Science.gov

Sample records for temperature creep deformation

  1. Tantalum alloys resist creep deformation at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Buckman, R. W., Jr.

    1966-01-01

    Dispersion-strengthened tantalum-base alloys possess high strength and good resistance to creep deformation at elevated temperatures in high vacuum environments. They also have ease of fabrication, good weldability, and corrosion resistance to molten alkali metals.

  2. Features of the low-temperature creep of a Nb-Ti alloy after large plastic deformations at 77 K

    NASA Astrophysics Data System (ADS)

    Aksenov, V. K.; Volchok, O. I.; Karaseva, E. V.; Starodubov, Ya. D.

    2004-04-01

    The low-temperature (77 K) creep and the corresponding changes in the resistivity of a niobium-titanium alloy subjected to plastic deformation by drawing at 77 K are investigated. It is shown that after large plastic deformations (ɛ>99%) one observes anomalies of the low-temperature creep which do not appear in tests of samples subjected to low and medium deformations. The creep rate in the transient stage is significantly higher than would follow from the classical ideas about the mechanisms of low-temperature creep (logarithmic law), and the time dependence of the creep deformations is described by a power law, which corresponds to recovery creep. In the creep process oscillations appear on the resistivity curves; these are especially pronounced after drawing in liquid nitrogen. Possible causes of the observed effects are discussed.

  3. Time-, stress-, and temperature-dependent deformation in nanostructured copper: Creep tests and simulations

    NASA Astrophysics Data System (ADS)

    Yang, Xu-Sheng; Wang, Yun-Jiang; Zhai, Hui-Ru; Wang, Guo-Yong; Su, Yan-Jing; Dai, L. H.; Ogata, Shigenobu; Zhang, Tong-Yi

    2016-09-01

    In the present work, we performed experiments, atomistic simulations, and high-resolution electron microscopy (HREM) to study the creep behaviors of the nanotwinned (nt) and nanograined (ng) copper at temperatures of 22 °C (RT), 40 °C, 50 °C, 60 °C, and 70 °C. The experimental data at various temperatures and different sustained stress levels provide sufficient information, which allows one to extract the deformation parameters reliably. The determined activation parameters and microscopic observations indicate transition of creep mechanisms with variation in stress level in the nt-Cu, i.e., from the Coble creep to the twin boundary (TB) migration and eventually to the perfect dislocation nucleation and activities. The experimental and simulation results imply that nanotwinning could be an effective approach to enhance the creep resistance of twin-free ng-Cu. The experimental creep results further verify the newly developed formula (Yang et al., 2016) that describes the time-, stress-, and temperature-dependent plastic deformation in polycrystalline copper.

  4. Microstructures of beta silicon carbide after irradiation creep deformation at elevated temperatures

    SciTech Connect

    Katoh, Yutai; Kondo, Sosuke; Snead, Lance Lewis

    2008-01-01

    Microstructures of silicon carbide were examined by transmission electron microscopy (TEM) after creep deformation under neutron irradiation. Thin strip specimens of polycrystalline and monocrystalline, chemically vapor-deposited, beta-phase silicon carbide were irradiated in the high flux isotope reactor to 0.7-4.2 dpa at nominal temperatures of 640-1080 C in an elastically pre-strained bend stress relaxation configuration with the initial stress of {approx}100 MPa. Irradiation creep caused permanent strains of 0.6 to 2.3 x 10{sup -4}. Tensile-loaded near-surface portions of the crept specimens were examined by TEM. The main microstructural features observed were dislocation loops in all samples, and appeared similar to those observed in samples irradiated in non-stressed conditions. Slight but statistically significant anisotropy in dislocation loop microstructure was observed in one irradiation condition, and accounted for at least a fraction of the creep strain derived from the stress relaxation. The estimated total volume of loops accounted for 10-45% of the estimated total swelling. The results imply that the early irradiation creep deformation of SiC observed in this work was driven by anisotropic evolutions of extrinsic dislocation loops and matrix defects with undetectable sizes.

