daniel; Kowaliński, Mirosław; Podgórski, Piotr; Hernandez, Jose; Shestov, Sergey

    2015-10-01

    We present the innovative soft X-ray spectro-polarimeter, SolpeX. This instrument consists of three functionally independent blocks. They are to be included into the Russian instrument KORTES, to be mounted onboard the ISS. The three SolpeX units are: a simple pin-hole X-ray spectral imager, a polarimeter, and a fast-rotating drum multiple-flat-crystal Bragg spectrometer. Such a combination of measuring blocks will offer a new opportunity to reliably measure possible X-ray polarization and spectra of solar flares, in particular during the impulsive phase. Polarized Bremsstrahlung and line emission due to the presence of directed particle beams will be detected, and measurements of the velocities of evaporated hot plasma will be made. In this paper we discuss the details of the construction of the SolpeX units. The delivery of KORTES with SolpeX to the ISS is expected to happen in 2017/2018.

  6. Escape of Pluto's Atmosphere: In Situ Measurements from the Pluto Energetic Particle Spectrometer Science Investigation (PEPSSI) instrument on New Horizons and Remote Observations from the Chandra X-ray observatory

    NASA Astrophysics Data System (ADS)

    McNutt, Ralph L.; Hill, Matthew E.; Lisse, Carey M.; Kollmann, Peter; Bagenal, Fran; Krimigis, Stamatios M.; McComas, David J.; Elliott, Heather A.; Wolk, Scott J.; Strobel, Darrell F.; Zhu, Xun; Stern, S. A.; Weaver, H. A.; Young, L. A.; Ennico, K.; Olkin, C. B.

    2015-11-01

    The escape rate of Pluto's atmosphere is of significant scientific interest. The Pluto Energetic Particle Spectrometer Science Investigation (PEPSSI) is a compact, energy by time-of-flight (TOF) instrument developed to help address this science goal. Pluto is known to have an atmosphere, and pre-encounter models have postulated a majority N2 composition with free escape of up to ~1028 molecules/sec. The expected major ionization product near Pluto is singly ionized N2 molecules with pickup energies sufficient to be measured with PEPSSI. In the process of measuring the local energetic particle environment, such measurements can also provide constraints on the local density of Pluto's extended atmosphere, which, along with plasma measurements from the Solar Wind Around Pluto (SWAP) instrument, also on New Horizons, could allow the inference of the strengh and extent of mass-loading of the solar wind due to Pluto's atmosphere. Pluto's neutral atmosphere also provides a source population for charge exchange of highly ionized, minor ions in the solar wind, such as O, C, and N. This process allows these ions to capture one electron and be left in an excited state. That state, in turn decays with the emission of a low-energy (100 eV to 1 keV) X-ray. Observations of such solar wind charge exchange (SWCX) X-rays have been made in the past of the Earth's geocorona and Mars's extended atmosphere. The award of almost 40 hours of Director's Discretionary Time (DDT) for observing Pluto with the Chandra X-ray observatory near the period of closest approach of New Horizons to Pluto potentially enabled a remote determination of Pluto's global outgassing rate using the local solar wind flux as measured by the SWAP instrument. Preliminary anaysis of data returned from these observations reveal a definite interaction of Pluto with the solar wind, but at a lower strength than had been predicted. This work was supported by NASA's New Horizons project.

  7. The X-Ray Spectrometer for Mercury MESSENGER

    NASA Technical Reports Server (NTRS)

    Starr, R. D.; Ho, G. C.; Schlemm, C.; Gold, R. E.; Goldsten, J. O.; Boynton, W. V.; Trombka, J. I.

    2001-01-01

    Mercury is the closest planet to the Sun and because it is so close, it is difficult to study from Earth-based observatories. Its proximity to the Sun has also limited the number of spacecraft to visit this tiny planet to just one, Mariner 10, which flew by Mercury twice in 1974 and once in 1975. Mariner 10 provided a wealth of new information about Mercury, yet much still remains unknown about Mercury's geologic history and the processes that led to its formation. The origin of Mercury's metal-rich composition is just one area of investigation awaiting more and improved data to sort between competing hypotheses. Mercury plays an important role in comparative planetology, and many of the processes that were important during its formation are relevant to the Earth's early history. MESSENGER (Mercury Surface, Space Environment, Geochemistry, and Ranging) is a Discovery mission that has been designed to fly by and orbit Mercury. It will launch in March 2004, flyby Mercury in 2007 and 2008 and enter an elliptical orbit in April 2009. During the one-year orbital phase, a suite of instruments on board the MESSENGER spacecraft will study the exosphere, magnetosphere, surface, and interior of Mercury. One of these instruments will be an X-Ray Spectrometer (XRS) that will measure surface elemental abundances. Remote X-ray spectroscopy has been accomplished before on the Apollo 15 and 16 missions, and more recently on NEAR Shoemaker. The MESSENGER XRS will measure characteristic X-ray emissions induced in the surface of Mercury by the incident solar flux. The Ka lines for the elements Mg, Al, Si, S, Ca, Ti, and Fe will be detected with spatial resolution on the order of 40 km when counting statistics are not a limiting factor. These measurements can be used to obtain quantitative information on elemental composition.

  8. Atmospheric Electron-Induced X-Ray Spectrometer (AEXS) Development

    NASA Technical Reports Server (NTRS)

    Wilcox, Jaroslava Z.; Urgiles, Eduardo; Toda, Risaku; George, Thomas; Douglas, Susanne; Crisp, Joy

    2005-01-01

    This paper describes the progress in the development of the so-called Atmospheric Electron X-ray Spectrometer (AEXS) instrument in our laboratory at JPL. The AEXS is a novel miniature instrument concept based on the excitation of characteristic X-Ray Fluorescence (XRF) and luminescence spectra using a focused electron beam, for non-destructive evaluation of surfaces of samples in situ, in planetary ambient atmosphere. In situ operation is obtained through the use of a thin electron transmissive membrane to isolate the vacuum within the AEXS electron source from the outside ambient atmosphere. By using a focused electron beam, the impinging electrons on samples in the external atmosphere excite XRF spectra from the irradiated spots with high-to-medium spatial resolution. The XRF spectra are analyzed using an energy-dispersive detector to determine surface elemental composition. The use of high- intensity electron beam results in rapid spectrum acquisition (several minutes), and consequently low energy consumption (several tens of Joules) per acquired XRF spectrum in comparison to similar portable instruments.

  9. Johann Spectrometer for High Resolution X-ray Spectroscopy

    SciTech Connect

    Machek, Pavel; Froeba, Michael; Welter, Edmund; Caliebe, Wolfgang; Brueggmann, Ulf; Draeger, Guenter

    2007-01-19

    A newly designed vacuum Johann spectrometer with a large focusing analyzer crystal for inelastic x-ray scattering and high resolution fluorescence spectroscopy has been installed at the DORIS III storage ring. Spherically bent crystals with a maximum diameter of 125 mm, and cylindrically bent crystals are employed as dispersive optical elements. Standard radius of curvature of the crystals is 1000 mm, however, the design of the mechanical components also facilitates measurements with smaller and larger bending radii. Up to four crystals are mounted on a revolving crystal changer which enables crystal changes without breaking the vacuum. The spectrometer works at fixed Bragg angle. It is preferably designed for the measurements in non-scanning mode with a broad beam spot, and offers a large flexibility to set the sample to the optimum position inside the Rowland circle. A deep depletion CCD camera is employed as a position sensitive detector to collect the energy-analyzed photons on the circumference of the Rowland circle. The vacuum in the spectrometer tank is typically 10-6 mbar. The sample chamber is separated from the tank either by 25 {mu}m thick Kapton windows, which allows samples to be measured under ambient conditions, or by two gate valves. The spectrometer is currently installed at wiggler beamline W1 whose working range is 4-10.5 keV with typical flux at the sample of 5x1010photons/s/mm2. The capabilities of the spectrometer are illustrated by resonant inelastic experiments on 3d transition metals and rare earth compounds, and by chemical shift measurements on chromium compounds.

  10. Johann Spectrometer for High Resolution X-ray Spectroscopy

    NASA Astrophysics Data System (ADS)

    Machek, Pavel; Welter, Edmund; Caliebe, Wolfgang; Brüggmann, Ulf; Dräger, Günter; Fröba, Michael

    2007-01-01

    A newly designed vacuum Johann spectrometer with a large focusing analyzer crystal for inelastic x-ray scattering and high resolution fluorescence spectroscopy has been installed at the DORIS III storage ring. Spherically bent crystals with a maximum diameter of 125 mm, and cylindrically bent crystals are employed as dispersive optical elements. Standard radius of curvature of the crystals is 1000 mm, however, the design of the mechanical components also facilitates measurements with smaller and larger bending radii. Up to four crystals are mounted on a revolving crystal changer which enables crystal changes without breaking the vacuum. The spectrometer works at fixed Bragg angle. It is preferably designed for the measurements in non-scanning mode with a broad beam spot, and offers a large flexibility to set the sample to the optimum position inside the Rowland circle. A deep depletion CCD camera is employed as a position sensitive detector to collect the energy-analyzed photons on the circumference of the Rowland circle. The vacuum in the spectrometer tank is typically 10-6 mbar. The sample chamber is separated from the tank either by 25 μm thick Kapton windows, which allows samples to be measured under ambient conditions, or by two gate valves. The spectrometer is currently installed at wiggler beamline W1 whose working range is 4-10.5 keV with typical flux at the sample of 5×1010photons/s/mm2. The capabilities of the spectrometer are illustrated by resonant inelastic experiments on 3d transition metals and rare earth compounds, and by chemical shift measurements on chromium compounds.

  11. High resolution, high rate X-ray spectrometer

    DOEpatents

    Goulding, Frederick S.; Landis, Donald A.

    1987-01-01

    A pulse processing system (10) for use in an X-ray spectrometer in which a ain channel pulse shaper (12) and a fast channel pulse shaper (13) each produce a substantially symmetrical triangular pulse (f, p) for each event detected by the spectrometer, with the pulse width of the pulses being substantially independent of the magnitude of the detected event and with the pulse width of the fast pulses (p) being substantially shorter than the pulse width of the main channel pulses (f). A pile-up rejector circuit (19) allows output pulses to be generated, with amplitudes linearly related to the magnitude of the detected events, whenever the peak of a main channel pulse (f) is not affected by a preceding or succeeding main channel pulse, while inhibiting output pulses wherein peak magnitudes of main channel pulses are affected by adjacent pulses. The substantially symmetrical triangular main channel pulses (f) are generated by the weighted addition (27-31) of successive RC integrations (24, 25, 26) of an RC differentiated step wave (23). The substantially symmetrical triangular fast channel pulses (p) are generated by the RC integration ( 43) of a bipolar pulse (o) in which the amplitude of the second half is 1/e that of the first half, with the RC time constant of integration being equal to one-half the width of the bipolar pulse.

  12. Conical focusing crystal spectrometers for cosmic X-ray astronomy

    NASA Technical Reports Server (NTRS)

    Woodgate, B. E.; Lowinger, T.; Schneider, M.

    1973-01-01

    A crystal spectrometer for rocket and satellite experiments is described. Parallel X rays from a stellar object are reflected at constant angle by Bragg crystals arranged around the sector of a cone so that a single wavelength is brought to a focus onto the axis of the cone. The aberrations produced when this array is tilted to change the wavelength are considered. It is shown that these are minimized by moving cone and detector in a nearly theta to two-theta motion and by using a small-angle sector. In a specific design for a satellite instrument using LiF crystal to observe a spectral region including the iron lines at 1.9 A, a spectral resolution of 3 mA over a spectral range of 1.6-2.1 A can be obtained, with the cosmic-ray background rate, and hence the time to detect a weak line decreased by a factor 80 compared to a flat crystal spectrometer. Examples of performance for a low energy rocket experiment are also given.

  13. The Spectrometer Telescope for Imaging X-rays STIX on Solar Orbiter

    NASA Astrophysics Data System (ADS)

    Csillaghy, A.; Battaglia, M.; Krucker, S.; Hurford, G. J.

    2012-12-01

    The Spectrometer Telescope for Imaging X-rays (STIX) will provide imaging spectroscopy of solar thermal and non-thermal X-ray emissions from ~4 to 150 keV. STIX will play an important role in answering two of Solar Orbiter's main science questions: (1) How and where are energetic particles accelerated at the Sun, and how are they transported into interplanetary space? X-ray images and spectra will provide information on the location, spectrum and intensity of flare accelerated electrons near the Sun. (2) What is the magnetic connection from Solar Orbiter back to the Sun? STIX will play a key role in linking remote sensing and in-situ observations on Solar Orbiter. Radio signatures of flare accelerated electrons will be observed by the Radio and Plasma wave instrument (RPW), while the SupraThermal Electron sensor (STE) of the Energetic Particle Detector suite (EPD) will detect electrons in-situ. Thus, the magnetic structure, field line length and connectivity can be tracked. STIX is based on a Fourier-transform imaging technique similar to that used successfully by the Hard X-ray Telescope (HXT) on the Japanese Yohkoh mission, and related to that used for the Reuven Ramaty High Energy Solar Spectroscopic Imager mission. STIX has a higher sensitivity than RHESSI, with comparable image quality and spectral and spatial resolution. It will be able to observe thermal and non-thermal emission from nanoflares up to the largest X- class events. STIX consists of three main parts: 1. An X-ray window, 2. An imager with 32 subcollimators, and 3. A spectrometer with 32 Cadmium Telluride (CdTe) X-ray detectors The transmission through the grid pairs to the detectors is a very sensitive function of the direction of incidence of the X-ray flux. The relative count rates of the detectors behind the different sets of grids encode the spatial information that can be subsequently decoded on the ground to reconstruct images of the source region at different X-ray energies.

  14. Soft x-ray spectrometer (SXS): the high-resolution cryogenic spectrometer onboard ASTRO-H

    NASA Astrophysics Data System (ADS)

    Mitsuda, Kazuhisa; Kelley, Richard L.; Akamatsu, Hiroki; Bialas, Thomas; Boyce, Kevin R.; Brown, Gregory V.; Canavan, Edgar; Chiao, Meng; Costantini, Elisa; den Herder, Jan-Willem; de Vries, Cor; DiPirro, Michael J.; Eckart, Megan E.; Ezoe, Yuichiro; Fujimoto, Ryuichi; Haas, Daniel; Hoshino, Akio; Ishikawa, Kumi; Ishisaki, Yoshitaka; Iyomoto, Naoko; Kilbourne, Caroline A.; Kimball, Mark; Kitamoto, Shunji; Konami, Saori; Leutenegger, Maurice A.; McCammon, Dan; Miko, Joseph; Mitsuishi, Ikuyuki; Murakami, Hiroshi; Murakami, Masahide; Noda, Hirofumi; Ogawa, Mina; Ohashi, Takaya; Okamoto, Atsushi; Ota, Naomi; Paltani, Stéphane; Porter, F. Scott; Sato, Kosuke; Sato, Yoichi; Sawada, Makoto; Seta, Hiromi; Shinozaki, Keisuke; Shirron, Peter J.; Sneiderman, Gary A.; Sugita, Hiroyuki; Szymkowiak, Andrew; Takei, Yoh; Tamagawa, Toru; Tashiro, Makoto S.; Terada, Yukikatsu; Tsujimoto, Masahiro; Yamada, Shinya; Yamasaki, Noriko Y.

    2014-07-01

    We present the development status of the Soft X-ray Spectrometer (SXS) onboard the ASTRO-H mission. The SXS provides the capability of high energy-resolution X-ray spectroscopy of a FWHM energy resolution of < 7eV in the energy range of 0.3 - 10 keV. It utilizes an X-ray micorcalorimeter array operated at 50 mK. The SXS microcalorimeter subsystem is being developed in an EM-FM approach. The EM SXS cryostat was developed and fully tested and, although the design was generally confirmed, several anomalies and problems were found. Among them is the interference of the detector with the micro-vibrations from the mechanical coolers, which is the most difficult one to solve. We have pursued three different countermeasures and two of them seem to be effective. So far we have obtained energy resolutions satisfying the requirement with the FM cryostat.

  15. ASIC for SDD-Based X-Ray Spectrometers

    SciTech Connect

    G De Geronimo; P Rehak; K Ackley; G Carini; W Chen; J Fried; J Keister; S Li; Z Li; et al.

    2011-12-31

    We present an application-specific integrated circuit (ASIC) for high-resolution x-ray spectrometers (XRS). The ASIC reads out signals from pixelated silicon drift detectors (SDDs). The pixel does not have an integrated field effect transistor (FET); rather, readout is accomplished by wire-bonding the anodes to the inputs of the ASIC. The ASIC dissipates 32 mW, and offers 16 channels of low-noise charge amplification, high-order shaping with baseline stabilization, discrimination, a novel pile-up rejector, and peak detection with an analog memory. The readout is sparse and based on custom low-power tristatable low-voltage differential signaling (LPT-LVDS). A unit of 64 SDD pixels, read out by four ASICs, covers an area of 12.8 cm{sup 2} and dissipates with the sensor biased about 15 mW/cm{sup 2}. As a tile-based system, the 64-pixel units cover a large detection area. Our preliminary measurements at -44 C show a FWHM of 145 eV at the 5.9 keV peak of a {sup 55}Fe source, and less than 80 eV on a test-pulse line at 200 eV.

  16. ASIC for SDD-Based X-ray Spectrometers

    SciTech Connect

    De Geronimo, G.; Fried, J.; Rehak, P.; Ackley, K.; Carini, G.; Chen, W.; Keister, J.; Li, S.; Li, Z.; Pinelli, D.A.; Siddons, D.P.; Vernon, E.; Gaskin, J.A.; Ramsey, B.D.; Tyson, T.A.

    2010-06-16

    We present an application-specific integrated circuit (ASIC) for high-resolution x-ray spectrometers (XRS). The ASIC reads out signals from pixelated silicon drift detectors (SDDs). The pixel does not have an integrated field effect transistor (FET); rather, readout is accomplished by wire-bonding the anodes to the inputs of the ASIC. The ASIC dissipates 32 mW, and offers 16 channels of low-noise charge amplification, high-order shaping with baseline stabilization, discrimination, a novel pile-up rejector, and peak detection with an analog memory. The readout is sparse and based on custom low-power tristatable low-voltage differential signaling (LPT-LVDS). A unit of 64 SDD pixels, read out by four ASICs, covers an area of 12.8 cm{sup 2} and dissipates with the sensor biased about 15 mW/cm{sup 2}. As a tile-based system, the 64-pixel units cover a large detection area. Our preliminary measurements at -44 C show a FWHM of 145 eV at the 5.9 keV peak of a {sup 55}Fe source, and less than 80 eV on a test-pulse line at 200 eV.

  17. New Solar Soft X-ray Observations from the X123 Spectrometer

    NASA Astrophysics Data System (ADS)

    Caspi, A.; McTiernan, J. M.; Warren, H. P.; Woods, T. N.

    2014-12-01

    The Amptek X123 is a new soft X-ray photon-counting spectrometer, based on a silicon drift detector with integrated thermoelectric cooler, vacuum housing, and multi-channel analyzer (including pulse pile-up rejection), capable of measuring solar line and continuum emission from ~0.5 to ~30 keV with ~0.15 keV FWHM resolution. It was flown on two recent SDO/EVE sounding rocket calibration underflights, is the primary science instrument on the upcoming Miniature X-ray Solar Spectrometer (MinXSS) NASA CubeSat, and is part of the proposed instrument payload for the CubeSat Imaging X-ray Solar Spectrometer (CubIXSS) mission concept. With the best resolution yet obtained from a broadband X-ray spectrometer, the X123 will enable new studies of plasma heating and particle acceleration, during flares and quiescent periods, and help to fill a crucial observational gap from ~0.2 to ~1.2 keV, not currently measured by existing instruments but critical for understanding solar-driven dynamics in Earth's upper atmosphere (ionosphere, thermosphere, mesosphere). We present results from a new analysis of X123 data obtained from the SDO/EVE rocket flights. In preparation for future MinXSS and CubIXSS data, we adapt a recently-developed technique combining EUV and X-ray spectra from SDO/EVE and RHESSI, respectively, to obtain a self-consistent differential emission measure (DEM) over the full range of coronal temperatures, ~2-50 MK. Including the X123 rocket X-ray spectra, we apply the adapted technique to examine both the coronal DEM and composition during quiescent (non-flaring) times with varying activity levels, obtaining constraints on the high-temperature extent of the quiescent DEM, the elemental abundances, and any potential non-thermal emission, and use the observations to extrapolate the spectrum to the poorly-observed ~0.2-1.2 keV band. We compare these results with those from a parallel technique using SDO/AIA imaging data. We discuss the implications for coronal plasma

  18. EXACT – The Solar X-Ray Spectrometer CubeSat

    NASA Astrophysics Data System (ADS)

    Knuth, Trevor; Glesener, Lindsay; Gebre-Egziabher, Demoz; Vogt, Ryan; Denis, Charles; Weiher, Hannah; Runnels, Joel; Vievering, Juliana

    2016-05-01

    The Experiment for X-ray Characterization and Timing (EXACT) mission will be a CubeSat based hard X-ray spectrometer used for viewing solar flares with high time precision. Solar flares and the related coronal mass ejections affect space weather and the near-Earth environment. EXACT can study the hard X-rays generated by the Sun in the declining phase of Solar Cycle 24 in order to probe electron acceleration in solar eruptive events while also serving as a precursor to future hard X-ray spectrometers that could monitor the Sun continuously.

  19. Development of Compton X-ray spectrometer for high energy resolution single-shot high-flux hard X-ray spectroscopy.

    PubMed

    Kojima, Sadaoki; Ikenouchi, Takahito; Arikawa, Yasunobu; Sakata, Shohei; Zhang, Zhe; Abe, Yuki; Nakai, Mitsuo; Nishimura, Hiroaki; Shiraga, Hiroyuki; Ozaki, Tetsuo; Miyamoto, Shuji; Yamaguchi, Masashi; Takemoto, Akinori; Fujioka, Shinsuke; Azechi, Hiroshi

    2016-04-01

    Hard X-ray spectroscopy is an essential diagnostics used to understand physical processes that take place in high energy density plasmas produced by intense laser-plasma interactions. A bundle of hard X-ray detectors, of which the responses have different energy thresholds, is used as a conventional single-shot spectrometer for high-flux (>10(13) photons/shot) hard X-rays. However, high energy resolution (Δhv/hv < 0.1) is not achievable with a differential energy threshold (DET) X-ray spectrometer because its energy resolution is limited by energy differences between the response thresholds. Experimental demonstration of a Compton X-ray spectrometer has already been performed for obtaining higher energy resolution than that of DET spectrometers. In this paper, we describe design details of the Compton X-ray spectrometer, especially dependence of energy resolution and absolute response on photon-electron converter design and its background reduction scheme, and also its application to the laser-plasma interaction experiment. The developed spectrometer was used for spectroscopy of bremsstrahlung X-rays generated by intense laser-plasma interactions using a 200 μm thickness SiO2 converter. The X-ray spectrum obtained with the Compton X-ray spectrometer is consistent with that obtained with a DET X-ray spectrometer, furthermore higher certainly of a spectral intensity is obtained with the Compton X-ray spectrometer than that with the DET X-ray spectrometer in the photon energy range above 5 MeV. PMID:27131669

  20. Development of Compton X-ray spectrometer for high energy resolution single-shot high-flux hard X-ray spectroscopy

    NASA Astrophysics Data System (ADS)

    Kojima, Sadaoki; Ikenouchi, Takahito; Arikawa, Yasunobu; Sakata, Shohei; Zhang, Zhe; Abe, Yuki; Nakai, Mitsuo; Nishimura, Hiroaki; Shiraga, Hiroyuki; Ozaki, Tetsuo; Miyamoto, Shuji; Yamaguchi, Masashi; Takemoto, Akinori; Fujioka, Shinsuke; Azechi, Hiroshi

    2016-04-01

    Hard X-ray spectroscopy is an essential diagnostics used to understand physical processes that take place in high energy density plasmas produced by intense laser-plasma interactions. A bundle of hard X-ray detectors, of which the responses have different energy thresholds, is used as a conventional single-shot spectrometer for high-flux (>1013 photons/shot) hard X-rays. However, high energy resolution (Δhv/hv < 0.1) is not achievable with a differential energy threshold (DET) X-ray spectrometer because its energy resolution is limited by energy differences between the response thresholds. Experimental demonstration of a Compton X-ray spectrometer has already been performed for obtaining higher energy resolution than that of DET spectrometers. In this paper, we describe design details of the Compton X-ray spectrometer, especially dependence of energy resolution and absolute response on photon-electron converter design and its background reduction scheme, and also its application to the laser-plasma interaction experiment. The developed spectrometer was used for spectroscopy of bremsstrahlung X-rays generated by intense laser-plasma interactions using a 200 μm thickness SiO2 converter. The X-ray spectrum obtained with the Compton X-ray spectrometer is consistent with that obtained with a DET X-ray spectrometer, furthermore higher certainly of a spectral intensity is obtained with the Compton X-ray spectrometer than that with the DET X-ray spectrometer in the photon energy range above 5 MeV.

