Science.gov

Sample records for portable field trihalomethane

  1. REAGENTLESS FIELD-USABLE FIXED-SITE AND PORTABLE ANALYZER FOR TRIHALOMETHANE (THM) CONCENTRATIONS IN DRINKING WATER - PHASE I

    EPA Science Inventory

    Environmental Protection Agency rules stipulate that corrective action be taken for drinking water distribution systems that exceed the maximum contaminant level (MCL) for total Trihalomethanes (TTHMs) 80μg/L.  Real-time, or even periodic, monitoring of drinking water i...

  2. Natural abiotic formation of trihalomethanes in soil: results from laboratory studies and field samples.

    PubMed

    Huber, Stefan G; Kotte, K; Schöler, Heinz F; Williams, J

    2009-07-01

    Trihalomethanes (THM), especially trichloromethane, play an important role in photochemical processes of the lower atmosphere, but the current knowledge of the known sources and sinks of trichloromethane is still incomplete. The trichloromethane flux through the environment is estimated at approximately 660 kt year(-1) and 90% of the emissions are of natural origin. Next to offshore seawater contributing approximately 360 kt year(-1) unknown soil processes are the most prominent source (approximately 220 kt year(-1)). This paper describes a new abiotic source of trichloromethane from the terrestrial environment induced by the oxidation of organic matter by iron(III) and hydrogen peroxide in the presence of chloride. Different organic-rich soils and a series of organic substances regarded as monomeric constituents of humus were investigated for their release of trichloromethene. The influence of iron(III), hydrogen peroxide, halide, and pH on its formation was assayed. The optimal reaction turn over for the representative compound catechol was 58.4 ng of CHCl3 from 1.8 mg of carbon applying chloride and 1.55 microg of CHBr3 from 1.8 mg of carbon applying bromide; resorcin and hydroquinone displayed similar numbers. Results presented in this paper pinpoint 1,2,4,5-tetrahydroxybenzene as playing a key role as intermediate in the formation pathway of the trihalomethanes. The highest THM yields were obtained when applying the oxidized form of 1,2,4,5-tetrahydroxybenzene as THM precursor. These findings are consistent with the well-known degradation pathway starting from resorcin-like dihydroxylated compounds proceeding via further hydroxylation and after halogenation finally ending up in trihalomethanes. In conclusion, Fenton-like reaction conditions (iron(III) and hydrogen peroxide), elevated halide content and an extended reaction time can be seen as the most important parameters required for an optimal THM formation. PMID:19673288

  3. Field-portable lensfree tomographic microscope†

    PubMed Central

    Isikman, Serhan O.; Bishara, Waheb; Sikora, Uzair; Yaglidere, Oguzhan; Yeah, John; Ozcan, Aydogan

    2011-01-01

    We present a field-portable lensfree tomographic microscope, which can achieve sectional imaging of a large volume (~20 mm3) on a chip with an axial resolution of <7 μm. In this compact tomographic imaging platform (weighing only ~110 grams), 24 light-emitting diodes (LEDs) that are each butt-coupled to a fibre-optic waveguide are controlled through a cost-effective micro-processor to sequentially illuminate the sample from different angles to record lensfree holograms of the sample that is placed on the top of a digital sensor array. In order to generate pixel super-resolved (SR) lensfree holograms and hence digitally improve the achievable lateral resolution, multiple sub-pixel shifted holograms are recorded at each illumination angle by electromagnetically actuating the fibre-optic waveguides using compact coils and magnets. These SR projection holograms obtained over an angular range of ~50° are rapidly reconstructed to yield projection images of the sample, which can then be back-projected to compute tomograms of the objects on the sensor-chip. The performance of this compact and light-weight lensfree tomographic microscope is validated by imaging micro-beads of different dimensions as well as a Hymenolepis nana egg, which is an infectious parasitic flatworm. Achieving a decent three-dimensional spatial resolution, this field-portable on-chip optical tomographic microscope might provide a useful toolset for telemedicine and high-throughput imaging applications in resource-poor settings. PMID:21573311

  4. Development of field portable sampling and analysis systems

    SciTech Connect

    Beals, D.

    2000-06-08

    A rapid field portable sample and analysis system has been demonstrated at the Savannah River Site and the Hanford Site. The portable system can be used when rapid decisions are needed in the field during scoping or remediation activities, or when it is impractical to bring large volumes of water to the lab for analysis.

  5. Digital radiography for the field: a portable prototype.

    PubMed

    Cho, Kenneth H; Freckleton, Michael W

    2002-01-01

    The US military has been investigating methods for improving radiographic support for field medical operations. The purpose of this project was to develop and test a portable digital radiography (DR) system to determine its feasibility for field operations. A prototype portable digital radiography device was designed and assembled using a commercially available DR sensor. The sensor and necessary hardware were mounted into a ruggedized aluminum case. The device underwent testing in the hospital and field environments. The prototype rapidly provided digital radiographs in a variety of settings. Shortcomings of the device affecting usability and reliable operation were identified. The successful construction and operation of a portable digital radiography prototype shows that such a device is feasible for field applications. The prototype requires further modification and testing to improve its usability and reliability, and to explore other potential applications, both military and civilian. PMID:12105726

  6. Portable instrumentation for environmental field studies

    NASA Astrophysics Data System (ADS)

    1980-09-01

    Low-power, portable instruments have been developed for measuring gas exchange on individual plant leaves, the aggregate carbon uptake and release of vast jungle and forest areas, and methane concentrations in and around the dense fog resulting from a liquefied-natural-gas (LNG) spill. The group includes a battery powered carbon dioxide sensor and three specialized instruments that incorporate it in various ways: a minicuvette gas-exchange monitor, a rapid-response carbon-dioxide-flux sensor with a high-speed, cooled IR detector, a response time of 10 ms and a sensitivity of about 0.03 ppm CO2, and a methane monitor with the optical path shortened to 5 cm and with a quadrupled IR output.

  7. FIELD COMPARISON OF PORTABLE GAS CHROMATOGRAPHS WITH METHOD TO-14

    EPA Science Inventory

    A field-deployable prototype fast gas chromatograph (FGC) and two commercially-available portable gas chromatographs (PGC) were evaluated by measuring organic vapors in ambient air at a field monitoring site in metropolitan San Juan, Puerto Rico. he data were compared with simult...

  8. The Formation of Trihalomethanes.

    ERIC Educational Resources Information Center

    Trussell, R. Rhodes; Umphres, Mark D.

    1978-01-01

    Reviewed are a number of factors important in the formation of trihalomethanes (THM) including the nature of aquatic humus and the influences of preozonation, bromide, pH, and chlorine. A brief investigation is also conducted into the kinetics of the THM reaction. Several major research needs are represented. (CS)

  9. Portable field kit for determining uranium in water

    USGS Publications Warehouse

    McHugh, John B.

    1979-01-01

    The pressing need for on-site field analyses of the uranium content of surface and ground waters has promoted the development of a simple, light-weight, relatively cheap, portable kit to make such determinations in the field. Forty to sixty water samples per day can be analyzed for uranium to less than 0.2 parts per billion. The kit was tested in the field with excellent results.

  10. Portable power tool machines weld joints in field

    NASA Technical Reports Server (NTRS)

    Spier, R. A.

    1966-01-01

    Portable routing machine for cutting precise weld joints required by nonstandard pipe sections used in the field for transfer of cryogenic fluids. This tool is adaptable for various sizes of pipes and has a selection of router bits for different joint configurations.

  11. Real-World Physics: A Portable MBL for Field Measurements.

    ERIC Educational Resources Information Center

    Albergotti, Clifton

    1994-01-01

    Uses a moderately priced digital multimeter that has output and software compatible with personal computers to make a portable, computer-based data-acquisition system. The system can measure voltage, current, frequency, capacitance, transistor hFE, and temperature. Describes field measures of velocity, acceleration, and temperature as function of…

  12. Portable Radiometer Identifies Minerals in the Field

    NASA Technical Reports Server (NTRS)

    Goetz, A. F. H.; Machida, R. A.

    1982-01-01

    Hand-held optical instrument aids in identifying minerals in field. Can be used in exploration for minerals on foot or by aircraft. The radiometer is especially suitable for identifying clay and carbonate minerals. Radiometer measures reflectances of mineral at two wavelengths, computes ratio of reflectances, and displays ratio to user.

  13. Field Testing of a Portable Radiation Detector and Mapping System

    SciTech Connect

    Hofstetter, K.J.; Hayes, D.W.; Eakle, R.F.

    1998-03-01

    Researchers at the Savannah River Site (SRS) have developed a man- portable radiation detector and mapping system (RADMAPS) which integrates the accumulation of radiation information with precise ground locations. RADMAPS provides field personnel with the ability to detect, locate, and characterize nuclear material at a site or facility by analyzing the gamma or neutron spectra and correlating them with position. the man-portable field unit records gamma or neutron count rate information and its location, along with date and time, using an embedded Global Positioning System (GPS). RADMAPS is an advancement in data fusion, integrating several off-the-shelf technologies with new computer software resulting in a system that is simple to deploy and provides information useful to field personnel in an easily understandable form. Decisions on subsequent actions can be made in the field to efficiently use available field resources. The technologies employed in this system include: recording GPS, radiation detection (typically scintillation detectors), pulse height analysis, analog-to-digital converters, removable solid-state (Flash or SRAM) memory cards, Geographic Information System (GIS) software and personal computers with CD-ROM supporting digital base maps. RADMAPS includes several field deployable data acquisition systems designed to simultaneously record radiation and geographic positions. This paper summarizes the capabilities of RADMAPS and some of the results of field tests performed with the system.

  14. Field-portable pixel super-resolution colour microscope.

    PubMed

    Greenbaum, Alon; Akbari, Najva; Feizi, Alborz; Luo, Wei; Ozcan, Aydogan

    2013-01-01

    Based on partially-coherent digital in-line holography, we report a field-portable microscope that can render lensfree colour images over a wide field-of-view of e.g., >20 mm(2). This computational holographic microscope weighs less than 145 grams with dimensions smaller than 17×6×5 cm, making it especially suitable for field settings and point-of-care use. In this lensfree imaging design, we merged a colorization algorithm with a source shifting based multi-height pixel super-resolution technique to mitigate 'rainbow' like colour artefacts that are typical in holographic imaging. This image processing scheme is based on transforming the colour components of an RGB image into YUV colour space, which separates colour information from brightness component of an image. The resolution of our super-resolution colour microscope was characterized using a USAF test chart to confirm sub-micron spatial resolution, even for reconstructions that employ multi-height phase recovery to handle dense and connected objects. To further demonstrate the performance of this colour microscope Papanicolaou (Pap) smears were also successfully imaged. This field-portable and wide-field computational colour microscope could be useful for tele-medicine applications in resource poor settings. PMID:24086742

  15. Field-Portable Pixel Super-Resolution Colour Microscope

    PubMed Central

    Greenbaum, Alon; Akbari, Najva; Feizi, Alborz; Luo, Wei; Ozcan, Aydogan

    2013-01-01

    Based on partially-coherent digital in-line holography, we report a field-portable microscope that can render lensfree colour images over a wide field-of-view of e.g., >20 mm2. This computational holographic microscope weighs less than 145 grams with dimensions smaller than 17×6×5 cm, making it especially suitable for field settings and point-of-care use. In this lensfree imaging design, we merged a colorization algorithm with a source shifting based multi-height pixel super-resolution technique to mitigate ‘rainbow’ like colour artefacts that are typical in holographic imaging. This image processing scheme is based on transforming the colour components of an RGB image into YUV colour space, which separates colour information from brightness component of an image. The resolution of our super-resolution colour microscope was characterized using a USAF test chart to confirm sub-micron spatial resolution, even for reconstructions that employ multi-height phase recovery to handle dense and connected objects. To further demonstrate the performance of this colour microscope Papanicolaou (Pap) smears were also successfully imaged. This field-portable and wide-field computational colour microscope could be useful for tele-medicine applications in resource poor settings. PMID:24086742

  16. Portable Imagery Quality Assessment Test Field for Uav Sensors

    NASA Astrophysics Data System (ADS)

    Dąbrowski, R.; Jenerowicz, A.

    2015-08-01

    Nowadays the imagery data acquired from UAV sensors are the main source of all data used in various remote sensing applications, photogrammetry projects and in imagery intelligence (IMINT) as well as in other tasks as decision support. Therefore quality assessment of such imagery is an important task. The research team from Military University of Technology, Faculty of Civil Engineering and Geodesy, Geodesy Institute, Department of Remote Sensing and Photogrammetry has designed and prepared special test field- The Portable Imagery Quality Assessment Test Field (PIQuAT) that provides quality assessment in field conditions of images obtained with sensors mounted on UAVs. The PIQuAT consists of 6 individual segments, when combined allow for determine radiometric, spectral and spatial resolution of images acquired from UAVs. All segments of the PIQuAT can be used together in various configurations or independently. All elements of The Portable Imagery Quality Assessment Test Field were tested in laboratory conditions in terms of their radiometry and spectral reflectance characteristics.

  17. A Field Portable Hyperspectral Goniometer for Coastal Characterization

    NASA Technical Reports Server (NTRS)

    Bachmann, Charles M.; Gray, Deric; Abelev, Andrei; Philpot, William; Fusina, Robert A.; Musser, Joseph A.; Vermillion, Michael; Doctor, Katarina; White, Maurice; Georgiev, Georgi

    2012-01-01

    During an airborne multi-sensor remote sensing experiment at the Virginia Coast Reserve (VCR) Long Term Ecological Research (LTER) site in June 2011 (VCR '11), first measurements were taken with the new NRL Goniometer for Outdoor Portable Hyperspectral Earth Reflectance (GOPHER). GOPHER measures the angular distribution of hyperspectral reflectance. GOPHER was constructed for NRL by Spectra Vista Corporation (SVC) and the University of Lethbridge through a capital equipment purchase in 2010. The GOPHER spectrometer is an SVC HR -1024, which measures hyperspectral reflectance over the range from 350 -2500 nm, the visible, near infrared, and short-wave infrared. During measurements, the spectrometer travels along a zenith quarter -arc track that can rotate in azimuth, allowing for measurement of the bi-directional reflectance distribution function (BRDF) over the whole hemisphere. The zenith arc has a radius of approximately 2m, and the spectrometer scan pattern can be programmed on the fly during calibration and validation efforts. The spectrometer and zenith arc assembly can be raised and lowered along a mast to allow for measurement of uneven terrain or vegetation canopies of moderate height. Hydraulics on the chassis allow for leveling of the instrument in the field. At just over 400 lbs, GOPHER is a field portable instrument and can be transformed into a compact trailer assembly for movement over long distances in the field.

  18. TRIHALOMETHANE LEVELS AND SEMEN QUALITY

    EPA Science Inventory

    Trihalomethanes (THMs) are common byproducts of chlorinating drinking water. The effects of disinfection byproducts on semen quality have not yet been studied in humans, despite animal studies linking exposure to sperm abnormalities. We are currently analyzing the relationship of...

  19. Development of a portable field monitor for PCBs. Final report

    SciTech Connect

    Bostick, W.D.; Denton, M.S.; Dinsmore, S.R.

    1983-01-01

    With the advent of recent regulations and those yet pending concerning allowable concentrations of polychlorinated biphenyls (PCBs), personnel in all aspects of the electric power industry, analytical support personnel, and those in the regulatory functions themselves have realized that the PCB problem, as well as these associated regulations, has far surpassed available monitoring capability. In short, detailed, stringent regulations are being set for contamination levels where no accepted ASTM procedure or instrumentation exists. The largest PCB problems occur in the form of PCB-contaminated oil in field transformers and storage containers, and pure askarel in transformers and capacitors. The most immediate need for a portable field instrument would be for use under PCB spill conditions. Portable monitors based on the principles of photoionization detection (PID) and infrared spectroscopy (IR) have been adapted and evaluated for this purpose. The latter includes both flow cell and horizontal multiple internal reflectance (HMIR) sampling configurations. Extensive work has also been performed on solvent-solvent and solvent-soil extractions, as well as PCB adsorption on packings, for use under spill conditions.

  20. Portable piezoelectric crystal detector for field monitoring of environmental pollutants

    SciTech Connect

    Ho, M.H.; Guilbault, G.G.; Rietz, B.

    1983-09-01

    A portable field monitor was constructed by using a coated piezoelectric crystal for direct monitoring of toluene in a Danish printing plant. Toluene vapor was adsorbed onto the Pluronic F-68 coating on a quartz crystal and a decrease in frequency was observed. Various substances which could interfere with toluene determination were tested. No interference from CO, NH/sub 3/, SO/sub 2/, HCl at 100 ppm are expected. Water vapor interfered and was selectively removed using a Nafion permeation tube. The readings from the piezoelectric detector were compared to two accepted procedures for monitoring toluene, the photoionization detector and the Drager tube. Results indicate that the piezoelectric detector gave data consistent with both other methods and with better relative standard deviations than the other two. 8 references, 2 figures, 1 table.

  1. A Portable, Field-Deployable Analyzer for Isotopic Water Measurements

    NASA Astrophysics Data System (ADS)

    Berman, E. S.; Gupta, M.; Huang, Y. W.; Lacelle, D.; McKay, C. P.; Fortson, S.

    2015-12-01

    Water stable isotopes have for many years been used to study the hydrological cycle, catchment hydrology, and polar climate among other applications. Typically, discrete water samples are collected and transported to a laboratory for isotope analysis. Due to the expense and labor associated with such sampling, isotope studies have generally been limited in scope and time-resolution. Field sampling of water isotopes has been shown in recent years to provide dense data sets with the increased time resolution illuminating substantially greater short term variability than is generally observed during discrete sampling. A truly portable instrument also opens the possibility to utilize the instrument as a tool for identifying which water samples would be particularly interesting for further laboratory investigation. To make possible such field measurements of liquid water isotopes, Los Gatos Research has developed a miniaturized, field-deployable liquid water isotope analyzer. The prototype miniature liquid water isotope analyzer (mini-LWIA) uses LGR's patented Off-Axis ICOS (Integrated Cavity Output Spectroscopy) technology in a rugged, Pelican case housing for easy transport and field operations. The analyzer simultaneously measures both δ2H and δ18O from liquid water, with both manual and automatic water introduction options. The laboratory precision for δ2H is 0.6 ‰, and for δ18O is 0.3 ‰. The mini-LWIA was deployed in the high Arctic during the summer of 2015 at Inuvik in the Canadian Northwest Territories. Samples were collected from Sachs Harbor, on the southwest coast of Banks Island, including buried basal ice from the Lurentide Ice Sheet, some ice wedges, and other types of ground ice. Methodology and water analysis results from this extreme field deployment will be presented.

  2. Detection of hazardous chemicals using field-portable Raman spectroscopy

    NASA Astrophysics Data System (ADS)

    Wright, Cherylyn W.; Harvey, Scott D.; Wright, Bob W.

    2003-07-01

    A major challenge confronting emergency response, border control, and other security-related functions is the accurate, rapid, and safe identification of potentially hazardous chemicals outside a laboratory environment. Raman spectroscopy is a rapid, non-intrusive technique that can be used to confidently identify many classes of hazardous and potentially explosive compounds based on molecular vibration information. Advances in instrumentation now allow reliable field - portable measurements to be made. Before the Raman technique can be effectively applied and be accepted within the scientific community, realistic studies must be performed to develop methods, define limitations, and rigorously evaluate its effectiveness. Examples of a variety of chemicals (including neat and diluted chemical warfare [CW] agents, a CW agent precursor, a biological warfare (BW)-related compound, an illicit drug, and explosives) identified using Raman spectroscopy in various types of containers and on surfaces are given, as well as results from a blind field test of 29 unknown samples which included CW agent precursors and/or degradation products, solvents associated with CW agent production, pesticides, explosives, and BW toxins (mostly mycotoxins). Additionally, results of experimental studies to evaluate the analysis of flammable organic solvents, propellants, military explosives, mixtures containing military explosives, shock-sensitive explosives, and gun powders are described with safety guidelines. Spectral masks for screening unknown samples for explosives and nerve agents are given.

  3. Development of a field-portable air monitor for Lewisite

    SciTech Connect

    Aldstadt, J.H.; Martin, A.F.; Olson, D.C. |

    1996-03-01

    The focus of this research is the development of a prototype field-portable ambient-air monitor for measuring trace levels of volatile organoarsenicals. Lewisite (dichloro[2-chlorovinyl]arsine) is a chemical warfare agent developed during World War I and stockpiled on a large scale by the former Soviet Union. A continuous air monitor for Lewisite at the eight-hour time-weighted-average concentration (3 {mu}g/m{sup 3}) is necessary to protect the safety and health of arms control treaty inspectors. Flow injection is used to integrate an air sampling device based on liquid-phase extraction with a flow-through detector based on potentiometric stripping analysis. We describe a method for the sampling and preconcentration of organoarsenicals from ambient air by using a gas permeation membrane sampler. The sampler is designed to selectively preconcentrate analyte that permeates a silicone rubber membrane into a caustic carrier stream. Instrument design is described for the sampling and detection methodologies.

  4. Portable narcotics detector and the results obtained in field tests

    NASA Astrophysics Data System (ADS)

    Tumer, Tumay O.; Su, Chih-Wu; Kaplan, Christopher R.; Rigdon, Stephen W.

    1997-02-01

    A compact integrated narcotics detection instrument (CINDI) has been developed at NOVA R&D, Inc. with funding provided by the U.S. Coast Guard. CINDI is designed as a portable sensitive neutron backscatter detector which has excellent penetration for thick and high Z compartment barriers. It also has a highly sensitive detection system for backscattered neutrons and, therefore, uses a very weak californium-252 neutron source. Neutrons backscatter profusely from materials that have a large hydrogen content, such as narcotics. The rate of backscattered neutrons detected is analyzed by a microprocessor and displayed on the control panel. The operator guides the detector along a suspected area and displays in real time the backscattered neutron rate. CINDI is capable of detecting narcotics effectively behind panels made of steel, wood, fiberglass, or even lead-lined materials. This makes it useful for inspecting marine vessels, ship bulkheads, automobiles, structure walls or small sealed containers. The strong response of CINDI to hydrogen-rich materials such as narcotics makes it an effective tool for detecting concealed drugs. Its response has been field tested by NOVA, the U.S. Coast Guard and Brewt Power Systems. The results of the tests show excellent response and specificity to narcotic drugs. Several large shipments of concealed drugs have been discovered during these trials and the results are presented and discussed.

  5. Portable Remote Imaging Spectrometer (PRISM): Laboratory and Field Calibration

    NASA Technical Reports Server (NTRS)

    Mouroulis, Pantazis; Van Gorp, Byron; Green, Robert O.; Eastwood, Michael; Boardman, Joseph; Richardson, Brandon S.; Rodriguez, Jose I.; Urquiza, Eugenio; Franklin, Brian D.; Gao, Bo-Cai

    2012-01-01

    We report the characteristics of the Portable Remote Imaging Spectrometer, an airborne sensor specifically designed for the challenges of coastal ocean research. PRISM has high signal to noise ratio and uniformity, as well as low polarization sensitivity. Acquisition of high quality data has been demonstrated with the first engineering flight.

  6. AN IMPROVED PORTABLE SURGICAL TABLE FOR THE FIELD AND LABORATORY

    EPA Science Inventory

    I substantially modified a portable surgical table design by Courtois (1981) to increase its durability and utility. The new design incorporated durable plastic components, a nonskid neoprene surgery surface, and surgical tool bins. The system was used to implant fish and amphibi...

  7. Portable multichannel fiber optic biosensor for field detection

    NASA Astrophysics Data System (ADS)

    Golden, Joel P.; Saaski, Elric W.; Shriver-Lake, Lisa C.; Anderson, George P.; Ligler, Frances S.

    1997-04-01

    A compact, portable fiber optic biosensor is developed that enables monitoring of up to four fiber optic probes simultaneously. The sensor employs a novel optical fiber bundle jumper for exciting and collecting fluorescence emission from the evanescent wave fiber optic probes. A single fiber in the center of the bundle couples laser excitation into the sensor probe, while the surrounding fibers collect the returning fluorescent emission light. This design requires no beamsplitter, enabling the detection optics and control circuitry to be reduced to a 4 X 6 in. circuit card. Four of these cards are integrated into a single portable system. Results from detection assays for hazardous biological agents and an environmental pollutant are shown.

  8. Field-usable portable analyzer for chlorinated organic compounds

    SciTech Connect

    Buttner, W.J.

    1994-12-31

    Using an advanced chemical sensor, a hand portable analytical instrument for selectively detecting vapors of chlorinated solvents was produced. Phase I involved the development and testing of the analyzer and samplers for vapors over a broad concentration range from different sample matrices. The instrument, the RCL MONITOR, was tested in actual hazardous waste site operations. Phase II (initiated June 1994) involves production of full scale units and deployment in actual DOE operations (Hanford, INEL, Savannah River).

  9. Tackling field-portable Raman spectroscopy of real world samples

    NASA Astrophysics Data System (ADS)

    Shand, Neil C.

    2008-10-01

    A major challenge confronting first responders, customs authorities and other security-related organisations is the accurate, rapid, and safe identification of potentially hazardous chemicals outside a laboratory environment. Currently, a range of hand portable Raman equipment is commercially available that is low cost and increasingly more sophisticated. These systems are generally based on the 785nm Stokes shifted Raman technique with many using dispersive grating spectrometers. This technique offers a broad range of capabilities including the ability to analyse illicit drugs, explosives, chemical weapons and pre-cursors but still has some fundamental constraints. 'Real world' samples, such as those found at a crime scene, will often not be presented in the most accessible manner. Simple issues such as glass fluorescence can make an otherwise tractable sample impossible to analyse in-situ. A new generation of portable Raman equipment is currently being developed to address these issues. Consideration is given to the use of longer wavelength for fluorescence reduction. Alternative optical designs are being tested to compensate for the signal reduction incurred by moving to longer wavelengths. Furthermore, the use of anti-Stokes spectroscopy is being considered as well as investigating the robustness and portability of traditional Fourier Transform interferometer designs along with future advances in detector technology and ultra small spectrometers.

  10. ANOLE Portable Radiation Detection System Field Test and Evaluation Campaign

    SciTech Connect

    Chris A. Hodge

    2007-07-12

    Handheld, backpack, and mobile sensors are elements of the Global Nuclear Detection System for the interdiction and control of illicit radiological and nuclear materials. They are used by the U.S. Department of Homeland Security (DHS) and other government agencies and organizations in various roles for border protection, law enforcement, and nonproliferation monitoring. In order to systematically document the operational performance of the common commercial off-the-shelf portable radiation detection systems, the DHS Domestic Nuclear Detection Office conducted a test and evaluation campaign conducted at the Nevada Test Site from January 18 to February 27, 2006. Named “Anole,” it was the first test of its kind in terms of technical design and test complexities. The Anole test results offer users information for selecting appropriate mission-specific portable radiation detection systems. The campaign also offered manufacturers the opportunity to submit their equipment for independent operationally relevant testing to subsequently improve their detector performance. This paper will present the design, execution, and methodologies of the DHS Anole portable radiation detection system test campaign.

  11. Implementation of a Portable HPGe for Field Contamination Assay.

    PubMed

    Hayes, Robert Bruce

    2016-06-01

    Using MCNP to construct a detector model based initially on x-ray images of a portable high purity germanium (HPGe) detector followed by normalizing covering material values to also agree with check source responses, a validation of the model was attained. By calibrating the detector parameters using large count spectra, rigorous reproducibility is attained for high activity measurements but does not prevent deviations from normality in error distributions at the very low count events where spectral peaks are not always identifiable. The resulting model was created to allow operational assay of contamination over large areal distributions that could not otherwise be measured, such as the exhaust shaft at the Waste Isolation Pilot Plant (WIPP). Results indicate that contamination levels of activity in the exhaust shaft can be assayed to within a factor of 2. Detection limits are evaluated to be well below the contamination levels, which would constitute a legal environmental release if unfiltered ventilation of the underground facility were used. PMID:27115224

  12. TESTING, PERFORMANCE VALIDATION AND QUALITY ASSURANCE/QUALITY CONTROL OF FIELD-PORTABLE INSTRUMENTATION

    EPA Science Inventory

    New technologies for field-portable monitoring instruments often have a long lead time in development and authorization. Some obstacles to the acceptance of these pilot technologies include concern about liabilities, reluctance to take risks on new technologies, and uncertainty a...

  13. ENVIRONMENTAL TECHNOLOGY VERIFICATION REPORT - FIELD PORTABLE X-RAY FLUORESCENCE ANALYZER - HNU SYSTEMS, SEFA-P

    EPA Science Inventory

    In April 1995, the Environmental Protection Agency (EPA) conducted a demonstration of field portable X-ray fluorescence (FPXRF) Analyzers. The primary objectives of this demonstration were (1) to determine how well FPXRF analyzers perform in comparison to a standard reference m...

  14. ENVIRONMENTAL TECHNOLOGY VERIFICATION REPORT - FIELD PORTABLE X-RAY FLUORESCENCE ANALYZER - SCITEC, MAP SPECTRUM ANALYZER

    EPA Science Inventory

    In April 1995, the U.S. Environmental Protection Agency (EPA) sponsored a demonstration of field portable X-ray fluorescence (FPXRF) analyzers. The primary objectives of this demonstration were (1) to determine how well FPXRF analyzers perform in comparison to standard reference...

  15. A Field-Portable X-Ray Fluorescence Instrument: Design and Applications

    SciTech Connect

    Civici, Nikolla

    2007-04-23

    The field portable XRF (FPXRF) spectrometer is composed of a measuring head that holds the detector (Si-PIN) and the excitation sources (Cd-109 and Am-241) and the spectrum acquisition system. The application of this system for the analysis of cultural heritage artifacts will be presented and discussed.

  16. CHARACTERIZATION OF CHROMIUM-CONTAMINATED SOILS USING FIELD-PORTABLE X-RAY FLUORESCENCE

    EPA Science Inventory

    A detailed characterization of the underlying and adjacent soils near a chrome plating shop utilized field-portable X- ray fluorescence (XRF) as a screening tool. XRF permitted real-time acquisition of estimates for total metal content of soils. A trailer-mounted soil coring unit...

  17. Design, construction and calibration of a portable boundary layer wind tunnel for field use

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Wind tunnels have been used for several decades to study wind erosion processes. Portable wind tunnels offer the advantage of testing natural surfaces in the field, but they must be carefully designed to insure that a logarithmic boundary layer is formed and that wind erosion processes may develop ...

  18. General purpose, field-portable cell-based biosensor platform.

    PubMed

    Gilchrist, K H; Barker, V N; Fletcher, L E; DeBusschere, B D; Ghanouni, P; Giovangrandi, L; Kovacs, G T

    2001-09-01

    There are several groups of researchers developing cell-based biosensors for chemical and biological warfare agents based on electrophysiologic monitoring of cells. In order to transition such sensors from the laboratory to the field, a general-purpose hardware and software platform is required. This paper describes the design, implementation, and field-testing of such a system, consisting of cell-transport and data acquisition instruments. The cell-transport module is a self-contained, battery-powered instrument that allows various types of cell-based modules to be maintained at a preset temperature and ambient CO(2) level while in transit or in the field. The data acquisition module provides 32 channels of action potential amplification, filtering, and real-time data streaming to a laptop computer. At present, detailed analysis of the data acquired is carried out off-line, but sufficient computing power is available in the data acquisition module to enable the most useful algorithms to eventually be run real-time in the field. Both modules have sufficient internal power to permit realistic field-testing, such as the example presented in this paper. PMID:11544049

  19. Preliminary field measurement of cotton fiber micronaire by portable NIR

    Technology Transfer Automated Retrieval System (TEKTRAN)

    The decline of the U.S. textile industry has led to the dramatic increase in the export of U.S. cotton. Improved quality measurement systems are needed to successfully compete in the global marketplace. One key need is the development of new breeder/producer quality tools for field and at-line mea...

  20. Field portable low temperature porous layer open tubular cryoadsorption headspace sampling and analysis part II: Applications.

    PubMed

    Harries, Megan; Bukovsky-Reyes, Santiago; Bruno, Thomas J

    2016-01-15

    This paper details the sampling methods used with the field portable porous layer open tubular cryoadsorption (PLOT-cryo) approach, described in Part I of this two-part series, applied to several analytes of interest. We conducted tests with coumarin and 2,4,6-trinitrotoluene (two solutes that were used in initial development of PLOT-cryo technology), naphthalene, aviation turbine kerosene, and diesel fuel, on a variety of matrices and test beds. We demonstrated that these analytes can be easily detected and reliably identified using the portable unit for analyte collection. By leveraging efficiency-boosting temperature control and the high flow rate multiple capillary wafer, very short collection times (as low as 3s) yielded accurate detection. For diesel fuel spiked on glass beads, we determined a method detection limit below 1 ppm. We observed greater variability among separate samples analyzed with the portable unit than previously documented in work using the laboratory-based PLOT-cryo technology. We identify three likely sources that may help explain the additional variation: the use of a compressed air source to generate suction, matrix geometry, and variability in the local vapor concentration around the sampling probe as solute depletion occurs both locally around the probe and in the test bed as a whole. This field-portable adaptation of the PLOT-cryo approach has numerous and diverse potential applications. PMID:26726934

  1. A portable modular optical sensor capable of measuring complex multi-axis strain fields

    NASA Astrophysics Data System (ADS)

    Zhao, Weixin; Beck, B. Terry; Peterman, Robert J.; Wu, Chih-Hang J.

    2012-10-01

    This paper presents a portable optical sensor capable of measuring complex multi-axis strain fields without the need for special surface preparation or stringent sensor-to-surface alignment. The sensor consists of three to four electronic speckle photography (ESP) modules. The design of each modular element is based on a previously developed 5-axis (five degree of freedom) surface displacement measurement technique, and is able to measure two dimensional in-plane surface movement, unaffected by other degrees of freedom (displacement and rotation) movement. Identical modular strain elements are arranged in a Rosette grid layout so that accurate and robust multi-axis surface strain measurement can be achieved. Experiments were conducted to demonstrate the multi-axis strain field measurement capability of this optical sensor by using a test bed that provided a known directional planar strain field, and excellent results were obtained. In particular, experiments have shown that the principle strain can be accurately extracted independent of the orientation of the device. This portable optical sensor will allow precise non-contact measurement of practical complex strain fields such as those encountered in bridge abutments, and portions of beams near critical infrastructure support locations; in other words, wherever plane strains depart from uni-axial behavior. Its unique hand-held portable capability offers distinct advantages over laboratory strain measurement setups, allowing accurate robust non-contact measurements to be achieved even in a harsh field application environment.

  2. Field-usable portable analyzer for chlorinated organic compounds

    SciTech Connect

    Buttner, W.J.; Penrose, W.R.; Stetter, J.R.

    1995-10-01

    Transducer Research, Inc. (TRI) has been working with the DOE Morgantown Energy Technology Center to develop a new chemical monitor based on a unique sensor which responds selectively to vapors of chlorinated solvents. We are also developing field applications for the monitor in actual DOE cleanup operations. During the initial phase, prototype instruments were built and field tested. Because of the high degree of selectivity that is obtained, no response was observed with common hydrocarbon organic compounds such as BTX (benzene, toluene, xylene) or POLs (petroleum, oil, lubricants), and in fact, no non-halogen-containing chemical has been identified which induces a measurable response. By the end of the Phase I effort, a finished instrument system was developed and test marketed. This instrument, called the RCL MONITOR, was designed to analyze individual samples or monitor an area with automated repetitive analyses. Vapor levels between 0 and 500 ppm can be determined in 90 s with a lower detection limit of 0.2 ppm using the handportable instrument. In addition to the development of the RCL MONITOR, advanced sampler systems are being developed to: (1) extend the dynamic range of the instrument through autodilution of the vapor and (2) allow chemical analyses to be performed on aqueous samples. When interfaced to the samplers, the RCL MONITOR is capable of measuring chlorinated solvent contamination in the vapor phase up to 5000 ppm and in water and other condensed media from 10 to over 10,000 ppb(wt)--without hydrocarbon and other organic interferences.

  3. Field tests of acoustic telemetry for a portable coastal observatory

    USGS Publications Warehouse

    Martini, M.; Butman, B.; Ware, J.; Frye, D.

    2006-01-01

    Long-term field tests of a low-cost acoustic telemetry system were carried out at two sites in Massachusetts Bay. At each site, an acoustic Doppler current profiler mounted on a bottom tripod was fitted with an acoustic modem to transmit data to a surface buoy; electronics mounted on the buoy relayed these data to shore via radio modem. The mooring at one site (24 m water depth) was custom-designed for the telemetry application, with a custom designed small buoy, a flexible electro-mechanical buoy to mooring joint using a molded chain connection to the buoy, quick-release electro-mechanical couplings, and dual hydrophones suspended 7 m above the bottom. The surface buoy at the second site (33 m water depth) was a U.S. Coast Guard (USCG) channel buoy fitted with telemetry electronics and clamps to hold the hydrophones. The telemetry was tested in several configurations for a period of about four years. The custom-designed buoy and mooring provided nearly error-free data transmission through the acoustic link under a variety of oceanographic conditions for 261 days at the 24 m site. The electro mechanical joint, cables and couplings required minimal servicing and were very reliable, lasting 862 days deployed before needing repairs. The acoustic communication results from the USCG buoy were poor, apparently due to the hard cobble bottom, noise from the all-steel buoy, and failure of the hydrophone assembly. Access to the USCG buoy at sea required ideal weather. ??2006 IEEE.

  4. Improvement of portable computed tomography system for on-field applications

    NASA Astrophysics Data System (ADS)

    Sukrod, K.; Khoonkamjorn, P.; Tippayakul, C.

    2015-05-01

    In 2010, Thailand Institute of Nuclear Technology (TINT) received a portable Computed Tomography (CT) system from the IAEA as part of the Regional Cooperative Agreement (RCA) program. This portable CT system has been used as the prototype for development of portable CT system intended for industrial applications since then. This paper discusses the improvements in the attempt to utilize the CT system for on-field applications. The system is foreseen to visualize the amount of agarwood in the live tree trunk. The experiments adopting Am-241 as the radiation source were conducted. The Am-241 source was selected since it emits low energy gamma which should better distinguish small density differences of wood types. Test specimens made of timbers with different densities were prepared and used in the experiments. The cross sectional views of the test specimens were obtained from the CT system using different scanning parameters. It is found from the experiments that the results are promising as the picture can clearly differentiate wood types according to their densities. Also, the optimum scanning parameters were determined from the experiments. The results from this work encourage the research team to advance into the next phase which is to experiment with the real tree on the field.

  5. Stroke at high altitude diagnosed in the field using portable ultrasound.

    PubMed

    Wilson, Mark H; Levett, Denny Z; Dhillon, Sundeep; Mitchell, Kay; Morgan, Jon; Grocott, Michael P W; Imray, Chris

    2011-03-01

    A tool that can differentiate ischemic stroke from other neurological conditions (eg, hemorrhagic stroke, high-altitude cerebral edema) in the field could enable more rapid thrombolysis when appropriate. The resources (eg, an MRI or CT scanner) to investigate stroke at high altitude may be limited, and hence a portable tool would be of benefit. Such a tool may also be of benefit in emergency departments when CT scanning is not available. We report a case of a 49-year-old man who, while climbing at 5900 m, suffered a left middle cerebral infarct. The clinical diagnosis was supported using 2D Power Doppler. The patient received aspirin and continuous transcranial Doppler was used for its potential therapeutic effects for 12 hours. The patient was then evacuated to a hospital in Kathmandu over the next 48 hours. This case report suggests that portable ultrasound could be used in the prehospital arena to enable early diagnosis of thrombotic stroke. PMID:21377120

  6. Portable, battery-operated, low-cost, bright field and fluorescence microscope.

    PubMed

    Miller, Andrew R; Davis, Gregory L; Oden, Z Maria; Razavi, Mohamad Reza; Fateh, Abolfazl; Ghazanfari, Morteza; Abdolrahimi, Farid; Poorazar, Shahin; Sakhaie, Fatemeh; Olsen, Randall J; Bahrmand, Ahmad Reza; Pierce, Mark C; Graviss, Edward A; Richards-Kortum, Rebecca

    2010-01-01

    This study describes the design and evaluation of a portable bright-field and fluorescence microscope that can be manufactured for $240 USD. The microscope uses a battery-operated LED-based flashlight as the light source and achieves a resolution of 0.8 microm at 1000x magnification in fluorescence mode. We tested the diagnostic capability of this new instrument to identify infections caused by the human pathogen, Mycobacterium tuberculosis. Sixty-four direct, decontaminated, and serially diluted smears were prepared from sputa obtained from 19 patients suspected to have M. tuberculosis infection. Slides were stained with auramine orange and evaluated as being positive or negative for M. tuberculosis with both the new portable fluorescence microscope and a laboratory grade fluorescence microscope. Concordant results were obtained in 98.4% of cases. This highly portable, low cost, fluorescence microscope may be a useful diagnostic tool to expand the availability of M. tuberculosis testing at the point-of-care in low resource settings. PMID:20694194

  7. Portable, battery-operated, fluorescence field microscope for the developing world

    NASA Astrophysics Data System (ADS)

    Miller, Andrew R.; Davis, Gregory; Pierce, Mark; Oden, Z. Maria; Richards-Kortum, Rebecca

    2010-02-01

    In many areas of the world, current methods for diagnosis of infectious diseases such as malaria and tuberculosis involve microscopic evaluation of a patient specimen. Advances in fluorescence microscopy can improve diagnostic sensitivity and reduce time and expertise necessary to interpret diagnostic results. However, modern research-grade microscopes are neither available nor appropriate for use in many settings in the developing world. To address this need, we designed, fabricated, and tested a portable, battery-powered, bright field and fluorescence inverted field microscope, optimized for infrastructural constraints of the developing world. We characterized an initial prototype constructed with rapidprototyping techniques, which utilized low-cost, over-the-counter components such as a battery-powered LED flashlight as the light source. The microscope exhibited suitable spatial resolution (0.8 μm) in fluorescence mode to resolve M. tuberculosis bacilli. In bright field mode, malaria parasites were resolvable at 1000x magnification. The initial prototype cost 480 USD and we estimate that the microscope can be manufactured for 230 USD. While future studies are planned to evaluate ease-of-use and reliability, our current system serves as a proof of concept that combined fluorescence and bright field microscopy is possible in a low-cost and portable system.

  8. Development of a miniaturized, light-weight magnetic sector for a field-portable mass spectrograph

    NASA Technical Reports Server (NTRS)

    Sinha, M. P.; Tomassian, A. D.

    1991-01-01

    A miniaturized, lightweight magnetic sector for a focal plane mass spectrograph (Mattauch-Herzog design) has been designed and fabricated by using a new high-energy-product magnet material (Nd-B-Fe alloy) and a high permeability magnet yoke material (V-Co-Fe alloy). The magnetic sector weighs less than 10 kg, has a focal plane of 5.1 cm in length, and covers a nominal mass range of 40-240 amu. Such a magnetic sector, in conjunction with an array detector and a short microbore capillary column, is well suited for the development of a field-portable gas chromatograph-mass spectrometer instrument of high performance.

  9. Feasibility of field portable near infrared (NIR) spectroscopy to determine cyanide concentrations in soil

    NASA Astrophysics Data System (ADS)

    Sut, Magdalena; Fischer, Thomas; Repmann, Frank; Raab, Thomas

    2013-04-01

    In Germany, at more than 1000 sites, soil is polluted with an anthropogenic contaminant in form of iron-cyanide complexes. These contaminations are caused by former Manufactured Gas Plants (MGPs), where electricity for lighting was produced in the process of coal gasification. The production of manufactured gas was restrained in 1950, which caused cessation of MGPs. Our study describes the application of Polychromix Handheld Field Portable Near-Infrared (NIR) Analyzer to predict the cyanide concentrations in soil. In recent times, when the soil remediation is of major importance, there is a need to develop rapid and non-destructive methods for contaminant determination in the field. In situ analysis enables determination of 'hot spots', is cheap and time saving in comparison to laboratory methods. This paper presents a novel usage of NIR spectroscopy, where a calibration model was developed, using multivariate calibration algorithms, in order to determine NIR spectral response to the cyanide concentration in soil samples. As a control, the contaminant concentration was determined using conventional Flow Injection Analysis (FIA). The experiments revealed that portable near-infrared spectrometers could be a reliable device for identification of contamination 'hot spots', where cyanide concentration are higher than 2400 mg kg-1 in the field and >1750 mg kg-1 after sample preparation in the laboratory, but cannot replace traditional laboratory analyses due to high limits of detection.

  10. A portable fluorescence spectroscopy imaging system for automated root phenotyping in soil cores in the field.

    PubMed

    Wasson, Anton; Bischof, Leanne; Zwart, Alec; Watt, Michelle

    2016-02-01

    Root architecture traits are a target for pre-breeders. Incorporation of root architecture traits into new cultivars requires phenotyping. It is attractive to rapidly and directly phenotype root architecture in the field, avoiding laboratory studies that may not translate to the field. A combination of soil coring with a hydraulic push press and manual core-break counting can directly phenotype root architecture traits of depth and distribution in the field through to grain development, but large teams of people are required and labour costs are high with this method. We developed a portable fluorescence imaging system (BlueBox) to automate root counting in soil cores with image analysis software directly in the field. The lighting system was optimized to produce high-contrast images of roots emerging from soil cores. The correlation of the measurements with the root length density of the soil cores exceeded the correlation achieved by human operator measurements (R (2)=0.68 versus 0.57, respectively). A BlueBox-equipped team processed 4.3 cores/hour/person, compared with 3.7 cores/hour/person for the manual method. The portable, automated in-field root architecture phenotyping system was 16% more labour efficient, 19% more accurate, and 12% cheaper than manual conventional coring, and presents an opportunity to directly phenotype root architecture in the field as part of pre-breeding programs. The platform has wide possibilities to capture more information about root health and other root traits in the field. PMID:26826219

  11. A portable fluorescence spectroscopy imaging system for automated root phenotyping in soil cores in the field

    PubMed Central

    Wasson, Anton; Bischof, Leanne; Zwart, Alec; Watt, Michelle

    2016-01-01

    Root architecture traits are a target for pre-breeders. Incorporation of root architecture traits into new cultivars requires phenotyping. It is attractive to rapidly and directly phenotype root architecture in the field, avoiding laboratory studies that may not translate to the field. A combination of soil coring with a hydraulic push press and manual core-break counting can directly phenotype root architecture traits of depth and distribution in the field through to grain development, but large teams of people are required and labour costs are high with this method. We developed a portable fluorescence imaging system (BlueBox) to automate root counting in soil cores with image analysis software directly in the field. The lighting system was optimized to produce high-contrast images of roots emerging from soil cores. The correlation of the measurements with the root length density of the soil cores exceeded the correlation achieved by human operator measurements (R 2=0.68 versus 0.57, respectively). A BlueBox-equipped team processed 4.3 cores/hour/person, compared with 3.7 cores/hour/person for the manual method. The portable, automated in-field root architecture phenotyping system was 16% more labour efficient, 19% more accurate, and 12% cheaper than manual conventional coring, and presents an opportunity to directly phenotype root architecture in the field as part of pre-breeding programs. The platform has wide possibilities to capture more information about root health and other root traits in the field. PMID:26826219

  12. Nanoparticle-Based Paper Sensors for Field-Portable Analysis of Antioxidants

    NASA Astrophysics Data System (ADS)

    Sharpe, Erica Marie

    Abstract & Overview: The goal of this thesis was to develop portable nanoparticle-based paper sensors for field analysis, with focus on antioxidant detection. The method introduces a novel concept in the sensing arena that relies on the use of redox active inorganic nanoparticles, primarily cerium oxide, as colorimetric probes to replace commonly used soluble dyes. The sensors have an integrated detection mechanism with all the reagents needed for analysis confined to the sensing platform. Research work in this thesis focuses on the study of the redox and surface chemistry of these particles, their reactivity with target analytes and integration into paper-based platforms. A unique feature of these particles is their ability to replace or stabilize enzymes and extend their operational lifetime providing additional opportunities for improved detection schemes for enzyme-based systems. We demonstrate the above principles for the construction of sensors for detection of analytes such as hydrogen peroxide, glucose, and polyphenolic antioxidants. The advantage of the newly designed system include, in addition to portability and stability, the low production costs, the rapid analysis time, and the ability to provide quantitative information without use of advanced instrumentation. The results of this work opened up new opportunities for designing portable easy-to- use sensors for field analysis. The developed assays are particularly appealing for remote sensing applications where specialized equipment is not available, and also for high throughput analysis of a large number of samples. Our investigation to demonstrate applicability of the system focused primarily on the detection of antioxidants. Therefore, the thesis highlights predominantly this application.

  13. A portable high-field pulsed magnet system for x-ray scattering studies.

    SciTech Connect

    Islam, Z.; Ruff, J.P.C.; Nojiri, H.; Matsuda, Y. H.; Ross, K. A.; Gaulin, B. D.; Qu, Z.; Lang, J. C.

    2009-01-01

    We present a portable pulsed-magnet system for x-ray studies of materials in high magnetic fields (up to 30 T). The apparatus consists of a split-pair of minicoils cooled on a closed-cycle cryostat, which is used for x-ray diffraction studies with applied field normal to the scattering plane. A second independent closed-cycle cryostat is used for cooling the sample to near liquid helium temperatures. Pulsed magnetic fields (- 1 ms in total duration) are generated by discharging a configurable capacitor bank into the magnet coils. Time-resolved scattering data are collected using a combination of a fast single-photon counting detector, a multichannel scaler, and a high-resolution digital storage oscilloscope. The capabilities of this instrument are used to study a geometrically frustrated system revealing strong magnetostrictive effects in the spin-liquid state.

  14. Rapid Measurements of Snow Stratigraphy Using A Portable Penetration Field Instrument

    NASA Astrophysics Data System (ADS)

    Foster, Robert; Louge, Michel; Clifford, Kelly; Decker, Rand

    We describe a new field-portable tool for avalanche forecasting and hydrology that can rapidly generate stratigraphic profiles of density, permittivity and temperature through the snow pack. This penetration instrument consists of a wedged capacitance tip mounted at the end of a pole and a mechanical depth gauge. By appropriate place- ment of its reference, guard and sensor conductive surfaces, the instrument sheds hor- izontal electric field lines resolving horizontal snow layers of 2.5mm thickness. The probe was tested under realistically cold conditions at the mountain resort of Alta near Salt Lake City, Utah. There, it recorded the stratigraphy of the real and imaginary parts of the dielectric constant at 3.9kHz and the temperature through a typical winter snow pack. The portable electronics was carried in a small backpack and the depth was recorded using a rotary digital encoder in frictional contact with the pole. The profiles were automatically acquired on a hand-held Personal Digital Assistant. Using independent calibrations, measurements of the real part provided an accurate profile of density later confirmed by the conventional excavation of a detailed snow cover profile. The ratio of the imaginary and real permittivities also revealed the signature of individual snow layers that could be identified in the excavation.

  15. The Development and Field Testing of the Portable Acousto-optic Spectrometer for Astrobiology

    NASA Astrophysics Data System (ADS)

    Chanover, Nancy J.; Uckert, Kyle; Voelz, David; Boston, Penelope

    2014-11-01

    The development of in situ instrumentation for the detection of biomarkers on planetary surfaces is critical for the search for evidence of present or past life in our solar system. In our earlier instrument development efforts we addressed this need through the development of a near-infrared point spectrometer intended for quick-look examinations of samples that could be subsequently analyzed with a laser desorption time-of-flight mass spectrometer. The point spectrometer utilized an acousto-optic tunable filter (AOTF) crystal as the wavelength selecting element. In parallel with the aforementioned development efforts we identified the need for a portable version of the AOTF spectrometer that we could test and demonstrate in a range of field locations on Earth chosen to serve as terrestrial analogs for extreme environments elsewhere in the solar system. Here we describe the development and field testing of the Portable Acousto-optic Spectrometer for Astrobiology (PASA). We demonstrated this instrument in two very different cave environments, a predominantly gypsum and calcite cave in New Mexico and an actively forming cave rich in hydrated sulfates in Tabasco, Mexico. Both of these microbially active environments contain evidence of biologic alteration of minerals, which can be detected using IR spectroscopy. We will describe the instrument operations and present some data acquired with PASA to demonstrate its efficacy as a tool for biomarker detection on planetary surfaces. This work was supported by NASA's EPSCoR program through grant number NNX12AK77A.

  16. Using Field-Metered Data to Quantify Annual Energy Use of Portable Air Conditioners

    SciTech Connect

    Burke, Thomas; Willem, Henry; Ni, Chun Chun; Stratton, Hannah; Chen, Yuting; Ganeshalingam, Mohan; Iyer, Maithili; Price, Sarah; Dunham, Camilla

    2014-12-01

    As many regions of the United States experience rising temperatures, consumers have come to rely increasingly on cooling appliances (including portable air conditioners) to provide a comfortable indoor temperature. Home occupants sometimes use a portable air conditioner (PAC) to maintain a desired indoor temperature in a single room or enclosed space. Although PACs in residential use are few compared to centrally installed and room air conditioning (AC) units, the past few years have witnessed an increase of PACs use throughout the United States. There is, however, little information and few research projects focused on the energy consumption and performance of PACs, particularly studies that collect information from field applications of PACs. The operation and energy consumption of PACs may differ among geographic locations and households, because of variations in cooling load, frequency, duration of use, and other user-selected settings. In addition, the performance of building envelope (thermal mass and air leakage) as well as inter-zonal mixing within the building would substantially influence the ability to control and maintain desirable indoor thermal conditions. Lawrence Berkeley National Laboratory (LBNL) conducted an initial field-metering study aimed at increasing the knowledge and data related to PAC operation and energy consumption in the United States.

  17. Field portable low temperature porous layer open tubular cryoadsorption headspace sampling and analysis part I: Instrumentation.

    PubMed

    Bruno, Thomas J

    2016-01-15

    Building on the successful application in the laboratory of PLOT-cryoadsorption as a means of collecting vapor (or headspace) samples for chromatographic analysis, in this paper a field portable apparatus is introduced. This device fits inside of a briefcase (aluminum tool carrier), and can be easily transported by vehicle or by air. The portable apparatus functions entirely on compressed air, making it suitable for use in locations lacking electrical power, and for use in flammable and explosive environments. The apparatus consists of four aspects: a field capable PLOT-capillary platform, the supporting equipment platform, the service interface between the PLOT-capillary and the supporting equipment, and the necessary peripherals. Vapor sampling can be done with either a hand piece (containing the PLOT capillary) or with a custom fabricated standoff module. Both the hand piece and the standoff module can be heated and cooled to facilitate vapor collection and subsequent vapor sample removal. The service interface between the support platform and the sampling units makes use of a unique counter current approach that minimizes loss of cooling and heating due to heat transfer with the surroundings (recuperative thermostatting). Several types of PLOT-capillary elements and sampling probes are described in this report. Applications to a variety of samples relevant to forensic and environmental analysis are discussed in a companion paper. PMID:26687166

  18. Moving your laboratories to the field – Advantages and limitations of the use of field portable instruments in environmental sample analysis

    SciTech Connect

    Gałuszka, Agnieszka; Migaszewski, Zdzisław M.; Namieśnik, Jacek

    2015-07-15

    The recent rapid progress in technology of field portable instruments has increased their applications in environmental sample analysis. These instruments offer a possibility of cost-effective, non-destructive, real-time, direct, on-site measurements of a wide range of both inorganic and organic analytes in gaseous, liquid and solid samples. Some of them do not require the use of reagents and do not produce any analytical waste. All these features contribute to the greenness of field portable techniques. Several stationary analytical instruments have their portable versions. The most popular ones include: gas chromatographs with different detectors (mass spectrometer (MS), flame ionization detector, photoionization detector), ultraviolet–visible and near-infrared spectrophotometers, X-ray fluorescence spectrometers, ion mobility spectrometers, electronic noses and electronic tongues. The use of portable instruments in environmental sample analysis gives a possibility of on-site screening and a subsequent selection of samples for routine laboratory analyses. They are also very useful in situations that require an emergency response and for process monitoring applications. However, quantification of results is still problematic in many cases. The other disadvantages include: higher detection limits and lower sensitivity than these obtained in laboratory conditions, a strong influence of environmental factors on the instrument performance and a high possibility of sample contamination in the field. This paper reviews recent applications of field portable instruments in environmental sample analysis and discusses their analytical capabilities. - Highlights: • Field portable instruments are widely used in environmental sample analysis. • Field portable instruments are indispensable for analysis in emergency response. • Miniaturization of field portable instruments reduces resource consumption. • In situ analysis is in agreement with green analytical chemistry

  19. Portable Upconversion Nanoparticles-Based Paper Device for Field Testing of Drug Abuse.

    PubMed

    He, Mengyuan; Li, Zhen; Ge, Yiying; Liu, Zhihong

    2016-02-01

    We report the first portable upconversion nanoparticles (UCNPs)-based paper device for road-side field testing of cocaine. Upon the recognition of cocaine by two pieces of rationally designed aptamer fragments, the luminescence of UCNPs immobilized on the paper is quenched by Au nanoparticles (AuNPs), which indicates the cocaine concentration. This device can give quantitative results in a short time with high sensitivity using only a smartphone as the apparatus. Moreover, this device is applicable in human saliva samples, and it also can be used to monitor the cocaine content change in blood samples. The results of this work demonstrate the prospect of developing UCNPs-based paper devices for field testing of drug abuse. PMID:26786499

  20. 100-OL-1 Operable Unit Field Portable X-Ray Fluorescence (XRF) Analyzer Pilot Study Plans

    SciTech Connect

    Bunn, Amoret L.; Fritz, Brad G.; Wellman, Dawn M.

    2014-07-15

    A pilot study is being conducted to support the approval of the Remedial Investigation/Feasibility Study (RI/FS) Work Plan to evaluate the 100-OL-1 Operable Unit (OU) pre-Hanford orchard lands. Based on comments received by the U.S. Environmental Protection Agency (EPA) and Washington State Department of Ecology, the pilot study will evaluate the use of field portable X-ray fluorescence (XRF) spectrometry measurements for evaluating lead and arsenic concentrations on the soil surface as an indicator of past use of lead arsenate pesticide residue in the OU. The work will be performed in the field during the summer of 2014, and assist in the planning for the characterization activities in the RI/FS.