  5. Creep Deformation of Allvac 718Plus

    NASA Astrophysics Data System (ADS)

    Hayes, Robert W.; Unocic, Raymond R.; Nasrollahzadeh, Maryam

    2015-01-01

    The creep deformation behavior of Allvac 718Plus was studied over the temperature range of 923 K to 1005 K (650 °C to 732 °C) at initial applied stress levels ranging from 517 to 655 MPa. Over the entire experimental temperature-stress regime this alloy exhibits Class M-type creep behavior with all creep curves exhibiting a decelerating strain rate with strain or time throughout primary creep. However, unlike pure metals or simple solid solution alloys, this gamma prime strengthened superalloy does not exhibit steady-state creep. Rather, primary creep is instantly followed by a long duration of accelerating strain rate with strain or time. These creep characteristics are common among the gamma prime strengthened superalloys. Allvac 718Plus also exhibits a very high temperature dependence of creep rate. Detailed TEM examination of the deformation structures of selected creep samples reveals dislocation mechanisms similar to those found in high volume fraction gamma prime strengthened superalloys. Strong evidence of microtwinning is found in several of the deformation structures. The presence of microtwinning may account for the strong temperature dependence of creep rate observed in this alloy. In addition, due to the presence of Nb and thus, grain boundary delta phase, matrix dislocation activity which is not present in non-Nb-bearing superalloys occurs in this alloy. The creep characteristics and dislocation mechanisms are presented and discussed in detail.

  6. Creep Deformation of Allvac 718Plus

    DOE PAGESBeta

    Hayes, Robert W.; Unocic, Raymond R.; Nasrollahzadeh, Maryam

    2014-11-11

    The creep deformation behavior of Allvac 718Plus was studied over the temperature range 650° to 732°C at initial applied stress levels ranging from 517 to 655 MPa. Over the entire experimental temperature stress regime this alloy exhibits Class M type creep behavior with all creep curves exhibiting a decelerating strain rate with strain or time throughout primary creep. However, unlike pure metals or simple solid solution alloys this gamma prime strengthened superalloy does not exhibit steady state creep. Rather, primary creep is instantly followed by a long duration of accelerating strain rate with strain or time. These creep characteristics aremore » common amongst the gamma prime strengthened superalloys. Allvac 718Plus also exhibits a very high temperature dependence of creep rate. Detailed TEM examination of the deformation structures of selected creep samples reveals dislocation mechanisms similar to those found in high volume fraction gamma prime strengthened superalloys. Strong evidence of microtwinning is found in several of the deformation structures. The presence of microtwinning may account for the strong temperature dependence of creep rate observed in this alloy. In addition, due to the presence of Nb and thus, grain boundary delta phase, matrix dislocation activity which is not present in non Nb bearing superalloys occurs in this alloy. The creep characteristics and dislocation mechanisms are presented and discussed in detail.« less

  7. Creep Deformation of Allvac 718Plus

    SciTech Connect

    Hayes, Robert W.; Unocic, Raymond R.; Nasrollahzadeh, Maryam

    2014-11-11

    The creep deformation behavior of Allvac 718Plus was studied over the temperature range 650° to 732°C at initial applied stress levels ranging from 517 to 655 MPa. Over the entire experimental temperature stress regime this alloy exhibits Class M type creep behavior with all creep curves exhibiting a decelerating strain rate with strain or time throughout primary creep. However, unlike pure metals or simple solid solution alloys this gamma prime strengthened superalloy does not exhibit steady state creep. Rather, primary creep is instantly followed by a long duration of accelerating strain rate with strain or time. These creep characteristics are common amongst the gamma prime strengthened superalloys. Allvac 718Plus also exhibits a very high temperature dependence of creep rate. Detailed TEM examination of the deformation structures of selected creep samples reveals dislocation mechanisms similar to those found in high volume fraction gamma prime strengthened superalloys. Strong evidence of microtwinning is found in several of the deformation structures. The presence of microtwinning may account for the strong temperature dependence of creep rate observed in this alloy. In addition, due to the presence of Nb and thus, grain boundary delta phase, matrix dislocation activity which is not present in non Nb bearing superalloys occurs in this alloy. The creep characteristics and dislocation mechanisms are presented and discussed in detail.

  8. Creep Deformation of B2 Alumindes

    NASA Technical Reports Server (NTRS)

    Nathal, M. V.

    1991-01-01

    The creep resistance and elevated temperature deformation mechanisms in CoAl, FeAl, and NiAl are reviewed. The stress and temperature dependencies of the steady state creep rate, the primary creep behavior, the dislocation substructure, and the response during transient tests are used as the main indicators of the deformation processes. In single phase intermetallics, the influence of grain size, stoichiometry, and solid solution hardening have been examined. In addition, the effect of adding dispersoids, precipitates, and other types of reinforcements to improve creep strength are compared.