  1. Calibration of an imaging crystal spectrometer for low x-ray energies

    SciTech Connect

    Lee, S. G.; Bak, J. G.; Bitter, M.

    2008-01-15

    An x-ray imaging crystal spectrometer was designed for the Hanbit magnetic mirror device to observe spectra of heliumlike neon at 13.4474 A. The spectrometer consists of a spherically bent mica crystal and an x-ray sensitive vacuum charge coupled device camera. This spectrometer can provide spatially resolved spectra, making it possible to obtain profiles of the ion charge state distribution from line ratios and profiles of the plasma rotation velocity from Doppler shift measurements. The paper describes measurements of spectral resolution of this instrument for low x-ray energies.

  2. Development of high throughput X-ray telescopes for X-ray imaging and dispersive spectrometers

    NASA Technical Reports Server (NTRS)

    Gorenstein, P.

    1986-01-01

    During the past year the technical approach to the realization of a high throughput Kirkpatrick-Baez X-ray mirror became better defined in terms of construction methodology and factors which affect maximum size. More progress was made than anticipated in the area of automatic figure formation. However, effort to improve the resolution of float glass by simple techniques were not successful. Mirror development, spectroscopy, all sky telescope, and explorer concept studies are discussed.

  3. Space-Resolved Spectrum Diagnose by Soft X-Ray Transmission Grating Spectrometer

    NASA Astrophysics Data System (ADS)

    Shang, Wanli; Zhao, Yang; Xiong, Gang; Yang, Jiamin; Zhu, Tuo

    2011-02-01

    A space-resolving transmission grating spectrometer is established on the “Shenguang-III" prototype laser facility and an iterative procedure for unfolding the X-ray spectrum with spatial resolution is described. The diagnostics is applied to measure the X-ray spectrum from laser-entered gold target and the typical space-resolved spectrum is provided. The relative standard uncertainty of the X-ray spectrum from the laser-generated plasma is also determined.

  4. The hard X-ray burst spectrometer event listing, 1980 - 1985

    NASA Technical Reports Server (NTRS)

    Dennis, B. R.; Orwig, L. E.; Kiplinger, A. L.; Gibson, B. R.; Kennard, G. S.; Tolbert, A. K.

    1985-01-01

    This event listing is a comprehensive reference for the hard X-ray bursts detected with the Hard X-Ray Burst Spectrometer on the Solar Maximum Mission from the time of launch on February 14, 1980 to September 1985. Over 8000 X-ray events were detected in the energy range from 30 to approx. 500 keV with the vast majority being solar flares. The listing includes the start time, peak time, duration and peak rate of each event.

  5. The hard X-ray burst spectrometer event listing 1980-1987

    NASA Technical Reports Server (NTRS)

    Dennis, B. R.; Orwig, L. E.; Kiplinger, A. L.; Schwartz, R. A.; Gibson, B. R.; Kennard, G. S.; Tolbert, A. K.; Biesecker, D. A.; Labow, G. J.; Shaver, A.

    1988-01-01

    This event listing is a comprehensive reference for the Hard X-ray bursts detected with the Hard X-ray Burst Spectrometer on the Solar Maximum Mission from the time of launch 14 February 1980 to December 1987. Over 8600 X-ray events were detected in the energy range from 30 to approx. 600 keV with the vast majority being solar flares. The listing includes the start time, peak time, duration and peak rate of each event.

  6. Pump-probe spectrometer for measuring x-ray induced strain.

    PubMed

    Loether, A; Adams, B W; DiCharia, A; Gao, Y; Henning, R; Walko, D A; DeCamp, M F

    2016-05-01

    A hard x-ray pump-probe spectrometer using a multi-crystal Bragg reflector is demonstrated at a third generation synchrotron source. This device derives both broadband pump and monochromatic probe pulses directly from a single intense, broadband x-ray pulse centered at 8.767 keV. We present a proof-of-concept experiment which directly measures x-ray induced crystalline lattice strain. PMID:27128053

  7. The hard X-ray burst spectrometer event listing 1980, 1981 and 1982

    NASA Technical Reports Server (NTRS)

    Dennis, B. R.; Frost, K. J.; Orwig, L. E.; Kiplinger, A.; Dennis, H. E.; Gibson, B. R.; Kennard, G. S.; Tolbert, A. K.

    1983-01-01

    A comprehensive reference for the hard X-ray bursts detected with the Hard X-Ray Burst Spectrometer on the Solar Maximum Mission for the time of launch on February 14, 1980 to March 1983 is provided. Over 6300 X-ray events were detected in the energy range from 30 to approx 500 keV with the vast majority being solar flares. The listing includes the start time, peak time, duration and peak rate of each event.

  8. The Soft X-Ray Spectrometer (SXS) for the ISAS/JAXA New Exploration X-Ray Telescope

    NASA Astrophysics Data System (ADS)

    Kelley, Richard L.; Kilbourne, C. A.; McCammon, D.; Mushotzky, R. F.; Okajima, T.; Petre, R.; Porter, F. S.; Serlemitsos, P. J.; Smith, R. K.; Soong, Y.; Szymkowiak, A. E.; Mitsuda, K.; Ohashi, T.; Ishisaki, Y.; Ezoe, Y.; Yamasaki, N. Y.; Shinozaki, K.; Fujimoto, R.; Kawaharada, M.

    2008-03-01

    The ISAS/JAXA New Exploration X-Ray Telescope (NEXT) is now under development for launch in 2013. The observatory is designed to provide extremely high spectral resolution with large collecting area below 10 keV using an x-ray calorimeter, and a very large band pass (up to 300 keV) with extraordinary sensitivity over the range 10-80 keV using focusing x-ray optics. In this talk we will discuss plans for the Soft X-Ray Spectrometer (SXS), which uses an x-ray calorimeter array to provide the high spectral resolution. The SXS is a joint effort between ISAS and NASA and recently proposed to NASA as a Mission of Opportunity for the US participation. The SXS incorporates a 6x6 calorimeter array that has strong heritage in the Suzaku program and better than 7 eV energy resolution, with 4-5 eV expected based on recent laboratory tests. The cryogenic system will be a hybrid design with both liquid helium and mechanical coolers to provide a robust, redundant system with long life (> 3 years). The x-ray optical system (6 m focal length) uses thin-foil conical optics to provide at least 220 square cm at 6 keV. The SXS will enable a wide variety of interesting science topics to be pursued, including testing theories of structure formation using velocity measurements of clusters of galaxies and inferring the energy output from the jets and winds of active galaxies. The SXS will accurately measure metal abundances in the oldest galaxies, providing unique information on the origin of the elements, and observe matter in extreme gravitational fields, enabling time-resolved spectra from material approaching the event horizon of a black hole. Along with providing the instrument, we have proposed a well supported guest investigator program that will enable full US participation.

  9. A Johann-type X-ray emission spectrometer at the Rossendorf beamline.

    PubMed

    Kvashnina, Kristina O; Scheinost, Andreas C

    2016-05-01

    This paper gives a detailed description, including equations, of the Johann-type X-ray emission spectrometer which has been recently installed and tested at the Rossendorf beamline (ROBL) of the European Synchrotron Radiation Facility. The spectrometer consists of a single spherically bent crystal analyzer and an avalanche photodiode detector positioned on the vertical Rowland cycle of 1 m diameter. The hard X-ray emission spectrometer (∼3.5-25 keV) operates at atmospheric pressure and covers the Bragg angles of 65°-89°. The instrument has been tested at high and intermediate incident energies, i.e. at the Zr K-edge and at the Au L3-edge, in the second experimental hutch of ROBL. The spectrometer is dedicated for studying actinides in materials and environmental samples by high-energy-resolution X-ray absorption and X-ray emission spectroscopies. PMID:27140166

  10. Future prospects for high resolution X-ray spectrometers

    NASA Technical Reports Server (NTRS)

    Canizares, C. R.

    1981-01-01

    Capabilities of the X-ray spectroscopy payloads were compared. Comparison of capabilities of AXAF in the context of the science to be achieved is reported. The Einstein demonstrated the tremendous scientific power of spectroscopy to probe deeply the astrophysics of all types of celestial X-ray source. However, it has limitations in sensitivity and resolution. Each of the straw man instruments has a sensitivity that is at least an order of magnitude better than that of the Einstein FPSC. The AXAF promises powerful spectral capability.

  11. Time-resolved x-ray transmission grating spectrometer for studying laser-produced plasmas.

    PubMed

    Ceglio, N M; Kauffman, R L; Hawryluk, A M; Medecki, H

    1983-01-15

    The development of a new time-resolved x-ray spectrometer is reported in which a free-standing x-ray transmission grating is coupled to a soft x-ray streak camera. The instrument measures continuous x-ray spectra with 20-psec temporal resolution and moderate spectral resolution (deltalambda >/= 1 A) over a broad spectral range (0.1-5 keV) with high sensitivity and large information recording capacity. Its capabilities are well suited to investigation of laser-generated plasmas, and they nicely complement the characteristics of other time-resolved spectroscopic techniques presently in use. The transmission grating spectrometer has been used on a variety of laser-plasma experiments. We report the first measurements of the temporal variation of continuous low-energy x-ray spectra from laser-irradiated disk targets. PMID:18195786

  12. Calibration of a high resolution grating soft x-ray spectrometer

    SciTech Connect

    Magee, E. W.; Dunn, J.; Brown, G. V.; Beiersdorfer, P.; Cone, K. V.; Park, J.; Porter, F. S.; Kilbourne, C. A.; Kelley, R. L.

    2010-10-15

    The calibration of the soft x-ray spectral response of a large radius of curvature, high resolution grating spectrometer (HRGS) with a back-illuminated charge-coupled device detector is reported. The instrument is cross-calibrated for the 10-50 A waveband at the Lawrence Livermore National Laboratory electron beam ion trap (EBIT) x-ray source with the EBIT calorimeter spectrometer. The HRGS instrument is designed for laser-produced plasma experiments and is important for making high dynamic range measurements of line intensities, line shapes, and x-ray sources.

  13. Calibration of a high resolution grating soft x-ray spectrometer.

    PubMed

    Magee, E W; Dunn, J; Brown, G V; Cone, K V; Park, J; Porter, F S; Kilbourne, C A; Kelley, R L; Beiersdorfer, P

    2010-10-01

    The calibration of the soft x-ray spectral response of a large radius of curvature, high resolution grating spectrometer (HRGS) with a back-illuminated charge-coupled device detector is reported. The instrument is cross-calibrated for the 10-50 Å waveband at the Lawrence Livermore National Laboratory electron beam ion trap (EBIT) x-ray source with the EBIT calorimeter spectrometer. The HRGS instrument is designed for laser-produced plasma experiments and is important for making high dynamic range measurements of line intensities, line shapes, and x-ray sources. PMID:21034013

  14. Cylindrical Crystal Imaging Spectrometer (CCIS) for cosmic X-ray spectroscopy

    NASA Technical Reports Server (NTRS)

    Schnopper, H. W.; Taylor, P. O.

    1981-01-01

    A "stigmatic" focusing, Bragg crystal spectrometer was developed and used for high spectral resolution X-ray emission line diagnostics on hot laboratory plasmas. The concept be applied at the focal plane of an orbiting X-ray telescope where it offers several advantages over conventional spectrometers, i.e., mechanical simplicity, high resolving power and sensitivity, simultaneous measurement of an extended segment of spectrum, and good imaging properties. The instrument features a simple, unambiguous, non-scanning spectrum readout that is not adversely affected by either spacecraft pointing error or source extent. The performance of the instrument is estimated in the context of the Advanced X-Ray Astrophysical Facility mission.

  15. Soft X-ray scanning transmission X-ray microscopy (STXM) of actinide particles.

    PubMed

    Nilsson, Hans J; Tyliszczak, Tolek; Wilson, Richard E; Werme, Lars; Shuh, David K

    2005-09-01

    A descriptive account is given of our most recent research on the actinide dioxides with the Advanced Light Source Molecular Environmental Science (ALS-MES) Beamline 11.0.2 soft X-ray scanning transmission X-ray microscope (STXM) at the Lawrence Berkeley National Laboratory (LBNL). The ALS-MES STXM permits near-edge X-ray absorption fine structure (NEXAFS) and imaging with 30-nm spatial resolution. The first STXM spectromicroscopy NEXAFS spectra at the actinide 4d5/2 edges of the imaged transuranic particles, NpO2 and PuO2, have been obtained. Radiation damage induced by the STXM was observed in the investigation of a mixed oxidation state particle (Np(V,VI)) and was minimized during collection of the actual spectra at the 4d5/2 edge of the Np(V,VI) solid. A plutonium elemental map was obtained from an irregular PuO2 particle with the dimensions of 650 x 650 nm. The Pu 4d5/2 NEXAFS spectra were collected at several different locations from the PuO2 particle and were identical. A representative oxygen K-edge spectrum from UO2 was collected and resembles the oxygen K-edge from the bulk material. The unique and current performance of the ALS-MES STXM at extremely low energies (ca. 100 eV) that may permit the successful measurement of the actinide 5d edge is documented. Finally, the potential of STXM as a tool for actinide investigations is briefly discussed. PMID:16021423

  16. Superconducting High-Resolution X-Ray Spectrometers for Chemical State Analysis of Dilute Samples

    SciTech Connect

    Friedrich, S; Drury, O B; Funk, T; Sherrell, D; Yachandra, V K; Labov, S E; Cramer, S P

    2003-09-02

    Cryogenic X-ray spectrometers operating at temperatures below 1 K combine high energy resolution with broadband efficiency for X-ray energies up to 10 keV. They offer advantages for chemical state analysis of dilute samples by fluorescence-detected X-ray absorption spectroscopy (XAS) in cases where conventional Ge or Si(Li) detectors lack energy resolution and grating spectrometers lack detection efficiency. We are developing soft X-ray spectrometers based on superconducting Nb-Al-AlOx-Al-Nb tunnel junction (STJ) technology. X-rays absorbed in one of the superconducting electrodes generate excess charge carriers in proportion to their energy, thereby producing a measurable temporary increase in tunneling current. For STJ operation at the synchrotron, we have designed a two-stage adiabatic demagnetization refrigerator (ADR) with a cold finger that holds a 3 x 3 array of STJs inside the UHV sample chamber at a temperature of {approx}0.1 K within {approx}15 mm of a room temperature sample. Our STJ spectrometer can have an energy resolution below 10 eV FWHM for X-ray energies up to 1 keV, and has total count rate capabilities above 100,000 counts/s. We will describe detector performance in synchrotron-based X-ray fluorescence experiments and demonstrate its use for XAS on a dilute metal site in a metalloprotein.

  17. Laboratory-based micro-X-ray fluorescence setup using a von Hamos crystal spectrometer and a focused beam X-ray tube

    SciTech Connect

    Kayser, Y.; Błachucki, W.; Dousse, J.-Cl.; Hoszowska, J.; Neff, M.; Romano, V.

    2014-04-15

    The high-resolution von Hamos bent crystal spectrometer of the University of Fribourg was upgraded with a focused X-ray beam source with the aim of performing micro-sized X-ray fluorescence (XRF) measurements in the laboratory. The focused X-ray beam source integrates a collimating optics mounted on a low-power micro-spot X-ray tube and a focusing polycapillary half-lens placed in front of the sample. The performances of the setup were probed in terms of spatial and energy resolution. In particular, the fluorescence intensity and energy resolution of the von Hamos spectrometer equipped with the novel micro-focused X-ray source and a standard high-power water-cooled X-ray tube were compared. The XRF analysis capability of the new setup was assessed by measuring the dopant distribution within the core of Er-doped SiO{sub 2} optical fibers.

  18. Laboratory-based micro-X-ray fluorescence setup using a von Hamos crystal spectrometer and a focused beam X-ray tube

    NASA Astrophysics Data System (ADS)

    Kayser, Y.; Błachucki, W.; Dousse, J.-Cl.; Hoszowska, J.; Neff, M.; Romano, V.

    2014-04-01

    The high-resolution von Hamos bent crystal spectrometer of the University of Fribourg was upgraded with a focused X-ray beam source with the aim of performing micro-sized X-ray fluorescence (XRF) measurements in the laboratory. The focused X-ray beam source integrates a collimating optics mounted on a low-power micro-spot X-ray tube and a focusing polycapillary half-lens placed in front of the sample. The performances of the setup were probed in terms of spatial and energy resolution. In particular, the fluorescence intensity and energy resolution of the von Hamos spectrometer equipped with the novel micro-focused X-ray source and a standard high-power water-cooled X-ray tube were compared. The XRF analysis capability of the new setup was assessed by measuring the dopant distribution within the core of Er-doped SiO2 optical fibers.

  19. Laboratory-based micro-X-ray fluorescence setup using a von Hamos crystal spectrometer and a focused beam X-ray tube.

    PubMed

    Kayser, Y; Błachucki, W; Dousse, J-Cl; Hoszowska, J; Neff, M; Romano, V

    2014-04-01

    The high-resolution von Hamos bent crystal spectrometer of the University of Fribourg was upgraded with a focused X-ray beam source with the aim of performing micro-sized X-ray fluorescence (XRF) measurements in the laboratory. The focused X-ray beam source integrates a collimating optics mounted on a low-power micro-spot X-ray tube and a focusing polycapillary half-lens placed in front of the sample. The performances of the setup were probed in terms of spatial and energy resolution. In particular, the fluorescence intensity and energy resolution of the von Hamos spectrometer equipped with the novel micro-focused X-ray source and a standard high-power water-cooled X-ray tube were compared. The XRF analysis capability of the new setup was assessed by measuring the dopant distribution within the core of Er-doped SiO2 optical fibers. PMID:24784587

  20. Soft X-Ray Spectrometer Using 100-Pixel STJ Detectors for Synchrotron Radiation

    SciTech Connect

    Shiki, Shigetomo; Zen, Nobuyuki; Ukibe, Masahiro; Ohkubo, Masataka

    2009-12-16

    Fluorescent X-ray absorption fine structure (XAFS) is an important tool for material analysis, especially for the measurement of chemical states or local structures of elements. Semiconductor detectors are usually used for separating the fluorescent of elements in question from background fluorescence. However, the semiconductor detectors cannot always discriminate K-lines of light elements and L-lines of various elements as different X-ray peaks at an energy range below about 3 keV. Superconducting tunnel junction (STJ) detectors are promising device for the soft X-ray at synchrotron radiation beam lines because of excellent energy resolution, high detection efficiency, and high counting rate. We are constructing a fluorescent X-ray spectrometer having 100-pixel array of STJs with 200 {mu}m square. The array detector is mounted on a liquid cryogen-free {sup 3}He cryostat. The sensitive area is the largest among the superconducting X-ray spectrometers operating at synchrotron beam lines. Each pixel is connected to a room temperature readout circuit that consists of a charge sensitive amplifier and a pulse height analyzer. The spectrometer will achieve a total solid angle of {approx}0.01 sr and a maximum counting rate of more than 1 M count per second. The present status of developments of our fluorescent X-ray spectrometer was reported.

  1. Passive Spectroscopy Bolometers, Grating- And X-Ray Imaging Crystal Spectrometers

    SciTech Connect

    Bitter, M; Hill, K W; Scott, S; Paul, S; Ince-Cushmann, A; Reinke, M; Rice, J; Beiersdorfer, P; Gu, M F; Lee, S G; Broennimann, C; Eikenberry, E F

    2007-11-07

    This tutorial gives a brief introduction into passive spectroscopy and describes the working principles of bolometers, a high-resolution grating spectrometer, and a novel X-ray imaging crystal spectrometer, which is of particular interest for profile measurements of the ion temperature and plasma rotation velocity on ITER and future burning plasma experiments.

  2. Passive Spectroscopy Bolometers, Grating- And X-ray Imaging Crystal Spectrometers

    SciTech Connect

    Bitter, M.; Hill, K. W.; Scott, S.; Paul, S.; Ince-Cushman, A.; Reinke, M.; Rice, J. E.; Beiersdorfer, P.; Gu, M. F.; Lee, S. G.; Broennimann, Ch.; Eikenberry, E. F.

    2008-03-12

    This tutorial gives a brief introduction into passive spectroscopy and describes the working principles of bolometers, a high-resolution grating spectrometer, and a novel X-ray imaging crystal spectrometer, which is also of particular interest for profile measurements of the ion temperature and plasma rotation velocity on ITER and future burning plasma experiments.

  3. A tube-excited x-ray fluorescence spectrometer for use in small-diameter boreholes

    SciTech Connect

    Reeves, J.H.; Arthur, R.J.; Brodzinski, R.L.; Shepard, C.L.

    1995-04-01

    A portable in-situ x-ray fluorescence analytical system that uses an x-ray tube excitation source and a cooled Si(Li) spectrometer for detecting characteristic emission x rays has been developed for use in small-diameter wells and boreholes. The 15-watt, iron-anode x-ray tube operates up to 30 kV. Three wells at the Sandia National Laboratory Chemical Waste Landfill, lined with 76 {mu} thick polyethylene, were logged specifically for Cr contamination. Detection limits below 50 ppM were achieved with counting intervals of 600 seconds and with the Si(Li) detector operating at 450-eV resolution (full width at half maximum [FWHM] for the Mn K-alpha x ray).

  4. Calibration of a Flat Field Soft X-ray Grating Spectrometer for Laser Produced Plasmas

    SciTech Connect

    Park, J; Brown, G V; Schneider, M B; Baldis, H A; Beiersdorfer, P; Cone, K V; Kelley, R L; Kilbourne, C A; Magee, E; May, M J; Porter, F S

    2010-05-12

    We have calibrated the x ray response of a variable line spaced grating spectrometer, known as the VSG, at the Fusion and Astrophysics Data and Diagnostic Calibration Facility at the Lawrence Livermore National Laboratory (LLNL). The VSG has been developed to diagnose laser produced plasmas, such as those created at the Jupiter Laser Facility and the National Ignition Facility at LLNL, and at both the Omega and Omega EP lasers at University of Rochester's Laboratory for Laser Energetics. The bandwidth of the VSG spans the range from {approx} 6 to 60 {angstrom}. The calibration results present here include the VSG's dispersion and quantum efficiency. The dispersion is determined by measuring the x rays emitted from hydrogen-like and helium-like ions of carbon, nitrogen, oxygen, neon, and aluminum. The quantum efficiency is calibrated to an accuracy of 30% or better by normalizing the x ray intensities recorded by the VSG to those simultaneously recorded by an x ray microcalorimeter spectrometer.

  5. Laser induced x-ray `RADAR' particle physics model

    NASA Astrophysics Data System (ADS)

    Lockley, D.; Deas, R.; Moss, R.; Wilson, L. A.; Rusby, D.; Neely, D.