  1. Field-portable reflection and transmission microscopy based on lensless holography.

    PubMed

    Lee, Myungjun; Yaglidere, Oguzhan; Ozcan, Aydogan

    2011-09-01

    We demonstrate a lensfree dual-mode holographic microscope that can image specimens in both transmission and reflection geometries using in-line transmission and off-axis reflection holography, respectively. This field-portable dual-mode holographic microscope has a weight of ~200 g with dimensions of 15 x 5.5 x 5cm, where a laser source is powered by two batteries. Based on digital in-line holography, our transmission microscope achieves a sub-pixel lateral resolution of ≤2 µm over a wide field-of-view (FOV) of ~24 mm(2) due to its unit fringe magnification geometry. Despite its simplicity and ease of operation, in-line transmission geometry is not suitable to image dense or connected objects such as tissue slides since the reference beam gets distorted causing severe aberrations in reconstruction of such objects. To mitigate this challenge, on the same cost-effective and field-portable assembly we built a lensless reflection mode microscope based on digital off-axis holography where a beam-splitter is used to interfere a tilted reference wave with the reflected light from the object surface, creating an off-axis hologram of the specimens on a CMOS sensor-chip. As a result of the reduced space-bandwidth product of the off-axis geometry compared to its in-line counterpart, the imaging FOV of our reflection mode is reduced to ~9 mm(2), while still achieving a similar sub-pixel resolution of ≤2 µm. We tested the performance of this compact dual-mode microscopy unit by imaging a US-air force resolution test target, various micro-particles as well as a histopathology slide corresponding to skin tissue. Due to its compact, cost-effective, and lightweight design, this dual-mode lensless holographic microscope might especially be useful for field-use or for conducting microscopic analysis in resource-poor settings. PMID:21991559

  2. Field-portable reflection and transmission microscopy based on lensless holography

    PubMed Central

    Lee, Myungjun; Yaglidere, Oguzhan; Ozcan, Aydogan

    2011-01-01

    We demonstrate a lensfree dual-mode holographic microscope that can image specimens in both transmission and reflection geometries using in-line transmission and off-axis reflection holography, respectively. This field-portable dual-mode holographic microscope has a weight of ~200 g with dimensions of 15 x 5.5 x 5cm, where a laser source is powered by two batteries. Based on digital in-line holography, our transmission microscope achieves a sub-pixel lateral resolution of ≤2 µm over a wide field-of-view (FOV) of ~24 mm2 due to its unit fringe magnification geometry. Despite its simplicity and ease of operation, in-line transmission geometry is not suitable to image dense or connected objects such as tissue slides since the reference beam gets distorted causing severe aberrations in reconstruction of such objects. To mitigate this challenge, on the same cost-effective and field-portable assembly we built a lensless reflection mode microscope based on digital off-axis holography where a beam-splitter is used to interfere a tilted reference wave with the reflected light from the object surface, creating an off-axis hologram of the specimens on a CMOS sensor-chip. As a result of the reduced space-bandwidth product of the off-axis geometry compared to its in-line counterpart, the imaging FOV of our reflection mode is reduced to ~9 mm2, while still achieving a similar sub-pixel resolution of ≤2 µm. We tested the performance of this compact dual-mode microscopy unit by imaging a US-air force resolution test target, various micro-particles as well as a histopathology slide corresponding to skin tissue. Due to its compact, cost-effective, and lightweight design, this dual-mode lensless holographic microscope might especially be useful for field-use or for conducting microscopic analysis in resource-poor settings. PMID:21991559

  3. TREATMENT TECHNIQUES FOR CONTROLLING TRIHALOMETHANES IN DRINKING WATER

    EPA Science Inventory

    In this volume, the authors attempt to bring together information developed over the past 6 years, on all aspects of trihalomethanes as they relate to drinking water. Section I summarizes with references to the primary literature the discovery of the trihalomethane problem, healt...

  4. FORMATION AND CONTROL OF NON-TRIHALOMETHANE BYPRODUCTS

    EPA Science Inventory

    Hundreds of organic byproducts of chlorination are now known to occur in drinking water along with the trihalomethanes. About twenty of these appear to be found with sufficient concentration are now known to occur in drinking water along with the trihalomethanes. bout twenty of t...

  5. Portable thin layer chromatography for field detection of explosives and propellants

    NASA Astrophysics Data System (ADS)

    Satcher, Joe H.; Maienschein, Jon L.; Pagoria, Philip F.; Racoveanu, Ana; Carman, M. Leslie; Whipple, Richard E.; Reynolds, John G.

    2012-06-01

    A field deployable detection kit for explosives and propellants using thin layer chromatography (TLC) has been developed at Lawrence Livermore National Laboratory (LLNL). The chemistry of the kit has been modified to allow for field detection of propellants (through propellant stabilizers), military explosives, peroxide explosives, nitrates and inorganic oxidizer precursors. For many of these target analytes, the detection limit is in the μg to pg range. A new miniaturized, bench prototype, field portable TLC (Micro TLC) kit has also been developed for the detection and identification of common military explosives. It has been demonstrated in a laboratory environment and is ready for field-testing. The kit is comprised of a low cost set of commercially available components specifically assembled for rapid identification needed in the field and identifies the common military explosives: HMX, RDX, Tetryl, Explosive D or picric acid, and TNT all on one plate. Additional modifications of the Micro TLC system have been made with fluorescent organosilicon co-polymer coatings to detect a large suite of explosives.

  6. A semi-automated, field-portable microscopy platform for clinical diagnostic applications

    NASA Astrophysics Data System (ADS)

    Jagannadh, Veerendra Kalyan; Srinivasan, Rajesh; Gorthi, Sai Siva

    2015-08-01

    Clinical microscopy is a versatile diagnostic platform used for diagnosis of a multitude of diseases. In the recent past, many microfluidics based point-of-care diagnostic devices have been developed, which serve as alternatives to microscopy. However, these point-of-care devices are not as multi-functional and versatile as clinical microscopy. With the use of custom designed optics and microfluidics, we have developed a versatile microscopy-based cellular diagnostic platform, which can be used at the point of care. The microscopy platform presented here is capable of detecting infections of very low parasitemia level (in a very small quantity of sample), without the use of any additional computational hardware. Such a cost-effective and portable diagnostic device, would greatly impact the quality of health care available to people living in rural locations of the world. Apart from clinical diagnostics, it's applicability to field research in environmental microbiology has also been outlined.

  7. Metal oxide based multisensor array and portable database for field analysis of antioxidants

    PubMed Central

    Sharpe, Erica; Bradley, Ryan; Frasco, Thalia; Jayathilaka, Dilhani; Marsh, Amanda; Andreescu, Silvana

    2014-01-01

    We report a novel chemical sensing array based on metal oxide nanoparticles as a portable and inexpensive paper-based colorimetric method for polyphenol detection and field characterization of antioxidant containing samples. Multiple metal oxide nanoparticles with various polyphenol binding properties were used as active sensing materials to develop the sensor array and establish a database of polyphenol standards that include epigallocatechin gallate, gallic acid, resveratrol, and Trolox among others. Unique charge-transfer complexes are formed between each polyphenol and each metal oxide on the surface of individual sensors in the array, creating distinct optically detectable signals which have been quantified and logged into a reference database for polyphenol identification. The field-portable Pantone/X-Rite© CapSure® color reader was used to create this database and to facilitate rapid colorimetric analysis. The use of multiple metal-oxide sensors allows for cross-validation of results and increases accuracy of analysis. The database has enabled successful identification and quantification of antioxidant constituents within real botanical extractions including green tea. Formation of charge-transfer complexes is also correlated with antioxidant activity exhibiting electron transfer capabilities of each polyphenol. The antioxidant activity of each sample was calculated and validated against the oxygen radical absorbance capacity (ORAC) assay showing good comparability. The results indicate that this method can be successfully used for a more comprehensive analysis of antioxidant containing samples as compared to conventional methods. This technology can greatly simplify investigations into plant phenolics and make possible the on-site determination of antioxidant composition and activity in remote locations. PMID:24610993

  8. Water-quality monitoring and studies of the formation and fate of trihalomethanes during the third injection, storage and recovery test at Lancaster, Antelope Valley, California, March 1998 through April 1999

    USGS Publications Warehouse

    Fram, Miranda S.; Berghouse, Joshua K.; Bergamaschi, Brian A.; Fujii, Roger; Goodwin, Kelly D.; Clark, Jordan F.

    2002-01-01

    The U.S. Geological Survey, in cooperation with the Los Angeles County Department of Public Works and the Antelope Valley-East Kern Water Agency, conducted three cycles of injection, storage, and recovery tests to evaluate the feasibility of artificially recharging ground water in the Lancaster area of Antelope Valley, California. During the third cycle (March 1998 through April 1999), the tests included investigations of the formation and fate of trihalomethanes in the aquifer. Trihalomethanes are disinfection by-products formed by reaction between natural dissolved organic carbon that is present in water and chlorine that is added during the drinking-water-treatment process. This report includes a discussion of the design of the investigation; descriptions of the sampling, analytical, and experimental methods used in the investigation; and a presentation of the data collected. During the third cycle, 60 million gallons of chlorinated water was injected into the aquifer through well 7N/12W-27P2 in the Los Angeles County Department of Public Works well field in Lancaster between April 15 and June 16, 1998. One hundred fifty million gallons of water was extracted from the same well between June 30, 1998, and April 29, 1999. Water-quality samples were collected during the entire cycle from the well and from a nearby set of nested piezometers, and were analyzed for residual chlorine, dissolved organic carbon, trihalomethane, major anion, and dissolved solid concentrations; ultraviolet absorbance spectra; and a number of field water-quality parameters. A statistical analysis was done to evaluate the analytical precision of the residual chlorine, dissolved organic carbon, trihalomethane, and ultraviolet absorbance measurements on these samples. The formation of trihalomethanes in the injection water was examined in laboratory experiments: Trihalomethane concentrations in samples of injection water were monitored during a storage period, and trihalomethane formation

  9. Least Squares Magnetic-Field Optimization for Portable Nuclear Magnetic Resonance Magnet Design

    SciTech Connect

    Paulsen, Jeffrey L; Franck, John; Demas, Vasiliki; Bouchard, Louis-S.

    2008-03-27

    Single-sided and mobile nuclear magnetic resonance (NMR) sensors have the advantages of portability, low cost, and low power consumption compared to conventional high-field NMR and magnetic resonance imaging (MRI) systems. We present fast, flexible, and easy-to-implement target field algorithms for mobile NMR and MRI magnet design. The optimization finds a global optimum ina cost function that minimizes the error in the target magnetic field in the sense of least squares. When the technique is tested on a ring array of permanent-magnet elements, the solution matches the classical dipole Halbach solution. For a single-sided handheld NMR sensor, the algorithm yields a 640 G field homogeneous to 16 100 ppm across a 1.9 cc volume located 1.5 cm above the top of the magnets and homogeneous to 32 200 ppm over a 7.6 cc volume. This regime is adequate for MRI applications. We demonstrate that the homogeneous region can be continuously moved away from the sensor by rotating magnet rod elements, opening the way for NMR sensors with adjustable"sensitive volumes."

  10. Mapping of a complex lava flow field using regular surveys with a portable thermal camera

    NASA Astrophysics Data System (ADS)

    Calvari, S.; Lodato, L.; Garfi, G.; Spampinato, L.; Andronico, D.

    2003-04-01

    The use of a portable thermal camera has been applied to routine monitoring of the 2002 Etna flank eruption. The eruption started on 27 October with the opening of a field of fissures on the north and south flanks of the volcano. Abundant ash emission from the whole length of the 10 km long fissure covered the lava flow field, making it impossible to approach the active lava even with helicopters. Additionally, the northern lava flows were spreading into a forest, causing fire and impeding routine measures in field and lava flow mapping from the ground. This situation continued for several days. The only way to obtain an approximate mapping of the flow field was to use a thermal camera from helicopter, obtaining inclined images of the lava flow field. This allowed: (1) an estimation of the speed of the spreading lava and (2) of the position of the lava flow fronts, (3) evaluation of effusion rate, (4) daily covered area, and (5) organisation of evacuation plans for people living close to the area affected by flows. All these information were essential for civil protection purposes. Emission of lava flows from the north fissure stopped on 5 November 2002. During the following phase of the eruption, when lava flows spread for over two months only on the southern flank of the volcano, little ash emission from the craters allowed us a better view of the lava flow field. However, since the active flows were spreading on a limited surface, flanking and overlapping each other several times, distinction between active and inactive lava flows was made possible only by using a thermal camera. This device allowed us to distinguish active lava flows, inflating flow fronts, lava tubes and ephemeral vents, giving us a comprehensive view of the evolution of the lava flow field. It also helped us discover new vent opening from the base of the cinder cone, in a way to advice the Civil Protection authorities about the future path of new lava flows.

  11. Design of an ultra-portable field transfer radiometer supporting automated vicarious calibration

    NASA Astrophysics Data System (ADS)

    Anderson, Nikolaus; Thome, Kurtis; Czapla-Myers, Jeffrey; Biggar, Stuart

    2015-09-01

    The University of Arizona Remote Sensing Group (RSG) began outfitting the radiometric calibration test site (RadCaTS) at Railroad Valley Nevada in 2004 for automated vicarious calibration of Earth-observing sensors. RadCaTS was upgraded to use RSG custom 8-band ground viewing radiometers (GVRs) beginning in 2011 and currently four GVRs are deployed providing an average reflectance for the test site. This measurement of ground reflectance is the most critical component of vicarious calibration using the reflectance-based method. In order to ensure the quality of these measurements, RSG has been exploring more efficient and accurate methods of on-site calibration evaluation. This work describes the design of, and initial results from, a small portable transfer radiometer for the purpose of GVR calibration validation on site. Prior to deployment, RSG uses high accuracy laboratory calibration methods in order to provide radiance calibrations with low uncertainties for each GVR. After deployment, a solar radiation based calibration has typically been used. The method is highly dependent on a clear, stable atmosphere, requires at least two people to perform, is time consuming in post processing, and is dependent on several large pieces of equipment. In order to provide more regular and more accurate calibration monitoring, the small portable transfer radiometer is designed for quick, one-person operation and on-site field calibration comparison results. The radiometer is also suited for laboratory calibration use and thus could be used as a transfer radiometer calibration standard for ground viewing radiometers of a RadCalNet site.

  12. ENVIRONMENTAL TECHNOLOGY VERIFICATION REPORT - FIELD PORTABLE X-RAY FLUORESCENCE ANALYZER - METOREX, INC. X-MET 920-P AND 940

    EPA Science Inventory

    In April 1995, the U.S. Environmental Protection Agency (EPA) sponsored a demonstration of field portable X-ray fluorescence (FPXRF) analyzers. The primary objectives of this demonstration were (1) to determine how well FPXRF analyzers perform in comparison to standard reference...

  13. FSR: a field portable spectral reflectometer to measure ground from NIR to LWIR

    NASA Astrophysics Data System (ADS)

    Moreau, Louis; Bourque, Hugo; Ouellet, Réal; Prel, Florent; Roy, Claude; Vallieres, Christian; Thériault, Guillaume

    2011-11-01

    ABB Bomem has recently designed a field-deployable reflectometer. The Full Spectrum Reflectometer (FSR) measures the diffuse reflectance of surfaces in the 0.7 μm to 13.5 μm spectral range. The spectral resolution is adjustable from 32 to 4 cm-1. The instrument is portable, battery-operated and designed for field usage in a single, lightweight and ruggedized package. In its simplest mode, the instrument is automated and can be operated by non-specialist personnel with minimal training. The FSR has a laboratory mode to measure targets brought to the instrument in a sampling cup and a field mode with automated measurement sequence. To facilitate the measurement of various ground surfaces, the instrument is packaged in a three-point mount for easy target access and stability. One of the mount is the sampling port. The instrument has its own built-in NIR and LWIR infrared sources to illuminate the ground area to be measured. The instrument includes two built-in references for calibration: a Spectralon diffuser and an Infragold diffuser. The first units were commissioned to build a spectral database of surfaces in various conditions (humidity, temperature, texture, mixing, etc.) and in the presence of interfering chemicals (oils, solvents, etc.) but the instrument can also serve other purposes such as the identification of unknown materials.

  14. Moving your laboratories to the field--Advantages and limitations of the use of field portable instruments in environmental sample analysis.

    PubMed

    Gałuszka, Agnieszka; Migaszewski, Zdzisław M; Namieśnik, Jacek

    2015-07-01

    The recent rapid progress in technology of field portable instruments has increased their applications in environmental sample analysis. These instruments offer a possibility of cost-effective, non-destructive, real-time, direct, on-site measurements of a wide range of both inorganic and organic analytes in gaseous, liquid and solid samples. Some of them do not require the use of reagents and do not produce any analytical waste. All these features contribute to the greenness of field portable techniques. Several stationary analytical instruments have their portable versions. The most popular ones include: gas chromatographs with different detectors (mass spectrometer (MS), flame ionization detector, photoionization detector), ultraviolet-visible and near-infrared spectrophotometers, X-ray fluorescence spectrometers, ion mobility spectrometers, electronic noses and electronic tongues. The use of portable instruments in environmental sample analysis gives a possibility of on-site screening and a subsequent selection of samples for routine laboratory analyses. They are also very useful in situations that require an emergency response and for process monitoring applications. However, quantification of results is still problematic in many cases. The other disadvantages include: higher detection limits and lower sensitivity than these obtained in laboratory conditions, a strong influence of environmental factors on the instrument performance and a high possibility of sample contamination in the field. This paper reviews recent applications of field portable instruments in environmental sample analysis and discusses their analytical capabilities. PMID:26051907

  15. Modeling trihalomethane formation potential from wastewater chlorination. Master's thesis

    SciTech Connect

    McCormick, C.A.

    1994-09-01

    The deletion of federally mandated fecal coliform limits has led many states to review and modify their wastewater disinfection requirements. One issue in analyzing wastewater disinfection is the discharge of potentially carcinogenic halogenated organics formed during the chlorination process. This research investigates the formation of one class of the halogenated organics, the trihalomethanes. The applicability of using drinking water trihalomethane formation models for use with wastewater effluent is examined. Three models are compared for predictive capability by using measured trihalomethane values from previous research data. The results show that a previously developed model is applicable for use based on assumptions stated. Results provide environmental managers with worst case predictions for a range of wastewater treatment plant (WWTP) parameters. Predictions indicate that trihalomethane formation from the chlorination of wastewater is typically lower than the Safe Drinking Water Act trihalomethane standard of 100 ug/L. The worst case model predictions reach, and in certain extreme cases, pass the standard of 100 ug/L. This level of trihalomethanes formed is minimized if aeration of the receiving bodies of water occurs. Based on this research, the risk of forming trihalomethanes as disinfection by-products from chlorination do not outweigh the benefits gained from proper chlorine disinfection of effluent.

  16. Portable Infrared Reflectometer Designed and Manufactured for Evaluating Emittance in the Laboratory or in the Field

    NASA Technical Reports Server (NTRS)

    Jaworske, Donald A.

    2000-01-01

    The optical properties of materials play a key role in spacecraft thermal control. In space, radiant heat transfer is the only mode of heat transfer that can reject heat from a spacecraft. One of the key properties for defining radiant heat transfer is emittance, a measure of how efficiently a surface can reject heat in comparison to a perfect black body emitter. Heat rejection occurs in the infrared region of the spectrum, nominally in the range of 2 to 25 mm. To calculate emittance, one obtains the reflectance over this spectral range, calculates spectral absorptance by difference, and then uses Kirchhoff s Law and the Stefan-Boltzmann equation to calculate emittance. A new portable infrared reflectometer, the SOC 400t, was designed and manufactured to evaluate the emittance of surfaces and coatings in the laboratory or in the field. It was developed by Surface Optics Corporation under a contract with the NASA Glenn Research Center at Lewis Field to replace the Center s aging Gier-Dunkle DB-100 infrared reflectometer. The specifications for the new instrument include a wavelength range of 2 to 25 mm; reflectance repeatability of +/-1 percent; self-calibrating, near-normal spectral reflectance measurements; a full scan measurement time of 3.5 min, a sample size of 1.27 cm (0.5 in.); a spectral resolution selectable from 4, 8, 16, or 32/cm; and optical property characterization utilizing an automatic integration to calculate total emittance in a selectable temperature range.

  17. Portable low-coherence interferometry for quantitatively imaging fast dynamics with extended field of view

    NASA Astrophysics Data System (ADS)

    Shaked, Natan T.; Girshovitz, Pinhas; Frenklach, Irena

    2014-06-01

    We present our recent advances in the development of compact, highly portable and inexpensive wide-field interferometric modules. By a smart design of the interferometric system, including the usage of low-coherence illumination sources and common-path off-axis geometry of the interferometers, spatial and temporal noise levels of the resulting quantitative thickness profile can be sub-nanometric, while processing the phase profile in real time. In addition, due to novel experimentally-implemented multiplexing methods, we can capture low-coherence off-axis interferograms with significantly extended field of view and in faster acquisition rates. Using these techniques, we quantitatively imaged rapid dynamics of live biological cells including sperm cells and unicellular microorganisms. Then, we demonstrated dynamic profiling during lithography processes of microscopic elements, with thicknesses that may vary from several nanometers to hundreds of microns. Finally, we present new algorithms for fast reconstruction (including digital phase unwrapping) of off-axis interferograms, which allow real-time processing in more than video rate on regular single-core computers.

  18. Supporting the joint warfighter by development, training, and fielding of man-portable UGVs

    NASA Astrophysics Data System (ADS)

    Ebert, Kenneth A.; Stratton, Benjamin V.

    2005-05-01

    The Robotic Systems Pool (RSP), sponsored by the Joint Robotics Program (JRP), is an inventory of small robotic systems, payloads, and components intended to expedite the development and integration of technology into effective, supportable, fielded robotic assets. The RSP loans systems to multiple users including the military, first-responders, research organizations, and academia. These users provide feedback in their specific domain, accelerating research and development improvements of robotic systems, which in turn allow the joint warfighter to benefit from such changes more quickly than from traditional acquisition cycles. Over the past year, RSP assets have been used extensively for pre-deployment operator and field training of joint Explosive Ordnance Disposal (EOD) teams, and for the training of Navy Reservist repair technicians. These Reservists are part of the Robotic Systems Combat Support Platoon (RSCSP), attached to Space and Naval Warfare Systems Center, San Diego. The RSCSP maintains and repairs RSP assets and provides deployable technical support for users of robotic systems. Currently, a small team from the RSCSP is deployed at Camp Victory repairing and maintaining man-portable unmanned ground vehicles (UGVs) used by joint EOD teams in Operation Iraqi Freedom. The focus of this paper is to elaborate on the RSP and RSCSP and their role as invaluable resources for spiral development in the robotics community by gaining first-hand technical feedback from the warfighter and other users.

  19. Miniaturized Explosive Preconcentrator for Use in a Man-Portable Field Detection System

    SciTech Connect

    Hannum, David W.; Linker, Kevin L.; Parmeter, John E.; Rhykerd, Charles L.; Varley, Nathan R.

    1999-08-02

    We discuss the design and testing of a miniaturized explosives preconcentrator that can be used to enhance the capabilities of man-portable field detection systems, such as those based on ion mobility spectrometry (IMS). The preconcentrator is a smaller version of a similar device that was developed recently at Sandia National Laboratories for use in a trace detection portal that screens personnel for explosives. Like its predecessor, this preconcentrator is basically a filtering device that allows a small amount of explosive residue in a large incoming airflow to be concentrated into a much smaller air volume via adsorption and resorption, prior to delivery into a chemical detector. We discuss laboratory testing of this preconcentrator interfaced to a commercially available IMS-based detection system, with emphasis on the explosives 2,4,6-trinitrotoluene (TNT) and cyclotrimethylenetrinitramine (RDX). The issues investigated include optimization of the preconcentrator volume and inlet airflow, the use of different types of adsorbing surfaces within the preconcentrator, Wd preconcentrator efficiency and concentration factor. We discuss potential field applications of the preconcentrator, as well as avenues for further investigations and improvements.

  20. Design Considerations for a Portable Raman Probe Spectrometer for Field Forensics

    SciTech Connect

    Kelly, James F.; Blake, Thomas A.; Bernacki, Bruce E.; Johnson, Timothy J.

    2012-01-01

    Raman spectroscopy has been shown to be a viable method for explosives detection. Currently most forensic Raman systems are either large, powerful instruments for laboratory experiments or handheld instruments forin situpoint detection. We have chosen to examine the performance of certain benchtop Raman probe systems with the goal of developing an inexpensive, portable system that could be used to operate in a field forensics laboratory to examine explosives-related residues or samples. To this end, a rugged, low distortion line imaging dispersive Raman spectrograph was configured to work at 830 nm laser excitation and was used to determine whether the composition of thin films of plastic explosives or small (e.g., ≤10 μm) particles of RDX or other explosives or oxidizers can be detected, identified, and quantified in the field. With 300 mW excitation energy, concentrations of RDX and PETN can be detected and reconstructed in the case of thin Semtex smears, but further work is needed to push detection limits of areal dosages to the ~1 μg/cm2level. We describe the performance of several probe/spectrograph combinations and show preliminary data for particle detection, calibration and detection linearity for mixed compounds, and so forth.

  1. Analysis of munitions constituents in groundwater using a field-portable GC-MS.

    PubMed

    Bednar, A J; Russell, A L; Hayes, C A; Jones, W T; Tackett, P; Splichal, D E; Georgian, T; Parker, L V; Kirgan, R A; MacMillan, D K

    2012-05-01

    The use of munitions constituents (MCs) at military installations can produce soil and groundwater contamination that requires periodic monitoring even after training or manufacturing activities have ceased. Traditional groundwater monitoring methods require large volumes of aqueous samples (e.g., 2-4 L) to be shipped under chain of custody, to fixed laboratories for analysis. The samples must also be packed on ice and shielded from light to minimize degradation that may occur during transport and storage. The laboratory's turn-around time for sample analysis and reporting can be as long as 45 d. This process hinders the reporting of data to customers in a timely manner; yields data that are not necessarily representative of current site conditions owing to the lag time between sample collection and reporting; and incurs significant shipping costs for samples. The current work compares a field portable Gas Chromatograph-Mass Spectrometer (GC-MS) for analysis of MCs on-site with traditional laboratory-based analysis using High Performance Liquid Chromatography with UV absorption detection. The field method provides near real-time (within ~1 h of sampling) concentrations of MCs in groundwater samples. Mass spectrometry provides reliable confirmation of MCs and a means to identify unknown compounds that are potential false positives for methods with UV and other non-selective detectors. PMID:22349064

  2. Detection of waterborne parasites using field-portable and cost-effective lensfree microscopy†

    PubMed Central

    Mudanyali, Onur; Oztoprak, Cetin; Tseng, Derek; Erlinger, Anthony; Ozcan, Aydogan

    2010-01-01

    Protection of human health and well-being through water quality management is an important goal for both the developed and the developing parts of the world. In the meantime, insufficient disinfection techniques still fail to eliminate pathogenic contaminants in freshwater as well as recreational water resources. Therefore, there is a significant need for screening of water quality to prevent waterborne outbreaks and incidents of water-related diseases. Toward this end, here we investigate the use of a field-portable and cost-effective lensfree holographic microscope to image and detect pathogenic protozoan parasites such as Giardia Lamblia and Cryptosporidium Parvum at low concentration levels. This compact lensless microscope (O. Mudanyali et al., Lab Chip, 2010, 10, 1417–1428), weighing ~46 grams, achieves a numerical aperture of ~0.1–0.2 over an imaging field of view that is more than an order of magnitude larger than a typical 10X objective lens, and therefore may provide an important high-throughput analysis tool for combating waterborne diseases especially in resource limited settings. PMID:20694255

  3. Quantitative assessment of historical coastal landfill contamination using in-situ field portable XRF (FPXRF)

    NASA Astrophysics Data System (ADS)

    O'Shea, Francis; Spencer, Kate; Brasington, James

    2014-05-01

    Historically, waste was deposited on low value, easily accessible coastal land (e.g. marsh land). Within England and Wales alone, there are over 5000 historical landfills situated within coastal areas at risk of flooding at a 1 in 100 year return period (Environment Agency, 2012). Historical sites were constructed prior to relevant legislation, and have no basal or side wall engineering, and the waste constituents are mostly unknown. In theory, contaminant concentrations should be reduced through natural attenuation as the leachate plume migrates through surrounding fine-grained inter-tidal sediments before reaching receptor waters. However, erosion resulting from rising sea level and increased storm intensity may re-distribute these sediments and release associated contaminants into the estuarine and coastal environment. The diffuse discharge from these sites has not been quantified and this presents a problem for those landfill managers who are required to complete EIAs. An earlier detailed field campaign at Newlands landfill site, on the Thames Estuary, UK identified a sub-surface (~2m depth) contaminant plume extending c. 20 m from the landfill boundary into surrounding fine-grained saltmarsh sediments. These saltmarsh sediments are risk of being eroded releasing their contaminant load to the Thames Estuary. The aims of this work were to; 1) assess whether this plume is representative of other historical landfills with similar characteristics and 2) to develop a rapid screening methodology using field portable XRF that could be used to identify potential risk of other coastal landfill sites. GIS was used to select landfill sites of similar age, hydrological regime and sedimentary setting in the UK, for comparison. Collection of sediment samples and analysis by ICP OES is expensive and time-consuming, therefore cores were extracted and analysed with a Niton Goldd XRF in-situ. Contaminant data were available immediately and the sampling strategy could be adapted

  4. Field portable mobile phone based fluorescence microscopy for detection of Giardia lamblia cysts in water samples

    NASA Astrophysics Data System (ADS)

    Ceylan Koydemir, Hatice; Gorocs, Zoltan; McLeod, Euan; Tseng, Derek; Ozcan, Aydogan

    2015-03-01

    Giardia lamblia is a waterborne parasite that causes an intestinal infection, known as giardiasis, and it is found not only in countries with inadequate sanitation and unsafe water but also streams and lakes of developed countries. Simple, sensitive, and rapid detection of this pathogen is important for monitoring of drinking water. Here we present a cost-effective and field portable mobile-phone based fluorescence microscopy platform designed for automated detection of Giardia lamblia cysts in large volume water samples (i.e., 10 ml) to be used in low-resource field settings. This fluorescence microscope is integrated with a disposable water-sampling cassette, which is based on a flow-through porous polycarbonate membrane and provides a wide surface area for fluorescence imaging and enumeration of the captured Giardia cysts on the membrane. Water sample of interest, containing fluorescently labeled Giardia cysts, is introduced into the absorbent pads that are in contact with the membrane in the cassette by capillary action, which eliminates the need for electrically driven flow for sample processing. Our fluorescence microscope weighs ~170 grams in total and has all the components of a regular microscope, capable of detecting individual fluorescently labeled cysts under light-emitting-diode (LED) based excitation. Including all the sample preparation, labeling and imaging steps, the entire measurement takes less than one hour for a sample volume of 10 ml. This mobile phone based compact and cost-effective fluorescent imaging platform together with its machine learning based cyst counting interface is easy to use and can even work in resource limited and field settings for spatio-temporal monitoring of water quality.

  5. Field analyses of (238)U and (226)Ra in two uranium mill tailings piles from Niger using portable HPGe detector.

    PubMed

    Déjeant, Adrien; Bourva, Ludovic; Sia, Radia; Galoisy, Laurence; Calas, Georges; Phrommavanh, Vannapha; Descostes, Michael

    2014-11-01

    The radioactivities of (238)U and (226)Ra in mill tailings from the U mines of COMINAK and SOMAÏR in Niger were measured and quantified using a portable High-Purity Germanium (HPGe) detector. The (238)U and (226)Ra activities were measured under field conditions on drilling cores with 600s measurements and without any sample preparation. Field results were compared with those obtained by Inductive Coupled Plasma Atomic Emission Spectroscopy (ICP-AES) and emanometry techniques. This comparison indicates that gamma-ray absorption by such geological samples does not cause significant deviations. This work shows the feasibility of using portable HPGe detector in the field as a preliminary method to observe variations of radionuclides concentration with the aim of identifying samples of interest. The HPGe is particularly useful for samples with strong secular disequilibrium such as mill tailings. PMID:25036918

  6. Field-Portable Immunoassay Instruments and Reagents to Measure Chelators and Mobile Forms of Uranium

    SciTech Connect

    Blake, Diane A.

    2006-01-23

    Progress Report Date: 01/23/06 (report delayed due to Hurricane Katrina) Report of results to date: The goals of this 3-year project are to: (1) update and successfully deploy our present immunosensors at DOE sites; (2) devise immunosensor-based assays for Pb(II), Hg(II), chelators, and/or Cr(III) in surface and groundwater; and (3) develop new technologies in antibody engineering that will enhance this immunosensor program. Note: Work on this project was temporarily disrupted when Hurricane Katrina shut down the University on August 29, 2005. While most of the reagents stored in our refrigerators and freezers were destroyed, all of our hybridoma cell lines were saved because they had been stored in liquid nitrogen. We set up new tissue culture reactors with the hybridomas that synthesize the anti-uranium antibodies, and are purifying new monoclonal antibodies from these culture supernatants. Both the in-line and the field-portable sensor were rescued from our labs in New Orleans in early October, and we continued experiments with these sensors in the temporary laboratory we set up in Hammond, LA at Southeastern Louisiana University.

  7. Nanofocus of tenth of joules and a portable plasma focus of few joules for field applications

    SciTech Connect

    Soto, Leopoldo; Pavez, Cristian; Moreno, Jose; Tarifeno, Ariel; Pedreros, Jose; Altamirano, Luis

    2009-01-21

    A repetitive pinch plasma focus that works with stored energy less than 1 J per shot has be developed at the Chilean Nuclear Energy Commission. The main features of this device, repetitive Nanofocus, are 5 nF of capacity, 5 nH of inductance, 5-10 kV charging voltage, 60-250 mJ stored energy, 5-10 kA current peak, per shot. The device has been operated at 20 Hz in hydrogen and deuterium. X-ray radiographs of materials of different thickness were obtained. Neutrons were detected using a system based upon {sup 3}He proportional counter in chare integrated mode. However, the reproducibility of this miniaturized device is low and several technological subjects have to be previously solved in order to produce neutrons for periods greater than minutes. Further studies in the Nanofocus are being carried out. In addition, a device with a stored energy of a few joules is being explored. A preliminary compact, low weight (3 kg), portable PF device (25 cmx5 cmx5 cm) for field applications has been designed. This device was designed to operate with few kilovolts (10 kV or less) with a stored energy of 2 J and a repetition rate of 10 Hz without cooling. A neutron flux of the order of 10{sup 4}-10{sup 5} n/s is expected.

  8. Field assessment of noncontact stream gauging using portable surface velocity radars (SVR)

    NASA Astrophysics Data System (ADS)

    Welber, Matilde; Le Coz, Jérôme; Laronne, Jonathan B.; Zolezzi, Guido; Zamler, Daniel; Dramais, Guillaume; Hauet, Alexandre; Salvaro, Martino

    2016-02-01

    The applicability of a portable, commercially available surface velocity radar (SVR) for noncontact stream gauging was evaluated through a series of field-scale experiments carried out in a variety of sites and deployment conditions. Comparisons with various concurrent techniques showed acceptable agreement with velocity profiles, with larger uncertainties close to the banks. In addition to discharge error sources shared with intrusive velocity-area techniques, SVR discharge estimates are affected by flood-induced changes in the bed profile and by the selection of a depth-averaged to surface velocity ratio, or velocity coefficient (α). Cross-sectional averaged velocity coefficients showed smaller fluctuations and closer agreement with theoretical values than those computed on individual verticals, especially in channels with high relative roughness. Our findings confirm that α = 0.85 is a valid default value, with a preferred site-specific calibration to avoid underestimation of discharge in very smooth channels (relative roughness ˜ 0.001) and overestimation in very rough channels (relative roughness > 0.05). Theoretically derived and site-calibrated values of α also give accurate SVR-based discharge estimates (within 10%) for low and intermediate roughness flows (relative roughness 0.001 to 0.05). Moreover, discharge uncertainty does not exceed 10% even for a limited number of SVR positions along the cross section (particularly advantageous to gauge unsteady flood flows and very large floods), thereby extending the range of validity of rating curves.

  9. Portable oral cancer detection using a miniature confocal imaging probe with a large field of view

    NASA Astrophysics Data System (ADS)

    Wang, Youmin; Raj, Milan; McGuff, H. Stan; Bhave, Gauri; Yang, Bin; Shen, Ting; Zhang, Xiaojing

    2012-06-01

    We demonstrate a MEMS micromirror enabled handheld confocal imaging probe for portable oral cancer detection, where a comparatively large field of view (FOV) was generated through the programmable Lissajous scanning pattern of the MEMS micromirror. Miniaturized handheld MEMS confocal imaging probe was developed, and further compared with the desktop confocal prototype under clinical setting. For the handheld confocal imaging system, optical design simulations using CODE VR® shows the lateral and axial resolution to be 0.98 µm and 4.2 µm, where experimental values were determined to be 3 µm and 5.8 µm, respectively, with a FOV of 280 µm×300 µm. Fast Lissajous imaging speed up to 2 fps was realized with improved Labview and Java based real-time imaging software. Properties such as 3D imaging through autofocusing and mosaic imaging for extended lateral view (6 mm × 8 mm) were examined for carcinoma real-time pathology. Neoplastic lesion tissues of giant cell fibroma and peripheral ossifying fibroma, the fibroma inside the paraffin box and ex vivo gross tissues were imaged by the bench-top and handheld imaging modalities, and further compared with commercial microscope imaging results. The MEMS scanner-based handheld confocal imaging probe shows great promise as a potential clinical tool for oral cancer diagnosis and treatment.

  10. Operational field evaluation of the PAC-MAG man-portable magnetometer array

    NASA Astrophysics Data System (ADS)

    Keranen, Joe; Topolosky, Zeke; Schultz, Gregory; Miller, Jonathan

    2013-06-01

    Detection and discrimination of unexploded ordnance (UXO) in areas of prior conflict is of high importance to the international community and the United States government. For humanitarian applications, sensors and processing methods need to be robust, reliable, and easy to train and implement using indigenous UXO removal personnel. This paper describes system characterization, system testing, and a continental United States (CONUS) Operational Field Evaluations (OFE) of the PAC-MAG man-portable UXO detection system. System testing occurred at a government test facility in June, 2010 and December, 2011 and the OFE occurred at the same location in June, 2012. NVESD and White River Technologies personnel were present for all testing and evaluation. The PAC-MAG system is a manportable magnetometer array for the detection and characterization of ferrous UXO. System hardware includes four Cesium vapor magnetometers for detection, a Real-time Kinematic Global Position System (RTK-GPS) for sensor positioning, an electronics module for merging array data and WiFi communications and a tablet computer for transmitting and logging data. An odometer, or "hipchain" encoder, provides position information in GPS-denied areas. System software elements include data logging software and post-processing software for detection and characterization of ferrous anomalies. The output of the post-processing software is a dig list containing locations of potential UXO(s), formatted for import into the system GPS equipment for reacquisition of anomalies. Results from system characterization and the OFE will be described.

  11. Advances in field-portable ion trap GC/MS instrumentation

    NASA Astrophysics Data System (ADS)

    Diken, Eric G.; Arno, Josep; Skvorc, Ed; Manning, David; Andersson, Greger; Judge, Kevin; Fredeen, Ken; Sadowski, Charles; Oliphant, Joseph L.; Lammert, Stephen A.; Jones, Jeffrey L.; Waite, Randall W.; Grant, Chad; Lee, Edgar D.

    2012-06-01

    The rapid and accurate detection and identification of chemical warfare agents and toxic industrial chemicals can be critical to the protection of military and civilian personnel. The use of gas chromatography (GC) - mass spectrometry (MS) can provide both the sensitivity and selectivity required to identify unknown chemicals in complex (i.e. real-world) environments. While most widely used as a laboratory-based technique, recent advances in GC, MS, and sampling technologies have led to the development of a hand-portable GC/MS system that is more practical for field-based analyses. The unique toroidal ion trap mass spectrometer (TMS) used in this instrument has multiple benefits related to size, weight, start-up time, ruggedness, and power consumption. Sample separation is achieved in record time (~ 3 minutes) and with high resolution using a state-of-the-art high-performance low-thermal-mass GC column. In addition to providing a system overview highlighting its most important features, the presentation will focus on the chromatographic and mass spectral performance of the system. Results from exhaustive performance testing of the new instrument will be introduced to validate its unique robustness and ability to identify targeted and unknown chemicals.

  12. Man-portable command, communication, and control systems for the next generation of unmanned field systems

    NASA Astrophysics Data System (ADS)

    Jacobus, Charles J.; Mitchell, Brian T.; Jacobus, Heidi N.; Watts, Russell C.; Taylor, Mark J.; Salazar, Alfonso

    1993-05-01

    New generations of military unmanned systems on the ground, at sea, and in the air will be driven by man-portable command units. In past efforts we implemented several prototypes of such units which provided display and capture of up to four video input channels, provided 4 color LCD screens and a larger status display LCD screen, provided drive input through two joysticks, and, through software, supported a flexible 'virtual' driver's interface. We have also performed additional trade analysis of prototype systems incorporating force feedback and extensive image-oriented processing facilities applied to man-controlled robotic control systems. This prior work has resulted in a database of practical design guidelines and a new generation of hardened compact robotic command center which is being designed and built to provide more advanced video capture, display, and interfacing features, supercomputer level computational performance, and ergonomic features for hard field use. In this paper we will summarize some past work and will project current performance to features likely to be common across most unmanned systems command, control, and communications subsystems of the near future.

  13. APPLICATION OF PORTABLE MICROPROCESSOR-BASED SYSTEM FOR ELECTROPHYSIOLOGICAL FIELD TESTING OF NEUROTOXICITY

    EPA Science Inventory

    A portable microprocessor-based system designated PEARL II has been developed for neurotoxicity testing in human populations. PEARL II provides a flexible and powerful data acquisition capability to record sensory evoked potentials (auditory, visual and somotosensory), event-rela...

  14. REMOVING TRIHALOMETHANES FROM DRINKING WATER - AN OVERVIEW OF TREATMENT TECHNIQUES

    EPA Science Inventory

    In 1974 trihalomethanes (chloroform, bromodichloromethane, dibromochloromethane, and bromoform) were discovered to be formed during the disinfection step of drinking water if free chlorine was the disinfectant. This, coupled with the perceived hazard to the consumer's health, led...

  15. Dissolved organic carbon concentrations and compositions, and trihalomethane formation potentials in waters from agricultural peat soils, Sacramento-San Joaquin Delta, California; implications for drinking-water quality

    USGS Publications Warehouse

    Fujii, Roger; Ranalli, Anthony J.; Aiken, George R.; Bergamaschi, Brian A.

    1998-01-01

    Water exported from the Sacramento-San Joaquin River delta (Delta) is an important drinking-water source for more than 20 million people in California. At times, this water contains elevated concentrations of dissolved organic carbon and bromide, and exceeds the U.S. Environmental Protection Agency's maximum contaminant level for trihalomethanes of 0.100 milligrams per liter if chlorinated for drinking water. About 20 to 50 percent of the trihalomethane precursors to Delta waters originates from drainage water from peat soils on Delta islands. This report elucidates some of the factors and processes controlling and affecting the concentration and quality of dissolved organic carbon released from peat soils and relates the propensity of dissolved organic carbon to form trihalomethanes to its chemical composition.Soil water was sampled from near-surface, oxidized, well-decomposed peat soil (upper soil zone) and deeper, reduced, fibrous peat soil (lower soil zone) from one agricultural field in the west central Delta over 1 year. Concentrations of dissolved organic carbon in the upper soil zone were highly variable, with median concentrations ranging from 46.4 to 83.2 milligrams per liter. Concentrations of dissolved organic carbon in samples from the lower soil zone were much less variable and generally slightly higher than samples from the upper soil zone, with median concentrations ranging from 49.3 to 82.3 milligrams per liter. The dissolved organic carbon from the lower soil zone had significantly higher aromaticity (as measured by specific ultraviolet absorbance) and contained significantly greater amounts of aromatic humic substances (as measured by XAD resin fractionation and carbon-13 nuclear magnetic resonance analysis of XAD isolates) than the dissolved organic carbon from the upper soil zone. These results support the conclusion that more aromatic forms of dissolved organic carbon are produced under anaerobic conditions compared to aerobic conditions

  16. Analysis of the elemental composition of marine litter by field-portable-XRF.

    PubMed

    Turner, Andrew; Solman, Kevin R

    2016-10-01

    Marine litter represents a pervasive environmental problem that poses direct threats to wildlife and habitats. Indirectly, litter can also act as a vehicle for the exposure and bioaccumulation of chemicals that are associated with manufactured or processed solids. In this study, we describe the use of a Niton field-portable-x-ray fluorescence (FP-XRF) spectrometer to determine the content of 17 elements in beached plastics, foams, ropes and painted items. The instrument was used in a 'plastics' mode configured for complex, low density materials, and employed a thickness correction algorithm to account for varying sample depth. Accuracy was evaluated by analysing two reference polyethylene discs and was better than 15% for all elements that had been artificially impregnated into the polymer. Regarding the litter samples, limits of detection for a 120s counting time varied between the different material categories and among the elements but were generally lowest for plastics and painted items with median concentrations of less than 10μgg(-1) for As, Bi, Br, Cr, Hg, Ni, Pb, Se and Zn. Concentrations returned by the XRF were highly sensitive to the thickness correction applied for certain elements (Ba, Cl, Cr, Cu, Fe, Sb, Ti, Zn) in all matrices tested, indicating that accurate measurement and application of the correct thickness is critical for acquiring reliable results. An independent measure of the elemental content of selected samples by ICP spectrometry following acid digestion returned concentrations that were significantly correlated with those returned by the XRF, and with an overall slope of [XRF]/[ICP]=0.85. Within the FP-XRF operating conditions, Cl, Cr, Fe, Ti and Zn were detected in more than 50% and Hg and Se in less than 1% of the 376 litter samples analysed. Significant from an environmental perspective were concentrations of the hazardous elements, Cd, Br and Pb, that exceeded several thousand μgg(-1) in many cases. PMID:27474307

  17. Modern, PC based, high resolution portable EDXRF analyzer offers laboratory performance for field, in-situ analysis of environmental contaminants

    NASA Astrophysics Data System (ADS)

    Piorek, Stanislaw

    1994-12-01

    The introduction of a new, high resolution, portable probe that has improved the sensitivity of the conventional field portable X-ray fluorescence (FPXRF) by up to an order of magnitude had been reported earlier [S. Piorek and J.R. Pasmore, Proc. 2nd Int. Symp. on Field Screening Methods for Hazardous Wastes and Toxic Chemicals, Las Vegas, 1991, p. 737]. A high resolution Si(Li) detector probe operates connected to a multichannel X-ray analyzer (2048 channels) which is housed in a portable, battery powered industrial computer. An improved energy resolution of the detector allows the implementation of more sophisticated data treatment methods to convert the measured intensities into mass concentrations of the analytes. A backscatter with a fundamental parameters approach (BFP) is one of the best methods, specifically for metallic contaminants in soil. A program has been written based on the BFP method for use with the new probe. The new software/probe combination enables one to quickly assess levels of contaminants on the site without the need of analyzed samples for instrument calibration. The performance of the EDXRF system in application to analysis of metals in contaminated soil is discussed in this paper. Also discussed is the extension of this method in the analysis of other types of environmental samples such as air particulates collected on filter paper.

  18. Programmable shunt valves: in vitro assessment of safety of the magnetic field generated by a portable game machine.

    PubMed

    Nakashima, Koji; Nakajo, Takato; Kawamo, Michiari; Kato, Akihito; Ishigaki, Seiichiro; Murakami, Hidetomo; Imaizumi, Yohichi; Izumiyama, Hitoshi

    2011-01-01

    Cerebrospinal fluid (CSF) shunts are frequently used to treat hydrocephalus. The use of a programmable shunt valve allows physicians to easily change the opening pressure. Since patients with adjustable CSF shunt valves may use portable game machines, the permanent magnets in these machines may alter the shunt valve programmed settings or permanently damage the device. This study investigated the risk of unintentional valve adjustment associated with the use of game machines in patients with programmable CSF shunt valves. Four adjustable valves from 4 different manufacturers, Sophysa Polaris model SPV (Polaris valve), Miethke proGAV (proGAV), Codman Hakim programmable valve (CHPV), and Strata II small valve (Strata valve), were evaluated. Magnetic field interactions were determined using the portable game machine, Nintendo DS Lite (DS). The maximum distance between the valve and the DS that affected the valve pressure setting was measured by x-ray cinematography. The Polaris valve and proGAV were immune to unintentional reprogramming by the DS. However, the settings of the CHPV and Strata valves were randomly altered by the DS. Patients with an implanted shunt valve should be made aware of the risks posed by the magnetic fields associated with portable game machines and commonly used home electronics. PMID:21946726

  19. Modeling the formation of trihalomethanes in drinking waters of Lebanon.

    PubMed

    Semerjian, Lucy; Dennis, John; Ayoub, George

    2009-02-01

    The current research aims at developing predictive models for trihalomethane (THM) formation in Lebanon based on field-scale investigations as well as laboratory controlled experimentations. Statistical analysis on field data revealed significant correlations for TTHM with chlorine dose, Specific UV-A, and UV(254) absorbing organics. Simulated distribution system-THM tests showed significant correlations with applied chlorine dose, total organic carbon, bromides, contact time, and temperature. Predictive models, formulated using multiple regression approaches, exhibiting the highest coefficients of determination were quadratic for the directly after chlorination (DAC; r(2) = 0.39, p < 0.036) and network (r(2) = 0.33, p < 0.064) THM databases, and logarithmic for the laboratory simulated THM database (r(2) = 0.70, p < 0.001). Computed r(2) values implied low correlations for the DAC and network THM database, and high correlation for the laboratory simulated THM database. Significance of the models were at the 0.05 level for DAC database, 0.10 level for the network database, and very high (<0.01 level) for the laboratory simulated THM database. It is noteworthy to mention that no previous attempts to assess, monitor, and predict THM concentrations in public drinking water have been reported for the country although a large fraction of the population consumes chlorinated public drinking water. PMID:18253848

  20. Field portable XRF as a tool for the assessment of contaminated peat soils

    NASA Astrophysics Data System (ADS)

    Shuttleworth, Emma; Evans, Martin; Rothwell, James; Hutchinson, Simon

    2013-04-01

    Upland blanket bogs in the UK have suffered severe erosion over the last millennium but there is evidence to show that this has increased in intensity in the last 250 years, coinciding with increased pressures on the land during the British Industrial Revolution. Upland peat soils in close proximity to urban and industrial areas can be contaminated with - and act as sinks for - high concentrations of atmospherically deposited lead. Atmospheric pollution has been shown to have had significant effects on blanket bog vegetation, the damage and removal of which makes the peat mass highly susceptible to erosion. Erosion of these soils has the potential to release lead into the fluvial system. Detailed quantification of lead concentrations across the surface of actively eroding peatlands is vital in order to understand lead storage and release in such environments. Previous attempts to quantify peatland lead pollution have been undertaken using the inventory approach. However, there can be significant within-site spatial heterogeneity in lead concentrations, highlighting the need for multiple samples to properly quantify lead storage. Lead concentrations in peat are traditionally derived through acid extraction followed by ICP-OES or AAS analyses, but these can be time consuming, expensive and destructive. By contrast, field portable x-ray fluorescence (FPXRF) analysers are relatively inexpensive, allow a large number of samples to be processed in a comparatively short time, giving a high level of detail with little disturbance to the surrounding area. FPXRF continues to gain acceptance in the study of metal contaminated soil but has not been used to conduct field surveys of contaminated peat soils due to their high moisture content. This study compares lead concentration data obtained in situ using a handheld Niton XL3t 900 XRF analyser with data derived from ex situ lab based analyses. In situ measurements were acquired across degraded and intact peatland sites in the

  1. Measurement capability of field portable organic vapor monitoring instruments under different experimental conditions.

    PubMed

    Coffey, Christopher C; Pearce, Terri A; Lawrence, Robert B; Hudnall, Judith B; Slaven, James E; Martin, Stephen B

    2009-01-01

    The performance of field portable direct-reading organic vapor monitors (DROVMs) was evaluated under a variety of experimental conditions. Four of the DROVMs had photoionization detectors (ppbRAE, IAQRAE, MultiRAE, and Century Toxic Vapor Analyzer), one had a flame ionization detector (Century Toxic Vapor Analyzer), and one was a single-beam infrared spectrophotometer (SapphIRe). Four of each DROVM (two Century Toxic Vapor Analyzers and SapphIRes) were tested. The DROVMs were evaluated at three temperatures (4 degrees C, 21 degrees C, and 38 degrees C), three relative humidities (30%, 60%, and 90%), and two hexane concentrations (5 ppm and 100 ppm). These conditions were selected to provide a range within the operational parameters of all the instruments. At least four replicate trials were performed across the 18 experimental conditions (3 temperatures x 3 relative humidities x 2 concentrations). To evaluate performance, the 4-hr time-weighted average readings from the DROVMs in a given trial were compared with the average of two charcoal tube concentrations using pairwise comparison. The pairwise comparison criterion was +/-25% measurement agreement between each individual DROVM and the DROVMs as a group and the average charcoal tube concentration. The ppbRAE group performed the best with 40% of all readings meeting the comparison criterion followed by the SapphIRe group at 39%. Among individual DROVMs, the best performer was a SapphIRe, with 57% of its readings meeting the criterion. The data was further analyzed by temperature, humidity, and concentration. The results indicated the performance of some DROVMs may be affected by temperature, humidity, and/or concentration. The ppbRAE group performed best at 21 degrees C with the percentage of readings meeting the criterion increasing to 63%. At the 5 ppm concentration, 44% of the ppbRAE group readings met the criterion, while at 100 ppm, only 35% did. The results indicate that monitors can be used as survey tools

  2. Ultrasonic extraction and field-portable anodic stripping voltammetry for the determination of lead in workplace air samples.

    PubMed

    Ashley, K; Mapp, K J; Millson, M

    1998-10-01

    An on-site, field-portable analytical method for the determination of lead in workplace air samples, based on the use of ultrasonic extraction and anodic stripping voltammetry (ASV), was evaluated. Workplace air samples were obtained using a standard method involving particulate collection onto mixed cellulose ester membrane filters. Samples were collected at work sites where airborne particulates were generated from the abrasive blasting of lead-containing paint on highway bridges. Ultrasonic extraction (UE) of air filter samples in diluted nitric acid, followed by portable ASV, was used for the determination of lead. Also, performance evaluation samples consisting of reference materials of known lead concentration were subjected to the UE-ASV procedure for lead determination. Confirmatory analyses of the air filters and performance evaluation samples subjected to the UE-ASV lead measurement method were conducted by hotplate digestion in concentrated nitric acid and 30% hydrogen peroxide, followed by inductively coupled plasma-atomic emission spectrometric (ICP-AES) determination of lead. Recoveries of lead from performance evaluation materials (when using the UE-ASV method) were found to be quantitative. The performance of the UE-ASV method for lead in air filters was found to be acceptable, as evaluated by comparison with results from hotplate strong acid digestion followed by ICP-AES analysis. Based on the results of this study, the ultrasonic extraction/portable ASV procedure demonstrates potential for the on-site determination of lead in personal breathing zone and area air samples. PMID:9794065

  3. Cometabolism of trihalomethanes by mixed culture nitrifiers.

    PubMed

    Wahman, David G; Henry, Andrea E; Katz, Lynn E; Speitel, Gerald E

    2006-10-01

    Three mixed-culture nitrifier sources degraded low concentrations (25-450 microg/L) of four trihalomethanes (THMs) (trichloromethane (TCM) or chloroform, bromodichloromethane (BDCM), dibromochloromethane (DBCM), tribromomethane (TBM) or bromoform) commonly found in treated drinking water. Individual THM rate constants (k1THM) increased with increasing THM bromine-substitution with TBM>DBCM>BDCM>TCM and were comparable to previous studies with the pure culture nitrifier, Nitrosomonas europaea. A decrease in temperature resulted in a decrease in both ammonia and THM degradation rates with ammonia rates affected to a greater extent than THM degradation rates. The significant effect of temperature indicates that seasonal variations in water temperature should be a consideration for technology implementation. Product toxicity, measured by transformation capacity (T(c)), was similar to that observed with N. europaea. Because both rate constants and product toxicities increase with increasing THM bromine-substitution, a water's THM speciation is an important consideration for process implementation during drinking water treatment. Even though a given water is kinetically favored, the resulting THM product toxicity may not allow stable treatment process performance. PMID:16970971

  4. Modeling of trihalomethane cometabolism in nitrifying biofilters.

    PubMed

    Wahman, David G; Katz, Lynn E; Speitel, Gerald E

    2007-01-01

    The computer program AQUASIM was used to model biofilter experiments seeded with Lake Austin, Texas mixed-culture nitrifiers. These biofilters degraded four trihalomethanes (THMs) (trichloromethane (TCM) or chloroform, bromodichloromethane (BDCM), dibromochloromethane (DBCM), tribromomethane (TBM) or bromoform) commonly found in treated drinking water. Apparent steady-state data from the biofilter experiments and supporting batch experiments were used to estimate kinetic parameters for TCM, DBCM and ammonia degradation. Subsequently, the model was verified against other experimental biofilter data. To allow for full-scale simulations, BDCM and TBM rate constants were estimated using data from batch kinetic studies. Finally, the model was used to simulate full-scale filter performance under different filter surface loading rates and THM speciation seen in practice. Overall, total THM removals ranged from 16% to 54% in these simulations with influent total THM concentrations of 75-82microg/L, which illustrates the potential of THM cometabolism to have a significant impact on treated water quality. PMID:17129595

  5. Formation of trihalomethanes in foods and beverages.

    PubMed

    Huang, A-T; Batterman, S

    2009-07-01

    Trihalomethanes (THMs) are suspected carcinogens and reproductive toxicants commonly found in chlorinated drinking water. This study investigates THM formation during the preparation of beverages and foods using chlorinated drinking water. A total of 11 foods and 17 beverages were tested. Under the experimental conditions, each food and beverage formed THMs, primarily chloroform, although low or trace levels of brominated THMs were also detected. Tea formed the highest THM levels (e.g., chloroform levels from 3 to 67 microg l(-1)), followed by coffee (from 3 to 13 microg l(-1)), rice (9 microg l(-1)), soups (from 0.4 to 3.0 microg l(-1)), vegetables (<1 microg l(-1)), and baby food (<0.7 microg l(-1)). Chloroform formation with instant tea, used as a highly reproducible model system, increased with free chlorine concentration, decreased with higher food (tea) concentration, and was unaffected by reaction (steeping) time and bromide ion concentration. These findings indicate that chlorine-food reactions are fast, but that formation decreases as the chlorine demand of the food system increases. THMs are formed in the preparation and cooking of a wide variety of foods if free chlorine is present, and our results suggest that tea can be a significant source of exposure to THMs. PMID:19680970

  6. Field comparison of portable and stationary instruments for outdoor urban air exposure assessments

    NASA Astrophysics Data System (ADS)

    Viana, M.; Rivas, I.; Reche, C.; Fonseca, A. S.; Pérez, N.; Querol, X.; Alastuey, A.; Álvarez-Pedrerol, M.; Sunyer, J.

    2015-12-01

    The performance of three portable monitors (micro-aethalometer AE51, DiscMini, Dusttrak DRX) was assessed for outdoor air exposure assessment in a representative Southern European urban environment. The parameters evaluated were black carbon, particle number concentration, alveolar lung-deposited surface area, mean particle diameter, PM10, PM2.5 and PM1. The performance was tested by comparison with widely used stationary instruments (MAAP, CPC, SMPS, NSAM, GRIMM aerosol spectrometer). Results evidenced a good agreement between most portable and stationary instruments, with R2 values mostly >0.80. Relative differences between portable and stationary instruments were mostly <20%, and <10% between different units of the same instrument. The only exception was found for the Dusttrak DRX measurements, for which occasional concentration jumps in the time series were detected. Our results validate the performance of the black carbon, particle number concentration, particle surface area and mean particle diameter monitors as indicative instruments (tier 2) for outdoor air exposure assessment studies.

  7. Portable raman explosives detection

    SciTech Connect

    Moore, David Steven; Scharff, Robert J

    2008-01-01

    Recent advances in portable Raman instruments have dramatically increased their application to emergency response and forensics, as well as homeland defense. This paper reviews the relevant attributes and disadvantages of portable Raman spectroscopy, both essentially and instrumentally, to the task of explosives detection in the field.

  8. Sensitization of a stray-field NMR to vibrations: A potential for MR elastometry with a portable NMR sensor

    NASA Astrophysics Data System (ADS)

    Mastikhin, Igor; Barnhill, Marie

    2014-11-01

    An NMR signal from a sample in a constant stray field of a portable NMR sensor is sensitized to vibrations. The CPMG sequence is synchronized to vibrations so that the constant gradient becomes an "effective" square-wave gradient, leading to the vibration-induced phase accumulation. The integrating nature of the spot measurement, combined with the phase distribution due to a non-uniform gradient and/or a wave field, leads to a destructive interference, the drop in the signal intensity and changes in the echo train shape. Vibrations with amplitudes as small as 140 nm were reliably detected with the permanent gradient of 12.4 T/m. The signal intensity depends on the phase offset between the vibrations and the pulse sequence. This approach opens the way for performing elastometry and micro-rheology measurements with portable NMR devices beyond the walls of a laboratory. Even without synchronization, if a vibration frequency is comparable to 1/2TE of the CPMG sequence, the signal can be severely affected, making it important for potential industrial applications of stray-field NMR.

