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Sample records for resonant third-integer extraction

  1. Tracking Simulation of Third-Integer Resonant Extraction for Fermilab's Mu2e Experiment

    SciTech Connect

    Park, Chong Shik; Amundson, James; Michelotti, Leo

    2015-02-13

    The Mu2e experiment at Fermilab requires acceleration and transport of intense proton beams in order to deliver stable, uniform particle spills to the production target. To meet the experimental requirement, particles will be extracted slowly from the Delivery Ring to the external beamline. Using Synergia2, we have performed multi-particle tracking simulations of third-integer resonant extraction in the Delivery Ring, including space charge effects, physical beamline elements, and apertures. A piecewise linear ramp profile of tune quadrupoles was used to maintain a constant averaged spill rate throughout extraction. To study and minimize beam losses, we implemented and introduced a number of features, beamline element apertures, and septum plane alignments. Additionally, the RF Knockout (RFKO) technique, which excites particles transversely, is employed for spill regulation. Combined with a feedback system, it assists in fine-tuning spill uniformity. Simulation studies were carried out to optimize the RFKO feedback scheme, which will be helpful in designing the final spill regulation system.

  2. AGS RESONANT EXTRACTION WITH HIGH INTENSITY BEAMS.

    SciTech Connect

    AHRENS,L.; BROWN,K.; GLENN,J.W.; ROSER,T.; TSOUPAS,N.; VANASSELT,W.

    1999-03-29

    The Brookhaven AGS third integer resonant extraction system allows the AGS to provide high quality, high intensity 25.5 GeV/c proton beams simultaneously to four target stations and as many as 8 experiments. With the increasing intensities (over 7 x 10{sup 13} protons/pulse) and associated longer spill periods (2.4 to 3 seconds long), we continue to run with low losses and high quality low modulation continuous current beams.[1] Learning to extract and transport these higher intensity beams has required a process of careful modeling and experimentation. We have had to learn how to correct for various instabilities and how to better match extraction and the transport lines to the higher emittance beams being accelerated in the AGS. Techniques employed include ''RF'' methods to smooth out momentum distributions and fine structure. We will present results of detailed multi-particle tracking modeling studies which enabled us to develop a clear understanding of beam loss mechanisms in the transport and extraction process. We will report on our status, experiences, and the present understanding of the intensity limitations imposed by resonant extraction and transport to fixed target stations.

  3. Third interger resonance slow extraction schemem for a mu->e experiment at Fermilab

    SciTech Connect

    Nagaslaev, V.; Amundson, J.; Johnstone, J.; Michelotti, L.; Park, C.S.; Werkema, S.; Syphers, M.; /Michigan State U.

    2010-09-01

    The current design of beam preparation for a proposed mu->e conversion experiment at Fermilab is based on slow resonant extraction of protons from the Debuncher. The Debuncher ring will have to operate with beam intensities of 3 x 10{sup 12} particles, approximately four orders of magnitude larger than its current value. The most challenging requirements on the beam quality are the spill uniformity and low losses in the presence of large space charge and momentum spread. We present results from simulations of third integer resonance extraction assisted by RF knock-out (RFKO), a technique developed for medical accelerators. Tune spreads up to 0.05 have been considered.

  4. DESIGN OF A RESONANT EXTRACTION SYSTEM FOR THE AGS BOOSTER.

    SciTech Connect

    BROWN,K.; CULLEN,J.; GLENN,J.W.; LEE,Y.Y.; MCNERNEY,A.; NIEDERER,J.; ROSER,T,; SOUKAS,A.; TUOZZOLO,J.; TSOUPAS,N.

    1999-03-29

    The Booster Application Facility (BAF) will employ heavy ion beams of many different ion species and at beam energies ranging from 0.04 to 3.07 GeV/nucleon. Resonant extraction is required in order to deliver a continuous stream of particles. In this report we describe the beam requirements and the system design. The basic design is a third integer resonant extraction process which employs a single thin magnetic septum and a thick septum ejector magnet The expected extraction efficiency is about 85%, based on the thin septum thickness and the predicted step size of the resonant beam at the septum. This is more than sufficient for the low intensity low energy heavy ion beams needed for the BAF. In this report we will present a detailed discussion of the design of the various elements and a discussion of the detailed modeling of resonant extraction from the AGS Booster. The extraction process was modeled using a BNL version of MAD which allowed us to interactively observe detailed particle tracking of the process. This was a key tool to have in hand which permitted us to pose and answer various questions in a very short period of time.

  5. Preliminaries toward studying resonant extraction from the Debuncher

    SciTech Connect

    Michelotti, Leo; Johnstone, John; /Fermilab

    2009-06-01

    A recent proposal to detect {mu} {yields} e direct conversion at Fermilab asks for slow extraction of protons from the antiproton source, specifically from the Debuncher. [1] A third-integer resonance originally was considered for this, partly because of the Debuncher's three-fold symmetry and partly because its operational horizontal tune, {nu}{sub x} {approx} 9.765, is already within 0.1 of {nu}{sub x} = 29/3. Using a half integer resonance, {nu}{sub x} = 19/2, though not part of the original proposal, has been suggested more recently because (a) Fermilab has had a good deal of experience with half-integer extraction from the Tevatron, the Main Injector and the erstwhile Main Ring, and (b) for reasons we shall examine later, it depopulates the entire bunch without an abort at the end. This memo presents considerations preliminary to studying both possibilities. It is meant only as a starting point for investigations to be carried out in the future. The working constraints and assumptions have oscillated between two extremes: (1) making minimal changes in the antiproton source to minimize cost and (2) building another machine in the same tunnel. In this memo we adopt an attitude aligned more toward the first. The assumed parameters are listed in Table 1. A few are not (easily) subject to change, such as those related to the beam's momentum and revolution frequency and the acceptance of the debuncher. Two resonance exemplars are presented in the next section, with an explanation of the analytic and semi-analytic calculations that can be done for each. Section 3 contains preliminary numerical work that was done to validate the exemplars within the context of extraction from the Debuncher. A final section contains a summary. Following the bibliography, appendices contain (a) a qualitative, conceptual discussion of extraction for the novice, (b) a telegraphic review of the perturbative incantations used to filter the exemplars as principal resonances of quadrupole

  6. Space charge effect of the high intensity proton beam during the resonance extraction for the Mu2e experiment at Fermilab

    SciTech Connect

    Park, Chong Shik; Amundson, James; Johnstone, John; Michelotti, Leo; Nagaslaev, Vladimir; Werkema, Steve; /Fermilab

    2011-03-01

    The proposed Mu2e experiment to search for direct {mu} {yields} e conversion at Fermilab plans slow, resonant extraction of a beam with 3 x 10{sup 12} protons from the Debuncher ring. Space charge of this high intensity beam is a critical factor, since it induces significant betatron tune spread and consequently affects resonance extraction processes, such as spill uniformity and beam losses. This study shows the multi-particle simulation results in the early stages of resonance extraction and spill uniformity in the presence of 2D and 3D space charge effects. We have presented the results of the third-integer resonance extraction in early stage for the Mu2e experiment in the presence of space charge effects. In order to track particles and to calculate self-consistent space charge effects, Synergia2 was used, which is capable of parallel computing. The space charge tune shift was computed and was reasonable value compared with the analytical calculation. Locations of the septum and Lambertson were chosen so that particles are kicked and extracted efficiently. The spill rates for with and without space charge effects were uniform, but should be improved for the early stage after the sextupole field ramping.

  7. Resonance extraction from the SAID analysis

    NASA Astrophysics Data System (ADS)

    Workman, Ron; Švarc, Alfred

    2016-05-01

    Resonances are extracted from a number of energy-dependent and single-energy fits to scattering data. The influence of recent, precise EPECUR data is investigated. Results for the single-energy fits are derived using the Laurent+Pietarinen (L+P) method of analysis and are compared to those obtained using contour integration applied to the global energy-dependent fits.

  8. From Extraction of Nucleon Resonances to LQCD

    NASA Astrophysics Data System (ADS)

    Lee, T.-S. H.; Wu, Jia-jun; Kamano, Hiroyuki

    2016-06-01

    The intrinsic difficulties in extracting the hadron resonances from reaction data are illustrated by using several exactly soluble π π scattering models. The finite-volume Hamiltonian method is applied to predict spectra using two meson-exchange Hamiltonians of π N reactions. Within a three-channel model with π N , π {Δ} and σ N channels, we show the advantage of the finite-volume Hamiltonian method over the approach using the Lüscher formula to test Lattice QCD calculations aimed at predicting nucleon resonances. We discuss the necessary steps for using the ANL-Osaka eight-channel Hamiltonian to predict the spectra for testing the LQCD calculations for determining the excited nucleon states up to invariant mass W= 2 GeV.

  9. CONTINUOUS EXTRACTED BEAM IN THE AGS FAST EXTERNAL BEAM LINE.

    SciTech Connect

    GLENN,J.W.; TSOUPAS,N.; BROWN,K.A.; BIRYUKOV,V.M.

    2001-06-18

    A method to split off a few percent of the 6 x 10{sup 13} AGS beam delivered to the Slow External Beam (SEB) lines and send it down the Fast External Beam line (FEB) has been developed. The mission is to feed a counter experiment off the FEB that directly measures the neutrino mass using the muon storage ring. The use of normal thin septum splitters would have an excessive loss overhead and been optically difficult. The AGS Slow Extraction uses a third integer resonance with sextuple strength so the resonance width is a few percent of the beam width. This results in a low density tail which will be clipped by a bent crystal and deflected into the FEB channel. This clipping off of the tail should reduce losses in the SEB transport line. Details of modeled orbits, particle distribution and extraction trajectories into and out off the crystal will be given.

  10. STATUS OF SLOW EXTRACTION OF HIGH INTENSITY PROTONS FROM BROOKHAVEN'S AGS.

    SciTech Connect

    BROWN,K.A.AHRENS,L.BRENNAN,J.M.GLENN,J.W.ROSER,T.RUSSO,T.TSOUPAS,N.SMITH,K.ZENO,K.

    2003-05-12

    The Brookhaven AGS third integer resonant extraction system allows the AGS to provide high quality, high intensity 25.5 GeV/c proton beams simultaneously to four target stations and as many as 8 experiments. With the increasing intensities (over 7 x 10{sup 13} protons/pulse) and associated longer spill periods (2.4 to 3 seconds long), we continue to run with low losses and high quality low modulation continuous current beams. We have an active program of high energy physics experiments, including the high precision measurement of the muons magnetic moment [1] and the discovery of the rare Kaon decay, K+ {yields} {pi} + {nu}{bar {nu}} [2]. This program is continuing into the future with the rare symmetry violating process experiments [3] currently being designed to operate at the AGS. In this paper, we will present results from operation of high intensity slow extraction, the problems we encounter, and our solutions to those problems.

  11. Extraction of resonant component from spin-polarization observables

    NASA Astrophysics Data System (ADS)

    Yamaguchi, Mitsutaka; Tagishi, Y.; Aoki, Y.; Yamato, Y.; Nagatomo, T.; Iizuka, T.; Yoshimaru, N.; Shinba, T.; Katabuchi, T.; Tanifugi, M.

    Recently, some groups studied about 6 Li(d,α) reaction near zero energy for astrophysical inter- ests. The reaction is affected by an 2+ resonant level below the reaction threshold. In this work, we measured the analyzing powers for this reaction at an very low incident energy and extracted 2+ component.

  12. Extracting Neutron Structure Functions in the Resonance Region

    SciTech Connect

    Yonatan Kahn

    2009-07-01

    A new iterative method is presented for extracting neutron structure functions from inclusive structure functions of nuclei, focusing specifically on the resonance region. Unlike earlier approaches, this method is applicable to both spin-averaged and spin-dependent structure functions. We show that in numerical tests, this method is able to reproduce known input functions of nearly arbitrary shape after only 5–10 iterations. We illustrate the method on extractions of F2n and g1,2n from data, and discuss the treatment of systematic errors from this extraction procedure.

  13. Comments on extracting the resonance strength parameter from yield data

    NASA Astrophysics Data System (ADS)

    Croft, Stephen; Favalli, Andrea

    2015-10-01

    The F(α,n) reaction is the focus of on-going research in part because it is an important source of neutrons in the nuclear fuel cycle which can be exploited to assay nuclear materials, especially uranium in the form of UF6 [1,2]. At the present time there remains some considerable uncertainty (of the order of ±20%) in the thick target integrated over angle (α,n) yield from 19F (100% natural abundance) and its compounds as discussed in [3,4]. An important thin target cross-section measurement is that of Wrean and Kavanagh [5] who explore the region from below threshold (2.36 MeV) to approximately 3.1 MeV with fine energy resolution. Integration of their cross-section data over the slowing down history of a stopping α-particle allows the thick target yield to be calculated for incident energies up to 3.1 MeV. This trend can then be combined with data from other sources to obtain a thick target yield curve over the wider range of interest to the fuel cycle (roughly threshold to 10 MeV to include all relevant α-emitters). To estimate the thickness of the CaF2 target they used, Wrean and Kavanagh separately measured the integrated yield of the 6.129 MeV γ-rays from the resonance at 340.5 keV (laboratory α-particle kinetic energy) in the 19F(p,αγ) reaction. To interpret the data they adopted a resonance strength parameter of (22.3±0.8) eV based on a determination by Becker et al [6]. The value and its uncertainty directly affects the thickness estimate and the extracted (α,n) cross-section values. In their citation to Becker et al's work, Wrean and Kavanagh comment that they did not make use of an alternative value of (23.7±1.0) eV reported by Croft [7] because they were unable to reproduce the value from the data given in that paper. The value they calculated for the resonance strength from the thick target yield given by Croft was 21.4 eV. The purpose of this communication is to revisit the paper by Croft published in this journal and specifically to

  14. Resonant slow extraction in synchrotrons using anti-symmetric sextupole fields

    NASA Astrophysics Data System (ADS)

    Zou, Ye; Tang, Jingyu; Yang, Jianquan

    2016-09-01

    This paper proposes a novel method for resonant slow extraction in synchrotrons by using special anti-symmetric sextupole fields, which can be produced by a special magnet structure. The method has potential in applications demanding very stable slow extraction from synchrotrons. Our studies show that slow extraction at the half-integer resonance by using an anti-symmetric sextupole field has some advantages compared to the standard sextupole field, which is widely used in the slow extraction method. One advantage is that it can work at a more distant tune from the resonance, so that it can reduce significantly the intensity variation of the extracted beam which is mainly caused by the ripples of magnet power supplies. Studies by both the Hamiltonian theory and numerical simulations show that the stable region near the half-integer resonance by anti-symmetric sextupole field is much smaller and flatter than the one by standard sextupole field at the third-order resonance. The particles outside the region will be driven out in two possible directions in quite a short transit time but with spiral steps similar to the third-order resonant extraction. By gradually increasing the field strength, the beam can be extracted with intensity more homogeneous than by the usual third-order resonant method, because of both smaller intensity variation and spike in the beginning spill. With the same field strength and tune distance to the resonance, the change in the stable region area due to the working point variation in the case of the anti-symmetric sextupole is about 1/14 of the one for the standard sextupole. Detailed studies including beam dynamic behaviors near other resonances, expression of the field in polynomial expansion, influence of 2-D field error, half-integer stop-band, and resonant slow extraction using a quadrupole field are also presented.

  15. Antioxidant activity of grape skin aqueous extracts from pressurized hot water extraction combined with electron paramagnetic resonance spectroscopy.

    PubMed

    Sťavíková, Lenka; Polovka, Martin; Hohnová, Barbora; Karásek, Pavel; Roth, Michal

    2011-09-30

    Pressurized hot water extraction (PHWE) was employed to prepare extracts from dried grape skin of two wine grape varieties (St. Laurent and Alibernet) at various temperatures (from 40 up to 120°C) and amounts of sample (0.5, 1.0 and 1.5 g). To assess the antioxidant activity of the extracts, electron paramagnetic resonance (EPR) spectroscopy was applied involving DPPH and ABTS(+) assays. Other extract characteristics including HPLC profile of anthocyanins and total phenolic compound content were obtained as well. PHWE has also been compared with earlier results of extractions of the same grape skin samples with compressed methanol and compressed ethanol under the conditions of pressurized fluid extraction (PFE). From this comparison, PHWE emerges as the more benign and efficient extraction method to recover valuable phenolic antioxidants from grape skins for the prospective use in functional food supplements. PMID:21872083

  16. Extraction of Meson Resonances from Three-pions Photo-production Reactions

    SciTech Connect

    S. X. Nakamura, H. Kamano, T.-S. H. Lee, T. Sato

    2012-12-01

    We have investigated the model dependence of meson resonance properties extracted from the Dalitz-plot analysis of the three-pions photoproduction reactions on the nucleon. Within a unitary model developed in Phys. Rev. D 84, 114019 (2011), we generate Dalitz-plot distributions as data to perform an isobar model fit that is similar to most of the previous analyses of three-pion production reactions. It is found that the resonance positions from the two models agree well when both fit the data accurately, except for the resonance poles near branch points. The residues of the resonant amplitudes extracted from the two models and by the usual Breit-Wigner procedure agree well only for the isolated resonances with narrow widths. For overlapping resonances, most of the extracted residues could be drastically different. Our results suggest that even with high precision data, the resonance extraction should be based on models within which the amplitude parametrization is constrained by three-particle unitarity condition.

  17. Extraction of P11 Resonance from pi-N Data and Its Stability

    SciTech Connect

    S. X. Nakamura, H. Kamano, T.-S. H. Lee, T. Sato

    2011-09-01

    An important question about resonance extraction is how much resonance poles and residues extracted from data depend on a model used for the extraction, and on the precision of data. We address this question with the dynamical coupled-channel (DCC) model developed in Excited Baryon Analysis Center (EBAC) at JLab. We focus on the P11 pi-N scattering. We examine the model-dependence of the poles by varying parameters to a large extent within the EBAC-DCC model. We find that two poles associated with the Roper resonance are fairly stable against the variation. We also develop a model with a bare nucleon, thereby examining the stability of the Roper poles against different analytic structure of the P11 amplitude below pi-N threshold. We again find a good stability of the Roper poles.

  18. Radio frequency spectral characterization and model parameters extraction of high Q optical resonators.

    PubMed

    Abdallah, Zeina; Boucher, Yann G; Fernandez, Arnaud; Balac, Stéphane; Llopis, Olivier

    2016-01-01

    A microwave domain characterization approach is proposed to determine the properties of high quality factor optical resonators. This approach features a very high precision in frequency and aims to acquire a full knowledge of the complex transfer function (amplitude and phase) characterizing an optical resonator using a microwave vector network analyzer. It is able to discriminate between the different coupling regimes, from the under-coupling to the selective amplification, and it is used together with a model from which the main resonator parameters are extracted, i.e. coupling factor, intrinsic losses, phase slope, intrinsic and external quality factor. PMID:27251460

  19. Radio frequency spectral characterization and model parameters extraction of high Q optical resonators

    NASA Astrophysics Data System (ADS)

    Abdallah, Zeina; Boucher, Yann G.; Fernandez, Arnaud; Balac, Stéphane; Llopis, Olivier

    2016-06-01

    A microwave domain characterization approach is proposed to determine the properties of high quality factor optical resonators. This approach features a very high precision in frequency and aims to acquire a full knowledge of the complex transfer function (amplitude and phase) characterizing an optical resonator using a microwave vector network analyzer. It is able to discriminate between the different coupling regimes, from the under-coupling to the selective amplification, and it is used together with a model from which the main resonator parameters are extracted, i.e. coupling factor, intrinsic losses, phase slope, intrinsic and external quality factor.

  20. Radio frequency spectral characterization and model parameters extraction of high Q optical resonators

    PubMed Central

    Abdallah, Zeina; Boucher, Yann G.; Fernandez, Arnaud; Balac, Stéphane; Llopis, Olivier

    2016-01-01

    A microwave domain characterization approach is proposed to determine the properties of high quality factor optical resonators. This approach features a very high precision in frequency and aims to acquire a full knowledge of the complex transfer function (amplitude and phase) characterizing an optical resonator using a microwave vector network analyzer. It is able to discriminate between the different coupling regimes, from the under-coupling to the selective amplification, and it is used together with a model from which the main resonator parameters are extracted, i.e. coupling factor, intrinsic losses, phase slope, intrinsic and external quality factor. PMID:27251460

  1. Extraction of Electromagnetic Transition Form Factors for Nucleon Resonances within a Dynamical Coupled-Channels Model

    SciTech Connect

    N. Suzuki, T. Sato, T.-S. H. Lee

    2010-10-01

    We explain the application of a recently developed analytic continuation method to extract the electromagnetic transition form factors for the nucleon resonances ($N^*$) within a dynamical coupled-channel model of meson-baryon reactions.Illustrative results of the obtained $N^*\\rightarrow \\gamma N$ transition form factors, defined at the resonance pole positions on the complex energy plane, for the well isolated $P_{33}$ and $D_{13}$, and the complicated $P_{11}$ resonances are presented. A formula has been developed to give an unified representation of the effects due to the first two $P_{11}$ poles, which are near the $\\pi\\Delta$ threshold, but are on different Riemann sheets. We also find that a simple formula, with its parameters determined in the Laurent expansions of $\\pi N \\rightarrow \\pi N$ and $\\gamma N \\rightarrow\\pi N$ amplitudes, can reproduce to a very large extent the exact solutions of the considered model at energies near the real parts of the extracted resonance positions. We indicate the differences between our results and those extracted from the approaches using the Breit-Wigner parametrization of resonant amplitudes to fit the data.

  2. Development of ion transportation, extraction and neutralization systems for atomic beam resonance method

    NASA Astrophysics Data System (ADS)

    Nagae, Daisuke; Asahi, Koichiro; Miyoshi, Hisanori; Shimada, Kenzi; Yoshimi, Akihiro; Ueno, Hideki; Murata, Jiro; Uchida, Makoto; Kameda, Daisuke; Kato, Go; Emori, Shoken; Kijima, Go; Oshima, Sachiko; Takemura, Makoto; Arai, Takemasa; Kobayashi, Yoshio; Haseyama, Tomohito; Schmidt-Ott, W. D.

    2005-11-01

    A device that produces a low-energy and largely spin polarized RI beam based on the atomic beam resonance method (RIABR) has been developed. We have performed measurements of stopping and drifting an incoming RI ion beam in a gas chamber, extraction of the ions into a vacuum region, and neutralization of the extracted low-energy ion beam. The drift efficiency of RI ions in a gas and the extraction efficiency at a Laval-type glass nozzle were found to be 0.72±0.04 and 0.033, respectively. The result of the experiment for the neutralization is also discussed.

  3. The Need for Polarization for Extracting Baryon Resonances and the NSTAR Program at CLAS

    SciTech Connect

    Cole, Philip L.

    2007-10-26

    We report on the NSTAR program in Hall B of JLab on using polarization observables to extract parameters of baryon resonances. The scientific purpose of the program is to improve the understanding of the underlying quark degrees of freedom, especially in the higher resonance regions, where we expect to uncover many of missing baryon resonances that mainly decay through multi-meson channels. With the high-quality beam of circularly- and linearly-polarized photons onto unpolarized and polarized proton and deteurium targets, and coupled with the nearly complete solid angle coverage of CLAS, we will extract the differential cross sections and associated polarization observables obtained by the photoproduction of vector mesons and kaons at center of mass energies of 1.7 to 2.2 GeV. The paper will primarily present the photon beam aspects of the excited baryon program.

  4. The Need for Polarization for Extracting Baryon Resonances and the NSTAR Program at CLAS

    SciTech Connect

    P.L. Cole

    2007-10-01

    We report on the NSTAR program in Hall B of JLab on using polarization observables to extract parameters of baryon resonances. The scientific purpose of the program is to improve the understanding of the underlying quark degrees of freedom, especially in the higher resonance regions, where we expect to uncover many of missing baryon resonances that mainly decay through multi-meson channels. With the high-quality beam of circularly- and linearly-polarized photons onto unpolarized and polarized proton and deteurium targets, and coupled with the nearly complete solid angle coverage of CLAS, we will extract the differential cross sections and associated polarization observables obtained by the photoproduction of vector mesons and kaons at center of mass energies of 1.7 to 2.2 GeV. The paper will primarily present the photon beam aspects of the excited baryon program.

  5. On the extraction of P11 resonances from πN data

    DOE PAGESBeta

    Hiroyuki Kamano; Nakamura, Satoshi X.; Lee, Tsung -Shung; Sato, Toru

    2010-06-22

    With the accuracy of the available P11 amplitudes of πΔ scattering, we show that two resonance poles near the pi Delta threshold, obtained in several analyses, are stable against large variations of parameters within a dynamical coupled-channels analysis. The number of poles in the 1.5 GeV < W < 2 GeV region could be more than one, depending on how the structure of the single-energy solution of SAID is fitted. Lastly, our results indicate the need of more accurate πN scattering data in the W > 1.6 GeV region for high precision resonance extractions.

  6. Multiaperture ion beam extraction from gas-dynamic electron cyclotron resonance source of multicharged ions

    SciTech Connect

    Sidorov, A.; Dorf, M.; Zorin, V.; Bokhanov, A.; Izotov, I.; Razin, S.; Skalyga, V.; Rossbach, J.; Spaedtke, P.; Balabaev, A.

    2008-02-15

    Electron cyclotron resonance ion source with quasi-gas-dynamic regime of plasma confinement (ReGIS), constructed at the Institute of Applied Physics, Russia, provides opportunities for extracting intense and high-brightness multicharged ion beams. Despite the short plasma lifetime in a magnetic trap of a ReGIS, the degree of multiple ionization may be significantly enhanced by the increase in power and frequency of the applied microwave radiation. The present work is focused on studying the intense beam quality of this source by the pepper-pot method. A single beamlet emittance measured by the pepper-pot method was found to be {approx}70 {pi} mm mrad, and the total extracted beam current obtained at 14 kV extraction voltage was {approx}25 mA. The results of the numerical simulations of ion beam extraction are found to be in good agreement with experimental data.

  7. Extraction of $P_{11}$ Resonance from piN Data and Its Stability

    SciTech Connect

    Satoshi Nakamura

    2011-10-01

    We address a question about how much resonance poles and residues extracted from data depend on a model used for the extraction, and on the precision of data. We focus on the P{sub 11} {pi}-N scattering and use the dynamical coupled-channel (DCC) model developed in Excited Baryon Analysis Center (EBAC) at JLab. We examine the model-dependence of the poles by varying parameters largely within the EBAC-DCC model. We find that two poles associated with the Roper resonance are fairly stable against the variation. We also study the stability of the Roper poles against different analytic structure of the P{sub 11} amplitude below {pi}-N threshold by using a bare nucleon model. We again find a good stability of the Roper poles.

  8. A proposed U.S./China theoretical/experimental collaborative effort on baryon resonance extraction

    SciTech Connect

    P.L. Cole

    2009-12-01

    In this paper we discuss the reasons for our work towards establishing a new collaboration between Jefferson Lab (JLab) and the Institute of High Energy Physics (IHEP) in Beijing. We seek to combine experimentalists and theorists into a dedicated group focused on better understanding the current and future data from JLab and from the Beijing Electron Positron Collider (BEPC). Recent JLab results on the extraction of single- and double-polarization observables in both the 1{pi}- and 2{pi}-channel show their high sensitivity to small production amplitudes and therefore their importance for the extraction of resonance parameters. The Beijing Electron Spectrometer (BES) at the BEPC has collected high statistics data on J/{Psi} production. Its decay into baryon-antibaryon channels offers a unique and complementary way of probing nucleon resonances. The CEBAF Large Acceptance Spectrometer, CLAS, has access to N* form factors at high Q{sup 2}, which is advantageous for the study of dynamical properties of nucleon resonances, while the low-background BES results will be able to provide guidance for the search for less-dominant excited states at JLab. Moreover, with the recently approved experimental proposal Nucleon Resonance Studies with CLAS12 and the high-quality data streaming from BES-III and CLAS, the time has come for forging a new Trans-Pacific collaboration of theorists and experimentalists on NSTAR physics.

  9. Electron cyclotron resonance 140 mA D(+) beam extraction optimization for IFMIF EVEDA accelerator.

    PubMed

    Delferrière, O; De Menezes, D; Gobin, R; Harrault, F; Tuske, O

    2008-02-01

    Based on the experience of the SILHI electron cyclotron resonance (ECR) ion source for the IPHI accelerator, which produces routinely 100-120 mA H(+) beam, the CEA-Saclay is in charge of the design and realization of the 140 mA cw deuteron source for the IFMIF project (International Fusion Materials Irradiation Facility). IFMIF is an accelerator-based neutron irradiation facility consisting of two accelerators of 125 mA D(+) beam at 40 MeV that hit in parallel a lithium target. IFMIF utilizes the deuteron-lithium (d-Li) neutron, producing a reaction to simulate the 14 MeV neutron environment in deuterium-tritium (D-T) fusion reactors. In the framework of the IFMIF EVEDA phase (Engineering Validation and Engineering Design Activities), we are studying a cw ECR ion source with a new extraction system to allow high current extraction while keeping a low divergence as well as a small emittance. Starting from SILHI five-electrode system with H(+) ions, the extracted beam characteristics as well as electric field conditions are compared with the cases of four- and three-electrode extraction systems. Experimental results made on the SILHI source with H(+) ions are briefly discussed. Extensive experimental results on the new source test bench BETSI are expected as soon as the design and fabrication of a dedicated extraction system with a new set of electrodes will be finished. PMID:18315214

  10. An Analysis Method for Superconducting Resonator Parameter Extraction with Complex Baseline Removal

    NASA Technical Reports Server (NTRS)

    Cataldo, Giuseppe

    2014-01-01

    A new semi-empirical model is proposed for extracting the quality (Q) factors of arrays of superconducting microwave kinetic inductance detectors (MKIDs). The determination of the total internal and coupling Q factors enables the computation of the loss in the superconducting transmission lines. The method used allows the simultaneous analysis of multiple interacting discrete resonators with the presence of a complex spectral baseline arising from reflections in the system. The baseline removal allows an unbiased estimate of the device response as measured in a cryogenic instrumentation setting.

  11. Model for the description of ion beam extraction from electron cyclotron resonance ion sources

    SciTech Connect

    Spaedtke, P.

    2010-02-15

    The finite difference method trajectory code KOBRA3-INP has been developed now for 25 years to perform the simulation of ion beam extraction in three dimensions. Meanwhile, the code has been validated for different applications: high current ion beam extraction from plasma sources for ion implantation technology, neutral gas heating in fusion devices, or ion thrusters for space propulsion. One major issue of the development of this code was to improve the flexibility of the applied model for the simulation of different types of particle sources. Fixed emitter sources might be simulated with that code as well as laser ion sources, Penning ion sources, electron cyclotron resonance ion sources (ECRISs), or H{sup -} sources, which require the simulation of negative ions, negative electrons, and positive charges simultaneously. The model which has been developed for ECRIS has now been used to explore the conditions for the ion beam extraction from a still nonexisting ion source, a so called ARC-ECRIS [P. Suominen and F. Wenander, Rev. Sci. Instrum. 79, 02A305 (2008)]. It has to be shown whether the plasma generator has similar properties like regular ECRIS. However, the emittance of the extracted beam seems to be much better compared to an ECRIS equipped with a hexapole.

