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Sample records for petra iii beamlines

  1. The Generic Beamline Concept of the PETRA III Undulator Beamlines

    SciTech Connect

    Hahn, U.; Peters, H. B.; Roehlsberger, R.; Schulte-Schrepping, H.

    2007-01-19

    The conversion of the PETRA storage ring at DESY to a third generation synchrotron radiation light source poses a challenge to the design of the beam transport system. The total power in the white beam will be as high as 7.5kW in the case of the 5m long undulator at 100mA. The power density will be 476 W/mm2 at 20m from the source. Upgrades to a beam current of 200mA have to be accounted for in the design of the beamline components. For the beam transport between the undulator and the experimental hall, the design of a generic beamline is presented. It contains all elements which are needed to guide the beam to the experiment. This generic beamline consists of the estimated maximum of components for this purpose. Special experimental needs may reduce the number of proposed devices in the generic part and add special optical devices close to the experiment, e. g. strong focusing. The paper focuses on the girder concept for all major beam transport components and the collimating shutter system which has to deal with the high power density of the PETRA III undulators.

  2. The High Energy Materials Science Beamline (HEMS) at PETRA III

    NASA Astrophysics Data System (ADS)

    Schell, Norbert; King, Andrew; Beckmann, Felix; Ruhnau, Hans-Ulrich; Kirchhof, René; Kiehn, Rüdiger; Müller, Martin; Schreyer, Andreas

    2010-06-01

    The HEMS Beamline at the German high-brilliance synchrotron radiation storage ring PETRA III is fully tunable between 30 and 250 keV and optimized for sub-micrometer focusing. Approximately 70 % of the beamtime will be dedicated to Materials Research. Fundamental research will encompass metallurgy, physics and chemistry with first experiments planned for the investigation of the relationship between macroscopic and micro-structural properties of polycrystalline materials, grain-grain-interactions, and the development of smart materials or processes. For this purpose a 3D-microsctructure-mapper has been designed. Applied research for manufacturing process optimization will benefit from high flux in combination with ultra-fast detector systems allowing complex and highly dynamic in-situ studies of micro-structural transformations, e.g. during welding processes. The beamline infrastructure allows accommodation of large and heavy user provided equipment. Experiments targeting the industrial user community will be based on well established techniques with standardized evaluation, allowing full service measurements, e.g. for tomography and texture determination. The beamline consists of a five meter in-vacuum undulator, a general optics hutch, an in-house test facility and three independent experimental hutches working alternately, plus additional set-up and storage space for long-term experiments. HEMS is under commissioning as one of the first beamlines running at PETRA III.

  3. The holography endstation of beamline P10 at PETRA III

    SciTech Connect

    Kalbfleisch, S.; Osterhoff, M.; Giewekemeyer, K.; Neubauer, H.; Krueger, S. P.; Hartmann, B.; Bartels, M.; Salditt, T.; Sprung, M.; Leupold, O.; Siewert, F.

    2010-06-23

    We present the design and instrumentation of a novel holography endstation for the P10 coherence beamline at PETRA III at DESY. The experimental imaging scheme is based on a highly coherent and divergent (cone) beam illumination, achieved by fixed curvature focusing mirrors with additional spatial and coherence filtering by x-ray waveguides. The optical elements along the beam path and the instrument under construction are described. Preliminary results obtained in a similar setting under comparable parameters are given as a benchmark, and first simulations of one of the two mirrors are presented to study the effect of imperfections on the field distribution in the focal plane.

  4. P05 imaging beamline at PETRA III: first results

    NASA Astrophysics Data System (ADS)

    Greving, Imke; Wilde, Fabian; Ogurreck, Malte; Herzen, Julia; Hammel, Jörg U.; Hipp, Alexander; Friedrich, Frank; Lottermoser, Lars; Dose, Thomas; Burmester, Hilmar; Müller, Martin; Beckmann, Felix

    2014-09-01

    The imaging beamline (IBL/P05) operated by Helmholtz Zentrum Geesthacht (HZG) at the DESY PETRA III storage ring consists of two experimental stations: A micro tomography and a nano tomography end station. Here an overview of the experimental setups and the data acquisition will be given. In addition some first results out of the wide range of applications using the micro tomography station at P05 will be shown. Furthermore, we present first results of the nano tomography end station. These were obtained with an x-ray microscopy setup, which currently operates at energies of 17.4 and 30 keV using polymer compound refractive lenses (CRLs) and rolled prism lenses. Taken together these results clearly show the high potential of the newly built imaging beamline IBL.

  5. Capabilities of the Extreme Conditions Beamline at PETRA III, DESY

    NASA Astrophysics Data System (ADS)

    Liermann, Hanns-Peter; Konôpková, Zuzana; Morgenroth, Wolfgang; Rothkirch, Andre; Wittich, Eugen; Delitz, Jan-Torben; Ehnes, Anita

    2013-06-01

    At the end of 2010 the Extreme Conditions Beamline (ECB) at PETRA III received first beam and entered the commissioning phase. Since 2012 we are offering beamtime to general users to conduct a variety of different experiments such as powder and single diffraction in the laser/resistive heated and cryogenically cooled Diamond Anvil Cell (DAC). Particularly attractive has been our ability to conducted diffraction experiments at high energies of 60 and 77 keV for pair distribution function (PDF) studies as well as possibility to preform time resolved powder diffraction experiments at 26 and 43 keV with a maximum time resolution of 15 Hz. Within we present some of the current capabilities of the beamline as well as future plans to promote single crystal diffraction at high pressures and temperatures using both monochromatic and pink beam. Finally, we emphasis the present and future time resolved capabilities to conduct powder and single crystal diffraction experiments under dynamic compression and heating conditions in the DAC. Part of this project was funded by the ``Bundesministerium fuer Bildung und Forschung'' under contracts 05KS7RF1 and 05K10RFA ``Verbundprojekt: Messeinrichtungen fuer die Material- und Strukturforschung an PETRA III, 2: Laserheizung for ``ECB''.

  6. The nanotomography endstation at the PETRA III Imaging Beamline

    NASA Astrophysics Data System (ADS)

    Ogurreck, M.; Wilde, F.; Herzen, J.; Beckmann, F.; Nazmov, V.; Mohr, J.; Haibel, A.; Müller, M.; Schreyer, A.

    2013-03-01

    The Imaging Beamline (IBL) operated by the Helmholtz-Zentrum Geesthacht (HZG) at the newly refurbished DESY PETRA III storage ring is dedicated to radiography and tomography and provides two experimental endstations, one for micro tomography and one for nano tomography. The technical specifications aim for 3D imaging with a spatial resolution of below 100 nm. This nanometer resolution will be achieved by using different combinations of compound refractive lenses as X-ray optics. In addition, a microscopic optic for magnifying the images after the converting in visible light will be used, too. The overall setup is designed to be very flexible, which allows also the implementation of other optical elements (e.g. Fresnel zoneplates, KB mirrors) as well as the application of different magnifying techniques like cone-beam tomography or X-ray microscopy. The accessible energy range for the nano tomography is 10 - 30 keV but the beamline is designed for an energy range of 5 - 50 keV and we aim to allow the same energy range for the nano tomography in the long run.

  7. Layout and first results of the nanotomography endstation at the P05 beamline at PETRA III

    NASA Astrophysics Data System (ADS)

    Ogurreck, M.; Greving, I.; Marschall, F.; Vogt, H.; Last, A.; do Rosario, J. J.; Leib, E. W.; Beckmann, F.; Wilde, F.; Müller, M.

    2016-01-01

    The Helmholtz-Zentrum Geesthacht operates the P05 Imaging Beamline at the DESY storage ring PETRA III. This beamline is dedicated to micro- and nanotomography with two endstations. This paper will present the nanotomography endstation layout and first results obtained from commissioning and test experiments. First tests have been performed with CRLs as X-ray objectives and newly developed rolled X-ray prism lenses as condenser optics. This setup allows a resolution of 100 nm half period with an effective detector pixel size of 15nm. A first tomograph of a photonic glass sample was measured in early 2014.

  8. The sapphire backscattering monochromator at the Dynamics beamline P01 of PETRA III

    DOE PAGESBeta

    Alexeev, P.; Asadchikov, V.; Bessas, D.; Butashin, A.; Deryabin, A.; Dill, F. -U.; Ehnes, A.; Herlitschke, M.; Hermann, R. P.; Jafari, A.; et al

    2016-02-23

    Here, we report on a high resolution sapphire backscattering monochromator installed at the Dynamics beamline P01 of PETRA III. The device enables nuclear resonance scattering experiments on M ossbauer isotopes with transition energies between 20 and 60 keV with sub-meV to meV resolution. In a first performance test with 119Sn nuclear resonance at a X-ray energy of 23.88 keV an energy resolution of 1.34 meV was achieved. Moreover, the device extends the field of nuclear resonance scattering at the PETRA III synchrotron light source to many further isotopes like 151Eu, 149Sm, 161Dy, 125Te and 121Sb.

  9. The sapphire backscattering monochromator at the Dynamics beamline P01 of PETRA III

    SciTech Connect

    Alexeev, Pavel; Asadchikov, Victor E; Bessas, D.; Butashin, A. V.; Deryabin, A. N.; Dill, F.-U.; Ehnes, A.; Herlitschke, Marcus; Hermann, Raphael P; Jafari, Atefeh; Prokhorov, I A; Roshchin, boris s; Roehlsberger, Ralf; Schlage, Kai; Sergueev, I.; Siemens, A.; Wille, Hans Christian

    2016-01-01

    We report on a high resolution sapphire backscattering monochromator installed at the Dynamics beamline P01 of PETRA III. The device enables nuclear resonance scattering experiments on M ossbauer isotopes with transition energies between 20 and 60 keV with sub-meV to meV resolution. In a first performance test with 119Sn nuclear resonance at a X-ray energy of 23.88 keV an energy resolution of 1.34 meV was achieved. The device extends the field of nuclear resonance scattering at the PETRA III synchrotron light source to many further isotopes like 151Eu, 149Sm, 161Dy, 125Te and 121Sb.

  10. Time-resolved pump and probe x-ray absorption fine structure spectroscopy at beamline P11 at PETRA III.

    PubMed

    Göries, D; Dicke, B; Roedig, P; Stübe, N; Meyer, J; Galler, A; Gawelda, W; Britz, A; Geßler, P; Sotoudi Namin, H; Beckmann, A; Schlie, M; Warmer, M; Naumova, M; Bressler, C; Rübhausen, M; Weckert, E; Meents, A

    2016-05-01

    We report about the development and implementation of a new setup for time-resolved X-ray absorption fine structure spectroscopy at beamline P11 utilizing the outstanding source properties of the low-emittance PETRA III synchrotron storage ring in Hamburg. Using a high intensity micrometer-sized X-ray beam in combination with two positional feedback systems, measurements were performed on the transition metal complex fac-Tris[2-phenylpyridinato-C2,N]iridium(III) also referred to as fac-Ir(ppy)3. This compound is a representative of the phosphorescent iridium(III) complexes, which play an important role in organic light emitting diode (OLED) technology. The experiment could directly prove the anticipated photoinduced charge transfer reaction. Our results further reveal that the temporal resolution of the experiment is limited by the PETRA III X-ray bunch length of ∼103 ps full width at half maximum (FWHM). PMID:27250401

  11. Double phase-retarder set-up at beamline P09 at PETRA III

    NASA Astrophysics Data System (ADS)

    Francoual, S.; Strempfer, J.; Reuther, D.; Shukla, D. K.; Skaugen, A.

    2013-03-01

    Beamline P09 at PETRA III, DESY, is designed for general diffraction and resonant X-ray scattering experiments at low temperatures and high magnetic fields. The dependence of the X-ray cross-sections (Thomson, non-resonant magnetic, resonant exchange scattering, ATS) on the polarization state of the incident X-rays is an important property that one might want to capitalize on in a diffraction experiment. To that purpose, P09 is equipped with a double phase-retarder and diamond phase-plates making for the production of linearly and circularly polarized X-rays in the energy range between 3.5 and 8.5 keV as yet. Here we describe the double phase-retarder setup at P09, its principles of operation and its performances with respect to the generation of linearly polarized incident X-rays rotated by a variable angle η around the X-ray beam using two quarter-wave plates in series or a single half-wave plate.

  12. Note: Comparison of grazing incidence small angle x-ray scattering of a titania sponge structure at the beamlines BW4 (DORIS III) and P03 (PETRA III)

    SciTech Connect

    Rawolle, M.; Koerstgens, V.; Ruderer, M. A.; Metwalli, E.; Guo, S.; Mueller-Buschbaum, P.; Herzog, G.; Benecke, G.; Schwartzkopf, M.; Buffet, A.; Perlich, J.; Roth, S. V.

    2012-10-15

    Grazing incidence small angle x-ray scattering (GISAXS) is a powerful technique for morphology investigation of nanostructured thin films. GISAXS measurements at the newly installed P03 beamline at the storage ring PETRA III in Hamburg, Germany, are compared to the GISAXS data from the beamline BW4 at the storage ring DORIS III, which had been used extensively for GISAXS investigations in the past. As an example, a titania thin film sponge structure is investigated. Compared to BW4, at beamline P03 the resolution of larger structures is slightly improved and a higher incident flux leads to a factor of 750 in scattered intensity. Therefore, the acquisition time in GISAXS geometry is reduced significantly at beamline P03.

  13. The Extreme Conditions Beamline at PETRA III, DESY: Possibilities to conduct time resolved monochromatic diffraction experiments in dynamic and laser heated DAC

    NASA Astrophysics Data System (ADS)

    Liermann, H.-P.; Morgenroth, W.; Ehnes, A.; Berghäuser, A.; Winkler, B.; Franz, H.; Weckert, E.

    2010-03-01

    We present plans for the new Extreme Conditions Beamline at PETRA III, DESY, Germany. The beamline is being designed and built with the specific goal to explore time resolved high-pressure and -temperature x-ray diffraction experiments in the dynamic and laser heated diamond anvil cell. Within we discuss the conceptual design of the optical components and experimental setup to conduct monochromatic high-pressure powder diffraction experiments in the sub-second time regime.

  14. Beamline P02.1 at PETRA III for high-resolution and high-energy powder diffraction

    PubMed Central

    Dippel, Ann-Christin; Liermann, Hanns-Peter; Delitz, Jan Torben; Walter, Peter; Schulte-Schrepping, Horst; Seeck, Oliver H.; Franz, Hermann

    2015-01-01

    Powder X-ray diffraction techniques largely benefit from the superior beam quality provided by high-brilliance synchrotron light sources in terms of photon flux and angular resolution. The High Resolution Powder Diffraction Beamline P02.1 at the storage ring PETRA III (DESY, Hamburg, Germany) combines these strengths with the power of high-energy X-rays for materials research. The beamline is operated at a fixed photon energy of 60 keV (0.207 Å wavelength). A high-resolution monochromator generates the highly collimated X-ray beam of narrow energy bandwidth. Classic crystal structure determination in reciprocal space at standard and non-ambient conditions are an essential part of the scientific scope as well as total scattering analysis using the real space information of the pair distribution function. Both methods are complemented by in situ capabilities with time-resolution in the sub-second regime owing to the high beam intensity and the advanced detector technology for high-energy X-rays. P02.1’s efficiency in solving chemical and crystallographic problems is illustrated by presenting key experiments that were carried out within these fields during the early stage of beamline operation. PMID:25931084

  15. Time-resolved soft X-ray microscopy of magnetic nanostructures at the P04 beamline at PETRA III

    NASA Astrophysics Data System (ADS)

    Wessels, P.; Ewald, J.; Wieland, M.; Nisius, T.; Abbati, G.; Baumbach, S.; Overbuschmann, J.; Vogel, A.; Neumann, A.; Viefhaus, J.; Oepen, H. P.; Meier, G.; Wilhein, T.; Drescher, M.

    2014-04-01

    We present first time-resolved measurements of a new mobile full-field transmission microscope [1] obtained at the soft X-ray beamline P04 at the high brilliance synchrotron radiation source PETRA III. A nanostructured magnetic permalloy (Ni80Fe20) sample can be excited by the magnetic field of a 400 ps full width at half maximum (FWHM) long electric current pulse in a coplanar waveguide. The full-field soft X-ray microscope successively probes the time evolution of the sample magnetization via X-ray magnetic circular dichroism (XMCD) [2] spectromicroscopy in a pump-probe scheme by varying the delay between pump and probe pulses electronically. Static and transient magnetic fields of a permanent magnet and a coil are available in the sample plane to reset the system and to provide external offset fields. The microscope generates a flat-top illumination field of 20 μm diameter by using a grating condenser [3] and the sample plane is directly imaged by a micro zone plate with 60 nm resolution onto a 2D gateable X-ray detector to select the particular bunch in the storage ring that contains the dynamic information. The setup is built into a mobile endstation vacuum system with in-house developed three-axis piezo motorized stages for high accuracy positioning of all microscopy-components inside the chambers.

  16. CVD diamond screens for photon beam imaging at PETRA III

    NASA Astrophysics Data System (ADS)

    Degenhardt, M.; Aprigliano, G.; Schulte-Schrepping, H.; Hahn, U.; Grabosch, H.-J.; Wörner, E.

    2013-03-01

    PETRA III, the most brilliant storage-ring-based synchrotron radiation source in the world, started its operation in 2009. It features 14 undulator beamlines and will be extended by further 10 beamlines in the PETRA III extension project. During the startup phase of the 14 PETRA III beamlines, fluorescence monitors based on CVD diamond screens have proven to be a very powerful tool for the monitoring of the attenuated undulator beams and for the commissioning of the optical components, e.g. slit systems and monochromators. They served as the essential instrument for the initial setup of the positron beam orbit to align the undulator photon beam along the beamline. The application of CVD diamond screens for the beam imaging at PETRA III beamlines is presented. Images taken during the beam adjustment and the beamline commissioning are shown.

  17. Use of intermediate focus for grazing incidence small and wide angle x-ray scattering experiments at the beamline P03 of PETRA III, DESY

    SciTech Connect

    Santoro, G.; Buffet, A.; Döhrmann, R.; Yu, S.; Roth, S. V.; Körstgens, V.; Müller-Buschbaum, P.; Gedde, U.; Hedenqvist, M.

    2014-04-15

    We describe the new experimental possibilities of the micro- and nanofocus X-ray scattering beamline P03 of the synchrotron source PETRA III at DESY, Hamburg (Germany), which arise from experiments with smaller beam sizes in the micrometer range. This beamline has been upgraded recently to perform new kinds of experiments. The use of an intermediate focus allows for reducing the beam size of microfocused hard X-rays while preserving a large working distance between the focusing elements and the focus position. For the first time, this well-known methodology has been employed to grazing incidence small- and wide-angle X-ray scattering (GISAXS/GIWAXS). As examples, we highlight the applications to in situ studies using microfluidic devices in GISAXS geometry as well as the investigation of the crystallinity of thin films in GIWAXS geometry.

  18. The Extreme Conditions Beamline P02.2 and the Extreme Conditions Science Infrastructure at PETRA III.

    PubMed

    Liermann, H P; Konôpková, Z; Morgenroth, W; Glazyrin, K; Bednarčik, J; McBride, E E; Petitgirard, S; Delitz, J T; Wendt, M; Bican, Y; Ehnes, A; Schwark, I; Rothkirch, A; Tischer, M; Heuer, J; Schulte-Schrepping, H; Kracht, T; Franz, H

    2015-07-01

    A detailed description is presented of the Extreme Conditions Beamline P02.2 for micro X-ray diffraction studies of matter at simultaneous high pressure and high/low temperatures at PETRA III, in Hamburg, Germany. This includes performance of the X-ray optics and instrumental resolution as well as an overview of the different sample environments available for high-pressure studies in the diamond anvil cell. Particularly emphasized are the high-brilliance and high-energy X-ray diffraction capabilities of the beamline in conjunction with the use of fast area detectors to conduct time-resolved compression studies in the millisecond time regime. Finally, the current capability of the Extreme Conditions Science Infrastructure to support high-pressure research at the Extreme Conditions Beamline and other PETRA III beamlines is described. PMID:26134794

  19. Versatile sample environments and automation for biological solution X-ray scattering experiments at the P12 beamline (PETRA III, DESY)

    PubMed Central

    Blanchet, Clement E.; Spilotros, Alessandro; Schwemmer, Frank; Graewert, Melissa A.; Kikhney, Alexey; Jeffries, Cy M.; Franke, Daniel; Mark, Daniel; Zengerle, Roland; Cipriani, Florent; Fiedler, Stefan; Roessle, Manfred; Svergun, Dmitri I.

    2015-01-01

    A high-brilliance synchrotron P12 beamline of the EMBL located at the PETRA III storage ring (DESY, Hamburg) is dedicated to biological small-angle X-ray scattering (SAXS) and has been designed and optimized for scattering experiments on macromolecular solutions. Scatterless slits reduce the parasitic scattering, a custom-designed miniature active beamstop ensures accurate data normalization and the photon-counting PILATUS 2M detector enables the background-free detection of weak scattering signals. The high flux and small beam size allow for rapid experiments with exposure time down to 30–50 ms covering the resolution range from about 300 to 0.5 nm. P12 possesses a versatile and flexible sample environment system that caters for the diverse experimental needs required to study macromolecular solutions. These include an in-vacuum capillary mode for standard batch sample analyses with robotic sample delivery and for continuous-flow in-line sample purification and characterization, as well as an in-air capillary time-resolved stopped-flow setup. A novel microfluidic centrifugal mixing device (SAXS disc) is developed for a high-throughput screening mode using sub-microlitre sample volumes. Automation is a key feature of P12; it is controlled by a beamline meta server, which coordinates and schedules experiments from either standard or nonstandard operational setups. The integrated SASFLOW pipeline automatically checks for consistency, and processes and analyses the data, providing near real-time assessments of overall parameters and the generation of low-resolution models within minutes of data collection. These advances, combined with a remote access option, allow for rapid high-throughput analysis, as well as time-resolved and screening experiments for novice and expert biological SAXS users. PMID:25844078

  20. Development of an in-vacuum x-ray microscope with cryogenic sample cooling for beamline P11 at PETRA III

    NASA Astrophysics Data System (ADS)

    Meents, Alke; Reime, Bernd; Stuebe, Nicolas; Fischer, Pontus; Warmer, Martin; Goeries, Dennis; Roever, Jan; Meyer, Jan; Fischer, Janine; Burkhardt, Anja; Vartiainen, Ismo; Karvinen, Petri; David, Christian

    2013-09-01

    Beamline P11 at PETRA III is dedicated to structural investigations of biological samples. It provides two experimental stations, one for macromolecular crystallography and one for X-ray microscopy. The microscope will provide full field Zernike phase contrast and scanning microscopy both in 2D and in tomographic mode. Full field microscopy with a field of view of 50 x 50 μm2 will allow to generate an overview of the sample and to select regions of interest for later inspection of the element distribution by X-ray fluorescence and diffraction in scanning mode. Central part of the microscope is an inhouse developed flexure based x,y,z scanner on top of a rotation stage. The scanner is operated in closed loop with piezo motors, has a travel range of 4 mm in horizontal and of 3 mm in vertical direction. With laser interferometers for closed loop operation a positioning accuracy of better than 5 nm is achieved in all directions. For precise sample rotation an in-vacuum air-bearing has been developed. An open bore in the center of the air-bearing allows cryogenic sample cooling by a cold He or N2 gas stream. Different optical elements such as beam defining pinholes, a condensor, zone plates, OSA, phase rings, etc. can be centered in the beam path by piezomotor driven x,y flexure elements mounted on a rail system which allows further positioning along the beam path. Different 2D detectors and two fluoresence detectors can be attached to the microscope.

  1. Single-crystal X-ray diffraction and resonant X-ray magnetic scattering at helium-3 temperatures in high magnetic fields at beamline P09 at PETRA III.

    PubMed

    Francoual, S; Strempfer, J; Warren, J; Liu, Y; Skaugen, A; Poli, S; Blume, J; Wolff-Fabris, F; Canfield, P C; Lograsso, T

    2015-09-01

    The resonant scattering and diffraction beamline P09 at PETRA III at DESY is equipped with a 14 T vertical field split-pair magnet. A helium-3 refrigerator is available that can be fitted inside the magnet's variable-temperature insert. Here the results of a series of experiments aimed at determining the beam conditions permitting operations with the He-3 insert are presented. By measuring the tetragonal-to-orthorhombic phase transition occurring at 2.1 K in the Jahn-Teller compound TmVO4, it is found that the photon flux at P09 must be attenuated down to 1.5 × 10(9) photons s(-1) for the sample to remain at temperatures below 800 mK. Despite such a reduction of the incident flux and the subsequent use of a Cu(111) analyzer, the resonant X-ray magnetic scattering signal at the Tm LIII absorption edge associated with the spin-density wave in TmNi2B2C below 1.5 K is intense enough to permit a complete study in magnetic field and at sub-Kelvin temperatures to be carried out. PMID:26289272

  2. Grating-based x-ray phase-contrast imaging at PETRA III

    NASA Astrophysics Data System (ADS)

    Hipp, A.; Beckmann, F.; Lytaev, P.; Greving, I.; Lottermoser, L.; Dose, T.; Kirchhof, R.; Burmester, H.; Schreyer, A.; Herzen, J.

    2014-09-01

    Conventional absorption-based imaging often lacks in good contrast at special applications like visualization of soft tissue or weak absorbing material in general. To overcome this limitation, several new X-ray phase-contrast imaging methods have been developed at synchrotron radiation facilities. Our aim was to establish the possibility of different phase-contrast imaging modalities at the Imaging Beamline (IBL, P05) and the High Energy Material Science beamline (HEMS, P07) at Petra III (DESY, Germany). Here we present the instrumentation and the status of the currently successfully established phase-contrast imaging techniques. First results from measurements of biomedical samples will be presented as demonstration.

  3. Radial X-Ray Diffraction at the Extreme Conditions Beamline of PETRA III: In-Situ Texture Analysis of a Mixture of Perovskite and Ferropericlase to 1100 K and 40 GPa

    NASA Astrophysics Data System (ADS)

    Miyagi, L. M.; Marquardt, H.; Speziale, S.; Liermann, H.

    2013-12-01

    Solid-state convection in the Earth interior is associated with the development of seismic anisotropy in many regions of the mantle. One of the main causes of observed seismic anisotropies is plastic deformation of the constituent minerals by dislocation glide, which produces lattice preferred orientation (LPO). If one has a sound understanding of the relationship between deformation and the development of anisotropy, observed anisotropies can be used to infer the dynamic state in the deep Earth. However, due to substantial experimental difficulties, direct in-situ determinations of LPO development at lower mantle conditions are extremely scarce in the literature and are typically limited to single phases. Thus little is known about the interactions between phases during deformation and questions remain as to what phase or phases control deformation and what phase or phases are responsible for observed anisotropies. This lack of information significantly limits our ability to interpret observations of seismic anisotropy in terms of mantle flow models. Substantial experimental progress is needed to investigate deformation of mixtures of lower mantle minerals at relevant pressures and temperatures. In order to extend our capability to deform complex multiphase mineral aggregates at simultaneous high pressures and temperatures exceeding 30 GPa at 1000 K a new experimental setup has been recently developed at the Extreme Conditions Beamline (ECB) P02.2 of PETRA III synchrotron in Hamburg. The new setup is dedicated to perform X-ray diffraction in radial geometry using a modified resistive-heated diamond anvil cell (RH-RDAC). The sample environment is heated by a graphite heater surrounding the sample assembly and diamonds. The DAC is enclosed in a dedicated vacuum vessel to preserve the diamonds and other sensitive components from oxidation at high temperature. Here we present in detail the features and the performance of this setup. We will also discuss results of

  4. The nuclear-resonance-scattering station at the PETRA II undulator beamline

    NASA Astrophysics Data System (ADS)

    Franz, H.; Hukelmann, B.; Schneider, J. R.

    2000-07-01

    PETRA II, a 12 GeV accelerator at DESY, Hamburg, is used to produce synchrotron radiation (SR) for experiments in the hard X-ray regime when it is not running as injector for HERA. The beam from an undulator is split by a diamond crystal in Laue geometry to feed two experimental stations, one of which is now dedicated for nuclear resonance experiments. The X-ray energy may be chosen in the range from 5 to 55 keV covering all isotopes already observed with SR and many interesting candidates for new resonances. Tuning may be performed by optimising the magnetic gap and the storage ring energy. In particular, the opportunities for timing experiments are unique due to a very flexible filling mode of the storage ring. The flux at the sample position is comparable to undulator beams at ESRF. The second beamline covers higher energies up to some 300 keV and may also be used for nuclear resonance experiments.

  5. Doublet III beamline: as-built

    SciTech Connect

    Harder, C.R.; Holland, M.M.; Parker, J.W.; Gunn, J.; Resnick, L.

    1980-03-01

    In order to fully exploit Doublet III capabilities and to study new plasma physics regimes, a Neutral Beam Injector System has been constructed. Initially, a two beamline system will supply 7 MW of heat to the plasma. The system is currently being expanded to inject approx. 20 MW of power (6 beamlines). Each beamline is equipped with two Lawrence Berkeley Laboratory type rectangular ion sources with 10 cm x 40 cm extraction grids. These sources will accelerate hydrogen ions to 80 keV, with extracted beam currents in excess of 80 A per source expected. The first completed source is currently being tested and conditioned on the High Voltage Test Stand at Lawrence Livermore Laboratory. This paper pictorially reviews the as-built Doublet III neutral beamline with emphasis on component relation and configuration relative to spatial and source imposed design constraints.

  6. Characterization of the Support and Drive System of the PETRA III APPLE Undulator

    NASA Astrophysics Data System (ADS)

    Bahrdt, J.; Bäcker, H.-J.; Frentrup, W.; Gaupp, A.; Gottschlich, S.; Kuhn, C.; Scheer, M.; Schulz, B.; Gast, M.; Englisch, U.; Schöps, A.; Tischer, M.

    2010-06-01

    Helmholtzzentrum Berlin has built an APPLE II undulator for the storage ring PETRA III. The device has a total length of 5m and a minimum gap of 11mm. The high magnetic forces in particular in the inclined mode have been analyzed by means of finite element methods (FEM). Specific mechanic components such as flexible joints have been optimized to cope with the gap- and shift-dependent 3D-forces and a sophisticated control and drive system has been implemented. After completion of the device, detailed laser interferometer measurements for all operation modes have been performed. The data are compared to the FEM simulations.

  7. Characterization of the Support and Drive System of the PETRA III APPLE Undulator

    SciTech Connect

    Bahrdt, J.; Baecker, H.-J.; Frentrup, W.; Gaupp, A.; Gottschlich, S.; Kuhn, C.; Scheer, M.; Schulz, B.; Gast, M.; Englisch, U.; Schoeps, A.; Tischer, M.

    2010-06-23

    Helmholtzzentrum Berlin has built an APPLE II undulator for the storage ring PETRA III. The device has a total length of 5m and a minimum gap of 11mm. The high magnetic forces in particular in the inclined mode have been analyzed by means of finite element methods (FEM). Specific mechanic components such as flexible joints have been optimized to cope with the gap- and shift-dependent 3D-forces and a sophisticated control and drive system has been implemented. After completion of the device, detailed laser interferometer measurements for all operation modes have been performed. The data are compared to the FEM simulations.

  8. Residual Gas X-ray Beam Position Monitor Development for PETRA III

    SciTech Connect

    Ilinski, P.; Hahn, U.; Schulte-Schrepping, H.; Degenhardt, M.

    2007-01-19

    The development effort is driven by the need for a new type of x-ray beam position monitor (XBPM), which will detect the centre of gravity of the undulator beam. XBPMs based on the ionization of a residual gas are considered being the candidate for this future ''white'' undulator beam XBPMs. A number of residual gas XBPM prototypes for the PETRA III storage ring were developed and tested. Tests were performed at DESY and the ESRF, resolution of beam position up to 5 {mu}m is reported. The further development of the RGXBPMs will be focused on improvements of resolution, readout speed and reliability.

  9. Vibration measurements of high-heat-load monochromators for DESY PETRA III extension

    PubMed Central

    Kristiansen, Paw; Horbach, Jan; Döhrmann, Ralph; Heuer, Joachim

    2015-01-01

    The requirement for vibrational stability of beamline optics continues to evolve rapidly to comply with the demands created by the improved brilliance of the third-generation low-emittance storage rings around the world. The challenge is to quantify the performance of the instrument before it is installed at the beamline. In this article, measurement techniques are presented that directly and accurately measure (i) the relative vibration between the two crystals of a double-crystal monochromator (DCM) and (ii) the absolute vibration of the second-crystal cage of a DCM. Excluding a synchrotron beam, the measurements are conducted under in situ conditions, connected to a liquid-nitrogen cryocooler. The investigated DCM utilizes a direct-drive (no gearing) goniometer for the Bragg rotation. The main causes of the DCM vibration are found to be the servoing of the direct-drive goniometer and the flexibility in the crystal cage motion stages. It is found that the investigated DCM can offer relative pitch vibration down to 48 nrad RMS (capacitive sensors, 0–5 kHz bandwidth) and absolute pitch vibration down to 82 nrad RMS (laser interferometer, 0–50 kHz bandwidth), with the Bragg axis brake engaged. PMID:26134790

  10. ASAP3 - New Data Taking and Analysis Infrastructure for PETRA III

    NASA Astrophysics Data System (ADS)

    Strutz, M.; Gasthuber, M.; Aplin, S.; Dietrich, S.; Kuhn, M.; Ensslin, U.; Smirnov, G.; Lewendel, B.; Guelzow, V.

    2015-12-01

    Data taking and analysis infrastructures in HEP (High Energy Physics) have evolved during many years to a well known problem domain. In contrast to HEP, third generation synchrotron light sources, existing and upcoming free electron lasers are confronted with an explosion in data rates driven primarily by recent developments in 2D pixel array detectors. The next generation of detectors will produce data in the region upwards of 50 Gbytes per second. At synchrotrons, data was traditionally taken away by users following data taking using portable media. This will clearly not scale at all. We present first experiences of our new architecture and underlying services based on results taken from the resumption of data taking in April 2015. Technology choices were undertaking over a period of twelve month. The work involved a close collaboration between central IT, beamline controls, and beamline support staff. In addition a cooperation was established between DESY IT and IBM to include industrial research and development experience and skills. Our approach integrates HPC technologies for storage systems and protocols. In particular, our solution uses a single file-system instance with a multiple protocol access, while operating within a single namespace.

  11. Analysis of coupled-bunch instabilities for the NSLS-II storage ring with a 500 MHz 7-cell PETRA-III cavity

    NASA Astrophysics Data System (ADS)

    Bassi, G.; Blednykh, A.; Cheng, W.; Gao, F.; Rose, J.; Teytelman, D.

    2016-02-01

    The NSLS-II storage ring is designed to operate with superconducting RF-cavities with the aim to store an average current of 500 mA distributed in 1080 bunches, with a gap in the uniform filling for ion clearing. At the early stage of the commissioning (phase 1), characterized by a bare lattice without damping wigglers and without Landau cavities, a normal conducting 7-cell PETRA-III RF-cavity structure has been installed with the goal to store an average current of 25 mA. In this paper we discuss our analysis of coupled-bunch instabilities driven by the Higher Order Modes (HOMs) of the 7-cell PETRA-III RF-cavity. As a cure of the instabilities, we apply a well-known scheme based on a proper detuning of the HOMs frequencies based upon cavity temperature change, and the use of the beneficial effect of the slow head-tail damping at positive chromaticity to increase the transverse coupled-bunch instability thresholds. In addition, we discuss measurements of coupled-bunch instabilities observed during the phase 1 commissioning of the NSLS-II storage ring. In our analysis we rely, in the longitudinal case, on the theory of coupled-bunch instability for uniform fillings, while in the transverse case we complement our studies with numerical simulations with OASIS, a novel parallel particle tracking code for self-consistent simulations of collective effects driven by short and long-range wakefields.

  12. Development of a scanning transmission x-ray microscope for the beamline P04 at PETRA III DESY

    NASA Astrophysics Data System (ADS)

    Andrianov, Konstantin; Ewald, Johannes; Nisius, Thomas; Lühl, Lars; Malzer, Wolfgang; Kanngießer, Birgit; Wilhein, Thomas

    2016-01-01

    We present a scanning transmission x-ray microscope (STXM) built on top of our existing modular platform for high resolution imaging experiments. This platform consists of up to three separate vacuum chambers and custom designed piezo stages. These piezo stages are able to move precisely in x-, y- and z-direction, this makes it possible to adjust the components for different imaging modes. During recent experiments the endstation was operated mainly as a transmission x-ray microscope (TXM) [1, 2].

  13. PETRA Yearbook 1992-1993.

    ERIC Educational Resources Information Center

    Commission of the European Communities, Brussels (Belgium).

    This yearbook of PETRA, the European Community's program for providing youths with vocational training and preparing them for adulthood and work, contains 14 articles: "PETRA's Added Value" (Welbers); "Beyond the Fallen Wall" (Hanf); "Project Report: A Flyweight Becomes a Bricklayer"; "PETRA's Southern Tip" (Kourkouta, Chatzipanagiotou);…

  14. Gradient-Modulated PETRA MRI

    PubMed Central

    Kobayashi, Naoharu; Goerke, Ute; Wang, Luning; Ellermann, Jutta; Metzger, Gregory J.; Garwood, Michael

    2015-01-01

    Image blurring due to off-resonance and fast T2* signal decay is a common issue in radial ultrashort echo time MRI sequences. One solution is to use a higher readout bandwidth, but this may be impractical for some techniques like pointwise encoding time reduction with radial acquisition (PETRA), which is a hybrid method of zero echo time and single point imaging techniques. Specifically, PETRA has severe specific absorption rate (SAR) and radiofrequency (RF) pulse peak power limitations when using higher bandwidths in human measurements. In this study, we introduce gradient modulation (GM) to PETRA to reduce image blurring artifacts while keeping SAR and RF peak power low. Tolerance of GM-PETRA to image blurring was evaluated in simulations and experiments by comparing with the conventional PETRA technique. We performed inner ear imaging of a healthy subject at 7T. GM-PETRA showed significantly less image blurring due to off-resonance and fast T2* signal decay compared to PETRA. In in vivo imaging, GM-PETRA nicely captured complex structures of the inner ear such as the cochlea and semicircular canals. Gradient modulation can improve the PETRA image quality and mitigate SAR and RF peak power limitations without special hardware modification in clinical scanners. PMID:26771005

  15. Petra and the Nabataeans

    NASA Astrophysics Data System (ADS)

    Belmonte, Juan Antonio; González-García, A. César

    The Nabataeans built several monuments in Petra and elsewhere displaying decoration with a certain preference for astronomical motifs. A statistical analysis of the orientation of their sacred monuments demonstrates that astronomical orientations were often part of an elaborate plan and possibly reflect traces of the astral nature of Nabataean religion. Petra and other monuments in the ancient Nabataean kingdom demonstrate the interaction between landscape features and astronomical events. Among other things, the famous Ad Deir has revealed a fascinating ensemble of light and shadow effects, perhaps connected with the bulk of Nabataean mythology, while a series of suggestive solstitial and equinoctial alignments emanate from the impressive Urn Tomb, which might have helped bring about its selection as the cathedral of the city.

  16. The Extreme Conditions Beamline P02.2 and the Extreme Conditions Science Infrastructure at PETRA III

    PubMed Central

    Liermann, H.-P.; Konôpková, Z.; Morgenroth, W.; Glazyrin, K.; Bednarčik, J.; McBride, E. E.; Petitgirard, S.; Delitz, J. T.; Wendt, M.; Bican, Y.; Ehnes, A.; Schwark, I.; Rothkirch, A.; Tischer, M.; Heuer, J.; Schulte-Schrepping, H.; Kracht, T.; Franz, H.

    2015-01-01

    A detailed description is presented of the Extreme Conditions Beamline P02.2 for micro X-ray diffraction studies of matter at simultaneous high pressure and high/low temperatures at PETRA III, in Hamburg, Germany. This includes performance of the X-ray optics and instrumental resolution as well as an overview of the different sample environments available for high-pressure studies in the diamond anvil cell. Particularly emphasized are the high-brilliance and high-energy X-ray diffraction capabilities of the beamline in conjunction with the use of fast area detectors to conduct time-resolved compression studies in the millisecond time regime. Finally, the current capability of the Extreme Conditions Science Infrastructure to support high-pressure research at the Extreme Conditions Beamline and other PETRA III beamlines is described. PMID:26134794

  17. A compact and low-weight sputtering unit for in situ investigations of thin film growth at synchrotron radiation beamlines

    SciTech Connect

    Walter, P.; Dippel, A.-C.; Pflaum, K.; Wernecke, J.; Blume, J.; Hurk, J. van den; Klemradt, U.

    2015-05-15

    In this work, we report on a highly variable, compact, and light high-vacuum sputter deposition unit designed for in situ experiments using synchrotron radiation facilities. The chamber can be mounted at various synchrotron beamlines for scattering experiments in grazing incidence geometry. The sample position and the large exit window allow to perform x-ray experiments up to large q values. The sputtering unit is easy to mount on existing experimental setups and can be remote-controlled. In this paper, we describe in detail the design and the performance of the new sputtering chamber and present the installation of the apparatus at different 3rd generation light sources. Furthermore, we describe the different measurement options and present some selected results. The unit has been successfully commissioned and is now available for users at PETRA III at DESY.

  18. Jet physics at PEP and PETRA

    SciTech Connect

    Hofmann, W.

    1987-09-01

    Recent data on the fragmentation of quarks at PEP and PETRA energies is discussed in the context of phenomenological models of parton fragmentation. Emphasis is placed on the experimental evidence for parton showers as compared to a fixed order QCD treatment, on new data on inclusive hadron production and on detailed studies of baryon production in jets. 63 refs., 22 figs., 3 tabs.

  19. Hadron production at PEP/PETRA

    SciTech Connect

    Yamamoto, H.

    1985-12-01

    Recent results on hadron production in e/sup +/e/sup -/ annihilation at PEP and PETRA are summarized. The topics included are: (1) inclusive hadron production, (2) gluon vs quark jet, (3) analysis of 3 jet events and (4) p - anti p correlations. Experimental data are compared with predictions of several models to reveal underlying physics. 47 refs., 18 figs.

  20. An integrated pipeline for sample preparation and characterization at the EMBL@PETRA3 synchrotron facilities.

    PubMed

    Boivin, Stephane; Kozak, Sandra; Rasmussen, Gry; Nemtanu, Ioana Maria; Vieira, Vanessa; Meijers, Rob

    2016-02-15

    The characterization of macromolecular samples at synchrotrons has traditionally been restricted to direct exposure to X-rays, but beamline automation and diversification of the user community has led to the establishment of complementary characterization facilities off-line. The Sample Preparation and Characterization (SPC) facility at the EMBL@PETRA3 synchrotron provides synchrotron users access to a range of biophysical techniques for preliminary or parallel sample characterization, to optimize sample usage at the beamlines. Here we describe a sample pipeline from bench to beamline, to assist successful structural characterization using small angle X-ray scattering (SAXS) or macromolecular X-ray crystallography (MX). The SPC has developed a range of quality control protocols to assess incoming samples and to suggest optimization protocols. A high-throughput crystallization platform has been adapted to reach a broader user community, to include chemists and biologists that are not experts in structural biology. The SPC in combination with the beamline and computational facilities at EMBL Hamburg provide a full package of integrated facilities for structural biology and can serve as model for implementation of such resources for other infrastructures. PMID:26255961

  1. Recent results on baryon production at PETRA

    SciTech Connect

    Wu, S.L.

    1982-01-01

    One of the recent excitements at PETRA is the observation of the copious production of baryons. About a year ago, TASSO observed the inclusive production of protons and antiprotons. More recently JADE confirmed the inclusive antiproton spectrum to about 1 GeV/c and also observed the inclusive anti ..lambda.. spectrum to about 1.4 GeV/c, while TASSO obtained the ..lambda.. and anti-..lambda.. spectrum all the way up 10 GeV/c in momentum.

  2. e/sup +/e/sup -/ collisions: results from PETRA

    SciTech Connect

    Hilger, E.

    1982-01-01

    A selection of most recent results obtained by the five experiments CELLO, JADE, MARK J, PLUTO, and TASSO at PETRA is presented. The many interesting new results include, for example, the observation of effects of 2nd order QCD, details of inclusive hadron production, and the measurement of the forward-backward asymmetry in lepton pair production due to weak and electromagnetic interference.

  3. Hutch for CSX Beamlines

    SciTech Connect

    Ed Haas

    2012-12-12

    NSLS-II will produce x-rays 10,000 times brighter than NSLS. To keep people safe from intense x-rays in the new facility, special enclosures, called hutches, will surround particular sections of beamlines.

  4. G4beamline

    Energy Science and Technology Software Center (ESTSC)

    2011-05-24

    G4beamline is a single-particle-tracking simulation code based on the Geant4 toolkit. It is specifically optimized for the realistic evaluation of beam lines. It is especially useful for evaluating future muon facilities.

  5. Hutch for CSX Beamlines

    ScienceCinema

    Ed Haas

    2013-07-17

    NSLS-II will produce x-rays 10,000 times brighter than NSLS. To keep people safe from intense x-rays in the new facility, special enclosures, called hutches, will surround particular sections of beamlines.

  6. The SLS optics beamline

    SciTech Connect

    Flechsig, U.; Abela, R.; Betemps, R.; Blumer, H.; Frank, K.; Jaggi, A.; MacDowell A.A.; Padmore, H.A.; Schonherr, V.; Ulrich, J.; Walther, H.; Zelenika, S.; Zumbach, C.

    2006-05-20

    A multipurpose beamline for tests and developments in the field of x-ray optics and synchrotron radiation instrumentation in general is under construction at the Swiss Light Source (SLS) bending magnet X05DA. The beamline uses a newly developed UHV compatible, 100 mm thick, brazed CVD diamond vacuum window. The very compact cryogenically cooled channel cut Si(111) monochromator and bendable 1:1 toroidal focusing mirror at 7:75 m from the source point are installed inside the shielding tunnel. The beamline covers a photon energy range of about 6 to 17 keV.We expect 5x1011 photons=s within a 100 mu m spot and a resolving power of 1300. The monochromator and focusing mirror can be retracted independently for unfocused monochromatic and focused ''white'' light operation respectively.

  7. The SLS Optics Beamline

    SciTech Connect

    Flechsig, U.; Abela, R.; Betemps, R.; Blumer, H.; Jaggi, A.; Schoenherr, V.; Ulrich, J.; Walther, H.; Zumbach, C.; Frank, K.; MacDowell, A. A.; Padmore, H. A.; Zelenika, S.

    2007-01-19

    A multipurpose beamline for tests and developments in the field of x-ray optics and synchrotron radiation instrumentation in general is under construction at the Swiss Light Source (SLS) bending magnet X05DA. The beamline uses a newly developed UHV compatible, 100 {mu}m thick, brazed CVD diamond vacuum window. The very compact cryogenically cooled channel cut Si(111) monochromator and bendable 1:1 toroidal focusing mirror at 7.75m from the source point are installed inside the shielding tunnel. The beamline covers a photon energy range of about 6 to 17 keV. We expect 5 {center_dot} 1011 photons/s within a 100 {mu}m spot and a resolving power of 1300. The monochromator and focusing mirror can be retracted independently for unfocused monochromatic and focused ''white'' light operation respectively.

  8. Automatic beamline calibration procedures

    SciTech Connect

    Corbett, W.J.; Lee, M.J.; Zambre, Y.

    1992-03-01

    Recent experience with the SLC and SPEAR accelerators have led to a well-defined set of procedures for calibration of the beamline model using the orbit fitting program, RESOLVE. Difference orbit analysis is used to calibrate quadrupole strengths, BPM sensitivities, corrector strengths, focusing effects from insertion devices, and to determine the source of dispersion and coupling errors. Absolute orbit analysis is used to locate quadrupole misalignments, BPM offsets, or beam loss. For light source applications, the photon beam source coordinates can be found. The result is an accurate model of the accelerator which can be used for machine control. In this paper, automatable beamline calibration procedures are outlined and illustrated with recent examples. 5 refs.

  9. Sun Cities: Thebes, Hattusha, and Petra: A Landscape Story

    NASA Astrophysics Data System (ADS)

    Belmonte, J. A.; González-García, A. C.

    2016-01-01

    The sky is a very important component of the landscape that has been lost in our modern, overcrowded, and excessively illuminated cities. However, this was not the case in the past. Astronomy played a highly relevant role in urban planning, especially in the organization of sacred spaces which were later surrounded by extensive civil urban areas. Today, archaeoastronomy approaches the minds of our ancestors studying the starry landscape and how it is printed in the terrain by the visualization and the orientation of sacred buildings. The sun was indeed the most important component of that celestial landscape and was the primary focus within a large set of unique cultures of great historical significance. In particular, we will study and compare the case of three sun cities: Thebes (Belmonte et al. 2009, Belmonte 2012), Hattusha (Gonzalez-Garcia & Belmonte 2011), and Petra (Belmonte et al. 2013), capitals of Egypt in the Middle and New Kingdoms, the Hittite Empire, and the Nabataean Kingdom, respectively. We will briefly discuss each of these cultures and will scrutinize their capital cities, showing how their strategic geographical position and orography were of key importance, but also how solar observation, and related hierophanies, played a relevant role in the orientation and location of some of their most significant monuments. In particular, we will focus on the great temple of Amun-Re in Karnak, Temple 1 in Hattusha (presumably devoted to the Solar Goddess of Arinna), and the “Monastery” at Petra.

  10. Ionic composition of wet precipitation in the Petra Region, Jordan

    NASA Astrophysics Data System (ADS)

    Al-Khashman, Omar A.

    2005-11-01

    The results of chemical analysis of precipitation samples collected in Petra between October 2002 and May 2004 are presented. All samples were analyzed for major cations (NH 4+, Na +, K +, Ca 2+ and Mg 2+), major anions (Cl -, NO 3-, HCO 3- and SO 42-), conductivity and pH. The daily sample pH values ranged from 5.71 to 8.15 with an average value of 6.85 ± 0.5. Rainwater quality is characterized by low salinity and neutralized pH. Generally, the pH is high due to dust in the atmosphere, which contains a large fraction of calcite. Factor analysis was used to identify the factors that affect the presence of ions in wet precipitation; these factors permitted the identification of three source groups, namely crustal dust, sea-salt spray and combustion products. In general, the results of the present study suggest that the atmospheric composition in the Petra region is strongly influenced by natural sources rather than anthropogenic sources.

  11. PLS photoemission electron microscopy beamline

    NASA Astrophysics Data System (ADS)

    Kang, Tai-Hee; Kim, Ki-jeong; Hwang, C. C.; Rah, S.; Park, C. Y.; Kim, Bongsoo

    2001-07-01

    The performance of a recently commissioned beamline at the Pohang Light Source (PLS) is described. The beamline, which is located at 4B1 at PLS, is a Varied Line Spacing (VLS) Plane Grating Monochromator (PGM) beamline. VLS PGM has become very popular because of the simple scanning mechanism and the fixed exit slit. The beamline which takes 3 mrad horizontal beam fan from bending magnet, covers the energy range 200-1000 eV for Photoemission Electron Microscopy (PEEM), X-ray Photoelectron Spectroscopy (XPS) and Magnetic Circular Dichroism (MCD) experiments. Simplicity of the optics and high flux with medium resolution were the design goals for these applications. The beamline consists of a horizontal focusing mirror, a vertical focusing mirror, VLS plane grating and exit slit. The source of PLS could be used as a virtual entrance slit because of its small size and stability. The flux and the resolution of the beamline at the experimental station have been measured using an ion chamber and a calibrated photodiode. Test images of PEEM from a standard sample were taken to illustrate the further performance of the beamline and PEEM station.

  12. SRI CAT Section 1 bending magnet beamline description

    SciTech Connect

    Srajer, G.; Rodricks, B.; Assoufid, L.; Mills, D.M.

    1994-03-10

    This report discusses: APS bending magnet source; beamline layout; beamline optical components; beamline operation; time-resolved studies station; polarization studies station; and commissioning and operational schedule.

  13. SPring-8 Structural Biology Beamlines / Automatic Beamline Operation at RIKEN Structural Genomics Beamlines

    SciTech Connect

    Ueno, Go; Hasegawa, Kazuya; Okazaki, Nobuo; Sakai, Hisanobu; Kumasaka, Takashi; Yamamoto, Masaki

    2007-01-19

    RIKEN Structural Genomics Beamlines (BL26B1 and BL26B2) at SPring-8 have been constructed for high throughput protein crystallography. The beamline operation is automated cooperating with the sample changer robot. The operation software provides a centralized control utilizing the client and server architecture. The sample management system with the networked database has been implemented to accept dry-shipped crystals from distant users.

  14. Enemy Images, Developmental Psychology, And Peace Education. Peace Education Miniprints No. 29. Petra Hesse and the Project "Preparedness for Peace."

    ERIC Educational Resources Information Center

    Lund Univ. (Sweden). Malmo School of Education.

    An interview on peace education with Petra Hesse, of the Center for Psychological Studies in the Nuclear Age (Cambridge, Massachusetts), is presented. The Center for Psychological Studies in the Nuclear Age was founded out of a concern about children's fears of the future and the risks of nuclear war. Petra Hesse coordinates a research project on…

  15. Advanced beamline automation for biological crystallography experiments.

    PubMed

    Cork, Carl; O'Neill, James; Taylor, John; Earnest, Thomas

    2006-08-01

    An automated crystal-mounting/alignment system has been developed at Lawrence Berkeley National Laboratory and has been installed on three of the protein-crystallography experimental stations at the Advanced Light Source (ALS); it is currently being implemented at synchrotron crystallography beamlines at CHESS, NSLS and the APS. The benefits to using an automounter system include (i) optimization of the use of synchrotron beam time, (ii) facilitation of advanced data-collection techniques, (iii) collection of higher quality data, (iv) reduction of the risk to crystals and (v) exploration of systematic studies of experimental protocols. Developments on the next-generation automounter with improvements in robustness, automated alignment and sample tracking are under way, with an end-to-end data-flow process being developed to allow remote data collection and monitoring. PMID:16855300

  16. Fast fluorescence techniques for crystallography beamlines

    PubMed Central

    Stepanov, Sergey; Hilgart, Mark; Yoder, Derek W.; Makarov, Oleg; Becker, Michael; Sanishvili, Ruslan; Ogata, Craig M.; Venugopalan, Nagarajan; Aragão, David; Caffrey, Martin; Smith, Janet L.; Fischetti, Robert F.

    2011-01-01

    This paper reports on several developments of X-ray fluorescence techniques for macromolecular crystallography recently implemented at the National Institute of General Medical Sciences and National Cancer Institute beamlines at the Advanced Photon Source. These include (i) three-band on-the-fly energy scanning around absorption edges with adaptive positioning of the fine-step band calculated from a coarse pass; (ii) on-the-fly X-ray fluorescence rastering over rectangular domains for locating small and invisible crystals with a shuttle-scanning option for increased speed; (iii) fluorescence rastering over user-specified multi-segmented polygons; and (iv) automatic signal optimization for reduced radiation damage of samples. PMID:21808424

  17. Decay of sandstone monuments in Petra (Jordan): Gravity-induced stress as a stabilizing factor

    NASA Astrophysics Data System (ADS)

    Řihošek, Jaroslav; Bruthans, Jiří; Mašín, David; Filippi, Michal; Schweigstillova, Jana

    2016-04-01

    As demonstrated by physical experiments and numerical modeling the gravity-induced stress (stress in further text) in sandstone massive reduces weathering and erosion rate (Bruthans et al. 2014). This finding is in contrast to common view that stress threatens stability of man-made monuments carved to sandstone. Certain low- levels of gravity-induced stress can in fact stabilize and protect these forms against weathering and disintegration. The purpose of this investigation is to evaluate the effect of the stress on weathering of sandstone monuments at the Petra World Heritage Site in Jordan via field observations, salt weathering experiments, and physical and numerical modeling. Previous studies on weathering of Petra monuments have neglected the impact of stress, but the ubiquitous presence of stress-controlled landforms in Petra suggests that it has a substantial effect on weathering and erosion processes on man-made monuments and natural surfaces. Laboratory salt weathering experiments with cubes of Umm Ishrin sandstone from Petra demonstrated the inverse relationship between stress magnitude and decay rate. Physical modeling with Strelec locked sand from the Czech Republic was used to simulate weathering and decay of Petra monuments. Sharp forms subjected to water erosion decayed to rounded shapes strikingly similar to tombs in Petra subjected to more than 2000 years of weathering and erosion. The physical modeling results enabled visualization of the recession of monument surfaces in high spatial and temporal resolution and indicate that the recession rate of Petra monuments is far from constant both in space and time. Numerical modeling of stress fields confirms the physical modeling results. This novel approach to investigate weathering clearly demonstrates that increased stress decreases the decay rate of Petra monuments. To properly delineate the endangered zones of monuments, the potential damage caused by weathering agents should be combined with stress

  18. High power photon beamline elements in the LBL/SSRL/EXXON Beamline VI

    SciTech Connect

    Hoyer, E.

    1992-09-01

    Beamline VI is a wiggler-based, multi-kilowatt, intense synchrotron radiation beamline installed SPEAR. The thermal design parameters for this beamline are presented and then design considerations and construction descriptions are given for many of the high-power photon beamline elements.

  19. Particle searches in e/sup +/e/sup -/ experiments at PEP and PETRA

    SciTech Connect

    Lau, K.H.

    1982-10-01

    This talk reviews recent results in new particle searches performed by experiments at the high energy e/sup +/e/sup -/ storage rings PEP and PETRA. It concentrates on recent searches for: hadrons with a new quark flavor, spin-1/2 charged heavy leptons, spin-0 charged leptons, spin-0 point-like scalars or pseudoscalars, and neutral heavy leptons.

  20. ALS beamline design requirements: A guide for beamline designers

    SciTech Connect

    1996-06-01

    This manual is written as a guide for researchers in designing beamlines and endstations acceptable for use at the ALS. It contains guidelines and policies related to personnel safety and equipment and vacuum protection. All equipment and procedures must ultimately satisfy the safety requirements set aside in the Lawrence Berkeley National Laboratory (LBNL) Health and Safety Manual (PUB-3000) which is available from the ALS User Office or on the World WideWeb from the LBNL Homepage (http:// www.lbl.gov).

  1. Beamline 10: A multipole wiggler beamline at SSRL

    SciTech Connect

    Karpenko, V.; Kinney, J. H.; Kulkarni, S.; Neufeld, K.; Poppe, C.; Tirsell, K. G.; Wong, J.; Cerino, J.; Troxel, T.; Yang, J.; and others

    1989-07-01

    A beamline has been constructed at Stanford Synchrotron Radiation Laboratory (SSRL) whose radiation source is a multipole permanent magnet wiggler installed in a straight section of the SPEAR 3--3.5 GeV electron storage ring. The wiggler is a hybrid design that utilizes Nd--Fe alloy magnet material combined with Vanadium Permendur poles. It is approximately 2 m long and has 15 full wiggler periods. Its field is regulated by varying its gap height. It has a peak operating field, limited by the electron beam vacuum chamber vertical aperture, of 1.4 T. The beamline consists of vacuum, safety, and optical components capable of transporting photons to one hard x-ray (3--30 keV) end station, with provisions for implementing up to two additional branch lines. The existing hard x-ray branch can be focused by a Pt-coated toroidal mirror with a cutoff energy of approximately 22 keV. The experimental end station is serviced by a Hower--Brown type double crystal monochromator. The wiggler and beamline construction was completed in the fall of 1987 and was operated for a brief period for characterization and experimental use. We present design details and results of the initial characterization studies.

  2. Beamline 10: A multipole wiggler beamline at SSRL (invited)

    NASA Astrophysics Data System (ADS)

    Karpenko, V.; Kinney, J. H.; Kulkarni, S.; Neufeld, K.; Poppe, C.; Tirsell, K. G.; Wong, J.; Cerino, J.; Troxel, T.; Yang, J.; Hoyer, E.; Green, M.; Humphries, D.; Marks, S.; Plate, D.

    1989-07-01

    A beamline has been constructed at Stanford Synchrotron Radiation Laboratory (SSRL) whose radiation source is a multipole permanent magnet wiggler installed in a straight section of the SPEAR 3-3.5 GeV electron storage ring. The wiggler is a hybrid design that utilizes Nd-Fe alloy magnet material combined with Vanadium Permendur poles. It is approximately 2 m long and has 15 full wiggler periods. Its field is regulated by varying its gap height. It has a peak operating field, limited by the electron beam vacuum chamber vertical aperture, of 1.4 T. The beamline consists of vacuum, safety, and optical components capable of transporting photons to one hard x-ray (3-30 keV) end station, with provisions for implementing up to two additional branch lines. The existing hard x-ray branch can be focused by a Pt-coated toroidal mirror with a cutoff energy of approximately 22 keV. The experimental end station is serviced by a Hower-Brown type double crystal monochromator. The wiggler and beamline construction was completed in the fall of 1987 and was operated for a brief period for characterization and experimental use. We present design details and results of the initial characterization studies.

  3. Design of the LBNF Beamline

    SciTech Connect

    Papadimitriou, V.; Andrews, R.; Hylen, J.; Kobilarcik, T.; Krafczyk, G.; Marchinonni, A.; Moore, C. D.; Schlabach, P.; Tariq, S.

    2015-08-30

    The Long Baseline Neutrino Facility (LBNF) will utilize a beamline located at Fermilab to carry out a compelling research program in neutrino physics. The facility will aim a wide band neutrino beam toward underground detectors placed at the SURF Facility in South Dakota, about 1,300 km away. The main elements of the facility are a primary proton beamline and a neutrino beamline. The primary proton beam (60-120 GeV) will be extracted from the MI-10 section of Fermilab’s Main Injector. Neutrinos are produced after the protons hit a solid target and produce mesons which are subsequently focused by magnetic horns into a 204 m long decay pipe where they decay into muons and neutrinos. The parameters of the facility were determined taking into account the physics goals, spacial and radiological constraints and the experience gained by operating the NuMI facility at Fermilab. The initial proton beam power is expected to be 1.2 MW; however, the facility is designed to be upgradeable to 2.4 MW. We discuss here the design status and the associated challenges as well as plans for improvements before baselining the facility.

  4. Design of the LBNE Beamline

    SciTech Connect

    Papadimitriou, Vaia; Andrews, Richard; Hylen, James; Kobilarcik, Thomas; Marchionni, Alberto; Moore, Craig D.; Schlabach, Phil; Tariq, Salman

    2015-02-05

    The Long Baseline Neutrino Experiment (LBNE) will utilize a beamline facility located at Fermilab to carry out a compelling research program in neutrino physics. The facility will aim a wide band beam of neutrinos toward a detector placed at the Sanford Underground Research Facility in South Dakota, about 1,300 km away. The main elements of the facility are a primary proton beamline and a neutrino beamline. The primary proton beam (60-120 GeV) will be extracted from the MI-10 section of Fermilab’s Main Injector. Neutrinos are produced after the protons hit a solid target and produce mesons which are sign selected and subsequently focused by a set of magnetic horns into a 204 m long decay pipe where they decay mostly into muons and neutrinos. The parameters of the facility were determined taking into account the physics goals, spacial and radiological constraints, and the experience gained by operating the NuMI facility at Fermilab. The initial beam power is expected to be ~1.2 MW; however, the facility is designed to be upgradeable for 2.3 MW operation. We discuss here the status of the design and the associated challenges.

  5. SPring-8 beamline control system.

    PubMed

    Ohata, T; Konishi, H; Kimura, H; Furukawa, Y; Tamasaku, K; Nakatani, T; Tanabe, T; Matsumoto, N; Ishii, M; Ishikawa, T

    1998-05-01

    The SPring-8 beamline control system is now taking part in the control of the insertion device (ID), front end, beam transportation channel and all interlock systems of the beamline: it will supply a highly standardized environment of apparatus control for collaborative researchers. In particular, ID operation is very important in a third-generation synchrotron light source facility. It is also very important to consider the security system because the ID is part of the storage ring and is therefore governed by the synchrotron ring control system. The progress of computer networking systems and the technology of security control require the development of a highly flexible control system. An interlock system that is independent of the control system has increased the reliability. For the beamline control system the so-called standard model concept has been adopted. VME-bus (VME) is used as the front-end control system and a UNIX workstation as the operator console. CPU boards of the VME-bus are RISC processor-based board computers operated by a LynxOS-based HP-RT real-time operating system. The workstation and the VME are linked to each other by a network, and form the distributed system. The HP 9000/700 series with HP-UX and the HP 9000/743rt series with HP-RT are used. All the controllable apparatus may be operated from any workstation. PMID:15263588

  6. After three decades of research, is the Nabataean city of Petra still under threat?

    NASA Astrophysics Data System (ADS)

    Gomez-Heras, M.; Lopez-Arce, P.; Bala'awi, F.; Ishakat, F.; Alvarez de Buergo, M.; Fort, R.; Wedekind, W.