  9. A portable high-field pulsed-magnet system for single-crystal x-ray scattering studies

    SciTech Connect

    Islam, Zahirul; Lang, Jonathan C.; Ruff, Jacob P. C.; Ross, Kathryn A.; Gaulin, Bruce D.; Nojiri, Hiroyuki; Matsuda, Yasuhiro H.; Qu Zhe

    2009-11-15

    We present a portable pulsed-magnet system for x-ray studies of materials in high magnetic fields (up to 30 T). The apparatus consists of a split-pair of minicoils cooled on a closed-cycle cryostat, which is used for x-ray diffraction studies with applied field normal to the scattering plane. A second independent closed-cycle cryostat is used for cooling the sample to near liquid helium temperatures. Pulsed magnetic fields ({approx}1 ms in total duration) are generated by discharging a configurable capacitor bank into the magnet coils. Time-resolved scattering data are collected using a combination of a fast single-photon counting detector, a multichannel scaler, and a high-resolution digital storage oscilloscope. The capabilities of this instrument are used to study a geometrically frustrated system revealing strong magnetostrictive effects in the spin-liquid state.

  10. A portable high-field pulsed-magnet system for single-crystal x-ray scattering studies

    NASA Astrophysics Data System (ADS)

    Islam, Zahirul; Ruff, Jacob P. C.; Nojiri, Hiroyuki; Matsuda, Yasuhiro H.; Ross, Kathryn A.; Gaulin, Bruce D.; Qu, Zhe; Lang, Jonathan C.

    2009-11-01

    We present a portable pulsed-magnet system for x-ray studies of materials in high magnetic fields (up to 30 T). The apparatus consists of a split-pair of minicoils cooled on a closed-cycle cryostat, which is used for x-ray diffraction studies with applied field normal to the scattering plane. A second independent closed-cycle cryostat is used for cooling the sample to near liquid helium temperatures. Pulsed magnetic fields (˜1 ms in total duration) are generated by discharging a configurable capacitor bank into the magnet coils. Time-resolved scattering data are collected using a combination of a fast single-photon counting detector, a multichannel scaler, and a high-resolution digital storage oscilloscope. The capabilities of this instrument are used to study a geometrically frustrated system revealing strong magnetostrictive effects in the spin-liquid state.

  11. A portable high-field pulsed-magnet system for single-crystal x-ray scattering studies.

    PubMed

    Islam, Zahirul; Ruff, Jacob P C; Nojiri, Hiroyuki; Matsuda, Yasuhiro H; Ross, Kathryn A; Gaulin, Bruce D; Qu, Zhe; Lang, Jonathan C

    2009-11-01

    We present a portable pulsed-magnet system for x-ray studies of materials in high magnetic fields (up to 30 T). The apparatus consists of a split-pair of minicoils cooled on a closed-cycle cryostat, which is used for x-ray diffraction studies with applied field normal to the scattering plane. A second independent closed-cycle cryostat is used for cooling the sample to near liquid helium temperatures. Pulsed magnetic fields (approximately 1 ms in total duration) are generated by discharging a configurable capacitor bank into the magnet coils. Time-resolved scattering data are collected using a combination of a fast single-photon counting detector, a multichannel scaler, and a high-resolution digital storage oscilloscope. The capabilities of this instrument are used to study a geometrically frustrated system revealing strong magnetostrictive effects in the spin-liquid state. PMID:19947737

  12. Field evaluation of a prototype man-portable GC/MS

    SciTech Connect

    Arnold, N.S.; Hall, D.L.; Du, W.H.; Sheya, S.A.; Mihamou, H.; Dworzanski, J.; McClennen, W.H.; Meuzelaar, H.L.C.

    1995-12-31

    In recent years, a man-portable gas chromatography/mass spectrometry (GC/MS) system has been developed based on a Hewlett Packard 5971 MSD and a unique automated vapor sampling (AVS) transfer-line (TL) GC system for direct sampling of ambient chemical vapors. The vacuum system and power supplies were replaced to facilitate operation on 24 Vdc batteries for up to 4 hours after startup on a transportable docking station. The gas chromatography was performed on a short (2 m) capillary column under isothermal conditions in a small oven to minimize power usage. Repetitive samples were taken at 10 to 60 s intervals using an automated vapor sampling inlet. In initial testing, the prototype system has been used for monitoring of gasoline vapors. Ambient levels of 6.0 ppm benzene, 4.1 ppm toluene, 0.22 ppm ethylbenzene, 1.1 ppm m- and p-xylene and 0.25 ppm o-xylene were measured near a busy gas station. The gradient mapping or source tracking capabilities of the backpack mounted system have also been demonstrated in tests with a simulated gasoline leak. This paper will describe recent work to further evaluate the capabilities and limitations of the prototype system. Results will be described in terms of the practical utility of portable GC/MS for identification and quantitation of unknown vapors.

  13. TRIHALOMETHANE PRECURSOR REMOVAL BY THE MAGNESIUM CARBONATE PROCESS

    EPA Science Inventory

    A project was conducted to determine and improve the ability of the magnesium carbonate process to remove trihalomethane (THM) precursors in treated drinking water. The project was conducted at a drinking water treatment plant in Melbourne, FL, which had been developed and instal...

  14. TRIHALOMETHANE LEVELS IN HOME TAP WATER AND SEMEN QUALITY

    EPA Science Inventory

    Trihalomethane Levels in Home Tap Water and Semen Quality
    Laura Fenster, 1 Kirsten Waller, 2 Gayle Windham, 1 Tanya Henneman, 2 Meredith Anderson, 2 Pauline Mendola, 3 James W. Overstreet, 4 Shanna H. Swan5

    1California Department of Health Services, Division of Environm...

  15. Analysis of Trihalomethanes in Soft Drinks: An Instrumental Analysis Experiment.

    ERIC Educational Resources Information Center

    Graham, Richard C.; Robertson, John K.

    1988-01-01

    Describes an experimental procedure for determining trihalomethanes (THMs) in liquids by gas chromatography. Provides recommendations for reactants and supplies to obtain acceptable results. Discusses the analysis of water from various sources: pools, lakes, and drinking water; compares these to three cola drinks. (ML)

  16. PILOT SCALE EVALUATION OF PHOTOLYTIC OZONATION FOR TRIHALOMETHANE PRECURSOR REMOVAL

    EPA Science Inventory

    The use of ozone combined with ultraviolet radiation has been studied at the pilot-scale for removing trihalomethane (THM) precursors from potable water. The effects of variations in ozone dose rate, UV intensity and other parameters were first studied using a synthetic feedwater...

  17. ALTERNATIVE OXIDANT AND DISINFECTANT TREATMENT STRATEGIES FOR CONTROLLING TRIHALOMETHANE FORMATION

    EPA Science Inventory

    To comply with the maximum contaminant level (MCL) for total trihalomethanes (TTHM), many utilities have modified their pre-oxidation and disinfection practices by switching to alternative oxidants and disinfectants in place of free chlorine. To evaluate the impact of these chang...

  18. Final Report on Portable Laser Coating Removal Systems Field Demonstrations and Testing

    NASA Technical Reports Server (NTRS)

    Rothgeb, Matthew J.; McLaughlin, Russell L.

    2008-01-01

    Processes currently used throughout the National Aeronautics and Space Administration (NASA) to remove corrosion and coatings from structures, ground service equipment and small components results in waste streams consisting of toxic chemicals, spent media blast materials, and waste water. When chemicals are used in these processes they are typically high in volatile organic compounds (VOC) and are considered hazardous air pollutants (HAP). When blast media is used, the volume of hazardous waste generated is increased significantly. Many of the coatings historically used within NASA contain toxic metals such as hexavalent chromium, and lead. These materials are highly regulated and restrictions on worker exposure continue to increase. Most recently the EPA reduced the permissible exposure limit (PEL) for hexavalent chromium. The new standard lowers OSHA's PEL for hexavalent chromium from 52 to 5 micrograms of Cr(V1) per cubic meter of air as an 8-hour time-weighted average. Hexavalent chromium is found in the pretreatment and primer coatings used within the Shuttle Program. In response to the need to continue to protect assets within the agency and the growing concern over these new regulations, NASA is researching different ways to continue the required maintenance of both facility and flight equipment in a safe, efficient and environmentally preferable manner. The use of laser energy to remove prepare surfaces for a variety of processes, such as corrosion and coating removal, weld preparation and non destructive evaluation is a relatively new technology that has shown itself to be environmentally preferable and in many cases less labor intensive than currently used removal methods. The development of a Portable Laser Coating Removal System (PLCRS) started as the goal of a Joint Group on Pollution Prevention (JG-PP) project, led by the Air Force, where several types of lasers in several configurations were thoroughly evaluated. Following this project, NASA decided

  19. Portable fuel cell systems for America's army: technology transition to the field

    NASA Astrophysics Data System (ADS)

    Patil, Ashok S.; Dubois, Terry G.; Sifer, Nicholas; Bostic, Elizabeth; Gardner, Kristopher; Quah, Michael; Bolton, Christopher

    The US Army Communications, Electronics Research Development and Engineering Center (CERDEC) envisions three thrust areas for portable fuel cell systems for military applications. These areas include soldier power (<500 W), sensor power (0-100 W), and auxiliary power units or APUs (0.5-10 kW). Soldier and sensor fuel cell systems may be man-portable/backpackable while APUs could be employed as squad battery chargers or as 'Silent Watch' APUs where low signature (acoustic, thermal, etc.) operation is a requirement. The Army's research and development efforts are focusing on methods of either storing or generating hydrogen on the battlefield. Hydrogen storage technology is considered critical to small military and/or commercial fuel cell systems, and is being pursued in a host of commercial and government programs. CERDEC, in a joint effort with the Army Research Office (ARO) and the Defense Advanced Research Projects Agency (DARPA), is developing several promising hydrogen generating technologies. The goal of this program is a safe, reliable hydrogen source that can provide rates up to 100 W with an energy density of greater than 1000 Wh/kg. For larger fuel cell units (>500 W), it is imperative that the fuel cell power units be able to operate on fuels within the military logistics chain [DOD 4140.25-M, DOD Directive 4140.25 (1993)]. CERDEC is currently conducting research on catalysts and microchannel fuel reformers that offer great promise for the reforming of diesel and JP-8 fuels into hydrogen. In addition to research work on PEM fuel cells and enabling technologies, the Army is also conducting research on direct methanol and solid oxide fuel cells, and combined heat and power applications utilizing new high temperature fuel cells.

  20. Small field of view, high-resolution, portable γ-camera for axillary sentinel node detection

    NASA Astrophysics Data System (ADS)

    Soluri, A.; Massari, R.; Trotta, C.; Tofani, A.; Di Santo, G.; Di Pietro, B.; Di Paolo, M. L.; Roncacci, A.; Amanti, C.; Scopinaro, F.

    2006-12-01

    Sentinel node (SN) biopsy is an established method for breast cancer staging. Many authors suggested lymphoscintigraphy (LS) in order to indicate the sentinel node; others adopted the vital dye method together with radiocolloids, but only with γ-probe detection during operation without preliminary Anger camera LS. The second method is more simple and fast when compared with LS plus radioguided surgery. The Imaging Probe (IP) is a portable, hand held, high-resolution mini γ-camera studied by our group since 1998. Initial studies on sentinel node biopsy were carried out by us with IP on small series of patients to validate and to demonstrate the effectiveness and usefulness of IP against conventional probes. The aim of the present study is to show that surgeon removes the mammary sentinel node quicker and safer when using IP and conventional γ-probe together than conventional probe only. The results of our study not only show that our device makes quicker and safer SN biopsy, but also that the number of detected nodes is larger with our method than with conventional diagnostic and surgical techniques.

  1. Courseware Portability.

    ERIC Educational Resources Information Center

    Fletcher, J. D.

    Portability enables interactive courseware (ICW) and associated application programs to operate on computer-based systems other than the ones on which they are developed. Courseware portability will increase sharing of ICW across a range of instructional settings within military services and across internationally allied military services. The…

  2. Field evaluation of portable and central site PM samplers emphasizing additive and differential mass concentration estimates

    NASA Astrophysics Data System (ADS)

    Chen, Fu-Lin; Vanderpool, Robert; Williams, Ronald; Dimmick, Fred; Grover, Brett D.; Long, Russell; Murdoch, Robert

    2011-08-01

    The US Environmental Protection Agency (EPA) published a National Ambient Air Quality Standard (NAAQS) and the accompanying Federal Reference Method (FRM) for PM 10 in 1987. The EPA revised the particle standards and FRM in 1997 to include PM 2.5. In 2005, EPA proposed revisions to this NAAQS to include PM 10-2.5 but only finalized revisions with a PM 2.5 FRM and the development of a national monitoring network in 2006. Presently, no EPA designated reference or equivalent method sampler has the ability to directly measure the mass concentrations of PM 10, PM 10-2.5, and PM 2.5 simultaneously. An additive approach has been used for samplers like the dichotomous monitors to calculate PM 10 mass concentrations from independent measures of PM 10-2.5 and PM 2.5 (i.e. PM 10 = PM 10-2.5 + PM 2.5). A differential approach has been used to calculate PM 10-2.5 from identical collocated PM 10 and PM 2.5 samplers (i.e. PM 10-2.5 = PM 10-PM 2.5). Since these two approaches have been used widely for PM measurements, it is informative to evaluate their precision and comparability. EPA performed collocated tests of five different particle samplers in the Research Triangle Park area of North Carolina to evaluate the comparability and to characterize the additive and differential approaches used to determine particle mass concentrations. The intra-sampler precision of MiniVol, Omni, and dichotomous samplers was less than 8.4%. The precision of PM 10 measurements using the additive approach with dichotomous samplers was less than 3.5%. The poorest precision of the various PM 10-2.5 differential approaches was less than 15.1%. No zero or negative PM 10-2.5 concentrations were calculated using the differential approach. A coefficient of determination of 0.81 or higher was obtained for all paired comparison of PM 10-2.5. The reported test results show that concentrations calculated from both the additive and differential approaches generally agree among the portable samplers, the more

  3. Final Report on NASA Portable Laser Coating Removal Systems Field Demonstrations and Testing

    NASA Technical Reports Server (NTRS)

    Rothgeb, Matthew J; McLaughlin, Russell L.

    2008-01-01

    Portable Laser Coating Removal System (PLCRS) started as the goal of a Joint Group on Pollution Prevention (JG-PP) project, led by the Air Force, where several types of lasers in several configurations were thoroughly evaluated. Following this project, NASA decided to evaluate the best performers on processes and coatings specific to the agency. Laser systems used during this project were all of a similar design, between 40 and 500 Watts, most of which had integrated vacuum systems in order to collect materials removed from substrate surfaces during operation.

  4. Preliminary Results from the Portable Imagery Quality Assessment Test Field (PIQuAT) of Uav Imagery for Imagery Reconnaissance Purposes

    NASA Astrophysics Data System (ADS)

    Dabrowski, R.; Orych, A.; Jenerowicz, A.; Walczykowski, P.

    2015-08-01

    The article presents a set of initial results of a quality assessment study of 2 different types of sensors mounted on an unmanned aerial vehicle, carried out over an especially designed and constructed test field. The PIQuAT (Portable Imagery Quality Assessment Test Field) field had been designed especially for the purposes of determining the quality parameters of UAV sensors, especially in terms of the spatial, spectral and radiometric resolutions and chosen geometric aspects. The sensor used include a multispectral framing camera and a high-resolution RGB sensor. The flights were conducted from a number of altitudes ranging from 10 m to 200 m above the test field. Acquiring data at a number of different altitudes allowed the authors to evaluate the obtained results and check for possible linearity of the calculated quality assessment parameters. The radiometric properties of the sensors were evaluated from images of the grayscale target section of the PIQuAT field. The spectral resolution of the imagery was determined based on a number of test samples with known spectral reflectance curves. These reference spectral reflectance curves were then compared with spectral reflectance coefficients at the wavelengths registered by the miniMCA camera. Before conducting all of these experiments in field conditions, the interior orientation parameters were calculated for the MiniMCA and RGB sensor in laboratory conditions. These parameters include: the actual pixel size on the detector, distortion parameters, calibrated focal length (CFL) and the coordinates of the principal point of autocollimation (miniMCA - for each of the six channels separately.

  5. FIELD SCREENING OF POLYCYCLIC HYDROCARBON CONTAMINATION IN SOIL USING A PORTABLE SYNCHRONOUS SCANNING SPECTROFLUOROMETER

    EPA Science Inventory

    Polycyclic aromatic hydrocarbon (PAH) contamination is a considerable problem at various hazardous waste sites. sources of PAH contamination include: incomplete combustion processes, wood preservatives, and the fuel industry. he development of rapid, cost-effective field screenin...

  6. A laboratory and field evaluation of a portable immunoassay test for triazine herbicides in environmental water samples

    USGS Publications Warehouse

    Schulze, P.A.; Capel, P.D.; Squillace, P.J.; Helsel, D.R.

    1993-01-01

    The usefulness and sensitivity, of a portable immunoassay test for the semiquantitative field screening of water samples was evaluated by means of laboratory and field studies. Laboratory results indicated that the tests were useful for the determination of atrazine concentrations of 0.1 to 1.5 μg/L. At a concentration of 1 μg/L, the relative standard deviation in the difference between the regression line and the actual result was about 40 percent. The immunoassay was less sensitive and produced similar errors for other triazine herbicides. After standardization, the test results were relatively insensitive to ionic content and variations in pH (range, 4 to 10), mildly sensitive to temperature changes, and quite sensitive to the timing of the final incubation step, variances in timing can be a significant source of error. Almost all of the immunoassays predicted a higher atrazine concentration in water samples when compared to results of gas chromatography. If these tests are used as a semiquantitative screening tool, this tendency for overprediction does not diminish the tests' usefulness. Generally, the tests seem to be a valuable method for screening water samples for triazine herbicides.

  7. Rapid and nondestructive measurement of labile Mn, Cu, Zn, Pb and As in DGT by using field portable-XRF.

    PubMed

    Chen, Zheng; Williams, Paul N; Zhang, Hao

    2013-09-01

    The technique of diffusive gradients in thin films (DGT) is often employed to quantify labile metals in situ; however, it is a challenge to perform the measurements in-field. This study evaluated the capability of field-portable X-ray fluorescence (FP-XRF) to swiftly generate elemental speciation information with DGT. Biologically available metal ions in environmental samples passively preconcentrate in the thin films of DGT devices, providing an ideal and uniform matrix for XRF nondestructive detection. Strong correlation coefficients (r > 0.992 for Mn, Cu, Zn, Pb and As) were obtained for all elements during calibration. The limits of quantitation (LOQ) for the investigated elements of FP-XRF on DGT devices are 2.74 for Mn, 4.89 for Cu, 2.89 for Zn, 2.55 for Pb, and 0.48 for As (unit: μg cm(-2)). When Pb and As co-existed in the solution trials, As did not interfere with Pb detection when using Chelex-DGT. However, there was a significant enhancement of the Pb reading attributed to As when ferrihydrite binding gels were tested, consistent with Fe-oxyhydroxide surfaces absorbing large quantities of As. This study demonstrates the value of the FP-XRF technique to rapidly and nondestructively detect the metals accumulated in DGT devices, providing a new and simple diagnostic tool for on-site environmental monitoring of labile metals/metalloids. PMID:23912422

  8. Detection of hexavalent uranium with inline and field-portable immunosensors

    SciTech Connect

    Melton, Scott J.; Yu, Haini; Ali, Mehnaaz F.; Williams, Kenneth H; Wilkins, Michael J.; Long, Philip E.; Blake, Diane A.

    2008-10-02

    An antibody that recognizes a chelated form of hexavalent uranium was used in the development of two different immunosensors for uranium detection. Specifically, these sensors were utilized for the analysis of groundwater samples collected during a 2007 field study of in situ bioremediation in a aquifer located at Rifle, CO. The antibody-based sensors provided data comparable to that obtained using Kinetic Phosphorescence Analysis (KPA). Thus, these novel instruments and associated reagents should provide field researchers and resource managers with valuable new tools for on-site data acquisition.

  9. A simple, accurate, field-portable mixing ratio generator and Rayleigh distillation device

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Routine field calibration of water vapor analyzers has always been a challenging problem for those making long-term flux measurements at remote sites. Automated sampling of standard gases from compressed tanks, the method of choice for CO2 calibration, cannot be used for H2O. Calibrations are typica...

  10. Field-testing a portable wind tunnel for fine dust emissions

    Technology Transfer Automated Retrieval System (TEKTRAN)

    A protable wind tunnel has been developed to allow erodibility and dust emissions testing of soil surfaces with the premise that dust concentration and properties are highly correlated with surface soil properties, as modified by crop management system. In this study we report on the field-testing ...

  11. Field portable detection of VOCs using a SAW/GC system

    SciTech Connect

    Staples, E.J.

    1995-10-01

    This paper describes research on a fast gas chromatography (GC) vapor analysis system which uses a new type of Surface Acoustic Wave detector technology to characterize organic contamination in soil and groundwater. The project was sponsored by the Department of Energy, Morgantown Energy Technology Center. The instrument was field tested at the Savannah River Plant.

  12. DETECTION AND IDENTIFICATION OF TOXIC AIR POLLUTANTS USING FIELD PORTABLE AND AIRBORNE REMOTE IMAGING SYSTEMS

    EPA Science Inventory

    Remote sensing technologies are a class of instrument and sensor systems that include laser imageries, imaging spectrometers, and visible to thermal infrared cameras. These systems have been successfully used for gas phase chemical compound identification in a variety of field e...

  13. Portable Planetarium.

    ERIC Educational Resources Information Center

    Stockdale, Dennis L.

    1997-01-01

    Describes a method that students can use to build portable planetariums. After building the models, students are familiar with the names of constellations and major stars and are able to share their projects with other students. (DDR)

  14. Technical design issues for a field-portable supercritical fluid extractor

    SciTech Connect

    Wright, B.W.; Zemanian, T.S.; Robins, W.H.; Wright, C.W.

    1995-01-01

    Supercritical fluid extraction is gaining acceptance as an alternative sample preparation method for trace organic analysis. The development of SFE instrumentation optimized for field use requires taking several technical design issues including size and weight requirements, user-friendly operation, and technical performance capabilities into consideration. Parameters associated with a prototype SFE instrument under development for potential use in conducting on-site inspections of the Chemical Weapons Convention and its preliminary technical and operational performance are described.

  15. Explosives detection in soil using a field-portable continuous flow immunosensor.

    PubMed

    Gauger, P R; Holt, D B; Patterson, C H; Charles, P T; Shriver-Lake, L; Kusterbeck, A W

    2001-05-01

    A field method for quantitative analysis of explosives in contaminated soil samples is described. The method is based on a displacement immunoassay performed in a commercial instrument, the FAST 2000, engineered by Research International Inc. The method can be used on-site to measure 2,4,6-trinitrotoluene (TNT) and hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) within 5min. For this study, replicate analyses were performed on soil extracts prepared from each field sample as well as appropriate controls, blanks, and laboratory standards. Statistical analyses were done to assess accuracy, bias, and predictability of the method. The results demonstrated that the immunosensor could be used effectively to screen environmental samples for the presence or absence of explosives. In most samples, the method also provided quantitative values that were in good agreement with standard laboratory analyses using HPLC. A limited number of sample matrices interfered with the immunoassay and produced results that varied significantly from the laboratory data. In each case, the compounds causing the problem have been identified and efforts are being made to minimize these matrix interferences in future field evaluations. PMID:11267745

  16. Portable light-emitting diode-based photometer with one-shot optochemical sensors for measurement in the field

    NASA Astrophysics Data System (ADS)

    Palma, A. J.; Ortigosa, J. M.; Lapresta-Fernández, A.; Fernández-Ramos, M. D.; Carvajal, M. A.; Capitán-Vallvey, L. F.

    2008-10-01

    This report describes the electronics of a portable, low-cost, light-emitting diode (LED)-based photometer dedicated to one-shot optochemical sensors. Optical detection is made through a monolithic photodiode with an on-chip single-supply transimpedance amplifier that reduces some drawbacks such as leakage currents, interferences, and parasitic capacitances. The main instrument characteristics are its high light source stability and thermal correction. The former is obtained by means of the optical feedback from the LED polarization circuit, implementing a pseudo-two light beam scheme from a unique light source with a built-in beam splitter. The feedback loop has also been used to adjust the LED power in several ranges. Moreover, the low-thermal coefficient achieved (-90 ppm/°C) is compensated by thermal monitoring and calibration function compensation in the digital processing. The hand-held instrument directly gives the absorbance ratio used as the analytical parameter and the analyte concentration after programming the calibration function in the microcontroller. The application of this photometer for the determination of potassium and nitrate, using one-shot sensors with ionophore-based chemistries is also demonstrated, with a simple analytical methodology that shortens the analysis time, eliminating some calibrating solutions (HCl, NaOH, and buffer). Therefore, this compact instrument is suitable for real-time analyte determination and operation in the field.

  17. Metals in boat paint fragments from slipways, repair facilities and abandoned vessels: an evaluation using field portable XRF.

    PubMed

    Turner, Andrew; Comber, Sean; Rees, Aldous B; Gkiokas, Dimitrios; Solman, Kevin

    2015-01-01

    Paint flaking off abandoned vessels or generated during boat repair is hazardous to human health and wildlife. In this study, a means of screening paint fragments using a field portable-X-ray fluorescence (FP-XRF) spectrometer is described. The technique is capable of delivering rapid, surficial measurements of Ba, Cu, Pb and Zn down to concentrations less than 150 μg g(-1), and Sn and Cr to concentrations of a few hundred μg g(-1). Application of the technique to fragments collected from slipways, yards, hardstandings, abandoned boats and ships undergoing maintenance throughout the EU reveal highly variable concentrations of metals among samples from the same environment or from the same region of a given boat; in many cases, variability is also evident in different areas or on different surfaces of the same fragment. Of particular concern are elevated concentrations of substances that have been restricted or banned (e.g. Sn, an indicator of organotin, and up to concentrations of 40,000 μg g(-1), and Pb up to concentrations of 200,000 μg g(-1)). Although FP-XRF can rapidly screen samples whose composition and origin are unknown and can assist in instantaneous decision making, a full risk assessment will rely on additional analyses of the precise species (including organo-forms) of the metals present. PMID:25281117

  18. Intraoperative Scintigraphy Using a Large Field-of-View Portable Gamma Camera for Primary Hyperparathyroidism: Initial Experience

    PubMed Central

    Hall, Nathan C.; Plews, Robert L.; Agrawal, Amit; Povoski, Stephen P.; Wright, Chadwick L.; Zhang, Jun; Martin, Edward W.; Phay, John

    2015-01-01

    Background. We investigated a novel technique, intraoperative 99 mTc-Sestamibi (MIBI) imaging (neck and excised specimen (ES)), using a large field-of-view portable gamma camera (LFOVGC), for expediting confirmation of MIBI-avid parathyroid adenoma removal. Methods. Twenty patients with MIBI-avid parathyroid adenomas were preoperatively administered MIBI and intraoperatively imaged prior to incision (neck) and immediately following resection (neck and/or ES). Preoperative and intraoperative serum parathyroid hormone monitoring (IOPTH) and pathology (path) were also performed. Results. MIBI neck activity was absent and specimen activity was present in 13/20 with imaging after initial ES removal. In the remaining 7/20 cases, residual neck activity and/or absent ES activity prompted excision of additional tissue, ultimately leading to complete hyperfunctioning tissue excision. Postexcision LFOVGC ES imaging confirmed parathyroid adenoma resection 100% when postresection imaging qualitatively had activity (ES) and/or no activity (neck). The mean ± SEM time saving using intraoperative LFOVGC data to confirm resection versus first IOPTH or path result would have been 22.0 ± 2 minutes (specimen imaging) and 26.0 ± 3 minutes (neck imaging). Conclusion. Utilization of a novel real-time intraoperative LFOVGC imaging approach can provide confirmation of MIBI-avid parathyroid adenoma removal appreciably faster than IOPTH and/or path and may provide a valuable adjunct to parathyroid surgery. PMID:25629056

  19. Field-Portable Immunoassay Instruments and Reagents to Measure Chelators and Mobile Forms of Uranium

    SciTech Connect

    Blake, Diane A.

    2003-06-01

    The goals for the 3-year project period are (1) to test and validate the present uranium sensor and develop protocols for its use at the NABIR Field Research Center; (2) to develop new reagents that will provide superior performance for the present hand-held immunosensor; and (3) to develop new antibodies that will permit this sensor to also measure other environmental contaminants (chromium, mercury, and/or DTPA). Sensor design modifications are underway via international collaborations. New reagents that will provide superior performance for the present hand-held immunosensor are being prepared and tested. New methods have been developed, to produce recombinant forms of metal-specific monoclonal antibodies for use with the sensor. Site-directed mutagenesis experiments are underway to determine the mechanisms of binding. Immunization experiments with sheep and rabbits to develop new recombinant forms of antibodies to metal-chelate complexes (chromium, mercury, and/or DTPA) have been initiated.

  20. Remote Sensing of Aircraft Contrails Using a Field Portable Digital Array Scanned Interferometer

    NASA Technical Reports Server (NTRS)

    Smith, William Hayden

    1997-01-01

    With a Digital Array Scanned Interferometer (DASI), we have obtained proof-of-concept observations with which we demonstrate DASI capabilities for the determination of contrail properties. These include the measurement of the cloud and soot microphysical parameters, as well, the abundances of specific pollutant species such as SO(sub x) or NO(sub x). From high quality hyperspectral data and using radiative transfer methods and atmospheric chemistry analysis in the data reduction and interpretation, powerful inferences concerning cloud formation, evolution and dissipation can be made. Under this sub-topic, we will integrate DASI with computer controlled scanning of the field-of-view to direct the sensor towards contrails and exhaust plumes for tracking the emitting vehicles. The optimum DASI wavelength sensitivity range for sensing contrails is 0.35 - 2.5 micron. DASI deploys on the ground or from aircraft to observe contrails in the vicinity. This enables rapid, accurate measurement of the temporal, spatial, and chemical evolution of contrails (or other plumes or exhaust sources) with a low cost, efficient sensor.

  1. ARCHAEO-SCAN: Portable 3D shape measurement system for archaeological field work

    NASA Astrophysics Data System (ADS)

    Knopf, George K.; Nelson, Andrew J.

    2004-10-01

    Accurate measurement and thorough documentation of excavated artifacts are the essential tasks of archaeological fieldwork. The on-site recording and long-term preservation of fragile evidence can be improved using 3D spatial data acquisition and computer-aided modeling technologies. Once the artifact is digitized and geometry created in a virtual environment, the scientist can manipulate the pieces in a virtual reality environment to develop a "realistic" reconstruction of the object without physically handling or gluing the fragments. The ARCHAEO-SCAN system is a flexible, affordable 3D coordinate data acquisition and geometric modeling system for acquiring surface and shape information of small to medium sized artifacts and bone fragments. The shape measurement system is being developed to enable the field archaeologist to manually sweep the non-contact sensor head across the relic or artifact surface. A series of unique data acquisition, processing, registration and surface reconstruction algorithms are then used to integrate 3D coordinate information from multiple views into a single reference frame. A novel technique for automatically creating a hexahedral mesh of the recovered fragments is presented. The 3D model acquisition system is designed to operate from a standard laptop with minimal additional hardware and proprietary software support. The captured shape data can be pre-processed and displayed on site, stored digitally on a CD, or transmitted via the Internet to the researcher's home institution.

  2. Field-usable portable analyzer for chlorinated organic compounds. Topical report, September 1992--May 1994

    SciTech Connect

    Buttner, W.J.; Williams, R.D.

    1995-05-01

    Through a U.S. DOE-funded program, an advanced chlorinated organic (RCL) vapor monitor has been built and tested in actual hazardous waste site operations. The monitor exploits the analytical capabilities of a solid-state sensor which was recently developed and has remarkable selectivity for chlorinated organic vapors at sub-parts-per-million sensitivity. The basic design goal of a user-friendly, reliable, instrument with a broad dynamic range for the selective detection of chlorinated solvent vapors was demonstrated. To date, no non-halogen-containing compound has been identified that induces a measurable response on the sensor, including commonly encountered contaminants such as BTXs (benzene, toluene, and xylenes) or POLs (petroleum, oils, lubricants). In addition to the development of the RCL MONITOR, advanced sampler systems were developed to further extend the analytical capability of this instrument, allowing chemical analyses to be performed for both vapor phase and condensed contamination. The sampling methods include fixed dilution, preconcentration, and closed-loop air stripping for condensed media. With uniform success, these different series of field tests were conducted at DOE facilities on several types of samples. Independent cost-benefit analysis has concluded that significant cost savings can be achieved using the RCL MONITOR in DOE applications. This effort provides a sound fundamental technology base for the development of advanced analytical methods that are needed by the US DOE. In addition, advanced methods for detecting chlorinated hydrocarbons that are made possible by this technology will save time, reduce costs, and improve human health and safety in restoration operations. To fully achieve all possible cost savings, continued effort is necessary to develop validated methods for the use of the RCL MONITOR. The development of methods through case studies is the theme of the Phase II effort, which is currently underway.

  3. Design of a portable wide field of view GPU-accelerated multiphoton imaging system for real-time imaging of breast surgical specimens

    NASA Astrophysics Data System (ADS)

    Giacomelli, Michael G.; Yoshitake, Tadayuki; Husvogt, Lennart; Cahill, Lucas; Ahsen, Osman; Vardeh, Hilde; Sheykin, Yury; Faulkner-Jones, Beverly E.; Hornegger, Joachim; Brooker, Jeff; Cable, Alex; Connolly, James L.; Fujimoto, James G.

    2016-03-01

    We present a portable multiphoton system designed for evaluating centimeter-scale surgical margins on surgical breast specimens in a clinical setting. The system is designed to produce large field of view images at a high frame rate, while using GPU processing to render low latency, video-rate virtual H&E images for real-time assessment. The imaging system and virtual H&E rendering algorithm are demonstrated by imaging unfixed human breast tissue in a clinical setting.

  4. Field detection of avian influenza virus in wild birds: evaluation of a portable rRT-PCR system and freeze-dried reagents.

    PubMed

    Takekawa, John Y; Iverson, Samuel A; Schultz, Annie K; Hill, Nichola J; Cardona, Carol J; Boyce, Walter M; Dudley, Joseph P

    2010-06-01

    Wild birds have been implicated in the spread of highly pathogenic avian influenza (HPAIV) of the H5N1 subtype, prompting surveillance along migratory flyways. Sampling of wild birds is often conducted in remote regions, but results are often delayed because of limited local analytical capabilities, difficulties with sample transportation and permitting, or problems keeping samples cold in the field. In response to these challenges, the performance of a portable real-time, reverse transcriptase-polymerase chain reaction (rRT-PCR) unit (RAPID((R)), Idaho Technologies, Salt Lake City, UT) that employed lyophilized reagents (Influenza A Target 1 Taqman; ASAY-ASY-0109, Idaho Technologies) was compared to virus isolation combined with real-time RT-PCR conducted in a laboratory. This study included both field- and experimental-based sampling. Field samples were collected from migratory shorebirds captured in northern California, while experimental samples were prepared by spiking fecal material with an H6N2 AIV isolate. Results indicated that the portable rRT-PCR unit had equivalent specificity to virus isolation with no false positives, but sensitivity was compromised at low viral titers. Use of portable rRT-PCR with lyophilized reagents may expedite surveillance results, paving the way to a better understanding of wild bird involvement in HPAIV H5N1 transmission. PMID:20206650

  5. Field detection of avian influenza virus in wild birds: evaluation of a portable rRT-PCR system and freeze-dried reagents

    USGS Publications Warehouse

    Takekawa, John Y.; Iverson, Samuel A.; Schultz, Annie K.; Hill, Nichola J.; Cardona, Carol J.; Boyce, Walter M.; Dudley, Joseph P.

    2010-01-01

    Wild birds have been implicated in the spread of highly pathogenic avian influenza (HPAIV) of the H5N1 subtype, prompting surveillance along migratory flyways. Sampling of wild birds is often conducted in remote regions, but results are often delayed because of limited local analytical capabilities, difficulties with sample transportation and permitting, or problems keeping samples cold in the field. In response to these challenges, the performance of a portable real-time, reverse transcriptase-polymerase chain reaction (rRT-PCR) unit (RAPID(Registered), Idaho Technologies, Salt Lake City, UT) that employed lyophilized reagents (Influenza A Target 1 Taqman; ASAY-ASY-0109, Idaho Technologies) was compared to virus isolation combined with real-time RT-PCR conducted in a laboratory. This study included both field and experimental-based sampling. Field samples were collected from migratory shorebirds captured in northern California, while experimental samples were prepared by spiking fecal material with an H6N2 AIV isolate. Results indicated that the portable rRT-PCR unit had equivalent specificity to virus isolation with no false positives, but sensitivity was compromised at low viral titers. Use of portable rRT-PCR with lyophilized reagents may expedite surveillance results, paving the way to a better understanding of wild bird involvement in HPAIV H5N1 transmission.

  6. Field Analysis of Polychlorinated Biphenyls (PCBs) in Soil Using Solid-Phase Microextraction (SPME) and a Portable Gas Chromatography-Mass Spectrometry System.

    PubMed

    Zhang, Mengliang; Kruse, Natalie A; Bowman, Jennifer R; Jackson, Glen P

    2016-05-01

    An expedited field analysis method was developed for the determination of polychlorinated biphenyls (PCBs) in soil matrices using a portable gas chromatography-mass spectrometry (GC-MS) instrument. Soil samples of approximately 0.5 g were measured with a portable scale and PCBs were extracted by headspace solid-phase microextraction (SPME) with a 100 µm polydimethylsiloxane (PDMS) fiber. Two milliliters of 0.2 M potassium permanganate and 0.5 mL of 6 M sulfuric acid solution were added to the soil matrices to facilitate the extraction of PCBs. The extraction was performed for 30 min at 100 ℃ in a portable heating block that was powered by a portable generator. The portable GC-MS instrument took less than 6 min per analysis and ran off an internal battery and helium cylinder. Six commercial PCB mixtures, Aroclor 1016, 1221, 1232, 1242, 1248, 1254, and 1260, could be classified based on the GC chromatograms and mass spectra. The detection limit of this method for Aroclor 1260 in soil matrices is approximately 10 ppm, which is sufficient for guiding remediation efforts in contaminated sites. This method was applicable to the on-site analysis of PCBs with a total analysis time of 37 min per sample. However, the total analysis time could be improved to less than 7 min per sample by conducting the rate-limiting extraction step for different samples in parallel. PMID:27170778

  7. Can field portable X-ray fluorescence (pXRF) produce high quality data for application in environmental contamination research?

    PubMed

    Rouillon, Marek; Taylor, Mark P

    2016-07-01

    This research evaluates the analytical capabilities of a field portable X-ray fluorescence spectrometer (pXRF) for the measurement of contaminated soil samples using a matrix-matched calibration. The calibrated pXRF generated exceptional data quality from the measurement of ten soil reference materials. Elemental recoveries improved for all 11 elements post-calibration with reduced measurement variation and detection limits in most cases. Measurement repeatability of reference values ranged between 0.2 and 10% relative standard deviation, while the majority (82%) of reference recoveries were between 90 and 110%. Definitive data quality, the highest of the US EPA's three level quality ranking, was achieved for 15 of 19 elemental datasets. Measurement comparability against inductively coupled plasma atomic emission spectrometry (ICP-AES) values was excellent for most elements (e.g, r(2) 0.999 for Mn and Pb, r(2) > 0.995 for Cu, Zn and Cd). Parallel measurement of reference materials revealed ICP-AES and ICP-MS measured Ti and Cr poorly when compared to pXRF. Individual recoveries of soil reference materials by both ICP-AES and pXRF showed that pXRF was equivalent to or better than ICP-AES values for all but two elements (Ni, As). This study demonstrates pXRF as a suitable alternative to ICP-AES analysis in the measurement of Ti, Cr, Mn, Fe, Cu, Zn, Sr, Cd, and Pb in metal-contaminated soils. Where funds are limited, pXRF provides a low-cost, high quality solution to increasing sample density for a more complete geochemical investigation. PMID:27100216

  8. Predicting Trihalomethanes (THMs) in the New York City Water Supply

    NASA Astrophysics Data System (ADS)

    Mukundan, R.; Van Dreason, R.

    2013-12-01

    Chlorine, a commonly used disinfectant in most water supply systems, can combine with organic carbon to form disinfectant byproducts including carcinogenic trihalomethanes (THMs). We used water quality data from 24 monitoring sites within the New York City (NYC) water supply distribution system, measured between January 2009 and April 2012, to develop site-specific empirical models for predicting total trihalomethane (TTHM) levels. Terms in the model included various combinations of the following water quality parameters: total organic carbon, pH, specific conductivity, and water temperature. Reasonable estimates of TTHM levels were achieved with overall R2 of about 0.87 and predicted values within 5 μg/L of measured values. The relative importance of factors affecting TTHM formation was estimated by ranking the model regression coefficients. Site-specific models showed improved model performance statistics compared to a single model for the entire system most likely because the single model did not consider locational differences in the water treatment process. Although never out of compliance in 2011, the TTHM levels in the water supply increased following tropical storms Irene and Lee with 45% of the samples exceeding the 80 μg/L Maximum Contaminant Level (MCL) in October and November. This increase was explained by changes in water quality parameters, particularly by the increase in total organic carbon concentration and pH during this period.

  9. Formation and speciation characteristics of brominated trihalomethanes in seawater chlorination.

    PubMed

    Padhi, R K; Sowmya, M; Mohanty, A K; Bramha, S N; Satpathy, K K

    2012-11-01

    Formation character of brominated-trihalomethanes (Br-THMs) in chlorinated seawater and its dependence on applied chlorine dose, reaction time, and temperature were investigated in the laboratory. Seawater was collected from the east coast of India and a chlorine dose of 1, 3, 5, and 10 ppm was each applied at a temperature of 20, 30, and 40 degrees C to investigate the yield and kinetics of Br-THMs formation. Qualitative and quantitative estimation of THM formation at various intervals of time ranging from 5 min to 168 h was determined by a gas chromatograph equipped with an electron capture detector (GC-ECD). Chlorine dose, chlorine contact time, and reaction temperature positively affected the load of THMs. The ratio of chlorine dose to halogen incorporation decreased from 12% to 5% with increasing applied chlorine dose from 1 to 10 ppm. Significant levels of THMs were found to be formed within 0.5 h of reaction, followed by a very slow rate of formation. Elevated temperature favored both increased rate of formation and overall THM yield. The formation order of different trihalomethane species at all studied temperatures was observed to be bromodichloromethane (CHCl2Br) < dibromochloromethane (CHClBr2) < bromoform (CHBr3). Formation of chloroform was not observed, and bromoform was the dominant (96% to 98%) among the three THM species formed. PMID:23356015

  10. Investigation of trihalomethanes formation potential in Karoon River water, Iran.

    PubMed

    Fooladvand, Moradali; Ramavandi, Bahman; Zandi, Keyvan; Ardestani, Mojtaba

    2011-07-01

    Organic matters in raw water have a potential to generate harmful disinfection by-products such as trihalomethanes (THMs) during the chlorination process. The objectives of this study were to investigate the trihalomethane formation potential (THMFP) in Karoon River water and to determine the effect of several factors including total organic carbon (TOC), pH, chlorine dosage, water temperature, and seasonal variation. The results showed that, among all factors, TOC and water temperature have a remarkable effect on THMFP. The experimental results from batch studies indicated that increasing of pH value yielded a greater THMFP concentration for Karoon River water. THMFP levels of Karoon River water in summer times, when water temperature exceeded 26°C, were 1.2-1.6 times higher than in the spring and fall seasons, when water temperature was below 15°C. It was found that the measured THMFP at Karoon River water in the spring and fall seasons were very rarely higher than 100 μg/L. PMID:20824334

  11. FieldSpec: A field portable mass spectrometer prototype for high frequency measurements of δ (2) H and δ (18) O ratios in water

    NASA Astrophysics Data System (ADS)

    López Días, Veneranda; Quang Hoang, Hung; Martínez-Carreras, Núria; Barnich, François; Wirtz, Tom; Pfister, Laurent; McDonnell, Jeffrey

    2016-04-01

    Hydrological studies relying on stable water isotopes to better understand water sources, flowpaths and transit times are currently limited by the coarse temporal resolution of sampling and analysis protocols. At present, two kinds of lab-based instruments are used : (i) the standard isotope ratio mass spectrometers (IRMS) [1] and (ii) the laser-based instruments [2, 3]. In both cases, samples need to be collected in the field and then transferred to the laboratory for the water isotopic ratio measurements (even further complex sample preparation is required for the IRMS). Hence, past and ongoing research targets the development of field deployable instruments for measuring stable water isotopes at high temporal frequencies. While recent studies have demonstrated that laser-based instruments may be taken to the field [4, 5], their size and power consumption still restrict their use to sites equipped with mains power or generators. Here, we present progress on the development of a field portable mass spectrometer (FieldSpec) for direct high frequency measurements of δ2H and δ18O ratios in water. The FieldSpec instrument is based upon the use of a double focusing magnetic sector mass spectrometer in combination with an electron impact ion source and a membrane dual inlet system. The instrument directly collects liquid water samples in the field, which are then converted into water vapour before being injected into the mass spectrometer for the stable isotope analysis. δ2H and δ18O are derived from the measured mass spectra. All the components are arranged in a vacuum case having a suit case type dimension with portable electronics and battery. Proof-of-concept experiments have been carried out to characterize the instrument. The results show that the FieldSpec instrument has good linearity (R2 = 0.99). The reproducibility of the instrument ranges between 1 and 4 ‰ for δ2H and between 0.1 and 0.4 ‰ for δ18O isotopic ratio measurements. A measurement

  12. Field Test Report: NETL Portable Raman Gas Composition Monitor - Initial Industrial tests at NETL and General Electric (GE)

    SciTech Connect

    Michael, Buric; Jessica, Mullen; Steven, Woodruff; Ben, Chorpening

    2012-02-24

    NETL has developed new technology which enables the use of Raman spectroscopy in the real-time measurement of gas mixtures. This technology uses a hollow reflective metal-lined capillary waveguide as a gas sampling cell which contains the sample gas, and efficiently collects optical Raman scattering from the gas sample, for measurement with a miniature spectrometer. The result is an optical Raman “fingerprint” for each gas which is tens or hundreds of times larger than that which can be collected with conventional free-space optics. In this manner, the new technology exhibits a combination of measurement speed and accuracy which is unprecedented for spontaneous Raman measurements of gases. This makes the system especially well-suited to gas turbine engine control based on a-priori measurement of incoming fuel composition. The system has been developed to produce a measurement of all of the common components of natural gas, including the lesser nitrogen, oxygen, carbon-dioxide, and carbon monoxide diluents to better than 1% concentration accuracy each second. The objective of this task under CRADA 10-N100 was to evaluate the capability of a laser Raman capillary gas sensor for combustion fuels. A portable version of the Raman gas sensor, constructed at NETL, was used for field-trials conducted in a cooperative research effort at a GE facility. Testing under the CRADA was performed in 5 parts. Parts 1-4 were successful in testing of the Raman Gas Composition Monitor with bottled calibration gases, and in continuous monitoring of several gas streams at low pressure, in comparison with an online mass spectrometer. In part 5, the Raman Gas Composition Monitor was moved outdoors for testing with high pressure gas supplies. Some difficulties were encountered during industrial testing including the condensation of heavy hydrocarbons inside the sample cell (in part 5), communication with the GE data collection system, as well as some drift in the optical noise

  13. Evaluation and refinement of a field-portable drinking water toxicity sensor utilizing electric cell-substrate impedance sensing and a fluidic biochip.

    PubMed

    Widder, Mark W; Brennan, Linda M; Hanft, Elizabeth A; Schrock, Mary E; James, Ryan R; van der Schalie, William H

    2015-07-01

    The US Army's need for a reliable and field-portable drinking water toxicity sensor was the catalyst for the development and evaluation of an electric cell-substrate impedance sensing (ECIS) device. Water testing technologies currently available to soldiers in the field are analyte-specific and have limited capabilities to detect broad-based water toxicity. The ECIS sensor described here uses rainbow trout gill epithelial cells seeded on fluidic biochips to measure changes in impedance for the detection of possible chemical contamination of drinking water supplies. Chemicals selected for testing were chosen as representatives of a broad spectrum of toxic industrial compounds. Results of a US Environmental Protection Agency (USEPA)-sponsored evaluation of the field portable device were similar to previously published US Army testing results of a laboratory-based version of the same technology. Twelve of the 18 chemicals tested following USEPA Technology Testing and Evaluation Program procedures were detected by the ECIS sensor within 1 h at USEPA-derived human lethal concentrations. To simplify field-testing methods further, elimination of a procedural step that acclimated cells to serum-free media streamlined the test process with only a slight loss of chemical sensitivity. For field use, the ECIS sensor will be used in conjunction with an enzyme-based sensor that is responsive to carbamate and organophosphorus pesticides. PMID:25231170

  14. Ammonia-Oxidizing Bacteria in Biofilters Removing Trihalomethanes Are Related to Nitrosomonas oligotropha

    EPA Science Inventory

    Nitrifying biofilters degrading the four regulated trihalomethanes (THMs) trichloromethane (TCM), bromodichloromethane (BDCM), dibromochloromethane (DBCM), and tribromomethane (TBM) -were analyzed for the presence and activity of ammonia-oxidizing bacteria (AOB). Biofilter perfor...

  15. BROMIDE-OXIDANT INTERACTIONS AND THM (TRIHALOMETHANE) FORMATION: A LITERATURE REVIEW

    EPA Science Inventory

    The review focuses on the interactions, not only of bromide and chlorine, but also of bromide and two common oxidation alternatives to chlorine--chlorine dioxide and monochloramine. The data evaluations include discussions of reaction products, potentials for trihalomethane (THM)...

  16. COMETABOLISM OF TRIHALOMETHANES BY NITRIFYING BIOFILTERS UNDER DRINKING WATER TREATMENT PLANT CONDITIONS

    EPA Science Inventory

    EPA Identifier: FP916412
    Title: Cometabolism of Trihalomethanes by Nitrifying Biofilters Under Drinking Water Treatment Plant Conditions
    Fellow (Principal Investigator): David G. Wahman
    Institution: University of Texas at Austin
    EPA ...

  17. INFLUENCE OF EXPOSURE ASSESSMENT METHOD IN AN EPIDEMIOLOGIC STUDY OF TRIHALOMETHANE EXPOSURE AND SPONTANEOUS ABORTION

    EPA Science Inventory

    Trihalomethanes are common contaminants of chlorinated drinking water. Studies of their health effects have been hampered by exposure misclassification, due in part to limitations inherent in using utility sampling records. We used two exposure assessment methods, one based on ut...

  18. EXPOSURES AND INTERNAL DOSES OF TRIHALOMETHANES IN HUMANS: MULTI-ROUTE CONTRIBUTIONS FROM DRINKING WATER (FINAL)

    EPA Science Inventory

    The National Center for Environmental Assessment (NCEA) has released a final report that presents and applies a method to estimate distributions of internal concentrations of trihalomethanes (THMs) in humans resulting from a residential drinking water exposure. The report presen...

  19. Pyrosequencing Analysis of Bench-Scale Nitrifying BiofiltersRemoving Trihalomethanes

    EPA Science Inventory

    The bacterial biofilm communities in four nitrifying biofilters degrading regulated drinking water trihalomethanes were characterized by 454 pyrosequencing. The three most abundant phylotypes based on total diversity were Nitrosomonas (70%), Nitrobacter (14%), and Chitinophagace...

  20. THM (TRIHALOMETHANES) AND TOX (TOTAL ORGANIC HALOGEN) FORMATION: ROUTES, RATES, AND PRECURSORS

    EPA Science Inventory

    Oxidation and substitution are important mechanisms in the interaction between disinfectants and naturally occurring organics in water. Oxidation processes are responsible for the removal of organic compounds and precursors of trihalomethanes (THMs) and total organic halogen (TOX...

  1. DECOMPOSITION OF TRIHALOACETIC ACIDS AND FORMATION OF THE CORRESPONDING TRIHALOMETHANES IN DRINKING WATER. (R826834)

    EPA Science Inventory

    The decomposition of trihaloacetic acids [bromodichloroacetic acid (BDCAA), dibromochloroacetic acid (DBCAA), tribromoacetic acid (TBAA)], and the formation of the corresponding trihalomethanes [bromodichloromethane (BDCM), dibromochloromethane (DBCM), tribromomethane (TBM)] w...

  2. Reaction by-products from high energy electron irradiation of aqueous solutions of trihalomethanes

    SciTech Connect

    Cadavid, E.M.; Cooper, W.J.; Nickelsen, M.G. ); Kurucz, C.N.; Waite, T.D. )

    1990-01-01

    Trihalomethanes (THMs) are formed in water when chlorine is used for disinfection. The THMs of interest are chloroform, bromodichloromethane, chlorodibromomethane and bromoform. This study was undertaken to study the removal of the trihalomethanes using an innovative treatment technique, high energy electrons, for drinking water treatment. In addition to removal studies experiments were undertaken at low radiation doses to determine whether other chlorinated compounds are formed as reaction by-products.

  3. Screening for volatile organic compounds in soil and groundwater by use of a portable gas chromatograph during field investigations at an Air Force installation in Ohio

    USGS Publications Warehouse

    Parnell, James M.

    1995-01-01

    The use of the portable gas chromatograph for screening of soil and water samples in the field was part of the drilling program for the installation of monitoring wells for a basewide ground-water monitoring program at Wright-Patterson Air Force Base, Ohio. Selected soil and ground-water samples were screened in the field for volatile organic compounds to determine if contamination was present, to define the vertical and lateral extent of contamination, and to aid in the placement of the well screens for optimal interception of contaminants. This report describes the screening methods, sample-collection, quality-assurance/quality-control methods, and data-interpretation procedures necessary for screening of soil and ground-water samples in the field during the water resources investigations.

  4. A novel portable device to measure the temperature of both the inner and the outer tubes of a parabolic receiver in the field

    NASA Astrophysics Data System (ADS)

    Hermoso, J. L. Navarro; Espinosa-Rueda, Guillermo; Martinez, Noelia; Heras, Carlos; Osta, Marta

    2016-05-01

    The performance of parabolic trough (PT) receiver tubes (RT) has a direct impact on Solar Thermal Energy (STE) plant production. As a result, one major need of operation and maintenance (O&M) in STE plants is to monitor the state of the receiver tube as a key element in the solar field. However the lack of specific devices so far has limited the proper evaluation of operating receiver tubés thermal performance. As a consequence non-accurate approximations have been accepted until now using infrared thermal images of the glass outer tube. In order to fulfill this need, Abengoa has developed a unique portable device for evaluating the thermal performance and vacuum state of parabolic trough receiver tubes placed in the field. The novel device described in this paper, simultaneously provides the temperature of both the inner steel tube and the outer glass tube enabling a check on manufacturers specifications. The on-field evaluation of any receiver tube at any operating temperature has become possible thanks to this new measuring device. The features and usability of this new measurement system as a workable portable device in operating solar fields provide a very useful tool for all companies in the sector contributing to technology progress. The originality of the device, patent pending P201431969, is not limited to the CSP sector, also having scientific significance in the general measuring instruments field. This paper presents the work carried out to develop and validate the device, also detailing its functioning properties and including the excellent results obtained in the laboratory to determine its accuracy and standard deviation. This information was validated with data collected by O&M teams using this instrument in a commercial CSP plant. The relevance of the device has been evidenced by evaluating a wide sample of RT and the results are discussed in this paper. Finally, all the on field collected data is used to demonstrate the high impact that using

  5. Predictors of Blood Trihalomethane Concentrations in NHANES 1999–2006

    PubMed Central

    Dhingra, Radhika; Blount, Benjamin C.; Steenland, Kyle

    2014-01-01

    Background: Trihalomethanes (THMs) are water disinfection by-products that have been associated with bladder cancer and adverse birth outcomes. Four THMs (bromoform, chloroform, bromodichloromethane, dibromochloromethane) were measured in blood and tap water of U.S. adults in the National Health and Nutrition Examination Survey (NHANES) 1999–2006. THMs are metabolized to potentially toxic/mutagenic intermediates by cytochrome p450 (CYP) 2D6 and CYP2E1 enzymes. Objectives: We conducted exploratory analyses of blood THMs, including factors affecting CYP2D6 and CYP2E1 activity. Methods: We used weighted multivariable regressions to evaluate associations between blood THMs and water concentrations, survey year, and other factors potentially affecting THM exposure or metabolism (e.g., prescription medications, cruciferous vegetables, diabetes, fasting, pregnancy, swimming). Results: From 1999 to 2006, geometric mean blood and water THM levels dropped in parallel, with decreases of 32%–76% in blood and 38%–52% in water, likely resulting, in part, from the lowering of the total THM drinking water standard in 2002–2004. The strongest predictors of blood THM levels were survey year and water concentration (n = 4,232 total THM; n = 4,080 bromoform; n = 4,582 chloroform; n = 4,374 bromodichloromethane; n = 4,464 dibromochloromethane). We detected statistically significant inverse associations with diabetes and eating cruciferous vegetables in all but the bromoform model. Medications did not consistently predict blood levels. Afternoon/evening blood samples had lower THM concentrations than morning samples. In a subsample (n = 230), air chloroform better predicted blood chloroform than water chloroform, suggesting showering/bathing was a more important source than drinking. Conclusions: We identified several factors associated with blood THMs that may affect their metabolism. The potential health implications require further study. Citation: Riederer AM, Dhingra R

  6. Field application of the Numobag as a portable disposable isolation unit and for treating chemical, radiological or biologically induced wounds.

    SciTech Connect

    Miller, Keith A.; Felton, Robert; Vaughan, Courtenay Thomas

    2005-04-01

    Numotech Inc. has developed the Numobag{trademark}, a disposable, lightweight, wound healing device which produces Topical Hyperbaric Oxygen Therapy (THOT). The Numobag{trademark} is cost effective and has been clinically validated to heal large skin lesions rapidly and has proven to arrest wound advancement from several insidious forms of biological attack including dermal anthrax, small pox, necrotizing fasciitis etc. The Numobag{trademark} can treat mass casualties wounded by chemical/radiological burns or damaging biological exposures. The Numobag{trademark} can be a frontline tool as an isolation unit, reducing cross-contamination and infection of medical personnel. The heightened oxygen content kills organisms on the skin and in the wound, avoids expensive hospital trash disposal procedures, and helps the flesh heal. The Numobag{trademark} requires high purity oxygen. Numotech Inc. is teaming with Sandia National Laboratories and Spektr Conversion in Russia to develop a cost effective, portable, low power oxygen generator.