  12. Dynamical coupled-channels model of K-p reactions. II. Extraction of Λ* and Σ* hyperon resonances

    NASA Astrophysics Data System (ADS)

    Kamano, H.; Nakamura, S. X.; Lee, T.-S. H.; Sato, T.

    2015-08-01

    Resonance parameters (pole masses and residues) associated with the excited states of hyperons, Λ* and Σ*, are extracted within a dynamical coupled-channels model developed recently by us [Phys. Rev. C 90, 065204 (2014)], 10.1103/PhysRevC.90.065204 through a comprehensive partial-wave analysis of the K-p →K ¯N ,π Σ ,π Λ ,η Λ ,K Ξ data up to invariant mass W =2.1 GeV. We confirm the existence of resonances corresponding to most, if not all, of the four-star resonances rated by the Particle Data Group. We also find several new resonances, and in particular propose a possible existence of a new narrow JP=3 /2+ Λ resonance that couples strongly to the η Λ channel. The JP=1 /2- Λ resonances located below the K ¯N threshold are also discussed. Comparing our extracted pole masses with the ones from a recent analysis by the Kent State University group, some significant differences in the extracted resonance parameters are found, suggesting the need of more extensive and accurate data of K-p reactions including polarization observables to eliminate such an analysis dependence of the resonance parameters. In addition, the determined large branching ratios of the decays of high-mass resonances to the π Σ* and K¯*N channels also suggest the importance of the data of 2 →3 reactions such as K-p →π π Λ and K-p →π K ¯N . Experiments on measuring cross sections and polarization observables of these fundamental reactions are highly desirable at hadron beam facilities such as J-PARC for establishing the Λ* and Σ* spectrum.

  13. Natural resonance extraction and annihilation filtering methods for radar target identification

    NASA Astrophysics Data System (ADS)

    Murphy, Timothy J.

    1990-09-01

    This thesis represents an initial attempt to demonstrate aspect independent target identification of complex radar targets using annihilation filters based on the natural resonances of the targets. The Cadzow-Solomon signal processing algorithm is tested to determine its suitability for the task of extracting the poles from complex targets to a degree of accuracy required for successful implementation of an annihilation filtering target identification system. This testing was conducted through the use of noise polluted synthetic data as well as measured transient scattering data from thin-wire and silver coated scale model aircraft targets. The testing revealed that the Cadzow-Solomon algorithm can return pole clusters at false pole locations when processing the scattered returns from complex targets. Properties of annihilation filters which may affect their ability to discriminate complex targets are examined.

  14. Investigations on the structure of the extracted ion beam from an electron cyclotron resonance ion source

    SciTech Connect

    Spaedtke, P.; Lang, R.; Maeder, J.; Rossbach, J.; Tinschert, K.; Maimone, F.

    2012-02-15

    Using improved beam diagnostic tools, the structure of an ion beam extracted from an electron cyclotron resonance ion source (ECRIS) becomes visible. Especially viewing targets to display the beam profile and pepper pot devices for emittance measurements turned out to be very useful. On the contrary, diagnostic tools integrating over one space coordinate like wire harps for profile measurements or slit-slit devices, respectively slit-grid devices to measure the emittance might be applicable for beam transport investigations in a quadrupole channel, but are not very meaningful for investigations regarding the given ECRIS symmetry. Here we try to reproduce the experimentally found structure on the ion beam by simulation. For the simulation, a certain model has to be used to reproduce the experimental results. The model is also described in this paper.

  15. Beam extraction and high stability operation of high current electron cyclotron resonance proton ion source

    SciTech Connect

    Roychowdhury, P. Mishra, L.; Kewlani, H.; Mittal, K. C.; Patil, D. S.

    2014-03-15

    A high current electron cyclotron resonance proton ion source is designed and developed for the low energy high intensity proton accelerator at Bhabha Atomic Research Centre. The plasma discharge in the ion source is stabilized by minimizing the reflected microwave power using four stub auto tuner and magnetic field. The optimization of extraction geometry is performed using PBGUNS code by varying the aperture, shape, accelerating gap, and the potential on the electrodes. While operating the source, it was found that the two layered microwave window (6 mm quartz plate and 2 mm boron nitride plate) was damaged (a fine hole was drilled) by the back-streaming electrons after continuous operation of the source for 3 h at beam current of 20–40 mA. The microwave window was then shifted from the line of sight of the back-streaming electrons and located after the water-cooled H-plane bend. In this configuration the stable operation of the high current ion source for several hours is achieved. The ion beam is extracted from the source by biasing plasma electrode, puller electrode, and ground electrode to +10 to +50 kV, −2 to −4 kV, and 0 kV, respectively. The total ion beam current of 30–40 mA is recorded on Faraday cup at 40 keV of beam energy at 600–1000 W of microwave power, 800–1000 G axial magnetic field and (1.2–3.9) × 10{sup −3} mbar of neutral hydrogen gas pressure in the plasma chamber. The dependence of beam current on extraction voltage, microwave power, and gas pressure is investigated in the range of operation of the ion source.

  16. Cerebral Glioma Grading Using Bayesian Network with Features Extracted from Multiple Modalities of Magnetic Resonance Imaging

    PubMed Central

    Wang, Huiting; Liu, Renyuan; Zhang, Xin; Li, Ming; Yang, Yongbo; Yan, Jing; Niu, Fengnan; Tian, Chuanshuai; Wang, Kun; Yu, Haiping; Chen, Weibo; Wan, Suiren; Sun, Yu; Zhang, Bing

    2016-01-01

    Many modalities of magnetic resonance imaging (MRI) have been confirmed to be of great diagnostic value in glioma grading. Contrast enhanced T1-weighted imaging allows the recognition of blood-brain barrier breakdown. Perfusion weighted imaging and MR spectroscopic imaging enable the quantitative measurement of perfusion parameters and metabolic alterations respectively. These modalities can potentially improve the grading process in glioma if combined properly. In this study, Bayesian Network, which is a powerful and flexible method for probabilistic analysis under uncertainty, is used to combine features extracted from contrast enhanced T1-weighted imaging, perfusion weighted imaging and MR spectroscopic imaging. The networks were constructed using K2 algorithm along with manual determination and distribution parameters learned using maximum likelihood estimation. The grading performance was evaluated in a leave-one-out analysis, achieving an overall grading accuracy of 92.86% and an area under the curve of 0.9577 in the receiver operating characteristic analysis given all available features observed in the total 56 patients. Results and discussions show that Bayesian Network is promising in combining features from multiple modalities of MRI for improved grading performance. PMID:27077923

  17. Resonance Raman Spectroscopy of Single-Wall Carbon Nanotubes Separated via Aqueous Two-Phase Extraction

    NASA Astrophysics Data System (ADS)

    Simpson, J. R.; Fagan, J. A.; Hight Walker, A. R.

    2014-03-01

    We report Resonance Raman Spectroscopy (RRS) measurements of single-wall carbon nanotube (SWCNT) samples dispersed in aqueous solutions via surfactant wrapping and separated using aqueous two-phase extraction (ATPE) into chirality-enriched semiconducting and metallic SWCNT species. ATPE provides a rapid, robust, and remarkably tunable separation technique that allows isolation of high-purity, individual SWCNT chiralities via modification of the surfactant environment. We report RRS measurements of individual SWCNT species of various chiral index including, armchair and zigzag metals. Raman provides a powerful technique to quantify the metallic SWCNTs in ATPE fractions separated for metallicity. We measure Raman spectra over a wide range of excitation wavelengths from 457 nm to 850 nm using a series of discrete and continuously tunable laser sources coupled to a triple-grating spectrometer with a liquid-nitrogen-cooled detector. The spectra reveal Raman-active vibrational modes, including the low-frequency radial breathing mode (RBM) and higher-order modes. SWCNT chiral vectors are determined from the Raman spectra, specifically the RBM frequencies and corresponding energy excitation profiles, together with input from theoretical models.

  18. Resonance Raman Spectroscopy of Single-Wall Carbon Nanotubes Separated via Aqueous Two-Phase Extraction

    NASA Astrophysics Data System (ADS)

    Simpson, J. R.; Fagan, J. A.; Hight Walker, A. R.

    2015-03-01

    We report resonance Raman Spectroscopy measurements of single-wall carbon nanotube (SWCNT) samples dispersed in aqueous solutions via surfactant wrapping and separated using aqueous two-phase extraction (ATPE) into chirality-enriched semiconducting and metallic SWCNT species. ATPE provides a rapid, robust, and remarkably tunable separation technique that allows isolation of high-purity, individual SWCNT chiralities via modification of the surfactant environment. We report RRS measurements of individual SWCNT species of various chiral index including, semiconductors, armchair and zigzag metals. Raman provides a powerful technique to quantify the metallic SWCNTs in ATPE fractions separated for metallicity. We measure Raman spectra over a wide range of excitation wavelengths from (457 to 850) nm using a series of discrete and continuously tunable laser sources coupled to a triple-grating spectrometer. The spectra reveal Raman-active vibrational modes, including the low-frequency radial breathing mode (RBM) and higher-order modes. SWCNT chiral vectors are determined from Raman spectra, specifically the RBM frequencies and corresponding energy excitation profiles, together with input from theoretical models.

  19. Studies of the beam extraction system of the GTS-LHC electron cyclotron resonance ion source at CERN.

    PubMed

    Toivanen, V; Küchler, D

    2016-02-01

    The 14.5 GHz GTS-LHC Electron Cyclotron Resonance Ion Source (ECRIS) provides multiply charged heavy ion beams for the CERN experimental program. The GTS-LHC beam formation has been studied extensively with lead, argon, and xenon beams with varied beam extraction conditions using the ion optical code IBSimu. The simulation model predicts self-consistently the formation of triangular and hollow beam structures which are often associated with ECRIS ion beams, as well as beam loss patterns which match the observed beam induced markings in the extraction region. These studies provide a better understanding of the properties of the extracted beams and a way to diagnose the extraction system performance and limitations, which is otherwise challenging due to the lack of direct diagnostics in this region and the limited availability of the ion source for development work. PMID:26932095

  20. Studies of the beam extraction system of the GTS-LHC electron cyclotron resonance ion source at CERN

    NASA Astrophysics Data System (ADS)

    Toivanen, V.; Küchler, D.

    2016-02-01

    The 14.5 GHz GTS-LHC Electron Cyclotron Resonance Ion Source (ECRIS) provides multiply charged heavy ion beams for the CERN experimental program. The GTS-LHC beam formation has been studied extensively with lead, argon, and xenon beams with varied beam extraction conditions using the ion optical code IBSimu. The simulation model predicts self-consistently the formation of triangular and hollow beam structures which are often associated with ECRIS ion beams, as well as beam loss patterns which match the observed beam induced markings in the extraction region. These studies provide a better understanding of the properties of the extracted beams and a way to diagnose the extraction system performance and limitations, which is otherwise challenging due to the lack of direct diagnostics in this region and the limited availability of the ion source for development work.

  1. Resonance

    NASA Astrophysics Data System (ADS)

    Perozzi, E.; Murdin, P.

    2000-11-01

    A resonance in CELESTIAL MECHANICS occurs when some of the quantities characterizing the motion of two or more celestial bodies can be considered as commensurable, i.e. their ratio is close to an integer fraction. In a simplified form, this can be expressed as ...

  2. Molecular characterization of inhibiting biochar water-extractable substances using electrospray ionization fourier transform ion cyclotron resonance mass spectrometry.

    PubMed

    Smith, Cameron R; Sleighter, Rachel L; Hatcher, Patrick G; Lee, James W

    2013-01-01

    Biochar has gained significant interest worldwide for its potential use as both a carbon sequestration technique and soil amendment. Recently, research has shown that pinewood-derived biochar water extracts inhibited the growth of aquatic photosynthetic microorganisms, both prokaryotic and eukaryotic algae, while chicken litter- and peanut shell-derived biochar water extracts showed no growth inhibition. With the use of electrodialysis, the pinewood-derived biochar water extract is separated into 3 fractions (anode-isolated, center chamber retained, and cathode-isolated substances) all with varying toxic effects. Because of its ultrahigh resolution and mass precision, electrospray ionization (ESI) coupled to Fourier transform ion cyclotron resonance mass spectrometry (FTICR-MS) is utilized in this study to analyze biochar water extracts at a molecular level to enhance our understanding of the toxic nature of pinewood-derived biochar water extracts as compared to benign peanut shell-derived biochar water extracts. The molecular composition of pinewood-derived biochar water extracts shows unique carbohydrate ligneous components and sulfur containing condensed ligneous components that are both absent from the peanut shell water extracts and more prevalent in the anode-isolated substances. Using Kendrick mass defect analysis, we also determine that the most likely inhibitor species contain carboxyl and hydroxyl homologous series, both of which are characteristic functional groups hypothesized in our previous research for the inhibitor species. We have suggested that inhibition of aquatic photosynthetic microorganism growth is most likely due to degraded lignin-like species rich in oxygen containing functionalities. From the study conducted here, we show the potential of ultrahigh resolution FTICR-MS as a valuable analytical technique for determining whether certain biochars are safe and benign for use as carbon sequestration and soil amendment. PMID:24180747

  3. Power penalty measurement and frequency chirp extraction in silicon microdisk resonator modulators.

    SciTech Connect

    Lentine, Anthony L.; Zortman, William A.; Trotter, Douglas Chandler; Watts, Michael R.

    2010-03-01

    We demonstrate 5 Gbs and 10 Gbs error free operation of silicon photonic microdisk resonant modulators to a distance of 70 km, measure dispersion power penalties and compare the experimental results with theoretically derived values.

  4. P_11 Resonance Extracted from pi-N Data and Its Stability

    SciTech Connect

    Satoshi Nakamura

    2012-04-01

    We study the stability of resonance poles in {pi}N P{sub 11} partial wave, particularly the Roper resonance, by varying parameters significantly within the EBAC dynamical coupled-channels model, keeping a good fit to the empirical amplitude. We find that two Roper poles are stable against the variation. However, for higher energies, the number of poles can change depending on how the parameters are fitted within error bars. We also developed a model with a bare nucleon which forms the physical nucleon by being dressed by the meson-cloud. We still find a good stability of the Roper poles.

  5. Spatially resolved charge-state and current-density distributions at the extraction of an electron cyclotron resonance ion source

    SciTech Connect

    Panitzsch, Lauri; Peleikis, Thies; Stalder, Michael; Wimmer-Schweingruber, Robert F.

    2011-09-15

    In this paper we present our measurements of charge-state and current-density distributions performed in very close vicinity (15 mm) of the extraction of our hexapole geometry electron cyclotron resonance ion source. We achieved a relatively high spatial resolution reducing the aperture of our 3D-movable extraction (puller) electrode to a diameter of only 0.5 mm. Thus, we are able to limit the source of the extracted ion beam to a very small region of the plasma electrode's hole (O = 4 mm) and therefore to a very small region of the neutral plasma sheath. The information about the charge-state distribution and the current density in the plane of the plasma electrode at each particular position is conserved in the ion beam. We determined the total current density distribution at a fixed coaxial distance of only 15 mm to the plasma electrode by remotely moving the small-aperture puller electrode which contained a dedicated Faraday cup (FC) across the aperture of the plasma electrode. In a second measurement we removed the FC and recorded m/q-spectra for the different positions using a sector magnet. From our results we can deduce that different ion charge-states can be grouped into bloated triangles of different sizes and same orientation at the extraction with the current density peaking at centre. This confirms observations from other groups based on simulations and emittance measurements. We present our measurements in detail and discuss possible systematic errors.

  6. Simultaneous slow resonant extractions from the SPS with horizontal tune-split

    SciTech Connect

    Gyr, M.; Kissler, K.H.; Pahud, J.D.; Peraire, S.

    1985-10-01

    With the upgrading of the West experimental area it became necessary to extract protons at 450 GeV/c simultaneously towards two experimental zones. However, the corresponding extraction systems are at locations which, when the normal periodicity is maintained, would not allow this procedure. During the time of extraction, the horizontal tune has therefore to be split unequally between two halves of the machine circumference such that the betatron phase difference between the electrostatic septa of the two extraction systems becomes a multiple of 2 . The separatrix then being the same at both septa entrances, the sharing ratio can easily be adjusted by changing the radial position of the circulating beam relative to the first septum with a compensated bump.

  7. Poles as the only true resonant-state signals extracted from a worldwide collection of partial-wave amplitudes using only one, well controlled pole-extraction method

    SciTech Connect

    Hadzimehmedovic, M.; Osmanovic, H.; Stahov, J.; Ceci, S.; Svarc, A.

    2011-09-15

    Each and every energy-dependent partial-wave analysis is parametrizing the pole positions in a procedure defined by the way the continuous energy dependence is implemented. These pole positions are, henceforth, inherently model dependent. To reduce this model dependence, we use only one, coupled-channel, unitary, fully analytic method based on the isobar approximation to extract the pole positions from each available member of the worldwide collection of partial-wave amplitudes, which are understood as nothing more but a good energy-dependent representation of genuine experimental numbers assembled in a form of partial-wave data. In that way, the model dependence related to the different assumptions on the analytic form of the partial-wave amplitudes is avoided, and the true confidence limit for the existence of a particular resonant state, at least in one model, is established. The way the method works and first results are demonstrated for the S{sub 11} partial wave.

  8. Automatic Mapping Extraction from Multiecho T2-Star Weighted Magnetic Resonance Images for Improving Morphological Evaluations in Human Brain

    PubMed Central

    Yu, Shaode; Xie, Yaoqin

    2013-01-01

    Mapping extraction is useful in medical image analysis. Similarity coefficient mapping (SCM) replaced signal response to time course in tissue similarity mapping with signal response to TE changes in multiecho T2-star weighted magnetic resonance imaging without contrast agent. Since different tissues are with different sensitivities to reference signals, a new algorithm is proposed by adding a sensitivity index to SCM. It generates two mappings. One measures relative signal strength (SSM) and the other depicts fluctuation magnitude (FMM). Meanwhile, the new method is adaptive to generate a proper reference signal by maximizing the sum of contrast index (CI) from SSM and FMM without manual delineation. Based on four groups of images from multiecho T2-star weighted magnetic resonance imaging, the capacity of SSM and FMM in enhancing image contrast and morphological evaluation is validated. Average contrast improvement index (CII) of SSM is 1.57, 1.38, 1.34, and 1.41. Average CII of FMM is 2.42, 2.30, 2.24, and 2.35. Visual analysis of regions of interest demonstrates that SSM and FMM show better morphological structures than original images, T2-star mapping and SCM. These extracted mappings can be further applied in information fusion, signal investigation, and tissue segmentation. PMID:24379892

  9. Key metabolites in tissue extracts of Elliptio complanata identified using 1H nuclear magnetic resonance spectroscopy

    PubMed Central

    Hurley-Sanders, Jennifer L.; Levine, Jay F.; Nelson, Stacy A. C.; Law, J. M.; Showers, William J.; Stoskopf, Michael K.

    2015-01-01

    We used 1H nuclear magnetic resonance spectroscopy to describe key metabolites of the polar metabolome of the freshwater mussel, Elliptio complanata. Principal components analysis documented variability across tissue types and river of origin in mussels collected from two rivers in North Carolina (USA). Muscle, digestive gland, mantle and gill tissues yielded identifiable but overlapping metabolic profiles. Variation in digestive gland metabolic profiles between the two mussel collection sites was characterized by differences in mono- and disaccharides. Variation in mantle tissue metabolomes appeared to be associated with sex. Nuclear magnetic resonance spectroscopy is a sensitive means to detect metabolites in the tissues of E. complanata and holds promise as a tool for the investigation of freshwater mussel health and physiology. PMID:27293708

  10. Non-classical nonlinear feature extraction from standard resonance vibration data for damage detection.

    PubMed

    Eiras, J N; Monzó, J; Payá, J; Kundu, T; Popovics, J S

    2014-02-01

    Dynamic non-classical nonlinear analyses show promise for improved damage diagnostics in materials that exhibit such structure at the mesoscale, such as concrete. In this study, nonlinear non-classical dynamic material behavior from standard vibration test data, using pristine and frost damaged cement mortar bar samples, is extracted and quantified. The procedure is robust and easy to apply. The results demonstrate that the extracted nonlinear non-classical parameters show expected sensitivity to internal damage and are more sensitive to changes owing to internal damage levels than standard linear vibration parameters. PMID:25234919

  11. Upgrade of the beam extraction system of the GTS-LHC electron cyclotron resonance ion source at CERN.

    PubMed

    Toivanen, V; Bellodi, G; Dimov, V; Küchler, D; Lombardi, A M; Maintrot, M

    2016-02-01

    Linac3 is the first accelerator in the heavy ion injector chain of the Large Hadron Collider (LHC), providing multiply charged heavy ion beams for the CERN experimental program. The ion beams are produced with GTS-LHC, a 14.5 GHz electron cyclotron resonance ion source, operated in afterglow mode. Improvement of the GTS-LHC beam formation and beam transport along Linac3 is part of the upgrade program of the injector chain in preparation for the future high luminosity LHC. A mismatch between the ion beam properties in the ion source extraction region and the acceptance of the following Low Energy Beam Transport (LEBT) section has been identified as one of the factors limiting the Linac3 performance. The installation of a new focusing element, an einzel lens, into the GTS-LHC extraction region is foreseen as a part of the Linac3 upgrade, as well as a redesign of the first section of the LEBT. Details of the upgrade and results of a beam dynamics study of the extraction region and LEBT modifications will be presented. PMID:26932084

  12. High intensity beams from electron cyclotron resonance ion sources: A study of efficient extraction and transport system (invited)

    NASA Astrophysics Data System (ADS)

    Gammino, S.; Ciavola, G.; Celona, L.; Andò, L.; Passarello, S.; Zhang, X. Zh.; Spädtke, P.; Winkler, M.

    2004-05-01

    A study of the design of extraction and transport system for high intensity beams that will be produced by the next generation electron cyclotron resonance ion source (ECRIS) was carried out in the frame of a European collaboration devoted to the definition of the main parameters of third generation ECRIS. High intensity production tests carried out in the previous years at INFN-LNS have shown evidence for the need to review the main concepts of the beam analysis and transport when high currents of low energy highly charged ions are extracted from the source. The transport of such low energy beams becomes critical as soon as the total current exceeds a few mA. The study reported here is based on the calculated parameters for the GyroSERSE source and the computer simulations have been carried out to obtain low emittance beams. The design of the extraction system was carried out by means of the KOBRA (three dimensional) code. The study of the beam line has been carried out with the codes GIOS, GICO, and TRANSPORT by taking into account both the phase space growth due to space charge and to the aberrations inside the magnets. The description of some different beam line options will be also given.

  13. Automatic bone segmentation and bone-cartilage interface extraction for the shoulder joint from magnetic resonance images

    NASA Astrophysics Data System (ADS)

    Yang, Zhengyi; Fripp, Jurgen; Chandra, Shekhar S.; Neubert, Aleš; Xia, Ying; Strudwick, Mark; Paproki, Anthony; Engstrom, Craig; Crozier, Stuart

    2015-02-01

    We present a statistical shape model approach for automated segmentation of the proximal humerus and scapula with subsequent bone-cartilage interface (BCI) extraction from 3D magnetic resonance (MR) images of the shoulder region. Manual and automated bone segmentations from shoulder MR examinations from 25 healthy subjects acquired using steady-state free precession sequences were compared with the Dice similarity coefficient (DSC). The mean DSC scores between the manual and automated segmentations of the humerus and scapula bone volumes surrounding the BCI region were 0.926  ±  0.050 and 0.837  ±  0.059, respectively. The mean DSC values obtained for BCI extraction were 0.806  ±  0.133 for the humerus and 0.795  ±  0.117 for the scapula. The current model-based approach successfully provided automated bone segmentation and BCI extraction from MR images of the shoulder. In future work, this framework appears to provide a promising avenue for automated segmentation and quantitative analysis of cartilage in the glenohumeral joint.

  14. Identification and quantitation of phosphorus metabolites in yeast neutral pH extracts by nuclear magnetic resonance spectroscopy.

    PubMed

    Teleman, A; Richard, P; Toivari, M; Penttilä, M

    1999-07-15

    (31)P NMR spectroscopy offers a possibility to obtain a survey of all low-molecular-weight phosphorylated compounds in yeast. The yeast cells have been extracted using chloroform into a neutral aqueous phase. The use of high fields and the neutral pH extracts, which are suitable for NMR analysis, results in well-resolved (31)P NMR spectra. Two-dimensional NMR experiments, such as proton-detected heteronuclear single quantum ((1)H-(31)P HSQC) and (31)P correlation spectroscopy ((31)P COSY), have been used to assign the resonances. In the phosphomonoester region many of the signals could be assigned to known metabolites in the glycolytic and pentose phosphate pathways, although some signals remain unidentified. Accumulation of ribulose 5-phosphate, xylulose 5-phosphate, and ribose 5-phosphate was observed in a strain lacking transketolase activity when grown in synthetic complete medium. No such accumulation occurred when the cells were grown in yeast-peptone-dextrose medium. Trimetaphosphate (intracellular concentration about 0.2 mM) was detected in both cold methanol-chloroform and perchloric acid extracts. PMID:10405295

  15. Upgrade of the beam extraction system of the GTS-LHC electron cyclotron resonance ion source at CERN

    NASA Astrophysics Data System (ADS)

    Toivanen, V.; Bellodi, G.; Dimov, V.; Küchler, D.; Lombardi, A. M.; Maintrot, M.

    2016-02-01

    Linac3 is the first accelerator in the heavy ion injector chain of the Large Hadron Collider (LHC), providing multiply charged heavy ion beams for the CERN experimental program. The ion beams are produced with GTS-LHC, a 14.5 GHz electron cyclotron resonance ion source, operated in afterglow mode. Improvement of the GTS-LHC beam formation and beam transport along Linac3 is part of the upgrade program of the injector chain in preparation for the future high luminosity LHC. A mismatch between the ion beam properties in the ion source extraction region and the acceptance of the following Low Energy Beam Transport (LEBT) section has been identified as one of the factors limiting the Linac3 performance. The installation of a new focusing element, an einzel lens, into the GTS-LHC extraction region is foreseen as a part of the Linac3 upgrade, as well as a redesign of the first section of the LEBT. Details of the upgrade and results of a beam dynamics study of the extraction region and LEBT modifications will be presented.

  16. Resolution of the multichannel anomaly in the extraction of S-matrix resonance-pole parameters

    SciTech Connect

    Ceci, Sasa; Stahov, Jugoslav; Svarc, Alfred; Zauner, Branimir; Watson, Shon

    2008-06-01

    Within the framework of a mathematically well-defined coupled-channel T-matrix model we have improved the existing multichannel pole-extraction procedure based on the numerical analytic continuation of the channel propagator, and for the first time we present the full set of pole parameters for already published amplitudes. Standard single-channel pole-extraction method (speed plot) was then applied to those amplitudes and resulting sets of T-matrix poles were inspected. The anomaly has been established that in some partial waves the pole values extracted using the standard single-channel methods differ not only from the values obtained using the analytic continuation method, but also change from one reaction to another. Inspired by this peculiarity, we have developed a new single-channel pole-extraction method based solely on the assumption of the partial wave analyticity. Since the speed plot turns out to be the lowest order term of the proposed method, the anomaly is understood and resolved.

  17. Note: resonant microwave compressor with two output ports for synchronous energy extraction.

    PubMed

    Avgustinovich, V A; Artemenko, S N; Kaminsky, V L; Novikov, S A; Yushkov, Yu G

    2011-04-01

    The brief theoretical analysis shows the resonant microwave compressor provides the output pulse power higher than the traveling wave power in the storage cavity. The experimental study was made with the model of the S-band microwave compressor. The power of pulses generated by the device reached the value three times as much as the value of the traveling wave power in the storage cavity at the maximum amplification 23 dB, peak power 400 MW, and pulse width 4-5 ns. PMID:21529048

  18. Results of Nucleon Resonance Extraction via Dynamical Coupled-Channels Analysis from Collaboration @ EBAC

    SciTech Connect

    Hiroyuki Kamano

    2012-04-01

    We review a global analysis of meson production reactions off the nucleons by a collaboration at Excited Baryon Analysis Center of Jefferson Lab. The analysis is pursued with a dynamical coupled-channels approach, within which the dynamics of multi-channel reaction processes are taken into account in a fully consistent way with the two-body as well as three-body unitarity of the S-matrix. With this approach, new features of nucleon excitations are revealed as resonant particles originating from the non-trivial multi-channel reaction dynamics, which cannot be addressed by static hadron models where the nucleon excitations are treated as stable particles.

  19. Extracting meson-baryon contributions to the electroexcitation of the N (1675)-5/2 nucleon resonance

    DOE PAGESBeta

    Aznauryan, Inna G.; Burkert, Volker D.

    2015-07-01

    We report on the determination of the electrocouplings for the transition from the proton to the N (1675)-5/2 resonance state using recent differential cross section data on ep → eπ+n by the CLAS collaboration at 1.8 ≤ Q² < 4.5GeV². The data have been analyzed using two different approaches, the unitary isobar model and fixed-t dispersion relations. The extracted γ*p → N (1675)-5/2 helicity amplitudes show considerable coupling through the AP1/2 amplitude, that is significantly larger than predicted three-quark contribution to this amplitude. The amplitude AP3/2 is much smaller. Both results are consistent with the predicted sizes of the meson-baryonmore » contributions at Q² ≥ 1.8 GeV² from the dynamical coupled-channel model.« less

  20. Extracting paramagnon excitations from resonant inelastic x-ray scattering experiments

    NASA Astrophysics Data System (ADS)

    Lamsal, Jagat; Montfrooij, Wouter

    2016-06-01

    Resonant x-ray scattering experiments on high-temperature superconductors and related cuprates have revealed the presence of intense paramagnon scattering at high excitation energies, of the order of several hundred meV. The excitation energies appear to show very similar behavior across all compounds, ranging from magnetically ordered, via superconductors, to heavy fermion systems. However, we argue that this apparent behavior has been inferred from the data through model fitting which implicitly imposes such similarities. Using model fitting that is free from such restrictions, we show that the paramagnons are not nearly as well defined as has been asserted previously, and that some paramagnons might not represent propagating excitations at all. Our work indicates that the data published previously in the literature will need to be reanalyzed with proper models.