    2012-04-01

    The year 2012 marks the 200th anniversary of the rediscovering of the Nabataean city of Petra (Jordan) by Swiss archaeologist Johann Ludwig Burckhardt. The city of Petra is one of the most singular built-heritage monumental sets in the world because of the size of the built structures, the extension in which these structures appear and the intricate relation between natural and built environment in the site. These are part of the reasons of its uniqueness that conducted to its inscription as a UNESCO World Heritage Site in 1985. However, the conservation and management of such a large archaeological site can be very challenging due to the diverse decay processes and agents operating on the site. As a result, the site conservation has been heavily hindered in the past and Petra was included in 1998, 2000 and 2002 in the former World Monuments Fund list of the one hundred most endangered sites (now World Monuments Watch). It also was described as one of the most endangered world heritage sites in the ICOMOS reports "Heritage at risk". Many studies on the decay processes that operate in Petra have been carried out from the point of view of earth sciences, from the first studies carried out in the 80's by many researchers from several countries, funded by very different funding schemes; sometimes working on different specific topics within the high variability of existing problems in Petra, but sometimes, working in parallel without communication. In addition to this, many of the studies carried out locally have not been published internationally and therefore neither have not reached the wider scientific community nor the local decision makers. Petra is, therefore, a good example of how a complex and large site may favour a research environment in which scientific results are fragmentary and synergies are not generated, moreover when it should be approached under inter and multidisciplinary teams. These synergies could be of great benefit, not only to the scientific

  7. Beamline 9.0.1 - a high-resolution undulator beamline for gas-phase spectroscopy

    SciTech Connect

    Bozek, J.D.; Heimann, P.A.; Mossessian, D.

    1997-04-01

    Beamline 9.0.1 at the Advanced Light Source is an undulator beamline with a Spherical Grating Monochromator (SGM) which provides very high resolution and flux over the photon energy range 20-320eV. The beamline has been used primarily by the atomic and molecular science community to conduct spectroscopy experiments using electron, ion and fluorescence photon detection. A description of the beamline and its performance will be provided in this abstract.

  8. Status of the crystallography beamlines at SSRF

    NASA Astrophysics Data System (ADS)

    He, Jianhua; Gao, Xingyu

    2015-02-01

    The Shanghai Synchrotron Radiation Facility (SSRF), an advanced intermediate-energy third-generation light source in China, was completed with seven phase-I beamlines opening to users in May 2009. Among these beamlines, there are two dedicated crystallography beamlines, one for macromolecular crystallography and one for crystallography in materials science, condensed matter physics and other relevant fields. The macromolecular crystallography beamline BL17U1, based on an in-vacuum undulator, has achieved very high brightness at the sample position with its flux of 4.1 × 1012 photons/s at 12 keV and focused beam size of FWHM (H × V) 67 × 23 μm2 in a small beam divergence over an energy range of 5-18 keV. Nowadays, there are about 200 user groups at this beamline with more than 330 structures solved each year. In the past, lots of significant results have been obtained at this beamline, such as the structural determination of important membrane proteins and proteins of viruses. In addition, three new macromolecular crystallography beamlines of different features have just been constructed and will soon open to users. To meet the rapidly growing user demands and the important scientific challenges, a few more dedicated crystallography beamlines have been proposed in the Phase-II Beamlines Project.

  9. Performance Measurements at the SLS Spectroscopy Beamline

    SciTech Connect

    Flechsig, U.; Patthey, L.; Schmidt, T.

    2004-05-12

    The Surfaces and Interfaces Spectroscopy beamline (SIS) started user operation in spring 2002 as one of the first beamlines at SLS. It is optimized for high resolution photo electron spectroscopy. The beamline concept with two helical undulators plus a plane grating monochromator with grazing- and normal incidence optics is very flexible and offers a well balanced performance from 10 eV to 800 eV. We report on beamline features and performance measurements. The final characterization is still in progress since not all options have been commissioned so far.

  10. Decontamination, Dismantling and Refurbishing of the PETRA Glove Box at the Tritium Laboratory, Karlsruhe

    SciTech Connect

    Caldwell-Nichols, C.J.; Glugla, M.; Doerr, L.; Berndt, U.

    2005-07-15

    The PETRA facility at the Tritium Laboratory Karlsruhe (TLK) has finished its useful life and the glove box and auxiliary systems are being refurbished. During the lifetime of PETRA the glove box became contaminated with a small amount of tritium but the source has not been positively identified. Removing large redundant components would be hazardous as this would require removing the glove box panels and thus exposing the inner surfaces to moist air which would release tritium. Over several months defined amounts of water have been introduced into the glove box daily which has liberated significant quantities of tritium which has subsequently been absorbed by the in-built tritium retention system. This technique has slowly reduced the tritium liberated at each step. The large components, such as a getter bed, catalyst bed and a permeator, have been detritiated as far as possible in-situ in readiness for disposal once it is safe to remove them from the glove box.

  11. Dismantling of the PETRA glove box: tritium contamination and inventory assessment

    SciTech Connect

    Wagner, R.

    2015-03-15

    The PETRA facility is the first installation in which experiments with tritium were carried out at the Tritium Laboratory Karlsruhe. After completion of two main experimental programs, the decommissioning of PETRA was initiated with the aim to reuse the glove box and its main still valuable components. A decommissioning plan was engaged to: -) identify the source of tritium release in the glove box, -) clarify the status of the main components, -) assess residual tritium inventories, and -) de-tritiate the components to be disposed of as waste. Several analytical techniques - calorimetry on small solid samples, wipe test followed by liquid scintillation counting for surface contamination assessment, gas chromatography on gaseous samples - were deployed and cross-checked to assess the remaining tritium inventories and initiate the decommissioning process. The methodology and the main outcomes of the numerous different tritium measurements are presented and discussed. (authors)

  12. An artistic and mythological study of a Nabatean female Sphinx from Petra, Jordan.

    NASA Astrophysics Data System (ADS)

    Almasri, Eyad R.; Al-Ajlouny, Fardous K.; Alghazawi, Raed Y.

    In 1967 the Group of Sculptures was discovered in Petra during clearance works organized by the Department of Antiquities in Jordan in the Temenos of Qasr el Bint around the Temenos Gate. One of these sculptures was a high relief statue of a female sphinx. Due to the paucity of information about this statue, this paper has been written to answer a number of questions: What was its original site or monument? When was it made? Who was the deity or deities it represented? Could there be another interpretation of its existence? The answers to the above provide enlightenment of Nabataean styles of carvings and an insight into their religious thoughts. Rgarding the interpretation of the Female Sphinx. Three ideas have been suggested. First, it can be the main Nabataean goddess Allat, "the mother of the gods". Second, it is an image of Petra as a goddess. Third, it is carved on the Temenos Gate as a guardian of Petra city in general and its holy monuments like temples and tombs in particular.

  13. BNL ATF II beamlines design

    SciTech Connect

    Fedurin, M.; Jing, Y.; Stratakis, D.; Swinson, C.

    2015-05-03

    The Brookhaven National Laboratory. Accelerator Test Facility (BNL ATF) is currently undergoing a major upgrade (ATF-II). Together with a new location and much improved facilities, the ATF will see an upgrade in its major capabilities: electron beam energy and quality and CO2 laser power. The electron beam energy will be increased in stages, first to 100-150 MeV followed by a further increase to 500 MeV. Combined with the planned increase in CO2 laser power (from 1-100 TW), the ATF-II will be a powerful tool for Advanced Accelerator research. A high-brightness electron beam, produced by a photocathode gun, will be accelerated and optionally delivered to multiple beamlines. Besides the energy range (up to a possible 500 MeV in the final stage) the electron beam can be tailored to each experiment with options such as: small transverse beam size (<10 um), short bunch length (<100 fsec) and, combined short and small bunch options. This report gives a detailed overview of the ATFII capabilities and beamlines configuration.

  14. 76 FR 54468 - Petra Pet, Inc. (a/k/a Petrapport) v. Panda Logistics Limited; Panda Logistics Co., Ltd. (f/k/a...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2011-09-01

    ... Petra Pet, Inc. (a/k/a Petrapport) v. Panda Logistics Limited; Panda Logistics Co., Ltd. (f/k/a panda... Petra Pet, Inc. (a/k/a Petrapport), hereinafter ``Complainant,'' against Respondents Panda Logistics Limited, Panda Logistics Co., Ltd. (f/k/a Panda Int'l Transportation Co., Ltd), and RDM Solutions...

  15. Diagnostic X-Multi-Axis Beamline

    SciTech Connect

    Paul, A C

    2000-04-05

    Tomographic reconstruction of explosive events require time resolved multipal lines of sight. Considered here is a four (or eight) line of sight beam layout for a nominal 20 MeV 2000 Ampere 2 microsecond electron beam for generation of x-rays 0.9 to 5 meters from a given point, the ''firing point''. The requirement of a millimeter spatial x-ray source requires that the electron beam be delivered to the converter targets with sub-millimeter precision independent of small variations in beam energy and initial conditions. The 2 usec electron beam pulse allows for four bursts in each line, separated in time by about 500 microseconds. Each burst is divided by a electro-magnetic kicker into four (or eight) pulses, one for each beamline. The arrival time of the four (or eight) beam pulses at the x-ray target can be adjusted by the kicker timing and the sequence that the beams of each burst are switched into the different beamlines. There exists a simple conceptual path from a four beamline to a eight beamline upgrade. The eight line beamline is built up from seven unique types of sub-systems or ''blocks''. The beamline consists of 22 of these functional blocks and contains a total of 455 individual magnets, figure 1. The 22 blocks are inter-connected by a total of 30 straight line inter-block sections (IBS). Beamlines 1-4 are built from 12 blocks with conceptual layout structure shown in figure 2. Beamlines 5-8 are built with an additional 10 blocks with conceptual layout structure shown in figure 3. This beamline can be thought of as looking like a lollipop consisting of a 42 meter long stick leading to a 60 by 70 meter rectangular candy blob consisting of the eight lines of sight. The accelerator providing the electron beam is at the end of the stick and the firing point is at the center of the blob. The design allows for a two stage implementation. Beamlines 1-3 can be installed to provide a tomographic azimuthal resolution of 45 degrees. An upgrade can later be made

  16. Innovations in the design of mechanical components for a beamline -- The SRl`95 Workshop 2 summary

    SciTech Connect

    Kuzay, T.M.; Warwick, T.

    1995-12-31

    The Synchrotron Radiation Instrumentation 1995 Conference (SRI`95) was hosted by the Advanced Photon Source (APS) at Argonne National Laboratory (ANL). Of the many workshops within the conference, the SRI`95 Workshop 2 was ``Innovations in the Design of Mechanical Components of a Beamline``. The workshop was attended well with over 140 registrants. The following topics were discussed. Industry`s perspective on the status and future was provided by Huber Diffrationtechnik, Oxford Instruments, and Kohzu Seiko Ltd. on goniometers/diffractometers, advanced manufacturing technique of high heat load components, such as the APS photon shutter, and the specialties of monochromators provided to the third-generation synchrotrons, respectively. This was followed by a description of the engineering of a dual function monochromator design for water-cooled diamond or cryogenically cooled silicon monochromators by CMC CAT/APS. Another category was the nagging problem of sensitivity of the photon beam position monitors (XBPM) to bending magnet radiation (``BM contamination``) and the undulator magnet gap changes. Problem descriptions and suggested solutions were provided by both the Advanced Light Source (ALS) and the APS. Other innovative ideas were the cooling schemes (enhanced cooling of beamline components using metallic porous meshes including cryo-cooled applications); Glidcop photon shutter design using microchannels at the ALS; and window/filter design, manufacture and operational experiences at CHESS and PETRA/HASYLAB. Additional discussions were held on designing for micromotions and precision in the optical support systems and smart user filter schemes. This is a summary of the presentations at the Workshop. 5 refs., 5 figs.

  17. Status of the crystallography beamlines at Elettra

    NASA Astrophysics Data System (ADS)

    Lausi, A.; Polentarutti, M.; Onesti, S.; Plaisier, J. R.; Busetto, E.; Bais, G.; Barba, L.; Cassetta, A.; Campi, G.; Lamba, D.; Pifferi, A.; Mande, S. C.; Sarma, D. D.; Sharma, S. M.; Paolucci, G.

    2015-03-01

    Elettra is one of the first 3rd-generation storage rings, recently upgraded to routinely operate in top-up mode at both 2.0 and 2.4 GeV. The facility hosts four dedicated beamlines for crystallography, two open to the users and two under construction, and expected to be ready for public use in 2015. In service since 1994, XRD1 is a general-purpose diffraction beamline. The light source for this wide (4-21 keV) energy range beamline is a permanent magnet wiggler. XRD1 covers experiments ranging from grazing incidence X-ray diffraction to macromolecular crystallography, from industrial applications of powder diffraction to X-ray phasing with long wavelengths. The bending magnet powder diffraction beamline MCX has been open to users since 2009, with a focus on microstructural investigations and studies under non-ambient conditions. A superconducting wiggler delivers a high photon flux to a new fully automated beamline dedicated to macromolecular crystallography and to a branch beamline hosting a high-pressure powder X-ray diffraction station (both currently under construction). Users of the latter experimental station will have access to a specialized sample preparation laboratory, shared with the SISSI infrared beamline. A high throughput crystallization platform equipped with an imaging system for the remote viewing, evaluation and scoring of the macromolecular crystallization experiments has also been established and is open to the user community.

  18. Real Beamline Optics from a Synthetic Beam

    SciTech Connect

    Ryan Bodenstein,Michael Tiefenback,Yves Roblin

    2010-05-01

    The Continuous Electron Beam Accelerator Facility (CEBAF) at Jefferson Lab can be described as a series of concatenated beamlines. Methods used to measure the Twiss parameters in closed orbit machines are not applicable in such open ended systems. We are using properly selected sets of real orbits in the accelerator, as one would for numerical analysis. The evolution of these trajectories along the beamline models the behavior of a synthetic beam which deterministically supplements beam profile-based Twiss parameter measurements and optimizes the efficiency of beamline tuning. Examples will be presented alongside a description of the process.

  19. A Dedicated THz Beamline At BESSY

    NASA Astrophysics Data System (ADS)

    Holldack, K.; Ponwitz, D.

    2007-01-01

    A special beamline dedicated to the Far Infrared (THz) region was successfully commissioned at BESSY for the spectral range between 50 GHz and 4.5 THz. The beamline accepts synchrotron radiation from a bend magnet source close to the interaction region of a femtosecond laser with the electron bunch. Either edge radiation as well as the regular bend magnet fan can be accepted. The beamline was tailored for diagnostics and experiments employing coherent synchrotron radiation (CSR) from regular and compressed bunches as well as from a laser-induced fs density modulation on the electron bunch. Besides a technical description of the beamlinethe the sources are compared using Fourier Transform Spectroscopy (FTIR).

  20. Microspectroscopy At Beamline 73 MAX-lab

    SciTech Connect

    Engdahl, Anders

    2010-02-03

    Presentation of some projects at the infrared microspectroscopy experimental station at beamline 73 MAX-lab. Among the subjects are found identification of organic residues in fossil material and examination of the chemistry in an old oak wood wreck.

  1. Ring beamlines and instrumentation for industrial applications

    NASA Astrophysics Data System (ADS)

    Pearce, W. Jorge; Trippe, Anthony P.

    1994-08-01

    Many recently constructed storage rings are catering to the needs of industrial applications in addition to providing the traditional services required for synchrotron radiation research. The Center for Advanced Microstructures and Devices (CAMD) was established by Louisiana State University to pioneer development of microfabrication while supporting research in basic science. Maxwell Laboratories designed, built, and successfully commissioned the 1.2 GeV, 400 mA light source for CAMD. Maxwell Laboratories has completed one X-ray lithography beamline at CAMD, and two more are now being manufactured. The completed beamline system, designed for thin resists, delivers photons up to 2 keV. The two beamlines currently under construction deliver photons up to 6 keV for thick (> 50 μm) resists, which play a role in the fabrication of 3-D nanostructures. One of the thick-resist beamlines includes an aspheric mirror that collimates the synchrotron-radiation beam in the horizontal plane while focusing it in the vertical direction - creating a sharp, uniform line image at the workpiece. The other thick-resist beamline has conventional planar optics. Beam position monitors (BPMs) developed for the CAMD beamlines provide a precise vertical profile of the beam by measuring differential photocurrents generated in the BPM probes. Beam power measurements are accomplished with a fixed-aperture calorimeter. Since each calorimeter is precisely calibrated before shipment, its thermal response in the beam is an accurate means to determine beam power for setting lithography exposure times or for computing beamline energy balance.

  2. Modeling of X-ray beamlines and devices

    SciTech Connect

    Ice, G.E.

    1996-12-31

    X-ray beamlines on synchrotron sources are similar in size and complexity to beamlines at state-of-the-art neutron sources. The design principles, tools, and optimization strategies for synchrotron beamlines are also similar to those of neutron beamlines. The authors describe existing design tools for modeling synchrotron radiation beamlines and describe how these tools have evolved over the last two decades. The development of increasingly powerful modeling tools has been driven by the escalating cost and sophistication of state-of-the-art beamlines and by a world-wide race to exploit advanced synchrotron radiation sources.

  3. National synchrotron light source user's manual: Guide to the VUV and x-ray beamlines: Third edition

    SciTech Connect

    Gmuer, N.F.; Thomlinson, W.; White-DePace, S.

    1989-01-01

    This report contains information on the following topics: A Word on the Writing of Beamline Descriptions; Beamline Equipment Utilization for General Users; the Vacuum Ultraviolet (VUV) Storage Ring and Beamlines; VUV Beamline Descriptions--An Explanation; VUV Beamline Descriptions; X-Ray Storage Ring and Beamlines; X-Ray Beamline Descriptions--An Explanation; and X-Ray Beamline Descriptions.

  4. New SRC APPLE II variable polarization beamline

    NASA Astrophysics Data System (ADS)

    Severson, M.; Bissen, M.; Fisher, M. V.; Rogers, G.; Reininger, R.; Green, M.; Eisert, D.; Tredinnick, B.

    2011-09-01

    SRC has recently commissioned a new Varied Line-Spacing Plane Grating Monochromator (VLS-PGM) utilizing as its source a 1 m long APPLE II insertion device in short-straight-section 9 of the Aladdin storage ring. The insertion device reliably delivers horizontal, vertical, and right and left circularly polarized light to the beamline. Measurements from an in situ polarimeter can be used for undulator corrections to compensate for depolarizing effects of the beamline. The beamline has only three optical elements and covers the energy range from 11.1 to 270 eV using two varied line-spacing gratings. A plane mirror rotates to illuminate the gratings at the correct angle to cancel the defocus term at all photon energies. An exit slit and elliptical-toroid refocusing mirror complete the beamline. Using a 50 μm exit slit, the beamline provides moderate to high resolution, with measured flux in the mid 10 12 (photons/s/200 mA) range, and a spot size of 400 μm horizontal by 30 μm vertical.

  5. New SRC APPLE ll Variable Polarization Beamline

    SciTech Connect

    M Severson; M Bissen; M Fisher; G Rogers; R Reininger; M Green; D Eisert; B Tredinnick

    2011-12-31

    SRC has recently commissioned a new Varied Line-Spacing Plane Grating Monochromator (VLS-PGM) utilizing as its source a 1 m long APPLE II insertion device in short-straight-section 9 of the Aladdin storage ring. The insertion device reliably delivers horizontal, vertical, and right and left circularly polarized light to the beamline. Measurements from an in situ polarimeter can be used for undulator corrections to compensate for depolarizing effects of the beamline. The beamline has only three optical elements and covers the energy range from 11.1 to 270 eV using two varied line-spacing gratings. A plane mirror rotates to illuminate the gratings at the correct angle to cancel the defocus term at all photon energies. An exit slit and elliptical-toroid refocusing mirror complete the beamline. Using a 50 {mu}m exit slit, the beamline provides moderate to high resolution, with measured flux in the mid 10{sup 12} (photons/s/200 mA) range, and a spot size of 400 {mu}m horizontal by 30 {mu}m vertical.

  6. Status of the Dortmund TGM3-Beamline

    SciTech Connect

    Berges, U.; Westphal, C.; Dreiner, S.; Krause, M.

    2004-05-12

    The former TGM3 beamline at BESSYI was rebuilt at the DELTA storage ring, University of Dortmund, Germany. The beamline uses synchrotron radiation from a dipole bending magnet. The previous design of the beamline had to be adapted to an operation at DELTA. This included a motorized rotation of the first mirror, since that mirror is located within the radiation shield wall at DELTA. Also, further minor components had to be modified, adapted, or replaced. During the set-up at DELTA, previously known operation problems due to mechanical vibrations were eliminated by a complete new mounting of the optical components. The measured performance parameters at BESSYI are compared with calculated results for an operation at DELTA. The first commissioning experiments are currently carried out.

  7. IR beamline at the Swiss Light Source

    NASA Astrophysics Data System (ADS)

    Ph, Lerch; L, Quaroni; J, Wambach; J, Schneider; B, Armstrong D.; D, Rossetti; L, Mueller F.; P, Peier; V, Schlott; L, Carroll; P, Friedli; H, Sigg; S, Stutz; M, Tran

    2012-05-01

    The infrared beamline at the Swiss light source uses dipole radiation and is designed to transport light to four experimental stations, A, B, C, D. Branch A is dedicated to far IR work in vacuum; branch B is a micro-spectrometer; branch C is dedicated to high resolution spectroscopy in the gas phase; branch D is a pump and probe set-up. This contribution describes the optical layout and provides a brief survey of currently available experimental stations. The beamline is in regular user operation since 2009.

  8. The First Group of CANDLE Beamlines

    SciTech Connect

    Aghasyan, M.; Grigoryan, A.; Mikaelyan, R.

    2004-05-12

    The Center for the Advancement of Natural Discoveries using Light Emission (CANDLE) is a 3 GeV intermediate energy light source project in Armenia. The paper presents the study and design futures of the first group of beamlines that are planed to run among with the facility operation scheduled for year 2007. Presented beamlines will cover the experimental researches based on diffraction and powder diffraction, XAS, Soft X-ray spectroscopy and microscopy, Small angle X-ray scattering, X-ray Imaging techniques and LIGA.

  9. Innovations in the design of mechanical components for a beamline-The SRI'95 Workshop 2 Summary (invited)

    NASA Astrophysics Data System (ADS)

    Kuzay, T. M.; Warwick, T.

    1996-09-01

    The Synchrotron Radiation Instrumentation 1995 Conference (SRI'95) was hosted by the Advanced Photon Source (APS) at Argonne National Laboratory (ANL). Of the many workshops within the conference, the SRI'95 Workshop 2 was ``Innovations in the Design of Mechanical Components of a Beamline.'' The workshop was well attended with over 140 registrants. The following topics were discussed. Industry's perspective on the status and future was provided by Huber Diffraktionstechnik GMBH on goniometers/diffractometers, Oxford Instruments on advanced manufacturing technique of high heat load components, such as the APS photon shutter, and Kohzu Seiki Co. Ltd. on the specialties of monochromators provided to the third-generation synchrotrons. This was followed by a description of the engineering of a dual function monochromator design for water-cooled diamond or cryogenically cooled silicon monochromators by CMC CAT/APS. Another category was the nagging problem of sensitivity of the photon beam position monitors (XBPM) to bending magnet radiation (``BM contamination'') and the undulator magnet gap changes. Problem descriptions and suggested solutions were provided by both the Advanced Light Source (ALS) and the APS. Other innovative ideas were the cooling schemes (enhanced cooling of beamline components using metallic porous meshes including cryo-cooled applications); Glidcop photon shutter design using microchannels at the ALS; and window/filter design, manufacture and operational experiences at CHESS and PETRA/HASYLAB. Additional discussions were held on designing for micromotions and precision in the optical support systems and smart user filter schemes. This is a summary of the presentations at the Workshop.

  10. Neutral beamline with improved ion energy recovery

    DOEpatents

    Dagenhart, William K.; Haselton, Halsey H.; Stirling, William L.; Whealton, John H.

    1984-01-01

    A neutral beamline generator with unneutralized ion energy recovery is provided which enhances the energy recovery of the full energy ion component of the beam exiting the neutralizer cell of the beamline. The unneutralized full energy ions exiting the neutralizer are deflected from the beam path and the electrons in the cell are blocked by a magnetic field applied transverse to the beamline in the cell exit region. The ions, which are generated at essentially ground potential and accelerated through the neutralizer cell by a negative acceleration voltage, are collected at ground potential. A neutralizer cell exit end region is provided which allows the magnetic and electric fields acting on the exiting ions to be closely coupled. As a result, the fractional energy ions exiting the cell with the full energy ions are reflected back into the gas cell. Thus, the fractional energy ions do not detract from the energy recovery efficiency of full energy ions exiting the cell which can reach the ground potential interior surfaces of the beamline housing.

  11. Human factors design for the BMIT biomedical beamlines

    NASA Astrophysics Data System (ADS)

    Miller, C. Denise; Wysokinski, Tomasz W.; Belev, George; Chapman, L. Dean

    2013-03-01

    Operation of a biomedical beamline poses a unique set of operational and instrumentation challenges for a synchrotron facility. From proper handling and care of live animals and animal tissues, to a user community drawn primarily from the medical and veterinary realms, the work of a biomedical beamline is unique when compared to other beamlines. At the Biomedical Imaging and Therapy (BMIT) beamlines at Canadian Light Source (CLS), operation of the beamlines is geared towards our user community of medical personnel, in addition to basic science researchers. Human factors considerations have been incorporated wherever possible on BMIT, including in the design of software and hardware, as well as ease-of-use features of beamline control stations and experiment hutches. Feedback from users continues to drive usability improvements to beamline operations.

  12. ELECTROMAGNETIC FIELD MEASUREMENT OF FUNDAMENTAL AND HIGHER-ORDER MODES FOR 7-CELL CAVITY OF PETRA-II

    SciTech Connect

    Kawashima, Y.; Blednykh, A.; Cupolo, J.; Davidsaver, M.; Holub, B.; Ma, H.; Oliva, J.; Rose, J.; Sikora, R.; Yeddulla, M.

    2011-03-28

    The booster synchrotron for NSLS-II will include a 7-cell PETRA cavity, which was manufactured for the PETRA-II project at DESY. The cavity fundamental frequency operates at 500 MHz. In order to verify the impedances of the fundamental and higher-order modes (HOM), which were calculated by computer code, we measured the magnitude of the electromagnetic field of the fundamental acceleration mode and HOM using the bead-pull method. To keep the cavity body temperature constant, we used a chiller system to supply cooling water at 20 degrees C. The bead-pull measurement was automated with a computer. We encountered some issues during the measurement process due to the difficulty in measuring the electromagnetic field magnitude in a multi-cell cavity. We describe the method and apparatus for the field measurement, and the obtained results.

  13. Synchrotron beamlines for x-ray lithography

    NASA Astrophysics Data System (ADS)

    Trippe, Anthony P.; Pearce, W. J.

    1994-02-01

    Louisiana State University established the J. Bennett Johnston, Sr., Center for Advanced Microstructures and Devices (CAMD). Designed and constructed by the Brobeck Division of Maxwell Laboratories, the CAMD synchrotron light source is the first electron storage ring to be built by a commercial company in the United States. The synchrotron x-ray radiation generated at CAMD is an extremely useful exposure source for both thin and thick film lithography. Passing through a beamline containing two plane mirrors, the synchrotron light is used to expose thin resists for lithography of patterns with feature sizes of 0.25 micron and smaller. Two thick-resist beamlines, one using a single aspheric (collimating) mirror and one using a plane mirror, provide the higher flux photons required for miniaturization in silicon to produce microscopic mechanical devices including gears, motors, filters, and valves.

  14. 1993 CAT workshop on beamline optical designs

    SciTech Connect

    Not Available

    1993-11-01

    An Advanced Photon Source (APS) Collaborative Access Team (CAT) Workshop on Beamline Optical Designs was held at Argonne National Laboratory on July 26--27, 1993. The goal of this workshop was to bring together experts from various synchrotron sources to provide status reports on crystal, reflecting, and polarizing optics as a baseline for discussions of issues facing optical designers for CAT beamlines at the APS. Speakers from the European Synchrotron Radiation Facility (ESRF), the University of Chicago, the National Synchrotron Light Source, and the University of Manchester (England) described single- and double-crystal monochromators, mirrors, glass capillaries, and polarizing optics. Following these presentations, the 90 participants divided into three working groups: Crystal Optics Design, Reflecting Optics, and Optics for Polarization Studies. This volume contains copies of the presentation materials from all speakers, summaries of the three working groups, and a ``catalog`` of various monochromator designs.

  15. Performance measurements at the SLS SIM beamline

    SciTech Connect

    Flechsig, U.; Nolting, F.; Fraile Rodriguez, A.; Krempasky, J.; Quitmann, C.; Schmidt, T.; Spielmann, S.; Zimoch, D.

    2010-06-23

    The Surface/Interface: Microscopy beamline of the Swiss Light Source started operation in 2001. In 2007 the beamline has been significantly upgraded with a second refocusing section and a blazed grating optimized for high photon flux. Two Apple II type undulators with a plane grating monochromator using the collimated light scheme deliver photons with an energy from 90eV to about 2keV with variable polarization for the photoemission electron microscope (PEEM) as the primary user station. We measured a focus of (45x60) {mu}m({nu}xh) and a photon flux > 10{sup 12} photon/s for all gratings. Polarization switching within a few seconds is realized with the small bandpass of the monochromator and a slight detuning of the undulator.

  16. How good can our beamlines be?

    PubMed Central

    Liebschner, Dorothee; Dauter, Miroslawa; Rosenbaum, Gerold; Dauter, Zbigniew

    2012-01-01

    The accuracy of X-ray diffraction data depends on the properties of the crystalline sample and on the performance of the data-collection facility (synchrotron beamline elements, goniostat, detector etc.). However, it is difficult to evaluate the level of performance of the experimental setup from the quality of data sets collected in rotation mode, as various crystal properties such as mosaicity, non-uniformity and radiation damage affect the measured intensities. A multiple-image experiment, in which several analogous diffraction frames are recorded consecutively at the same crystal orientation, allows minimization of the influence of the sample properties. A series of 100 diffraction images of a thaumatin crystal were measured on the SBC beamline 19BM at the APS (Argonne National Laboratory). The obtained data were analyzed in the context of the performance of the data-collection facility. An objective way to estimate the uncertainties of individual reflections was achieved by analyzing the behavior of reflection intensities in the series of analogous diffraction images. The multiple-image experiment is found to be a simple and adequate method to decompose the random errors from the systematic errors in the data, which helps in judging the performance of a data-collection facility. In particular, displaying the intensity as a function of the frame number allows evaluation of the stability of the beam, the beamline elements and the detector with minimal influence of the crystal properties. Such an experiment permits evaluation of the highest possible data quality potentially achievable at the particular beamline. PMID:22993097

  17. Nomenclature of SLC Arc beamline components

    SciTech Connect

    Silva, J.; Weng, W.T.

    1986-04-10

    This note defines I and C formal names for beamline components in the Arc as specified in the TRANSPORT decks ARCN FINAL and ARCS FINAL of June 5, 1985. The formal name consists of three fields: the primary name, the zone and the unit number. The general principles and guidelines are explained in Reference 1. The rationale and the final resolutions of the naming conventions for the Arc are explained.

  18. An Updated AP2 Beamline TURTLE Model

    SciTech Connect

    Gormley, M.; O'Day, S.

    1991-08-23

    This note describes a TURTLE model of the AP2 beamline. This model was created by D. Johnson and improved by J. Hangst. The authors of this note have made additional improvements which reflect recent element and magnet setting changes. The magnet characteristics measurements and survey data compiled to update the model will be presented. A printout of the actual TURTLE deck may be found in appendix A.

  19. Beryllium window for an APS diagnostics beamline

    SciTech Connect

    Sheng, I.C.; Yang, B.X.; Sharma, Y.S.

    1997-09-01

    A beryllium (Be) window for an Advanced Photon Source (APS) diagnostics beamline has been designed and built. The window, which has a double concave axisymmetrical profile with a thickness of 0.5 mm at the center, receives 160 W/mm{sup 2} (7 GeV/100 mA stored beam) from an undulator beam. The window design as well as thermal and thermomechanical analyses, including thermal buckling of the Be window, are presented.

  20. How good can our beamlines be?

    SciTech Connect

    Liebschner, Dorothee; Dauter, Miroslawa; Rosenbaum, Gerold Dauter, Zbigniew

    2012-10-01

    A repetitive measurement of the same diffraction image allows to judge the performance of a data collection facility. The accuracy of X-ray diffraction data depends on the properties of the crystalline sample and on the performance of the data-collection facility (synchrotron beamline elements, goniostat, detector etc.). However, it is difficult to evaluate the level of performance of the experimental setup from the quality of data sets collected in rotation mode, as various crystal properties such as mosaicity, non-uniformity and radiation damage affect the measured intensities. A multiple-image experiment, in which several analogous diffraction frames are recorded consecutively at the same crystal orientation, allows minimization of the influence of the sample properties. A series of 100 diffraction images of a thaumatin crystal were measured on the SBC beamline 19BM at the APS (Argonne National Laboratory). The obtained data were analyzed in the context of the performance of the data-collection facility. An objective way to estimate the uncertainties of individual reflections was achieved by analyzing the behavior of reflection intensities in the series of analogous diffraction images. The multiple-image experiment is found to be a simple and adequate method to decompose the random errors from the systematic errors in the data, which helps in judging the performance of a data-collection facility. In particular, displaying the intensity as a function of the frame number allows evaluation of the stability of the beam, the beamline elements and the detector with minimal influence of the crystal properties. Such an experiment permits evaluation of the highest possible data quality potentially achievable at the particular beamline.

  1. Shielding Calculations for NSLS-II Beamlines.

    SciTech Connect

    Job,P.K.; Casey, W.R.

    2008-04-13

    Brookhaven National Laboratory is in the process of designing a new Electron Synchrotron for scientific research using synchrotron radiation. This facility, called the 'National Synchrotron Light Source II' (NSLS-II), will provide x-ray radiation of ultra-high brightness and exceptional spatial and energy resolution. It will also provide advanced insertion devices, optics, detectors, and robotics, and a suite of scientific instruments designed to maximize the scientific output of the facility. The project scope includes the design, construction, installation, and commissioning of the following accelerators: a 200 MeV linac, a booster accelerator operating from 200 MeV to 3.0 GeV, the storage ring which stores 500 mA current of electrons at an energy of 3.0 GeV and 56 beamlines for experiments. It is planned to operate the facility primarily in a top-off mode, thereby maintaining the maximum variation in stored beam current to < 1%. Because of the very demanding requirements for beam emittance and synchrotron radiation brilliance, the beam life-time is expected to be quite low, on the order of 2 hours. Each of the 56 beamlines will be unique in terms of the source properties and configuration. The shielding designs for five representative beamlines are discussed in this paper.

  2. Undulator based beamline studies on U5

    NASA Astrophysics Data System (ADS)

    McDonnell, L.; Johnson, P.; Klaffky, R. W.; Smith, N. V.

    An undulator installed on beamline U5 at NSLS is expected to produce an intense flux of photons into a highly collimated beam. At normal operating energies (750 MeV) the FEL undulator is expected to have a fundamental harmonic at wavelength lambda = 300A for magnetic strength parameter K = 1. A simple beamline has been constructed to allow measurements of the absolute photon flux available from this device at wavelengths in the long wavelength tail of the fundamental. The central element of this beamline is a small monochromator based on the chromatic aberration properties of a LiF lens. This lens focuses different wavelengths at different points along the optical axis and monochromatization is achieved by moving the lens to focus different wavelengths onto a fixed 200 microns wide exit slit. Photoelectron spectroscopy was carried out with a CMA; photoelectrons being ejected from a freshly evaporated gold surface. Examination of a typical series of EDC's recorded on this system allows measurements of the bandwidth of the monochromator to be made. By measuring the total yield of electrons from the surface and comparing with previously published electron yield measurements from the same surface it is possible to obtain the total flux of photons from the undultor source.

  3. Beamline Performance Simulations for the Fundamental Neutron Physics Beamline at the Spallation Neutron Source

    PubMed Central

    Huffman, P. R.; Greene, G. L.; Allen, R. R.; Cianciolo, V.; Huerto, R. R.; Koehler, P.; Desai, D.; Mahurin, R.; Yue, A.; Palmquist, G. R.; Snow, W. M.

    2005-01-01

    Monte Carlo simulations are being performed to design and characterize the neutron optics components for the two fundamental neutron physics beamlines at the Spallation Neutron Source. Optimization of the cold beamline includes characterization of the guides and benders, the neutron transmission through the 0.89 nm monochromator, and the expected performance of the four time-of-flight choppers. The locations and opening angles of the choppers have been studied using a simple spreadsheet-based analysis that was developed for other SNS chopper instruments. The spreadsheet parameters are then optimized using Monte Carlo techniques to obtain the results presented in this paper. Optimization of the 0.89 nm beamline includes characterizing the double crystal monochromator and the downstream guides. The simulations continue to be refined as components are ordered and their exact size and performance specifications are determined.

  4. Chemical and Mineralogical study of Nabataean painted pottery from Petra, Jordan.

    NASA Astrophysics Data System (ADS)

    Alawneh, Firas; Bala'awi, Fadi

    Nabataean pottery is distinguished by the thinness of its walls, which were sometimes only 1.5 mm thick. It was a pinkish/red color, often decorated by hand with dark brown flower and leaf designs. The typical (egg-shell) shallow open bowls productions were very difficult to make on the potter's wheel, demonstrating how skilled their craftsmen were Nabataean painted pottery from Petra Jordan were examined in order to determine the mineralogical characteristics of the raw pigment materials used for their production and to elucidate the ceramic manufacturing technologies employed. Optical microscopy, X-ray diffraction analysis (XRD) and scanning electron microscopy (SEM-EDS) were the analytical techniques used. The initial examination of the ceramic shreds in optical microscopy showed all samples to be identical in their paint and paste textures. The mineralogical composition of the paste (unpainted outer surface) is typical of a clay poor in calcium and fired at moderate-high temperature in an oxidizing atmosphere. The paste is composed of quartz, plagioclase, potassium feldspar, hematite, dolomite, and calcite. The latter two phases might be attributed to post-depositional contamination, since examination with both optical and scanning electron microscopes show fine carbonate particles deposited in the pores and cracks of the shred. The paint on the inner surface of the vessel, on the other hand is composed of hematite as a major phase with only some quartz and plagioclase.

  5. Recent results from the JADE collaboration at PETRA on e+e- annihilation to multihadrons

    SciTech Connect

    O'Neill, L.H. Jr.

    1981-01-01

    A search for production of a new quark flavor in multihadronic states from e+e- annihilation has been made up to an energy of 35.8 GeV in the center of mass. No evidence is seen for such production. A new statistical analysis by the JADE collaboration of the combined data of four PETRA experiments from a fine energy scan in the region 29.90 to 31.46 GeV in the center of mass sets new upper limits on the integrated cross section for a bound state consisting of a new flavor quark and antiquark. The ability of the JADE detector to measure dE/dx provides new upper bounds on the production of fractionally charged particles such as free quarks, or of heavy, integrally charged states such as long-lived B mesons. Finally the fractions of the final state energy carried by gamma rays and by neutral particles of all kinds are measured at center of mass energies from 12 to 35 GeV. The gamma ray and neutral energy fractions are approximately 26% and 38% respectively, while the fractional energy carried by neutrinos is less than 15%.

  6. Macromolecular crystallography beamline X25 at the NSLS

    PubMed Central

    Héroux, Annie; Allaire, Marc; Buono, Richard; Cowan, Matthew L.; Dvorak, Joseph; Flaks, Leon; LaMarra, Steven; Myers, Stuart F.; Orville, Allen M.; Robinson, Howard H.; Roessler, Christian G.; Schneider, Dieter K.; Shea-McCarthy, Grace; Skinner, John M.; Skinner, Michael; Soares, Alexei S.; Sweet, Robert M.; Berman, Lonny E.

    2014-01-01

    Beamline X25 at the NSLS is one of the five beamlines dedicated to macromolecular crystallography operated by the Brookhaven National Laboratory Macromolecular Crystallography Research Resource group. This mini-gap insertion-device beamline has seen constant upgrades for the last seven years in order to achieve mini-beam capability down to 20 µm × 20 µm. All major components beginning with the radiation source, and continuing along the beamline and its experimental hutch, have changed to produce a state-of-the-art facility for the scientific community. PMID:24763654

  7. Design of Beamline BL9 at Saga Light Source

    SciTech Connect

    Tanaka, Tooru; Ogawa, Hiroshi; Kamada, Masao; Nishio, Mitsuhiro; Guo, Qixin; Masuda, Masataka; Motooka, Teruaki; Kondo, Yuzi; Hayashida, Kazuki; Yoshimura, Daisuke; Setoyama, Hiroyuki; Okajima, Toshihiro

    2007-01-19

    Saga Light Source (SAGA-LS), which has been constructed at Tosu city in Saga prefecture, is a compact synchrotron light source with storage electron energy of 1.4 GeV. A new beamline for the development of advanced materials and processing has been designed, and is now under construction at BL9 of SAGA-LS. This beamline is one of the three bending magnet beamlines (BL9, BL12, and BL15) constructed by Saga Prefectural Government. In this paper, we describe the design and the expected optical performance of the beamline BL9 at SAGA-LS.

  8. A new compact soft x-ray spectrometer for resonant inelastic x-ray scattering studies at PETRA III

    NASA Astrophysics Data System (ADS)

    Yin, Z.; Peters, H. B.; Hahn, U.; Agâker, M.; Hage, A.; Reininger, R.; Siewert, F.; Nordgren, J.; Viefhaus, J.; Techert, S.

    2015-09-01

    We present a newly designed compact grating spectrometer for the energy range from 210 eV to 1250 eV, which would include the Kα1,2 emission lines of vital elements like C, N, and O. The spectrometer is based on a grazing incidence spherical varied line spacing grating with 2400 l/mm at its center and a radius of curvature of 58 542 mm. First, results show a resolving power of around 1000 at an energy of 550 eV and a working spectrometer for high vacuum (10-4 mbar) environment without losing photon intensity.

  9. A new compact soft x-ray spectrometer for resonant inelastic x-ray scattering studies at PETRA III

    SciTech Connect

    Yin, Z. E-mail: simone.techert@desy.de; Peters, H. B.; Hahn, U.; Viefhaus, J.; Agåker, M.; Nordgren, J.; Hage, A.; Reininger, R.; Siewert, F.; Techert, S. E-mail: simone.techert@desy.de

    2015-09-15

    We present a newly designed compact grating spectrometer for the energy range from 210 eV to 1250 eV, which would include the Kα{sub 1,2} emission lines of vital elements like C, N, and O. The spectrometer is based on a grazing incidence spherical varied line spacing grating with 2400 l/mm at its center and a radius of curvature of 58 542 mm. First, results show a resolving power of around 1000 at an energy of 550 eV and a working spectrometer for high vacuum (10{sup −4} mbar) environment without losing photon intensity.

  10. Functional description of APS beamline front ends

    SciTech Connect

    Kuzay, T.

    1993-02-01

    Traditional synchrotron sources were designed to produce bending magnet radiation and have proven to be an essential scientific tool. Currently, a new generation of synchrotron sources is being built that will be able to accommodate a large number of insertion device (ID) and high quality bending magnet (BM) sources. One example is the 7-GeV Advanced Photon Source (APS) now under construction at Argonne National Laboratory. The research and development effort at the APS is designed to fully develop the potential of this new generation of synchrotron sources. Of the 40 straight sections in the APS storage ring, 34 will be available for IDs. The remaining six sections are reserved for the storage ring hardware and diagnostics. Although the ring incorporates 80 BMs, only 40 of them can be used to extract radiation. The accelerator hardware shadows five of these 40 bending magnets, so the maximum number of BM sources on the lattice is 35. Generally, a photon beamline consists of four functional sections. The first section is the ID or the BM, which provides the radiation source. The second section, which is immediately outside the storage ring but inside a concrete shielding tunnel, is the front end, which is designed to control, define, and/or confine the x-ray beam. In the case of the APS, the front ends are designed to confine the photon beam. The third section, just outside the concrete shielding tunnel and on the experimental floor, is the first optics enclosure, which contains optics to filter and monochromatize the photon beam. The fourth section of a beamline consists of beam transports, additional optics, and experiment stations to do the scientific investigations. This document describes only the front ends of the APS beamlines.

  11. Protecting Unesco World Heritage PROPERTIES'S Integrity: the Role of Recording and Documentation in Risk Management for PETRA

    NASA Astrophysics Data System (ADS)

    Santana Quintero, M.; Cesaro, G.; Ishakat, F.; Vandesande, A.; Vileikis, O.; Vadafari, A.; Paolini, A.; Van Balen, K.; Fakhoury, L.

    2012-07-01

    Risk management - as it has been defined - involves the decision-making process following a risk assessment (Ball, Watt, 2003). It is the process that involves managing to minimize losses and impacts on the significant of historic structures and to reach the balance between gaining and losing opportunities. This contribution explains the "heritage information" platform developed using low-cost recording, documentation and information management tools to serve as container for assessments resulting from the application of a risk methodology at a pilot area of the Petra Archaeological Park, in particular those that permit digitally and cost effective to prepare an adequate baseline record to identify disturbances and threats. Furthermore, this paper will reflect on the issue of mapping the World Heritage property's boundaries by illustrating a methodology developed during the project and further research to overcome the lack of boundaries and buffer zone for the protection of the Petra World Heritage site, as identified in this project. This paper is based on on-going field project from a multidisciplinary team of experts from the Raymond Lemaire International Centre for Conservation (University of Leuven), UNESCO Amman, Petra Development Tourism and Region Authority (PDTRA), and Jordan's Department of Antiquities (DoA), as well as, experts from Jordan. The recording and documentation approach included in this contribution is part of an on-going effort to develop a methodology for mitigating (active and preventive) risks on the Petra Archaeological Park (Jordan). The risk assessment has been performed using non-intrusive techniques, which involve simple global navigation satellite system (GNSS), photography, and structured visual inspection, as well as, a heritage information framework based on Geographic Information Systems. The approach takes into consideration the comparison of vulnerability to sites with the value assessment to prioritize monuments at risk based

  12. Possibility of observing color-symmetry violation in the two-photon experiments of PLUTO at PETRA

    SciTech Connect

    Efremov, A.; Ivanov, S.

    1982-01-01

    The two-photon processes being studied by the PLUTO group at PETRA are discussed from the point of view of study of color symmetry. The reaction which is cleanest theoretically is the annihilation of two photons into two hadron jets with large transverse momentum. The PLUTO results for this process are compared with calculations using QCD and the calculations in the model of electrostrong interactions with violation of color symmetry. It is not clear whether the departure of the experimental results from QCD is due to an important role of higher twists or to the violation of color symmetry. (AIP)

  13. The Dutch-Belgian beamline at the ESRF.

    PubMed

    Borsboom, M; Bras, W; Cerjak, I; Detollenaere, D; Glastra Van Loon, D; Goedtkindt, P; Konijnenburg, M; Lassing, P; Levine, Y K; Munneke, B; Oversluizen, M; Van Tol, R; Vlieg, E

    1998-05-01

    A brief description is given of the design principles and layout of the Dutch-Belgian beamline at the ESRF. This beamline optimizes the use of the available bending-magnet radiation fan by splitting the beam into two branches, each accommodating two experimental techniques. PMID:15263564

  14. Damage Assessment and Digital 2D-3D Documentation of PetraTreasury

    NASA Astrophysics Data System (ADS)

    Bala'awi, Fadi; Alshawabkeh, Yahya; Alawneh, Firas; Masri, Eyed al

    The treasury is the icon monument of the world heritage site of ancient Petra city. Unfortunately, this important part of the world's cultural heritage is gradually being diminished due to weathering and erosion problems. This give rise to the need to have a comprehensive study and full documentation of the monument in order to evaluate its status. In this research a comprehensive approach utilizing 2D-3D documentation of the structure using laser scanner and photogrammetry is carried parallel with a laboratory analysis and a correlation study of the salt content and the surface weathering forms. In addition, the research extends to evaluate a set of chemical and physical properties of the case study monument. Studies of stone texture and spatial distribution of soluble salts were carried out at the monument in order to explain the mechanism of the weathering problem. Then a series of field work investigations and laboratory work were undertaken to study the effect of relative humidity, temperature, and wind are the main factors in the salt damage process. The 3D modelling provides accurate geometric and radiometric properties of the damage shape. In order to support the visual quality of 3D surface details and cracks, a hybrid approach combining data from the laser scanner and the digital imagery was developed. Based on the findings, salt damage appears to be one of the main problems at this monument. Although, the total soluble salt content are quite low, but the salts contamination is all over the tested samples in all seasons, with higher concentrations at deep intervals. The thermodynamic calculations carried out by this research have also shown that salt damage could be minimised by controlling the surrounding relative humidity conditions. This measure is undoubtedly the most challenging of all, and its application, if deemed feasible, should be carried out in parallel with other conservation measures.

  15. G4beamline Particle Tracking in Matter Dominated Beam Lines

    SciTech Connect

    T.J. Roberts, K.B. Beard, S. Ahmed, D. Huang, D.M. Kaplan

    2011-03-01

    The G4beamline program is a useful and steadily improving tool to quickly and easily model beam lines and experimental equipment without user programming. It has both graphical and command-line user interfaces. Unlike most accelerator physics codes, it easily handles a wide range of materials and fields, being particularly well suited for the study of muon and neutrino facilities. As it is based on the Geant4 toolkit, G4beamline includes most of what is known about the interactions of particles with matter. We are continuing the development of G4beamline to facilitate its use by a larger set of beam line and accelerator developers. A major new feature is the calculation of space-charge effects. G4beamline is open source and freely available at http://g4beamline.muonsinc.com

  16. The mammography project at the SYRMEP beamline.

    PubMed

    Dreossi, D; Abrami, A; Arfelli, F; Bregant, P; Casarin, K; Chenda, V; Cova, M A; Longo, R; Menk, R-H; Quai, E; Quaia, E; Rigon, L; Rokvic, T; Sanabor, D; Tonutti, M; Tromba, G; Vascotto, A; Zanconati, F; Castelli, E

    2008-12-01

    A clinical program for X-ray phase contrast (PhC) mammography with synchrotron radiation (SR) has been started in March 2006 at the SYRMEP beamline of Elettra, the SR facility in Trieste, Italy. The original beamline layout has been modified substantially and a clinical facility has been realized. In order to fulfill all security requirements, dedicated systems have been designed and implemented, following redundancy criteria and "fail safe" philosophy. Planar radiographic images are obtained by scanning simultaneously the patient and the detector through the stationary and laminar SR beam. In this first phase of the project a commercial screen-film system has been used as image receptor. Upon approval by the respective authorities, the mammography program is about half way to conclusion. Up to now about 50 patients have been examined. The patients are volunteers recruited by the radiologist after conventional examinations at the hospital resulted in an uncertain diagnosis. As an example one case of PhC SR mammography is shown and compared to conventional digital mammography. Preliminary analysis shows the high diagnostic quality of the PhC SR images that were acquired with equal or less delivered dose compared to the conventional ones. PMID:18617344

  17. Diagnostics Beamline for the SRF Gun Project

    SciTech Connect

    T. Kamps; V. Durr; K. Goldammer; D. Kramer; P. Kuske; J. Kuszynski; D. Lipka; F. Marhauser; T. Quast; D. Richter; U. Lehnert; P. Michel; J. Teichert; P. Evtushenko; I. Will

    2005-08-22

    A superconducting radio-frequency photo electron injector (SRF gun) is currently under construction by a collaboration of BESSY, DESY, FZR and MBI. The project aims at the design and setup of a CW SRF gun including a diagnostics beamline for the ELBE FEL and to address R&D issues on low emittance injectors for future light sources such as the BESSY FEL. Of critical importance for the injector performance is the control of the electron beam parameters. For this reason a compact diagnostics beamline is under development serving a multitude of operation settings ranging from low-charge (77pC), low-emittance (1 mm mrad) mode to high-charge (2.5nC) operation of the gun. For these operation modes beam dynamics simulations are resulting in boundary conditions for the beam instrumentation. Proven and mature technology is projected wherever possible, for example for current and beam position monitoring. The layout of the beam profile and emittance measurement systems is described. For the bunch length, which varies between 5 ps and 50 ps, two schemes using electro-optical sampling and Cherenkov radiation are detailed. The beam energy and energy spread is measured with a 180-degree spectrometer.

  18. The Infrared Microspectroscopy Beamline at CAMD

    SciTech Connect

    Kizilkaya, O.; Singh, V.; Desta, Y.; Pease, M.; Roy, A.; Scott, J.; Goettert, J.; Morikawa, E.; Hormes, J.; Prange, A.

    2007-01-19

    The first infrared microspectroscopy beamline at the Louisiana State University, Center for Advanced Microstructures and Devices (LSU-CAMD) has been constructed and dedicated to investigation of samples from various disciplines including chemistry, geology, biology, and material sciences. The beamline comprises a simple optical configuration. A planar and toroidal mirror pair collects 50 and 15 mrad synchrotron radiation in horizontal and vertical directions, respectively, and focuses the beam through a diamond window located outside of the shielding wall. This focus acts as a new source point for the rest of the optical systems. The synchrotron beam spot size of 35 {mu}m and 12 {mu}m is measured in the x and y direction of the sample stage position of the microscope. This small beam spot has a superior brightness compared to conventional IR sources and allows spatially resolved measurements with very good signal/noise ratio. Compared to a conventional thermal source, synchrotron radiation provides 30 times better intensity and a two orders of magnitude greater signal/noise ratio when measuring with microscope aperture size of 15 x 15 {mu}m{sup 2}. The results of the studies on the fungus-plant interaction with its resultant effects on the healthy leaves, and bacterial growth process in the crystallization of gordaite, a mineral, are presented.

  19. Neutral beamline with improved ion energy recovery

    DOEpatents

    Kim, Jinchoon

    1984-01-01

    A neutral beamline employing direct energy recovery of unneutralized residual ions is provided which enhances the energy recovery of the full energy ion component of the beam exiting the neutralizer cell, and thus improves the overall neutral beamline efficiency. The unneutralized full energy ions exiting the neutralizer are deflected from the beam path and the electrons in the cell are blocked by a magnetic field applied transverse to the beam direction in the neutral izer exit region. The ions which are generated at essentially ground potential and accelerated through the neutralizer cell by a negative acceleration voltage are collected at ground potential. A neutralizer cell exit end region is provided which allows the magnetic and electric fields acting on the exiting ions to be loosely coupled. As a result, the fractional energy ions exiting the cell are reflected onto and collected at an interior wall of the neutralizer formed by the modified end geometry, and thus do not detract from the energy recovery efficiency of full energy ions exiting the cell. Electrons within the neutralizer are prevented from exiting the neutralizer end opening by the action of crossed fields drift (ExB) and are terminated to a collector collar around the downstream opening of the neutralizer. The correct combination of the extended neutralizer end structure and the magnet region is designed so as to maximize the exit of full energy ions and to contain the fractional energy ions.

  20. A Remote and Virtual Synchrotron Beamline

    NASA Astrophysics Data System (ADS)

    Jackson, J. M.; Alp, E.; Sturhahn, W.

    2012-12-01

    National facilities offer one-of-a-kind opportunities to apply state-of-the-art experimental techniques to the pressing scientific problems of today. Yet, few students are able to experience research projects at national facilities due to limited accessibility caused in part by limited involvement in the local academic institution, constrained working areas at the experimental stations, and/or travel costs. We present a virtual and remote beam-line for Earth science studies using nuclear resonant and inelastic x-ray scattering methods at Sector 3 of the Advanced Photon Source at Argonne National Laboratory. Off-site students have the capability of controlling their measurements via secure internet connections and webcams. Students can access a 'view only mode' for ease of interaction and safety-control. More experienced users have exclusive control of the experiment and can remotely change variables within the experimental setup. Students may also access the virtual aspects these experiments by simulating certain conditions with our newly developed software. We evaluate such a tool by giving "before" and "after" assignments to students at different levels. These levels include high-school students from the Pasadena and greater Los Angeles area school districts, undergraduate students from Caltech's SURF/MURF program, and graduate students at Caltech. We specifically target underrepresented groups. Our results thus far show that the capabilities offered by our remote and virtual beamline show improved knowledge and understanding of applying experimental-based studies at the synchrotron to solve problems in the Earth sciences.

  1. The ACCM Beamlines For Bioscience Studies

    NASA Astrophysics Data System (ADS)

    Ma, C. I.; Chang, S. H.; Liu, C. Y.; Juang, J. M.; Chang, C. H.; Tsang, K. L.

    2007-01-01

    To meet the increasing demand of X-ray beamlines for bioscience research, we have designed two high-performance, side-branch, asymmetric-cut curved crystal monochromator (ACCM) beamlines to fully utilize the sideway output of the superconducting wiggler SW6 at NSRRC. Each of these two beamlines (BL13A and BL13C) collects 1 mrad of the radiation fan in the horizontal direction, one centered at 3 mrad and the other at 4 mrad away from the central line of the wiggler output. The newly designed ACCMs are capable of energy scanning from 12 keV to 14 keV and offer good performances in terms of flux, resolution and stability. The ACCMs are designed and built in-house, combining efficient cooling and bending mechanisms in a compact unit that allows precise adjustments on a goniometer assembly. The bender is specially designed with symmetrically driven piezo-actuators that minimize center displacement during bending. Both direct and indirect cooling methods were tested; the former using Ga/In directly under the beam footprint and the latter using both sides of the crystal clamping area for cooling. Performance of the beamlines employing both cooling methods has been measured. The indirect cooling method provides 4.9 × 1010 photons/sec through a pair of 100 μm slits (H × V) with energy resolution of 5.3 × 10-3 (ΔE/E) at 12.7 keV. Higher energy resolution in the 10-4 range can be achieved by adjusting the horizontal source fan or the crystal radius at the expense of flux. The direct cooling method provides 1.4 × 1010 photons/sec through a pair of 100 μm slits (H × V) with energy resolution of 1.2 × 10-3 (ΔE/E) at 12.7 keV. The FWHM of the focused beam profile in the indirect cooling mode is 800 × 109 μm (H × V), and 800 × 283 μm (H × V) in the direct cooling mode with some horizontal tail, the latter being larger due to influence of the Ga/In layer on the crystal shape. Cooling efficiency is excellent in the direct cooling mode, in which the performance

  2. A heat transfer study for beamline components in high-power wiggler and undulator beamlines. Part I. Beam stops

    SciTech Connect

    Bedzyk, M. J.; Keeffe, M. J.; Schildkamp, W.; Shen, Q.

    1989-07-01

    The heat transfer capabilities of beam stops in CHESS wiggler and undulator beamlines is described. The thermal analysis for the design of these crucial in-vacuum beamline components is based on the use of a finite element analysis computer calculation and experimental heat loading tests.

  3. Innovations in the design of mechanical components for a beamline{emdash}The SRI{close_quote}95 Workshop 2 Summary

    SciTech Connect

    Kuzay, T.; Warwick, T. |

    1996-09-01

    The Synchrotron Radiation Instrumentation 1995 Conference (SRI{close_quote}95) was hosted by the Advanced Photon Source (APS) at Argonne National Laboratory (ANL). Of the many workshops within the conference, the SRI{close_quote}95 Workshop 2 was {open_quote}{open_quote}Innovations in the Design of Mechanical Components of a Beamline.{close_quote}{close_quote} The workshop was well attended with over 140 registrants. The following topics were discussed. Industry{close_quote}s perspective on the status and future was provided by Huber Diffraktionstechnik GMBH on goniometers/diffractometers, Oxford Instruments on advanced manufacturing technique of high heat load components, such as the APS photon shutter, and Kohzu Seiki Co. Ltd. on the specialties of monochromators provided to the third-generation synchrotrons. This was followed by a description of the engineering of a dual function monochromator design for water-cooled diamond or cryogenically cooled silicon monochromators by CMC CAT/APS. Another category was the nagging problem of sensitivity of the photon beam position monitors (XBPM) to bending magnet radiation ({open_quote}{open_quote}BM contamination{close_quote}{close_quote}) and the undulator magnet gap changes. Problem descriptions and suggested solutions were provided by both the Advanced Light Source (ALS) and the APS. Other innovative ideas were the cooling schemes (enhanced cooling of beamline components using metallic porous meshes including cryo-cooled applications); Glidcop photon shutter design using microchannels at the ALS; and window/filter design, manufacture and operational experiences at CHESS and PETRA/HASYLAB. Additional discussions were held on designing for micromotions and precision in the optical support systems and smart user filter schemes. This is a summary of the presentations at the Workshop. {copyright} {ital 1996 American Institute of Physics.}

  4. Mirrors for synchrotron-radiation beamlines

    SciTech Connect

    Howells, M.R.

    1993-09-01

    The authors consider the role of mirrors in synchrotron-radiation beamlines and discuss the optical considerations involved in their design. They discuss toroidal, spherical, elliptical, and paraboloidal mirrors in detail with particular attention to their aberration properties. They give a treatment of the sine condition and describe its role in correcting the coma of axisymmetric systems. They show in detail how coma is inevitable in single-reflection, grazing-incidence systems but correctable in two-reflection systems such as those of the Wolter type. In an appendix, they give the theory of point aberrations of reflectors of a general shape and discuss the question of correct naming of aberrations. In particular, a strict definition of coma is required if attempts at correction are to be based on the sine condition.

  5. Commissioning of a microprobe-XRF beamline (BL-16) on Indus-2 synchrotron source

    SciTech Connect

    Tiwari, M. K.; Gupta, P.; Sinha, A. K.; Garg, C. K.; Singh, A. K.; Kane, S. R.; Garg, S. R.; Lodha, G. S.

    2012-06-05

    We report commissioning of the microprobe-XRF beamline on Indus-2 synchrotron source. The beamline has been recently made operational and is now open for the user's experiments. The beamline comprises of Si(111) double crystal monochromator and Kirkpatrick-Baez focusing optics. The beamline covers wide photon energy range of 4 - 20 keV using both collimated and micro-focused beam modes. The design details and the first commissioning results obtained using this beamline are presented.

  6. An approach to better understanding of salt weathering on stone monuments - the "petraSalt" research project

    NASA Astrophysics Data System (ADS)

    Heinrichs, K.; Azzam, R.

    2012-04-01

    Salt weathering is known as a major cause of damage on stone monuments. However, processes and mechanisms of salt weathering still can not be explained satisfactorily. From the expertś point of view, better understanding of salt weathering deserves further comprehensive in-situ investigation jointly addressing active salt weathering processes and controlling factors. The 'petraSalt' research project takes this approach. The rock-cut monuments of Petra / Jordan were selected for studies, since stone type and spectra of monument exposure regimes, environmental influences, salt loading and weathering damage are representative for many stone monuments worldwide. The project aims at real-time / real-scale weathering models that depict characteristic interdependencies between stone properties, monument exposure regimes, environmental influences, salt loading and salt weathering damage. These models are expected to allow reliable rating and interpretation of aggressiveness and damage potential of the salt weathering regimes considering their variability under range of lithology, monument exposure scenarios, environmental conditions and time. The methodological approach systematically combines assessment of weathering damage (type, extent, spatial distribution and progression of damage), assessment of monument exposure characteristics and environmental influences acting on the monuments (monument orientation / geometry, lithology, rain impact, water run-off, rising humidity, wind impact, insolation, heating-cooling and drying-wetting behaviour, etc.), engineering geological studies (structural discontinuities and related failure processes) and investigation of salt loading (type, concentration, spatial distribution and origin of salt, salt crystallization / dissolution, phase transitions, etc.). Besides established methods, very innovative technologies are applied in the course of investigation such as high-resolution 3D terrestrial laser scanning (TLS) and wireless

  7. A hard X-ray nanoprobe beamline for nanoscale microscopy

    PubMed Central

    Winarski, Robert P.; Holt, Martin V.; Rose, Volker; Fuesz, Peter; Carbaugh, Dean; Benson, Christa; Shu, Deming; Kline, David; Stephenson, G. Brian; McNulty, Ian; Maser, Jörg

    2012-01-01

    The Hard X-ray Nanoprobe Beamline (or Nanoprobe Beamline) is an X-ray microscopy facility incorporating diffraction, fluorescence and full-field imaging capabilities designed and operated by the Center for Nanoscale Materials and the Advanced Photon Source at Sector 26 of the Advanced Photon Source at Argonne National Laboratory. This facility was constructed to probe the nanoscale structure of biological, environmental and material sciences samples. The beamline provides intense focused X-rays to the Hard X-ray Nanoprobe (or Nanoprobe) which incorporates Fresnel zone plate optics and a precision laser sensing and control system. The beamline operates over X-ray energies from 3 to 30 keV, enabling studies of most elements in the periodic table, with a particular emphasis on imaging transition metals. PMID:23093770

  8. Transport from the Recycler Ring to the Antiproton Source Beamlines

    SciTech Connect

    Xiao, M.; /Fermilab

    2012-05-14

    In the post-NOvA era, the protons are directly transported from the Booster ring to the Recycler ring rather than the Main Injector. For Mu2e and g-2 project, the Debuncher ring will be modified into a Delivery ring to deliver the protons to both Mu2e and g-2 experiments. Therefore, it requires the transport of protons from the Recycler Ring to the Delivery ring. A new transfer line from the Recycler ring to the P1 beamline will be constructed to transport proton beam from the Recycler Ring to existing Antiproton Source beamlines. This new beamline provides a way to deliver 8 GeV kinetic energy protons from the Booster to the Delivery ring, via the Recycler, using existing beam transport lines, and without the need for new civil construction. This paper presents the Conceptual Design of this new beamline.