  7. Trihalomethane determination and removals from the main discharge channel of Konya City (Turkey).

    PubMed

    Ozdemir, C; Dursun, S

    2004-09-01

    Konya Main Discharge Channel is a very important environmental problem due to carrying the domestic waste water of Konya city centre as well as industrial waste water. Lowest flow rate of the channel was observed in October about 2 10(4) m3d(-1). In this period, channel water is not only waste water but includes more rain water coming from Gölyazi region. Discharge channel water can only reach to Tuz Lake for three months in a year. At other times of the year, water cannot reach the lake because of high evaporation, infiltration and usage of the water for irrigation. The land irrigated with the waste water tends to lose its productivity. In this study, water samples were collected and analysed from one hourly period for 2 days (24 x 2 = 48), daily period for 3 weeks (7 x 3 = 21) and monthly samples for a year (9 months). The samples were analysed as to whether these contained trihalomethanes or not, also results were compared with disinfection method that is used for drinking water, and samples were collected from ten different points on the channel. Pollution level of the channel water was controlled in accordance with the Turkish Water Pollution Control Law. In addition to trihalomethanes analysis, the effect of aeration on trihalomethanes was investigated. Collected samples (given above) were analysed for trihalomethanes compounds, and the relationship between disinfection type and dosage method on trihalomethanes formation was compared in this study. PMID:15515275

  8. Performance and biofilm activity of nitrifying biofilters removing trihalomethanes.

    PubMed

    Wahman, David G; Katz, Lynn E; Speitel, Gerald E

    2011-02-01

    Nitrifying biofilters seeded with three different mixed-culture sources removed trichloromethane (TCM) and dibromochloromethane (DBCM) with removals reaching 18% for TCM and 75% for DBCM. In addition, resuspended biofilm removed TCM, bromodichloromethane (BDCM), DBCM, and tribromomethane (TBM) in backwash batch kinetic tests, demonstrating that the biofilters contained organisms capable of biotransforming the four regulated trihalomethanes (THMs) commonly found in treated drinking water. Upon the initial and subsequent increased TCM addition, total ammonia nitrogen (TOTNH(3)) removal decreased and then reestablished, indicating an adjustment by the biofilm bacteria. In addition, changes in DBCM removal indicated a change in activity related to DBCM. The backwash batch kinetic tests provided a useful tool to evaluate the biofilm's bacteria. Based on these experiments, the biofilters contained bacteria with similar THM removal kinetics to those seen in previous batch kinetic experiments. Overall, performance or selection does not seem based specifically on nutrients, source water, or source cultures and most likely results from THM product toxicity, and the use of GAC media appeared to offer benefits over anthracite for biofilter stability and long-term performance, although the reasons for this advantage are not apparent based on research to date. PMID:21195446

  9. Removal of trihalomethane from chlorinated seawater using gamma radiation.

    PubMed

    Rajamohan, R; Natesan, Usha; Venugopalan, V P; Rajesh, Puspalata; Rangarajan, S

    2015-12-01

    Chlorine addition as a biocide in seawater results in the formation of chlorination by-products such as trihalomethanes (THMs). Removal of THMs is of importance as they are potential mutagenic and carcinogenic agents. In this context, a study was conducted that used ionizing radiation to remove THMs from chlorinated (1, 3, and 5 mg/L) seawater by applying various dosages (0.4-5.0 kGy) of gamma radiation. Bromoform (BF) showed a faster rate of degradation as compared to other halocarbons such as bromodichloromethane (BDCM) and dibromochloromethane (DBCM). In chlorine-dosed seawater, total irradiation dose of 0.4 to 5 kGy caused percentage reduction in the range of 6.9 to 76.7%, 2.3 to 99.6%, and 45.7 to 98.3% for BDCM, DBCM, and BF, respectively. During the irradiation process, pH of the chlorinated seawater decreased with increase in the absorbed dose; however, no change in total organic carbon (TOC) was observed. The results show that gamma dose of 2.5 kGy was adequate for maximum degradation of THM; but for complete mineralization, higher dose would be required. PMID:26199004

  10. Portable shift register

    SciTech Connect

    Halbig, J.K.; Bourret, S.C.; Hansen, W.J.; Hicks, D.V.; Klosterbuer, S.F.; Krick, M.S.

    1994-01-01

    An electronics package for a small, battery-operated, self-contained, neutron coincidence counter based on a portable shift-register (PSR) has been developed. The counter was developed for applications not adequately addressed by commercial packages, including in-plant measurements to demonstrate compliance with regulations (domestic and international), in-plant process control, and in-field measurements (environmental monitoring or safeguards). Our package's features, which address these applications, include the following: Small size for portability and ease of installation;battery or mains operation; a built-in battery to power the unit and a typical detector such as a small sample counter, for over 6 h if power lines are bad or noisy, if there is a temporary absence of power, or if portability is desired; complete support, including bias, for standard neutron detectors; a powerful communications package to easily facilitate robust external control over a serial port; and a C-library to simplify creating external control programs in computers or other controllers. Whereas the PSR specifically addresses the applications mentioned above, it also performs all the measurements made by previous electronics packages for neutron coincidence counters developed at Los Alamos and commercialized. The PSR electronics package, exclusive of carrying handle, is 8 by 10 by 20 cm; it contains the circuit boards, battery, and bias supply and weighs less than 2 kg. This instrument package is the second in an emerging family of portable measurement instruments being developed; the first was the Miniature and Modular Multichannel Analyzer (M[sup 3]CA). The PSR makes extensive use of hardware and software developed for the M[sup 3]CA; like the M[sup 3]CA, it is intended primarily for use with an external controller interfaced over a serial channel.

  11. Evaluation of a Field-Portable DNA Microarray Platform and Nucleic Acid Amplification Strategies for the Detection of Arboviruses, Arthropods, and Bloodmeals

    PubMed Central

    Grubaugh, Nathan D.; Petz, Lawrence N.; Melanson, Vanessa R.; McMenamy, Scott S.; Turell, Michael J.; Long, Lewis S.; Pisarcik, Sarah E.; Kengluecha, Ampornpan; Jaichapor, Boonsong; O'Guinn, Monica L.; Lee, John S.

    2013-01-01

    Highly multiplexed assays, such as microarrays, can benefit arbovirus surveillance by allowing researchers to screen for hundreds of targets at once. We evaluated amplification strategies and the practicality of a portable DNA microarray platform to analyze virus-infected mosquitoes. The prototype microarray design used here targeted the non-structural protein 5, ribosomal RNA, and cytochrome b genes for the detection of flaviviruses, mosquitoes, and bloodmeals, respectively. We identified 13 of 14 flaviviruses from virus inoculated mosquitoes and cultured cells. Additionally, we differentiated between four mosquito genera and eight whole blood samples. The microarray platform was field evaluated in Thailand and successfully identified flaviviruses (Culex flavivirus, dengue-3, and Japanese encephalitis viruses), differentiated between mosquito genera (Aedes, Armigeres, Culex, and Mansonia), and detected mammalian bloodmeals (human and dog). We showed that the microarray platform and amplification strategies described here can be used to discern specific information on a wide variety of viruses and their vectors. PMID:23249687

  12. Rapid determination of ETS markers with a prototype field-portable GC employing a microsensor array detector.

    PubMed

    Zhong, Qiongyan; Veeneman, Rebecca A; Steinecker, William H; Jia, Chunrong; Batterman, Stuart A; Zellers, Edward T

    2007-05-01

    The adaptation of a portable gas chromatograph (GC) prototype with several unique design features to the determination of vapor-phase markers of environmental tobacco smoke (ETS) is described. This instrument employs a dual-stage adsorbent preconcentrator, two series-coupled separation columns that can be independently temperature programmed, and a detector consisting of an array of nanoparticle-coated chemiresistors, whose response patterns are used together with retention times for vapor recognition. An adsorbent pre-trap was developed to remove semi-volatile organics from the sample stream. Conditions were established to quantitatively capture two ETS markers, 2,5-dimethylfuran (2,5-DMF) and 4-ethenylpyridine (4-EP, as a surrogate for 3-EP), and to separate them from the 34 most prominent co-contaminants present in ETS using ambient air as the carrier gas. A complete analysis can be performed every 15 min. Projected detection limits are 0.58 and 0.08 ppb for 2,5-DMF and 4-EP, respectively, assuming a 1 L sample volume, which are sufficiently low to determine these markers in typical smoking-permitted environments. PMID:17492089

  13. Characteristics of the SAR distributions in a head exposed to electromagnetic fields radiated by a hand-held portable radio

    SciTech Connect

    Watanabe, Soichi; Taki, Masao; Nojima, Toshio; Fujiwara, Osamu

    1996-10-01

    This paper presents characteristics of the specific absorption rate (SAR) distributions calculated by the finite-difference time-domain (FDTD) method using a heterogeneous and realistic head model and a realistic hand-held portable radio model. The difference between the SAR distributions produced by a 1/4-wavelength monopole antenna and those produced by a 1/2-wavelength dipole antenna is investigated. The dependence of the maximum local SAR on the distance d{sub a} between the auricle of the head and the antenna of the radio is evaluated. It is shown that the maximum local SAR decreases as the antenna length extends from 1/4 to 1/2 of the wavelength. The maximum local SAR`s in a head model with auricles are larger than those in one without auricles. The dependence of the SAR on the electrical inhomogeneity of the tissues in the head model is not significant with regard to the surface distribution and the maximum local SAR when the radio is near the head. It is also shown that the maximum local SAR is not strongly dependent on the position of the hand when the hand does not shade the antenna. Furthermore, the SAR`s experimentally measured in a homogeneous head phantom are compared with the calculated SAR`s.

  14. Technical Report for Water Circulation Pumping System for Trihalomethanes (THMs)

    SciTech Connect

    Bellah, W.

    2015-06-08

    The TSWWS was added as an active source of supply to the permit (No. 03-10-13P-003) in 2010, but has never been used due to the potential for formation of trihalomethanes (THMs) in the distribution system. THMs are formed as a by-product when chlorine is used to disinfect water for drinking. THMs are a group of chemicals generally referred to as disinfection by-products (DBPs). THMs result from the reaction of chlorine with organic matter that is present in the water. Some of the THMs are volatile and may easily vaporize into the air. This fact forms the basis of the design of the system discussed in this technical report. In addition, the design is based on the results of a study that has shown success using aeration as a means to reduce TTHMs to within allowable concentration levels with turn-over times as long as ten days. The Primary Drinking Water Standards of Regulated Contaminants Maximum Contaminant Level (MCL) for TTHMs is 80 parts per billion (ppb). No other changes to the existing drinking water distribution system and chlorination operations are anticipated before switching to the TSWWS as the primary drinking water source. The two groundwater wells (Wells 20 and 18) which are currently the primary and backup water sources for the system would be maintained for use as backup supply. In the future, one of the wells may be removed from the system. A permit amendment would be filed at that time if this modification was deemed appropriate.

  15. Trihalomethane hydrolysis in drinking water at elevated temperatures.

    PubMed

    Zhang, Xiao-Lu; Yang, Hong-Wei; Wang, Xiao-Mao; Karanfil, Tanju; Xie, Yuefeng F

    2015-07-01

    Hydrolysis could contribute to the loss of trihalomethanes (THMs) in the drinking water at elevated temperatures. This study was aimed at investigating THM hydrolysis pertaining to the storage of hot boiled water in enclosed containers. The water pH value was in the range of 6.1-8.2 and the water temperature was varied from 65 to 95 °C. The effects of halide ions, natural organic matter, and drinking water matrix were investigated. Results showed that the hydrolysis rates declined in the order following CHBrCl2 > CHBr2Cl > CHBr3 > CHCl3. THM hydrolysis was primarily through the alkaline pathway, except for CHCl3 in water at relatively low pH value. The activation energies for the alkaline hydrolysis of CHCl3, CHBrCl2, CHBr2Cl and CHBr3 were 109, 113, 115 and 116 kJ/mol, respectively. No hydrolysis intermediates could accumulate in the water. The natural organic matter, and probably other constituents, in drinking water could substantially decrease THM hydrolysis rates by more than 50%. When a drinking water was at 90 °C or above, the first order rate constants for THM hydrolysis were in the magnitude of 10(-2)‒10(-1) 1/h. When the boiled real tap water was stored in an enclosed container, THMs continued increasing during the first few hours and then kept decreasing later on due to the competition between hydrolysis and further formation. The removal of THMs, especially brominated THMs, by hydrolysis would greatly reduce one's exposure to disinfection by-products by consuming the boiled water stored in enclosed containers. PMID:25898249

  16. Exogenous and Endogenous Determinants of Blood Trihalomethane Levels after Showering

    PubMed Central

    Backer, Lorraine C.; Lan, Qing; Blount, Benjamin C.; Nuckols, J.R.; Branch, Robert; Lyu, Christopher W.; Kieszak, Stephanie M.; Brinkman, Marielle C.; Gordon, Sydney M.; Flanders, W. Dana; Romkes, Marjorie; Cantor, Kenneth P.

    2008-01-01

    Background We previously conducted a study to assess whether household exposures to tap water increased an individual’s internal dose of trihalomethanes (THMs). Increases in blood THM levels among subjects who showered or bathed were variable, with increased levels tending to cluster in two groups. Objectives Our goal was to assess the importance of personal characteristics, previous exposures, genetic polymorphisms, and environmental exposures in determining THM concentrations in blood after showering. Methods One hundred study participants completed a health symptom questionnaire, a 48-hr food and water consumption diary, and took a 10-min shower in a controlled setting. We examined THM levels in blood samples collected at baseline and 10 and 30 min after the shower. We assessed the significance of personal characteristics, previous exposures to THMs, and specific gene polymorphisms in predicting postshower blood THM concentrations. Results We did not observe the clustering of blood THM concentrations observed in our earlier study. We found that environmental THM concentrations were important predictors of blood THM concentrations immediately after showering. For example, the chloroform concentration in the shower stall air was the most important predictor of blood chloroform levels 10 min after the shower (p < 0.001). Personal characteristics, previous exposures to THMs, and specific polymorphisms in CYP2D6 and GSTT1 genes were significant predictors of both baseline and postshowering blood THM concentrations as well as of changes in THM concentrations associated with showering. Conclusion The inclusion of information about individual physiologic characteristics and environmental measurements would be valuable in future studies to assess human health effects from exposures to THMs in tap water. PMID:18197300

  17. Developments and field tests of low-frequency portable acoustic transducers for a mobile exploration and time lapse experiment of a sea-bottom reservoir

    NASA Astrophysics Data System (ADS)

    Tsuruga, K.; Kasahara, J.; Hasada, Y.; Kondo, H.

    2013-12-01

    Depth, scale and resolutions of geophysical explorations for mineral resources are controlled by transmitted seismic energy and wavelength (frequency range). Most explorations in marine have been conducted by survey ship system with arrayed acoustic sources whose dominant frequency range is about 10 to 500 Hz. On the other hand, for shallow parts of sea bottom structure survey, some sub-bottom profilers with frequency range around 3.5kHz are used. To monitor a time lapse of a sea bottom reservoir such as an oil, gas, or methane hydrate reservoir as well as to exploit a mobile survey near a sea bottom by AUVs, it is necessary to use a broadband portable acoustic transducer with a dominant frequency range of 500 Hz to 5 kHz. We have been developing several types of portable acoustic transducers and a transmitting and recording system which is accurately controlled by a GPS clock (Tsuruga et al., 2012). In this pater, we report the new broadband acoustic portable transducers which have larger power than the original cylindrical acoustic transducers in a low frequency range (<5 kHz), partly funded by JOGMEC, and show the preliminary results of field tests at the shallow sea bottom around 32 m deep by means of the transducers and hydrophone receivers array. Each transducer repeatedly transmitted Chirp signals with a unit period of 500 msec in two frequency ranges of 0.5k-4.5kHz and 4k-16kHz . We stacked 500-ms data by 28 times to obtain a transfer function of each source-receiver pair in the time and frequency domains. The preliminary results suggest as the follows: (i) it is successful to broaden the frequency bandwidth (i.e., 2k-10kHz) by extending a geometrical resonance length of a cylindrical acoustic transducers, and (ii) the observation at the sea bottom with accurately controlled timing systems of transmitter and data-logger is very useful to identify the stable and/or unstable seismic phases, that is, waves propagating in a underground and/or in a sea water as

  18. Exploring the Integration of Field Portable Instrumentation into Real-Time Surface Science Operations with the RIS4E SSERVI Team

    NASA Astrophysics Data System (ADS)

    Young, K. E.; Bleacher, J. E.; Rogers, D.; Garry, W. B.; McAdam, A.; Scheidt, S. P.; Carter, L. M.; Glotch, T. D.

    2015-12-01

    The Remote, In Situ, and Synchrotron Studies for Science (RIS4E) team represents one node of the Solar System Exploration Research Virtual Institute (SSERVI) program. While the RIS4E team consists of four themes, each dedicated to a different aspect of airless body exploration, this submission details the RIS4E work underway to maximize an astronaut's effectiveness while conducting surface science. The next generation of surface science operations will look quite different than the EVAs (extravehicular activities) conducted during Apollo. Astronauts will possess data of much higher resolution than the Apollo reconnaissance data, and the EVAs will thus be designed to answer targeted science questions. Additionally, technological advancements over the last several decades have made it possible to conduct in situ analyses of a caliber much greater than was achievable during Apollo. For example, lab techniques such as x-ray fluorescence, x-ray diffraction, and multi-spectral imaging are now available in field portable formats, meaning that astronauts can gain real-time geochemical awareness during sample collection. The integration of these instruments into EVA operations, however, has not been widely tested. While these instruments will provide the astronaut with a high-resolution look at regional geochemistry and structure, their implementation could prove costly to the already constrained astronaut EVA timeline. The RIS4E team, through fieldwork at the December 1974 lava flow at Kilauea Volcano, HI, investigates the incorporation of portable technologies into planetary surface exploration and explores the relationship between science value added from these instruments and the cost associated with integrating them into an EVA timeline. We also consider what an appropriate instrumentation suite would be for the exploration of a volcanic terrain using this ideal terrestrial analog (see Rogers et al., Young et al., Bleacher et al., and Yant et al., this meeting).

  19. U.S.-MEXICO BORDER PROGRAM ARIZONA BORDER STUDY--STANDARD OPERATING PROCEDURE FOR OPERATION, CALIBRATION, AND ROUTINE USE OF THE SPECTRACE 9000 FIELD PORTABLE X-RAY FLUORESCENCE ANALYZER (UA-L-10.1)

    EPA Science Inventory

    The purpose of this SOP is to describe the procedures for operating and calibrating the Spectrace 9000 field portable X-ray fluorescence analyzer. This procedure applies to the determination of metal concentrations in samples during the Arizona NHEXAS project and the Border stud...

  20. NHEXAS PHASE I ARIZONA STUDY--STANDARD OPERATING PROCEDURE FOR OPERATION, CALIBRATION AND ROUTINE USE OF THE SPECTRACE 9000 FIELD PORTABLE X-RAY FLUORESCENCE ANALYZER (UA-L-10.1)

    EPA Science Inventory

    The purpose of this SOP is to describe the procedures for operating and calibrating the Spectrace 9000 field portable X-ray fluorescence analyzer. This procedure applies to the determination of metal concentrations in samples during the Arizona NHEXAS project and the "Border" st...

  1. Development of a Portable Field Imaging Spectrometer: Application for the Identification of Sun-Dried and Sulfur-Fumigated Chinese Herbals.

    PubMed

    Zhang, Hongming; Wu, Taixia; Zhang, Lifu; Zhang, Peng

    2016-05-01

    We fabricated a visible-near-infrared (Vis-NIR) portable field imaging spectrometer with a prism-grating-prism element and a scanning mirror. The developed Vis-NIR imaging spectrometer, consisting of an INFINITY 3-1 detector and a V10E spectrometer from Specim Corporation, is designed to measure the spectral range between 0.4 and 1 µm with spectral resolution of 2-4 nm. In recent years, sulfur fumigation has been abused during the processing of certain freshly harvested Chinese herbs. Fourier transform infrared spectroscopy, fiber optic NIR spectrometry, and liquid chromatography-mass spectrometry are typically used to analyze the chemical profiles of sulfur-fumigated and sun-dried Chinese herbs. Field imaging spectrometry is rarely used to identify sulfur-fumigated herbs. In this study, field imaging spectrometry, principal component analysis, and the partial least squares-discriminant analysis multivariate data analysis method are used to distinguish sun-dried and sulfur-fumigated Chinese medicinal herbs with a sensitivity of 96.4% and a specificity of 98.3% for RPA identification. These results suggest that hyperspectral imaging is a potential technique to control medicine quality for medical applications. PMID:27006019

  2. Portable Technology Comes of Age

    ERIC Educational Resources Information Center

    Wangemann, Paul; Lewis, Nina; Squires, David A.

    2003-01-01

    The PDA was originally conceived of as a portable handheld electronic device that provided a user with a tool to organize his or her life through easy access to a personal calendar, daily planner, and address book. Over the years, these devices have expanded to include many new functions, which have helped more applications in diverse fields. This…

  3. REDUCTION OF INGESTION EXPOSURE TO TRIHALOMETHANES DUE TO VOLATILIZATION. (R825362)

    EPA Science Inventory

    Ingestion of tap water is one of the principal exposure
    pathways for disinfection byproducts (DBPs). One major
    class of DBPs, trihalomethanes (THM), are highly volatile,
    and volatilization will tend to lower ingestion exposures.
    This study quantifies volatilization...

  4. ANALYSIS OF IN VITRO AND IN VIVO DNA STRAND BREAKS INDUCED BY TRIHALOMETHANES (THMS)

    EPA Science Inventory

    Analysis of In Vitro and In Vivo DNA Strand Breaks Induced by Trihalomethanes (TRMs)

    The THMs are the most widely distributed and the most concentrated of the cWorine disinfection by-products (D BPs) found in finished drinking water. All of the THMs, cWoroform (CHCI3), br...

  5. ANALYSIS OF IN VIVO AND IN VITRO DNA STRAND BREAKS FROM TRIHALOMETHANE EXPOSURE

    EPA Science Inventory

    Abstract
    Background: Epidemiological studies have linked the consumption of chlorinated surface waters to an increased risk of two major causes of human mortality, colorectal and bladder cancer. Trihalomethanes (THMs) are by-products formed when chlorine is used to disinfect d...

  6. JOURNAL ARTICLE: ANALYSIS OF IN VIVO AND IN VITRO DNA STRAND BREAKS FROM TRIHALOMETHANE EXPOSURE

    EPA Science Inventory

    Epidemiological studies have linked the consumption of chlorinated surface waters to an increased risk of two major causes of human mortality, colorectal and bladder cancer. Trihalomethanes (THMs) are by-products formed when chlorine is used to disinfect drinking water. The pur...

  7. INDUCTION OF DNA STRAND BREAKS BY TRIHALOMETHANES IN PRIMARY HUMAN LUNG EPITHELIAL CELLS

    EPA Science Inventory


    Abstract

    Trihalomethanes (TEMs) are disinfection by-products and suspected human carcinogens present in chlorinated drinking water. Previous studies have shown that many THMs induce sister chromatid exchanges and DNA strand breaks in human peripheral blood lymphocyte...

  8. ENTERIC VIRUS AND INDICATOR BACTERIA LEVELS IN A WATER TREATMENT SYSTEM MODIFIED TO REDUCE TRIHALOMETHANE PRODUCTION

    EPA Science Inventory

    A drinking water treatment plant with high concentrations of trihalomethanes (THMs) in its finished water and large numbers of viruses in its source water was located. This plant was used to study the effect of an alteration in the point of chlorination from the first to last ste...

  9. TIME TO PREGNANCY IN RELATION TO TOTAL TRIHALOMETHANE LEVELS IN TAP WATER

    EPA Science Inventory

    Time to pregnancy in relation to total trihalomethane levels in tap water
    Shanna H. Swan, Cuirong Ren, Gayle C. Windham, Laura Fenster, Kirsten Waller. (University of Missouri and California Department of Health Services).

    We have previously reported increased risks o...

  10. 40 CFR 142.60 - Variances from the maximum contaminant level for total trihalomethanes.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 23 2011-07-01 2011-07-01 false Variances from the maximum contaminant level for total trihalomethanes. 142.60 Section 142.60 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS (CONTINUED) NATIONAL PRIMARY DRINKING WATER REGULATIONS IMPLEMENTATION Identification of Best...

  11. 40 CFR 142.60 - Variances from the maximum contaminant level for total trihalomethanes.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 22 2010-07-01 2010-07-01 false Variances from the maximum contaminant level for total trihalomethanes. 142.60 Section 142.60 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS (CONTINUED) NATIONAL PRIMARY DRINKING WATER REGULATIONS IMPLEMENTATION Identification of Best...

  12. 40 CFR 142.60 - Variances from the maximum contaminant level for total trihalomethanes.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 24 2012-07-01 2012-07-01 false Variances from the maximum contaminant level for total trihalomethanes. 142.60 Section 142.60 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) WATER PROGRAMS (CONTINUED) NATIONAL PRIMARY DRINKING WATER REGULATIONS IMPLEMENTATION Identification of Best...

  13. COST AND PERFORMANCE EVALUATION OF IN-PLANT TRIHALOMETHANE CONTROL TECHNIQUES

    EPA Science Inventory

    Bench-, pilot-, or full-scale studies were conducted to evaluate the cost and performance of selected treatment technologies for reducing trihalomethane concentrations in drinking water. The four Florida plant sites that were selected for study used highly organic surface or grou...

  14. Assessment of Preparation of Samples Under the Field Conditions and a Portable Real-Time RT-PCR Assay for the Rapid On-Site Detection of Newcastle Disease Virus.

    PubMed

    Liu, L; Benyeda, Z; Zohari, S; Yacoub, A; Isaksson, M; Leijon, M; LeBlanc, N; Benyeda, J; Belák, S

    2016-04-01

    Newcastle disease virus (NDV), also known as virulent forms of avian paramyxovirus serotype 1 (AMPV-1), is the causative agent of Newcastle disease affecting many species of birds and causing heavy losses to the poultry industry worldwide. Early, rapid and sensitive detection of the viruses or the viral nucleic acids is very important for disease diagnosis and control. This study aimed to evaluate sample preparation under field conditions and the application of a real-time RT-PCR method in the portable T-COR4 platform for the rapid, on-site detection of NDV on a farm. In the laboratory setting, the portable real-time RT-PCR assay had a similar performance compared with that obtained with a larger, stationary Rotor Gene real-time thermocycler. In the field conditions, viral nucleic acids were manually extracted just outside of animal units with minimal equipment and real-time RT-PCR detection was performed with the portable thermocycler T-COR4 placed in a nearby room. The portable assay at the farm detected viral RNA in 15 samples and reached an agreement of 83% (39/47) when the same RNA preparations were tested in the Rotor Gene thermocycler under the laboratory setting. The results demonstrated the feasibility of performing field detection but also the need to improve and further simplify sample preparation procedures. PMID:25209697

  15. Portable MRI

    SciTech Connect

    Espy, Michelle A.

    2012-06-29

    This project proposes to: (1) provide the power of MRI to situations where it presently isn't available; (2) perform the engineering required to move from lab to a functional prototype; and (3) leverage significant existing infrastructure and capability in ultra-low field MRI. The reasons for doing this: (1) MRI is the most powerful tool for imaging soft-tissue (e.g. brain); (2) Billions don't have access due to cost or safety issues; (3) metal will heat/move in high magnetic fields; (4) Millions of cases of traumatic brain injury in US alone; (5) even more of non-traumatic brain injury; (6) (e.g. stroke, infection, chemical exposure); (7) Need for early diagnostic; (8) 'Signature' wound of recent conflicts; (9) 22% of injuries; (10) Implications for post-traumatic stress disorder; and (11) chronic traumatic encephalopathy.

  16. Carbon isotopic constraints on the contribution of plant material to the natural precursors of trihalomethanes

    USGS Publications Warehouse

    Bergamaschi, B.A.; Fram, M.S.; Kendall, C.; Silva, S.R.; Aiken, G.R.; Fujii, R.

    1999-01-01

    The ??13C values of individual trihalomethanes (THM) formed on reaction of chlorine with dissolved organic carbon (DOC) leached from maize (corn, Zea maize L) and Scirpus acutus (an aquatic bulrush), and with DOC extracted from agricultural drainage waters were determined using purge and trap introduction into a gas chromatograph-combustion-isotope ratio monitoring mass spectrometer. We observed a 1-6.8??? difference between the ??13C values of THM produced from the maize and Scirpus leachates, similar to the isotopic difference between the whole plant materials. Both maize and Scirpus formed THM 12??? lower in 13C than whole plant material. We suggest that the low value of the THM relative to the whole plant material is evidence of distinct pools of THM-forming DOC, representing different biochemical types or chemical structures, and possessing different environmental reactivity Humic extracts of waters draining an agricultural field containing Scirpus peat soils and planted with maize formed THM with isotopic values intermediate between those of maize and Scirpus leachates, indicating maize may contribute significantly to the THM-forming DOC. The difference between the ??13C values of the whole isolate and that of the THM it yielded was 3 9???, however, suggesting diagenesis plays a role in determining the ??13C value of THM-forming DOC in the drainage waters, and precluding the direct use of isotopic mixing models to quantitatively attribute sources.The ??13C values of individual trihalomethanes (THM) formed on reaction of chlorine with dissolved organic carbon (DOC) leached from maize (corn; Zea maize L.) and Scirpus acutus (an aquatic bulrush), and with DOC extracted from agricultural drainage waters were determined using purge and trap introduction into a gas chromatograph-combustion-isotope ratio monitoring mass spectrometer. We observed a 16.8qq difference between the ??13C values of THM produced from the maize and Scirpus leachates, similar to the isotopic

  17. Quantification of trace arsenic in soils by field-portable X-ray fluorescence spectrometry: considerations for sample preparation and measurement conditions.

    PubMed

    Parsons, Chris; Margui Grabulosa, Eva; Pili, Eric; Floor, Geerke H; Roman-Ross, Gabriela; Charlet, Laurent

    2013-11-15

    Recent technological improvements have led to the widespread adoption of field portable energy dispersive X-ray fluorescence (FP-XRF) by governmental agencies, environmental consultancies and research institutions. FP-XRF units often include analysis modes specifically designed for the quantification of trace elements in soils. Using these modes, X-ray tube based FP-XRF units can offer almost "point and shoot" ease of use and results comparable to those of laboratory based instruments. Nevertheless, FP-XRF analysis is sensitive to spectral interferences as well as physical and chemical matrix effects which can result in decreased precision and accuracy. In this study, an X-ray tube-based FP-XRF analyser was used to determine trace (low ppm) concentrations of As in a floodplain soil. The effect of different sample preparation and analysis conditions on precision and accuracy were systematically evaluated. We propose strategies to minimise sources of error and maximise data precision and accuracy, achieving in situ limits of detection and precision of 6.8 ppm and 14.4%RSD, respectively for arsenic. We demonstrate that soil moisture, even in relatively dry soils, dramatically affects analytical performance with a signal loss of 37% recorded for arsenic at 20 wt% soil moisture relative to dry soil. We also highlight the importance of the use of certified reference materials and independent measurement methods to ensure accurate correction of field values. PMID:22819961

  18. A portable x-ray source with a nanostructured Pt-coated silicon field emission cathode for absorption imaging of low-Z materials

    NASA Astrophysics Data System (ADS)

    Basu, Anirban; Swanwick, Michael E.; Fomani, Arash A.; Velásquez-García, Luis Fernando

    2015-06-01

    We report the design, fabrication, and characterization of a portable x-ray generator for imaging of low-atomic number materials such as biological soft tissue. The system uses a self-aligned, gated, Pt-coated silicon field emitter cathode with two arrays of 62 500 nano-sharp tips arranged in a square grid with 10 μm emitter pitch, and a natural convection-cooled reflection anode composed of a Cu bar coated with a thin Mo film. Characterization of the field emitter array demonstrated continuous emission of 1 mA electron current (16 mA cm  -  2) with  >95% current transmission at a 150 V gate-emitter bias voltage for over 20 h with no degradation. The emission of the x-ray source was characterized across a range of anode bias voltages to maximize the fraction of photons from the characteristic K-shell peaks of the Mo film to produce a quasi-monochromatic photon beam, which enables capturing high-contrast images of low-atomic number materials. The x-ray source operating at the optimum anode bias voltage, i.e. 35 kV, was used to image ex vivo and nonorganic samples in x-ray fluoroscopic mode while varying the tube current; the images resolve feature sizes as small as ~160 µm.

  19. Portable data acquisition system

    SciTech Connect

    Bowers, J; Rogers, H

    1999-05-03

    Lawrence Livermore National Laboratory (LLNL) has developed a Portable Data Acquisition (DAQ) System that is basically a laboratory-scale of Program Logic Control (PLC). This DAQ system can obtain signals from numerous sensors (e.g., pH, level, pressure, flow meters), open and close valves, and turn on and off pumps. The data can then be saved on a spreadsheet or displayed as a graph/indicator in real-time on a computer screen. The whole DAQ system was designed to be portable so that it could sit on a bench top during laboratory-scale treatability studies, or moved out into the field during larger studies. This DAQ system is also fairly simple to use. All that is required is some working knowledge of LabVIEW 4.1, and how to properly wire the process equipment. The DAQ system has been used during treatability studies on cesium precipitation, controlled hydrolysis of water- reactive wastes, and other waste treatment studies that enable LLNL to comply with the Federal Facility Compliance Act (FFCAct). Improved data acquisition allows the study to be better monitored, and therefore better controlled, and can be used to determine the results of the treatment study more effectively. This also contributes to the design of larger treatment processes.

  20. Portable waveguide display system with a large field of view by integrating freeform elements and volume holograms

    PubMed Central

    Han, Jian; Liu, Juan; Yao, Xincheng; Wang, Yongtian

    2015-01-01

    A compact waveguide display system integrating freeform elements and volume holograms is presented here for the first time. The use of freeform elements can broaden the field of view, which limits the applications of a holographic waveguide. An optimized system can achieve a diagonal field of view of 45° when the thickness of the waveguide planar is 3mm. Freeform-elements in-coupler and the volume holograms out-coupler were designed in detail in our study, and the influence of grating configurations on diffraction efficiency was analyzed thoroughly. The off-axis aberrations were well compensated by the in-coupler and the diffraction efficiency of the optimized waveguide display system could reach 87.57%. With integrated design, stability and reliability of this monochromatic display system were achieved and the alignment of the system was easily controlled by the record of the volume holograms, which makes mass production possible. PMID:25836207

  1. A portable automated system for trace gas sampling in the field and stable isotope analysis in the laboratory.

    PubMed

    Theis, Daniel E; Saurer, Matthias; Blum, Herbert; Frossard, Emmanuel; Siegwolf, Rolf T W

    2004-01-01

    A computer-controllable mobile system is presented which enables the automatic collection of 33 air samples in the field and the subsequent analysis for delta13C and delta18O stable isotope ratios of a carbon-containing trace gas in the laboratory, e.g. CO2, CO or CH4. The system includes a manifold gas source input for profile sampling and an infrared gas analyzer for in situ CO2 concentration measurements. Measurements of delta13C and delta18O of all 33 samples can run unattended and take less than six hours for CO2. Laboratory tests with three gases (compressed air with different pCO2 and stable isotope compositions) showed a measurement precision of 0.03 per thousand for delta13C and 0.02 per thousand for delta18O of CO2 (standard error (SE), n = 11). A field test of our system, in which 66 air samples were collected within a 24-hour period above grassland, showed a correlation of 0.99 (r2) between the inverse of pCO2 and delta13C of CO2. Storage of samples until analysis is possible for about 1 week; this can be an important factor for sampling in remote areas. A wider range of applications in the field is open with our system, since sampling and analysis of CO and CH4 for stable isotope composition is also possible. Samples of compressed air had a measurement precision (SE, n = 33) of 0.03 per thousand for delta13C and of 0.04 per thousand for delta18O on CO and of 0.07 per thousand for delta13C on CH4. Our system should therefore further facilitate research of trace gases in the context of the carbon cycle in the field, and opens many other possible applications with carbon- and possibly non-carbon-containing trace gases. PMID:15317047

  2. Feasibility Study on a Portable Field Pest Classification System Design Based on DSP and 3G Wireless Communication Technology

    PubMed Central

    Han, Ruizhen; He, Yong; Liu, Fei

    2012-01-01

    This paper presents a feasibility study on a real-time in field pest classification system design based on Blackfin DSP and 3G wireless communication technology. This prototype system is composed of remote on-line classification platform (ROCP), which uses a digital signal processor (DSP) as a core CPU, and a host control platform (HCP). The ROCP is in charge of acquiring the pest image, extracting image features and detecting the class of pest using an Artificial Neural Network (ANN) classifier. It sends the image data, which is encoded using JPEG 2000 in DSP, to the HCP through the 3G network at the same time for further identification. The image transmission and communication are accomplished using 3G technology. Our system transmits the data via a commercial base station. The system can work properly based on the effective coverage of base stations, no matter the distance from the ROCP to the HCP. In the HCP, the image data is decoded and the pest image displayed in real-time for further identification. Authentication and performance tests of the prototype system were conducted. The authentication test showed that the image data were transmitted correctly. Based on the performance test results on six classes of pests, the average accuracy is 82%. Considering the different live pests’ pose and different field lighting conditions, the result is satisfactory. The proposed technique is well suited for implementation in field pest classification on-line for precision agriculture. PMID:22736996

  3. Feasibility study on a portable field pest classification system design based on DSP and 3G wireless communication technology.

    PubMed

    Han, Ruizhen; He, Yong; Liu, Fei

    2012-01-01

    This paper presents a feasibility study on a real-time in field pest classification system design based on Blackfin DSP and 3G wireless communication technology. This prototype system is composed of remote on-line classification platform (ROCP), which uses a digital signal processor (DSP) as a core CPU, and a host control platform (HCP). The ROCP is in charge of acquiring the pest image, extracting image features and detecting the class of pest using an Artificial Neural Network (ANN) classifier. It sends the image data, which is encoded using JPEG 2000 in DSP, to the HCP through the 3G network at the same time for further identification. The image transmission and communication are accomplished using 3G technology. Our system transmits the data via a commercial base station. The system can work properly based on the effective coverage of base stations, no matter the distance from the ROCP to the HCP. In the HCP, the image data is decoded and the pest image displayed in real-time for further identification. Authentication and performance tests of the prototype system were conducted. The authentication test showed that the image data were transmitted correctly. Based on the performance test results on six classes of pests, the average accuracy is 82%. Considering the different live pests' pose and different field lighting conditions, the result is satisfactory. The proposed technique is well suited for implementation in field pest classification on-line for precision agriculture. PMID:22736996

  4. A field-portable membrane introduction mass spectrometer for real-time quantitation and spatial mapping of atmospheric and aqueous contaminants.

    PubMed

    Bell, Ryan J; Davey, Nicholas G; Martinsen, Morten; Collin-Hansen, Christian; Krogh, Erik T; Gill, Christopher G

    2015-02-01

    Environmental concentrations of volatile and semivolatile organic compounds (VOC/SVOCs) can vary dramatically in time and space under the influence of environmental conditions. In an industrial setting, multiple point and diffuse sources can contribute to fugitive emissions. Assessments and monitoring programs using periodic grab sampling provide limited information, often with delay times of days or weeks. We report the development and use of a novel, portable membrane introduction mass spectrometry (MIMS) system capable of resolving and quantifying VOC and SVOCs with high spatial and temporal resolution, in the field, in real-time. An electron impact ionization cylindrical ion trap mass spectrometer modified with a capillary hollow fiber polydimethylsiloxane membrane interface was used for continuous air and water sampling. Tandem mass spectrometry and selected ion monitoring scans performed in series allowed for the quantitation of target analytes, and full scan mode was used to survey for unexpected analytes. Predeployment and in-field external calibrations were combined with a continuously infused internal standard to enable real-time quantitation and monitor instrument performance. The system was operated in a moving vehicle with internet-linked data processing and storage. Software development to integrate MIMS and relevant meta-data for visualization and geospatial presentation in Google Earth is presented. Continuous quantitation enables the capture of transient events that may be missed or under-represented by traditional grab sampling strategies. Real-time geospatial maps of chemical concentration enable adaptive sampling and in-field decision support. Sample datasets presented in this work were collected in Northern Alberta in 2010-2012. PMID:25477082

  5. A Field-Portable Membrane Introduction Mass Spectrometer for Real-time Quantitation and Spatial Mapping of Atmospheric and Aqueous Contaminants

    NASA Astrophysics Data System (ADS)

    Bell, Ryan J.; Davey, Nicholas G.; Martinsen, Morten; Collin-Hansen, Christian; Krogh, Erik T.; Gill, Christopher G.

    2015-02-01

    Environmental concentrations of volatile and semivolatile organic compounds (VOC/SVOCs) can vary dramatically in time and space under the influence of environmental conditions. In an industrial setting, multiple point and diffuse sources can contribute to fugitive emissions. Assessments and monitoring programs using periodic grab sampling provide limited information, often with delay times of days or weeks. We report the development and use of a novel, portable membrane introduction mass spectrometry (MIMS) system capable of resolving and quantifying VOC and SVOCs with high spatial and temporal resolution, in the field, in real-time. An electron impact ionization cylindrical ion trap mass spectrometer modified with a capillary hollow fiber polydimethylsiloxane membrane interface was used for continuous air and water sampling. Tandem mass spectrometry and selected ion monitoring scans performed in series allowed for the quantitation of target analytes, and full scan mode was used to survey for unexpected analytes. Predeployment and in-field external calibrations were combined with a continuously infused internal standard to enable real-time quantitation and monitor instrument performance. The system was operated in a moving vehicle with internet-linked data processing and storage. Software development to integrate MIMS and relevant meta-data for visualization and geospatial presentation in Google Earth is presented. Continuous quantitation enables the capture of transient events that may be missed or under-represented by traditional grab sampling strategies. Real-time geospatial maps of chemical concentration enable adaptive sampling and in-field decision support. Sample datasets presented in this work were collected in Northern Alberta in 2010-2012.

  6. EFFECTS OF DEFINED MIXTURES OF TRIHALOMETHANES AND HALOACETIC ACIDS ON PREGNANCY MAINTENANCE AND EYE DEVELOPMENT IN F 344 RATS

    EPA Science Inventory

    Although disinfection of drinking water is important for control of microbial contamination, it results in the formation of hundreds of disinfection by-products (DBPs). The most prevalent DBPs are trihalomethanes (THMs; chloroform, bromodichloromethane, chlorodibromomethane, bro...

  7. Application of portable X-ray fluorescence (pXRF) for heavy metal analysis of soils in crop fields near abandoned mine sites.

    PubMed

    Jang, Min

    2010-06-01

    To get representative soil samples, a sampling method was verified for crop fields in the vicinity of abandoned mine sites. Application of appropriate sampling or analytical methods is very important as it affects the costs, time, and accuracy of the refined investigation of soil contamination. Two-time sampling for each crop field was conducted to verify the reproducibility of a zigzag method for soil sampling. The soil analysis using a portable X-ray fluorescence (pXRF) device was conducted to measure concentrations of metal species in soils, and its results were compared to the extracted concentrations by the Korean Standard Test (KST) for soils. As a result, the determination coefficient (R (2)) of linear regression analysis for data obtained by ex situ precise measurement or in situ field screening using pXRF was closely related with the ratio of the extracted concentration by KST to interference-free detection limits (IFDL) of pXRF (designated as KST/IFDL). As the specific metal species had a higher ratio of KST/IFDL, its R (2) was even higher in the field screening tests. However, the slopes of linear regression analysis for most metal species extracted by aqua-regia were close to 1.0 so that extracted concentrations by aqua-regia were similar to the analytical values obtained by pXRF, whereas extraction using a weak acid (0.1 M HCl) had different slopes for soils contaminated with different ranges of concentrations of metal species. Especially Zn showed not only high ratios of KST/IFDL because of aqua regia extraction, but also high determination coefficients. Because of its simple, rapid, and accurate capacities for metal analysis, the pXRF analysis showed high applicability in ex situ precise measurements or in situ field screening of metal analysis. In terms of applicability for regulation, especially in situ pXRF field screening with the zigzag method could be effectively applied to achieve an economical survey by determining hot spots or non

  8. Portable multiplicity counter

    DOEpatents

    Newell, Matthew R.; Jones, David Carl

    2009-09-01

    A portable multiplicity counter has signal input circuitry, processing circuitry and a user/computer interface disposed in a housing. The processing circuitry, which can comprise a microcontroller integrated circuit operably coupled to shift register circuitry implemented in a field programmable gate array, is configured to be operable via the user/computer interface to count input signal pluses receivable at said signal input circuitry and record time correlations thereof in a total counting mode, coincidence counting mode and/or a multiplicity counting mode. The user/computer interface can be for example an LCD display/keypad and/or a USB interface. The counter can include a battery pack for powering the counter and low/high voltage power supplies for biasing external detectors so that the counter can be configured as a hand-held device for counting neutron events.

  9. Neutron Damage in Mechanically-Cooled High-Purity Germanium Detectors for Field-Portable Prompt Gamma Neutron Activation Analysis (PGNAA) Systems

    SciTech Connect

    E.H. Seabury; C.J. Wharton; A.J. Caffrey; J.B. McCabe; C. DeW. Van Siclen

    2013-10-01

    Prompt Gamma Neutron Activation (PGNAA) systems require the use of a gamma-ray spectrometer to record the gamma-ray spectrum of an object under test and allow the determination of the object’s composition. Field-portable systems, such as Idaho National Laboratory’s PINS system, have used standard liquid-nitrogen-cooled high-purity germanium (HPGe) detectors to perform this function. These detectors have performed very well in the past, but the requirement of liquid-nitrogen cooling limits their use to areas where liquid nitrogen is readily available or produced on-site. Also, having a relatively large volume of liquid nitrogen close to the detector can impact some assessments, possibly leading to a false detection of explosives or other nitrogen-containing chemical. Use of a mechanically-cooled HPGe detector is therefore very attractive for PGNAA applications where nitrogen detection is critical or where liquid-nitrogen logistics are problematic. Mechanically-cooled HPGe detectors constructed from p-type germanium, such as Ortec’s trans-SPEC, have been commercially available for several years. In order to assess whether these detectors would be suitable for use in a fielded PGNAA system, Idaho National Laboratory (INL) has been performing a number of tests of the resistance of mechanically-cooled HPGe detectors to neutron damage. These detectors have been standard commercially-available p-type HPGe detectors as well as prototype n-type HPGe detectors. These tests compare the performance of these different detector types as a function of crystal temperature and incident neutron fluence on the crystal.

  10. Field portable detection of VOCs using a SAW/GC system. Final report, June 21, 1994--September 21, 1996

    SciTech Connect

    Chang, F.; Staples, E.J.

    1998-06-01

    This report describes research on a fast GC vapor analysis system which uses a new type of Surface Acoustic Wave detector technology to characterize organic contamination in soil and groundwater. The project was sponsored by the Department of Energy, Morgantown Energy Technology Center, whose mission, in addition to other goals, is the development of tools and methods for characterization, remediation, and monitoring of underground environmental conditions. The research tasks were to demonstrate detectability and specificity of a Surface Acoustic Wave Gas Chromatograph (SAW/GC) to a representative number of VOC materials followed by field demonstrations of the new technology at a DOE site. All tasks of the project were successfully carried out and a fast vapor analysis system based upon a new type of Surface Acoustic Wave detector technology was developed. The prototype analyzer has the ability to characterize organic contamination in soil and groundwater at the part per billion level in less than 10 seconds. The detector is unique because it utilized an uncoated quartz crystal, contrary to current developments of using coated crystals.

  11. Portable Instrumented Communication Library

    Energy Science and Technology Software Center (ESTSC)

    1993-06-10

    PICL is a subroutine library that can be used to develop parallel programs that are portable across several distributed-memory multiprocessors. PICL provides a portable syntax for key communication primitives and related system calls. It also provides portable routines to perform certain widely-used, high-level communication operations, such as global broadcast and global summation. PICL provides execution tracing that can be used to monitor performance or to aid in debugging.

  12. Method of Analysis by the U.S. Geological Survey California District Sacramento Laboratory?Determination of Trihalomethane Formation Potential, Method Validation, and Quality-Control Practices

    USGS Publications Warehouse

    Crepeau, Kathryn L.; Fram, Miranda S.; Bush, Noel

    2004-01-01

    An analytical method for the determination of the trihalomethane formation potential of water samples has been developed. The trihalomethane formation potential is measured by dosing samples with chlorine under specified conditions of pH, temperature, incubation time, darkness, and residual-free chlorine, and then analyzing the resulting trihalomethanes by purge and trap/gas chromatography equipped with an electron capture detector. Detailed explanations of the method and quality-control practices are provided. Method validation experiments showed that the trihalomethane formation potential varies as a function of time between sample collection and analysis, residual-free chlorine concentration, method of sample dilution, and the concentration of bromide in the sample.

  13. Trihalomethane and nonpurgeable total organic-halide formation potentials of the Mississippi river

    USGS Publications Warehouse

    Rathbun, R.E.

    1996-01-01

    Trihalomethane and nonpurgeable total organic-hallide formation potentials were determined for water samples from 12 sites along the Mississippi River from Minneapolis, MN, to New Orleans, LA, for the summer and fall of 1991 and the spring of 1992. The formation potentials increased with distance upstream, approximately paralleling the increase of the dissolved organic- carbon concentration. The pH and the dissolved organic-carbon and free- chlorine concentrations were significant variables in the prediction of the formation potentials. The trihalomethane formation potential increased as the pH increased, whereas the nonpurgeable total organic-halide formation potential decreased. All formation potentials increased as the dissolved organic-carbon and free-chlorine concentrations increased, with the dissolved organic-carbon concentration having a much greater effect.

  14. Multipathway risk assessment of trihalomethane exposure in drinking water of Lebanon.

    PubMed

    Semerjian, Lucy; Dennis, John

    2007-12-01

    The toxicological risks and lifetime cancer risks of trihalomethanes through oral ingestion, dermal absorption, and inhalation exposure from tap water in selected regions in Lebanon are estimated. Existing trihalomethane concentrations do not pose any non-carcinogenic and developmental risks in the exposed population via oral ingestion. Among the three pathways, residents have a higher risk of cancer through oral ingestion than through the other two pathways. The lifetime cancer risk through oral ingestion for dibromochloromethane makes the highest contribution to total risks, followed by bromodichloromethane, bromoform, and chloroform. The total multipathway cancer risk analysis suggests that no cancer risks exist during the summer and winter seasons; however, in the spring the total cancer risks exceeds the USEPA acceptable level of 10(-6) by a factor of 10.7. PMID:17878564

  15. Analysis of Twenty-Two Performance Properties of Diesel, Gasoline, and Jet Fuels Using a Field-Portable Near-Infrared (NIR) Analyzer.

    PubMed

    Brouillette, Carl; Smith, Wayne; Shende, Chetan; Gladding, Zack; Farquharson, Stuart; Morris, Robert E; Cramer, Jeffrey A; Schmitigal, Joel

    2016-05-01

    The change in custody of fuel shipments at depots, pipelines, and ports could benefit from an analyzer that could rapidly verify that properties are within specifications. To meet this need, the design requirements for a fuel analyzer based on near-infrared (NIR) spectroscopy, such as spectral region and resolution, were examined. It was found that the 1000 to 1600 nm region, containing the second CH overtone and combination vibrational modes of hydrocarbons, provided the best near-infrared to fuel property correlations when path length was taken into account, whereas 4 cm(-1) resolution provided only a modest improvement compared to 16 cm(-1) resolution when four or more latent variables were used. Based on these results, a field-portable near-infrared fuel analyzer was built that employed an incandescent light source, sample compartment optics to hold 2 mL glass sample vials with ∼1 cm path length, a transmission grating, and a 256 channel InGaAs detector that measured the above stated wavelength range with 5-6 nm (∼32 cm(-1)) resolution. The analyzer produced high signal-to-noise ratio (SNR) spectra of samples in 5 s. Twenty-two property correlation models were developed for diesel, gasoline, and jet fuels with root mean squared error of correlation - cross-validated values that compared favorably to corresponding ASTM reproducibility values. The standard deviations of predicted properties for repeat measurements at 4, 24, and 38℃ were often better than ASTM documented repeatability values. The analyzer and diesel property models were tested by measuring seven diesel samples at a local ASTM certification laboratory. The standard deviations between the analyzer determined values and the ASTM measured values for these samples were generally better than the model root mean squared error of correlation-cross-validated values for each property. PMID:27006025

  16. Metal contamination at recreational boatyards linked to the use of antifouling paints-investigation of soil and sediment with a field portable XRF.

    PubMed

    Lagerström, Maria; Norling, Matz; Eklund, Britta

    2016-05-01

    The application of a field portable X-ray fluorescence spectrometer (FPXRF) to measure Cu, Zn, and Pb in soil and sediments at recreational boatyards by Lake Mälaren in Sweden was investigated. Confirmatory chemical analysis on freeze-dried samples shows that, ex situ, the FPXRF produces definitive level data for Cu and Zn and quantitative screening data for Pb, according to USEPA criteria for data quality. Good agreement was also found between the ex situ measurements and the in situ screening. At each of the two studied boatyards, >40 in situ soil measurements were carried out. Statistical differences in soil concentration based on land use were consequently found: the areas used for boat storage and maintenance were significantly higher in Cu and Zn than the areas used for car parking and transportation. The metal pollution in the boat storage areas is therefore shown to be directly linked to hull maintenance activities during which metal-containing antifouling paint particles are shed, end up on the ground, and consequently pollute the soil. In the boat storage areas, the Cu and Zn concentrations often exceeded the national guideline values for soil. In this study, they were also shown to increase with increasing age of the boatyard operation. Pb soil concentrations were only elevated at a few measurement points, reflecting the phasing out of Pb compounds from antifouling products over the past 2 decades. In the surface sediments, concentrations of Cu and Zn were 2-3 times higher compared to deeper levels. No decrease in metal concentration with time was found in the sediments, indicating that boat owners are not complying with the ban of biocide-containing paints in freshwater introduced over 20 years ago. PMID:26873824

  17. A new portable infrared laser spectrometer for field measurements of N2O and CH4 emissions at the air / land interface

    NASA Astrophysics Data System (ADS)

    Guimbaud, Christophe; Catoire, Valéry; Gogo, Sébastien; Robert, Claude; Laggoun-Defarge, Fatima; Nicoullaud, Bernard; Richard, Guy

    2010-05-01

    A new type of portable infra red spectrometer (SPIRIT : SPectromètre Infra-Rouge In situ Troposphérique) using a quantum cascade laser and a patented new long multipass optical cell has been set up for the simultaneous flux measurements of two Greenhouse Gases (GHG): nitrous oxide (N2O) and methane (CH4), at the air land interface. The basics of the instrument, the data derivation for trace gas concentration determination in the atmosphere, and the chamber method to derive emission fluxes of these GHG from lands are described. The analytical performances of SPIRIT are tested in two types of lands in Region Centre (France): (i) an anthropogenized sphagnum peatland (Laguette; Neuvy sur Barangeon) characterized by vascular plants invasion (ii) a sandy soil in the site of INRA-Orléans. The ability of SPIRIT to assess with precision spatial and temporal dependence emissions of these GHG in the field is demonstrated. In addition emission modes (diffusive episodes and bubbling events) can be observed and quantified due to the high frequency (1 Hz) of the concentration measured. SPIRIT adaptation for detailed process-oriented studies of GHG flux emissions is also demonstrated by the investigation of emission dependence as a function of biotic and abiotic parameters (including diurnal cycle sensibility and emission modes); processes of C exchanges between different compartments of the biota can be studied. Such investigations are required for a better understanding of the lands to atmosphere exchange mechanisms of GHG and for the prediction of feedbacks on GHG emissions in response to anthropogenic or climate change perturbations of terrestrial ecosystems. Implications of SPIRIT in other air lands studies are also presented.

  18. PORTABLE ACOUSTIC MONITORING PACKAGE (PAMP)

    SciTech Connect

    John L. Loth; Gary J. Morris; George M. Palmer; Richard Guiler; Patrick Browning

    2004-07-20

    The Portable Acoustic Monitoring Package (PAMP) has been designed to record and monitor the acoustic signal in natural gas transmission lines. In particular the three acoustic signals associated with a line leak. The system is portable ({approx}30 lbs) and is designed for line pressures up to 1000 psi. It has become apparent that cataloging of the various background acoustic signals in natural gas transmission line is very important if a system to identify leak signals is to be developed. The low-pressure (0-200 psig) laboratory test phase has been completed and a number of field trials have been conducted. Before the cataloging phase could begin, a few problems identified in field trials identified had to be corrected such as: (1) Decreased microphone sensitivity at line pressures above 250 psig. (2) The inability to deal with large data sets collected when cataloging the variety of signals in a transmission line. (3) The lack of an available online acoustic calibration system. These problems have been solved and the WVU PAMP is now fully functional over the entire pressure range found in the Natural Gas transmission lines in this region. Field portability and reliability have been greatly improved. Data collection and storage have also improved to the point were the full acoustic spectrum of acoustic signals can be accurately cataloged, recorded and described.

  19. Portable chemiluminescence detector for nickel carbonyl

    SciTech Connect

    Hikade, D.A.; Stedman, D.H.; Walega, J.G.

    1984-08-01

    This article describes a portable chemiluminescent detector for Ni(CO)/sub 4/ containing two innovative components, a self-contained carbon monoxide source which provides a greater degree of portability and a thermal differentiator to improve selectivity. The instrument is capable of measuring parts-per-billion levels of Ni(CO)/sub 4/, Fe(CO)/sub 5/, and NO. The instrument was used to measure carbonyl concentrations in the field and in cigarette smoke.

  20. Portable modular detection system

    DOEpatents

    Brennan, James S.; Singh, Anup; Throckmorton, Daniel J.; Stamps, James F.

    2009-10-13

    Disclosed herein are portable and modular detection devices and systems for detecting electromagnetic radiation, such as fluorescence, from an analyte which comprises at least one optical element removably attached to at least one alignment rail. Also disclosed are modular detection devices and systems having an integrated lock-in amplifier and spatial filter and assay methods using the portable and modular detection devices.

  1. Portable peak flow meters.

    PubMed

    McNaughton, J P

    1997-02-01

    There are several portable peak flow meters available. These instruments vary in construction and performance. Guidelines are recommended for minimum performance and testing of portable peak flow meters, with the aim of establishing a procedure for standardizing all peak flow meters. Future studies to clarify the usefulness of mechanical test apparatus and clinical trials of peak flow meters are also recommended. PMID:9098706

  2. Portable seat lift

    NASA Technical Reports Server (NTRS)

    Weddendorf, Bruce (Inventor)

    1994-01-01

    A portable seat lift that can help individuals either (1) lower themselves to a sitting position or (2) raise themselves to a standing position is presented. The portable seat lift consists of a seat mounted on a base with two levers, which are powered by a drive unit.

  3. Portable Medical Laboratory Applications Software

    PubMed Central

    Silbert, Jerome A.

    1983-01-01

    Portability implies that a program can be run on a variety of computers with minimal software revision. The advantages of portability are outlined and design considerations for portable laboratory software are discussed. Specific approaches for achieving this goal are presented.

  4. Portable sensor for hazardous waste

    SciTech Connect

    Piper, L.G.; Fraser, M.E.; Davis, S.J.

    1995-10-01

    We are beginning the second phase of a three and a half year program designed to develop a portable monitor for sensitive hazardous waste detection. The ultimate goal of the program is to develop our concept to the prototype instrument level. Our monitor will be a compact, portable instrument that will allow real-time, in situ, monitoring of hazardous wastes. This instrument will be able to provide the means for rapid field screening of hazardous waste sites to map the areas of greatest contamination. Remediation efforts can then focus on these areas. Further, our instrument can show whether cleanup technologies are successful at reducing hazardous materials concentrations below regulated levels, and will provide feedback to allow changes in remediation operations, if necessary, to enhance their efficacy.

  5. Rapid diagnosis of avian influenza virus in wild birds: Use of a portable rRT-PCR and freeze-dried reagents in the field

    USGS Publications Warehouse

    Takekawa, J.Y.; Hill, N.J.; Schultz, A.K.; Iverson, S.A.; Cardona, C.J.; Boyce, W.M.; Dudley, J.P.