  9. Dislocation creep accommodated Grain Boundary Sliding: A high strain rate/low temperature deformation mechanism in calcite ultramylonites

    NASA Astrophysics Data System (ADS)

    Rogowitz, Anna; Grasemann, Bernhard

    2014-05-01

    Grain boundary sliding (GBS) is an important grain size sensitive deformation mechanism that is often associated with extreme strain localization and superplasticity. Another mechanism has to operate simultaneously to GBS in order to prevent overlaps and voids between sliding grains. One of the most common accommodating mechanisms is diffusional creep but, recently, dislocation creep has been reported to operate simultaneous to GBS. Due to the formation of a flanking structure in nearly pure calcite marble on Syros (Cyclades, Greece) at lower greenschist facies conditions, an extremely fine grained ultramylonite developed. The microstructure of the layer is characterized by (1) calcite grains with an average grain size of 3.6 µm (developed by low temperature/high strain rate grain boundary migration recrystallization, BLG), (2) grain boundary triple junctions with nearly 120° angles and (3) small cavities preferentially located at triple junctions and at grain boundaries in extension. These features suggest that the dominant deformation mechanism was GBS. In order to get more information on the accommodation mechanism detailed microstructural and textural analyses have been performed on a FEI Quanta 3D FEG instrument equipped with an EDAX Digiview IV EBSD camera. The misorientation distribution curves for correlated and uncorrelated grains follow almost perfect the calculated theoretical curve for a random distribution, which is typical for polycrystalline material deformed by GBS. However, the crystallographic preferred orientation indicates that dislocation creep might have operated simultaneously. We also report Zener-Stroh cracks resulting from dislocation pile up, indicating that dislocation movement was active. We, therefore, conclude that the dominant deformation mechanism was dislocation creep accommodated grain boundary sliding. This is consistent with the observed grain size range that plots at the field boundary between grain size insensitive and grain

  10. Elevated Temperature Creep Deformation in Solid Solution <001> NiAL-3.6Ti Single Crystals

    NASA Technical Reports Server (NTRS)

    Whittenberger, J. Daniel; Noebe, Ronald D.; Darolia, Ram

    2003-01-01

    The 1100 to 1500 K slow plastic strain rate compressive properties of <001> oriented NiAl-3.6Ti single crystals have been measured, and the results suggests that two deformation processes exist. While the intermediate temperature/faster strain rate mechanism is uncertain, plastic flow at elevated temperature/slower strain rates in NiAl-3.6Ti appears to be controlled by solute drag as described by the Cottrell-Jaswon solute drag model for gliding b = a(sub 0)<101> dislocations. While the calculated activation energy of deformation is much higher (approximately 480 kJ/mol) than the activation energy for diffusion (approximately 290 kJ/mol) used in the Cottrell-Jaswon creep model, a forced temperature compensated - power law fit using the activation energy for diffusion was able to adequately (greater than 90%) predict the observed creep properties. Thus we conclude that the rejection of a diffusion controlled mechanism can not be simply based on a large numerical difference between the activation energies for deformation and diffusion.

  11. High-temperature measurements of lattice parameters and internal stresses of a creep-deformed monocrystalline nickel-base superalloy

    NASA Astrophysics Data System (ADS)

    Biermann, Horst; Strehler, Marcus; Mughrabi, Haël

    1996-04-01

    High-temperature X-ray line profile measurements were performed to maximal temperatures of 1050 °C on samples of the nickel-base superalloy SRR 99. The samples with rod axes near the [001] direction were investigated in the initially undeformed state and after creep deformation at different temperatures and stresses. For the measurements of the (002) and (020) line profiles, a special X-ray double crystal diffractometer with negligible line broadening was used which was equipped with a high-temperature vacuum chamber. The line profiles were evaluated for the lattice parameters of the matrix phase γ and the precipitated γ' phase and for values of the lattice mismatch parallel and perpendicular to the stress axis, respectively, which were found to be different. Elastic, tetragonal distortions of the phases γ and γ' could be determined between room temperature and about 900 °C. These distortions are thermally induced due to the different thermal expansion coefficients of the two phases and deformation induced due to interfacial dislocation networks which were built up during deformation. At the high temperatures of the X-ray measurements, at least partial recovery of the deformation-induced internal stresses occurred, depending on the temperature of the X-ray measurements. The results are discussed and compared with data obtained by complementary techniques.