    2016-05-01

    The technique of high-power laser-induced plasma acceleration can be used to generate a variety of diverse effects including the emission of X-rays, electrons, neutrons, protons and radio-frequency radiation. A compact variable source of this nature could support a wide range of potential applications including single-sided through-barrier imaging, cargo and vehicle screening, infrastructure inspection, oncology and structural failure analysis. This paper presents a verified particle physics simulation which replicates recent results from experiments conducted at the Central Laser Facility at Rutherford Appleton Laboratory (RAL), Didcot, UK. The RAL experiment demonstrated the generation of backscattered X-rays from test objects via the bremsstrahlung of an incident electron beam, the electron beam itself being produced by Laser Wakefield Acceleration. A key initial objective of the computer simulation was to inform the experimental planning phase on the predicted magnitude of the backscattered X-rays likely from the test objects. This objective was achieved and the computer simulation was used to show the viability of the proposed concept (Laser-induced X-ray `RADAR'). At the more advanced stages of the experimental planning phase, the simulation was used to gain critical knowledge of where it would be technically feasible to locate key diagnostic equipment within the experiment. The experiment successfully demonstrated the concept of X-ray `RADAR' imaging, achieved by using the accurate timing information of the backscattered X-rays relative to the ultra-short laser pulse used to generate the electron beam. By using fast response X-ray detectors it was possible to derive range information for the test objects being scanned. An X-ray radar `image' (equivalent to a RADAR B-scan slice) was produced by combining individual X-ray temporal profiles collected at different points along a horizontal distance line scan. The same image formation process was used to generate

  6. Spherical crystal imaging spectrometer (SCIS) for cosmic x-ray spectroscopy.

    PubMed

    Schnopper, H W; Taylor, P O

    1980-10-01

    The application of a spherically bent crystal x-ray spectrometer to cosmic x-ray problems is discussed. This is the only geometry whose diffraction properties are preserved under all rotations of the spacecraft. The combination of Bragg reflection and spherical aberration provides for stigmatic imaging of extended sources and minimum spatial and/or spectral resolution loss arising from source extent and spacecraft pointing errors. The sensitivity of the instrument is discussed in the context of a Spacelab mission. PMID:20234612

  7. High Gain, Fast Scan, Broad Spectrum, Parallel Beam Wavelength Dispersive X-ray Spectrometer for SEM

    SciTech Connect

    David OHara; Dr. Eric Lochmer

    2003-09-12

    Parallax Research, Inc. proposes to produce a new type of x-ray spectrometer for use with Scanning Electron Microscopy (SEM) that would have the energy resolution of WDS and the ease of use of EDS with sufficient gain for lower energies that it can be used at low beam currents as is EDS. Parallax proposes to do this by development of new multiple reflection x-ray collimation optics, new diffractor technology, new detector technology and new scan algorithms.

  8. The complete Hard X Ray Burst Spectrometer event list, 1980-1989

    NASA Technical Reports Server (NTRS)

    Dennis, B. R.; Orwig, L. E.; Kennard, G. S.; Labow, G. J.; Schwartz, R. A.; Shaver, A. R.; Tolbert, A. K.

    1991-01-01

    This event list is a comprehensive reference for all Hard X ray bursts detected with the Hard X Ray Burst Spectrometer on the Solar Maximum Mission from the time of launch on Feb. 14, 1980 to the end of the mission in Dec. 1989. Some 12,776 events were detected in the energy range 30 to 600 keV with the vast majority being solar flares. This list includes the start time, peak time, duration, and peak rate of each event.

  9. Spectral resolution measurement of an x-ray imaging crystal spectrometer for KSTAR

    SciTech Connect

    Lee, S. G.; Bak, J. G.; Nam, U. W.; Moon, M. K.; Cheon, J. K.; Bitter, M.; Hill, K.

    2008-10-15

    A spectral resolution measurement of the x-ray imaging crystal spectrometer for the Korea Superconducting Tokamak Advanced Research machine utilizing a segmented position-sensitive detector and time-to-digital converter based delay-line readout electronics was performed by using an x-ray tube in a laboratory. The measured spectral resolution is about 12 600, which means the actual energy resolution is 0.32 eV for the x-ray tube's bremsstrahlung peak energy of 4 keV. The results from the spectral resolution measurement are described.

  10. Spectral resolution measurement of an x-ray imaging crystal spectrometer for KSTAR.

    PubMed

    Lee, S G; Bak, J G; Nam, U W; Moon, M K; Cheon, J K; Bitter, M; Hill, K

    2008-10-01

    A spectral resolution measurement of the x-ray imaging crystal spectrometer for the Korea Superconducting Tokamak Advanced Research machine utilizing a segmented position-sensitive detector and time-to-digital converter based delay-line readout electronics was performed by using an x-ray tube in a laboratory. The measured spectral resolution is about 12,600, which means the actual energy resolution is 0.32 eV for the x-ray tube's bremsstrahlung peak energy of 4 keV. The results from the spectral resolution measurement are described. PMID:19044479

  11. Volume 1. Preliminary design study: AXAF x ray calibration spectrometers. Volume 2. Revised preliminary design study: AXAF x ray calibration spectrometers

    NASA Technical Reports Server (NTRS)

    1992-01-01

    The objective of this work was to provide a preliminary design concept for a Flux Monitor Spectrometer (FMS) for use at the X Ray Astrophysics Facility (XRAF) during High Resolution Mirror Assembly (HRMA) testing that met the requirements of SAO-AXAF-88-025 dated July 31, 1991. The calibration test team determined that the spectral resolution of the FMS had to be greater than or equal to twice that of all the AXAF spectrometers throughout the 0.1 to 10 KeV range of x-ray energies. Since this effectively doubled the resolution required by SAO-AXAF-88-025, a change order was approved by the Marshall Space Flight Center and given to Radiation Sciences to revise their study.

  12. High gain, Fast Scan, Broad Spectrum Parallel Beam Wavelength Dispersive X-ray Spectrometer for SEM

    SciTech Connect

    OHara, David

    2009-05-08

    During contract # DE-FG02-ER83545, Parallax Research, Inc. developed a High gain, Fast Scan Broad Spectrum Parallel beam Wavelength Dispersive X-ray Spectrometer for use on Scanning Electron Microscopes (SEM). This new spectrometer allows very fast high resolution elemental analysis of samples in an electron microscope. By comparison to previous WDS spectrometers, it can change from one energy position to another very quickly and has an extended range compared to some similar products.

  13. Time-resolved near-edge x-ray absorption fine structure spectroscopy on photo-induced phase transitions using a tabletop soft-x-ray spectrometer

    NASA Astrophysics Data System (ADS)

    Grossmann, P.; Rajkovic, I.; Moré, R.; Norpoth, J.; Techert, S.; Jooss, C.; Mann, Klaus

    2012-05-01

    We present a table-top soft-x-ray spectrometer for the wavelength range λ = 1-5 nm based on a stable laser-driven x-ray source, making use of a gas-puff target. With this setup, optical light-pump/soft-x-ray probe near-edge x-ray absorption fine structure (NEXAFS) experiments with a temporal resolution of about 230 ps are feasible. Pump-probe NEXAFS measurements were carried out in the "water-window" region (2.28 nm-4.36 nm) on the manganite Pr0.7Ca0.3MnO3, investigating diminutive changes of the oxygen K edge that derive from an optically induced phase transition. The results show the practicability of the table-top soft-x-ray spectrometer on demanding investigations so far exclusively conducted at synchrotron radiation sources.

  14. Spectrometer for hard X-ray free-electron laser based on diffraction focusing.

    PubMed

    Kohn, V G; Gorobtsov, O Y; Vartanyants, I A

    2013-03-01

    X-ray free-electron lasers (XFELs) generate sequences of ultra-short spatially coherent pulses of X-ray radiation. A diffraction focusing spectrometer (DFS), which is able to measure the whole energy spectrum of the radiation of a single XFEL pulse with an energy resolution of ΔE/E 2 × 10(-6), is proposed. This is much better than for most modern X-ray spectrometers. Such resolution allows one to resolve the fine spectral structure of the XFEL pulse. The effect of diffraction focusing occurs in a single-crystal plate due to dynamical scattering, and is similar to focusing in a Pendry lens made from a metamaterial with a negative refraction index. Such a spectrometer is easier to operate than those based on bent crystals. It is shown that the DFS can be used in a wide energy range from 5 keV to 20 keV. PMID:23412482

  15. Double conical crystal x-ray spectrometer for high resolution ultrafast x-ray absorption near-edge spectroscopy of Al K edge

    NASA Astrophysics Data System (ADS)

    Levy, A.; Dorchies, F.; Fourment, C.; Harmand, M.; Hulin, S.; Santos, J. J.; Descamps, D.; Petit, S.; Bouillaud, R.

    2010-06-01

    An x-ray spectrometer devoted to dynamical studies of transient systems using the x-ray absorption fine spectroscopy technique is presented in this article. Using an ultrafast laser-induced x-ray source, this optical device based on a set of two potassium acid phthalate conical crystals allows the extraction of x-ray absorption near-edge spectroscopy structures following the Al absorption K edge. The proposed experimental protocol leads to a measurement of the absorption spectra free from any crystal reflectivity defaults and shot-to-shot x-ray spectral fluctuation. According to the detailed analysis of the experimental results, a spectral resolution of 0.7 eV rms and relative fluctuation lower than 1% rms are achieved, demonstrated to be limited by the statistics of photon counting on the x-ray detector.

  16. A preliminary design study for a cosmic X-ray spectrometer

    NASA Technical Reports Server (NTRS)

    1972-01-01

    The results are described of theoretical and experimental investigations aimed at the development of a curved crystal cosmic X-ray spectrometer to be used at the focal plane of the large orbiting X-ray telescope on the third High Energy Astronomical Observatory. The effort was concentrated on the development of spectrometer concepts and their evaluation by theoretical analysis, computer simulation, and laboratory testing with breadboard arrangements of crystals and detectors. In addition, a computer-controlled facility for precision testing and evaluation of crystals in air and vacuum was constructed. A summary of research objectives and results is included.

  17. Portable x-ray fluorescence spectrometer. Innovative technology summary report

    SciTech Connect

    1998-12-01

    This report describes the application of portable X-ray fluorescence (XRF) spectrometry to characterize materials related to deactivation and decommissioning (D and D) of contaminated facilities. Two portable XRF instruments manufactured by TN Spectrace were used in a technology evaluation as part of the Large-Scale Demonstration Project (LSDP) held at the Chicago Pile-5 Research Reactor (CP-5) located at Argonne National Laboratory (ANL). The LSDP is sponsored by the US Department of Energy (DOE), Office of Science and Technology, Deactivation and Decommissioning Focus Are (DDFA). The objective of the LSDP is to demonstrate innovative technologies or technology applications potentially beneficial to the D and D of contaminated facilities. The portable XRF technology offers several potential benefits for rapid characterization of facility components and contaminants, including significant cost reduction, fast turnaround time,a nd virtually no secondary waste. Field work for the demonstration of the portable XRF technology was performed from August 28--September 3, 1996 and October 30--December 13, 1996.

  18. Toward a soft x-ray Fourier-transform spectrometer

    SciTech Connect

    Howells, M.R.; Frank, K.; Hussain, Z.; Moler, E.J.; Reich, T. |; Moeller, D.; Shirley, D.A.

    1993-10-29

    The use of Fourier transform spectroscopy (FTS) in the soft x-ray region is advocated as a possible route to spectral resolution superior to that attainable with a grating system. A technical plan is described for applying FTS to the study of the absorption spectrum of helium in the region of double ionization around 60--80 eV. The proposed scheme includes a Mach-Zehnder interferometer deformed into a rhombus shape to provide grazing incidence reflections. The path difference between the interfering beams is to be tuned by translation of a table carrying four mirrors over a range {+-}1 cm which, in the absence of errors generating relative tilts of the wave fronts, would provide a resolving power equal to the number of waves of path difference: half a million at 65 eV, for example. The signal-to-noise ratio of the spectrum is analyzed and for operation on an Advanced Light Source bending magnet beam line should be about 330.

  19. Convex crystal x-ray spectrometer for laser plasma experiments

    SciTech Connect

    May, M.; Heeter, R.; Emig, J.

    2004-10-01

    Measuring time and space-resolved spectra is important for understanding Hohlraum and Halfraum plasmas. Experiments at the OMEGA laser have used the Nova TSPEC which was not optimized for the OMEGA diagnostic space envelope or for the needed spectroscopic coverage and resolution. An improved multipurpose spectrometer snout, the MSPEC, has been constructed and fielded on OMEGA. The MSPEC provides the maximal internal volume for mounting crystals without any beam interferences at either 2x or 3x magnification. The RAP crystal is in a convex mounting geometry bent to a 20 cm radius of curvature. The spectral resolution, E/dE, is about 200 at 2.5 keV. The spectral coverage is 2 to 4.5 keV. The MSPEC can record four separate spectra on the framing camera at time intervals of up to several ns. The spectrometer design and initial field-test performance will be presented and compared to that of the TSPEC.

  20. A table-top femtosecond time-resolved soft x-ray transient absorption spectrometer

    SciTech Connect

    Leone, Stephen; Loh, Zhi-Heng; Khalil, Munira; Correa, Raoul E.; Leone, Stephen R.

    2008-05-21

    A laser-based, table-top instrument is constructed to perform femtosecond soft x-ray transient absorption spectroscopy. Ultrashort soft x-ray pulses produced via high-order harmonic generation of the amplified output of a femtosecond Ti:sapphire laser system are used to probe atomic core-level transient absorptions in atoms and molecules. The results provide chemically specific, time-resolved dynamics with sub-50-fs time resolution. In this setup, high-order harmonics generated in a Ne-filled capillary waveguide are refocused by a gold-coated toroidal mirror into the sample gas cell, where the soft x-ray light intersects with an optical pump pulse. The transmitted high-order harmonics are spectrally dispersed with a home-built soft x-ray spectrometer, which consists of a gold-coated toroidal mirror, a uniform-line spaced plane grating, and a soft x-ray CCD camera. The optical layout of the instrument, design of the soft x-ray spectrometer, and spatial and temporal characterization of the high-order harmonics are described. Examples of static and time-resolved photoabsorption spectra collected on this apparatus are presented.

  1. Calibrated time-resolved transmission grating spectrometer for the study of ultrafast x-ray sources.

    PubMed

    Pelletier, J F; Chaker, M; Kieffer, J C

    1996-01-01

    A transmission grating spectrometer has been coupled to a high-temporal-resolution soft x-ray streak camera for the study of picosecond laser-plasma x-ray sources. A procedure to deconvolve the overlapping contributions of diffraction orders and to calibrate the instrument has been established in order to obtain absolute time-resolved x-ray emission spectra in the 0.1-1.2 keV spectral region. The deconvolution and calibration techniques are presented along with measurements establishing the temporal resolution of this diagnostic at ~2 ps. Examples of calibrated spectra of laser-plasma x-ray sources created by 400 fs laser pulses at intensities of 1018 W/cm2 are also shown. PMID:21307534

  2. A large-area lithium-fluoride Bragg spectrometer for stellar X-ray astronomy

    NASA Technical Reports Server (NTRS)

    Stockman, H. S., Jr.; Woodgate, B. E.; Nidey, R. A.; Angel, J. R. P.

    1975-01-01

    A large-area Bragg spectrometer used to search for the Fe XXV X-ray emission lines of Sco X-1 is described. The device has 3400 sq cm of LiF on nine crystal panels aligned perpendicular to the longitudinal axis of the rocket. X rays satisfying the Bragg condition reflect into an array of nine companion proportional counters. A pointing system incorporating a free gyroscope with 2 degrees of freedom assures that target X rays are reflected at the required angle and produces repeated spectral scans of the X-ray continuum, which are later superimposed to correct temporal effects. The instrument is capable of detecting a narrow line flux from Sco X-1 of about .01 photons/sq cm/sec.

  3. Rest-wavelength Fiducials for the ITER Core Imaging X-ray Spectrometer

    NASA Technical Reports Server (NTRS)

    Beiersdorfer, P.; Brown, G. V.; Graf, A. T.; Bitter, M.; Hill, K. W.; Kelley, R. L.; Kilbourne, C. A.; Leutenegger, M. A.; Porter, F. S.

    2012-01-01

    Absolute wavelength references are needed to derive the plasma velocities from the Doppler shift of a given line emitted by a moving plasma. We show that such reference standards exist for the strongest x-ray line in neonlike W64+, which has become the line of choice for the ITER (Latin the way) core imaging x-ray spectrometer. Close-by standards are the Hf L3 line and the Ir L2 line, which bracket the W64+ line by 30 eV; other standards are given by the Ir L1 and L2 lines and the Hf L1 and L2 lines, which bracket the W64+ line by 40 and 160 eV, respectively. The reference standards can be produced by an x-ray tube built into the ITER spectrometer. We present spectra of the reference lines obtained with an x-ray microcalorimeter and compare them to spectra of the W64+ line obtained both with an x-ray microcalorimeter and a crystal spectrometer

  4. Rest-wavelength fiducials for the ITER core imaging x-ray spectrometer.

    PubMed

    Beiersdorfer, P; Brown, G V; Graf, A T; Bitter, M; Hill, K W; Kelley, R L; Kilbourne, C A; Leutenegger, M A; Porter, F S

    2012-10-01

    Absolute wavelength references are needed to derive the plasma velocities from the Doppler shift of a given line emitted by a moving plasma. We show that such reference standards exist for the strongest x-ray line in neonlike W(64+), which has become the line of choice for the ITER (Latin "the way") core imaging x-ray spectrometer. Close-by standards are the Hf Lβ(3) line and the Ir Lα(2) line, which bracket the W(64+) line by ±30 eV; other standards are given by the Ir Lα(1) and Lα(2) lines and the Hf Lβ(1) and Lβ(2) lines, which bracket the W(64+) line by ±40 and ±160 eV, respectively. The reference standards can be produced by an x-ray tube built into the ITER spectrometer. We present spectra of the reference lines obtained with an x-ray microcalorimeter and compare them to spectra of the W(64+) line obtained both with an x-ray microcalorimeter and a crystal spectrometer. PMID:23126933

  5. High Resolution, Non-Dispersive X-Ray Calorimeter Spectrometers on EBITs and Orbiting Observatories

    NASA Technical Reports Server (NTRS)

    Porter, Frederick S.

    2010-01-01

    X-ray spectroscopy is the primary tool for performing atomic physics with Electron beam ion trap (EBITs). X-ray instruments have generally fallen into two general categories, 1) dispersive instruments with very high spectral resolving powers but limited spectral range, limited count rates, and require an entrance slit, generally, for EBITs, defined by the electron beam itself, and 2) non-dispersive solid-state detectors with much lower spectral resolving powers but that have a broad dynamic range, high count rate ability and do not require a slit. Both of these approaches have compromises that limit the type and efficiency of measurements that can be performed. In 1984 NASA initiated a program to produce a non-dispersive instrument with high spectral resolving power for x-ray astrophysics based on the cryogenic x-ray calorimeter. This program produced the XRS non-dispersive spectrometers on the Astro-E, Astro-E2 (Suzaku) orbiting observatories, the SXS instrument on the Astro-H observatory, and the planned XMS instrument on the International X-ray Observatory. Complimenting these spaceflight programs, a permanent high-resolution x-ray calorimeter spectrometer, the XRS/EBIT, was installed on the LLNL EBIT in 2000. This unique instrument was upgraded to a spectral resolving power of 1000 at 6 keV in 2003 and replaced by a nearly autonomous production-class spectrometer, the EBIT Calorimeter Spectrometer (ECS), in 2007. The ECS spectrometer has a simultaneous bandpass from 0.07 to over 100 keV with a spectral resolving power of 1300 at 6 keV with unit quantum efficiency, and 1900 at 60 keV with a quantum efficiency of 30%. X-ray calorimeters are event based, single photon spectrometers with event time tagging to better than 10 us. We are currently developing a follow-on instrument based on a newer generation of x-ray calorimeters with a spectral resolving power of 3000 at 6 keV, and improved timing and measurement cadence. The unique capabilities of the x-ray

  6. Convex Crystal X-ray Spectrometer for Laser Plasma Experiments

    SciTech Connect

    May, M; Heeter, R; Emig, J

    2004-04-15

    Measuring time and space-resolved spectra is important for understanding Hohlraum and Halfraum plasmas. Experiments at the OMEGA laser have used the Nova TSPEC which was not optimized for the OMEGA diagnostic space envelope or for the needed spectroscopic coverage and resolution. An improved multipurpose spectrometer snout, the MSPEC, has been constructed and fielded on OMEGA. The MSPEC provides the maximal internal volume for mounting crystals without any beam interferences at either 2x or 3x magnification. The RAP crystal is in a convex mounting geometry bent to a 20 cm radius of curvature. The spectral resolution, E/dE, is about 200 at 2.5 keV. The spectral coverage is 2 to 4.5 keV. The MSPEC can record four separate spectra on the framing camera at time intervals of up to several ns. The spectrometer design and initial field-test performance will be presented and compared to that of the TSPEC. Work supported by U. S. DoE/UC LLNL contract W-7405-ENG-48

  7. Rocket studies of solar corona and transition region. [X-Ray spectrometer/spectrograph telescope

    NASA Technical Reports Server (NTRS)

    Acton, L. W.; Bruner, E. C., Jr.; Brown, W. A.; Nobles, R. A.

    1979-01-01

    The XSST (X-Ray Spectrometer/Spectrograph Telescope) rocket payload launched by a Nike Boosted Black Brant was designed to provide high spectral resolution coronal soft X-ray line information on a spectrographic plate, as well as time resolved photo-electric records of pre-selected lines and spectral regions. This spectral data is obtained from a 1 x 10 arc second solar region defined by the paraboloidal telescope of the XSST. The transition region camera provided full disc images in selected spectral intervals originating in lower temperature zones than the emitting regions accessible to the XSST. A H-alpha camera system allowed referencing the measurements to the chromospheric temperatures and altitudes. Payload flight and recovery information is provided along with X-ray photoelectric and UV flight data, transition camera results and a summary of the anomalies encountered. Instrument mechanical stability and spectrometer pointing direction are also examined.

  8. Cooling system for the soft x-ray spectrometer (SXS) onboard ASTRO-H

    NASA Astrophysics Data System (ADS)

    Fujimoto, Ryuichi; Mitsuda, Kazuhisa; Yamasaki, Noriko; Takei, Yoh; Tsujimoto, Masahiro; Sugita, Hiroyuki; Sato, Yoichi; Shinozaki, Keisuke; Okamoto, Atsushi; Ohashi, Takaya; Ishisaki, Yoshitaka; Ezoe, Yuichiro; Ishikawa, Kumi; Murakami, Masahide; Kitamoto, Shunji; Murakami, Hiroshi; Tamagawa, Toru; Kawaharada, Madoka; Yamaguchi, Hiroya; Sato, Kosuke; Hoshino, Akio; Kanao, Kenichi; Yoshida, Seiji; Miyaoka, Mikio; Dipirro, Michael; Shirron, Peter; Sneiderman, Gary; Kelley, Richard L.; Porter, F. Scott; Kilbourne, Caroline A.; Crow, John; Mattern, Andrea; Kashani, Ali; McCammon, Dan

    2010-07-01

    The Soft X-ray Spectrometer (SXS) is a cryogenic high resolution X-ray spectrometer onboard the X-ray astronomy satellite ASTRO-H. The detector array is cooled down to 50 mK using a 3-stage adiabatic demagnetization refrigerator (ADR). The cooling chain from room temperature to the ADR heat-sink is composed of superfluid liquid He, a 4He Joule-Thomson cryocooler, and 2-stage Stirling cryocoolers. It is designed to keep 30 L of liquid He for more than 3 years in the nominal case. It is also designed with redundant subsystems throughout from room temperature to the ADR heat-sink, to alleviate failure of a single cryocooler or loss of liquid He.

  9. Calibration of a gated flat field spectrometer as a function of x-ray intensity

    SciTech Connect

    Xiong, Gang; Yang, Guohong; Li, Hang; Zhang, Jiyan Zhao, Yang; Hu, Zhimin; Wei, Minxi; Qing, Bo; Yang, Jiamin; Liu, Shenye; Jiang, Shaoen

    2014-04-15

    We present an experimental determination of the response of a gated flat-field spectrometer at the Shenguang-II laser facility. X-rays were emitted from a target that was heated by laser beams and then were divided into different intensities with a step aluminum filter and collected by a spectrometer. The transmission of the filter was calibrated using the Beijing Synchrotron Radiation Facility. The response characteristics of the spectrometer were determined by comparing the counts recorded by the spectrometer with the relative intensities of the x-rays transmitted through the step aluminum filter. The response characteristics were used to correct the transmission from two shots of an opacity experiment using the same samples. The transmissions from the two shots are consistent with corrections, but discrepant without corrections.