    2011-01-01

    Wild birds have been implicated in the spread of highly pathogenic avian influenza (HPAI) of the H5N1 subtype, prompting surveillance along migratory flyways. Sampling of wild birds for avian influenza virus (AIV) is often conducted in remote regions, but results are often delayed because of the need to transport samples to a laboratory equipped for molecular testing. Real-time reverse transcriptase polymerase chain reaction (rRT-PCR) is a molecular technique that offers one of the most accurate and sensitive methods for diagnosis of AIV. The previously strict lab protocols needed for rRT-PCR are now being adapted for the field. Development of freeze-dried (lyophilized) reagents that do not require cold chain, with sensitivity at the level of wet reagents has brought on-site remote testing to a practical goal. Here we present a method for the rapid diagnosis of AIV in wild birds using an rRT-PCR unit (Ruggedized Advanced Pathogen Identification Device or RAPID, Idaho Technologies, Salt Lake City, UT) that employs lyophilized reagents (Influenza A Target 1 Taqman; ASAY-ASY-0109, Idaho Technologies). The reagents contain all of the necessary components for testing at appropriate concentrations in a single tube: primers, probes, enzymes, buffers and internal positive controls, eliminating errors associated with improper storage or handling of wet reagents. The portable unit performs a screen for Influenza A by targeting the matrix gene and yields results in 2-3 hours. Genetic subtyping is also possible with H5 and H7 primer sets that target the hemagglutinin gene. The system is suitable for use on cloacal and oropharyngeal samples collected from wild birds, as demonstrated here on the migratory shorebird species, the western sandpiper (Calidrus mauri) captured in Northern California. Animal handling followed protocols approved by the Animal Care and Use Committee of the U.S. Geological Survey Western Ecological Research Center and permits of the U.S. Geological Survey

  6. Human portable preconcentrator system

    DOEpatents

    Linker, Kevin L.; Bouchier, Francis A.; Hannum, David W.; Rhykerd, Jr., Charles L.

    2003-01-01

    A preconcentrator system and apparatus suited to human portable use wherein sample potentially containing a target chemical substance is drawn into a chamber and through a pervious screen. The screen is adapted to capture target chemicals and then, upon heating, to release those chemicals into the chamber. Chemicals captured and then released in this fashion are then carried to a portable chemical detection device such as a portable ion mobility spectrometer. In the preferred embodiment, the means for drawing sample into the chamber comprises a reversible fan which, when operated in reverse direction, creates a backpressure that facilitates evolution of captured target chemicals into the chamber when the screen is heated.

  7. Inexpensive portable drug detector

    NASA Technical Reports Server (NTRS)

    Dimeff, J.; Heimbuch, A. H.; Parker, J. A.

    1977-01-01

    Inexpensive, easy-to-use, self-scanning, self-calibrating, portable unit automatically graphs fluorescence spectrum of drug sample. Device also measures rate of movement through chromatographic column for forensic and medical testing.

  8. Portable beveling tool

    NASA Technical Reports Server (NTRS)

    Snowden, R. H.

    1972-01-01

    Portable tool was designed to semiautomatically bevel end surfaces of tubular or cylindrical components. Tool may be used for fabrication of elbow assembly which requires mating flange and elbow by fusion butt welding.

  9. Portable Dental System

    NASA Technical Reports Server (NTRS)

    1980-01-01

    Portable dental system provides dental care in isolated communities. System includes a patient's chair and a dentist's stool, an X-ray machine and a power unit, all of which fold into compact packages. A large yellow "pumpkin" is a collapsible compressed air tank. Portable system has been used successfully in South America in out of the way communities with this back-packable system, and in American nursing homes. This product is no longer manufactured.

  10. Portable treatment systems study

    SciTech Connect

    Sherick, M.J.; Schwinkendorf, W.E.; Bechtold, T.E.; Cole, L.T.

    1997-03-01

    In developing their Site Treatment Plans (STPs), many of the Department of Energy installations identified some form of portable treatment, to facilitate compliant disposition of select mixed low-level wastestreams. The Environmental Management Office of Science and Technology requested that a systems study be performed to better define the potential role of portable treatment with respect to mixed low-level waste, highlight obstacles to implementation, and identify opportunities for future research and development emphasis. The study was performed by first establishing a representative set of mixed waste, then formulating portable treatment system concepts to meet the required processing needs for these wastes. The portable systems that were conceptualized were evaluated and compared to a fixed centralized treatment alternative. The system evaluations include a life-cycle cost analysis and an assessment of regulatory, institutional, and technical issues associated with the potential use of portable systems. The results of this study show that when all costs are included, there are no significant cost differences between portable systems and fixed systems. However, it is also emphasized that many uncertainties exist that could impact the cost of implementing portable treatment systems. Portable treatment could be made more attractive through private sector implementation, although there is little economic incentive for a commercial vendor to develop small, specialized treatment capabilities with limited applicability. Alternatively, there may also be valid reasons why fixed units cannot be used for some problematic wastestreams. In any event, there are some site-specific problems that still need to be addressed, and there may be some opportunity for research and development to make a positive impact in these areas.

  11. Advanced oxidation of bromide-containing drinking water: a balance between bromate and trihalomethane formation control.

    PubMed

    Wang, Yongjing; Yu, Jianwei; Han, Po; Sha, Jing; An, Tao; Li, Wei; Liu, Juan; Yang, Min

    2013-11-01

    Addition of H202 has been employed to repress bromate formation during ozonation of bromide-containing source water. However, the addition of H2O2 will change the oxidation pathways of organic compounds due to the generation of abundant hydroxyl radicals, which could affect the removal efficacy of trihalomethane precursors via the combination of ozone and biological activated carbon (O3-BAC). In this study, we evaluated the effects of H2O2 addition on bromate formation and trihalomethane formation potential (THMFP) reduction during treatment of bromide-containing (97.6-129.1 microg/L) source water by the O3-BAC process. At an ozone dose of 4.2 mg/L, an H2O2/O3 (g/g) ratio of over 1.0 was required to maintain the bromate concentration below 10.0 microg/L, while a much lower H2O2/O3 ratio was sufficient for a lower ozone dose. An H2O2/O3 (g/g) ratio below 0.3 should be avoided since the bromate concentration will increase with increasing H2O2 dose below this ratio. However, the addition of H202 at an ozone dose of 3.2 mg/L and an H2O2/O3 ratio of 1.0 resulted in a 43% decrease in THMFP removal when comparedwith the O3-BAC process. The optimum H2O2/O3 (g/g) ratio for balancing bromate and trihalomethane control was about 0.7-1.0. Fractionation of organic materials showed that the addition of H2O2 decreased the removal efficacy of the hydrophilic matter fraction of DOC by ozonation and increased the reactivity of the hydrophobic fractions during formation of trihalomethane, which may be the two main reasons responsible for the decrease in THMFP reduction efficacy. Overall, this study clearly demonstrated that it is necessary to balance bromate reduction and THMFP control when adopting an H2O2 addition strategy. PMID:24552044

  12. Cancer incidence and trihalomethane concentrations in a public drinking water system

    SciTech Connect

    Carlo, G.L.; Mettlin, C.L.

    1980-05-01

    Four thousand two hundred fifty-five cases of esophageal, stomach, colon, rectal, bladder, and pancreatic cancer reported from Erie County, NY between 1973 and 1976 were analyzed in terms of their relationship to type of water source, level of trihalomethane (THM) and various social and economic parameters. Among white males, a significant positive correlation existed between pancreatic cancer incidence rates and THM level. No other significant correlations were observed. This research lends little or no support to the hypothesis that THM levels which meet present standards are related to the incidence of human cancer.

  13. Portable smartphone optical fibre spectrometer

    NASA Astrophysics Data System (ADS)

    Hossain, Md. Arafat; Canning, John; Cook, Kevin; Jamalipour, Abbas

    2015-09-01

    A low cost, optical fibre based spectrometer has been developed on a smartphone platform for field-portable spectral analysis. Light of visible wavelength is collected using a multimode optical fibre and diffracted by a low cost nanoimprinted diffraction grating. A measurement range over 300 nm span (λ = 400 to 700 nm) is obtained using the smartphone CMOS chip. The spectral resolution is Δλ ~ 0.42 nm/screen pixel. A customized Android application processed the spectra on the same platform and shares with other devices. The results compare well with commercially available spectrometer.

  14. Second-order chlorine decay and trihalomethanes formation in a pilot-scale water distribution systems.

    PubMed

    Li, Cong; Yang, Y Jeffrey; Yu, Jieze; Zhang, Tu-qiao; Mao, Xinwei; Shao, Weiyun

    2012-08-01

    It is well known that model-building of chlorine decay in real water distribution systems is difficult because chlorine decay is influenced by many factors (e.g., bulk water demand, pipe-wall demand, piping material, flow velocity, and residence time). In this paper, experiments were run to investigate the kinetic model of chlorine decay and the formation model of trihalomethanes (THMs) in pilot-scale water distribution systems. Experimental results show that the rate constants of chlorine decay, including wall decay and bulk decay, increasing with temperature. Moreover, the kinetic model of chlorine decay and the formation model of THMs describe experiment data of pilot-scale water distribution systems. The effect of different piping material on chlorine decay and THMs formation were also investigated. The rate constants of chlorine decay are ranked in order: stainless steel pipe, ductile iron pipe, and last, polyethelene pipe because wall decay is the largest in stainless steel pipe than that in other piping material. Correspondingly, the rate of THMs formation follows the order of stainless steel pipe, ductile iron pipe, and last, polyethelene pipe because of less chlorine in bulk water reacting with the trihalomethane formation potential (THMFP). PMID:22953450

  15. Factors affecting trihalomethane formation and speciation during chlorination of reclaimed water.

    PubMed

    Ma, Defang; Gao, Baoyu; Wang, Yan; Yue, Qinyan; Li, Qian

    2015-01-01

    A hybrid process with membrane bioreactor (MBR) and powdered activated carbon (PAC), PAC/MBR, was used for real municipal wastewater treatment and reuse. The roles of chlorine dose, contact time, pH and bromide in trihalomethane (THM) formation and speciation during chlorination of the reclaimed water were investigated. Total trihalomethane (TTHM) yield exponentially increased to maximum with increasing chlorine dose (correlation coefficient R2=0.98). Prolonging substrate chlorine contact time significantly promoted TTHM formation. Less than 40% of THMs formed in the first 24 h, indicating that the PAC/MBR effluent organic matters were mostly composed of slow-reacting precursors. Increasing pH and bromide concentration facilitated THM formation. Higher chlorine dose and contact time enhanced chloro-THM formation. The bromo-THM formation was favored at near neutral condition. Despite the variation of chlorine dose, contact time and pH, the yield of THM species in order was usually CHCl3>CHBrCl2>CHBr2Cl>CHBr3. However, THM speciation shifted from chlorinated species to brominated species with increasing bromide concentration. PMID:26247761

  16. Portable Applications in Mobile Education. Technical Evaluation Report 57

    ERIC Educational Resources Information Center

    Baggaley, Jon

    2006-01-01

    Portable software applications can be carried on a convenient storage medium such as a USB drive, and offer numerous benefits to mobile teachers and learner. The article illustrates the growing field of "portable apps" in reviews of seven contrasting products. These represent the major categories of document editing, email maintenance, Internet…

  17. Human portable preconcentrator system

    DOEpatents

    Linker, Kevin L.; Brusseau, Charles A.; Hannum, David W.; Puissant, James G.; Varley, Nathan R.

    2003-08-12

    A preconcentrator system and apparatus suited to human portable use wherein sample potentially containing a target chemical substance is drawn into a chamber and through a pervious screen. The screen is adapted to capture target chemicals and then, upon heating, to release those chemicals into the chamber. Chemicals captured and then released in this fashion are then carried to a portable chemical detection device such as a portable ion mobility spectrometer. In the preferred embodiment, the means for drawing sample into the chamber comprises a reversible fan which, when operated in reverse direction, creates a backpressure that facilitates evolution of captured target chemicals into the chamber when the screen is heated. The screen can be positioned directly in front of the detector prior to heating to improve detection capability.

  18. Portable biochip scanner device

    DOEpatents

    Perov, Alexander; Sharonov, Alexei; Mirzabekov, Andrei D.

    2002-01-01

    A portable biochip scanner device used to detect and acquire fluorescence signal data from biological microchips (biochips) is provided. The portable biochip scanner device employs a laser for emitting an excitation beam. An optical fiber delivers the laser beam to a portable biochip scanner. A lens collimates the laser beam, the collimated laser beam is deflected by a dichroic mirror and focused by an objective lens onto a biochip. The fluorescence light from the biochip is collected and collimated by the objective lens. The fluorescence light is delivered to a photomultiplier tube (PMT) via an emission filter and a focusing lens. The focusing lens focuses the fluorescence light into a pinhole. A signal output of the PMT is processed and displayed.

  19. Deflectometry using portable devices

    NASA Astrophysics Data System (ADS)

    Butel, Guillaume P.; Smith, Greg A.; Burge, James H.

    2015-02-01

    Deflectometry is a powerful metrology technique that uses off-the-shelf equipment to achieve nanometer-level accuracy surface measurements. However, there is no portable device to quickly measure eyeglasses, lenses, or mirrors. We present an entirely portable new deflectometry technique that runs on any Android™ smartphone with a front-facing camera. Our technique overcomes some specific issues of portable devices like screen nonlinearity and automatic gain control. We demonstrate our application by measuring an amateur telescope mirror and simulating a measurement of the faulty Hubble Space Telescope primary mirror. Our technique can, in less than 1 min, measure surface errors with accuracy up to 50 nm RMS, simply using a smartphone.

  20. EFFECTS OF FOUR TRIHALOMETHANES ON DNA STRAND BREAKS, RENAL HYALINE DROPLET FORMATION AND SERUM TESTOSTERONE IN MALE F-344 RATS

    EPA Science Inventory

    All four possible trihalomethanes (THMs) containing bromine and chlorine, as well as perchloroethylene (PCE), were evaluated for their ability to produce DNA strand breaks, a2u-globulin rich renal deposits, and testosterone changes in male F-344 rats. Rats received daily equimola...

  1. On-field monitoring of fruit ripening evolution and quality parameters in olive mutants using a portable NIR-AOTF device.

    PubMed

    Cirilli, Marco; Bellincontro, Andrea; Urbani, Stefania; Servili, Maurizio; Esposto, Sonia; Mencarelli, Fabio; Muleo, Rosario

    2016-05-15

    This study optimizes the application of portable Near Infrared-Acousto Optically Tunable Filter (NIR) device to meet the increasing demand for cost-effective, non-invasive and easy-to-use methods for measuring physical and chemical properties during olive fruit development. Fruits from different phenotypically cultivars were sampled for firmness, total and specific phenols detection by HPLC, total anthocyanins, chlorophyll and carotenoids detection by spectrophotometry. On the same fruits, a portable NIR device in diffuse reflectance mode was employed for spectral detections. Predictive models for firmness, chlorophyll, anthocyanins, carotenoids and rutin were developed by Partial Least Square analysis. Oleuropein, verbascoside, 3,4-DHPEA-EDA, and total phenols were used to develop a validation model. Internal cross-validation was applied for calibration and predictive models. The standard errors for calibration, cross-validation, prediction, and RPD ratios (SD/SECV) were calculated as references for the model effectiveness. The determination of the optimal harvesting time facilitates the production of high quality extra virgin olive oil and table olives. PMID:26775949

  2. Portable Data Logger for Photovoltaic Panels

    NASA Technical Reports Server (NTRS)

    Cole, S. W.

    1983-01-01

    Instrument measures rapidly changing knee of V-I curve with extra care. Portable data logger runs on own batteries. Includes microcomputer, which controls voltage-, current-measurement increment, and solid state memory, which stores data until transferred to EPROM module. Data logger is light, compact and easily caried to remote field locations.

  3. Fixed Facts about Portable Classrooms.

    ERIC Educational Resources Information Center

    Sturgeon, Julie

    1998-01-01

    Discusses the easing of overcrowded schools through the use of portable classrooms and provides an example from Elk Grove Unified School District (California) which has opened entire elementary schools using only portables. Fifteen tips for installing relocatables are highlighted. (GR)

  4. Portable nanoparticle based sensors for antioxidant analysis.

    PubMed

    Sharpe, Erica; Andreescu, Silvana

    2015-01-01

    Interest in portable sensing devices has increased throughout the past decade. Portable sensors are convenient for use in remote locations and in places with limited resources for advanced instrumentation. Often such devices utilize advanced technology that allows the final user to simply deposit the sample onto the sensing platform without preparation of multiple reagents. Herein, we describe preparation and characterization of a colorimetric paper-based metal oxide sensing array designed for the field detection of polyphenolic antioxidants. This sensor is a good candidate for use in analysis of the antioxidant character of food, drink, botanical medicines, physiological fluids, and more. PMID:25323510

  5. Portable dynamic fundus instrument

    NASA Technical Reports Server (NTRS)

    Taylor, Gerald R. (Inventor); Meehan, Richard T. (Inventor); Hunter, Norwood R. (Inventor); Caputo, Michael P. (Inventor); Gibson, C. Robert (Inventor)

    1992-01-01

    A portable diagnostic image analysis instrument is disclosed for retinal funduscopy in which an eye fundus image is optically processed by a lens system to a charge coupled device (CCD) which produces recordable and viewable output data and is simultaneously viewable on an electronic view finder. The fundus image is processed to develop a representation of the vessel or vessels from the output data.

  6. Portable Suction Lysimeter

    DOEpatents

    Hubbell, Joel M.; Sisson, James B.

    2004-07-13

    A portable lysimeter including a collection vessel having an inflatable bladder and a semi-permeable member assembly at least partially movable in response to inflation of the bladder, a sample conduit in fluid communication with the semi-permeable member and a reservoir in fluid communication with the sample conduit.

  7. Portable Chamfering Tool

    NASA Technical Reports Server (NTRS)

    Berson, Leo A.

    1987-01-01

    Portable machine tool precisely cuts chamfer on valve seat. With tool, delicate machining operation done without removing part to machine shop. Taken to part and used wherever pressurized air and electric power available. Plug and bushing nest in bore chamfered. They guide steady cutter rod as it cuts 15 degrees chamfer on top edge of bore.

  8. Portable oven air circulator

    DOEpatents

    Jorgensen, Jorgen A.; Nygren, Donald W.

    1983-01-01

    A portable air circulating apparatus for use in cooking ovens which is used to create air currents in the oven which transfer heat to cooking foodstuffs to promote more rapid and more uniform cooking or baking, the apparatus including a motor, fan blade and housing of metallic materials selected from a class of heat resistant materials.

  9. Mobility, Portability, and Placelessness

    ERIC Educational Resources Information Center

    Kupfer, Joseph

    2007-01-01

    Electronic technology has created a revolution in portability of information, documentation, and communication. We are now able to connect with people, information, organizations, and merchandise from anywhere at practically any time. As electronically fabricated environments replace actual physical surroundings, however, we become displaced.…

  10. Portable Weld Tester.

    ERIC Educational Resources Information Center

    Eckert, Douglas

    This training manual, which was developed for employees of an automotive plant, is designed to teach trainees to operate a portable weld tester (Miyachi MM-315). In chapter 1, the weld tester's components are illustrated and described, and the procedure for charging its batteries is explained. Chapter 2 illustrates the weld tester's parts,…

  11. PORTABLE SOURCE OF RADIOACTIVITY

    DOEpatents

    Goertz, R.C.; Ferguson, K.R.; Rylander, E.W.; Safranski, L.M.

    1959-06-16

    A portable source for radiogiaphy or radiotherapy is described. It consists of a Tl/sup 170/ or Co/sup 60/ source mounted in a rotatable tungsten alloy plug. The plug rotates within a brass body to positions of safety or exposure. Provision is made for reloading and carrying the device safely. (T.R.H.)

  12. Portable Aerosol Contaminant Extractor

    DOEpatents

    Carlson, Duane C.; DeGange, John J.; Cable-Dunlap, Paula

    2005-11-15

    A compact, portable, aerosol contaminant extractor having ionization and collection sections through which ambient air may be drawn at a nominal rate so that aerosol particles ionized in the ionization section may be collected on charged plate in the collection section, the charged plate being readily removed for analyses of the particles collected thereon.

  13. Portable Lifting Seat

    NASA Technical Reports Server (NTRS)

    Weddendorf, Bruce

    1993-01-01

    Portable lifting machine assists user in rising from seated position to standing position, or in sitting down. Small and light enough to be carried like briefcase. Used on variety of chairs and benches. Upholstered aluminum box houses mechanism of lifting seat. Springs on outer shaft-and-arm subassembly counterbalance part of user's weight to assist motor.

  14. Portable sensor for hazardous waste

    SciTech Connect

    Piper, L.G.; Hunter, A.J.R.; Fraser, M.E.; Davis, S.J.

    1996-12-31

    We are part-way through the second phase of a 4-year program designed to develop a portable monitor for sensitive hazardous waste detection. The ultimate goal of the program is to develop our concept to the prototype instrument level. Our monitor will be a compact, portable instrument that will allow real-time, in situ, monitoring of hazardous wastes. This instrument will be able to provide the means for rapid field screening of hazardous waste sites to map the areas of greatest contamination. Remediation efforts can then focus on these areas. Our analysis approach is to excite atomic and molecular fluorescence by the technique of active nitrogen energy transfer (ANET). The active nitrogen is made in a dielectric-barrier (D-B) discharge in nitrogen at atmospheric pressure. Only a few emission lines or bands are excited for each hazardous species, so spectral resolution requirements are greatly simplified over those of other spectroscopic techniques. The D-B discharge is compact, 1 to 2 cm in diameter and 1 to 10 cm long. Furthermore, the discharge power requirements are quite modest, so that the unit can be powered by batteries. Thus an instrument based on ANET can readily be made portable. Our results indicate that ANET is a very sensitive technique for monitoring heavy metals and chlorinated hydrocarbons. We have demonstrated an overall detection sensitivity for most species that is at or below ppb levels. ANET alone, however, appears to be most successful in treating hazardous species that have been atomized. We are therefore developing a hybrid technique which combines a miniature, solid-state laser for sample collection and vaporization with ANET for subsequent detection. This approach requires no special sample preparation, can operate continuously, and lends itself well to compact packaging.

  15. Development of Portable Beta Spectrometer for Sr-90 Activity Measurements in Field Conditions and Its Application in Rehabilitation Activities at RRC Kurchatov Institute

    SciTech Connect

    Potapov, V.N.; Volkovich, A.G.; Ivanov, O.P.; Stepanov, V.E.; Smirnov, S.V.; Volkov, V.G.

    2006-07-01

    A new method to measure the Sr-90 ground specific activity in situ was developed. It is based on the count-rates determination in selected energy ranges of two registered apparatus spectra: total {beta} + {gamma} spectrum and {gamma} spectrum. A numerical simulation of the detector performance defined these energy ranges used for calculation of activity. For implementation of the proposed method a portable instrument was developed and manufactured. Parameters of the instrument are the following: the range of measurement for a specific activity mode - (60 - 3.0x10{sup 6}) Bq/kg; the range for total activity countable mode (0.5 - 2.0x10{sup 4}) Bq; minimum measurable specific activity Sr-90 for samples containing natural radionuclides - 60 Bq/kg, minimum measurable activity for samples not containing NRN - 0.5 Bq. (authors)

  16. Hand-portable liquid chromatographic instrumentation.

    PubMed

    Sharma, Sonika; Tolley, Luke T; Tolley, H Dennis; Plistil, Alex; Stearns, Stanley D; Lee, Milton L

    2015-11-20

    Over the last four decades, liquid chromatography (LC) has experienced an evolution to smaller columns and particles, new stationary phases and low flow rate instrumentation. However, the development of person-portable LC has not followed, mainly due to difficulties encountered in miniaturizing pumps and detectors, and in reducing solvent consumption. The recent introduction of small, non-splitting pumping systems and UV-absorption detectors for use with capillary columns has finally provided miniaturized instrumentation suitable for high-performance hand-portable LC. Fully integrated microfabricated LC still remains a significant challenge. Ion chromatography (IC) has been successfully miniaturized and applied for field analysis; however, applications are mostly limited to inorganic and small organic ions. This review covers advancements that make possible more rapid expansion of portable forms of LC and IC. PMID:26592464

  17. The Application of Physiologically Based Pharmacokinetic Modeling to Determine Route-Specific Contributions to Tissue Dosimetry of Trihalomethanes in Drinking Water

    EPA Science Inventory

    This project summary describes an improved approach for estimating route-specific exposures and tissue doses for trihalomethane (THM) compounds found in drinking water.

  1. Influence of Water Table Depth on Pore Water Chemistry and Trihalomethane Formation Potential in Peatlands.

    PubMed

    Gough, Rachel; Holliman, Peter J; Fenner, Nathalie; Peacock, Mike; Freeman, Christopher

    2016-02-01

    Drained peatland catchments are reported to produce more colored, dissolved organic carbon (DOC)-rich water, presenting problems for potable water treatment. The blocking of peatland drainage ditches to restore the water table is increasingly being considered as a strategy to address this deterioration in water quality. However, the effect of ditch blocking on the potential of DOC to form trihalomethanes (THMs) has not been assessed. In this study, the effect of peat rewetting on pore water DOC concentration and characteristics (including THM formation potential [THMFP]) was assessed over 12 months using peat cores collected from two drained peatland sites. The data show little evidence of differences in DOC concentration or characteristics between the different treatments. The absence of any difference in the THMFP of pore water between treatments suggests that, in the short term at least, ditch blocking may not have an effect on the THMFP of waters draining peatland catchments. PMID:26803099

  2. Removal of trihalomethanes from aqueous solution through armchair carbon nanotubes: a molecular dynamics study.

    PubMed

    Azamat, Jafar; Khataee, Alireza; Joo, Sang Woo; Yin, Binfeng

    2015-04-01

    Molecular dynamics simulations were performed to investigate the removal of trihalomethanes (THMs) including CH3Cl, CH2Cl2 and CHCl3 from aqueous solutions by armchair carbon nanotubes (CNTs) under induced pressure. The studied system involved the armchair CNTs embedded between two graphene sheets with an aqueous solution of THMs in the simulation box. An external pressure was applied to the system along the z-axis of the simulation box. Six types of armchair CNTs with different diameter were used in this work, included (4,4), (5,5), (6,6), (7,7), (8,8) and (9,9) CNTs. The results of molecular dynamics simulation display that the armchair CNTs behave differently relative to THMs and water molecules. The permeation of THMs and water molecules through the armchair CNTs was dependent on the diameter of CNTs and the applied pressure. PMID:25682360

  3. Molecular dynamics simulations of trihalomethanes removal from water using boron nitride nanosheets.

    PubMed

    Azamat, Jafar; Khataee, Alireza; Joo, Sang Woo

    2016-04-01

    Molecular dynamics simulations were performed to investigate the separation of trihalomethanes (THMs) from water using boron nitride nanosheets (BNNSs). The studied systems included THM molecules and a functionalized BNNS membrane immersed in an aqueous solution. An external pressure was applied to the z axis of the systems. Two functionalized BNNSs with large fluorinated-hydrogenated pore (F-H-pores) and small hydrogen-hydroxyl pore (H-OH-pores) were used. The pores of the BNNS membrane were obtained by passivating each nitrogen and boron atoms at the pore edges with fluorine and hydrogen atoms in the large pore or with hydroxyl and hydrogen atoms in the small pore. The results show that the BNNS with a small functionalized pore was impermeable to THM molecules, in contrast to the BNNS with a large functionalized pore. Using these membranes, water contaminants can be removed at lower cost. PMID:26983611

  4. Formation of trihalomethanes of dissolved organic matter fractions in reservoir and canal waters.

    PubMed

    Musikavong, Charongpun; Srimuang, Kanjanee; Tachapattaworakul Suksaroj, Thunwadee; Suksaroj, Chaisri

    2016-07-28

    The formation of trihalomethanes (THMs) of hydrophobic organic fraction (HPO), transphilic organic fraction (TPI), and hydrophilic organic fraction (HPI) of reservoir and canal waters from the U-Tapao River Basin, Songkhla, Thailand was investigated. Water samples were collected three times from two reservoirs, upstream, midstream, and downstream of the U-Tapao canal. The HPO was the major dissolved organic matter (DOM) fraction in reservoir and canal waters. On average, the HPO accounted for 53 and 45% of the DOM in reservoir and canal waters, respectively. The TPI of 19 and 23% in reservoir and canal waters were determined, respectively. The HPI of 29% of the reservoir water and HPI of 32% of the canal water were detected. For the reservoir water, the highest trihalomethane formation potential (THMFP)/dissolved organic carbon (DOC) was determined for the HPI, followed by the TPI and HPO, respectively. The average values of the THMFP/DOC of the HPI, TPI, and HPO of the reservoir water were 78, 52, and 49 µg THMs/mg C, respectively. The highest THMFP/DOC of the canal water was detected for the HPI, followed by HPO and TPI, respectively. Average values of the THMFP/DOC of HPI of water at upstream and midstream locations of 58 µg THMs/mg C and downstream location of 113 µg THMs/mg C were determined. Average values of THMFP/DOC of HPO of water at upstream and midstream and downstream locations were 48 and 93 µg THMs/mg C, respectively. For the lowest THMFP/DOC fraction, the average values of THMFP/DOC of TPI of water at upstream and midstream and downstream locations were 35 and 73 µg THMs/mg C, respectively. PMID:27166524

  5. The impact of bromide/iodide concentration and ratio on iodinated trihalomethane formation and speciation.

    PubMed

    Jones, Darryl B; Saglam, Aysenur; Song, Hocheol; Karanfil, Tanju

    2012-01-01

    The objective of this study was to evaluate the formation and speciation of iodinated trihalomethanes (I-THMs) from preformed chloramination of waters containing bromide (Br(-)) and iodide (I(-)) at a Br(-)/I(-) weight ratio of 10:1. The factors investigated were pH, iodide to dissolved organic carbon (I(-)/DOC) ratio, and NOM characteristics, specifically SUVA(254). A Br(-)/I(-) ratio of 1:2 was also evaluated to determine the importance of Br(-) and I(-) concentrations and ratio on I-THM formation and speciation. Regulated triholamethanes (THMs) were measured alongside I-THMs for a more complete understanding of trihalomethane formation. The results showed that, in general, both I-THM and THM formation increased with decreased pH. Greater formation at lower pH was likely attributed to monochloramine decomposition and the formation of additional oxidants and substituting agents, most notably chlorine. For pH ≥ 7.5, I-THM yield increased with increasing I(-)/DOC ratio and decreasing specific ultraviolet absorbance (SUVA(254)) of the water. The Br(-)/I(-), Br(-)/DOC and I(-)/DOC ratios were important factors for I-THM and THM speciation. At pH 6, dichloroiodomethane (CHCl(2)I) and bromochloroiodomethane (CHBrClI) were the dominant species at the common bromide and iodide levels. For pH ≥ 7.5 and for elevated bromide and iodide levels, iodoform (CHI(3)) was always the dominant specie regardless of the Br(-)/I(-) ratio. The results demonstrated that it is important to examine I-THM formation and speciation at typical Br(-)/I(-) ratios (≈ 10) of natural waters, which have often been overlooked in previous investigations, in order to obtain practical and relevant results. PMID:22078225

  6. Alveolar breath sampling and analysis to assess trihalomethane exposures during competitive swimming training.

    PubMed Central

    Lindstrom, A B; Pleil, J D; Berkoff, D C

    1997-01-01

    Alveolar breath sampling was used to assess trihalomethane (THM) exposures encountered by collegiate swimmers during a typical 2-hr training period in an indoor natatorium. The breath samples were collected at regular intervals before, during, and for 3 hr after a moderately intense training workout. Integrated and grab whole-air samples were collected during the training period to help determine inhalation exposures, and pool water samples were collected to help assess dermal exposures. Resulting breath samples collected during the workout demonstrated a rapid uptake of two THMs (chloroform and bromodichloromethane), with chloroform concentrations exceeding the natatorium air levels within 8 min after the exposure began. Chloroform levels continued to rise steeply until they were more than two times the indoor levels, providing evidence that the dermal route of exposure was relatively rapid and ultimately more important than the inhalation route in this training scenario. Chloroform elimination after the exposure period was fitted to a three compartment model that allowed estimation of compartmental half-lives, resulting minimum bloodborne dose, and an approximation of the duration of elevated body burdens. We estimated the dermal exposure route to account for 80% of the blood chloroform concentration and the transdermal diffusion efficiency from the water to the blood to in excess of 2%. Bromodichloromethane elimination was fitted to a two compartment model which provided evidence of a small, but measurable, body burden of this THM resulting from vigorous swim training. These results suggest that trihalomethane exposures for competitive swimmers under prolonged, high-effort training are common and possibly higher than was previously thought and that the dermal exposure route is dominant. The exposures and potential risks associated with this common recreational activity should be more thoroughly investigated. Images Figure 1. Figure 2. Figure 3. Figure 4. Figure

  7. Portable outgas detection apparatus

    SciTech Connect

    Haney, Steven Julian; Malinowski, Michael E.

    2004-05-11

    A portable device for detecting surface outgas contaminants of an article includes: (i) a portable housing that has a chamber which is in communication with a port that is adapted to be sealably attached to a surface of the article; (ii) a mass spectrometer that is coupled to the chamber for analyzing gaseous materials in the chamber; and (iii) means for generating a vacuum within the chamber thereby drawing outgas contaminants from the surface of the article into the chamber for analysis by the mass spectrometer. By performing a mass spectrometric analysis of the surface of interest and comparing the data with mass spectrometric data ascertained with the device from a clean surface, the type and amount of outgas contaminants, if any, can be determined.

  8. Portable Laser Laboratory

    SciTech Connect

    Weir, J.T.

    1994-07-01

    A Portable Laser Laboratory (PLL) is being designed and built for the CALIOPE Program tests which will begin in October of 1994. The PLL is designed to give maximum flexibility for evolving laser experiments and can be readily moved by loading it onto a standard truck trailer. The internal configuration for the October experiments will support a two line DIAL system running in the mid-IR. Brief descriptions of the laser and detection systems are included.

  9. Portable Planetariums Teach Science

    NASA Technical Reports Server (NTRS)

    2015-01-01

    With the Internet proving to be the wave of the future, in the 1990s Johnson Space Center awarded grants to Rice University in Houston for developing the world's first Internet-accessible museum kiosk. Further grants were awarded to the school for creating educational software for use in homes and schools, leading to the creation of Museums Teaching Planet Earth Inc. The company has gone on to develop and sell portable planetariums and accompanying educational shows.

  10. Portable cutting apparatus

    DOEpatents

    Gilmore, R.F.

    1984-07-17

    A remotely operable, portable cutting apparatus detachably secured to the workpiece by laterally spaced clamp assemblies engagable with the workpiece on opposite sides of the intended line of cut. A reciprocal cutter head is mounted between the clamp assemblies and is provided with a traveling abrasive cutting wire adapted to sever the workpiece normal to the longitudinal axis thereof. Dust and debris are withdrawn from the cutting area by a vacuum force through a nozzle mounted on the cutting head.

  11. Portable cutting apparatus

    DOEpatents

    Gilmore, Richard F.

    1986-04-01

    A remotely operable, portable cutting apparatus detachably secured to the workpiece by laterally spaced clamp assemblies engageable with the workpiece on opposite sides of the intended line of cut. A reciprocal cutter head is mounted between the clamp assemblies and is provided with a traveling abrasive cutting wire adapted to sever the workpiece normal to the longitudinal axis thereof. Dust and debris are withdrawn from the cutting area by a vacuum force through a nozzle mounted on the cutting head.

  12. Portable cutting apparatus

    DOEpatents

    Gilmore, Richard F.

    1986-01-01

    A remotely operable, portable cutting apparatus detachably secured to the workpiece by laterally spaced clamp assemblies engageable with the workpiece on opposite sides of the intended line of cut. A reciprocal cutter head is mounted between the clamp assemblies and is provided with a traveling abrasive cutting wire adapted to sever the workpiece normal to the longitudinal axis thereof. Dust and debris are withdrawn from the cutting area by a vacuum force through a nozzle mounted on the cutting head.

  13. Portable Spray Booth

    NASA Technical Reports Server (NTRS)

    Hansen, Timothy D.; Bardwell, Micheal J.

    1996-01-01

    Portable spray booth provides for controlled application of coating materials with high solvent contents. Includes contoured shroud and carbon filter bed limiting concentration of fumes in vicinity. Designed to substitute spraying for brush application of solvent-based adhesive prior to installing rubber waterproof seals over joints between segments of solid-fuel rocket motor. With minor adjustments and modifications, used to apply other solvent-based adhesives, paints, and like.

  14. Field measurements of biogenic volatile organic compounds in the atmosphere by dynamic solid-phase microextraction and portable gas chromatography-mass spectrometry

    NASA Astrophysics Data System (ADS)

    Barreira, Luís Miguel Feijó; Parshintsev, Jevgeni; Kärkkäinen, Niina; Hartonen, Kari; Jussila, Matti; Kajos, Maija; Kulmala, Markku; Riekkola, Marja-Liisa

    2015-08-01

    Biogenic volatile organic compounds (BVOCs) participate in many physicochemical processes in the atmosphere. Studies indicate that some of these volatile compounds can be photo-oxidized to non-volatile species that contribute to atmospheric formation and growth of secondary organic aerosols (SOA). In this study, the applicability of dynamic solid-phase microextraction (SPME) for the sampling of atmospheric BVOCs and their oxidation products was tested. These compounds were then analysed via portable gas chromatography-mass spectrometry (GC-MS). The measurements were performed in mid-summer 2013 at the Station for Measuring Ecosystem-Atmosphere Relations, SMEAR II in Hyytiälä, Finland. Numerous classes of compounds were efficiently sampled on PDMS/DVB coated SPME, thermally desorbed and analysed by GC-MS, including monoterpenes, their oxidation products, and amines. Results were analysed against meteorological conditions observed during the sampling campaign and the total amount of monoterpenes obtained by proton-transfer-reaction mass spectrometry (PTR-MS). The comparison of the referred data with obtained results demonstrated the capability of the dynamic SPME method for fast in-situ sampling and analysis of organic gaseous compounds in the atmosphere with minimal analytical steps.

  15. Military display market segment: wearable and portable

    NASA Astrophysics Data System (ADS)

    Desjardins, Daniel D.; Hopper, Darrel G.

    2003-09-01

    The military display market (MDM) is analyzed in terms of one of its segments, wearable and portable displays. Wearable and portable displays are those embedded in gear worn or carried by warfighters. Categories include hand-mobile (direct-view and monocular/binocular), palm-held, head/helmet-mounted, body-strapped, knee-attached, lap-born, neck-lanyard, and pocket/backpack-stowed. Some 62 fielded and developmental display sizes are identified in this wearable/portable MDM segment. Parameters requiring special consideration, such as weight, luminance ranges, light emission, viewing angles, and chromaticity coordinates, are summarized and compared. Ruggedized commercial versus commercial off-the-shelf designs are contrasted; and a number of custom displays are also found in this MDM category. Display sizes having aggregate quantities of 5,000 units or greater or having 2 or more program applications are identified. Wearable and portable displays are also analyzed by technology (LCD, LED, CRT, OLED and plasma). The technical specifications and program history of several high-profile military programs are discussed to provide a systems context for some representative displays and their function. As of August 2002 our defense-wide military display market study has documented 438,882 total display units distributed across 1,163 display sizes and 438 weapon systems. Wearable and portable displays account for 202,593 displays (46% of total DoD) yet comprise just 62 sizes (5% of total DoD) in 120 weapons systems (27% of total DoD). Some 66% of these wearable and portable applications involve low information content displays comprising just a few characters in one color; however, there is an accelerating trend towards higher information content units capable of showing changeable graphics, color and video.

  16. Portable vapor diffusion coefficient meter

    DOEpatents

    Ho, Clifford K.

    2007-06-12

    An apparatus for measuring the effective vapor diffusion coefficient of a test vapor diffusing through a sample of porous media contained within a test chamber. A chemical sensor measures the time-varying concentration of vapor that has diffused a known distance through the porous media. A data processor contained within the apparatus compares the measured sensor data with analytical predictions of the response curve based on the transient diffusion equation using Fick's Law, iterating on the choice of an effective vapor diffusion coefficient until the difference between the predicted and measured curves is minimized. Optionally, a purge fluid can forced through the porous media, permitting the apparatus to also measure a gas-phase permeability. The apparatus can be made lightweight, self-powered, and portable for use in the field.

  17. Compact portable electric power sources

    SciTech Connect

    Fry, D.N.; Holcomb, D.E.; Munro, J.K.; Oakes, L.C.; Matson, M.J.

    1997-02-01

    This report provides an overview of recent advances in portable electric power source (PEPS) technology and an assessment of emerging PEPS technologies that may meet US Special Operations Command`s (SOCOM) needs in the next 1--2- and 3--5-year time frames. The assessment was performed through a literature search and interviews with experts in various laboratories and companies. Nineteen PEPS technologies were reviewed and characterized as (1) PEPSs that meet SOCOM requirements; (2) PEPSs that could fulfill requirements for special field conditions and locations; (3) potentially high-payoff sources that require additional R and D; and (4) sources unlikely to meet present SOCOM requirements. 6 figs., 10 tabs.

  18. Effect of powdered activated carbon (PAC) on MBR performance and effluent trihalomethane formation: At the initial stage of PAC addition.

    PubMed

    Gao, Yue; Ma, Defang; Yue, Qinyan; Gao, Baoyu; Huang, Xia

    2016-09-01

    In this study, the MBR was used to treat municipal wastewater for reuse. Effects of powdered activated carbon (PAC) addition on MBR system in terms of effluent water quality, trihalomethane (THM) formation and membrane organic fouling tendency of MBR sludge supernatant at the initial stage of PAC addition were investigated. Effects of chlorine dose and contact time on THM formation and speciation were also studied. PAC addition enhanced the removal of organic matters, especially aromatic components, which improved the UV254 removal rate from 34% to 83%. PAC addition greatly reduced the membrane organic fouling tendency of MBR sludge supernatant. PAC addition reduced the MBR effluent trihalomethane formation potential (THMFP) from 351.29 to 241.95μg/L, while increased THM formation reactivity by 42%. PAC addition enhanced the formation of higher toxic bromine-containing THMs. High chlorine dose and contact time resulted in higher THM formation but lower proportion of bromine-containing THMs. PMID:27318162

  19. PORTABLE ACOUSTIC MONITORING PACKAGE (PAMP)

    SciTech Connect

    John l. Loth; Gary J. Morris; George M. Palmer; Richard Guiler; Deepak Mehra

    2003-07-01

    The 1st generation acoustic monitoring package was designed to detect and analyze weak acoustic signals inside natural gas transmission lines. Besides a microphone it housed a three-inch diameter aerodynamic acoustic signal amplifier to maximize sensitivity to leak induced {Delta}p type signals. The theory and test results of this aerodynamic signal amplifier was described in the master's degree thesis of our Research Assistant Deepak Mehra who is about to graduate. To house such a large three-inch diameter sensor required the use of a steel 300-psi rated 4 inch weld neck flange, which itself weighed already 29 pounds. The completed 1st generation Acoustic Monitoring Package weighed almost 100 pounds. This was too cumbersome to mount in the field, on an access port at a pipeline shut-off valve. Therefore a 2nd generation and truly Portable Acoustic Monitor was built. It incorporated a fully self-contained {Delta}p type signal sensor, rated for line pressures up to 1000 psi with a base weight of only 6 pounds. This is the Rosemont Inc. Model 3051CD-Range 0, software driven sensor, which is believed to have industries best total performance. Its most sensitive unit was purchased with a {Delta}p range from 0 to 3 inch water. This resulted in the herein described 2nd generation: Portable Acoustic Monitoring Package (PAMP) for pipelines up to 1000 psi. Its 32-pound total weight includes an 18-volt battery. Together with a 3 pound laptop with its 4-channel data acquisition card, completes the equipment needed for field acoustic monitoring of natural gas transmission pipelines.

  20. Portable emittance measurement device

    SciTech Connect

    Liakin, D.; Seleznev, D.; Orlov, A.; Kuibeda, R.; Kropachev, G.; Kulevoy, T.; Yakushin, P.

    2010-02-15

    In Institute for Theoretical and Experimental Physics (ITEP) the portable emittance measurements device is developed. It provides emittance measurements both with ''pepper-pot'' and ''two slits'' methods. Depending on the method of measurements, either slits or pepper-pot mask with scintillator are mounted on the two activators and are installed in two standard Balzer's cross chamber with CF-100 flanges. To match the angle resolution for measured beam, the length of the stainless steel pipe between two crosses changes is adjusted. The description of the device and results of emittance measurements at the ITEP ion source test bench are presented.

  1. Portable data collection device

    DOEpatents

    French, Patrick D.

    1996-01-01

    The present invention provides a portable data collection device that has a variety of sensors that are interchangeable with a variety of input ports in the device. The various sensors include a data identification feature that provides information to the device regarding the type of physical data produced by each sensor and therefore the type of sensor itself. The data identification feature enables the device to locate the input port where the sensor is connected and self adjust when a sensor is removed or replaced. The device is able to collect physical data, whether or not a function of a time.

  2. Portable pathogen detection system

    DOEpatents

    Colston, Billy W.; Everett, Matthew; Milanovich, Fred P.; Brown, Steve B.; Vendateswaran, Kodumudi; Simon, Jonathan N.

    2005-06-14

    A portable pathogen detection system that accomplishes on-site multiplex detection of targets in biological samples. The system includes: microbead specific reagents, incubation/mixing chambers, a disposable microbead capture substrate, and an optical measurement and decoding arrangement. The basis of this system is a highly flexible Liquid Array that utilizes optically encoded microbeads as the templates for biological assays. Target biological samples are optically labeled and captured on the microbeads, which are in turn captured on an ordered array or disordered array disposable capture substrate and then optically read.

  3. Portable wastewater flow meter

    DOEpatents

    Hunter, Robert M.

    1999-02-02

    A portable wastewater flow meter particularly adapted for temporary use at a single location in measuring the rate of liquid flow in a circular entrance conduit of a sewer manhole both under free flow and submerged, open channel conditions and under fill pipe, surcharged conditions, comprising an apparatus having a cylindrical external surface and an inner surface that constricts the flow through the apparatus in such a manner that a relationship exists between (1) the difference between the static pressure head of liquid flowing through the entrance of the apparatus and the static pressure head of liquid flowing through the constriction, and (2) the rate of liquid flow through the apparatus.

  4. Portable wastewater flow meter

    DOEpatents

    Hunter, Robert M.

    1990-01-01

    A portable wastewater flow meter particularly adapted for temporary use at a single location in measuring the rate of liquid flow in a circular entrance conduit of a sewer manhole both under free flow and submerged, open channel conditions and under full pipe, surcharged conditions, comprising an apparatus having a cylindrical external surface and an inner surface that constricts the flow through the apparatus in such a manner that a relationship exists between (1) the difference between the static pressure head of liquid flowing through the entrance of the apparatus and the static pressure head of liquid flowing through the constriction, and (2) the rate of liquid flow through the apparatus.

  5. Portable Extensible Viewer

    NASA Technical Reports Server (NTRS)

    Horowitz, Jay G.

    1997-01-01

    The use of Nonuniform Rational B-Splines (NURBS) to represent geometry and data offers a standard way to facilitate the multidisciplinary analysis and design of aeropropulsion products. Using standard geometry defined by NURBS throughout design, analysis, part definition, manufacture, and test processes saves money and time. The Portable Extensible Viewer (PEV) offers engineers of different disciplines a means to view and manipulate NURBS geometry and associated data. Under the guidance of a team of Lewis, Boeing Company, and Navy personnel, PEV was developed by NASA Lewis Research Center's Computer Services Division for Lewis' Interdisciplinary Technology Office. The aeropropulsion industry provided input to the design requirements.

  6. Portable data collection device

    DOEpatents

    French, P.D.

    1996-06-11

    The present invention provides a portable data collection device that has a variety of sensors that are interchangeable with a variety of input ports in the device. The various sensors include a data identification feature that provides information to the device regarding the type of physical data produced by each sensor and therefore the type of sensor itself. The data identification feature enables the device to locate the input port where the sensor is connected and self adjust when a sensor is removed or replaced. The device is able to collect physical data, whether or not a function of a time. 7 figs.

  7. Portable hydrogenerating apparatus

    SciTech Connect

    Borgren, P.M.

    1982-04-13

    Apparatus for generating hydroelectric power comprising a portable collector tube assembly which can be transported to the site of a water source having a waterfall sufficient in magnitude to provide a pressure head for driving a turbine generator. The tube assembly comprises telescopically arranged inner and outer tubes, and means for rotating the tube assembly and extending the inner tube so as to place the upper, extended end thereof in a position within and below the top of the waterfall so as to take advantage of the resulting hydrodynamic and hydrostatic forces.

  8. Application of hollow fiber liquid phase microextraction for simultaneous determination of regulated and emerging iodinated trihalomethanes in drinking water.

    PubMed

    Domínguez-Tello, A; Arias-Borrego, A; García-Barrera, T; Gómez-Ariza, J L

    2015-07-10

    Trihalomethanes (THMs) are regulated disinfection by-products (DBPs) most commonly analyzed in quality control water supply due to their harmful effects on health. However, few data exist about the content of emerging iodo-trihalomethanes (I-THMs) which are present in drinking water at very low concentrations (in the order of ngL(-1)). For this reason a two-phase hollow fiber liquid phase microextraction method for the simultaneous determination of four regulated trihalomethanes and six emerging iodo-trihalomethanes using GC-μECD and GC-MS with detection limits in the range of few ngL(-1) has been developed. A central composite design was used to optimize conditions for simultaneous extraction. The best extraction recovery was obtained with 19.2min at 27.1°C and 900rpm, without salt addition, using a supported hollow fiber membrane of 10.5cm (0.6mm id) and 1-octanol as acceptor phase. The limits of detection for the regulated THMs and I-THMs were 3-44ngL(-1) and 1-3ngL(-1), respectively. The calibration curves showed good linearity (R(2)>0.995) and good repeatibility (3-22%). The relative recoveries in water were between 96.5% and 105.2%. The method was applied for the simultaneous determination of trihalomethanes in supply water samples from seven water distribution systems (WDS) in the Huelva area, located at the southwest Spain, which use different water-treatment processes. The highest concentrations of I-THMs, particularly CHBrClI and CHCl2I, were detected in water treated with advanced treatment process using pre-ozonation, however these compounds were not detected or decreased along distribution system. In the samples of treated water with conventional treatment, using pre-oxidation by permanganate and distribution network, CHCl2I, CHBrClI, CHClI2, CHBrI2 and CHI3 were detected at very low concentrations (1-18ngL(-1)). Finally, in water samples from underground origin without oxidation treatment, in which only disinfection with sodium hypochlorite was

  9. [Theoretical and Experimental Dosimetry in Evaluation of Biological Effects of Electromagnetic Field for Portable Radio Transmitters. Report 2. Homogeneous Human Head Phantom].

    PubMed

    Perov, S Yu; Bogacheva, E V

    2015-01-01

    Results of theoretical (numerical) and experimental electromagnetic field dosimetry for homogeneous human head phantoms are considered. The simulation and measurement results are shown. This paper presents the results of Specific Absorption Rate (SAR) evaluation in the "special anthropomorphic model" of human head, when a source of electromagnetic radio frequency field is placed in front of the face. The minimal difference is shown between measurements and simulation results in Head Simulating Liquid, which makes it possible to conduct further brain tissue simulations. The investigations show that the type of electromagnetic field source and phantom form play an important part for SAR distribution. PMID:26601543

  10. Power to the portables.

    PubMed

    Specthrie, L; Berg, W; Fishman, S; Walker, L; Gapay, L

    1992-08-01

    Portable computing devices generally are classified into four categories: laptop, palmtop, notebook, and pen-based computers. If a portable unit weighs over eight pounds, call it a laptop. If a stylus is used to input data, call it pen-based or a pen computer. Palmtops frequently are electronic organizers or resources: Sharp's Wizard line stores appointments and addresses; Franklin's Med-Spell contains Stedman's medical dictionary. Notebooks often incorporate a QWERT keyboard, and sometimes include a pointing device. NEC's notebooks in 1988 were the first sub-laptop computers. According to a 1992 report from Market Intelligence Research Corp., Mountain View, Calif., 4.6 million sub-laptops were sold in 1991 for $2.6 billion. By 1998 the market may reach $25 billion. The report predicts that one sub-category of pen computers, which are designed to be held in one hand while information is input with a pen-like stylus, will prove most useful to the health-care industry. Pen tablets, as opposed to pen clipboards, use faster, more expensive processors, store more data, and "are expected to allow [caregivers] to carry full patient charting with them ... and allow information to be recorded directly to patient files." Sub-laptops are on-line in many healthcare facilities: Greenwich hospital, Stanford University Medical Clinic, Humana Hospital Audubon, Rancho Los Amigos Medical Center, and others. PMID:10121047

  11. The Evaluation of Two Commercially Available, Portable Raman Systems

    PubMed Central

    Mosier-Boss, Pamela A.; Putnam, Michael D.

    2013-01-01

    Raman spectroscopy and surface enhanced Raman spectroscopy (SERS) have many attributes that make them attractive for field detection of environmental contaminants, industrial process control, as well as materials detection/identification in agriculture, pharmaceuticals, law enforcement/first responders, geology, and archeology. However, portable, robust, inexpensive Raman systems are required for these applications. In this communication, the performances of two commercially available, portable Raman systems are evaluated. PMID:24115834

  12. PEMS (PORTABLE EMISSONS MEASUREMENT SYSTEM)

    EPA Science Inventory

    PEMS is a generic term that encompasses all portable emissions measurement systems. Two EPA-developed examples are ROVER (Real-time On-Vehicle Emissions Reporter) for on-highway applications, and SPOT (Simple Portable On-vehicle Tester) for non-road applications. Now, however, ...

  13. Detecting trihalomethanes using nanoporous-carbon coated surface-acoustic-wave sensors

    DOE PAGESBeta

    Siegal, Michael P.; Mowry, Curtis D.; Pfeifer, Kent B.; Gallis, Dorina F. S.

    2015-03-07

    We study nanoporous-carbon (NPC) grown via pulsed laser deposition (PLD) as a sorbent coating on 96.5-MHz surface-acoustic-wave (SAW) devices to detect trihalomethanes (THMs), regulated byproducts from the chemical treatment of drinking water. Using both insertion-loss and isothermal-response measurements from known quantities of chloroform, the highest vapor pressure THM, we optimize the NPC mass-density at 1.05 ± 0.08 g/cm3 by controlling the background argon pressure during PLD. Precise THM quantities in a chlorobenzene solvent are directly injected into a separation column and detected as the phase-angle shift of the SAW device output compared to the drive signal. Using optimized NPC-coated SAWs,more » we study the chloroform response as a function of operating temperatures ranging from 10–50°C. Finally, we demonstrate individual responses from complex mixtures of all four THMs, with masses ranging from 10–2000 ng, after gas chromatography separation. As a result, estimates for each THM detection limit using a simple peak-height response evaluation are 4.4 ng for chloroform and 1 ng for bromoform; using an integrated-peak area response analysis improves the detection limits to 0.73 ng for chloroform and 0.003 ng bromoform.« less

  14. A comparison of iodinated trihalomethane formation from chlorine, chlorine dioxide and potassium permanganate oxidation processes.

    PubMed

    Zhang, Tian-Yang; Xu, Bin; Hu, Chen-Yan; Lin, Yi-Li; Lin, Lin; Ye, Tao; Tian, Fu-Xiang

    2015-01-01

    This study compared the formation of iodinated trihalomethanes (I-THMs) from iodide-containing raw waters oxidized by chlorine, chlorine dioxide (ClO₂) and potassium permanganate (KMnO₄) at different oxidant concentrations, reaction times, pHs, initial iodide concentrations and bromide to iodide mass ratios. Among the six investigated I-THMs, iodoform was the major species formed during the oxidation using chlorine, ClO₂ and KMnO₄. When oxidant concentration increased from 0.1 to 3.0 mg/L, the formation of I-THMs increased and then decreased for chlorine and ClO₂, but kept increasing for KMnO₄. As the reaction time went by, I-THM concentration increased to a plateau within 10 h (ClO₂ within only 1 h, especially) for all the three oxidants. I-THM formation gradually increased from pH 3.0 to 9.0 and remained stable at pH values higher than 7.5 for chlorine; however, for ClO₂ and KMnO₄ the highest I-THM formation showed at pH 7.0 and 7.5, respectively. As initial iodide concentration increased from 20 to 800 μg/L, the total amount and species of I-THMs increased for the three oxidants. Iodide contributed to I-THM formation much more significantly than bromide. PMID:25462746

  15. Human health risk assessment from exposure to trihalomethanes in Canadian cities.

    PubMed

    Chowdhury, Shakhawat; Hall, Kevin

    2010-07-01

    Lifetime exposure to trihalomethanes (THMs) through ingestion, inhalation and dermal contacts may pose risks to human health. Current approaches may under predict THMs exposure by using THMs in cold water during showering and bathing. Warming of chlorinated water during showering may increase THMs formation through reactions between organics and residual chlorine, which can increase human health risks. In this study, THMs concentrations in shower water were estimated using THMs rate increase model. Using cold water THMs, exposure through ingestion was estimated, while THMs exposure during showering was estimated using THMs in warm water. Human health cancer risks and additional expenses for 20 most populated Canadian cities from exposure to THMs were estimated. Inhalation and dermal contact during showering contributed 30% to 50% of total cancer risks, while risks from inhalation and dermal contacts were comparable for all cities. Overall cancer risks were estimated between 7.2 x 10(-6) and 6.4 x 10(-5) for these cities. Cancer incidents were estimated highest for Montreal (94/year) followed by Toronto (53/year), which may require additional medical expenses of 18.8 and 10.7 million dollars/year for Montreal and Toronto respectively. Cancer risks from exposure to THMs can be controlled by reducing THMs in water supply and varying shower stall volume, shower duration and air exchange rate in shower stall. PMID:20434775

  16. Predictors of Third Trimester Blood Trihalomethanes and Urinary Trichloroacetic Acid Concentrations among Pregnant Women.

    PubMed

    Zeng, Qiang; Cao, Wen-Cheng; Zhou, Bin; Yang, Pan; Wang, Yi-Xin; Huang, Zhen; Li, Jin; Lu, Wen-Qing

    2016-05-17

    Prenatal exposure to disinfection byproducts (DBPs) has been associated with a variety of adverse birth outcomes. However, little is known about predictors of prenatal biomarkers of exposure to DBPs among pregnant women. We aimed to identify predictors of third trimester blood trihalomethanes (THMs) and urinary trichloroacetic acid (TCAA) concentrations, two biomarkers of exposure to DBPs, among pregnant women. Blood samples, urine samples, and questionnaires on individual characteristics and water-use activities were collected from 893 pregnant women in a Chinese cohort study. Maternal blood THM [chloroform (TCM), bromodichloromethane (BDCM), dibromochloromethane (DBCM), and bromoform (TBM)] and urinary TCAA concentrations were measured. We used multivariable linear regression to identify the predictors of third trimester blood THM and creatinine-adjusted urinary TCAA concentrations. The geometric mean of blood TTHM (sum of TCM, BDCM, DBCM, and TBM) and creatinine-adjusted urinary TCAA concentrations were 51.90 ng/L and 9.66 μg/g creatinine, respectively. Study city was the strongest significant predictors of blood THM and creatinine-adjusted urinary TCAA concentrations. Prenatal body mass index (BMI) was associated with decreased blood THM and decreased creatinine-adjusted urinary TCAA concentrations. Age was associated with increased blood Br-THM (sum of BDCM, DBCM, and TBM) concentrations. Intake of boiled water and passive smoking were associated with lower blood THM concentrations. The predictors of blood THM and urinary TCAA concentrations identified in this study provide potential health implications on how to reduce DBP exposure during pregnancy. PMID:27095243

  17. Drinking water and pregnancy outcome in central North Carolina: source, amount, and trihalomethane levels.

    PubMed

    Savitz, D A; Andrews, K W; Pastore, L M

    1995-06-01

    In spite of the recognition of potentially toxic chemicals in chlorinated drinking water, few studies have evaluated reproductive health consequences of such exposure. Using data from a case-control study of miscarriage, preterm delivery, and low birth weight in central North Carolina, we evaluated risk associated with water source, amount, and trihalomethane (THM) concentration. Water source was not related to any of those pregnancy outcomes, but an increasing amount of ingested water was associated with decreased risks of all three outcomes (odds ratios around 1.5 for 0 glasses per day relative to 1-3 glasses per day, falling to 0.8 for 4+ glasses per day). THM concentration and dose (concentration x amount) were not related to pregnancy outcome, with the possible exception of an increased risk of miscarriage in the highest sextile of THM concentration (adjusted odds ratio = 2.8, 95% confidence interval = 1.1-2.7), which was not part of an overall dose-response gradient. These data do not indicate a strong association between chlorination by-products and adverse pregnancy outcome, but given the limited quality of our exposure assessment and the increased miscarriage risk in the highest exposure group, more refined evaluation is warranted. PMID:7556013

  18. Effects of operating conditions on trihalomethanes formation and speciation during chloramination in reclaimed water.