  12. On The Creep Behavior and Deformation Mechanisms Found in an Advanced Polycrystalline Nickel-Base Superalloy at High Temperatures

    NASA Astrophysics Data System (ADS)

    Deutchman, Hallee Zox

    Polycrystalline Ni-base superalloys are used as turbine disks in the hot section in jet engines, placing them in a high temperature and stress environment. As operating temperatures increase in search of better fuel efficiency, it becomes important to understand how these higher temperatures are affecting mechanical behavior and active deformation mechanisms in the substructure. Not only are operating temperatures increasing, but there is a drive to design next generation alloys in shorter time periods using predictive modeling capabilities. This dissertation focuses on mechanical behavior and active deformation mechanisms found in two different advanced polycrystalline alloy systems, information which will then be used to build advanced predictive models to design the next generation of alloys. The first part of this dissertation discusses the creep behavior and identifying active deformation mechanisms in an advanced polycrystalline Ni-based superalloy (ME3) that is currently in operation, but at higher temperatures and stresses than are experienced in current engines. Monotonic creep tests were run at 700°C and between 655-793MPa at 34MPa increments, on two microstructures (called M1 and M2) produced by different heat treatments. All tests were crept to 0.5% plastic strain. Transient temperature and transient stress tests were used determine activation energy and stress exponents of the M1 microstructure. Constant strain rate tests (at 10-4s-1) were performed on both microstructures as well. Following creep testing, both M1 and M2 microstructures were fully characterized using Scanning Electron Microscopy (SEM) for basic microstructure information, and Scanning Transmission Electron Microscopy (STEM) to determine active deformation mechanism. It was found that in the M1 microstructure, reorder mediated activity (such as discontinuous faulting and microtwinning) is dominant at low stresses (655-724 MPa). Dislocations in the gamma matrix, and overall planar

  13. The high temperature creep deformation of Si3N4-6Y2O3-2Al2O3

    NASA Technical Reports Server (NTRS)

    Todd, J. A.; Xu, Zhi-Yue

    1988-01-01

    The creep properties of silicon nitride containing 6 wt percent yttria and 2 wt percent alumina have been determined in the temperature range 1573 to 1673 K. The stress exponent, n, in the equation epsilon dot varies as sigma sup n, was determined to be 2.00 + or - 0.15 and the true activation energy was found to be 692 + or - 25 kJ/mol. Transmission electron microscopy studies showed that deformation occurred in the grain boundary glassy phase accompanied by microcrack formation and cavitation. The steady state creep results are consistent with a diffusion controlled creep mechanism involving nitrogen diffusion through the grain boundary glassy phase.

  14. Room temperature creep in metals and alloys

    SciTech Connect

    Deibler, Lisa Anne

    2014-09-01

    Time dependent deformation in the form of creep and stress relaxation is not often considered a factor when designing structural alloy parts for use at room temperature. However, creep and stress relaxation do occur at room temperature (0.09-0.21 Tm for alloys in this report) in structural alloys. This report will summarize the available literature on room temperature creep, present creep data collected on various structural alloys, and finally compare the acquired data to equations used in the literature to model creep behavior. Based on evidence from the literature and fitting of various equations, the mechanism which causes room temperature creep is found to include dislocation generation as well as exhaustion.

  15. Creep deformation mechanisms in modified 9Cr-1Mo steel

    NASA Astrophysics Data System (ADS)

    Shrestha, Triratna; Basirat, Mehdi; Charit, Indrajit; Potirniche, Gabriel P.; Rink, Karl K.; Sahaym, Uttara

    2012-04-01

    Modified 9Cr-1Mo (Grade 91) steel is currently considered as a candidate material for reactor pressure vessels (RPVs) and reactor internals for the Very High Temperature Reactor (VHTR). The tensile creep behavior of modified 9Cr-1Mo steel (Grade 91) was studied in the temperature range of 873-1023 K and stresses between 35 MPa and 350 MPa. Analysis of creep results yielded stress exponents of ∼9-11 in the higher stress regime and ∼1 in the lower stress regime. The high stress exponent in the power-law creep regime was rationalized by invoking the concept of threshold stress, which represents the lattice diffusion controlled dislocation climb process. Without threshold stress compensation, the activation energy was 510 ± 51 kJ/mol, while after correcting for the threshold stress, the activation energy decreased to 225 ± 24 kJ/mol. This value is close to the activation energy for lattice self-diffusion in α-Fe. Threshold stress calculations were performed for the high stress regime at all test temperatures. The calculated threshold stress showed a strong dependence on temperature. The creep behavior of Grade 91 steel was described by the modified Bird-Mukherjee-Dorn relation. The rate controlling creep deformation mechanism in the high stress regime was identified as the edge dislocation climb with a stress exponent of n = 5. On the other hand, the deformation mechanism in the Newtonian viscous creep regime (n = 1) was identified as the Nabarro-Herring creep.