  1. A UV resonance Raman (UVRR) spectroscopic study on the extractable compounds in Scots pine ( Pinus sylvestris) wood . Part II. Hydrophilic compounds

    NASA Astrophysics Data System (ADS)

    Nuopponen, M.; Willför, S.; Jääskeläinen, A.-S.; Vuorinen, T.

    2004-11-01

    Hydrophilic extracts of Scots pine ( Pinus sylvestris) heartwood and sapwood and a solid Scots pine knotwood sample were studied by UV resonance Raman spectroscopy (UVRRS). In addition, UVRR spectra of two hydrophilic model compounds (pinosylvin and chrysin) were analysed. UV Raman spectra were collected using 244 and 257 nm excitation wavelengths. The chemical composition of the acetone:water (95:5 v/v) extracts were also determined by gas chromatography. The aromatic and oleophilic structures of pinosylvin and chrysin showed three intense resonance enhanced bands in the spectral region of 1649-1548 cm -1. Pinosylvin showed also a relatively intense band in the aromatic substitution region at 996 cm -1. The spectra of the heartwood acetone:water extract showed many bands typical of pinosylvin. In addition, the extract included bands distinctive for resin and fatty acids. The sapwood acetone:water extract showed bands due to oleophilic structures at 1655-1650 cm -1. The extract probably also contained oligomeric lignans because the UVRR spectra were in parts similar to that of guaiacyl lignin. The characteristic band of pinosylvin (996 cm -1) was detected in the UVRR spectrum of the resin rich knotwood. In addition, several other bands typical for wood resin were observed, which indicated that the wood resin in the knotwood was resonance enhanced even more than lignin.

  2. A UV resonance Raman (UVRR) spectroscopic study on the extractable compounds in Scots pine (Pinus sylvestris) wood. Part II. Hydrophilic compounds.

    PubMed

    Nuopponen, M; Willför, S; Jääskeläinen, A-S; Vuorinen, T

    2004-11-01

    Hydrophilic extracts of Scots pine (Pinus sylvestris) heartwood and sapwood and a solid Scots pine knotwood sample were studied by UV resonance Raman spectroscopy (UVRRS). In addition, UVRR spectra of two hydrophilic model compounds (pinosylvin and chrysin) were analysed. UV Raman spectra were collected using 244 and 257 nm excitation wavelengths. The chemical composition of the acetone:water (95:5 v/v) extracts were also determined by gas chromatography. The aromatic and oleophilic structures of pinosylvin and chrysin showed three intense resonance enhanced bands in the spectral region of 1649-1548 cm(-1). Pinosylvin showed also a relatively intense band in the aromatic substitution region at 996 cm(-1). The spectra of the heartwood acetone:water extract showed many bands typical of pinosylvin. In addition, the extract included bands distinctive for resin and fatty acids. The sapwood acetone:water extract showed bands due to oleophilic structures at 1655-1650 cm(-1). The extract probably also contained oligomeric lignans because the UVRR spectra were in parts similar to that of guaiacyl lignin. The characteristic band of pinosylvin (996 cm(-1)) was detected in the UVRR spectrum of the resin rich knotwood. In addition, several other bands typical for wood resin were observed, which indicated that the wood resin in the knotwood was resonance enhanced even more than lignin. PMID:15477131

  3. Sequential application of viscous opening and lower leveling for three-dimensional brain extraction on magnetic resonance imaging T1

    NASA Astrophysics Data System (ADS)

    Mendiola-Santibañez, Jorge Domingo; Gallegos-Duarte, Martín; Arias-Estrada, Miguel Octavio; Santillán-Méndez, Israel Marcos; Rodríguez-Reséndiz, Juvenal; Terol-Villalobos, Iván Ramón

    2014-05-01

    A composition of the viscous opening and the lower leveling is introduced to extract brain in magnetic resonance imaging T1. The innovative transformation disconnects chained components and has better control on the reconstruction process of the marker inside of the original image. However, the sequential operator requires setting several parameters, making its application difficult. Due to this situation, a simplification is carried out on it to obtain a more practical method. The proposed morphological transformations were tested with the Internet Brain Segmentation Repository (IBSR) database, which is used as a benchmark among the community. The results are compared using the Jaccard and Dice indices with respect to (i) manual segmentations obtained from the IBSR, (ii) mean indices reported in the current literature, and (iii) segmentations obtained from the Brain Extraction Tool, since this is one of the most popular algorithms used for brain segmentation. The average indices of Jaccard and Dice indicate that the reduced transformation produces similar results to the other methods reported in the literature while the sequential operator presents a better performance.

  4. Nuclear resonant inelastic x-ray scattering: Methodology and extraction of vibrational properties of minerals

    NASA Astrophysics Data System (ADS)

    Hu, M. Y.; Alp, E. E.; Bi, W.; Sturhahn, W.; Toellner, T. S.; Zhao, J.

    2013-12-01

    Nuclear resonant inelastic x-ray scattering (NRIXS) is a synchrotron radiation based experimental method [1]. Since its introduction almost 20 years ago [2], NRIXS has found an expanding range of applications of studying lattice dynamics in condensed matter physics, materials science, high-pressure research, geosciences, and biophysics. After the first high pressure application in geophysics of measuring sound velocity of iron up to 153 GPa [3], it has become a widely used method to investigate deep earth compositions through sound velocity measurements [4,5]. Thermodynamic properties are also explored, in particular Grueneisen parameters [6]. Later, it was realized that isotope fractionaton factors can be derived from NRIXS measurements [7,8]. Sum rules and moments of NRIXS is a critical part of this methodology [9,10]. We will discuss this and in general the data analysis of NRIXS which enables the above mentioned applications. [1] Alp et al. Hyperfine Interactions 144/145, 3 (2002) [2] Sturhahn et al., PRL 74, 3832 (1995) [3] Mao et al., Science 292, 914 (2001) [4] Hu et al., PRB 67, 094304 (2003) [5] Sturhahn & Jackson, GSA special paper 421 (2007) [6] Murphy et al., Geophys. Res. Lett. 38, L24306 (2011) [7] Polyakov, Science 323, 912 (2009) [8] Dauphas et al., Geochimica et Cosmochimica Acta 94, 254 (2012) [9] Lipkin, PRB 52, 10073 (1995) [10] Hu et al., PRB 87, 064301 (2013)

  5. Extracting the resonance parameters from experimental data on scattering of charged particles

    NASA Astrophysics Data System (ADS)

    Vaandrager, P.; Rakityansky, S. A.

    2016-02-01

    A new parametrization of the multi-channel S-matrix is used to fit scattering data and then to locate the resonances as its poles. The S-matrix is written in terms of the corresponding “in” and “out” Jost matrices which are expanded in the Taylor series of the collision energy E around an appropriately chosen energy E0. In order to do this, the Jost matrices are written in a semi-analytic form where all the factors (involving the channel momenta and Sommerfeld parameters) responsible for their “bad behavior” (i.e., responsible for the multi-valuedness of the Jost matrices and for branching of the Riemann surface of the energy) are given explicitly. The remaining unknown factors in the Jost matrices are analytic and single-valued functions of the variable E and are defined on a simple energy plane. The expansion is done for these analytic functions and the expansion coefficients are used as the fitting parameters. The method is tested on a two-channel model, using a set of artificially generated data points with typical error bars and a typical random noise in the positions of the points.

  6. Automated Feature Extraction in Brain Tumor by Magnetic Resonance Imaging Using Gaussian Mixture Models

    PubMed Central

    Chaddad, Ahmad

    2015-01-01

    This paper presents a novel method for Glioblastoma (GBM) feature extraction based on Gaussian mixture model (GMM) features using MRI. We addressed the task of the new features to identify GBM using T1 and T2 weighted images (T1-WI, T2-WI) and Fluid-Attenuated Inversion Recovery (FLAIR) MR images. A pathologic area was detected using multithresholding segmentation with morphological operations of MR images. Multiclassifier techniques were considered to evaluate the performance of the feature based scheme in terms of its capability to discriminate GBM and normal tissue. GMM features demonstrated the best performance by the comparative study using principal component analysis (PCA) and wavelet based features. For the T1-WI, the accuracy performance was 97.05% (AUC = 92.73%) with 0.00% missed detection and 2.95% false alarm. In the T2-WI, the same accuracy (97.05%, AUC = 91.70%) value was achieved with 2.95% missed detection and 0.00% false alarm. In FLAIR mode the accuracy decreased to 94.11% (AUC = 95.85%) with 0.00% missed detection and 5.89% false alarm. These experimental results are promising to enhance the characteristics of heterogeneity and hence early treatment of GBM. PMID:26136774

  7. Emittance balancing technique for the resonant slow extraction from a synchrotron

    NASA Astrophysics Data System (ADS)

    Tang, J. Y.; Liu, L.; Yang, Z.; Fang, S. X.; Guan, X. L.

    2009-05-01

    A new method is proposed to produce identical beam emittances in the transverse phase planes from a severely asymmetric beam extracted from a slow-cycling synchrotron. This is important to obtain a good beam distribution at the irradiation spot when the spot scanning method is used for the treatment in hadron therapy. The method makes use of the beam rotation effect either by a solenoid or by a rotational quadrupole section, referred to as rotator, to produce identical emittances in the two transverse phase planes. It is also helpful for the stabilization of the beam spot at the irradiation point. Simulation studies with an artificially generated beam have been carried out to prove the principle. The method is not only applicable to fixed treatment nozzles but also to rotational gantry nozzles. Both a solenoid and a section of quadrupole rotator can be used, with the former being ideal for proton gantries and the latter for fixed carbon nozzles. There is a practical limit in using room-temperature solenoid due to the high beam rigidity in the case of a carbon beam, for which a superconducting solenoid has to be used. The comparison with other methods and the practical applications of the method are also presented.

  8. Determination of trace uranium by resonance fluorescence method coupled with photo-catalytic technology and dual cloud point extraction.

    PubMed

    Li, Jiekang; Li, Guirong; Han, Qian

    2016-12-01

    In this paper, two kinds of salophens (Sal) with different solubilities, Sal1 and Sal2, have been respectively synthesized, and they all can combine with uranyl to form stable complexes: [UO2(2+)-Sal1] and [UO2(2+)-Sal2]. Among them, [UO2(2+)-Sal1] was used as ligand to extract uranium in complex samples by dual cloud point extraction (dCPE), and [UO2(2+)-Sal2] was used as catalyst for the determination of uranium by photocatalytic resonance fluorescence (RF) method. The photocatalytic characteristic of [UO2(2+)-Sal2] on the oxidized pyronine Y (PRY) by potassium bromate which leads to the decrease of RF intensity of PRY were studied. The reduced value of RF intensity of reaction system (ΔF) is in proportional to the concentration of uranium (c), and a novel photo-catalytic RF method was developed for the determination of trace uranium (VI) after dCPE. The combination of photo-catalytic RF techniques and dCPE procedure endows the presented methods with enhanced sensitivity and selectivity. Under optimal conditions, the linear calibration curves range for 0.067 to 6.57ngmL(-1), the linear regression equation was ΔF=438.0 c (ngmL(-1))+175.6 with the correlation coefficient r=0.9981. The limit of detection was 0.066ngmL(-1). The proposed method was successfully applied for the separation and determination of uranium in real samples with the recoveries of 95.0-103.5%. The mechanisms of the indicator reaction and dCPE are discussed. PMID:27380304

  9. Extracting S-matrix poles for resonances from numerical scattering data: Type-II Padé reconstruction

    NASA Astrophysics Data System (ADS)

    Sokolovski, D.; Akhmatskaya, E.; Sen, S. K.

    2011-02-01

    We present a FORTRAN 77 code for evaluation of resonance pole positions and residues of a numerical scattering matrix element in the complex energy (CE) as well as in the complex angular momentum (CAM) planes. Analytical continuation of the S-matrix element is performed by constructing a type-II Padé approximant from given physical values (Bessis et al. (1994) [42]; Vrinceanu et al. (2000) [24]; Sokolovski and Msezane (2004) [23]). The algorithm involves iterative 'preconditioning' of the numerical data by extracting its rapidly oscillating potential phase component. The code has the capability of adding non-analytical noise to the numerical data in order to select 'true' physical poles, investigate their stability and evaluate the accuracy of the reconstruction. It has an option of employing multiple-precision (MPFUN) package (Bailey (1993) [45]) developed by D.H. Bailey wherever double precision calculations fail due to a large number of input partial waves (energies) involved. The code has been successfully tested on several models, as well as the F + H 2 → HF + H, F + HD → HF + D, Cl + HCl → ClH + Cl and H + D 2 → HD + D reactions. Some detailed examples are given in the text. Program summaryProgram title: PADE II Catalogue identifier: AEHO_v1_0 Program summary URL:http://cpc.cs.qub.ac.uk/summaries/AEHO_v1_0.html Program obtainable from: CPC Program Library, Queen's University, Belfast, N. Ireland Licensing provisions: Standard CPC licence, http://cpc.cs.qub.ac.uk/licence/licence.html No. of lines in distributed program, including test data, etc.: 19 959 No. of bytes in distributed program, including test data, etc.: 158 380 Distribution format: tar.gz Programming language: FORTRAN 77 Computer: Any computer equipped with a FORTRAN 90 compiler Operating system: UNIX, LINUX RAM: 256 Mb Classification: 16.8 External routines: NAG Program Library ( http://www.nag.co.uk/numeric/fl/FLdescription.asp) Nature of problem: The package extracts the positions and

  10. A UV resonance Raman (UVRR) spectroscopic study on the extractable compounds of Scots pine ( Pinus sylvestris) wood . Part I: Lipophilic compounds

    NASA Astrophysics Data System (ADS)

    Nuopponen, M.; Willför, S.; Jääskeläinen, A.-S.; Sundberg, A.; Vuorinen, T.

    2004-11-01

    The wood resin in Scots pine ( Pinus sylvestris) stemwood and branch wood were studied using UV resonance Raman (UVRR) spectroscopy. UVRR spectra of the sapwood and heartwood hexane extracts, solid wood samples and model compounds (six resin acids, three fatty acids, a fatty acid ester, sitosterol and sitosterol acetate) were collected using excitation wavelengths of 229, 244 and 257 nm. In addition, visible Raman spectra of the fatty and resin acids were recorded. Resin compositions of heartwood and sapwood hexane extracts were determined using gas chromatography. Raman signals of both conjugated and isolated double bonds of all the model compounds were resonance enhanced by UV excitation. The oleophilic structures showed strong bands in the region of 1660-1630 cm -1. Distinct structures were enhanced depending on the excitation wavelength. The UVRR spectra of the hexane extracts showed characteristic bands for resin and fatty acids. It was possible to identify certain resin acids from the spectra. UV Raman spectra collected from the solid wood samples containing wood resin showed a band at ˜1650 cm -1 due to unsaturated resin components. The Raman signals from extractives in the resin rich branch wood sample gave even more strongly enhanced signals than the aromatic lignin.

  11. A UV resonance Raman (UVRR) spectroscopic study on the extractable compounds of Scots pine (Pinus sylvestris) wood. Part I: lipophilic compounds.

    PubMed

    Nuopponen, M; Willför, S; Jääskeläinen, A-S; Sundberg, A; Vuorinen, T

    2004-11-01

    The wood resin in Scots pine (Pinus sylvestris) stemwood and branch wood were studied using UV resonance Raman (UVRR) spectroscopy. UVRR spectra of the sapwood and heartwood hexane extracts, solid wood samples and model compounds (six resin acids, three fatty acids, a fatty acid ester, sitosterol and sitosterol acetate) were collected using excitation wavelengths of 229, 244 and 257 nm. In addition, visible Raman spectra of the fatty and resin acids were recorded. Resin compositions of heartwood and sapwood hexane extracts were determined using gas chromatography. Raman signals of both conjugated and isolated double bonds of all the model compounds were resonance enhanced by UV excitation. The oleophilic structures showed strong bands in the region of 1660-1630 cm(-1). Distinct structures were enhanced depending on the excitation wavelength. The UVRR spectra of the hexane extracts showed characteristic bands for resin and fatty acids. It was possible to identify certain resin acids from the spectra. UV Raman spectra collected from the solid wood samples containing wood resin showed a band at approximately 1650 cm(-1) due to unsaturated resin components. The Raman signals from extractives in the resin rich branch wood sample gave even more strongly enhanced signals than the aromatic lignin. PMID:15477130

  12. Preliminary results of the ion extraction simulations applied to the MONO1000 and SUPERSHyPIE electron cyclotron resonance ion sourcesa)

    NASA Astrophysics Data System (ADS)

    Pierret, C.; Maunoury, L.; Biri, S.; Pacquet, J. Y.; Tuske, O.; Delferriere, O.

    2008-02-01

    The goal of this article is to present simulations on the extraction from an electron cyclotron resonance ion source (ECRIS). The aim of this work is to find out an extraction system, which allows one to reduce the emittances and to increase the current of the extracted ion beam at the focal point of the analyzing dipole. But first, we should locate the correct software which is able to reproduce the specific physics of an ion beam. To perform the simulations, the following softwares have been tested: SIMION 3D, AXCEL, CPO 3D, and especially, for the magnetic field calculation, MATHEMATICA coupled with the RADIA module. Emittance calculations have been done with two types of ECRIS: one with a hexapole and one without a hexapole, and the difference will be discussed.

  13. Preliminary results of the ion extraction simulations applied to the MONO1000 and SUPERSHyPIE electron cyclotron resonance ion sources.

    PubMed

    Pierret, C; Maunoury, L; Biri, S; Pacquet, J Y; Tuske, O; Delferriere, O

    2008-02-01

    The goal of this article is to present simulations on the extraction from an electron cyclotron resonance ion source (ECRIS). The aim of this work is to find out an extraction system, which allows one to reduce the emittances and to increase the current of the extracted ion beam at the focal point of the analyzing dipole. But first, we should locate the correct software which is able to reproduce the specific physics of an ion beam. To perform the simulations, the following softwares have been tested: SIMION 3D, AXCEL, CPO 3D, and especially, for the magnetic field calculation, MATHEMATICA coupled with the RADIA module. Emittance calculations have been done with two types of ECRIS: one with a hexapole and one without a hexapole, and the difference will be discussed. PMID:18315194

  14. Studies of extraction and transport system for highly charged ion beam of 18 GHz superconducting electron cyclotron resonance ion source at Research Center for Nuclear Physics

    SciTech Connect

    Yorita, T. Hatanaka, K.; Fukuda, M.; Ueda, H.; Yasuda, Y.; Morinobu, S.; Tamii, A.; Kamakura, K.

    2014-02-15

    An 18 GHz superconducting electron cyclotron resonance ion source is installed to increase beam currents and to extend the variety of ions especially for highly charged heavy ions which can be accelerated by cyclotrons of Research Center for Nuclear Physics (RCNP), Osaka University. The beam production developments of several ions from B to Xe have been already done [T. Yorita, K. Hatanaka, M. Fukuda, M. Kibayashi, S. Morinobu, H.Okamura, and A. Tamii, Rev. Sci. Instrum. 79, 02A311 (2008) and T. Yorita, K. Hatanaka, M. Fukuda, M. Kibayashi, S. Morinobu, H.Okamura, and A. Tamii, Rev. Sci. Instrum. 81, 02A332 (2010)] and the further studies for those beam extraction and its transport have been done in order to increase the beam current more. The plasma electrode, extraction electrode, and einzel lens are modified. Especially extraction electrode can be applied minus voltage for the beam extraction and it works well to improve the extracted beam current. The extraction voltage dependences of transmission and emittance also have been studied for beam current improvement which is injected into azimuthally varying field cyclotron at RCNP.

  15. New opportunities of the application of natural herb and spice extracts in plant oils: application of electron paramagnetic resonance in examining the oxidative stability.

    PubMed

    Kozłowska, Mariola; Szterk, Arkadiusz; Zawada, Katarzyna; Ząbkowski, Tomasz

    2012-09-01

    The aim of this study was to establish the applicability of natural water-ethanol extracts of herbs and spices in increasing the oxidative stability of plant oils and in the production of novel food. Different concentrations (0, 100, 300, 500, and 700 ppm) of spice extracts and butylated hydroxyanisole (BHA) (100 ppm) were added to the studied oils. The antioxidant activity of spice extracts was determined with electron paramagnetic resonance (EPR) spectroscopy using 2,2-diphenyl-1-picrylhydrazyl (DPPH) radical assay. The study showed that the extracts significantly increased the oxidative stability of the examined oils when compared to one of the strongest synthetic antioxidants--BHA. The applied simple production technology and addition of herb and spice extracts to plant oils enabled enhancement of their oxidative stability. The extracts are an alternative to the oils aromatized with an addition of fresh herbs, spices, and vegetables because it did not generate additional flavors thus enabling the maintenance of the characteristic ones. Moreover, it will increase the intake of natural substances in human diet, which are known to possess anticarcinogenic properties. PMID:22900972

  16. Studies of extraction and transport system for highly charged ion beam of 18 GHz superconducting electron cyclotron resonance ion source at Research Center for Nuclear Physics.

    PubMed

    Yorita, T; Hatanaka, K; Fukuda, M; Ueda, H; Yasuda, Y; Morinobu, S; Tamii, A; Kamakura, K

    2014-02-01

    An 18 GHz superconducting electron cyclotron resonance ion source is installed to increase beam currents and to extend the variety of ions especially for highly charged heavy ions which can be accelerated by cyclotrons of Research Center for Nuclear Physics (RCNP), Osaka University. The beam production developments of several ions from B to Xe have been already done [T. Yorita, K. Hatanaka, M. Fukuda, M. Kibayashi, S. Morinobu, H.Okamura, and A. Tamii, Rev. Sci. Instrum. 79, 02A311 (2008) and T. Yorita, K. Hatanaka, M. Fukuda, M. Kibayashi, S. Morinobu, H.Okamura, and A. Tamii, Rev. Sci. Instrum. 81, 02A332 (2010)] and the further studies for those beam extraction and its transport have been done in order to increase the beam current more. The plasma electrode, extraction electrode, and einzel lens are modified. Especially extraction electrode can be applied minus voltage for the beam extraction and it works well to improve the extracted beam current. The extraction voltage dependences of transmission and emittance also have been studied for beam current improvement which is injected into azimuthally varying field cyclotron at RCNP. PMID:24593475

  17. A study of coal extraction with electron paramagnetic resonance (EPR) and proton nuclear magnetic resonance relaxation techniques. Quarterly technical progress report, April 1, 1993--June 30, 1993

    SciTech Connect

    Doetschman, D.C.; Mehlenbacher, R.C.; Ito, O.

    1993-09-01

    An electron spin and proton magnetic relaxation study is presented on the effects of the solvent extraction of coal on the macromoleculer network of the coal and on the mobile molecular species that are initially within the coal. The eight Argonne Premium coals were extracted at room temperature with a 1:1 (v/v) N-methylpyrrolidinone (NMP)-CS2 solvent mixture under an inert atmosphere. As much solvent as possible was removed from extract and residue by treatment in a vacuum. The mobilization of molecular free radicals by the solvent and the exposure of free radicals in the macromoleculer matrix to solvent or to species dissolved in the solvent, results in a preferential survival of residue radicals of types that depend on the particular coal and results in the apparently fairly uniform loss of all types of radicals in bituminous coal extracts. The surviving extract and residue free radicals are more predominantly of the odd- alternate hydrocarbon free radical type. The spin-lattice relaxation (SLR) of these coal free radicals has previously been inferred (Doetschman and Dwyer, Energy Fuels, 1992, 6, 783) to be from the modulation of the intramolecular electron-nuclear dipole-interactions of the CH groups in a magnetic field by rocldng motions of the radical in the coal matrix. Such a modulation would depend not only on the rocking amplitude and frequency but also upon the electron spin density at the CH groups in the radical. The observed SLR rates decrease with coal rank in agreement with the smaller spin densities and the lower rocidng amplitudes that are expected for the larger polycondensed ring systems in coals of higher rank. The SLR rates are found to be generally faster in the extracts (than residues) where the molecular species would be expected to have a smaller polycondensed ring system than in the macromoleculer matrix of the residue.

  18. Direct assessment by electron spin resonance spectroscopy of the antioxidant effects of French maritime pine bark extract in the maxillofacial region of hairless mice

    PubMed Central

    Yoshida, Ayaka; Yoshino, Fumihiko; Tsubata, Masahito; Ikeguchi, Motoya; Nakamura, Takeshi; Lee, Masaichi-Chang-il

    2011-01-01

    Flavangenol, one of extract of French maritime pine bark, is a complex mixture of bioflavonoids with oligometric proanthocyanidins as the major constituents. These constituents, catechin and procyanidin B1, are water-soluble derivatives of flavangenol. In this study, we investigated the antioxidant effects of flavangenol on reactive oxygen species such as hydroxyl radical, superoxide anion and singlet oxygen using electron spin resonance and spin trapping. The effect of flavangenol on oxidative stress in the skin from the maxillofacial region of hairless mice was investigated using an in vivo L-band electron spin resonance imaging system. Flavangenol attenuated oxidative stress in the maxillofacial skin by acting as a reactive oxygen species scavenger, as demonstrated by in vitro and in vivo electron spin resonance imaging analysis. The absorption and metabolism of flavangenol were also examined. After oral administration of flavangenol in human and rat, most of the catechin in plasma was in the conjugated form, while 45% to 78% of procyanidin B1 was unconjugated, indicating that non-conjugated procyanidin B1 would be active in the circulation. The ability of flavangenol to reduce reactive oxygen species levels in the circulation of the maxillofacial region suggests that this extract may be beneficial for skin protection from exposure to ultraviolet irradiation. PMID:21980222

  19. On-Demand Single Photons with High Extraction Efficiency and Near-Unity Indistinguishability from a Resonantly Driven Quantum Dot in a Micropillar.

    PubMed

    Ding, Xing; He, Yu; Duan, Z-C; Gregersen, Niels; Chen, M-C; Unsleber, S; Maier, S; Schneider, Christian; Kamp, Martin; Höfling, Sven; Lu, Chao-Yang; Pan, Jian-Wei

    2016-01-15

    Scalable photonic quantum technologies require on-demand single-photon sources with simultaneously high levels of purity, indistinguishability, and efficiency. These key features, however, have only been demonstrated separately in previous experiments. Here, by s-shell pulsed resonant excitation of a Purcell-enhanced quantum dot-micropillar system, we deterministically generate resonance fluorescence single photons which, at π pulse excitation, have an extraction efficiency of 66%, single-photon purity of 99.1%, and photon indistinguishability of 98.5%. Such a single-photon source for the first time combines the features of high efficiency and near-perfect levels of purity and indistinguishabilty, and thus opens the way to multiphoton experiments with semiconductor quantum dots. PMID:26824530

  20. Extracting the cross section angular distributions for 15C high-energy resonance excited via the (18O,16O) two-neutron transfer reaction

    NASA Astrophysics Data System (ADS)

    Carbone, D.; Agodi, C.; Cappuzzello, F.; Cavallaro, M.; Foti, A.; Linares, R.

    2016-05-01

    The 13C(18O,16O)15C reaction has been studied at 84 MeV incident energy. The ejectiles have been momentum analized by the MAGNEX spectrometer and 15C excitation energy spectra have been obtained up to about 20 MeV. In the region above the two-neutron separation energy, a bump has been observed at 13.7 MeV. The extracted cross section angular distribution for this structure, obtained by using different models for background, displays a clear oscillating pattern, typical of resonant state of the residual nucleus.

  1. pH recycling aqueous two-phase systems applied in extraction of Maitake β-Glucan and mechanism analysis using low-field nuclear magnetic resonance.

    PubMed

    Hou, Huiyun; Cao, Xuejun

    2015-07-31

    In this paper, a recycling aqueous two-phase systems (ATPS) based on two pH-response copolymers PADB and PMDM were used in purification of β-Glucan from Grifola frondosa. The main parameters, such as polymer concentration, type and concentration of salt, extraction temperature and pH, were investigated to optimize partition conditions. The results demonstrated that β-Glucan was extracted into PADB-rich phase, while impurities were extracted into PMDM-rich phase. In this 2.5% PADB/2.5% PMDM ATPS, 7.489 partition coefficient and 96.92% extraction recovery for β-Glucan were obtained in the presence of 30mmol/L KBr, at pH 8.20, 30°C. The phase-forming copolymers could be recycled by adjusting pH, with recoveries of over 96.0%. Furthermore, the partition mechanism of Maitake β-Glucan in PADB/PMDM aqueous two-phase systems was studied. Fourier transform infrared spectra, ForteBio Octet system and low-field nuclear magnetic resonance (LF-NMR) were introduced for elucidating the partition mechanism of β-Glucan. Especially, LF-NMR was firstly used in the mechanism analysis in partition of aqueous two-phase systems. The change of transverse relaxation time (T2) in ATPS could reflect the interaction between polymers and β-Glucan. PMID:26094138

  2. Combined use of high-resolution α-glucosidase inhibition profiling and high-performance liquid chromatography-high-resolution mass spectrometry-solid-phase extraction-nuclear magnetic resonance spectroscopy for investigation of antidiabetic principles in crude plant extracts.