    PubMed

    Wang, Fang; Gao, Baoyu; Ma, Defang; Li, Ruihua; Sun, Shenglei; Yue, Qinyan; Wang, Yan; Li, Qian

    2016-01-01

    In this study, a hybrid powdered activated carbon-membrane bioreactor (PAC-MBR) system was used to treat municipal wastewater in northern China intended for recycle. In order to control microbiological hazards in PAC-MBR effluent, chloramine was chosen as the disinfectant which could reduce the disinfection by-product yields. Effects of reaction time, chloramines dose, pH value, and bromide ion concentration on trihalomethanes (THMs) formation and speciation during chloramination of the reclaimed effluent were investigated. Study results indicated that the yield of total THMs (TTHM) increased at higher reaction time and chloramines dose. The trend of growth showed that slow reacting precursors were the main components of dissolved organic matter (DOM) in PAC-MBR effluent. THMs formation potential of PAC-MBR effluent achieved the maximum at chloramines dosage of 20 mg/L. Meanwhile, THMs formation was enhanced evidently under alkaline conditions. The yields of THMs species were in following order: CHCl3 > CHBrCl2 > CHBr2Cl > CHBr3, although in different reaction time, chloramines dose, and pH value. Furthermore, the formation of Br-THMs was promoted by the increasing concentration of bromide ion. PMID:26377970

  19. Trihalomethane formation potential of aquatic and terrestrial fulvic and humic acids: Sorption on activated carbon.

    PubMed

    Abouleish, Mohamed Y Z; Wells, Martha J M

    2015-07-15

    Humic substances (HSs) are precursors for the formation of hazardous disinfection by-products (DBPs) during chlorination of water. Various surrogate parameters have been used to investigate the generation of DBPs by HS precursors and the removal of these precursors by activated carbon treatment. Dissolved organic carbon (DOC)- and ultraviolet absorbance (UVA254)-based isotherms are commonly reported and presumed to be good predictors of the trihalomethane formation potential (THMFP). However, THMFP-based isotherms are rarely published such that the three types of parameters have not been compared directly. Batch equilibrium experiments on activated carbon were used to generate constant-initial-concentration sorption isotherms for well-characterized samples obtained from the International Humic Substances Society (IHSS). HSs representing type (fulvic acid [FA], humic acid [HA]), origin (aquatic, terrestrial), and geographical source (Nordic, Suwannee, Peat, Soil) were examined at pH6 and pH9. THMFP-based isotherms were generated and compared to determine if DOC- and UVA254-based isotherms were good predictors of the THMFP. The sorption process depended on the composition of the HSs and the chemical nature of the activated carbon, both of which were influenced by pH. Activated carbon removal of THM-precursors was pH- and HS-dependent. In some instances, the THMFP existed after UVA254 was depleted. PMID:25847173

  20. Multi-pathway risk assessment of trihalomethanes exposure in Istanbul drinking water supplies.

    PubMed

    Uyak, Vedat

    2006-01-01

    The lifetime cancer risk and the hazard index of trihalomethanes (THMs) through oral ingestion, dermal absorption, and inhalation exposure from tap water of 15 districts in Istanbul are estimated. The most dominant THM compounds are chloroform, bromodichloromethane (BDCM), and dibromochloromethane (DBCM) in Istanbul tap water. The results indicate that within three different pathways, Istanbul residents had a higher cancer risk through oral ingestion than through the other two pathways. The lifetime cancer risks of oral ingestion for total THMs was highest in Esenyurt district, while the lowest lifetime cancer risk for total THMs was in Basaksehir district. The lifetime cancer risks of chloroform, BDCM, and DBCM from tap water of all 15 districts were higher than 10(-6), the negligible risk level defined by the USEPA. Among the 15 districts, people living in Esenyurt have the highest risk of cancer due to the THM exposure through the multi-pathways, mainly because of the exposure to BDCM and DBCM. The total cancer risk analysis concluded that each year approximately 5 of the 8 million Istanbul residents could get cancer from the daily intake of tap water. PMID:16154195

  1. N-nitrosodimethylamine and trihalomethane formation and minimisation in Southeast Queensland drinking water.

    PubMed

    Knight, Nicole; Watson, Kalinda; Farré, Maria José; Shaw, Glen

    2012-07-01

    This study assesses the prevalence of disinfection by-product (DBP) precursors in some Southeast Queensland drinking water sources by conducting formation potential experiments for the four regulated trihalomethanes (THMs), and the potent carcinogen, N-nitrosodimethylamine (NDMA). NDMA formation potentials were consistently low (<5-21 ng/L), and total THM (tTHM) formation potentials were consistently below the Australian Drinking Water Guideline (250 μg/L). NDMA concentration of finished drinking waters was also monitored and found to be <5 ng/L in all cases. The effect of coagulation and advanced oxidation on the formation of NDMA and THMs is also reported. UV/H(2)O(2) pre-treatment was effective in producing water with very low THMs concentrations, and UV irradiation was an effective method for NDMA degradation. H(2)O(2) was not required for the observed NDMA degradation to occur. Coagulation using alum, ferric chloride or poly(diallyldimethylammonium chloride) (polyDADMAC) was ineffective in removing DBPs precursors from the source water studied, irrespective of the low dissolved organic carbon (DOC) and dissolved organic nitrogen (DON) attained. Rather, coagulation with polyDADMAC caused an increase in NDMA formation potential upon chloramination, and all coagulants led to an increased tTHM formation potential upon chlorination due to the high bromide concentration of the source water studied. PMID:21792515

  2. Bromine incorporation factors for trihalomethane formation for the Mississippi, Missouri, and Ohio Rivers

    USGS Publications Warehouse

    Rathbun, R.E.

    1996-01-01

    The bromine incorporation factor describes the distribution of the four trihalomethane compounds in the mixture formed when a natural water is chlorinated. This factor was determined for the Mississippi, Missouri, and Ohio Rivers by chlorinating water samples at three levels each of pH and free chlorine concentration. Samples were collected during the summer, fall, and spring seasons of the year at 12 sites on the Mississippi River from Minneapolis, MN, to New Orleans, LA, and on the Missouri and Ohio Rivers 1.6 kilometers upstream from their confluences with the Mississippi. The bromine incorporation factor increased as the bromide concentration increased, and decreased as the pH, initial free-chlorine and dissolved organic-carbon concentrations increased. Variation of the bromine incorporation factor with distance along the Mississippi River approximately paralleled the variation of the bromide concentration with distance along the river, with the Missouri River samples having the highest bromine incorporation factors for all combinations of pH and free-chlorine concentration.

  3. Formation of iodinated trihalomethanes during UV/chloramination with iodate as the iodine source.

    PubMed

    Zhang, Tian-Yang; Lin, Yi-Li; Wang, An-Qi; Tian, Fu-Xiang; Xu, Bin; Xia, Sheng-Ji; Gao, Nai-Yun

    2016-07-01

    Iodinated trihalomethanes (I-THMs) are a group of emerging disinfection by-products with high toxicity, and iodide (I(-)) as well as iodinated organic compounds are expected to be their iodine sources. Nevertheless, in this study, iodate (IO3(-)) was proven to be a new iodine source of I-THM formation during UV/chloramination. In the iodate-containing waters (without any other iodine sources), I-THM formation increased with the increase of UV dose, IO3(-) and NH2Cl concentrations. With the increase of Br(-)/IO3(-) molar ratio, I-THM formation (especially for the brominated species) increased. Besides, NOM species could affect I-THM formation from IO3(-) during UV/chloramination. Fulvic acid could promote IO3(-) phototransformation to I(-) but humic acid impeded the production of I(-) during UV irradiation. Under realistic drinking water treatment conditions (DOC = 5.0 mg-C/L, IO3(-) = 12.7 μg-I/L, UV dose = 50 mJ/cm(2), NH2Cl = 5 mg-Cl2/L), CHCl2I was detected as 0.17 μg/L using solid-phase microextraction method, and the production rate of I-THMs from IO3(-) was about 7% of that from I(-). PMID:27105034

  4. Effects of chlorination operating conditions on trihalomethane formation potential in polyaluminum chloride-polymer coagulated effluent.

    PubMed

    Li, Ruihua; Gao, Baoyu; Ma, Defang; Rong, Hongyan; Sun, Shenglei; Wang, Fang; Yue, Qinyan; Wang, Yan

    2015-03-21

    In this study, coagulation performance of polyaluminum chloride (PAC) and PAC-lignin acrylamide (PAC+LAM) in reservoir water treatment was contrastively analyzed. Effects of operating conditions including chlorine dose, contact time and pH on the formation potential of trihalomethanes (THMs) during chlorination in coagulated effluent were also investigated. Comparing with PAC, PAC+LAM achieved higher efficiency in the removal of THMs precursors. TTHM yield in unfiltered water samples (UW) was greater than that of filtered water (FW) due to the residual dissolved organic matter (DOM) in the suspended particles or micro flocs. Meanwhile, operating conditions during chlorination had a significant influence on THMs formation potential. With chlorine dose rising, mass ratio of CHCl3 to TTHM increased, whereas that of CHBr2Cl decreased due to higher Cl2/Br(-) molar ratio. TTHM and CHCl3 levels rose with the increase of pH. Under a given chlorination condition, there was a minor effect of contact time on THM speciation. PMID:25497022

  5. Modelling the regional variability of the probability of high trihalomethane occurrence in municipal drinking water.

    PubMed

    Cool, Geneviève; Lebel, Alexandre; Sadiq, Rehan; Rodriguez, Manuel J

    2015-12-01

    The regional variability of the probability of occurrence of high total trihalomethane (TTHM) levels was assessed using multilevel logistic regression models that incorporate environmental and infrastructure characteristics. The models were structured in a three-level hierarchical configuration: samples (first level), drinking water utilities (DWUs, second level) and natural regions, an ecological hierarchical division from the Quebec ecological framework of reference (third level). They considered six independent variables: precipitation, temperature, source type, seasons, treatment type and pH. The average probability of TTHM concentrations exceeding the targeted threshold was 18.1%. The probability was influenced by seasons, treatment type, precipitations and temperature. The variance at all levels was significant, showing that the probability of TTHM concentrations exceeding the threshold is most likely to be similar if located within the same DWU and within the same natural region. However, most of the variance initially attributed to natural regions was explained by treatment types and clarified by spatial aggregation on treatment types. Nevertheless, even after controlling for treatment type, there was still significant regional variability of the probability of TTHM concentrations exceeding the threshold. Regional variability was particularly important for DWUs using chlorination alone since they lack the appropriate treatment required to reduce the amount of natural organic matter (NOM) in source water prior to disinfection. Results presented herein could be of interest to authorities in identifying regions with specific needs regarding drinking water quality and for epidemiological studies identifying geographical variations in population exposure to disinfection by-products (DBPs). PMID:26563233

  6. Mechanisms and kinetics study on the trihalomethanes formation with carbon nanoparticle precursors.

    PubMed

    Du, Tingting; Wang, Yingying; Yang, Xin; Wang, Wei; Guo, Haonan; Xiong, Xinyu; Gao, Rui; Wuli, Xiati; Adeleye, Adeyemi S; Li, Yao

    2016-07-01

    With lots of carbon nanoparticles (CNPs) applied in the industry, the possibilities of their environmental release have received much attention. As the CNPs may enter drinking water systems, and persist in water and wastewater treatment systems, their possible reaction with disinfectants should be studied. In this study, the formation of trihalomethanes (THMs) with 5 types of carbon nanotubes (CNTs), graphene oxide (GO) and reduced graphene oxide (rGO) was investigated. All CNPs could act as precursors of THMs in aqueous phase. Total concentrations of THMs formed with CNPs varied from 0.24 to 0.95 μM, much lower than that formed from chlorinated Suwannee River Natural Organic Matter (SRNOM) (approximately 9 μM). The kinetics of THMs formation with GO was 0.0814 M(-1) s(-1), which is higher than most of the chlorinated humic acid obtained from different natural waters. The study indicates that during chlorination, C-Cl bond could be formed on the surface of CNPs. However, carbon atoms at the middle of two meta-positioned OH groups on the benzene ring are more active and may prefer to form THMs with chlorine oxidation. The influences of pH and reactant doses on the formation of THMs were also discussed. PMID:27077535

  7. Improved (and Singular) Disinfectant Protocol for Indirectly Assessing Organic Precursor Concentrations of Trihalomethanes and Dihaloacetonitriles.

    PubMed

    Do, Thien D; Chimka, Justin R; Fairey, Julian L

    2015-08-18

    Measurements of disinfection byproduct (DBP) organic precursor concentrations (OPCs) are crucial to assess and improve DBP control processes. Typically, formation potential tests - specified in Standard Methods (SM) 5710-B/D - are used to measure OPCs. Here, we highlight several limitations of this protocol for dihaloacetonitriles and trihalomethanes and validate a novel Alternative Method (AM). The effects of pH, disinfectant type (free chlorine and monochloramine), and chlor(am)ine residual (CR) were examined on DBP formation in a suite of waters. Using the SM, DHAN decreased 43-47% as the CR increased from 3 to 5 mg L(-1) as Cl2, compromising OPC assessments. In contrast, a high monochloramine dose (250 mg L(-1) as Cl2) at pH 7.0 (the AM) accurately reflected OPCs. The two methods were compared for assessing DBP precursor removal through three granular activated carbon (GAC) columns in series. Breakthrough profiles assessed using the AM only showed DBP precursor sorption occurred in each column that decreased over time (p = 0.0001). Similarly, the AM facilitated ranking of three types of GAC compared in parallel columns, whereas the SM produced ambiguous results. Fluorescence intensity of a humic-like fluorophore (i.e., I345/425) correlated strongly to precursor removal in the GAC columns. The practical implications of the results are discussed. PMID:26167626

  8. Trihalomethanes formed from natural organic matter isolates: Using isotopic and compositional data to help understand sources

    USGS Publications Warehouse

    Bergamaschi, B.A.; Fram, M.S.; Fujii, R.; Aiken, G.R.; Kendall, C.; Silva, S.R.

    2000-01-01

    Over 20 million people drink water from the Sacramento-San Joaquin Delta despite problematic levels of natural organic matter (NOM) and bromide in Delta water, which can form trihalomethanes (THMs) during the treatment process. It is widely believed that NOM released from Delta peat islands is a substantial contributor to the pool of THM precursors present in Delta waters. Dissolved NOM was isolated from samples collected at five channel sites within the Sacramento-San Joaquin Rivers and Delta, California, USA, and from a peat island agricultural drain. To help understand the sources of THM precursors, samples were analyzed to determine their chemical and isotopic composition, their propensity to form THMs, and the isotopic composition of the THMs. The chemical composition of the isolates was quite variable, as indicated by significant differences in carbon-13 nuclear magnetic resonance spectra and carbon-to-nitrogen concentration ratios. The lowest propensity to form THMs per unit of dissolved organic carbon was observed in the peat island agricultural drain isolate, even though it possessed the highest fraction of aromatic material and the highest specific ultraviolet absorbance. Changes in the chemical and isotopic composition of the isolates and the isotopic composition of the THMs suggest that the source of the THMs precursors was different between samples and between isolates. The pattern of variability in compositional and isotopic data for these samples was not consistent with simple mixing of river- and peat-derived organic material.

  9. Detecting trihalomethanes using nanoporous-carbon coated surface-acoustic-wave sensors

    SciTech Connect

    Siegal, Michael P.; Mowry, Curtis D.; Pfeifer, Kent B.; Gallis, Dorina F. S.

    2015-03-07

    We study nanoporous-carbon (NPC) grown via pulsed laser deposition (PLD) as a sorbent coating on 96.5-MHz surface-acoustic-wave (SAW) devices to detect trihalomethanes (THMs), regulated byproducts from the chemical treatment of drinking water. Using both insertion-loss and isothermal-response measurements from known quantities of chloroform, the highest vapor pressure THM, we optimize the NPC mass-density at 1.05 ± 0.08 g/cm3 by controlling the background argon pressure during PLD. Precise THM quantities in a chlorobenzene solvent are directly injected into a separation column and detected as the phase-angle shift of the SAW device output compared to the drive signal. Using optimized NPC-coated SAWs, we study the chloroform response as a function of operating temperatures ranging from 10–50°C. Finally, we demonstrate individual responses from complex mixtures of all four THMs, with masses ranging from 10–2000 ng, after gas chromatography separation. As a result, estimates for each THM detection limit using a simple peak-height response evaluation are 4.4 ng for chloroform and 1 ng for bromoform; using an integrated-peak area response analysis improves the detection limits to 0.73 ng for chloroform and 0.003 ng bromoform.

  10. Portable Medical System

    NASA Technical Reports Server (NTRS)

    1982-01-01

    Portable Medical Status and Treatment System (PMSTS) is designed for use in remote areas where considerable time may elapse before a patient can be transported to a hospital. First units were delivered to the Department of Transportation last year and tested in two types of medical emergency environments: one in a rural Pennsylvania community and another aboard a U.S. Coast Guard rescue helicopter operating along Florida's Gulf Coast. The system has the capability to transmit vital signs to a distantly located physician, who can perform diagnosis and relay treatment instructions to the attendant at the scene. The battery powered PMSTS includes a vital signs monitor and a defibrillator. Narco has also developed a companion system, called Porta-Fib III designed for use in a hospital environment with modifications accordingly. Both systems are offshoots of an earlier NASA project known as the Physician's Black Bag developed by Telecare, Inc., a company now acquired by NARCO.

  11. Portable appliance security apparatus

    NASA Technical Reports Server (NTRS)

    Kerley, J. J. (Inventor)

    1981-01-01

    An apparatus for securing a small computer, or other portable appliance, against theft is described. It is comprised of a case having an open back through which the computer is installed or removed. Guide members in the form of slots are formed in a rear portion of opposite walls of the case for receiving a back plate to cover the opening and thereby secure the computer within the case. An opening formed in the top wall of the case exposes the keyboard and display of the computer. The back plate is locked in the closed position by a key-operated plug type lock. The lock is attached to one end of a hold down cable, the opposite end thereof being secured to a desk top or other stationary object. Thus, the lock simultaneously secures the back plate to the case and retains the case to the stationary object.

  12. Portable active interrogation system.

    SciTech Connect

    Moss, C. E.; Brener, M. W.; Hollas, C. L.; Myers, W. L.

    2004-01-01

    The system consists of a pulsed DT neutron generator (5 x 10{sup 7} n/s) and a portable but high intrinsic efficiency, custom-designed, polyethylene-moderated {sup 3}He neutron detector. A multichannel scaler card in a ruggedized laptop computer acquires the data. A user-friendly LabVIEW program analyzes and displays the data. The program displays a warning message when highly enriched uranium or any other fissionable materials is detected at a specified number of sigmas above background in the delayed region between pulses. This report describes the system and gives examples of the response of the system to highly enriched uranium and some other fissionable materials, at several distances and with various shielding materials.

  13. Portable Cooler/Warmers

    NASA Technical Reports Server (NTRS)

    1994-01-01

    Early in the space program, NASA recognized the need to replace bulky coils, compressers, and motors for refrigeration purposes by looking at existing thermoelectric technology. This effort resulted in the development of miniaturized thermoelectric components and packaging to accommodate tight confines of spacecraft. Koolatron's portable electronic refrigerators incorporate this NASA technology. Each of the cooler/warmers employs one or two miniaturized thermoelectric modules. Although each module is only the size of a book of matches, it delivers the cooling power of a 10-pound block of ice. In some models, the cooler can be converted to a warmer. There are no moving parts. The Koolatrons can be plugged into auto cigarette lighters, recreational vehicles, boats or motel outlets.

  14. Portable intensity interferometry

    NASA Astrophysics Data System (ADS)

    Horch, Elliott P.; Camarata, Matthew A.

    2012-07-01

    A limitation of the current generation of long baseline optical interferometers is the need to make the light interfere prior to detection. This is unlike the radio regime where signals can be recorded fast enough to use electronics to accomplish the same result. This paper describes a modern optical intensity interferometer based on electronics with picosecond timing resolution. The instrument will allow for portable optical interferometry with much larger baselines than currently possible by using existing large telescopes. With modern electronics, the limiting magnitude of the technique at a 4-m aperture size becomes competitive with some amplitude-based interferometers. The instrumentation will permit a wireless mode of operation with GPS clocking technology, extending the work to extremely large baselines. We discuss the basic observing strategy, a planned observational program at the Lowell Observatory 1.8-m and 1.0-m telescopes, and the science that can realistically be done with this instrumentation.

  15. Portable Radiation Detectors

    NASA Technical Reports Server (NTRS)

    1997-01-01

    Through a Small Business Innovation Research (SBIR) contract from Kennedy Space Center, General Pneumatics Corporation's Western Research Center satisfied a NASA need for a non-clogging Joule-Thomson cryostat to provide very low temperature cooling for various sensors. This NASA-supported cryostat development played a key part in the development of more portable high-purity geranium gamma-ray detectors. Such are necessary to discern between the radionuclides in medical, fuel, weapon, and waste materials. The outcome of the SBIR project is a cryostat that can cool gamma-ray detectors, without vibration, using compressed gas that can be stored compactly and indefinitely in a standby mode. General Pneumatics also produces custom J-T cryostats for other government, commercial and medical applications.

  16. Hand portable thin-layer chromatography system

    DOEpatents

    Haas, Jeffrey S.; Kelly, Fredrick R.; Bushman, John F.; Wiefel, Michael H.; Jensen, Wayne A.

    2000-01-01

    A hand portable, field-deployable thin-layer chromatography (TLC) unit and a hand portable, battery-operated unit for development, illumination, and data acquisition of the TLC plates contain many miniaturized features that permit a large number of samples to be processed efficiently. The TLC unit includes a solvent tank, a holder for TLC plates, and a variety of tool chambers for storing TLC plates, solvent, and pipettes. After processing in the TLC unit, a TLC plate is positioned in a collapsible illumination box, where the box and a CCD camera are optically aligned for optimal pixel resolution of the CCD images of the TLC plate. The TLC system includes an improved development chamber for chemical development of TLC plates that prevents solvent overflow.

  17. A Trusted Portable Computing Device

    NASA Astrophysics Data System (ADS)

    Ming-wei, Fang; Jun-jun, Wu; Peng-fei, Yu; Xin-fang, Zhang

    A trusted portable computing device and its security mechanism were presented to solve the security issues, such as the attack of virus and Trojan horse, the lost and stolen of storage device, in mobile office. It used smart card to build a trusted portable security base, virtualization to create a secure virtual execution environment, two-factor authentication mechanism to identify legitimate users, and dynamic encryption to protect data privacy. The security environment described in this paper is characteristic of portability, security and reliability. It can meet the security requirement of mobile office.

  18. Calibration of a field-portable gamma detector to obtain in situ measurements of the 137Cs inventories of cultivated soils and floodplain sediments.

    PubMed

    He, Q; Walling, D E

    2000-04-01

    Over the past 10 years, a number of studies have exploited the potential for using measurements of fallout 137Cs inventories to document rates and patterns of soil erosion on cultivated land and to estimate rates of overbank sedimentation on river floodplains. Traditional procedures for applying the 137Cs technique involve the collection of soil or sediment cores from a study site and their subsequent transfer to the laboratory for preparation and analysis by gamma spectrometry. Such procedures are time consuming and there may be a considerable delay before the results are available. It is therefore difficult to obtain preliminary results, which could be used to guide the development of an ongoing sampling programme. The use of in situ gamma spectrometry measurements to quantify 137Cs inventories in soils and sediments offers a number of potential advantages over traditional procedures. However, in order to derive a reliable estimate of the 137Cs inventory for a measurement point, it is necessary to take account of the attenuation of 137Cs gamma rays by the soil matrix and information on the depth distribution of 137Cs in the soil or sediment is therefore required. In the present study, empirical relationships between in situ measurements of 137Cs activity and total 137Cs inventories have been established for soils from a cultivated field and for floodplain sediments, based on information on the vertical distribution of 137Cs in the soils and sediments provided by the forward scattering ratio derived from the field measured spectra. These relationships have been used to estimate 137Cs inventories from in situ measurements of 137Cs activity at other locations. PMID:10800723

  19. Freely Oriented, Portable Superconducting Magnet

    NASA Astrophysics Data System (ADS)

    Schmierer, E. N.; Charles, B.; Efferson, R.; Hill, D.; Jankowski, T.; Laughon, G.; Prenger, C.

    2008-03-01

    A high-field low-temperature superconducting solenoidal magnet was developed that is portable and can be operated in any orientation relative to gravity. The design consists of several features that make this feasible; 1) bulk liquid cryogen storage occurs in a separate Dewar rather than as part of the magnet assembly, which allows single-person transport due to each component of the system having low relative weight, 2) vapor generated pressurization that circulates cryogenic fluid to and from the magnet with flexible transfer lines allowing operation in any orientation, and 3) composite, low-conducting structural members are used to suspend the magnet and shield layers within the vacuum vessel that provide a robust low heat loss design. Cooling is provided to the magnet through fluid channels that are in thermal contact with the magnet. The overall design of this magnet system, some of the analyses performed that address unique behavior of this system (pressure rise during a magnet quench and transient cooldown), and test results are presented.

  20. Portable rotating discharge plasma device

    NASA Astrophysics Data System (ADS)

    Dwyer, B. L.; Brooks, N. H.; Lee, R. L.

    2011-10-01

    We constructed two devices for the purpose of educational demonstration: a rotating tube containing media of two densities to demonstrate axial confinement and a similar device that uses pressure variation to convert a long plasma glow discharge into a long straight arc. In the first device, the buoyant force is countered by the centripetal force, which confines less dense materials to the center of the column. Similarly, a plasma arc heats the gas through which it passes, creating a hot gaseous bubble that is less dense than the surrounding medium. Rotating its containment envelope stabilizes this gas bubble in an analogous manner to an air bubble in a rotating tube of water. In addition to stabilization, the rotating discharge also exhibits a decrease in buoyancy-driven convection currents. This limits the power loss to the walls, which decreases the field strength requirement for maintaining the arc. These devices demonstrate principles of electrodynamics, plasma physics, and fluid mechanics. They are portable and safe for classroom use. Work supported by US DOE under DE-FC02-04ER54698 and the National Undergraduate Fellowship in Fusion Science and Engineering.

  1. A Portable Infrasonic Detection System

    NASA Technical Reports Server (NTRS)

    Shams, Qamar A.; Burkett, Cecil G.; Zuckerwar, Allan J.; Lawrenson, Christopher C.; Masterman, Michael

    2008-01-01

    During last couple of years, NASA Langley has designed and developed a portable infrasonic detection system which can be used to make useful infrasound measurements at a location where it was not possible previously. The system comprises an electret condenser microphone, having a 3-inch membrane diameter, and a small, compact windscreen. Electret-based technology offers the lowest possible background noise, because Johnson noise generated in the supporting electronics (preamplifier) is minimized. The microphone features a high membrane compliance with a large backchamber volume, a prepolarized backplane and a high impedance preamplifier located inside the backchamber. The windscreen, based on the high transmission coefficient of infrasound through matter, is made of a material having a low acoustic impedance and sufficiently thick wall to insure structural stability. Close-cell polyurethane foam has been found to serve the purpose well. In the proposed test, test parameters will be sensitivity, background noise, signal fidelity (harmonic distortion), and temporal stability. The design and results of the compact system, based upon laboratory and field experiments, will be presented.

  2. Trihalomethanes in liver pathology: Mitochondrial dysfunction and oxidative stress in the mouse.

    PubMed

    Faustino-Rocha, Ana I; Rodrigues, D; da Costa, R Gil; Diniz, C; Aragão, S; Talhada, D; Botelho, M; Colaço, A; Pires, M J; Peixoto, F; Oliveira, P A

    2016-08-01

    Trihalomethanes (THMs) are disinfection byproducts found in chlorinated water, and are associated with several different kinds of cancer in human populations and experimental animal models. Metabolism of THMs proceeds through enzymes such as GSTT1 and CYP2E1 and gives rise to reactive intermediates, which form the basis for their toxic activities. The aim of this study was to assess the mitochondrial dysfunction caused by THMs at low levels, and the resulting hepatic histological and biochemical changes in the mouse. Male ICR mice were administered with two THMs: dibromochloromethane (DBCM) and bromodichloromethane (BDCM); once daily, by gavage, to a total of four administrations. Animals were sacrificed four weeks after DBCM and BDCM administrations. Blood biochemistry was performed for alanine aminotransferase (ALT), aspartate aminotransferase (AST), alkaline phosphatase (ALP), total bilirubin (TB), albumin (Alb), total protein (TP), creatinine, and urea. Animals exposed to DBCM and BDCM showed elevated ALT and TB levels (p < 0.05) as compared with controls. Histological analysis confirmed the presence of vacuolar degenerescence and a multifocal necrotizing hepatitis in 33% of animals (n = 2). Mitochondrial analysis showed that THMs reduced mitochondrial bioenergetic activity (succinate dehydrogenase (SQR), cytochrome c oxidase (COX), and ATP synthase) and increased oxidative stress (glutathione S-transferase (GST)) in hepatic tissues (p < 0.05). These results add detail to the current understanding of the mechanisms underlying THM-induced toxicity, supporting the role of mitochondrial dysfunction and oxidative stress in liver toxicity caused by DBCM and BDCM. © 2015 Wiley Periodicals, Inc. Environ Toxicol 31: 1009-1016, 2016. PMID:25640707

  3. Characterization of haloacetaldehyde and trihalomethane formation potentials during drinking water treatment.

    PubMed

    Mao, Yu-Qin; Wang, Xiao-Mao; Guo, Xian-Fen; Yang, Hong-Wei; Xie, Yuefeng F

    2016-09-01

    Haloacetaldehydes (HAs) are the third prevalent group of disinfection by-products (DBPs) of great health concern. In this study, their formation and speciation during chlorination were investigated for raw and process waters collected at three O3-biological activated carbon (BAC) advanced drinking water treatment plants. The results showed that all HA formation potentials (HAFPs) were highly enhanced whenever ozone was applied before or after conventional treatment. Sand filtration and BAC filtration could substantially reduce HAFPs. Trihalomethanes (THMs) were also measured to better understand the role of HAs in DBPs. Very different from HAFPs, THMFPs kept decreasing with the progress of treatment steps, which was mainly attributed to the different precursors for HAs and THMs. Brominated HAs were detected in bromide-containing waters. Chloral hydrate (CH) contributed from 25% to 48% to the total HAs formed in waters containing 100-150 μg L(-1) bromide, indicating the wide existence of other HAs after chlorination besides CH production. In addition, bromide incorporation factor (BIF) in HAs and THMs increased with the progress of treatment steps and the BIF values of THMs were generally higher than those of HAs. The BAC filtration following ozonation could significantly reduce HA precursors produced from ozonation but without complete removal. The brominated HAFPs in the outflow of BAC were still higher than their levels in the raw water. As a result, O3-BAC combined treatment was effective at controlling the total HAs, whereas it should be cautious for waters with high bromide levels. PMID:27318452

  4. Trihalomethane occurrence in chlorinated reclaimed water at full-scale wastewater treatment plants in NE Spain.

    PubMed

    Matamoros, Víctor; Mujeriego, Rafael; Bayona, Josep M

    2007-08-01

    Total trihalomethane (TTHM) concentrations were determined in three chlorinated effluents (i.e. secondary and tertiary) from full-scale wastewater treatment plants (WWTP) in NE Spain over a 2-year monitoring period (May 2003-February 2005). Low TTHM concentrations (2-30 microg L(-1)), according to international standards for drinking water (80-150 microg L(-1)), were obtained in all samples analysed. The effects of (a) ammonia nitrogen and bromide concentrations, (b) UV light exposure, (c) tank storage, and (d) water temperature were evaluated. Two chlorination strategies were adopted: low chlorine dosages (2-5 mg Cl2 L(-1)) and a high-chlorine dosage (16 mg Cl2 L(-1)). The effects of storing chlorinated reclaimed water and of UV light exposure before chlorination were also evaluated. Samples collected over the 2-year monitoring period offered the possibility to assess the numerous variables affecting THM formation. A statistical evaluation of Platja d'Aro WWTP data set shows a low TTHM formation in the presence of high ammonia nitrogen concentration (p<0.05). That result can be attributed to the formation of chloramines by reaction with added chlorine, at doses below breakpoint chlorination. An increase in TTHM concentration in the presence of bromide (0-1 mg L(-1)) was also recorded (p<0.05). In contrast to published reports, TOC had a negative effect on TTHM formation. COD and turbidity had no statistical significance on TTHM formation. As expected, chlorination promoted TTHM formation in the three water reclamation plants monitored. Nevertheless, no statistical difference was observed when chlorinated effluents were kept in storage tanks. Exposure to UV light did not affect either formation or removal of TTHM. The relative production of TTHM during warm and cold seasons was also evaluated. TTHM production decreased with higher temperatures, but that could be attributed to the increase of ammonia nitrogen concentration observed during the warm summer seasons

  5. Influence of physical activity in the intake of trihalomethanes in indoor swimming pools.

    PubMed

    Marco, Esther; Lourencetti, Carolina; Grimalt, Joan O; Gari, Mercè; Fernández, Pilar; Font-Ribera, Laia; Villanueva, Cristina M; Kogevinas, Manolis

    2015-07-01

    This study describes the relationship between physical activity and intake of trihalomethanes (THMs), namely chloroform (CHCl3), bromodichloromethane (CHCl2Br), dibromochloromethane (CHClBr2) and bromoform (CHBr3), in individuals exposed in two indoor swimming pools which used different disinfection agents, chlorine (Cl-SP) and bromine (Br-SP). CHCl3 and CHBr3 were the dominant compounds in air and water of the Cl-SP and Br-SP, respectively. Physical exercise was assessed from distance swum and energy expenditure. The changes in exhaled breath concentrations of these compounds were measured from the differences after and before physical activity. A clear dependence between distance swum or energy expenditure and exhaled breath THM concentrations was observed. The statistically significant relationships involved higher THM concentrations at higher distances swum. However, air concentration was the major factor determining the CHCl3 and CHCl2Br intake in swimmers whereas distance swum was the main factor for CHBr3 intake. These two causes of THM incorporation into swimmers concurrently intensify the concentrations of these compounds into exhaled breath and pointed to inhalation as primary mechanism for THM uptake. Furthermore, the rates of THM incorporation were proportionally higher as higher was the degree of bromination of the THM species. This trend suggested that air-water partition mechanisms in the pulmonary system determined higher retention of the THM compounds with lower Henry's Law volatility constants than those of higher constant values. Inhalation is therefore the primary mechanisms for THM exposure of swimmers in indoor buildings. PMID:25885117

  6. Trihalomethanes in Lisbon indoor swimming pools: occurrence, determining factors, and health risk classification.

    PubMed

    Silva, Zelinda Isabel; Rebelo, Maria Helena; Silva, Manuela Manso; Alves, Ana Martins; Cabral, Maria da Conceição; Almeida, Ana Cristina; Aguiar, Fátima Rôxo; de Oliveira, Anabela Lopes; Nogueira, Ana Cruz; Pinhal, Hermínia Rodrigues; Aguiar, Pedro Manuel; Cardoso, Ana Sofia

    2012-01-01

    Characterization of water quality from indoor swimming pools, using chorine-based disinfection techniques, was performed during a 6-mo period to study the occurrence, distribution, and concentration factors of trihalomethanes (THM). Several parameters such as levels of water THM, water and air chloroform, water bromodichloromethane (BDCM), water dibromochloromethane (DBCM), water bromoform (BF), free residual chlorine (FrCl), pH, water and air temperature, and permanganate water oxidizability (PWO) were determined in each pool during that period. Chloroform (CF(W)) was the THM detected at higher concentrations in all pools, followed by BDCM, DBCM, and BF detected at 99, 34, and 6% of the samples, respectively. Water THM concentrations ranged from 10.1 to 155 μg/L, with 6.5% of the samples presenting values above 100 μg/L (parametric value established in Portuguese law DL 306/2007). In this study, air chloroform (CF(Air)) concentrations ranged from 45 to 373 μg/m³ with 24% of the samples presenting values above 136 μg/m³ (considered high exposure value). Several significant correlations were observed between total THM and other parameters, namely, CF(W), CF(Air), FrCl, water temperature (T(W)), and PWO. These correlations indicate that FrCl, T(W) and PWO are parameters that influence THM formation. The exposure criterion established for water THM enabled the inclusion of 67% of Lisbon pools in the high exposure group, which reinforces the need for an improvement in pool water quality. PMID:22788374

  7. Ternary Model of the Speciation of I-/Br-/Cl-Trihalomethanes Formed in Chloraminated Surface Waters.

    PubMed

    Yan, Mingquan; Li, Mingyang; Roccaro, Paolo; Korshin, Gregory V

    2016-04-19

    This study examined the effects of the iodide concentration and pH on yields and speciation of the entire group of 10 species of iodine-, bromine-, and chlorine-containing trihalomethanes (THMs) formed at pH values from 6.5 to 8.5 in chloraminated surface waters in the presence of bromide and iodide. Pathways of iodine, bromine, and chlorine incorporation in the active sites in dissolved organic matter (DOM) were examined on the basis of a ternary halogenation/THM speciation model. The model assumed the occurrence of sequential three-step halogenation of the active site and competition of iodine, bromine, and chlorine species at each node of the halogenation sequence. A comparison of experimentally measured and modeled speciation coefficients and also iodine and bromine incorporation factors calculated for 10 THM species showed that the developed approach was sufficient to closely model the observed trends. Interpretation of preferred iodine incorporation pathways associated with the generation of THMs in all examined conditions showed that the susceptibility of the halogenated intermediates to iodine incorporation increases rapidly with the number of iodine atoms that have already been incorporated into the reaction site. In contrast, the incorporation of bromine and chlorine atoms in the intermediates involved in the generation of THMs makes them largely inactive in iodine incorporation reactions. The presented approach allows for a further understanding of the mechanisms of DOM/halogen interactions and prediction of the speciation of THMs formed at varying pH values, iodide concentrations, and other system conditions. PMID:27007081

  8. Photodegradation of iodinated trihalomethanes in aqueous solution by UV 254 irradiation.

    PubMed

    Xiao, Yongjun; Fan, Rongli; Zhang, Lifeng; Yue, Junqi; Webster, Richard D; Lim, Teik-Thye

    2014-02-01

    Photodegradation of 6 iodinated trihalomethanes (ITHMs) under UV irradiation at 254 nm was investigated in this study. ITHMs underwent a rapid photodegradation process through cleavage of carbon-halogen bond with first-order rate constants in the range of 0.1-0.6 min(-1). The effects of matrix species including nitrate, humic acid (HA), bicarbonate, sulfate, and chloride were evaluated. The degradation rate increased slightly in the presence of nitrate possibly due to generation of HO at a low quantum yield via direct photolysis of nitrate, while HA lowered the photodegradation rate of ITHMs due to its competitive UV absorption. Moreover, bicarbonate, sulfate, and chloride had no significant effect on photodegradation kinetics, as there is no UV absorption for these 3 species. In the study using surface water, treated water, and secondary effluent from a wastewater treatment plant, high turbidity and natural organic matters present in the water inhibited the photodegradation of ITHMs. The degradation rates of 6 ITHMs in UV/H2O2 system were rather comparable and significantly higher than those achieved in the UV system without H2O2. To develop a quantitative structure-reactivity relationship (QSAR) model, the logarithm of measured first-order rate constants was correlated with a number of molecular descriptors. The best correlation was obtained with a combination of 3 molecular descriptors, namely the bond strength of carbon-halogen to be broken in the rate-determining step, steric and electronic effects of all substituents to the carbon center. PMID:24355288

  9. Occurrence and variability of iodinated trihalomethanes concentrations within two drinking-water distribution networks.

    PubMed

    Ioannou, Panagiotis; Charisiadis, Pantelis; Andra, Syam S; Makris, Konstantinos C

    2016-02-01

    Non-iodo-containing trihalomethanes (TTHM) are frequently detected in chlorinated tap water and currently regulated against their carcinogenic potential. Iodinated THM (ITHM) may also form in disinfected with chlorine waters that are high in iodine content, but little is known about their magnitude and variability within the drinking-water pipe distribution network of urban areas. The main objective of this study was to determine the magnitude and variability of ITHM and TTHM levels and their corresponding daily intake estimates within the drinking water distribution systems of Limassol and Nicosia cities of Cyprus, using tap samples collected from individual households (n=37). In Limassol, mean household tap water ITHM and TTHM levels was 0.58 and 38 μg L(-1), respectively. Dichloroiodomethane (DCIM) was the dominant species of the two measured ITHM compounds accounting for 77% of total ITHM and in the range of 0.032 and 1.65 μg L(-1). The range of DCIM concentrations in Nicosia tap water samples was narrower (0.032 - 0.848 μg L(-1)). Mean total iodine concentration in tap water samples from the seaside city of Limassol was 15 μg L(-1) and approximately twice to those observed in samples from the mainland Nicosia city. However, iodine concentrations did not correlate with the ITHM levels. The calculated chronic daily intake rates of ITHM were low when compared with those of TTHM, but because of their widespread occurrence in tap water and their enhanced mammalian cell toxicity, additional research is warranted to assess the magnitude and variability of human ITHM exposures. PMID:26599150

  10. Microbial degradation of plant leachate alters lignin phenols and trihalomethane precursors

    USGS Publications Warehouse

    Pellerin, Brian A.; Hernes, Peter J.; Saraceno, John Franco; Spencer, Robert G.M.; Bergamaschi, Brian A.

    2010-01-01

    Although the importance of vascular plant-derived dissolved organic carbon (DOC) in freshwater systems has been studied, the role of leached DOC as precursors of disinfection byproducts (DBPs) during drinking water treatment is not well known. Here we measured the propensity of leachates from four crops and four aquatic macrophytes to form trihalomethanes (THMs)—a regulated class of DBPs—before and after 21 d of microbial degradation. We also measured lignin phenol content and specific UV absorbance (SUVA254) to test the assumption that aromatic compounds from vascular plants are resistant to microbial degradation and readily form DBPs. Leaching solubilized 9 to 26% of total plant carbon, which formed 1.93 to 6.72 mmol THM mol C-1 However, leachate DOC concentrations decreased by 85 to 92% over the 21-d incubation, with a concomitant decrease of 67 to 92% in total THM formation potential. Carbon-normalized THM yields in the residual DOC pool increased by 2.5 times on average, consistent with the preferential uptake of nonprecursor material. Lignin phenol concentrations decreased by 64 to 96% over 21 d, but a lack of correlation between lignin content and THM yields or SUVA254 suggested that lignin-derived compounds are not the source of increased THM precursor yields in the residual DOC pool. Our results indicate that microbial carbon utilization alters THM precursors in ecosystems with direct plant leaching, but more work is needed to identify the specific dissolved organic matter components with a greater propensity to form DBPs and affect watershed management, drinking water quality, and human health.

  11. Exposure assessment for trihalomethanes in municipal drinking water and risk reduction strategy.

    PubMed

    Chowdhury, Shakhawat

    2013-10-01

    Lifetime exposure to disinfection byproducts (DBPs) in municipal water may pose risks to human health. Current approaches of exposure assessments use DBPs in cold water during showering, while warming of chlorinated water during showering may increase trihalomethane (THM) formation in the presence of free residual chlorine. Further, DBP exposure through dermal contact during showering is estimated using steady-state condition between the DBPs in shower water impacting on human skin and skin exposed to shower water. The lag times to achieve steady-state condition between DBPs in shower water and human skin can vary in the range of 9.8-391.2 min, while shower duration is often less than the lag times. Assessment of exposure without incorporating these factors might have misinterpreted DBP exposure in some previous studies. In this study, exposure to THMs through ingestion was estimated using cold water THMs, while THM exposure through inhalation and dermal contact during showering was estimated using THMs in warm water. Inhalation of THMs was estimated using THM partition into the shower air, while dermal uptake was estimated by incorporating lag times (e.g., unsteady and steady-state phases of exposure) during showering. Probabilistic approach was followed to incorporate uncertainty in the assessment. Inhalation and dermal contact during showering contributed 25-60% of total exposure. Exposure to THMs during showering can be controlled by varying shower stall volume, shower duration and air exchange rate following power law equations. The findings might be useful in understanding exposure to THMs, which can be extended to other volatile compounds in municipal water. PMID:23872246

  12. Formation, modeling and validation of trihalomethanes (THM) in Malaysian drinking water: a case study in the districts of Tampin, Negeri Sembilan and Sabak Bernam, Selangor, Malaysia.

    PubMed

    Abdullah, Md Pauzi; Yew, C H; Ramli, Mohamad Salleh bin

    2003-11-01

    A modeling procedure that predicts trihalomethane (THM) formation from field sampling at the treatment plant and along its distribution system using Tampin district, Negeri Sembilan and Sabak Bernam district, Selangor as sources of data were studied and developed. Using Pearson method of correlation, the organic matter measured as TOC showed a positive correlation with formation of THM (r=0.380,P=0.0001 for Tampin and r=0.478,P=0.0001 for Sabak Bernam). Similar positive correlation was also obtained for pH in both districts with Tampin (r=0.362,P=0.0010) and Sabak Bernam (r=0.215,P=0.0010). Chlorine dosage was also found to have low correlation with formation of THM for the two districts with Tampin (r=0.233,P=0.0230) and Sabak Bernam (r=0.505,P=0.0001). Distance from treatment plant was found to have correlation with formation of THM for Tampin district with r=0.353 and P=0.0010. Other parameters such as turbidity, ammonia, temperature and residue chlorine were found to have no correlation with formation of THM. Linear and non-linear models were developed for these two districts. The results obtained were validated using three different sets of field data obtained from own source and district of Seremban (Pantai and Sg. Terip), Negeri Sembilan. Validation results indicated that there was significant difference in the predictive and determined values of THM when two sets of data from districts of Seremban were used with an exception of field data of Sg. Terip for non-linear model developed for district of Tampin. It was found that a non-linear model is slightly better than linear model in terms of percentage prediction errors. The models developed were site specific and the predictive capabilities in the distribution systems vary with different environmental conditions. PMID:14568050

  13. EVALUATION OF PORTABLE GAS CHROMATOGRAPHS

    EPA Science Inventory

    Limits of detection, linearity of responses, and stability of response factors and retention times for five commercially-available portable gas chromatographs (PGC) were determined during laboratory evaluation. he PGCs were also operated at the French Limited Superfund site near ...

  14. Portable classroom leads to partnership.

    PubMed

    Le Ber, Jeanne Marie; Lombardo, Nancy T; Weber, Alice; Bramble, John

    2004-01-01

    Library faculty participation on the School of Medicine Curriculum Steering Committee led to a unique opportunity to partner technology and teaching utilizing the library's portable wireless classroom. The pathology lab course master expressed a desire to revise the curriculum using patient cases and direct access to the Web and library resources. Since the pathology lab lacked computers, the library's portable wireless classroom provided a solution. Originally developed to provide maximum portability and flexibility, the wireless classroom consists of ten laptop computers configured with wireless cards and an access point. While the portable wireless classroom led to a partnership with the School of Medicine, there were additional benefits and positive consequences for the library. PMID:15148018

  15. Portable Source Identification Device

    SciTech Connect

    Andersen, Eric S.; Samuel, Todd J.; Gervais, Kevin L.

    2005-08-01

    U.S. Customs and Border Protection (CBP) is the primary enforcement agency protecting the nation’s ports of entry. CBP is enhancing its capability to interdict the illicit import of nuclear and radiological materials and devices that may be used by terrorists. Pacific Northwest National Laboratory (PNNL) is providing scientific and technical support to CBP in their goal to enable rapid deployment of nuclear and radiation detection systems at U. S. ports of entry to monitor 100% of the incoming international traffic and cargo while not adversely impacting the operations or throughput of the ports. As the deployment of radiation detection systems proceeds, there is a need to adapt the baseline radiation portal monitor (RPM) system technology to operations at these diverse ports of entry. When screening produces an alarm in the primary inspection RPM, the alarming vehicle is removed from the flow of commerce and the alarm is typically confirmed in a secondary inspection RPM. The portable source identification device (PSID) is a radiation sensor panel (RSP), based on thallium-doped sodium iodide (NaI(Tl)) scintillation detector and gamma spectroscopic analysis hardware and software, mounted on a scissor lift on a small truck. The lift supports a box containing a commercial off-the-shelf (COTS) sodium iodide detector that provides real-time isotopic identification, including neutron detectors to interdict Weapons of Mass Destruction (WMD) and radiation dispersion devices (RDD). The scissor lift will lower the detectors to within a foot off the ground and raise them to approximately 24 feet in the air, allowing a wide vertical scanning range.

  16. Portable source identification device

    NASA Astrophysics Data System (ADS)

    Andersen, Eric S.; Samuel, Todd J.; Gervais, Kevin L.

    2005-05-01

    U.S. Customs and Border Protection (CBP) is the primary enforcement agency protecting the nation"s ports of entry. CBP is enhancing its capability to interdict the illicit import of nuclear and radiological materials and devices that may be used by terrorists. Pacific Northwest National Laboratory (PNNL) is providing scientific and technical support to CBP in their goal to enable rapid deployment of nuclear and radiation detection systems at U. S. ports of entry to monitor 100% of the incoming international traffic and cargo while not adversely impacting the operations or throughput of the ports. As the deployment of radiation detection systems proceeds, there is a need to adapt the baseline radiation portal monitor (RPM) system technology to operations at these diverse ports of entry. When screening produces an alarm in the primary inspection RPM, the alarming vehicle is removed from the flow of commerce and the alarm is typically confirmed in a secondary inspection RPM. The portable source identification device (PSID) is a radiation sensor panel (RSP), based on thallium-doped sodium iodide (NaI(Tl)) scintillation detector and gamma spectroscopic analysis hardware and software, mounted on a scissor lift on a small truck. The lift supports a box containing a commercial off-the-shelf (COTS) sodium iodide detector that provides real-time isotopic identification, including neutron detectors to interdict Weapons of Mass Destruction (WMD) and radiation dispersion devices (RDD). The scissor lift will lower the detectors to within a foot off the ground and raise them to approximately 24 feet (7.3 m) in the air, allowing a wide vertical scanning range.

  17. Portable Multiplex Pathogen Detector

    SciTech Connect

    Visuri, S; McBride, M T; Matthews, D; Rao, R

    2002-07-15

    Tumor marker concentrations in serum provide useful information regarding clinical stage and prognosis of cancer and can thus be used for presymptomatic diagnostic purposes. Currently, detection and identification of soluble analytes in biological fluids is conducted by methods including bioassays, ELISA, PCR, DNA chip or strip tests. While these technologies are generally sensitive and specific, they are time consuming, labor intensive and cannot be multiplexed. Our goal is to develop a simple, point-of-care, portable, liquid array-based immunoassay device capable of simultaneous detection of a variety of cancer markers. Here we describe the development of assays for the detection of Serum Prostate Specific Antigen, and Ovalbumin from a single sample. The multiplexed immunoassays utilize polystyrene microbeads. The beads are imbedded with precise ratios of red and orange fluorescent dyes yielding an array of 100 beads, each with a unique spectral address (Figure 1). Each bead can be coated with capture antibodies specific for a given antigen. After antigen capture, secondary antibodies sandwich the bound antigen and are indirectly labeled by the fluorescent reporter phycoerythrin (PE). Each optically encoded and fluorescently-labeled microbead is then individually interrogated. A red laser excites the dye molecules imbedded inside the bead and classifies the bead to its unique bead set, and a green laser quantifies the assay at the bead surface. This technology has been proven to be comparable to the ELISA in terms of sensitivity and specificity. We also describe the laser-based instrumentation used to acquire fluorescent bead images Following the assay, droplets of bead suspension containing a mixture of bead classes were deposited onto filters held in place by a disposable plexiglass device and the resultant arrays viewed under the fluorescent imaging setup. Using the appropriate filter sets to extract the necessary red, orange and green fluorescence from the

  18. Effect of alum treatment on the trihalomethane formation and bacterial regrowth potential of natural and synthetic waters.

    PubMed

    Page, D W; van Leeuwen, J A; Spark, K M; Drikas, M; Withers, N; Mulcahy, D E

    2002-11-01

    Waters from five reservoirs and "synthetic waters", prepared using terrestrially derived dissolved organic matter (DOM) extracted from vegetation and reservoir catchment soils, were studied for their treatability with alum using a jar test procedure. DOM in drinking water is a precursor for the formation of trihalomethanes (THM) following chlorine disinfection and can also be a substrate for microbial growth in the drinking water distribution system. The trihalomethane formation potential (THMFP) represents an upper concentration limit on THMs formed by chlorination, while bacterial regrowth potential (BRP) is an indicator of the bioavailability of DOM. BRP and THMFP were measured before and after alum treatment and the results were related to the source of the DOM. It was found that freshly derived terrestrial DOM in synthetic water resulted in higher THMFP and BRP than DOM in reservoir waters. For the samples investigated, conventional alum treatment did not always reduce the THM precursor levels formed in laboratory tests below the NH&MRC (1996) guideline level of 250 microg/L nor produce microbially stable waters. PMID:12448532

  19. Characterization of dissolved organic matter for prediction of trihalomethane formation potential in surface and sub-surface waters.

    PubMed

    Awad, John; van Leeuwen, John; Chow, Christopher; Drikas, Mary; Smernik, Ronald J; Chittleborough, David J; Bestland, Erick

    2016-05-01

    Dissolved organic matter (DOM) in surface waters used for drinking purposes can vary markedly in character dependent on their sources within catchments. The character of DOM further influences the formation of disinfection by products when precursor DOM present in drinking water reacts with chlorine during disinfection. Here we report the development of models that describe the formation potential of trihalomethanes (THMFP) dependent on the character of DOM in waters from discrete catchments with specific land-use and soil textures. DOM was characterized based on UV absorbance at 254 nm, apparent molecular weight and relative abundances of protein-like and humic-like compounds. DOM character and Br concentration (up to 0.5 mg/L) were used as variables in models (R(2)>0.93) of THMFP, which ranged from 19 to 649 μg/L. Chloroform concentration (12-594 μg/L) and relative abundance (27-99%) were first modeled (R(2)>0.85) and from these, the abundances of bromodichloromethane and chlorodibromomethane estimated using power and exponential functions, respectively (R(2)>0.98). From these, the abundance of bromoform is calculated. The proposed model may be used in risk assessment of catchment factors on formation of trihalomethanes in drinking water, in context of treatment efficiency for removal of organic matter. PMID:26874432

  20. Improved portable lighting for visual aircraft inspection

    SciTech Connect

    Shagam, R.N.; Lerner, J.; Shie, R.

    1995-04-01

    The most common tool used by aircraft inspectors is the personal flashlight. While it is compact and very portable, it is generally typified by poor beam quality which can interfere with the ability for an inspector to detect small defects and anomalies, such as cracks and corrosion sites, which may be indicators of major structural problems. A Light Shaping Diffuser{trademark} (LSD) installed in a stock flashlight as a replacement to the lens can improve the uniformity of an average flashlight and improve the quality of the inspection. Field trials at aircraft maintenance facilities have demonstrated general acceptance of the LSD by aircraft inspection and maintenance personnel.

  1. A portable free space optical system

    NASA Astrophysics Data System (ADS)

    Ai, Yong; Lu, Xingguang; Yang, Jinglin; Chen, Jing; Hao, Zhonggang

    2005-08-01

    A portable protocol independent free space optical communication terminal was developed, which enables customer to quickly deploy optical bandwidth services for applications such as fiber extension, wild field point to point communication and wireless backhaul while avoiding costly and time-consuming fiber installation. By using specially designed optical components and optical-mechanical structure, the system is very compact and effective, can establish optical link within a few minutes, with total weight 4kg, size 160 x 360 x 155 mm, effective transmitting/receiving aperture 40mm, data rate 100Mbps, maximum communication distance 1500m. The system and experiments are presented in the paper.

  2. Improved portable lighting for visual aircraft inspection

    NASA Astrophysics Data System (ADS)

    Shagam, Richard N.; Lerner, Jeremy M.; Shie, Rick

    1995-07-01

    The most common tool used by aircraft inspectors is the personal flashlight. While it is compact and very portable, it is generally typified by poor beam quality which can interfere with the ability for an inspector to detect small defects and anomalies, such as cracks and corrosion sites, which may be indicators of major structural problems. A Light Shaping Diffuser TM (LSD) installed in a stock flashlight as a replacement to the lens can improve the uniformity of an average flashlight and improve the quality of the inspection. Field trials at aircraft maintenance facilities have demonstrated general acceptance of the LSD by aircraft inspection and maintenance personnel.

  3. Portable Habitat for Antarctic Scientific Research (PHASR)

    NASA Technical Reports Server (NTRS)

    Griswold, Samantha S.

    1992-01-01

    The Portable Habitat for Antarctic Scientific Research, PHASR, is designed as a versatile, general purpose habitat system that addresses the problem of functional space and environmental soundness in a partially fabric-covered shelter. PHASR is used for remote field site applications that can be quickly deployed. PHASR will also provide four scientists with a comfortable and efficient use of interior space. PHASR is a NASA/USRA Advanced Design Program project conducted at the University of Houston College of Architecture, Sasadawa International Center for Space Architecture (SICSA). This report is prepared for NASA/USRA.

  4. THE INDUCTION OF COLORECTAL NEOPLASIA BY A MIXTURE HIGH IN BROMINATED TRIHALOMETHANES (THMS) ADMINISTERED IN THE DRINKING WATER TO MALE F344/N RATS

    EPA Science Inventory

    THE INDUCTION OF COLORECTAL NEOPLASIA BY A MIXTURE HIGH IN BROMINA TED TRIHALOMETHANES (THMS) ADMINISTERED IN THE DRINKING W A TER TO MALE F344/N RA TS.

    Abstract:

    The THMs are the most widely distributed and concentrated of the chlorine disinfection by-products (D...

  5. USEPA (U.S. ENVIRONMENTAL PROTECTION AGENCY) METHOD STUDY, METHOD 510.1: THE DETERMINATION OF THE MAXIMUM TOTAL TRIHALOMETHANE POTENTIAL

    EPA Science Inventory

    A method validation study of the Method, 510.1: 'The Determination of Maximum Total Trihalomethane Potential'. The MTP determination maximizes the formation of TTHM concentration could become under conditions favoring TTHM formation. It may be used by systems employing ground wat...

  6. Passive exposures of children to volatile trihalomethanes during domestic cleaning activities of their parents

    SciTech Connect

    Andra, Syam S.; Charisiadis, Pantelis; Karakitsios, Spyros; Sarigiannis, Denis A.; Makris, Konstantinos C.