  16. Spatial fluctuations in transient creep deformation

    NASA Astrophysics Data System (ADS)

    Laurson, Lasse; Rosti, Jari; Koivisto, Juha; Miksic, Amandine; Alava, Mikko J.

    2011-07-01

    We study the spatial fluctuations of transient creep deformation of materials as a function of time, both by digital image correlation (DIC) measurements of paper samples and by numerical simulations of a crystal plasticity or discrete dislocation dynamics model. This model has a jamming or yielding phase transition, around which power law or Andrade creep is found. During primary creep, the relative strength of the strain rate fluctuations increases with time in both cases—the spatially averaged creep rate obeys the Andrade law epsilont ~ t - 0.7, while the time dependence of the spatial fluctuations of the local creep rates is given by Δepsilont ~ t - 0.5. A similar scaling for the fluctuations is found in the logarithmic creep regime that is typically observed for lower applied stresses. We review briefly some classical theories of Andrade creep from the point of view of such spatial fluctuations. We consider these phenomenological, time-dependent creep laws in terms of a description based on a non-equilibrium phase transition separating evolving and frozen states of the system when the externally applied load is varied. Such an interpretation is discussed further by the data collapse of the local deformations in the spirit of absorbing state/depinning phase transitions, as well as deformation-deformation correlations and the width of the cumulative strain distributions. The results are also compared with the order parameter fluctuations observed close to the depinning transition of the 2d linear interface model or the quenched Edwards-Wilkinson equation.

  17. Homogenized Creep Behavior of CFRP Laminates at High Temperature

    NASA Astrophysics Data System (ADS)

    Fukuta, Y.; Matsuda, T.; Kawai, M.

    In this study, creep behavior of a CFRP laminate subjected to a constant stress is analyzed based on the time-dependent homogenization theory developed by the present authors. The laminate is a unidirectional carbon fiber/epoxy laminate T800H/#3631 manufactured by Toray Industries, Inc. Two kinds of creep analyses are performed. First, 45° off-axis creep deformation of the laminate at high temperature (100°C) is analyzed with three kinds of creep stress levels, respectively. It is shown that the present theory accurately predicts macroscopic creep behavior of the unidirectional CFRP laminate observed in experiments. Then, high temperature creep deformations at a constant creep stress are simulated with seven kinds of off-axis angles, i.e., θ = 0°, 10°, 30°, 45°, 60°, 75°, 90°. It is shown that the laminate has marked in-plane anisotropy with respect to the creep behavior.

  18. Fluctuations and Scaling in Creep Deformation

    NASA Astrophysics Data System (ADS)

    Rosti, Jari; Koivisto, Juha; Laurson, Lasse; Alava, Mikko J.

    2010-09-01

    The spatial fluctuations of deformation are studied in the creep in Andrade’s power law and the logarithmic phases, using paper samples. Measurements by the digital image correlation technique show that the relative strength of the strain rate fluctuations increases with time, in both creep regimes. In the Andrade creep phase characterized by a power-law decay of the strain rate γt˜t-θ, with θ≈0.7, the fluctuations obey Δγt˜t-γ, with γ≈0.5. The local deformation follows a data collapse appropriate for a phase transition. Similar behavior is found in a crystal plasticity model, with a jamming or yielding transition.

  19. Deformation Microstructures and Creep Mechanisms in Advanced ZR-Based Cladding Under Biazal Loading

    SciTech Connect

    K. Linga Murty

    2008-08-11

    Investigate creep behavior of Zr-based cladding tubes with attention to basic creep mechanisms and transitions in them at low stresses and/or temperatures and study the dislocation microstructures of deformed samples for correlation with the underlying micromechanism of creep

  20. Mapping microscale strain heterogeneity during creep deformation

    NASA Astrophysics Data System (ADS)

    Quintanilla Terminel, A.; Evans, J.