  9. Moly99 Production Facility: Report on Beamline Components, Requirements, Costs

    SciTech Connect

    Bishofberger, Kip A.

    2015-12-23

    In FY14 we completed the design of the beam line for the linear accelerator production design concept. This design included a set of three bending magnets, quadrupole focusing magnets, and octopoles to flatten the beam on target. This design was generic and applicable to multiple different accelerators if necessary. In FY15 we built on that work to create specifications for the individual beam optic elements, including power supply requirements. This report captures the specification of beam line components with initial cost estimates for the NorthStar production facility.This report is organized as follows: The motivation of the beamline design is introduced briefly, along with renderings of the design. After that, a specific list is provided, which accounts for each beamline component, including part numbers and costs, to construct the beamline. After that, this report details the important sections of the beamline and individual components. A final summary and list of follow-on activities completes this report.

  10. New HMI hard X-ray Diffraction Beamlines at BESSY

    SciTech Connect

    Denks, I. A.; Genzel, C.; Dudzik, E.; Feyerherm, R.; Klaus, M.; Wagener, G.

    2007-01-19

    Since April 2005 the Hahn-Meitner-Institute is operating two new beamlines for energy dispersive diffraction experiments (EDDI) and for (resonant) magnetic scattering (MAGS) at BESSY. The source for both beamlines is a superconducting 7 T multipole wiggler which provides hard X-ray photons with energies between 4 and 150 keV. The EDDI beamline uses the white beam and is intended for residual stress measurements on small samples as well as heavy engineering parts. The MAGS beamline delivers a focussed monochromatic beam with photon fluxes in the 1012 (s 100 mA 0.1 % bandwidth)-1 range at energies from 4 to 30 keV. It is equipped for single crystal diffraction and resonant (magnetic) scattering experiments as well as for the study of thin films, micro-, and nanostructures in materials science.

  11. New HMI hard X-ray Diffraction Beamlines at BESSY

    NASA Astrophysics Data System (ADS)

    Denks, I. A.; Genzel, C.; Dudzik, E.; Feyerherm, R.; Klaus, M.; Wagener, G.

    2007-01-01

    Since April 2005 the Hahn-Meitner-Institute is operating two new beamlines for energy dispersive diffraction experiments (EDDI) and for (resonant) magnetic scattering (MAGS) at BESSY. The source for both beamlines is a superconducting 7 T multipole wiggler which provides hard X-ray photons with energies between 4 and 150 keV. The EDDI beamline uses the white beam and is intended for residual stress measurements on small samples as well as heavy engineering parts. The MAGS beamline delivers a focussed monochromatic beam with photon fluxes in the 1012 (s 100 mA 0.1 % bandwidth)-1 range at energies from 4 to 30 keV. It is equipped for single crystal diffraction and resonant (magnetic) scattering experiments as well as for the study of thin films, micro-, and nanostructures in materials science.

  12. New Large Volume Press Beamlines at the Canadian Light Source

    NASA Astrophysics Data System (ADS)

    Mueller, H. J.; Hormes, J.; Lauterjung, J.; Secco, R.; Hallin, E.

    2013-12-01

    The Canadian Light Source, the German Research Centre for Geosciences and the Western University recently agreed to establish two new large volume press beamlines at the Canadian Lightsource. As the first step a 250 tons DIA-LVP will be installed at the IDEAS beamline in 2014. The further development is associated with the construction of a superconducting wiggler beamline at the Brockhouse sector. A 1750 tons DIA LVP will be installed there about 2 years later. Up to the completion of this wiggler beamline the big press will be used for offline high pressure high temperature experiments under simulated Earth's mantle conditions. In addition to X-ray diffraction, all up-to-date high pressure techniques as ultrasonic interferometry, deformation analyses by X-radiography, X-ray densitometry, falling sphere viscosimetry, multi-staging etc. will be available at both beamlines. After the required commissioning the beamlines will be open to the worldwide user community from Geosciences, general material sciences, physics, chemistry, biology etc. based on the evaluation and ranking of the submitted user proposals by an international review panel.

  13. Provenance of white marbles from the nabatean sites of Qase Al Bint and colonnaded street baths at Petra, Jordan

    NASA Astrophysics Data System (ADS)

    Abu-Jaber, Nizar; al-Saad, Ziad; Shiyyab, Adnan; Degryse, Patrick

    Intercultural relations and trade are important components of understanding of historical interrelationships between regions and cultures. One of the most interesting objects of trade is stone, because of the expense and difficulty of its transport. Thus, the source of marble used in the Nabatean city of Petra was investigated using established petrological, geochemical and isotopic analyses. Specifically, marble from Qasr al Bint and the Colonnaded Street baths were sampled and investigated. The results of these analyses show that the marbles came from sources in Asia Minora and Greece. The most likely sources of the marble are the quarries of Thasos, Penteli, Prokennesos and Dokimeion. The choice of marble followed the desired utilitarian and aesthetic function of the stone. These results show that active trade in stone was part of the cultural interaction of the period.

  14. A tunable wedge-shaped absorber for hard X-ray synchrotron applications.

    PubMed

    Krywka, C; Brix, M; Müller, M

    2014-07-01

    The concept of a concave aluminium wedge-shaped absorber for hard X-ray synchrotron beamlines is presented. Unlike the commonly used absorber types (fixed-thickness absorber sheets or binary exchangers of individual fixed absorbers), this concept allows a compact system, controlled with a single linear positioner, and provides a wide attenuation range as well as a precise tunability over a large energy range. Data were recorded at the Nanofocus Endstation of the MINAXS beamline, PETRA III, Hamburg, Germany. PMID:24971979

  15. D3, the new diffractometer for the macromolecular crystallography beamlines of the Swiss Light Source

    PubMed Central

    Fuchs, Martin R.; Pradervand, Claude; Thominet, Vincent; Schneider, Roman; Panepucci, Ezequiel; Grunder, Marcel; Gabadinho, Jose; Dworkowski, Florian S. N.; Tomizaki, Takashi; Schneider, Jörg; Mayer, Aline; Curtin, Adrian; Olieric, Vincent; Frommherz, Uli; Kotrle, Goran; Welte, Jörg; Wang, Xinyu; Maag, Stephan; Schulze-Briese, Clemens; Wang, Meitian

    2014-01-01

    A new diffractometer for microcrystallography has been developed for the three macromolecular crystallography beamlines of the Swiss Light Source. Building upon and critically extending previous developments realised for the high-resolution endstations of the two undulator beamlines X06SA and X10SA, as well as the super-bend dipole beamline X06DA, the new diffractometer was designed to the following core design goals. (i) Redesign of the goniometer to a sub-micrometer peak-to-peak cylinder of confusion for the horizontal single axis. Crystal sizes down to at least 5 µm and advanced sample-rastering and scanning modes are supported. In addition, it can accommodate the new multi-axis goniometer PRIGo (Parallel Robotics Inspired Goniometer). (ii) A rapid-change beam-shaping element system with aperture sizes down to a minimum of 10 µm for microcrystallography measurements. (iii) Integration of the on-axis microspectrophotometer MS3 for microscopic sample imaging with 1 µm image resolution. Its multi-mode optical spectroscopy module is always online and supports in situ UV/Vis absorption, fluorescence and Raman spectroscopy. (iv) High stability of the sample environment by a mineral cast support construction and by close containment of the cryo-stream. Further features are the support for in situ crystallization plate screening and a minimal achievable detector distance of 120 mm for the Pilatus 6M, 2M and the macromolecular crystallography group’s planned future area detector Eiger 16M. PMID:24562555

  16. ALS beamlines for independent investigators: A summary of the capabilities and characteristics of beamlines at the ALS

    SciTech Connect

    Not Available

    1992-08-01

    There are two mods of conducting research at the ALS: To work as a member of a participating research team (PRT). To work as a member of a participating research team (PRT); to work as an independent investigator; PRTs are responsible for building beamlines, end stations, and, in some cases, insertion devices. Thus, PRT members have privileged access to the ALS. Independent investigators will use beamline facilities made available by PRTs. The purpose of this handbook is to describe these facilities.

  17. Beamline Insertions Manager at Jefferson Lab

    SciTech Connect

    Johnson, Michael C.

    2015-09-01

    The beam viewer system at Jefferson Lab provides operators and beam physicists with qualitative and quantitative information on the transverse electron beam properties. There are over 140 beam viewers installed on the 12 GeV CEBAF accelerator. This paper describes an upgrade consisting of replacing the EPICS-based system tasked with managing all viewers with a mixed system utilizing EPICS and high-level software. Most devices, particularly the beam viewers, cannot be safely inserted into the beam line during high-current beam operations. Software is partly responsible for protecting the machine from untimely insertions. The multiplicity of beam-blocking and beam-vulnerable devices motivates us to try a data-driven approach. The beamline insertions application components are centrally managed and configured through an object-oriented software framework created for this purpose. A rules-based engine tracks the configuration and status of every device, along with the beam status of the machine segment containing the device. The application uses this information to decide on which device actions are allowed at any given time.

  18. Status of the LBNE Neutrino Beamline

    SciTech Connect

    Papadimitriou, Vaia; /Fermilab

    2011-12-01

    The Long Baseline Neutrino Experiment (LBNE) will utilize a neutrino beamline facility located at Fermilab to carry out a compelling research program in neutrino physics. The facility will aim a beam of neutrinos toward a detector placed at the Homestake Mine in South Dakota. The neutrinos are produced in a three-step process. First, protons from the Main Injector (60-120 GeV) hit a solid target and produce mesons. Then, the charged mesons are focused by a set of focusing horns into the decay pipe, towards the far detector. Finally, the mesons that enter the decay pipe decay into neutrinos. The parameters of the facility were determined taking into account several factors including the physics goals, the Monte Carlo modeling of the facility, spacial and radiological constraints and the experience gained by operating the NuMI facility at Fermilab. The initial beam power is expected to be {approx}700 kW, however some of the parameters were chosen to be able to deal with a beam power of 2.3 MW. We discuss here the status of the conceptual design and the associated challenges.

  19. Diamond beamline I07: a beamline for surface and interface diffraction.

    PubMed

    Nicklin, Chris; Arnold, Tom; Rawle, Jonathan; Warne, Adam

    2016-09-01

    Beamline I07 at Diamond Light Source is dedicated to the study of the structure of surfaces and interfaces for a wide range of sample types, from soft matter to ultrahigh vacuum. The beamline operates in the energy range 8-30 keV and has two endstations. The first houses a 2+3 diffractometer, which acts as a versatile platform for grazing-incidence techniques including surface X-ray diffraction, grazing-incidence small- (and wide-) angle X-ray scattering, X-ray reflectivity and grazing-incidence X-ray diffraction. A method for deflecting the X-rays (a double-crystal deflector) has been designed and incorporated into this endstation, extending the surfaces that can be studied to include structures formed on liquid surfaces or at liquid-liquid interfaces. The second experimental hutch contains a similar diffractometer with a large environmental chamber mounted on it, dedicated to in situ ultrahigh-vacuum studies. It houses a range of complementary surface science equipment including a scanning tunnelling microscope, low-energy electron diffraction and X-ray photoelectron spectroscopy ensuring that correlations between the different techniques can be performed on the same sample, in the same chamber. This endstation allows accurate determination of well ordered structures, measurement of growth behaviour during molecular beam epitaxy and has also been used to measure coherent X-ray diffraction from nanoparticles during alloying. PMID:27577783

  20. Diamond beamline I07: a beamline for surface and interface diffraction

    PubMed Central

    Nicklin, Chris; Arnold, Tom; Rawle, Jonathan; Warne, Adam

    2016-01-01

    Beamline I07 at Diamond Light Source is dedicated to the study of the structure of surfaces and interfaces for a wide range of sample types, from soft matter to ultrahigh vacuum. The beamline operates in the energy range 8–30 keV and has two endstations. The first houses a 2+3 diffractometer, which acts as a versatile platform for grazing-incidence techniques including surface X-ray diffraction, grazing-incidence small- (and wide-) angle X-ray scattering, X-ray reflectivity and grazing-incidence X-ray diffraction. A method for deflecting the X-rays (a double-crystal deflector) has been designed and incorporated into this endstation, extending the surfaces that can be studied to include structures formed on liquid surfaces or at liquid–liquid interfaces. The second experimental hutch contains a similar diffractometer with a large environmental chamber mounted on it, dedicated to in situ ultrahigh-vacuum studies. It houses a range of complementary surface science equipment including a scanning tunnelling microscope, low-energy electron diffraction and X-ray photoelectron spectroscopy ensuring that correlations between the different techniques can be performed on the same sample, in the same chamber. This endstation allows accurate determination of well ordered structures, measurement of growth behaviour during molecular beam epitaxy and has also been used to measure coherent X-ray diffraction from nanoparticles during alloying. PMID:27577783

  1. Performance of Doublet III neutral beam injector cryopumping system

    SciTech Connect

    Langhorn, A.R.; Kim, J.; Tupper, M.L.; Williams, J.P.; Fasolo, J.

    1984-04-01

    The Doublet III neutral beam injector system is based on three beamlines; each beamline employs two 80 kV/80 A hydrogen ion sources. Two liquid helium (LHe) cooled cryopanel arrays were designed as an integral part of the beamline in order to provide high differential pumping of hydrogen gas along the beamline. The cryopanel arrays consist of a front (nearer to the torus) disk panel (3 m/sup 2/ each side) with liquid nitrogen (LN/sub 2/) cooled chevrons and a rear cylindrical panel of modified Santeler panels (8 m/sup 2/) which also employs LN/sub 2/ cooled surfaces shielding LHe cooled surfaces. These cryopanels are piped in series. The LHe delivery is based on a closed-loop, forced-flow scheme intended for variable panel temperatures (3.7 to 4.3 K). It uses small tubes for mechanical flexibility and thermal resiliency providing ease of economic defrosting. The cryogenic system consists of a liquefier (100 l/h), a large Dewar, a heat exchanger, and a liquid ring pump. Three beamlines are serviced simultaneously by the system. Pumping speeds measured locally at ionization gauges, were well in excess of the 1.4 x 10/sup 6/ l/s design goal.

  2. The Scanning Nanoprobe Beamline Nanoscopium at Synchrotron Soleil

    NASA Astrophysics Data System (ADS)

    Somogyi, A.; Kewish, C. M.; Polack, F.; Moreno, T.

    2011-09-01

    The Nanoscopium beamline at Synchrotron Soleil will offer advanced scanning-based hard x-ray imaging techniques in the 5- to 20-keV energy range, for user communities working in the earth, environmental, and life sciences. Two dedicated end stations will exploit x-ray coherence to produce images in which contrast is based on a range of physical processes. In the first experiment hutch, coherent scatter imaging techniques will produce images in which contrast arises from spatial variations in the complex refractive index, and orientation in the nanostructure of samples. In the second experiment hutch, elemental mapping will be carried out at the trace (ppm) level by scanning x-ray fluorescence, speciation mapping by XANES, and phase gradient mapping by scanning differential phase contrast imaging. The beamline aims to reach sub-micrometric, down to 30 nm, spatial resolution. This ˜155-meter-long beamline will share the straight section with a future tomography beamline by using canted undulators having 6.5-mrad separation angle. The optical design of Nanoscopium aims to reduce the effect of instabilities on the probing nanobeam by utilizing an all-horizontal geometry for the reflections of the primary beamline mirrors, which focus onto a slit, creating an over-filled secondary source. Kirkpatrick-Baez mirrors and Fresnel zone plates will be used as focusing devices in the experiment hutches. Nanoscopium is expected to commence user operation in 2013.

  3. A beamline for macromolecular crystallography at the Advanced Light Source

    SciTech Connect

    Padmore, H.A.; Earnest, T.; Kim, S.H.; Thompson, A.C.; Robinson, A.L.

    1994-08-01

    A beamline for macromolecular crystallography has been designed for the ALS. The source will be a 37-pole wiggler with a, 2-T on-axis peak field. The wiggler will illuminate three beamlines, each accepting 3 mrad of horizontal aperture. The central beamline will primarily be used for multiple-wavelength anomalous dispersion measurements in the wavelength range from 4 to 0.9 {angstrom}. The beamline optics will comprise a double-crystal monochromator with a collimating pre-mirror and a double-focusing mirror after the monochromator. The two side stations will be used for fixed-wavelength experiments within the wavelength range from 1.5 to 0.95 {angstrom}. The optics will consist of a conventional vertically focusing cylindrical mirror followed by an asymmetrically cut curved-crystal monochromator. This paper presents details of the optimization of the wiggler source for crystallography, gives a description of the beamline configuration, and discusses the reasons for the choices made.

  4. ACRIM III

    Atmospheric Science Data Center

    2015-12-30

    ACRIM III Data and Information Active Cavity Radiometer Irradiance ... the ACRIMSAT spacecraft on December 20, 1999. ACRIM III data are reprocessed every 90 days to utilize instrument recalibration.   ... ACRIM III Instrument Team Page ACRIM II Data Sets SCAR-B Block:  SCAR-B Products ...

  5. An XAFS Beamline at the SAGA Light Source

    SciTech Connect

    Okajima, Toshihiro; Hara, Kazuhiro; Tabata, Masaaki; Setoyama, Hiroyuki; Yoshimura, Daisuke; Chikaura, Yoshinori

    2007-02-02

    A new hard X-ray beamline, BL15, has been designed and constructed at the SAGA-Light Source. The beamline is optimized for industrial applications of the synchrotron light. X-rays with photon energies from 2.1 keV to 14.2 keV are delivered to the experimental station passing a fixed-exit double-crystal Si(111) monochromator and a bent cylindrical mirror. Basic experimental equipments for XAFS measurement, high resolution diffractometry, various kinds of X-ray imaging and energy-dispersive diffractometry have been prepared for the station. From our initial commissioning and performance testing of the beamline, we show that BL15 can perform XAFS measurements.

  6. Upgrade of Saga-university beamline in SAGA-LS

    NASA Astrophysics Data System (ADS)

    Takahashi, K.; Imamura, M.; Yamamoto, I.; Azuma, J.; Ogawa, K.; Kamada, M.; Ohkuma, H.; Yamamoto, S.

    2013-03-01

    Saga-university beamline has been upgraded by installing a new planar-typ e undulator for advanced researches on nano-surfaces and interfaces in the soft X-ray region. The magnetic field of the undulator along the electron beam trajectory was measured at the magnetic gap width between 30 and 150 mm. After the installation of the undulator in a 2.7-m straight section of the Saga-LS storage ring, the performance of the beamline with varied line spacing plane grating monochromator was examined by measurements of peak energy, photon flux, and energy resolution. The beamline is opened for the experimental use in the energy region between 32 and 800 eV using fundamental and the higher harmonics.

  7. Status and evolution of the ESRF beamline ID19

    SciTech Connect

    Weitkamp, Timm; Tafforeau, Paul; Boller, Elodie; Cloetens, Peter; Valade, Jean-Paul; Bernard, Pascal; Baruchel, Jose; Peyrin, Francoise; Helfen, Lukas

    2010-04-06

    The ESRF synchrotron beamline ID19, dedicated to full-field parallel-beam imaging techniques such as phase-contrast and absorption microtomography and X-ray topography, is one of the most versatile instruments of its kind. This paper presents key characteristics of ID19 in its present form, names examples for research and development performed on the beamline, and outlines the plans for an upgrade on the beamline in coming years, to adapt to the growing needs of the user community. The technical goals envisioned include an increase in available beam size and maximum photon energy, and a substantial increase in flux density for applications using beams of small and intermediate size.

  8. The Fundamental Neutron Physics Beamline at the Spallation Neutron Source

    PubMed Central

    Greene, Geoffrey; Cianciolo, Vince; Koehler, Paul; Allen, Richard; Snow, William Michael; Huffman, Paul; Gould, Chris; Bowman, David; Cooper, Martin; Doyle, John

    2005-01-01

    The Spallation Neutron Source (SNS), currently under construction at Oak Ridge National Laboratory with an anticipated start-up in early 2006, will provide the most intense pulsed beams of cold neutrons in the world. At a projected power of 1.4 MW, the time averaged fluxes and fluences of the SNS will approach those of high flux reactors. One of the flight paths on the cold, coupled moderator will be devoted to fundamental neutron physics. The fundamental neutron physics beamline is anticipated to include two beam-lines; a broad band cold beam, and a monochromatic beam of 0.89 nm neutrons for ultracold neutron (UCN) experiments. The fundamental neutron physics beamline will be operated as a user facility with experiment selection based on a peer reviewed proposal process. An initial program of five experiments in neutron decay, hadronic weak interaction and time reversal symmetry violation have been proposed. PMID:27308112

  9. Far-Infrared Beamline at the Canadian Light Source

    NASA Astrophysics Data System (ADS)

    Billinghurst, Brant E.; May, Tim E.

    2014-06-01

    The far-infrared beamline at the Canadian Light Source is a state of the art user facility, which offers significantly more far-infrared brightness than conventional globar sources. The infrared radiation is collected from a bending magnet through a 55 X 37 mrad2 port to a Bruker IFS 125 HR spectrometer, which is equipped with a nine compartment scanning arm, allowing it to achieve spectral resolution better than 0.001 cm-1. Currently the beamline can achieve signal to noise ratios up to 8 times that which can be achieved using a traditional thermal source. This talk will provide an overview of the the beamline, and the capabilities available to users, recent and planned improvements including the addition of a Glow Discharge cell and advances in Coherent Synchrotron Radiation. Furthermore, the process of acquiring access to the facility will be covered.

  10. The Far-Infrared Beamline at the Canadian Light Source

    NASA Astrophysics Data System (ADS)

    Billinghurst, Brant; May, Tim

    2009-06-01

    The far-infrared beamline at the Canadian Light Source. is a state of the art facility, which offers significantly more far-infrared brightness than conventional globar sources. While there is the potential to direct this advantage to many research areas, to date most of the effort has been directed toward high-resolution gas phase studies. The infrared radiation is collected from a bending magnet through a 55 X 37 mrad^{2} port to a Bruker IFS 125 HR spectrometer, which is equipped with a nine compartment scanning arm, allowing it to achieve spectral resolution better than 0.001 cm^{-1}. Currently the beamline can achieve signal to noise ratios up to 8 times that which can be achieved using a traditional thermal source. Data from the recently completed commissioning experiments will be presented along with a general overview of the beamline.

  11. True 3D kinematic analysis for slope instability assessment in the Siq of Petra (Jordan), from high resolution TLS

    NASA Astrophysics Data System (ADS)

    Gigli, Giovanni; Margottini, Claudio; Spizzichino, Daniele; Ruther, Heinz; Casagli, Nicola

    2016-04-01

    Most classifications of mass movements in rock slopes use relatively simple, idealized geometries for the basal sliding surface, like planar sliding, wedge sliding, toppling or columnar failures. For small volumes, the real sliding surface can be often well described by such simple geometries. Extended and complex rock surfaces, however, can exhibit a large number of mass movements, also showing various kind of kinematisms. As a consequence, the real situation in large rock surfaces with a complicate geometry is generally very complex and a site depending analysis, such as fieldwork and compass, cannot be comprehensive of the real situation. Since the outstanding development of terrestrial laser scanner (TLS) in recent years, rock slopes can now be investigated and mapped through high resolution point clouds, reaching the resolution of few mm's and accuracy less than a cm in most advanced instruments, even from remote surveying. The availability of slope surface digital data can offer a unique chance to determine potential kinematisms in a wide distributed area for all the investigated geomorphological processes. More in detail the proposed method is based on the definition of least squares fitting planes on clusters of points extracted by moving a sampling cube on the point cloud. If the associated standard deviation is below a defined threshold, the cluster is considered valid. By applying geometric criteria it is possible to join all the clusters lying on the same surface; in this way discontinuity planes can be reconstructed, rock mass geometrical properties are calculated and, finally, potential kinematisms established. The Siq of Petra (Jordan), is a 1.2 km naturally formed gorge, with an irregular horizontal shape and a complex vertical slope, that represents the main entrance to Nabatean archaeological site. In the Siq, discontinuities of various type (bedding, joints, faults), mainly related to geomorphological evolution of the slope, lateral stress

  12. Distributed control of protein crystallography beamline 5.0 using CORBA

    SciTech Connect

    Timossi, Chris

    1999-09-24

    The Protein Crystallography Beamline at Berkeley Lab's Advanced Light Source is a facility that is being used to solve the structure of proteins. The software that is being used to control this beamline uses Java for user interface applications which communicate via CORBA with workstations that control the beamline hardware. We describe the software architecture for the beamline and our experiences after two years of operation.

  13. APS beamline standard components handbook, Version 1. 3

    SciTech Connect

    Hahn, U.; Shu, D.; Kuzay, T.M.

    1993-02-01

    This Handbook in its current version (1.3) contains descriptions, specifications, and preliminary engineering design drawings for many of the standard components. The design status and schedules have been provided wherever possible. In the near future, the APS plans to update engineering drawings of identified standard beamline components and complete the Handbook. The completed version of this Handbook will become available to both the CATs and potential vendors. Use of standard components should result in major cost reductions for CATs in the areas of beamline design and construction.

  14. Kinematic mounting systems for NSLS beamlines and experiments

    SciTech Connect

    Oversluizen, T.; Stoeber, W.; Johnson, E.D.

    1991-01-01

    Methods for kinematically mounting equipment are well established, but applications at synchrotron radiation facilities are subject to constraints not always encountered in more traditional laboratory settings. Independent position adjustment of beamline components can have significant benefits in terms of minimizing time spent aligning, and maximizing time spent acquiring data. In this paper, we use examples taken from beamlines at the NSLS to demonstrate approaches for optimization of the reproducibility, stability, excursion, and set-up time for various situations. From our experience, we extract general principles which we hope will be useful for workers at other synchrotron radiation facilities. 7 refs., 4 figs.

  15. The Materials Science beamline upgrade at the Swiss Light Source

    PubMed Central

    Willmott, P. R.; Meister, D.; Leake, S. J.; Lange, M.; Bergamaschi, A.; Böge, M.; Calvi, M.; Cancellieri, C.; Casati, N.; Cervellino, A.; Chen, Q.; David, C.; Flechsig, U.; Gozzo, F.; Henrich, B.; Jäggi-Spielmann, S.; Jakob, B.; Kalichava, I.; Karvinen, P.; Krempasky, J.; Lüdeke, A.; Lüscher, R.; Maag, S.; Quitmann, C.; Reinle-Schmitt, M. L.; Schmidt, T.; Schmitt, B.; Streun, A.; Vartiainen, I.; Vitins, M.; Wang, X.; Wullschleger, R.

    2013-01-01

    The Materials Science beamline at the Swiss Light Source has been operational since 2001. In late 2010, the original wiggler source was replaced with a novel insertion device, which allows unprecedented access to high photon energies from an undulator installed in a medium-energy storage ring. In order to best exploit the increased brilliance of this new source, the entire front-end and optics had to be redesigned. In this work, the upgrade of the beamline is described in detail. The tone is didactic, from which it is hoped the reader can adapt the concepts and ideas to his or her needs. PMID:23955029

  16. Upgrades to the Fermilab NuMI beamline

    SciTech Connect

    Martens, Michael A.; Childress, Sam; Grossman, Nancy; Hurh, Patrick; Hylen, James; Marchionni, Alberto; McCluskey, Elaine; Moore, Craig Damon; Reilly, Robert; Tariq, Salman; Wehmann, Alan; /Fermilab

    2007-06-01

    The NuMI beamline at Fermilab has been delivering high-intensity muon neutrino beams to the MINOS experiment since the spring of 2005. A total of 3.4 x 10{sup 20} protons has been delivered to the NuMI target and a maximum beam power of 320 kW has been achieved. An upgrade of the NuMI facility increasing the beam power capability to 700 kW is planned as part of the NOvA experiment. The plans for this upgrade are presented and the possibility of upgrading the NuMI beamline to handle 1.2 MW is considered.

  17. The Materials Science beamline upgrade at the Swiss Light Source.

    PubMed

    Willmott, P R; Meister, D; Leake, S J; Lange, M; Bergamaschi, A; Böge, M; Calvi, M; Cancellieri, C; Casati, N; Cervellino, A; Chen, Q; David, C; Flechsig, U; Gozzo, F; Henrich, B; Jäggi-Spielmann, S; Jakob, B; Kalichava, I; Karvinen, P; Krempasky, J; Lüdeke, A; Lüscher, R; Maag, S; Quitmann, C; Reinle-Schmitt, M L; Schmidt, T; Schmitt, B; Streun, A; Vartiainen, I; Vitins, M; Wang, X; Wullschleger, R

    2013-09-01

    The Materials Science beamline at the Swiss Light Source has been operational since 2001. In late 2010, the original wiggler source was replaced with a novel insertion device, which allows unprecedented access to high photon energies from an undulator installed in a medium-energy storage ring. In order to best exploit the increased brilliance of this new source, the entire front-end and optics had to be redesigned. In this work, the upgrade of the beamline is described in detail. The tone is didactic, from which it is hoped the reader can adapt the concepts and ideas to his or her needs. PMID:23955029

  18. Front end for high-repetition rate thin disk-pumped OPCPA beamline at ELI-beamlines

    NASA Astrophysics Data System (ADS)

    Green, Jonathan T.; Novák, Jakub; Antipenkov, Roman; Batysta, František; Zervos, Charalampos; Naylon, Jack A.; Mazanec, TomáÅ.¡; Horáček, Martin; Bakule, Pavel; Rus, Bedřich

    2015-02-01

    The ELI-Beamlines facility, currently under construction in Prague, Czech Republic, will house multiple high power laser systems with varying pulse energies, pulse durations, and repetition rates. Here we present the status of a high repetition rate beamline currently under construction with target parameters of 20 fs pulse duration, 100 mJ pulse energy, and 1 kHz repetition rate. Specifically we present the Yb:YAG thin disk lasers which are intended to pump picosecond OPCPA, synchronization between pump and signal pulses in the OPCPA, and the first stages of OPCPA.

  19. Beamline Control and Instrumentation System using Industrial Interface Techniques

    NASA Astrophysics Data System (ADS)

    Enz, F.

    2010-06-01

    How should a beamline be designed, which satisfies the needs and requirements of scientists and is easy to build and operate? Today, most control and instrumentation systems for beamlines are based on scientific requirements. Scientific details of the beamline, e.g. vacuum and beam physics details; are usually extensively described. However, control system specifications are often reduced to few requirements, e.g. which beam-related device to use. Lots of these systems work perfectly from the physicist's point of view, but are hard to bring into service and operate and difficult to extend with additional equipment. To overcome this, the engineering company ENZ has developed components using industrial standard interfaces to guarantee high flexibility for equipment extension. Using special interface boards and galvanic isolation offers increased stability of motion control axes. This saves resources during commissioning and service. A control system was developed and installed at a Soft-X-ray beamline at ASP Melbourne. It is operated under EPICs on distributed embedded IOC's based on PC-hardware. Motion and vacuum systems, measurement devices, e.g. a Low-Current Monitor (LoCuM) for beam position monitoring, and parts of the equipment protection system were developed and most of them tested in cooperation with DELTA at the Technical University of Dortmund.

  20. Beamline Control and Instrumentation System using Industrial Interface Techniques

    SciTech Connect

    Enz, F.

    2010-06-23

    How should a beamline be designed, which satisfies the needs and requirements of scientists and is easy to build and operate? Today, most control and instrumentation systems for beamlines are based on scientific requirements. Scientific details of the beamline, e.g. vacuum and beam physics details; are usually extensively described. However, control system specifications are often reduced to few requirements, e.g. which beam-related device to use. Lots of these systems work perfectly from the physicist's point of view, but are hard to bring into service and operate and difficult to extend with additional equipment. To overcome this, the engineering company ENZ has developed components using industrial standard interfaces to guarantee high flexibility for equipment extension. Using special interface boards and galvanic isolation offers increased stability of motion control axes. This saves resources during commissioning and service. A control system was developed and installed at a Soft-X-ray beamline at ASP Melbourne. It is operated under EPICs on distributed embedded IOC's based on PC-hardware. Motion and vacuum systems, measurement devices, e.g. a Low-Current Monitor (LoCuM) for beam position monitoring, and parts of the equipment protection system were developed and most of them tested in cooperation with DELTA at the Technical University of Dortmund.

  1. Pulsed Magnetic Fields for an XAS Energy Dispersive Beamline

    SciTech Connect

    Linden, Peter van der; Mathon, Olivier; Neisius, Thomas

    2007-01-19

    Pulsed magnetic fields constitute an attractive alternative to superconducting magnets for many x-ray techniques. The ESRF ID24 energy dispersive beamline was used for pulsed magnetic field room temperature XMCD measurements on GdCo3. The signal has been measured up to a magnetic field of 5.5 Tesla without signs of deterioration.

  2. A synchrotron beamline for delivering high purity vacuum ultraviolet photons

    SciTech Connect

    Cavasso Filho, R. L.; Homen, M. G. P.; Fonseca, P. T.; Naves de Brito, A.

    2007-11-15

    We report on the current status and performance of the toroidal grating monochromator beamline at the Brazilian Synchrotron Light Laboratory (Laboratorio Nacional de Luz Sincrotron). This beamline provides photons in the vacuum ultraviolet and soft x-ray regions from 12 to 330 eV with three interchangeable gratings. We report on the improvement, which allows the possibility of choosing the light polarization degree from linear to almost circular. Here, we also describe the development of a new apparatus, namely, the mirror-inserted harmonic attenuator and calibrating-device with a long length (MIRHACLLE). All beamlines based on diffraction gratings suffer from the problem of high harmonics contaminations to some extent. The MIRHACLLE provides a way to efficiently suppress high harmonics from 25% to 1 ppm in a grazing incidence bending magnet beamline. Its principle of operation relays on the absorption of the high energy photons in a gas phase region. It allows negligible high harmonics contamination for photon energies ranging from 12 eV to the gas first ionization threshold, 21.6 eV, in the case of neon. We also demonstrate the possibility to use this device for energy calibration and resolution evaluation together with any experiment needing its filtering capabilities. The device is also very cost effective compared to other filters presented previously in the literature.

  3. Description and calibration beamline SEM/Ion Chamber Current Digitizer

    SciTech Connect

    Schoo, D.

    1994-05-01

    This report discusses the following on beamline SEM/ion chamber current digitizers: Module description; testing and calibration; common setup procedures; summary of fault indications and associated causes; summary of input and output connections; SEM conversion constant table; ion chamber conversion constant table; hexadecimal to decimal conversion table; and schematic diagram.

  4. A modular optics design for the LBNE beamline

    SciTech Connect

    Johnstone, John A.; /Fermilab

    2010-10-01

    Protons extracted from the Main Injector (MI) in the MI-60 straight section are transported 84 m through quadrupole Q106 in the NuMI stub, at which point two 6-3-120 vertical switching magnets, followed by three EPB vertical dipoles, steer the beam into the main body of the LBNE beamline. From Q106 in NuMI the LBNE beamline transports these protons 722.0 m to the LBNE target, located 41.77 m (137.0 ft) below the MI beamline center (BLC) elevation, on a trajectory aimed towards DUSEL. Bending is provided (predominantly) by 34 long (6 m) MI-style IDA/IDB and 8 short (4 m) IDC/IDD dipoles [through 48.36{sup o} horizontally and -5.844{sup o} (net) vertically]. Optical properties are defined by 49 quadrupoles (grouped functionally into 44 focusing centers) of the proven MI beamline-style 3Q60/3Q120 series. All focusing centers are equipped with redesigned MI-style IDS orbit correctors and dual-plane beam position monitors (BPM's). Ample space is available in each arc cell to accommodate ion pumps and diagnostic instrumentation. Parameters of the main magnets are listed in a table.

  5. VESPERS: A Beamline for Combined XRF and XRD Measurements

    NASA Astrophysics Data System (ADS)

    Feng, Renfei; Gerson, Andrea; Ice, Gene; Reininger, Ruben; Yates, Brian; McIntyre, Stewart

    2007-01-01

    VESPERS (VEry Sensitive Elemental and Structural Probe Employing Radiation from a Synchrotron) is a bending magnet beamline that is just beginning construction at the Canadian Light Source. The beamline has several novel design elements that are intended to increase its operating flexibility and availability to users. First, there is a requirement to deliver a microscopic beam with a variable bandwidth, thus enabling the generation of Laue diffraction patterns and high yield X-ray fluorescence spectra from the same region preferably simultaneously. Thus, the bandpass of the VESPERS monochromator can be readily changed to focus radiation into the same 2-4 micron diameter area that is either polychromatic or having a bandwidth of 10%, 1.6% or 0.01%. This allows the user to change the diffraction pattern to suit the complexity of the crystal and the spectral signal to noise ratio to suit the detection sensitivity required. Second, the beamline is designed to have two branches capable of operating simultaneously and virtually independently using the same primary optics. These design features are accomplished using four separate beams originating at four pinholes at the entry to the Primary Optical Enclosure. The compound focus design uses spherical mirrors to focus both polychromatic and pre-monochromatic beams onto the intermediate slits. A pair of bendable K-B mirrors in the experimental hutch is used to demagnify the beam further down to micron size. The photon energy of this beamline is 6-30 keV.

  6. VESPERS: A Beamline for Combined XRF and XRD Measurements

    SciTech Connect

    Feng Renfei; Yates, Brian; Gerson, Andrea; Ice, Gene; Reininger, Ruben; McIntyre, Stewart

    2007-01-19

    VESPERS (VEry Sensitive Elemental and Structural Probe Employing Radiation from a Synchrotron) is a bending magnet beamline that is just beginning construction at the Canadian Light Source. The beamline has several novel design elements that are intended to increase its operating flexibility and availability to users. First, there is a requirement to deliver a microscopic beam with a variable bandwidth, thus enabling the generation of Laue diffraction patterns and high yield X-ray fluorescence spectra from the same region preferably simultaneously. Thus, the bandpass of the VESPERS monochromator can be readily changed to focus radiation into the same 2-4 micron diameter area that is either polychromatic or having a bandwidth of 10%, 1.6% or 0.01%. This allows the user to change the diffraction pattern to suit the complexity of the crystal and the spectral signal to noise ratio to suit the detection sensitivity required. Second, the beamline is designed to have two branches capable of operating simultaneously and virtually independently using the same primary optics. These design features are accomplished using four separate beams originating at four pinholes at the entry to the Primary Optical Enclosure. The compound focus design uses spherical mirrors to focus both polychromatic and pre-monochromatic beams onto the intermediate slits. A pair of bendable K-B mirrors in the experimental hutch is used to demagnify the beam further down to micron size. The photon energy of this beamline is 6-30 keV.

  7. The Nanoscience Beamline (I06) at Diamond Light Source

    SciTech Connect

    Dhesi, S. S.; Cavill, S. A.; Potenza, A.; Marchetto, H.; Mott, R. A.; Steadman, P.; Peach, A.; Shepherd, E. L.; Ren, X.; Wagner, U. H.; Reininger, R.

    2010-06-23

    The Nanoscience beamline (I06) is one of seven Diamond Phase-I beamlines which has been operational since January 2007 delivering polarised soft x-rays, for a PhotoEmission Electron Microscope (PEEM) and branchline, in the energy range 80-2100 eV. The beamline is based on a collimated plane grating monochromator with sagittal focusing elements, utilising two APPLE II helical undulator sources, and has been designed for high flux density at the PEEM sample position. A {approx}5 {mu}m ({sigma}) diameter beam is focussed onto the sample in the PEEM allowing a range of experiments using x-ray absorption spectroscopy (XAS), x-ray magnetic circular dichroism (XMCD) and x-ray magnetic linear dichroism (XMLD) as contrast mechanisms. The beamline is also equipped with a branchline housing a 6T superconducting magnet for XMCD and XMLD experiments. The magnet is designed to move on and off the branchline which allows a diverse range of experiments.

  8. The Nanoscience Beamline (I06) at Diamond Light Source

    NASA Astrophysics Data System (ADS)

    Dhesi, S. S.; Cavill, S. A.; Potenza, A.; Marchetto, H.; Mott, R. A.; Steadman, P.; Peach, A.; Shepherd, E. L.; Ren, X.; Wagner, U. H.; Reininger, R.

    2010-06-01

    The Nanoscience beamline (I06) is one of seven Diamond Phase-I beamlines which has been operational since January 2007 delivering polarised soft x-rays, for a PhotoEmission Electron Microscope (PEEM) and branchline, in the energy range 80-2100 eV. The beamline is based on a collimated plane grating monochromator with sagittal focusing elements, utilising two APPLE II helical undulator sources, and has been designed for high flux density at the PEEM sample position. A ˜5 μm (σ) diameter beam is focussed onto the sample in the PEEM allowing a range of experiments using x-ray absorption spectroscopy (XAS), x-ray magnetic circular dichroism (XMCD) and x-ray magnetic linear dichroism (XMLD) as contrast mechanisms. The beamline is also equipped with a branchline housing a 6T superconducting magnet for XMCD and XMLD experiments. The magnet is designed to move on and off the branchline which allows a diverse range of experiments.

  9. Aberration analysis calculations for synchrotron radiation beamline design

    SciTech Connect

    McKinney, W.R.; Howells, M.; Padmore, H.A.

    1997-09-01

    The application of ray deviation calculations based on aberration coefficients for a single optical surface for the design of beamline optical systems is reviewed. A systematic development is presented which allows insight into which aberration may be causing the rays to deviate from perfect focus. A new development allowing analytical calculation of line shape is presented.

  10. Neutral beamline with improved ion-energy recovery

    SciTech Connect

    Dagenhart, W.K.; Haselton, H.H.; Stirling, W.L.; Whealton, J.H.

    1981-04-13

    A neutral beamline generator with unneutralized ion energy recovery is provided which enhances the energy recovery of the full energy ion component of the beam exiting the neutralizer cell of the beamline. The unneutralized full energy ions exiting the neutralizer are deflected from the beam path and the electrons in the cell are blocked by a magnetic field applied transverse to the beamline in the cell exit region. The ions, which are generated at essentially ground potential and accelerated through the neutralizer cell by a negative acceleration voltage, are collected at ground potential. A neutralizer cell exit end region is provided which allows the magnetic and electric fields acting on the exiting ions to be closely coupled. As a result, the fractional energy ions exiting the cell with the full energy ions are reflected back into the gas cell. Thus, the fractional energy ions do not detract from the energy recovery efficiency of full energy ions exiting the cell which can reach the ground potential interior surfaces of the beamline housing.

  11. The INE-Beamline for actinide science at ANKA

    NASA Astrophysics Data System (ADS)

    Rothe, J.; Butorin, S.; Dardenne, K.; Denecke, M. A.; Kienzler, B.; Löble, M.; Metz, V.; Seibert, A.; Steppert, M.; Vitova, T.; Walther, C.; Geckeis, H.

    2012-04-01

    Since its inauguration in 2005, the INE-Beamline for actinide research at the synchrotron source ANKA (KIT North Campus) provides dedicated instrumentation for x-ray spectroscopic characterization of actinide samples and other radioactive materials. R&D work at the beamline focuses on various aspects of nuclear waste disposal within INE's mission to provide the scientific basis for assessing long-term safety of a final nuclear waste repository. The INE-Beamline is accessible for the actinide and radiochemistry community through the ANKA proposal system and the European Union Integrated Infrastructure Initiative ACTINET-I3. Experiments with activities up to 1 × 10+6 times the European exemption limit are feasible within a safe but flexible containment concept. Measurements with monochromatic radiation are performed at photon energies varying between ˜2.1 keV (P K-edge) and ˜25 keV (Pd K-edge), including the lanthanide L-edges and the actinide M- and L3-edges up to Cf. The close proximity of the INE-Beamline to INE controlled area labs offers infrastructure unique in Europe for the spectroscopic and microscopic characterization of actinide samples. The modular beamline design enables sufficient flexibility to adapt sample environments and detection systems to many scientific questions. The well-established bulk techniques x-ray absorption fine structure (XAFS) spectroscopy in transmission and fluorescence mode have been augmented by advanced methods using a microfocused beam, including (confocal) XAFS/x-ray fluorescence detection and a combination of (micro-)XAFS and (micro-)x-ray diffraction. Additional instrumentation for high energy-resolution x-ray emission spectroscopy has been successfully developed and tested.

  12. The INE-Beamline for actinide science at ANKA

    SciTech Connect

    Rothe, J.; Dardenne, K.; Denecke, M. A.; Kienzler, B.; Loeble, M.; Metz, V.; Steppert, M.; Vitova, T.; Geckeis, H.; Butorin, S.; Seibert, A.; Walther, C.

    2012-04-15

    Since its inauguration in 2005, the INE-Beamline for actinide research at the synchrotron source ANKA (KIT North Campus) provides dedicated instrumentation for x-ray spectroscopic characterization of actinide samples and other radioactive materials. R and D work at the beamline focuses on various aspects of nuclear waste disposal within INE's mission to provide the scientific basis for assessing long-term safety of a final nuclear waste repository. The INE-Beamline is accessible for the actinide and radiochemistry community through the ANKA proposal system and the European Union Integrated Infrastructure Initiative ACTINET-I3. Experiments with activities up to 1 x 10{sup +6} times the European exemption limit are feasible within a safe but flexible containment concept. Measurements with monochromatic radiation are performed at photon energies varying between {approx}2.1 keV (P K-edge) and {approx}25 keV (Pd K-edge), including the lanthanide L-edges and the actinide M- and L3-edges up to Cf. The close proximity of the INE-Beamline to INE controlled area labs offers infrastructure unique in Europe for the spectroscopic and microscopic characterization of actinide samples. The modular beamline design enables sufficient flexibility to adapt sample environments and detection systems to many scientific questions. The well-established bulk techniques x-ray absorption fine structure (XAFS) spectroscopy in transmission and fluorescence mode have been augmented by advanced methods using a microfocused beam, including (confocal) XAFS/x-ray fluorescence detection and a combination of (micro-)XAFS and (micro-)x-ray diffraction. Additional instrumentation for high energy-resolution x-ray emission spectroscopy has been successfully developed and tested.

  13. Instrumentation and Experimental Developments for the Beamlines at the Synchrotron SOLEIL

    SciTech Connect

    Prigent, P.; Bac, S.; Blanchandin, S.; Cauchon, G.; David, G.; Fernandez Varela, P.; Kubsky, S.; Picca, F.

    2010-06-23

    This paper presents an overview of the instrumentation and experiments developed for the beamlines at Synchrotron SOLEIL in France. Currently fourteen beamlines are opened to users out of the twenty six scheduled. About half of the beamlines cover the soft x-rays region using spectroscopy and imagery techniques. The second half covers the hard x-rays field studying diffraction of matter. Some sample environments carried out for beamlines, for biology, chemistry and surface sciences are described. For the soft x-rays beamlines, carbon contamination of optics is a crucial issue. Different experiments are currently under study in order to reduce or even avoid this effect. Other studies relate to the improvement of metrological methods for beamline optics, to the reduction of vibrational effects for the microbeams and development of computer control for diffractometers. The various types of instruments and experiments will be presented both with an overview of the status of the beamlines in operation and under construction.

  14. Beamline 9.3.2 - a high-resolution, bend-magnet beamline with circular polarization capability

    SciTech Connect

    Moler, E.J.; Hussain, Z.; Howells, M.R.

    1997-04-01

    Beamline 9.3.2 is a high resolution, SGM beamline on an ALS bending magnet with access to photon energies from 30-1500 eV. Features include circular polarization capability, a rotating chamber platform that allows switching between experiments without breaking vacuum, an active feedback system that keeps the beam centered on the entrance slit of the monochromator, and a bendable refocusing mirror. The beamline optics consist of horizontally and vertically focussing mirrors, a Spherical Grating Monochromator (SGM) with movable entrance and exit slits, and a bendable refocussing mirror. In addition, a movable aperature has been installed just upstream of the vertically focussing mirror which can select the x-rays above or below the plane of the synchrotron storage ring, allowing the user to select circularly or linearly polarized light. Circularly polarized x-rays are used to study the magnetic properties of materials. Beamline 9.3.2 can supply left and right circularly polarized x-rays by a computer controlled aperture which may be placed above or below the plane of the synchrotron storage ring. The degree of linear and circular polarization has been measured and calibrated.

  15. SAGE III

    Atmospheric Science Data Center

    2016-06-15

    SAGE III Data and Information The Stratospheric Aerosol and Gas ... on the spacecraft. SAGE III produced L1 and L2 scientific data from 5/07/2002 until 12/31/2005. The flight of the second instrument is as ... Guide Documents:  Project Guide Data Products User's Guide  (PDF) Relevant Documents:  ...

  16. The ID23-2 structural biology microfocus beamline at the ESRF

    PubMed Central

    Flot, David; Mairs, Trevor; Giraud, Thierry; Guijarro, Matias; Lesourd, Marc; Rey, Vicente; van Brussel, Denis; Morawe, Christian; Borel, Christine; Hignette, Olivier; Chavanne, Joel; Nurizzo, Didier; McSweeney, Sean; Mitchell, Edward

    2010-01-01

    The first phase of the ESRF beamline ID23 to be constructed was ID23-1, a tunable MAD-capable beamline which opened to users in early 2004. The second phase of the beamline to be constructed is ID23-2, a monochromatic microfocus beamline dedicated to macromolecular crystallography experiments. Beamline ID23-2 makes use of well characterized optical elements: a single-bounce silicon (111) monochromator and two mirrors in Kirkpatrick–Baez geometry to focus the X-ray beam. A major design goal of the ID23-2 beamline is to provide a reliable, easy-to-use and routine microfocus beam. ID23-2 started operation in November 2005, as the first beamline dedicated to microfocus macromolecular crystallography. The beamline has taken the standard automated ESRF macromolecular crystallography environment (both hardware and software), allowing users of ID23-2 to be rapidly familiar with the microfocus environment. This paper describes the beamline design, the special considerations taken into account given the microfocus beam, and summarizes the results of the first years of the beamline operation. PMID:20029119

  17. The crystallography beamline I711 at MAX II.

    PubMed

    Cerenius, Y; Ståhl, K; Svensson, L A; Ursby, T; Oskarsson, A; Albertsson, J; Liljas, A

    2000-07-01

    A new X-ray crystallographic beamline is operational at the MAX II synchrotron in Lund. The beamline has been in regular use since August 1998 and is used both for macro- and small molecule diffraction as well as powder diffraction experiments. The radiation source is a 1.8 T multipole wiggler. The beam is focused vertically by a bendable mirror and horizontally by an asymmetrically cut Si(111) monochromator. The wavelength range is 0.8-1.55 A with a measured flux at 1 A of more than 10(11) photons s(-1) in 0.3 mm x 0.3 mm at the sample position. The station is currently equipped with a Mar345 imaging plate, a Bruker Smart 1000 area CCD detector and a Huber imaging-plate Guinier camera. An ADSC 210 area CCD detector is planned to be installed during 2000. PMID:16609196

  18. Simulations of proton beam characteristics for ELIMED Beamline

    NASA Astrophysics Data System (ADS)

    Psikal, Jan; Limpouch, Jiri; Klimo, Ondrej; Vyskocil, Jiri; Margarone, Daniele; Korn, Georg

    2016-03-01

    ELIMED Beamline should demonstrate the capability of laser-based particle accelerators for medical applications, mainly for proton radiotherapy of tumours which requires a sufficient number of accelerated protons with energy about 60 MeV at least. In this contribution, we study the acceleration of protons by laser pulse with parameters accessible for ELIMED Beamline (intensity ∼ 1022 W/cm2, pulse length ∼ 30 fs). In our two-dimensional particle-incell simulations, we observed higher energies of protons for linear than for circular polarization. Oblique incidence of the laser pulse on target does not seem to be favourable for proton acceleration at such high intensities as the accelerated protons are deflected from target normal axis and their energy and numbers are slightly decreased. The expected numbers of accelerated protons in the energy interval 60 MeV ± 5% are calculated between 109 and 1010 per laser shot with estimated proton beam divergence about 20° (FWHM).

  19. MONO: A program to calculate synchrotron beamline monochromator throughputs

    SciTech Connect

    Chapman, D.

    1989-01-01

    A set of Fortran programs have been developed to calculate the expected throughput of x-ray monochromators with a filtered synchrotron source and is applicable to bending magnet and wiggler beamlines. These programs calculate the normalized throughput and filtered synchrotron spectrum passed by multiple element, flat un- focussed monochromator crystals of the Bragg or Laue type as a function of incident beam divergence, energy and polarization. The reflected and transmitted beam of each crystal is calculated using the dynamical theory of diffraction. Multiple crystal arrangements in the dispersive and non-dispersive mode are allowed as well as crystal asymmetry and energy or angle offsets. Filters or windows of arbitrary elemental composition may be used to filter the incident synchrotron beam. This program should be useful to predict the intensities available from many beamline configurations as well as assist in the design of new monochromator and analyzer systems. 6 refs., 3 figs.

  20. Performance of Saga-University Beamline with Planer Undulator

    SciTech Connect

    Azuma, J.; Takahashi, K.; Kamada, M.; Ohkuma, H.; Yamamoto, S.

    2010-06-23

    A planer undulator consisted of 24 periods of an 85-mm length has been installed in a 2.7-m straight section of the SAGA-LS, in order to provide brilliant soft x-rays for advanced researches on nano-surfaces and interfaces at the Saga-university beamline BL13. The photon flux of 2x10{sup 11} photons/100 mA was obtained at 133 eV, and the available photon energy was beyond 800 eV using higher harmonics. The achieved resolving power of the varied-line-spacing (VLS) monochromator system was 8,670 at 130 eV with slits of 15 um. This agrees very well with the value of 8,790 expected from the ray-tracing calculation. The details in the performance tests will be reported, indicating the high performance of the beamline BL13 for photoelectron spectroscopy in the soft x-ray region.

  1. An Undulator-Wiggler Beamline for Spectromicroscopy at SRC

    NASA Astrophysics Data System (ADS)

    Reininger, R.; De Stasio, G.; Bissen, M.; Severson, M.

    2004-05-01

    A high-flux medium-energy-resolution beamline based on an existing insertion device is being constructed at SRC. The insertion device will be operated as an undulator up to ˜400 eV and as a wiggler at higher energies. The beamline will be dedicated mainly to X-ray PhotoElectron Emission spectroMicroscopy (X-PEEM) and will cover the energy range 75-2000 eV. The most relevant requirement for high-resolution and high-sensitivity X-PEEM is a high flux density on the sample surface. This will allow spatial resolutions on the order of a few nanometers, and a minimum detection limit on the order of 10 parts per million, using the already existing Spectromicroscope for PHotoelectron Imaging of Nanostructures with X-rays (SPHINX). To maximize the flux at the sample position, the beamline does not include an entrance slit and has only three optical elements on the beam path: an ellipsoidal mirror, a variable-line-spacing plane grating, and a re-focusing ellipsoidal mirror. The first ellipsoidal mirror provides the converging light to one of the three gratings needed to cover the beamline energy range. The position of the fixed exit slit is at the focus of the ellipsoidal mirror when the grating is tuned to zero order. The second ellipsoidal mirror demagnifies the beam at the exit slit plane by a factor of two. More than 1012 photons/s are expected at the sample position between 100 and 1200 eV onto a spot having a FWHM of 25 μm vertical and 70 μm horizontal at a resolving power of ˜1000.

  2. An Undulator-Wiggler Beamline for Spectromicroscopy at SRC

    SciTech Connect

    Reininger, R.; De Stasio, G.; Bissen, M.; Severson, M.

    2004-05-12

    A high-flux medium-energy-resolution beamline based on an existing insertion device is being constructed at SRC. The insertion device will be operated as an undulator up to {approx}400 eV and as a wiggler at higher energies. The beamline will be dedicated mainly to X-ray PhotoElectron Emission spectroMicroscopy (X-PEEM) and will cover the energy range 75-2000 eV. The most relevant requirement for high-resolution and high-sensitivity X-PEEM is a high flux density on the sample surface. This will allow spatial resolutions on the order of a few nanometers, and a minimum detection limit on the order of 10 parts per million, using the already existing Spectromicroscope for PHotoelectron Imaging of Nanostructures with X-rays (SPHINX). To maximize the flux at the sample position, the beamline does not include an entrance slit and has only three optical elements on the beam path: an ellipsoidal mirror, a variable-line-spacing plane grating, and a re-focusing ellipsoidal mirror. The first ellipsoidal mirror provides the converging light to one of the three gratings needed to cover the beamline energy range. The position of the fixed exit slit is at the focus of the ellipsoidal mirror when the grating is tuned to zero order. The second ellipsoidal mirror demagnifies the beam at the exit slit plane by a factor of two. More than 1012 photons/s are expected at the sample position between 100 and 1200 eV onto a spot having a FWHM of 25 {mu}m vertical and 70 {mu}m horizontal at a resolving power of {approx}1000.

  3. MERLIN - A meV Resolution Beamline at the ALS

    SciTech Connect

    Reininger, Ruben; Bozek, John; Chuang, Y.-D.; Howells, Malcolm; Kelez, Nicholas; Prestemon, Soren; Marks, Steve; Warwick, Tony; Hussain, Zahid; Jozwiak, Chris; Lanzara, Alessandra; Hasan, M. Zahid

    2007-01-19

    An ultra-high resolution beamline is being constructed at the Advanced Light Source (ALS) for the study of low energy excitations in strongly correlated systems with the use of high-resolution inelastic scattering and angle-resolved photoemission. This new beamline, given the acronym Merlin (for meV resolution line), will cover the energy range 10-150 eV. The monochromator has fixed entrance and exit slits and a plane mirror that can illuminate a spherical grating at the required angle of incidence (as in the SX-700 mechanism). The monochromator can be operated in two different modes. In the highest resolution mode, the energy scanning requires translating the monochromator chamber (total travel 1.1 m) as well as rotating the grating and the plane mirror in front of the grating. The resolution in this mode is practically determined by the slits width. In the second mode, the scanning requires rotating the grating and the plane mirror. This mode can be used to scan a few eV without a significant resolution loss. The source for the beamline is a 1.9 m long, 90 mm period quasi periodic EPU. The expected flux at the sample is higher than 1011 photons/s at a resolving power of 5 x 104 in the energy range 16-130 eV. A second set of gratings can be used to obtain higher flux at the expense of resolution.

  4. Design and Simulation of the nuSTORM Pion Beamline

    SciTech Connect

    Liu, A.; Neuffer, D.; Bross, A.

    2015-08-15

    The nuSTORM (neutrinos from STORed Muons) proposal presents a detailed design for a neutrino facility based on a muon storage ring, with muon decay in the production straight section of the ring providing well defined neutrino beams. The facility includes a primary high-energy proton beam line, a target station with pion production and collection, and a pion beamline for pion transportation and injection into a muon decay ring. The nuSTORM design uses “stochastic injection”, in which pions are directed by a chicane, referred to as the Orbit Combination Section (OCS), into the production straight section of the storage ring. Pions that decay within that straight section provide muons within the circulating acceptance of the ring. Furthermore, the design enables injection without kickers or a separate pion decay transport line. The beam line that the pions traverse before being extracted from the decay ring is referred to as the pion beamline. Our paper describes the design and simulation of the pion beamline, and includes full beam dynamics simulations of the system.

  5. Design and Simulation of the nuSTORM Pion Beamline

    DOE PAGESBeta

    Liu, A.; Neuffer, D.; Bross, A.

    2015-08-15

    The nuSTORM (neutrinos from STORed Muons) proposal presents a detailed design for a neutrino facility based on a muon storage ring, with muon decay in the production straight section of the ring providing well defined neutrino beams. The facility includes a primary high-energy proton beam line, a target station with pion production and collection, and a pion beamline for pion transportation and injection into a muon decay ring. The nuSTORM design uses “stochastic injection”, in which pions are directed by a chicane, referred to as the Orbit Combination Section (OCS), into the production straight section of the storage ring. Pionsmore » that decay within that straight section provide muons within the circulating acceptance of the ring. Furthermore, the design enables injection without kickers or a separate pion decay transport line. The beam line that the pions traverse before being extracted from the decay ring is referred to as the pion beamline. Our paper describes the design and simulation of the pion beamline, and includes full beam dynamics simulations of the system.« less

  6. Attosecond beamline with actively stabilized and spatially separated beam paths.

    PubMed

    Huppert, M; Jordan, I; Wörner, H J

    2015-12-01

    We describe a versatile and compact beamline for attosecond spectroscopy. The setup consists of a high-order harmonic source followed by a delay line that spatially separates and then recombines the extreme-ultraviolet (XUV) and residual infrared (IR) pulses. The beamline introduces a controlled and actively stabilized delay between the XUV and IR pulses on the attosecond time scale. A new active-stabilization scheme combining a helium-neon-laser and a white-light interferometer minimizes fluctuations and allows to control delays accurately (26 as rms during 1.5 h) over long time scales. The high-order-harmonic-generation region is imaged via optical systems, independently for XUV and IR, into an interaction volume to perform pump-probe experiments. As a consequence of the spatial separation, the pulses can be independently manipulated in intensity, polarization, and frequency content. The beamline can be combined with a variety of detectors for measuring attosecond dynamics in gases, liquids, and solids. PMID:26724005

  7. ADLIB—A simple database framework for beamline codes

    NASA Astrophysics Data System (ADS)

    Mottershead, C. Thomas

    1993-12-01

    There are many well developed codes available for beamline design and analysis. A significant fraction of each of these codes is devoted to processing its own unique input language for describing the problem. None of these large, complex, and powerful codes does everything. Adding a new bit of specialized physics can be a difficult task whose successful completion makes the code even larger and more complex. This paper describes an attempt to move in the opposite direction, toward a family of small, simple, single purpose physics and utility modules, linked by an open, portable, public domain database framework. These small specialized physics codes begin with the beamline parameters already loaded in the database, and accessible via the handful of subroutines that constitute ADLIB. Such codes are easier to write, and inherently organized in a manner suitable for incorporation in model based control system algorithms. Examples include programs for analyzing beamline misalignment sensitivities, for simulating and fitting beam steering data, and for translating among MARYLIE, TRANSPORT, and TRACE3D formats.

  8. Attosecond beamline with actively stabilized and spatially separated beam paths

    NASA Astrophysics Data System (ADS)

    Huppert, M.; Jordan, I.; Wörner, H. J.

    2015-12-01

    We describe a versatile and compact beamline for attosecond spectroscopy. The setup consists of a high-order harmonic source followed by a delay line that spatially separates and then recombines the extreme-ultraviolet (XUV) and residual infrared (IR) pulses. The beamline introduces a controlled and actively stabilized delay between the XUV and IR pulses on the attosecond time scale. A new active-stabilization scheme combining a helium-neon-laser and a white-light interferometer minimizes fluctuations and allows to control delays accurately (26 as rms during 1.5 h) over long time scales. The high-order-harmonic-generation region is imaged via optical systems, independently for XUV and IR, into an interaction volume to perform pump-probe experiments. As a consequence of the spatial separation, the pulses can be independently manipulated in intensity, polarization, and frequency content. The beamline can be combined with a variety of detectors for measuring attosecond dynamics in gases, liquids, and solids.

  9. MARS, a new beamline for radioactive matter studies at SOLEIL

    NASA Astrophysics Data System (ADS)

    Solari, Pier Lorenzo; Schlutig, Sandrine; Hermange, Hervé; Sitaud, Bruno

    2009-11-01

    MARS (Multi Analyses on Radioactive Samples) beamline is the hard X-ray bending magnet beamline dedicated to the study of radioactive matter of the new French synchrotron SOLEIL. The beamline, which has been built thanks to a close partnership and support by the CEA, has been designed to provide X-rays in the energy range of 3.5 keV to 35 keV. This allows to encompass M and L absorption edges of actinides, as well as K edges of transition metals (that are present in alloys and fuel claddings) up to heavy halogens, rare gases and alkalis (fission products in nuclear fuels). The MARS project aims to extend the possibilities of synchrotron based X-ray characterizations towards a wider variety of radioactive elements and a wider variety of techniques than what is currently available at other facilities. Thus, its specific and innovative infrastructure has been optimized in order to carry out analyses on materials with activities up to 18.5 GBq per sample for α and β emitters and 2 GBq for γ and n emitters. So, today, more than 70 different elements and more than 350 different isotopes have been proposed for studies on the beamline by the involved user community. The arrangement of the different elements in the optics hutch is based on an original scheme which permits to have two alternative optical configurations (monochromatic or dispersive) depending on the nature of experiments to be performed. At least three main techniques are progressively being proposed on the three complementary end-stations located in the experimental hutch: transmission and high resolution powder diffraction (TXRD and HRXRD), standard and dispersive X-ray absorption spectroscopy (XAS and EDXAS) and X-ray fluorescence (XRF). In addition, by using the KB optics, a micro-focused beam will be available on the second station of the monochromatic branch. The beamline is currently under commissioning. The first two experimental stations, using the monochromatic branch, are scheduled to be

  10. Advanced light source vacuum policy and vacuum guidelines for beamlines and experiment endstations

    SciTech Connect

    Hussain, Z.