  10. A Soft X-ray Spectrometer using a Highly Dispersive Multilayer Grating

    SciTech Connect

    Warwick, Tony; Padmore, Howard; Voronov, Dmitriy; Yashchuk, Valeriy

    2010-01-31

    There is a need for higher resolution spectrometers as a tool for inelastic x-ray scattering. Currently, resolving power around R = 10,000 is advertised. Measured RIXS spectra are often limited by this instrumental resolution and higher resolution spectrometers using conventional gratings would be prohibitively large. We are engaged in a development program to build blazed multilayer grating structures for diffracting soft x-rays in high order. This leads to spectrometers with dispersion much higher than is possible using metal coated-gratings. The higher dispersion then provides higher resolution and the multilayer gratings are capable of operating away from grazing incidence as required. A spectrometer design is presented with a total length 3.8m and capable of 10{sup 5} resolving power.

  11. Preliminary testing of a prototype portable X-ray fluorescence spectrometer

    NASA Technical Reports Server (NTRS)

    Patten, L. L.; Anderson, N. B.; Stevenson, J. J.

    1982-01-01

    A portable X-ray fluorescence spectrometer for use as an analyzer in mineral resource investigative work was built and tested. The prototype battery powered spectrometer, measuring 11 by 12 by 5 inches and weighing only about 15 pounds, was designed specifically for field use. The spectrometer has two gas proportional counters and two radioactive sources, Cd (10a) and Fe (55). Preliminary field and laboratory tests on rock specimens and rock pulps have demonstrated the capability of the spectrometer to detect 33 elements to date. Characteristics of the system present some limitations, however, and further improvements are recommended.

  12. Atomic data for the ITER Core Imaging X-ray Spectrometer

    SciTech Connect

    Clementson, J; Beiersdorfer, P; Biedermann, C; Bitter, M; Delgado-Aparicio, L F; Graf, A; Gu, M F; Hill, K W; Barnsley, R

    2012-06-15

    The parameters of the ITER core plasmas will be measured using the Core Imaging X-ray Spectrometer (CIXS), a high-resolution crystal spectrometer focusing on the L-shell spectra of highly ionized tungsten atoms. In order to correctly infer the plasma properties accurate atomic data are required. Here, some aspects of the underlying physics are discussed using experimental data and theoretical predictions from modeling.

  13. A spaceworthy ADR - Recent developments. [Adiabatic Demagnetization Refrigerator for X ray spectrometer

    NASA Technical Reports Server (NTRS)

    Serlemitsos, Aristides T.; Warner, Brent A.; Sansebastian, Marcelino; Kunes, Evan

    1990-01-01

    Recent developments concerning the performance and reliability of a spaceworthy adiabatic demagnetization refrigerator (ADR) for the AXAF X-ray spectrometer are considered. They include a procedure for growing the salt pill around a harness made up of 6080 gold-plated copper wires, a totally modular gas gap heat switch, and a suspension system utilizing Kevlar fibers.

  14. Apollo lunar orbital sciences program alpha and X-ray spectrometers

    NASA Technical Reports Server (NTRS)

    1972-01-01

    The development of the alpha and X-ray spectrometers which were used on the Apollo 15 and 16 flights is discussed. Specific subjects presented are: (1) lunar program management, (2) scientific and technical approach, (3) major test programs, (4) reliability, quality assurance, and safety, and (5) subcontract management.

  15. REgolith X-Ray Imaging Spectrometer (REXIS) Aboard NASA’s OSIRIS-REx Mission

    NASA Astrophysics Data System (ADS)

    Hong, JaeSub; Allen, Branden; Grindlay, Jonathan E.; Binzel, Richard P.; Masterson, Rebecca; Inamdar, Niraj K; Chodas, Mark; Smith, Matthew W; Bautz, Mark W.; Kissel, Steven E; Villasenor, Jesus Noel; Oprescu, Antonia

    2014-06-01

    The REgolith X-Ray Imaging Spectrometer (REXIS) is a student-led instrument being designed, built, and operated as a collaborative effort involving MIT and Harvard. It is a part of NASA's OSIRIS-REx mission, which is scheduled for launch in September of 2016 for a rendezvous with, and collection of a sample from the surface of the primitive carbonaceous chondrite-like asteroid 101955 Bennu in 2019. REXIS will determine spatial variations in elemental composition of Bennu's surface through solar-induced X-ray fluorescence. REXIS consists of four X-ray CCDs in the detector plane and an X-ray mask. It is the first coded-aperture X-ray telescope in a planetary mission, which combines the benefit of high X-ray throughput of wide-field collimation with imaging capability of a coded-mask, enabling detection of elemental surface distributions at approximately 50-200 m scales. We present an overview of the REXIS instrument and the expected performance.

  16. New Views of Southern Nearside Lunar Highland Composition from the Chandrayaan-1 X-ray Spectrometer (C1XS)

    NASA Astrophysics Data System (ADS)

    Athiray, P. S.; Narendranath, S.; Sreekumar, P.; C1XS Team

    2016-05-01

    Lunar surface elemental abundances - Results from Chandrayaan-1 X-ray Spectrometer (C1XS) on-board Chandrayaan-1 and goals for the upcoming Chandrayaan-2 Large Area Soft X-ray Spectrometer (CLASS) experiment on-board Chandrayaan-2.

  17. Determining x-ray spectra of radiographic sources with a Compton spectrometer

    NASA Astrophysics Data System (ADS)

    Gehring, Amanda E.; Espy, Michelle A.; Haines, Todd J.; Hunter, James F.; King, Nick S. P.; Manard, Manuel J.; Merrill, Frank E.; Morgan, George L.; Sedillo, Robert; Trainham, Rusty; Urbaitis, Algis V.; Volegov, Petr

    2014-09-01

    Flash radiography is a diagnostic with many physics applications, and the characterization of the energy spectra of such sources is of interest. A Compton spectrometer has been proposed to conduct these measurements. Our Compton spectrometer is a 300 kg neodymium-iron magnet constructed by Morgan et al1, and it is designed to measure spectra in the <1 MeV to 20 MeV range. In this device, the x-rays from a radiographic source are collimated into a narrow beam directed on a converter foil. The forward-selected Compton electrons that are ejected from the foil enter the magnetic field region of the spectrometer. The electrons are imaged on a focal plane, with their position determined as a function of their energy. The x-ray spectrum is then reconstructed. Challenges in obtaining these measurements include limited dose of x-rays and the short pulse duration (about 50 ns) for time-resolved measurements. Here we present energy calibration measurements of the spectrometer using a negative ion source. The resolution of the spectrometer was measured in previous calibration experiments to be the greater of 1% or 0.1 MeV/c1. The reconstruction of spectra from a bremsstrahlung source and Co-60 source are also presented.

  18. Energy calibration of a high-resolution inelastic x-ray scattering spectrometer.

    PubMed

    Verbeni, Roberto; D'Astuto, Matteo; Krisch, Michael; Lorenzen, Maren; Mermet, Alain; Monaco, Giulio; Requardt, Herwig; Sette, Francesco

    2008-08-01

    The energy scale of a triple-axis x-ray spectrometer with meV energy resolution based on perfect silicon crystal optics is calibrated, utilizing the most recent determination of the silicon lattice parameter and its thermal expansion coefficient and recording the dispersion of longitudinal acoustic and optical phonons in a diamond single crystal and the molecular vibration mode in liquid nitrogen. Comparison of the x-ray results with previous inelastic neutron and Raman scattering results as well as with ab initio phonon dispersion calculations yields an overall agreement better than 2%. PMID:19044359

  19. Energy calibration of a high-resolution inelastic x-ray scattering spectrometer

    SciTech Connect

    Verbeni, Roberto; D'Astuto, Matteo; Krisch, Michael; Lorenzen, Maren; Mermet, Alain; Monaco, Giulio; Requardt, Herwig; Sette, Francesco

    2008-08-15

    The energy scale of a triple-axis x-ray spectrometer with meV energy resolution based on perfect silicon crystal optics is calibrated, utilizing the most recent determination of the silicon lattice parameter and its thermal expansion coefficient and recording the dispersion of longitudinal acoustic and optical phonons in a diamond single crystal and the molecular vibration mode in liquid nitrogen. Comparison of the x-ray results with previous inelastic neutron and Raman scattering results as well as with ab initio phonon dispersion calculations yields an overall agreement better than 2%.

  20. Wavelength calibration of x-ray imaging crystal spectrometer on Joint Texas Experimental Tokamak

    SciTech Connect

    Yan, W.; Chen, Z. Y. Jin, W.; Huang, D. W.; Ding, Y. H.; Li, J. C.; Zhang, X. Q.; Zhuang, G.; Lee, S. G.; Shi, Y. J.

    2014-11-15

    The wavelength calibration of x-ray imaging crystal spectrometer is a key issue for the measurements of plasma rotation. For the lack of available standard radiation source near 3.95 Å and there is no other diagnostics to measure the core rotation for inter-calibration, an indirect method by using tokamak plasma itself has been applied on joint Texas experimental tokamak. It is found that the core toroidal rotation velocity is not zero during locked mode phase. This is consistent with the observation of small oscillations on soft x-ray signals and electron cyclotron emission during locked-mode phase.

  1. Wavelength calibration of x-ray imaging crystal spectrometer on Joint Texas Experimental Tokamak.

    PubMed

    Yan, W; Chen, Z Y; Jin, W; Huang, D W; Ding, Y H; Li, J C; Zhang, X Q; Lee, S G; Shi, Y J; Zhuang, G

    2014-11-01

    The wavelength calibration of x-ray imaging crystal spectrometer is a key issue for the measurements of plasma rotation. For the lack of available standard radiation source near 3.95 Å and there is no other diagnostics to measure the core rotation for inter-calibration, an indirect method by using tokamak plasma itself has been applied on joint Texas experimental tokamak. It is found that the core toroidal rotation velocity is not zero during locked mode phase. This is consistent with the observation of small oscillations on soft x-ray signals and electron cyclotron emission during locked-mode phase. PMID:25430323

  2. Measuring Curved Crystal Performance for a High Resolution, Imaging X-ray Spectrometer

    SciTech Connect

    Michael Haugh and Richard Stewart

    2010-06-07

    This paper describes the design, crystal selection, and crystal testing for a vertical Johann spectrometer operating in the 13 keV range to measure ion Doppler broadening in inertial confinement plasmas. The spectrometer is designed to use thin, curved, mica crystals to achieve a resolving power of E/ΔE>2000. A number of natural mica crystals were screened for flatness and X-ray diffraction width to find samples of sufficient perfection for use in the instrument. Procedures to select and mount high quality mica samples are discussed. A diode-type X-ray source coupled to a dual goniometer arrangement was used to measure the crystal reflectivity curve. A procedure was developed for evaluating the goniometer performance using a set of diffraction grade Si crystals. This goniometer system was invaluable for identifying the best original crystals for further use and developing the techniques to select satisfactory curved crystals for the spectrometer.

  3. Observation of solar high energy gamma and X-ray emission and solar energetic particles

    NASA Astrophysics Data System (ADS)

    Struminsky, A.; Gan, W.

    2015-08-01

    We considered 18 solar flares observed between June 2010 and July 2012, in which high energy >100 MeV γ-emission was registered by the Large Area Telescope (LAT) aboard FermiGRO. We examined for these γ-events soft X-ray observations by GOES, hard X-ray observations by the Anti-Coincidence Shield of the SPectrometer aboard INTEGRAL (ACS SPI) and the Gamma-Ray burst Monitor (GBM) aboard FermiGRO. Hard X-ray and π0-decay γ-ray emissions are used as tracers of electron and proton acceleration, respectively. Bursts of hard X-ray were observed by ACS SPI during impulsive phase of 13 events. Bursts of hard X- ray >100 keV were not found during time intervals, when prolonged hard y-emission was registered by LAT/FermiGRO. Those events showing prolonged high-energy gamma-ray emission not accompanied by >100 keV hard X-ray emission are interpreted as an indication of either different acceleration processes for protons and electrons or as the presence of a proton population accelerated during the impulsive phase of the flare and subsequently trapped by some magnetic structure. In-situ energetic particle measurements by GOES and STEREO (High Energy Telescope, HET) shows that five of these y-events were not accompanied by SEP events at 1 AU, even when multi-point measurements including STEREO are taken into account. Therefore accelerated protons are not always released into the heliosphere. A longer delay between the maximum temperature and the maximum emission measure characterises flares with prolonged high energy γ-emission and solar proton events.

  4. X-ray crystal spectrometer upgrade for ITER-like wall experiments at JET

    SciTech Connect

    Shumack, A. E.; Rzadkiewicz, J.; Chernyshova, M.; Czarski, T.; Karpinski, L.; Jakubowska, K.; Scholz, M.; Byszuk, A.; Cieszewski, R.; Kasprowicz, G.; Pozniak, K.; Wojenski, A.; Zabolotny, W.; Dominik, W.; Conway, N. J.; Dalley, S.; Tyrrell, S.; Zastrow, K.-D.; Figueiredo, J. [EFDA-CSU, Culham Science Centre, Abingdon OX14 3DB; Associação EURATOM and others

    2014-11-15

    The high resolution X-Ray crystal spectrometer at the JET tokamak has been upgraded with the main goal of measuring the tungsten impurity concentration. This is important for understanding impurity accumulation in the plasma after installation of the JET ITER-like wall (main chamber: Be, divertor: W). This contribution provides details of the upgraded spectrometer with a focus on the aspects important for spectral analysis and plasma parameter calculation. In particular, we describe the determination of the spectrometer sensitivity: important for impurity concentration determination.

  5. X-ray crystal spectrometer upgrade for ITER-like wall experiments at JET.

    PubMed

    Shumack, A E; Rzadkiewicz, J; Chernyshova, M; Jakubowska, K; Scholz, M; Byszuk, A; Cieszewski, R; Czarski, T; Dominik, W; Karpinski, L; Kasprowicz, G; Pozniak, K; Wojenski, A; Zabolotny, W; Conway, N J; Dalley, S; Figueiredo, J; Nakano, T; Tyrrell, S; Zastrow, K-D; Zoita, V

    2014-11-01

    The high resolution X-Ray crystal spectrometer at the JET tokamak has been upgraded with the main goal of measuring the tungsten impurity concentration. This is important for understanding impurity accumulation in the plasma after installation of the JET ITER-like wall (main chamber: Be, divertor: W). This contribution provides details of the upgraded spectrometer with a focus on the aspects important for spectral analysis and plasma parameter calculation. In particular, we describe the determination of the spectrometer sensitivity: important for impurity concentration determination. PMID:25430332

  6. Imaging x-ray Thomson scattering spectrometer design and demonstration (invited).

    PubMed

    Gamboa, E J; Huntington, C M; Trantham, M R; Keiter, P A; Drake, R P; Montgomery, D S; Benage, J F; Letzring, S A

    2012-10-01

    In many laboratory astrophysics experiments, intense laser irradiation creates novel material conditions with large, one-dimensional gradients in the temperature, density, and ionization state. X-ray Thomson scattering is a powerful technique for measuring these plasma parameters. However, the scattered signal has previously been measured with little or no spatial resolution, which limits the ability to diagnose inhomogeneous plasmas. We report on the development of a new imaging x-ray Thomson spectrometer (IXTS) for the Omega laser facility. The diffraction of x-rays from a toroidally curved crystal creates high-resolution images that are spatially resolved along a one-dimensional profile while spectrally dispersing the radiation. This focusing geometry allows for high brightness while localizing noise sources and improving the linearity of the dispersion. Preliminary results are presented from a scattering experiment that used the IXTS to measure the temperature profile of a shocked carbon foam. PMID:23126930

  7. Imaging x-ray Thomson scattering spectrometer design and demonstration (invited)a)

    NASA Astrophysics Data System (ADS)

    Gamboa, E. J.; Huntington, C. M.; Trantham, M. R.; Keiter, P. A.; Drake, R. P.; Montgomery, D. S.; Benage, J. F.; Letzring, S. A.

    2012-10-01

    In many laboratory astrophysics experiments, intense laser irradiation creates novel material conditions with large, one-dimensional gradients in the temperature, density, and ionization state. X-ray Thomson scattering is a powerful technique for measuring these plasma parameters. However, the scattered signal has previously been measured with little or no spatial resolution, which limits the ability to diagnose inhomogeneous plasmas. We report on the development of a new imaging x-ray Thomson spectrometer (IXTS) for the Omega laser facility. The diffraction of x-rays from a toroidally curved crystal creates high-resolution images that are spatially resolved along a one-dimensional profile while spectrally dispersing the radiation. This focusing geometry allows for high brightness while localizing noise sources and improving the linearity of the dispersion. Preliminary results are presented from a scattering experiment that used the IXTS to measure the temperature profile of a shocked carbon foam.

  8. Imaging x-ray Thomson scattering spectrometer design and demonstration (invited)

    SciTech Connect

    Gamboa, E. J.; Huntington, C. M.; Trantham, M. R.; Keiter, P. A.; Drake, R. P.; Montgomery, D. S.; Benage, J. F.; Letzring, S. A.

    2012-10-15

    In many laboratory astrophysics experiments, intense laser irradiation creates novel material conditions with large, one-dimensional gradients in the temperature, density, and ionization state. X-ray Thomson scattering is a powerful technique for measuring these plasma parameters. However, the scattered signal has previously been measured with little or no spatial resolution, which limits the ability to diagnose inhomogeneous plasmas. We report on the development of a new imaging x-ray Thomson spectrometer (IXTS) for the Omega laser facility. The diffraction of x-rays from a toroidally curved crystal creates high-resolution images that are spatially resolved along a one-dimensional profile while spectrally dispersing the radiation. This focusing geometry allows for high brightness while localizing noise sources and improving the linearity of the dispersion. Preliminary results are presented from a scattering experiment that used the IXTS to measure the temperature profile of a shocked carbon foam.

  9. Laue diffraction hard x-ray spectrometer for laser fusion diagnostics

    SciTech Connect

    Priedhorsky, W.C.; Lier, D.W.; Day, R.H.

    1983-12-01

    We show that a crystal spectrometer used in the Laue mode is a useful diagnostic of high-energy x-ray emission from laser fusion plasmas. It has good collection efficiency and adequate energy resolution for continuum measurements. The instrument measures time integrated x-ray spectra with a resolving power E/..delta..Eroughly-equal10 for photon energies between 60 and 300 keV. A strong signal and no detectable background are obtained in laser fusion experiments where approx.15 J of x rays are released in a pulsed (1 ns), hard (kTroughly-equal200 keV) spectrum. A Lanex/Tri-X phosphor/film combination is used as a focal plane detector; we report its relative energy calibration. Because of the imperfection of available crystals, detailed measurements of reflectivity along the crystal are required to achieve absolute calibration.

  10. Laué diffraction hard x-ray spectrometer for laser fusion diagnostics

    NASA Astrophysics Data System (ADS)

    Priedhorsky, W. C.; Lier, D. W.; Day, R. H.

    1983-12-01

    We show that a crystal spectrometer used in the Laué mode is a useful diagnostic of high-energy x-ray emission from laser fusion plasmas. It has good collection efficiency and adequate energy resolution for continuum measurements. The instrument measures time integrated x-ray spectra with a resolving power E/ΔE≊10 for photon energies between 60 and 300 keV. A strong signal and no detectable background are obtained in laser fusion experiments where ˜15 J of x rays are released in a pulsed (1 ns), hard (kT≊200 keV) spectrum. A Lanex/Tri-X phosphor/film combination is used as a focal plane detector; we report its relative energy calibration. Because of the imperfection of available crystals, detailed measurements of reflectivity along the crystal are required to achieve absolute calibration.

  11. Two facets of the x-ray microanalysis at low voltage: The secondary fluorescence x-rays emission and the microcalorimeter energy-dispersive spectrometer

    NASA Astrophysics Data System (ADS)

    Demers, Hendrix

    The best spatial resolution, for a microanalysis with a scanning electron microscope (SEND, is achieved by using a low voltage electron beam. But the x-ray microanalysis was developed for high electron beam energy (greater than 10 keV). Also, the specimen will often contain light and medium elements and the analyst will have to use a mixture of K, L, and sometime M x-ray peaks for the x-ray microanalysis. With a mixture of family lines, it will be common to have secondary fluorescence x-rays emission by K--L and L--K interactions. The accuracy of the fluorescence correction models presently used by the analyst are not well known for these interactions. This work shows that the modified secondary fluorescence x-rays emission correction models can improve the accuracy of the microanalysis for K--L and L--K interactions. The general equation derived in this work allows the identification of three factors which influence the secondary fluorescence x-rays emission. The fluorescence production factor epsilonƒ can be used to predict the importance of the secondary fluorescence x-rays emission. A large value of epsilonƒ indicates that a fluorescence correction is needed. Another disadvantage of using a low voltage is that there are more frequent occurrences of x-ray peaks overlap. A new microanalysis instruments that combines the high-spatial resolution and high-energy resolution for x-ray detection is needed. The microcalorimeter energy-dispersive spectrometer (muEDS) should improve the low voltage microanalysis, but the maturity of this technology has to be evaluated first. One of the first commercial muEDS for x-ray microanalysis in a SEM is studied and analyzed in this work. This commercial muEDS has an excellent energy resolution (˜ 15 eV) and can detect x-rays of low energy. This x-ray detector can be used as a high-spatial resolution and high-energy resolution microanalysis instrument. There are still hurdles that this technology must overcome before its

  12. Particle Spectrometers for FRIB

    NASA Astrophysics Data System (ADS)

    Amthor, A. M.

    2014-09-01

    FRIB promises to dramatically expand the variety of nuclear systems available for direct experimental study by providing rates of many rare isotopes orders of magnitude higher than those currently available. A new generation of experimental systems, including new particle spectrometers will be critical to our ability to take full advantage of the scientific opportunities offered by FRIB. The High-Rigidity Spectrometer (HRS) will allow for experiments with the most neutron-rich and short-lived isotopes produced by in-flight fragmentation at FRIB. The bending capability of the HRS (8 Tm) matches to the rigidity for which rare isotopes are produced at the highest intensity in the FRIB fragment separator. The experimental program will be focused on nuclear structure and astrophysics, and allow for the use of other cutting-edge detection systems for gamma, neutron, and charged-particle detection. Stopped and reaccelerated beam studies will be an important compliment to in-flight techniques at FRIB, providing world-unique, high quality, intense rare isotope beams at low energies up to and beyond the Coulomb barrier--with the completion of ReA12--and serving many of the science goals of the broader facility, from nuclear structure and astrophysics to applications. Two specialized recoil spectrometers are being developed for studies with reaccelerated beams. SECAR, the Separator for Capture Reactions, will be built following ReA3, coupled to a windowless gas jet target, JENSA, and will focus on radiative capture reactions for astrophysics, particularly those needed to improve our understanding of novae and X-ray bursts. A recoil separator following ReA12 is proposed to address a variety of physics cases based on fusion-evaporation, Coulomb excitation, transfer, and deep-inelastic reactions by providing a large angular, momentum and charge state acceptance; a high mass resolving power; and the flexibility to couple to a variety of auxiliary detector systems. Two designs

  13. Designing the X-Ray Microcalorimeter Spectrometer for Optimal Science Return

    NASA Technical Reports Server (NTRS)

    Ptak, Andrew; Bandler, Simon R.; Bookbinder, Jay; Kelley, Richard L.; Petre, Robert; Smith, Randall K.; Smith, Stephen

    2013-01-01

    Recent advances in X-ray microcalorimeters enable a wide range of possible focal plane designs for the X-ray Microcalorimeter Spectrometer (XMS) instrument on the future Advanced X-ray Spectroscopic Imaging Observatory (AXSIO) or X-ray Astrophysics Probe (XAP). Small pixel designs (75 microns) oversample a 5-10" PSF by a factor of 3-6 for a 10 m focal length, enabling observations at both high count rates and high energy resolution. Pixel designs utilizing multiple absorbers attached to single transition-edge sensors can extend the focal plane to cover a significantly larger field of view, albeit at a cost in maximum count rate and energy resolution. Optimizing the science return for a given cost and/or complexity is therefore a non-trivial calculation that includes consideration of issues such as the mission science drivers, likely targets, mirror size, and observing efficiency. We present a range of possible designs taking these factors into account and their impacts on the science return of future large effective-area X-ray spectroscopic missions.