    2013-12-01

    We use a new technique combining microfabrication technology and compression tests to map the strain field at a micrometric scale in polycrystalline materials. This technique allows us to map local strain while measuring macroscopic strain and rheological properties, and provides insight into the relative contribution of various plasticity mechanisms under varying creep conditions. The micro-strain mapping technique was applied to Carrara Marble under different deformation regimes, at 300 MPa and temperatures ranging from 200 to 700 °C. At 600 °C, strain of 10%, and strain rate of 3e-5s-1, the local strain at twin and grain boundaries is up to 5 times greater than the average sample strain. At these conditions, strains averaged across a particular grain may vary by as much as 100%, but the strain field becomes more homogeneous with increasing strain. For example, for the analyzed experiments, the average wavelength of the strain heterogeneity is 70 micrometers at 10% strain, but increases to 110 micrometers at 20%. For a strain of 10%, heterogeneity is increased at slower strain rate (at 1e-5s-1). This increase seems to be associated with a more important role of twin boundary and grain boundary migration. As expected, twin densities are markedly greater at the lower temperature, though it is still unclear whether the relative twin volume is greater. However, twin strains are still important at 600 °C and accommodate an average of 14 % of the total strain at 10% deformation and a strain rate of 3e-5s-1.

  1. Creep deformation of an unirradiated zircaloy nuclear fuel cladding tube under dry storage conditions

    NASA Astrophysics Data System (ADS)

    Mayuzumi, Masami; Onchi, Takeo

    1990-05-01

    Measurements of creep deformation were made on an internally gas pressurized tubular Zircaloy-4 specimen with plugs welded to its ends. Creep tests were conducted at temperatures between 577 and 693 K for holding times of up to 26640 ks, to formulate the creep equation needed for predicting creep strain during dry storage of spent fuel. Discussion was also given to the difference of creep behaviour between irradiated and unirradiated fuel cladding, indicating that the equation derived is applicable for predicting creep strain of spent fuel cladding during dry storage.

  2. Temperature, Thermal Stress, And Creep In A Structure

    NASA Technical Reports Server (NTRS)

    Jenkins, Jerald M.

    1991-01-01

    Report presents comparison of predicted and measured temperatures, thermal stresses, and residual creep stresses in heated and loaded titanium structure. Study part of continuing effort to develop design capability to predict and reduce deleterious effects of creep, which include excessive deformations, residual stresses, and failure.

  3. Analysis of Slip Activity and Deformation Modes in Tension and Tension-Creep Tests of Cast Mg-10Gd-3Y-0.5Zr (Wt Pct) at Elevated Temperatures Using In Situ SEM Experiments

    NASA Astrophysics Data System (ADS)

    Wang, Huan; Boehlert, Carl J.; Wang, Qudong; Yin, Dongdi; Ding, Wenjiang

    2016-05-01

    The tension and tension-creep deformation behavior at elevated temperatures of a cast Mg-10Gd-3Y-0.5Zr (wt pct, GW103) alloy was investigated using in situ scanning electron microscopy. The tests were performed at temperatures ranging from 473 K to 598 K (200 °C to 325 °C). The active slip systems were identified using an EBSD-based slip trace analysis methodology. The results showed that for all of the tests, basal slip was the most likely system to be activated, and non-basal slip was activated to some extent depending on the temperature. No twinning was observed. For the tension tests, non-basal slip consisted of ~35 pct of the deformation modes at low temperatures (473 K and 523 K (200 °C and 250 °C)), while non-basal slip accounted for 12 and 7 pct of the deformation modes at high temperatures (573 K and 598 K (300 °C and 325 °C)), respectively. For the tension-creep tests, non-basal slip accounted for 31 pct of the total slip systems at low temperatures, while this value decreased to 10 to 16 pct at high temperatures. For a given temperature, the relative activity for prismatic slip in the tension-creep tests was slightly greater than that for the tension tests, while the activity for pyramidal slip was lower. Slip-transfer in neighboring grains was observed for the low-temperature tests. Intergranular cracking was the main cracking mode, while some intragranular cracks were observed for the tension-creep tests at high temperature and low stress. Grain boundary ledges were prevalently observed for both the tension and tension-creep tests at high temperatures, which suggests that besides dislocation slip, grain boundary sliding also contributed to the deformation.