    PubMed

    Kongstad, Kenneth T; Özdemir, Ceylan; Barzak, Asmah; Wubshet, Sileshi G; Staerk, Dan

    2015-03-01

    Type 2 diabetes is a metabolic disorder affecting millions of people worldwide, and new drug leads or functional foods containing selective α-glucosidase inhibitors are needed. Crude extract of 24 plants were assessed for α-glucosidase inhibitory activity. Methanol extracts of Cinnamomum zeylanicum bark, Rheum rhabarbarum peel, and Rheum palmatum root and ethyl acetate extracts of C. zeylanicum bark, Allium ascalonicum peel, and R. palmatum root showed IC50 values below 20 μg/mL. Subsequently, high-resolution α-glucosidase profiling was used in combination with high-performance liquid chromatography-high-resolution mass spectrometry-solid-phase extraction-nuclear magnetic resonance spectroscopy for identification of metabolites responsible for the α-glucosidase inhibitory activity. Quercetin (1) and its dimer (2), trimer (3), and tetramer (4) were identified as main α-glucosidase inhibitors in A. ascalonicum peel, whereas (E)-piceatannol 3'-O-β-D-glucopyranoside (5), (E)-rhapontigenin 3'-O-β-D-glucopyranoside (6), (E)-piceatannol (8), and emodin (12) were identified as main α-glucosidase inhibitors in R. palmatum root. PMID:25652946

  3. Measurements of e p →e'π+n at 1.6 extraction of nucleon resonance electrocouplings at CLAS

    NASA Astrophysics Data System (ADS)

    Park, K.; Aznauryan, I. G.; Burkert, V. D.; Adhikari, K. P.; Amaryan, M. J.; Pereira, S. Anefalos; Avakian, H.; Battaglieri, M.; Badui, R.; Bedlinskiy, I.; Biselli, A. S.; Bono, J.; Briscoe, W. J.; Brooks, W. K.; Carman, D. S.; Celentano, A.; Chandavar, S.; Charles, G.; Colaneri, L.; Cole, P. L.; Contalbrigo, M.; Cortes, O.; Crede, V.; D'Angelo, A.; Dashyan, N.; De Vita, R.; De Sanctis, E.; Deur, A.; Djalali, C.; Doughty, D.; Dupre, R.; Egiyan, H.; Alaoui, A. El; Elouadrhiri, L.; Fassi, L. El; Eugenio, P.; Fedotov, G.; Fegan, S.; Fersch, R.; Filippi, A.; Fleming, J. A.; Garillon, B.; Garçon, M.; Gevorgyan, N.; Gilfoyle, G. P.; Giovanetti, K. L.; Girod, F. X.; Joo, H. S.; Goetz, J. T.; Golovatch, E.; Gothe, R. W.; Griffioen, K. A.; Guegan, B.; Guidal, M.; Guo, L.; Hakobyan, H.; Hanretty, C.; Hattawy, M.; Hicks, K.; Holtrop, M.; Hughes, S. M.; Hyde, C. E.; Ilieva, Y.; Ireland, D. G.; Ishkhanov, B. S.; Isupov, E. L.; Jenkins, D.; Jiang, H.; Jo, H. S.; Joo, K.; Joosten, S.; Keller, D.; Khandaker, M.; Kim, A.; Kim, W.; Klein, A.; Klein, F. J.; Kubarovsky, V.; Kuhn, S. E.; Kuleshov, S. V.; Lenisa, P.; Livingston, K.; Lu, H. Y.; MacGregor, I. J. D.; Markov, N.; Martinez, D.; McKinnon, B.; Mokeev, V.; Montgomery, R. A.; Moutarde, H.; Camacho, C. Munoz; Nadel-Turonski, P.; Niccolai, S.; Niculescu, G.; Niculescu, I.; Osipenko, M.; Ostrovidov, A. I.; Paolone, M.; Pasyuk, E.; Peng, P.; Phelps, W.; Phillips, J. J.; Pisano, S.; Pogorelko, O.; Price, J. W.; Procureur, S.; Prok, Y.; Protopopescu, D.; Puckett, A. J. R.; Raue, B. A.; Ripani, M.; Rizzo, A.; Rosner, G.; Rossi, P.; Roy, P.; Sabatié, F.; Salgado, C.; Schott, D.; Schumacher, R. A.; Seder, E.; Sharabian, Y. G.; Simonyan, A.; Skorodumina, Iu.; Smith, E. S.; Smith, G. D.; Sparveris, N.; Stoler, P.; Strakovsky, I. I.; Strauch, S.; Sytnik, V.; Taiuti, M.; Tang, W.; Taylor, C. E.; Tian, Ye; Trivedi, A.; Ungaro, M.; Voskanyan, H.; Voutier, E.; Walford, N. K.; Watts, D. P.; Wei, X.; Weinstein, L. B.; Wood, M. H.; Zachariou, N.; Zana, L.; Zhang, J.; Zhao, Z. W.; Zonta, I.; CLAS Collaboration

    2015-04-01

    Differential cross sections of the exclusive process e p →e'π+n were measured with good precision in the range of the photon virtuality Q2=1.8 -4.5 GeV2 and the invariant mass range of the π+n final state W =1.6 -2.0 GeV using the Continuous Electron Beam Accelerator Facility Large Acceptance Spectrometer. Data were collected with nearly complete coverage in the azimuthal and polar angles of the n π+ center-of-mass system. More than 37 000 cross-section points were measured. The contributions of the isospin I =1/2 resonances N (1675 ) 5/2-,N (1680 ) 5/2+ , and N (1710 ) 1/2+ were extracted at different values of Q2 using a single-channel, energy-dependent resonance amplitude analysis. Two different approaches, the unitary isobar model and the fixed-t dispersion relations, were employed in the analysis. We observe significant strength of the N (1675 ) 5/2- in the A1 /2 amplitude, which is in strong disagreement with quark models that predict both transverse amplitudes to be strongly suppressed. For the N (1680 ) 5/2+ we observe a slow changeover from the dominance of the A3 /2 amplitude at the real photon point (Q2=0 ) to a Q2 where A1 /2 begins to dominate. The scalar amplitude S1 /2 drops rapidly with Q2 consistent with quark model prediction. For the N (1710 ) 1/2+ resonance our analysis shows significant strength for the A1 /2 amplitude at Q2<2.5 GeV2.

  4. Extracting partial decay rates of helium from complex rotation: autoionizing resonances of the one-dimensional configurations

    NASA Astrophysics Data System (ADS)

    Zimmermann, Klaus; Lugan, Pierre; Jörder, Felix; Heitz, Nicolai; Schmidt, Maximilian; Bouri, Celsus; Rodriguez, Alberto; Buchleitner, Andreas

    2015-01-01

    Partial autoionization rates of doubly excited one-dimensional helium in the collinear Zee and eZe configuration are obtained by means of the complex rotation method. The approach presented here relies on a projection of back-rotated resonance wave functions onto singly ionized H{{e}+} channel wave functions and the computation of the corresponding particle fluxes. In spite of the long-range nature of the Coulomb potential between the electrons and the nucleus, an asymptotic region where the fluxes are stationary is clearly observed. Low-lying doubly excited states are found to decay predomintantly into the nearest single-ionization continuum. This approach paves the way for a systematic analysis of the decay rates observed in higher-dimensional models, and of the role of electronic correlations and atomic structure in recent photoionization experiments.

  5. Bayesian Extraction of Deep UV Resonance Raman Signature of Fibrillar Cross-β Sheet Core based on H-D Exchange Data

    NASA Astrophysics Data System (ADS)

    Shashilov, V. A.; Lednev, I. K.

    2007-11-01

    Amyloid fibrils are associated with many neurodegenerative diseases. The application of conventional biophysical techniques including solution NMR and X-ray crystallography for structural characterization of fibrils is limited because they are neither crystalline nor soluble. The Bayesian approach was utilized for extracting the deep UV resonance Raman (DUVRR) spectrum of the lysozyme fibrillar β-sheet based on the hydrogen-deuterium exchange spectral data. The problem was shown to be unsolvable when using blind source separation or conventional chemometrics methods because of the 100% correlation of the concentration profiles of the species under study. Information about the mixing process was incorporated by forcing the columns of the concentration matrix to be proportional to the expected concentration profiles. The ill-conditioning of the matrix was removed by concatenating it to the diagonal matrix with entries corresponding to the known pure spectra (sources). Prior information about the spectral features and characteristic bands of the spectra was taken into account using the Bayesian signal dictionary approach. The extracted DUVRR spectrum of the cross-β sheet core exhibited sharp bands indicating the highly ordered structure. Well resolved sub-bands in Amide I and Amide III regions enabled us to assign the fibril core structure to anti-parallel β-sheet and estimate the amide group facial angle Ψ in the cross-β structure. The elaborated Bayesian approach was demonstrated to be applicable for studying correlated biochemical processes.

  6. Metabonomic analysis of water extracts from different angelica roots by ¹H-nuclear magnetic resonance spectroscopy.

    PubMed

    Chan, Pui Hei; Zhang, Wendy L; Lau, Chung-Ho; Cheung, Chi Yuen; Keun, Hector C; Tsim, Karl W K; Lam, Henry

    2014-01-01

    Angelica Radix, the roots of the genus Angelica, has been used for more than 2,000 years as a traditional medicine in Eastern Asia. The Chinese Pharmacopoeia records more than 100 herbal formulae containing Angelica roots. There are two common sources of Angelica roots, Angelica sinensis from China and A. gigas from Korea. The two species of Angelica roots differ in their chemical compositions, pharmacological properties and clinical efficacy. ¹H-NMR metabolic profiling has recently emerged as a promising quality control method for food and herbal chemistry. We explored the use of ¹H-NMR metabolic profiling for the quality control of Angelica Radix. Unlike previous work, we performed the metabolic profiling on hot water extracts, so as to mimic the clinically relevant preparation method. Unsupervised principle component analyses of both the full spectral profile and a selection of targeted molecules revealed a clear differentiation of three types of Angelica roots. In addition, the levels of 13 common metabolites were measured. Statistically significant differences in the levels of glucose, fructose and threonine were found between different sources of Angelica. Ferulic acid, a marker commonly used to evaluate Angelica root, was detected in our samples, but the difference in ferulic acid levels between the samples was not statistically significant. Overall, we successfully applied ¹H-NMR metabolic profiling with water extraction to discriminate all three sources of Angelica roots, and obtained quantitative information of many common metabolites. PMID:24658570

  7. Neuroimaging measures of error-processing: Extracting reliable signals from event-related potentials and functional magnetic resonance imaging.

    PubMed

    Steele, Vaughn R; Anderson, Nathaniel E; Claus, Eric D; Bernat, Edward M; Rao, Vikram; Assaf, Michal; Pearlson, Godfrey D; Calhoun, Vince D; Kiehl, Kent A

    2016-05-15

    Error-related brain activity has become an increasingly important focus of cognitive neuroscience research utilizing both event-related potentials (ERPs) and functional magnetic resonance imaging (fMRI). Given the significant time and resources required to collect these data, it is important for researchers to plan their experiments such that stable estimates of error-related processes can be achieved efficiently. Reliability of error-related brain measures will vary as a function of the number of error trials and the number of participants included in the averages. Unfortunately, systematic investigations of the number of events and participants required to achieve stability in error-related processing are sparse, and none have addressed variability in sample size. Our goal here is to provide data compiled from a large sample of healthy participants (n=180) performing a Go/NoGo task, resampled iteratively to demonstrate the relative stability of measures of error-related brain activity given a range of sample sizes and event numbers included in the averages. We examine ERP measures of error-related negativity (ERN/Ne) and error positivity (Pe), as well as event-related fMRI measures locked to False Alarms. We find that achieving stable estimates of ERP measures required four to six error trials and approximately 30 participants; fMRI measures required six to eight trials and approximately 40 participants. Fewer trials and participants were required for measures where additional data reduction techniques (i.e., principal component analysis and independent component analysis) were implemented. Ranges of reliability statistics for various sample sizes and numbers of trials are provided. We intend this to be a useful resource for those planning or evaluating ERP or fMRI investigations with tasks designed to measure error-processing. PMID:26908319

  8. Determination of oxygen extraction fraction using magnetic resonance imaging in canine models with internal carotid artery occlusion.

    PubMed

    Chang, Fei-Yan; Xiao, Jiang-Xi; Xie, Sheng; Yu, Lei; Zhang, Zhen-Xia; Wang, Wu; Luo, Jie; Zhang, Zhong-Ping; Guo, Hua

    2016-01-01

    Perfusion of the penumbra tissue below the flow threshold for functional disturbance but above that for the maintenance of morphological integrity is the target for therapy in acute ischaemic stroke. The measurement of the oxygen extraction fraction (OEF) may provide a direct assessment of tissue viability, so that irreversible tissue damage and penumbra can be reliably identified. By using an asymmetric spin echo single-shot echo planar imaging (ASE-SSEPI) sequence, the quantitative OEF was obtained in the ischaemic brain tissues of canine models with internal carotid artery occlusion. TTC staining, which delineated the regions of infarct and penumbra, was used for defining the corresponding regions on OEF maps. The threshold of the OEF to discriminate the infarct cores and penumbral tissues was then determined according to the OEF values at different times. With repeated-measures ANOVA, the OEF of the infarcted regions was found to be time dependent. An OEF greater than 0.48 best predicted cortical infarction at 1.5 hr, with an area under the receiving operating characteristic curve of 0.968, a sensitivity of 97.5%, and a specificity of 92.5%. Our results may be helpful in the evaluation of tissue viability during stroke events. PMID:27443195

  9. Determination of oxygen extraction fraction using magnetic resonance imaging in canine models with internal carotid artery occlusion

    PubMed Central

    Chang, Fei-Yan; Xiao, Jiang-Xi; Xie, Sheng; Yu, Lei; Zhang, Zhen-Xia; Wang, Wu; Luo, Jie; Zhang, Zhong-Ping; Guo, Hua

    2016-01-01

    Perfusion of the penumbra tissue below the flow threshold for functional disturbance but above that for the maintenance of morphological integrity is the target for therapy in acute ischaemic stroke. The measurement of the oxygen extraction fraction (OEF) may provide a direct assessment of tissue viability, so that irreversible tissue damage and penumbra can be reliably identified. By using an asymmetric spin echo single-shot echo planar imaging (ASE-SSEPI) sequence, the quantitative OEF was obtained in the ischaemic brain tissues of canine models with internal carotid artery occlusion. TTC staining, which delineated the regions of infarct and penumbra, was used for defining the corresponding regions on OEF maps. The threshold of the OEF to discriminate the infarct cores and penumbral tissues was then determined according to the OEF values at different times. With repeated-measures ANOVA, the OEF of the infarcted regions was found to be time dependent. An OEF greater than 0.48 best predicted cortical infarction at 1.5 hr, with an area under the receiving operating characteristic curve of 0.968, a sensitivity of 97.5%, and a specificity of 92.5%. Our results may be helpful in the evaluation of tissue viability during stroke events. PMID:27443195

  10. Direct proof by 13C-nuclear magnetic resonance of semi-purified extract and isolation of ent-Catechin from leaves of Eucalyptus cinerea

    PubMed Central

    Silva, Sayonara Mendes; Abe, Simone Yae; Bueno, Fernanda Giacomini; Lopes, Norberto Peporine; de Mello, João Carlos Palazzo; Nakashima, Tomoe

    2014-01-01

    Background: Eucalyptus cinerea F. Muell. ex Benth. is native to Australia and acclimatized to Southern Brazil. Its aromatic leaves are used for ornamental purposes and have great potential for essential oil production, although reports of its use in folk medicine are few. Objective: This study evaluated the composition of E. cinerea leaves using the solid state 13C-nuclear magnetic resonance (NMR) and isolation of the compound from the semipurified extract (SE). Materials and Methods: The SE of E. cinerea leaves was evaluated in the solid state by 13C-NMR spectrum, and the SE was chromatographed on a Sephadex LH-20 column, followed by high-speed counter-current chromatography to isolate the compound. The SE was analyzed by 13C-NMR and matrix-assisted laser desorption/ionization-time-of-flight spectra. Results: Flavan-3-ol units were present, suggesting the presence of proanthocyanidins as well as a gallic acid unit. The uncommon ent-catechin was isolated. Conclusion: The presence of ent-catechin is reported for the first time in this genus and species. PMID:25210302

  11. Extracting meson-baryon contributions to the electroexcitation of the N (1675)-5/2 nucleon resonance

    SciTech Connect

    Aznauryan, Inna G.; Burkert, Volker D.

    2015-07-01

    We report on the determination of the electrocouplings for the transition from the proton to the N (1675)-5/2 resonance state using recent differential cross section data on ep → eπ+n by the CLAS collaboration at 1.8 ≤ Q² < 4.5GeV². The data have been analyzed using two different approaches, the unitary isobar model and fixed-t dispersion relations. The extracted γ*p → N (1675)-5/2 helicity amplitudes show considerable coupling through the AP1/2 amplitude, that is significantly larger than predicted three-quark contribution to this amplitude. The amplitude AP3/2 is much smaller. Both results are consistent with the predicted sizes of the meson-baryon contributions at Q² ≥ 1.8 GeV² from the dynamical coupled-channel model.

  12. Research efforts in support of resonance extraction studies. Volume 1: Improvement and validation of TWFD (Thin-Wire Frequency-Domain): A thin-wire frequency-domain scattering code

    NASA Astrophysics Data System (ADS)

    Auton, J. R.; Larry, T. L.; Vanblaricum, M. L.

    1984-11-01

    The development of a thin-wire frequency-domain (TWFD) method of moments code was discussed in a previous report 1. Since that time this code has undergone further development and numerical testing. The purpose of the code is to provide a theoretical and numerical basis to aid in understanding the resonance region electromagnetic scattering from thin-wire stick models. This frequency domain code augments a time-domain code (TWTD) which calculates the scattered transient response for an impulsive incident field. The outputs from both of these codes have provided numerical predictions which have been indispensible in assessing our ability to extract resonance information from actual scattering range data.

  13. Resonances and resonance widths

    SciTech Connect

    Collins, T.

    1986-05-01

    Two-dimensional betatron resonances are much more important than their simple one-dimensional counterparts and exhibit a strong dependence on the betatron phase advance per cell. A practical definition of ''width'' is expanded upon in order to display these relations in tables. A primarily pedagogical introduction is given to explain the tables, and also to encourage a wider capability for deriving resonance behavior and wider use of ''designer'' resonances.

  14. Slow extraction of LAMPF 2

    NASA Astrophysics Data System (ADS)

    Colton, E. P.

    Half integer resonant extraction are used to slowly extract the 45 GeV proton beam from the LAMPF II main ring during a time spread of 1/6 sec. High extraction efficiency is obtained by performing the extraction in a high beta long straight section and by utilizing an electrostatic wire septum and iron septum.

  15. Slow extraction at LAMPF II

    SciTech Connect

    Colton, E.P.

    1985-10-01

    Half-integer resonant extraction will be used to slow extract the 45 GeV proton beam from the LAMPF II main ring during a time spread of 1/6 sec. High extraction efficiency is obtained by performing the extraction in a high-beta long straight section and by utilizing an electrostatic wire septum and iron septum.

  16. A study on prevention of an electric discharge at an extraction electrode of an electron cyclotron resonance ion source for cancer therapy

    SciTech Connect

    Kishii, Y. Kawasaki, S.; Kitagawa, A.; Muramatsu, M.; Uchida, T.

    2014-02-15

    A compact ECR ion source has utilized for carbon radiotherapy. In order to increase beam intensity with higher electric field at the extraction electrode and be better ion supply stability for long periods, electric geometry and surface conditions of an extraction electrode have been studied. Focusing attention on black deposited substances on the extraction electrode, which were observed around the extraction electrode after long-term use, the relation between black deposited substances and the electrical insulation property is investigated. The black deposited substances were inspected for the thickness of deposit, surface roughness, structural arrangement examined using Raman spectroscopy, and characteristics of electric discharge in a test bench, which was set up to simulate the ECR ion source.

  17. 13C/15N‐Enriched l‐Dopa as a Triple‐Resonance NMR Probe to Monitor Neurotransmitter Dopamine in the Brain and Liver Extracts of Mice

    PubMed Central

    Kameda, Tetsuro; Kimura, Yu; Imai, Hirohiko; Matsuda, Tetsuya; Sando, Shinsuke; Toshimitsu, Akio

    2015-01-01

    Abstract In an attempt to monitor μm‐level trace constituents, we applied here 1H‐{13C‐15N} triple‐resonance nuclear magnetic resonance (NMR) to 13C/15N‐enriched l‐Dopa as the inevitable precursor of the neurotransmitter dopamine in the brain. The perfect selectivity (to render endogenous components silent) and μm‐level sensitivity (700 MHz spectrometer equipped with a cryogenic probe) of triple‐resonance allowed the unambiguous and quantitative metabolic and pharmacokinetic analyses of administered l‐Dopa/dopamine in the brain and liver of mice. The level of dopamine generated in the brain (within the range 7–76 μm, which covers the typical stimulated level of ∼30 μm) could be clearly monitored ex vivo, but was slightly short of the detection limit of a 7 T MR machine for small animals. This work suggests that μm‐level trace constituents are potential targets of ex vivo monitoring as long as they contain N atom(s) and their appropriate 13C/15N‐enrichment is synthetically accessible. PMID:27308224

  18. Epitope extraction technique using a proteolytic magnetic reactor combined with Fourier-transform ion cyclotron resonance mass spectrometry as a tool for the screening of potential vaccine lead peptides.

    PubMed

    Bílková, Z; Stefanescu, R; Cecal, R; Korecká, L; Ouzká, S; Jezová, J; Viovy, J-L; Przybylski, M

    2005-01-01

    Epitope extraction technique is based on the specific digestion of a target protein followed by immunoaffinity isolation of a specific recognition peptide. This technique, in combination with mass spectrometry, has been efficiently used for epitope identification. The major goal of this work was to utilize newly developed enzyme and immunoaffinity magnetic reactors for the epitope extraction procedure and confirm the efficiency of this improved system for epitope screening of proteins. Alginic acid-coated magnetite microparticles with immobilized TPCK-trypsin provided high working efficiency with low non-specific adsorption, digestion time in minutes and low frequency of missed cleavages. The sensitivity and specificity of tryptic fragmentation of the beta-amyloid-peptide Abeta (1-40) as a model polypeptide was confirmed by Fourier-transform ion cyclotron resonance mass spectrometry analysis. The Sepharose reactor or immunoaffinity magnetic reactors, both with anti-amyloid-beta monoclonal antibodies, were used for specific isolation and identification of target peptides. In this way, the epitope extraction technique combined with mass spectrometric analysis is shown to be an excellent base for molecular screening of potential vaccine lead proteins. PMID:16322655

  19. Slow extraction at LAMPF II

    SciTech Connect

    Colton, E.P.

    1985-01-01

    Half-integer resonant extraction will be used to slow extract the 45 GeV proton beam from the LAMPF II main ring during a time spread of 1/6 sec. High extration efficiency is obtained by performing the extraction in a high-beta long straight section and by utilizing an electrostatic wire septum and iron septum. 3 refs., 4 figs.

  20. Measurements of $ep \\to e^\\prime π^+n$ at W = 1.6 - 2.0 GeV and extraction of nucleon resonance electrocouplings at CLAS

    SciTech Connect

    Park, Kijun; Aznauryan, I. G.; Burkert, V. D.; Adhikari, K. P.; Amaryan, M. J.; Pereira, S. Anefalos; Avakian, H.; Battaglieri, M.; Badui, R.; Bedlinskiy, I.; Biselli, A. S.; Bono, J.; Briscoe, W. J.; Brooks, W. K.; Carman, D. S.; Celentano, A.; Chandavar, S.; Charles, G.; Colaneri, L.; Cole, P. L.; Contalbrigo, M.; Cortes, O.; Crede, V.; D'Angelo, A.; Dashyan, N.; De Vita, R.; De Sanctis, E.; Deur, A.; Djalali, C.; Doughty, D.; Dupre, R.; Egiyan, H.; Alaoui, A. El; Elouadrhiri, L.; Fassi, L. El; Eugenio, P.; Fedotov, G.; Fegan, S.; Fersch, R.; Filippi, A.; Fleming, J. A.; Garillon, B.; Garcon, M.; Gevorgyan, N.; Gilfoyle, G. P.; Giovanetti, K. L.; Girod, F. X.; Joo, H. S.; Goetz, J. T.; Golovatch, E.; Gothe, R. W.; Griffioen, K. A.; Guegan, B.; Guidal, M.; Guo, L.; Hakobyan, H.; Hanretty, C.; Hattawy, M.; Hicks, K.; Holtrop, M.; Hughes, S. M.; Hyde, C. E.; Ilieva, Y.; Ireland, D. G.; Ishkhanov, B. S.; Isupov, E. L.; Jenkins, D.; Jiang, H.; Jo, H. S.; Joo, K.; Joosten, S.; Keller, D.; Khandaker, M.; Kim, A.; Kim, W.; Klein, A.; Klein, F. J.; Kubarovsky, V.; Kuhn, S. E.; Kuleshov, S. V.; Lenisa, P.; Livingston, K.; Lu, H. Y.; MacGregor, I. J.; Markov, N.; Martinez, D.; McKinnon, B.; Mokeev, V.; Montgomery, R. A.; Moutarde, H.; Camacho, C. Munoz; Nadel-Turonski, P.; Niccolai, S.; Niculescu, G.; Niculescu, I.; Osipenko, M.; Ostrovidov, A. I.; Paolone, M.; Pasyuk, E.; Peng, P.; Phelps, W.; Phillips, J. J.; Pisano, S.; Pogorelko, O.; Price, J. W.; Procureur, S.; Prok, Y.; Protopopescu, D.; Puckett, A. J.; Raue, B. A.; Ripani, M.; Rizzo, A.; Rosner, G.; Rossi, P.; Roy, P.; Sabati??, F.; Salgado, C.; Schott, D.; Schumacher, R. A.; Seder, E.; Sharabian, Y. G.; Simonyan, A.; Skorodumina, Iu.; Smith, E. S.; Smith, G. D.; Sparveris, N.; Stoler, P.; Strakovsky, I. I.; Strauch, S.; Sytnik, V.; Taiuti, M.; Tang, W.; Taylor, C. E.; Tian, Ye; Trivedi, A.; Ungaro, M.; Voskanyan, H.; Voutier, E.; Walford, N. K.; Watts, D. P.; Wei, X.; Weinstein, L. B.; Wood, M. H.; Zachariou, N.; Zana, L.; Zhang, J.; Zhao, Z. W.; Zonta, I.

    2015-04-01

    Differential cross sections of the exclusive process $e p \\to e^\\prime \\pi^+ n$ were measured with good precision in the range of the photon virtuality $Q^2 = 1.8 - 4.5$ GeV$^2$, and the invariant mass range of the $\\pi^+ n$ final state W = 1.6 - 2.0 GeV using the CEBAF Large Acceptance Spectrometer. Data were collected with nearly complete coverage in the azimuthal and polar angles of the $n\\pi^+$ center-of-mass system. More than 37,000 cross section points were measured. The contributions of the isospin $I = {1\\over 2}$ resonances $N(1675){5\\over 2}^-$, $N(1680){5\\over 2}^+$ and $N(1710){1\\over 2}^+$ were extracted at different values of $Q^2$ using a single-channel, energy-dependent resonance amplitude analysis. Two different approaches, the unitary isobar model and the fixed-$t$ dispersion relations, were employed in the analysis. We observe significant strength of the $N(1675){5\\over 2}^-$ in the $A_{1/2}$ amplitude, which is in strong disagreement with quark models that predict both transverse amplitudes to be strongly suppressed. For the $N(1680){5\\over 2}^+$ we observe a slow changeover from the dominance of the $A_{3/2}$ amplitude at the real photon point ($Q^2=0$) to a $Q^2$ where $A_{1/2}$ begins to dominate. The scalar amplitude $S_{1/2}$ drops rapidly with $Q^2$ consistent with quark model prediction. For the $N(1710){1\\over 2}^+$ resonance our analysis shows significant strength for the $A_{1/2}$ amplitude at $Q^2 < 2.5$ GeV$^2$.

  1. Measurements of $$ep \\to e^\\prime π^+n$$ at W = 1.6 - 2.0 GeV and extraction of nucleon resonance electrocouplings at CLAS

    DOE PAGESBeta

    Park, Kijun; Aznauryan, I. G.; Burkert, V. D.; Adhikari, K. P.; Amaryan, M. J.; Pereira, S. Anefalos; Avakian, H.; Battaglieri, M.; Badui, R.; Bedlinskiy, I.; et al

    2015-04-01

    Differential cross sections of the exclusive processmore » $$e p \\to e^\\prime \\pi^+ n$$ were measured with good precision in the range of the photon virtuality $Q^2 = 1.8 - 4.5$ GeV$^2$, and the invariant mass range of the $$\\pi^+ n$$ final state W = 1.6 - 2.0 GeV using the CEBAF Large Acceptance Spectrometer. Data were collected with nearly complete coverage in the azimuthal and polar angles of the $$n\\pi^+$$ center-of-mass system. More than 37,000 cross section points were measured. The contributions of the isospin $$I = {1\\over 2}$$ resonances $$N(1675){5\\over 2}^-$$, $$N(1680){5\\over 2}^+$$ and $$N(1710){1\\over 2}^+$$ were extracted at different values of $Q^2$ using a single-channel, energy-dependent resonance amplitude analysis. Two different approaches, the unitary isobar model and the fixed-$t$ dispersion relations, were employed in the analysis. We observe significant strength of the $$N(1675){5\\over 2}^-$$ in the $$A_{1/2}$$ amplitude, which is in strong disagreement with quark models that predict both transverse amplitudes to be strongly suppressed. For the $$N(1680){5\\over 2}^+$$ we observe a slow changeover from the dominance of the $$A_{3/2}$$ amplitude at the real photon point ($Q^2=0$) to a $Q^2$ where $$A_{1/2}$$ begins to dominate. The scalar amplitude $$S_{1/2}$$ drops rapidly with $Q^2$ consistent with quark model prediction. For the $$N(1710){1\\over 2}^+$$ resonance our analysis shows significant strength for the $$A_{1/2}$$ amplitude at $Q^2 < 2.5$ GeV$^2$.« less

  2. Coal liquefaction process streams characterization and evaluation. Characterization of coal-derived materials by field desorption mass spectrometry, two-dimensional nuclear magnetic resonance, supercritical fluid extraction, and supercritical fluid chromatography/mass spectrometry

    SciTech Connect

    Campbell, J.A.; Linehan, J.C.; Robins, W.H.

    1992-07-01

    Under contract from the DOE , and in association with CONSOL Inc., Battelle, Pacific Northwest Laboratory (PNL) evaluated four principal and several complementary techniques for the analysis of non-distillable direct coal liquefaction materials in support of process development. Field desorption mass spectrometry (FDMS) and nuclear magnetic resonance (NMR) spectroscopic methods were examined for potential usefulness as techniques to elucidate the chemical structure of residual (nondistillable) direct coal liquefaction derived materials. Supercritical fluid extraction (SFE) and supercritical fluid chromatography/mass spectrometry (SFC/MS) were evaluated for effectiveness in compound-class separation and identification of residual materials. Liquid chromatography (including microcolumn) separation techniques, gas chromatography/mass spectrometry (GC/MS), mass spectrometry/mass spectrometry (MS/MS), and GC/Fourier transform infrared (FTIR) spectroscopy methods were applied to supercritical fluid extracts. The full report authored by the PNL researchers is presented here. The following assessment briefly highlights the major findings of the project, and evaluates the potential of the methods for application to coal liquefaction materials. These results will be incorporated by CONSOL into a general overview of the application of novel analytical techniques to coal-derived materials at the conclusion of CONSOL`s contract.

  3. Head-to-Head Comparison of Ultra-High-Performance Liquid Chromatography with Diode Array Detection versus Quantitative Nuclear Magnetic Resonance for the Quantitative Analysis of the Silymarin Complex in Silybum marianum Fruit Extracts.