  14. Wavelength dispersing devices for soft and ultrasoft x-ray spectrometers

    SciTech Connect

    Arai, Tomoya; Ryon, R.W.; Shoji, Takashi

    1984-01-01

    Monochromatization combining total reflection by a selected mirror and an appropriate filter offered an alternative approach in order to increase measurable intensity with reasonable spectral resolution. Recently, the use of synthetic multilayers, which are prepared by sputter/evaporation techniques, has been introduced for the detection of soft and ultrasoft x-rays. Studies on the use of these new wavelength dispersing devices have been conducted and it has been found that the reflectivity of these devices is very high compared with single crystals and soap multilayers and that their resolving power is fairly good. This report makes comparisons regarding efficiency of reflection, resolving power and x-ray analytical problems for practical applications among long spacing single crystals, soap multilayers, total reflection combined with a selected mirror and filtering and synthetic multilayers. The x-ray analytical capablities are shown based upon a standard x-ray fluorescence spectrometer equipped with a sealed-off x-ray tube and a gas flow proportional counter with thin film detector window.

  15. Application of a transmission crystal x-ray spectrometer to moderate-intensity laser driven sources

    SciTech Connect

    Mao, J. Y.; Chen, L. M.; Zhang, L.; Sun, Y. Q.; Lin, X. X.; Hudson, L. T.; Seely, J. F.; Zhang, J.

    2012-04-15

    In the pursuit of novel, laser-produced x-ray sources for medical imaging applications, appropriate instrumental diagnostics need to be developed concurrently. A type of transmission crystal spectroscopy has previously been demonstrated as a survey tool for sources produced by high-power and high-energy lasers. The present work demonstrates the extension of this method into the study of medium-intensity laser driven hard x-ray sources with a design that preserves resolving power while maintaining high sensitivity. Specifically, spectroscopic measurements of characteristic K{alpha} and K{beta} emissions were studied from Mo targets irradiated by a 100 fs, 200 mJ, Ti: sapphire laser with intensity of 10{sup 17} W/cm{sup 2} to 10{sup 18} W/cm{sup 2} per shot. Using a transmission curved crystal spectrometer and off-Rowland circle imaging, resolving powers (E/{Delta}E) of around 300 for Mo K{alpha}{sub 2} at 17.37 keV were obtained with an end-to-end spectrometer efficiency of (1.13 {+-} 0.10) x 10{sup -5}. This sensitivity is sufficient for registering x-ray lines with high signal to background from targets following irradiation by a single laser pulse, demonstrating the utility of this method in the study of the development of medium-intensity laser driven x-ray sources.

  16. Calibration of a flat field soft x-ray grating spectrometer for laser produced plasmas.

    PubMed

    Park, J; Brown, G V; Schneider, M B; Baldis, H A; Beiersdorfer, P; Cone, K V; Kelley, R L; Kilbourne, C A; Magee, E W; May, M J; Porter, F S

    2010-10-01

    We have calibrated the x-ray response of a variable line spaced grating spectrometer, known as the VSG, at the Fusion and Astrophysics Data and Diagnostic Calibration Facility at the Lawrence Livermore National Laboratory (LLNL). The VSG has been developed to diagnose laser produced plasmas, such as those created at the Jupiter Laser Facility and the National Ignition Facility at LLNL and at both the Omega and Omega EP lasers at the University of Rochester's Laboratory for Laser Energetics. The bandwidth of the VSG spans the range of ∼6-60 Å. The calibration results presented here include the VSG's dispersion and quantum efficiency. The dispersion is determined by measuring the x rays emitted from the hydrogenlike and heliumlike ions of carbon, nitrogen, oxygen, neon, and aluminum. The quantum efficiency is calibrated to an accuracy of 30% or better by normalizing the x-ray intensities recorded by the VSG to those simultaneously recorded by an x-ray microcalorimeter spectrometer. PMID:21034017

  17. High Performance Non-Dispersive X-Ray Spectrometers for Charge Exchange Measurements

    NASA Technical Reports Server (NTRS)

    Porter Frederick; Adams, J.; Beiersdorfer, P.; Brown, G. V.; Karkatoua, D.; Kelley, R. L.; Kilbourne, C. A.; Lautenagger, M.

    2010-01-01

    Currently, the only measurements of cosmological charge exchange have been made using low resolution, non-dispersive spectrometers like the PSPC on ROSAT and the CCD instruments on Chandra and XMM/Newton. However, upcoming cryogenic spectrometers on Astro-H and IXO will add vast new capabilities to investigate charge exchange in local objects such as comets and planetary atmospheres. They may also allow us to observe charge exchange in extra-solar objects such as galactic supernova remnants. With low spectral resolution instruments such as CCDs, x-ray emission due to charge exchange recombination really only provides information on the acceptor species, such as the solar wind. With the new breed of x-ray calorimeter instruments, emission from charge exchange becomes highly diagnostic allowing one to uniquely determine the acceptor species, ionization state, donor species and ionization state, and the relative velocity of the interaction. We will describe x-ray calorimeter instrumentation and its potential for charge exchange measurements in the near term. We will also touch on the instrumentation behind a decade of high resolution measurements of charge exchange using an x-ray calorimeter at the Lawrence Livermore National Laboratory.

  18. LabVIEW control software for scanning micro-beam X-ray fluorescence spectrometer.

    PubMed

    Wrobel, Pawel; Czyzycki, Mateusz; Furman, Leszek; Kolasinski, Krzysztof; Lankosz, Marek; Mrenca, Alina; Samek, Lucyna; Wegrzynek, Dariusz

    2012-05-15

    Confocal micro-beam X-ray fluorescence microscope was constructed. The system was assembled from commercially available components - a low power X-ray tube source, polycapillary X-ray optics and silicon drift detector - controlled by an in-house developed LabVIEW software. A video camera coupled to optical microscope was utilized to display the area excited by X-ray beam. The camera image calibration and scan area definition software were also based entirely on LabVIEW code. Presently, the main area of application of the newly constructed spectrometer is 2-dimensional mapping of element distribution in environmental, biological and geological samples with micrometer spatial resolution. The hardware and the developed software can already handle volumetric 3-D confocal scans. In this work, a front panel graphical user interface as well as communication protocols between hardware components were described. Two applications of the spectrometer, to homogeneity testing of titanium layers and to imaging of various types of grains in air particulate matter collected on membrane filters, were presented. PMID:22483897

  19. Highly efficient beamline and spectrometer for inelastic soft X-ray scattering at high resolution.

    PubMed

    Lai, C H; Fung, H S; Wu, W B; Huang, H Y; Fu, H W; Lin, S W; Huang, S W; Chiu, C C; Wang, D J; Huang, L J; Tseng, T C; Chung, S C; Chen, C T; Huang, D J

    2014-03-01

    The design, construction and commissioning of a beamline and spectrometer for inelastic soft X-ray scattering at high resolution in a highly efficient system are presented. Based on the energy-compensation principle of grating dispersion, the design of the monochromator-spectrometer system greatly enhances the efficiency of measurement of inelastic soft X-rays scattering. Comprising two bendable gratings, the set-up effectively diminishes the defocus and coma aberrations. At commissioning, this system showed results of spin-flip, d-d and charge-transfer excitations of NiO. These results are consistent with published results but exhibit improved spectral resolution and increased efficiency of measurement. The best energy resolution of the set-up in terms of full width at half-maximum is 108 meV at an incident photon energy tuned about the Ni L3-edge. PMID:24562553

  20. X-ray rocking curve measurements of bent crystals. [used in High Resolution Spectrometer in Advanced X-ray Astrophysics Facility

    NASA Technical Reports Server (NTRS)

    Hakim, M. B.; Muney, W. S.; Fowler, W. B.; Woodgate, B. E.

    1988-01-01

    A three-crystal laboratory X-ray spectrometer is used to measure the Bragg reflection from concave cylindrically curved crystals to be used in the high-resolution X-ray spectrometer of the NASA Advanced X-ray Astrophysics Facility (AXAF). The first two crystals, in the dispersive (1.1) arrangement, select a narrow collimated monochromatic beam in the Cu K-alpha(1) line at 1.5 A (8.1 keV), which illuminates the test crystal. The angular centroids of rocking curves measured along the surface provide a measure of the conformity of the crystal to the desired radius of curvature. Individual and combined rocking-curve widths and areas provide a measure of the resolution and efficiency at 1.54 A. The crystals analyzed included LiF(200), PET, and acid phthalates such as TAP.

  1. A high resolution x-ray fluorescence spectrometer for near edge absorption studies

    SciTech Connect

    Stojanoff, V.; Hamalainen, K.; Siddons, D.P.; Hastings, J.B.; Berman, L.E.; Cramer, S.; Smith, G.

    1991-01-01

    A high resolution fluorescence spectrometer using a Johann geometry in a back scattering arrangement was developed. The spectrometer, with a resolution of 0.3 eV at 6.5 keV, combined with an incident beam, with a resolution of 0.7 eV, form the basis of a high resolution instrument for measuring x-ray absorption spectra. The advantages of the instrument are illustrated with the near edge absorption spectrum of dysprosium nitrate. 10 refs., 4 figs.

  2. A high resolution x-ray fluorescence spectrometer for near edge absorption studies

    SciTech Connect

    Stojanoff, V.; Hamalainen, K.; Siddons, D.P.; Hastings, J.B.; Berman, L.E.; Cramer, S.; Smith, G.

    1991-12-31

    A high resolution fluorescence spectrometer using a Johann geometry in a back scattering arrangement was developed. The spectrometer, with a resolution of 0.3 eV at 6.5 keV, combined with an incident beam, with a resolution of 0.7 eV, form the basis of a high resolution instrument for measuring x-ray absorption spectra. The advantages of the instrument are illustrated with the near edge absorption spectrum of dysprosium nitrate. 10 refs., 4 figs.

  3. An imaging spectrometer with a convex crystal for pulsed x rays in plasma experiments

    NASA Astrophysics Data System (ADS)

    Yanagidaira, Takeshi; Shimoda, Katsuji; Ono, Yasushi; Hirano, Katsumi

    2000-01-01

    An imaging spectrometer with a convex rubidium acid phthalate (RbAP) crystal is designed and examined. Using the ray tracing technique based on the kinematical theory of diffraction, resolution power, dispersion, linearity, spatial resolution and dynamic range of the monochromatic image are discussed. Broadening by a rocking curve is also taken into account. Performance of the spectrometer is successfully examined using the so-called hot spots as the soft x-ray source which are generated in the pinched plasma by the plasma focus facility with an additional gas puff.

  4. Laboratory studies on a spherically curved Bragg spectrometer for cosmic X-ray spectroscopy

    NASA Technical Reports Server (NTRS)

    Cantin, M.; Koch-Miramond, L.; Mougin, B.; Rocchia, R.

    1981-01-01

    A spherical array of twenty LiF 200 crystals was built to test the performances of a freestanding, self-focussing spherical crystal cosmic X-ray spectrometer. Measurements presently available show that the size of the image for a point source at infinite distance would be 3 mm (FWHM) along the focalisation axis and 2.1 mm (FWHM) along the dispersion axis. The mosaic spread on individual crystals is less than 0.1 degree. A slightly systematic deviation from the ideal bending (0.1 degree) is observed at the edges of most crystals and this appears to be the major limitation to spectrometer performance.

  5. Future Development Trajectories for Imaging X-rays Spectrometers Based on Microcalorimeters

    NASA Technical Reports Server (NTRS)

    Kilbourne, Caroline A.; Bandler, Simon R.

    2013-01-01

    Future development trajectories for imaging x-ray spectrometers based on microcalorimeters. Since their invention 30 years ago, the capability of X-ray microcalorimeters has increased steadily, with continual improvements in energy resolution, speed, and array size. Arrays of up to 1024 pixels have been produced, and resolution better than 1 eV at 1.5 keV has been achieved. These detectors can be optimized for the highest priority science, such as designing for the highest resolving power at low energies at the expense of dynamic range, or the greatest focal-plane coverage at the expense of speed. Three types of X-ray microcalorimeters presently dominate the field, each characterized by the thermometer technology. The first two types use temperature-sensitive resistors: semiconductors in the metal-insulator transition and superconductors operated in the superconducting-normal transition. The third type uses a magnetically coupled thermometer, and is at an earlier stage of development than the other two. The Soft X-ray Spectrometer (SXS) on Astro-H, expected to launch in 2015, will use an array of silicon thermistors with HgTe X-ray absorbers that will operate at 50 mK. Both the semiconductor and superconductor calorimeters have been implemented in small arrays. Kilopixel arrays of the superconducting calorimeters are being produced, and much larger arrays may require the non-dissipative advantage of magnetically coupled thermometers. I will project the development trajectories of these detectors and their read-out technologies and assess what their capabilities and limitations will be 10 - 20 years from now.

  6. Energy resolution and high count rate performance of superconducting tunnel junction x-ray spectrometers

    SciTech Connect

    Frank, M.; Hiller, L.J.; le Grand, J.B.; Mears, C.A.; Labov, S.E.; Lindeman, M.A.; Netel, H.; Chow, D.; Barfknecht, A.

    1998-01-01

    We present experimental results obtained with a cryogenically cooled, high-resolution x-ray spectrometer based on a 141{mu}m{times}141{mu}m Nb-Al-Al{sub 2}O{sub 3}-Al-Nb superconducting tunnel junction (STJ) detector in a demonstration experiment. Using monochromatized synchrotron radiation we studied the energy resolution of this energy-dispersive spectrometer for soft x rays with energies between 70 and 700 eV and investigated its performance at count rates up to nearly 60000 cps. At count rates of several 100 cps we achieved an energy resolution of 5.9 eV (FWHM) and an electronic noise of 4.5 eV for 277 eV x rays (the energy corresponding to C K). Increasing the count rate, the resolution 277 eV remained below 10 eV for count rates up to {approximately}10000cps and then degraded to 13 eV at 23000 cps and 20 eV at 50000 cps. These results were achieved using a commercially available spectroscopy amplifier with a baseline restorer. No pile-up rejection was applied in these measurements. Our results show that STJ detectors can operate at count rates approaching those of semiconductor detectors while still providing a significantly better energy resolution for soft x rays. Thus STJ detectors may prove very useful in microanalysis, synchrotron x-ray fluorescence (XRF) applications, and XRF analysis of light elements (K lines) and transition elements (L lines). {copyright} {ital 1998 American Institute of Physics.}

  7. High energy resolution x-ray spectrometer for high count rate XRF applications

    SciTech Connect

    Rossington, C.S.; Madden, N.W.; Chapman, K.

    1993-08-01

    A new x-ray spectrometer has been constructed which incorporates a novel large area, low capacitance Si(Li) detector and a low noise JFET (junction field effect transistor) pr- eamplifier. The spectrometer operates at high count rates without the conventional compromise in energy resolution. For example, at an amplifier peaking time of 1 {mu}sec and a throughput count rate of 145,000 counts sec{sup {minus}1}, the energy resolution at 5.9 key is 220 eV FWHM. Commercially available spectrometers utilizing conventional geometry Si(Li) detectors with areas equivalent to the new detector have resolutions on the order of 540 eV under the same conditions. Conventional x-ray spectrometers offering high energy resolution must employ detectors with areas one-tenth the size of the new LBL detector (20 mm{sup 2} compared with 200 mm{sup 2}). However, even with the use of the smaller area detectors, the energy resolution of a commercial system is typically limited to approximately 300 eV (again, at 1 {mu}sec and 5.9 keV) due to the noise of the commercially available JFET`S. The new large area detector is useful in high count rate applications, but is also useful in the detection of weak photon signals, in which it is desirable to subtend as large an angle of the available photon flux as possible, while still maintaining excellent energy resolution. X-ray fluorescence data from the new spectrometer is shown in comparison to a commercially available system in the analysis of a dilute multi-element material, and also in conjunction with high count rate synchrotron EXAMS applications.

  8. CALIBRATION STANDARDS FOR X-RAY SPECTROMETERS USED FOR POLLUTION SAMPLE ANALYSIS

    EPA Science Inventory

    A technique is described for making aerosol standards for x-ray fluorescence analysis by depositing sized particles suspended in a carrier solution onto the surface of a polycarbonate filter. Size is controlled by a separate sedimentation step following grinding in a boron carbid...

  9. POLYMER FILM STANDARDS FOR X-RAY FLUORESCENCE SPECTROMETERS (JOURNAL VERSION)

    EPA Science Inventory

    Sets of thin polymer films were developed to serve as standards for XRF analysis of the following 18 elements in aerosol particle samples: Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ge, As, Rb, Sr, Zr, Cd, Sb, Ba, and Pb. Each film contains a pair of elements having non-interfering x-ray...

  10. Ground calibrations of the X-ray detector system of the Solar Intensity X-ray Spectrometer (SIXS) on board BepiColombo

    NASA Astrophysics Data System (ADS)

    Huovelin, Juhani; Lehtolainen, Arto; Genzer, Maria; Korpela, Seppo; Esko, Eero; Andersson, Hans

    2014-05-01

    SIXS includes X-ray and particle detector systems for the BepiColombo Mercury Planetary Orbiter (MPO). Its task is to monitor the direct solar X-rays and energetic particles in a wide field of view in the energy range of 1-20 keV (X-rays), 0.1-3 MeV (electrons) and 1-30 MeV (protons). The main purpose of these measurements is to provide quantitative information on the high energy radiation incident on Mercury's surface which causes the X-ray glow of the planet measured by the MIXS instrument. The X-ray and particle measurements of SIXS are also useful for investigations of the solar corona and the magnetosphere of Mercury. The ground calibrations of the X-ray detectors of the SIXS flight model were carried out in the X-ray laboratory of the Helsinki University during May and June 2012. The aim of the ground calibrations was to characterize the performance of the SIXS instrument's three High-Purity Silicon PIN X-ray detectors and verify that they fulfil their scientific performance requirements. The calibrations included the determination of the beginning of life energy resolution at different operational temperatures, determination of the detector's sensitivity within the field of view as a function of the off-axis and roll angles, pile-up tests for determining the speed of the read out electronics, measurements of the low energy threshold of the energy scale, a cross-calibration with the SMART-1 XSM flight spare detector, and the determination of the temperature dependence of the energy scale. An X-ray tube and the detectors' internal Ti coated 55Fe calibration sources were used as primary X-ray sources. In addition, two external fluorescence sources were used as secondary X-ray sources in the determination of the energy resolutions and in the comparison calibration with the SMART-1 XSM. The calibration results show that the detectors fulfill all of the scientific performance requirements. The ground calibration data combined with the instrument house-keeping data

  11. Modeling the expected performance of the REgolith X-ray Imaging Spectrometer (REXIS)

    NASA Astrophysics Data System (ADS)

    Inamdar, Niraj K.; Binzel, Richard P.; Hong, Jae Sub; Allen, Branden; Grindlay, Jonathan; Masterson, Rebecca A.

    2014-09-01

    OSIRIS-REx is the third spacecraft in the NASA New Frontiers Program and is planned for launch in 2016. OSIRIS-REx will orbit the near-Earth asteroid (101955) Bennu, characterize it, and return a sample of the asteroid's regolith back to Earth. The Regolith X-ray Imaging Spectrometer (REXIS) is an instrument on OSIRIS-REx designed and built by students at MIT and Harvard. The purpose of REXIS is to collect and image sun-induced fluorescent X-rays emitted by Bennu, thereby providing spectroscopic information related to the elemental makeup of the asteroid regolith and the distribution of features over its surface. Telescopic reflectance spectra suggest a CI or CM chondrite analog meteorite class for Bennu, where this primitive nature strongly motivates its study. A number of factors, however, will influence the generation, measurement, and interpretation of the X-ray spectra measured by REXIS. These include: the compositional nature and heterogeneity of Bennu, the time-variable solar state, X-ray detector characteristics, and geometric parameters for the observations. In this paper, we will explore how these variables influence the precision to which REXIS can measure Bennu's surface composition. By modeling the aforementioned factors, we place bounds on the expected performance of REXIS and its ability to ultimately place Bennu in an analog meteorite class.

  12. The High-Resolution X-Ray Microcalorimeter Spectrometer, SXS, on Astro-H

    NASA Technical Reports Server (NTRS)

    Mitsuda, Kazuhisa; Kelley, Richard L.; Boyce, Kevin R.; Brown, Gregory V.; Costantini, Elisa; DiPirro, Michael J.; Ezoe, Yuichiro; Fujimoto, Ryuichi; Gendreau, Keith C.; denHerder, Jan-Willem; Hoshino, Akio; Ishisaki, Yoshitaka; Kilbourne, Caroline A.; Kitamoto, Shunji; McCammon, Dan; Murakami, Masahide; Murakami, Hiroshi; Ogawa, Mina; Ohashi, Takaya; Okamoto, Atsushi; Paltani, Stephane; Pohl, Martin; Porter, F. Scott; Sato, Yoichi; Shinozaki, Keisuke

    2012-01-01

    The science and an overview of the Soft X-ray Spectrometer onboard the STRO-H mission are presented. The SXS consists of X-ray focusing mirrors and a microcalorimeter array and is developed by international collaboration lead by JAXA and NASA with European participation. The detector is a 6 x 6 format microcalorimeter array operated at a cryogenic temperature of 50 mK and covers a 3' x 3' field of view of the X-ray telescope of 5.6 m focal length. We expect an energy resolution better than 7 eV (FWHM, requirement) with a goal of 4 eV. The effective area of the instrument will be 225 square centimeters at 7 keV; by a factor of about two larger than that of the X-ray microcalorimeter on board Suzaku. One of the main scientific objectives of the SXS is to investigate turbulent and/or macroscopic motions of hot gas in clusters of galaxies.

  13. The High-Resolution X-Ray Microcalorimeter Spectrometer, SXS, on Astro-H

    NASA Astrophysics Data System (ADS)

    Mitsuda, Kazuhisa; Kelley, Richard L.; Boyce, Kevin R.; Brown, Gregory V.; Costantini, Elisa; DiPirro, Michael J.; Ezoe, Yuichiro; Fujimoto, Ryuichi; Gendreau, Keith C.; den Herder, Jan-Willem; Hoshino, Akio; Ishisaki, Yoshitaka; Kilbourne, Caroline A.; Kitamoto, Shunji; McCammon, Dan; Murakami, Masahide; Murakami, Hiroshi; Ogawa, Mina; Ohashi, Takaya; Okamoto, Atsushi; Paltani, Stéphane; Pohl, Martin; Porter, F. Scott; Sato, Yoichi; Shinozaki, Keisuke; Shirron, Peter J.; Sneiderman, Gary A.; Sugita, Hiroyuki; Szymkowiak, Andrew; Takei, Yoh; Tamagawa, Toru; Tashiro, Makoto; Terada, Yukikatsu; Tsujimoto, Masahiro; de Vries, Cor; Yamasaki, Noriko Y.

    2012-06-01

    The science and an overview of the Soft X-ray Spectrometer onboard the STRO-H mission are presented. The SXS consists of X-ray focusing mirrors and a microcalorimeter array and is developed by international collaboration lead by JAXA and NASA with European participation. The detector is a 6×6 format microcalorimeter array operated at a cryogenic temperature of 50 mK and covers a 3'×3' field of view of the X-ray telescope of 5.6 m focal length. We expect an energy resolution better than 7 eV (FWHM, requirement) with a goal of 4 eV. The effective area of the instrument will be 225 cm2 at 7 keV; by a factor of about two larger than that of the X-ray microcalorimeter on board Suzaku. One of the main scientific objectives of the SXS is to investigate turbulent and/or macroscopic motions of hot gas in clusters of galaxies.

  14. Calibration sources for the soft x-ray spectrometer instrument on ASTRO-H

    NASA Astrophysics Data System (ADS)

    de Vries, C. P.; Lowes, P.; den Herder, J. W.; Aarts, H.; Haas, D.; Mitsuda, K.; Yamasaki, N. Y.; Kelley, R.; Kilbourne, C.; Gendreau, K.