    1995-08-01

    The purpose of this document is to: (1) Explain the ALS vacuum policy and specifications for beamlines and experiment endstations. (2) Provide guidelines related to ALS vacuum policy to assist in designing beamlines which are in accordance with ALS vacuum policy. This document supersedes LSBL-116. The Advanced Light Source is a third generation synchrotron radiation source whose beam lifetime depends on the quality of the vacuum in the storage ring and the connecting beamlines. The storage ring and most of the beamlines share a common vacuum and are operated under ultra-high-vacuum (UHV) conditions. All endstations and beamline equipment must be operated so as to avoid contamination of beamline components, and must include proper safeguards to protect the storage ring vacuum from an accidental break in the beamline or endstation vacuum systems. The primary gas load during operation is due to thermal desorption and electron/photon induced desorption of contaminants from the interior of the vacuum vessel and its components. The desorption rates are considerably higher for hydrocarbon contamination, thus considerable emphasis is placed on eliminating these sources of contaminants. All vacuum components in a beamline and endstation must meet the ALS vacuum specifications. The vacuum design of both beamlines and endstations must be approved by the ALS Beamline Review Committee (BRC) before vacuum connections to the storage ring are made. The vacuum design is first checked during the Beamline Design Review (BDR) held before construction of the beamline equipment begins. Any deviation from the ALS vacuum specifications must be approved by the BRC prior to installation of the equipment on the ALS floor. Any modification that is incorporated into a vacuum assembly without the written approval of the BRC is done at the user`s risk and may lead to rejection of the whole assembly.

  11. The beamlines of ELETTRA and their application to structural biology.

    PubMed

    Zanini, F; Lausi, A; Savoia, A

    1999-01-01

    Protein crystallographers are nowadays regular users of synchrotron radiation (SR) facilities for several applications. The goal of majority of users is simply to extract more accurate, higher resolution data from existing crystals; they use monochromatic radiation and the rotation method, in order to get a complete survey of the reciprocal space in a short time. In fact the brilliance of SR is essential, due to the weak scattering power of the samples, and because of their sensibility to radiation damage. Over the last few years, however, a general increase of interest for measurements at multiple wavelengths, which exploit the anomalous dispersion for the phase problem (multiwavelength anomalous diffraction--MAD), has generated the need of intense tuneable sources. For these applications, the emphasis is on accurate measurements of the small differences between the intensities of Bragg reflections at various energies across the absorption edge of an element present in the sample. The macromolecular diffraction beamline at ELETTRA, which is now running routinely since spring 1995, has been designed to provide a high flux--highly collimated tuneable X-rays source in the spectral range between 4 and 25 keV. The radiation source is the 57-pole wiggler, which delivers a very intense radiation up to 25 keV, and is shared and used simultaneously with the small angle X-ray scattering (SAXS) beamline. The front-end filter system has a cut-off energy at about 4 keV. The beamline optics consists of a pseudo-channel-cut double-crystal monochromator followed by a double focusing toroidal mirror. The tunability and the stability of the monochromator allows the user to perform MAD experiments, and for this purpose, a fluorescence probe for the exact calibration of the absorption edge is available on-line. The experimental station is based on an imaging plate area detector from MarResearch, with a sensible area of 345 mm in diameter. A cooled N2-stream is available to cool the

  12. HERMES: a soft X-ray beamline dedicated to X-ray microscopy.

    PubMed

    Belkhou, Rachid; Stanescu, Stefan; Swaraj, Sufal; Besson, Adrien; Ledoux, Milena; Hajlaoui, Mahdi; Dalle, Didier

    2015-07-01

    The HERMES beamline (High Efficiency and Resolution beamline dedicated to X-ray Microscopy and Electron Spectroscopy), built at Synchrotron SOLEIL (Saint-Auban, France), is dedicated to soft X-ray microscopy. The beamline combines two complementary microscopy methods: XPEEM (X-ray Photo Emitted Electron Microscopy) and STXM (Scanning Transmission X-ray Microscopy) with an aim to reach spatial resolution below 20 nm and to fully exploit the local spectroscopic capabilities of the two microscopes. The availability of the two methods within the same beamline enables the users to select the appropriate approach to study their specific case in terms of sample environment, spectroscopy methods, probing depth etc. In this paper a general description of the beamline and its design are presented. The performance and specifications of the beamline will be reviewed in detail. Moreover, the article is aiming to demonstrate how the beamline performances have been specifically optimized to fulfill the specific requirements of a soft X-ray microscopy beamline in terms of flux, resolution, beam size etc. Special attention has been dedicated to overcome some limiting and hindering problems that are usually encountered on soft X-ray beamlines such as carbon contamination, thermal stability and spectral purity. PMID:26134801

  13. Further measurements of bremsstrahlung from the insertion device beamlines of the Advanced Photon Source.

    SciTech Connect

    Job, P. K.

    1998-09-16

    Bremsstrahlung is produced in the Advanced Photon Source (APS) storage ring when the positron beam interacts with the storage-ring components or with the residual gas molecules in the storage-ring vacuum. The interaction of the positrons with the gas molecules occurs continually during storage ring operation. Bremsstrahlung is important at the insertion device straight sections because the contribution from each interaction adds up to produce a narrow mono-directional beam that travel down the beamlines. At the APS, with long storage ring beam straight paths (15.38 meters), gas bremsstrahlung in the insertion device beamlines can be significant. The preliminary results of the bremsstrahlung measurements in the insertion device beamlines of the APS was presented at SATIF3. This paper presents the results of further measurements at the two insertion device (ID) beamlines with higher statistics in the data collection. The beam current and the vacuum normalized bremsstrahlung power is fairly constant in a beamline for a given storage ring fill pattern, but may vary from beamline to beamline. The average bremsstrahlung power is measured as 118 {+-} 9 GeV/s/nT/mA at beamline 11 ID and as 36 {+-} 2 GeV/s/nT/mA at beamline 6 ID. These results, along with the results from the four previous independent bremsstrahlung measurements, enabled us to conclude upon the various reasons causing this variation.

  14. Welding III.

    ERIC Educational Resources Information Center

    Allegheny County Community Coll., Pittsburgh, PA.

    Instructional objectives and performance requirements are outlined in this course guide for Welding III, an advanced course in arc welding offered at the Community College of Allegheny County to provide students with the proficiency necessary for industrial certification. The course objectives, which are outlined first, specify that students will…

  15. LANDVIEW III

    EPA Science Inventory

    LandView III is a desktop mapping system that includes database extracts from the Environmental Protection Agency, the Bureau of the Census, The U.S. Geological Survey, the Nuclear Regulatory Commission, the Department of Transportation, and the Federal Emergency Management Agenc...

  16. The BALDER Beamline at the MAX IV Laboratory

    NASA Astrophysics Data System (ADS)

    Klementiev, K.; Norén, K.; Carlson, S.; Sigfridsson Clauss, K. G. V.; Persson, I.

    2016-05-01

    X-ray absorption spectroscopy (XAS) includes well-established methods to study the local structure around the absorbing element - extended X-ray absorption fine structure (EXAFS), and the effective oxidation number or to quantitatively determine the speciation of an element in a complex matrix - X-ray absorption near-edge structure (XANES). The increased brilliance and intensities available at the new generation of synchrotron light sources makes it possible to study, in-situ and in-operando, much more dilute systems with relevance for natural systems, as well as the micro-scale variability and dynamics of chemical reactions on the millisecond time-scale. The design of the BALDER beamline at the MAX IV Laboratory 3 GeV ring has focused on a high flux of photons in a wide energy range, 2.4-40 keV, where the K-edge is covered for the elements S to La, and the L 3-edge for all elements heavier than Sb. The overall design of the beamline will allow large flexibility in energy range, beam size and data collection time. The other focus of the beamline design is the possibility to perform multi-technique analyses on samples. Development of sample environment requires focus on implementation of auxiliary methods in such a way that techniques like Fourier transform infrared (FTIR) spectroscopy, UV-Raman spectroscopy, X-ray diffraction and/or mass spectrometry can be performed simultaneously as the XAS study. It will be a flexible system where different instruments can be plugged in and out depending on the needs for the particular investigation. Many research areas will benefit from the properties of the wiggler based light source and the capabilities to perform in-situ and in-operando measurements, for example environmental and geochemical sciences, nuclear chemistry, catalysis, materials sciences, and cultural heritage.

  17. ELIMED, MEDical and multidisciplinary applications at ELI-Beamlines

    NASA Astrophysics Data System (ADS)

    Schillaci, F.; Anzalone, A.; Cirrone, G. A. P.; Carpinelli, M.; Cuttone, G.; Cutroneo, M.; De Martinis, C.; Giove, D.; Korn, G.; Maggiore, M.; Manti, L.; Margarone, D.; Musumarra, A.; Perozziello, F. M.; Petrovic, I.; Pisciotta, P.; Renis, M.; Ristic-Fira, A.; Romano, F.; Romano, F. P.; Schettino, G.; Scuderi, V.; Torrisi, L.; Tramontana, A.; Tudisco, S.

    2014-04-01

    ELI-Beamlines is one of the pillars of the pan-European project ELI (Extreme Light Infrastructure). It will be an ultra high-intensity, high repetition-rate, femtosecond laser facility whose main goal is generation and applications of high-brightness X-ray sources and accelerated charged particles in different fields. Particular care will be devoted to the potential applicability of laser-driven ion beams for medical treatments of tumors. Indeed, such kind of beams show very interesting peculiarities and, moreover, laser-driven based accelerators can really represent a competitive alternative to conventional machines since they are expected to be more compact in size and less expensive. The ELIMED project was launched thanks to a collaboration established between FZU-ASCR (ELI-Beamlines) and INFN-LNS researchers. Several European institutes have already shown a great interest in the project aiming to explore the possibility to use laser-driven ion (mostly proton) beams for several applications with a particular regard for medical ones. To reach the project goal several tasks need to be fulfilled, starting from the optimization of laser-target interaction to dosimetric studies at the irradiation point at the end of a proper designed transport beam-line. Researchers from LNS have already developed and successfully tested a high-dispersive power Thomson Parabola Spectrometer, which is the first prototype of a more performing device to be used within the ELIMED project. Also a Magnetic Selection System able to produce a small pencil beam out of a wide energy distribution of ions produced in laser-target interaction has been realized and some preliminary work for its testing and characterization is in progress. In this contribution the status of the project will be reported together with a short description of the of the features of device recently developed.

  18. Time-resolved neutron imaging at ANTARES cold neutron beamline

    NASA Astrophysics Data System (ADS)

    Tremsin, A. S.; Dangendorf, V.; Tittelmeier, K.; Schillinger, B.; Schulz, M.; Lerche, M.; Feller, W. B.

    2015-07-01

    In non-destructive evaluation with X-rays light elements embedded in dense, heavy (or high-Z) matrices show little contrast and their structural details can hardly be revealed. Neutron radiography, on the other hand, provides a solution for those cases, in particular for hydrogenous materials, owing to the large neutron scattering cross section of hydrogen and uncorrelated dependency of neutron cross section on the atomic number. The majority of neutron imaging experiments at the present time is conducted with static objects mainly due to the limited flux intensity of neutron beamline facilities and sometimes due to the limitations of the detectors. However, some applications require the studies of dynamic phenomena and can now be conducted at several high intensity beamlines such as the recently rebuilt ANTARES beam line at the FRM-II reactor. In this paper we demonstrate the capabilities of time resolved imaging for repetitive processes, where different phases of the process can be imaged simultaneously and integrated over multiple cycles. A fast MCP/Timepix neutron counting detector was used to image the water distribution within a model steam engine operating at 10 Hz frequency. Within <10 minutes integration the amount of water was measured as a function of cycle time with a sub-mm spatial resolution, thereby demonstrating the capabilities of time-resolved neutron radiography for the future applications. The neutron spectrum of the ANTARES beamline as well as transmission spectra of a Fe sample were also measured with the Time Of Flight (TOF) technique in combination with a high resolution beam chopper. The energy resolution of our setup was found to be ~ 0.8% at 5 meV and ~ 1.7% at 25 meV. The background level (most likely gammas and epithermal/fast neutrons) of the ANTARES beamline was also measured in our experiments and found to be on the scale of 3% when no filters are installed in the beam. Online supplementary data available from stacks.iop.org/jinst/10

  19. Implementation of the beamline controls at the Florence accelerator laboratory

    NASA Astrophysics Data System (ADS)

    Carraresi, L.; Mirto, F. A.

    2008-05-01

    The new Tandetron accelerator in Florence, with many different beamlines, has required a new organization of all the control signals of the used equipment (slow control). We present our solution, which allows us the control of all the employed instruments simultaneously from a number of different workplaces. All of our equipment has been designed to be Ethernet based and this is the key to accomplish two very important requirements: simultaneous remote control from many computers and electrical isolation to achieve a lower noise level. The control of the instruments requires only one Ethernet network and no particular interfaces or drivers on the computers.

  20. Advanced Beamline Design for Fermilab's Advanced Superconducting Test Accelerator

    SciTech Connect

    Prokop, Christopher

    2014-01-01

    The Advanced Superconducting Test Accelerator (ASTA) at Fermilab is a new electron accelerator currently in the commissioning stage. In addition to testing superconducting accelerating cavities for future accelerators, it is foreseen to support a variety of Advanced Accelerator R&D (AARD) experiments. Producing the required electron bunches with the expected flexibility is challenging. The goal of this dissertation is to explore via numerical simulations new accelerator beamlines that can enable the advanced manipulation of electron bunches. The work especially includes the design of a low-energy bunch compressor and a study of transverse-to-longitudinal phase space exchangers.

  1. The performance of a cryogenically cooled monochromator for an in-vacuum undulator beamline.

    PubMed

    Zhang, Lin; Lee, Wah Keat; Wulff, Michael; Eybert, Laurent

    2003-07-01

    The channel-cut silicon monochromator on beamline ID09 at the European Synchrotron Radiation Facility is indirectly cooled from the sides by liquid nitrogen. The thermal slope error of the diffracting surface is calculated by finite-element analysis and the results are compared with experiments. The slope error is studied as a function of cooling coefficients, beam size, position of the footprint and power distribution. It is found that the slope error versus power curve can be divided into three regions: (i). The linear region: the thermal slope error is linearly proportional to the power. (ii). The transition region: the temperature of the Si crystal is close to 125 K; the thermal slope error is below the straight line extrapolated from the linear curve described above. (iii). The non-linear region: the temperature of the Si crystal is higher than 125 K and the thermal slope error increases much faster than the power. Heat-load tests were also performed and the measured rocking-curve widths are compared with those calculated by finite-element modeling. When the broadening from the intrinsic rocking-curve width and mounting strain are included, the calculated rocking-curve width versus heat load is in excellent agreement with experiment. PMID:12824931

  2. LISA: the Italian CRG beamline for x-ray Absorption Spectroscopy at ESRF

    NASA Astrophysics Data System (ADS)

    d'Acapito, F.; Trapananti, A.; Puri, A.

    2016-05-01

    LISA is the acronym of Linea Italiana per la Spettroscopia di Assorbimento di raggi X (Italian beamline for X-ray Absorption Spectroscopy) and is the upgrade of the former GILDA beamline installed on the BM08 bending magnet port of European Synchrotron Radiation Facility (ESRF). Within this contribution a full description of the project is provided.

  3. Micro-Soft X-Ray Spectroscopy with the LUCIA Beamline

    SciTech Connect

    Lagarde, P.; Flank, A.-M.; Vantelon, D.; Janousch, M.

    2007-02-02

    With the development of new synchrotron radiation machines, which have seen, in the last ten years, the emittance of the beam decreased by several orders of magnitude, new beamlines have been developed which make full use of these improvements. We describe here the LUCIA beamline, which has been implemented at the Swiss Light Source in a collaboration between PSI, SOLEIL and the CNRS.

  4. FINAL REPORT. CONSTRUCTION OF BENDING MAGNET BEAMLINE AT THE APS FOR ENVIRONMENTAL STUDIES

    EPA Science Inventory

    Design and construction of a bending magnet beamline at the Advanced Photon Source (APS) by the Pacific Northwest Consortium-Collaborative Access Team (PNC-CAT). The beamline will be optimized for x-ray absorption spectroscopy (XAS) studies with a major focus on environmental iss...

  5. The Protein Micro-Crystallography Beamlines for Targeted Protein Research Program

    NASA Astrophysics Data System (ADS)

    Hirata, Kunio; Yamamoto, Masaki; Matsugaki, Naohiro; Wakatsuki, Soichi

    In order to collect proper diffraction data from outstanding micro-crystals, a brand-new data collection system should be designed to provide high signal-to noise ratio in diffraction images. SPring-8 and KEK-PF are currently developing two micro-beam beamlines for Targeted Proteins Research Program by MEXT of Japan. The program aims to reveal the structure and function of proteins that are difficult to solve but have great importance in both academic research and industrial application. At SPring-8, a new 1-micron beam beamline for protein micro-crystallography, RIKEN Targeted Proteins Beamline (BL32XU), is developed. At KEK-PF a new low energy micro-beam beamline, BL-1A, is dedicated for SAD micro-crystallography. The two beamlines will start operation in the end of 2010. The present status of the research and development for protein micro-crystallography will be presented.

  6. Commissioning and first results of scanning type EXAFS beamline (BL-09) at INDUS-2 synchrotron source

    SciTech Connect

    Poswal, A. K. Agrawal, A. Yadav, A. K. Nayak, C. Basu, S. Bhattachryya, D.; Jha, S. N.; Sahoo, N. K.; Kane, S. R.; Garg, C. K.

    2014-04-24

    An Energy Scanning X-ray Absorption Fine Structure spectroscopy beamline has recently been installed and commissioned at BL-09 bending magnet port of INDUS-2 synchrotron source, Indore. The beamline uses an UHV compatible fixed exit double crystal monochromator (DCM) with two Si (111) crystals. Two grazing incidence cylindrical mirrors are also used in this beamline; the pre-mirror is used as a collimating mirror while the post mirror is used for vertical focusing and higher harmonic rejection. In this beamline it is possible to carry out EXAFS measurements both in transmission and fluorescence mode on various types of samples, using Ionization chamber detectors and solid state drift detector respectively. In this paper, results from first experiments of the Energy Scanning EXAFS beamline are presented.

  7. Performance of beamline 9.3.1 at the ALS: Flux and resolution measurements

    SciTech Connect

    Uehara, Y.; Fischer, G.; Kring, J.; Perera, R.C.C.

    1997-04-01

    Beamline 9.3.1 at the ALS is a windowless beamline, covering the 1-6 keV photon-energy range. This beamline is the first monochromatic hard x-ray beamline in the ALS, and designed to achieve the goals of high energy resolution, and preservation of the high brightness from the ALS. It consists of a new {open_quotes}Cowan type{close_quotes} double-crystal monochromator and two toroidal mirrors which are positioned before and after the monochromator. The construction of the beamline was completed in December of 1995, with imperfect mirrors. In this report, the authors describe the experimental results of absolute flux measurements and x-ray absorption measurements of gases and solid samples using the present set of mirrors.

  8. The macromolecular crystallography beamline I911-3 at the MAX IV laboratory

    PubMed Central

    Ursby, Thomas; Unge, Johan; Appio, Roberto; Logan, Derek T.; Fredslund, Folmer; Svensson, Christer; Larsson, Krister; Labrador, Ana; Thunnissen, Marjolein M. G. M.

    2013-01-01

    The macromolecular crystallography beamline I911-3, part of the Cassiopeia/I911 suite of beamlines, is based on a superconducting wiggler at the MAX II ring of the MAX IV Laboratory in Lund, Sweden. The beamline is energy-tunable within a range between 6 and 18 keV. I911-3 opened for users in 2005. In 2010–2011 the experimental station was completely rebuilt and refurbished such that it has become a state-of-the-art experimental station with better possibilities for rapid throughput, crystal screening and work with smaller samples. This paper describes the complete I911-3 beamline and how it is embedded in the Cassiopeia suite of beamlines. PMID:23765310

  9. Present Status of the NIMS Contract Beamline BL15XU at SPring-8

    SciTech Connect

    Ueda, Shigenori; Tanaka, Masahiko; Yoshikawa, Hideki; Yamashita, Yoshiyuki; Matsushita, Yoshitaka; Kobayashi, Keisuke; Katsuya, Yoshio; Ishimaru, Satoshi

    2010-06-23

    The revolver undulator beamline BL15XU at SPring-8, which is the contract beamline of National Institute for Materials Science (NIMS), was established for materials science using soft-and-hard X-ray photoelectron spectroscopy (XPS) and high-resolution powder X-ray diffraction (XRD). We have performed beamline reconstruction for further developments of the experiments in the research field of materials science. The flat double-crystal monochromator (DCM) with liquid nitrogen cooling, X-ray total reflection double-mirror system with (+,-) geometry, and high-energy-resolution channel-cut monochromator have been installed into the beamline. The refined beamline provides monochromatic X-rays from 2 to 36 keV. The improvement of the photon flux density at the XRD and XPS experimental stations was confirmed. The photon flux was estimated to be several 10{sup 12} photons/sec with {Delta}E/E of {approx}10{sup -4}.

  10. Dedicated Beamline Facilities for Catalytic Research. Synchrotron Catalysis Consortium (SCC)

    SciTech Connect

    Chen, Jingguang; Frenkel, Anatoly; Rodriguez, Jose; Adzic, Radoslav; Bare, Simon R.; Hulbert, Steve L.; Karim, Ayman; Mullins, David R.; Overbury, Steve

    2015-03-04

    Synchrotron spectroscopies offer unique advantages over conventional techniques, including higher detection sensitivity and molecular specificity, faster detection rate, and more in-depth information regarding the structural, electronic and catalytic properties under in-situ reaction conditions. Despite these advantages, synchrotron techniques are often underutilized or unexplored by the catalysis community due to various perceived and real barriers, which will be addressed in the current proposal. Since its establishment in 2005, the Synchrotron Catalysis Consortium (SCC) has coordinated significant efforts to promote the utilization of cutting-edge catalytic research under in-situ conditions. The purpose of the current renewal proposal is aimed to provide assistance, and to develop new sciences/techniques, for the catalysis community through the following concerted efforts: Coordinating the implementation of a suite of beamlines for catalysis studies at the new NSLS-II synchrotron source; Providing assistance and coordination for catalysis users at an SSRL catalysis beamline during the initial period of NSLS to NSLS II transition; Designing in-situ reactors for a variety of catalytic and electrocatalytic studies; Assisting experimental set-up and data analysis by a dedicated research scientist; Offering training courses and help sessions by the PIs and co-PIs.

  11. High pressure experiments at the XAFS Beamline, INDUS-2

    NASA Astrophysics Data System (ADS)

    Ramanan, Nitya; Lahiri, Debdutta; Garg, Nandini; Bhattacharyya, D.; Jha, S. N.; Sahoo, N. K.; Sharma, Surinder M.

    2012-07-01

    The dispersive XAFS beamline BL-08 at the INDUS-2 synchrotron radiation source, RRCAT, Indore uses a bent Si (111) crystal as dispersive-cum-focusing element and a position sensitive CCD detector to enable instantaneous measurement of the whole XAFS spectrum around the absorption edge of interest. This beamline is ideal for characterisation of materials under high pressure using Diamond Anvil Cell with ~50 μm spot size. For this setup, the theoretically determined spot size (Horizontal × Vertical) varies between 17 × 137 μm and 37 × 142 μm for the x-ray energy range 5 keV-20 keV. To reduce the vertical spot size to <50 μm, we have designed an additional focusing mirror between the polychromator and sample position. The mirror, procured from SESO (France), will be installed shortly. Meanwhile, we have developed a dummy mirror bender setup at CDM (B ARC) and have carried out feasibility tests to confirm reduction in spot size using the same. We have also conducted preliminary XAFS experiments (at BL-08) on SrRuO3 at ~16 keV, under ambient conditions and inside diamond anvil cell, in order to assess the signal intensity and quality. We have obtained reasonably good signal.

  12. Design, Installation, and Initial Commissioning of the MTA Beamline

    SciTech Connect

    Moore, Craig; Anderson, John; Garcia, Fernanda; Gerardi, Michael; Johnstone, Carol; Kobilarcik, Thomas; Kucera, Michael; Kufer, Mathew; Newhart, Duane; Rakhno, Igor; Vogel, Gregory; /Fermilab

    2010-05-01

    A new experimental area designed to develop, test and verify muon ionization cooling apparatus using the 400-MeV Fermilab Linac proton beam has been fully installed and is presently being commissioned. Initially, this area was used for cryogenic tests of liquid-hydrogen absorbers for the MUCOOL R&D program and, now, for high-power beam tests of absorbers, high-gradient rf cavities in the presence of magnetic fields (including gas-filled cavities), and other prototype muon-cooling apparatus. The experimental scenarios being developed for muon facilities involve collection, capture, and cooling of large-emittance, high-intensity muon beams--{approx}10{sup 13} muons, so that conclusive tests of the apparatus require full Linac beam, which is 1.6 x 10{sup 13} p/pulse. To support the muon cooling facility, this new primary beamline extracts and transports beam directly from the Linac to the test facility. The design concept for the MuCool facility is taken from an earlier proposal [1], but modifications were necessary to accommodate high-intensity beam, cryogenics, and the increased scale of the cooling experiments. Further, the line incorporates a specialized section and utilizes a different mode of operation to provide precision measurements of Linac beam parameters. This paper reports on the technical details of the MuCool beamline for both modes.

  13. Microfocusing at the PG1 beamline at FLASH

    SciTech Connect

    Dziarzhytski, Siarhei; Gerasimova, Natalia; Goderich, Rene; Mey, Tobias; Reininger, Ruben; Rübhausen, Michael; Siewert, Frank; Weigelt, Holger; Brenner, Günter

    2016-01-01

    The Kirkpatrick–Baez (KB) refocusing mirror system installed at the PG1 branch of the plane-grating monochromator beamline at the soft X-ray/XUV free-electron laser in Hamburg (FLASH) is designed to provide tight aberration-free focusing down to 4 µm x 6 µm full width at half-maximum (FWHM) on the sample. Such a focal spot size is mandatory to achieve ultimate resolution and to guarantee best performance of the vacuum-ultraviolet (VUV) off-axis parabolic double-monochromator Raman spectrometer permanently installed at the PG1 beamline as an experimental end-station. The vertical beam size on the sample of the Raman spectrometer, which operates without entrance slit, defines and limits the energy resolution of the instrument which has an unprecedented design value of 2 meV for photon energies below 70 eV and about 15 meV for higher energies up to 200 eV. In order to reach the designed focal spot size of 4 µm FWHM (vertically) and to hold the highest spectrometer resolution, special fully motorized in-vacuum manipulators for the KB mirror holders have been developed and the optics have been aligned employing wavefront-sensing techniques as well as ablative imprints analysis. Aberrations like astigmatism were minimized. In this article the design and layout of the KB mirror manipulators, the alignment procedure as well as microfocus optimization results are presented.

  14. The BESSY wiggler/undulator-TGM-5 beamline

    SciTech Connect

    Peatman, W.; Carbone, C.; Gudat, W.; Heinen, W.; Kuske, P.; Pfluger, J.; Schafers, F.; Schroeter, T.

    1989-07-01

    In actual performance, the 35 pole wiggler/undulator (W/U) at BESSY has been shown to deliver 50 to 250 times more flux than a TGM with 10 mrad of dipole radiation under otherwise comparable conditions. The beamline, laid out for photon energies from 15 to 400 eV, has been calibrated and the resolution measured at several energies. Interactions of the W/U with the storage ring have been studied and, in part, corrected for: the working point does not change in either direction (/lt/10%) as the gap is varied and the electron beam position in the ring remains constant to within 10 /mu/m and the angle of emission of the SR from the ring to within 5 /mu/rad for /ital K//le/2.7. The reduction of the lifetime of the electron beam in the ring and the change in the vertical size of the beam as a function of the gap are typical of the problems associated with the interaction of such a device on a high brightness ring. The beamline has been in normal user operation for over a year.

  15. NSLS transvenous coronary angiography beamline upgrade and advanced technology initiatives

    SciTech Connect

    Gmuer, N.F.; Chapman, D.; Thomlinson, W. ); Thompson, A.C. ); Lavender, W.M. ); Scalia, K.; Malloy, N. ); Mangano, J.; Jacob, J. )

    1995-02-01

    Since October 1990, the coronary anatomies of a total of 16 patients (male and female) have been imaged at the National Synchrotron Light Source (NSLS) as part of the Dual Energy Digital Subtraction Transvenous Coronary Angiography research program. This program takes place in the Synchrotron Medical Research Facility (SMERF) on the X17B2 wiggler beamline. Encouraged by the success of the initial patient images, the NSLS has recently embarked on an ambitious upgrade effort. This effort covers all aspects of the X17B2 beamline and includes improved radiation shielding, a Laue monochromator assembly, a computer-controlled five motion patient scanning chair assembly, a fast low-noise image acquisition system, and a modularized patient safety system. These improvements will allow major advances in imaging patients based on ECG signal gating and multiple view imaging. Two advanced technology initiatives are underway with industrial collaborators. One will develop real-time image acquisition and display of the subtracted digital images. The second will develop a compact x-ray source of medical imaging. The source will be a linear electron accelerator creating characteristic radiation line emissions.

  16. NSLS transvenous coronary angiography beamline upgrade and advanced technology initiatives

    SciTech Connect

    Gmuer, N.F.; Chapman, D.; Thomlinson, W.; Thompson, A.C.; Lavender, W.M.; Scalia, K.; Malloy, N.; Mangano, J.; Jacob, J.

    1994-11-01

    Since October 1990, the coronary anatomies of a total of 16 patients (male and female) have been imaged at the National Synchrotron Light Source (NSLS) as part of the Dual Energy Digital Subtraction Transvenous Coronary Angiography research program. This program takes place in the Synchrotron Medical Research Facility (SMERF) on the X17B2 wiggler beamline. Encouraged by the success of the initial patient images, the NSLS has recently embarked on an ambitious upgrade effort. This effort covers all aspects of the X17B2 beamline and includes improved radiation shielding, a Laue monochromator assembly, a computer-controlled 5 motion patient scanning chair assembly, a fast low-noise image acquisition system, and a modularized patient safety system. These improvements will allow major advances in imaging patients based on ECG signal gating and multiple view imaging. Two advanced technology initiatives are underway with industrial collaborators. One will develop real-time image acquisition and display of the subtracted digital images. The second will develop a compact x-ray source for medical imaging. The source will be a linear electron accelerator creating characteristic radiation line emissions.

  17. The Diamond Beamline I13L for Imaging and Coherence

    SciTech Connect

    Rau, C.; Wagner, U.; Peach, A.; Singh, B.; Wilkin, G.; Jones, C.; Robinson, I. K.

    2010-06-23

    I13L is the first long beamline at Diamond dedicated to imaging and coherence. Two independent branches will operate in the energy range of 6-30 keV with spatial resolution on the micro- to nano-lengthscale. The Imaging branch is dedicated to imaging and tomography with In-line phase contrast and full-field microscopy on the micron to nano-length scale. Ultimate resolution will be achieved on the Coherence branch at I13L with imaging techniques in the reciprocal space. The experimental stations will be located about 250 m from the source, taking advantage of the coherence properties of the source. The beamline has some outstanding features such as the mini-beta layout of the storage ring's straight section. The optical layout is optimized for beam stability and high optical quality to preserve the coherent radiation. In the experimental stations several methods will be available, starting for the first user with in-line phase contrast imaging on the imaging branch and Coherent X-ray Diffraction (CXRD) on the coherence branch.

  18. Microfocusing at the PG1 beamline at FLASH

    SciTech Connect

    Dziarzhytski, Siarhei; Gerasimova, Natalia; Goderich, Rene; Mey, Tobias; Reininger, Ruben; Rubhausen, Michael; Siewert, Frank; Weigelt, Holger; Brenner, Gunter

    2016-01-01

    The Kirkpatrick–Baez (KB) refocusing mirror system installed at the PG1 branch of the plane-grating monochromator beamline at the soft X-ray/XUV free-electron laser in Hamburg (FLASH) is designed to provide tight aberration-free focusing down to 4 µm × 6 µm full width at half-maximum (FWHM) on the sample. Such a focal spot size is mandatory to achieve ultimate resolution and to guarantee best performance of the vacuum-ultraviolet (VUV) off-axis parabolic double-monochromator Raman spectrometer permanently installed at the PG1 beamline as an experimental end-station. The vertical beam size on the sample of the Raman spectrometer, which operates without entrance slit, defines and limits the energy resolution of the instrument which has an unprecedented design value of 2 meV for photon energies below 70 eV and about 15 meV for higher energies up to 200 eV. In order to reach the designed focal spot size of 4 µm FWHM (vertically) and to hold the highest spectrometer resolution, special fully motorized in-vacuum manipulators for the KB mirror holders have been developed and the optics have been aligned employing wavefront-sensing techniques as well as ablative imprints analysis. Lastly, aberrations like astigmatism were minimized. In this article the design and layout of the KB mirror manipulators, the alignment procedure as well as microfocus optimization results are presented.

  19. Parametric Optimization of Undulators for NSLS-II Project Beamlines

    NASA Astrophysics Data System (ADS)

    Chubar, O.; Bengtsson, J.; Berman, L.; Broadbent, A.; Cai, Y. Q.; Hulbert, S.; Shen, Q.; Tanabe, T.

    2010-06-01

    General optimization procedure, computation methods used, and the obtained optimal parameters of undulators for the NSLS-II project beamlines are reported. The optimization starts with high-accuracy calculation of undulator magnetic fields, using Radia magnetostatics code, for a large set of periods and vertical gaps of a given undulator type, given magnetic materials and a scalable magnet geometry. From the resulting magnetic fields, a sub-set of undulator periods and the corresponding vertical gaps, providing the required low-energy cut-off values of spectral harmonics for each particular beamline, is determined. In parallel, from the same Radia undulator models, angular magnetic kick maps are calculated, and the insertion device effect on electron beam is simulated using Tracy-2 tracking code based on symplectic integrator. After these simulations, magnet parameters are fine-tuned and the maximal acceptable undulator lengths are determined for different straight sections, as functions of minimal gap and with due regard for the electron beam vertical "stay clear" constraint in the case of in-vacuum undulators. Finally, the optimal undulator period and length are determined as the values providing maximal spectral flux among the pre-selected undulator cases, already satisfying the requirements concerning the harmonic cut-off values and the effect on electron beam.

  20. Microfocusing at the PG1 beamline at FLASH

    DOE PAGESBeta

    Dziarzhytski, Siarhei; Gerasimova, Natalia; Goderich, Rene; Mey, Tobias; Reininger, Ruben; Rubhausen, Michael; Siewert, Frank; Weigelt, Holger; Brenner, Gunter

    2016-01-01

    The Kirkpatrick–Baez (KB) refocusing mirror system installed at the PG1 branch of the plane-grating monochromator beamline at the soft X-ray/XUV free-electron laser in Hamburg (FLASH) is designed to provide tight aberration-free focusing down to 4 µm × 6 µm full width at half-maximum (FWHM) on the sample. Such a focal spot size is mandatory to achieve ultimate resolution and to guarantee best performance of the vacuum-ultraviolet (VUV) off-axis parabolic double-monochromator Raman spectrometer permanently installed at the PG1 beamline as an experimental end-station. The vertical beam size on the sample of the Raman spectrometer, which operates without entrance slit, defines andmore » limits the energy resolution of the instrument which has an unprecedented design value of 2 meV for photon energies below 70 eV and about 15 meV for higher energies up to 200 eV. In order to reach the designed focal spot size of 4 µm FWHM (vertically) and to hold the highest spectrometer resolution, special fully motorized in-vacuum manipulators for the KB mirror holders have been developed and the optics have been aligned employing wavefront-sensing techniques as well as ablative imprints analysis. Lastly, aberrations like astigmatism were minimized. In this article the design and layout of the KB mirror manipulators, the alignment procedure as well as microfocus optimization results are presented.« less

  1. Shielding Design Aspects of SR Beamlines for 3-GeV And 8-GeV Class Synchrotron Radiation Facilities

    SciTech Connect

    Asano, Yoshihiro; Liu, James C.; Rokni, Sayed; /SLAC

    2007-09-24

    Differences in synchrotron radiation beamline shielding design between the facilities of 3 GeV class and 8 GeV class are discussed with regard to SLAC SSRL and SPring-8 beamlines. Requirements of beamline shielding as well as the accelerator shielding depend on the stored electron energy, and here some factors in beamline shielding depending on the stored energy in particular, are clarified, namely the effect of build up, the effect of double scattering of photons at branch beamlines, and the spread of gas bremsstrahlung.

  2. The ELIMED transport and dosimetry beamline for laser-driven ion beams

    NASA Astrophysics Data System (ADS)

    Romano, F.; Schillaci, F.; Cirrone, G. A. P.; Cuttone, G.; Scuderi, V.; Allegra, L.; Amato, A.; Amico, A.; Candiano, G.; De Luca, G.; Gallo, G.; Giordanengo, S.; Guarachi, L. Fanola; Korn, G.; Larosa, G.; Leanza, R.; Manna, R.; Marchese, V.; Marchetto, F.; Margarone, D.; Milluzzo, G.; Petringa, G.; Pipek, J.; Pulvirenti, S.; Rizzo, D.; Sacchi, R.; Salamone, S.; Sedita, M.; Vignati, A.

    2016-09-01

    A growing interest of the scientific community towards multidisciplinary applications of laser-driven beams has led to the development of several projects aiming to demonstrate the possible use of these beams for therapeutic purposes. Nevertheless, laser-accelerated particles differ from the conventional beams typically used for multiscipilinary and medical applications, due to the wide energy spread, the angular divergence and the extremely intense pulses. The peculiarities of optically accelerated beams led to develop new strategies and advanced techniques for transport, diagnostics and dosimetry of the accelerated particles. In this framework, the realization of the ELIMED (ELI-Beamlines MEDical and multidisciplinary applications) beamline, developed by INFN-LNS (Catania, Italy) and that will be installed in 2017 as a part of the ELIMAIA beamline at the ELI-Beamlines (Extreme Light Infrastructure Beamlines) facility in Prague, has the aim to investigate the feasibility of using laser-driven ion beams for multidisciplinary applications. In this contribution, an overview of the beamline along with a detailed description of the main transport elements as well as the detectors composing the final section of the beamline will be presented.

  3. Undulator beamline of the Brockhouse sector at the Canadian Light Source

    SciTech Connect

    Diaz, B. E-mail: skycia@uoguelph.ca; Gomez, A.; Duffy, A.; Hallin, E.; Meyer, B.; Kycia, S. E-mail: skycia@uoguelph.ca

    2014-08-15

    The Brockhouse project at the Canadian Light Source plans the construction of three beamlines, two wiggler beamlines, and one undulator beamline, that will be dedicated to x-ray diffraction and scattering. In this work, we will describe the undulator beamline main components and performance parameters, obtained from ray tracing using XOP-SHADOW codes. The undulator beamline will operate from 4.95 to 21 keV, using a 20 mm period hybrid undulator placed upstream of the wiggler in the same straight section. The beamline optics design was developed in cooperation with the Brazilian Synchrotron - LNLS. The beamline will have a double crystal monochromator with the options of Si(111) or Si(311) crystal pairs followed by two mirrors in the KB configuration to focus the beam at the sample position. The high brilliance of the undulator source will produce a very high flux of ∼10{sup 13} photons/s and high energy resolution into a small focus of 170 μm horizontal and 20-60 μm vertical, depending on the optical configuration and energy chosen. Two multi-axis goniometer experimental stations with area detectors and analyzers are foreseen to enable diffraction, resonant and inelastic scattering experiments, and SAXS/WAXS experiments with high resolution and time resolving capabilities.

  4. High heat flux mirror design for an undulator beamline

    NASA Astrophysics Data System (ADS)

    Tonnessen, Thomas W.; Fisher, Steven E.; Anthony, Frank M.; Lunt, David L.; Khounsary, Ali M.; Randall, Kevin J.; Gluskin, Efim S.; Yun, Wenbing

    1993-11-01

    A-high-heat-load, horizontally deflecting/focusing mirror is designed for installation on an APS undulator beamline. The main design objective has been to keep the total tangential RMS slope error, including the thermally induced component, to less than 2 (mu) rad with an absorbed beam power on the mirror of 2 kW and a peak flux of 3.2 W/mm2. Extensive examination of various design parameters and detailed thermal/structural analyses has resulted in a mirror design that meets the tight slope-error requirement. Design features include a silicon substrate, a tailored pin-post cooling scheme, a moderate coolant flow rate, primary and secondary cooling areas, a multi-strip coating on the reflecting surface, and inlet/outlet cooling manifolds through an attached Ni-Fe mounting structure.

  5. Optimized baffle and aperture placement in neutral beamlines

    NASA Astrophysics Data System (ADS)

    Stone, R.; Duffy, T.; Vetrovec, J.

    1983-11-01

    Most neutral beamlines contain an iron-core ion-bending magnet that requires shielding between the end of the neutralizer and this magnet. This shielding allows the gas pressure to drop prior to the beam entering the magnet and therefore reduces beam losses in this drift region. The beam losses are reduced even further by eliminating the iron-core magnet and the magnetic shielding altogether. The required bending field is supplied by current coils without the iron poles. In addition, placement of the baffles and apertures affects the cold gas entering the plasma region and the losses in the neutral beam due to re-ionization. The placement of the baffles which, determine the amount of pumping in each chamber, and the apertures, which determine the beam loss were varied. A baffler/aperture configuration is for either minimum cold gas into the plasma region or minimum beam losses, but not both.

  6. Development of a Niobium Bellow for Beamline Connections

    SciTech Connect

    Larry Turlington; John Brawley; Robert Manus; Stephen Manning; Samuel Morgan; Gary Slack; Peter Kneisel

    2003-09-01

    Superconducting cavities in an accelerator assembly are usually connected at the beampipes by stainless steel bellows. They operate at an intermediate temperature, compensating for alignment tolerances on the cavity beamlines and for thermal contraction during cooldown to cryogenic temperatures. This transition from one cavity to the next in a cavity string is typically of the order of 3/2 wavelength along with approximately half a wavelength taken up by the bellows. If one could incorporate a niobium bellows in the beam pipe, this distance could be reduced by half a wave length. In the case of a big accelerator such as TESLA the overall cavity length for the accelerator could be reduced by roughly 10% or 2000 m. In terms of cost savings this would amount to several million dollars. Based on this estimate we have begun to develop a niobium bellows to be used on a 2.75 inch diameter beamline. It is made from 0.3 mm thick niobium sheet, rolled into a tube and secured by a longitudinal full penetration electron beam weld; the weld is made with a high speed a narrow, focused beam reducing the heat affected zone, thus limiting the grain growth, which could affect the formability. Subsequently, two convolutions have been pressed into this tube in a 2-stage process, using an external die and a polyurethane internal expander. Niobium cuffs and flanges were electron beam welded to the formed bellows, which facilitated leak testing and allowed some measurements of compression/expansion and bending. In this contribution the fabrication process and the subsequent mechanical and vacuum tests with the bellows will be described.

  7. Microfocusing at the PG1 beamline at FLASH.

    PubMed

    Dziarzhytski, Siarhei; Gerasimova, Natalia; Goderich, Rene; Mey, Tobias; Reininger, Ruben; Rübhausen, Michael; Siewert, Frank; Weigelt, Holger; Brenner, Günter

    2016-01-01

    The Kirkpatrick-Baez (KB) refocusing mirror system installed at the PG1 branch of the plane-grating monochromator beamline at the soft X-ray/XUV free-electron laser in Hamburg (FLASH) is designed to provide tight aberration-free focusing down to 4 µm × 6 µm full width at half-maximum (FWHM) on the sample. Such a focal spot size is mandatory to achieve ultimate resolution and to guarantee best performance of the vacuum-ultraviolet (VUV) off-axis parabolic double-monochromator Raman spectrometer permanently installed at the PG1 beamline as an experimental end-station. The vertical beam size on the sample of the Raman spectrometer, which operates without entrance slit, defines and limits the energy resolution of the instrument which has an unprecedented design value of 2 meV for photon energies below 70 eV and about 15 meV for higher energies up to 200 eV. In order to reach the designed focal spot size of 4 µm FWHM (vertically) and to hold the highest spectrometer resolution, special fully motorized in-vacuum manipulators for the KB mirror holders have been developed and the optics have been aligned employing wavefront-sensing techniques as well as ablative imprints analysis. Aberrations like astigmatism were minimized. In this article the design and layout of the KB mirror manipulators, the alignment procedure as well as microfocus optimization results are presented. PMID:26698054

  8. Microfocusing at the PG1 beamline at FLASH

    PubMed Central

    Dziarzhytski, Siarhei; Gerasimova, Natalia; Goderich, Rene; Mey, Tobias; Reininger, Ruben; Rübhausen, Michael; Siewert, Frank; Weigelt, Holger; Brenner, Günter

    2016-01-01

    The Kirkpatrick–Baez (KB) refocusing mirror system installed at the PG1 branch of the plane-grating monochromator beamline at the soft X-ray/XUV free-electron laser in Hamburg (FLASH) is designed to provide tight aberration-free focusing down to 4 µm × 6 µm full width at half-maximum (FWHM) on the sample. Such a focal spot size is mandatory to achieve ultimate resolution and to guarantee best performance of the vacuum-ultraviolet (VUV) off-axis parabolic double-monochromator Raman spectrometer permanently installed at the PG1 beamline as an experimental end-station. The vertical beam size on the sample of the Raman spectrometer, which operates without entrance slit, defines and limits the energy resolution of the instrument which has an unprecedented design value of 2 meV for photon energies below 70 eV and about 15 meV for higher energies up to 200 eV. In order to reach the designed focal spot size of 4 µm FWHM (vertically) and to hold the highest spectrometer resolution, special fully motorized in-vacuum manipulators for the KB mirror holders have been developed and the optics have been aligned employing wavefront-sensing techniques as well as ablative imprints analysis. Aberrations like astigmatism were minimized. In this article the design and layout of the KB mirror manipulators, the alignment procedure as well as microfocus optimization results are presented. PMID:26698054

  9. Conceptual Design of the Small Angle Scattering Beamline at the Australian Synchrotron

    NASA Astrophysics Data System (ADS)

    Kirby, N.; Boldeman, J. W.; Gentle, I.; Cookson, D.

    2007-01-01

    A high performance small angle and wide angle x-ray scattering (SAXS/WAXS) beamline is one of the initial suite of beamlines to be built at the 3 GeV Australian Synchrotron. This beamline will be ready for use in 2008, for structural analysis across a wide range of research applications over length scales of ˜ 1 to greater than 5000 Å. The instrument is intended for advanced analysis capabilities only possible using synchrotron radiation, such as time, space and energy resolved analysis, and for weak scattering systems. Photon energies will be readily variable between 5.2 and 20 keV.

  10. First results from the high-brightness x-ray spectroscopy beamline at ALS

    SciTech Connect

    Perera, R.C.C.; Ng, W.; Jones, G.

    1997-04-01

    Beamline 9.3.1 at the Advanced Light Source (ALS) is a windowless beamline, covering the 1-6 keV photon-energy range, designed to achieve the goal of high brightness at the sample for use in the X-ray Atomic and Molecular Spectroscopy (XAMS) science, surface and interface science, biology and x-ray optical development programs at ALS. X-ray absorption and time of flight photo emission measurements in 2 - 5 keV photon energy in argon along with the flux, resolution, spot size and stability of the beamline will be discussed. Prospects for future XAMS measurements will also be presented.

  11. Progress of projection computed tomography by upgrading of the beamline 37XU of SPring-8

    NASA Astrophysics Data System (ADS)

    Terada, Yasuko; Suzuki, Yoshio; Uesugi, Kentaro; Miura, Keiko

    2016-01-01

    Beamline 37XU at SPring-8 has been upgraded for nano-focusing applications. The length of the beamline has been extended to 80 m. By utilizing this length, the beamline has advantages for experiments such as X-ray focusing, X-ray microscopic imaging and X-ray computed tomography. Projection computed tomography measurements were carried out at experimental hutch 3 located 80 m from the light source. CT images of a microcapsule have been successfully obtained with a wide X-ray energy range.

  12. Imaging in real and reciprocal space at the Diamond beamline I13

    NASA Astrophysics Data System (ADS)

    Rau, C.; Wagner, U. H.; Vila-Comamala, J.; Bodey, A.; Parson, A.; García-Fernández, M.; De Fanis, A.; Pešić, Z.

    2016-01-01

    The Diamond Imaging and Coherence beamline I13 consists of two independent branchlines for imaging in real and reciprocal space. Different microscopies are available providing a range of spatial resolution from 5µm to potentially 5nm. The beamline operates in the energy range of 6-35keV covering different scientific areas such as biomedicine, materials science and geophysics. Several original devices have been developed at the beamline, such as the EXCALIBUR photon counting detector and the combined robot arms for coherent X-ray diffraction.

  13. XAFS at the new materials science beamline 10 at the DELTA storage ring

    NASA Astrophysics Data System (ADS)

    Lützenkirchen-Hecht, D.; Wagner, R.; Frahm, R.

    2016-05-01

    The layout and the characteristics of the hard X-ray beamline BL 10 at the superconducting asymmetric wiggler at the 1.5 GeV Dortmund Electron Accelerator DELTA are described. Equipped with a stable and robust Si(111) channel-cut monochromator, this beamline is suited for XAFS studies in the spectral range from about 4 keV to ca. 16 keV photon energy. We will illustrate the performance of the beamline, and present EXAFS data obtained from several reference compounds. XANES data measured for dilute sample systems as well as surface sensitive grazing incidence EXAFS obtained from thin film samples will also be discussed.

  14. Characterization of the new NSLS infrared microspectroscopy beamline U10B

    SciTech Connect

    Carr, G.L.

    1999-07-19

    The first of several new infrared beamlines, built on a modified bending magnet port of the NSLS VUV ring, is now operational for mid-infrared microspectroscopy. The port simultaneously delivers 40 mrad by 40 mrad to two separate beamlines and spectrometer endstations designated U10A and U10B. The latter is equipped with a scanning infrared microspectrometer. The combination of this instrument and high brightness synchrotron radiation makes diffraction-limited microspectroscopy practical. This paper describes the beamline's performance and presents quantitative information on the diffraction-limited resolution.

  15. CHARACTERIZATION OF THE NEW NSLS INFARED MICROSPECTROSCOPY BEAMLINE U10B.

    SciTech Connect

    CARR,G.L.

    1999-07-19

    The first of several new infrared beamlines, built on a modified bending magnet port of the NSLS VUV ring, is now operational for mid-infrared microspectroscopy. The port simultaneously delivers 40 mrad by 40 mrad to two separate beamlines and spectrometer endstations designated U10A and U10B. The latter is equipped with a scanning infrared microspectrometer. The combination of this instrument and high brightness synchrotron radiation makes diffraction-limited microspectroscopy practical. This paper describes the beamline's performance and presents quantitative information on the diffraction-limited resolution.

  16. Recent Major Improvements to the ALS Sector 5 MacromolecularCrystallography Beamlines

    SciTech Connect

    Morton, Simon A.; Glossinger, James; Smith-Baumann, Alexis; McKean, John P.; Trame, Christine; Dickert, Jeff; Rozales, Anthony; Dauz,Azer; Taylor, John; Zwart, Petrus; Duarte, Robert; Padmore, Howard; McDermott, Gerry; Adams, Paul

    2007-07-01

    Although the Advanced Light Source (ALS) was initially conceived primarily as a low energy (1.9GeV) 3rd generation source of VUV and soft x-ray radiation it was realized very early in the development of the facility that a multipole wiggler source coupled with high quality, (brightness preserving), optics would result in a beamline whose performance across the optimal energy range (5-15keV) for macromolecular crystallography (MX) would be comparable to, or even exceed, that of many existing crystallography beamlines at higher energy facilities. Hence, starting in 1996, a suite of three beamlines, branching off a single wiggler source, was constructed, which together formed the ALS Macromolecular Crystallography Facility. From the outset this facility was designed to cater equally to the needs of both academic and industrial users with a heavy emphasis placed on the development and introduction of high throughput crystallographic tools, techniques, and facilities--such as large area CCD detectors, robotic sample handling and automounting facilities, a service crystallography program, and a tightly integrated, centralized, and highly automated beamline control environment for users. This facility was immediately successful, with the primary Multiwavelength Anomalous Diffraction beamline (5.0.2) in particular rapidly becoming one of the foremost crystallographic facilities in the US--responsible for structures such as the 70S ribosome. This success in-turn triggered enormous growth of the ALS macromolecular crystallography community and spurred the development of five additional ALS MX beamlines all utilizing the newly developed superconducting bending magnets ('superbends') as sources. However in the years since the original Sector 5.0 beamlines were built the performance demands of macromolecular crystallography users have become ever more exacting; with growing emphasis placed on studying larger complexes, more difficult structures, weakly diffracting or smaller

  17. Safety Analysis Report: X17B2 beamline Synchrotron Medical Research Facility

    SciTech Connect

    Gmuer, N.F.; Thomlinson, W.

    1990-02-01

    This report contains a safety analysis for the X17B2 beamline synchrotron medical research facility. Health hazards, risk assessment and building systems are discussed. Reference is made to transvenous coronary angiography. (LSP)

  18. Development of soft X-ray polarized light beamline on Indus-2 synchrotron radiation source

    SciTech Connect

    Phase, D. M. Gupta, Mukul Potdar, S. Behera, L. Sah, R. Gupta, Ajay

    2014-04-24

    This article describes the development of a soft x-ray beamline on a bending magnet source of Indus-2 storage ring (2.5 GeV) and some preliminary results of x-ray absorption spectroscopy (XAS) measurements using the same. The beamline layout is based on a spherical grating monochromator. The beamline is able to accept synchrotron radiation from the bending magnet port BL-1 of the Indus-2 ring with a wide solid angle. The large horizontal and vertical angular acceptance contributes to high photon flux and selective polarization respectively. The complete beamline is tested for ultrahigh vacuum (UHV) ∼ 10{sup −10} mbar. First absorption spectrum was obtained on HOPG graphite foil. Our performance test indicates that modest resolving power has been achieved with adequate photon flux to carry out various absorption experiments.

  19. The Design and Performance of Beamline BL15 at SAGA Light Source

    SciTech Connect

    Okajima, T.; Chikaura, Y.; Suzuki, Y.; Tabata, M.; Soejima, Y.; Haruki, R.; Hara, K.; Nagata, K.; Hiramatsu, N.; Kohno, A.; Takumi, M.; Setoyama, H.; Yoshimura, D.

    2007-01-19

    A new X-ray beamline has been designed and constructed at SAGA Light Source. The beamline, named BL15, covers an energy range from 2.1 to 14.2 keV and is intended for the characterization of various materials developed for industrial purposes. The beamline has an experimental station for the performance of several experiments: e.g. X-ray absorption fine structure (XAFS) measurement; high resolution diffractometry; topographic imaging; energy-dispersive four-circle diffractometry. The photon flux passing through a receiving slit at XAFS measurement position is more than 1 x 1011 photons/sec with focusing mirror in the energy range of less than 8keV. The XANES spectra measurements of Cu and Ti K-edge show that the beamline has a good energy resolution.

  20. New Soft X-ray Beamline (BL10) at the SAGA Light Source

    NASA Astrophysics Data System (ADS)

    Yoshimura, D.; Setoyama, H.; Okajima, T.

    2010-06-01

    A new soft X-ray beamline (BL10) at the SAGA Light Source (SAGA-LS) was constructed at the end of 2008. Commissioning of this new beamline started at the beginning of 2009. Synchrotron radiation from a variably polarizing undulator (APPLE-II) can be used in this beamline. The obtained light is monochromatized by a varied-line-spacing plane grating monochromator with the variable included angle mechanism. Its designed resolving power and photon flux are 3,000-10,000 and 1012-109 photons/s at 300 mA, respectively. The performance test results were generally satisfactory. An overview of the optical design of the beamline and the current status of commissioning are reported.

  1. New soft X-ray beamline BL07LSU at SPring-8

    PubMed Central

    Yamamoto, Susumu; Senba, Yasunori; Tanaka, Takashi; Ohashi, Haruhiko; Hirono, Toko; Kimura, Hiroaki; Fujisawa, Masami; Miyawaki, Jun; Harasawa, Ayumi; Seike, Takamitsu; Takahashi, Sunao; Nariyama, Nobuteru; Matsushita, Tomohiro; Takeuchi, Masao; Ohata, Toru; Furukawa, Yukito; Takeshita, Kunikazu; Goto, Shunji; Harada, Yoshihisa; Shin, Shik; Kitamura, Hideo; Kakizaki, Akito; Oshima, Masaharu; Matsuda, Iwao

    2014-01-01

    A new soft X-ray beamline, BL07LSU, has been constructed at SPring-8 to perform advanced soft X-ray spectroscopy for materials science. The beamline is designed to achieve high energy resolution (E/ΔE> 10000) and high photon flux [>1012 photons s−1 (0.01% bandwidth)−1] in the photon energy range 250–2000 eV with controllable polarization. To realise this state-of-the-art performance, a novel segmented cross undulator was developed and adopted as a light source. The details of the undulator light source and beamline monochromator design are described. The achieved performance of the beamline, such as the photon flux, energy resolution and the state of polarization, is reported. PMID:24562556

  2. New Soft X-ray Beamline (BL10) at the SAGA Light Source

    SciTech Connect

    Yoshimura, D.; Setoyama, H.; Okajima, T.

    2010-06-23

    A new soft X-ray beamline (BL10) at the SAGA Light Source (SAGA-LS) was constructed at the end of 2008. Commissioning of this new beamline started at the beginning of 2009. Synchrotron radiation from a variably polarizing undulator (APPLE-II) can be used in this beamline. The obtained light is monochromatized by a varied-line-spacing plane grating monochromator with the variable included angle mechanism. Its designed resolving power and photon flux are 3,000-10,000 and 10{sup 12}-10{sup 9} photons/s at 300 mA, respectively. The performance test results were generally satisfactory. An overview of the optical design of the beamline and the current status of commissioning are reported.

  3. The electron spectro-microscopy beamline at National Synchrotron Light Source II: A wide photon energy range, micro-focusing beamline for photoelectron spectro-microscopies

    SciTech Connect

    Reininger, R.; Hulbert, S. L.; Chubar, O.; Vescovo, E.; Johnson, P. D.; Valla, T.; Sadowski, J. T.; Starr, D. E.

    2012-02-15

    A comprehensive optical design for a high-resolution, high-flux, wide-energy range, micro-focused beamline working in the vacuum ultraviolet and soft x-ray photon energy range is proposed. The beamline is to provide monochromatic radiation to three photoelectron microscopes: a full-field x-ray photoelectron emission microscope and two scanning instruments, one dedicated to angle resolved photoemission spectroscopy ({mu}-ARPES) and one for ambient pressure x-ray photoelectron spectroscopy and scanning photoelectron microscopy (AP-XPS/SPEM). Microfocusing is achieved with state of the art elliptical cylinders, obtaining a spot size of 1 {mu}m for ARPES and 0.5 {mu}m for AP-XPS/SPEM. A detailed ray tracing analysis quantitatively evaluates the overall beamline performances.

  4. Fundamental neutron physics beamline at the spallation neutron source at ORNL

    DOE PAGESBeta

    Fomin, N.; Greene, G. L.; Allen, R. R.; Cianciolo, V.; Crawford, C.; Tito, T. M.; Huffman, P. R.; Iverson, E. B.; Mahurin, R.; Snow, W. M.

    2014-11-04

    In this paper, we describe the Fundamental Neutron Physics Beamline (FnPB) facility located at the Spallation Neutron Source at Oak Ridge National Laboratory. The FnPB was designed for the conduct of experiments that investigate scientific issues in nuclear physics, particle physics, astrophysics and cosmology using a pulsed slow neutron beam. Finally, we present a detailed description of the design philosophy, beamline components, and measured fluxes of the polychromatic and monochromatic beams.

  5. An Extreme Flux Vacuum Ultraviolet/Ultraviolet Beamline For The Measurement Of Biological Circular Dichroism

    SciTech Connect

    Clarke, D.T.; Vasanthi, N.; Shaw, D.; Brown, A.; Todd, B.; Grant, A.F.; Flaherty, J.V.; Mullacrane, I.D.; Miller, M.J.; Bowler, M.A.; Jones, G.R.; Mythen, C.

    2004-05-12

    A new extreme flux vacuum ultraviolet bending magnet beamline (CD12) has been commission at the SRS, Daresbury. The beamline has met all of its designed performance parameters and these are detailed. The clear advantages of SRCD over CD undertaken on conventional instruments are discussed and examples of its capabilities in terms of measurement precision and enhanced signal-to-noise for both steady-state CD and time-resolved CD are given.

  6. The Low Density Matter (LDM) beamline at FERMI: optical layout and first commissioning

    PubMed Central

    Svetina, Cristian; Grazioli, Cesare; Mahne, Nicola; Raimondi, Lorenzo; Fava, Claudio; Zangrando, Marco; Gerusina, Simone; Alagia, Michele; Avaldi, Lorenzo; Cautero, Giuseppe; de Simone, Monica; Devetta, Michele; Di Fraia, Michele; Drabbels, Marcel; Feyer, Vitaliy; Finetti, Paola; Katzy, Raphael; Kivimäki, Antti; Lyamayev, Viktor; Mazza, Tommaso; Moise, Angelica; Möller, Thomas; O’Keeffe, Patrick; Ovcharenko, Yevheniy; Piseri, Paolo; Plekan, Oksana; Prince, Kevin C.; Sergo, Rudi; Stienkemeier, Frank; Stranges, Stefano; Coreno, Marcello; Callegari, Carlo

    2015-01-01

    The Low Density Matter (LDM) beamline has been built as part of the FERMI free-electron laser (FEL) facility to serve the atomic, molecular and cluster physics community. After the commissioning phase, it received the first external users at the end of 2012. The design and characterization of the LDM photon transport system is described, detailing the optical components of the beamline. PMID:25931066

  7. A modified post damping ring bunch compressor beamline for the TESLA linear collider

    SciTech Connect

    Philippe R.-G. Piot; Winfried Decking

    2004-03-23

    We propose a modified bunch compressor beamline, downstream of the damping ring, for the TESLA linear collider. This modified beamline uses a third harmonic radio-frequency section based on the 3.9 GHz superconducting cavity under development at Fermilab. In our design the beam deceleration is about {approx}50 MeV instead of {approx}450 MeV in the original design proposed.

  8. Implementation of remote monitoring and diffraction evaluation systems at the Photon Factory macromolecular crystallography beamlines

    PubMed Central

    Yamada, Yusuke; pHonda, Nobuo; Matsugaki, Naohiro; Igarashi, Noriyuki; Hiraki, Masahiko; Wakatsuki, Soichi

    2008-01-01

    Owing to recent advances in high-throughput technology in macromolecular crystallography beamlines, such as high-brilliant X-ray sources, high-speed readout detectors and robotics, the number of samples that can be examined in a single visit to the beamline has increased dramatically. In order to make these experiments more efficient, two functions, remote monitoring and diffraction image evaluation, have been implemented in the macromolecular crystallography beamlines at the Photon Factory (PF). Remote monitoring allows scientists to participate in the experiment by watching from their laboratories, without having to come to the beamline. Diffraction image evaluation makes experiments easier, especially when using the sample exchange robot. To implement these two functions, two independent clients have been developed that work specifically for remote monitoring and diffraction image evaluation. In the macromolecular crystallography beamlines at PF, beamline control is performed using STARS (simple transmission and retrieval system). The system adopts a client–server style in which client programs communicate with each other through a server process using the STARS protocol. This is an advantage of the extension of the system; implementation of these new functions required few modifications of the existing system. PMID:18421163

  9. MxCuBE: a synchrotron beamline control environment customized for macromolecular crystallography experiments

    PubMed Central

    Gabadinho, José; Beteva, Antonia; Guijarro, Matias; Rey-Bakaikoa, Vicente; Spruce, Darren; Bowler, Matthew W.; Brockhauser, Sandor; Flot, David; Gordon, Elspeth J.; Hall, David R.; Lavault, Bernard; McCarthy, Andrew A.; McCarthy, Joanne; Mitchell, Edward; Monaco, Stéphanie; Mueller-Dieckmann, Christoph; Nurizzo, Didier; Ravelli, Raimond B. G.; Thibault, Xavier; Walsh, Martin A.; Leonard, Gordon A.; McSweeney, Sean M.