    PubMed

    Cheilari, Antigoni; Sturm, Sonja; Intelmann, Daniel; Seger, Christoph; Stuppner, Hermann

    2016-02-24

    Quantitative nuclear magnetic resonance (qNMR) spectroscopy is known as an excellent alternative to chromatography-based mixture analysis. NMR spectroscopy is a non-destructive method, needs only limited sample preparation, and can be readily automated. A head-to-head comparison of qNMR to an ultra-high-performance liquid chromatography with diode array detection (uHPLC-DAD)-based quantitative analysis of six flavonolignan congeners (silychristin, silydianin, silybin A, silybin B, isosilybin A, and isosilybin B) of the Silybum marianum silymarin complex is presented. Both assays showed similar performance characteristics (linear range, accuracy, precision, and limits of quantitation) with analysis times below 30 min/sample. The assays were applied to industrial S. marianum extracts (AC samples) and to extracts locally prepared from S. marianum fruits (PL samples). An assay comparison by Bland-Altman plots (relative method bias AC samples, -0.1%; 2SD range, ±5.1%; relative method bias PL samples, -0.3%; 2SD range, ±7.8%) and Passing-Bablok regression analysis (slope and intercept for AC and PL samples not significantly different from 1.00 and 0.00, respectively; Spearman's coefficient of rank correlation, >0.99) did show that qNMR and uHPLC-DAD can be used interchangeably to quantitate flavonolignans in the silymarin complex. PMID:26806429

  4. A comparative study of feature extraction and blind source separation of independent component analysis (ICA) on childhood brain tumour 1H magnetic resonance spectra.

    PubMed

    Hao, Jie; Zou, Xin; Wilson, Martin P; Davies, Nigel P; Sun, Yu; Peet, Andrew C; Arvanitis, Theodoros N

    2009-10-01

    Independent component analysis (ICA) has the potential of determining automatically the metabolite signals which make up MR spectra. However, the reliability with which this is accomplished and the optimal approach for investigating in vivo MRS have not been determined. Furthermore, the properties of ICA in brain tumour MRS with respect to dataset size and data quality have not been systematically explored. The two common techniques for applying ICA, blind source separation (BSS) and feature extraction (FE) were examined in this study using simulated data and the findings confirmed on patient data. Short echo time (TE 30 ms), low and high field (1.5 and 3 T) in vivo brain tumour MR spectra of childhood astrocytoma, ependymoma and medulloblastoma were generated by using a quantum mechanical simulator with ten metabolite and lipid components. Patient data (TE 30 ms, 1.5 T) were acquired from children with brain tumours. ICA of simulated data shows that individual metabolite components can be extracted from a set of MRS data. The BSS method generates independent components with a closer correlation to the original metabolite and lipid components than the FE method when the number of spectra in the dataset is small. The experiments also show that stable results are achieved with 300 MRS at an SNR equal to 10. The FE method is relatively insensitive to different ranges of full width at half maximum (FWHM) (from 0 to 3 Hz), whereas the BSS method degrades on increasing the range of FWHM. The peak frequency variations do not affect the results within the range of +/-0.08 ppm for the FE method, and +/-0.05 ppm for the BSS method. When the methods were applied to the patient dataset, results consistent with the synthesized experiments were obtained. PMID:19431141

  5. Detection of oligonucleotide hybridization at femtomolar level and sequence-specific gene analysis of the Arabidopsis thaliana leaf extract with an ultrasensitive surface plasmon resonance spectrometer

    PubMed Central

    Song, Fayi; Zhou, Feimeng; Wang, Jun; Tao, Nongjian; Lin, Jianqiao; Vellanoweth, Robert L.; Morquecho, Yvonne; Wheeler-Laidman, Janel

    2002-01-01

    A flow-injection (FI) device is combined, through the use of a low-volume (4 µl) flow cell, with an ultrasensitive surface plasmon resonance (SPR) spectrometer equipped with a bi-cell photodiode detector. The application of this novel FI–SPR device for sequence-specific ultratrace analysis of oligodeoxynucleotides (ODNs) and polydeoxynucleotides was demonstrated. Self-assembled monolayers of ODN probes are tethered onto Au films with a mercaptohexyl group at the 3′ ends. The FI–SPR provides a detection level (≤54 fM) 2–3 orders of magnitude lower than other SPR devices and compares well with several ultrasensitive detection methods for labeled DNA targets (e.g. fluorophore-tagged and radiolabeled DNA samples). The technique is also highly selective, since a 47mer ODN target with a single-base mismatch yielded a much smaller SPR signal, and a specific interaction was detected when the complementary target was present at 0.001% of the total DNA. The FI–SPR was extended to the measurement of two individual genes in a cDNA mixture transcribed from an Arabidopsis thaliana leaf mRNA pool. The greatly enhanced sensitivity not only obviates the necessity of DNA labeling, but also significantly reduces sample consumption, allowing direct quantification of low abundance mRNAs in cellular samples without amplification. PMID:12136120

  6. A derivatization strategy for the detection and identification of volatile trialkylphosphites using liquid chromatography-online solid phase extraction and offline nuclear magnetic resonance spectroscopy.

    PubMed

    Mazumder, Avik; Gutch, Pranav K; Dubey, Devendra K

    2015-05-01

    We demonstrate herein the application of selective derivatization method that converts volatile and labile trialkylphosphites (TAPs) into virtually non-volatile, thermally stable, and UV absorbing derivatives. After simple sample preparation, purification/enrichment of the derivatives was achieved by using high performance liquid chromatography (HPLC) coupled to on-line post column solid phase extraction (SPE) system. These derivatives were subjected to (31)P{(1)H} NMR and 1D-selTOCSY experiments. Conclusive identification was achieved on the basis of their HPLC retention time and NMR spectral signatures ( [Formula: see text] , (n)JH-H, and (3)JP-H). This method was tested for the unambiguous identification of a mixture containing low concentrations (∼10μgmL(-1)) of trimethylphosphite (TMP), triethylphosphite (TEP), triisopropylphosphite (TIP), and tributylphosphite (TBP) along with a high concentration of irrelevant background chemicals. It offered a high dynamic range and good detection limit and recovery (>75%) without the need for special NMR probe heads or exotic NMR experiments. PMID:25840658

  7. Damping of nanomechanical resonators.

    PubMed

    Unterreithmeier, Quirin P; Faust, Thomas; Kotthaus, Jörg P

    2010-07-01

    We study the transverse oscillatory modes of nanomechanical silicon nitride strings under high tensile stress as a function of geometry and mode index m≤9. Reproducing all observed resonance frequencies with classical elastic theory we extract the relevant elastic constants. Based on the oscillatory local strain we successfully predict the observed mode-dependent damping with a single frequency-independent fit parameter. Our model clarifies the role of tensile stress on damping and hints at the underlying microscopic mechanisms. PMID:20867737

  8. Optical resonator

    NASA Technical Reports Server (NTRS)

    Taghavi-Larigani, Shervin (Inventor); Vanzyl, Jakob J. (Inventor); Yariv, Amnon (Inventor)

    2006-01-01

    The invention discloses a semi-ring Fabry-Perot (SRFP) optical resonator structure comprising a medium including an edge forming a reflective facet and a waveguide within the medium, the waveguide having opposing ends formed by the reflective facet. The performance of the SRFP resonator can be further enhanced by including a Mach-Zehnder interferometer in the waveguide on one side of the gain medium. The optical resonator can be employed in a variety of optical devices. Laser structures using at least one SRFP resonator are disclosed where the resonators are disposed on opposite sides of a gain medium. Other laser structures employing one or more resonators on one side of a gain region are also disclosed.

  9. Resonance scraping

    SciTech Connect

    Collins, T.

    1986-06-01

    Protons lost in a ring leave at a few preferred locations, determined by some non-linear property of the dipoles. This paper suggests taking control of lost protons by beating the magnets at their own game - by means of a designed resonance used as a beam scraper. It is a study of suitable resonances, including estimates of the required multipole element strengths. The appropriate resonances are two-dimensional. A large number of figures is included.

  10. Fluorescence resonance energy transfer-based real-time polymerase chain reaction method without DNA extraction for the genotyping of F5, F2, F12, MTHFR, and HFE.

    PubMed

    Martinez-Serra, Jordi; Robles, Juan; Nicolàs, Antoni; Gutierrez, Antonio; Ros, Teresa; Amat, Juan Carlos; Alemany, Regina; Vögler, Oliver; Abelló, Aina; Noguera, Aina; Besalduch, Joan

    2014-01-01

    Blood samples are extensively used for the molecular diagnosis of many hematological diseases. The daily practice in a clinical laboratory of molecular diagnosis in hematology involves using a variety of techniques, based on the amplification of nucleic acids. Current methods for polymerase chain reaction (PCR) use purified genomic DNA, mostly isolated from total peripheral blood cells or white blood cells (WBC). In this paper we describe a real-time fluorescence resonance energy transfer-based method for genotyping directly from blood cells. Our strategy is based on an initial isolation of the WBCs, allowing the removal of PCR inhibitors, such as the heme group, present in the erythrocytes. Once the erythrocytes have been lysed, in the LightCycler(®) 2.0 Instrument, we perform a real-time PCR followed by a melting curve analysis for different genes (Factors 2, 5, 12, MTHFR, and HFE). After testing 34 samples comparing the real-time crossing point (CP) values between WBC (5×10(6) WBC/mL) and purified DNA (20 ng/μL), the results for F5 Leiden were as follows: CP mean value for WBC was 29.26±0.566 versus purified DNA 24.79±0.56. Thus, when PCR was performed from WBC (5×10(6) WBC/mL) instead of DNA (20 ng/μL), we observed a delay of about 4 cycles. These small differences in CP values were similar for all genes tested and did not significantly affect the subsequent analysis by melting curves. In both cases the fluorescence values were high enough, allowing a robust genotyping of all these genes without a previous DNA purification/extraction. PMID:25028568

  11. High-resolution PTP1B inhibition profiling combined with high-performance liquid chromatography-high-resolution mass spectrometry-solid-phase extraction-nuclear magnetic resonance spectroscopy: Proof-of-concept and antidiabetic constituents in crude extract of Eremophila lucida.

    PubMed

    Tahtah, Yousof; Wubshet, Sileshi G; Kongstad, Kenneth T; Heskes, Allison Maree; Pateraki, Irini; Møller, Birger Lindberg; Jäger, Anna K; Staerk, Dan

    2016-04-01

    Type 2 diabetes (T2D) constituted 90% of the global 387 million diabetes cases in 2014. The enzyme protein-tyrosine phosphatase 1B (PTP1B) has been recognized as a therapeutic target for treatment of T2D and its adverse complications. With the aim of accelerating the investigation of complex natural sources, such as crude plant extracts, for potential PTP1B inhibitors, we have developed a bio-analytical platform combining high-resolution PTP1B inhibition profiling and high-performance liquid chromatography-high-resolution mass spectrometry-solid-phase extraction-nuclear magnetic resonance spectroscopy, i.e., HR-bioassay/HPLC-HRMS-SPE-NMR. Human recombinant PTP1B enzyme was used for the microplate-based PTP1B inhibition assay, which was optimized for pH and substrate concentration to be compatible with rate measurements within the 10 min incubation time. Subsequently, analytical-scale HPLC-based microfractionation followed by colorimetric microplate-based PTP1B bioassaying enabled construction of a high-resolution inhibition profile corresponding to the HPLC profile. The high-resolution PTP1B inhibition profiling was validated using an artificial mixture of known PTP1B inhibitors and non-inhibiting compounds as negative controls. Finally, a proof-of-concept study with a real sample was performed using crude ethyl acetate extract of the phytochemically hitherto unexplored plant Eremophila lucida. This led to the identification of the first viscidane type diterpene, i.e., 5-hydroxyviscida-3,14-dien-20-oic acid (9) as PTP1B inhibitor with an IC50 value of 42.0 ± 5.9 μM. In addition, a series of flavonoids, i.e., luteolin (1), dinatin (3a), tricin (3b), 3,6-dimethoxyapigenin (4), jaceidin (5), and cirsimaritin (6) as well as a cembrene diterpene, (3Z, 7E, 11Z)-15-hydroxycembra-3,7,11-trien-19-oic acid (8), were also identified for the first time from E. lucida. PMID:26882973

  12. Discrete resonances

    NASA Astrophysics Data System (ADS)

    Vivaldi, Franco

    2015-12-01

    The concept of resonance has been instrumental to the study of Hamiltonian systems with divided phase space. One can also define such systems over discrete spaces, which have a finite or countable number of points, but in this new setting the notion of resonance must be re-considered from scratch. I review some recent developments in the area of arithmetic dynamics which outline some salient features of linear and nonlinear stable (elliptic) orbits over a discrete space, and also underline the difficulties that emerge in their analysis.

  13. Discrete resonances

    NASA Astrophysics Data System (ADS)

    Vivaldi, Franco

    The concept of resonance has been instrumental to the study of Hamiltonian systems with divided phase space. One can also define such systems over discrete spaces, which have a finite or countable number of points, but in this new setting the notion of resonance must be re-considered from scratch. I review some recent developments in the area of arithmetic dynamics which outline some salient features of linear and nonlinear stable (elliptic) orbits over a discrete space, and also underline the difficulties that emerge in their analysis.

  14. Laser Resonator

    NASA Technical Reports Server (NTRS)

    Harper, L. L. (Inventor)

    1983-01-01

    An optical resonator cavity configuration has a unitary mirror with oppositely directed convex and concave reflective surfaces disposed into one fold and concertedly reversing both ends of a beam propagating from a laser rod disposed between two total internal reflection prisms. The optical components are rigidly positioned with perpendicularly crossed virtual rooflines by a compact optical bed. The rooflines of the internal reflection prisms, are arranged perpendicularly to the axis of the laser beam and to the optical axes of the optical resonator components.

  15. Hadron Resonances from QCD

    NASA Astrophysics Data System (ADS)

    Dudek, Jozef J.

    2016-03-01

    I describe how hadron-hadron scattering amplitudes are related to the eigenstates of QCD in a finite cubic volume. The discrete spectrum of such eigenstates can be determined from correlation functions computed using lattice QCD, and the corresponding scattering amplitudes extracted. I review results from the Hadron Spectrum Collaboration who have used these finite volume methods to study ππ elastic scattering, including the ρ resonance, as well as coupled-channel πK, ηK scattering. The very recent extension to the case where an external current acts is also presented, considering the reaction πγ* → ππ, from which the unstable ρ → πγ transition form factor is extracted. Ongoing calculations are advertised and the outlook for finite volume approaches is presented.

  16. Beam transfer and extraction at LAMPF II

    SciTech Connect

    Colton, E.P.

    1983-01-01

    Protons will be single-turn extracted from the LAMPF II synchrotron at 30 Hz. On alternate pulses they will be single-turn injected into a storage ring. Both processes utilize fast kickers and Lambertson septum magnets. Half-integer resonant extraction will be used to slow-extract the beam from the storage ring over a time spread of 1/15 s. The slow extraction occurs using electrostatic wire and iron septa.

  17. Resonant Tunneling Spin Pump

    NASA Technical Reports Server (NTRS)

    Ting, David Z.

    2007-01-01

    The resonant tunneling spin pump is a proposed semiconductor device that would generate spin-polarized electron currents. The resonant tunneling spin pump would be a purely electrical device in the sense that it would not contain any magnetic material and would not rely on an applied magnetic field. Also, unlike prior sources of spin-polarized electron currents, the proposed device would not depend on a source of circularly polarized light. The proposed semiconductor electron-spin filters would exploit the Rashba effect, which can induce energy splitting in what would otherwise be degenerate quantum states, caused by a spin-orbit interaction in conjunction with a structural-inversion asymmetry in the presence of interfacial electric fields in a semiconductor heterostructure. The magnitude of the energy split is proportional to the electron wave number. Theoretical studies have suggested the possibility of devices in which electron energy states would be split by the Rashba effect and spin-polarized currents would be extracted by resonant quantum-mechanical tunneling.

  18. Resonant behavior of dielectric objects (electrostatic resonances).

    PubMed

    Fredkin, D R; Mayergoyz, I D

    2003-12-19

    Resonant behavior of dielectric objects occurs at certain frequencies for which the object permittivity is negative and the free-space wavelength is large in comparison with the object dimensions. Unique physical features of these resonances are studied and a novel technique for the calculation of resonance values of permittivity, and hence resonance frequencies, is proposed. Scale invariance of resonance frequencies, unusually strong orthogonality properties of resonance modes, and a two-dimensional phenomenon of "twin" spectra are reported. The paper concludes with brief discussions of optical controllability of these resonances in semiconductor nanoparticles and a plausible, electrostatic resonance based, mechanism for nucleation and formation of ball lightning. PMID:14754117

  19. Disentangling the Dynamical Origin of P11 Nucleon Resonances

    SciTech Connect

    Nobuhiko Suzuki, Bruno Julia Diaz, Hiroyuki Kamano, Tsung-Shung Lee, Akihiko Matsuyama, Toru Sato

    2010-01-01

    The dynamical origins of the two poles associated with the Roper resonance are examined. Both of them together with the next higher resonance in the P11 partial wave are found to have the same originating bare state, indicating that the coupling to the meson-baryon continuum induces multiple observed resonances from the same bare state. Concerning other partial waves, the resonance poles extracted within the same multi-channels multi-resonances model of pi N reactions are compared to those listed by the Particle Data Group (PDG). Within our reaction model, all the identified resonances consist of a core state and meson-baryon components.

  20. If It's Resonance, What is Resonating?

    ERIC Educational Resources Information Center

    Kerber, Robert C.

    2006-01-01

    The phenomenon under the name "resonance," which, is based on the mathematical analogy between mechanical resonance and the behavior of wave functions in quantum mechanical exchange phenomena was described. The resonating system does not have a structure intermediate between those involved in the resonance, but instead a structure which is further…

  1. Accurate Extraction of Nanometer Distances in Multimers by Pulse EPR

    PubMed Central

    Valera, Silvia; Ackermann, Katrin; Pliotas, Christos; Huang, Hexian; Naismith, James H.

    2016-01-01

    Abstract Pulse electron paramagnetic resonance (EPR) is gaining increasing importance in structural biology. The PELDOR (pulsed electron–electron double resonance) method allows extracting distance information on the nanometer scale. Here, we demonstrate the efficient extraction of distances from multimeric systems such as membrane‐embedded ion channels where data analysis is commonly hindered by multi‐spin effects. PMID:26865468

  2. Direct measurement of the intrinsic linewidth of a resonant state

    NASA Astrophysics Data System (ADS)

    Kobos, Zachary; Reed, Mark

    2015-03-01

    We have applied inelastic electron tunneling spectroscopy (IETS) techniques to a resonantly-coupled system to determine quantitative differences in resonant versus non-resonant IETS. We use as a model system a set of GaAs-AlGaAs resonant tunneling diodes (RTDs)(footnote: with different barrier widths to tune resonant state linewidths and transmission coefficients. Modulation-broadening studies confirm theoretical predictions; however, the thermal dependence is markedly different than expected from classical IETS theory. An analysis of resonance shut-off reveals that the thermal dependence reflects the thermal broadening of the injector and resonant state density of states. Using this analysis, we show that one can extract both the transmission coefficient and the intrinsic linewidth of the resonant state. This is compared for RTDs of different tunneling barrier widths, and we observe the expected increase in resonance width for thinner barriers. This work was supported by the National Science Foundation.

  3. Slow extraction from the Fermilab Main Injector

    SciTech Connect

    Craig D. Moore et al.

    2001-07-20

    Slow resonant extraction from the Fermilab Main Injector through the extraction channel was achieved in February, 2000, with a spill length of 0.3 sec. Beam losses were small. Excellent wire chamber profiles were obtained and analyzed. The duty factor was not very good and needs to be improved.

  4. Resonances in pi-K scattering

    SciTech Connect

    Wilson, David J.

    2014-06-23

    We have obtained clear signals of resonances in coupled-channel pi K - eta K scattering. Using distillation and a large basis of operators we are able to extract a precise spectrum of energy levels using the variational method. These energies are analysed using inelastic extensions of the Luescher method to obtain scattering amplitudes that clearly describe S, P and D wave resonances, corresponding to the physical K_0^*(1430), the K^*(892) and the K_2^*(1430).

  5. Microwave energy storage in resonant cavities

    SciTech Connect

    Alvarez, R.A.

    1983-02-01

    One method of generating short, high-power microwave pulses is to store rf energy in a resonant cavity over a relatively long fill time and extract is rapidly. A power gain roughly equal to the ratio of fill time to extraction time can be obtained. During the filling of a resonant cavity some of the energy is lost in heating the cavity walls, and some will generally be reflected at the input coupling of the cavity. In this paper we discuss the time dependence of the stored energy and related quantities and the way in which it depends on the coupling of the source to the cavity.

  6. Probabilistic interpretation of compositeness relation for resonances

    NASA Astrophysics Data System (ADS)

    Guo, Zhi-Hui; Oller, J. A.

    2016-05-01

    Bound, antibound and resonance states are associated to poles in the on-shell partial wave amplitudes. We show here that from the residues of the pole a rank 1 projection operator associated with any of these states can be extracted, in terms of which a sum rule related to the composition of the state can be derived. Although typically it involves complex coefficients for the compositeness and elementariness, except for the bound state case, we demonstrate that one can formulate a meaningful compositeness relation with only positive coefficients for resonances whose associated Laurent series in the variable s converges in a region of the physical axis around Re sP , with sP the pole position of the resonance. It is also shown that this result can be considered as an analytical extrapolation in sP of the clear narrow resonance case. We exemplify this formalism to study the two-body components of several resonances of interest.

  7. Regenerative feedback resonant circuit

    DOEpatents

    Jones, A. Mark; Kelly, James F.; McCloy, John S.; McMakin, Douglas L.

    2014-09-02

    A regenerative feedback resonant circuit for measuring a transient response in a loop is disclosed. The circuit includes an amplifier for generating a signal in the loop. The circuit further includes a resonator having a resonant cavity and a material located within the cavity. The signal sent into the resonator produces a resonant frequency. A variation of the resonant frequency due to perturbations in electromagnetic properties of the material is measured.

  8. MARS Tracking Simulations for the Mu2e Slow Extracted Proton Beam

    SciTech Connect

    Nagaslaev, Vladimir; Rakhno, Igor

    2015-06-01

    Particle tracking taking into account interactions with fields and materials is necessary for proper evaluation of the resonant extraction losses and geometry optimization for the extraction beam line. This paper describes the tracking simulations for the Mu2e Resonant Extraction and discusses the geometry choices made based on these simulations.

  9. Measuring frequency response of surface-micromachined resonators

    NASA Astrophysics Data System (ADS)

    Cowan, William D.; Bright, Victor M.; Dalton, George C.

    1997-09-01

    Resonator structures offer a unique mechanism for characterizing MEMS materials, but measuring the resonant frequency of microstructures is challenging. In this effort a network analyzer system was used to electrically characterize surface-micromachined resonator structures in a carefully controlled pressure and temperature environment.A microscope laser interferometer was used to confirm actual device deflections.Cantilever, comb, and piston resonators fabricated in the DARPA-sponsored MUMPs process were extensively tested. Measured resonator frequency results show reasonable agreement with analytic predictions computed using manufacturer measured film thickness and residual material stress. Alternatively the measured resonant frequency data can be used to extract materials data. Tuning of resonant frequency with DC bias was also investigated. Because the tested devices vary widely in complexity, form a simple cantilever beam to a comb resonator, the data collected is especially well suited for validation testing of MEMS modeling codes.

  10. A combination strategy for extraction and isolation of multi-component natural products by systematic two-phase solvent extraction-(13)C nuclear magnetic resonance pattern recognition and following conical counter-current chromatography separation: Podophyllotoxins and flavonoids from Dysosma versipellis (Hance) as examples.

    PubMed

    Yang, Zhi; Wu, Youqian; Wu, Shihua

    2016-01-29

    Despite of substantial developments of extraction and separation techniques, isolation of natural products from natural resources is still a challenging task. In this work, an efficient strategy for extraction and isolation of multi-component natural products has been successfully developed by combination of systematic two-phase liquid-liquid extraction-(13)C NMR pattern recognition and following conical counter-current chromatography separation. A small-scale crude sample was first distributed into 9 systematic hexane-ethyl acetate-methanol-water (HEMWat) two-phase solvent systems for determination of the optimum extraction solvents and partition coefficients of the prominent components. Then, the optimized solvent systems were used in succession to enrich the hydrophilic and lipophilic components from the large-scale crude sample. At last, the enriched components samples were further purified by a new conical counter-current chromatography (CCC). Due to the use of (13)C NMR pattern recognition, the kinds and structures of major components in the solvent extracts could be predicted. Therefore, the method could collect simultaneously the partition coefficients and the structural information of components in the selected two-phase solvents. As an example, a cytotoxic extract of podophyllotoxins and flavonoids from Dysosma versipellis (Hance) was selected. After the systematic HEMWat system solvent extraction and (13)C NMR pattern recognition analyses, the crude extract of D. versipellis was first degreased by the upper phase of HEMWat system (9:1:9:1, v/v), and then distributed in the two phases of the system of HEMWat (2:8:2:8, v/v) to obtain the hydrophilic lower phase extract and lipophilic upper phase extract, respectively. These extracts were further separated by conical CCC with the HEMWat systems (1:9:1:9 and 4:6:4:6, v/v). As results, total 17 cytotoxic compounds were isolated and identified. In general, whole results suggested that the strategy was very

  11. Detection of kestoses and kestose-related oligosaccharides in extracts of Festuca arundinacea, Dactylis glomerate L. , and Asparagus officinalis L. root cultures and invertase by sup 13 C and sup 1 H nuclear magnetic resonance spectroscopy

    SciTech Connect

    Forsythe, K.L.; Feather, M.S.; Gracz, H.; Wong, T.C. )

    1990-04-01

    Previous studies show that {sup 13}C nuclear magnetic resonance spectroscopy can be used to detect and identify mixtures of 1-kestose and neokestose after conversion to the acetate derivatives. In this study, unequivocal assignments are made for the anomeric carbon and proton signals for the above two trisaccharide acetates as well as for 6-kestose hendecaacetate and for nystose tetradecaacetate (a 1-kestose-derived tetrasaccharide). A number of oligosaccharide fractions were isolated from several plant species, converted to the acetates, and nuclear magnetic resonance spectra obtained. Using the above reference data, the following information was obtained. The trisaccharide fraction from Dactylis gomerata L. stem tissue and Asparagus officinalis L. roots contain both 1-kestose and neokestose, and the tetrasaccharide fractions contain three components, one of which is nystose. Penta- and hexasaccharide acetates were also isolated from A. officinalis L. roots and were found to contain, respectively, four and at least five components. All components of both of the above species appear to contain a kestose residue and to be produced by the sequential addition of fructofuranosyl units to these. The trisaccharide fraction from Festuca arundinacea is complex, and contains at least five different components, two of which appear to be 1-kestose and neokestose.

  12. Automated protein NMR resonance assignments.

    PubMed

    Wan, Xiang; Xu, Dong; Slupsky, Carolyn M; Lin, Guohui

    2003-01-01

    NMR resonance peak assignment is one of the key steps in solving an NMR protein structure. The assignment process links resonance peaks to individual residues of the target protein sequence, providing the prerequisite for establishing intra- and inter-residue spatial relationships between atoms. The assignment process is tedious and time-consuming, which could take many weeks. Though there exist a number of computer programs to assist the assignment process, many NMR labs are still doing the assignments manually to ensure quality. This paper presents (1) a new scoring system for mapping spin systems to residues, (2) an automated adjacency information extraction procedure from NMR spectra, and (3) a very fast assignment algorithm based on our previous proposed greedy filtering method and a maximum matching algorithm to automate the assignment process. The computational tests on 70 instances of (pseudo) experimental NMR data of 14 proteins demonstrate that the new score scheme has much better discerning power with the aid of adjacency information between spin systems simulated across various NMR spectra. Typically, with automated extraction of adjacency information, our method achieves nearly complete assignments for most of the proteins. The experiment shows very promising perspective that the fast automated assignment algorithm together with the new score scheme and automated adjacency extraction may be ready for practical use. PMID:16452794

  13. Bevalac extraction

    SciTech Connect

    Kalnins, J.G.; Krebs, G.; Tekawa, M.; Cowles, D.; Byrne, T.

    1992-02-01

    This report will describe some of the general features of the Bevatron extraction system, primarily the dependence of the beam parameters and extraction magnet currents on the Bevalac field. The extraction magnets considered are: PFW, XPl, XP2, XS1, XS2, XM1, XM2, XM3, XQ3A and X03B. This study is based on 84 past tunes (from 1987 to the present) of various ions (p,He,O,Ne,Si,S,Ar,Ca,Ti,Fe,Nb,La,Au and U), for Bevalac fields from 1.749 to 12.575 kG, where all tunes included a complete set of beam line wire chamber pictures. The circulating beam intensity inside the Bevalac is measured with Beam Induction Electrodes (BIE) in the South Tangent Tank. The extracted beam intensity is usually measured with the Secondary Emission Monitor (SEM) in the F1-Box. For most of the tunes the extraction efficiency, as given by the SEM/BIE ratio, was not recorded in the MCR Log Book, but plotting the available Log Book data as a function of the Bevalac field, see Fig.9, we find that the extraction efficiency is typically between 30->60% with feedback spill.

  14. Fluid extraction

    DOEpatents

    Wai, Chien M.; Laintz, Kenneth E.

    1999-01-01

    A method of extracting metalloid and metal species from a solid or liquid material by exposing the material to a supercritical fluid solvent containing a chelating agent is described. The chelating agent forms chelates that are soluble in the supercritical fluid to allow removal of the species from the material. In preferred embodiments, the extraction solvent is supercritical carbon dioxide and the chelating agent is a fluorinated .beta.-diketone. In especially preferred embodiments the extraction solvent is supercritical carbon dioxide, and the chelating agent comprises a fluorinated .beta.-diketone and a trialkyl phosphate, or a fluorinated .beta.-diketone and a trialkylphosphine oxide. Although a trialkyl phosphate can extract lanthanides and actinides from acidic solutions, a binary mixture comprising a fluorinated .beta.-diketone and a trialkyl phosphate or a trialkylphosphine oxide tends to enhance the extraction efficiencies for actinides and lanthanides. The method provides an environmentally benign process for removing contaminants from industrial waste without using acids or biologically harmful solvents. The method is particularly useful for extracting actinides and lanthanides from acidic solutions. The chelate and supercritical fluid can be regenerated, and the contaminant species recovered, to provide an economic, efficient process.

  15. Cavity- and waveguide-resonators in electron paramagnetic resonance, nuclear magnetic resonance, and magnetic resonance imaging.

    PubMed

    Webb, Andrew

    2014-11-01

    Cavity resonators are widely used in electron paramagnetic resonance, very high field magnetic resonance microimaging and also in high field human imaging. The basic principles and designs of different forms of cavity resonators including rectangular, cylindrical, re-entrant, cavity magnetrons, toroidal cavities and dielectric resonators are reviewed. Applications in EPR and MRI are summarized, and finally the topic of traveling wave MRI using the magnet bore as a waveguide is discussed. PMID:25456314

  16. Magnetic resonance of slotted circular cylinder resonators

    NASA Astrophysics Data System (ADS)

    Du, Junjie; Liu, Shiyang; Lin, Zhifang; Chui, S. T.