    2012-09-01

    The SXS instrument is the Soft X-ray micro-calorimeter Spectrometer planned for the Japanese ASTRO-H satellite, scheduled to be launched in 2014. In this paper we describe the X-ray calibration sources used in this instrument. These sources use light sensitive photo-cathodes to generate electrons, which in turn generate the X-rays. This design has the unique property to allow for fast discrete pulsations of the generated X-rays. This enables the energy scale calibration of the instrument simultaneously with astronomical observations, without adding to the background in the astronomical data. Flight-model sources have been made, and a number of them have been operating in the past several months to monitor their behaviour. Here we report on the characterisation and performance of these sources. In addition, we will elaborate on the nature and expected accuracy of the energy calibration, in relation to the expected stability of the instrument, given the calibration source strength and its mode of operation.

  15. Future lunar mission Active X-ray Spectrometer development: Surface roughness and geometry studies

    NASA Astrophysics Data System (ADS)

    Naito, M.; Hasebe, N.; Kusano, H.; Nagaoka, H.; Kuwako, M.; Oyama, Y.; Shibamura, E.; Amano, Y.; Ohta, T.; Kim, K. J.; Lopes, J. A. M.

    2015-07-01

    The Active X-ray Spectrometer (AXS) is considered as one of the scientific payload candidates for a future Japanese mission, SELENE-2. The AXS consists of pyroelectric X-ray generators and a Silicon Drift Detector to conduct X-Ray Fluorescence spectroscopy (XRF) on the Moon to measure major elements: Mg, Al, Si, Ca, Ti, and Fe; minor elements: Na, K, P, S, Cr and Mn; and the trace element Ni depending on their concentration. Some factors such as roughness, grain size and porosity of sample, and the geometry of X-ray incidence, emission and energy will affect the XRF measurements precision. Basic studies on the XRF are required to develop the AXS. In this study, fused samples were used to make homogeneous samples free from the effect of grain size and porosity. Experimental and numerical studies on the XRF were conducted to evaluate the effects from incidence and emission angles and surface roughness. Angle geometry and surface roughness will be optimized for the design of the AXS on future missions from the results of the experiment and the numerical simulation.

  16. Design Study of an X-ray Crystal Spectrometer for the HANBIT Mirror Machine

    NASA Astrophysics Data System (ADS)

    Lee, S. G.; Hwang, S. M.; Bitter, M. L.

    1997-11-01

    X-ray crystal spectroscopy is expected to play a major role for the diagnostics of the reactor-like plasmas produced in future large tokamaks, such as KSTAR and ITER. However, it is also desirable to extend the observable spectral range to longer wavelengths (7-15 dotA), which is of interest for the diagnostics of plasmas with much lower electron densities (10^11-10^12 cm-3) and electron temperatures (100 - 200 eV) in other magnetic-confinement experiments, such as the HANBIT mirror machine. The construction of crystal spectrometers for this wavelength range and these plasma conditions is challenging because of the low X-ray emissivity and the fact that the low-energy X-rays are strongly attenuated by even very thin foils or windows. New types of detectors other than the presently used multi-wire proportional counters are therefore needed to obtain a high detection efficiency. In this paper, we present a design study for a vacuum spectrometer with a CCD array detector and detailed estimates of the instrument performance for the observation of spectra from O, Ne and Al ions.

  17. The spectrometer telescope for imaging X-rays (STIX) on board Solar Orbiter

    NASA Astrophysics Data System (ADS)

    Vilmer, Nicole; Krucker, Samuel; Karol Seweryn, D..; Orleanski, Piotr; Limousin, Olivier; Meuris, Aline; Brun, Allan Sacha; Grimm, Oliver; Groebelbauer, HansPeter; Rendtel, J.

    The Spectrometer Telescope for Imaging X-rays (STIX) is one of 10 instruments on board Solar Orbiter, a confirmed M-class mission of the European Space Agency (ESA) within the Cosmic Vision program scheduled to be launched in 2017. STIX applies a Fourier-imaging technique using a set of tungsten grids (at pitches from 0.038 to 1 mm) in front of 32 pixelized CdTe detectors to provide imaging spectroscopy of solar thermal and non-thermal hard X-ray emissions from 4 to 150 keV. The paper presents the status of the instrument for the Critical Design Review to be held with ESA in June 2014. Particular emphasis is given to the CdTe hybrid detector called Caliste-SO for high resolution hard X-ray spectroscopy from 4 to 150 keV: Characterizations of the first production batch are reported. Caliste-SO spectrometer units could also fulfill the needs for the SORENTO instrument of the Russian Interhelioprobe mission currently in assessment study.

  18. ComIXS on BACH: a compact soft x-ray spectrometer operating at Elettra

    SciTech Connect

    Cocco, Daniele; Matteucci, Maurizio; Zangrando, Marco; Bondino, Federica; Zacchigna, Michele; Plate, Mauro; Parmigiani, Fulvio; Nelles, Bruno; Prince, Kevin C.

    2004-05-12

    To accommodate increasing interest in soft x-ray inelastic scattering, a new spectrometer has been designed, constructed and commissioned at Elettra. This instrument uses as the dispersive element one of two interchangeable Variable Line Spacing (VLS) spherical gratings. The energy scan is performed by a 7 cm linear translation of a back illuminated CCD which also collects the zero order light, facilitating alignment and calibration. The two gratings have the same radius of curvature while the groove densities and the groove density variations differ by a factor four. Thus the energies focused by the gratings at a particular position differ by a factor of four. The total length of the instrument is 60 cm, the energy range covered is roughly 25-1000 eV and the expected resolving power ranges from 1000 to 5000. The spectrometer is now operating on the beamline Bach. It takes advantage of the small size of the photon spot in the experimental chamber and of the possibility to control the polarization of the incoming radiation. The small spot constitutes the virtual entrance slit, and the spectrometer collects the photons emitted in a solid angle of about 30x10 mrad2. The instrument, named ComIXS (Compact Inelastic X-ray Spectrometer), has been routinely operating since October 2002. Several experiments have already been carried out, and some results illustrating the characteristics of the instrument are described. The manufacture and testing of the blaze gratings are also discussed.

  19. ComIXS on BACH: a compact soft x-ray spectrometer operating at Elettra

    NASA Astrophysics Data System (ADS)

    Cocco, Daniele; Zangrando, Marco; Matteucci, Maurizio; Bondino, Federica; Platè, Mauro; Zacchigna, Michele; Parmigiani, Fulvio; Nelles, Bruno; Prince, Kevin C.

    2004-05-01

    To accommodate increasing interest in soft x-ray inelastic scattering, a new spectrometer has been designed, constructed and commissioned at Elettra. This instrument uses as the dispersive element one of two interchangeable Variable Line Spacing (VLS) spherical gratings. The energy scan is performed by a 7 cm linear translation of a back illuminated CCD which also collects the zero order light, facilitating alignment and calibration. The two gratings have the same radius of curvature while the groove densities and the groove density variations differ by a factor four. Thus the energies focused by the gratings at a particular position differ by a factor of four. The total length of the instrument is 60 cm, the energy range covered is roughly 25-1000 eV and the expected resolving power ranges from 1000 to 5000. The spectrometer is now operating on the beamline Bach. It takes advantage of the small size of the photon spot in the experimental chamber and of the possibility to control the polarization of the incoming radiation. The small spot constitutes the virtual entrance slit, and the spectrometer collects the photons emitted in a solid angle of about 30×10 mrad2. The instrument, named ComIXS (Compact Inelastic X-ray Spectrometer), has been routinely operating since October 2002. Several experiments have already been carried out, and some results illustrating the characteristics of the instrument are described. The manufacture and testing of the blaze gratings are also discussed.

  20. Soft x-ray blazed transmission grating spectrometer with high resolving power and extended bandpass

    NASA Astrophysics Data System (ADS)

    Heilmann, Ralf K.; Bruccoleri, Alexander Robert; Schattenburg, Mark

    2016-04-01

    A number of high priority questions in astrophysics can be addressed by a state-of-the-art soft x-ray grating spectrometer, such as the role of Active Galactic Nuclei in galaxy and star formation, characterization of the Warm-Hot Intergalactic Medium and the “missing baryon” problem, characterization of halos around the Milky Way and nearby galaxies, as well as stellar coronae and surrounding winds and disks. An Explorer-scale, large-area (> 1,000 cm2), high resolving power (R = λ/Δλ > 3,000) soft x-ray grating spectrometer is highly feasible based on Critical-Angle Transmission (CAT) grating technology. Still significantly higher performance can be provided by a CAT grating spectrometer on an X-ray-Surveyor-type mission. CAT gratings combine the advantages of blazed reflection gratings (high efficiency, use of higher diffraction orders) with those of conventional transmission gratings (low mass, relaxed alignment tolerances and temperature requirements, transparent at higher energies) with minimal mission resource requirements. They are high-efficiency blazed transmission gratings that consist of freestanding, ultra-high aspect-ratio grating bars fabricated from silicon-on-insulator (SOI) wafers using advanced anisotropic dry and wet etch techniques. Blazing is achieved through grazing-incidence reflection off the smooth grating bar sidewalls. The reflection properties of silicon are well matched to the soft x-ray band. Nevertheless, CAT gratings with sidewalls made of higher atomic number elements allow extension of the CAT grating principle to higher energies and larger dispersion angles. We show x-ray data from metal-coated CAT gratings and demonstrate efficient blazing to higher energies and larger blaze angles than possible with silicon alone. We also report on measurements of the resolving power of a breadboard CAT grating spectrometer consisting of a Wolter-I slumped-glass focusing mirror pair from Goddard Space Flight Center and CAT gratings, to be

  1. Is Asteroid 433 Eros Compositionally Homogeneous? New Analyses of NEAR-Shoemaker X-Ray Spectrometer Data

    NASA Technical Reports Server (NTRS)

    Nittler, L. R.; Trombka, J. I.

    2001-01-01

    We present new analysis techniques for NEAR-Shomaker X-ray spectrometer data to infer the compositional heterogeneity of asteroid 433 Eros. Preliminary results indicate a largely chondritic, homogeneous composition. Additional information is contained in the original extended abstract.

  2. Development of soft X-ray emission spectrometer for EPMA/SEM and its application

    NASA Astrophysics Data System (ADS)

    Takahashi, H.; Murano, T.; Takakura, M.; Asahina, S.; Terauchi, M.; Koike, M.; Imazono, T.; Koeda, M.; Nagano, T.

    2016-02-01

    A newly developed wavelength-dispersive soft X-ray emission spectrometer (WD-SXES) with two kinds of gratings, JS50XL and JS200N, were installed on electron probe microanalysers (EPMA) and scanning electron microscopes (SEM). The new detector covers the energy range from 50 to 210 eV with an energy resolution of better than 0.2 eV at Al-L emission on Al metal. With this low energy range and high energy resolution, various kinds of X-ray lines of K, L, M, N emission spectra from lithium to uranium could be observed and chemical state analysis carried out. This WD-SXES has also a high potential for analysing trace light elements under 100 ppm. The design, having no mechanically scanning components, allows parallel spectral acquisition over the entire energy range of each grating (50 to 170 eV and 70 to 210 eV).

  3. A soft x-ray transmission grating imaging-spectrometer for the National Ignition Facility

    NASA Astrophysics Data System (ADS)

    Moore, A. S.; Guymer, T. M.; Kline, J. L.; Morton, J.; Taccetti, M.; Lanier, N. E.; Bentley, C.; Workman, J.; Peterson, B.; Mussack, K.; Cowan, J.; Prasad, R.; Richardson, M.; Burns, S.; Kalantar, D. H.; Benedetti, L. R.; Bell, P.; Bradley, D.; Hsing, W.; Stevenson, M.

    2012-10-01

    A soft x-ray transmission grating spectrometer has been designed for use on high energy-density physics experiments at the National Ignition Facility (NIF); coupled to one of the NIF gated x-ray detectors it records 16 time-gated spectra between 250 and 1000 eV with 100 ps temporal resolution. The trade-off between spectral and spatial resolution leads to an optimized design for measurement of emission around the peak of a 100-300 eV blackbody spectrum. Performance qualification results from the NIF, the Trident Laser Facility and vacuum ultraviolet beamline at the National Synchrotron Light Source, evidence a <100 μm spatial resolution in combination with a source-size limited spectral resolution that is <10 eV at photon energies of 300 eV.

  4. A soft x-ray transmission grating imaging-spectrometer for the National Ignition Facility.

    PubMed

    Moore, A S; Guymer, T M; Kline, J L; Morton, J; Taccetti, M; Lanier, N E; Bentley, C; Workman, J; Peterson, B; Mussack, K; Cowan, J; Prasad, R; Richardson, M; Burns, S; Kalantar, D H; Benedetti, L R; Bell, P; Bradley, D; Hsing, W; Stevenson, M

    2012-10-01

    A soft x-ray transmission grating spectrometer has been designed for use on high energy-density physics experiments at the National Ignition Facility (NIF); coupled to one of the NIF gated x-ray detectors it records 16 time-gated spectra between 250 and 1000 eV with 100 ps temporal resolution. The trade-off between spectral and spatial resolution leads to an optimized design for measurement of emission around the peak of a 100-300 eV blackbody spectrum. Performance qualification results from the NIF, the Trident Laser Facility and vacuum ultraviolet beamline at the National Synchrotron Light Source, evidence a <100 μm spatial resolution in combination with a source-size limited spectral resolution that is <10 eV at photon energies of 300 eV. PMID:23126953

  5. Use of mercuric iodide X-ray detectors with alpha backscattering spectrometers for space applications

    NASA Technical Reports Server (NTRS)

    Iwanczyk, J. S.; Wang, Y. J.; Dorri, N.; Dabrowski, A. J.; Economou, T. E.

    1991-01-01

    The authors present X-ray fluorescence (XRF) spectra of different extraterrestrial samples taken with a mercuric iodide (HgI2) spectrometer inserted into an alpha backscattering instrument identical to that used in the Soviet Phobos mission. The results obtained with the HgI2 ambient temperature detector are compared with those obtained using an Si(Li) cryogenically cooled detector. Efforts to design an optimized instrument for space application are also described. The results presented indicate that the energy resolution and sensitivity of HgI2 detectors are adequate to meet the performance needs of a number of proposed space applications, particularly those in which cooled silicon X-ray detectors are impractical or even not usable, such as for the target science programs on geoscience opportunities for lunar surface, Mars surface, and other comet and planetary missions being planned by NASA and ESA.

  6. The spectrometer telescope for imaging x-rays on board the Solar Orbiter mission

    NASA Astrophysics Data System (ADS)

    Benz, A. O.; Krucker, S.; Hurford, G. J.; Arnold, N. G.; Orleanski, P.; Gröbelbauer, H.-P.; Klober, S.; Iseli, L.; Wiehl, H. J.; Csillaghy, A.; Etesi, L.; Hochmuth, N.; Battaglia, M.; Bednarzik, M.; Resanovic, R.; Grimm, O.; Viertel, G.; Commichau, V.; Meuris, A.; Limousin, O.; Brun, S.; Vilmer, N.; Skup, K. R.; Graczyk, R.; Stolarski, M.; Michalska, M.; Nowosielski, W.; Cichocki, A.; Mosdorf, M.; Seweryn, K.; Przepiórka, A.; Sylwester, J.; Kowalinski, M.; Mrozek, T.; Podgorski, P.; Mann, G.; Aurass, H.; Popow, E.; Onel, H.; Dionies, F.; Bauer, S.; Rendtel, J.; Warmuth, A.; Woche, M.; Plüschke, D.; Bittner, W.; Paschke, J.; Wolker, D.; Van Beek, H. F.; Farnik, F.; Kasparova, J.; Veronig, A. M.; Kienreich, I. W.; Gallagher, P. T.; Bloomfield, D. S.; Piana, M.; Massone, A. M.; Dennis, B. R.; Schwarz, R. A.; Lin, R. P.

    2012-09-01

    The Spectrometer Telescope for Imaging X-rays (STIX) is one of 10 instruments on board Solar Orbiter, a confirmed Mclass mission of the European Space Agency (ESA) within the Cosmic Vision program scheduled to be launched in 2017. STIX applies a Fourier-imaging technique using a set of tungsten grids (at pitches from 0.038 to 1 mm) in front of 32 pixelized CdTe detectors to provide imaging spectroscopy of solar thermal and non-thermal hard X-ray emissions from 4 to 150 keV. The status of the instrument reviewed in this paper is based on the design that passed the Preliminary Design Review (PDR) in early 2012. Particular emphasis is given to the first light of the detector system called Caliste-SO.

  7. Balloon-Borne Hard X-Ray Spectrometer Using CdTe Detectors

    NASA Astrophysics Data System (ADS)

    Kobayashi, K.; Tsuneta, S.; Tamura, T.; Kumagai, K.; Katsukawa, Y.; Kubo, M.; Sakamoto, Y.; Kohara, N.; Yamagami, T.; Saito, Y.; Mori, K.

    2008-08-01

    Spectroscopic observation of solar flares in the hard X-ray energy range, particularly the 20 ˜ 100 keV region, is an invaluable tool for investigating the flare mechanism. This paper describes the design and performance of a balloon-borne hard X-ray spectrometer using CdTe detectors developed for solar flare observation. The instrument is a small balloon payload (gondola weight 70 kg) with sixteen 10×10×0.5 mm CdTe detectors, designed for a 1-day flight at 41 km altitude. It observes in an energy range of 20-120 keV and has an energy resolution of 3 keV at 60 keV. The second flight on 24 May 2002 succeeded in observing a class M1.1 flare.

  8. A soft x-ray transmission grating imaging-spectrometer for the National Ignition Facility

    SciTech Connect

    Moore, A S; Guymer, T M; Kline, J L; Morton, J; Taccetti, M; Lanier, N E; Bentley, C; Workman, J; Peterson, B; Mussack, K; Cowan, J; Prasad, R; Richardson, M; Burns, S; Kalantar, D H; Benedetti, L R; Bell, P; Bradley, D; Hsing, W; Stevenson, M

    2012-05-01

    A soft x-ray transmission grating spectrometer has been designed for use on high energy-density physics experiments at the National Ignition Facility (NIF); coupled to one of the NIF gated x-ray detectors (GXD) it records sixteen time-gated spectra between 250 and 1000eV with 100ps temporal resolution. The trade-off between spectral and spatial resolution leads to an optimized design for measurement of emission around the peak of a 100-300eV blackbody spectrum. Performance qualification results from the NIF, the Trident Laser Facility and VUV beamline at the National Synchrotron Light Source (NSLS), evidence a <100{micro}m spatial resolution in combination with a source-size limited spectral resolution that is <10eV at photon energies of 300eV.

  9. The hard X-ray burst spectrometer on the solar maximum mission

    NASA Technical Reports Server (NTRS)

    Orwig, L. E.; Frost, K. J.; Dennis, B. R.

    1979-01-01

    The primary scientific objective of the spectrometer is to provide a greater understanding of the role of energetic electrons in solar flares. This will be achieved by observations of high energy X-rays in the energy range from 20 to 200 keV with time resolution of 0.128s on a continuous basis and as short as 1 ms for limited intervals. The X-ray detector is an actively shielded CsI(Na) crystal with a thickness of 0.635 cm and a sensitive area of 71 sq cm. In the first year after launch, it is expected that approximately 1000 flares above the sensitivity threshold of 0.2 photons/(sq cm s) lasting for one second, will be detected.

  10. A Versatile Medium-Resolution X-ray Emission Spectrometer for Diamond Anvil Cell Applications

    SciTech Connect

    Mortensen, Devon R.; Seidler, G. T.; Bradley, J. A.; Lipp, M. J.; Evans, W. J.; Chow, P.; Xiao, Y. M.; Boman, G.; Bowden, Mark E.

    2013-08-28

    We present design and performance details for a polycapillary-coupled x-ray spectrometer that provides very high collection efficiency at a moderate energy resolution suitable for many studies of nonresonant x-ray emission spectroscopy, especially for samples of heavy elements under high pressures. Using a single Bragg analyzer operating close to a backscattering so as to minimize the effect of the weak divergence of the quasicollimated exit beam from the polycapillary optic, this instrument can maintain a typical energy resolution of 5 eV over photon energies from 5 keV to 10 keV. We find dramatically improved count rates as compared to a traditional higher-resolution instrument based on a single spherically-bent crystal analyzer.

  11. A versatile medium-resolution x-ray emission spectrometer for diamond anvil cell applications

    SciTech Connect

    Mortensen, D. R.; Seidler, G. T.; Bradley, J. A.; Lipp, M. J.; Evans, W. J.; Chow, P.; Xiao, Y.-M.; Boman, G.; Bowden, M. E.

    2013-08-15

    We present design and performance details for a polycapillary-coupled x-ray spectrometer that provides very high collection efficiency at a moderate energy resolution suitable for many studies of nonresonant x-ray emission spectroscopy, especially for samples of heavy elements under high pressures. Using a single Bragg analyzer operating close to backscattering geometry so as to minimize the effect of the weak divergence of the quasicollimated exit beam from the polycapillary optic, this instrument can maintain a typical energy resolution of 5 eV over photon energies from 5 keV to 10 keV. We find dramatically improved count rates as compared to a traditional higher-resolution instrument based on a single spherically bent crystal analyzer.

  12. A single-shot transmissive spectrometer for hard x-ray free electron lasers

    SciTech Connect

    Zhu Diling; Cammarata, Marco; Feldkamp, Jan M.; Fritz, David M.; Hastings, Jerome B.; Lee, Sooheyong; Lemke, Henrik T.; Robert, Aymeric; Turner, James L.; Feng Yiping

    2012-07-16

    We report hard x-ray single-shot spectral measurements of the Linac Coherent Light Source. The spectrometer is based on a 10 {mu}m thick cylindrically bent Si single crystal operating in the symmetric Bragg geometry to provide dispersion and high transmission simultaneously. It covers a spectral range >1% using the Si(111) reflection. Using the Si(333) reflection, it reaches a resolving power of better than 42 000 and transmits >83% of the incident flux at 8.3 keV. The high resolution enabled the observation of individual spectral spikes characteristic of a self-amplified spontaneous emission x-ray free electron laser source. Potential applications of the device are discussed.

  13. X-ray observations of MeV electron precipitation with a balloon-borne germanium spectrometer

    NASA Astrophysics Data System (ADS)

    Millan, Robyn Margaret

    The MAXIS (MeV Auroral X-ray Imaging and Spectroscopy) balloon payload was launched on a long duration balloon from McMurdo, Antarctica on Jan. 12, 2000. The high spectral resolution germanium spectrometer aboard MAXIS detected nine X-ray bursts with significant flux extending above 0.5 MeV during the 18 day flight. The X-rays are bremsstrahlung produced by precipitating electrons and the events are characterized by an extremely flat X-ray spectrum (˜E-2) similar to the first MeV event discovered in 1996, indicating relativistic parent electrons. The bursts were detected between magnetic latitudes 58°--68° (IGRF L-values of 3.8--6.7) with durations varying from several minutes to several hours and occurred only in the late afternoon/dusk sectors (14:30--00:00 MLT) while softer precipitation was detected at all magnetic local times. In addition, the MeV events were associated with substorm activity and several events showed Ultra Low Frequency (mHz) modulation of the X-ray count rate. Spacecraft and ground-based observations indicate the presence of ULF wave activity near the time and location of the events which may be causing the modulation by some mechanism that is not understood. The MeV events are well modeled by a very flat exponential precipitating electron distribution and the average flux of precipitating electrons with E ≥ 0.5 MeV is estimated to be ˜360 cm-2 s-1. This corresponds to about 5 x 1025 precipitated electrons in this latitude range during the eight day observing interval compared to ˜2 x 10 25 trapped 0.5--3.6 MeV electrons estimated using GPS electron measurements. The MAXIS observations indicate that these electron precipitation events are common and may be the primary loss mechanism for outer zone relativistic electrons. Individual events were also compared with measurements of the trapped electrons from which it is estimated that only a few percent of the loss cone is being filled by the mechanism acting to precipitate the particles

  14. Analysis and implementation of a space resolving spherical crystal spectrometer for x-ray Thomson scattering experiments

    SciTech Connect

    Harding, E. C.; Ao, T.; Bailey, J. E.; Loisel, G.; Sinars, D. B.; Geissel, M.; Rochau, G. A.; Smith, I. C.