    2010-01-01

    The design and features of a beamline control software system for macromolecular crystallography (MX) experiments developed at the European Synchrotron Radiation Facility (ESRF) are described. This system, MxCuBE, allows users to easily and simply interact with beamline hardware components and provides automated routines for common tasks in the operation of a synchrotron beamline dedicated to experiments in MX. Additional functionality is provided through intuitive interfaces that enable the assessment of the diffraction characteristics of samples, experiment planning, automatic data collection and the on-line collection and analysis of X-ray emission spectra. The software can be run in a tandem client-server mode that allows for remote control and relevant experimental parameters and results are automatically logged in a relational database, ISPyB. MxCuBE is modular, flexible and extensible and is currently deployed on eight macromolecular crystallography beamlines at the ESRF. Additionally, the software is installed at MAX-lab beamline I911-3 and at BESSY beamline BL14.1. PMID:20724792

  10. Remote access to crystallography beamlines at SSRL: novel tools for training, education and collaboration

    PubMed Central

    Smith, Clyde A.; Card, Graeme L.; Cohen, Aina E.; Doukov, Tzanko I.; Eriksson, Thomas; Gonzalez, Ana M.; McPhillips, Scott E.; Dunten, Pete W.; Mathews, Irimpan I.; Song, Jinhu; Soltis, S. Michael

    2010-01-01

    For the past five years, the Structural Molecular Biology group at the Stanford Synchrotron Radiation Lightsource (SSRL) has provided general users of the facility with fully remote access to the macromolecular crystallography beamlines. This was made possible by implementing fully automated beamlines with a flexible control system and an intuitive user interface, and by the development of the robust and efficient Stanford automated mounting robotic sample-changing system. The ability to control a synchrotron beamline remotely from the comfort of the home laboratory has set a new paradigm for the collection of high-quality X-ray diffraction data and has fostered new collaborative research, whereby a number of remote users from different institutions can be connected at the same time to the SSRL beamlines. The use of remote access has revolutionized the way in which scientists interact with synchrotron beamlines and collect diffraction data, and has also triggered a shift in the way crystallography students are introduced to synchrotron data collection and trained in the best methods for collecting high-quality data. SSRL provides expert crystallographic and engineering staff, state-of-the-art crystallography beamlines, and a number of accessible tools to facilitate data collection and in-house remote training, and encourages the use of these facilities for education, training, outreach and collaborative research. PMID:22184477

  11. Measurement of thermal contact conductance of SPring-8 beamline components

    NASA Astrophysics Data System (ADS)

    Mochizuki, Tetsuro; Ohashi, Haruhiko; Sano, Mutsumi; Takahashi, Sunao; Goto, Shunji

    2007-09-01

    Direct cooling is adopted for most high heat load components in SPring-8 beamlines. On the other hand, contact cooling is employed for some components such as a graphite filter, aluminum filter, mirror, and cryogenic monochromator silicon crystal. For the thermal design of the contact cooling components, it is important to obtain reliable thermal contact conductance value. The conductance depends on many parameters such as the surface materials, surface roughness, flatness of the surface, interstitial materials, temperature of the contact surface, and contact pressure. An experimental setup is fablicated to measure the conductance at liquid nitrogen temperature and room temperature. The thermal contact conductance of a Si-Cu interface and that of a Si-In-Cu interface are measured at cryogenic temperature at contact pressures ranging from 0.1-1.1 MPa. The conductance of an Al-Cu interface and that of a graphite-Cu interface are measured using gold and silver foils as interstitial materials. The measurements are performed at room temperature and at pressures ranging from 0.5-4 MPa. The experimental setup and the results obtained are presented.

  12. Neutrino Flux Prediction for the NuMI Beamline

    SciTech Connect

    Soplin, Leonidas Aliaga

    2016-01-01

    The determination of the neutrino flux in any conventional neutrino beam presents a challenge for the current and future short and long baseline neutrino experiments. The uncertainties associated with the production and attenuation of the hadrons in the beamline materials along with those associated with the beam optics have a big effect in the flux spectrum knowledge. For experiments like MINERvA, understanding the flux is crucial since it enters directly into every neutrino-nucleus cross-sections measurements. The foundation of this work is predicting the neutrino flux at MINERvA using dedicated measurements of hadron production in hadron-nucleus collisions and incorporating in-situ MINERvA data that can provide additional constraints. This work also includes the prospect for predicting the flux at other detectors like the NOvA Near detector. The procedure and conclusions of this thesis will have a big impact on future hadron production experiments and on determining the flux for the upcoming DUNE experiment.

  13. Neutrino Flux Prediction for the NuMI Beamline

    SciTech Connect

    Aliaga Soplin, Leonidas

    2016-01-01

    The determination of the neutrino flux in any conventional neutrino beam presents a challenge for the current and future short and long baseline neutrino experiments. The uncertainties associated with the production and attenuation of the hadrons in the beamline materials along with those associated with the beam optics have a big effect in the flux spectrum knowledge. For experiments like MINERvA, understanding the flux is crucial since it enters directly into every neutrino-nucleus cross-sections measurements. The foundation of this work is predicting the neutrino flux at MINERvA using dedicated measurements of hadron production in hadron-nucleus collisions and incorporating in-situ MINERvA data that can provide additional constraints. This work also includes the prospect for predicting the flux at other detectors like the NOvA Near detector. The procedure and conclusions of this thesis will have a big impact on future hadron production experiments and on determining the fl ux for the upcoming DUNE experiment.

  14. Automatic sample Dewar for MX beam-line

    NASA Astrophysics Data System (ADS)

    Charignon, T.; Tanchon, J.; Trollier, T.; Ravex, A.; Theveneau, P.

    2014-01-01

    It is very common for crystals of large biological macromolecules to show considerable variation in quality of their diffraction. In order to increase the number of samples that are tested for diffraction quality before any full data collections at the ESRF*, an automatic sample Dewar has been implemented. Conception and performances of the Dewar are reported in this paper. The automatic sample Dewar has 240 samples capability with automatic loading/unloading ports. The storing Dewar is capable to work with robots and it can be integrated in a full automatic MX** beam-line. The samples are positioned in the front of the loading/unloading ports with and automatic rotating plate. A view port has been implemented for data matrix camera reading on each sample loaded in the Dewar. At last, the Dewar is insulated with polyurethane foam that keeps the liquid nitrogen consumption below 1.6 L/h. At last, the static insulation also makes vacuum equipment and maintenance unnecessary. This Dewar will be useful for increasing the number of samples tested in synchrotrons.

  15. Improved monochromator design for high heat load beamlines at CHESS

    SciTech Connect

    Smolenski, K.; Pahl, R.; Doing, P.; Conolly, C.; Clark, B.; Ehen, J.; Shen, Q.

    1996-09-01

    The use of water-cooling channels in silicon x-ray monochromators for the Cornell High Energy Synchrotron Source (CHESS) high power wiggler beamlines has been studied by finite element analysis. The efficiency from channels of different dimensions, ranging from 25 mm to 2 mm width and 5 mm depth, has been calculated. The new crystals are designed to replace the indirect cooled monochromators currently used at CHESS wiggler stations. At typical operation parameters of 150 mA electron current at 5.3 GeV and a gap of 40 mm, the 24-pole wiggler at CHESS provides an x-ray beam with a total power of 2.7 kW at the monochromator. Procedures have been developed for fabrication of internally cooled crystals using a silver-glass dye attach paste. Tests of a new crystal with a conventional x-ray source revealed very small amounts of residual strain. Experiments with synchrotron radiation are scheduled in the near future. {copyright} {ital 1996 American Institute of Physics.}

  16. Status of the Design of the LBNE Neutrino Beamline

    SciTech Connect

    Andrews, R.; Chen, A.Z.; Childress, S.C.; Moore, C.D.; Papadimitriou, V.; Campbell, M.R.; /Fermilab

    2012-05-01

    The Long Baseline Neutrino Experiment (LBNE) will utilize a neutrino beamline facility located at Fermilab to carry out a compelling research program in neutrino physics. The facility will aim a beam of neutrinos toward a detector placed at the Homestake Mine in South Dakota, about 1300 km away. The neutrinos are produced as follows: First, protons extracted from the MI-10 section of the Main Injector (60-120 GeV) hit a solid target above grade and produce mesons. Then, the charged mesons are focused by a set of focusing horns into a 200 m long decay pipe, towards the far detector. Finally, the mesons that enter the decay pipe decay into neutrinos. The parameters of the facility were determined taking into account several factors including the physics goals, the modelling of the facility, spacial and radiological constraints and the experience gained by operating the NuMI facility at Fermilab. The initial beam power is expected to be {approx}700 kW, however some of the parameters were chosen to be able to deal with a beam power of 2.3 MW in order to enable the facility to run with an upgraded accelerator complex. We discuss here the status of the design and the associated challenges.

  17. Students on the Beamline: classroom, research, and discovery

    NASA Astrophysics Data System (ADS)

    Patry, J.; Walker, T.

    2012-12-01

    High level research is mainly the focus of trained scientists who possess a science specific background. The Canadian Light Source outreach service has developed a two stage research immersion approach which brings together students, teachers, and renowned scientists: Students on the Beamline. The first stage offers a training session for teachers to develop their professional competencies in regards to authentic science research and the synchrotron facility. During the second stage, students from classrooms apply a research protocol of their own design with the help of their teacher and synchrotron scientists. During this presentation, we will first explain the professional approach of the training. In the second part, two experiments designed by students will be presented which are geophysically based so to speak: Study of the Meteoritic Melt Sheet of the Manicouagan Basin and Effects of Olivine on the capture of NOx. Results have shown that teachers bring in the classroom a more authentic and new experience in research application. As for the students, their unique research has contributed to the increase of our knowledge and a better understanding of the scientific inquiry process.Scientist and teacher working together on the synchrotron

  18. Automatic sample Dewar for MX beam-line

    SciTech Connect

    Charignon, T.; Tanchon, J.; Trollier, T.; Ravex, A.; Theveneau, P.

    2014-01-29

    It is very common for crystals of large biological macromolecules to show considerable variation in quality of their diffraction. In order to increase the number of samples that are tested for diffraction quality before any full data collections at the ESRF*, an automatic sample Dewar has been implemented. Conception and performances of the Dewar are reported in this paper. The automatic sample Dewar has 240 samples capability with automatic loading/unloading ports. The storing Dewar is capable to work with robots and it can be integrated in a full automatic MX** beam-line. The samples are positioned in the front of the loading/unloading ports with and automatic rotating plate. A view port has been implemented for data matrix camera reading on each sample loaded in the Dewar. At last, the Dewar is insulated with polyurethane foam that keeps the liquid nitrogen consumption below 1.6 L/h. At last, the static insulation also makes vacuum equipment and maintenance unnecessary. This Dewar will be useful for increasing the number of samples tested in synchrotrons.

  19. Three Biomedical Beamlines at NSLS-II for Macromolecular Crystallography and Small-Angle Scattering

    NASA Astrophysics Data System (ADS)

    Schneider, D. K.; Berman, L. E.; Chubar, O.; Hendrickson, W. A.; Hulbert, S. L.; Lucas, M.; Sweet, R. M.; Yang, L.

    2013-03-01

    We report on the status of the development of three beamlines for the National Synchrotron Light Source-II (NSLS-II), two for macromolecular crystallography (MX), and one for wide- and small-angle x-ray scattering (SAXS). Funded by the National Institutes of Health, this suite of Advanced Beamlines for Biological Investigations with X-rays (ABBIX) is scheduled to begin operation by 2015. The two MX beamlines share a sector with identical canted in-vacuum undulators (IVU21). The microfocusing FMX beamline on the inboard branch employs a two-stage horizontal source demagnification scheme, will cover an energy range of 5 - 23 keV, and at 12.7 keV will focus a flux of up to 1013 ph/s into a spot of 1 μm width. The companion AMX beamline on the short outboard branch of the sector is tunable in the range of 5 - 18 keV and has a native focus of 4 μm (h) × 2 μm (v). This robust beamline will be highly automated, have high throughput capabilities, and with larger beams and low divergence will be well suited for structure determinations on large complexes. The high brightness SAXS beamline, LIX, will provide multiple dynamic and static experimental systems to support scientific programs in solution scattering, membrane structure determination, and tissue imaging. It will occupy a different sector, equipped with a single in-vacuum undulator (IVU23). It can produce beams as small as 1 μm across, and with a broad energy range of 2.1 - 18 keV it will support anomalous SAXS.

  20. DESIGN OF VISIBLE DIAGNOSTIC BEAMLINE FOR NSLS2 STORAGE RING

    SciTech Connect

    Cheng, W.; Fernandes, H.; Hseuh, H.; Kosciuk, B.; Krinsky, S.; Singh, O.

    2011-03-28

    A visible synchrotron light monitor (SLM) beam line has been designed at the NSLS2 storage ring, using the bending magnet radiation. A retractable thin absorber will be placed in front of the first mirror to block the central x-rays. The first mirror will reflect the visible light through a vacuum window. The light is guided by three 6-inch diameter mirrors into the experiment hutch. In this paper, we will describe design work on various optical components in the beamline. The ultra high brightness NSLS-II storage ring is under construction at Brookhaven National Laboratory. It will have 3GeV, 500mA electron beam circulating in the 792m ring, with very low emittance (0.9nm.rad horizontal and 8pm.rad vertical). The ring is composed of 30 DBA cells with 15 fold symmetry. Three damping wigglers will be installed in long straight sections 8, 18 and 28 to lower the emittance. While electrons pass through the bending magnet, synchrotron radiation will be generated covering a wide spectrum. There are other insertion devices in the storage ring which will generate shorter wavelength radiation as well. Synchrotron radiation has been widely used as diagnostic tool to measure the transverse and longitudinal profile. Three synchrotron light beam lines dedicated for diagnostics are under design and construction for the NSLS-II storage ring: two x-ray beam lines (pinhole and CRL) with the source points from Cell 22 BM{_}A (first bending in the DBA cell) and Cell22 three-pole wiggler; the third beam line is using visible part of radiation from Cell 30 BM{_}B (second bending magnet from the cell). Our paper focuses on the design of the visible beam line - SLM.

  1. High resolution neutron imaging capabilities at BOA beamline at Paul Scherrer Institut

    NASA Astrophysics Data System (ADS)

    Tremsin, A. S.; Morgano, M.; Panzner, T.; Lehmann, E.; Filgers, U.; Vallerga, J. V.; McPhate, J. B.; Siegmund, O. H. W.; Feller, W. B.

    2015-06-01

    The cold neutron spectrum of the Beamline for neutron Optics and other Applications (BOA) at Paul Scherrer Institut enables high contrast neutron imaging because neutron cross sections for many materials increase with neutron wavelength. However, for many neutron imaging applications, spatial resolution can be as important as contrast. In this paper the neutron transmission imaging capabilities of an MCP/Timepix detector installed at the BOA beamline are presented, demonstrating the possibilities for studying sub-20 μm features in various samples. In addition to conventional neutron radiography and microtomography, the high degree of neutron polarization at the BOA beamline can be very attractive for imaging of magnetic fields, as demonstrated by our measurements. We also show that a collimated cold neutron beamline combined with a high resolution detector can produce image artifacts, (e.g. edge enhancements) due to neutron refraction and scattering. The results of our experiments indicate that the BOA beamline is a valuable addition to neutron imaging facilities, providing improved and sometimes unique capabilities for non-destructive studies with cold neutrons.

  2. The vacuum ultraviolet beamline/endstations at NSRL dedicated to combustion research.

    PubMed

    Zhou, Zhongyue; Du, Xuewei; Yang, Jiuzhong; Wang, Yizun; Li, Chaoyang; Wei, Shen; Du, Liangliang; Li, Yuyang; Qi, Fei; Wang, Qiuping

    2016-07-01

    An undulator-based vacuum ultraviolet (VUV) beamline (BL03U), intended for combustion chemistry studies, has been constructed at the National Synchrotron Radiation Laboratory (NSRL) in Hefei, China. The beamline is connected to the newly upgraded Hefei Light Source (HLS II), and could deliver photons in the 5-21 eV range, with a photon flux of 10(13) photons s(-1) at 10 eV when the beam current is 300 mA. The monochromator of the beamline is equipped with two gratings (200 lines mm(-1) and 400 lines mm(-1)) and its resolving power is 3900 at 7.3 eV for the 200 lines mm(-1) grating and 4200 at 14.6 eV for the 400 lines mm(-1) grating. The beamline serves three endstations which are designed for respective studies of premixed flame, fuel pyrolysis in flow reactor, and oxidation in jet-stirred reactor. Each endstation contains a reactor chamber, an ionization chamber where the molecular beam intersects with the VUV light, and a home-made reflectron time-of-flight mass spectrometer. The performance of the beamline and endstations with some preliminary results is presented here. The ability to detect reactive intermediates (e.g. H, O, OH and hydroperoxides) is advantageous in combustion chemistry research. PMID:27359154

  3. Investigation of the heat handling capabilities of DIII-D neutral beamline internal components

    SciTech Connect

    Phillips, J.C.; Baxi, C.B.; Hong, R.

    1993-10-01

    The current DIII-D neutral beam system is a nominal five second pulse length upgrade of a previous design rated for only 500 msec operation. While the ion sources are rated for 60 sec operation, in practice pulse lengths are limited both by the beamline internal components ability to handle the fraction of the power which is scraped off, and by the power supplies ability to provide pulse lengths of greater than 5 sec. This paper examines the capability of the existing DIII-D neutral beamline heat removing components both in terms of present and desired operating parameters. To date, at 2.5 MW per ion source, pulses are limited to 3.5 sec by beamline internal components, while at lower ratings of 2.0 MW per ion source, up to 5 sec pulses have been achieved. Recent advances and demonstration of the extraction of 3.5 MW per DIII-D ion source give an even wider window of operating conditions. A full series of beamline thermocouple data has been collected to determine the heat loading and implied surface temperatures for the various DIII-D neutral beamline internal components. These data will be presented along with an analysis of the needs for specific component upgrades, given a desire for 10 sec operation.

  4. CAT Guide and Beamline Directory. A key to APS Collaborative Access Teams

    SciTech Connect

    1999-07-08

    The Advanced Photon Source (APS), a national user facility for synchrotrons radiation research, is located at Argonne National Laboratory, approximately 25 miles southwest of Chicago, Illinois. The APS is considered a third-generation synchrotrons radiation facility (specifically designed to accommodate insertion devices to serve as radiation sources) and is one of three such facilities in the world. Currently, it is the most brilliant source in the United States for research in such diverse fields as biology, medicine, materials science, chemistry, geology, agriculture and soil science, physics, and manufacturing technology. Researchers use the APS either as members of Collaborative Access Teams (CATS) or as Independent Investigators (IIs). CATS are responsible for designing, building, and operating beamlines in one or more sectors, each sector consisting of an insertion-device (ID) beamline and a bending-magnet (BM) beamline. Each beamline is designed to accommodate a specific type of research program(s) and is optimized accordingly. CAT members are entitled to use 75% of the available beam time to pursue CAT research goals. The remaining 25% of the available beam time must be made available to IIs. This document was written to help prospective IIs determine which beamlines are suitable for their specific experiments.

  5. Tolerancing of diffraction-limited Kirkpatrick-Baez synchrotron beamline optics for extreme-ultraviolet metrology.

    PubMed

    Naulleau, P P; Goldberg, K A; Batson, P J; Jeong, S; Underwood, J H

    2001-08-01

    The recent interest in extreme-ultraviolet (EUV) lithography has led to the development of an array of at-wavelength metrologies implemented on synchrotron beamlines. These beamlines commonly use Kirkpatrick-Baez (K-B) systems consisting of two perpendicular, elliptically bent mirrors in series. To achieve high-efficiency focusing into a small spot, unprecedented fabrication and assembly tolerance is required of these systems. Here we present a detailed error-budget analysis and develop a set of specifications for diffraction-limited performance for the K-B optic operating on the EUV interferometry beamline at Lawrence Berkeley National Laboratory's Advanced Light Source. The specifications are based on code v modeling tools developed explicitly for these optical systems. Although developed for one particular system, the alignment sensitivities presented here are relevant to K-B system designs in general. PMID:18360402

  6. Neutron imaging options at the BOA beamline at Paul Scherrer Institut

    NASA Astrophysics Data System (ADS)

    Morgano, M.; Peetermans, S.; Lehmann, E. H.; Panzner, T.; Filges, U.

    2014-08-01

    The BOA beamline at the Swiss spallation neutron source SINQ at Paul Scherrer Institut is a flexible instrument used mainly for testing novel techniques and devices for neutron scattering and optics, but, due to the large and relatively homogeneous field of view, it can be successfully used for experiments in the field of neutron imaging. The beamline allows also for the exploitation of advanced imaging concepts such as polarized neutron imaging and diffractive neutron imaging. In this paper we present the characterization of the BOA beamline in the light of its neutron imaging capabilities. We show also the different techniques that can be employed there as user-friendly plugins for non-standard neutron imaging experiments.

  7. Commissioning of a new beamline and station for ARPES at NSRL

    NASA Astrophysics Data System (ADS)

    Zou, Chongwen; Sun, Bai; Zhang, Wenhua; Wang, Guodong; Xu, Pengshou; Wang, Qiuping; Xu, Faqiang; Pan, Haibin

    2005-08-01

    The commissioning of a new beamline and station for angle-resolved photoelectron spectroscopy (ARPES) at the National Synchrotron Radiation Laboratory (NSRL) in Hefei is described. The beamline employs a variable angle spherical grating monochromator (VASGM) covering the photon energy from about 10 to 300 eV. The resolution and the flux of the beamline have been measured using a gas cell and a calibrated photodiode. The whole range resolving power is better than 1000 and the flux is better than 4×10 10photons/s/100 mA which have reached the specification of original design. By using the method of second harmonic spectra for high energy and the valence band spectra for low energy, the whole range incident photon energies have been calibrated. Finally, an ARPES experiment from a standard Cu sample is taken to illustrate the performance of the whole system.

  8. Mirror and grating surface figure requirements for grazing incidence synchrotron radiation beamlines: Power loading effects

    SciTech Connect

    Hulbert, S.L.; Sharma, S.

    1987-01-01

    At present, grazing incidence mirrors are used almost exclusively as the first optical element in VUV and soft x-ray synchrotron radiation beamlines. The performance of these mirrors is determined by thermal and mechanical stress-induced figure errors as well as by figure errors remaining from the grinding and polishing process. With the advent of VUV and soft x-ray undulators and wigglers has come a new set of thermal stress problems related to both the magnitude and the spatial distribution of power from these devices. In many cases the power load on the entrance slits and gratings in these beamlines is no longer negligible. The dependence of thermally-induced front-end mirror figure errors on various storage ring and insertion device parameters (especially those at the National Synchrotron Light Source) and the effects of these figure errors on two classes of soft x-ray beamlines are presented.

  9. Development and Application of the STARS-based Beamline Control System at the Photon Factory

    NASA Astrophysics Data System (ADS)

    Kosuge, Takashi; Nigorikawa, Kazuyuki; Nagatani, Yasuko; Saito, Yuuki

    2010-06-01

    STARS[1-2] (Simple Transmission and Retrieval System) is a message transferring software for small-scale control systems with TCP/IP sockets, originally developed at the Photon Factory (PF). Because it has a server-client architecture using TCP/IP sockets and can work on various types of operating systems, the design and application are quite flexible. We have developed a common low-level beamline control system based on the STARS technology. Many kinds of useful STARS clients (device drivers, data acquisitions, user interfaces etc.) are available now, and so far, the system has been installed at 22 PF beamlines. We will describe the development and generalize of the STARS-based beamline control system at the PF.

  10. High heat load crystal cooling strategies for an APS wiggler beamline

    SciTech Connect

    Beno, M.A.; Knapp, G.S.; Engbretson, M.

    1997-07-01

    High energy wigglers produce extremely high total powers. For example, the insertion device for one beamline of the Basic Energy Sciences Synchrotron Research Center (BESSRC) is an elliptical multipole wiggler (EMPW) which can generate circularly polarized X-rays on axis and produces a total power of {approximately}8 kW. This insertion device will be used to simultaneously provide x-rays to three branch lines, a branch equipped with a normal double crystal monochromator feeding a scattering and spectroscopy station, and two branches with single-bounce horizontally deflecting monochromators for Compton scattering and High Energy Diffraction. The crystal optics for this type of device require substantially different heat load solutions than those used for undulator beamlines. We will discuss how the beam is split and shared among the beamline branch lines and present the crystal cooling strategies employed for both the double-crystal monochromator and horizontally deflecting single-bounce monochromators.

  11. The Design of Superconducting Wiggler Beamline BL7 at SAGA-LS

    SciTech Connect

    Kawamoto, M.; Sumitani, K.; Okajima, T.

    2010-06-23

    A new hard X-ray beamline has been designed at Saga Light Source. The beamline, named BL7, uses a newly developed 4-Tesla superconducting wiggler as a light source in order to cover a wide energy range to 30 keV. This beamline has a simple optics: a double-crystal monochromator and a Rh-coated bent-cylindrical mirror and can supply a focused beam with a photon flux about 1x10{sup 10} photons/s and a sub-millimeter size. Several experiments will be performed in the experimental station: e.g. protein crystallography; X-ray micro computed tomography; X-ray absorption fine structure measurement.

  12. The infrared microspectroscopy beamline at CAMD and its application in plant pathogen interactions

    NASA Astrophysics Data System (ADS)

    Kizilkaya, O.; Prange, A.; Steiner, U.; Oerke, E.-C.; Scott, J. D.; Morikawa, E.; Hormes, J.

    2007-11-01

    At the beginning of 2006, the first infrared microspectroscopy beamline at the Louisiana State University, Center for Advanced Microstructures and Devices (CAMD) storage ring came into operation. The infrared microscope has recently been upgraded with a new liquid nitrogen-cooled mercury-cadmium-telluride detector, MCT-A, and a new dipole chamber to improve the signal-to-noise ratio and extend the beamline capability to far-IR region. In this contribution, we report first results, by using the microspectroscopy beamline, in the investigation of plant-pathogen interactions: apple- Venturia inaequalis causing scab. The infrared spectra of the healthy plant leaves were compared to those obtained from the infected ones. These spatially resolved data are used to understand the dynamics of physiological modifications, which occur during pathogenesis.

  13. Soft x-ray spectroscopy undulator beamline at the Advanced Photon Source

    SciTech Connect

    Randall, K.J.; Xu, Z.; Moore, J.F.; Gluskin, E.

    1997-09-01

    Construction of the high-resolution soft x ray spectroscopy undulator beamline, 2ID-C, at the Advanced Photon Source (APS) has been completed. The beamline, one of two soft x ray beamlines at the APS, will cover the photon energy range from 500 to 3,000 eV, with a maximum resolving power between 7,000 and 14,000. The optical design is based on a spherical grating monochromator (SGM) giving both high resolution and high flux throughput. Photon flux is calculated to be approximately 10{sup 12}--10{sup 13} photons per second with a beam size of approximately 1 x 1 mm{sup 2} at the sample.

  14. Diffraction applications using the energy dispersive beamline, X6A, at NSLS

    NASA Astrophysics Data System (ADS)

    Lee, P. L.; Beno, M. A.; Knapp, G. S.; Jennings, G.; Ogata, C. M.

    1994-08-01

    The energy dispersive beamline X6A, at the National Synchrotron Light Source (NSLS) employs a curved crystal monochromator (polychromator) which focuses a range (approximately 1 keV) of x-ray energies into a narrow (100-120 micron) line image. Although this beamline was constructed primarily for time dependent EXAFS experiments, the authors have begun to explore the use of this instrument for energy dispersive diffraction experiments with different types of sample including macromolecular crystals. The tunability (E = 6.5 keV to 21 keV) and flexibility ((Delta)E = 100-1,000 eV) of the instrument makes the beamline ideal as a test bed for the application of polychromatic single crystal diffraction techniques to different chemical or biological materials.

  15. Development and Application of the STARS-based Beamline Control System at the Photon Factory

    SciTech Connect

    Kosuge, Takashi; Nigorikawa, Kazuyuki; Nagatani, Yasuko; Saito, Yuuki

    2010-06-23

    STARS{sup [1-2]}(Simple Transmission and Retrieval System) is a message transferring software for small-scale control systems with TCP/IP sockets, originally developed at the Photon Factory (PF). Because it has a server-client architecture using TCP/IP sockets and can work on various types of operating systems, the design and application are quite flexible. We have developed a common low-level beamline control system based on the STARS technology. Many kinds of useful STARS clients (device drivers, data acquisitions, user interfaces etc.) are available now, and so far, the system has been installed at 22 PF beamlines. We will describe the development and generalize of the STARS-based beamline control system at the PF.

  16. A telescope proton recoil spectrometer for fast neutron beam-lines

    NASA Astrophysics Data System (ADS)

    Cazzaniga, C.; Rebai, M.; Tardocchi, M.; Croci, G.; Nocente, M.; Ansell, S.; Frost, C. D.; Gorini, G.

    2015-07-01

    Fast neutron measurements were performed on the VESUVIO beam-line at the ISIS spallation source using a new telescope proton recoil spectrometer. Neutrons interact on a plastic target. Proton production is mainly due to elastic scattering on hydrogen nuclei and secondly due to interaction with carbon nuclei. Recoil protons are measured by a proton spectrometer, which uses in coincidence a 2.54 cm thick YAP scintillator and a 500μm thick silicon detector, measuring the full proton recoil energy and the partial deposited energy in transmission, respectively. Recoil proton spectroscopy measurements (up to Ep = 60MeV) have been interpreted by using Monte Carlo simulations of the beam-line. This instrument is of particular interest for the characterization of the ChipIr beam-line at ISIS, which was designed to feature an atmospheric-like neutron spectrum for the irradiation of micro-electronics.

  17. The SEXTANTS beamline at SOLEIL: a new facility for elastic, inelastic and coherent scattering of soft X-rays

    NASA Astrophysics Data System (ADS)

    Sacchi, M.; Jaouen, N.; Popescu, H.; Gaudemer, R.; Tonnerre, J. M.; Chiuzbaian, S. G.; Hague, C. F.; Delmotte, A.; Dubuisson, J. M.; Cauchon, G.; Lagarde, B.; Polack, F.

    2013-03-01

    SEXTANTS is a new SOLEIL beamline dedicated to soft X-ray scattering techniques. The beamline, covering the 50-1700 eV energy range, features two Apple-II undulators for polarization control and a fixed-deviation monochromator. Two branch-lines host three end-stations for elastic, inelastic and coherent scattering experiments.

  18. The macromolecular crystallography beamlines at BESSY II of the Helmholtz-Zentrum Berlin: Current status and perspectives

    NASA Astrophysics Data System (ADS)

    Mueller, Uwe; Förster, Ronald; Hellmig, Michael; Huschmann, Franziska U.; Kastner, Alexandra; Malecki, Piotr; Pühringer, Sandra; Röwer, Martin; Sparta, Karine; Steffien, Michael; Ühlein, Monika; Wilk, Piotr; Weiss, Manfred S.

    2015-07-01

    For a little over a decade now, the Macromolecular Crystallography (MX) group at the Helmholtz-Zentrum Berlin (HZB) has been operating three state-of-the-art synchrotron beamlines for MX at the BESSY II storage ring in Berlin. The three HZB-MX beamlines, BL14.1, BL14.2 and BL14.3, serve a stable and growing user community of currently more than 100 independent research groups from Berlin, Germany and Europe. Every year, the beamlines provide close to 200 days of MX-beamtime. Over time, the HZB-MX beamlines and endstations, in particular BL14.1, have been continually developed and upgraded and, since 2010, they operate as the most productive MX beamlines in Germany. The environment of the beamlines includes various ancillary equipment as well as additional facilities, such as office space adjacent to the beamlines, a sample preparation laboratory, a safety level 1 biology laboratory (HZB-MX BioLab) and all necessary computing resources. In this paper, the current status of the beamlines as well as the ongoing developments are described.

  19. A summary of recent experimental results from Mark J: High energy e/sup +/e/sup /minus// collisions at PETRA: Report Number 131

    SciTech Connect

    Adeva, B.; Barber, D.P.; Becker, U.; Berdugo, J.; Bohm, A.; Branson, J.G.; Burger, J.D.; Capell, M.; Cerrada, M.; Chang, C.C.

    1983-12-01

    The PETRA electron-positron collider at DESY in Hamburg, Federal Republic of Germany, began operating in 1978, with four intersection regions devoted to experiments. In the intervening five years, five detector devices, CELLO, JADE, MARK-J, PLUTO and TASSO have accumulated and published a substantial variety of experimental results. The limits of validity of Quantum Electro-Dynamics (QED) have been extended; the pointlike nature of leptons and quarks have been probed at exceedingly small distances; the Glashow, Weinberg and Salam (GWS) '' standard electroweak model'' has been tested and found to describe interactions remarkably well; the predicted interference between electromagnetic and weak forces has been conclusively demonstrated; events with three jets have been discovered and interpreted as resulting from gluons, as predicted by Quantum Chromo-Dynamics (QCD); the sixth, ''top,'' quark has not been found yet, although an energy search for ''toponium'' (top + antitop) has been carried out up to 43.1 GeV center of mass energy. An integrated luminosity of about 100 pb/sup /minus/1/ mostly at energies above 30 GeV, has produced a very large sample of events. The present paper is a complete review and up-dating of all MARK-J physics results either published or unpublished. Since the amount of interesting information is so large, we realized that a coherent summation could be of substantial usefulness to the community. In order that this review can serve many needs, we include, a brief description of the apparatus and the data acquisition and analysis.

  20. High-brightness beamline for x-ray spectroscopy at the ALS

    SciTech Connect

    Perera, R.C.C.; Jones, G.; Lindle, D.W.

    1997-04-01

    Beamline 9.3.1 at the Advanced Light Source (ALS) is a windowless beamline, covering the 1-6 keV photon-energy range, designed to achieve the goals of high energy resolution, high flux, and high brightness at the sample. When completed later this year, it will be the first ALS monochromatic hard x-ray beamline, and its brightness will be an order of magnitude higher than presently available in this energy range. In addition, it will provide flux and resolution comparable to any other beamline now in operation. To achieve these goals, two technical improvements, relative to existing x-ray beamlines, were incorporated. First, a somewhat novel optical design for x-rays, in which matched toroidal mirrors are positioned before and after the double-crystal monochromator, was adopted. This configuration allows for high resolution by passing a collimated beam through the monochromator, and for high brightness by focusing the ALS source on the sample with unit magnification. Second, a new {open_quotes}Cowan type{close_quotes} double-crystal monochromator based on the design used at NSLS beamline X-24A was developed. The measured mechanical precision of this new monochromator shows significant improvement over existing designs, without using positional feedback available with piezoelectric devices. Such precision is essential because of the high brightness of the radiation and the long distance (12 m) from the source (sample) to the collimating (focusing) mirror. This combination of features will provide a bright, high resolution, and stable x-ray beam for use in the x-ray spectroscopy program at the ALS.

  1. Laser-driven electron beamlines generated by coupling laser-plasma sources with conventional transport systems

    SciTech Connect

    Antici, P.; Benedetti, C.; Lancia, L.; Migliorati, M.; Mostacci, A.; Palumbo, L.

    2012-08-15

    Laser-driven electron beamlines are receiving increasing interest from the particle accelerator community. In particular, the high initial energy, low emittance, and high beam current of the plasma based electron source potentially allow generating much more compact and bright particle accelerators than what conventional accelerator technology can achieve. Using laser-generated particles as injectors for generating beamlines could significantly reduce the size and cost of accelerator facilities. Unfortunately, several features of laser-based particle beams need still to be improved before considering them for particle beamlines and thus enable the use of plasma-driven accelerators for the multiple applications of traditional accelerators. Besides working on the plasma source itself, a promising approach to shape the laser-generated beams is coupling them with conventional accelerator elements in order to benefit from both a versatile electron source and a controllable beam. In this paper, we perform start-to-end simulations to generate laser-driven beamlines using conventional accelerator codes and methodologies. Starting with laser-generated electrons that can be obtained with established multi-hundred TW laser systems, we compare different options to capture and transport the beams. This is performed with the aim of providing beamlines suitable for potential applications, such as free electron lasers. In our approach, we have analyzed which parameters are critical at the source and from there evaluated different ways to overcome these issues using conventional accelerator elements and methods. We show that electron driven beamlines are potentially feasible, but exploiting their full potential requires extensive improvement of the source parameters or innovative technological devices for their transport and capture.

  2. Soft-x-ray and vacuum-ultraviolet beamlines at the National Synchrotron Light Source 700-MeV storage ring

    SciTech Connect

    Williams, G.P.; Howells, M.R.

    1982-01-01

    We summarize the characteristics of the first beamlines which are being installed and commissioned at the National Synchrotron Light Source (NSLS) 700 MeV storage ring at Brookhaven National Laboratory. We also give a progress report as of July 1982 on the early stages of beamline alignment and operation in which particular attention is paid to the 5 beamlines which NSLS has developed. The report describes in detail a novel method for beamline alignment which is of general application.

  3. High Precision Mechanical Components for Soft X-ray Beamline: Engineering Goal and Testing Results

    SciTech Connect

    Kaznacheyev, K. V.; Karunakaran, Ch.; Sitnikov, A.; Loken, D.; Warwick, T.; Nagy, M.; Hitchcock, A. P.

    2007-01-19

    As the emittance of SR rings approaches the diffraction limit for soft x-rays, one requires not only excellence in design and performance of the optical elements, but also precision and performance of mechanical components, such as mirror manipulators, monochromator scanners and exit slits. We will present simple but efficient solutions for the mechanical systems of this type, commonly encountered in soft x-ray beamlines. These solutions have been implemented and their performance evaluated with test results from the spectromicroscopy beamline at the Canadian Light Source.

  4. Beamline BL-07 at Indus-2: a facility for microfabrication research.

    PubMed

    Dhamgaye, V P; Lodha, G S; Gowri Sankar, B; Kant, C

    2014-01-01

    The X-ray lithography beamline on Indus-2 is now operational, with two modes of operation. With a pair of X-ray mirrors it is possible to tune the energy spectrum between 1 and 20 keV with a controlled spectral bandwidth. In its 'no optics' mode, hard X-rays up to 40 keV are available. Features and performance of the beamline are presented along with some example structures. Structures fabricated include honeycomb structures in PMMA using a stainless steel stencil mask and a compound refractive X-ray lens using a polyimide-gold mask in SU-8. PMID:24365946

  5. The X-ray microscopy beamline UE46-PGM2 at BESSY

    NASA Astrophysics Data System (ADS)

    Follath, R.; Schmidt, J. S.; Weigand, M.; Fauth, K.

    2010-06-01

    The Max Planck Institute for Metal Physics in Stuttgart and the Helmholtz Center Berlin operate a soft X-ray microscopy beamline at the storage ring BESSY II. A collimated PGM serves as monochromator for a scanning X-ray microscope and a full field X-ray microscope at the helical undulator UE46. The selection between both instruments is accomplished via two switchable focusing mirrors. The scanning microscope (SM) is based on the ALS STXM microscope and fabricated by the ACCEL company. The full field microscope (FFM) is currently in operation at the U41-SGM beamline and will be relocated to its final location this year.

  6. High Precision Mechanical Components for Soft X-ray Beamline: Engineering Goal and Testing Results

    NASA Astrophysics Data System (ADS)

    Kaznacheyev, K. V.; Karunakaran, Ch.; Sitnikov, A.; Loken, D.; Warwick, T.; Nagy, M.; Hitchcock, A. P.

    2007-01-01

    As the emittance of SR rings approaches the diffraction limit for soft x-rays, one requires not only excellence in design and performance of the optical elements, but also precision and performance of mechanical components, such as mirror manipulators, monochromator scanners and exit slits. We will present simple but efficient solutions for the mechanical systems of this type, commonly encountered in soft x-ray beamlines. These solutions have been implemented and their performance evaluated with test results from the spectromicroscopy beamline at the Canadian Light Source.

  7. Data acquisition and control software for XRD beamline at Indus-2

    NASA Astrophysics Data System (ADS)

    Kane, Sanjeev R.; Garg, C. K.; Sinha, A. K.

    2010-06-01

    X-ray diffraction (XRD) beamline is under commissioning on Indus-2 synchrotron radiation facility. The experimental setup of XRD beamline consists of a six-circle diffractometer and various detector systems such as scintillation detector, ionization chamber and image plate. The diffractometer can be controlled via EIA232 serial interface or Ethernet. Standard data acquisition software with a graphical user interface has been developed using LabVIEW. A firm safety and error handling scheme is implemented for failsafe operation of the experimental station. This paper describes in detail the data acquisition and control software for the experimental station.

  8. Data acquisition and control software for XRD beamline at Indus-2

    SciTech Connect

    Kane, Sanjeev R.; Garg, C. K.; Sinha, A. K.

    2010-06-23

    X-ray diffraction (XRD) beamline is under commissioning on Indus-2 synchrotron radiation facility. The experimental setup of XRD beamline consists of a six-circle diffractometer and various detector systems such as scintillation detector, ionization chamber and image plate. The diffractometer can be controlled via EIA232 serial interface or Ethernet. Standard data acquisition software with a graphical user interface has been developed using LabVIEW. A firm safety and error handling scheme is implemented for failsafe operation of the experimental station. This paper describes in detail the data acquisition and control software for the experimental station.

  9. Positron beam optics for the 2D-ACAR spectrometer at the NEPOMUC beamline

    NASA Astrophysics Data System (ADS)

    Ceeh, H.; Weber, J. A.; Hugenschmidt, C.; Leitner, M.; Boni, P.

    2014-04-01

    In the last year a conventional 2D-ACAR spectrometer has been set up and brought to operation at TUM. Once the NEPOMUC beamline is extended to the new experimental hall at the research reactor FRM-II the conventional 2D-ACAR spectrometer will be upgraded with a second sample chamber in order to be integrated to the NEPOMUC beamline facility. This spectrometer will add a complete new quality to 2D-ACAR experiments as it allows to track the evolution of the electronic structure from the surface to the bulk. We present the design features of the positron beam optics and the sample environment.

  10. Design of the First Infrared Beamline at the Siam Photon Laboratory

    SciTech Connect

    Pattanasiriwisawa, W.; Songsiriritthigul, P.; Dumas, P.

    2010-06-23

    This report presents the optical design and optical simulations for the first infrared beamline at the Siam Photon Laboratory. The beamline collects the edge radiation and bending magnet radiation, producing from the BM4 bending magnet of the 1.2 GeV storage ring of the Siam Photon Source. The optical design is optimized for the far- to mid-infrared spectral range (4000-100 cm{sup -1}) for microspectroscopic applications. The optical performance has been examined by computer simulations.

  11. The 7BM beamline at the APS: a facility for time-resolved fluid dynamics measurements

    PubMed Central

    Kastengren, Alan; Powell, Christopher F.; Arms, Dohn; Dufresne, Eric M.; Gibson, Harold; Wang, Jin

    2012-01-01

    In recent years, X-ray radiography has been used to probe the internal structure of dense sprays with microsecond time resolution and a spatial resolution of 15 µm even in high-pressure environments. Recently, the 7BM beamline at the Advanced Photon Source (APS) has been commissioned to focus on the needs of X-ray spray radiography measurements. The spatial resolution and X-ray intensity at this beamline represent a significant improvement over previous time-resolved X-ray radiography measurements at the APS. PMID:22713903

  12. High-performance soft x-ray spectromicroscopy beamline at SSRF.

    PubMed

    Xue, Chaofan; Wang, Yong; Guo, Zhi; Wu, Yanqing; Zhen, Xiangjun; Chen, Min; Chen, Jiahua; Xue, Song; Peng, Zhongqi; Lu, Qipeng; Tai, Renzhong

    2010-10-01

    The Shanghai Synchrotron Radiation Facility (SSRF) is the first third-generation synchrotron facility in China and operated at an electron energy of 3.5 GeV. One of the seven beamlines in the first construction phase is devoted to soft x-ray spectromicroscopy and is equipped with an elliptically polarized undulator light source, a plane grating monochromator, and a scanning transmission x-ray microscope end station. Initial results reveal the high performance of this beamline, with an energy resolving power estimated to be over 10,000 at the argon L-edge and a spatial resolution better than 30 nm. PMID:21034086

  13. Optimization of the soft x-ray transmission microscopy beamline at the ALBA light source

    NASA Astrophysics Data System (ADS)

    Sorrentino, Andrea; Pereiro, Eva; Valcárcel, Ricardo; Ferrer, Salvador; Nicolas, Josep

    2013-09-01

    Mistral is the soft X-ray full field microscopy beamline at the ALBA light source. The beamline is designed to have large source acceptance and to provide constant magnification at the exit slit for photon energies between 270 and 2600 eV. The monochromator is a variation of the Petersen plane grating monochromator in which a variable line spacing grating is used to maintain the beam focused at the exit slit, independently of the fixed focus constant, and to cancel aberrations. We present the alignment strategy used to compensate errors of the optical elements, and report about the commissioning results.

  14. High-performance soft x-ray spectromicroscopy beamline at SSRF

    NASA Astrophysics Data System (ADS)

    Xue, Chaofan; Wang, Yong; Guo, Zhi; Wu, Yanqing; Zhen, Xiangjun; Chen, Min; Chen, Jiahua; Xue, Song; Peng, Zhongqi; Lu, Qipeng; Tai, Renzhong

    2010-10-01

    The Shanghai Synchrotron Radiation Facility (SSRF) is the first third-generation synchrotron facility in China and operated at an electron energy of 3.5 GeV. One of the seven beamlines in the first construction phase is devoted to soft x-ray spectromicroscopy and is equipped with an elliptically polarized undulator light source, a plane grating monochromator, and a scanning transmission x-ray microscope end station. Initial results reveal the high performance of this beamline, with an energy resolving power estimated to be over 10 000 at the argon L-edge and a spatial resolution better than 30 nm.

  15. New developments in high pressure x-ray spectroscopy beamline at High Pressure Collaborative Access Team

    SciTech Connect

    Xiao, Y. M. Chow, P.; Boman, G.; Bai, L. G.; Rod, E.; Bommannavar, A.; Kenney-Benson, C.; Sinogeikin, S.; Shen, G. Y.

    2015-07-15

    The 16 ID-D (Insertion Device - D station) beamline of the High Pressure Collaborative Access Team at the Advanced Photon Source is dedicated to high pressure research using X-ray spectroscopy techniques typically integrated with diamond anvil cells. The beamline provides X-rays of 4.5-37 keV, and current available techniques include X-ray emission spectroscopy, inelastic X-ray scattering, and nuclear resonant scattering. The recent developments include a canted undulator upgrade, 17-element analyzer array for inelastic X-ray scattering, and an emission spectrometer using a polycapillary half-lens. Recent development projects and future prospects are also discussed.

  16. Analysis of the optical design of the NSLS-II coherent hard x-ray beamline

    NASA Astrophysics Data System (ADS)

    Fluerasu, Andrei; Chubar, Oleg; Kaznatcheev, Konstantine; Baltser, Jana; Wiegart, Lutz; Evans-Lutterodt, Kenneth; Carlucci-Dayton, Mary; Berman, Lonny

    2011-09-01

    Ultra-low emittance third-generation synchrotron radiation sources such as the NSLS-II offer excellent opportunities for the development of experimental techniques exploiting x-ray coherence. Coherent light scattered by a heterogeneous sample produces a speckle pattern characteristic for the specific arrangement of the scatterers. This may vary over time, and the resultant intensity fluctuations can be measured and analyzed to provide information about the sample dynamics. X-ray photon correlation spectroscopy (XPCS) extends the capability of dynamic light scattering to opaque and turbid samples and extends the measurements of time evolution to nanometer length scales. As a consequence XPCS became crucial in the study of dynamics in systems including, but not being limited to, colloids, polymers, complex fluids, surfaces and interfaces, phase ordering alloys, etc. In this paper we present the conceptual optical design and the theoretical performance of the Coherent Hard X-ray (CHX) beamline at NSLS-II, dedicated to XPCS and other coherent scattering techniques. For the optical design of this beamline, there is a tradeoff between the coherence needed to distinguish individual speckles and the phase acceptance (high intensity) required to measure fast dynamics with an adequate signal-to-noise level. As XPCS is a "photon hungry" technique, the beamline optimization requires maximizing the signal-to-noise ratio of the measured intensity-intensity autocorrelation function. The degree of coherence, as measured by a two-slit (Young) experiment, is used to characterize the speckle pattern visibilities. The beamline optimization strategy consists of maximization of the on-sample intensity while keeping the degree of coherence within the 0.1-0.5 range. The resulted design deviates substantially from an ad-hoc modification of a hard x-ray beamline for XPCS measurements. The CHX beamline will permit studies of complex systems and measurements of bulk dynamics down to the

  17. Analysis of the optical design of the NSLS-II Coherent Hard X-ray beamline

    SciTech Connect

    Fluerasu A.; Chubar, O.; Kaznatcheev, K.; Baltser, J.; Wiegart, Lutz; Evans-Lutterodt, K.; Carlucci-Dayton, M.; Berman, L.

    2011-08-21

    Ultra-low emittance third-generation synchrotron radiation sources such as the NSLS-II offer excellent opportunities for the development of experimental techniques exploiting x-ray coherence. Coherent light scattered by a heterogeneous sample produces a speckle pattern characteristic for the specific arrangement of the scatterers. This may vary over time, and the resultant intensity fluctuations can be measured and analyzed to provide information about the sample dynamics. X-ray photon correlation spectroscopy (XPCS) extends the capability of dynamic light scattering to opaque and turbid samples and extends the measurements of time evolution to nanometer length scales. As a consequence XPCS became crucial in the study of dynamics in systems including, but not being limited to, colloids, polymers, complex fluids, surfaces and interfaces, phase ordering alloys, etc. In this paper we present the conceptual optical design and the theoretical performance of the Coherent Hard X-ray (CHX) beamline at NSLS-II, dedicated to XPCS and other coherent scattering techniques. For the optical design of this beamline, there is a tradeoff between the coherence needed to distinguish individual speckles and the phase acceptance (high intensity) required to measure fast dynamics with an adequate signal-to-noise level. As XPCS is a 'photon hungry' technique, the beamline optimization requires maximizing the signal-to-noise ratio of the measured intensity-intensity autocorrelation function. The degree of coherence, as measured by a two-slit (Young) experiment, is used to characterize the speckle pattern visibilities. The beamline optimization strategy consists of maximization of the on-sample intensity while keeping the degree of coherence within the 0.1-0.5 range. The resulted design deviates substantially from an ad-hoc modification of a hard x-ray beamline for XPCS measurements. The CHX beamline will permit studies of complex systems and measurements of bulk dynamics down to the

  18. The New Structural Materials Science Beamlines BL8A and 8B at Photon Factory

    SciTech Connect

    Nakao, A.; Sugiyama, H.; Koyama, A.; Watanabe, K.

    2010-06-23

    BL8A and 8B are new beamlines for structural materials science at Photon Factory. The primary characteristics of both beamlines are similar. The incident beam is monochromatized by the Si(111) double-flat crystal monochromator and focused at the sample position by a Rh-coated bent cylindrical quartz mirror. The Weissenberg-camera-type imaging-plate (IP) diffractometers were installed. The X-ray diffraction experiments for structural studies of strongly correlated materials, such as transition metals, molecular conductors, endohedral fullerenes, nano-materials, etc, are conducted at these stations.

  19. APS beamline standard components handbook, Version 1.3. Revision 1

    SciTech Connect

    Hahn, U.; Shu, D.; Kuzay, T.M.

    1993-02-01

    This Handbook in its current version (1.3) contains descriptions, specifications, and preliminary engineering design drawings for many of the standard components. The design status and schedules have been provided wherever possible. In the near future, the APS plans to update engineering drawings of identified standard beamline components and complete the Handbook. The completed version of this Handbook will become available to both the CATs and potential vendors. Use of standard components should result in major cost reductions for CATs in the areas of beamline design and construction.

  20. Time-resolved X-ray powder diffraction on a three-way catalyst at the GILDA beamline.

    PubMed

    Martorana, A; Deganello, G; Longo, A; Deganello, F; Liotta, L; Macaluso, A; Pantaleo, G; Balerna, A; Meneghini, C; Mobilio, S

    2003-03-01

    Time-resolved X-ray diffraction experiments carried out at the beamline BM08-GILDA of ESRF allowed a study of the structural modifications taking place in a Pt/ceria-zirconia catalyst while the CO oxidation reaction was in progress. The capillary tube in which the sample is stored acts effectively as a chemical microreactor that ensures homogeneity of the sample treatments and minimization of diffusion effects. During the flowing of the reactant CO/He mixture, the investigated catalyst undergoes a fast Ce(IV)-Ce(III) partial reduction that involves the release of one O atom for every two reduced Ce cations. Because Ce(III) has a larger ionic radius than Ce(IV), the structural modification produces an increase of the lattice constant of the ceria-zirconia mixed oxide, and this increase is monitored by the translating imaging-plate device implemented at GILDA. The CO(2) resulting from the oxidation of the fluxed CO is monitored by a quadrupole mass spectrometer during the recording of the time-resolved X-ray diffraction pattern. The chemical and structural information was combined to show that the CO(2) yield is nearly constant until the catalytic system can provide oxygen for the reaction, while the structural rearrangement of the catalyst is delayed with respect to the switching on of the CO/He flux. After this induction time, during which CO(2) is produced with no structural modification of the catalyst, a fast increase of the lattice constant takes place. PMID:12606797

  1. Diamond monochromators for APS undulator-A beamlines

    SciTech Connect

    Blasdell, R.C.; Assoufid, L.A.; Mills, D.M.

    1995-09-01

    There has been considerable interest in the use of diamonds in high heat load monochromators (HHLMs) in the last several years. The superb thermal and mechanical properties of single crystal diamonds serve to minimize distortions caused by a given thermal load, while the low x-ray absorption cross-section reduces both the total power deposited in the crystal as well as the peak (volumetric) power density. The primary obstacle for the widespread use of diamonds at present is a lack of ready availability of perfect single crystals of the desired size and orientation. Although it is possible to obtain near-perfect natural diamonds of the size and orientation required for use on an undulator beamline, the selection process is generally one of trial and error. Near perfect synthetic diamonds can currently be obtained in the minimum necessary size (typically 4-5 mm on a side). A collaborative agreement has been made between the staff of the Advanced Photon Source (APS), the European Synchrotron Radiation Facility (ESRF), and the Super Photon Ring-8 GeV (SPring-8) to explore the use of diamonds as high heat load monochromators and is on-going. One of the avenues of research is to push for improved perfection and size of synthetic diamonds. Sumitomo Electric Corporation of Japan has agreed to work with staff from SPring-8 to grow [100] oriented perfect single crystal diamonds of 10 x 10 x 1 mm{sup 3} size by 1996/1997 (from which one could also cut pieces with the large face parallel to the (111) planes). They have taken the first step in producing an essentially perfect 4 x 4 x 1 mm{sup 3} type II diamond with less than 5 {mu}rad (1 arc second) strain (measured over the entire surface). The authors believe progress in the production of synthetic diamonds, as well as improvement in ties with suppliers of natural diamonds, should make available a relatively large number of high quality diamonds of moderate size within the next several years.

  2. Correlated Single-Crystal Electronic Absorption Spectroscopy and X-ray Crystallography at NSLS Beamline X26-C

    SciTech Connect

    A Orville; R Buono; M Cowan; A Heroux; G Shea-McCarthy; D Schneider; J Skinner; M Skinner; D Stoner-Ma; R Sweet

    2011-12-31

    The research philosophy and new capabilities installed at NSLS beamline X26-C to support electronic absorption and Raman spectroscopies coupled with X-ray diffraction are reviewed. This beamline is dedicated full time to multidisciplinary studies with goals that include revealing the relationship between the electronic and atomic structures in macromolecules. The beamline instrumentation has been fully integrated such that optical absorption spectra and X-ray diffraction images are interlaced. Therefore, optical changes induced by X-ray exposure can be correlated with X-ray diffraction data collection. The installation of Raman spectroscopy into the beamline is also briefly reviewed. Data are now routinely generated almost simultaneously from three complementary types of experiments from the same sample. The beamline is available now to the NSLS general user population.

  3. Correlated single-crystal electronic absorption spectroscopy and X-ray crystallography at NSLS beamline X26-C

    SciTech Connect

    Orville, A.M.; Buono, R.; Cowan, M.; Heroux, A.; Shea-McCarthy, G.; Schneider, D. K.; Skinner, J. M.; Skinner, M. J.; Stoner-Ma, D.; Sweet, R. M.

    2011-05-01

    The research philosophy and new capabilities installed at NSLS beamline X26-C to support electronic absorption and Raman spectroscopies coupled with X-ray diffraction are reviewed. This beamline is dedicated full time to multidisciplinary studies with goals that include revealing the relationship between the electronic and atomic structures in macromolecules. The beamline instrumentation has been fully integrated such that optical absorption spectra and X-ray diffraction images are interlaced. Therefore, optical changes induced by X-ray exposure can be correlated with X-ray diffraction data collection. The installation of Raman spectroscopy into the beamline is also briefly reviewed. Data are now routinely generated almost simultaneously from three complementary types of experiments from the same sample. The beamline is available now to the NSLS general user population.

  4. Note: Construction of x-ray scattering and x-ray absorption fine structure beamline at the Pohang Light Source

    SciTech Connect

    Lee, Ik-Jae; Yu, Chung-Jong; Yun, Young-Duck; Lee, Chae-Soon; Seo, In Deuk; Kim, Hyo-Yun; Lee, Woul-Woo; Chae, Keun Hwa

    2010-02-15

    A new hard x-ray beamline, 10B KIST-PAL beamline (BL10B), has been designed and constructed at the Pohang Light Source (PLS) in Korea. The beamline, operated by Pohang Accelerator Laboratory-Korean Institute of Science and Technology consortium, is dedicated to x-ray scattering (XRS) and x-ray absorption fine structure (XAFS) experiments. X rays with photon energies from 4.0 to 16.0 keV are delivered to the experimental station passing a collimating mirror, a fixed-exit double-crystal Si(111) monochromator, and a toroidal mirror. Basic experimental equipments for XAFS measurement, a high resolution diffractometry, an image plate detector system, and a hot stage have been prepared for the station. From our initial commissioning and performance testing of the beamline, it is observed that BL10B beamline can perform XRS and XAFS measurements successfully.

  5. Correlated single-crystal electronic absorption spectroscopy and X-ray crystallography at NSLS beamline X26-C

    PubMed Central

    Orville, Allen M.; Buono, Richard; Cowan, Matt; Héroux, Annie; Shea-McCarthy, Grace; Schneider, Dieter K.; Skinner, John M.; Skinner, Michael J.; Stoner-Ma, Deborah; Sweet, Robert M.

    2011-01-01

    The research philosophy and new capabilities installed at NSLS beamline X26-C to support electronic absorption and Raman spectroscopies coupled with X-ray diffraction are reviewed. This beamline is dedicated full time to multidisciplinary studies with goals that include revealing the relationship between the electronic and atomic structures in macromolecules. The beamline instrumentation has been fully integrated such that optical absorption spectra and X-ray diffraction images are interlaced. Therefore, optical changes induced by X-ray exposure can be correlated with X-ray diffraction data collection. The installation of Raman spectroscopy into the beamline is also briefly reviewed. Data are now routinely generated almost simultaneously from three complementary types of experiments from the same sample. The beamline is available now to the NSLS general user population. PMID:21525643

  6. Wavefront propagation simulations for a UV/soft x-ray beamline: Electron Spectro-Microscopy beamline at NSLS-II

    NASA Astrophysics Data System (ADS)

    Canestrari, N.; Bisogni, V.; Walter, A.; Zhu, Y.; Dvorak, J.; Vescovo, E.; Chubar, O.

    2014-09-01

    A "source-to-sample" wavefront propagation analysis of the Electron Spectro-Microscopy (ESM) UV / soft X-ray beamline, which is under construction at the National Synchrotron Light Source II (NSLS-II) in the Brookhaven National Laboratory, has been conducted. All elements of the beamline - insertion device, mirrors, variable-line-spacing gratings and slits - are included in the simulations. Radiation intensity distributions at the sample position are displayed for representative photon energies in the UV range (20 - 100 eV) where diffraction effects are strong. The finite acceptance of the refocusing mirrors is the dominating factor limiting the spatial resolution at the sample (by ~3 μm at 20 eV). Absolute estimates of the radiation flux and energy resolution at the sample are also obtained from the electromagnetic calculations. The analysis of the propagated UV range undulator radiation at different deflection parameter values demonstrates that within the beamline angular acceptance a slightly "red-shifted" radiation provides higher flux at the sample and better energy resolution compared to the on-axis resonant radiation of the fundamental harmonic.

  7. Status of the SG-III solid state laser project

    NASA Astrophysics Data System (ADS)

    Peng, Hansheng; Zhang, Xiao Min; Wei, XiaoFeng; Zheng, Wanguo; Jing, Feng; Sui, Zhan; Fan, Dianyuan; Lin, Zunqi

    1999-07-01

    High power solid state laser technologies for application to inertial confinement fusion have been developed over the past three decades in China. The XG-1 laser facility was built in 1984 and upgraded into XG-II in 1993. The SG-1 was completed in 1985 and the upgrade into SG-II will be finished in a few months. As the next step, the SG-III laser facility has been proposed to produce 60-kJ blue light for ICF target physics experiments and is one being conceptually designed. A preliminary baseline design suggest that he SG- III be a 64-beam facility with an output beam size of 25 cm X 25cm. The main amplifier column of 4 high by 2 wide has been chosen as a module. New laser technologies, including multipass amplification, large aperture plasma electrode switches, fast growth of KDP, laser glass with fewer platinum grains, Ce-doped quartz long flash lamps, capacitors with higher energy density, Ce-doped quartz long flash lamps, capacitors with higher energy density and precision manufacturing technique of large optical components have been developed to meet the requirements of the SG-III Project. In addition, numerical simulations are being conducted to optimize the optical design of the facility. The technical integration line with a 4 X 2 segmented aperture array of the amplifiers as a prototype beamline of the SG-III has been scheduled for the next few years.

  8. Characterization of the high-energy neutron beam of the PRISMA beamline using a diamond detector

    NASA Astrophysics Data System (ADS)

    Cazzaniga, C.; Frost, C. D.; Minniti, T.; Schooneveld, E.; Perelli Cippo, E.; Tardocchi, M.; Rebai, M.; Gorini, G.

    2016-07-01

    The high-energy neutron component (En > 10 MeV) of the neutron spectrum of PRISMA, a beam-line at the ISIS spallation source, has been characterized for the first time. Neutron measurements using a Single-crystal Diamond Detector at a short-pulse source are obtained by a combination of pulse height and time of flight analysis. An XY scan provides a 2D map of the high-energy neutron beam which has a diameter of about 40 mm. The high neutron flux, that has been found to be (3.8 ± 0.7) · 105 cm‑2s‑1 for En > 10 MeV in the centre, opens up for a possible application of the beam-line as a high-energy neutron irradiation position. Results are of interest for the development of the ChipIR beam-line, which will feature an atmospheric-like neutron spectrum for chip irradiation experiment. Furthermore, these results demonstrate that diamond detectors can be used at spallation sources to investigate the transport of high-energy neutrons down instruments which is of interest in general to designers as high-energy neutrons are a source of background in thermal beamlines.

  9. Thermal management for LLNL/UC/SSRL bending magnet beamline VIII at Stanford Synchrotron Radiation Laboratory

    SciTech Connect

    Berglin, E.J.; Younger, F.C.

    1986-05-01

    All the important heat loads on the elements of Beamline VIII are cataloged. The principal elements are identified and their heat loads tabulated for various loading scenarios. The expected heat loads are those from normal operations including the anticipated performance improvements planned for the SPEAR ring and from abnormal operations due to positional perturbations of the electron beam. (LEW)

  10. Characteristics and performance of the Los Alamos VUV beamline at the NSLS

    NASA Astrophysics Data System (ADS)

    Bartlett, R. J.; Trela, W. J.; Michaud, F. D.; Southworth, S. H.; Alkire, R. W.; Roy, P.; Rothe, R.; Walsh, P. J.; Shinn, N.

    1988-04-01

    We describe the design and performance of the Los Alamos VUV synchrotron radiation beamline, U3C, on the VUV ring of the National Synchrotron Light Source at Brookhaven National Laboratory. The beamline uses separate function optics to collect and focus the horizontally and vertically diverging beam. The monochromator is a grazing incidence Rowland circle instrument of the extended grasshopper design (ERG). A postmonochromator refocusing mirror is used to focus or collimate the diverging beam from the monochromator. The beamline control and diagnostics systems are also discussed. Particular emphasis in the design has been placed on the reduction of stray and harmonic light. Higher order light is reduced by a grazing angle mirror low pass filter installed immediately downstream from the monochromator while stray light is reduced through the use of baffles and thin film filters. Also included in the line is a differential pumping section that permits gas phase and other experiments requiring pressures in the 10 -5 to 10 -4 Torr range to be coupled to the beamline.