    2008-07-01

    By a rigorous full-wave approach, a systemic study is made on the magnetic resonance of slotted circular cylinder resonators (SCCRs) made of a perfect conductor for the lossless case. This is a two-dimensional analog of the split-ring resonator and may serve as an alternative type of essential constituent of electromagnetic metamaterials. It is found that the resonance frequency can be modulated by changing the geometrical parameters and the dielectrics filling in the cavity and the slot. An approximate empirical expression is presented for magnetic resonance frequency of SCCRs from the viewpoint of an L-C circuit system. Finally, it is demonstrated that the SCCR structure can be miniaturized to less than 1/150 resonant wavelength in size with the dielectrics available currently.

  17. Narrowband feedback for narrowband control of resonant and non-resonant vibration

    NASA Astrophysics Data System (ADS)

    Kim, Sang-Myeong; Brennan, Michael J.; Abreu, Gustavo L. C. M.

    2016-08-01

    This paper presents a simple feedback methodology that uses second order filters to control narrowband resonant and non-resonant vibration of a structural system. In particular, a single degree-of-freedom system is studied throughout the paper. The idea of the methodology is based on the fact that direct feedback is effective for in-phase vibration control. Thus, the position, velocity and acceleration are respectively fed back to control the low, resonant and high frequency vibration of the system. Each of these is passed through a band pass filter of second order that is inserted to extract and feed back the in-phase signal component only. This is called narrowband feedback. It is demonstrated with experiments that narrowband feedback is useful for narrowband control of resonant and non-resonant vibration.

  18. High-Field Electron Paramagnetic Resonance and Density Functional Theory Study of Stable Organic Radicals in Lignin: Influence of the Extraction Process, Botanical Origin, and Protonation Reactions on the Radical g Tensor.

    PubMed

    Bährle, Christian; Nick, Thomas U; Bennati, Marina; Jeschke, Gunnar; Vogel, Frédéric

    2015-06-18

    The radical concentrations and g factors of stable organic radicals in different lignin preparations were determined by X-band EPR at 9 GHz. We observed that the g factors of these radicals are largely determined by the extraction process and not by the botanical origin of the lignin. The parameter mostly influencing the g factor is the pH value during lignin extraction. This effect was studied in depth using high-field EPR spectroscopy at 263 GHz. We were able to determine the gxx, gyy, and gzz components of the g tensor of the stable organic radicals in lignin. With the enhanced resolution of high-field EPR, distinct radical species could be found in this complex polymer. The radical species are assigned to substituted o-semiquinone radicals and can exist in different protonation states SH3+, SH2, SH1-, and S2-. The proposed model structures are supported by DFT calculations. The g principal values of the proposed structure were all in reasonable agreement with the experiments. PMID:25978006

  19. Unstable resonators with excited converging wave

    SciTech Connect

    Hodgson, N. ); Weber, H. )

    1990-04-01

    This paper reports the properties of unstable resonators with an additional mirror inside or outside the resonator investigated, both experimentally and theoretically. The additional mirror excites the converging wave, and by this, output coupling is decreased without affecting beam quality. Experiments were performed with a pulsed Nd:YAG system. The theoretical model was based on the coupled Kirchhoff integrals and solved numerically. Agreement between theory and experiments indicates that this kind of resonator provides high focusability and maximum extraction efficiency simultaneously, even with low-gain media. This enables one to apply unstable resonators to solid-state lasers with low small-signal gain, like alexandrite or CW-pumped Nd:YAG.

  20. Two-color resonant filamentation in gases

    NASA Astrophysics Data System (ADS)

    Doussot, J.; Béjot, P.; Faucher, O.

    2016-07-01

    In this paper, it is shown that two-photon resonance involving a fundamental field and one of its odd harmonic strongly influences the filamentation process, i.e., the nonlinear propagation of an ultrashort and ultraintense laser field. This particular situation happens, for instance, when a 400 nm fundamental field propagates together with its third harmonic in krypton. Using three-dimensional ab initio calculations, the optical response of krypton is evaluated and the underlying nonlinear refractive indices are extracted. It is found that the resonance also exacerbates higher-order nonlinear processes. Injecting the retrieved higher-order Kerr indices in a nonlinear propagation solver, it is found that the resonance leads to an enhanced defocusing cross-phase modulation that strongly participates to the filament stabilization. This work sheds a light on the mechanism of filamentation, in particular, in the ultraviolet range, where two-color two-photon resonances are expected to occur in many atomic gases.

  1. Simple method for locking birefringent resonators.

    PubMed

    Libson, Adam; Brown, Nicolas; Buikema, Aaron; López, Camilo Cela; Dordevic, Tamara; Heising, Matthew; Evans, Matthew

    2015-02-01

    We report on a simple method of locking a laser to a birefringent cavity using polarization spectroscopy. The birefringence of the resonator permits the simple extraction of an error signal by using one polarization state as a phase reference for another state. No modulation of the light or the resonator is required, reducing the complexity of the laser locking setup. This method of producing an error signal can be used on most birefringent optical resonators, even if the details of birefringence and eigenpolarizations are not known. This technique is particularly well suited for fiber ring resonators due to the inherent birefringence of the fiber and the unknown nature of that birefringence. We present an experimental demonstration of this technique using a fiber ring. PMID:25836232

  2. Extractant composition

    DOEpatents

    Smith, Barbara F.; Jarvinen, Gordon D.; Ryan, Robert R.

    1990-01-01

    An organic extracting solution useful for separating elements of the actinide series of the periodic table from elements of the lanthanide series, where both are in trivalent form. The extracting solution consists of a primary ligand and a secondary ligand, preferably in an organic solvent. The primary ligand is a substituted monothio-1,3-dicarbonyl, which includes a substituted 4-acyl-2-pyrazolin-5-thione, such as 4-benzoyl-2,4-dihydro-5-methyl-2-phenyl-3H-pyrazol-3-thione (BMPPT). The secondary ligand is a substituted phosphine oxide, such as trioctylphosphine oxide (TOPO).

  3. Integral resonator gyroscope

    NASA Technical Reports Server (NTRS)

    Shcheglov, Kirill V. (Inventor); Challoner, A. Dorian (Inventor); Hayworth, Ken J. (Inventor); Wiberg, Dean V. (Inventor); Yee, Karl Y. (Inventor)

    2008-01-01

    The present invention discloses an inertial sensor having an integral resonator. A typical sensor comprises a planar mechanical resonator for sensing motion of the inertial sensor and a case for housing the resonator. The resonator and a wall of the case are defined through an etching process. A typical method of producing the resonator includes etching a baseplate, bonding a wafer to the etched baseplate, through etching the wafer to form a planar mechanical resonator and the wall of the case and bonding an end cap wafer to the wall to complete the case.

  4. Resonant cortical dynamics of speech perception

    NASA Astrophysics Data System (ADS)

    Grossberg, Stephen

    2003-04-01

    What is the neural representation of a speech code as it evolves in time? How do listeners integrate temporally distributed phonemic information into coherent representations of syllables and words? How does the brain extract invariant properties of variable-rate speech? This talk describes a neural model that suggests answers to these questions, while quantitatively simulating speech and word recognition data. The conscious speech and word recognition code is suggested to be a resonant wave, and a percept of silence a temporal discontinuity in the rate that resonance evolves. A resonant wave emerges when sequential activation and storage of phonemic items in working memory provides bottom-up input to list chunks that group together sequences of items of variable length. The list chunks compete and winning chunks activate top-down expectations that amplify and focus attention on consistent working memory items, while suppressing inconsistent ones. The ensuing resonance boosts activation levels of selected items and chunks. Because resonance occurs after working memory activation, it can incorporate information presented after intervening silence intervals, so future sounds can influence how we hear past sounds. The model suggests that resonant dynamics enable the brain to learn quickly without suffering catastrophic forgetting, as described within Adaptive Resonance Theory.

  5. Extractable resources

    NASA Technical Reports Server (NTRS)

    1975-01-01

    The use of information from space systems in the operation of extractive industries, particularly in exploration for mineral and fuel resources was reviewed. Conclusions and recommendations reported are based on the fundamental premise that survival of modern industrial society requires a continuing secure flow of resources for energy, construction and manufacturing, and for use as plant foods.

  6. Nanomechanical resonance detector

    DOEpatents

    Grossman, Jeffrey C; Zettl, Alexander K

    2013-10-29

    An embodiment of a nanomechanical frequency detector includes a support structure and a plurality of elongated nanostructures coupled to the support structure. Each of the elongated nanostructures has a particular resonant frequency. The plurality of elongated nanostructures has a range of resonant frequencies. An embodiment of a method of identifying an object includes introducing the object to the nanomechanical resonance detector. A resonant response by at least one of the elongated nanostructures of the nanomechanical resonance detector indicates a vibrational mode of the object. An embodiment of a method of identifying a molecular species of the present invention includes introducing the molecular species to the nanomechanical resonance detector. A resonant response by at least one of the elongated nanostructures of the nanomechanical resonance detector indicates a vibrational mode of the molecular species.

  7. Neutron resonance averaging

    SciTech Connect

    Chrien, R.E.

    1986-10-01

    The principles of resonance averaging as applied to neutron capture reactions are described. Several illustrations of resonance averaging to problems of nuclear structure and the distribution of radiative strength in nuclei are provided. 30 refs., 12 figs.

  8. Analysis and calibration techniques for superconducting resonators

    NASA Astrophysics Data System (ADS)

    Cataldo, Giuseppe; Wollack, Edward J.; Barrentine, Emily M.; Brown, Ari D.; Moseley, S. Harvey; U-Yen, Kongpop

    2015-01-01

    A method is proposed and experimentally explored for in-situ calibration of complex transmission data for superconducting microwave resonators. This cryogenic calibration method accounts for the instrumental transmission response between the vector network analyzer reference plane and the device calibration plane. Once calibrated, the observed resonator response is analyzed in detail by two approaches. The first, a phenomenological model based on physically realizable rational functions, enables the extraction of multiple resonance frequencies and widths for coupled resonators without explicit specification of the circuit network. In the second, an ABCD-matrix representation for the distributed transmission line circuit is used to model the observed response from the characteristic impedance and propagation constant. When used in conjunction with electromagnetic simulations, the kinetic inductance fraction can be determined with this method with an accuracy of 2%. Datasets for superconducting microstrip and coplanar-waveguide resonator devices were investigated and a recovery within 1% of the observed complex transmission amplitude was achieved with both analysis approaches. The experimental configuration used in microwave characterization of the devices and self-consistent constraints for the electromagnetic constitutive relations for parameter extraction are also presented.

  9. Analysis and calibration techniques for superconducting resonators.

    PubMed

    Cataldo, Giuseppe; Wollack, Edward J; Barrentine, Emily M; Brown, Ari D; Moseley, S Harvey; U-Yen, Kongpop

    2015-01-01

    A method is proposed and experimentally explored for in-situ calibration of complex transmission data for superconducting microwave resonators. This cryogenic calibration method accounts for the instrumental transmission response between the vector network analyzer reference plane and the device calibration plane. Once calibrated, the observed resonator response is analyzed in detail by two approaches. The first, a phenomenological model based on physically realizable rational functions, enables the extraction of multiple resonance frequencies and widths for coupled resonators without explicit specification of the circuit network. In the second, an ABCD-matrix representation for the distributed transmission line circuit is used to model the observed response from the characteristic impedance and propagation constant. When used in conjunction with electromagnetic simulations, the kinetic inductance fraction can be determined with this method with an accuracy of 2%. Datasets for superconducting microstrip and coplanar-waveguide resonator devices were investigated and a recovery within 1% of the observed complex transmission amplitude was achieved with both analysis approaches. The experimental configuration used in microwave characterization of the devices and self-consistent constraints for the electromagnetic constitutive relations for parameter extraction are also presented. PMID:25638068

  10. An Inexpensive Resonance Demonstration

    ERIC Educational Resources Information Center

    Dukes, Phillip

    2005-01-01

    The phenomenon of resonance is applicable to almost every branch of physics. Without resonance, there wouldn't be televisions or stereos, or even swings on the playground. However, resonance also has undesirable side effects such as irritating noises in the car and the catastrophic events such as helicopters flying apart. In this article, the…

  11. Nuclear Magnetic Resonance

    NASA Astrophysics Data System (ADS)

    Andrew, E. R.

    2009-06-01

    Author's preface; 1. Introduction; 2. Basic theory; 3. Experimental methods; 4. Measurement of nuclear properties and general physical applications; 5. Nuclear magnetic resonance in liquids and gases; 6. Nuclear magnetic resonance in non-metallic solids; 7. Nuclear magnetic resonance in metals; 8. Quadrupole effects; Appendices 1-6; Glossary of symbols; Bibliography and author index; Subject index.

  12. Magnetic Resonance Imaging (MRI)

    MedlinePlus

    ... How Can I Help a Friend Who Cuts? Magnetic Resonance Imaging (MRI) KidsHealth > For Teens > Magnetic Resonance Imaging (MRI) Print A A A Text Size What's ... Exam Safety Getting Your Results What Is MRI? Magnetic resonance imaging (MRI) is a type of safe, painless testing ...

  13. Photoacoustic resonance spectroscopy for biological tissue characterization

    NASA Astrophysics Data System (ADS)

    Gao, Fei; Feng, Xiaohua; Zheng, Yuanjin; Ohl, Claus-Dieter

    2014-06-01

    By "listening to photons," photoacoustics allows the probing of chromosomes in depth beyond the optical diffusion limit. Here we report the photoacoustic resonance effect induced by multiburst modulated laser illumination, which is theoretically modeled as a damped mass-string oscillator and a resistor-inductor-capacitor (RLC) circuit. Through sweeping the frequency of multiburst modulated laser, the photoacoustic resonance effect is observed experimentally on phantoms and porcine tissues. Experimental results demonstrate different spectra for each phantom and tissue sample to show significant potential for spectroscopic analysis, fusing optical absorption and mechanical vibration properties. Unique RLC circuit parameters are extracted to quantitatively characterize phantom and biological tissues.

  14. Photoacoustic resonance spectroscopy for biological tissue characterization.

    PubMed

    Gao, Fei; Feng, Xiaohua; Zheng, Yuanjin; Ohl, Claus-Dieter

    2014-06-01

    By "listening to photons," photoacoustics allows the probing of chromosomes in depth beyond the optical diffusion limit. Here we report the photoacoustic resonance effect induced by multiburst modulated laser illumination, which is theoretically modeled as a damped mass-string oscillator and a resistor-inductor-capacitor (RLC) circuit. Through sweeping the frequency of multiburst modulated laser, the photoacoustic resonance effect is observed experimentally on phantoms and porcine tissues. Experimental results demonstrate different spectra for each phantom and tissue sample to show significant potential for spectroscopic analysis, fusing optical absorption and mechanical vibration properties. Unique RLC circuit parameters are extracted to quantitatively characterize phantom and biological tissues. PMID:24928154

  15. URANIUM EXTRACTION

    DOEpatents

    Harrington, C.D.; Opie, J.V.

    1958-07-01

    The recovery of uranium values from uranium ore such as pitchblende is described. The ore is first dissolved in nitric acid, and a water soluble nitrate is added as a salting out agent. The resulting feed solution is then contacted with diethyl ether, whereby the bulk of the uranyl nitrate and a portion of the impurities are taken up by the ether. This acid ether extract is then separated from the aqueous raffinate, and contacted with water causing back extractioa of the uranyl nitrate and impurities into the water to form a crude liquor. After separation from the ether extract, this crude liquor is heated to about 118 deg C to obtain molten uranyl nitrate hexahydratc. After being slightly cooled the uranyl nitrate hexahydrate is contacted with acid free diethyl ether whereby the bulk of the uranyl nitrate is dissolved into the ethcr to form a neutral ether solution while most of the impurities remain in the aqueous waste. After separation from the aqueous waste, the resultant ether solution is washed with about l0% of its volume of water to free it of any dissolved impurities and is then contacted with at least one half its volume of water whereby the uranyl nitrate is extracted into the water to form an aqueous product solution.

  16. Ovenized microelectromechanical system (MEMS) resonator

    SciTech Connect

    Olsson, Roy H; Wojciechowski, Kenneth; Kim, Bongsang

    2014-03-11

    An ovenized micro-electro-mechanical system (MEMS) resonator including: a substantially thermally isolated mechanical resonator cavity; a mechanical oscillator coupled to the mechanical resonator cavity; and a heating element formed on the mechanical resonator cavity.

  17. Optical Helmholtz resonators

    NASA Astrophysics Data System (ADS)

    Chevalier, Paul; Bouchon, Patrick; Haïdar, Riad; Pardo, Fabrice

    2014-08-01

    Helmholtz resonators are widely used acoustic components able to select a single frequency. Here, based on an analogy between acoustics and electromagnetism wave equations, we present an electromagnetic 2D Helmholtz resonator made of a metallic slit-box structure. At the resonance, the light is funneled in the λ/800 apertures, and is subsequently absorbed in the cavity. As in acoustics, there is no higher order of resonance, which is an appealing feature for applications such as photodetection or thermal emission. Eventually, we demonstrate that the slit is of capacitive nature while the box behaves inductively. We derive an analytical formula for the resonance wavelength, which does not rely on wave propagation and therefore does not depend on the permittivity of the material filling the box. Besides, in contrast with half-wavelength resonators, the resonance wavelength can be engineered by both the slit aspect ratio and the box area.

  18. Contrasting Extraction Types.

    ERIC Educational Resources Information Center

    Postal, Paul M.

    1994-01-01

    This paper grounds a novel typology yielding three major types of English (L(eft)-extraction, defined by their relationship to resumptive pronouns (RPs): (1) B-extractions, which require RPs in their extraction sites, (2) A1-extractions, which allow RPs in their extraction sites, and (3) A2-extractions, which forbid RPs in their extraction sites.…

  19. Magnetic resonance energy and topological resonance energy.

    PubMed

    Aihara, Jun-Ichi

    2016-04-28

    Ring-current diamagnetism of a polycyclic π-system is closely associated with thermodynamic stability due to the individual circuits. Magnetic resonance energy (MRE), derived from the ring-current diamagnetic susceptibility, was explored in conjunction with graph-theoretically defined topological resonance energy (TRE). For many aromatic molecules, MRE is highly correlative with TRE with a correlation coefficient of 0.996. For all π-systems studied, MRE has the same sign as TRE. The only trouble with MRE may be that some antiaromatic and non-alternant species exhibit unusually large MRE-to-TRE ratios. This kind of difficulty can in principle be overcome by prior geometry-optimisation or by changing spin multiplicity. Apart from the semi-empirical resonance-theory resonance energy, MRE is considered as the first aromatic stabilisation energy (ASE) defined without referring to any hypothetical polyene reference. PMID:26878709

  20. Resonance splitting in gyrotropic ring resonators.

    PubMed

    Jalas, Dirk; Petrov, Alexander; Krause, Michael; Hampe, Jan; Eich, Manfred

    2010-10-15

    We present the theoretical concept of an optical isolator based on resonance splitting in a silicon ring resonator covered with a magneto-optical polymer cladding. For this task, a perturbation method is derived for the modes in the cylindrical coordinate system. A polymer magneto-optical cladding causing a 0.01 amplitude of the off-diagonal element of the dielectric tensor is assumed. It is shown that the derived resonance splitting of the clockwise and counterclockwise modes increases for smaller ring radii. For the ring with a radius of approximately 1.5μm, a 29GHz splitting is demonstrated. An integrated optical isolator with a 10μm geometrical footprint is proposed based on a critically coupled ring resonator. PMID:20967092

  1. Optical Fano resonance of an individual semiconductor nanostructure.

    PubMed

    Fan, Pengyu; Yu, Zongfu; Fan, Shanhui; Brongersma, Mark L

    2014-05-01

    Fano resonances with a characteristic asymmetric line shape can be observed in light scattering, transmission and reflection spectra of resonant optical systems. They result from interference between direct and indirect, resonance-assisted pathways. In the nanophotonics field, Fano effects have been observed in a wide variety of systems, including metallic nanoparticle assemblies, metamaterials and photonic crystals. Their unique properties find extensive use in applications, including optical filtering, polarization selectors, sensing, lasers, modulators and nonlinear optics. We report on the observation of a Fano resonance in a single semiconductor nanostructure, opening up opportunities for their use in active photonic devices. We also show that Fano-resonant semiconductor nanostructures afford the intriguing opportunity to simultaneously measure the far-field scattering response and the near-field energy storage by extracting photogenerated charge. Together they can provide a complete experimental characterization of this type of resonance. PMID:24747781

  2. Characterization of energy trapping in a bulk acoustic wave resonator

    NASA Astrophysics Data System (ADS)

    Kokkonen, Kimmo; Meltaus, Johanna; Pensala, Tuomas; Kaivola, Matti

    2010-12-01

    Acoustic wave fields both within the active electrode area of a solidly mounted 1.8 GHz bulk acoustic wave resonator, and around it in the surrounding region, are measured using a heterodyne laser interferometer. Plate-wave dispersion diagrams for both regions are extracted from the measurement data. The experimental dispersion data reveal the cutoff frequencies of the acoustic vibration modes in the region surrounding the resonator, and, therefore, the energy trapping range of the resonator can readily be determined. The measured dispersion properties of the surrounding region, together with the abruptly diminishing amplitude of the dispersion curves in the resonator, signal the onset of acoustic leakage from the resonator. This information is important for verifying and further developing the simulation tools used for the design of the resonators. Experimental wave field images, dispersion diagrams for both regions, and the threshold for energy leakage are discussed.

  3. Unstable resonator with reduced output coupling.

    PubMed

    Pargmann, Carsten; Hall, Thomas; Duschek, Frank; Grünewald, Karin Maria; Handke, Jürgen

    2012-06-20

    The properties of a laser beam coupled out of a standard unstable laser resonator are heavily dependent on the chosen resonator magnification. A higher magnification results in a higher output coupling and a better beam quality. But in some configurations, an unstable resonator with a low output coupling in combination with a good beam quality is desirable. In order to reduce the output coupling for a particular resonator, magnification fractions of the outcoupled radiation are reflected back into the cavity. In the confocal case, the output mirror consists of a spherical inner section with a high reflectivity and a flat outer section with a partial reflectivity coating. With the application of the unstable resonator with reduced output coupling (URROC), magnification and output coupling can be adjusted independently from each other and it is possible to get a good beam quality and a high power extraction for lasers with a large low gain medium. The feasibility of this resonator design is examined numerically and experimentally with the help of a chemical oxygen iodine laser. PMID:22722301

  4. Resonator response to Non-Newtonian fluids

    SciTech Connect

    Martin, S.J.; Schneider, T.W.; Frye, G.C.; Cernosek, R.W.; Senturia, S.D.

    1994-06-01

    The thickness-shear mode (TSM) resonator typically consists of a thin disk of AT-cut quartz with circular electrodes patterned on both sides. An RF voltage applied between these electrodes excites a shear mode mechanical resonance when the excitation frequency matches the crystal resonant frequency. When the TSM resonator is operated in contact with a liquid, the shear motion of the surface generates motion in the contacting liquid. The liquid velocity field, v{sub x}(y), can be determined by solving the one-dimensional Navier-Stokes equation. Newtonian fluids cause an equal increase in resonator motional resistance and reactance, R{sub 2}{sup (N)} = X{sub 2}{sup (N)}, with the response depending only on the liquid density-viscosity product ({rho}{eta}). Non-Newtonian fluids, as illustrated by the simple example of a Maxwell fluid, can cause unequal increases in motional resistance and reactance. For the Maxwell fluid, R{sub 2}{sup (M)} > X{sub 2}{sup (M)}, with relaxation time {tau} proportional to the difference between R{sub 2}{sup (M)}and X{sub 2}{sup (M)}. Early results indicate that a TSM resonator can be used to extract properties of non-Newtonian fluids.

  5. Extracting excited mesons from the finite volume

    SciTech Connect

    Doring, Michael

    2014-12-01

    As quark masses come closer to their physical values in lattice simulations, finite volume effects dominate the level spectrum. Methods to extract excited mesons from the finite volume are discussed, like moving frames in the presence of coupled channels. Effective field theory can be used to stabilize the determination of the resonance spectrum.

  6. Acoustic wave flow sensor using quartz thickness shear mode resonator.

    PubMed

    Qin, Lifeng; Zeng, Zijing; Cheng, Hongbin; Wang, Qing-Ming

    2009-09-01

    A quartz thickness shear mode (TSM) bulk acoustic wave resonator was used for in situ and real-time detection of liquid flow rate in this study. A special flow chamber made of 2 parallel acrylic plates was designed for flow measurement. The flow chamber has a rectangular flow channel, 2 flow reservoirs for stabilizing the fluid flow, a sensor mounting port for resonator holding, one inlet port, and one outlet port for pipe connection. A 5-MHz TSM quartz resonator was edge-bonded to the sensor mounting port with one side exposed to the flowing liquid and other side exposed to air. The electrical impedance spectra of the quartz resonator at different volumetric flow rate conditions were measured by an impedance analyzer for the extraction of the resonant frequency through a data-fitting method. The fundamental, 3rd, 5th, 7th, and 9th resonant frequency shifts were found to be around 920, 3572, 5947, 8228, and 10,300 Hz for flow rate variation from 0 to 3000 mL/min, which had a corresponding Reynolds number change from 0 to 822. The resonant frequency shifts of different modes are found to be quadratic with flow rate, which is attributed to the nonlinear effect of quartz resonator due to the effective normal pressure imposing on the resonator sensor by the flowing fluid. The results indicate that quartz TSM resonators can be used for flow sensors with characteristics of simplicity, fast response, and good repeatability. PMID:19811997

  7. Excitonic surface lattice resonances

    NASA Astrophysics Data System (ADS)

    Humphrey, A. D.; Gentile, M. J.; Barnes, W. L.

    2016-08-01

    Electromagnetic resonances are important in controlling light at the nanoscale. The most studied such resonance is the surface plasmon resonance that is associated with metallic nanostructures. Here we explore an alternative resonance, the surface exciton-polariton resonance, one based on excitonic molecular materials. Our study is based on analytical and numerical modelling. We show that periodic arrays of suitable molecular nanoparticles may support surface lattice resonances that arise as a result of coherent interactions between the particles. Our results demonstrate that excitonic molecular materials are an interesting alternative to metals for nanophotonics; they offer the prospect of both fabrication based on supramolecular chemistry and optical functionality arising from the way the properties of such materials may be controlled with light.

  8. Large mode radius resonators

    NASA Technical Reports Server (NTRS)

    Harris, Michael R.

    1987-01-01

    Resonator configurations permitting operation with large mode radius while maintaining good transverse mode discrimination are considered. Stable resonators incorporating an intracavity telescope and unstable resonator geometries utilizing an output coupler with a Gaussian reflectivity profile are shown to enable large radius single mode laser operation. Results of heterodyne studies of pulsed CO2 lasers with large (11mm e sup-2 radius) fundamental mode sizes are presented demonstrating minimal frequency sweeping in accordance with the theory of laser-induced medium perturbations.

  9. Fabrication and Characterization of Superconducting Resonators.

    PubMed

    Cataldo, Giuseppe; Barrentine, Emily M; Brown, Ari D; Moseley, Samuel H; U-Yen, Kongpop; Wollack, Edward J

    2016-01-01

    Superconducting microwave resonators are of interest for a wide range of applications, including for their use as microwave kinetic inductance detectors (MKIDs) for the detection of faint astrophysical signatures, as well as for quantum computing applications and materials characterization. In this paper, procedures are presented for the fabrication and characterization of thin-film superconducting microwave resonators. The fabrication methodology allows for the realization of superconducting transmission-line resonators with features on both sides of an atomically smooth single-crystal silicon dielectric. This work describes the procedure for the installation of resonator devices into a cryogenic microwave testbed and for cool-down below the superconducting transition temperature. The set-up of the cryogenic microwave testbed allows one to do careful measurements of the complex microwave transmission of these resonator devices, enabling the extraction of the properties of the superconducting lines and dielectric substrate (e.g., internal quality factors, loss and kinetic inductance fractions), which are important for device design and performance. PMID:27284966

  10. Resonances in heavy systems

    SciTech Connect

    Betts, R.R.

    1983-01-01

    The experimental situation for the study of resonances in heavy-ion collisions is reviewed, with emphasis on the heaviest systems. New data are presented which show some of the systematics of this phenomenon. The narrow resonance structures are established as a feature of the nuclear structure of the composite system rather than a purely entrance channel effect.

  11. Unstable optical resonators.

    PubMed

    Kahn, W K

    1966-03-01

    A technique, firmly based on a development from ray optics, is presented for calculating the loss due to the finite sizes of curved mirrors when these form an unstable optical resonator. If paraxial rays launched within such a resonator are confined near the resonator axis, the resonator is termed stable; otherwise it is termed unstable, and is known to have high losses. Siegman has recently presented a geometrical method, brilliantly constructed ad hoc, for calculating these losses in unstable resonators, and indicated where these might be advantageous in laser application. The ray optical theory presented here, which employs the concept of ray modes in an equivalent beam waveguide, is shown to yield results equivalent to those of Siegman for all cases considered by him. However, being derived from conventional ray optics, the validity of the formulas is independently established, and these formulas are immediately applicable to re-entrant resonators and resonators containing inhomogeneous media. The fractional loss per resonator pass is equal to 1-|lambda(2)|, where |lambda(2)| < this 1 is an eigenvalue of the transfer matrix T, representing the corresponding ray transformation. PMID:20048863

  12. The resonator handbook

    NASA Technical Reports Server (NTRS)

    Cook, Jerry D.; Zhou, Shiliang

    1993-01-01

    The purpose of this work is to extend resonator theory into the region in which the planar mirror is quite small. Results of the theoretical description are then extended to resonator design and experimental arrangements as discussed in further sections of this work. Finally, a discussion of dielectric measurements for small samples is included as a specific application of this work.

  13. The Concept of Resonance

    ERIC Educational Resources Information Center

    Truhlar, Donald G.

    2007-01-01

    A general example of a delocalization system associated with a higher energy than the localized one, which suggests that it is wrong to consider delocalization as equivalent to resonance stabilization, is presented. The meaning of resonance energy as it appears in valence bond theory is described as the lowering of the calculated ground-state…

  14. Narrowband resonant transmitter

    DOEpatents

    Hutchinson, Donald P.; Simpson, Marcus L.; Simpson, John T.

    2004-06-29

    A transverse-longitudinal integrated optical resonator (TLIR) is disclosed which includes a waveguide, a first and a second subwavelength resonant grating in the waveguide, and at least one photonic band gap resonant structure (PBG) in the waveguide. The PBG is positioned between the first and second subwavelength resonant gratings. An electro-optic waveguide material may be used to permit tuning the TLIR and to permit the TLIR to perform signal modulation and switching. The TLIR may be positioned on a bulk substrate die with one or more electronic and optical devices and may be communicably connected to the same. A method for fabricating a TLIR including fabricating a broadband reflective grating is disclosed. A method for tuning the TLIR's transmission resonance wavelength is also disclosed.