    2015-01-15

    Domestic cleaning has been proposed as a determinant of trihalomethanes (THMs) exposure in adult females. We hypothesized that parental housekeeping activities could influence children's passive exposures to THMs from their mere physical presence during domestic cleaning. In a recent cross-sectional study (n=382) in Cyprus [41 children (<18y) and 341 adults (≥18y)], we identified 29 children who met the study's inclusion criteria. Linear regression models were applied to understand the association between children sociodemographic variables, their individual practices influencing ingestion and noningestion exposures to ΣTHMs, and their urinary THMs levels. Among the children-specific variables, age alone showed a statistically significant inverse association with their creatinine-adjusted urinary ΣTHMs (r{sub S}=−0.59, p<0.001). A positive correlation was observed between urinary ΣTHMs (ng g{sup −1}) of children and matched-mothers (r{sub S}=0.52, p=0.014), but this was not the case for their matched-fathers (r{sub S}=0.39, p=0.112). Time spent daily by the matched-mothers for domestic mopping, toilet and other cleaning activities using chlorine-based cleaning products was associated with their children's urinary THMs levels (r{sub S}=0.56, p=0.007). This trend was not observed between children and their matched-fathers urinary ΣTHMs levels, because of minimum amount of time spent by the latter in performing domestic cleaning. The proportion of variance of creatinine-unadjusted and adjusted urinary ΣTHMs levels in children that was explained by the matched-mothers covariates was 76% and 74% (p<0.001), respectively. A physiologically-based pharmacokinetic model adequately predicted urinary chloroform excretion estimates, being consistent with the corresponding measured levels. Our findings highlighted the influence of mothers' domestic cleaning activities towards enhancing passive THMs exposures of their children. The duration of such activities could be

  7. Role of NOM molecular size on iodo-trihalomethane formation during chlorination and chloramination.

    PubMed

    Zhang, Jie; Chen, Dan-Dan; Li, Lei; Li, Wen-Wei; Mu, Yang; Yu, Han-Qing

    2016-10-01

    Natural organic matter (NOM) is the major precursor for the generation of disinfection byproducts (DBPs) during disinfection, but the role of the NOM molecular size on the formation of iodinated DBPs (I-DBPs) is still unclear. The objective of this study was to evaluate the function of the NOM molecular size on the formation of iodo-trihalomethane (I-THMs) during chlorination and chloramination. Humic acid was adopted as the NOM matrix and fractionated into four molecular weight (MW) groups. Various parameters, including iodide, bromide, NOM concentrations, pH, and pre-chlorination time, were investigated for each MW fraction. During chlorination, high MW fractions (i.e., MW > 100 K Da and 50 K < MW < K00 K Da) produced more I-THMs compared with small MW fractions (i.e., MW < 3 K Da and 3 K < MW < 50 K Da). With the increase in the I(-) or NOM concentration, the formation of I-THMs increased for small MW fractions, while a slight reduction occurred for high MW fractions during chlorination. Higher pH resulted in more I-THM formation for small MW fractions, while the opposite was true for high MW fractions during chlorination. Compared to small MW fractions, bromide was relatively more reactive with high MW fractions in the formation of I-THMs during chlorination. During chloramination, the I-THM yields decreased with the increasing NOM concentration for high MW fractions. The concentration of bromine-containing I-THMs decreased with increasing pH for all MW fractions during chloramination. Additionally, with the prolongation of pre-chlorination time, the total amount of I-THMs decreased remarkably for MWs higher than 3 K Da, while a slight change for MW lower than 3 K Da occurred during chloramination. The results from this study suggest that the molecular weight of the NOM plays an important role in the formation of I-THMs during chlorination and chloramination. PMID:27423047

  8. Passive exposures of children to volatile trihalomethanes during domestic cleaning activities of their parents.

    PubMed

    Andra, Syam S; Charisiadis, Pantelis; Karakitsios, Spyros; Sarigiannis, Denis A; Makris, Konstantinos C

    2015-01-01

    Domestic cleaning has been proposed as a determinant of trihalomethanes (THMs) exposure in adult females. We hypothesized that parental housekeeping activities could influence children's passive exposures to THMs from their mere physical presence during domestic cleaning. In a recent cross-sectional study (n = 382) in Cyprus [41 children (< 18 y) and 341 adults (≥ 18 y)], we identified 29 children who met the study's inclusion criteria. Linear regression models were applied to understand the association between children sociodemographic variables, their individual practices influencing ingestion and noningestion exposures to ΣTHMs, and their urinary THMs levels. Among the children-specific variables, age alone showed a statistically significant inverse association with their creatinine-adjusted urinary ΣTHMs (rS = -0.59, p < 0.001). A positive correlation was observed between urinary ΣTHMs (ng g(-1)) of children and matched-mothers (rS = 0.52, p = 0.014), but this was not the case for their matched-fathers (rS = 0.39, p = 0.112). Time spent daily by the matched-mothers for domestic mopping, toilet and other cleaning activities using chlorine-based cleaning products was associated with their children's urinary THMs levels (rS = 0.56, p = 0.007). This trend was not observed between children and their matched-fathers urinary ΣTHMs levels, because of minimum amount of time spent by the latter in performing domestic cleaning. The proportion of variance of creatinine-unadjusted and adjusted urinary ΣTHMs levels in children that was explained by the matched-mothers covariates was 76% and 74% (p < 0.001), respectively. A physiologically-based pharmacokinetic model adequately predicted urinary chloroform excretion estimates, being consistent with the corresponding measured levels. Our findings highlighted the influence of mothers' domestic cleaning activities towards enhancing passive THMs exposures of their children. The duration of such activities could be further

  9. Association between exposures to brominated trihalomethanes, hepatic injury and type II diabetes mellitus.

    PubMed

    Makris, Konstantinos C; Andrianou, Xanthi D; Charisiadis, Pantelis; Burch, James B; Seth, Ratanesh K; Ioannou, Androniki; Picolos, Michael; Christophi, Costas A; Chatterjee, Saurabh

    2016-01-01

    Non-alcoholic fatty liver disease (NAFLD) is considered the most common liver disorder in the Western world, commonly diagnosed in the majority of obese patients with type 2 diabetes mellitus (T2DM). Metabolic disrupting chemicals with short half-lives, such as those of halogenated structure (trihalomethanes, THM) have been linked with hepatic insulin resistance phenomena in animal studies. However, human studies evaluating the role of THM exposure on liver pathogenesis and T2DM disease process are scarce. The objectives of this study were to: i) determine the association of urinary brominated THM (BrTHM) levels and T2DM disease status, and ii) investigate the association between urinary BrTHM levels and serum alanine aminotransferase (ALT) concentrations, often used as surrogate markers of NAFLD. A pilot case-control study was conducted in Nicosia, Cyprus (n=95). Cases were physician-diagnosed T2DM patients and controls were healthy individuals. Liver enzymes, leptin and TNF-α were measured in sera, while urinary THM levels were measured using tandem mass spectrometry. Diabetics had higher levels of serum leptin, body mass index and ALT than the controls. Among all study participants those with serum ALT levels above the median (17IU/L) had higher mean tribromomethane (TBM) concentrations compared to those with serum ALT below 17IU/L. A significant increase in the odds of having above the median serum ALT levels [OR 6.38, 95% CI: 1.11, 42.84 (p=0.044)] was observed for each unit increase in creatinine-unadjusted urinary TBM levels, along with BMI and past smoking, after adjusting for possible confounders, such as urinary creatinine, age, sex, and leptin; no other THM compound showed a significant association with serum ALT. Logistic regression models for T2DM using the urinary BrTHM as exposure variables did not reach the predetermined level of significance. The interplay between exposures to BrTHM and the initiation of key pathophysiological events relating to

  10. Small portable speed calculator

    NASA Technical Reports Server (NTRS)

    Burch, J. L.; Billions, J. C.

    1973-01-01

    Calculator is adapted stopwatch calibrated for fast accurate measurement of speeds. Single assembled unit is rugged, self-contained, and relatively inexpensive to manufacture. Potential market includes automobile-speed enforcement, railroads, and field-test facilities.

  11. Portable Heat Pump Testing Device

    NASA Astrophysics Data System (ADS)

    Kłosowiak, R.; Bartoszewicz, J.; Urbaniak, R.

    2015-08-01

    The aim of this paper is to present the design and working principle of a portable testing device for heat pumps in the energy recirculation system. The presented test stand can be used for any refrigerating/reverse flow cycle device to calculate the device energy balance. The equipment is made of two portable containers of the capacity of 250 liters to simulate the air heat source and ground heat source with a system of temperature stabilization, compressor heat pump of the coefficient of performance (COP) of = 4.3, a failsafe system and a control and measurement system.

  12. Freely oriented portable superconducting magnet

    DOEpatents

    Schmierer, Eric N.; Prenger, F. Coyne; Hill, Dallas D.

    2010-01-12

    A freely oriented portable superconducting magnet is disclosed. Coolant is supplied to the superconducting magnet from a repository separate from the magnet, enabling portability of the magnet. A plurality of support assemblies structurally anchor and thermally isolate the magnet within a thermal shield. A plurality of support assemblies structurally anchor and thermally isolate the thermal shield within a vacuum vessel. The support assemblies restrain movement of the magnet resulting from energizing and cooldown, as well as from changes in orientation, enabling the magnet to be freely orientable.

  13. Installing Portable Classrooms With Good Air Quality.

    ERIC Educational Resources Information Center

    Godfrey, Ray

    2000-01-01

    Discusses the advantages of modular classrooms and improvements made in indoor air quality, including the pros and cons of portables, challenges districts face when planning and installing portables, and cost considerations. Concluding comments highlight system costs and maintenance required. (GR)

  14. 49 CFR 172.326 - Portable tanks.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... the portable tank are not visible. (d) NON-ODORIZED marking on portable tanks containing LPG. After...-ODORIZED or NOT ODORIZED on two opposing sides near the marked proper shipping name required by...

  15. Taking It with You: Portable PCs.

    ERIC Educational Resources Information Center

    Crawford, Walt

    1993-01-01

    Discussion of DOS computing focuses on portable personal computers. Reviews based on "PC Magazine" for each year since 1985 for portables, laptops, notebooks, and subnotebooks that include prices are provided; and vendor reliability is considered. (LRW)

  16. Identification of chemical warfare agents from vapor samples using a field-portable capillary gas chromatography/membrane-interfaced electron ionization quadrupole mass spectrometry instrument with Tri-Bed concentrator.

    PubMed

    Nagashima, Hisayuki; Kondo, Tomohide; Nagoya, Tomoki; Ikeda, Toru; Kurimata, Naoko; Unoke, Shohei; Seto, Yasuo

    2015-08-01

    A field-portable gas chromatograph-mass spectrometer (Hapsite ER system) was evaluated for the detection of chemical warfare agents (CWAs) in the vapor phase. The system consisted of Tri-Bed concentrator gas sampler (trapping time: 3s(-1)min), a nonpolar low thermal-mass capillary gas chromatography column capable of raising temperatures up to 200°C, a hydrophobic membrane-interfaced electron ionization quadrupole mass spectrometer evacuated by a non-evaporative getter pump for data acquisition, and a personal computer for data analysis. Sample vapors containing as little as 22μg sarin (GB), 100μg soman (GD), 210μg tabun (GA), 55μg cyclohexylsarin (GF), 4.8μg sulfur mustard, 390μg nitrogen mustard 1, 140μg of nitrogen mustard 2, 130μg nitrogen mustard 3, 120μg of 2-chloroacetophenone and 990μg of chloropicrin per cubic meter could be confirmed after Tri-Bed micro-concentration (for 1min) and automated AMDIS search within 12min. Using manual deconvolution by background subtraction of neighboring regions on the extracted ion chromatograms, the above-mentioned CWAs could be confirmed at lower concentration levels. The memory effects were also examined and we found that blister agents showed significantly more carry-over than nerve agents. Gasoline vapor was found to interfere with the detection of GB and GD, raising the concentration limits for confirmation in the presence of gasoline by both AMDIS search and manual deconvolution; however, GA and GF were not subject to interference by gasoline. Lewisite 1, and o-chlorobenzylidene malononitrile could also be confirmed by gas chromatography, but it was hard to quantify them. Vapors of phosgene, chlorine, and cyanogen chloride could be confirmed by direct mass spectrometric detection at concentration levels higher than 2, 140, and 10mg/m(3) respectively, by bypassing the micro-concentration trap and gas chromatographic separation. PMID:26118803

  17. Portable infrared pupillometry: a review.

    PubMed

    Larson, Merlin D; Behrends, Matthias

    2015-06-01

    Portable infrared pupillometers provide an objective measure of pupil size and pupillary reflexes, which for most clinicians was previously only a visual impression. But despite the fact that pupillometry can uncover aspects of how the human pupil reacts to drugs and noxious stimulation, the use of pupillometry has not gained widespread use among anesthesiologists and critical care physicians. The present review is an introduction to the physiology of pupillary reflexes and the currently established clinical applications of infrared pupillometry, which will hopefully encourage physicians to use this diagnostic tool in their clinical practice. Portable infrared pupillometry was introduced in 1989. The technology involves flooding the eye with infrared light and then measuring the reflected image on an infrared sensor. Pupil size, along with variables of the pupillary light reflex and pupillary reflex dilation, is calculated by the instrument and displayed on a screen immediately after each time-stamped measurement. Use of these instruments has uncovered aspects of how the human pupil reacts to drugs and noxious stimulation. The primary clinical applications for portable pupillometry have been in the assessment of brainstem function. Portable pupillometry is useful in the management of pain because it allows for assessments of the effect of opioids and in the titration of combined regional-general anesthetics. PMID:25988634

  18. Portable Pallet-Weighing Apparatus

    NASA Technical Reports Server (NTRS)

    Day, R. M.

    1983-01-01

    Portable apparatus intended for standard four-trunnion pallets readily adaptable to any large payload or other loads where shifting of cargo is to be avoided. Device lifts trunnion of pallet short distance above its resting place. Weight at trunnion applied to load cell. Similar units placed at all four trunnions.

  19. Portable Positron Measurement System (PPMS)

    SciTech Connect

    2011-01-01

    Portable Positron Measurement System (PPMS) is an automated, non-destructive inspection system based on positron annihilation, which characterizes a material's in situatomic-level properties during the manufacturing processes of formation, solidification, and heat treatment. Simultaneous manufacturing and quality monitoring now are possible. Learn more about the lab's project on our facebook site http://www.facebook.com/idahonationallaboratory.

  20. Portable sandblaster cleans small areas

    NASA Technical Reports Server (NTRS)

    Severin, H. J.

    1966-01-01

    Portable sandblasting unit rapidly and effectively cleans localized areas on a metal surface. The unit incorporates a bellows enclosure, masking plate, sand container, and used sand accummulator connected to a vacuum system. The bellows is equipped with an inspection window and light for observation of the sanding operation.

  1. Portable File Format (PFF) specifications.

    SciTech Connect

    Dolan, Daniel H.,

    2015-02-01

    Created at Sandia National Laboratories, the Portable File Format (PFF) allows binary data transfer across computer platforms. Although this capability is supported by many other formats, PFF files are still in use at Sandia, particularly in pulsed power research. This report provides detailed PFF specifications for accessing data without relying on legacy code.

  2. Portable vacuum object handling device

    DOEpatents

    Anderson, Gordon H.

    1983-08-09

    The disclosure relates to a portable device adapted to handle objects which are not to be touched by hand. A piston and bore wall form a vacuum chamber communicating with an adaptor sealably engageable with an object to be lifted. The piston is manually moved and set to establish vacuum. A valve is manually actuatable to apply the vacuum to lift the object.

  3. Portable Positron Measurement System (PPMS)

    ScienceCinema

    None

    2013-05-28

    Portable Positron Measurement System (PPMS) is an automated, non-destructive inspection system based on positron annihilation, which characterizes a material's in situatomic-level properties during the manufacturing processes of formation, solidification, and heat treatment. Simultaneous manufacturing and quality monitoring now are possible. Learn more about the lab's project on our facebook site http://www.facebook.com/idahonationallaboratory.

  4. Apollo Portable Life Support System

    NASA Technical Reports Server (NTRS)

    1968-01-01

    With its exterior removed, the Apollo portable life support system (PLSS) can be studied. The PLSS is worn as a backpack over the extravehicular mobility unit (EMU), a multi-layered spacesuit used for outside the spacecraft activity. This is a close-up of the working parts of the PLSS.

  5. Apollo Portable Life Support System

    NASA Technical Reports Server (NTRS)

    1968-01-01

    With its exterior removed, the Apollo portable life support system (PLSS) can be studied. The PLSS is worn as a backpack over the extravehicular mobility unit (EMU), a multi-layered spacesuit used for outside the spacecraft activity. This is a wider view of the exposed interior working parts of the PLSS and its removed cover.

  6. Portable thermo-powered high-throughput visual electrochemiluminescence sensor.

    PubMed

    Hao, Nan; Xiong, Meng; Zhang, Jia-dong; Xu, Jing-Juan; Chen, Hong-Yuan

    2013-12-17

    This paper describes a portable thermo-powered high-throughput visual electrochemiluminescence (ECL) sensor for the first time. This sensor is composed of a tiny power supply device based on thermal-electrical conversion and a facile prepared array electrode. The ECL detection could be conducted with thermo-power, which is easily accessible. For example, hot water, a bonfire, or a lighted candle enables the detection to be conducted. And the assay can be directly monitored by the naked eye semiquantitatively or smart phones quantitatively. Combined with transparent electrode and array microreactors, a portable high-throughput sensor was achieved. The portable device, avoiding the use of an electrochemical workstation to generate potential and a photomultiplier tube to receive the signal, is not only a valuable addition for traditional methods but also a suitable device for field operation or point-of-care testing. PMID:24215560

  7. Impacts of powdered activated carbon addition on trihalomethane formation reactivity of dissolved organic matter in membrane bioreactor effluent.

    PubMed

    Ma, Defang; Gao, Yue; Gao, Baoyu; Wang, Yan; Yue, Qinyan; Li, Qian

    2014-12-01

    Characteristics and trihalomethane (THM) formation reactivity of dissolved organic matter (DOM) in effluents from two membrane bioreactors (MBRs) with and without powdered activated carbon (PAC) addition (referred to as PAC/MBR and MBR, respectively) were examined to investigate the effects of PAC addition on THM formation of MBR effluent during chlorination. PAC addition increased the specific UV absorbance. Hydrophobic DOM especially hydrophobic acids in PAC/MBR effluent (50%) were more than MBR effluent (42%). DOM with molecular weight <1 kDa constituted 12% of PAC/MBR effluent DOM, which was less than that of MBR effluent (16%). Data obtained from excitation and emission matrix fluorescence spectroscopy revealed that PAC/MBR effluent DOM contained more simple aromatic protein, but had less fulvic acid-like and soluble microbial by-product-like. PAC addition reduced the formation of bromine-containing THMs during chlorination of effluents, but increased THM formation reactivity of effluent DOM. PMID:25150685

  8. 49 CFR 176.137 - Portable magazine.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... type 3 magazine under 27 CFR part 555 subpart K may be used for the stowage of Class 1 (explosive... 49 Transportation 2 2012-10-01 2012-10-01 false Portable magazine. 176.137 Section 176.137... Requirements for Class 1 (Explosive) Materials Stowage § 176.137 Portable magazine. (a) Each portable...

  9. 48 CFR 1837.170 - Pension portability.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 48 Federal Acquisition Regulations System 6 2010-10-01 2010-10-01 true Pension portability. 1837... ADMINISTRATION SPECIAL CATEGORIES OF CONTRACTING SERVICE CONTRACTING Service Contracts-General 1837.170 Pension portability. (a) It is NASA's policy not to require pension portability in service contracts. However,...

  10. 48 CFR 1837.170 - Pension portability.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 48 Federal Acquisition Regulations System 6 2011-10-01 2011-10-01 false Pension portability. 1837... ADMINISTRATION SPECIAL CATEGORIES OF CONTRACTING SERVICE CONTRACTING Service Contracts-General 1837.170 Pension portability. (a) It is NASA's policy not to require pension portability in service contracts. However,...

  11. 46 CFR 120.430 - Portable lights.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Portable lights. 120.430 Section 120.430 Shipping COAST... Systems § 120.430 Portable lights. Each vessel must be equipped with at least two operable portable battery lights. One of these lights must be located at the operating station and the other at the...

  12. 46 CFR 183.430 - Portable lights

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 7 2011-10-01 2011-10-01 false Portable lights 183.430 Section 183.430 Shipping COAST...) ELECTRICAL INSTALLATION Lighting Systems § 183.430 Portable lights Each vessel must be equipped with at least two operable portable battery lights. One of these lights must be located at the operating station...

  13. 46 CFR 183.430 - Portable lights

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 7 2012-10-01 2012-10-01 false Portable lights 183.430 Section 183.430 Shipping COAST...) ELECTRICAL INSTALLATION Lighting Systems § 183.430 Portable lights Each vessel must be equipped with at least two operable portable battery lights. One of these lights must be located at the operating station...

  14. 46 CFR 120.430 - Portable lights.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false Portable lights. 120.430 Section 120.430 Shipping COAST... Systems § 120.430 Portable lights. Each vessel must be equipped with at least two operable portable battery lights. One of these lights must be located at the operating station and the other at the...

  15. 46 CFR 183.430 - Portable lights

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 7 2013-10-01 2013-10-01 false Portable lights 183.430 Section 183.430 Shipping COAST...) ELECTRICAL INSTALLATION Lighting Systems § 183.430 Portable lights Each vessel must be equipped with at least two operable portable battery lights. One of these lights must be located at the operating station...

  16. 46 CFR 120.430 - Portable lights.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false Portable lights. 120.430 Section 120.430 Shipping COAST... Systems § 120.430 Portable lights. Each vessel must be equipped with at least two operable portable battery lights. One of these lights must be located at the operating station and the other at the...

  17. 46 CFR 120.430 - Portable lights.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false Portable lights. 120.430 Section 120.430 Shipping COAST... Systems § 120.430 Portable lights. Each vessel must be equipped with at least two operable portable battery lights. One of these lights must be located at the operating station and the other at the...

  18. 46 CFR 183.430 - Portable lights

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 7 2014-10-01 2014-10-01 false Portable lights 183.430 Section 183.430 Shipping COAST...) ELECTRICAL INSTALLATION Lighting Systems § 183.430 Portable lights Each vessel must be equipped with at least two operable portable battery lights. One of these lights must be located at the operating station...

  19. 46 CFR 120.430 - Portable lights.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Portable lights. 120.430 Section 120.430 Shipping COAST... Systems § 120.430 Portable lights. Each vessel must be equipped with at least two operable portable battery lights. One of these lights must be located at the operating station and the other at the...

  20. 46 CFR 183.430 - Portable lights

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 7 2010-10-01 2010-10-01 false Portable lights 183.430 Section 183.430 Shipping COAST...) ELECTRICAL INSTALLATION Lighting Systems § 183.430 Portable lights Each vessel must be equipped with at least two operable portable battery lights. One of these lights must be located at the operating station...

  1. Los Alamos portable beta-ray spectrometer

    NASA Astrophysics Data System (ADS)

    Erkkila, B. H.; Brake, R. J.; Waechter, D. A.

    The integration of a beta ray detector to multichannel analyzer and computer has resulted in a portable spectrometer for studying beta rays in the field. The detector is a 5 cm diameter by 2 cm thick plastic scintillator. Other detectors can easily be integrated into the package. The integral instrument package is 15 cm wide by 15 cm high by 25 cm long and weighs less than 10 pounds. Internal rechargeable batteries for 8 hours of field operation are included. The instrument contains a detector, an amplifier, a multichannel analyzer, and a liquid crystal display (LCD). A microprocessor controls all the functions of the instrument and is programmed to display all necessary information and 128 channel spectra on the LCD.

  2. Portable sensor technology for rotational ground motions

    NASA Astrophysics Data System (ADS)

    Bernauer, Felix; Wassermann, Joachim; Guattari, Frédéric; Igel, Heiner

    2016-04-01

    In this contribution we present performance characteristics of a single component interferometric fiber-optic gyroscope (IFOG). The prototype sensor is provided by iXBlue, France. It is tested in the framework of the European Research Council Project, ROMY (Rotational motions - a new observable for seismology), on its applicability as a portable and field-deployable sensor for rotational ground motions. To fully explore the benefits of this new seismic observable especially in the fields of vulcanology, ocean generated noise and geophysical exploration, such a sensor has to fulfill certain requirements regarding portability, power consumption, time stamping stability and dynamic range. With GPS-synchronized time stamping and miniseed output format, data acquisition is customized for the use in seismology. Testing time stamping accuracy yields a time shift of less than 0.0001 s and a correlation coefficient of 0.99 in comparison to a commonly used data acquisition system, Reftek 120. Sensor self-noise is below 5.0 ṡ 10‑8 rads‑1Hz‑1/2 for a frequency band from 0.001 Hz to 5.0 Hz. Analysis of Allan deviation shows an angle random walk of 3.5 ṡ 10‑8 rads‑1Hz‑1/2. Additionally, the operating range diagram is shown and ambient noise analysis is performed. The sensitivity of sensor self-noise to variations in surrounding temperature and magnetic field is tested in laboratory experiments. With a power consumption of less than 10 W, the whole system (single component sensor + data acquisition) is appropriate for field use with autonomous power supply.

  3. Portable top drive cuts horizontal drilling costs

    SciTech Connect

    Jackson, B.; Yager, D.

    1993-11-01

    Economic analysis of a seven-well, long-reach horizontal drilling program into an unconsolidated, heavy-oil-bearing reservoir in Winter field near the Alberta/Saskatchewan border in Canada reveals that -- in the right application -- renting a portable top drive drilling system can reduce total drilling costs. Use of the portable top drive combined with other cost-saving measures enabled Saskoil, one of Canada`s larger independents, to drill more cheaply, on a cost-per-meter basis, in 1993 than in 1992. This was despite significant rental rates for drilling rigs and directional drilling services caused by increased demand in Western Canada. Total cost savings of 10% on wells that would otherwise cost in the (C) $500,000 range are believed realistic. Based on this year`s performance, Saskoil recommends top drive for the company`s future horizontal wells in this area. This article describes the operator`s horizontal well program, advantages of top drive in that program and how it was installed and applied. Estimated time savings for six wells, plus other ways top drive can cut costs and improve operations are discussed.

  4. Intelligent hand-portable proliferation sensing system

    SciTech Connect

    Dieckman, S.L.; Bostrom, G.A.; Waterfield, L.G.; Jendrzejczyk, J.A.; Ahuja, S.; Raptis, A.C.

    1997-08-01

    Argonne National Laboratory, with support from DOE`s Office of Nonproliferation and National Security, is currently developing an intelligent hand-portable sensor system. This system is designed specifically to support the intelligence community with the task of in-field sensing of nuclear proliferation and related activities. Based upon pulsed laser photo-ionization time-of-flight mass spectrometry technology, this novel sensing system is capable of quickly providing a molecular or atomic analysis of specimens. The system is capable of analyzing virtually any gas phase molecule, or molecule that can be induced into the gas phase by (for example) sample heating. This system has the unique advantages of providing unprecedented portability, excellent sensitivity, tremendous fieldability, and a high performance/cost ratio. The system will be capable of operating in a highly automated manner for on-site inspections, and easily modified for other applications such as perimeter monitoring aboard a plane or drone. The paper describes the sensing system.

  5. Application of portable Raman instruments for fast and non-destructive detection of minerals on outcrops.

    PubMed

    Jehlicka, J; Vítek, P; Edwards, H G M; Heagraves, M; Capoun, T

    2009-08-01

    Raman spectral signatures have been obtained in situ for a series of minerals using portable Raman instruments. Cerussite, anglesite, wulfenite, titanite, calcite, tremolite, andradite and quartz were detected using portable Raman spectrometer First Defender XL (Ahura). Baryte, almandine and realgar Raman spectra obtained by this instrument in the field were compared to the data measured by the other mobile Raman instrument Inspector Raman (DeltaNu). Bench Raman dispersive microspectrometer (InVia Reflex, Renishaw) was used for comparative purposes. All spectra were obtained using a 785nm diode excitation. Although displaying lower spectral resolution comparing with the laboratory confocal instrument both portable instruments permit unambiguous detection of minerals in the field. These possibilities designate portable Raman machines as excellent tools for field geological applications. Miniaturised Raman instrument combined with LIBS will be included in the payload of the EXO Mars mission and would open interesting research possibilities in other in situ field planetary studies. PMID:18993111

  6. Onsite Portable Alarm System - Its Merit and Application

    NASA Astrophysics Data System (ADS)

    Saita, J.; Sato, T.; Nakamura, Y.

    2007-12-01

    wave alarms was actually issued by three times during the rescue work. Although this is one example for the actual application of portable onsite alarm, it is possible to apply the other field as the construction field. In this presentation, Portable Onsite Alarm is discussed from views of its necessity and application.

  7. Microprocessor controlled portable TLD system.

    PubMed

    Apathy, I; Deme, S; Feher, I

    1996-01-01

    An up-to-date microprocessor controlled thermoluminescence dosemeter (TLD) system for environmental and space dose measurements has been developed. The earlier version of the portable TLD system, Pille, was successfully used on Soviet orbital stations as well as on the US Space Shuttle, and for environmental monitoring. The new portable TLD system, Pille'95, consists of a reader and TL bulb dosemeters, and each dosemeter is provided with an EEPROM chip for automatic identification. The glow curve data are digitised and analysed by the program of the reader. The measured data and the identification number appear on the LED display of the reader. Up to several thousand measured data together with the glow curves can be stored on a removable flash memory card. The whole system is supplied either from built-in rechargeable batteries or from the mains of the space station. PMID:11540052

  8. Portable code development in C

    SciTech Connect

    Brown, S.A.

    1990-11-06

    With a new generation of high performance computers appearing around us on a time scale of months, a new challenge for developers of simulation codes is to write and maintain production codes that are both highly portable and maximally efficient. My contention is that C is the language that is both best suited to that goal and is widely available today. GLF is a new code written mainly in C which is intended to have all of the XRASER physics and run on any platform of interest. It demonstrates the power of the C paradigm for code developers and flexibility and ease of use for the users. Three fundamental problems are discussed: the C/UNIX development environment; the supporting tools and libraries which handle data and graphics portability issues; and the advantages of C in numerical simulation code development.

  9. Microprocessor controlled portable TLD system

    NASA Technical Reports Server (NTRS)

    Apathy, I.; Deme, S.; Feher, I.

    1996-01-01

    An up-to-date microprocessor controlled thermoluminescence dosemeter (TLD) system for environmental and space dose measurements has been developed. The earlier version of the portable TLD system, Pille, was successfully used on Soviet orbital stations as well as on the US Space Shuttle, and for environmental monitoring. The new portable TLD system, Pille'95, consists of a reader and TL bulb dosemeters, and each dosemeter is provided with an EEPROM chip for automatic identification. The glow curve data are digitised and analysed by the program of the reader. The measured data and the identification number appear on the LED display of the reader. Up to several thousand measured data together with the glow curves can be stored on a removable flash memory card. The whole system is supplied either from built-in rechargeable batteries or from the mains of the space station.

  10. Portable liquid collection electrostatic precipitator

    DOEpatents

    Carlson, Duane C.; DeGange, John J.; Halverson, Justin E.

    2005-10-18

    A portable liquid collection electrostatic collection precipitator for analyzing air is provided which is a relatively small, self-contained device. The device has a tubular collection electrode, a reservoir for a liquid, and a pump. The pump pumps the liquid into the collection electrode such that the liquid flows down the exterior of the collection electrode and is recirculated to the reservoir. An air intake is provided such that air to be analyzed flows through an ionization section to ionize analytes in the air, and then flows near the collection electrode where ionized analytes are collected. A portable power source is connected to the air intake and the collection electrode. Ionizable constituents in the air are ionized, attracted to the collection electrode, and precipitated in the liquid. The precipitator may also have an analyzer for the liquid and may have a transceiver allowing remote operation and data collection.

  11. Portable telepathology: methods and tools.

    PubMed

    Alfaro, Luis; Roca, Ma José

    2008-01-01

    Telepathology is becoming easier to implement in most pathology departments. In fact e-mail image transmit can be done from almost any pathologist as a simplistic telepathology system. We tried to develop a way to improve capabilities of communication among pathologists with the idea that the system should be affordable for everybody. We took the premise that any pathology department would have microscopes and computers with Internet connection, and selected a few elements to convert them into a telepathology station. Needs were reduced to a camera to collect images, a universal microscope adapter for the camera, a device to connect the camera to the computer, and a software for the remote image transmit. We found out a microscope adapter (MaxView Plus) that allowed us connect almost any domestic digital camera to any microscope. The video out signal from the camera was sent to the computer through an Aver Media USB connector. At last, we selected a group of portable applications that were assembled into a USB memory device. Portable applications are computer programs that can be carried generally on USB flash drives, but also in any other portable device, and used on any (Windows) computer without installation. Besides, when unplugging the device, none of personal data is left behind. We selected open-source applications, and based the pathology image transmission to VLC Media Player due to its functionality as streaming server, portability and ease of use and configuration. Audio transmission was usually done through normal phone lines. We also employed alternative videoconferencing software, SightSpeed for bi-directional image transmission from microscopes, and conventional cameras allowing visual communication and also image transmit from gross pathology specimens. All these elements allowed us to install and use a telepathology system in a few minutes, fully prepared for real time image broadcast. PMID:18673507

  12. Compact portable diffraction moire interferometer

    DOEpatents

    Deason, V.A.; Ward, M.B.

    1988-05-23

    A compact and portable moire interferometer used to determine surface deformations of an object. The improved interferometer is comprised of a laser beam, optical and fiber optics devices coupling the beam to one or more evanescent wave splitters, and collimating lenses directing the split beam at one or more specimen gratings. Observations means including film and video cameras may be used to view and record the resultant fringe patterns. 7 figs.

  13. Compact portable diffraction moire interferometer

    DOEpatents

    Deason, Vance A.; Ward, Michael B.

    1989-01-01

    A compact and portable moire interferometer used to determine surface deformations of an object. The improved interferometer is comprised of a laser beam, optical and fiber optics devices coupling the beam to one or more evanescent wave splitters, and collimating lenses directing the split beam at one or more specimen gratings. Observation means including film and video cameras may be used to view and record the resultant fringe patterns.

  14. Portable Immune-Assessment System

    NASA Technical Reports Server (NTRS)

    Pierson, Duane L.; Stowe, Raymond P.; Mishra, Saroj K.

    1995-01-01

    Portable immune-assessment system developed for use in rapidly identifying infections or contaminated environment. System combines few specific fluorescent reagents for identifying immune-cell dysfunction, toxic substances, buildup of microbial antigens or microbial growth, and potential identification of pathogenic microorganisms using fluorescent microplate reader linked to laptop computer. By using few specific dyes for cell metabolism, DNA/RNA conjugation, specific enzyme activity, or cell constituents, one makes immediate, onsite determination of person's health or of contamination of environment.

  15. Portable vacuum object handling device

    DOEpatents

    Anderson, G.H.

    1983-08-09

    The disclosure relates to a portable device adapted to handle objects which are not to be touched by hand. A piston and bore wall form a vacuum chamber communicating with an adaptor sealably engageable with an object to be lifted. The piston is manually moved and set to establish vacuum. A valve is manually actuatable to apply the vacuum to lift the object. 1 fig.

  16. Portable Presentation And Instruction Unit

    NASA Technical Reports Server (NTRS)

    Christman, L.; Hoang, N.

    1994-01-01

    Proposed electronic display unit reminiscent of kiosk serves as portable, interactive, multimedia information terminal. Used as traveling science exhibit, aid for teaching science in schools, or training and skill-refresher device for space flight crews. Provides interactive video and audio displays, including three-dimensional-appearing video simulations. Speeds learning and improves retention by applying principles of scientific visualization. Also helps previously trained but recently unpracticed personnel relearn special skills and procedures quickly.

  17. Software Complexity Threatens Performance Portability

    SciTech Connect

    Gamblin, T.

    2015-09-11

    Modern HPC software packages are rarely self-contained. They depend on a large number of external libraries, and many spend large fractions of their runtime in external subroutines. Performance portability depends not only on the effort of application teams, but also on the availability of well-tuned libraries. At most sites, the burden of maintaining libraries is shared by code teams and facilities. Facilities typically provide well-tuned default versions, but code teams frequently build with bleeding-edge compilers to achieve high performance. For this reason, HPC has no “standard” software stack, unlike other domains where performance is not critical. Incompatibilities among compilers and software versions force application teams and facility staff to re-build custom versions of libraries for each new toolchain. Because the number of potential configurations is combinatorial, and because HPC software is notoriously difficult to port to new machines [3, 7, 8], the tuning effort required to support and maintain performance-portable libraries outstrips the available manpower at most sites. Software complexity is a growing obstacle to performance portability for HPC.

  18. Development of a portable ambient temperature radiometric assaying instrument

    SciTech Connect

    Lavietes, A.D.; McQuaid, J.H.; Ruhter, W.D.

    1994-10-01

    There is a strong need for portable radiometric instrumentation that can accurately confirm the presence of nuclear materials and allow isotopic analysis of radionuclides in the field. To fulfill this need we are developing a hand-held, non-cryogenic, low-power gamma- and x-ray measurement and analysis instrument that can both search and then accurately verify the presence of nuclear materials. We report on the use of cadmium zinc telluride detectors, signal processing electronics, and the new field-portable instrument based on the MicroNOMAD Multichannel Analyzer from EG&G ORTBC. We also describe the isotopic analysis that allows uranium enrichment measurements to be made accurately in the field.

  19. Portable gas chromatograph-mass spectrometer

    DOEpatents

    Andresen, Brian D.; Eckels, Joel D.; Kimmons, James F.; Myers, David W.

    1996-01-01

    A gas chromatograph-mass spectrometer (GC-MS) for use as a field portable organic chemical analysis instrument. The GC-MS is designed to be contained in a standard size suitcase, weighs less than 70 pounds, and requires less than 600 watts of electrical power at peak power (all systems on). The GC-MS includes: a conduction heated, forced air cooled small bore capillary gas chromatograph, a small injector assembly, a self-contained ion/sorption pump vacuum system, a hydrogen supply, a dual computer system used to control the hardware and acquire spectrum data, and operational software used to control the pumping system and the gas chromatograph. This instrument incorporates a modified commercial quadrupole mass spectrometer to achieve the instrument sensitivity and mass resolution characteristic of laboratory bench top units.

  20. Portable gas chromatograph-mass spectrometer

    DOEpatents

    Andresen, B.D.; Eckels, J.D.; Kimmons, J.F.; Myers, D.W.

    1996-06-11

    A gas chromatograph-mass spectrometer (GC-MS) is described for use as a field portable organic chemical analysis instrument. The GC-MS is designed to be contained in a standard size suitcase, weighs less than 70 pounds, and requires less than 600 watts of electrical power at peak power (all systems on). The GC-MS includes: a conduction heated, forced air cooled small bore capillary gas chromatograph, a small injector assembly, a self-contained ion/sorption pump vacuum system, a hydrogen supply, a dual computer system used to control the hardware and acquire spectrum data, and operational software used to control the pumping system and the gas chromatograph. This instrument incorporates a modified commercial quadrupole mass spectrometer to achieve the instrument sensitivity and mass resolution characteristic of laboratory bench top units. 4 figs.

  1. Portable gas chromatograph-mass spectrometer

    SciTech Connect

    Andresen, B.D.; Eckels, J.D.; Kimmins, J.F.; Myers, D.W.

    1994-12-31

    A gas chromatograph-mass spectrometer (GC-MS) for use as a field portable organic chemical analysis instrument. The GC-MS is designed to be contained in a standard size suitcase, weighs less than 70 pounds, and requires less than 600 watts of electrical power at peak power (all systems on). The GC-MS includes: a conduction heated, forced air cooled small bore capillary gas chromatograph, a small injector assembly, a self-contained ion/sorption pump vacuum system, a hydrogen supply, a dual computer system used to control the hardware and acquire spectrum data, and operational software used to control the pumping system and the gas chromatograph. This instrument incorporates a modified commercial quadrupole mass spectrometer to achieve the instrument sensitivity and mass resolution characteristic of laboratory bench top units.

  2. Portable radiation detector and mapping system

    SciTech Connect

    Hofstetter, K.J.; Hayes, D.W.; Eakle, R.F.

    1995-12-31

    A portable radiation detector and mapping system (RADMAPS) has been developed to detect, locate, and plot nuclear radiation intensities on commercially available digital maps and other images. The field unit records gamma-ray spectra or neutron signals together with positions from a global positioning system (GPS) on flash memory cards. The recorded information is then transferred to a laptop computer for spectral data analyses and then georegistered graphically on maps, photographs, etc. RADMAPS integrates several existing technologies to produce a preprogrammable field unit uniquely suited for each survey, as required. The system records spectra from a NaI(Tl) gamma-ray detector or an enriched {sup 6}Li doped glass neutron scintillator. Standard Geographic Information System (GIS) software installed in a lap-top, complete with CD-ROM supporting digitally imaged maps, permits the characterization of nuclear material in the field when the presence of such material is not otherwise documented. This paper gives the results of a typical site survey of the Savannah River site (SRS) using RADMAPS. The ability to provide rapid field data should be of use in treaty verification, safeguards, decontamination, and nuclear weapons dismantlement.

  3. Portable x-ray fluorescence spectrometer. Innovative technology summary report

    SciTech Connect

    1998-12-01

    This report describes the application of portable X-ray fluorescence (XRF) spectrometry to characterize materials related to deactivation and decommissioning (D and D) of contaminated facilities. Two portable XRF instruments manufactured by TN Spectrace were used in a technology evaluation as part of the Large-Scale Demonstration Project (LSDP) held at the Chicago Pile-5 Research Reactor (CP-5) located at Argonne National Laboratory (ANL). The LSDP is sponsored by the US Department of Energy (DOE), Office of Science and Technology, Deactivation and Decommissioning Focus Are (DDFA). The objective of the LSDP is to demonstrate innovative technologies or technology applications potentially beneficial to the D and D of contaminated facilities. The portable XRF technology offers several potential benefits for rapid characterization of facility components and contaminants, including significant cost reduction, fast turnaround time,a nd virtually no secondary waste. Field work for the demonstration of the portable XRF technology was performed from August 28--September 3, 1996 and October 30--December 13, 1996.

  4. 75 FR 5013 - Local Number Portability Porting Interval and Validation Requirements; Telephone Number Portability

    Federal Register 2010, 2011, 2012, 2013, 2014

    2010-02-01

    ... From the Federal Register Online via the Government Publishing Office FEDERAL COMMUNICATIONS COMMISSION 47 CFR Part 52 Local Number Portability Porting Interval and Validation Requirements; Telephone Number Portability AGENCY: Federal Communications Commission. ACTION: Proposed rule. SUMMARY:...

  5. 33 CFR 145.01 - Portable and semi-portable fire extinguishers.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ...-portable fire extinguishers. On all manned platforms and on all unmanned platforms where crews are...-portable fire extinguishers shall be installed and maintained. On all unmanned platforms where crews...

  6. 33 CFR 145.01 - Portable and semi-portable fire extinguishers.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ...-portable fire extinguishers. On all manned platforms and on all unmanned platforms where crews are...-portable fire extinguishers shall be installed and maintained. On all unmanned platforms where crews...

  7. 33 CFR 145.01 - Portable and semi-portable fire extinguishers.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ...-portable fire extinguishers. On all manned platforms and on all unmanned platforms where crews are...-portable fire extinguishers shall be installed and maintained. On all unmanned platforms where crews...

  8. 33 CFR 145.01 - Portable and semi-portable fire extinguishers.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ...-portable fire extinguishers. On all manned platforms and on all unmanned platforms where crews are...-portable fire extinguishers shall be installed and maintained. On all unmanned platforms where crews...

  9. 33 CFR 145.01 - Portable and semi-portable fire extinguishers.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ...-portable fire extinguishers. On all manned platforms and on all unmanned platforms where crews are...-portable fire extinguishers shall be installed and maintained. On all unmanned platforms where crews...

  10. Portable atomic frequency standard based on coherent population trapping

    NASA Astrophysics Data System (ADS)

    Shi, Fan; Yang, Renfu; Nian, Feng; Zhang, Zhenwei; Cui, Yongshun; Zhao, Huan; Wang, Nuanrang; Feng, Keming

    2015-05-01

    In this work, a portable atomic frequency standard based on coherent population trapping is designed and demonstrated. To achieve a portable prototype, in the system, a single transverse mode 795nm VCSEL modulated by a 3.4GHz RF source is used as a pump laser which generates coherent light fields. The pump beams pass through a vapor cell containing atom gas and buffer gas. This vapor cell is surrounded by a magnetic shield and placed inside a solenoid which applies a longitudinal magnetic field to lift the Zeeman energy levels' degeneracy and to separate the resonance signal, which has no first-order magnetic field dependence, from the field-dependent resonances. The electrical control system comprises two control loops. The first one locks the laser wavelength to the minimum of the absorption spectrum; the second one locks the modulation frequency and output standard frequency. Furthermore, we designed the micro physical package and realized the locking of a coherent population trapping atomic frequency standard portable prototype successfully. The short-term frequency stability of the whole system is measured to be 6×10-11 for averaging times of 1s, and reaches 5×10-12 at an averaging time of 1000s.

  11. Portable punch and die jig

    DOEpatents

    Lewandowski, Edward F.; Anderson, Petrus A.

    1978-01-01

    A portable punch and die jig includes a U-shaped jig of predetermined width having a slot of predetermined width in the base thereof extending completely across the width of the jig adapted to fit over the walls of rectangular tubes and a punch and die assembly disposed in a hole extending through the base of the jig communicating with the slot in the base of the jig for punching a hole in the walls of the rectangular tubes at precisely determined locations.

  12. Improved Portable Ultrasonic Leak Detectors

    NASA Technical Reports Server (NTRS)

    Youngquist, Robert C.; Moerk, John S.; Haskell, William D.; Cox, Robert B.; Polk, Jimmy D.; Strobel, James P.; Luaces, Frank

    1995-01-01

    Improved portable ultrasonic leak detector features three interchangeable ultrasonic-transducer modules, each suited for operation in unique noncontact or contact mode. One module equipped with ultrasound-collecting horn for use in scanning to detect leaks from distance; horn provides directional sensitivity pattern with sensitivity multiplied by factor of about 6 in forward direction. Another module similar, does not include horn; this module used for scanning close to suspected leak, where proximity of leak more than offsets loss of sensitivity occasioned by lack of horn. Third module designed to be pressed against leaking vessel; includes rugged stainless-steel shell. Improved detectors perform significantly better, smaller, more rugged, and greater sensitivity.

  13. Portable receiver for radar detection

    DOEpatents

    Lopes, Christopher D.; Kotter, Dale K.

    2008-10-14

    Various embodiments are described relating to a portable antenna-equipped device for multi-band radar detection. The detection device includes a plurality of antennas on a flexible substrate, a detection-and-control circuit, an indicator and a power source. The antenna may include one or more planar lithographic antennas that may be fabricated on a thin-film substrate. Each antenna may be tuned to a different selection frequency or band. The antennas may include a bolometer for radar detection. Each antenna may include a frequency selective surface for tuning to the selection frequency.

  14. Portable X-Ray Device

    NASA Technical Reports Server (NTRS)

    1983-01-01

    Portable x-ray instrument developed by NASA now being produced commercially as an industrial tool may soon find further utility as a medical system. The instrument is Lixiscope - Low Intensity X-Ray Imaging Scope -- a self-contained, battery-powered fluoroscope that produces an instant image through use of a small amount of radioactive isotope. Originally developed by Goddard Space Flight Center, Lixiscope is now being produced by Lixi, Inc. which has an exclusive NASA license for one version of the device.

  15. Portable Ethylene Oxide Sterilization Chamber

    PubMed Central

    Songer, J. R.; Mathis, R. G.

    1969-01-01

    A portable ethylene oxide sterilization chamber was designed, constructed, and tested for use in the sterilization of embolectomy catheters. The unit can accommodate catheters up to 40 inches (101.6 cm) in length and can be operated for less than 4 cents per cycle. A constant concentration of 500 mg of ethylene oxide per liter of space and holding periods of 4 and 6 hr at 43 and 22 C, respectively, were adequate when tested with B. subtilis spores. The estimated cost of construction was $165.00. If temperature control is unnecessary, the cost is approximately $80.00. Images PMID:4977644

  16. Portability Support for High Performance Computing

    NASA Technical Reports Server (NTRS)

    Cheng, Doreen Y.; Cooper, D. M. (Technical Monitor)

    1994-01-01

    While a large number of tools have been developed to support application portability, high performance application developers often prefer to use vendor-provided, non-portable programming interfaces. This phenomena indicates the mismatch between user priorities and tool capabilities. This paper summarizes the results of a user survey and a developer survey. The user survey has revealed the user priorities and resulted in three criteria for evaluating tool support for portability. The developer survey has resulted in the evaluation of portability support and indicated the possibilities and difficulties of improvements.

  17. 46 CFR 119.458 - Portable fuel systems.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Portable fuel systems. 119.458 Section 119.458 Shipping... Machinery Requirements § 119.458 Portable fuel systems. (a) Portable fuel systems, including portable tanks and related fuel lines and accessories, are prohibited except where used for portable dewatering...

  18. 46 CFR 119.458 - Portable fuel systems.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false Portable fuel systems. 119.458 Section 119.458 Shipping... Machinery Requirements § 119.458 Portable fuel systems. (a) Portable fuel systems, including portable tanks and related fuel lines and accessories, are prohibited except where used for portable dewatering...

  19. 46 CFR 119.458 - Portable fuel systems.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false Portable fuel systems. 119.458 Section 119.458 Shipping... Machinery Requirements § 119.458 Portable fuel systems. (a) Portable fuel systems, including portable tanks and related fuel lines and accessories, are prohibited except where used for portable dewatering...

  20. New designs for portable Raman instrumentation in defense applications

    NASA Astrophysics Data System (ADS)

    Carron, Keith; Ray, Bryan; Buller, Shane; Strickland, Aaron

    2016-05-01

    The realization of global terrorism after the September 11 attacks led immediately to a need for rapid field analysis of materials. Colorimetric test kits existed, but they are very subjective to interpret and they require contact with the sample. A push for handheld spectrometers quickly led to FTIR systems with ATR sampling, handheld IMS systems, and handheld Raman spectrometers. No single technique solves all of the problems of field detection. We will discuss the development of Raman instrumentation and, in particular, cover the advantages and the problems that are inherent in Raman portability. Portable Raman instrumentation began with a limited number of accessories: a point-and-shoot and some sort of vial adaptor. Currently this has expanded to stand-off attachments for measurements at a distance, air sampling to look for toxic gasses or aerosols, Orbital Raster Scan (ORS) to spatially average over samples, SERS attachments for trace detection, and fiber optic probes.

  1. Portable electrocardiograph through android application.

    PubMed

    De Oliveira, Igor H; Cene, V H; Balbinot, A

    2015-01-01

    An electrocardiograph was designed and implemented, being capable of obtaining electrical signals from the heart, and sending this data via Bluetooth to a tablet, in which the signals are graphically shown. The user interface is developed as an Android application. Because of the technological progress and the increasing use of full portable systems, such as tablets and cell phones, it is important to understand the functioning and development of an application, which provides a basis for conducting studies using this technology as an interface. The project development includes concepts of electronics and its application to achieve a portable and functional final project, besides using a specific programmable integrated circuit for electrocardiogram, electroencephalogram and electromyogram, the ADS1294. Using a simulator of cardiac signals, 36 different waveforms were recorded, including normal sinus rhythm, arrhythmias and artifacts. Simulations include variations of heart rate from 30 to 190 beats per minute (BPM), with variations in peak amplitude of 1 mV to 2 mV. Tests were performed with a subject at rest and in motion, observing the signals obtained and the damage to their interpretation due to the introduction of muscle movement artifacts in motion situations. PMID:26737850

  2. A portable accelerator control toolkit

    SciTech Connect

    Watson, W.A. III

    1997-06-01

    In recent years, the expense of creating good control software has led to a number of collaborative efforts among laboratories to share this cost. The EPICS collaboration is a particularly successful example of this trend. More recently another collaborative effort has addressed the need for sophisticated high level software, including model driven accelerator controls. This work builds upon the CDEV (Common DEVice) software framework, which provides a generic abstraction of a control system, and maps that abstraction onto a number of site-specific control systems including EPICS, the SLAC control system, CERN/PS and others. In principle, it is now possible to create portable accelerator control applications which have no knowledge of the underlying and site-specific control system. Applications based on CDEV now provide a growing suite of tools for accelerator operations, including general purpose displays, an on-line accelerator model, beamline steering, machine status displays incorporating both hardware and model information (such as beam positions overlaid with beta functions) and more. A survey of CDEV compatible portable applications will be presented, as well as plans for future development.

  3. Portable Health Algorithms Test System

    NASA Technical Reports Server (NTRS)

    Melcher, Kevin J.; Wong, Edmond; Fulton, Christopher E.; Sowers, Thomas S.; Maul, William A.

    2010-01-01

    A document discusses the Portable Health Algorithms Test (PHALT) System, which has been designed as a means for evolving the maturity and credibility of algorithms developed to assess the health of aerospace systems. Comprising an integrated hardware-software environment, the PHALT system allows systems health management algorithms to be developed in a graphical programming environment, to be tested and refined using system simulation or test data playback, and to be evaluated in a real-time hardware-in-the-loop mode with a live test article. The integrated hardware and software development environment provides a seamless transition from algorithm development to real-time implementation. The portability of the hardware makes it quick and easy to transport between test facilities. This hard ware/software architecture is flexible enough to support a variety of diagnostic applications and test hardware, and the GUI-based rapid prototyping capability is sufficient to support development execution, and testing of custom diagnostic algorithms. The PHALT operating system supports execution of diagnostic algorithms under real-time constraints. PHALT can perform real-time capture and playback of test rig data with the ability to augment/ modify the data stream (e.g. inject simulated faults). It performs algorithm testing using a variety of data input sources, including real-time data acquisition, test data playback, and system simulations, and also provides system feedback to evaluate closed-loop diagnostic response and mitigation control.

  4. a Portable Pulsed Neutron Generator

    NASA Astrophysics Data System (ADS)

    Skoulakis, A.; Androulakis, G. C.; Clark, E. L.; Hassan, S. M.; Lee, P.; Chatzakis, J.; Bakarezos, M.; Dimitriou, V.; Petridis, C.; Papadogiannis, N. A.; Tatarakis, M.

    2014-02-01

    The design and construction of a pulsed plasma focus device to be used as a portable neutron source for material analysis such as explosive detection using gamma spectroscopy is presented. The device is capable of operating at a repetitive rate of a few Hz. When deuterium gas is used, up to 105 neutrons per shot are expected to be produced with a temporal pulse width of a few tens of nanoseconds. The pulsed operation of the device and its portable size are its main advantage in comparison with the existing continuous neutron sources. Parts of the device include the electrical charging unit, the capacitor bank, the spark switch (spark gap), the trigger unit and the vacuum-fuel chamber / anode-cathode. Numerical simulations are used for the simulation of the electrical characteristics of the device including the scaling of the capacitor bank energies with total current, the pinch current, and the scaling of neutron yields with energies and currents. The MCNPX code is used to simulate the moderation of the produced neutrons in a simplified geometry and subsequently, the interaction of thermal neutrons with a test target and the corresponding prompt γ-ray generation.

  5. Portable radiation detector and mapping system

    SciTech Connect

    Hofstetter, K.J.; Hayes, D.W.; Eakle, R.F.

    1995-09-01

    A portable radiation detector and mapping system (RADMAPS) has been developed to detect, locate and plot nuclear radiation intensities on commercially available digital maps and other images. The field unit records gamma-ray spectra or neutron signals together with positions from a Global Positioning System (GPS) on flash memory cards. The recorded information is then transferred to a lap-top computer for spectral data analyses and then georegistered graphically on maps, photographs, etc. RADMAPS integrates several existing technologies to produce a preprogrammable field unit uniquely suited for each survey, as required. The system presently records spectra from a Nal(Tl) gamma-ray detector or an enriched Li-6 doped glass neutron scintillator. Standard Geographic Information System software installed in a lap-top, complete with CD-ROM supporting digitally imaged maps, permits the characterization of nuclear material in the field when the presence of such material is not otherwise documented. This paper gives the results of a typical site survey of the Savannah River Site (SRS) using RADMAPS.

  6. The fate of haloacetic acids and trihalomethanes in an aquifer storage and recovery program, Las Vegas, Nevada

    USGS Publications Warehouse

    Thomas, J.M.; McKay, W.A.; Colec, E.; Landmeyer, J.E.; Bradley, P.M.

    2000-01-01

    The fate of disinfection byproducts during aquifer storage and recovery (ASR) is evaluated for aquifers in Southern Nevada. Rapid declines of haloacetic acid (HAA) concentrations during ASR, with associated little change in Cl concentration, indicate that HAAs decline primarily by in situ microbial oxidation. Dilution is only a minor contributor to HAA concentration declines during ASR. Trihalomethane (THM) concentrations generally increased during storage of artificial recharge (AR) water and then declined during recovery. The decline of THM concentrations during recovery was primarily from dilution of current season AR water with residual AR water remaining in the aquifer from previous ASR seasons and native ground water. In more recent ASR seasons, for wells with the longest history of ASR, brominated THMs declined during storage and recovery by processes in addition to dilution. These conclusions about THMs are indicated by THM/Cl values and supported by a comparison of measured and model predicted THM concentrations. Geochemical mixing models were constructed using major-ion chemistry of the three end-member waters to calculate predicted THM concentrations. The decline in brominated THM concentrations in addition to that from dilution may result from biotransformation processes.

  7. Factors associated with sources, transport, and fate of chloroform and three other trihalomethanes in untreated groundwater used for drinking water

    USGS Publications Warehouse

    Carter, Janet M.; Moran, Michael J.; Zogorski, John S.; Price, Curtis V.

    2012-01-01

    Multiple lines of evidence for indicating factors associated with the sources, transport, and fate of chloroform and three other trihalomethanes (THMs) in untreated groundwater were revealed by evaluating low-level analytical results and logistic regression results for THMs. Samples of untreated groundwater from wells used for drinking water were collected from 1996-2007 from 2492 wells across the United States and analyzed for chloroform, bromodichloromethane, dibromochloromethane, and bromoform by a low-level analytical method implemented in April 1996. Using an assessment level of 0.02 μg/L, chloroform was detected in 36.5% of public-well samples and 17.6% of domestic-well samples, with most concentrations less than 1 μg/L. Brominated THMs occurred less frequently than chloroform but more frequently in public-well samples than domestic-well samples. For both public and domestic wells, THMs occurred most frequently in urban areas. Logistic regression analyses showed that the occurrence of THMs was related to nonpoint sources such as urban land use and to point sources like septic systems. The frequent occurrence and concentration distribution pattern of THMs, as well as their frequent co-occurrence with other organic compounds and nitrate, all known to have anthropogenic sources, and the positive associations between THM occurrence and dissolved oxygen and recharge indicate the recycling of water that contains THMs and other anthropogenic contaminants.

  8. Single-step microwave assisted headspace liquid-phase microextraction of trihalomethanes and haloketones in biological samples.