  11. Neutrinos from the NuMI beamline in the MiniBooNE detector

    SciTech Connect

    Aguilar-Arevalo, Alexis A.

    2006-07-11

    With the startup of the NuMI beamline early in 2005, the MiniBooNE detector has the unique opportunity to be the first user of an off-axis neutrino beam (110 mrad off-axis). MiniBooNE is assembling a rich sample of neutrino interactions from this source.

  12. Properties of ion implanted Ti-6Al-4V processed using beamline and PSII techniques

    SciTech Connect

    Walter, K.C.; Woodring, J.S.; Nastasi, M.; Munson, C.M.; Williams, J.M.; Poker, D.B.

    1996-12-31

    The surface of Ti-6Al-4V (Ti64) alloy has been modified using beamline implantation of boron. In separate experiments, Ti64 has been implanted with nitrogen using a plasma source ion implantation (PSII) technique utilizing either ammonia (NH{sub 3}), nitrogen (N{sub 2}), or their combinations as the source of nitrogen ions. Beamline experiments have shown the hardness of the N-implanted surface saturates at a dose level of {approximately} 4 {times} 10{sup 17} at/cm{sup 2} at {approximately} 10 GPa. The present work makes comparisons of hardness and tribological tests of (1) B implantation using beamline techniques, and (2) N implanted samples using ammonia and/or nitrogen gas in a PSII process. The results show that PSII using N{sub 2} or NH{sub 3} gives similar hardness as N implantation using a beamline process. The presence of H in the Ti alloy surface does not affect the hardness of the implanted surface. Boron implantation increased the surface hardness by as much as 2.5x at the highest dose level. Wear testing by a pin-on-disk method indicated that nitrogen implantation reduced the wear rate by as much as 120x, and boron implantation reduced the wear rate by 6.5x. Increased wear resistance was accompanied by a decreased coefficient of friction.

  13. Mass and charge overlaps in beamline implantation into compound semiconductor materials

    SciTech Connect

    Current, M. I.; Eddy, R.; Hudak, C.; Serfass, J.; Mount, G.

    2012-11-06

    Mass overlaps occurring as a result of extraction of ions from an arc discharge and gas collisions, producing molecular break up and charge exchange in the accelerator beamline, are examined for ion implantation into compound semiconductors. The effects of the choice of plasma gas elements for Be{sup +} implants are examined as an example.

  14. Mass and charge overlaps in beamline implantation into compound semiconductor materials

    NASA Astrophysics Data System (ADS)

    Current, M. I.; Eddy, R.; Hudak, C.; Serfass, J.; Mount, G.

    2012-11-01

    Mass overlaps occurring as a result of extraction of ions from an arc discharge and gas collisions, producing molecular break up and charge exchange in the accelerator beamline, are examined for ion implantation into compound semiconductors. The effects of the choice of plasma gas elements for Be+ implants are examined as an example.

  15. A dedicated micro-CT beamline for the Australian Synchrotron and the Remote-CT project

    NASA Astrophysics Data System (ADS)

    Mayo, S. C.; Gureyev, T. E.; Nesterets, Y. I.; Thompson, D. A.; Siu, K. K. W.; Wallwork, K.

    2013-10-01

    A dedicated micro-CT beamline is planned for the Australian Synchrotron which will extend the synchrotron's imaging and tomography capability down to the smaller scale, incorporating phase-contrast and absorption-contrast, and an additional focussing-based mode for high-resolution. The beamline will use multi-layer mirror monochromators for enhanced flux, and will focus particularly on dynamic and high throughput studies in both monochromatic and pink-beam mode. Together with the existing Imaging and Medical beamline, this beamline will produce numerous large datasets of 10 GB or more, providing a significant data-processing challenge. The Remote-CT project addresses this by combining the "MASSIVE" supercomputing GPU cluster with XLI / X-TRACT software, developed at CSIRO. This software has extensive functionality for both processing and simulation of absorption and phase-contrast tomography data and has now been modified for parallel operation on a GPU cluster to take maximum advantage of the speed-up this enables.

  16. The Structural Biology Center 19ID undulator beamline: facility specifications and protein crystallographic results

    PubMed Central

    Rosenbaum, Gerd; Alkire, Randy W.; Evans, Gwyndaf; Rotella, Frank J.; Lazarski, Krzystof; Zhang, Rong-Guang; Ginell, Stephan L.; Duke, Norma; Naday, Istvan; Lazarz, Jack; Molitsky, Michael J.; Keefe, Lisa; Gonczy, John; Rock, Larry; Sanishvili, Ruslan; Walsh, Martin A.; Westbrook, Edwin; Joachimiak, Andrzej

    2008-01-01

    The 19ID undulator beamline of the Structure Biology Center has been designed and built to take full advantage of the high flux, brilliance and quality of X-ray beams delivered by the Advanced Photon Source. The beamline optics are capable of delivering monochromatic X-rays with photon energies from 3.5 to 20 keV (3.5–0.6 Å wavelength) with fluxes up to 8–18 × 1012 photons s−1 (depending on photon energy) onto cryogenically cooled crystal samples. The size of the beam (full width at half-maximum) at the sample position can be varied from 2.2 mm × 1.0 mm (horizontal × vertical, unfocused) to 0.083 mm × 0.020 mm in its fully focused configuration. Specimen-to-detector distances of between 100 mm and 1500 mm can be used. The high flexibility, inherent in the design of the optics, coupled with a κ-geometry goniometer and beamline control software allows optimal strategies to be adopted in protein crystallographic experiments, thus maximizing the chances of their success. A large-area mosaic 3 × 3 CCD detector allows high-quality diffraction data to be measured rapidly to the crystal diffraction limits. The beamline layout and the X-ray optical and endstation components are described in detail, and the results of representative crystallographic experiments are presented. PMID:16371706

  17. Investigation of collisional effects within the bending magnet region of a DIII-D neutral beamline

    SciTech Connect

    Kessler, D.N.; Hong, R.; Kellman, D.H.

    1993-10-01

    The region between the pole faces of the DIII-D neutral beamline residual ion bending magnets is an area of transient high gas pressure which may cause beam defocusing and increased heating of beamline internal components due to collisional effects. An investigation of these effects helps in understanding residual ion trajectories and in providing information for studying in the beamline capability for operation with increased pulse duration. Examination of collisional effects, and of the possible existence of space charge blow-up, was carried out by injecting deuterium gas into the region between the magnet pole faces with rates varying from 0 to 18 torr-{ell}/sec. Thermocouple and waterflow calorimetry data were taken to measure the beamline component heating and beam powder deposition on the magnet pole shields, magnet louvers, ion dump, beam collimators, and calorimeter. Data was also taken at gas flow rates varying from 0 to 25 torr-{ell}/sec into the neutralizer cell and is compared with the magnet region gas injection data obtained. Results show that both collisional effects and space charge blow-up play a role in magnet region component heating and that neutralizer gas flow sufficiently reduces component heating without incurring unacceptable power losses through collisional effects.

  18. Partially coherent wavefront propagation simulations for inelastic x-ray scattering beamline including crystal optics

    NASA Astrophysics Data System (ADS)

    Suvorov, Alexey; Cai, Yong Q.; Sutter, John P.; Chubar, Oleg

    2014-09-01

    Up to now simulation of perfect crystal optics in the "Synchrotron Radiation Workshop" (SRW) wave-optics computer code was not available, thus hindering the accurate modelling of synchrotron radiation beamlines containing optical components with multiple-crystal arrangements, such as double-crystal monochromators and high-energy-resolution monochromators. A new module has been developed for SRW for calculating dynamical diffraction from a perfect crystal in the Bragg case. We demonstrate its successful application to the modelling of partially-coherent undulator radiation propagating through the Inelastic X-ray Scattering (IXS) beamline of the National Synchrotron Light Source II (NSLS-II) at Brookhaven National Laboratory. The IXS beamline contains a double-crystal and a multiple-crystal highenergy- resolution monochromator, as well as complex optics such as compound refractive lenses and Kirkpatrick-Baez mirrors for the X-ray beam transport and shaping, which makes it an excellent case for benchmarking the new functionalities of the updated SRW codes. As a photon-hungry experimental technique, this case study for the IXS beamline is particularly valuable as it provides an accurate evaluation of the photon flux at the sample position, using the most advanced simulation methods and taking into account parameters of the electron beam, details of undulator source, and the crystal optics.

  19. Protein crystallography beamline (PX-BL21) at Indus-2 synchrotron.

    PubMed

    Kumar, Ashwani; Ghosh, Biplab; Poswal, H K; Pandey, K K; Hosur, M V; Dwivedi, Abhilash; Makde, Ravindra D; Sharma, Surinder M

    2016-03-01

    The protein crystallography beamline (PX-BL21), installed at the 1.5 T bending-magnet port at the Indian synchrotron (Indus-2), is now available to users. The beamline can be used for X-ray diffraction measurements on a single crystal of macromolecules such as proteins, nucleic acids and their complexes. PX-BL21 has a working energy range of 5-20 keV for accessing the absorption edges of heavy elements commonly used for phasing. A double-crystal monochromator [Si(111) and Si(220)] and a pair of rhodium-coated X-ray mirrors are used for beam monochromatization and manipulation, respectively. This beamline is equipped with a single-axis goniometer, Rayonix MX225 CCD detector, fluorescence detector, cryogenic sample cooler and automated sample changer. Additional user facilities include a workstation for on-site data processing and a biochemistry laboratory for sample preparation. In this article the beamline, other facilities and some recent scientific results are briefly described. PMID:26917153

  20. White-beam X-ray radioscopy and tomography with simultaneous diffraction at the EDDI beamline.

    PubMed

    García-Moreno, F; Jiménez, C; Kamm, P H; Klaus, M; Wagener, G; Banhart, J; Genzel, Ch

    2013-09-01

    A set-up for simultaneous imaging and diffraction that yields radiograms with up to 200 frames per second and 5.6 µm effective pixel size is presented. Tomograms and diffractograms are acquired together in 10 s. Two examples illustrate the attractiveness of combining these methods at the EDDI beamline for in situ studies. PMID:23955047

  1. Design and Performance of the Compact YAG Imaging System for Diagnostics at GMCA Beamlines at APS

    SciTech Connect

    Xu Shenglan; Fischetti, Robert F.; Benn, Richard; Corcoran, Stephen

    2007-01-19

    A compact YAG (Chromium Doped Yttrium Aluminum Garnet - Cr4+:YAG) imaging system has been designed as a diagnostic tool for monochromatic x-rays emanating from the first 'Hard' x-ray dual-canted undulator at the Advanced Photon Source at Argonne National Laboratory. This imaging system consists of a flat YAG crystal, right angle prism/mirror, video camera and monitor. A flat YAG crystal with a diameter of 10 mm has been installed in vacuum and positioned downstream of the monochromator of the insertion device beamline. Another 20 mm diameter YAG crystal has been installed in vacuum after the horizontal deflecting mirrors of the second insertion device beamline. CCD cameras are mounted in air close to the window of the vacuum ports to image the fluorescence of the YAG crystals. An additional 25 mm diameter YAG crystal has been used for K-B (Kirkpatrick-Baez) mirror focusing and beamline alignment. These YAG imaging systems have greatly facilitated beamline commissioning as well as sample alignment to the x-ray beam in the macromolecular crystallography endstation. An overview of the optics design, mechanical design and the performance of these devices will be presented in the paper.

  2. A comparison of three different ray trace programs for x-ray and infrared synchrotron beamline designs

    SciTech Connect

    Irick, S.C.; Jung, C.R.

    1997-07-01

    There are a number of ray trace programs currently used for the design of synchrotron beamlines. While several of these programs have been written and used mostly within the programmer`s institution, many have also been available to the general public. This paper discusses three such programs. One is a commercial product oriented for the general optical designer (not specifically for synchrotron beamlines). One is designed for synchrotron beamlines and is free with restricted availability. Finally, one is designed for synchrotron beamlines and is used primarily in one institution. The wealth of information from general optical materials and components catalogs is readily available in the commercial program for general optical designs. This makes the design of an infrared beamline easier from the standpoint of component selection. However, this program is not easily configured for synchrotron beamline designs, particularly for a bending magnet source. The synchrotron ray trace programs offer a variety of sources, but generally are not as easy to use from the standpoint of the user interface. This paper shows ray traces of the same beamline Optikwerks, SHADOW, and RAY, and compares the results.

  3. 7-GeV advanced photon source beamline initiative: Conceptual design report

    SciTech Connect

    Not Available

    1993-05-01

    The DOE is building a new generation 6-7 GeV Synchrotron Radiation Source known as the Advanced Photon Source (APS) at Argonne National Laboratory. This facility, to be completed in FY 1996, can provide 70 x-ray sources of unprecedented brightness to meet the research needs of virtually all scientific disciplines and numerous technologies. The technological research capability of the APS in the areas of energy, communications and health will enable a new partnership between the DOE and US industry. Current funding for the APS will complete the current phase of construction so that scientists can begin their applications in FY 1996. Comprehensive utilization of the unique properties of APS beams will enable cutting-edge research not currently possible. It is now appropriate to plan to construct additional radiation sources and beamline standard components to meet the excess demands of the APS users. In this APS Beamline Initiative, 2.5-m-long insertion-device x-ray sources will be built on four straight sections of the APS storage ring, and an additional four bending-magnet sources will also be put in use. The front ends for these eight x-ray sources will be built to contain and safeguard access to these bright x-ray beams. In addition, funds will be provided to build standard beamline components to meet scientific and technological research demands of the Collaborative Access Teams. The Conceptual Design Report (CDR) for the APS Beamline Initiative describes the scope of all the above technical and conventional construction and provides a detailed cost and schedule for these activities. The document also describes the preconstruction R&D plans for the Beamline Initiative activities and provides the cost estimates for the required R&D.

  4. Nanoscopium: a Scanning Hard X-ray Nanoprobe Beamline at Synchrotron Soleil

    NASA Astrophysics Data System (ADS)

    Somogyi, A.; Polack, F.; Moreno, T.

    2010-06-01

    Nanoscopium is the single scanning hard X-ray nano-probe beamline planned at SOLEIL. This ˜155 m long beamline will fully exploit the high brilliance and coherence characteristics of the X-ray beam both for diffraction limited focusing and for contrast formation. It will offer the most advanced imaging techniques in multimodal mode and will be a research tool for a wide user community working in the fields of earth-, environmental-, and life-sciences. The different μ-μnano-probe techniques offered by the beamline will permit elemental mapping at trace (ppm) levels (scanning XRF), speciation mapping (XANES), phase gradient mapping (scanning differential phase contrast), and density-contrast based imaging of internal structures (coherent diffraction imaging) in the 30 nm to 1 μm spatial resolution range, also in "in situ conditions". Nanoscopium will cover the 5-20 keV energy range. The stability of the nanobeam will be ensured by horizontally reflecting beamline optics (a sagitally and a tangentially pre-focusing mirror, horizontally reflecting monochromators) in front of the overfilled secondary source. Trade-off between high energy resolution (ΔE/E˜10-4) and high flux (1011 ph/s with ΔE/E˜10-2) will be achieved by two interchangeable monochromators (a double crystal and a double multilayer one). KB mirror and FZP lenses will be used as focusing devices. The beamline is in the design and construction phase. It is foreseen to be open for users at the beginning of 2013.

  5. Discerning total salt contents and surface humidity on building stone with a portable moisture meter (Protimeter) in the region of Petra (Jordan)

    NASA Astrophysics Data System (ADS)

    Gomez-Heras, M.; Wedekind, W.; Lopez-Arce, P.

    2012-04-01

    Water and moisture are some of the main decay agents of building stone and, in general of any stone structure. Several non-invasive methods are used to quantify moisture in building stone, many of them based on the fact that moist stone presents different electrical properties than dry stone. This is the case of resistance-based sensing equipment, such as "Protimeter" portable moisture meters. Although originally designed to measure moisture contents in wood, this sensing equipment is commonly used to measure the so-called "Wood Moisture Equivalent" (WME) in other building materials, such stone and mortar. However, this type of resistance-based sensors pose a degree of uncertainty, as there are other factors that modify electrical properties, such as porosity and salt content. When assessing the overall state of decay of a structure, it might not be crucial, in some cases, to discern between salt and water content: both high moisture levels and high salt content give high WME values, and both are usually related to areas with overall poor state of conservation and/or more prone to decay. However, discerning these two factors is crucial when trying to understand the dynamics of how some decay patterns are formed. This is the case of surface runoff in vertical façades and how it leads to the formation of alveoli and tafoni through salt weathering. Surface runoff and associated salt weathering are among the main decay processes found at the archaeological site of Petra (Jordan) and its understanding is of paramount importance for the conservation of this site. Some "Protimeter" sensors include a capacitance sensor in addition to the usual resistance sensing pins, which allows to measure sub-surface electrical properties. This paper presents results on how the combination of these two measurement modes could be used to discern if high WME values are caused by high surface humidity or by high salt contents in the context of Surface runoff and associated salt weathering

  6. MASSIF-1: a beamline dedicated to the fully automatic characterization and data collection from crystals of biological macromolecules.

    PubMed

    Bowler, Matthew W; Nurizzo, Didier; Barrett, Ray; Beteva, Antonia; Bodin, Marjolaine; Caserotto, Hugo; Delagenière, Solange; Dobias, Fabian; Flot, David; Giraud, Thierry; Guichard, Nicolas; Guijarro, Mattias; Lentini, Mario; Leonard, Gordon A; McSweeney, Sean; Oskarsson, Marcus; Schmidt, Werner; Snigirev, Anatoli; von Stetten, David; Surr, John; Svensson, Olof; Theveneau, Pascal; Mueller-Dieckmann, Christoph

    2015-11-01

    MASSIF-1 (ID30A-1) is an ESRF undulator beamline operating at a fixed wavelength of 0.969 Å (12.8 keV) that is dedicated to the completely automatic characterization of and data collection from crystals of biological macromolecules. The first of the ESRF Upgrade MASSIF beamlines to be commissioned, it has been open since September 2014, providing a unique automated data collection service to academic and industrial users. Here, the beamline characteristics and details of the new service are outlined. PMID:26524320

  7. MASSIF-1: a beamline dedicated to the fully automatic characterization and data collection from crystals of biological macromolecules

    PubMed Central

    Bowler, Matthew W.; Nurizzo, Didier; Barrett, Ray; Beteva, Antonia; Bodin, Marjolaine; Caserotto, Hugo; Delagenière, Solange; Dobias, Fabian; Flot, David; Giraud, Thierry; Guichard, Nicolas; Guijarro, Mattias; Lentini, Mario; Leonard, Gordon A.; McSweeney, Sean; Oskarsson, Marcus; Schmidt, Werner; Snigirev, Anatoli; von Stetten, David; Surr, John; Svensson, Olof; Theveneau, Pascal; Mueller-Dieckmann, Christoph

    2015-01-01

    MASSIF-1 (ID30A-1) is an ESRF undulator beamline operating at a fixed wavelength of 0.969 Å (12.8 keV) that is dedicated to the completely automatic characterization of and data collection from crystals of biological macromolecules. The first of the ESRF Upgrade MASSIF beamlines to be commissioned, it has been open since September 2014, providing a unique automated data collection service to academic and industrial users. Here, the beamline characteristics and details of the new service are outlined. PMID:26524320

  8. Structure determination by multiple-wavelength anomalous dispersion (MAD) at the Pr L III edge

    PubMed Central

    Puehringer, Sandra; Hellmig, Michael; Liu, Sunbin; Weiss, Manfred S.; Wahl, Markus C.; Mueller, Uwe

    2012-01-01

    The use of longer X-ray wavelengths in macromolecular crystallography has grown significantly over the past few years. The main reason for this increased use of longer wavelengths has been to utilize the anomalous signal from sulfur, providing a means for the experimental phasing of native proteins. Here, another possible application of longer X-ray wavelengths is presented: MAD at the L III edges of various lanthanide compounds. A first experiment at the L III edge of Pr was conducted on HZB MX beamline BL14.2 and resulted in the successful structure determination of the C-terminal domain of a spliceosomal protein. This experiment demonstrates that L III edges of lanthanides constitute potentially attractive targets for long-wavelength MAD experiments. PMID:22869138

  9. Preliminary Commissioning and Performance of the Soft X-ray Micro-characterization Beamline at the Canadian Light Source

    SciTech Connect

    Hu, Y. F.; Coulthard, I.; Chevrier, D.; Wright, G.; Igarashi, R.; Sitnikov, A.; Yates, B. W.; Hallin, E. L.; Sham, T. K.; Reininger, R.

    2010-06-23

    The Soft X-ray Micro-characterization Beamline (SXRMB) is a medium energy, bending magnet based beamline, designed to cover an energy range of 1.7-10 keV using two sets of crystals--InSb(111) and Si(111). The design goal is to deliver a flux of 2x10{sup 11} photons sec{sup -1}/100 mA with a resolution up to 10,000 for X-ray Absorption Spectroscopy. A KB mirror stage is designed to provide microprobe capability, with a spot size of 10x10 {mu}m{sup 2} and a flux of >10{sup 9} at the microprobe station. The beamline has been in the commissioning phase since 2008, and access to the X-ray absorption endstation is now open to general users. The optical commissioning and performance of the beamline is presented with some early experimental results.

  10. National Synchrotron Light Source user`s manual: Guide to the VUV and x-ray beamlines. Fifth edition

    SciTech Connect

    Gmuer, N.F.

    1993-04-01

    The success of the National Synchrotron Light Source is based, in large part, on the size of the user community and the diversity of the scientific and technical disciplines represented by these users. As evidence of this success, the VUV Ring has just celebrated its 10th anniversary and the X-ray Ring will do the same in 1995. In order to enhance this success, the NSLS User`s Manual: Guide to the VUV and X-Ray Beamlines - Fifth Edition, is being published. This Manual presents to the scientific community-at-large the current and projected architecture, capabilities and research programs of the various VUV and X-ray beamlines. Also detailed is the research and computer equipment a General User can expect to find and use at each beamline when working at the NSLS. The Manual is updated periodically in order to keep pace with the constant changes on these beamlines.

  11. 2-ps Hard X-Ray Streak Camera Measurements at Sector 7 Beamline of the Advanced Photon Source

    SciTech Connect

    Chollet, M.; Ahr, B.; Walko, D.A.; Rose-Petruck, C.; Adams, B.

    2011-08-02

    A hard X-ray streak camera capable of 2-ps time resolution is in operation at the Sector 7 beamline of the Advanced Photon Source. It is used for laser-pump, X-ray probe experiments using the Ti:Sapphire femtosecond laser system installed on the beamline. This streak camera, combined with standardized and prealigned experimental setups, can perform time-resolved liquid-phase absorption spectroscopy, reflectivity, and diffraction experiments.

  12. Recent developments on techniques for differential phase imaging at the medical beamline of ELETTRA

    NASA Astrophysics Data System (ADS)

    Arfelli, F.; Pelliccia, D.; Cedola, A.; Astolfo, A.; Bukreeva, I.; Cardarelli, P.; Dreossi, D.; Lagomarsino, S.; Longo, R.; Rigon, L.; Sodini, N.; Menk, R. H.

    2013-06-01

    Over the last decade different phase contrast approaches have been exploited at the medical beamline SYRMEP of the synchrotron radiation facility Elettra in Trieste, Italy. In particular special focus has been drawn to analyzer based imaging and the associated imaging theory and processing. Analyzer based Imaging (ABI) and Diffraction Enhanced Imaging (DEI) techniques have been successfully applied in several biomedical applications. Recently it has been suggested to translate the acquired knowledge in this field towards a Thomson Backscattering Source (TBS), which is presently under development at the Frascati National Laboratories of INFN (Istituto Nazionale di Fisica Nucleare) in Rome, Italy. Such source is capable of producing intense and quasi-monochromatic hard X-ray beams. For the technical implementation of biomedical phase imaging at the TBS a grating interferometer for differential phase contrast imaging has been designed and successfully tested at SYRMEP beamline.

  13. Indus-2 X-ray lithography beamline for X-ray optics and material science applications

    SciTech Connect

    Dhamgaye, V. P. Lodha, G. S.

    2014-04-24

    X-ray lithography is an ideal technique by which high aspect ratio and high spatial resolution micro/nano structures are fabricated using X-rays from synchrotron radiation source. The technique has been used for fabricating optics (X-ray, visible and infrared), sensors and actuators, fluidics and photonics. A beamline for X-ray lithography is operational on Indus-2. The beamline offers wide lithographic window from 1-40keV photon energy and wide beam for producing microstructures in polymers upto size ∼100mm × 100mm. X-ray exposures are possible in air, vacuum and He gas environment. The air based exposures enables the X-ray irradiation of resist for lithography and also irradiation of biological and liquid samples.

  14. Energy optimization of a regular macromolecular crystallography beamline for ultra-high-resolution crystallography

    SciTech Connect

    Rosenbaum, Gerd; Ginell, Stephan L.; Chen, Julian C.-H.

    2015-01-01

    In this study, a practical method for operating existing undulator synchrotron beamlines at photon energies considerably higher than their standard operating range is described and applied at beamline 19-ID of the Structural Biology Center at the Advanced Photon Source enabling operation at 30 keV. Adjustments to the undulator spectrum were critical to enhance the 30 keV flux while reducing the lower- and higher-energy harmonic contamination. A Pd-coated mirror and Al attenuators acted as effective low- and high-bandpass filters. The resulting flux at 30 keV, although significantly lower than with X-ray optics designed and optimized for this energy, allowed for accurate data collection on crystals of the small protein crambin to 0.38 Å resolution.

  15. A Superbend X-Ray Microdiffraction Beamline at the Advanced Light Source

    SciTech Connect

    Tamura, N.; Kunz, M.; Chen, K.; Celestre, R.S.; MacDowell, A.A.; Warwick, T.

    2009-03-10

    Beamline 12.3.2 at the Advanced Light Source is a newly commissioned beamline dedicated to x-ray microdiffraction. It operates in both monochromatic and polychromatic radiation mode. The facility uses a superconducting bending magnet source to deliver an X-ray spectrum ranging from 5 to 22 keV. The beam is focused down to {approx} 1 um size at the sample position using a pair of elliptically bent Kirkpatrick-Baez mirrors enclosed in a vacuum box. The sample placed on high precision stages can be raster-scanned under the microbeam while a diffraction pattern is taken at each step. The arrays of diffraction patterns are then analyzed to derive distribution maps of phases, strain/stress and/or plastic deformation inside the sample.

  16. The PGM-Beamline at the Undulator U55 at DELTA

    SciTech Connect

    Berges, U.; Westphal, C.; Krause, M.; Schuermann, M.; Dreiner, S.; Follath, R.; Schaefers, F.

    2004-05-12

    A beamline for linearly polarized light radiation from an undulator is being commissioned at DELTA, an University synchrotron facility. The electron beam in the undulator as a radiation source is mapped by the first optical element onto an intermediate focus. Mirror M1 has a large acceptance angle in order to provide a stable performance if small electron beam displacements occur. The intermediate focus is demagnified onto the sample providing a focus spot size of 70 x 30{mu}m2. The PGM (Plane Grating Monochromator) based beamline works with collimated light allowing a flexible use of the monochromator. Depending on user demands, it can be operated by at high spectral resolution, high flux mode, or at high order suppression.

  17. Undulator beamline optimization with integrated chicanes for X-ray free-electron-laser facilities.

    PubMed

    Prat, Eduard; Calvi, Marco; Ganter, Romain; Reiche, Sven; Schietinger, Thomas; Schmidt, Thomas

    2016-07-01

    An optimization of the undulator layout of X-ray free-electron-laser (FEL) facilities based on placing small chicanes between the undulator modules is presented. The installation of magnetic chicanes offers the following benefits with respect to state-of-the-art FEL facilities: reduction of the required undulator length to achieve FEL saturation, improvement of the longitudinal coherence of the FEL pulses, and the ability to produce shorter FEL pulses with higher power levels. Numerical simulations performed for the soft X-ray beamline of the SwissFEL facility show that optimizing the advantages of the layout requires shorter undulator modules than the standard ones. This proposal allows a very compact undulator beamline that produces fully coherent FEL pulses and it makes possible new kinds of experiments that require very short and high-power FEL pulses. PMID:27359133

  18. Energy optimization of a regular macromolecular crystallography beamline for ultra-high-resolution crystallography

    DOE PAGESBeta

    Rosenbaum, Gerd; Ginell, Stephan L.; Chen, Julian C.-H.

    2015-01-01

    In this study, a practical method for operating existing undulator synchrotron beamlines at photon energies considerably higher than their standard operating range is described and applied at beamline 19-ID of the Structural Biology Center at the Advanced Photon Source enabling operation at 30 keV. Adjustments to the undulator spectrum were critical to enhance the 30 keV flux while reducing the lower- and higher-energy harmonic contamination. A Pd-coated mirror and Al attenuators acted as effective low- and high-bandpass filters. The resulting flux at 30 keV, although significantly lower than with X-ray optics designed and optimized for this energy, allowed for accuratemore » data collection on crystals of the small protein crambin to 0.38 Å resolution.« less

  19. Calibration and standards beamline 6.3.2 at the ALS

    SciTech Connect

    Underwood, J.H.; Gullikson, E.M.; Koike, M.

    1997-04-01

    More sophisticated optics for the x-ray, soft x-ray and far ultraviolet spectral regions being developed for synchrotron radiation research and many other applications, require accurate calibration and standards facilities for measuring reflectivity of mirrors and multilayer coatings, transmission of thin films, bandpass of multilayers, efficiency of gratings or detectors, etc. For this purpose beamline 6.3.2 was built at the ALS. Its energy coverage, versatility, simplicity and convenience also make it useful for a wide range of other experiments. The paper describes the components of this beamline, consisting of: a four jaw aperture; a horizontal focusing mirror; a monochromator; exit slit; vertical focusing mirror; mechanical and vacuum system; reflectometer; filter wheels; and data acquisition system.

  20. Automated laboratory based X-ray beamline with multi-capillary sample chamber

    NASA Astrophysics Data System (ADS)

    Purushothaman, S.; Gauthé, B. L. L. E.; Brooks, N. J.; Templer, R. H.; Ces, O.

    2013-08-01

    An automated laboratory based X-ray beamline with a multi-capillary sample chamber capable of undertaking small angle X-ray scattering measurements on a maximum of 104 samples at a time as a function of temperature between 5 and 85 °C has been developed. The modular format of the system enables the user to simultaneously equilibrate samples at eight different temperatures with an accuracy of ±0.005 °C. This system couples a rotating anode generator and 2D optoelectronic detector with Franks X-ray optics, leading to typical exposure times of less than 5 min for lyotropic liquid crystalline samples. Beamline control including sample exchange and data acquisition has been fully automated via a custom designed LabVIEW framework.

  1. Automated laboratory based X-ray beamline with multi-capillary sample chamber

    SciTech Connect

    Purushothaman, S.; Gauthé, B. L. L. E.; Brooks, N. J.; Templer, R. H.; Ces, O.

    2013-08-15

    An automated laboratory based X-ray beamline with a multi-capillary sample chamber capable of undertaking small angle X-ray scattering measurements on a maximum of 104 samples at a time as a function of temperature between 5 and 85 °C has been developed. The modular format of the system enables the user to simultaneously equilibrate samples at eight different temperatures with an accuracy of ±0.005 °C. This system couples a rotating anode generator and 2D optoelectronic detector with Franks X-ray optics, leading to typical exposure times of less than 5 min for lyotropic liquid crystalline samples. Beamline control including sample exchange and data acquisition has been fully automated via a custom designed LabVIEW framework.

  2. A Compensating Monochromator Crystal Bender at the HMI Multipole Wiggler Beamline MAGS

    SciTech Connect

    Dudzik, E.; Feyerherm, R.; Frahm, R.

    2007-01-19

    A compensating watercooled crystal bender for high heat loads has been built and successfully commissioned at the new multipole wiggler beamline MAGS of the Hahn-Meitner-Institute at the synchrotron radiation source BESSY. The beamline takes a 3 x 0.3 mrad fan of the wiggler beam, corresponding to a heat load of up to 2000 W. Although the crystal bender was originally designed for maximum heat loads of 600 W, it was found to work with heat loads of up to 800 W, reducing the Si(111) rocking curve width from 17.2 to 8.3 arcsec at the Cu K-edge (8.9 keV). In addition, the good mechanical reproducibility of the device is illustrated.

  3. A Compensating Monochromator Crystal Bender at the HMI Multipole Wiggler Beamline MAGS

    NASA Astrophysics Data System (ADS)

    Dudzik, E.; Feyerherm, R.; Waterstradt, T.; Schröder, L.-E.; Diete, W.; Frahm, R.

    2007-01-01

    A compensating watercooled crystal bender for high heat loads has been built and successfully commissioned at the new multipole wiggler beamline MAGS of the Hahn-Meitner-Institute at the synchrotron radiation source BESSY. The beamline takes a 3 × 0.3 mrad fan of the wiggler beam, corresponding to a heat load of up to 2000 W. Although the crystal bender was originally designed for maximum heat loads of 600 W, it was found to work with heat loads of up to 800 W, reducing the Si(111) rocking curve width from 17.2 to 8.3 arcsec at the Cu K-edge (8.9 keV). In addition, the good mechanical reproducibility of the device is illustrated.

  4. Beam-line considerations for experiments with highly-charged ions

    SciTech Connect

    Johnson, B.M.

    1990-01-01

    The APS offers exciting possibilities for a bright future in x-ray research. For example, measurements on the inner-shell photoionization of ions will be feasible using stored ions in ions traps or ion beams from an electron-cyclotron-resonance ion source, or perhaps even a heavy-ion storage ring. Such experiments with ionic targets are the focus for the discussion given here on the optimization of photon flux on a generic beamline at the APS. The performance of beam lines X26C, X26A, and X17 on the x-ray ring of the National Synchrotron Light Source will be discussed as specific examples of beam-line design considerations.

  5. PARALLEL MEASUREMENT AND MODELING OF TRANSPORT IN THE DARHT II BEAMLINE ON ETA II

    SciTech Connect

    Chambers, F W; Raymond, B A; Falabella, S; Lee, B S; Richardson, R A; Weir, J T; Davis, H A; Schultze, M E

    2005-05-31

    To successfully tune the DARHT II transport beamline requires the close coupling of a model of the beam transport and the measurement of the beam observables as the beam conditions and magnet settings are varied. For the ETA II experiment using the DARHT II beamline components this was achieved using the SUICIDE (Simple User Interface Connecting to an Integrated Data Environment) data analysis environment and the FITS (Fully Integrated Transport Simulation) model. The SUICIDE environment has direct access to the experimental beam transport data at acquisition and the FITS predictions of the transport for immediate comparison. The FITS model is coupled into the control system where it can read magnet current settings for real time modeling. We find this integrated coupling is essential for model verification and the successful development of a tuning aid for the efficient convergence on a useable tune. We show the real time comparisons of simulation and experiment and explore the successes and limitations of this close coupled approach.

  6. Dedicated Max-Planck beamline for the in situ investigation of interfaces and thin films

    SciTech Connect

    Stierle, A.; Steinhaeuser, A.; Ruehm, A.; Renner, F.U.; Weigel, R.; Kasper, N.; Dosch, H.

    2004-12-01

    A dedicated beamline for the Max-Planck-Institut fuer Metallforschung was recently taken into operation at the Angstroemquelle Karlsruhe (ANKA). Here we describe the layout of the beamline optics and the experimental end-station, consisting of a heavy duty multiple circle diffractometer. For both a new design was realized, combining a maximum flexibility in the beam properties [white, pink (focused) monochromatic, energy range 6-20 keV] with a special diffractometer for heavy sample environments up to 500 kg, that can be run in different geometrical modes. In addition the angular-reciprocal space transformations for the diffractometer in use are derived, which allows an operation of the instrument in the convenient six circle mode. As an example, results from surface x-ray diffraction on a Cu{sub 3}Au(111) single crystal are presented.

  7. Jefferson Lab Hall A Beamline Instrumentation and Calibration for GMP experiment

    NASA Astrophysics Data System (ADS)

    Gautam, Thir Narayan

    2015-10-01

    The nucleon electromagnetic form factors characterize the distributions of electric charge and magnetization current inside the nucleon and thus reflect the internal structure determined by Quantum Chromodynamics. The GMp experiment is a first experiment run in Hall A at Jefferson Lab after the upgrade to double the beam energy with the goal to precisely measure electron-proton elastic cross section in the Q2 range of 7 to 17 GeV2 with an accuracy of better than 2%; several time better than existing data at the highest Q2. In order to achieve this accuracy, a determination of the accumulated beam charge of better than 0.5% is required. The new 12 GeV beamline was commissioned during the spring of 2015, with the main instrumentation consisting of beam charge and position monitors. In this talk, the procedures and the results of the calibrations of these beamline components will be presented.

  8. New developments at the INE-Beamline for actinide research at ANKA

    NASA Astrophysics Data System (ADS)

    Brendebach, B.; Dardenne, K.; Denecke, M. A.; Rothe, J.; Vitova, T.

    2007-11-01

    The INE-Beamline for actinide research at the synchrotron source Ångströmquelle Karlsruhe (ANKA) completed its first year of operation in October 2006. Experiments on radioactive samples with activities up to 10 6 times the limit of exemption at X-ray energies from around 2.1 keV (P K-edge) to 25 keV (Pd K-edge) are possible. Three recent instrumental developments at the Nuclear Waste Disposal (INE)-Beamline are presented: a Quick-XAFS mode of operating the Lemonnier-type monochromator in fixed exit for time-resolved experiments, total electron yield detection, and the use of one-dimensional compound refractive lenses, fabricated at the Institut für Mikrostrukturtechnik (IMT) at Forschungszentrum Karlsruhe (FZK), as a virtual slit for surface sensitive X-ray studies. Future upgrades for lowering the attainable energy, installing a microfocus option, and commissioning a cryostat for radioactive samples are planned.

  9. Directly water-cooled crystal development for SPring-8 bending magnet beamlines

    NASA Astrophysics Data System (ADS)

    Takeshita, Kunikazu; Goto, Shunji; Ishikawa, Tetsuya

    2007-09-01

    The directly water-cooled first crystal of the SPring-8 standard monochromator for bending magnet beamlines has been developed. Thanks to the bonding technique, the performance of the new crystal has been improved without decreasing the cooling efficiency. The finite element analyses show the deformation of the crystal by the hydraulic pressure and by the crystal clamping is negligible small, which were dominated for the previous crystal. Both Si(111) and Si(311) crystal were evaluated in SPring-8 beamlines, the deformation induced while the bonding process is comparable to the thermal deformation. and long-term endurance test shows the lifetime of the O-ring becomes long because they are not on the direct path of the SR beam. Although the overall performance is insufficient, much improvement was shown.

  10. A soft X-ray beamline for transmission X-ray microscopy at ALBA.

    PubMed

    Pereiro, E; Nicolás, J; Ferrer, S; Howells, M R

    2009-07-01

    The MISTRAL beamline is one of the seven phase-I beamlines at the ALBA synchrotron light source (Barcelona, Spain) that will be opened to users at the end of 2010. MISTRAL will be devoted to cryotomography in the water window and multi-keV spectral regions for biological applications. The optics design consists of a plane-grating monochromator that has been implemented using variable-line-spacing gratings to fulfil the requirements of X-ray microscopy using a reflective condenser. For instance, a fixed-focus condition independent of the included angle, constant magnification as well as coma and spherical aberration corrections are achieved with this system. The reported design is of wider use. PMID:19535865

  11. Optical design and performance of the inelastic scattering beamline at the National Synchrotron Light Source

    SciTech Connect

    Kao, C.C.; Siddons, D.P.; Oversluizen, T.; Hastings, J.B.; Hamalainen, K.; Krisch, M.

    1994-12-31

    Phase I of the X21 beamline at the National Synchrotron Light Source was commissioned during 1993. The research program at the X21 beamline is focused on the study of electronic excitations in condensed matter with total energy resolution of 0.1 eV to 1.0 eV. The source is a 27 pole hybrid wiggler. A water-cooled horizontal focusing Si(220) monochromator and a spherically bent Si(444) analyzer were installed and commissioned. At 8 keV the energy resolution of the monochromator is about 0.7 eV, and the energy resolution of the analyzer is about 0.1 eV. Results from several selected experiments are also discussed.

  12. Characterization of wax as a potential diffraction intensity standard for macromolecular crystallography beamlines.

    PubMed

    Brandao-Neto, J; Thompson, S P; Lennie, A R; Ferreira, F F; Tang, C C

    2010-01-01

    A number of commercially available waxes in the form of thin disc samples have been investigated as possible diffraction intensity standards for macromolecular crystallography synchrotron beamlines. Synchrotron X-ray powder diffraction measurements show that beeswax offers the best performance of these waxes owing to its polycrystallinity. Crystallographic lattice parameters and diffraction intensities were examined between 281 and 309 K, and show stable and predictable thermal behaviour. Using an X-ray beam of known incident flux at lambda = 1 A, the diffraction power of two strong Bragg reflections for beeswax were quantified as a function of sample thickness and normalized to 10(10) photons s(-1). To demonstrate its feasibility as a diffraction intensity standard, test measurements were then performed on a new third-generation macromolecular crystallography synchrotron beamline. PMID:20029111

  13. Surveying and optical tooling technologies combined to align a skewed beamline at the LAMPF accelerator

    SciTech Connect

    Bauke, W.; Clark, D.A.; Trujillo, P.B.

    1985-01-01

    Optical Tooling evolved from traditional surveying, and both technologies are sometimes used interchangeably in large industrial installations, since the instruments and their specialized adapters and supports complement each other well. A unique marriage of both technologies was accomplished in a novel application at LAMPF, the Los Alamos Meson Physics Facility. LAMPF consists of a linear accelerator with multiple target systems, one of which had to be altered to accommodate a new beamline for a neutrino experiment. The new line was to be installed into a crowded beam tunnel and had to be skewed and tilted in compound angles to avoid existing equipment. In this paper we describe how Optical Tooling was used in conjunction with simple alignment and reference fixtures to set fiducials on the magnets and other mechanical components of the beamline, and how theodolites and sight levels were then adapted to align these components along the calculated skew planes. Design tolerances are compared with measured alignment results.

  14. SUPERSTARS III: K-2.

    ERIC Educational Resources Information Center

    North Carolina State Dept. of Public Education, Raleigh.

    SUPERSTARS III is a K-8 program designed as an enrichment opportunity for self-directed learners in mathematics. The basic purpose of SUPERSTARS III is to provide the extra challenge that self-motivated students need in mathematics and to do so in a structured, long-term program that does not impinge on the normal classroom routine or the…

  15. CITY III Player's Manual.

    ERIC Educational Resources Information Center

    Envirometrics, Inc., Washington, DC.

    CITY III is a computer-assisted simulation game in which participants make decisions affecting the economic, governmental, and social conditions of a simulated urban area. In CITY III, the computer stores all the relevant statistics for the area, updates data when changes are made, and prints out yearly reports. The computer also simulates…

  16. CITY III Operator's Manual.

    ERIC Educational Resources Information Center

    Envirometrics, Inc., Washington, DC.

    CITY III is a computer-assisted simulation game of an urban system involving player operation of and interaction with economic, social, and government components. The role of operator in the game is to take the handwritten inputs (decisions) from the CITY III participants, process them, and return output which initiates the next round of…

  17. Optimizing the Stark-decelerator beamline for the trapping of cold molecules using evolutionary strategies

    SciTech Connect

    Gilijamse, Joop J.; Kuepper, Jochen; Hoekstra, Steven; Vanhaecke, Nicolas; Meerakker, Sebastiaan Y. T. van de; Meijer, Gerard

    2006-06-15

    We demonstrate feedback control optimization for the Stark deceleration and trapping of neutral polar molecules using evolutionary strategies. In a Stark-decelerator beamline, pulsed electric fields are used to decelerate OH radicals and subsequently store them in an electrostatic trap. The efficiency of the deceleration and trapping process is determined by the exact timings of the applied electric field pulses. Automated optimization of these timings yields an increase of 40% of the number of trapped OH radicals.

  18. Beamline Front-End for Minipole Undulator at the Photon Factory Storage Ring

    SciTech Connect

    Miyauchi, Hiroshi; Tahara, Toshihiro; Asaoka, Seiji

    2010-06-23

    The straight-section upgrade project of the Photon Factory created four new short straight sections capable of housing in-vacuum minipole undulators. The first to third minipole undulators SGU no. 17, SGU no. 03 and SGU no. 01 were installed at the 2.5-GeV Photon Factory storage ring in 2005, 2006 and 2009, respectively. The beamline front ends for SGU0 no. 3 and SGU0 no. 1 are described in this paper.

  19. Confirmation and Readjustment of Bending Magnet Beam-Line Optics Using SHADOW

    NASA Astrophysics Data System (ADS)

    Matsubara, Takahiro; Kanda, Kazuhiro; Kato, Yuri; Hisao, Shintarou; Shoji, Yoshihiko

    2007-01-01

    Optical alignment of the NewSUBARU beam-line 6 (BL6) is discussed by comparing the observed SR profiles with the calculated results of ray-tracing using SHADOW. A new screen monitor was mounted downstream of the first mirror to observe the synchrotron radiation profile. The distorted profile downstream of the second mirror was attributed to the rotation of the first mirror along the vertical axis. The distortion was successfully improved by a re-adjustment according to the calculations.

  20. Use of object-oriented techniques in a beam-line control system

    SciTech Connect

    Myers, D.R.; Rueden, W. von; Butler, H.; Yang, J.

    1994-12-31

    The authors describe the use of object-oriented programming in the control and data-acquisition system for the upgraded CERN neutrino beam-line. C++ in conjunction with Posix threads running under Lynx-OS have been used in several front-end PCs. These communicate using Remote Procedure Calls over ethernet with a workstation running the commercial supervisory package, FactoryLink.

  1. A microtomography beamline at the Louisiana State University Center for Advanced Microstructures and Devices synchrotron

    NASA Astrophysics Data System (ADS)

    Ham, Kyungmin; Jin, Hua; Butler, Leslie G.; Kurtz, Richard L.

    2002-03-01

    A microtomography beamline has been recently assembled and is currently operating at the Louisiana State University's Center for Advanced Microstructures and Devices synchrotron (CAMD). It has been installed on a bending magnet white-light beamline at port 7A. With the storage ring operating at 1.5 GeV, this beamline has a maximum usable x-ray energy of ˜15 keV. The instrumentation consists of computer-controlled positioning stages for alignment and rotation, a CsI(Tl) phosphor screen, a reflecting mirror, a microscope objective (1:1, 1:4), and Linux/LabVIEW-controlled charge coupled device. With the 1:4 objective, the maximum spatial resolution is 2.25 μm. The positioning and image acquisition computers communicate via transfer control protocol/internet protocol (TCP/IP). A small G4/Linux cluster has been installed for the purpose of on-site reconstruction. Instrument, alignment and reconstruction programs are written in MATLAB, IDL, and C. The applications to date are many and we present several examples. Several biological samples have been studied as part of an effort on biological visualization and computation. Future improvements to this microtomography station include the addition of a double-multilayer monochromator, allowing one to evaluate the three-dimensional elemental composition of materials. Plans also include eventual installation at the CAMD 7 T wiggler beamline, providing x rays in excess of 50 keV to provide better penetration of higher mass-density materials.

  2. Ultrahigh contrast from a frequency-doubled chirped-pulse-amplification beamline.

    PubMed

    Hillier, David; Danson, Colin; Duffield, Stuart; Egan, David; Elsmere, Stephen; Girling, Mark; Harvey, Ewan; Hopps, Nicholas; Norman, Michael; Parker, Stefan; Treadwell, Paul; Winter, David; Bett, Thomas

    2013-06-20

    This paper describes frequency-doubled operation of a high-energy chirped-pulse-amplification beamline. Efficient type-I second-harmonic generation was achieved using a 3 mm thick 320 mm aperture KDP crystal. Shots were fired at a range of energies achieving more than 100 J in a subpicosecond, 527 nm laser pulse with a power contrast of 10(14). PMID:23842168

  3. Radiation field characterization and shielding studies for the ELI Beamlines facility

    NASA Astrophysics Data System (ADS)

    Ferrari, A.; Amato, E.; Margarone, D.; Cowan, T.; Korn, G.

    2013-05-01

    The ELI (Extreme Light Infrastructure) Beamlines facility in the Czech Republic, which is planned to complete the installation in 2015, is one of the four pillars of the ELI European project. Several laser beamlines with ultrahigh intensities and ultrashort pulses are foreseen, offering versatile radiation sources in an unprecedented energy range: laser-driven particle beams are expected to range between 1 and 50 GeV for electrons and from 100 MeV up to 3 GeV for protons. The number of particles delivered per laser shot is estimated to be 109-1010 for the electron beams and 1010-1012 for the proton beams. The high energy and current values of the produced particles, together with the potentiality to operate at 10 Hz laser repetition rate, require an accurate study of the primary and secondary radiation fields to optimize appropriate shielding solutions: this is a key issue to minimize prompt and residual doses in order to protect the personnel, reduce the radiation damage of electronic devices and avoid strong limitations in the operational time. A general shielding study for the 10 PW (0.016 Hz) and 2 PW (10 Hz) laser beamlines is presented here. Starting from analytical calculations, as well as from dedicated simulations, the main electron and proton fields produced in the laser-matter interaction have been described and used to characterize the "source terms" in full simulations with the Monte Carlo code FLUKA. The secondary radiation fields have been then analyzed to assess a proper shielding. The results of this study and the proposed solutions for the beam dumps of the high energy beamlines, together with a cross-check analysis performed with the Monte Carlo code GEANT4, are presented.

  4. G4BEAMLINE Simulations of Parametric Resonance Ionization Cooling of Muon Beams

    SciTech Connect

    Beard, Kevin; Bogacz, S. Alex; Derbenev, Yaroslav; Yonehara, Katsuya; Johnson, Rolland P.; Paul, Kevin; Roberts, Thomas J.

    2006-03-20

    The technique of using a parametric resonance to allow better ionization cooling is being developed to create small emittance beams so that high collider luminosity can be achieved with fewer muons. While parametric resonance ionization cooling (PIC) of muons has been shown to work in matrix-based simulations using OptiM when the system is properly tuned, doing the same using a much more detailed GEANT-based g4beamline simulation has been more difficult.

  5. High-throughput beamline for attosecond pulses based on toroidal mirrors with microfocusing capabilities

    SciTech Connect

    Frassetto, F.; Poletto, L.; Trabattoni, A.; Anumula, S.; Sansone, G.; Calegari, F.; Nisoli, M.

    2014-10-15

    We have developed a novel attosecond beamline designed for attosecond-pump/attosecond probe experiments. Microfocusing of the Extreme-ultraviolet (XUV) radiation is obtained by using a coma-compensated optical configuration based on the use of three toroidal mirrors controlled by a genetic algorithm. Trains of attosecond pulses are generated with a measured peak intensity of about 3 × 10{sup 11} W/cm{sup 2}.

  6. Phase-space analysis and experimental results for secondary focusing at X-ray beamlines

    SciTech Connect

    Huang, Rong; Meron, Mati; Kujala, Naresh; Barrea, Raul A.

    2011-11-17

    Micro-focusing optical devices at synchrotron beamlines usually have a limited acceptance, but more flux can be intercepted if such optics are used to focus secondary sources created by the primary optics. Flux throughput can be maximized by placing the secondary focusing optics close to or exactly at the secondary source position. However, standard methods of beamline optics analysis, such as the lens equation or matching the mirror surface to an ellipse, work poorly when the source-to-optics distance is very short. In this paper the general characteristics of the focusing of beams with Gaussian profiles by a 'thin lens' are analysed under the paraxial approximation in phase space, concluding that the focusing of a beam with a short source-to-optics distance is distinct from imaging the source; slope errors are successfully included in all the formulas so that they can be used to calculate beamline focusing with good accuracy. A method is also introduced to use the thin-lens result to analyse the micro-focusing produced by an elliptically bent trapezoid-shaped Kirkpatrick-Baez mirror. The results of this analysis are in good agreement with ray-tracing simulations and are confirmed by the experimental results of the secondary focusing at the 18-ID Bio-CAT beamline (at the APS). The result of secondary focusing carried out at 18-ID using a single-bounce capillary can also be explained using this phase-space analysis. A discussion of the secondary focusing results is presented at the end of this paper.

  7. Conceptual design for a dispersive XAFS beamline in the compact storage ring MIRRORCLE

    NASA Astrophysics Data System (ADS)

    Canestrari, N.; Roger, V.; Jeantet, P.; Leynaud, O.; Ortega, L.; Yamada, H.; Hanashima, T.; Lorenzo, J. E.; Sanchez del Rio, M.

    2011-09-01

    We present the conceptual design of a dispersive X-ray Absorption Fine Structure (XAFS) beamline for MIRRORCLE, a new compact laboratory X-ray source. This machine accelerates electrons up to 1,4,6 or 20MeV (depending upon the model) in a ring and produces X-rays when the electrons collide onto a thin target. The radiation emitted has a white spectrum due to both synchrotron and bremsstrahlung emission. A substantial part of the electrons are recovered after collisions, and the emitted light has high flux, wide energy spectrum and a large angular dispersion. We have opted for a simple beamline design using a collimator, slits, a curved crystal, the sample environment and a CCD. The beamline parameters (position of the mirror, ray of curvature, slit aperture, reflecting angle, etc.) have been optimized by defining and improving a figure of merit. This optimization allows for room constraints (distances among elements), mechanical constraints (minimum curvature radii available) and optical constraints. Further ray tracing simulations using SHADOW3 have been performed to check all the theoretical results, refine the final parameters, quantitative flux calculations and for simulating the image on the CCD camera.

  8. The status of the macromolecular crystallography beamlines at the European Synchrotron Radiation Facility

    NASA Astrophysics Data System (ADS)

    Mueller-Dieckmann, Christoph; Bowler, Matthew W.; Carpentier, Philippe; Flot, David; McCarthy, Andrew A.; Nanao, Max H.; Nurizzo, Didier; Pernot, Petra; Popov, Alexander; Round, Adam; Royant, Antoine; de Sanctis, Daniele; von Stetten, David; Leonard, Gordon A.

    2015-04-01

    The European Synchrotron Radiation Facility (ESRF) is the oldest and most powerful 3rd generation synchrotron in Europe, providing X-rays to more than 40 experimental stations welcoming several thousand researchers per year. A major success story has been the ESRF's facilities for macromolecular crystallography (MX). These are grouped around 3 straight sections: On ID23 canted undulators accommodate ID23-1, a mini-focus tuneable energy end station and ID23-2, the world's first micro-focus beamline dedicated to MX; ID29 houses a single, mini-focus, tuneable energy end station; ID30 will provide three end stations for MX due in operation from mid-2014 to early 2015. Here, one branch of a canted X-ray source feeds two fixed-energy end stations (MASSIF-1, MASSIF-3). The second feeds ID30B, a variable focus, tuneable energy beamline. MASSIF-1 is optimised for automatic high-throughput experiments requiring a relatively large beam size at the sample position, MASSIF-3 is a high-intensity, micro-focus facility designed to complement ID23-2. All end stations are highly automated, equipped with sample mounting robots and large area, fast-readout photon-counting detectors. Experiment control and tracking is achieved via a combination of the MXCuBE2 graphical user interface and the ISPyB database, the former allowing user-friendly control of all beamline components, the latter providing data tracking before, after and during experiments.

  9. Minimisation of the Hydrogenic Inventory of the ITER Neutral Beamline and Torus Cryo-Sorption Pumps

    SciTech Connect

    Wykes, M

    2005-07-15

    The tritium inventory of all the ITER torus cryopumps open to the vacuum vessel has an administrative limit of 120 g, including tritium bound to hydrocarbon compounds formed by combination of fuel gas with carbon plasma-facing components. The total hydrogenic inventory of each of the torus cryopumps has to be less than that resulting in a deflagration pressure of 0.2 MPa (the design pressure of the ITER vacuum vessel of which the torus and neutral beam cryopump pressure boundaries are a part) following a hydrogen-air ignition. Since the neutral beamline fuelling is with protium and deuterium only, these pumps do not significantly contribute to the 120 g tritium limit. The hydrogenic inventories of both the torus and neutral beam cryopumps add to the total for the vacuum vessel following an in-vessel ingress of coolant from a failed water-cooled component, wherein hydrogen is produced from steam reacting with hot metallic dust. There is therefore a large incentive to keep the peak inventories of both the torus and neutral beamline cryopumps as low as practicable. The paper describes the regeneration patterns of the torus and neutral beamline cryopumps that are used to attain this goal while achieving the required vacuum conditions commensurate with the reference ITER pulse scenarios.

  10. Recent advances in software for beamline design, accelerator operations and personnel training

    NASA Astrophysics Data System (ADS)

    Gillespie, George H.; Hill, Barrey W.; Martono, Hendy; Moore, John M.

    2000-03-01

    Accelerators are finding new applications in research, industry, medicine, as well as other fields, and there is a growing need for new tools to improve the productivity of scientists and engineers involved with these emerging accelerator applications. Several advances in computer software have been made that focus on meeting those needs. This paper summarizes recent work in the development of a unique software framework designed specifically to support the accelerator community: the Multi-Platform Shell for Particle Accelerator Related Codes (SPARC MP). SPARC MP includes a sophisticated beamline object model, an extensive library of GUI components, and supports a variety of particle optics codes and add-on tools. This framework has been used to create the Particle Beam Optics Laboratory (PBO Lab TM) family of software applications. PBO Lab has been used for beamline design, as a computer aid for teaching particle optics, and to support accelerator operations. Several popular charged particle optics programs, including MARYLIE, TRANSPORT, TURTLE and TRACE 3-D, have been integrated with a new version of PBO Lab. The modeling and simulation capabilities of these codes allow PBO Lab to support a wide spectrum of accelerator types. New external data interface tools are available to import beamline parameters from other sources, for example, to utilize magnet strengths generated by a control system. An overview of the new version of PBO Lab is presented.

  11. The materials science X-ray beamline BL8 at the DELTA storage ring

    SciTech Connect

    Luetzenkirchen-Hecht, D.; Wagner, R.; Frahm, R.; Herdt, A.

    2010-06-23

    The instrumentation of the hard X-ray beamline BL8 at the 1.5 GeV Dortmund Electron Accelerator DELTA is described, and the properties of the X-ray optical elements are presented together with experimental data of different fields of research. The beamline, which makes use of the photons emitted by a superconducting asymmetric wiggler, is dedicated to X-ray studies--especially X-ray absorption spectroscopy (XAS)--in the spectral range from about 1 keV to ca. 25 keV photon energy using three different monochromators, namely YB{sub 66}(400), Si(111) and Si(311). The endstation comprises a 6-axis diffractometer that is capable of carrying heavy loads related to non-ambient sample environments such as high pressure cells, cryostats or even complete ultrahigh vacuum systems. X-ray absorption spectra from several reference compounds illustrate the performance of the beamline optics concerning e.g. energy range, energy resolution and beam stability. Fluorescence detection enables the investigation of dilute sample systems, and surface sensitive reflection mode experiments are possible for thin film studies.

  12. MagneDyn: the beamline for magneto dynamics studies at FERMI.

    PubMed

    Svetina, Cristian; Mahne, Nicola; Raimondi, Lorenzo; Caretta, Antonio; Casarin, Barbara; Dell'Angela, Martina; Malvestuto, Marco; Parmigiani, Fulvio; Zangrando, Marco

    2016-01-01

    The future Magneto Dynamics (MagneDyn) beamline will be devoted to study the electronic states and the local magnetic properties of excited and transient states of complex systems by means of the time-resolved X-ray absorption spectroscopy technique. The beamline will use FERMI's high-energy source covering the wavelength range from 60 nm down to 1.3 nm. An on-line photon energy spectrometer will allow spectra to be measured with high resolution while delivering most of the beam to the end-stations. Downstream the beam will be possibly split and delayed, by means of a delay line, and then focused with a set of active Kirkpatrick-Baez mirrors. These mirrors will be able to focus the radiation in one of the two MagneDyn experimental chambers: the electromagnet end-station and the resonant inelastic X-ray scattering end-station. After an introduction of the MagneDyn scientific case, the layout will be discussed showing the expected performances of the beamline. PMID:26698050

  13. Beamlines at synchrotron radiation facilities: The link between the user and the machine

    SciTech Connect

    Johnson, E.D.; Hulbert, S.L.; Berman, L.E.

    1991-12-01

    At this point in time the literature is full of excellent review articles which describe the operating principles of optical systems for utilizing the unique radiation provided by synchrotron storage rings. In general, the perspective provided by this body of work is that of the end user-experimenter cum optics designer. Nominal design specifications of the accelerator are usually assumed, and the impact of operation in a performance envelope which may represent either degraded or enhanced machine performance is seldom considered. In this article, we have attempted to remove ourselves from this (our own usual) perspective and look instead at the beamline as a transfer function to map from the machine to the users experiment. We open first with an introduction to the perspective of the experimentalist, and some general considerations for the interaction of beamline hardware with the machine. We then discuss phase space representations of some common components of beamlines, and then treat some important classes of crystal and geometric optics in monochromators. We then close with a discussion of some of the common features of these optical systems, and the impact of the machine on user experiments.

  14. Hard X-ray XAFS beamline, BL5S1, at AichiSR

    NASA Astrophysics Data System (ADS)

    Tabuchi, M.; Asakura, H.; Morimoto, H.; Watanabe, N.; Takeda, Y.

    2016-05-01

    A XAFS beamline, BL5S1, had been operated at Aichi Synchrotron Radiation Center, Japan since March 2013. The beamline was designed for the measurements in the energy range from 5 to 20 keV. The photon flux of 6 x 1010 at around 9 keV and beam spot size of 0.5 x 0.3 mm at sample position are as good as designed. For the standard transmission XAFS measurement, both of the step- and quick- scan modes are available. Energy resolution at around 9keV is good enough to discuss the energy shift of the order of 0.1 eV or higher even when the measurements are conducted in the quick-scan mode. With several kinds of detectors for fluorescence and/or CEY detection mode measurements, and various kinds of sample holders which are supported by the XAFS measurement software, users easily obtain spectra for their samples. Such a standard, well operated and easy to access XAFS beamline must be very important to broaden the base of the XAFS society further.

  15. Characterization of radioactive materials using the MARS beamline at the synchrotron SOLEIL

    NASA Astrophysics Data System (ADS)

    Sitaud, Bruno; Solari, Pier Lorenzo; Schlutig, Sandrine; Llorens, Isabelle; Hermange, Hervé

    2012-06-01

    Since 2004 numerous efforts have been done at the new French SOLEIL synchrotron to construct a beamline for studying radioactive matter in general and nuclear materials in particular. This Multi Analyses on Radioactive Samples (MARS) beamline has been designed and built thanks to a close partnership with the French Alternative Energies and Atomic Energy Commission (CEA). The optics and the experimental stations have been optimized to perform X-ray characterizations (diffraction, scattering, absorption spectroscopy and fluorescence imaging) on a large variety of radioactive elements. The special infrastructure of this beamline has been defined to be in conformity with the French safety regulations for the manipulation of relatively high activity samples (α, β, γ and n emitters) with an activity up to 18.5 GBq per sample. Several relevant results obtained during the commissioning of the experimental end-stations are presented and discussed in the frame of the near future characterizations of nuclear materials by X-ray diffraction and absorption spectroscopy.

  16. Suite of three protein crystallography beamlines with single superconducting bend magnet as the source

    SciTech Connect

    MacDowell, Alastair A.; Celestre, Richard S.; Howells, Malcolm; McKinney, Wayne; Krupnick, James; Cambie, Daniella; Domning, Edward E; Duarte, Robert M.; Kelez, Nicholas; Plate, David W.; Cork, Carl W.; Earnest, Thomas N.; Dickert, Jeffery; Meigs, George; Ralston, Corie; Holton, James M.; Alber, Thomas; Berger, James M.; Agard, David A.; Padmore, Howard A.

    2004-08-01

    At the Advanced Light Source (ALS), three protein crystallography (PX) beamlines have been built that use as a source one of the three 6 Tesla single pole superconducting bending magnets (superbends) that were recently installed in the ring. The use of such single pole superconducting bend magnets enables the development of a hard x-ray program on a relatively low energy 1.9 GeV ring without taking up insertion device straight sections. The source is of relatively low power, but due to the small electron beam emittance, it has high brightness. X-ray optics are required to preserve the brightness and to match the illumination requirements for protein crystallography. This was achieved by means of a collimating premirror bent to a plane parabola, a double crystal monochromator followed by a toroidal mirror that focuses in the horizontal direction with a 2:1 demagnification. This optical arrangement partially balances aberrations from the collimating and toroidal mirrors such that a tight focused spot size is achieved. The optical properties of the beamline are an excellent match to those required by the small protein crystals that are typically measured. The design and performance of these new beamlines are described.