  15. Resonant snubber inverter

    DOEpatents

    Lai, J.S.; Young, R.W. Sr.; Chen, D.; Scudiere, M.B.; Ott, G.W. Jr.; White, C.P.; McKeever, J.W.

    1997-06-24

    A resonant, snubber-based, soft switching, inverter circuit achieves lossless switching during dc-to-ac power conversion and power conditioning with minimum component count and size. Current is supplied to the resonant snubber branches solely by the main inverter switches. Component count and size are reduced by use of a single semiconductor switch in the resonant snubber branches. Component count is also reduced by maximizing the use of stray capacitances of the main switches as parallel resonant capacitors. Resonance charging and discharging of the parallel capacitances allows lossless, zero voltage switching. In one embodiment, circuit component size and count are minimized while achieving lossless, zero voltage switching within a three-phase inverter. 14 figs.

  16. Resonant snubber inverter

    DOEpatents

    Lai, Jih-Sheng; Young, Sr., Robert W.; Chen, Daoshen; Scudiere, Matthew B.; Ott, Jr., George W.; White, Clifford P.; McKeever, John W.

    1997-01-01

    A resonant, snubber-based, soft switching, inverter circuit achieves lossless switching during dc-to-ac power conversion and power conditioning with minimum component count and size. Current is supplied to the resonant snubber branches solely by the main inverter switches. Component count and size are reduced by use of a single semiconductor switch in the resonant snubber branches. Component count is also reduced by maximizing the use of stray capacitances of the main switches as parallel resonant capacitors. Resonance charging and discharging of the parallel capacitances allows lossless, zero voltage switching. In one embodiment, circuit component size and count are minimized while achieving lossless, zero voltage switching within a three-phase inverter.

  17. Modelling resonant planetary systems

    NASA Astrophysics Data System (ADS)

    Emel'yanenko, V.

    2012-09-01

    Many discovered multi-planet systems are in meanmotion resonances. The aim of this work is to study dynamical processes leading to the formation of resonant configurations on the basis of a unified model described earlier [1]. The model includes gravitational interactions of planets and migration of planets due to the presence of a gas disc. For the observed systems 24 Sex, HD 37124, HD 73526, HD 82943, HD 128311, HD 160691, Kepler 9, NN Ser with planets moving in the 2:1 resonance, it is shown that the capture in this resonance occurs at very wide ranges of parameters of both type I and type II migration. Conditions of migration leading to the formation of the resonant systems HD 45364 и HD 200964 (3:2 and 4:3, respectively) are obtained. Formation scenarios are studied for the systems HD 102272, HD 108874, HD 181433, HD 202206 with planets in high order resonances. We discuss also how gravitational interactions of planets and planetesimal discs lead to the breakup of resonant configurations and the formation of systems similar to the 47 UMa system.

  18. LABCOM resonator Phase 3

    SciTech Connect

    Keres, L.J.

    1990-11-01

    The purpose of this project was to develop quartz crystal resonator designs, production processes, and test capabilities for 5-MHz, 6.2-MHz, and 10-MHz resonators for Tactical Miniature Crystal Oscillator (TMXO) applications. GE Neutron Devices (GEND) established and demonstrated the capability to produce and test quartz crystal resonators for use in the TMXO developed by the US Army ERADCOM (now LABCOM). The goals in this project were based on the ERADCOM statement of work. The scope of work indicated that the resonator production facilities for this project would not be completely independent, but that they would be supported in part by equipment and processes in place at GEND used in US Department of Energy (DOE) work. In addition, provisions for production test equipment or or eventual technology transfer costs to a commercial supplier were clearly excluded from the scope of work. The demonstrated technical capability of the deep-etched blank design is feasible and practical. It can be manufactured in quantity with reasonable yield, and its performance is readily predictable. The ceramic flatpack is a very strong package with excellent hermeticity. The four-point mount supports the crystal to reasonable shock levels and does not perturb the resonator's natural frequency-temperature behavior. The package can be sealed with excellent yields. The high-temperature, high-vacuum processing developed for the TMXO resonator, including bonding the piezoid to its mount with conductive polyimide adhesive, is consistent with precision resonator fabrication. 1 fig., 6 tabs.

  19. Apparatus for hydrocarbon extraction

    DOEpatents

    Bohnert, George W.; Verhulst, Galen G.

    2013-03-19

    Systems and methods for hydrocarbon extraction from hydrocarbon-containing material. Such systems and methods relate to extracting hydrocarbon from hydrocarbon-containing material employing a non-aqueous extractant. Additionally, such systems and methods relate to recovering and reusing non-aqueous extractant employed for extracting hydrocarbon from hydrocarbon-containing material.

  20. Spin resonance strength calculations

    SciTech Connect

    Courant,E.D.

    2008-10-06

    In calculating the strengths of depolarizing resonances it may be convenient to reformulate the equations of spin motion in a coordinate system based on the actual trajectory of the particle, as introduced by Kondratenko, rather than the conventional one based on a reference orbit. It is shown that resonance strengths calculated by the conventional and the revised formalisms are identical. Resonances induced by radiofrequency dipoles or solenoids are also treated; with rf dipoles it is essential to consider not only the direct effect of the dipole but also the contribution from oscillations induced by it.

  1. Tunable multiwalled nanotube resonator

    DOEpatents

    Zettl, Alex K.; Jensen, Kenneth J.; Girit, Caglar; Mickelson, William E.; Grossman, Jeffrey C.

    2011-03-29

    A tunable nanoscale resonator has potential applications in precise mass, force, position, and frequency measurement. One embodiment of this device consists of a specially prepared multiwalled carbon nanotube (MWNT) suspended between a metal electrode and a mobile, piezoelectrically controlled contact. By harnessing a unique telescoping ability of MWNTs, one may controllably slide an inner nanotube core from its outer nanotube casing, effectively changing its length and thereby changing the tuning of its resonance frequency. Resonant energy transfer may be used with a nanoresonator to detect molecules at a specific target oscillation frequency, without the use of a chemical label, to provide label-free chemical species detection.

  2. Tunable multiwalled nanotube resonator

    DOEpatents

    Jensen, Kenneth J; Girit, Caglar O; Mickelson, William E; Zettl, Alexander K; Grossman, Jeffrey C

    2013-11-05

    A tunable nanoscale resonator has potential applications in precise mass, force, position, and frequency measurement. One embodiment of this device consists of a specially prepared multiwalled carbon nanotube (MWNT) suspended between a metal electrode and a mobile, piezoelectrically controlled contact. By harnessing a unique telescoping ability of MWNTs, one may controllably slide an inner nanotube core from its outer nanotube casing, effectively changing its length and thereby changing the tuning of its resonance frequency. Resonant energy transfer may be used with a nanoresonator to detect molecules at a specific target oscillation frequency, without the use of a chemical label, to provide label-free chemical species detection.

  3. Unfolding the Second Riemann sheet with Pade Approximants: hunting resonance poles

    SciTech Connect

    Masjuan, Pere

    2011-05-23

    Based on Pade Theory, a new procedure for extracting the pole mass and width of resonances is proposed. The method is systematic and provides a model-independent treatment for the prediction and the errors of the approximation.

  4. Micro-machined resonator

    DOEpatents

    Godshall, N.A.; Koehler, D.R.; Liang, A.Y.; Smith, B.K.

    1993-03-30

    A micro-machined resonator, typically quartz, with upper and lower micro-machinable support members, or covers, having etched wells which may be lined with conductive electrode material, between the support members is a quartz resonator having an energy trapping quartz mesa capacitively coupled to the electrode through a diaphragm; the quartz resonator is supported by either micro-machined cantilever springs or by thin layers extending over the surfaces of the support. If the diaphragm is rigid, clock applications are available, and if the diaphragm is resilient, then transducer applications can be achieved. Either the thin support layers or the conductive electrode material can be integral with the diaphragm. In any event, the covers are bonded to form a hermetic seal and the interior volume may be filled with a gas or may be evacuated. In addition, one or both of the covers may include oscillator and interface circuitry for the resonator.

  5. Micro-machined resonator

    DOEpatents

    Godshall, Ned A.; Koehler, Dale R.; Liang, Alan Y.; Smith, Bradley K.

    1993-01-01

    A micro-machined resonator, typically quartz, with upper and lower micro-machinable support members, or covers, having etched wells which may be lined with conductive electrode material, between the support members is a quartz resonator having an energy trapping quartz mesa capacitively coupled to the electrode through a diaphragm; the quartz resonator is supported by either micro-machined cantilever springs or by thin layers extending over the surfaces of the support. If the diaphragm is rigid, clock applications are available, and if the diaphragm is resilient, then transducer applications can be achieved. Either the thin support layers or the conductive electrode material can be integral with the diaphragm. In any event, the covers are bonded to form a hermetic seal and the interior volume may be filled with a gas or may be evacuated. In addition, one or both of the covers may include oscillator and interface circuitry for the resonator.

  6. Resonances in QCD

    NASA Astrophysics Data System (ADS)

    Lutz, Matthias F. M.; Lange, Jens Sören; Pennington, Michael; Bettoni, Diego; Brambilla, Nora; Crede, Volker; Eidelman, Simon; Gillitzer, Albrecht; Gradl, Wolfgang; Lang, Christian B.; Metag, Volker; Nakano, Takashi; Nieves, Juan; Neubert, Sebastian; Oka, Makoto; Olsen, Stephen L.; Pappagallo, Marco; Paul, Stephan; Pelizäus, Marc; Pilloni, Alessandro; Prencipe, Elisabetta; Ritman, Jim; Ryan, Sinead; Thoma, Ulrike; Uwer, Ulrich; Weise, Wolfram

    2016-04-01

    We report on the EMMI Rapid Reaction Task Force meeting 'Resonances in QCD', which took place at GSI October 12-14, 2015. A group of 26 people met to discuss the physics of resonances in QCD. The aim of the meeting was defined by the following three key questions: What is needed to understand the physics of resonances in QCD? Where does QCD lead us to expect resonances with exotic quantum numbers? What experimental efforts are required to arrive at a coherent picture? For light mesons and baryons only those with up, down and strange quark content were considered. For heavy-light and heavy-heavy meson systems, those with charm quarks were the focus. This document summarizes the discussions by the participants, which in turn led to the coherent conclusions we present here.

  7. Resonant ultrasound spectroscopy

    DOEpatents

    Migliori, Albert

    1991-01-01

    A resonant ultrasound spectroscopy method provides a unique characterization of an object for use in distinguishing similar objects having physical differences greater than a predetermined tolerance. A resonant response spectrum is obtained for a reference object by placing excitation and detection transducers at any accessible location on the object. The spectrum is analyzed to determine the number of resonant response peaks in a predetermined frequency interval. The distribution of the resonance frequencies is then characterized in a manner effective to form a unique signature of the object. In one characterization, a small frequency interval is defined and stepped though the spectrum frequency range. Subsequent objects are similarly characterized where the characterizations serve as signatures effective to distinguish objects that differ from the reference object by more than the predetermined tolerance.

  8. Resonances in Positronium Hydride

    NASA Technical Reports Server (NTRS)

    DiRienzi, Joseph; Drachman, Richard J.; Fisher, Richard R. (Technical Monitor)

    2001-01-01

    We re-examine the problem of calculating the positions and widths of the lowest-lying resonances in the Ps + H scattering system which consists of two electrons, one positron and one proton. The first of these resonances, for L=0, was found by the methods of complex rotation and stabilization, and later described as a Feshbach resonance lying close to a bound state in the closed-channel e (+) + H (-) system. Recently, results for the L=1 and 2 scattering states were published, and it was found, surprisingly, that there is a larae shift in the positions of these resonances. In this work we repeat the analysis for L=1 and find an unexpected explanation for the shift.

  9. Cylindrical laser resonator

    DOEpatents

    Casperson, Lee W.

    1976-02-24

    The properties of an improved class of lasers is presented. In one configuration of these lasers the radiation propagates radially within the amplifying medium, resulting in high fields and symmetric illumination at the resonator axis. Thus there is a strong focusing of energy at the axis of the resonator. In a second configuration the radiation propagates back and forth in a tubular region of space.

  10. Resonant dielectric metamaterials

    SciTech Connect

    Loui, Hung; Carroll, James; Clem, Paul G; Sinclair, Michael B

    2014-12-02

    A resonant dielectric metamaterial comprises a first and a second set of dielectric scattering particles (e.g., spheres) having different permittivities arranged in a cubic array. The array can be an ordered or randomized array of particles. The resonant dielectric metamaterials are low-loss 3D isotropic materials with negative permittivity and permeability. Such isotropic double negative materials offer polarization and direction independent electromagnetic wave propagation.

  11. Hexagonal quartz resonator

    DOEpatents

    Peters, Roswell D. M.

    1982-01-01

    A generally flat, relatively thin AT-cut piezoelectric resonator element structured to minimize the force-frequency effect when mounted and energized in a housing. The resonator is in the form of an equilateral hexagon with the X crystallographic axis of the crystal passing through one set of opposing corners with mounting being effected at an adjacent set of corners respectively .+-.60.degree. away from the X axis which thereby results in a substantially zero frequency shift of the operating frequency.

  12. Injector with integrated resonator

    SciTech Connect

    Johnson, Thomas Edward; Ziminsky, Willy Steve; York, William David; Stevenson, Christian Xavier

    2014-07-29

    The system may include a turbine engine. The turbine engine may include a fuel nozzle. The fuel nozzle may include an air path. The fuel nozzle may also include a fuel path such that the fuel nozzle is in communication with a combustion zone of the turbine engine. Furthermore, the fuel nozzle may include a resonator. The resonator may be disposed in the fuel nozzle directly adjacent to the combustion zone.

  13. Plasmofluidic Disk Resonators

    NASA Astrophysics Data System (ADS)

    Kwon, Min-Suk; Ku, Bonwoo; Kim, Yonghan

    2016-03-01

    Waveguide-coupled silicon ring or disk resonators have been used for optical signal processing and sensing. Large-scale integration of optical devices demands continuous reduction in their footprints, and ultimately they need to be replaced by silicon-based plasmonic resonators. However, few waveguide-coupled silicon-based plasmonic resonators have been realized until now. Moreover, fluid cannot interact effectively with them since their resonance modes are strongly confined in solid regions. To solve this problem, this paper reports realized plasmofluidic disk resonators (PDRs). The PDR consists of a submicrometer radius silicon disk and metal laterally surrounding the disk with a 30-nm-wide channel in between. The channel is filled with fluid, and the resonance mode of the PDR is strongly confined in the fluid. The PDR coupled to a metal-insulator-silicon-insulator-metal waveguide is implemented by using standard complementary metal oxide semiconductor technology. If the refractive index of the fluid increases by 0.141, the transmission spectrum of the waveguide coupled to the PDR of radius 0.9 μm red-shifts by 30 nm. The PDR can be used as a refractive index sensor requiring a very small amount of analyte. Plus, the PDR filled with liquid crystal may be an ultracompact intensity modulator which is effectively controlled by small driving voltage.

  14. Plasmofluidic Disk Resonators

    PubMed Central

    Kwon, Min-Suk; Ku, Bonwoo; Kim, Yonghan

    2016-01-01

    Waveguide-coupled silicon ring or disk resonators have been used for optical signal processing and sensing. Large-scale integration of optical devices demands continuous reduction in their footprints, and ultimately they need to be replaced by silicon-based plasmonic resonators. However, few waveguide-coupled silicon-based plasmonic resonators have been realized until now. Moreover, fluid cannot interact effectively with them since their resonance modes are strongly confined in solid regions. To solve this problem, this paper reports realized plasmofluidic disk resonators (PDRs). The PDR consists of a submicrometer radius silicon disk and metal laterally surrounding the disk with a 30-nm-wide channel in between. The channel is filled with fluid, and the resonance mode of the PDR is strongly confined in the fluid. The PDR coupled to a metal-insulator-silicon-insulator-metal waveguide is implemented by using standard complementary metal oxide semiconductor technology. If the refractive index of the fluid increases by 0.141, the transmission spectrum of the waveguide coupled to the PDR of radius 0.9 μm red-shifts by 30 nm. The PDR can be used as a refractive index sensor requiring a very small amount of analyte. Plus, the PDR filled with liquid crystal may be an ultracompact intensity modulator which is effectively controlled by small driving voltage. PMID:26979929

  15. Resonant nonlinear ultrasound spectroscopy

    DOEpatents

    Johnson, Paul A.; TenCate, James A.; Guyer, Robert A.; Van Den Abeele, Koen E. A.

    2001-01-01

    Components with defects are identified from the response to strains applied at acoustic and ultrasound frequencies. The relative resonance frequency shift .vertline..DELTA..function./.function..sub.0.vertline., is determined as a function of applied strain amplitude for an acceptable component, where .function..sub.0 is the frequency of the resonance peak at the lowest amplitude of applied strain and .DELTA..function. is the frequency shift of the resonance peak of a selected mode to determine a reference relationship. Then, the relative resonance frequency shift .vertline..DELTA..function./.function..sub.0 is determined as a function of applied strain for a component under test, where fo .function..sub.0 the frequency of the resonance peak at the lowest amplitude of applied strain and .DELTA..function. is the frequency shift of the resonance peak to determine a quality test relationship. The reference relationship is compared with the quality test relationship to determine the presence of defects in the component under test.

  16. Neutral Pion Electroproduction in the Delta Resonance Region

    SciTech Connect

    Villano, Anthony

    2007-11-01

    The electroproduction of baryon resonances at high Q2 is examined. Analysis focuses on the Delta(1232) resonance via exclusive pseudoscalar meson production of À0 particles. Differential cross sections are extracted for exclusive À0 electroproduction. In the central invariant mass (W) region the cross sections are used to extract resonant multipole amplitudes. In particular, the ratio of the electric quadrupole to magnetic dipole amplitudes (E2/M1) will be discussed for the Delta(1232) resonance. The transition to pQCD is discussed in terms of E2/M1 and other multipoles. The helicity amplitude A3/2 can be used as a baryon helicity conservation meter in this context and will be discussed. The fast shrinking of the resonant contribution in the Delta region is observed at this high momentum transfer. Apart from the observables related to pQCD scaling, the transition form factor G M is extracted along with the scalar to magnetic dipole ratio C2/M1.

  17. Spectral correlation of wideband target resonances

    NASA Astrophysics Data System (ADS)

    Sabio, Vincent

    1995-07-01

    The potential for automatic target recognition (ATR) processing of foliage-penetrating (FOPEN) synthetic-aperture radar (SAR) imagery requires very high bandwidth occupancies to achieve sufficient range resolution for the ATR task. The U.S. Army Research Laboratory (ARL) ultra-wideband (UWB) FOPEN SAR -- with greater than 95 percent bandwidth occupancy -- provides a suitable testbed for evaluation of resonance-based ATR approaches. Current resonance-extraction techniques (e.g., SEM) typically have poor performance in the presence of noise, and are often computationally intensive. Recently developed at ARL, the `spectral correlation method' uses linear transforms -- such as Fourier and wavelets -- to resolve resonant components; these transforms are generally quite fast, and have straightforward implementations. Creating a synthetic version of the ringdown and projecting onto the desired transform basis provides a set of expected spectral coefficients (the `spectral template'). The spectral template is correlated with the spectral coefficients acquired from the projection of the focused image data onto the same basis function set; the correlation coefficient is then passed through a simple threshold detector. This yields a fast, efficient scheme for recognition of target resonance effects in UWB imagery. Recent advances in this area include a reduction in false-alarm rate by two orders of magnitude, a reduction in processing time by three orders of magnitude, and recognition of a tactical target.

  18. Resonance-assisted decay of nondispersive wave packets.

    PubMed

    Wimberger, Sandro; Schlagheck, Peter; Eltschka, Christopher; Buchleitner, Andreas

    2006-07-28

    We present a quantitative semiclassical theory for the decay of nondispersive electronic wave packets in driven, ionizing Rydberg systems. Statistically robust quantities are extracted combining resonance-assisted tunneling with subsequent transport across chaotic phase space and a final ionization step. PMID:16907569

  19. Tunable Resonant Scanners

    NASA Astrophysics Data System (ADS)

    Montagu, Jean I.

    1987-01-01

    The most attractive features of resonant scanners are high reliability and eternal life as well as extremely low wobble and jitter. Power consumption is also low, electronic drive is simple, and the device is capable of handling large beams. All of these features are delivered at a low cost in a small package. The resonant scanner's use in numerous high precision applications, however, has been limited because of the difficulty in controlling its phase and resonant frequency. This paper introduces the concept of tunable/controllable resonant scanners, discusses their features, and offers a number of tuning techniques. It describes two angular scanner designs and presents data on tunable range and life tests. It also reviews applications for these new tunable resonant scanners that preserve the desirable features of earlier models while removing the old problems with synchronization or time base flexibility. The three major types of raster scanning applications where the tunable resonant scanner may be of benefit are: 1. In systems with multiple time bases such as multiple scanner networks or with scanners keyed to a common clock (the line frequency or data source) or a machine with multiple resonant scanners. A typical application is image and text transmission, also a printer with a large data base where a buffer is uneconomical. 2. In systems sharing data processing or laser equipment for reasons of cost or capacity, typically multiple work station manufacturing processes or graphic processes. 3. In systems with extremely precise time bases where the frequency stability of conventional scanners cannot be relied upon.

  20. Rho resonance parameters from lattice QCD

    NASA Astrophysics Data System (ADS)

    Guo, Dehua; Alexandru, Andrei; Molina, Raquel; Döring, Michael

    2016-08-01

    We perform a high-precision calculation of the phase shifts for π -π scattering in the I =1 , J =1 channel in the elastic region using elongated lattices with two mass-degenerate quark flavors (Nf=2 ). We extract the ρ resonance parameters using a Breit-Wigner fit at two different quark masses, corresponding to mπ=226 MeV and mπ=315 MeV , and perform an extrapolation to the physical point. The extrapolation is based on a unitarized chiral perturbation theory model that describes well the phase shifts around the resonance for both quark masses. We find that the extrapolated value, mρ=720 (1 )(15 ) MeV , is significantly lower that the physical rho mass and we argue that this shift could be due to the absence of the strange quark in our calculation.

  1. Chaotic spectra: How to extract dynamic information

    SciTech Connect

    Taylor, H.S.; Gomez Llorente, J.M.; Zakrzewski, J.; Kulander, K.C.

    1988-10-01

    Nonlinear dynamics is applied to chaotic unassignable atomic and molecular spectra with the aim of extracting detailed information about regular dynamic motions that exist over short intervals of time. It is shown how this motion can be extracted from high resolution spectra by doing low resolution studies or by Fourier transforming limited regions of the spectrum. These motions mimic those of periodic orbits (PO) and are inserts into the dominant chaotic motion. Considering these inserts and the PO as a dynamically decoupled region of space, resonant scattering theory and stabilization methods enable us to compute ladders of resonant states which interact with the chaotic quasi-continuum computed in principle from basis sets placed off the PO. The interaction of the resonances with the quasicontinuum explains the low resolution spectra seen in such experiments. It also allows one to associate low resolution features with a particular PO. The motion on the PO thereby supplies the molecular movements whose quantization causes the low resolution spectra. Characteristic properties of the periodic orbit based resonances are discussed. The method is illustrated on the photoabsorption spectrum of the hydrogen atom in a strong magnetic field and on the photodissociation spectrum of H/sub 3//sup +/. Other molecular systems which are currently under investigation using this formalism are also mentioned. 53 refs., 10 figs., 2 tabs.

  2. RF voltage modulation at discrete frequencies with applications to crystal channeling extraction

    SciTech Connect

    Gabella, W.; Rosenzweig, J. . Dept. of Physics); Kick, R. ); Peggs, S. )

    1992-05-01

    RF voltage modulation at a finite number of discrete frequencies is described in a Hamiltonian resonance framework. The theory is applied to the problem of parasitic extraction of a fixed target beam from a high energy proton collider, using a bent crystal as a thin septum'' within an effective width of about one micron. Three modes of employment of discrete resonances are proposed.First, a single relatively strong static drive'' resonance may be used to excite a test proton so that it will penetrate deeply into the channeling crystal. Second, a moderately strong feed'' resonance with a ramped modulation tune may be used to adiabatically trap protons near the edge of the beam core, and transport them to the drive resonance. Third, several weak resonances may be overlapped to create a chaotic amplitude band, either to transport protons to the drive resonance, or to provide a pulse stretching'' buffer between a feed resonance and the drive resonance. Extraction efficiency is semi- quantitatively described in terms of characteristic penetration,'' depletion,'' and repetition'' times. simulations are used to quantitatively confirm the fundamental results of the theory, and to show that a prototypical extraction scheme using all three modes promises good extraction performance.

  3. Resonant ultrasound spectrometer

    DOEpatents

    Migliori, Albert; Visscher, William M.; Fisk, Zachary

    1990-01-01

    An ultrasound resonant spectrometer determines the resonant frequency spectrum of a rectangular parallelepiped sample of a high dissipation material over an expected resonant response frequency range. A sample holder structure grips corners of the sample between piezoelectric drive and receive transducers. Each transducer is mounted on a membrane for only weakly coupling the transducer to the holder structure and operatively contacts a material effective to remove system resonant responses at the transducer from the expected response range. i.e., either a material such as diamond to move the response frequencies above the range or a damping powder to preclude response within the range. A square-law detector amplifier receives the response signal and retransmits the signal on an isolated shield of connecting cabling to remove cabling capacitive effects. The amplifier also provides a substantially frequency independently voltage divider with the receive transducer. The spectrometer is extremely sensitive to enable low amplitude resonance to be detected for use in calculating the elastic constants of the high dissipation sample.

  4. Resonances in Positronium Hydride

    NASA Technical Reports Server (NTRS)

    Drachman, Richard J.; Fisher, Richard R. (Technical Monitor)

    2001-01-01

    Recently, Ho and his colleagues have calculated the positions and widths of a series of resonances in the Ps+H scattering system, using the complex -rotation method and have compared them with estimates that I made many years ago using a quite different technique. I assumed that the resonance mechanism was the existence in the rearrangement channel [e+ + H-] of an infinite series of perturbed Coulomb bound states. Although these must be broadened and shifted by coupling with the open scattering channel, I expected them to lie very close to the actual resonance positions. To verify this, I did a model calculation for S-waves, including the coupling, and found that the first two resonances were not shifted very far from their unperturbed position. The new, detailed calculation agrees with this result, but when the P-wave was examined it was found, surprisingly, that the lowest resonance indeed moved up in energy by a large amount. With the help of Joseph DiRienzi of the College of Notre Dame of Maryland I am now extending the old calculation to P- and D-waves, in an attempt to understand this unexpected energy shift. Results will be presented at the Workshop.

  5. MACHINERY RESONANCE AND DRILLING

    SciTech Connect

    Leishear, R.; Fowley, M.

    2010-01-23

    New developments in vibration analysis better explain machinery resonance, through an example of drill bit chattering during machining of rusted steel. The vibration of an operating drill motor was measured, the natural frequency of an attached spring was measured, and the two frequencies were compared to show that the system was resonant. For resonance to occur, one of the natural frequencies of a structural component must be excited by a cyclic force of the same frequency. In this case, the frequency of drill bit chattering due to motor rotation equaled the spring frequency (cycles per second), and the system was unstable. A soft rust coating on the steel to be drilled permitted chattering to start at the drill bit tip, and the bit oscillated on and off of the surface, which increased the wear rate of the drill bit. This resonant condition is typically referred to as a motor critical speed. The analysis presented here quantifies the vibration associated with this particular critical speed problem, using novel techniques to describe resonance.

  6. Hadron scattering and resonances in QCD

    NASA Astrophysics Data System (ADS)

    Dudek, Jozef J.

    2016-05-01

    I describe how hadron-hadron scattering amplitudes are related to the eigenstates of QCD in a finite cubic volume. The discrete spectrum of such eigenstates can be determined from correlation functions computed using lattice QCD, and the corresponding scattering amplitudes extracted. I review results from the Hadron Spectrum Collaboration who have used these finite volume methods to study ππ elastic scattering, including the ρ resonance, as well as coupled-channel π >K, ηK scattering. Ongoing calculations are advertised and the outlook for finite volume approaches is presented.

  7. Review: Magnetic resonance imaging techniques in ophthalmology

    PubMed Central

    Fagan, Andrew J.

    2012-01-01

    Imaging the eye with magnetic resonance imaging (MRI) has proved difficult due to the eye’s propensity to move involuntarily over typical imaging timescales, obscuring the fine structure in the eye due to the resulting motion artifacts. However, advances in MRI technology help to mitigate such drawbacks, enabling the acquisition of high spatiotemporal resolution images with a variety of contrast mechanisms. This review aims to classify the MRI techniques used to date in clinical and preclinical ophthalmologic studies, describing the qualitative and quantitative information that may be extracted and how this may inform on ocular pathophysiology. PMID:23112569

  8. Collider Signal I :. Resonance

    NASA Astrophysics Data System (ADS)

    Tait, Tim M. P.

    2010-08-01

    These TASI lectures were part of the summer school in 2008 and cover the collider signal associated with resonances in models of physics beyond the Standard Model. I begin with a review of the Z boson, one of the best-studied resonances in particle physics, and review how the Breit-Wigner form of the propagator emerges in perturbation theory and discuss the narrow width approximation. I review how the LEP and SLAC experiments could use the kinematics of Z events to learn about fermion couplings to the Z. I then make a brief survey of models of physics beyond the Standard Model which predict resonances, and discuss some of the LHC observables which we can use to discover and identify the nature of the BSM physics. I finish up with a discussion of the linear moose that one can use for an effective theory description of a massive color octet vector particle.

  9. Three-pion resonances

    NASA Astrophysics Data System (ADS)

    Garcilazo, H.; Mathelitsch, L.

    1994-03-01

    We investigate the continuum three-pion problem within a relativistic three-body model that takes into account the ππ S and P waves. The dynamical input of the two-body subsystem is given by separable potentials, which yield a good fit to the ππ scattering data and resonance parameters up to a two-body invariant mass of 900MeV. We introduce a parameter ν expressing the ambiguity in the reduction of a fully relativistic theory to a three-dimensional one. The masses and widths of the ω, a 1(1260), and π(1300) mesons, which decay predominantly into three pions, are reasonably well described by our model. The h 1(1170) meson, however, which also decays into three pions, cannot be explained as a three-pion resonance. Some πρ Argand diagrams are shown in those channels where resonances exist.