    PubMed

    Alsharaa, Abdulnaser; Basheer, Chanbasha; Sajid, Muhammad

    2015-12-15

    A single-step microwave assisted headspace liquid-phase microextraction (MA-HS-LPME) method was developed for determination of trihalomethanes (THMs) and haloketones (HKs) in biological samples. In this method, a porous membrane envelope was filled with few microliters of extraction solvent and then placed inside the microwave extraction vial. A PTFE ring was designed to support the membrane envelope over a certain height inside the vial. An optimum amount of biological sample was placed in the vial equipped with magnetic stirrer. After that nitric acid was added to the vial for digestion of biological sample. The sample was digested and the volatile THMs and HKs were extracted at headspace in the solvent containing porous membrane. After simultaneous digestion and extraction, the extract was injected to gas chromatography/mass spectrometry for analysis. Factors affecting the extraction efficiency were optimized to achieve higher extraction performance. Quantification was carried out over a concentration range of 0.3-100ngg(-1) for brominated compounds while for the chlorinated ones linear range was between 0.5-100ngg(-1). Limit of detections (LODs) were ranged from 0.051 to 0.110ngg(-1) while limit of quantification (LOQ) were in the range of 0.175-0.351ngg(-1). The relative standard deviations (RSDs) of the calibrations were ranged between 1.1 and 6.8%. The MA-HS-LPME was applied for the determination of trace level THMs and HKs in fish tissue and green alga samples. PMID:26571453

  9. Characteristics and trihalomethane formation reactivity of dissolved organic matter in effluents from membrane bioreactors with and without filamentous bulking.

    PubMed

    Xia, Chufan; Ma, Defang; Gao, Baoyu; Hu, Xinxiao; Yue, Qinyan; Meng, Yingjie; Kang, Shuyu; Zhang, Bei; Qi, Yuanfeng

    2016-07-01

    In this study, synthetic wastewater was treated by two identical membrane bioreactors (MBRs): the normal sludge MBR (NS-MBR) and the bulking sludge MBR (BS-MBR). Effects of filamentous bulking on the characteristics and trihalomethane (THM) formation reactivity of MBR effluent dissolved organic matter (EfOM) were investigated. Filamentous sludge bulking had no significant influence on the regulated MBR effluent water quality except NO2-N and NO3-N. NS-MBR effluent had more low molecular weight (LMW) (<5kDa) EfOM (92.43%) than BS-MBR (75.18%). About two-thirds of EfOM from BS-MBR were hydrophilic substances. On the contrary, EfOM from NS-MBR exhibited higher hydrophobicity. The ratio of polysaccharides and proteins in MBR effluents increased after filamentous bulking. There were more protein-like materials, fulvic acid-like and humic acid-like in BS-MBR EfOM. The THM formation reactivity of BS-MBR EfOM was 30.15% of NS-MBR EfOM, whereas BS-MBR EfOM exhibited higher formation reactivity of bromine containing species. PMID:27017128

  10. Static headspace-gas chromatography-mass spectrometry for the simultaneous determination of trihalomethanes and haloacetic acids in canned vegetables.

    PubMed

    Cardador, Maria Jose; Gallego, Mercedes

    2016-07-01

    Canned vegetables appear to be a possible exposure pathway for hazardous disinfection by-products due to the use of sanitizers and treated water by the canning industry in the preparation of these foods. This work reports on two static headspace-gas chromatography-mass spectrometry methods for the simultaneous determination of 10 trihalomethanes (THMs) and 13 haloacetic acids (HAAs) in both solid and liquid phases of the canned vegetables. Both methods carry out the whole process (including the leaching of target analytes from the vegetable), derivatization of HAAs and volatilization of THMs and HAA esters, in a single step within a static headspace unit. The methods proposed provide an efficient and simple tool for the determination of regulated disinfection by-products in canned vegetables. Average limits of detection for THMs and HAAs were 0.19 and 0.45μg/kg, respectively, in the solid phase of canned vegetables, and 0.05 and 0.09μg/L, respectively, in the liquid phase. Satisfactory recoveries (90-99%) and precision, calculated as relative standard deviations (RSD≤10%), were obtained in both phases of canned vegetables. The methods proposed were applied for the analysis of frequently-used canned vegetables and confirmed the presence of up to 3 THMs and 5 HAAs at microgram per kilogram or liter levels in both phases of the samples. PMID:27268517

  11. A sensitive and fast method for trihalomethanes in urine using gas chromatography-triple quadrupole mass spectrometry.

    PubMed

    Charisiadis, Pantelis; Makris, Konstantinos C

    2014-02-01

    Because of the plethora of exposure sources and routes through which humans are exposed to trihalomethanes (THM), the limitation of their short half-lives could be overcome, if a highly sensitive method was available to quantify urinary THM concentrations at sub-ppb levels. The objective of this study was to develop a fast and reliable method for the determination of the four THM analytes in human urine. A sensitive methodology was developed for THM in urine samples using gas chromatography coupled with triple quadrupole mass spectrometry (GC-QqQ-MS/MS) promoting its use in epidemiological and biomonitoring studies. The proposed methodology enjoys limits of detection similar to those reported in the literature (11-80 ng L(-1)) and the advantages of small initial urine volumes (15 mL) and fast analysis per sample (12 min) when compared with other methods. This is the first report using GC-QqQ-MS/MS for the determination of THM in urine samples. Because of its simplicity and less time-consuming nature, the proposed method could be incorporated into detailed (hundreds of participants' urine samples) exposure assessment protocols providing valuable insight into the dose-response relationship of THM and cancer or pregnancy anomalies. PMID:24370554

  12. Fibre selection based on an overall analytical feature comparison for the solid-phase microextraction of trihalomethanes from drinking water.

    PubMed

    San Juan, Pedro Manuel; Carrillo, José David; Tena, María Teresa

    2007-01-12

    This paper describes the optimization of solid-phase microextraction (SPME) conditions for three different fibres (Carboxen-polydimethylsiloxane (CAR-PDMS), divinylbenzene-Carboxen-polydimethylsiloxane (DVB-CAR-PDMS) and polydimethylsiloxane-divinylbenzene (PDMS-DVB)) used to determine trihalomethanes (THMs) in water by headspace solid-phase microextraction and gas chromatography (HS-SPME-GC). The influence of temperature and salting-out effect was examined using a central composite design for each fibre. Extraction time was studied separately at the optimum values found for temperature and sodium chloride concentration (40 degrees C and 0.36g mL-1). The HS-SPME-GC-MS method for each fibre was characterised in terms of linearity, detection (LOD) and quantification (LOQ) limits and repeatability. The fibre PDMS-DVB was selected as it provided a broader linear range, better repeatability and lower detection and quantification limits than the others, particularly CAR-PDMS fibre. The accuracy of the proposed method using the PDMS-DVB fibre was checked by a recovery study in both ultrapure and tap water. A blank analysis study showed the absence of memory effects for this fibre. The reproducibility (expressed as a percentage of relative standard deviation) was 6-11% and the detection limits were between 0.078 and 0.52microgL-1 for bromoform and chloroform, respectively. Finally, the method was applied to determine THM concentration in two drinking water samples. PMID:17109874

  13. 46 CFR 25.30-10 - Hand-portable fire extinguishers and semi-portable fire-extinguishing systems.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 1 2013-10-01 2013-10-01 false Hand-portable fire extinguishers and semi-portable fire... UNINSPECTED VESSELS REQUIREMENTS Fire Extinguishing Equipment § 25.30-10 Hand-portable fire extinguishers and semi-portable fire-extinguishing systems. (a) Hand portable fire extinguishers and semiportable...

  14. 46 CFR 25.30-10 - Hand-portable fire extinguishers and semi-portable fire-extinguishing systems.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 1 2010-10-01 2010-10-01 false Hand-portable fire extinguishers and semi-portable fire... UNINSPECTED VESSELS REQUIREMENTS Fire Extinguishing Equipment § 25.30-10 Hand-portable fire extinguishers and semi-portable fire-extinguishing systems. (a) Hand portable fire extinguishers and semiportable...

  15. 46 CFR 25.30-10 - Hand-portable fire extinguishers and semi-portable fire-extinguishing systems.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 1 2014-10-01 2014-10-01 false Hand-portable fire extinguishers and semi-portable fire... UNINSPECTED VESSELS REQUIREMENTS Fire Extinguishing Equipment § 25.30-10 Hand-portable fire extinguishers and semi-portable fire-extinguishing systems. (a) Hand portable fire extinguishers and semiportable...

  16. 29 CFR 1917.119 - Portable ladders.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 29 Labor 7 2012-07-01 2012-07-01 false Portable ladders. 1917.119 Section 1917.119 Labor Regulations Relating to Labor (Continued) OCCUPATIONAL SAFETY AND HEALTH ADMINISTRATION, DEPARTMENT OF LABOR (CONTINUED) MARINE TERMINALS Terminal Facilities § 1917.119 Portable ladders. (a) Scope and applicability. This section applies to all...

  17. 29 CFR 1917.119 - Portable ladders.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 29 Labor 7 2013-07-01 2013-07-01 false Portable ladders. 1917.119 Section 1917.119 Labor Regulations Relating to Labor (Continued) OCCUPATIONAL SAFETY AND HEALTH ADMINISTRATION, DEPARTMENT OF LABOR (CONTINUED) MARINE TERMINALS Terminal Facilities § 1917.119 Portable ladders. (a) Scope and applicability. This section applies to all...

  18. Portable Micros: Potentials for Information Management.

    ERIC Educational Resources Information Center

    Davis, Charles H.

    1984-01-01

    Description of portable microcomputers discusses design features of Tandy TRS-80, Nippon Electric Company PC-8200, Epson HX-20, Texas Instruments TI CC 40, and Convergent Technologies' Workslate and provides several caveats and recommendations to those making purchasing decisions. Potential uses for portable microcomputers in education are also…

  19. 46 CFR 129.450 - Portable lighting.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false Portable lighting. 129.450 Section 129.450 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OFFSHORE SUPPLY VESSELS ELECTRICAL INSTALLATIONS Lighting Systems § 129.450 Portable lighting. Each vessel must be equipped with at least...

  20. 46 CFR 129.450 - Portable lighting.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false Portable lighting. 129.450 Section 129.450 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OFFSHORE SUPPLY VESSELS ELECTRICAL INSTALLATIONS Lighting Systems § 129.450 Portable lighting. Each vessel must be equipped with at least...

  1. 46 CFR 129.450 - Portable lighting.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false Portable lighting. 129.450 Section 129.450 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OFFSHORE SUPPLY VESSELS ELECTRICAL INSTALLATIONS Lighting Systems § 129.450 Portable lighting. Each vessel must be equipped with at least...

  2. 46 CFR 129.450 - Portable lighting.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Portable lighting. 129.450 Section 129.450 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OFFSHORE SUPPLY VESSELS ELECTRICAL INSTALLATIONS Lighting Systems § 129.450 Portable lighting. Each vessel must be equipped with at least...

  3. 46 CFR 129.450 - Portable lighting.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Portable lighting. 129.450 Section 129.450 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OFFSHORE SUPPLY VESSELS ELECTRICAL INSTALLATIONS Lighting Systems § 129.450 Portable lighting. Each vessel must be equipped with at least...

  4. 46 CFR 169.567 - Portable extinguishers.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 7 2013-10-01 2013-10-01 false Portable extinguishers. 169.567 Section 169.567 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS SAILING SCHOOL VESSELS Lifesaving and Firefighting Equipment Firefighting Equipment § 169.567 Portable extinguishers. (a)...

  5. 46 CFR 169.567 - Portable extinguishers.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 7 2014-10-01 2014-10-01 false Portable extinguishers. 169.567 Section 169.567 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS SAILING SCHOOL VESSELS Lifesaving and Firefighting Equipment Firefighting Equipment § 169.567 Portable extinguishers. (a)...

  6. 46 CFR 169.567 - Portable extinguishers.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 7 2012-10-01 2012-10-01 false Portable extinguishers. 169.567 Section 169.567 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS SAILING SCHOOL VESSELS Lifesaving and Firefighting Equipment Firefighting Equipment § 169.567 Portable extinguishers. (a)...

  7. 46 CFR 169.567 - Portable extinguishers.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 7 2010-10-01 2010-10-01 false Portable extinguishers. 169.567 Section 169.567 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS SAILING SCHOOL VESSELS Lifesaving and Firefighting Equipment Firefighting Equipment § 169.567 Portable extinguishers. (a)...

  8. 46 CFR 169.567 - Portable extinguishers.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 7 2011-10-01 2011-10-01 false Portable extinguishers. 169.567 Section 169.567 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS SAILING SCHOOL VESSELS Lifesaving and Firefighting Equipment Firefighting Equipment § 169.567 Portable extinguishers. (a)...

  9. The Economics of Educational Software Portability.

    ERIC Educational Resources Information Center

    Oliveira, Joao Batista Araujo e

    1990-01-01

    Discusses economic issues that affect the portability of educational software. Topics discussed include economic reasons for portability, including cost effectiveness; the nature and behavior of educational computer software markets; the role of producers, buyers, and consumers; potential effects of government policies; computer piracy; and…

  10. Do Portable Classrooms Impact Teaching and Learning?

    ERIC Educational Resources Information Center

    Chan, Tak Cheung

    2009-01-01

    Purpose: The purpose of this paper is to examine the possible impact portable classrooms have on the teaching and learning process by exploring current related literature. Design/methodology/approach: This paper takes a synthesis approach, analyzing current studies to assess the impact of portable classrooms on teaching and learning. Findings: No…

  11. 47 CFR 51.203 - Number portability.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 3 2012-10-01 2012-10-01 false Number portability. 51.203 Section 51.203 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) COMMON CARRIER SERVICES (CONTINUED) INTERCONNECTION Obligations of All Local Exchange Carriers § 51.203 Number portability. The rules governing number...

  12. 47 CFR 51.203 - Number portability.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 3 2010-10-01 2010-10-01 false Number portability. 51.203 Section 51.203 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) COMMON CARRIER SERVICES (CONTINUED) INTERCONNECTION Obligations of All Local Exchange Carriers § 51.203 Number portability. The rules governing number...

  13. 47 CFR 51.203 - Number portability.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 3 2013-10-01 2013-10-01 false Number portability. 51.203 Section 51.203 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) COMMON CARRIER SERVICES (CONTINUED) INTERCONNECTION Obligations of All Local Exchange Carriers § 51.203 Number portability. The rules governing number...

  14. 47 CFR 51.203 - Number portability.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 3 2014-10-01 2014-10-01 false Number portability. 51.203 Section 51.203 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) COMMON CARRIER SERVICES (CONTINUED) INTERCONNECTION Obligations of All Local Exchange Carriers § 51.203 Number portability. The rules governing number...

  15. 47 CFR 51.203 - Number portability.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 3 2011-10-01 2011-10-01 false Number portability. 51.203 Section 51.203 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) COMMON CARRIER SERVICES (CONTINUED) INTERCONNECTION Obligations of All Local Exchange Carriers § 51.203 Number portability. The rules governing number...

  16. Precise time dissemination via portable atomic clocks

    NASA Technical Reports Server (NTRS)

    Putkovich, K.

    1982-01-01

    The most precise operational method of time dissemination over long distances presently available to the Precise Time and Time Interval (PTTI) community of users is by means of portable atomic clocks. The Global Positioning System (GPS), the latest system showing promise of replacing portable clocks for global PTTI dissemination, was evaluated. Although GPS has the technical capability of providing superior world-wide dissemination, the question of present cost and future accessibility may require a continued reliance on portable clocks for a number of years. For these reasons a study of portable clock operations as they are carried out today was made. The portable clock system that was utilized by the U.S. Naval Observatory (NAVOBSY) in the global synchronization of clocks over the past 17 years is described and the concepts on which it is based are explained. Some of its capabilities and limitations are also discussed.

  17. Satellite sound broadcasting system, portable reception

    NASA Technical Reports Server (NTRS)

    Golshan, Nasser; Vaisnys, Arvydas

    1990-01-01

    Studies are underway at JPL in the emerging area of Satellite Sound Broadcast Service (SSBS) for direct reception by low cost portable, semi portable, mobile and fixed radio receivers. This paper addresses the portable reception of digital broadcasting of monophonic audio with source material band limited to 5 KHz (source audio comparable to commercial AM broadcasting). The proposed system provides transmission robustness, uniformity of performance over the coverage area and excellent frequency reuse. Propagation problems associated with indoor portable reception are considered in detail and innovative antenna concepts are suggested to mitigate these problems. It is shown that, with the marriage of proper technologies a single medium power satellite can provide substantial direct satellite audio broadcast capability to CONUS in UHF or L Bands, for high quality portable indoor reception by low cost radio receivers.

  18. An XML portable chart format.

    PubMed Central

    Chueh, H. C.; Raila, W. F.; Berkowicz, D. A.; Barnett, G. O.

    1998-01-01

    The clinical chart remains the fundamental record of outpatient clinical care. As this information migrates to electronic form, there is an opportunity to create standard formats for transmitting these charts. This paper describes work toward a Portable Chart Format (PCF) that can represent the relevant aspects of an outpatient chart. The main goal of the format is to provide a packaging medium for outpatient clinical charts in a transfer of care scenario. A secondary goal is to support the aggregation of comparable clinical data for outcomes analysis. The syntax used for PCF is Extended Markup Language (XML), a W3C standard. The structure of the PCF is based on a clinically relevant view of the data. The data definitions and nomenclature used are based primarily on existing clinical standards. PMID:9929315

  19. Evaluation of portable gas chromatographs

    SciTech Connect

    Berkley, R.E.; Miller, M.; Chang, J.C.; Oliver, K.; Fortune, C.

    1993-01-01

    Limits of detection, linearity of responses, and stability of response factors and retention times for five commercially-available portable gas chromatographs (PGC) were determined during laboratory evaluation. The PGCs were also operated at the French Limited Superfund site near Houston, TX during startup of bioremediation. Concentrations of volatile organic compounds (VOC) at the site were slightly above ambient background levels. Concurrent collocated grab samples were collected periodically in canisters and analyzed by Method TO-14 using a mass-selective detector. Canister data were taken to indicate correct concentrations and were used to assess the accuracy of PGC data. Durability, reliability, and complexity of operation of PGCs were also evaluated. The principal goal of the study was to determine the best way to use each instrument as a monitor for airborne VOCs.

  20. RTOS kernel in portable electrocardiograph

    NASA Astrophysics Data System (ADS)

    Centeno, C. A.; Voos, J. A.; Riva, G. G.; Zerbini, C.; Gonzalez, E. A.

    2011-12-01

    This paper presents the use of a Real Time Operating System (RTOS) on a portable electrocardiograph based on a microcontroller platform. All medical device digital functions are performed by the microcontroller. The electrocardiograph CPU is based on the 18F4550 microcontroller, in which an uCOS-II RTOS can be embedded. The decision associated with the kernel use is based on its benefits, the license for educational use and its intrinsic time control and peripherals management. The feasibility of its use on the electrocardiograph is evaluated based on the minimum memory requirements due to the kernel structure. The kernel's own tools were used for time estimation and evaluation of resources used by each process. After this feasibility analysis, the migration from cyclic code to a structure based on separate processes or tasks able to synchronize events is used; resulting in an electrocardiograph running on one Central Processing Unit (CPU) based on RTOS.

  1. A Portable Diode Array Spectrophotometer.

    PubMed

    Stephenson, David

    2016-05-01

    A cheap portable visible light spectrometer is presented. The spectrometer uses readily sourced items and could be constructed by anyone with a knowledge of electronics. The spectrometer covers the wavelength range 450-725 nm with a resolution better than 5 nm. The spectrometer uses a diffraction grating to separate wavelengths, which are detected using a 128-element diode array, the output of which is analyzed using a microprocessor. The spectrum is displayed on a small liquid crystal display screen and can be saved to a micro SD card for later analysis. Battery life (2 × AAA) is estimated to be 200 hours. The overall dimensions of the unit are 120 × 65 × 60 mm, and it weighs about 200 g. PMID:27036399

  2. Portable convertible blast effects shield

    DOEpatents

    Pastrnak, John W.; Hollaway, Rocky; Henning, Carl D.; Deteresa, Steve; Grundler, Walter; Hagler, Lisle B.; Kokko, Edwin; Switzer, Vernon A

    2007-05-22

    A rapidly deployable portable convertible blast effects shield/ballistic shield includes a set two or more telescoping cylindrical rings operably connected to each other to convert between a telescopically-collapsed configuration for storage and transport, and a telescopically-extended upright configuration forming an expanded inner volume. In a first embodiment, the upright configuration provides blast effects shielding, such as against blast pressures, shrapnel, and/or fire balls. And in a second embodiment, the upright configuration provides ballistic shielding, such as against incoming weapons fire, shrapnel, etc. Each ring has a high-strength material construction, such as a composite fiber and matrix material, capable of substantially inhibiting blast effects and impinging projectiles from passing through the shield. And the set of rings are releasably securable to each other in the telescopically-extended upright configuration, such as by click locks.

  3. Portable convertible blast effects shield

    DOEpatents

    Pastrnak, John W.; Hollaway, Rocky; Henning, Carl D.; Deteresa, Steve; Grundler, Walter; Hagler, Lisle B.; Kokko, Edwin; Switzer, Vernon A.

    2011-03-15

    A rapidly deployable portable convertible blast effects shield/ballistic shield includes a set two or more frusto-conically-tapered telescoping rings operably connected to each other to convert between a telescopically-collapsed configuration for storage and transport, and a telescopically-extended upright configuration forming an expanded inner volume. In a first embodiment, the upright configuration provides blast effects shielding, such as against blast pressures, shrapnel, and/or fire balls. And in a second embodiment, the upright configuration provides ballistic shielding, such as against incoming weapons fire, shrapnel, etc. Each ring has a high-strength material construction, such as a composite fiber and matrix material, capable of substantially inhibiting blast effects and impinging projectiles from passing through the shield. And the set of rings are releasably securable to each other in the telescopically-extended upright configuration by the friction fit of adjacent pairs of frusto-conically-tapered rings to each other.

  4. Portable convertible blast effects shield

    DOEpatents

    Pastrnak, John W.; Hollaway, Rocky; Henning, Carl D.; Deteresa, Steve; Grundler, Walter; Hagler,; Lisle B.; Kokko, Edwin; Switzer, Vernon A

    2010-10-26

    A rapidly deployable portable convertible blast effects shield/ballistic shield includes a set two or more telescoping cylindrical rings operably connected to each other to convert between a telescopically-collapsed configuration for storage and transport, and a telescopically-extended upright configuration forming an expanded inner volume. In a first embodiment, the upright configuration provides blast effects shielding, such as against blast pressures, shrapnel, and/or fire balls. And in a second embodiment, the upright configuration provides ballistic shielding, such as against incoming weapons fire, shrapnel, etc. Each ring has a high-strength material construction, such as a composite fiber and matrix material, capable of substantially inhibiting blast effects and impinging projectiles from passing through the shield. And the set of rings are releasably securable to each other in the telescopically-extended upright configuration, such as by click locks.

  5. Portable Handheld Optical Window Inspection Device

    NASA Technical Reports Server (NTRS)

    Ihlefeld, Curtis; Dokos, Adam; Burns, Bradley

    2010-01-01

    The Portable Handheld Optical Window Inspection Device (PHOWID) is a measurement system for imaging small defects (scratches, pits, micrometeor impacts, and the like) in the field. Designed primarily for window inspection, PHOWID attaches to a smooth surface with suction cups, and raster scans a small area with an optical pen in order to provide a three-dimensional image of the defect. PHOWID consists of a graphical user interface, motor control subsystem, scanning head, and interface electronics, as well as an integrated camera and user display that allows a user to locate minute defects before scanning. Noise levels are on the order of 60 in. (1.5 m). PHOWID allows field measurement of defects that are usually done in the lab. It is small, light, and attaches directly to the test article in any orientation up to vertical. An operator can scan a defect and get useful engineering data in a matter of minutes. There is no need to make a mold impression for later lab analysis.

  6. United States Coast Guard portable salvage computer. Final report

    SciTech Connect

    Allen, S.J.

    1986-07-01

    The US Coast Guard's interest in marine salvage arises from its responsibility under the Federal Water Pollution Control Act and other laws dealing with oil spills. At vessel stranding situations, which could result in significant environmental damage through the release of oil or hazardous chemicals, the Coast Guard is represented by an On-Scene Coordinator (OSC), who must evaluate whether or not appropriate salvage techniques are applied to the stranded vessel by commercial salvors. To assist the OSC, who may not be trained in marine salvage, and other Coast Guard personnel assigned to such salvage operations, a portable salvage computer has been programmed to accomplish salvage calculations in a user-friendly manner. In this final report, the development of the salvage program and selection of a portable computer are described along with results of field testing with actual stranding situations.

  7. Occupational Exposure to Trichloramine and Trihalomethanes in Swedish Indoor Swimming Pools: Evaluation of Personal and Stationary Monitoring

    PubMed Central

    Westerlund, Jessica; Graff, Pål; Bryngelsson, Ing-Liss; Westberg, Håkan; Eriksson, Kåre; Löfstedt, Håkan

    2015-01-01

    Introduction: Chlorination is a method commonly used to keep indoor swimming pool water free from pathogens. However, chlorination of swimming pools produces several potentially hazardous by-products as the chlorine reacts with nitrogen containing organic matter. Up till now, exposure assessments in indoor swimming pools have relied on stationary measurements at the poolside, used as a proxy for personal exposure. However, measurements at fixed locations are known to differ from personal exposure. Methods: Eight public swimming pool facilities in four Swedish cities were included in this survey. Personal and stationary sampling was performed during day or evening shift. Samplers were placed at different fixed positions around the pool facilities, at ~1.5 m above the floor level and 0–1 m from the poolside. In total, 52 personal and 110 stationary samples of trichloramine and 51 personal and 109 stationary samples of trihalomethanes, were collected. Results: The average concentration of trichloramine for personal sampling was 71 µg m−3, ranging from 1 to 240 µg m−3 and for stationary samples 179 µg m−3, ranging from 1 to 640 µg m−3. The air concentrations of chloroform were well below the occupational exposure limit (OEL). For the linear regression analysis and prediction of personal exposure to trichloramine from stationary sampling, only data from personal that spent >50% of their workday in the pool area were included. The linear regression analysis showed a correlation coefficient (r 2) of 0.693 and a significant regression coefficient β of 0.621; (95% CI = 0.329–0.912, P = 0.001). Conclusion: The trichloramine exposure levels determined in this study were well below the recommended air concentration level of 500 µg m−3; a WHO reference value based on stationary sampling. Our regression data suggest a relation between personal exposure and area sampling of 1:2, implying an OEL of 250 µg m−3 based on personal sampling. PMID:26155991

  8. Exposure to Trihalomethanes through Different Water Uses and Birth Weight, Small for Gestational Age, and Preterm Delivery in Spain

    PubMed Central

    Gracia-Lavedán, Esther; Ibarluzea, Jesús; Santa Marina, Loreto; Ballester, Ferran; Llop, Sabrina; Tardón, Adonina; Fernández, Mariana F.; Freire, Carmen; Goñi, Fernando; Basagaña, Xavier; Kogevinas, Manolis; Grimalt, Joan O.; Sunyer, Jordi

    2011-01-01

    Background: Evidence associating exposure to water disinfection by-products with reduced birth weight and altered duration of gestation remains inconclusive. Objective: We assessed exposure to trihalomethanes (THMs) during pregnancy through different water uses and evaluated the association with birth weight, small for gestational age (SGA), low birth weight (LBW), and preterm delivery. Methods: Mother–child cohorts set up in five Spanish areas during the years 2000–2008 contributed data on water ingestion, showering, bathing, and swimming in pools. We ascertained residential THM levels during pregnancy periods through ad hoc sampling campaigns (828 measurements) and regulatory data (264 measurements), which were modeled and combined with personal water use and uptake factors to estimate personal uptake. We defined outcomes following standard definitions and included 2,158 newborns in the analysis. Results: Median residential THM ranged from 5.9 μg/L (Valencia) to 114.7 μg/L (Sabadell), and speciation differed across areas. We estimated that 89% of residential chloroform and 96% of brominated THM uptakes were from showering/bathing. The estimated change of birth weight for a 10% increase in residential uptake was –0.45 g (95% confidence interval: –1.36, 0.45 g) for chloroform and 0.16 g (–1.38, 1.70 g) for brominated THMs. Overall, THMs were not associated with SGA, LBW, or preterm delivery. Conclusions: Despite the high THM levels in some areas and the extensive exposure assessment, results suggest that residential THM exposure during pregnancy driven by inhalation and dermal contact routes is not associated with birth weight, SGA, LBW, or preterm delivery in Spain. PMID:21810554

  9. Influence of tap water quality and household water use activities on indoor air and internal dose levels of trihalomethanes.

    PubMed

    Nuckols, John R; Ashley, David L; Lyu, Christopher; Gordon, Sydney M; Hinckley, Alison F; Singer, Philip

    2005-07-01

    Individual exposure to trihalomethanes (THMs) in tap water can occur through ingestion, inhalation, or dermal exposure. Studies indicate that activities associated with inhaled or dermal exposure routes result in a greater increase in blood THM concentration than does ingestion. We measured blood and exhaled air concentrations of THM as biomarkers of exposure to participants conducting 14 common household water use activities, including ingestion of hot and cold tap water beverages, showering, clothes washing, hand washing, bathing, dish washing, and indirect shower exposure. We conducted our study at a single residence in each of two water utility service areas, one with relatively high and the other low total THM in the residence tap water. To maintain a consistent exposure environment for seven participants, we controlled water use activities, exposure time, air exchange, water flow and temperature, and nonstudy THM sources to the indoor air. We collected reference samples for water supply and air (pre-water use activity), as well as tap water and ambient air samples. We collected blood samples before and after each activity and exhaled breath samples at baseline and post-activity. All hot water use activities yielded a 2-fold increase in blood or breath THM concentrations for at least one individual. The greatest observed increase in blood and exhaled breath THM concentration in any participant was due to showering (direct and indirect), bathing, and hand dishwashing. Average increase in blood THM concentration ranged from 57 to 358 pg/mL due to these activities. More research is needed to determine whether acute and frequent exposures to THM at these concentrations have public health implications. Further research is also needed in designing epidemiologic studies that minimize data collection burden yet maximize accuracy in classification of dermal and inhalation THM exposure during hot water use activities. PMID:16002374

  10. Multi-route trihalomethane exposure in households using municipal tap water treated with chlorine or ozone-chlorine.

    PubMed

    Jo, Wan-Kuen; Kwon, Ki-Dong; Dong, Jong-In; Chung, Yong

    2005-03-01

    In Korea, data for multi-route trihalomethane (THM) exposure in households using municipal tap water treated with ozone-chlorine or chlorine are unavailable or very limited. Accordingly, the present study was designed to obtain those data by measurements of the THM concentrations in the tap water and indoor and outdoor air in the two types of households, along with an estimation of THM exposure from water ingestion, showering, and the inhalation of indoor air. Chloroform was the most abundant THM in all three media, yet no bromoform was detected in any sample. Similar to previous findings, the winter chloroform concentration in tap water treated with chlorine (22.1 microg/l, median) was significantly higher than that in the tap water treated with ozone-chlorine (16.8 microg/l, median). However, the summer water chloroform concentrations and summer and winter water concentrations of the other two THMs (bromodichloromethane and dibromochloromethane) exhibited no significant difference between the chlorine and ozone-chlorine-treated water. It was suggested that the effects of the water parameters including biochemical oxygen demand of raw water entering water treatment plants should be considered when evaluating the advantage of ozone-chlorine disinfection for THM formation over chlorine disinfection. The indoor air THM concentration trend was also consistent with the water concentration trend. The indoor to outdoor air concentration ratios were comparable with previous studies. The THM exposure estimates from water ingestion, showering, and the inhalation of apartment indoor air when not in the shower suggested that, for residents living in the surveyed households, their exposure to THMs in the home was mostly associated with their household water uses. The THM exposure estimates from tap water ingestion were similar to those from showering. PMID:15740765

  11. The influence of physicochemical properties on the internal dose of trihalomethanes in humans following a controlled showering exposure.

    PubMed

    Silva, Lalith K; Backer, Lorraine C; Ashley, David L; Gordon, Sydney M; Brinkman, Marielle C; Nuckols, John R; Wilkes, Charles R; Blount, Benjamin C

    2013-01-01

    Although disinfection of domestic water supply is crucial for protecting public health from waterborne diseases, this process forms potentially harmful by-products, such as trihalomethanes (THMs). We evaluated the influence of physicochemical properties of four THMs (chloroform, bromodichloromethane, dibromochloromethane, and bromoform) on the internal dose after showering. One hundred volunteers showered for 10 min in a controlled setting with fixed water flow, air flow, and temperature. We measured THMs in shower water, shower air, bathroom air, and blood samples collected at various time intervals. The geometric mean (GM) for total THM concentration in shower water was 96.2 μg/l. The GM of total THM in air increased from 5.8 μg/m(3) pre shower to 351 μg/m(3) during showering. Similarly, the GM of total-blood THM concentration increased from 16.5 ng/l pre shower to 299 ng/l at 10 min post shower. THM levels were significantly correlated between different matrices (e.g. dibromochloromethane levels) in water and air (r=0.941); blood and water (r=0.845); and blood and air (r=0.831). The slopes of best-fit lines for THM levels in water vs air and blood vs air increased with increasing partition coefficient of water/air and blood/air. The slope of the correlation plot of THM levels in water vs air decreased in a linear (r=0.995) fashion with increasing Henry's law constant. The physicochemical properties (volatility, partition coefficients, and Henry's law constant) are useful parameters for predicting THM movement between matrices and understanding THM exposure during showering. PMID:22829048

  12. Joint effects of trihalomethanes and trichloroacetic acid on semen quality: A population-based cross-sectional study in China.

    PubMed

    Zeng, Qiang; Zhou, Bin; He, Dong-Liang; Wang, Yi-Xin; Wang, Mu; Yang, Pan; Huang, Zhen; Li, Jin; Lu, Wen-Qing

    2016-05-01

    Exposure to trihalomethanes (THMs) and haloacetic acids (HAAs) has been individually associated with adverse male reproductive effects; however, their joint male reproductive toxicity is largely unknown. This study aimed to explore the joint effects of THMs and trichloroacetic acid (TCAA) on semen quality in a Chinese population. A total of 337 men presenting to the Reproductive Center of Tongjing Hospital, in Wuhan, China to seek semen analysis were included this study. Baseline blood THMs [chloroform (TCM), bromodichloromethane (BDCM), dibromochloromethane (DBCM), and bromoform (TBM)] and urinary TCAA were analyzed and dichotomized at their median levels. The joint effects of THMs and TCAA on below-reference semen quality parameters were evaluated by calculating the relative excess risk due to interaction (RERI). After adjusting for potential confounders, we found a suggestive synergistic effect between Br-THMs (sum of BDCM, DBCM, and TBM) and TCAA for below-reference sperm count (RERI = 2.14, 95% CI: -0.37, 4.91) (P = 0.076); men with high Br-THMs and TCAA levels (above the median) had 3.31 times (95% CI: 1.21, 9.07) elevated risk of having below-reference sperm count than men with low Br-THMs and TCAA levels (below the median). No apparent joint effects were observed between THMs and TCAA for other semen quality parameters. Our results suggest that co-exposure to Br-THMs and TCAA is associated with additive effects on decreased semen quality. However, further studies in a larger sample size and mechanistic studies are needed to confirm the findings. PMID:26975004

  13. Trihalomethane, haloacetonitrile, and chloral hydrate formation potentials of organic carbon fractions from sub-tropical forest soils.

    PubMed

    Zhang, Qian; Kuang, Wan-fang; Liu, Lu-ying; Li, Kexin; Wong, Kin-hang; Chow, Alex T; Wong, Po-keung

    2009-12-30

    Forest landscapes represent the major land-cover type for the watersheds of the East River, which is the source of water for 40 million people in South China. Forest soils with high levels of organic carbon are a potential terrestrial source of dissolved organic carbon (DOC) into the East River. DOC is of great concern, since it can form carcinogenic disinfection byproducts (DBPs) during drinking water treatment. In this study, soils from three altitudes (200, 450 and 900 m) in the Xiangtou Mountain Nature Reserve in South China, representing soils from evergreen moon forest, transitional evergreen broadleaf forest, and evergreen broadleaf forest, respectively, were evaluated for their potential contributions of DBP precursors into the East River. The water extractable organic carbon (WEOC) in three forest soils was physically and chemically fractionated into particulate organic carbon (1.2-0.45 microm), colloidal organic carbon (0.45-0.22 microm), and dissolved organic carbon (DOC) (<0.22 microm), hydrophobic acid (HPOA), transphilic acid and hydrophilic acid and were analysed for the formation potentials of trihalomethanes (THMs), haloacetonitriles (HANs), and chloral hydrate (CHD). Also, soils were incubated at 15, 25 and 35 degrees C for 14d in darkness to examine the impact of temperature effects on the availability and characteristics of WEOC. The extraction study showed that the amount of WEOC was proportional to soil organic carbon content, of which about 1% was water extractable. Regardless of soil type, DOC and HPOA were the most reactive fractions in forming THMs, CHD, and HANs. Production of DOC and HPOA in WEOC increased over 14 d incubation as incubation temperature increased, but the temperature did not alter the distribution of physical and chemical fractions and their reactivity in DBP formation. Results suggest higher inputs of DOC and DBP precursors from forest watersheds into source water may result in a warmer environment. PMID:19695772

  14. Seasonal and spatial evolution of trihalomethanes in a drinking water distribution system according to the treatment process.

    PubMed

    Domínguez-Tello, A; Arias-Borrego, A; García-Barrera, Tamara; Gómez-Ariza, J L

    2015-11-01

    This paper comparatively shows the influence of four water treatment processes on the formation of trihalomethanes (THMs) in a water distribution system. The study was performed from February 2005 to January 2012 with analytical data of 600 samples taken in Aljaraque water treatment plant (WTP) and 16 locations along the water distribution system (WDS) in the region of Andévalo and the coast of Huelva (southwest Spain), a region with significant seasonal and population changes. The comparison of results in the four different processes studied indicated a clear link of the treatment process with the formation of THM along the WDS. The most effective treatment process is preozonation and activated carbon filtration (P3), which is also the most stable under summer temperatures. Experiments also show low levels of THMs with the conventional process of preoxidation with potassium permanganate (P4), delaying the chlorination to the end of the WTP; however, this simple and economical treatment process is less effective and less stable than P3. In this study, strong seasonal variations were obtained (increase of THM from winter to summer of 1.17 to 1.85 times) and a strong spatial variation (1.1 to 1.7 times from WTP to end points of WDS) which largely depends on the treatment process applied. There was also a strong correlation between THM levels and water temperature, contact time and pH. On the other hand, it was found that THM formation is not proportional to the applied chlorine dose in the treatment process, but there is a direct relationship with the accumulated dose of chlorine. Finally, predictive models based on multiple linear regressions are proposed for each treatment process. PMID:26431706

  15. DNA methylation levels and long-term trihalomethane exposure in drinking water: an epigenome-wide association study

    PubMed Central

    Salas, Lucas A; Bustamante, Mariona; Gonzalez, Juan R; Gracia-Lavedan, Esther; Moreno, Victor; Kogevinas, Manolis; Villanueva, Cristina M

    2015-01-01

    Trihalomethanes (THM) are undesired disinfection byproducts (DBPs) formed during water treatment. Mice exposed to DBPs showed global DNA hypomethylation and c-myc and c-jun gene-specific hypomethylation, while evidence of epigenetic effects in humans is scarce. We explored the association between lifetime THM exposure and DNA methylation through an epigenome-wide association study. We selected 138 population-based controls from a case-control study of colorectal cancer conducted in Barcelona, Spain, exposed to average lifetime THM levels ≤85 μg/L vs. >85 μg/L (N = 68 and N = 70, respectively). Mean age of participants was 70 years, and 54% were male. Average lifetime THM level in the exposure groups was 64 and 130 µg/L, respectively. DNA was extracted from whole blood and was bisulphite converted to measure DNA methylation levels using the Illumina HumanMethylation450 BeadChip. Data preprocessing was performed using RnBeads. Methylation was compared between exposure groups using empirical Bayes moderated linear regression for CpG sites and Gaussian kernel for CpG regions. ConsensusPathDB was used for gene set enrichment. Statistically significant differences in methylation between exposure groups was found in 140 CpG sites and 30 gene-related regions, after false discovery rate <0.05 and adjustment for age, sex, methylation first principal component, and blood cell proportion. The annotated genes were localized to several cancer pathways. Among them, 29 CpGs had methylation levels associated with THM levels (|Δβ|≥0.05) located in 11 genes associated with cancer in other studies. Our results suggest that THM exposure may affect DNA methylation in genes related to tumors, including colorectal and bladder cancers. Future confirmation studies are required. PMID:26039576

  16. Portable instrument for inspecting irradiated nuclear fuel assemblies

    DOEpatents

    Nicholson, Nicholas; Dowdy, Edward J.; Holt, David M.; Stump, Jr., Charles J.

    1985-01-01

    A portable instrument for measuring induced Cerenkov radiation associated with irradiated nuclear fuel assemblies in a water-filled storage pond is disclosed. The instrument includes a photomultiplier tube and an image intensifier which are operable in parallel and simultaneously by means of a field lens assembly and an associated beam splitter. The image intensifier permits an operator to aim and focus the apparatus on a submerged fuel assembly. Once the instrument is aimed and focused, an illumination reading can be obtained with the photomultiplier tube. The instrument includes a lens cap with a carbon-14/phosphor light source for calibrating the apparatus in the field.

  17. Evaluating Performance Portability of OpenACC

    SciTech Connect

    Sabne, Amit J; Sakdhnagool, Putt; Lee, Seyong; Vetter, Jeffrey S

    2015-01-01

    Accelerator-based heterogeneous computing is gaining momentum in High Performance Computing arena. However, the increased complexity of the accelerator architectures demands more generic, high-level programming models. OpenACC is one such attempt to tackle the problem. While the abstraction endowed by OpenACC offers productivity, it raises questions on its portability. This paper evaluates the performance portability obtained by OpenACC on twelve OpenACC programs on NVIDIA CUDA, AMD GCN, and Intel MIC architectures. We study the effects of various compiler optimizations and OpenACC program settings on these architectures to provide insights into the achieved performance portability.

  18. Characterizing solar mirror materials using portable reflectometers

    SciTech Connect

    Pettit, R.B.

    1982-09-01

    Currently available portable instrumentation for hemispherical and specular reflectance measurements of solar mirror materials is discussed. Particular attention is given to the wavelength dependence of the measurement spectrum, which in most cases does not approximate a solar spectral distribution, and to other limitations of each instrument. Because a portable instrument is not available that can determine the solar averaged specular reflectance from a single measurement, two procedures are recommended for obtaining a reasonable estimate for this quantity using the existing portable equipment. Finally, future developments in this area are briefly discussed.

  19. A Portable, High Resolution, Surface Measurement Device

    NASA Technical Reports Server (NTRS)

    Ihlefeld, Curtis M.; Burns, Bradley M.; Youngquist, Robert C.

    2012-01-01

    A high resolution, portable, surface measurement device has been demonstrated to provide micron-resolution topographical plots. This device was specifically developed to allow in-situ measurements of defects on the Space Shuttle Orbiter windows, but is versatile enough to be used on a wide variety of surfaces. This paper discusses the choice of an optical sensor and then the decisions required to convert a lab bench optical measurement device into an ergonomic portable system. The necessary trade-offs between performance and portability are presented along with a description of the device developed to measure Orbiter window defects.

  20. Portable Unit for Metabolic Analysis

    NASA Technical Reports Server (NTRS)

    Dietrich, Daniel L.; Pitch, Nancy D.; Lewis, Mark E.; Juergens, Jeffrey R.; Lichter, Michael J.; Stuk, Peter M.; Diedrick, Dale M.; Valentine, Russell W.; Pettegrew, Richard D.

    2007-01-01

    The Portable Unit for Metabolic Analysis (PUMA) is an instrument that measures several quantities indicative of human metabolic function. Specifically, this instrument makes time-resolved measurements of temperature, pressure, flow, and the partial pressures of oxygen and carbon dioxide in breath during both inhalation and exhalation. Portable instruments for measuring these quantities have been commercially available, but the response times of those instruments are too long to enable temporal resolution of phenomena on the time scales of human respiration cycles. In contrast, the response time of the PUMA is significantly shorter than characteristic times of human respiration phenomena, making it possible to analyze varying metabolic parameters, not only on sequential breath cycles but also at successive phases of inhalation and exhalation within the same breath cycle. In operation, the PUMA is positioned to sample breath near the subject s mouth. Commercial off-the-shelf sensors are used for three of the measurements: a miniature pressure transducer for pressure, a thermistor for temperature, and an ultrasonic sensor for flow. Sensors developed at Glenn Research Center are used for measuring the partial pressures of oxygen and carbon dioxide: The carbon dioxide sensor exploits the relatively strong absorption of infrared light by carbon dioxide. Light from an infrared source passes through the stream of inhaled or exhaled gas and is focused on an infrared- sensitive photodetector. The oxygen sensor exploits the effect of oxygen in quenching the fluorescence of ruthenium-doped organic molecules in a dye on the tip of an optical fiber. A blue laser diode is used to excite the fluorescence, and the optical fiber carries the fluorescent light to a photodiode, the temporal variation of the output of which bears a known relationship with the rate of quenching of fluorescence and, hence, with the partial pressure of oxygen. The outputs of the sensors are digitized

  1. Whip antenna design for portable rf systems

    NASA Astrophysics Data System (ADS)

    Ponnapalli, Saila; Canora, Frank J.

    1995-12-01

    Whip type antennas are probably the most commonly used antennas in portable rf systems, such as cordless and cellular phones, rf enabled laptop computers, personal digital assistants (PDAs), and handheld computers. Whip antennas are almost always mounted on the chassis which contains the radio and other electronics. The chassis is usually a molded plastic which is coated with a conducting paint for EMI purposes. The chassis which appears as a lossy conductor to the antenna, has several effects -- detuning, altering the gain of the antenna, and shadowing its radiation pattern. Extensive modeling and measurements must be performed in order to fully characterize the affects of the chassis on the whip antenna, and to optimize antenna type, orientation and position. In many instances, modeling plays a more important role in prediction of the performance of whip antennas, since measurements become difficult due to the presence of common mode current on feed cables. In this paper models and measurements are used to discuss the optimum choice of whip antennas and the impact of the chassis on radiation characteristics. A modeling tool which has been previously described and has been successfully used to predict radiated field patterns is used for simulations, and measured and modeled results are shown.

  2. Thermophotovoltaic and thermoelectric portable power generators

    NASA Astrophysics Data System (ADS)

    Chan, Walker R.; Waits, Christopher M.; Joannopoulos, John D.; Celanovic, Ivan

    2014-06-01

    The quest for developing clean, quiet, and portable high energy density, and ultra-compact power sources continues. Although batteries offer a well known solution, limits on the chemistry developed to date constrain the energy density to 0.2 kWh/kg, whereas many hydrocarbon fuels have energy densities closer to 13 kWh/kg. The fundamental challenge remains: how efficiently and robustly can these widely available chemical fuels be converted into electricity in a millimeter to centimeter scale systems? Here we explore two promising technologies for high energy density power generators: thermophotovoltaics (TPV) and thermoelectrics (TE). These heat to electricity conversion processes are appealing because they are fully static leading to quiet and robust operation, allow for multifuel operation due to the ease of generating heat, and offer high power densities. We will present some previous work done in the TPV and TE fields. In addition we will outline the common technological barriers facing both approaches, as well as outline the main differences. Performance for state of the art research generators will be compared as well as projections for future practically achievable systems. A viable TPV or TE power source for a ten watt for one week mission can be built from a <10% efficient device which is achievable with current state of the art technology such as photonic crystals or advanced TE materials.

  3. Medipix2/USB Portable Radiation Camera

    SciTech Connect

    Vykydal, Z.; Holy, T.; Jakubek, J.; Platkevic, M.; Pospisil, S.

    2007-11-26

    Advances in the field of semiconductor technologies in the last years make possible to develop new types of ionizing radiation detectors. The Medipix2 readout ASIC is an example of such a device. It is the hybrid single photon counting imaging chip (sensor and readout chips are fabricated separately). With an appropriate sensor chip on the top, it can count single X-ray photons, without any noise or dark current, at high fluxes (several Gigaphotons per cm{sup 2} per second). It also offers excellent radiation hardness and good position resolution (256x256 pixels, each pixel has a 55x55 {mu}m{sup 2} area). To make the Medipix2 imaging chip more portable for specific applications a microprocessor controlled read-out system based on the USB (Universal Serial Bus) interface has been developed. It integrates all necessary detector support into one compact device (75x46 mm{sup 2}). All power supplies including sensor bias (up to 100 V) are internally derived from the voltage provided by the USB connection.

  4. Development of portable fuel cells

    SciTech Connect

    Nakatou, K.; Sumi, S.; Nishizawa, N.

    1996-12-31

    Sanyo Electric has been concentrating on developing a marketable portable fuel cell using phosphoric acid fuel cells (PAFC). Due to the fact that this power source uses PAFC that operate at low temperature around 100{degrees} C, they are easier to handle compared to conventional fuel cells that operate at around 200{degrees} C , they can also be expected to provide extended reliable operation because corrosion of the electrode material and deterioration of the electrode catalyst are almost completely nonexistent. This power source is meant to be used independently and stored at room temperature. When it is started up, it generates electricity itself using its internal load to raise the temperature. As a result, the phosphoric acid (the electolyte) absorbs the reaction water when the temperature starts to be raised (around room temperature). At the same time the concentration and volume of the phosphoric acid changes, which may adversely affect the life time of the cell. We have studied means for starting, operating PAFC stack using methods that can simply evaluate changes in the concentration of the electrolyte in the stack with the aim of improving and extending cell life and report on them in this paper.

  5. Portable Microleak-Detection System

    NASA Technical Reports Server (NTRS)

    Rivers, H. Kevin; Sikora, Joseph G.; Sankaran, Sankara N.

    2007-01-01

    The figure schematically depicts a portable microleak-detection system that has been built especially for use in testing hydrogen tanks made of polymer-matrix composite materials. (As used here, microleak signifies a leak that is too small to be detectable by the simple soap-bubble technique.) The system can also be used to test for microleaks in tanks that are made of other materials and that contain gases other than hydrogen. Results of calibration tests have shown that measurement errors are less than 10 percent for leak rates ranging from 0.3 to 200 cm3/min. Like some other microleak-detection systems, this system includes a vacuum pump and associated plumbing for sampling the leaking gas, and a mass spectrometer for analyzing the molecular constituents of the gas. The system includes a flexible vacuum chamber that can be attached to the outer surface of a tank or other object of interest that is to be tested for leakage (hereafter denoted, simply, the test object). The gas used in a test can be the gas or vapor (e.g., hydrogen in the original application) to be contained by the test object. Alternatively, following common practice in leak testing, helium can be used as a test gas. In either case, the mass spectrometer can be used to verify that the gas measured by the system is the test gas rather than a different gas and, hence, that the leak is indeed from the test object.

  6. Portable system to luminaries characterization

    NASA Astrophysics Data System (ADS)

    Tecpoyotl-Torres, M.; Vera-Dimas, J. G.; Koshevaya, S.; Escobedo-Alatorre, J.; Cisneros-Villalobos, L.; Sanchez-Mondragon, J.

    2014-09-01

    For illumination sources designers is important to know the illumination distribution of their products. They can use several viewers of IES files (standard file format determined by Illuminating Engineering Society). This files are necessary not only know the distribution of illumination, but also to plain the construction of buildings by means of specialized softwares, such as Autodesk Revit. In this paper, a complete portable system for luminaries' characterization is given. The components of the systems are: Irradiance profile meter, which can generate photometry of luminaries of small sizes which covers indoor illumination requirements and luminaries for general areas. One of the meteŕs attributes is given by the color sensor implemented, which allows knowing the color temperature of luminary under analysis. The Graphic Unit Interface (GUI) has several characteristics: It can control the meter, acquires the data obtained by the sensor and graphs them in 2D under Cartesian and polar formats or 3D, in Cartesian format. The graph can be exported to png, jpg, or bmp formats, if necessary. These remarkable characteristics differentiate this GUI. This proposal can be considered as a viable option for enterprises of illumination design and manufacturing, due to the relatively low investment level and considering the complete illumination characterization provided.

  7. Portable engine-pump assembly

    SciTech Connect

    Eberhardt, H.A.

    1987-02-17

    This patent describes a portable engine-pump assembly that is compact and light in weight comprising: an internal combustion engine mounted with its crankshaft extending vertically, a centrifugal pump having an impeller mounted for rotation on a pump shaft within a volute chamber, means mounting the pump on and immediately beneath the engine with the pump shaft extending vertically in accurate alignment and concentricity with the engine crankshaft, means coupling the engine crankshaft and the pump shaft together so that the engine crankshaft drives the pump shaft, the pump comprising a pump body defining the volute chamber and providing a pump inlet passage and a pump discharge passage oriented in generally horizontal directions, the pump body defining an inlet chamber providing passages for the flow of liquid from the pump inlet passage into the impeller from both above and below same and including an upper body portion and a lower body portion, and an exhaust system for the engine including an exhaust passage contained in the upper body portion, a muffler having an inlet, and means providing flow communication between the exhaust passage and the inlet of the muffler.

  8. Portable walking beam pump jack

    SciTech Connect

    Laney, R.N.

    1986-02-25

    This patent describes a portable walking beam pump jack for use in pumping liquids from an oil well. This jack consists of: an elongated frame having a longitudinal axis and front and rear ends, the frame also including first and second support seats; a towing receptacle, an axle connected transversely across the frame; ground engaging wheels connected to the axle for supporting the frame for rolling transportation; stabilizing means for securing the frame with respect to a ground location; a walking beam having a first end, a midportion and a second end, the second end being adapted for connection to a pumping rod; an engine mounted on the frame; a pair of arms counterweighted for balancing a pumping rod connected to the walking beam, a drive yoke, a support assembly foldably mounted on the frame and upon which the midportion of the walking beam is pivotally connected, the support assembly the arms and the drive yoke being foldable together, from a first, fixed position in which the walking beam arms and yoke are supported in a raised position for rocking in a pumping motion to a second, fixed position disposed downwardly and forwardly from the first fixed position and in which the walking beam arms and yoke are held in a lowered position for transportation; a front support and a hydraulic cylinder connected between the frame and the support assembly for moving the support assembly between the first, fixed position and the second fixed position.

  9. High intensity portable fluorescent light

    NASA Technical Reports Server (NTRS)

    Kendall, F. B.

    1972-01-01

    Eight high intensity portable fluorescent lights were produced. Three prototype lights were also produced, two of which were subsequently updated to the physical and operational configuration of the qualification and flight units. Positioning of lamp apertures and reflectors in these lights is such that the light is concentrated and intensified in a specific pattern rather than widely diffused. Indium amalgam control of mercury vapor pressure in the lamp gives high output at lamp ambient temperatures up to 105 C. A small amount of amalgam applied to each electrode stem helps to obtain fast warm-up. Shrinking a Teflon sleeve on the tube and potting metal caps on each end of the lamp minimizes dispersion of mercury vapor and glass particles in the event of accidental lamp breakage. Operation at 20 kHz allows the lamps to consume more power than at low frequency, thus increasing their light output and raising their efficiency. When used to expose color photographic film, light from the lamps produces results approximately equal to sunlight.

  10. Portable basketball rim testing device

    SciTech Connect

    Abbott, W. Bruce; Davis, Karl C.

    1993-01-01

    A portable basketball rim rebound testing device 10 is illustrated in two preferred embodiments for testing the rebound or energy absorption characteristics of a basketball rim 12 and its accompanying support to determine likely rebound or energy absorption charcteristics of the system. The apparatus 10 includes a depending frame 28 having a C-clamp 36 for releasably rigidly connecting the frame to the basketball rim 12. A glide weight 60 is mounted on a guide rod 52 permitting the weight 60 to be dropped against a calibrated spring 56 held on an abutment surface on the rod to generate for deflecting the basketball rim and then rebounding the weight upwardly. A photosensor 66 is mounted on the depending frame 28 to sense passage of reflective surfaces 75 on the weight to thereby obtain sufficient data to enable a processing means 26 to calculate the rebound velocity and relate it to an energy absorption percentage rate of the rim system 12. A readout is provided to display the energy absorption percentage.

  11. CARTOGAM: a portable gamma camera

    NASA Astrophysics Data System (ADS)

    Gal, O.; Izac, C.; Lainé, F.; Nguyen, A.

    1997-02-01

    The gamma camera is devised to establish the cartography of radioactive sources against a visible background in quasi real time. This device is designed to spot sources from a distance during the preparation of interventions on active areas of nuclear installations. This implement will permit to optimize interventions especially on the dosimetric level. The camera consists of a double cone collimator, a scintillator and an intensified CCD camera. This chain of detection provides the formation of both gamma images and visible images. Even though it is wrapped in a denal shield, the camera is still portable (mass < 15 kg) and compact (external diameter = 8 cm). The angular resolution is of the order of one degree for gamma rays of 1 MeV. In a few minutes, the device is able to measure a dose rate of 10 μGy/h delivered for instance by a source of 60Co of 90 mCi located at 10 m from the detector. The first images recorded in the laboratory will be presented and will illustrate the performances obtained with this camera.

  12. Portable or Modular? There Is a Difference....

    ERIC Educational Resources Information Center

    Morton, Mike

    2002-01-01

    Describes differences between two types of school facilities: portable (prebuilt, temporary wood structure installed on site) and modular (method of construction for permanent buildings). Provides details of modular construction. (PKP)

  13. Portable Zika Test Shows Promise in Monkeys

    MedlinePlus

    ... nih.gov/medlineplus/news/fullstory_158704.html Portable Zika Test Shows Promise in Monkeys Easy-to-use ... News) -- A fast, inexpensive test that detects the Zika virus in monkeys might be useful for doctors ...

  14. Portable breathing apparatus for coal mines

    NASA Technical Reports Server (NTRS)

    Vandolah, R. W.

    1972-01-01

    The state of the art in portable oxygen breathing equipment is reported. Considered are self-containing as well as chemically generating oxygen sources and their effectiveness and limitations in mine rescue operations.

  15. The Portable War Room Research Project

    NASA Technical Reports Server (NTRS)

    Govers, Francis X., III; Fry, Mark

    1997-01-01

    The Portable War Room is an internal TASC project to research and develop a visualization and simulation environment to provide for decision makers the power to review the past, understand the present, and peer into the future.

  16. Portable Zika Test Shows Promise in Monkeys

    MedlinePlus

    ... https://medlineplus.gov/news/fullstory_158704.html Portable Zika Test Shows Promise in Monkeys Easy-to-use ... News) -- A fast, inexpensive test that detects the Zika virus in monkeys might be useful for doctors ...

  17. A Machine-Portable CDC UPDATE Emulator.

    Energy Science and Technology Software Center (ESTSC)

    1987-09-01

    Version 01 UPEML is a machine-portable CDC UPDATE emulation program. It is capable of emulating a significant subset of the standard CDC UPDATE functions, including program library creation and subsequent modification.

  18. 46 CFR 196.37-47 - Portable magazine chests.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 7 2014-10-01 2014-10-01 false Portable magazine chests. 196.37-47 Section 196.37-47... Markings for Fire and Emergency Equipment, etc. § 196.37-47 Portable magazine chests. (a) Portable magazine chests shall be marked in letters at least 3 inches high: PORTABLE MAGAZINE CHEST — FLAMMABLE —...

  19. 46 CFR 108.651 - Portable magazine chests.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false Portable magazine chests. 108.651 Section 108.651... AND EQUIPMENT Equipment Markings and Instructions § 108.651 Portable magazine chests. Each portable magazine chest must be marked: “PORTABLE MAGAZINE CHEST—FLAMMABLE—KEEP LIGHTS AND FIRE AWAY” in letters...

  20. 46 CFR 196.37-47 - Portable magazine chests.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 7 2013-10-01 2013-10-01 false Portable magazine chests. 196.37-47 Section 196.37-47... Markings for Fire and Emergency Equipment, etc. § 196.37-47 Portable magazine chests. (a) Portable magazine chests shall be marked in letters at least 3 inches high: PORTABLE MAGAZINE CHEST — FLAMMABLE —...