  17. Thin conductive diamond films as beam intensity monitors for soft x-ray beamlines.

    PubMed

    Kummer, K; Fondacaro, A; Yakhou-Harris, F; Sessi, V; Pobedinskas, P; Janssens, S D; Haenen, K; Williams, O A; Hees, J; Brookes, N B

    2013-03-01

    Quantitative analysis of X-ray absorption and dichroism data requires knowledge of the beamline photon flux during the measurements. We show that thin conductive (B-doped) diamond thin films can be an alternative to the widely used gold meshes for monitoring the beam intensity of soft X-ray beamlines in situ. Limited by the carbon extended x-ray absorption fine structure oscillations, the diamond films become applicable beginning from about 600 eV photon energy, where the important transition metal edges and the rare-earth edges are found. The 100 nm and 250 nm thick free-standing diamond films were grown and tested against standard gold meshes in real-life dichroism experiments performed at beamline ID08 of the European Synchrotron Radiation Facility, Grenoble, France. Quantitative agreement was found between the two experimental data sets. The films feature an extremely high transmission of about 90% and, at the same time, yield a sufficiently strong and clean reference signal. Furthermore, the thin films do not affect the shape of the transmitted beam. X-rays passing mesh-type monitors are subject to diffraction effects, which widen the beam and become particularly disturbing for small beamsizes in the micrometer range. PMID:23556850

  18. Thin conductive diamond films as beam intensity monitors for soft x-ray beamlines

    SciTech Connect

    Kummer, K.; Fondacaro, A.; Yakhou-Harris, F.; Sessi, V.; Brookes, N. B.; Pobedinskas, P.; Janssens, S. D.; Haenen, K.; Williams, O. A.; Hees, J.

    2013-03-15

    Quantitative analysis of X-ray absorption and dichroism data requires knowledge of the beamline photon flux during the measurements. We show that thin conductive (B-doped) diamond thin films can be an alternative to the widely used gold meshes for monitoring the beam intensity of soft X-ray beamlines in situ. Limited by the carbon extended x-ray absorption fine structure oscillations, the diamond films become applicable beginning from about 600 eV photon energy, where the important transition metal edges and the rare-earth edges are found. The 100 nm and 250 nm thick free-standing diamond films were grown and tested against standard gold meshes in real-life dichroism experiments performed at beamline ID08 of the European Synchrotron Radiation Facility, Grenoble, France. Quantitative agreement was found between the two experimental data sets. The films feature an extremely high transmission of about 90% and, at the same time, yield a sufficiently strong and clean reference signal. Furthermore, the thin films do not affect the shape of the transmitted beam. X-rays passing mesh-type monitors are subject to diffraction effects, which widen the beam and become particularly disturbing for small beamsizes in the micrometer range.

  19. Importance of components cleaning in the ultrahigh vacuum performance of beamline front ends

    SciTech Connect

    Liu, C.; Collins, J.T.; Nielsen, R.W.; Kruy, T.L.; Ramanathan, M.; Kuzay, T.M.

    1996-09-01

    The Advanced Photon Source (APS) has 40 beamline front ends in its initial phase of operations; eventually a total of 69 beamline front ends will be connected to the storage ring. The ultrahigh vacuum performance of these front ends will have a significant impact on the storage ring vacuum and on the lifetime of the positron beam. In this paper we emphasize the importance of proper component cleaning to the ultrahigh vacuum performance of beamline front ends. Critical issues in the cleaning process include using environmentally friendly cleaning agents and applications of ultrasonic agitation, thorough deionized water rinsing, and vacuum furnace baking. A simple and cost-effective cleaning facility consisting of ultrasonic cleaning tanks, a drying tank, and a vacuum furnace has been set up. The effectiveness of component cleaning is evaluated by the base pressure achievable in comparison to what is expected according to vacuum calculations using available outgassing rates for the components. Each major component is vacuum tested before final assembly. Vacuum comparisons in some vendor-provided components before and after additional cleaning will be discussed. {copyright} {ital 1996 American Institute of Physics.}

  20. Time-resolved XAS (Bonn-SUT-SLRI) beamline at SLRI.

    PubMed

    Poo-arporn, Yingyot; Chirawatkul, Prae; Saengsui, Worasarit; Chotiwan, Siwarak; Kityakarn, Sutasinee; Klinkhieo, Supat; Hormes, Josef; Songsiriritthigul, Prayoon

    2012-11-01

    An energy-dispersive X-ray absorption spectroscopy beamline has been constructed at the Synchrotron Light Research Institute, Thailand. The beamline was designed to utilize the synchrotron radiation with photon energies between 2400 and 8000 eV. The horizontal focusing of the bent crystal in the energy-dispersive monochromator offers a small polychromatic focal spot of 1 mm at the sample position. By employing an energy-dispersive scheme, the whole X-ray absorption near-edge structure (XANES) can be obtained simultaneously using a position-sensitive detector with a fastest readout speed of 25 ms. The short data collection time opens a new opportunity for time-resolved X-ray absorption spectroscopy (XAS) experiments such as studies of changes of the electronic structures or the local coordination environments of an atom during a change in thermodynamic conditions. For this purpose, an in situ cell was designed and fabricated for the beamline. Thermal oxidation of TiO(2) was chosen as an in situ experiment example. The structural change of TiO(2) as a function of temperatures was monitored from the change in the measured XAS spectra. The obtained Ti K-edge XANES spectra clearly show the formation of an anatase phase when the temperature was raised to 673 K. PMID:23093752

  1. Measurement of diffraction gratings with a long trace profiler with applications for synchrotron beamline gratings

    SciTech Connect

    Irick, S.C.; McKinney, W.R.

    1997-06-01

    The Long Trace Profiler (LTP) is used primarily for measuring the figure of long synchrotron beamline mirrors. The LTP has also been used for measuring the figure of the substrate of beamline gratings. We propose a method for measuring the effective figure that comes from the gratings groove pattern on the substrate of long beamline gratings. Analysis of gratings groove patterns can be useful in determining cause of poor imaging of the diffracted light, but requires investigation of small changes of the groove frequency over the entire clear aperture of the grating. A diffraction grating that is small enough to be measured by a general purpose six inch aperture interferometer is measured by both this interferometer and the LTP, so that results for two different instruments may be compared. The height profile of the substrate light (m = 0) measurement is subtracted from the height profile of the diffracted light (m = 1) measurement, and the result is the effect of only the diffraction f rom the grooves along the entire surface. This procedure is also used for a diffraction grating that is too long to be measured by the general purpose interferometer, but is easily measured by the LTP.

  2. Measurement of diffraction gratings with a long trace profiler with application for synchrotron beamline gratings

    SciTech Connect

    Irick, S. C.; McKinney, W. R.

    1997-07-01

    The Long Trace Profiler (LTP) is used primarily for measuring the figure of long synchrotron beamline mirrors. The LTP has also been used for measuring the figure of the substrate of beamline gratings. We propose a method for measuring the effective figure that comes from the grating groove pattern on the substrate of long beamline gratings. Analysis of grating groove patterns can be useful in determining cause of poor imaging of the diffracted light, but requires investigation of small changes of the groove frequency over the entire clear aperture of the grating. A diffraction grating that is small enough to be measured by a general purpose six inch aperture interferometer is measured by both this interferometer and the LTP, so that results for two different instruments may be compared. The height profile of the substrate light (m=0) measurement is subtracted from the height profile of the diffracted light (m=1) measurement, and the result is the effect of only the diffraction from the grooves along the entire surface. This procedure is also used for a diffraction grating that is too long to be measured by the general purpose interferometer, but is easily measured by the LTP.

  3. Measurement of diffraction gratings with a long trace profiler with application for synchrotron beamline gratings

    SciTech Connect

    Irick, S.C.; McKinney, W.R.

    1997-07-01

    The Long Trace Profiler (LTP) is used primarily for measuring the figure of long synchrotron beamline mirrors. The LTP has also been used for measuring the figure of the substrate of beamline gratings. We propose a method for measuring the effective figure that comes from the grating groove pattern on the substrate of long beamline gratings. Analysis of grating groove patterns can be useful in determining cause of poor imaging of the diffracted light, but requires investigation of small changes of the groove frequency over the entire clear aperture of the grating. A diffraction grating that is small enough to be measured by a general purpose six inch aperture interferometer is measured by both this interferometer and the LTP, so that results for two different instruments may be compared. The height profile of the substrate light (m=0) measurement is subtracted from the height profile of the diffracted light (m=1) measurement, and the result is the effect of only the diffraction from the grooves along the entire surface. This procedure is also used for a diffraction grating that is too long to be measured by the general purpose interferometer, but is easily measured by the LTP. {copyright} {ital 1997 American Institute of Physics.}

  4. Time-Resolved Research at the Advanced Photon Source Beamline 7-ID

    SciTech Connect

    Dufresne, Eric M.; Adams, Bernhard; Arms, Dohn A.; Chollet, Matthieu; Li, Yuelin; Walko, Donald A.; Wang Jin; Landahl, Eric C.

    2010-06-23

    The Sector 7 undulator beamline (7-ID) of the Advanced Photon Source (APS) is dedicated to time-resolved x-ray research and is capable of ultrafast measurements on the order of 100 ps. Beamline 7-ID has a laser laboratory featuring a Ti:Sapphire system (average power of 2.5 W, pulse duration <50 fs, repetition rate 1-5 kHz) that can be synchronized to the bunch pattern of the storage ring. The laser is deliverable to x-ray enclosures, which contain diffractometers, as well as motorized optical tables for table-top experiments. Beamline 7-ID has a single APS Undulator A and uses a diamond (111) double-crystal monochromator, providing good energy resolution over a range of 6-24 keV. Available optics include Kirkpatrick-Baez (KB) mirrors to microfocus the x-ray beam. A variety of time-resolved diffraction and spectroscopy research is available at 7-ID, with experiments being done in the atomic, molecular, optical, chemistry, and solid state (bulk and surface) fields.

  5. Time-Resolved Research at the Advanced Photon Source Beamline 7-ID

    SciTech Connect

    Dufresne, Eric M.; Adams, Bernhard; Arms, Dohn A.; Chollet, Matthieu; Landahl, Eric C.; Li, Yuelin; Walko, Donald A.; Wang, Jin

    2010-08-02

    The Sector 7 undulator beamline (7-ID) of the Advanced Photon Source (APS) is dedicated to time-resolved x-ray research and is capable of ultrafast measurements on the order of 100 ps. Beamline 7-ID has a laser laboratory featuring a Ti:Sapphire system (average power of 2.5W, pulse duration <50 fs, repetition rate 1-5 kHz) that can be synchronized to the bunch pattern of the storage ring. The laser is deliverable to x-ray enclosures, which contain diffractometers, as well as motorized optical tables for table-top experiments. Beamline 7-ID has a single APS Undulator A and uses a diamond (111) double-crystal monochromator, providing good energy resolution over a range of 6-24 keV. Available optics include Kirkpatrick-Baez (KB) mirrors to microfocus the x-ray beam. A variety of time-resolved diffraction and spectroscopy research is available at 7-ID, with experiments being done in the atomic, molecular, optical, chemistry, and solid state (bulk and surface) fields.

  6. The first microbeam synchrotron X-ray fluorescence beamline at the Siam Photon Laboratory.

    PubMed

    Tancharakorn, Somchai; Tanthanuch, Waraporn; Kamonsutthipaijit, Nuntaporn; Wongprachanukul, Narupon; Sophon, Methee; Chaichuay, Sarunyu; Uthaisar, Chunmanus; Yimnirun, Rattikorn

    2012-07-01

    The first microbeam synchrotron X-ray fluorescence (µ-SXRF) beamline using continuous synchrotron radiation from Siam Photon Source has been constructed and commissioned as of August 2011. Utilizing an X-ray capillary half-lens allows synchrotron radiation from a 1.4 T bending magnet of the 1.2 GeV electron storage ring to be focused from a few millimeters-sized beam to a micrometer-sized beam. This beamline was originally designed for deep X-ray lithography (DXL) and was one of the first two operational beamlines at this facility. A modification has been carried out to the beamline in order to additionally enable µ-SXRF and synchrotron X-ray powder diffraction (SXPD). Modifications included the installation of a new chamber housing a Si(111) crystal to extract 8 keV synchrotron radiation from the white X-ray beam (for SXPD), a fixed aperture and three gate valves. Two end-stations incorporating optics and detectors for µ-SXRF and SXPD have then been installed immediately upstream of the DXL station, with the three techniques sharing available beam time. The µ-SXRF station utilizes a polycapillary half-lens for X-ray focusing. This optic focuses X-ray white beam from 5 mm × 2 mm (H × V) at the entrance of the lens down to a diameter of 100 µm FWHM measured at a sample position 22 mm (lens focal point) downstream of the lens exit. The end-station also incorporates an XYZ motorized sample holder with 25 mm travel per axis, a 5× ZEISS microscope objective with 5 mm × 5 mm field of view coupled to a CCD camera looking to the sample, and an AMPTEK single-element Si (PIN) solid-state detector for fluorescence detection. A graphic user interface data acquisition program using the LabVIEW platform has also been developed in-house to generate a series of single-column data which are compatible with available XRF data-processing software. Finally, to test the performance of the µ-SXRF beamline, an elemental surface profile has been obtained for

  7. Optical Design in Phase-Space for the I13L X-Ray Imaging and Coherence Beamline at Diamond using XPHASY

    NASA Astrophysics Data System (ADS)

    Wagner, Ulrich H.; Rau, Christoph

    2010-06-01

    I13L is a 250 m long beamline for imaging and coherent diffraction currently under construction at the Diamond Light Source. For modeling the beamline optics the phase-space based ray-tracing code XPHASY was developed, as general ray-tracing codes for x-rays do not easily allow studying the propagation of coherence along the beamline. In contrast to computational intensive wave-front propagation codes, which fully describe the propagation of a photon-beam along a beamline but obscure the impact of individual optical components onto the beamline performance, this code allows to quickly calculate the photon-beam propagation along the beamline and estimate the impact of individual components. In this paper we will discuss the optical design of the I13L coherence branch from the perspective of phase-space by using XPHASY. We will demonstrate how the phase-space representation of a photon-beam allows estimating the coherence length at any given position along the beamline. The impact of optical components on the coherence length and the effect of vibrations on the beamline performance will be discussed. The paper will demonstrate how the phase-space representation of photon-beams allows a more detailed insight into the optical performance of a coherence beamline than ray-tracing in real space.

  8. Antithrombin III blood test

    MedlinePlus

    ... AT III) is a protein that helps control blood clotting. A blood test can determine the amount of ... may mean you have an increased risk of blood clotting. This can occur when there is not enough ...

  9. Antithrombin III blood test

    MedlinePlus

    ... be due to: Bone marrow transplant Disseminated intravascular coagulation (DIC) AT III deficiency, an inherited condition Liver ... Schmaier AH, Miller JL. Coagulation and fibrinolysis. In: McPherson ... Management by Laboratory Methods . 22nd ed. Philadelphia, PA: ...

  10. BioSAXS Sample Changer: a robotic sample changer for rapid and reliable high-throughput X-ray solution scattering experiments.

    PubMed

    Round, Adam; Felisaz, Franck; Fodinger, Lukas; Gobbo, Alexandre; Huet, Julien; Villard, Cyril; Blanchet, Clement E; Pernot, Petra; McSweeney, Sean; Roessle, Manfred; Svergun, Dmitri I; Cipriani, Florent

    2015-01-01

    Small-angle X-ray scattering (SAXS) of macromolecules in solution is in increasing demand by an ever more diverse research community, both academic and industrial. To better serve user needs, and to allow automated and high-throughput operation, a sample changer (BioSAXS Sample Changer) that is able to perform unattended measurements of up to several hundred samples per day has been developed. The Sample Changer is able to handle and expose sample volumes of down to 5 µl with a measurement/cleaning cycle of under 1 min. The samples are stored in standard 96-well plates and the data are collected in a vacuum-mounted capillary with automated positioning of the solution in the X-ray beam. Fast and efficient capillary cleaning avoids cross-contamination and ensures reproducibility of the measurements. Independent temperature control for the well storage and for the measurement capillary allows the samples to be kept cool while still collecting data at physiological temperatures. The Sample Changer has been installed at three major third-generation synchrotrons: on the BM29 beamline at the European Synchrotron Radiation Facility (ESRF), the P12 beamline at the PETRA-III synchrotron (EMBL@PETRA-III) and the I22/B21 beamlines at Diamond Light Source, with the latter being the first commercial unit supplied by Bruker ASC. PMID:25615861

  11. BioSAXS Sample Changer: a robotic sample changer for rapid and reliable high-throughput X-ray solution scattering experiments

    PubMed Central

    Round, Adam; Felisaz, Franck; Fodinger, Lukas; Gobbo, Alexandre; Huet, Julien; Villard, Cyril; Blanchet, Clement E.; Pernot, Petra; McSweeney, Sean; Roessle, Manfred; Svergun, Dmitri I.; Cipriani, Florent

    2015-01-01

    Small-angle X-ray scattering (SAXS) of macromolecules in solution is in increasing demand by an ever more diverse research community, both academic and industrial. To better serve user needs, and to allow automated and high-throughput operation, a sample changer (BioSAXS Sample Changer) that is able to perform unattended measurements of up to several hundred samples per day has been developed. The Sample Changer is able to handle and expose sample volumes of down to 5 µl with a measurement/cleaning cycle of under 1 min. The samples are stored in standard 96-well plates and the data are collected in a vacuum-mounted capillary with automated positioning of the solution in the X-ray beam. Fast and efficient capillary cleaning avoids cross-contamination and ensures reproducibility of the measurements. Independent temperature control for the well storage and for the measurement capillary allows the samples to be kept cool while still collecting data at physiological temperatures. The Sample Changer has been installed at three major third-generation synchrotrons: on the BM29 beamline at the European Synchrotron Radiation Facility (ESRF), the P12 beamline at the PETRA-III synchrotron (EMBL@PETRA-III) and the I22/B21 beamlines at Diamond Light Source, with the latter being the first commercial unit supplied by Bruker ASC. PMID:25615861

  12. Mini-beam collimator enables micro-crystallography experiments on standard beamlines.

    SciTech Connect

    Fischetti, R. F.; Xu, S.; Yoder, D. W.; Becker, M.; Venugopalan, N.; Sanishvili, R.; Hilgart, M. C.; Stepanov, S.; Makarov, O.; Smith, J. L.; Biosciences Division

    2009-01-01

    The high-brilliance X-ray beams from undulator sources at third-generation synchrotron facilities are excellent tools for solving crystal structures of important and challenging biological macromolecules and complexes. However, many of the most important structural targets yield crystals that are too small or too inhomogeneous for a 'standard' beam from an undulator source, 25-50 {micro}m (FWHM) in the vertical and 50-100 {micro}m in the horizontal direction. Although many synchrotron facilities have microfocus beamlines for other applications, this capability for macromolecular crystallography was pioneered at ID-13 of the ESRF. The National Institute of General Medical Sciences and National Cancer Institute Collaborative Access Team (GM/CA-CAT) dual canted undulator beamlines at the APS deliver high-intensity focused beams with a minimum focal size of 20 {micro}m x 65 {micro}m at the sample position. To meet growing user demand for beams to study samples of 10 {micro}m or less, a 'mini-beam' apparatus was developed that conditions the focused beam to either 5 {micro}m or 10 {micro}m (FWHM) diameter with high intensity. The mini-beam has a symmetric Gaussian shape in both the horizontal and vertical directions, and reduces the vertical divergence of the focused beam by 25%. Significant reduction in background was achieved by implementation of both forward- and back-scatter guards. A unique triple-collimator apparatus, which has been in routine use on both undulator beamlines since February 2008, allows users to rapidly interchange the focused beam and conditioned mini-beams of two sizes with a single mouse click. The device and the beam are stable over many hours of routine operation. The rapid-exchange capability has greatly facilitated sample screening and resulted in several structures that could not have been obtained with the larger focused beam.

  13. Simulation of the Performance of a Fundamental Neutron Physics Beamline at the High Flux Isotope Reactor.

    PubMed

    Mahurin, Rob; Greene, Geoffrey; Kohler, Paul; Cianciolo, Vince

    2005-01-01

    We study the expected performance of the proposed fundamental neutron physics beamline at the upgraded High Flux Isotope Reactor at Oak Ridge National Laboratory. A curved neutron guide transmits the neutrons from the new cold source into a guide hall. A novel feature of the proposed guide is the use of vertical focussing to increase the flux for experiments that require relatively small cross-section beams. We use the simulation code IB to model straight, multi-channel curved, and tapered guides of various m values. Guide performance for the current NPDGamma and proposed abBA experiments is evaluated. PMID:27308114

  14. FXI: a full-field imaging beamline at NSLS-II

    NASA Astrophysics Data System (ADS)

    Lee, Wah-Keat; Reininger, Ruben; Loo, William; Gambella, Richard; O'Hara, Steven; Chu, Yong S.; Zhong, Zhong; Wang, Jun

    2015-09-01

    The Full-field X-ray Imaging (FXI) beamline at the NSLS-II is designed for optimum performance of a transmission x-ray microscope (TXM). When complete, FXI will enable the TXM to obtain individual 2D projection images at 30 nm spatial resolution and up to 40 microns field of view (FOV) with exposure times of < 50 ms per image. A complete 3D nanotomography data set should take less than 1 minute. This will open opportunities for many real-time in-operando studies.

  15. SUNY beamline facilities at the National Synchrotron Light Source (Final Report)

    SciTech Connect

    Coppens, Philip

    2003-06-22

    The DOE sponsored SUNY synchrotron project has involved close cooperation among faculty at several SUNY campuses. A large number of students and postdoctoral associates have participated in its operation which was centered at the X3 beamline of the National Synchrotron Light Source at Brookhaven National Laboratory. Four stations with capabilities for Small Angle Scattering, Single Crystal and Powder and Surface diffraction and EXAFS were designed and operated with capability to perform experiments at very low as well as elevated temperatures and under high vacuum. A large amount of cutting-edge science was performed at the facility, which in addition provided excellent training for students and postdoctoral scientists in the field.

  16. The Stanford Automated Mounter: pushing the limits of sample exchange at the SSRL macromolecular crystallography beamlines

    PubMed Central

    Russi, Silvia; Song, Jinhu; McPhillips, Scott E.; Cohen, Aina E.

    2016-01-01

    The Stanford Automated Mounter System, a system for mounting and dismounting cryo-cooled crystals, has been upgraded to increase the throughput of samples on the macromolecular crystallography beamlines at the Stanford Synchrotron Radiation Lightsource. This upgrade speeds up robot maneuvers, reduces the heating/drying cycles, pre-fetches samples and adds an air-knife to remove frost from the gripper arms. Sample pin exchange during automated crystal quality screening now takes about 25 s, five times faster than before this upgrade. PMID:27047309

  17. The New X-Ray Lithography Beamline BL1 At DELTA

    SciTech Connect

    Lietz, D.; Paulus, M.; Sternemann, C.; Berges, U.; Hippert, B.; Tolan, M.

    2010-06-23

    Lithography using synchrotron radiation in the x-ray regime provides a powerful method to produce mechanical components of sub-millimeter size with a very good quality for microtechnological applications. In recent years the demand for x-ray lithography beamtime for industrial production of microparts increased rapidly resulting in the development of new experimental endstations at synchrotron radiation sources dedicated for the production of micromechanical devices. We present in this work the layout of the new x-ray lithography beamline BL1 at the synchrotron radiation source DELTA in Dortmund and discuss first results of exposure tests.

  18. Simulation of the Performance of a Fundamental Neutron Physics Beamline at the High Flux Isotope Reactor

    SciTech Connect

    Mahurin, R.; Greene, Geoffrey L; Koehler, Paul Edward; Cianciolo, Vince

    2005-05-01

    We study the expected performance of the proposed fundamental neutron physics beamline at the upgraded High Flux Isotope Reactor at Oak Ridge National Laboratory. A curved neutron guide transmits the neutrons from the new cold source into a guide hall. A novel feature of the proposed guide is the use of vertical focusing to increase the flux for experiments that require relatively small cross-section beams. We use the simulation code IB to model straight, multi-channel curved, and tapered guides of various m values. Guide performance for the current NPDGamma and proposed abBA experiments is evaluated.

  19. SYNCH: A program for design and analysis of synchrotrons and beamlines -- user`s guide

    SciTech Connect

    Garren, A.A.; Kenney, A.S.; Courant, E.D.; Russell, A.D.; Syphers, M.J.

    1993-12-31

    SYNCH is a computer program for use in the design and analysis of synchrotrons, storage rings, and beamlines. It has a large repertoire of commands that can be accessed in a flexible way. The input statements and the results of the calculations they invoke are saved in an internal database so that this information may be shared by other statements. SYNCH is the first accelerator program to organize its input in the form of a language. The statements, which resemble sentences, provide a natural way of describing lattices and invoking relevant calculations. The organization of the program is modular, so that it has been possible to expand its capabilities progressively.

  20. Synchrotron total reflection X-ray fluorescence at BL-16 microfocus beamline of Indus-2

    NASA Astrophysics Data System (ADS)

    Tiwari, M. K.; Singh, A. K.; Das, Gangadhar; Chowdhury, Anupam; Lodha, G. S.

    2014-04-01

    Determination of ultra trace elements is important in many disciplines both in basic and applied sciences. Numerous applications show their importance in medical science, environmental science, materials science, food processing and semiconductor industries and in maintaining the quality control of ultra pure chemicals and reagents. We report commissioning of a synchrotron based total reflection x-ray fluorescence (TXRF) facility on the BL-16 microfocus beamline of Indus-2. This paper describes the performance of the BL-16 TXRF spectrometer and the detailed description of its capabilities through examples of measured results.

  1. CDApps: integrated software for experimental planning and data processing at beamline B23, Diamond Light Source

    PubMed Central

    Hussain, Rohanah; Benning, Kristian; Javorfi, Tamas; Longo, Edoardo; Rudd, Timothy R.; Pulford, Bill; Siligardi, Giuliano

    2015-01-01

    The B23 Circular Dichroism beamline at Diamond Light Source has been operational since 2009 and has seen visits from more than 200 user groups, who have generated large amounts of data. Based on the experience of overseeing the users’ progress at B23, four key areas requiring the most assistance are identified: planning of experiments and note-keeping; designing titration experiments; processing and analysis of the collected data; and production of experimental reports. To streamline these processes an integrated software package has been developed and made available for the users. The subsequent article summarizes the main features of the software. PMID:25723950

  2. Target and orbit feedback simulations of a muSR beamline at BNL

    SciTech Connect

    MacKay, W. W.; Fischer, W.; Blaskiewicz, M.; Pile, P.

    2015-05-03

    Well-polarized positive surface muons are a tool to measure the magnetic properties of materials since the precession rate of the spin can be determined from the observation of the positron directions when the muons decay. The use of the AGS complex at BNL has been explored for a muSR facility previously. Here we report simulations of a beamline with a target inside a solenoidal field, and of an orbit feed-back system with single muon beam positioning monitors based on technology available today

  3. X-ray Experiments for Students at the SLS Optics Beamline

    SciTech Connect

    Flechsig, U.; Jaggi, A.; Krempasky, J.; Oberta, P.; Spielmann, S.; Veen, J. F. van der; Als-Nielsen, J.

    2010-06-23

    We present a X-ray training course for students. The course covers fundamental properties of synchrotron radiation and basic techniques like scattering and absorption. We prepared ten experiments together with a tutorial. The whole course takes about a week. A first student group from the University of Copenhagen passed the course in June 2009. The experiments were performed at the optics beamline of the Swiss Light Source which can be part-time allocated for training purposes. Two experiments are described in more detail: scattering from a hanging drop of water turning into ice and measurement of the power of a pink synchrotron beam using a simple calorimeter.

  4. Simulation of the Performance of a Fundamental Neutron Physics Beamline at the High Flux Isotope Reactor

    PubMed Central

    Mahurin, Rob; Greene, Geoffrey; Kohler, Paul; Cianciolo, Vince

    2005-01-01

    We study the expected performance of the proposed fundamental neutron physics beamline at the upgraded High Flux Isotope Reactor at Oak Ridge National Laboratory. A curved neutron guide transmits the neutrons from the new cold source into a guide hall. A novel feature of the proposed guide is the use of vertical focussing to increase the flux for experiments that require relatively small cross-section beams. We use the simulation code IB to model straight, multi-channel curved, and tapered guides of various m values. Guide performance for the current NPDGamma and proposed abBA experiments is evaluated. PMID:27308114

  5. Pulse generation and preamplification for long pulse beamlines of Orion laser facility.

    PubMed

    Hillier, David I; Winter, David N; Hopps, Nicholas W

    2010-06-01

    We describe the pulse generation, shaping, and preamplification system for the nanosecond beamlines of the Orion laser facility. The system generates shaped laser pulses of up to approximately 1 J of 100 ps-5 ns duration with a programmable temporal profile. The laser has a 30th-power supergaussian spatial profile and is diffraction limited. The system is capable of imposing 2D smoothing by spectral dispersion upon the beam, which will produce a nonuniformity of 10% rms at the target. PMID:20517369

  6. Thermal effects and mirror surface figure requirements for a diagnostic beamline at the Advanced Light Source

    SciTech Connect

    Warwick, T. ); Sharma, S. )

    1991-10-28

    An imaging beamline based on a Kirkpatrick-Baez mirror configuration has been designed to image the electron beam in the ALS storage ring, to measure its size and shape. The electron beam emittance will be small ({epsilon}h = 3.4 {times} 10{sup {minus}9} m rad) and the quality of the image is extremely sensitive to surface figure distortion of the mirrors. Thermal distortions and surface temperatures have been calculated for radiatively cooled mirrors of various materials in a search for a simple design which avoids water cooling. The choice of mirror material and the thermal and mechanical design is discussed. 6 refs.

  7. Development of High Pressure Single Crystal X-Ray Diffraction Study at ESRF ID 30 Beamline

    SciTech Connect

    Dhaussy, A.C.; Mezouar, M.; Mentre, O.

    2004-05-12

    We report about the newly single crystal diffraction set-up development at ID30 beamline at the European Synchrotron Radiation Facility (ESRF). To illustrate the experimental performance of this set-up, we also present X-ray diffraction spectra recorded at high pressure (HP) using dedicated diamond anvil cell (DAC). Using this new setup, high quality synchrotron single crystal X-ray diffraction measurements of Pb2V3O9 have been performed at HP. We evidenced a reordering in the distorted system by resorbing the existing twin. The structure was partially solved by direct methods and refined by the use of the BRUKER suite of programs package.

  8. Beamline considerations for a compact, high current, high power linear RF electron accelerator

    SciTech Connect

    Marder, B.

    1987-06-01

    A design for a compact, high current, high power linear electron accelerator using an rf power source is investigated. It consists of adjacent cavities into which rf power is injected and through which electron pulses pass. The source is assumed to be capable of delivering sufficient rf power to the desired location at the proper phase. Beamline issues such as cavity loading, energy extraction, longitudinal and transverse pulse focusing, and beam breakup are considered. A device which, given the required source, can deliver beam parameters comparable to existing induction accelerators but which is more than an order of magnitude smaller appears feasible.

  9. Synchrotron total reflection X-ray fluorescence at BL-16 microfocus beamline of Indus-2

    SciTech Connect

    Tiwari, M. K. Singh, A. K. Das, Gangadhar Chowdhury, Anupam Lodha, G. S.

    2014-04-24

    Determination of ultra trace elements is important in many disciplines both in basic and applied sciences. Numerous applications show their importance in medical science, environmental science, materials science, food processing and semiconductor industries and in maintaining the quality control of ultra pure chemicals and reagents. We report commissioning of a synchrotron based total reflection x-ray fluorescence (TXRF) facility on the BL-16 microfocus beamline of Indus-2. This paper describes the performance of the BL-16 TXRF spectrometer and the detailed description of its capabilities through examples of measured results.

  10. Justification for the development of a bending magnet beamline at sector 10 at the APS.

    SciTech Connect

    Kemner, K. M.; Biosciences Division

    2006-09-18

    The long-planned and much-needed merger of EnviroCAT into the Materials Research Collaborative Access Team (MR-CAT) will provide dedicated state-of-the-art facilities that are critical to research on a broad range of issues in environmental sciences. These CATs will focus on developing a bending magnet (BM) beamline for x-ray absorption fine structure (XAFS) and micro x-ray analysis of environmental samples through integration with existing insertion device (ID) capabilities in XAFS, micro x-ray analysis, and x-ray scattering. In addition, the expanded MR-CAT will serve as the hub of personnel and laboratory infrastructure support for molecular environmental science and biogeochemical science at the Advanced Photon Source (APS). In conjunction with the merger of EnviroCAT into MR-CAT, the US Environmental Protection Agency (EPA) will become a member institution of MR-CAT, joining the present members (University of Notre Dame, Illinois Institute of Technology, University of Florida, British Petroleum, and Argonne's Chemical Engineering and Biosciences Division). The motivation for blending capabilities meeting the needs of EnviroCAT users into the MR-CAT facilities is the explosion of synchrotron-radiation-based research in the field known as molecular environmental science (MES). This research is driven largely by the need to remediate contaminated environmental materials and to understand the scientific foundations that govern contaminant transport in the environment. Synchrotron radiation is playing a crucial role in solving environmental science problems by offering x-ray-based analytical techniques for detailed molecular- and atomic-level studies of these systems. This document focuses on the scientific justification for developing a specific type of BM beamline capability at Sector 10 for XAFS and micro x-ray analysis to support the growing MES community. However, the modification of Sector 10 will meet other future needs by providing (1) an existing undulator

  11. Beamline I11 at Diamond: A new instrument for high resolution powder diffraction

    NASA Astrophysics Data System (ADS)

    Thompson, S. P.; Parker, J. E.; Potter, J.; Hill, T. P.; Birt, A.; Cobb, T. M.; Yuan, F.; Tang, C. C.

    2009-07-01

    The performance characteristics of a new synchrotron x-ray powder diffraction beamline (I11) at the Diamond Light Source are presented. Using an in-vacuum undulator for photon production and deploying simple x-ray optics centered around a double-crystal monochromator and a pair of harmonic rejection mirrors, a high brightness and low bandpass x-ray beam is delivered at the sample. To provide fast data collection, 45 Si(111) analyzing crystals and detectors are installed onto a large and high precision diffractometer. High resolution powder diffraction data from standard reference materials of Si, α-quartz, and LaB6 are used to characterize instrumental performance.

  12. Active mirror amplifiers for HiPER kiloJoule beamlines

    NASA Astrophysics Data System (ADS)

    Chanteloup, J.-C.; Lucianetti, A.

    2013-11-01

    A major challenge the HiPER [1] project is facing is to derive laser architectures satisfying simultaneously all HiPER requirements; among them, high wall-plug efficiency (15 to 20%) and repetition rate (around 10 Hz) are the most challenging constraints. Several groups over the world are actively pursuing research in the field of High average power Diode Pumped Solid State Lasers (DPSSL) [2]. We propose a comprehensive solution for a 1 kJ DPSSL beamline as the unit brick of a 12 beams bundle.

  13. 100-J level amplifier concepts for HiLASE and ELI-Beamlines

    NASA Astrophysics Data System (ADS)

    Sikocinski, P.; Divoky, M.; Lucianetti, A.; Sawicka, M.; Novak, J.; Rus, B.; Mocek, T.

    2012-07-01

    We present comparison of two alternative layouts of a 100 J cryogenically cooled Yb:YAG multi-slab laser system operating at 10 Hz for HiLASE and ELI Beamlines projects. In the first approach, the 100 J slab amplifier consists of a preamplifier and power amplifier, while in the second approach it uses single power amplifier with two amplifier heads. These two concepts are compared, with respect to output power, B-integral, accumulated B-integral, and peak fluence. Results are obtained by simulating beam propagation in MIRÓ code and calculating stored energy in the amplifier by homemade ray-tracing MATLAB code for amplified spontaneous emission evaluation.

  14. The Stanford Automated Mounter: Pushing the limits of sample exchange at the SSRL macromolecular crystallography beamlines

    DOE PAGESBeta

    Russi, Silvia; Song, Jinhu; McPhillips, Scott E.; Cohen, Aina E.

    2016-02-24

    The Stanford Automated Mounter System, a system for mounting and dismounting cryo-cooled crystals, has been upgraded to increase the throughput of samples on the macromolecular crystallography beamlines at the Stanford Synchrotron Radiation Lightsource. This upgrade speeds up robot maneuvers, reduces the heating/drying cycles, pre-fetches samples and adds an air-knife to remove frost from the gripper arms. As a result, sample pin exchange during automated crystal quality screening now takes about 25 s, five times faster than before this upgrade.

  15. Vacuum upgrade and enhanced performances of the double imaging electron/ion coincidence end-station at the vacuum ultraviolet beamline DESIRS

    NASA Astrophysics Data System (ADS)

    Tang, Xiaofeng; Garcia, Gustavo A.; Gil, Jean-François; Nahon, Laurent

    2015-12-01

    We report here the recent upgrade of the SAPHIRS permanent photoionization end-station at the DESIRS vacuum ultraviolet beamline of synchrotron SOLEIL, whose performances have been enhanced by installing an additional double-skimmer differential chamber. The smaller molecular beam profile obtained at the interaction region has increased the mass resolution of the double imaging photoelectron photoion coincidence (i2PEPICO) spectrometer, DELICIOUS III, installed in the photoionization chamber of the SAPHIRS endstation, by a factor of two, to M/ΔM ˜ 1700 (FWHM). The electron kinetic energy resolution offered by the velocity map imaging (VMI) part of the spectrometer has been improved down to 2.8% (ΔE/E) as we show on the N2 photoionization case in the double skimmer configuration. As a representative example of the overall state-of-the-art i2PEPICO performances, experimental results of the dissociation of state-selected O2+ (B 2 ∑ g - , v+ = 0-6) molecular ions performed at the fixed photon energy of hν = 21.1 eV are presented.

  16. Vacuum upgrade and enhanced performances of the double imaging electron/ion coincidence end-station at the vacuum ultraviolet beamline DESIRS.

    PubMed

    Tang, Xiaofeng; Garcia, Gustavo A; Gil, Jean-François; Nahon, Laurent

    2015-12-01

    We report here the recent upgrade of the SAPHIRS permanent photoionization end-station at the DESIRS vacuum ultraviolet beamline of synchrotron SOLEIL, whose performances have been enhanced by installing an additional double-skimmer differential chamber. The smaller molecular beam profile obtained at the interaction region has increased the mass resolution of the double imaging photoelectron photoion coincidence (i(2)PEPICO) spectrometer, DELICIOUS III, installed in the photoionization chamber of the SAPHIRS endstation, by a factor of two, to M/ΔM ∼ 1700 (FWHM). The electron kinetic energy resolution offered by the velocity map imaging (VMI) part of the spectrometer has been improved down to 2.8% (ΔE/E) as we show on the N2 photoionization case in the double skimmer configuration. As a representative example of the overall state-of-the-art i(2)PEPICO performances, experimental results of the dissociation of state-selected O2(+)(B(2)∑(g)(-), v(+) = 0-6) molecular ions performed at the fixed photon energy of hν = 21.1 eV are presented. PMID:26724007

  17. Fusion Power Demonstration III

    SciTech Connect

    Lee, J.D.

    1985-07-01

    This is the third in the series of reports covering the Fusion Power Demonstration (FPD) design study. This volume considers the FPD-III configuration that incorporates an octopole end plug. As compared with the quadrupole end-plugged designs of FPD-I and FPD-II, this octopole configuration reduces the number of end cell magnets and shortens the minimum ignition length of the central cell. The end-cell plasma length is also reduced, which in turn reduces the size and cost of the end cell magnets and shielding. As a contiuation in the series of documents covering the FPD, this report does not stand alone as a design description of FPD-III. Design details of FPD-III subsystems that do not differ significantly from those of the FPD-II configuration are not duplicated in this report.

  18. In crystallo optical spectroscopy (icOS) as a complementary tool on the macromolecular crystallography beamlines of the ESRF

    PubMed Central

    von Stetten, David; Giraud, Thierry; Carpentier, Philippe; Sever, Franc; Terrien, Maxime; Dobias, Fabien; Juers, Douglas H.; Flot, David; Mueller-Dieckmann, Christoph; Leonard, Gordon A.; de Sanctis, Daniele; Royant, Antoine

    2015-01-01

    The analysis of structural data obtained by X-ray crystallo­graphy benefits from information obtained from complementary techniques, especially as applied to the crystals themselves. As a consequence, optical spectroscopies in structural biology have become instrumental in assessing the relevance and context of many crystallographic results. Since the year 2000, it has been possible to record such data adjacent to, or directly on, the Structural Biology Group beamlines of the ESRF. A core laboratory featuring various spectrometers, named the Cryobench, is now in its third version and houses portable devices that can be directly mounted on beamlines. This paper reports the current status of the Cryobench, which is now located on the MAD beamline ID29 and is thus called the ID29S-Cryobench (where S stands for ‘spectroscopy’). It also reviews the diverse experiments that can be performed at the Cryobench, highlighting the various scientific questions that can be addressed. PMID:25615856

  19. DEIMOS: A beamline dedicated to dichroism measurements in the 350–2500 eV energy range

    SciTech Connect

    Ohresser, P. Otero, E.; Choueikani, F.; Chen, K.; Stanescu, S.; Deschamps, F.; Moreno, T.; Polack, F.; Lagarde, B.; Daguerre, J.-P.; Marteau, F.; Scheurer, F.; Joly, L.; Muller, B.; Kappler, J.-P.; Bunau, O.; Sainctavit, Ph.

    2014-01-15

    The DEIMOS (Dichroism Experimental Installation for Magneto-Optical Spectroscopy) beamline was part of the second phase of the beamline development at French Synchrotron SOLEIL (Source Optimisée de Lumière à Energie Intermédiaire du LURE) and opened to users in March 2011. It delivers polarized soft x-rays to perform x-ray absorption spectroscopy, x-ray magnetic circular dichroism, and x-ray linear dichroism in the energy range 350–2500 eV. The beamline has been optimized for stability and reproducibility in terms of photon flux and photon energy. The main end-station consists in a cryo-magnet with 2 split coils providing a 7 T magnetic field along the beam or 2 T perpendicular to the beam with a controllable temperature on the sample from 370 K down to 1.5 K.

  20. Photon transport of the superradiant TeraFERMI THz beamline at the FERMI free-electron laser.

    PubMed

    Svetina, Cristian; Mahne, Nicola; Raimondi, Lorenzo; Perucchi, Andrea; Di Pietro, Paola; Lupi, Stefano; Schmidt, Bernhard; Zangrando, Marco

    2016-01-01

    TeraFERMI is the new terahertz (THz) beamline for pump-probe studies on the femtosecond time-scale, under construction at the FERMI free-electron laser (FEL) facility in Trieste, Italy. The beamline will take advantage of the coherent radiation emitted by the spent electrons from the FEL undulators, before being dumped. This will result in short, coherent, high-power THz pulses to be used as a pump beam, in order to modulate structural properties of matter, thereby inducing phase transitions. The TeraFERMI beamline collects THz radiation in the undulator hall and guides it along a beam pipe which is approximately 30 m long, extending across the safety hutch and two shielding walls. Here the optical design, which will allow the efficient transport of the emitted THz radiation in the experimental hall, is presented. PMID:26698051

  1. Parallel-beam imaging at the ESRF beamline ID19: current status and plans for the future

    SciTech Connect

    Weitkamp, T.; Tafforeau, P.; Boller, E.; Cloetens, P.; Valade, J.-P.; Bernard, P.; Baruchel, J.; Peyrin, F.; Helfen, L.

    2010-06-23

    The ESRF synchrotron beamline ID19, dedicated to full-field parallel-beam imaging techniques such as phase-contrast and absorption microtomography and X-ray topography, is one of the most versatile instruments of its kind. This paper presents key characteristics of ID19 in its present form, names examples for research and development performed on the beamline, and outlines the plans for an upgrade on the beamline in coming years, to adapt to the growing needs of the user community. The technical goals envisioned include an increase in available beam size and maximum photon energy, and a substantial increase in flux density for applications using beams of small and intermediate size.

  2. Commissioning and performance of the variable line spacing plane grating monochromator beamline at the Canadian Light Source

    SciTech Connect

    Hu, Y. F.; Zuin, L.; Wright, G.; Igarashi, R.; McKibben, M.; Wilson, T.; Chen, S. Y.; Johnson, T.; Maxwell, D.; Yates, B. W.; Sham, T. K.; Reininger, R.

    2007-08-15

    The variable line spacing plane grating monochromator beamline at the Canadian Light Source (CLS) employs three grazing incidence variable line spacing gratings to cover a photon energy range of 5-250 eV. It uses a 185 mm period length planar permanent magnet insertion device as the photon source, sharing a straight section with another soft x-ray beamline at the CLS. The commissioning and performance of the beamline is reported. The high resolution photoabsorption spectra of Ar and PF{sub 5} gases are reported. A resolving power of over 40 000 for photons in the low energy region and >10 000 for a wider energy range (8-200 eV) can be achieved. A photon flux of up to 2x10{sup 12} photons/s per 100 mA with slit settings of 50 {mu}m has been measured.

  3. Pioneer III Probe

    NASA Technical Reports Server (NTRS)

    1961-01-01

    Looking more like surgeons, these technicians wearing 'cleanroom' attire inspect the Pioneer III probe before shipping it to Cape Canaveral, Florida. Pioneer III was launched on December 6, 1958 aboard a Juno II rocket at the Atlantic Missile Range, Cape Canaveral, Florida. The mission objectives were to measure the radiation intensity of the Van Allen radiation belt, test long range communication systems, the launch vehicle and other subsystems. The Juno II failed to reach proper orbital escape velocity. The probe re-entered the Earth's atmosphere on December 7th ending its brief mission.

  4. An X-ray microsource based system for crystal screening and beamline development during synchrotron shutdown periods

    PubMed Central

    Miller, Mitchell D.; Deacon, Ashley M.

    2007-01-01

    Crystallographic end-stations require a significant investment in state-of-the-art equipment, as well as a significant effort in software development. The equipment often sits idle during annual maintenance shutdowns. In order to utilize the existing hardware and software during these shutdowns, we installed a sealed-tube microsource X-ray generator in the beamline 9-2 hutch at Stanford Synchrotron Radiation Laboratory. A multi-layer optic provides good flux and spectral purity. The small physical size of the source, the long optic to focus distance (635 mm) and the short source to optic distance (65 mm) allowed the use of existing beamline components, without any significant modification. The system replaces a short section of beam pipe upstream of the beam conditioning slits and shutter. The system can be installed and removed from the beamline in less than 1 day. The Joint Center for Structural Genomics (JCSG) and SSRL Structural Molecular Biology group developed the Stanford Automated Mounting (SAM) system and installed it on beamlines at SSRL. The JCSG relies on this system to test crystals for diffraction. The installation of the X-ray microsource in beamline 9-2 allowed crystal screening to continue during SSRL shutdowns. Using a standard screening protocol of two 10 minute exposures, separated by a 90° phi rotation, the system was capable of screening up to 400 crystals per week and was left to run unattended for up to 4 days. Over 8200 crystals were screened during the last four SSRL shutdown periods. An X-ray generator can also be useful for ongoing beamline development. Shutdown periods provide easier access to the experimental hardware, however, some tests require beam. The X-ray microsource offers the ability to conduct these tests during periods when users are not scheduled. PMID:19005562

  5. Facilitating best practices in collecting anomalous scattering data for de novo structure solution at the ESRF Structural Biology Beamlines

    PubMed Central

    de Sanctis, Daniele; Oscarsson, Marcus; Popov, Alexander; Svensson, Olof; Leonard, Gordon

    2016-01-01

    The constant evolution of synchrotron structural biology beamlines, the viability of screening protein crystals for a wide range of heavy-atom derivatives, the advent of efficient protein labelling and the availability of automatic data-processing and structure-solution pipelines have combined to make de novo structure solution in macromolecular crystallography a less arduous task. Nevertheless, the collection of diffraction data of sufficient quality for experimental phasing is still a difficult and crucial step. Here, some examples of good data-collection practice for projects requiring experimental phasing are presented and recent developments at the ESRF Structural Biology beamlines that have facilitated these are illustrated. PMID:26960128

  6. Development of diffraction enhanced imaging at beamline BL07 at the SAGA Light Source and its application

    NASA Astrophysics Data System (ADS)

    Sumitani, Kazushi; Ishiji, Kotaro; Kawamoto, Masahide; Yoneyama, Akio; Tabata, Masaaki; Okajima, Toshihiro; Hirai, Yasuharu

    2013-03-01

    We have developed a diffraction enhanced imaging (DEI) system at beamline BL07 at the SAGA Light Source. BL07 is a beamline for using high energy X-rays up to 35 keV generated from a superconducting wiggler placed in the straight section of the storage ring. The DEI measurement system is composed of a Si(220) asymmetric crystal for expanding the beam, a Si(220) crystal analyser, and a high-resolution CCD camera. We demonstrated the observation of a rope recovered from the ruins of the Mietsu Navy in Japan.

  7. Measurement of the repeatability of the prompt flashlamp-induced wavefront aberration on beamlines at the National Ignition Facility

    NASA Astrophysics Data System (ADS)

    Homoelle, Doug; Bowers, Mark W.; Budge, Tracy; Haynam, Chris; Heebner, John; Hermann, Mark; Jancaitis, Ken; Jarboe, Jeff; Lafortune, Kai; Thaddeus Salmon, Joseph; Schindler, Tania; Shaw, Mike

    2011-08-01

    We have undertaken a measurement campaign to determine the repeatability of the prompt flashlamp-induced wavefront aberration on beamlines at the National Ignition Facility (NIF) and determine the extent to which shot-to-shot variations in this aberration may degrade the performance of a proposed adaptive optics system for the short-pulse Advanced Radiographic Capability beamline on NIF. In this paper we will describe the unique NIF configuration that was required to make this measurement, present the results of the experiment, and discuss the implications of these results for the adaptive optics system design.

  8. Design, development and first experiments on the X-ray imaging beamline at Indus-2 synchrotron source RRCAT, India.

    PubMed

    Agrawal, A K; Singh, B; Kashyap, Y S; Shukla, M; Sarkar, P S; Sinha, Amar

    2015-11-01

    A full-field hard X-ray imaging beamline (BL-4) was designed, developed, installed and commissioned recently at the Indus-2 synchrotron radiation source at RRCAT, Indore, India. The bending-magnet beamline is operated in monochromatic and white beam mode. A variety of imaging techniques are implemented such as high-resolution radiography, propagation- and analyzer-based phase contrast imaging, real-time imaging, absorption and phase contrast tomography etc. First experiments on propagation-based phase contrast imaging and micro-tomography are reported. PMID:26524319

  9. Non-destructive single-pass low-noise detection of ions in a beamline.

    PubMed

    Schmidt, Stefan; Murböck, Tobias; Andelkovic, Zoran; Birkl, Gerhard; Nörtershäuser, Wilfried; Stahl, Stefan; Vogel, Manuel

    2015-11-01

    We have conceived, built, and operated a device for the non-destructive single-pass detection of charged particles in a beamline. The detector is based on the non-resonant pick-up and subsequent low-noise amplification of the image charges induced in a cylindrical electrode surrounding the particles' beam path. The first stage of the amplification electronics is designed to be operated from room temperature down to liquid helium temperature. The device represents a non-destructive charge counter as well as a sensitive timing circuit. We present the concept and design details of the device. We have characterized its performance and show measurements with low-energy highly charged ions (such as Ar(13+)) passing through one of the electrodes of a cylindrical Penning trap. This work demonstrates a novel approach of non-destructive, low noise detection of charged particles which is, depending on the bunch structure, suitable, e.g., for ion traps, low-energy beamlines or accelerator transfer sections. PMID:26628124

  10. Non-destructive single-pass low-noise detection of ions in a beamline

    SciTech Connect

    Schmidt, Stefan; Murböck, Tobias; Birkl, Gerhard; Andelkovic, Zoran; Vogel, Manuel; Nörtershäuser, Wilfried; Stahl, Stefan

    2015-11-15

    We have conceived, built, and operated a device for the non-destructive single-pass detection of charged particles in a beamline. The detector is based on the non-resonant pick-up and subsequent low-noise amplification of the image charges induced in a cylindrical electrode surrounding the particles’ beam path. The first stage of the amplification electronics is designed to be operated from room temperature down to liquid helium temperature. The device represents a non-destructive charge counter as well as a sensitive timing circuit. We present the concept and design details of the device. We have characterized its performance and show measurements with low-energy highly charged ions (such as Ar{sup 13+}) passing through one of the electrodes of a cylindrical Penning trap. This work demonstrates a novel approach of non-destructive, low noise detection of charged particles which is, depending on the bunch structure, suitable, e.g., for ion traps, low-energy beamlines or accelerator transfer sections.

  11. Ultrafast beam dump materials and mirror coatings tested with the ELI beamlines LIDT test station

    NASA Astrophysics Data System (ADS)

    Durák, Michal; Kramer, Daniel; Velpula, Praveen K.; Cupal, Josef; Medřík, TomáÅ.¡; Hřebíček, Jan; Golasowski, Jiří; Peceli, Davorin; Fekete, Ladislav; Å tepán, Václav; Kozlová, Michaela; Rus, Bedřich

    2015-11-01

    The ELI Beamlines project will deliver ultrafast laser pulses with peak powers up to 10PW available every minute and PW class beams at 10Hz complemented by a 10TW 1kHz beamline. To properly determine damage thresholds of involved optical components in conditions similar to the operational environment and with expected laser parameters, a high vacuum LIDT test station was constructed at PALS facility. Our study presents results of ISO based S-on-1 and R-on-1 tests in femtosecond regime (50fs, 800nm, 10Hz/1kHz) performed on two different types of coatings: a) highabsorption black coatings with low outgassing rates, intended for use as a beam dump surface; and b) high-reflectivity, low-dispersion 45° AOI ultrafast mirror coatings. Testing of absorptive coatings was accompanied with QMS residual gas analysis to verify, that high intensity laser radiation approaching the damage threshold does not increase concentration of volatile organic compounds in the vacuum chamber. In case of HR mirror coatings, we also investigate the effect of cleaning on LIDT value, comparing characteristic S-on-1 curves of given sample with values obtained after 12h immersion in ethanol-water solution.

  12. Apparatus to study crystal channeling and volume reflection phenomena at the SPS H8 beamline

    SciTech Connect

    Scandale, Walter; Efthymiopoulos, Ilias; Still, Dean A.; Carnera, Alberto; De Salvador, Davide; Della Mea, Gianantonio; Milan, Riccardo; Vomiero, Alberto; Baricordi, Stefano; Chiozzi, Stefano; Dalpiaz, Pietro; Damiani, Chiara; Fiorini, Massimiliano; Guidi, Vincenzo; Martinelli, Giuliano; Mazzolari, Andrea; Milan, Emiliano; Ambrosi, Giovanni; Azzarello, Philipp; Battiston, Roberto

    2008-02-15

    A high performance apparatus has been designed and built by the H8-RD22 collaboration for the study of channeling and volume reflection phenomena in the interaction of 400 GeV/c protons with bent silicon crystals, during the 2006 data taking in the external beamline H8 of the CERN SPS. High-quality silicon short crystals were bent by either anticlastic or quasimosaic effects. Alignment with the highly parallel (8 {mu}rad divergence) proton beam was guaranteed through a submicroradian goniometric system equipped with both rotational and translational stages. Particle tracking was possible by a series of silicon microstrip detectors with high-resolution and a parallel plate gas chamber, triggered by various scintillating detectors located along the beamline. Experimental observation of volume reflection with 400 GeV/c protons proved true with a deflection angle of (10.4{+-}0.5) {mu}rad with respect to the unperturbed beam, with a silicon crystal whose (111) planes were parallel to the beam.

  13. The life science X-ray scattering beamline at NSLS-II

    SciTech Connect

    DiFabio, Jonathan; Yang, Lin; Chodankar, Shirish; Pjerov, Sal; Jakoncic, Jean; Lucas, Michael; Krywka, Christina; Graziano, Vito

    2015-09-30

    We report the current development status of the High Brightness X-ray Scattering for Life Sciences (or Life Science X-ray Scattering, LiX) beamline at the NSLS-II facility of Brookhaven National Laboratory. This instrument will operate in the x-ray energy range of 2.1-18 keV, provide variable beam sizes from 1 micron to ~0.5 mm, and support user experiments in three scientific areas: (1) high-throughput solution scattering, in-line size exclusion chromatography and flow mixers-based time-resolved solution scattering of biological macro-molecules, (2) diffraction from single- and multi-layered lipid membranes, and (3) scattering-based scanning probe imaging of biological tissues. In order to satisfy the beam stability required for these experiments and to switch rapidly between different types of experiments, we have adopted a secondary source with refractive lenses for secondary focusing, a detector system consisting of three Pilatus detectors, and specialized experimental modules that can be quickly exchanged and each dedicated to a defined set of experiments. The construction of this beamline is on schedule for completion in September 2015. User experiments are expected to start in Spring 2016.

  14. Particle optics and accelerator modeling software for industrial and laboratory beamline design

    NASA Astrophysics Data System (ADS)

    Gillespie, George H.; Hill, Barrey W.

    1998-04-01

    The expanding variety of accelerator applications in research and industry places increased demands upon scientists and engineers involved in developing new accelerator and beamline designs. Computer codes for particle optics simulation have always played an important role in the design process and enhanced software tools offer the promise of improved productivity for beamline designers. This paper summarizes recent work on the development of advanced graphic user interface (GUI) software components, that can be linked directly to many of the standard particle optics programs used in the accelerator community, and which are aimed at turning that promise of improved productivity into a reality. An object oriented programming (OOP) approach has been adopted and a number of GUI components have been developed that run on several different operating systems. The emphasis is on assisting users in the setup and running of the optics programs without requiring any knowledge of the format, syntax, or similar requirements of the input. The components are being linked with several popular optics programs, including TRANSPORT, TURTLE, TRACE 3-D and PARMILA, to form integrated easy-to-use applications. Several advanced applications linking the GUI components with Lie algebra and other high-order simulation codes, as well as system level and facility modeling codes, are also under development. An overview of the work completed to date is presented, and examples of the new tools running on the Windows 95 operating system are illustrated.

  15. g4beamline Simulations of Parametric Resonance Ionization Cooling of Muon Beams

    SciTech Connect

    Kevin Beard; Slawomir Bogacz; Yaroslav Derbenev; Katsuya Yonehara; Rolland P. Johnson; Kevin Paul; Thomas J. Roberts

    2005-09-19

    The technique of using a parametric resonance to allow better ionization cooling is being developed to create small beams so that high collider luminosity can be achieved with fewer muons. While parametric resonance ionization (PIC) cooling of muons has been shown to work in matrix-based simulations when the system is properly tuned, doing the same using a much more detailed GEANT-based g4beamline [1] simulation has proven more difficult. The starting point for this work is a the linear channel; a half integer resonance is induced such that the normal elliptical motion of particles in x-x' phase space becomes hyperbolic, with particles moving to smaller x and larger x' as they pass down the channel. Thin absorbers placed at the focal points of the channel then cool the angular divergence of the beam by the usual ionization cooling mechanism where each absorber is followed by RF cavities. Thus the phase space of the beam is compressed in transverse position by the dynamics of the resonance and its angular divergence is compressed by the ionization cooling mechanism. The g4beamline and OptiM [2] simulations show the importance of synchrotron motion as an averaging mechanism for chromatic detuning. Multiple scattering and energy straggling play a significant role that must be addressed via further optimizations and additional compensation solutions.

  16. A new paradigm for macromolecular crystallography beamlines derived from high-pressure methodology and results

    PubMed Central

    Fourme, Roger; Girard, Eric; Dhaussy, Anne-Claire; Medjoubi, Kadda; Prangé, Thierry; Ascone, Isabella; Mezouar, Mohamed; Kahn, Richard

    2011-01-01

    Biological structures can now be investigated at high resolution by high-pressure X-ray macromolecular crystallography (HPMX). The number of HPMX studies is growing, with applications to polynucleotides, monomeric and multimeric proteins, complex assemblies and even a virus capsid. Investigations of the effects of pressure perturbation have encompassed elastic compression of the native state, study of proteins from extremophiles and trapping of higher-energy conformers that are often of biological interest; measurements of the compressibility of crystals and macromolecules were also performed. HPMX results were an incentive to investigate short and ultra-short wavelengths for standard biocrystallography. On cryocooled lysozyme crystals it was found that the data collection efficiency using 33 keV photons is increased with respect to 18 keV photons. This conclusion was extended from 33 keV down to 6.5 keV by exploiting previously published data. To be fully exploited, the potential of higher-energy photons requires detectors with a good efficiency. Accordingly, a new paradigm for MX beamlines was suggested, using conventional short and ultra-short wavelengths, aiming at the collection of very high accuracy data on crystals under standard conditions or under high pressure. The main elements of such beamlines are outlined. PMID:21169687

  17. First tests of the ion irradiation and implantation beamline at the CMAM

    NASA Astrophysics Data System (ADS)

    Jiménez-Rey, D.; Benedicto, M.; Muñoz-Martín, A.; Bachiller-Perea, D.; Olivares, J.; Climent-Font, A.; Gómez-Ferrer, B.; Rodríguez, A.; Narros, J.; Maira, A.; Álvarez, J.; Nakbi, A.; Zucchiatti, A.; de Aragón, F.; García, J. M.; Vila, R.

    2014-07-01

    The implantation and irradiation beamline of the Tandem ion accelerator of the Centro de Micro Análisis de Materiales (CMAM), in Madrid, has been recently completed with a beam sweep and monitoring system, and a cryostat/furnace. These new implementations convert the beamline into a versatile tool to implant ions, between H and Au2, in different materials with precise control of the sample temperature, which may be varied between -180 °C and 600 °C. The size of the swept area on target may be as large as 10 × 10 cm2. The implantation chamber also allows carrying out in situ or/and on line analyses during the irradiations by means of advanced optical measurements, as well as ion beam analyses (IBA). These advancements can be employed in novel applications such as the fabrication of optical waveguides and irradiation tests of structural and functional materials for future fusion reactors. The results of beam tests and first experiments are shown.

  18. A short-pulse X-ray beamline for spectroscopy and scattering.

    PubMed

    Reininger, R; Dufresne, E M; Borland, M; Beno, M A; Young, L; Evans, P G

    2014-09-01

    Experimental facilities for picosecond X-ray spectroscopy and scattering based on RF deflection of stored electron beams face a series of optical design challenges. Beamlines designed around such a source enable time-resolved diffraction, spectroscopy and imaging studies in chemical, condensed matter and nanoscale materials science using few-picosecond-duration pulses possessing the stability, high repetition rate and spectral range of synchrotron light sources. The RF-deflected chirped electron beam produces a vertical fan of undulator radiation with a correlation between angle and time. The duration of the X-ray pulses delivered to experiments is selected by a vertical aperture. In addition to the radiation at the fundamental photon energy in the central cone, the undulator also emits the same photon energy in concentric rings around the central cone, which can potentially compromise the time resolution of experiments. A detailed analysis of this issue is presented for the proposed SPXSS beamline for the Advanced Photon Source. An optical design that minimizes the effects of off-axis radiation in lengthening the duration of pulses and provides variable X-ray pulse duration between 2.4 and 16 ps is presented. PMID:25178012

  19. The life science X-ray scattering beamline at NSLS-II

    DOE PAGESBeta

    DiFabio, Jonathan; Yang, Lin; Chodankar, Shirish; Pjerov, Sal; Jakoncic, Jean; Lucas, Michael; Krywka, Christina; Graziano, Vito

    2015-09-30

    We report the current development status of the High Brightness X-ray Scattering for Life Sciences (or Life Science X-ray Scattering, LiX) beamline at the NSLS-II facility of Brookhaven National Laboratory. This instrument will operate in the x-ray energy range of 2.1-18 keV, provide variable beam sizes from 1 micron to ~0.5 mm, and support user experiments in three scientific areas: (1) high-throughput solution scattering, in-line size exclusion chromatography and flow mixers-based time-resolved solution scattering of biological macro-molecules, (2) diffraction from single- and multi-layered lipid membranes, and (3) scattering-based scanning probe imaging of biological tissues. In order to satisfy the beammore » stability required for these experiments and to switch rapidly between different types of experiments, we have adopted a secondary source with refractive lenses for secondary focusing, a detector system consisting of three Pilatus detectors, and specialized experimental modules that can be quickly exchanged and each dedicated to a defined set of experiments. The construction of this beamline is on schedule for completion in September 2015. User experiments are expected to start in Spring 2016.« less

  20. Scheme of Laser-Compton Gamma-ray Beamline in SAGA-LS

    SciTech Connect

    Ohgaki, H.; Koda, S.; Iwasaki, Y.; Takabayashi, Y.; Yoshida, K.; Tomimasu, T.; Uozumi, Y.; Ishibashi, K.