    2015-04-15

    The application of a space-resolving spectrometer to X-ray Thomson Scattering (XRTS) experiments has the potential to advance the study of warm dense matter. This has motivated the design of a spherical crystal spectrometer, which is a doubly focusing geometry with an overall high sensitivity and the capability of providing high-resolution, space-resolved spectra. A detailed analysis of the image fluence and crystal throughput in this geometry is carried out and analytical estimates of these quantities are presented. This analysis informed the design of a new spectrometer intended for future XRTS experiments on the Z-machine. The new spectrometer collects 6 keV x-rays with a spherically bent Ge (422) crystal and focuses the collected x-rays onto the Rowland circle. The spectrometer was built and then tested with a foam target. The resulting high-quality spectra prove that a spherical spectrometer is a viable diagnostic for XRTS experiments.

  15. Analysis and implementation of a space resolving spherical crystal spectrometer for x-ray Thomson scattering experiments.

    PubMed

    Harding, E C; Ao, T; Bailey, J E; Loisel, G; Sinars, D B; Geissel, M; Rochau, G A; Smith, I C

    2015-04-01

    The application of a space-resolving spectrometer to X-ray Thomson Scattering (XRTS) experiments has the potential to advance the study of warm dense matter. This has motivated the design of a spherical crystal spectrometer, which is a doubly focusing geometry with an overall high sensitivity and the capability of providing high-resolution, space-resolved spectra. A detailed analysis of the image fluence and crystal throughput in this geometry is carried out and analytical estimates of these quantities are presented. This analysis informed the design of a new spectrometer intended for future XRTS experiments on the Z-machine. The new spectrometer collects 6 keV x-rays with a spherically bent Ge (422) crystal and focuses the collected x-rays onto the Rowland circle. The spectrometer was built and then tested with a foam target. The resulting high-quality spectra prove that a spherical spectrometer is a viable diagnostic for XRTS experiments. PMID:25933859

  16. Total reflection X-ray fluorescence spectrometers for multielement analysis: status of equipment

    NASA Astrophysics Data System (ADS)

    Ayala Jiménez, Rony E.

    2001-11-01

    Multielement analysis by total reflection X-ray fluorescence spectrometry has evolved during two decades. At present commercial equipment is available for chemical analysis of all types of biological and mineral samples. The electronic industry has also benefited from scientific and technological developments in this field due to new instrumentation to determine contamination on the surface of silicon wafers (the equipment will not be covered in this paper). The basic components of the spectrometers can be summarized as follows: (a) excitation source; (b) geometric arrangement (optics) for collimation and monochromatization of the primary radiation; (c) X-ray detector; and (d) software for operation of the instrument, data acquisition and spectral deconvolution to determine the concentrations of the elements (quantitative analysis). As an optional feature one manufacturer offers a conventional 45° geometry for direct excitation. Personal communications of the author and commercial brochures available have allowed us to list the components used in TXRF for multielement analysis. Excitation source: high-power sealed X-ray tubes, output from 1300 to 3000 W, different mixed alloy anodes Mo/W are used but molybdenum, tungsten and copper are common; single anode metal ceramic low power X-ray tubes, output up to 40 W. Excitation systems can be customized according to the requirements of the laboratory. Detector: silicon-lithium drifted semiconductor detector liquid nitrogen cooled; or silicon solid state thermoelectrically cooled detector (silicon drift detector SDD and silicon-PIN diode detector). Optics: multilayer monochromator of silicon-tungsten, nickel-carbon or double multilayer monochromator. Electronics: spectroscopy amplifier, analog to digital converter adapted to a PC compatible computer with software in a Windows environment for the whole operation of the spectrometer and for qualitative/quantitative analysis of samples are standard features in the

  17. Very high resolution soft x-ray spectrometer for an electron beam ion trap

    SciTech Connect

    Beiersdorfer, P.; Crespo Lopez-Urrutia, J.R.; Foerster, E.; Mahiri, J. |; Widmann, K.

    1997-01-01

    A very high resolution vacuum flat-crystal spectrometer was constructed for analyzing soft x rays emitted by an electron beam ion trap. The spectrometer was designed to operate at large Bragg angles ({theta}{le}85{degree}) in order to maximize the spectral dispersion and thus the resolving power. Using a quartz (100) crystal at a Bragg angle of 82{degree}, a measurement of the 2p{sub 1/2}, 2p{sub 3/2}{r_arrow}1s{sub 1/2} transitions in hydrogenic Mg{sup 11+} situated near 8.42 {Angstrom} was made. The nominal resolving power of the instrument was better than 30000 allowing us to infer the ion temperature (246{plus_minus}20 eV) from the observed line widths. A comparison with an existing flat-crystal spectrometer demonstrates the great improvement in resolving power achieved. {copyright} {ital 1997 American Institute of Physics.}

  18. Preliminary results from the soft x-ray crystal spectrometer on Alcator C-Mod

    SciTech Connect

    Ince-Cushman, A.; Rice, J. E.; Lee, S. G.; Bitter, M.; Reinke, M.; Podpaly, Y.

    2006-10-15

    A high resolution ({lambda}/{delta}{lambda}{approx}2000) soft x-ray spectrometer has been installed on the Alcator C-Mod tokamak. The system was designed to measure emission line spectra from heliumlike neon (1s{sup 1}2p{sup 1}{yields}1s{sup 2}) in a narrow spectral band centered on {lambda}=13.5 A (920 eV). The instrument is mounted with a poloidal view 20 cm below the midplane (r/a{approx}0.85). In addition to the neon emission lines, strong fluorine, xenon, iron, and manganese lines have been observed.

  19. Combined backscatter Moessbauer spectrometer/x ray fluorescence analyzer (BaMS/XRF) for extraterrestrial surfaces

    NASA Technical Reports Server (NTRS)

    Shelfer, T. D.; Wills, E. L.; Agresti, D. G.; Pimperl, M. M.; Shen, M. H.; Morris, R. V.; Nguyen, T.

    1993-01-01

    We have designed and tested a prototype combined backscatter Moessbauer spectrometer and x-ray fluorescence analyzer (BaMS/XRF). A space qualified instrument based on this design would be suitable for in-situ use on planetary missions to the surfaces of the Moon (Artemis and lunar outpost), Mars (MESUR), asteroids, or other solid solar system objects. The BaMS/XRF instrument is designed to be capable of concurrent sample analyses for the mineralogy of iron-bearing phases and elemental composition without the need for sample preparation.

  20. Abundance of Iron on Mercury's Surface from MESSENGER X-Ray Spectrometer Data

    NASA Astrophysics Data System (ADS)

    Weider, S. Z.; Nittler, L. R.; Starr, R. D.; Evans, L. G.; McCoy, T. J.; Solomon, S. C.

    2012-12-01

    Early orbital results from the MErcury Surface, Space ENvironment, GEochemistry, and Ranging (MESSENGER) X-Ray Spectrometer (XRS) revealed that Mercury's surface has a low Fe content. The reported Fe/Si ratios (~0.03 to 0.15) gave an upper limit of ~4 wt% Fe. This limit is consistent with the bulk estimate provided by the Gamma-Ray Spectrometer (Fe/Si: ~0.12) and the upper limit of ~6 wt % FeO in silicate minerals that is constrained by reflectance spectroscopy. Reliable Fe abundance estimates are difficult to obtain from XRS data for several reasons, including: (i) strong solar flares are required to excite Fe X-ray fluorescence, and such flares occur rarely; and (ii) energetic particle events often accompany the strongest solar flares, causing fluorescence of the instrument's Cu collimators and spectral contamination close to the Fe K lines at 6.4-7 keV. Forward modeling of XRS data from more than 30 flares during the first year of MESSENGER's orbit reveal that Fe is ubiquitously lower on Mercury (Fe/Si ranging from 0.02 to 0.18, with a peak in the distribution at ~0.06, or ~1.5 wt% Fe) than on other terrestrial planets. Although the abundance of Mg across the surface of Mercury is known to vary according to geological terrain, our data indicate that this variation is not a result of Fe substitution for Mg in mafic silicates. A correlation between Ca and S (and to a lesser extent between Mg and S) has previously been reported from the XRS data. Mercury's high S contents likely reflect the presence of abundant sulfide minerals, such as oldhamite (Ca,Mg,Fe)S. Our data reveal further correlations between Fe and Ca, and between Fe and Mg, suggesting that sulfides (most likely troilite, FeS, and/or oldhamite) are a major carrier of Fe on Mercury's surface. The low Fe content of Mercury's surface supports the very low FeO contents that are predicted from both melting experiments on enstatite chondrites and from thermodynamic modeling. However, even the few wt% Fe on

  1. Hard x-ray transmission crystal spectrometer at the OMEGA-EP laser facility

    SciTech Connect

    Seely, J. F.; Szabo, C. I.; Feldman, U.; Hudson, L. T.; Henins, A.; Audebert, P.; Brambrink, E.

    2010-10-15

    The transmission crystal spectrometer (TCS) is approved for taking data at the OMEGA-EP laser facility since 2009 and will be available for the OMEGA target chamber in 2010. TCS utilizes a Cauchois type cylindrically bent transmission crystal geometry with a source to crystal distance of 600 mm. Spectral images are recorded by image plates in four positions, one IP on the Rowland circle and three others at 200, 400, and 600 mm beyond the Rowland circle. An earlier version of TCS was used at LULI on experiments that determined the x-ray source size from spectral line broadening on one IP positioned behind the Rowland circle. TCS has recorded numerous backlighter spectra at EP for point projection radiography and for source size measurements. Hard x-ray source size can be determined from the source broadening of both K shell emission lines and from K absorption edges in the bremsstrahlung continuum, the latter being a new way to measure the spatial extent of the hard x-ray bremsstrahlung continuum.

  2. Dual x-ray fluorescence spectrometer and method for fluid analysis

    DOEpatents

    Wilson, Bary W.; Shepard, Chester L.

    2005-02-22

    Disclosed are an X-ray fluorescence (SRF) spectrometer and method for on-site and in-line determination of contaminant elements in lubricating oils and in fuel oils on board a marine vessel. An XRF source block 13 contains two radionuclide sources 16, 17 (e.g. Cd 109 and Fe 55), each oriented 180 degrees from the other to excite separate targets. The Cd 109 source 16 excites sample lube oil flowing through a low molecular weight sample line 18. The Fe 55 source 17 excites fuel oil manually presented to the source beam inside a low molecular weight vial 26 or other container. Two separate detectors A and B are arranged to detect the fluorescent x-rays from the targets, photons from the analyte atoms in the lube oil for example, and sulfur identifying x-rays from bunker fuel oil for example. The system allows both automated in-line and manual on-site analysis using one set of signal processing and multi-channel analyzer electronics 34, 37 as well as one computer 39 and user interface 43.

  3. Equation-of-State Measurements of Resorcinol Formaldehyde Foam Using Imaging X-Ray Thomson Spectrometer

    NASA Astrophysics Data System (ADS)

    Belancourt, Patrick; Theobald, W.; Keiter, P. A.; Collins, T. J. B.; Bonino, M. J.; Kozlowski, P.; Drake, R. P.

    2015-11-01

    Understanding the equation of state of materials under shocked conditions is important for laboratory astrophysics and high-energy-density physics experiments. This talk will focus on experiments dedicated to developing a platform for measuring the equation of state of shocked foams on OMEGA EP. The foam used in the development of this platform is resorcinol formaldehyde foam with an initial density of 0.34 g/cc. One OMEGA EP beam drives a shock into the foam, while the remaining three beams irradiate a nickel foil to create the x-ray backlighter. The primary diagnostic for this platform, the imaging x-ray Thomson spectrometer (IXTS), spectrally resolves the scattered x-ray beam while imaging in one spatial dimension. The IXTS is ideally suited to measure plasma conditions upstream, downstream and at the shock front in the foam. Preliminary results from these experiments will be shown. This material is based upon work supported by the Department of Energy National Nuclear Security Administration under Award Number DE-NA0001944, the NNSA-DS and SC-OFES Joint Program in High-Energy-Density Laboratory Plasmas DE-NA0001840, and by the National Laser User Facility Program DE-NA0000850.

  4. The High Resolution X-ray Spectrometer, SXS, on the Astro-H mission

    NASA Astrophysics Data System (ADS)

    Mitsuda, K.

    2009-09-01

    We will present the science and an overview of the the Soft X-ray Spectrometer onboard the Astro-H mission (formerly known as NeXT). The SXS consists of X-ray focussing mirrors and a microcalorimeter array and is developed by international collaboration lead by JAXA and NASA. The effective area of the instrument will be 290 cm^2 at 6 keV; by a factor of about two larger than that of the X-ray microcalorimeter on board Suzaku. The baseline detector is a 6x6 format array which covers a 2.8 x 2.8 arcmin^2 filed of view, while a larger format array of 8x8 format is being developed. We expect an energy resolution of 6 eV (FWHM) or better at 6 keV. One of the main scientific objectives of the SXS is to determine turbulent and/or macroscopic velocities in the hot gas of clusters of galaxies up to z ~ 1.

  5. Hard x-ray transmission crystal spectrometer at the OMEGA-EP laser facilitya)

    NASA Astrophysics Data System (ADS)

    Seely, J. F.; Szabo, C. I.; Feldman, U.; Hudson, L. T.; Henins, A.; Audebert, P.; Brambrink, E.

    2010-10-01

    The transmission crystal spectrometer (TCS) is approved for taking data at the OMEGA-EP laser facility since 2009 and will be available for the OMEGA target chamber in 2010. TCS utilizes a Cauchois type cylindrically bent transmission crystal geometry with a source to crystal distance of 600 mm. Spectral images are recorded by image plates in four positions, one IP on the Rowland circle and three others at 200, 400, and 600 mm beyond the Rowland circle. An earlier version of TCS was used at LULI on experiments that determined the x-ray source size from spectral line broadening on one IP positioned behind the Rowland circle. TCS has recorded numerous backlighter spectra at EP for point projection radiography and for source size measurements. Hard x-ray source size can be determined from the source broadening of both K shell emission lines and from K absorption edges in the bremsstrahlung continuum, the latter being a new way to measure the spatial extent of the hard x-ray bremsstrahlung continuum.

  6. Hard x-ray transmission crystal spectrometer at the OMEGA-EP laser facility.

    PubMed

    Seely, J F; Szabo, C I; Feldman, U; Hudson, L T; Henins, A; Audebert, P; Brambrink, E

    2010-10-01

    The transmission crystal spectrometer (TCS) is approved for taking data at the OMEGA-EP laser facility since 2009 and will be available for the OMEGA target chamber in 2010. TCS utilizes a Cauchois type cylindrically bent transmission crystal geometry with a source to crystal distance of 600 mm. Spectral images are recorded by image plates in four positions, one IP on the Rowland circle and three others at 200, 400, and 600 mm beyond the Rowland circle. An earlier version of TCS was used at LULI on experiments that determined the x-ray source size from spectral line broadening on one IP positioned behind the Rowland circle. TCS has recorded numerous backlighter spectra at EP for point projection radiography and for source size measurements. Hard x-ray source size can be determined from the source broadening of both K shell emission lines and from K absorption edges in the bremsstrahlung continuum, the latter being a new way to measure the spatial extent of the hard x-ray bremsstrahlung continuum. PMID:21034000

  7. Progress report on the Astro-H Soft X-Ray Spectrometer

    NASA Astrophysics Data System (ADS)

    Kelley, Richard L.; Mitsuda, Kazuhisa

    2016-04-01

    We describe the initial in-orbit operations and performance of the Astro-H Soft X-Ray Spectrometer (SXS). Astro-H, JAXA's sixth X-ray observatory, is scheduled for launch on February 12, 2016, from the Tanegashima Space Center in Japan abord an H-IIA rocket. The instrument is based on a 36-pixel array of microcalorimeters designed for high resolution over the 0.3-12 keV energy band at the focus of a high throughput, grazing-incidence x-ray mirror. The instrument is the result of a joint collaboration between the JAXA Institute of Space and Astronautical Science and many partners in Japan, and the NASA/Goddard Space Flight Center and collaborators in the US. The principal components of the spectrometer are the microcalorimeter detector system, a low-temperature anticoincidence detector, a 3-stage adiabatic demagnetization refrigerator (ADR) to maintain 50 mK operation under both cryogen and cryogen-free operation, a hybrid liquid helium/cryogen-free dewar with both Stirling and Joule-Thomson coolers, electronics for reading out the array, processing the x-ray data for spectroscopy, and operating the ADR and cryocoolers. The dewar is closed out by an aperture system with five thin-film filters designed to provide high x-ray transmission with low heat loads to the dewar and detector system, and prevent contamination from condensing on the filters. The instrument was designed to have better than 7 eV energy resolution, and was demonstrated to achieve 4-5 eV resolution across the array at the full spacecraft level of integration during extensive ground testing prior to launch. The overall cooling chain has been designed to provide a lifetime of at least 3 years in orbit, and continue to operate without liquid helium to provide redundancy and the longest operational lifetime for the instrument. In this presentation, we will describe the early phases of the SXS instrument in orbit and provide a sense of the astronomical results that can be expected. This presentation is

  8. Venus Measurements by the MESSENGER Gamma-Ray and X-Ray Spectrometers

    NASA Astrophysics Data System (ADS)

    Rhodes, E. A.; Starr, R. D.; Goldsten, J. O.; Schlemm, C. E.; Boynton, W. V.

    2007-12-01

    The Gamma-Ray Spectrometer (GRS), which is a part of the Gamma-Ray and Neutron Spectrometer Instrument, and the X-Ray Spectrometer (XRS) on the MESSENGER spacecraft made calibration measurements during the Venus flyby on June 5, 2007. The purpose of these instruments is to determine elemental abundances on the surface of Mercury. The GRS measures gamma-rays emitted from element interactions with cosmic rays impinging on the surface, while the XRS measures X-ray emissions induced on the surface by the incident solar flux. The GRS sensor is a high-resolution high-purity Ge detector cooled by a Stirling cryocooler, surrounded by a borated-plastic anticoincidence shield. The GRS is sensitive to gamma-rays up to ~10 MeV and can identify most major elements, sampling down to depths of about ten centimeters. Only the shield was powered on for this flyby in order to conserve cooler lifetime. Gamma-rays were observed coming from Venus as well as from the spacecraft. Although the Venus gamma-rays originate from its thick atmosphere rather than its surface, the GRS data from this encounter will provide useful calibration data from a source of known composition. In particular, the data will be useful for determining GRS sensitivity and pointing options for the Mercury flybys, the first of which will be in January 2008. The X-ray spectrum of a planetary surface is dominated by a combination of the fluorescence and scattered solar X-rays. The most prominent fluorescent lines are the Kα lines from the major elements Mg, Al, Si, S, Ca, Ti, and Fe (1-10 keV). The sampling depth is less than 100 u m. The XRS is similar in design to experiments flown on Apollo 15 and 16 and the NEAR-Shoemaker mission. Three large-area gas-proportional counters view the planet, and a small Si-PIN detector mounted on the spacecraft sunshade monitors the Sun. The energy resolution of the gas proportional counters (~850 eV at 5.9 keV) is sufficient to resolve the X-ray lines above 2 keV, but Al and Mg

  9. The Marshall Grazing Incidence X-ray Spectrometer (MaGIXS)

    NASA Astrophysics Data System (ADS)

    Champey, P. R.; Winebarger, A. R.; Kobayashi, K.; Savage, S. L.; Cirtain, J. W.; Cheimets, P.; Hertz, E.; Golub, L.; Ramsey, B.; McCracken, J.; Heilmann, R.; Schattenburg, M.; Bruccoleri, A.

    2015-12-01

    The Marshall Grazing Incidence X-ray Spectrometer (MaGIXS) is a NASA soundingrocket instrument designed to observe soft X-ray emissions at 0.5 - 2.0 keV energies in thesolar atmosphere. The primary science goal is to differentiate steady, low-frequency heatingevents from sporadic, high-frequency heating events in the active region core For the first time, high-temperature, low-emission plasma will be observed directly with 5 arcsec spatialand 22 mÅ spectral resolution. The novel optical design consists of a Wolter I telescope anda 3-optic grazing-incidence spectrograph. The X-ray spectrograph utilizes a finite conjugatemirror pair and a planar, nanoprinted-silicon varied line space grating, which is being devel-oped by the Massachusetts Institute of Technology (MIT). The telescope and spectrographmirrors will be nickel replicated and coated with iridium. Mandrel fabrication and nickelreplication will be done at MSFC as part of its replicated X-ray optics program. Mounting,alignment, and integration of the ight optics will be performed at the Harvard-SmithsonianCenter for Astrophysics (SAO). The MaGIXS science camera is being developed at MSFCand is based on CLASP heritage, which obtained read noise performance of 5.5 e?- RMS. Thecamera will include a e2v Technologies 2kx2k frame transfer CCD with 4-channel readout(500 kpixel/s/channel). We will present an overview of the MaGIXS optical system andfabrication of the telescope and spectrograph mirrors.

  10. Future Development Trajectories for Imaging X-ray Spectrometers Based on Microcalorimeters

    NASA Astrophysics Data System (ADS)

    Kilbourne, Caroline; Bandler, S.

    2013-04-01

    Since their invention 30 years ago, the capability of X-ray microcalorimeters has increased steadily, with continual improvements in energy resolution, speed, and array size. Arrays of up to 1024 pixels have been produced, and resolution better than 1 eV at 1.5 keV has been achieved. These detectors can be optimized for the highest priority science, such as designing for the highest resolving power at low energies at the expense of dynamic range, or the greatest focal-plane coverage at the expense of speed. Three types of X-ray microcalorimeters presently dominate the field, each characterized by the thermometer technology. The first two types use temperature-sensitive resistors: semiconductors in the metal-insulator transition and superconductors operated in the superconducting-normal transition. The third type uses a magnetically coupled thermometer, and is at an earlier stage of development than the other two. The Soft X-ray Spectrometer (SXS) on Astro-H, expected to launch in 2015, will use an array of silicon thermistors with HgTe X-ray absorbers that will operate at 50 mK. Both the semiconductor and superconductor calorimeters have been implemented in small arrays. Kilopixel arrays of the superconducting calorimeters are being produced, and much larger arrays may require the non-dissipative advantage of magnetically coupled thermometers. I will project the development trajectories of these detectors and their read-out technologies and assess what their capabilities and limitations will be 10 - 20 years from now.

  11. Using ACIS on the Chandra X-ray Observatory as a Particle Radiation Monitor II

    NASA Technical Reports Server (NTRS)

    Grant, C. E.; Ford, P. G.; Bautz, M. W.; ODell, S. L.

    2012-01-01

    The Advanced CCD Imaging Spectrometer is an instrument on the Chandra X-ray Observatory. CCDs are vulnerable to radiation damage, particularly by soft protons in the radiation belts and solar storms. The Chandra team has implemented procedures to protect ACIS during high-radiation events including autonomous protection triggered by an on-board radiation monitor. Elevated temperatures have reduced the effectiveness of the on-board monitor. The ACIS team has developed an algorithm which uses data from the CCDs themselves to detect periods of high radiation and a flight software patch to apply this algorithm is currently active on-board the instrument. In this paper, we explore the ACIS response to particle radiation through comparisons to a number of external measures of the radiation environment. We hope to better understand the efficiency of the algorithm as a function of the flux and spectrum of the particles and the time-profile of the radiation event.

  12. Thermal design and performance of the REgolith x-ray imaging spectrometer (REXIS) instrument

    NASA Astrophysics Data System (ADS)

    Stout, Kevin D.; Masterson, Rebecca A.