  10. Magnetostrictive resonance excitation

    DOEpatents

    Schwarz, Ricardo B.; Kuokkala, Veli-Tapani

    1992-01-01

    The resonance frequency spectrum of a magnetostrictive sample is remotely determined by exciting the magnetostrictive property with an oscillating magnetic field. The permeability of a magnetostrictive material and concomitant coupling with a detection coil varies with the strain in the material whereby resonance responses of the sample can be readily detected. A suitable sample may be a magnetostrictive material or some other material having at least one side coated with a magnetostrictive material. When the sample is a suitable shape, i.e., a cube, rectangular parallelepiped, solid sphere or spherical shell, the elastic moduli or the material can be analytically determined from the measured resonance frequency spectrum. No mechanical transducers are required and the sample excitation is obtained without contact with the sample, leading to highly reproducible results and a measurement capability over a wide temperature range, e.g. from liquid nitrogen temperature to the Curie temperature of the magnetostrictive material.

  11. Quartz resonator processing system

    DOEpatents

    Peters, Roswell D. M.

    1983-01-01

    Disclosed is a single chamber ultra-high vacuum processing system for the oduction of hermetically sealed quartz resonators wherein electrode metallization and sealing are carried out along with cleaning and bake-out without any air exposure between the processing steps. The system includes a common vacuum chamber in which is located a rotatable wheel-like member which is adapted to move a plurality of individual component sets of a flat pack resonator unit past discretely located processing stations in said chamber whereupon electrode deposition takes place followed by the placement of ceramic covers over a frame containing a resonator element and then to a sealing stage where a pair of hydraulic rams including heating elements effect a metallized bonding of the covers to the frame.

  12. Resonance absorption of magnetohydrodynamic surface waves Physical discussion

    NASA Technical Reports Server (NTRS)

    Hollweg, Joseph V.

    1987-01-01

    It is shown how the phenomenon of MHD surface wave resonance absorption can be described in simple terms, both physically and mathematically, by applying the 'thin flux tube equations' to the finite-thickness transition layer which supports the surface wave. The thin flux tubes support incompressible slow-mode waves that are driven by fluctuations in the total pressure which exist due to the presence of the surface wave. It is shown that the equations for the slow-mode waves can be reduced to a simple equation, equivalent to a driven harmonic oscillator. Certain field lines within the transition layer are equivalent to a harmonic oscillator driven at resonance, and neighboring field lines are effectively driven at resonance as long as a given condition is satisfied. Thus, a layer which secularly extracts energy from the surface wave develops. The analysis indicates that nonlinear effects may destroy the resonance which is crucial to the whole effect.

  13. Resonant optical gun.

    PubMed

    Maslov, A V; Bakunov, M I

    2014-05-01

    We propose a concept of a structure-a resonant optical gun-to realize an efficient propulsion of dielectric microparticles by light forces. The structure is based on a waveguide in which a reversal of the electromagnetic momentum flow of the incident mode is realized by exciting a whispering gallery resonance in the microparticle. The propelling force can reach the value up to the theoretical maximum of twice the momentum flow of the initial wave. The force density oscillates along the particle periphery and has very large amplitude. PMID:24784113

  14. Magnetic resonance annual, 1988

    SciTech Connect

    Kressel, H.Y.

    1987-01-01

    This book features reviews of high-resolution MRI of the knee, MRI of the normal and ischmeic hip, MRI of the heart, and temporomandibular joint imaging, as well as thorough discussion on artifacts in magnetic resonance imaging. Contributors consider the clinical applications of gadolinium-DTPA in magnetic resonance imaging and the clinical use of partial saturation and saturation recovery sequences. Timely reports assess the current status of rapid MRI and describe a new rapid gated cine MRI technique. Also included is an analysis of cerebrospinal fluid flow effects during MRI of the central nervous system.

  15. Pygmy resonances and nucleosynthesis

    NASA Astrophysics Data System (ADS)

    Tsoneva, Nadia; Lenske, Horst

    2015-05-01

    A microscopic theoretical approach based on a self-consistent density functional theory for the nuclear ground state and QRPA formalism extended with multi-phonon degrees of freedom for the nuclear excited states is implemented in investigations of new low-energy modes called pygmy resonances. Advantage of the method is the unified description of low-energy multiphonon excitations, pygmy resonances and core polarization effects. This is found of crucial importance for the understanding of the fine structure of nuclear response functions at low energies. Aspects of the precise knowledge of nuclear response functions around the neutron threshold are discussed in a connection to nucleosynthesis.

  16. Method for resonant measurement

    DOEpatents

    Rhodes, George W.; Migliori, Albert; Dixon, Raymond D.

    1996-01-01

    A method of measurement of objects to determine object flaws, Poisson's ratio (.sigma.) and shear modulus (.mu.) is shown and described. First, the frequency for expected degenerate responses is determined for one or more input frequencies and then splitting of degenerate resonant modes are observed to identify the presence of flaws in the object. Poisson's ratio and the shear modulus can be determined by identification of resonances dependent only on the shear modulus, and then using that shear modulus to find Poisson's ratio using other modes dependent on both the shear modulus and Poisson's ratio.

  17. Physics of Sports: Resonances

    NASA Astrophysics Data System (ADS)

    Browning, David

    2000-04-01

    When force is applied by an athlete to sports equipment resonances can occur. Just a few examples are: the ringing of a spiked volleyball, the strumming of a golf club shaft during a swing, and multiple modes induced in an aluminum baseball bat when striking a ball. Resonances produce acoustic waves which, if conditions are favorable, can be detected off the playing field. This can provide a means to evaluate athletic performance during game conditions. Results are given from the use of a simple hand-held acoustic detector - by a spectator sitting in the stands - to determine how hard volleyballs were spiked during college and high school games.

  18. Method for resonant measurement

    DOEpatents

    Rhodes, G.W.; Migliori, A.; Dixon, R.D.

    1996-03-05

    A method of measurement of objects to determine object flaws, Poisson`s ratio ({sigma}) and shear modulus ({mu}) is shown and described. First, the frequency for expected degenerate responses is determined for one or more input frequencies and then splitting of degenerate resonant modes are observed to identify the presence of flaws in the object. Poisson`s ratio and the shear modulus can be determined by identification of resonances dependent only on the shear modulus, and then using that shear modulus to find Poisson`s ratio using other modes dependent on both the shear modulus and Poisson`s ratio. 1 fig.

  19. Field resonance propulsion concept

    NASA Technical Reports Server (NTRS)

    Holt, A. C.

    1979-01-01

    A propulsion concept was developed based on a proposed resonance between coherent, pulsed electromagnetic wave forms, and gravitational wave forms (or space-time metrics). Using this concept a spacecraft propulsion system potentially capable of galactic and intergalactic travel without prohibitive travel times was designed. The propulsion system utilizes recent research associated with magnetic field line merging, hydromagnetic wave effects, free-electron lasers, laser generation of megagauss fields, and special structural and containment metals. The research required to determine potential, field resonance characteristics and to evaluate various aspects of the spacecraft propulsion design is described.

  20. Hexagonal quartz resonator

    DOEpatents

    Peters, R.D.M.

    1982-11-02

    A generally flat, relatively thin AT-cut piezoelectric resonator element structured to minimize the force-frequency effect when mounted and energized in a housing. The resonator is in the form of an equilateral hexagon with the X crystallographic axis of the crystal passing through one set of opposing corners with mounting being effected at an adjacent set of corners respectively [+-]60[degree] away from the X axis which thereby results in a substantially zero frequency shift of the operating frequency. 3 figs.

  1. Azimuthally unstable resonators for high-power CO[sub 2] lasers with annular gain media

    SciTech Connect

    Ehrlichmann, D.; Habich, U.; Plum, H.D.; Loosen, P.; Herziger, G. )

    1994-06-01

    Stable-unstable resonators have proved suitable for the extraction of a high-quality beam from a gain area that consists of a rectangular slab. Such gain areas have two substantially different transverse dimensions, and the resonators are stable in the small dimension while unstable in the larger one. Using off-axis unstable resonators avoids a central beam obscuration and improves beam quality. The adaptation of stable-unstable resonators to annular gain areas is described in this paper. The resulting resonators are stable in the radial direction and unstable in the azimuthal direction. Different unstable resonators, wound to match the annular geometry, are presented. The resonator modes are calculated numerically using a 3D-diffraction code that considers gain and misalignment. Resonator design parameters are obtained from a geometrical description of the resonator. Experimental results from a diffusion-cooled CO[sub 2] laser confirm theoretical predictions and show that the resonators are capable of extracting beams that are nearly diffraction-limited with high efficiency from an annular gain medium. Output powers of 2 kW have been obtained from a gain length of 1.8 m.

  2. Extraction of electromagnetic properties of the {Delta}(1232) excitation from pion photoproduction

    SciTech Connect

    Wilbois, T.; Wilhelm, P.; Arenhoevel, H.

    1998-01-01

    Several methods for the treatment of pion photoproduction in the region of the {Delta}(1232) resonance are discussed, in particular the effective Lagrangian approach and the speed plot analysis are compared to a dynamical treatment. As a main topic, we discuss the extraction of the genuine resonance parts of the magnetic dipole and electric quadrupole multipoles of the electromagnetic excitation of the resonance. To this end, we try to relate the various values for the ratio R{sub EM} of the E2 to M1 multipole excitation strengths for the {Delta}(1232) resonance as extracted by the different methods to corresponding ratios of a dynamical model. Moreover, it is confirmed that all methods for extracting resonance properties suffer from an unitary ambiguity which is due to some phenomenological contributions entering the models. {copyright} {ital 1998} {ital The American Physical Society}

  3. Quantify Resonance Inspection with Finite Element-Based Modal Analyses

    SciTech Connect

    Lai, Canhai; Sun, Xin; Dasch, Cameron; Harmon, George; Jones, Martin

    2011-06-01

    Resonance inspection uses the natural acoustic resonances of a part to identify anomalous parts. Modern instrumentation can measure the many resonant frequencies rapidly and accurately. Sophisticated sorting algorithms trained on sets of good and anomalous parts can rapidly and reliably inspect and sort parts. This paper aims at using finite-element-based modal analysis to put resonance inspection on a more quantitative basis. A production-level automotive steering knuckle is used as the example part for our study. First, the resonance frequency spectra for the knuckle are measured with two different experimental techniques. Next, scanning laser vibrometry is used to determine the mode shape corresponding to each resonance. The material properties including anisotropy are next measured to high accuracy using resonance spectroscopy on cuboids cut from the part. Then, finite element model (FEM) of the knuckle is generated by meshing the actual part geometry obtained with computed tomography (CT). The resonance frequencies and mode shapes are next predicted with a natural frequency extraction analysis after extensive mesh size sensitivity study. The good comparison between the predicted and the experimentally measured resonance spectra indicate that finite-element-based modal analyses have the potential to be a powerful tool in shortening the training process and improving the accuracy of the resonance inspection process for a complex, production level part. The finite element based analysis can also provide a means to computationally test the sensitivity of the frequencies to various possible defects such as porosity or oxide inclusions especially in the high stress regions that the part will experience in service.

  4. Quantify Resonance Inspection with Finite Element-Based Modal Analyses

    SciTech Connect

    Sun, Xin; Lai, Canhai; Dasch, Cameron

    2010-11-10

    Resonance inspection uses the natural acoustic resonances of a part to identify anomalous parts. Modern instrumentation can measure the many resonant frequencies rapidly and accurately. Sophisticated sorting algorithms trained on sets of good and anomalous parts can rapidly and reliably inspect and sort parts. This paper aims at using finite-element-based modal analysis to put resonance inspection on a more quantitative basis. A production-level automotive steering knuckle is used as the example part for our study. First, the resonance frequency spectra for the knuckle are measured with two different experimental techniques. Next, scanning laser vibrometry is used to determine the mode shape corresponding to each resonance. The material properties including anisotropy are next measured to high accuracy using resonance spectroscopy on cuboids cut from the part. Then, finite element model (FEM) of the knuckle is generated by meshing the actual part geometry obtained with computed tomography (CT). The resonance frequencies and mode shapes are next predicted with a natural frequency extraction analysis after extensive mesh size sensitivity study. The good comparison between the predicted and the experimentally measured resonance spectra indicate that finite-element-based modal analyses have the potential to be a powerful tool in shortening the training process and improving the accuracy of the resonance inspection process for a complex, production level part. The finite element based analysis can also provide a means to computationally test the sensitivity of the frequencies to various possible defects such as porosity or oxide inclusions especially in the high stress regions that the part will experience in service.

  5. Extraction and characterization of montmorency (Prunus cerasus L.) sour cherry pit oil

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Montmorency sour cherry (Prunus cerasus L.) pit oil was extracted and characterized by various methods including: gas chromatography (GC), liquid chromatography coupled with mass spectrometry (LC-MS), nuclear magnetic resonance (NMR), thermogravimetric analysis (TGA), differential scanning calorime...

  6. Analysis of transmission lines loaded with pairs of coupled resonant elements and application to sensors

    NASA Astrophysics Data System (ADS)

    Naqui, J.; Su, L.; Mata, J.; Martín, F.

    2015-06-01

    This paper is focused on the analysis of transmission lines loaded with pairs of magnetically coupled resonators. We have considered two different structures: (i) a microstrip line loaded with pairs of stepped impedance resonators (SIRs), and (ii) a coplanar waveguide (CPW) transmission line loaded with pairs of split ring resonators (SRRs). In both cases, the line exhibits a single resonance frequency (transmission zero) if the resonators are identical (symmetric structure with regard to the line axis), and this resonance is different to the one of the line loaded with a single resonator due to inter-resonator coupling. If the structures are asymmetric, inter-resonator coupling enhances the distance between the two split resonance frequencies that arise. In spite that the considered lines and loading resonators are very different and are described by different lumped element equivalent circuit models, the phenomenology associated to the effects of coupling is exactly the same, and the resonance frequencies are given by identical expressions. The reported lumped element circuit models of both structures are validated by comparing the circuit simulations with extracted parameters with both electromagnetic simulations and experimental data. These structures can be useful for the implementation of microwave sensors based on symmetry properties.

  7. Extraction of carboxylic acids by amine extractants

    SciTech Connect

    Tamada, Janet Ayako; King, C.J.

    1989-01-01

    This work examines the chemistry of solvent extraction by long-chain amines for recovery of carboxylic acids from dilute aqueous solution. Long-chain amines act as complexing agents with the acid, which facilitates distribution of the acid into the organic phase. The complexation is reversible, allowing for recovery of the acid from the organic phase and regeneration of the extractant. Batch extraction experiments were performed to study the complexation of acetic, lactic, succinic, malonic, fumaric, and maleic acids with Alamine 336, an aliphatic, tertiary amine extractant, dissolved in various diluents. Results were interpreted by a ''chemical'' model, in which stoichiometric ratios of acid and amine molecules are assumed to form complexes in the solvent phase. From fitting of the extraction data, the stoichiometry of complexes formed and the corresponding equilibrium constants were obtained. The results of the model were combined with infrared spectroscopic experiments and results of past studies to analyze the chemical interactions that are responsible for extraction behavior. The information from the equilibrium studies was used to develop guidelines for large-scale staged extraction and regeneration schemes. A novel scheme, in which the diluent composition is shifted between extraction and regeneration, was developed which could achieve both high solute recovery and high product concentration. 169 refs., 57 figs., 15 tabs.

  8. Width of nonlinear resonance

    SciTech Connect

    Ohnuma, S.

    1984-03-01

    Two approximations are made, one essential and the other not so essential but convenient to keep the analytical treatment manageable: (1) Only one nonlinear resonance is considered at a time so that the treatment is best suited when the tune is close to one resonance only. To improve this approximation, one must go to the next order which involves a canonical transformation of dynamical variables. Analytical treatment of more than one resonance is not possible for general cases. (2) In the formalism using the action-angle variables, the Hamiltonian can have terms which are independent of the angle variables. These terms are called phase-independent terms or shear terms. The tune is then a function of the oscillation amplitudes. In the lowest-order treatment, the (4N)-pole components but not the (4N + 2)-pole components contribute to this dependence. In deriving the resonance width analytically, one ignores these terms in the Hamiltonian for the sake of simplicity. If these are retained, one needs at least three extra parameters and the analytical treatment becomes rather unwieldy.

  9. Double resonator cantilever accelerometer

    DOEpatents

    Koehler, Dale R.

    1984-01-01

    A digital quartz accelerometer includes a pair of spaced double-ended tuning forks fastened at one end to a base and at the other end through a spacer mass. Transverse movement of the resonator members stresses one and compresses the other, providing a differential frequency output which is indicative of acceleration.

  10. Double resonator cantilever accelerometer

    DOEpatents

    Koehler, D.R.

    1982-09-23

    A digital quartz accelerometer includes a pair of spaced double-ended tuning forks fastened at one end to a base and at the other end through a spacer mass. Transverse movement of the resonator members stresses one and compresses the other, providing a differential frequency output which is indicative of acceleration.

  11. Single spin magnetic resonance

    NASA Astrophysics Data System (ADS)

    Wrachtrup, Jörg; Finkler, Amit

    2016-08-01

    Different approaches have improved the sensitivity of either electron or nuclear magnetic resonance to the single spin level. For optical detection it has essentially become routine to observe a single electron spin or nuclear spin. Typically, the systems in use are carefully designed to allow for single spin detection and manipulation, and of those systems, diamond spin defects rank very high, being so robust that they can be addressed, read out and coherently controlled even under ambient conditions and in a versatile set of nanostructures. This renders them as a new type of sensor, which has been shown to detect single electron and nuclear spins among other quantities like force, pressure and temperature. Adapting pulse sequences from classic NMR and EPR, and combined with high resolution optical microscopy, proximity to the target sample and nanoscale size, the diamond sensors have the potential to constitute a new class of magnetic resonance detectors with single spin sensitivity. As diamond sensors can be operated under ambient conditions, they offer potential application across a multitude of disciplines. Here we review the different existing techniques for magnetic resonance, with a focus on diamond defect spin sensors, showing their potential as versatile sensors for ultra-sensitive magnetic resonance with nanoscale spatial resolution.

  12. Magnetoelectric resonance engine

    SciTech Connect

    Moscrip, W.M.

    1992-09-15

    This patent describes a magnetoelectric resonance thermal machine. It comprises a reciprocating, multiple-piston, Alpha-type Stirling-cycle mechanical assembly; an electronic quadrature phase-lock circuit; an ancillary external energy and mass transfer subsystem; and a master microcomputer control system.

  13. Functional Magnetic Resonance Imaging

    ERIC Educational Resources Information Center

    Voos, Avery; Pelphrey, Kevin

    2013-01-01

    Functional magnetic resonance imaging (fMRI), with its excellent spatial resolution and ability to visualize networks of neuroanatomical structures involved in complex information processing, has become the dominant technique for the study of brain function and its development. The accessibility of in-vivo pediatric brain-imaging techniques…

  14. Improved ultraviolet resonance lamp

    NASA Technical Reports Server (NTRS)

    Bass, A. M.

    1970-01-01

    Removal of the seal area from the path of the lamp discharge eliminates the gradual deterioration of lithium fluoride window surfaces from condensation of products formed by interaction of a resonant rare-gas discharge with window sealing materials. The discharge is confined to the inner tube.

  15. Micromachined double resonator

    NASA Technical Reports Server (NTRS)

    Gutierrez, Roman (Inventor); Tang, Tony K. (Inventor); Shcheglov, Kirill (Inventor)

    2002-01-01

    A micromachined resonator mountable to an external support structure has a proof mass coupled to a base structure by a first spring structure, the base structure having a plurality of electrodes, and a second spring structure coupling the base structure to the external support structure.

  16. Magnetic resonance imaging

    SciTech Connect

    Stark, D.D.; Bradley, W.G. Jr.

    1988-01-01

    The authors present a review of magnetic resonance imaging. Many topics are explored from instrumentation, spectroscopy, blood flow and sodium imaging to detailed clinical applications such as the differential diagnosis of multiple sclerosis or adrenal adenoma. The emphasis throughout is on descriptions of normal multiplanar anatomy and pathology as displayed by MRI.

  17. Proton resonance spectroscopy

    SciTech Connect

    Shriner, J.F. Jr.

    1991-11-01

    This report discusses the following topics: Complete Level Scheme for {sup 30}P; A Search for Resonances Suitable for Tests of Detailed-Balance Violation; The Fourier Transform as a Tool for Detecting Chaos; Entrance Channel Correlations in p + {sup 27}Al; The Parity Dependence of Level Densities in {sup 49}V; and A Computer Program for the Calculation of Angular Momentum Coupling.

  18. Magnetic Resonance Annual, 1985

    SciTech Connect

    Kressel, H.Y.

    1985-01-01

    The inaugural volume of Magnetic Resonance Annual includes reviews of MRI of the posterior fossa, cerebral neoplasms, and the cardiovascular and genitourinary systems. A chapter on contrast materials outlines the mechanisms of paramagnetic contrast enhancement and highlights several promising contrast agents.

  19. Screening Resonances In Plasmas

    SciTech Connect

    Winkler, P.

    1998-12-01

    When it was suggested that a new recombination mechanism (Resonant Radiative Recombination (RRR)) which, based on very general physical arguments, should happen in dense plasmas and promises to provide useful information for the local temperature and density diagnostics of plasmas, they assumed the existence of screening resonances. For model potentials the existence of screening resonances has been demonstrated beyond reasonable doubt in a number of calculations. The key question, how well those potentials describe the dominant effects of a real plasma remains open. The relation of theoretical predictions to experimentally measurable effects is an important issue at the present stage of their research. In particular, RRR is expected to account for enhanced recombination rates of low energetic electrons with their ions, since the first stage is the resonant capture of a slow electron by an atom or ion. The mechanism that traps an electron is a combination of complicated many-body interactions of the ions and electrons. For clarity they start here, however, with a discussion in terms of local potential traps the shapes of which are determined predominantly and in an average way by two factors: the degree of screening present at the ionic site and the degree of short-range order in the immediate neighborhood of this ion.

  20. Single spin magnetic resonance.

    PubMed

    Wrachtrup, Jörg; Finkler, Amit

    2016-08-01

    Different approaches have improved the sensitivity of either electron or nuclear magnetic resonance to the single spin level. For optical detection it has essentially become routine to observe a single electron spin or nuclear spin. Typically, the systems in use are carefully designed to allow for single spin detection and manipulation, and of those systems, diamond spin defects rank very high, being so robust that they can be addressed, read out and coherently controlled even under ambient conditions and in a versatile set of nanostructures. This renders them as a new type of sensor, which has been shown to detect single electron and nuclear spins among other quantities like force, pressure and temperature. Adapting pulse sequences from classic NMR and EPR, and combined with high resolution optical microscopy, proximity to the target sample and nanoscale size, the diamond sensors have the potential to constitute a new class of magnetic resonance detectors with single spin sensitivity. As diamond sensors can be operated under ambient conditions, they offer potential application across a multitude of disciplines. Here we review the different existing techniques for magnetic resonance, with a focus on diamond defect spin sensors, showing their potential as versatile sensors for ultra-sensitive magnetic resonance with nanoscale spatial resolution. PMID:27378060

  1. Resonance Ionization, Mass Spectrometry.

    ERIC Educational Resources Information Center

    Young, J. P.; And Others

    1989-01-01

    Discussed is an analytical technique that uses photons from lasers to resonantly excite an electron from some initial state of a gaseous atom through various excited states of the atom or molecule. Described are the apparatus, some analytical applications, and the precision and accuracy of the technique. Lists 26 references. (CW)

  2. RESONANT CAVITY EXCITATION SYSTEM

    DOEpatents

    Baker, W.R.

    1959-08-01

    A cavity excitation circuit is described for rapidly building up and maintaining high-level oscillations in a resonant cavity. The circuit overcomes oscillation buildup slowing effects such as ion locking in the cavity by providing for the selective application of an amplified accelerating drive signal to the main cavity exciting oscillator during oscillation buildup and a direct drive signal to the oscillator thereafter.

  3. RESONATOR PARTICLE SEPARATOR

    DOEpatents

    Blewett, J.P.; Kiesling, J.D.

    1963-06-11

    A wave-guide resonator structure is designed for use in separating particles of equal momentum but differing in mass, having energies exceeding one billion eiectron volts. The particles referred to are those of sub-atomic size and are generally produced as a result of the bombardment of a target by a beam such as protons produced in a high energy accelerator. In the resonator a travelling electric wave is produced which travels at the same rate of speed as the unwanted particle which is thus deflected continuously over the length of the resonator. The wanted particle is slightly out of phase with the travelling wave so that over the whole length of the resonator it has a net deflection of substantially zero. The travelling wave is established in a wave guide of rectangular cross section in which stubs are provided to store magnetic wave energy leaving the electric wave energy in the main structure to obtain the desired travelling wave and deflection. The stubs are of such shape and spacing to establish a critical mathemitical relationship. (AEC)

  4. Experiment study of an electron cyclotron resonant ion source based on a tapered resonance cavity

    NASA Astrophysics Data System (ADS)

    Yang, Juan; Shi, Feng; Jin, Yizhou; Wang, Yunmin; Komurasaki, Kimiya

    2013-12-01

    Electron cyclotron resonant plasma is one type of magnetised plasma generated by continuous microwave energy. It has the property of high degree of ionization and large volume at low gas pressure, which makes it useful for space propulsion and material processing. This article presents the experiment study of the plasma properties and ion beam extraction from an electron cyclotron resonant ion source based on a tapered resonance cavity. Optical emission spectroscopy based on a simple collisional radiation model was used for plasma diagnosis. Experiment results show that, at microwave power setting ranging from 7.06 to 17.40 W and mass flow rate ranging from 1 to 10 sccm, argon gas can be ionized. Ion beam of 109.1 mA from the ion source can be extracted at microwave power of 30 W, mass flow rate of 10 sccm, and accel voltage of 800 V. The diagnosed plasma temperature and density are 2.4-5.2 eV and 2 × 1016-4.8 × 1017 m-3, respectively.

  5. Experiment study of an electron cyclotron resonant ion source based on a tapered resonance cavity

    SciTech Connect

    Yang, Juan; Shi, Feng; Jin, Yizhou; Wang, Yunmin; Komurasaki, Kimiya

    2013-12-15

    Electron cyclotron resonant plasma is one type of magnetised plasma generated by continuous microwave energy. It has the property of high degree of ionization and large volume at low gas pressure, which makes it useful for space propulsion and material processing. This article presents the experiment study of the plasma properties and ion beam extraction from an electron cyclotron resonant ion source based on a tapered resonance cavity. Optical emission spectroscopy based on a simple collisional radiation model was used for plasma diagnosis. Experiment results show that, at microwave power setting ranging from 7.06 to 17.40 W and mass flow rate ranging from 1 to 10 sccm, argon gas can be ionized. Ion beam of 109.1 mA from the ion source can be extracted at microwave power of 30 W, mass flow rate of 10 sccm, and accel voltage of 800 V. The diagnosed plasma temperature and density are 2.4–5.2 eV and 2 × 10{sup 16}–4.8 × 10{sup 17} m{sup −3}, respectively.

  6. Energy saver prototype accelerating resonator

    SciTech Connect

    Kerns, Q.; May, M.; Miller, H.W.; Reid, J.; Turkot, F.; Webber, R.; Wildman, D.

    1981-06-01

    A fixed frequency rf accelerating resonator has been built and tested for the Fermilab Energy Saver. The design parameters and prototype resonator test results are given. The resonator features a high permeability nickel alloy resistor which damps unwanted modes and corona rolls designed with the aid of the computer code SUPERFISH. In bench measurements, the prototype resonator has achieved peak accelerating voltages of 500 kV for a 1% duty cycle and cw operation at 360 kV. 4 refs.

  7. Microwave Resonators Containing Diamond Disks

    NASA Technical Reports Server (NTRS)

    Dick, G. John; Maleki, Lutfollah; Wang, Rabi T.

    1996-01-01

    Synthetic diamond dielectric bodies proposed for use in cylindrical resonators helping to stabilize frequencies of some microwave oscillators. Acting in conjunction with metal resonator cavities in which mounted, such dielectric bodies support "whispering-gallery" waveguide modes characterized by desired frequencies of resonance and by electro-magnetic-field configurations limiting dissipation of power on metal surfaces outside dielectric bodies. Performances at room temperature might exceed those of liquid-nitrogen-cooled sapphire-based resonators.

  8. Exhaustive extraction of peptides by electromembrane extraction.

    PubMed

    Huang, Chuixiu; Gjelstad, Astrid; Pedersen-Bjergaard, Stig

    2015-01-01

    This fundamental work illustrates for the first time the possibility of exhaustive extraction of peptides using electromembrane extraction (EME) under low system-current conditions (<50 μA). Bradykinin acetate, angiotensin II antipeptide, angiotensin II acetate, neurotensin, angiotensin I trifluoroacetate, and leu-enkephalin were extracted from 600 μL of 25 mM phosphate buffer (pH 3.5), through a supported liquid membrane (SLM) containing di-(2-ethylhexyl)-phosphate (DEHP) dissolved in an organic solvent, and into 600 μL of an acidified aqueous acceptor solution using a thin flat membrane-based EME device. Mass transfer of peptides across the SLM was enhanced by complex formation with the negatively charged DEHP. The composition of the SLM and the extraction voltage were important factors influencing recoveries and current with the EME system. 1-nonanol diluted with 2-decanone (1:1 v/v) containing 15% (v/v) DEHP was selected as a suitable SLM for exhaustive extraction of peptides under low system-current conditions. Interestingly, increasing the SLM volume from 5 to 10 μL was found to be beneficial for stable and efficient EME. The pH of the sample strongly affected the EME process, and pH 3.5 was found to be optimal. The EME efficiency was also dependent on the acceptor solution composition, and the extraction time was found to be an important element for exhaustive extraction. When EME was carried out for 25 min with an extraction voltage of 15 V, the system-current across the SLM was less than 50 μA, and extraction recoveries for the model peptides were in the range of 77-94%, with RSD values less than 10%. PMID:25467476

  9. Update on beam extraction

    SciTech Connect

    Keller, L.P.

    1983-08-26

    At the time of the 1981 Workshop on Experimental Use of the SLC, we published an extraction scheme for the MINIQUAD final focus (FF) optics. Since then a different FF optics design has been selected. With the same achromat section and outboard telescope, it allows a number of options for the inboard telescope. This note describes the new extraction system and briefly considers electron-electron extraction and the consequences of an extraction kicker malfunction. 4 references, 7 figures, 1 table.

  10. Method of infusion extraction

    NASA Technical Reports Server (NTRS)

    Chang-Diaz, Franklin R. (Inventor)

    1989-01-01

    Apparatus and method of removing desirable constituents from an infusible material by infusion extraction, where a piston operating in a first chamber draws a solvent into the first chamber where it may be heated, and then moves the heated solvent into a second chamber containing the infusible material, and where infusion extraction takes place. The piston then moves the solvent containing the extract through a filter into the first chamber, leaving the extraction residue in the second chamber.