    2007-01-19

    A Laser-Compton Gamma-ray beamline in SAGA-LS has been planned to investigate the nuclear science and technology. The electron beam energy of 1.4 GeV and a small emittance are attractive to generate an intense and narrow energy bandwidth of Laser-Compton gamma-ray beam in MeV-region. Thus a design work for a gamma-ray beamline has been performed. Since the electron energy will be fixed, 1.4 GeV, for SR users, the laser wavelength should be variable to tune the energy of the gamma-ray beam. An OPO-DFG laser is one of candidate for this purpose. However, the laser power is not high enough to obtain the gamma-ray yield of -106 photons/s/100mA. The other method to tune the energy of gamma-ray beam is selecting the scattering angle by using a collimator and an absorber. However, simulation shows that the collimator-absorber scheme produce a poor bandwidth of the gamma-ray beam. An acceptable performance beam can be obtained by controlling the energy of electron beam at present stage.

  1. Elliptically polarizing undulator beamline 4.0.1 for magnetic spectroscopy at the Advanced Light Source

    SciTech Connect

    Martynov, V.V.; Young, A.T.; Padmore, H.A.

    1996-08-01

    A beamline for high resolution spectroscopy with elliptically polarized X-rays is described.The working energy range is large, from 20 eV to above 1800 eV. The resolving power is on the order of 10,000 at low energies (20-200 eV) and 6000 at high energies (200-1800 eV). This is achieved using a variable deviation angle plane grating monochromator. A single grating, with one line density and a varying groove depth, is used to cover the entire energy range. The beamline has been designed to operate with either one or two x-ray beams propagating simultaneously through the monochromator and to the experimental station. Switching between polarizations at rates of 0.1 Hz and slower is accomplished in the single beam mode by alternating the output of the elliptically polarized undulator source between left and right polarization. Fast polarization switching, at rates of 100-1000 Hz, is provided in the two beam mode by mechanical chopping between two photon beams, one of which is right circularly polarized, and the other left circularly polarized.

  2. Support for the Advanced Polymers Beamline at the National Synchrotron Light Source

    SciTech Connect

    Hsiao, Benjamin S

    2008-10-01

    The primary focus of the X27C beamline is to investigate frontier polymer science and engineering problems with emphasis on real-time studies of structures, morphologies and dynamics from atomic, nanoscopic, microscopic to mesoscopic scales using simultaneous small-angle X-ray scattering (SAXS) and wide-angle X-ray diffraction (WAXD) techniques. The scientific merit of this project is as follows. Currently, many unique sample chambers for in-situ synchrotron studies, developed by the PI (B. Hsiao) and Co-PI (B. Chu), are available for general users of X27C at NSLS. These instruments include a gel/melt spinning apparatus, a continuous fiber drawing apparatus, a tensile stretching apparatus, a high pressure X-ray cell using supercritical carbon dioxide, a parallel plate strain-controlled shear stage and a dynamic rheometer for small-strain oscillatory deformation study. Based on the use of these instruments in combination with synchrotron X-rays, many new insights into the relationships between processing and structure have been obtained in recent years. The broader impact of this project is as follows. The X27C beamline is the first synchrotron facility in the United States dedicated to chemistry/materials research (with emphasis on polymers). The major benefit of this facility to the materials community is that no extensive synchrotron experience and equipment preparation are required from general users to carry out cutting-edge experiments.

  3. Evaluation of different synchrotron beamline configurations for X-ray fluorescence analysis of environmental samples.

    PubMed

    Barberie, Sean R; Iceman, Christopher R; Cahill, Catherine F; Cahill, Thomas M

    2014-08-19

    Synchrotron radiation X-ray fluorescence (SR-XRF) is a powerful elemental analysis tool, yet synchrotrons are large, multiuser facilities that are generally not amenable to modification. However, the X-ray beamlines from synchrotrons can be modified by simply including X-ray filters or removing monochromators to improve the SR-XRF analysis. In this study, we evaluated four easily applied beamline configurations for the analysis of three representative environmental samples, namely a thin aerosol sample, an intermediate thickness biological sample, and a thick rare earth mineral specimen. The results showed that the "white beam" configuration, which was simply the full, polychromatic output of the synchrotron, was the optimal configuration for the analysis of thin samples with little mass. The "filtered white beam" configuration removed the lower energy X-rays from the excitation beam so it gave better sensitivity for elements emitting more energetic X-rays. The "filtered white beam-filtered detector" configuration sacrifices the lower energy part of the spectrum (<15 keV) for improved sensitivity in the higher end (∼26 to 48 keV range). The use of a monochromatic beam, which tends to be the standard mode of operation for most SR-XRF analyses reported in the literature, gave the least sensitive analysis. PMID:25025342

  4. New Developments at the XMaS Beamline For Magnetic and High Resolution Diffraction

    SciTech Connect

    Thompson, P.B.J.; Bouchenoire, L.; Brown, S.D.; Mannix, D.; Paul, D.F.; Lucas, C.; Kervin, J.; Cooper, M.J.; Arakawa, P.; Laughon, G.

    2004-05-12

    We report here on a number of developments that include enhancements of the sample environment on the XMaS beamline and the flux available at low energy. A 4 Tesla superconducting magnet has been designed to fit within the Euler cradle of a six circle Huber diffractometer, allowing scattering in both horizontal and vertical planes. The geometry of the magnet allows the application of longitudinal, transverse horizontal, and vertical fields. A further conventional magnet ({approx} 0.1 T) to minimize air absorption at low energies ({approx} 3KeV) has been designed for two circle applications, such as reflectivity. A novel in-vacuum slit screen has been developed, also minimizing absorption at low energies. New equipment for performing in-situ studies of surfaces in the electrochemical environment has been developed to allow control of the solution and sample temperature over the region of -5C to 80C. Preliminary experiments on the surface reconstructions of Au(111) in an electrolyte have been performed, whilst commissioning at the same time a MAR CCD detector for the beamline.

  5. UV-CD12: synchrotron radiation circular dichroism beamline at ANKA

    PubMed Central

    Bürck, Jochen; Roth, Siegmar; Windisch, Dirk; Wadhwani, Parvesh; Moss, David; Ulrich, Anne S.

    2015-01-01

    Synchrotron radiation circular dichroism (SRCD) is a rapidly growing technique for structure analysis of proteins and other chiral biomaterials. UV-CD12 is a high-flux SRCD beamline installed at the ANKA synchrotron, to which it had been transferred after the closure of the SRS Daresbury. The beamline covers an extended vacuum-UV to near-UV spectral range and has been open for users since October 2011. The current end-station allows for temperature-controlled steady-state SRCD spectroscopy, including routine automated thermal scans of microlitre volumes of water-soluble proteins down to 170 nm. It offers an excellent signal-to-noise ratio over the whole accessible spectral range. The technique of oriented circular dichroism (OCD) was recently implemented for determining the membrane alignment of α-helical peptides and proteins in macroscopically oriented lipid bilayers as mimics of cellular membranes. It offers improved spectral quality <200 nm compared with an OCD setup adapted to a bench-top instrument, and accelerated data collection by a factor of ∼3. In addition, it permits investigations of low hydrated protein films down to 130 nm using a rotatable sample cell that avoids linear dichroism artifacts. PMID:25931105

  6. Commissioning and performance of X-ray absorption spectroscopy beamline at the Siam Photon Laboratory

    NASA Astrophysics Data System (ADS)

    Klysubun, W.; Sombunchoo, P.; Wongprachanukul, N.; Tarawarakarn, P.; Klinkhieo, S.; Chaiprapa, J.; Songsiriritthigul, P.

    2007-11-01

    We report commissioning results and performance of X-ray absorption spectroscopy (XAS) beamline, BL-8, at the Siam Photon Laboratory. BL-8 has been opened for users since the year 2006. It is tunable by a fixed-exit double crystal monochromator equipped with InSb(1 1 1), Si(1 1 1), and Ge(2 2 0) crystals covering photon energy from 1830 to 9000 eV. Thus elemental absorption K-edges of silicon up to copper can be investigated. Other heavier elements may be studied via their L or M edges. The front end is windowless and the beamline is terminated with a Kapton window followed by the XAS station equipped with ionization chambers for transmission-mode measurements. The measured photon flux at sample is approximately 10 8-10 10 photons/s/100 mA for the 1 mm×10 mm beam size. The commissioning XANES spectra of sulfur standards and EXAFS spectra of copper are presented.

  7. Surface and interface analysis of nanomaterials at microfocus beamline (BL-16) of Indus-2

    NASA Astrophysics Data System (ADS)

    Das, Gangadhar; Khooha, Ajay; Kane, S. R.; Singh, A. K.; Tiwari, M. K.

    2016-05-01

    Analysis of chemical nature and electronic structure at the interface of a thin film medium is important in many technological applications as well as to understand overall efficiency of a thin film device. Synchrotron radiation based x-ray spectroscopy is a promising technique to study interface nature of the nanomaterials with atomic resolutions. A combined x-ray reflectivity and grazing incidence x-ray fluorescence measurement facility has been recently constructed at the BL-16 microfocus beamline of Indus-2 synchrotron facility to accomplish surface-interface microstructural characterization of thin layered materials. It is also possible to analyze contaminates or adsorbed ad-atoms on the surface of the thin nanostructure materials. The BL-16 beamline also provides an attractive platform to perform a variety of analytical research activities especially in the field of micro x-ray fluorescence and ultra-trace elements analysis using Synchrotron radiation. We describe various salient features of the BL-16 reflectometer experimental station and the detailed description of its capabilities through the measured results, obtained for various thin layered nanomaterials.

  8. Beamline and exposure station for deep x-ray lithography at the Advanced Photon Source

    SciTech Connect

    Lai, B.; Mancini, D.C.; Yun, W.; Gluskin, E.

    1996-12-31

    APS is a third-generation synchrotron radiation source. With an x-ray energy of 19.5 keV and highly collimated beam (<0.1 mrad), APS is well suited for producing high-aspect-ratio microstructures in thick resist films (> 1 mm) using deep x-ray lithography (DXRL). The 2-BM beamline was constructed and will be used for DXRL at APS. Selection of appropriate x-ray energy range is done through a variable-angle mirror and various filters in the beamline. At the exposure station, the beam size will be 100(H) x 5(V) mm{sup 2}. Uniform exposure will be achieved by a high-speed (100 mm/sec) vertical scanner, which allows precise angular ({approximately}0.1 mrad) and positional (< 1 {mu}m) control of the sample, allowing full use of the highly collimated beam for lateral accuracy and control of sidewall slopes during exposure of thick resists, as well as generation of conicals and other profiles. For 1-mm-thick PMMA, a 100 x 25 mm{sup 2} area can be fully exposed in about 1/2 hr, while even 10-mm-thick PMMA will require only 2-3 hours.

  9. Advanced photon source undulator beamline tests of a contact-cooled silicon u-shaped monochromator

    SciTech Connect

    Lee, W.K.; Fernandez, P.B.; Khounsary, A.

    1997-09-01

    At the Advanced Photon Source (APS), undulator insertion devices are capable of producing x-ray beams with total power of about 5 kW and normal incidence heat fluxes of about 170 W/mm{sup 2} at 30 m from the source. On beamlines in which the first optical element is a mirror, the reflected beam from the mirror still carries considerable power and power density. Depending on its location, the monochromator downstream of the mirror might be subject to 300 W total power and 5 W/mm{sup 2} normal incidence heat flux. Thus, it is still necessary to carefully design a monochromator that provides acceptable performance under these heat loads. A contact-cooled u-shaped monochromator may be used in this case. The main feature of the u-shaped monochromator is that, by carefully selecting the geometry and cooling locations, is passively corrects for some of the thermally induced crystal distortions. We present experimental and computational results of a contact cooled u-shaped monochromator tested on an APS undulator beamline. The results are encouraging and compare favorably with liquid-gallium internally cooled crystals.

  10. A new paradigm for macromolecular crystallography beamlines derived from high-pressure methodology and results.

    PubMed

    Fourme, Roger; Girard, Eric; Dhaussy, Anne Claire; Medjoubi, Kadda; Prangé, Thierry; Ascone, Isabella; Mezouar, Mohamed; Kahn, Richard

    2011-01-01

    Biological structures can now be investigated at high resolution by high-pressure X-ray macromolecular crystallography (HPMX). The number of HPMX studies is growing, with applications to polynucleotides, monomeric and multimeric proteins, complex assemblies and even a virus capsid. Investigations of the effects of pressure perturbation have encompassed elastic compression of the native state, study of proteins from extremophiles and trapping of higher-energy conformers that are often of biological interest; measurements of the compressibility of crystals and macromolecules were also performed. HPMX results were an incentive to investigate short and ultra-short wavelengths for standard biocrystallography. On cryocooled lysozyme crystals it was found that the data collection efficiency using 33 keV photons is increased with respect to 18 keV photons. This conclusion was extended from 33 keV down to 6.5 keV by exploiting previously published data. To be fully exploited, the potential of higher-energy photons requires detectors with a good efficiency. Accordingly, a new paradigm for MX beamlines was suggested, using conventional short and ultra-short wavelengths, aiming at the collection of very high accuracy data on crystals under standard conditions or under high pressure. The main elements of such beamlines are outlined. PMID:21169687

  11. Neutral beamline with ion energy recovery based on magnetic blocking of electrons

    DOEpatents

    Stirling, William L.

    1982-01-01

    A neutral beamline generator with energy recovery of the full-energy ion ponent of the beam based on magnetic blocking of electrons is provided. Ions from a positive ion source are accelerated to the desired beam energy from a slightly positive potential level with respect to ground through a neutralizer cell by means of a negative acceleration voltage. The unneutralized full-energy ion component of the beam exiting the neutralizer are retarded and slightly deflected and the electrons in the neutralizer are blocked by a magnetic field generated transverse to the beamline. An electron collector in the form of a coaxial cylinder surrounding and protruding axial a few centimeters beyond the neutralizer exit terminates the electrons which exit the neutralizer in an E x B drift to the collector when the collector is biased a few hundred volts positive with respect to the neutralizer voltage. The neutralizer is operated at the negative acceleration voltage, and the deflected full energy ions are decelerated and the charge collected at ground potential thereby expending none of their energy received from the acceleration power supply.

  12. Neutral beamline with ion energy recovery based on magnetic blocking of electrons

    DOEpatents

    Stirling, W.L.

    1980-07-01

    A neutral beamline generator with energy recovery of the full-energy ion component of the beam based on magnetic blocking of electrons is provided. Ions from a positive ion source are accelerated to the desired beam energy from a slightly positive potential level with respect to ground through a neutralizer cell by means of a negative acceleration voltage. The unneutralized full-energy ion component of the beam exiting the neutralizer are retarded and slightly deflected and the elecrons in the neutralizer are blocked by a magnetic field generated transverse to the beamline. An electron collector in the form of a coaxial cylinder surrounding and protruding axial a few centimeters beyond the neutralizer exit terminates the electrons which exit the neutralizer in an E x B drift to the collector when the collector is biased a few hundred volts positive with respect to the neutralizer voltage. The neutralizer is operated at the negative acceleration voltage. The neutralizer is operated at the negative acceleration voltage, and the deflected full energy ions are decelerated and the charge collected at ground potential thereby expending none of their energy received from the acceleration power supply.

  13. Summary of Session III

    SciTech Connect

    Furman, M.A.

    2002-06-19

    This is a summary of the talks presented in Session III ''Simulations of Electron-Cloud Build Up'' of the Mini-Workshop on Electron-Cloud Simulations for Proton and Positron Beams ECLOUD-02, held at CERN, 15-18 April 2002.

  14. The Apple III.

    ERIC Educational Resources Information Center

    Ditlea, Steve

    1982-01-01

    Describes and evaluates the features, performance, peripheral devices, available software, and capabilities of the Apple III microcomputer. The computer's operating system, its hardware, and the commercially produced software it accepts are discussed. Specific applications programs for financial planning, accounting, and word processing are…

  15. CITY III Director's Guide.

    ERIC Educational Resources Information Center

    Envirometrics, Inc., Washington, DC.

    CITY III is a computer-assisted simulation game which allows the participants to make decisions affecting various aspects of the economic, governmental, and social sectors of a simulated urban area. The game director selects one of five possible starting city configurations, may set a number of conditions in the city before the start of play, and…

  16. Hyper III on ramp

    NASA Technical Reports Server (NTRS)

    1969-01-01

    The Hyper III was a full-scale lifting-body remotely piloted research vehicle (RPRV) built at what was then the NASA Flight Research Center located at Edwards Air Force Base in Southern California. The Flight Research Center (FRC--as Dryden was named from 1959 until 1976) already had experience with testing small-scale aircraft using model-airplane techniques, but the first true remotely piloted research vehicle was the Hyper III, which flew only once in December 1969. At that time, the Center was engaged in flight research with a variety of reentry shapes called lifting bodies, and there was a desire both to expand the flight research experience with maneuverable reentry vehicles, including a high-performance, variable-geometry craft, and to investigate a remotely piloted flight research technique that made maximum use of a research pilot's skill and experience by placing him 'in the loop' as if he were in the cockpit. (There have been, as yet, no female research pilots assigned to Dryden.) The Hyper III as originally conceived was a stiletto-shaped lifting body that had resulted from a study at NASA's Langley Research Center in Hampton, Virginia. It was one of a number of hypersonic, cross-range reentry vehicles studied at Langley. (Hypersonic means Mach 5--five times the speed of sound--or faster; cross-range means able to fly a considerable distance to the left or right of the initial reentry path.) The FRC added a small, deployable, skewed wing to compensate for the shape's extremely low glide ratio. Shop personnel built the 32-foot-long Hyper III and covered its tubular frame with dacron, aluminum, and fiberglass, for about $6,500. Hyper III employed the same '8-ball' attitude indicator developed for control-room use when flying the X-15, two model-airplane receivers to command the vehicle's hydraulic controls, and a telemetry system (surplus from the X-15 program) to transmit 12 channels of data to the ground not only for display and control but for data

  17. Research at and Operation of the Materials Science Beamline (X-11) at the National Synchrotron Light Source. Final Report

    SciTech Connect

    Sayers, Dale E.

    2003-10-15

    This is the final report for DOE DE-FG02-89ER45384. An overview of the operational history and status of beamline X-11A at the end of the contract period, and a brief review of the core science program at NCSU and the scientific results of X-11A since the last progress report is also presented.

  18. A new optical scheme for large-extraction small-aberration vacuum-ultraviolet synchrotron radiation beamlines.

    PubMed

    Moreno, Thierry

    2016-09-01

    Vacuum-ultraviolet radiation delivered by bending-magnet sources is used at numerous synchrotron radiation facilities worldwide. As bending-magnet radiation is inherently much less collimated compared with undulator sources, the generation of high-quality intense bending-magnet vacuum-ultraviolet photon beams is extremely demanding in terms of the optical layout due to the necessary larger collection apertures. In this article, an optimized optical layout which takes into account both the optical and electron beam properties is proposed. This layout delivers an improved beam emittance of over one order of magnitude compared with existing vacuum-ultraviolet bending-magnet beamlines that, up to now, do not take into account electron beam effects. The arrangement is made of two dedicated mirrors, a cylindrical and a cone-shaped one, that focus independently both the horizontal and the vertical emission of a bending-magnet source, respectively, and has been already successfully applied in the construction of the infrared beamline at the Brazilian synchrotron. Using this scheme, two vacuum-ultraviolet beamline designs based on a SOLEIL synchrotron bending-magnet source are proposed and analysed. They would be useful for future upgrades to the DISCO beamline at SOLEIL and could be readily implemented at other synchrotron radiation facilities. PMID:27577766

  19. Fueling type III secretion

    PubMed Central

    Lee, Pei-Chung

    2015-01-01

    Type III secretion systems are complex nanomachines that export proteins from the bacterial cytoplasm across the cell envelope in a single step. They are at the core of the machinery used to assemble the bacterial flagellum, and the needle complex many Gram-negative pathogens use to inject effector proteins into host cells and cause disease. Several models have been put forward to explain how this export is energized, and the mechanism has been the subject of considerable debate. Here we present an overview of these models and discuss their relative merits. Recent evidence suggests that the proton motive force is the primary energy source for type III secretion, although contribution from refolding of secreted proteins has not been ruled out. The mechanism, by which the proton motive force is converted to protein export, remains enigmatic. PMID:25701111

  20. Cranial mononeuropathy III - diabetic type

    MedlinePlus

    ... gov/ency/article/000692.htm Cranial mononeuropathy III - diabetic type To use the sharing features on this page, please enable JavaScript. Cranial mononeuropathy III -- diabetic type -- is usually a complication of diabetes that causes ...

  1. Migration Type III

    NASA Astrophysics Data System (ADS)

    Artymowicz, Pawel

    2004-03-01

    Migration type IIIMigration of objects embedded in disks (and the accompanying eccentricity evolution) is becoming a major theme in planetary system formation.The underlying physics can be distilled into the notion of disk-planet coupling via Lindblad resonances, which launch waves, sometimes spectacular spiral shock waves in gas disks. The wave pattern exchanges angular momentum with the planet. That causes (i) migration, (ii) eccentricity evolution, and (iii) gap opening by sufficiently massive planets.A competing source of disk-planet interaction, the corotationaltorques, are much less conspicuous (corotation does not produce easilydetectable waves, as galaxy observers can attest) and have often been missed in the analysis of planet migration. If spiral waves are like waves at Goleta beach, then the corotation acts more like a stealthy riptide. Corotationalflows lie at the basis of a new, surprisingly rapid, mode of migration (type III),superseding the standard type II migration (with a gap), and revising the speed of type I migration (without a gap). The talk will contain results obtained at KITP, e.g., an analytical derivation of da/dt in type III motion. It will be illustrated by videos of high-resolution numerical simulations obtained with different implementations of the Piecewise Parabolic Method hydrodynamics.

  2. Evaluation of SNS Beamline Shielding Configurations using MCNPX Accelerated by ADVANTG

    SciTech Connect

    Risner, Joel M; Johnson, Seth R.; Remec, Igor; Bekar, Kursat B.

    2015-01-01

    Shielding analyses for the Spallation Neutron Source (SNS) at Oak Ridge National Laboratory pose significant computational challenges, including highly anisotropic high-energy sources, a combination of deep penetration shielding and an unshielded beamline, and a desire to obtain well-converged nearly global solutions for mapping of predicted radiation fields. The majority of these analyses have been performed using MCNPX with manually generated variance reduction parameters (source biasing and cell-based splitting and Russian roulette) that were largely based on the analyst's insight into the problem specifics. Development of the variance reduction parameters required extensive analyst time, and was often tailored to specific portions of the model phase space. We previously applied a developmental version of the ADVANTG code to an SNS beamline study to perform a hybrid deterministic/Monte Carlo analysis and showed that we could obtain nearly global Monte Carlo solutions with essentially uniform relative errors for mesh tallies that cover extensive portions of the model with typical voxel spacing of a few centimeters. The use of weight window maps and consistent biased sources produced using the FW-CADIS methodology in ADVANTG allowed us to obtain these solutions using substantially less computer time than the previous cell-based splitting approach. While those results were promising, the process of using the developmental version of ADVANTG was somewhat laborious, requiring user-developed Python scripts to drive much of the analysis sequence. In addition, limitations imposed by the size of weight-window files in MCNPX necessitated the use of relatively coarse spatial and energy discretization for the deterministic Denovo calculations that we used to generate the variance reduction parameters. We recently applied the production version of ADVANTG to this beamline analysis, which substantially streamlined the analysis process. We also tested importance function

  3. A New Tomography Beamline at a Wiggler Port at the Center for Advanced Microstructures and Devices (CAMD) Storage Ring

    SciTech Connect

    Ham, Kyungmin; Morris, Kevin J.; Tittsworth, Roland C.; Scott, John D.; Barnett, Heath A.; Butler, Leslie G.; Willson, Clinton S.

    2007-01-19

    A new tomography beamline has been built and commissioned at the 7 T wiggler of the CAMD storage ring. This beamline is equipped with two monochromators that can be used interchangeably for X-ray absorption spectroscopy or high resolution X-ray tomography, at best 2-3 {mu}m pixel size. The high-flux double multilayer-mirror monochromator (W-B4C multilayers) can be used in the energy range from 6 to 35 keV with a resolution ({delta}E/E ) between 0.01-0.03. The second is a channel-cut Si(311)-crystal monochromator with a range of 15 to 36 keV and resolution of ca. 10-4, this is not yet tested. Tomography has the potential for high-throughput materials analysis; however, there are some significant obstacles to be overcome in the areas of data acquisition, reconstruction, visualization and analysis. Data acquisition is facilitated by the multilayer monochromator as this provides high photon flux, thus reducing measurement time. At the beamline, Matlab(c) routines provide simple x,y,z fly-throughs of the sample. Off-beamline processing with Amira(c) can yield more sophisticated inspection of the sample. Standard data acquisition based on fixed angle increments is not optimal, however, new patterns based on Greek golden ratio angle increments offer faster convergence to a high signal-to-noise-ratio image. The image reconstruction has traditionally been done by back-projection reconstruction. In this presentation we will show first results from samples studied at the new beamline.

  4. Developments in optics and performance at BL13-XALOC, the macromolecular crystallography beamline at the Alba Synchrotron

    PubMed Central

    Juanhuix, Jordi; Gil-Ortiz, Fernando; Cuní, Guifré; Colldelram, Carles; Nicolás, Josep; Lidón, Julio; Boter, Eva; Ruget, Claude; Ferrer, Salvador; Benach, Jordi

    2014-01-01

    BL13-XALOC is currently the only macromolecular crystallography beamline at the 3 GeV ALBA synchrotron near Barcelona, Spain. The optics design is based on an in-vacuum undulator, a Si(111) channel-cut crystal monochromator and a pair of KB mirrors. It allows three main operation modes: a focused configuration, where both mirrors can focus the beam at the sample position to 52 µm × 5.5 µm FWHM (H × V); a defocused configuration that can match the size of the beam to the dimensions of the crystals or to focus the beam at the detector; and an unfocused configuration, where one or both mirrors are removed from the photon beam path. To achieve a uniform defocused beam, the slope errors of the mirrors were reduced down to 55 nrad RMS by employing a novel method that has been developed at the ALBA high-accuracy metrology laboratory. Thorough commissioning with X-ray beam and user operation has demonstrated an excellent energy and spatial stability of the beamline. The end-station includes a high-accuracy single-axis diffractometer, a removable mini-kappa stage, an automated sample-mounting robot and a photon-counting detector that allows shutterless operation. The positioning tables of the diffractometer and the detector are based on a novel and highly stable design. This equipment, together with the operation flexibility of the beamline, allows a large variety of types of crystals to be tackled, from medium-sized crystals with large unit-cell parameters to microcrystals. Several examples of data collections measured during beamline commissioning are described. The beamline started user operation on 18 July 2012. PMID:24971961

  5. Versatile variable temperature insert at the DEIMOS beamline for in situ electrical transport measurements.

    PubMed

    Joly, L; Muller, B; Sternitzky, E; Faullumel, J G; Boulard, A; Otero, E; Choueikani, F; Kappler, J P; Studniarek, M; Bowen, M; Ohresser, P

    2016-05-01

    The design and the first experiments are described of a versatile cryogenic insert used for its electrical transport capabilities. The insert is designed for the cryomagnet installed on the DEIMOS beamline at the SOLEIL synchrotron dedicated to magnetic characterizations through X-ray absorption spectroscopy (XAS) measurements. This development was spurred by the multifunctional properties of novel materials such as multiferroics, in which, for example, the magnetic and electrical orders are intertwined and may be probed using XAS. The insert thus enables XAS to in situ probe this interplay. The implementation of redundant wiring and careful shielding also enables studies on operating electronic devices. Measurements on magnetic tunnel junctions illustrate the potential of the equipment toward XAS studies of in operando electronic devices. PMID:27140143

  6. CCD detector development projects by the Beamline Technical Support Group at the Advanced Photon Source

    NASA Astrophysics Data System (ADS)

    Lee, John H.; Fernandez, Patricia; Madden, Tim; Molitsky, Michael; Weizeorick, John

    2007-11-01

    This paper will describe two ongoing detector projects being developed by the Beamline Technical Support Group at the Advanced Photon Source (APS) at Argonne National Laboratory (ANL). The first project is the design and construction of two detectors: a single-CCD system and a two-by-two Mosaic CCD camera for Small-Angle X-ray Scattering (SAXS). Both of these systems utilize the Kodak KAF-4320E CCD coupled to fiber optic tapers, custom mechanical hardware, electronics, and software developed at ANL. The second project is a Fast-CCD (FCCD) detector being developed in a collaboration between ANL and Lawrence Berkeley National Laboratory (LBNL). This detector will use ANL-designed readout electronics and a custom LBNL-designed CCD, with 480×480 pixels and 96 outputs, giving very fast readout.

  7. CCD detector development projects by the beamline technical support group at the Advanced Photon Source.

    SciTech Connect

    Lee, J. H.; Fernandez, P.; Madden, T.; Molitsky, M.; Weizeorick, J.

    2007-11-11

    This paper will describe two ongoing detector projects being developed by the Beamline Technical Support Group at the Advanced Photon Source (APS) at Argonne National Laboratory (ANL). The first project is the design and construction of two detectors: a single-CCD system and a two-by-two Mosaic CCD camera for Small-Angle X-ray Scattering (SAXS). Both of these systems utilize the Kodak KAF-4320E CCD coupled to fiber optic tapers, custom mechanical hardware, electronics, and software developed at ANL. The second project is a Fast-CCD (FCCD) detector being developed in a collaboration between ANL and Lawrence Berkeley National Laboratory (LBNL). This detector will use ANL-designed readout electronics and a custom LBNL-designed CCD, with 480 x 480 pixels and 96 outputs, giving very fast readout.

  8. Opportunities for Time Resolved Studies at the ID24 Energy Dispersive XAS Beamline of the ESRF

    SciTech Connect

    Mathon, O.; Aquilanti, G.; Guilera, G.; Labiche, J.-C.; Linden, P. van der; Newton, M. A.; Ponchut, C.; Trapananti, A.; Pascarelli, S.

    2007-01-19

    ID24 is the energy dispersive beamline of the European Synchrotron Radiation Facility dedicated to X-ray Absorption Spectroscopy (XAS). Thanks to the parallel acquisition mode that allows data in a large energy range to be collected simultaneously, XAS using dispersive optics is particularly suited for the study of time dependent processes. The techniques that can be used to study such systems vary according to the timescale of the phenomena under investigation. They take advantage of the temporal structure of the synchrotron radiation in case of time resolution of the order of the intrinsic duration of the x-ray pulse (100 ps), while for time scales above 100 {mu}s or below 100 ps, the x-ray beam can be considered continuous and the time resolution is determined by the different detection systems.

  9. Acoustic methods for high-throughput protein crystal mounting at next-generation macromolecular crystallographic beamlines.

    PubMed

    Roessler, Christian G; Kuczewski, Anthony; Stearns, Richard; Ellson, Richard; Olechno, Joseph; Orville, Allen M; Allaire, Marc; Soares, Alexei S; Héroux, Annie

    2013-09-01

    To take full advantage of advanced data collection techniques and high beam flux at next-generation macromolecular crystallography beamlines, rapid and reliable methods will be needed to mount and align many samples per second. One approach is to use an acoustic ejector to eject crystal-containing droplets onto a solid X-ray transparent surface, which can then be positioned and rotated for data collection. Proof-of-concept experiments were conducted at the National Synchrotron Light Source on thermolysin crystals acoustically ejected onto a polyimide `conveyor belt'. Small wedges of data were collected on each crystal, and a complete dataset was assembled from a well diffracting subset of these crystals. Future developments and implementation will focus on achieving ejection and translation of single droplets at a rate of over one hundred per second. PMID:23955046

  10. HARWI-II, The New High-Energy Beamline for Materials Science at HASYLAB/DESY

    SciTech Connect

    Beckmann, Felix; Lippmann, Thomas; Metge, Joachim; Dose, Thomas; Donath, Tilman; Schreyer, Andreas; Tischer, Markus; Liss, Klaus Dieter

    2004-05-12

    The GKSS Forschungszentrum Geesthacht, Germany, will setup a new high-energy beamline specialized for texture, strain and imaging measurements for materials science at the Hamburger Synchrotronstrahlungslabor HASYLAB of the Deutsches Elektronen-Synchrotron DESY. Four different experiments will be installed at the new wiggler HARWI-II. The high pressure cell will be run by the GFZ Potsdam, Germany, the high-energy diffractometer together with a microtomography camera will be run by the GKSS. A further station will allow space for the diffraction enhanced imaging setup. The optics will provide for a small white beam (0.5 mm x 0.5 mm) and a large monochromatic X-ray beam (50 mm x 10 mm) with an energy range of 20 to 250 keV.

  11. A Johann-type X-ray emission spectrometer at the Rossendorf beamline.

    PubMed

    Kvashnina, Kristina O; Scheinost, Andreas C

    2016-05-01

    This paper gives a detailed description, including equations, of the Johann-type X-ray emission spectrometer which has been recently installed and tested at the Rossendorf beamline (ROBL) of the European Synchrotron Radiation Facility. The spectrometer consists of a single spherically bent crystal analyzer and an avalanche photodiode detector positioned on the vertical Rowland cycle of 1 m diameter. The hard X-ray emission spectrometer (∼3.5-25 keV) operates at atmospheric pressure and covers the Bragg angles of 65°-89°. The instrument has been tested at high and intermediate incident energies, i.e. at the Zr K-edge and at the Au L3-edge, in the second experimental hutch of ROBL. The spectrometer is dedicated for studying actinides in materials and environmental samples by high-energy-resolution X-ray absorption and X-ray emission spectroscopies. PMID:27140166

  12. Mirror and grating surface figure requirements for grazing incidence synchrotron radiation beamlines: Power loading effects

    SciTech Connect

    Hulbert, S.L.; Sharma, S.

    1987-10-21

    At present, grazing incidence mirrors are used almost exclusively as the first optical element in VUV and soft x-ray synchrotron radiation beam lines. The performance of these mirrors is determined by thermal and mechanical stress-induced figure errors as well as by figure errors remaining from the grinding and polishing process. With the advent of VUV and soft x-ray undulators and wigglers has come a new set of thermal stress problems related to both the magnitude and the spatial distribution of power from these devices. In many cases the power load on the entrance slits and gratings in these beamlines is no longer negligible. The dependence of thermally-induced front-end mirror figure errors on various storage ring and insertion device parameters (especially those at the NSLS) and the effects of these figure errors on a class of soft x-ray beam lines are presented. 17 refs., 5 figs., 2 tabs.

  13. Design Updates of the X-ray Beam Position Monitor for Beamline Front Ends

    NASA Astrophysics Data System (ADS)

    Shu, Deming; Singh, Om; Hahne, Michael; Decker, Glenn

    2007-01-01

    At the Advanced Photon Source (APS), each insertion device (ID) beamline front end has two x-ray beam position monitors (XBPMs) to monitor the x-ray beam position in both the vertical and horizontal directions. The XBPMs measure photoelectrons generated from the CVD-diamond-based sensory blades and deduce the beam position by comparison of the relative signals from the blades. Using the method proposed by G. Decker, which involves the introduction of a chicane into the accelerator lattice that directs unwanted x-rays away from the photosensitive XBPM blades, the photon source stability has been improved by addition of XBPMs in the storage ring global orbit feedback. In recent years, design updates for the XBPM mechanical structure and geometric configuration have been made to improve its performance. We present these design updates in this paper. Test results of the XBPM design updates are also discussed here.

  14. The Scanning X-Ray Microprobe at the Esrf ``X-Ray Microscopy'' Beamline

    NASA Astrophysics Data System (ADS)

    Susini, J.; Salomé, M.; Fayard, B.; Ortega, R.; Kaulich, B.

    The development of high brilliance X-ray sources coupled with advances in manufacturing technologies of focusing optics has led to significant improvements in submicrometer probes for spectroscopy, diffraction and imaging applications. For instance, X-ray microscopy in the 1-10 keV energy range is better-suited for analyzing trace elements in fluorescence yield. This article will be biased towards submicron fluorescence microscopy developed on the ID21 beamline at the ESRF. The main technical developments, involving new focusing lenses or novel phase contrast method, are presented. Strengths and weaknesses of X-ray microscopy and spectromicroscopy techniques are discussed and illustrated by examples in biology, materials science and geology.

  15. Advanced photoelectric effect experiment beamline at Elettra: A surface science laboratory coupled with Synchrotron Radiation

    SciTech Connect

    Panaccione, G.; Vobornik, I.; Fujii, J.; Krizmancic, D.; Annese, E.; Giovanelli, L.; Maccherozzi, F.; Salvador, F.; De Luisa, A.; Benedetti, D.; Gruden, A.; Bertoch, P.; Rossi, G.; Polack, F.; Cocco, D.; Sostero, G.; Diviacco, B.; Hochstrasser, M.; Maier, U.; Pescia, D.; and others

    2009-04-15

    We report the main characteristics of the advanced photoelectric effect experiments beamline, operational at Elettra storage ring, featuring a fully independent double branch scheme obtained by the use of chicane undulators and able to keep polarization control in both linear and circular mode. The paper describes the novel technical solutions adopted, namely, (a) the design of a quasiperiodic undulator resulting in optimized suppression of higher harmonics over a large photon energy range (10-100 eV), (b) the thermal stability of optics under high heat load via cryocoolers, and (c) the end station interconnected setup allowing full access to off-beam and on-beam facilities and, at the same time, the integration of users' specialized sample growth chambers or modules.

  16. Highly efficient beamline and spectrometer for inelastic soft X-ray scattering at high resolution.

    PubMed

    Lai, C H; Fung, H S; Wu, W B; Huang, H Y; Fu, H W; Lin, S W; Huang, S W; Chiu, C C; Wang, D J; Huang, L J; Tseng, T C; Chung, S C; Chen, C T; Huang, D J

    2014-03-01

    The design, construction and commissioning of a beamline and spectrometer for inelastic soft X-ray scattering at high resolution in a highly efficient system are presented. Based on the energy-compensation principle of grating dispersion, the design of the monochromator-spectrometer system greatly enhances the efficiency of measurement of inelastic soft X-rays scattering. Comprising two bendable gratings, the set-up effectively diminishes the defocus and coma aberrations. At commissioning, this system showed results of spin-flip, d-d and charge-transfer excitations of NiO. These results are consistent with published results but exhibit improved spectral resolution and increased efficiency of measurement. The best energy resolution of the set-up in terms of full width at half-maximum is 108 meV at an incident photon energy tuned about the Ni L3-edge. PMID:24562553

  17. Strategies and limitations for fluorescence detection of XAFS at high flux beamlines

    PubMed Central

    Heald, Steve M.

    2015-01-01

    The issue of detecting the XAFS signal from dilute samples is discussed in detail with the aim of making best use of high flux beamlines that provide up to 1013 photons s−1. Various detection methods are compared, including filters with slits, solid state detectors, crystal analyzers and combinations of these. These comparisons rely on simulations that use experimentally determined parameters. It is found that inelastic scattering places a fundamental limit on detection, and that it is important to take proper account of the polarization dependence of the signals. The combination of a filter–slit system with a solid state detector is a promising approach. With an optimized system good performance can be obtained even if the total count rate is limited to 107 Hz. Detection schemes with better energy resolution can help at the largest dilutions if their collection efficiency and count rate limits can be improved. PMID:25723945

  18. Report of the Census Task Force on beamline control system requirements

    SciTech Connect

    Barsotti, E.J.; Bartlett, J.F.; Bogert, V.D.; Borcherding, F.O.; Butler, J.; Czarapata, P.C.; Spalding, W.J.; Thomas, A.D.

    1986-10-02

    A special task force was appointed to study the experience with the present beamline control system at Fermilab and to make recommendations in this area. The charge of the committee and the list of its members are appended. In order to carry out its assignment, the committee conducted a series of meetings in which it discussed the controls situation in general and the best way to approach the user community. The various groups of users were identified, and a letter was written to representatives of these groups asking questions concerning the present system and future needs. The committee met with each group to discuss the response to these questions. Written summaries of the discussions are appended. Conclusions are drawn regarding current problems, systematic upgrades and specific recommendations. (LEW)

  19. First photon-shutter development for APS insertion device beamline front ends

    NASA Astrophysics Data System (ADS)

    Shu, Deming; Nian, H. L. Thomas; Wang, Zhibi; Collins, Jeffrey T.; Ryding, David G.; Kuzay, Tuncer M.

    1993-02-01

    One of the most critical components on the Advanced Photon Source (APS) insertion device (ID) beamline front ends is the first photon shutter. It operates in two modes to fully intercept the high total power and high-heat-flux ID photon beam in seconds (normal mode) or in less than 100 ms (emergency fast mode). It is designed to operate in ultra high vacuum (UHV). The design incorporates a multi-channel rectangular bar, bent in a `hockey stick' configuration, with two-point suspension. The flanged end is an articulated bellows with rolling hinges. The actuation end is a spring-assisted, pneumatic fail-safe flexural pivot type. The coolant (water) channels incorporate brazed copper foam to enhance the heat transfer, a tube technology particular to the APS. The design development, and material aspects, as well as the extensive thermal and vibrational analyses in support of the design, are presented in this paper.

  20. Stress mitigation of x-ray beamline monochromators using topography test unit.

    SciTech Connect

    Maj, J.; Waldschmidt, G.; Baldo, P.; Macrander, A.; Koshelev, I.; Huang, R.; Maj, L.; Maj, A.; Univ. of Chicago; Northeastern Ohio Univ. Coll. of Medicine; Rosalind Franklin Univ. of Medicine and Science

    2007-01-01

    Silicon and diamond monochromators (crystals), often used in the Advanced Photon Source X-ray beamlines, require a good quality surface finish and stress-free installation to ensure optimal performance. The device used to mount the crystal has been shown to be ajor contributing source of stress. In this case, an adjustable mounting device is an effective method of reducing stresses and improve the rocking curve to levels much closer to ideal. Analysis by a topography test unit has been used to determine the distribution of stresses and to measure the rocking curve, as well as create CCD images of the crystal. This paper describes the process of measuring these stresses and manipulating the mounting device and crystal to create a substantially improved monochromator.

  1. Improved High-Heat-Load Graphite Filter Design At CHESS Wiggler Beamlines

    SciTech Connect

    Savino, James J.; Shen Qun; Strieter, Gretchen; Fontes, Ernest; Pauling, Alan K.

    2004-05-12

    Conductively cooled highly-oriented pyrolytic graphite (HOPG) filters have been used at CHESS wiggler beamlines to protect downstream beryllium windows under high heat loads. In the past beam currents above 350 mA have caused excessively high temperatures on the existing HOPG filters, resulting in rapid sublimation of the graphite and drastic shortening of filter lifetimes. A new filter design which eliminates some drawbacks of the existing design is described. The new design utilizes a slotted water jet, which cools a thin, 'compliant' graphite-copper braze joint. Heat-transfer enhancements should enable an installed filter to survive beam currents of 450 mA. Optimization of design features and analysis results are discussed.

  2. Report on the value engineering workshop on APS beamline front ends

    SciTech Connect

    Kuzay, T.

    1993-01-01

    A formal value engineering evaluation process was developed to address the front end components of the beamlines for the Advanced Photon Source (APS). This process (described in Section 2) involved an information phase, a creative phase, a judgment phase, a development phase, and a recommendation phase. Technical experts from other national laboratories and industry were invited to a two-day Value Engineering Workshop on November 5-6, 1992. The results of this Workshop are described in Section 4. Following the Workshop, various actions by the APS staff led to the redesign of the front end components, which are presented in Sections 5 and 6. The cost benefit analysis is presented in Section 7. It is important of realize that an added benefit of the Workshop was to obtain numerous design evaluations and enhancements of the front end components by experts in the field. As the design work proceeds to Title II completion, the APS staff is including many of these suggestions.

  3. Achieving Vibration Stability of the NSLS-II Hard X-ray Nanoprobe Beamline

    SciTech Connect

    Simos, N.; Chu, Y. N.; Broadbent, A.; Nazaretski, E.; Margulies, L.; Dyling, O.; Shen, Q.; Fallier, M.

    2010-08-30

    The Hard X-ray Nanoprobe (HXN) Beamline of National Synchrotron Light Source II (NSLS-lI) requires high levels of stability in order to achieve the desired instrument resolution. To ensure that the design of the endstation helps meet the stringent criteria and that natural and cultural vibration is mitigated both passively and actively, a comprehensive study complimentary to the design process has been undertaken. Vibration sources that have the potential to disrupt sensitive experiments such as wind, traffic and NSLS II operating systems have been studied using state of the art simulations and an array of field data. Further, final stage vibration isolation principles have been explored in order to be utilized in supporting endstation instruments. This paper presents results of the various study aspects and their influence on the HXN design optimization.

  4. Benchtop Nonresonant X-ray Emission Spectroscopy: Coming Soon to Laboratories and XAS Beamlines Near You?

    NASA Astrophysics Data System (ADS)

    Mortensen, Devon R.; Seidler, Gerald T.; Ditter, Alexander S.; Glatzel, Pieter

    2016-05-01

    Recently developed instrumentation at the University of Washington has allowed for nonresonant x-ray emission spectra (XES) to be measured in a laboratory-setting with an inexpensive, easily operated system. We present a critical evaluation of this equipment by means of Kβ and valence-level XES measurements for several Co compounds. We find peak count rates of ∼5000/s for concentrated samples and a robust relative energy scale with reproducibility of 25 meV or better. We furthermore find excellent agreement with synchrotron measurements with only modest loss in energy resolution. Instruments such as ours, based on only conventional sources that are widely sold for elemental analysis by x-ray fluorescence, can fill an important role to diversify the research applications of XES both by their presence in non-synchrotron laboratories and by their use in conjunction with XAFS beamlines where the complementarity of XAFS and XES holds high scientific potential.

  5. An in-situ heater for the XAS beamline (12-ID) in Australia

    NASA Astrophysics Data System (ADS)

    Johannessen, B.; Hussain, Z. S.; East, D. R.; Gibson, M. A.

    2013-04-01

    To accommodate for a growing number of requests by our user community an in-situ heater has been commissioned for the X-ray absorption spectroscopy (XAS) beamline 12-ID at the Australian Synchrotron. Here, we present an in-situ method for calibrating the temperature of the heating stage based on an anharmonic, correlated Einstein model. Specifically, we show that a temperature-dependant study of a bulk metallic foil (7.5 μm Cu) can be used to accurately calibrate the temperature of the heater. We also present the temperature-dependant coordination number, bond length, Debye-Waller factor, and third order cumulant to the bond length distribution function of the material from 18K to 1074K. At the higher temperatures we find that the atomic structure is comparable to that of an amorphous or liquid material indicating a gradual transition from crystalline to disordered atomic structure.

  6. The SYRMEP Beamline of Elettra: Clinical Mammography and Bio-medical Applications

    SciTech Connect

    Tromba, G.; Abrami, A.; Casarin, K.; Chenda, V.; Dreossi, D.; Mancini, L.; Menk, R. H.; Quai, E.; Sodini, N.; Vascotto, A.; Longo, R.; Arfelli, F.; Castelli, E.; Astolfo, A.; Bregant, P.; Brun, F.; Hola, M.; Kaiser, J.

    2010-07-23

    At the SYnchrotron Radiation for MEdical Physics (SYRMEP) beamline of Elettra Synchrotron Light Laboratory in Trieste (Italy), an extensive research program in bio-medical imaging has been developed since 1997. The core program carried out by the SYRMEP collaboration concerns the use of Synchrotron Radiation (SR) for clinical mammography with the aim of improving the diagnostic performance of the conventional technique. The first protocol with patients, started in 2006 has been completed at the end of 2009 and the data analysis is now in progress.Regarding applications different from clinical imaging, synchrotron X-ray computed microtomography (micro-CT) is the most used technique, both in absorption and phase contrast. A new software tool, Pore3D, has been developed to perform a quantitative morphological analysis on the reconstructed slices and to access textural information of the sample under study.

  7. Strategies and limitations for fluorescence detection of XAFS at high flux beamlines

    SciTech Connect

    Heald, Steve M.

    2015-02-17

    The issue of detecting the XAFS signal from dilute samples is discussed in detail with the aim of making best use of high flux beamlines that provide up to 1013photons-1. Various detection methods are compared, including filters with slits, solid state detectors, crystal analyzers and combinations of these. These comparisons rely on simulations that use experimentally determined parameters. It is found that inelastic scattering places a fundamental limit on detection, and that it is important to take proper account of the polarization dependence of the signals. The combination of a filter–slit system with a solid state detector is a promising approach. With an optimized system good performance can be obtained even if the total count rate is limited to 107Hz. Detection schemes with better energy resolution can help at the largest dilutions if their collection efficiency and count rate limits can be improved.

  8. Strategies and limitations for fluorescence detection of XAFS at high flux beamlines

    DOE PAGESBeta

    Heald, Steve M.

    2015-02-17

    The issue of detecting the XAFS signal from dilute samples is discussed in detail with the aim of making best use of high flux beamlines that provide up to 1013photons-1. Various detection methods are compared, including filters with slits, solid state detectors, crystal analyzers and combinations of these. These comparisons rely on simulations that use experimentally determined parameters. It is found that inelastic scattering places a fundamental limit on detection, and that it is important to take proper account of the polarization dependence of the signals. The combination of a filter–slit system with a solid state detector is a promisingmore » approach. With an optimized system good performance can be obtained even if the total count rate is limited to 107Hz. Detection schemes with better energy resolution can help at the largest dilutions if their collection efficiency and count rate limits can be improved.« less

  9. Development of diamond-based X-ray detection for high-flux beamline diagnostics

    PubMed Central

    Bohon, Jen; Muller, Erik; Smedley, John

    2010-01-01

    High-quality single-crystal and polycrystalline chemical-vapor-deposition diamond detectors with platinum contacts have been tested at the white-beam X28C beamline at the National Synchrotron Light Source under high-flux conditions. The voltage dependence of these devices has been measured under both DC and pulsed-bias conditions, establishing the presence or absence of photoconductive gain in each device. Linear response consistent with the theoretically determined ionization energy has been achieved over eleven orders of magnitude when combined with previous low-flux studies. Temporal measurements with single-crystal diamond detectors have resolved the nanosecond-scale pulse structures of both the NSLS and the APS. Prototype single-crystal quadrant detectors have provided the ability to simultaneously resolve the X-ray beam position and obtain a quantitative measurement of the flux. PMID:20975215

  10. Contact-cooled U-monochromators for high heat load x-ray beamlines

    SciTech Connect

    Khounsary, A.; Yun, W.; Trakhtenberg, E.; Xu, S.; Assoufid, L.; Lee, W.K.

    1996-12-31

    This paper describes the design, expected performance, and preliminary test results of a contact-cooled monochromator for use on high heat load x-ray beamlines. The monochromator has a cross section in the shape of the letter U. This monochromator should be suitable for handing heat fluxes up to 5 W/square millimeter. As such, for the present application, it is compatible with the best internally cooled crystal monochromators. There are three key features in the design of this monochromator. First, it is contact cooled, thereby eliminating fabrication of cooling channels, bonding, and undesirable strains in the monochromator due to coolant-manifold-to-crystal-interface. Second, by illuminating the entire length of the crystal and extracting the central part of the reflected beam, sharp slope changes in the beam profile and thus slope errors are avoided. Last, by appropriate cooling of the crystal, tangential slope error can be substantially reduced.

  11. Contact-cooled U-monochromators for high heat load x-ray beamlines

    SciTech Connect

    Khounsary, A.; Yun, W.; Trakhtenberg, E.; Xu, S.; Assoufid, L.; Lee, W.K.

    1996-12-31

    This paper describes the design, expected performance, and preliminary test results of a contact-cooled monochromator for use on high heat load x-ray beamlines. The monochromator has a cross section in the shape of the letter U. This monochromator should be suitable for handling heat fluxes up to 5 W/mm{sup 2}. As such, for the present application, it is compatible with the best internally cooled silicon crystal monochromators operating at room temperature. There are three key features in the design of this monochromator. First, it is contact cooled, thereby eliminating fabrication of cooling channels, bonding, and undesirable strains in the monochromator due to coolant-manifold-to-crystal-interface. Second, by illuminating the entire length of the crystal and extracting the central part of the reflected beam, sharp slope changes in the beam profile and thus slope errors are avoided. Last, by selecting appropriate crystal geometry and cooling locations, tangential slope error can be substantially reduced.

  12. ELI-Beamlines: development of next generation short-pulse laser systems

    NASA Astrophysics Data System (ADS)

    Rus, B.; Bakule, P.; Kramer, D.; Naylon, J.; Thoma, J.; Green, J. T.; Antipenkov, R.; Fibrich, M.; Novák, J.; Batysta, F.; Mazanec, T.; Drouin, M. A.; Kasl, K.; Baše, R.; Peceli, D.; Koubíková, L.; Trojek, P.; Boge, R.; Lagron, J. C.; Vyhlídka, Å.; Weiss, J.; Cupal, J.,; Hřebíček, J.; Hříbek, P.; Durák, M.; Polan, J.; Košelja, M.; Korn, G.; Horáček, M.; Horáček, J.; Himmel, B.; Havlíček, T.; Honsa, A.; Korouš, P.; Laub, M.; Haefner, C.; Bayramian, A.; Spinka, T.; Marshall, C.; Johnson, G.; Telford, S.; Horner, J.; Deri, B.; Metzger, T.; Schultze, M.; Mason, P.; Ertel, K.; Lintern, A.; Greenhalgh, J.; Edwards, C.; Hernandez-Gomez, C.; Collier, J.; Ditmire, T.,; Gaul, E.; Martinez, M.; Frederickson, C.; Hammond, D.; Malato, C.; White, W.; Houžvička, J.

    2015-05-01

    Overview of the laser systems being built for ELI-Beamlines is presented. The facility will make available high-brightness multi-TW ultrashort laser pulses at kHz repetition rate, PW 10 Hz repetition rate pulses, and kilojoule nanosecond pulses for generation of 10 PW peak power. The lasers will extensively employ the emerging technology of diode-pumped solid-state lasers (DPSSL) to pump OPCPA and Ti:sapphire broadband amplifiers. These systems will provide the user community with cutting-edge laser resources for programmatic research in generation and applications of high-intensity X-ray sources, in particle acceleration, and in dense-plasma and high-field physics.

  13. Coherent Bragg nanodiffraction at the hard X-ray Nanoprobe beamline

    PubMed Central

    Hruszkewycz, S. O.; Holt, M. V.; Maser, J.; Murray, C. E.; Highland, M. J.; Folkman, C. M.; Fuoss, P. H.

    2014-01-01

    Bragg coherent diffraction with nanofocused hard X-ray beams provides unique opportunities for quantitative in situ studies of crystalline structure in nanoscale regions of complex materials and devices by a variety of diffraction-based techniques. In the case of coherent diffraction imaging, a major experimental challenge in using nanoscale coherent beams is maintaining a constant scattering volume such that coherent fringe visibility is maximized and maintained over the course of an exposure lasting several seconds. Here, we present coherent Bragg diffraction patterns measured from different nanostructured thin films at the Sector 26 Nanoprobe beamline at the Advanced Photon Source and demonstrate that with nanoscale positional control, coherent diffraction patterns can be measured with source-limited fringe visibilities more than 50% suitable for imaging by coherent Bragg ptychography techniques. PMID:24470418

  14. Preliminary measurements on the new TOF system installed at the AMS beamline of INFN-LABEC

    NASA Astrophysics Data System (ADS)

    Palla, L.; Castelli, L.; Czelusniak, C.; Fedi, M. E.; Giuntini, L.; Liccioli, L.; Mandò, P. A.; Martini, M.; Mazzinghi, A.; Ruberto, C.; Schiavulli, L.; Sibilia, E.; Taccetti, F.

    2015-10-01

    A high resolution time of flight (TOF) system has been developed at LABEC, the 3 MV Tandem accelerator laboratory in Florence, in order to improve the sensitivity of AMS measurements on carbon samples with ultra-low concentration and also to measure other isotopes, such as 129I. The system can be employed to detect and identify residual interfering particles originated from the break-up of molecular isobars. The set-up has been specifically designed for low energy heavy ions: it consists of two identical time pick-off stations, each made up of a thin conductive foil and a Micro-Channel Plate (MCP) multiplier. The beamline is also equipped with a silicon detector, installed downstream the stop TOF station. In this paper the design of the new system and the implemented readout electronics are presented. The tests performed on the single time pick-off station are reported: they show that the maximum contribution to the timing resolution given by both the intrinsic MCP resolution and the electronics is ⩽500 ps (FWHM). For these tests, single particle pulsed beams of 2-5 MeV protons and 10 MeV 12C3+ ions, to simulate typical AMS conditions, were used. The preliminary TOF and TOF-E (TOF-energy) measurements performed with carbon beams after the installation of the new system on the AMS beam line are also discussed. These measurements were performed using the foil-MCP as the start stage and a silicon detector as the stop stage. The spectra acquired with carbon ions suggest the presence of a small residual background from neighboring masses reaching the end of the beamline with the same energy as the rare isotope.

  15. Universal imaging: Dissociative ionization of polyatomic molecules, chemical dynamics beamline 9.0.2

    SciTech Connect

    Ahmed, M.; Chen, D.; Suits, A.G.

    1997-04-01

    A third endstation was recently added to the Chemical Dynamics beamline, designed to exploit the high flux broadband undulator light for a range of studies of reactive scattering, photochemistry and photoionization processes using time-of-flight mass spectroscopy coupled with position-sensitive detection. Two molecular beam sources are fixed at right angles, with the undulator light, or laser beams, intersecting the molecular beams at 45{degrees}. To date, beamline experiments have included a study of dissociative photoionization of a variety of molecules including N{sub 2}O and SF{sub 6}. In this mode, a single molecular beam source is used, with the tunable undulator light inducing, in SF{sub 6} for example, the process SF{sub 6} {r_arrow} SF{sub 6}{sup +} + e{sup {minus}} {r_arrow} SF{sub 5}{sup +} + F + e{sup {minus}}. The SF{sub 5}{sup +} ions are accelerated up the flight tube, mass selected and detected as a function of position on a phosphor screen viewed by a CCD camera. The position directly reveals the recoil speed (or translational energy release) and angular distribution for the dissociative ionization process. Furthermore, this measurement is obtained for all recoil speeds and angles simultaneously. Such detailed angular information has not previously been obtained for dissociative ionization processes; typically ion time-of-flight profiles are deconvoluted to yield rough insight into the angular distributions. The recorded image is actually a 2-dimensional projection of the nascent 3-dimensional velocity distribution, but established tomographic techniques enable the authors to reconstruct the 3-D distribution.

  16. BACH, the beamline for advanced dichroic and scattering experiments at ELETTRA

    NASA Astrophysics Data System (ADS)

    Zangrando, M.; Finazzi, M.; Paolucci, G.; Comelli, G.; Diviacco, B.; Walker, R. P.; Cocco, D.; Parmigiani, F.

    2001-02-01

    A beamline for advanced dichroism (BACH), to perform light polarization dependent experiments in the 35-1600 eV photon energy range is under construction at the ELETTRA Synchrotron Radiation Source in Trieste, Italy. The radiation source, based on two APPLE-II helical undulators, is designed for high photon flux and high resolving powers. The photons dispersion system is based on a Padmore variable angle spherical grating monochromator with a typical resolving power of 20 000-6000, 20 000-6000, and 15 000-5000 in the energy ranges 35-200 eV, 200-500 eV, and 500-1600 eV, respectively. Two separate branches after the monochromator allow setting two independent experimental chambers. The photon flux in the experimental chamber(s), calculated at the best resolutions achievable and with the aperture of the slits set at 10 μm, is expected to be above 1011 photons's with linearly or circularly polarized light. In addition, a fourth grating operates in the 400-1600 eV range to provide a higher flux, 1012 photons's with smaller resolving power (10 000-2000), allowing fluorescence and x-ray scattering experiments. The refocusing section(s), based on plane elliptical mirrors in a Kirkpatrick-Baez scheme, will provide on the sample, a nearly free-aberration spot(s), whose dimensions are expected to be 200×10 μm2 (horizontal×vertical). In the following, the general layout of the beamline is reported and the characteristics of the optical elements, as well as the optical performances (resolving powers and efficiencies of the monochromator, flux, and spot dimensions) are described in detail.

  17. Conceptual design of the neutral beamline for TPX long pulse operation

    SciTech Connect

    Wright, K.E.; Dahlgren, F.; Fan, H.M.; Grisham, L.R.; Hammersand, F.G.; Kamperschroer, J.H.; Lontai, L.M.; Oldaker, M.E.; Rogoff, P.

    1993-11-01

    The Tokamak Physics Experiment (TPX) will require a minimum of 8.0 megawatts of Neutral Beam beating power to be injected into the plasma for pulse lengths up to one thousand (1000) seconds to meet the experimental objectives. The Neutral Beam Injection System (NBIS) for initial operation on TPX will consist of one neutral beamline (NBL) with three Ion sources. Provisions will be made for a total of three NBLs. The NBIS will provide S.S MW of 120 keV D{sup 0} and 2.S MW of partial-energy D{sup 0} at 60 keV and 40 keV. The system also provides for measuring the neutral beam power, limits excess cold gas from entering the torus, and provides independent power, control, and protection for each individual ion source and accelerating structure. The Neutral Beam/Torus Connecting Duct (NB/TCD) includes a vacuum valve, an electrical insulating break, alignment bellows, vacuum seals, internal energy absorbing protective elements, beam diagnostics and bakeout capability. The NBL support structure will support the NBL, which will weigh approximately 80 tons at the proper elevation and withstand a seismic event. The NBIS currently operational on the Tokamak Fusion Test Reactor (TFTR) at the Princeton Plasma Physics Laboratory (PPPL) is restricted to injection pulse lengths of two (2) seconds by the limited capability of various energy absorbers. This paper describes the modifications and improvements which will be implemented for the TFTR Neutral Beamlines and the NB/TCD to satisfy the TPX requirements.

  18. Commissioning of a Soft X-ray Beamline PF-BL-16A with a Variable-Included-Angle Varied-Line-Spacing Grating Monochromator

    SciTech Connect

    Amemiya, Kenta; Toyoshima, Akio; Kikuchi, Takashi; Kosuge, Takashi; Nigorikawa, Kazuyuki; Sumii, Ryohei; Ito, Kenji

    2010-06-23

    The design and commissioning of a new soft X-ray beamline, BL-16A, at the Photon Factory is presented. The beamline consists of a pre-focusing mirror, an entrance slit, a variable-included-angle varied-line-spacing plane grating monochromator, and a post-focusing system as usual, and provides circularly and linearly polarized soft X rays in the energy range 200-1500 eV with an APPLE-II type undulator. The commissioning procedure for the beamline optics is described in detail, especially the check of the focal position for the zero-th order and diffracted X rays.

  19. The CAT-ACT Beamline at ANKA: A new high energy X-ray spectroscopy facility for CATalysis and ACTinide research

    NASA Astrophysics Data System (ADS)

    Zimina, A.; Dardenne, K.; Denecke, M. A.; Grunwaldt, J. D.; Huttel, E.; Lichtenberg, H.; Mangold, S.; Pruessmann, T.; Rothe, J.; Steininger, R.; Vitova, T.

    2016-05-01

    A new hard X-ray beamline for CATalysis and ACTinide research has been built at the synchrotron radiation facility ANKA. The beamline design is dedicated to X-ray spectroscopy, including ‘flux hungry’ photon-in/photon-out and correlative techniques with a special infrastructure for radionuclide and catalysis research. The CAT-ACT beamline will help serve the growing need for high flux/hard X-ray spectroscopy in these communities. The design, the first spectra and the current status of this project are reported.

  20. POPULATION III HYPERNOVAE

    SciTech Connect

    Smidt, Joseph; Whalen, Daniel J.; Wiggins, Brandon K.; Even, Wesley; Fryer, Chris L.; Johnson, Jarrett L.

    2014-12-20

    Population III supernovae have been of growing interest of late for their potential to directly probe the properties of the first stars, particularly the most energetic events that are visible near the edge of the observable universe. Until now, hypernovae, the unusually energetic Type Ib/c supernovae that are sometimes associated with gamma-ray bursts, have been overlooked as cosmic beacons at the highest redshifts. In this, the latest of a series of studies on Population III supernovae, we present numerical simulations of 25-50 M {sub ☉} hypernovae and their light curves done with the Los Alamos RAGE and SPECTRUM codes. We find that they will be visible at z = 10-15 to the James Webb Space Telescope and z = 4-5 to the Wide-Field Infrared Survey Telescope, tracing star formation rates in the first galaxies and at the end of cosmological reionization. If, however, the hypernova crashes into a dense shell ejected by its progenitor, it is expected that a superluminous event will occur that may be seen at z ∼ 20 in the first generation of stars.