    2014-08-01

    The REgolith X-ray Imaging Spectrometer (REXIS) instrument is a student collaboration instrument on the OSIRIS-REx asteroid sample return mission scheduled for launch in September 2016. The REXIS science mission is to characterize the elemental abundances of the asteroid Bennu on a global scale and to search for regions of enhanced elemental abundance. The thermal design of the REXIS instrument is challenging due to both the science requirements and the thermal environment in which it will operate. The REXIS instrument consists of two assemblies: the spectrometer and the solar X-ray monitor (SXM). The spectrometer houses a 2x2 array of back illuminated CCDs that are protected from the radiation environment by a one-time deployable cover and a collimator assembly with coded aperture mask. Cooling the CCDs during operation is the driving thermal design challenge on the spectrometer. The CCDs operate in the vicinity of the electronics box, but a 130 °C thermal gradient is required between the two components to cool the CCDs to -60 °C in order to reduce noise and obtain science data. This large thermal gradient is achieved passively through the use of a copper thermal strap, a large radiator facing deep space, and a two-stage thermal isolation layer between the electronics box and the DAM. The SXM is mechanically mounted to the sun-facing side of the spacecraft separately from the spectrometer and characterizes the highly variable solar X-ray spectrum to properly interpret the data from the asteroid. The driving thermal design challenge on the SXM is cooling the silicon drift detector (SDD) to below -30 °C when operating. A two-stage thermoelectric cooler (TEC) is located directly beneath the detector to provide active cooling, and spacecraft MLI blankets cover all of the SXM except the detector aperture to radiatively decouple the SXM from the flight thermal environment. This paper describes the REXIS thermal system requirements, thermal design, and analyses, with

  13. Tunable hard X-ray spectrometer utilizing asymmetric planes of a quartz transmission crystal

    NASA Astrophysics Data System (ADS)

    Seely, John F.; Henins, Albert; Feldman, Uri

    2016-05-01

    A Cauchois type hard x-ray spectrometer was developed that utilizes the (301) diffraction planes at an asymmetric angle of 23.51° to the normal to the surface of a cylindrically curved quartz transmission crystal. The energy coverage is tunable by rotating the crystal and the detector arm, and spectra were recorded in the 8 keV to 20 keV range with greater than 2000 resolving power. The high resolution results from low aberrations enabled by the nearly perpendicular angle of the diffracted rays with the back surface of the crystal. By using other asymmetric planes of the same crystal and rotating to selected angles, the spectrometer can operate with high resolution up to 50 keV.

  14. [Establishment and Improvement of Portable X-Ray Fluorescence Spectrometer Detection Model Based on Wavelet Transform].

    PubMed

    Li, Fang; Wang, Ji-hua; Lu, An-xiang; Han, Ping

    2015-04-01

    The concentration of Cr, Cu, Zn, As and Pb in soil was tested by portable X-ray fluorescence spectrometer. Each sample was tested for 3 times, then after using wavelet threshold noise filtering method for denoising and smoothing the spectra, a standard curve for each heavy metal was established according to the standard values of heavy metals in soil and the corresponding counts which was the average of the 3 processed spectra. The signal to noise ratio (SNR), mean square error (MSE) and information entropy (H) were taken to assess the effects of denoising when using wavelet threshold noise filtering method for determining the best wavelet basis and wavelet decomposition level. Some samples with different concentrations and H3 B03 (blank) were chosen to retest this instrument to verify its stability. The results show that: the best denoising result was obtained with the coif3 wavelet basis at the decomposition level of 3 when using the wavelet transform method. The determination coefficient (R2) range of the instrument is 0.990-0.996, indicating that a high degree of linearity was found between the contents of heavy metals in soil and each X-ray fluorescence spectral characteristic peak intensity with the instrument measurement within the range (0-1,500 mg · kg(-1)). After retesting and calculating, the results indicate that all the detection limits of the instrument are below the soil standards at national level. The accuracy of the model has been effectively improved, and the instrument also shows good precision with the practical application of wavelet transform to the establishment and improvement of X-ray fluorescence spectrometer detection model. Thus the instrument can be applied in on-site rapid screening of heavy metal in contaminated soil. PMID:26197612

  15. Krypton K-Shell X-Ray Spectra Recorded by the HENEX Spectrometer

    SciTech Connect

    J. Seely; C. Back; C. Constantin, R. Lee; H. Chung; L. Hudson; C. Szabo; A. Henins; G. Holland; R. Atkin; L. Marlin

    2005-01-04

    High resolution x-ray spectra were recorded by the High Energy Electronic X-Ray (HENEX) spectrometer from a variety of targets irradiated by the Omega laser at the Laboratory for Laser Energetics. The HENEX spectrometer utilizes four reflection crystals covering the 1 keV to 20 keV energy range and one quartz(10-11) transmission crystal (Lau geometry) covering the 11 keV to 40 keV range. The time-integrated spectral images were recorded on five CMOS x-ray detectors. In the spectra recorded from krypton-filled gasbag and hohlraum targets, the helium-like K-shell transitions n=1-2, 1-3, and 1-4 appeared in the 13 keV to 17 keV energy range. A number of additional spectral features were observed at energies lower than the helium-like n=1-3 and n=1-4 transitions. Based on computational simulations of the spectra using the FLYCHK/FLYSPEC codes, which included opacity effects, these additional features are identified to be inner-shell transitions from the Li-like through N-like krypton charge states. The comparisons of the calculated and observed spectra indicate that these transitions are characteristic of the plasma conditions immediately after the laser pulse when the krypton density is 2x1018 cm-3 and the electron temperature is in the range 2.8 keV to 3.2 keV. These spectral features represent a new diagnostic for the charge state distribution, the density and electron temperature, and the plasma opacity. Laboratory experiments indicate that it is feasible to record K-shell spectra from gold and higher Z targets in the > 60 keV energy range using a Ge(220) transmission crystal.

  16. The High Resolution Microcalorimeter Soft X-ray Spectrometer for the Astro-H Mission

    NASA Astrophysics Data System (ADS)

    Kelley, Richard L.; Mitsuda, K.; International SXS Team

    2013-04-01

    We are developing the Soft X-Ray Spectrometer (SXS) for the JAXA Astro-H mission. The instrument is based on a 36-pixel array of semiconductor micro calorimeters that provides high spectral resolution over the 0.3-12 keV energy band at the focus of a high throughput, grazing-incidence x-ray mirror, giving a 3 x 3 arcmin field of view and more than 200 cm2 of collecting area at 6 keV. The instrument is a collaboration between the JAXA Institute of Space and Astronautical Science and their partners in Japan, the NASA/Goddard Space Flight Center, the University of Wisconsin, the Space Research Organization of the Netherlands, and Geneva University. The principal components of the spectrometer are the microcalorimeter detector system, low-temperature anticoincidence detector, 3-stage ADR and dewar. The dewar is a long-life, hybrid design with a superfluid helium cryostat, Joule-Thomson cooler, and Stirling coolers. The instrument is capable of achieving 4-5 eV resolution across the array and is designed to operate for at least three years in orbit, and can operate either without liquid helium or the cooling power of the Joule-Thomson cooler. In this presentation we describe the design and status of the Astro-H/SXS instrument.

  17. Arcus: an ISS-attached high-resolution x-ray grating spectrometer

    NASA Astrophysics Data System (ADS)

    Smith, R. K.; Ackermann, M.; Allured, R.; Bautz, M. W.; Bregman, J.; Bookbinder, J.; Burrows, D.; Brenneman, L.; Brickhouse, N.; Cheimets, P.; Carrier, A.; Freeman, M.; Kaastra, J.; McEntaffer, R.; Miller, J.; Ptak, A.; Petre, R.; Vacanti, G.

    2014-07-01

    We present the design and scientific motivation for Arcus, an X-ray grating spectrometer mission to be deployed on the International Space Station. This mission will observe structure formation at and beyond the edges of clusters and galaxies, feedback from supermassive black holes, the structure of the interstellar medium and the formation and evolution of stars. The mission requirements will be R>2500 and >600 cm2 of effective area at the crucial O VII and O VIII lines, values similar to the goals of the IXO X-ray Grating Spectrometer. The full bandpass will range from 8-52Å (0.25-1.5 keV), with an overall minimum resolution of 1300 and effective area >150 cm2. We will use the silicon pore optics developed at cosine Research and proposed for ESA's Athena mission, paired with off-plane gratings being developed at the University of Iowa and combined with MIT/Lincoln Labs CCDs. This mission achieves key science goals of the New Worlds, New Horizons Decadal survey while making effective use of the International Space Station (ISS).

  18. High-Resolution X-ray Spectroscopy with a Grating Spectrometer Explorer on the ISS

    NASA Astrophysics Data System (ADS)

    Smith, Randall

    We present the design and scientific motivation for a X-ray grating spectrometer mission to be deployed on the International Space Station. This mission would observe the Warm-Hot Intergalactic Medium, feedback from supermassive black holes, and the structure of the interstellar medium and halo of the Milky Way, amongst other goals. The mission requirements are similar to those of the IXO X-ray Grating Spectrometer of R=3000 and 1000 cm(2) \\ of effective area at 0.5 keV, with a full bandpass covering at least between 0.3-1 keV. Our initial design baselines the silicon pore optics proposed for ESA's Athena mission with a 4.3 m focal length, paired with off-plane gratings being developed at the University of Iowa combined with MIT/Lincoln Labs CCDs. This mission would achieve core science described in the 2010 New Worlds, New Horizons Decadal survey performed by the US National Research Council while effectively using the ISS and at low cost and low risk.

  19. Arcus:An X-ray Grating Spectrometer on the ISS: Mission Overview

    NASA Astrophysics Data System (ADS)

    Bookbinder, Jay A.

    2014-08-01

    Arcus is an X-ray grating spectrometer mission to be deployed on the International Space Station in response to NASA’s Astrophysics Division plan to announce a SMEX call in Fall 2014 with a cost cap of $125M (FY15). The baseline design uses sub-apertured X-ray silicon pore optics feeding into off-plane gratings to achieve both high spectral resolution with a large effective area. The detector focal plane uses Suzaku-type CCDs. The mission would be ready to be launched and mounted on the ISS in 2020. The mission parameters are R=2800 and ~800 sq. cm at the critical O VII wavelength near 21Å 0.5 keV), with an overall bandpass from 8-52Å (0.25-1.5 keV), enabling a wide range of science objectives. These values are similar to those of the grating spectrometers considered as part of the proposed Constellation-X and IXO missions, which were highly ranked by two Decadal surveys.

  20. Design and performance of AERHA, a high acceptance high resolution soft x-ray spectrometer

    NASA Astrophysics Data System (ADS)

    Chiuzbǎian, Sorin G.; Hague, Coryn F.; Avila, Antoine; Delaunay, Renaud; Jaouen, Nicolas; Sacchi, Maurizio; Polack, François; Thomasset, Muriel; Lagarde, Bruno; Nicolaou, Alessandro; Brignolo, Stefania; Baumier, Cédric; Lüning, Jan; Mariot, Jean-Michel

    2014-04-01

    A soft x-ray spectrometer based on the use of an elliptical focusing mirror and a plane varied line spacing grating is described. It achieves both high resolution and high overall efficiency while remaining relatively compact. The instrument is dedicated to resonant inelastic x-ray scattering studies. We set out how this optical arrangement was judged best able to guarantee performance for the 50 - 1000 eV range within achievable fabrication targets. The AERHA (adjustable energy resolution high acceptance) spectrometer operates with an effective angular acceptance between 100 and 250 μsr (energy dependent) and a resolving power well in excess of 5000 according to the Rayleigh criterion. The high angular acceptance is obtained by means of a collecting pre-mirror. Three scattering geometries are available to enable momentum dependent measurements with 135°, 90°, and 50° scattering angles. The instrument operates on the Synchrotron SOLEIL SEXTANTS beamline which serves as a high photon flux 2 × 200 μm2 focal spot source with full polarization control.

  1. Design and performance of AERHA, a high acceptance high resolution soft x-ray spectrometer

    SciTech Connect

    Chiuzbăian, Sorin G. Hague, Coryn F.; Brignolo, Stefania; Baumier, Cédric; Lüning, Jan; Avila, Antoine; Delaunay, Renaud; Mariot, Jean-Michel; Jaouen, Nicolas; Polack, François; Thomasset, Muriel; Lagarde, Bruno; Nicolaou, Alessandro; Sacchi, Maurizio

    2014-04-15

    A soft x-ray spectrometer based on the use of an elliptical focusing mirror and a plane varied line spacing grating is described. It achieves both high resolution and high overall efficiency while remaining relatively compact. The instrument is dedicated to resonant inelastic x-ray scattering studies. We set out how this optical arrangement was judged best able to guarantee performance for the 50 − 1000 eV range within achievable fabrication targets. The AERHA (adjustable energy resolution high acceptance) spectrometer operates with an effective angular acceptance between 100 and 250 μsr (energy dependent) and a resolving power well in excess of 5000 according to the Rayleigh criterion. The high angular acceptance is obtained by means of a collecting pre-mirror. Three scattering geometries are available to enable momentum dependent measurements with 135°, 90°, and 50° scattering angles. The instrument operates on the Synchrotron SOLEIL SEXTANTS beamline which serves as a high photon flux 2 × 200 μm{sup 2} focal spot source with full polarization control.

  2. Horizontal Ampoule Growth and Characterization of Mercuric Iodide at Controlled Gas Pressures for X-Ray and Gamma Ray Spectrometers

    SciTech Connect

    McGregor, Douglas S.; Ariesanti, Elsa; Corcoran, Bridget

    2004-04-30

    The project developed a new method for producing high quality mercuric iodide crystals of x-ray and gamma spectrometers. Included are characterization of mercuric iodide crystal properties as a function of growth environment and fabrication and demonstration of room-temperature-operated high-resolution mercuric iodide spectrometers.

  3. Spectroscopic investigations of highly charged ions using x-ray calorimeter spectrometers

    NASA Astrophysics Data System (ADS)

    Thorn, Daniel Bristol

    Spectroscopy of K-shell transitions in highly charged heavy ions, like hydrogenlike uranium, has the potential to yield information about quantum electrodynamics (QED) in extremely strong nuclear fields as well as tests of the standard model, specifically parity violation in atomic systems. These measurements would represent the 'holy grail' in high-Z atomic spectroscopy. However, the current state-of-the-art detection schemes used for recording the K-shell spectra from highly charged heavy ions does not yet have the resolving power to be able to attain this goal. As such, to push the field of high-Z spectroscopy forward, new detectors must be found. Recently, x-ray calorimeter spectrometers have been developed that promise to make such measurements. In an effort to make the first steps towards attaining the 'holy grail', measurements have been performed with two x-ray calorimeter spectrometers (the XRS/EBIT and the ECS) designed and built at Goddard Space Flight Center in Greenbelt, MD. The calorimeter spectrometers have been used to record the K-shell spectra of highly charged ions produced in the SuperEBIT electron beam ion trap at Lawrence Livermore National Laboratory in Livermore, CA. Measurements performed with the XRS/EBIT calorimeter array found that the theoretical description of well-above threshold electron-impact excitation cross sections for hydrogenlike iron and nickel ions are correct. Furthermore, the first high-resolution spectrum of hydrogenlike through carbonlike praseodymium ions was recorded with a calorimeter. In addition, the new high-energy array on the EBIT Calorimeter Spectrometer (ECS) was used to resolve the K-shell x-ray emission spectrum of highly charged xenon ions, where a 40 ppm measurement of the energy of the K-shell resonance transition in heliumlike xenon was achieved. This is the highest precision result, ever, for an element with such high atomic number. In addition, a first-of-its-kind measurement of the effect of the

  4. Spectroscopic Investigations of Highly Charged Ions using X-Ray Calorimeter Spectrometers

    SciTech Connect

    Thorn, Daniel Bristol

    2008-11-19

    Spectroscopy of K-shell transitions in highly charged heavy ions, like hydrogen-like uranium, has the potential to yield information about quantum electrodynamics (QED) in extremely strong nuclear fields as well as tests of the standard model, specifically parity violation in atomic systems. These measurements would represent the 'holy grail' in high-Z atomic spectroscopy. However, the current state-of-the-art detection schemes used for recording the K-shell spectra from highly charged heavy ions does not yet have the resolving power to be able to attain this goal. As such, to push the field of high-Z spectroscopy forward, new detectors must be found. Recently, x-ray calorimeter spectrometers have been developed that promise to make such measurements. In an effort to make the first steps towards attaining the 'holy grail', measurements have been performed with two x-ray calorimeter spectrometers (the XRS/EBIT and the ECS) designed and built at Goddard Space Flight Center in Greenbelt, MD. The calorimeter spectrometers have been used to record the K-shell spectra of highly charged ions produced in the SuperEBIT electron beam ion trap at Lawrence Livermore National Laboratory in Livermore, CA. Measurements performed with the XRS/EBIT calorimeter array found that the theoretical description of well-above threshold electron-impact excitation cross sections for hydrogen-like iron and nickel ions are correct. Furthermore, the first high-resolution spectrum of hydrogen-like through carbon-like praseodymium ions was recorded with a calorimeter. In addition, the new high-energy array on the EBIT Calorimeter Spectrometer (ECS) was used to resolve the K-shell x-ray emission spectrum of highly charged xenon ions, where a 40 ppm measurement of the energy of the K-shell resonance transition in helium-like xenon was achieved. This is the highest precision result, ever, for an element with such high atomic number. In addition, a first-of-its-kind measurement of the effect of the

  5. Reflection grating spectrometer onboard the ESA x-ray multi-mirror (XMM) mission

    NASA Astrophysics Data System (ADS)

    den Herder, Jan-Willem; Aarts, Henry J.; van den Berg, Marcel L.; Bixler, Jay V.; den Boggende, Antonius J.; Branduardi-Raymont, G.; Brinkman, Albert C.; Decker, Todd A.; Dubbeldam, Luc; Hailey, Charles J.; Jansen, Fred A.; Kahn, Steven M.; de Korte, Piet A.; Mauche, C. W.; Montesanti, Richard C.; Paerels, Frits B.; Spruijt, Hugo; Thomsen, K.; Verhoeve, P.; Zehnder, A.

    1994-09-01

    The Reflection Grating Spectrometer (RGS) onboard the ESA satellite XMM (X-ray Multi Mirror mission) combines a high resolving power (approximately 400 at 0.5 keV) with a large effective area (approximately 200 cm(superscript 2)). The spectral range selected for RGS (5 - 35 angstroms) contains the K shell transitions of N, O, Ne, Mg, Al, Si and S as well as the important L shell transitions of FE. The resolving power allows the study of a wide variety of challenging scientific questions. Detailed temperature diagnostics are feasible as the ionization balance is a unique function of the distribution of the electron temperature. Density diagnostics are provided by studying He-like triplets where the ratio of the forbidden to intercombination lines varies with density. Other fields of interest include the determination of elemental abundances, the study of optical depth effects, velocity diagnostics by measuring Doppler shifts and the estimate of magnetic fields through the observation of Zeeman splitting. The resolving power is obtained by an array of 240 gratings placed behind the mirrors of the telescope, dispersing about half of the X-rays in two spectroscopic orders. The X-rays are recorded by an array of 9 large format CCDs. These CCDs are operated in the frame transfer mode. They are back illuminated as the quantum efficiency of front illuminated devices is poor at low energies because of their poly-silicon gate structure. To suppress dark current the CCDs are passively cooled. In order to obtain the effective area of about 200 cm(superscript 2), grating arrays and CCD cameras are placed behind two of the three XMM telescopes. A model of RGS was tested last autumn ('93) at the Panter long beam X-ray facility in Munich. The model consisted of a subset of four mirrors, eight representative gratings covering a small section of the inner mirror shells and a CCD camera containing three CCDs. The purpose of these tests was to verify the resolution and sensitivity of

  6. Cooled window for X-rays or charged particles

    DOEpatents

    Logan, Clinton M.

    1996-01-01

    A window that provides good structural integrity and a very high capacity for removal of the heat deposited by x-rays, electrons, or ions, with minimum attenuation of the desired beam. The window is cooled by providing microchannels therein through which a coolant is pumped. For example, the window may be made of silicon with etched microchannels therein and covered by a silicon member. A window made of silicon with a total thickness of 520 .mu.m transmits 96% of the x-rays at an energy of 60 keV, and the transmission is higher than 90% for higher energy photons.

  7. Cooled window for X-rays or charged particles

    DOEpatents

    Logan, C.M.

    1996-04-16

    A window is disclosed that provides good structural integrity and a very high capacity for removal of the heat deposited by x-rays, electrons, or ions, with minimum attenuation of the desired beam. The window is cooled by providing microchannels therein through which a coolant is pumped. For example, the window may be made of silicon with etched microchannels therein and covered by a silicon member. A window made of silicon with a total thickness of 520 {micro}m transmits 96% of the x-rays at an energy of 60 keV, and the transmission is higher than 90% for higher energy photons. 1 fig.

  8. Improved micro x-ray fluorescence spectrometer for light element analysis

    SciTech Connect

    Smolek, Stephan; Streli, Christina; Zoeger, Norbert; Wobrauschek, Peter

    2010-05-15

    Since most available micro x-ray fluorescence (micro-XRF) spectrometers operate in air, which does not allow the analysis of low-Z elements (Z{<=}14), a special micro-XRF spectrometer has been designed to extend the analytical range down to light elements (Z{>=}6). It offers improved excitation and detection conditions necessary for light element analysis. To eliminate absorption of the exciting and fluorescent radiation, the system operates under vacuum condition. Sample mapping is automated and controlled by specialized computer software developed for this spectrometer. Several different samples were measured to test and characterize the spectrometer. The spot size has been determined by scans across a 10 {mu}m Cu wire which resulted in a full width at half maximum of 31 {mu}m for Mo K{alpha} line (17.44 keV) and 44 {mu}m effective beam size for the Cu K edge and 71 {mu}m effective beam size for the Cu L edge. Lower limits of detection in the picogram range for each spot (or {mu}g/cm{sup 2}) were obtained by measuring various thin metal foils under different conditions. Furthermore, detection limits in the parts per million range were found measuring NIST621 standard reference material. Area scans of a microscopic laser print and NaF droplet were performed to show mapping capabilities.

  9. High-resolution Bent-crystal Spectrometer for the Ultra-soft X-ray Region

    DOE R&D Accomplishments Database

    Beiersdorfer, P.; von Goeler, S.; Bitter, M.; Hill, K. W.; Hulse, R. A.; Walling, R. S.

    1988-10-01

    A multichannel vacuum Brag-crystal spectrometer has been developed for high-resolution measurements of the line emission from tokamak plasmas in the wavelength region between 4 and 25 angstrom. The spectrometer employs a bent crystal in Johann geometry and a microchannel-plate intensified photodiode array. The instrument is capable of measuring high-resolution spectra (lambda/..delta..lambda approx. 3000) with fast time resolution (4 msec per spectrum) and good spatial resolution (3 cm). The spectral bandwidth is ..delta..lambda/lambda{sub 0} = 8 angstrom. A simple tilt mechanism allows access to different wavelength intervals. In order to illustrate the utility of the new spectrometer, time- and space-resolved measurements of the n = 3 to n = 2 spectrum of selenium from the Princeton Large Torus tokamak plasmas are presented. The data are used to determine the plasma transport parameters and to infer the radial distribution of fluorinelike, neonlike, and sodiumlike ions of selenium in the plasma. The new ultra-soft x-ray spectrometer has thus enabled us to demonstrate the utility of high-resolution L-shell spectroscopy of neonlike ions as a fusion diagnostic.

  10. High-resolution bent-crystal spectrometer for the ultra-soft x-ray region

    SciTech Connect

    Beiersdorfer, P.; von Goeler, S.; Bitter, M.; Hill, K.W.; Hulse, R.A.; Walling, R.S.

    1988-10-01

    A multichannel vacuum Brag-crystal spectrometer has been developed for high-resolution measurements of the line emission from tokamak plasmas in the wavelength region between 4 and 25 /angstrom/. The spectrometer employs a bent crystal in Johann geometry and a microchannel-plate intensified photodiode array. The instrument is capable of measuring high-resolution spectra (lambda/..delta..lambda approx. 3000) with fast time resolution (4 msec per spectrum) and good spatial resolution (3 cm). The spectral bandwidth is ..delta..lambda/lambda/sub 0/ = 8/angstrom/. A simple tilt mechanism allows access to different wavelength intervals. In order to illustrate the utility of the new spectrometer, time- and space-resolved measurements of the n = 3 to n = 2 spectrum of selenium from the Princeton Large Torus tokamak plasmas are presented. The data are used to determine the plasma transport parameters and to infer the radial distribution of fluorinelike, neonlike, and sodiumlike ions of selenium in the plasma. The new ultra-soft x-ray spectrometer has thus enabled us to demonstrate the utility of high-resolution L-shell spectroscopy of neonlike ions as a fusion diagnostic. 43 refs., 23 figs.