  4. Creep deformation behavior in eutectic Sn-Ag solder joints using a novel mapping technique

    SciTech Connect

    Lucas, J.P.; Guo, F.; McDougall, J.; Bieler, T.R.; Subramanian, K.N.; Park, J.K.

    1999-11-01

    Creep deformation behavior was measured for 60--100 {micro}m thick solder joints. The solder joints investigated consisted of: (1) non-composite solder joints made with eutectic Sn-Ag solder, and (2) composite solder joints with eutectic Sn-Ag solder containing 20 vol.%, 5 {micro}m diameter in-situ Cu{sub 6}Sn{sub 5} intermetallic reinforcements. All creep testing in this study was carried out at room temperature. Qualitative and quantitative assessment of creep deformation was characterized on the solder joints. Creep deformation was analyzed using a novel mapping technique where a geometrical-regular line pattern was etched over the entire solder joint using excimer laser ablation. During creep, the laser-ablation (LA) pattern becomes distorted due to deformation in the solder joint. By imaging the distortion of laser-ablation patterns using the SEM, actual deformation mapping for the entire solder joint is revealed. The technique involves sequential optical/digital imaging of the deformation versus time history during creep. By tracing and recording the deformation of the LA patterns on the solder over intervals of time, local creep data are obtained in many locations in the joint. This analysis enables global and localized creep shear strains and strain rate to be determined.

  5. A TEM Study of Creep Deformation Mechanisms in Allvac 718Plus

    SciTech Connect

    Unocic, Raymond R; Unocic, Kinga A; Hayes, Robert; Daehn, Glenn; Mills, Michael J.

    2010-01-01

    A preliminary study on the evolution of creep deformation substructure in Ni-base superalloy Allvac 718Plus has been performed. Specimens crept at 620 MPa and at temperatures ranging from 690-732 C were examined utilizing diffraction contrast TEM characterization techniques. Creep was interrupted at 1-2.5% strain in order to study the deformation substructure following a limited amount of deformation. The dominant deformation modes at each of the test temperatures were highly planar in nature and involved shearing of the matrix and precipitates on {111} glide planes. In addition, paired a/2<110> dislocations were evident which suggest an antiphase boundary shearing mechanism. Creep induced microtwinning was also observed at the highest creep temperature which was created by identical a/6<112> Shockley partial dislocations that shear the matrix and precipitates on consecutive close packed {111} glide planes.

  6. On the creep deformation mechanisms of an advanced disk nickel-base superalloy

    NASA Astrophysics Data System (ADS)

    Unocic, Raymond R.

    The main objective of this research was aimed at investigating the fundamental relationship between microstructure and creep deformation mechanisms using a variety of electron microscopy characterization techniques. The alloy used in this research, Rene 104, is a newer generation powder metallurgy Ni-base superalloy that was developed specifically for aircraft gas turbine disk applications with extended service durability at temperatures exceeding 650°C. The influence of stress and temperature was studied first and it was found that during creep deformation at temperatures between 677--815°C and stresses between 345--724MPa a variety of distinctly different creep deformation mechanisms were operative. In addition to identifying the creep deformation mechanisms an attempt was made to determine the creep rate limiting process so that an improved understanding of the fundamental processes that control deformation can be better understood. Microtwinning was found to the dominant deformation mechanism following creep at 677°C/690MPa and 704°C/724MPa. Microtwins form by the motion of paired a/6<112> Shockley partial dislocations that shear both the gamma matrix and gamma' precipitates. The rate limiting process in this mechanism is diffusion mediated atomic reordering that occurs in the wake of the shearing, twinning partial dislocations in order to maintain the ordered L12 structure of the gamma' precipitates. This reordering process helps to fundamentally explain the temperature and rate dependence of microtwinning under creep conditions within this temperature and stress regime. At a slightly higher temperature but lower stress (760°C and 345MPa), a stacking fault related shearing mechanism, which typically spanned only a few micrometers in length, was the principle deformation mode. The faults left behind in the gamma' precipitates determined to be extrinsic in nature. During creep at the highest temperature and lowest stress (815°C and 345MPa) a thermally

  7. Creep deformation of a soft magnetic iron-cobalt alloy

    NASA Astrophysics Data System (ADS)

    Fingers, R. T.; Coate, J. E.; Dowling, N. E.

    1999-04-01

    The U.S. Air Force is in the process of developing magnetic bearings, as well as an aircraft integrated power unit and an internal starter/generator for main propulsion engines. These developments are the driving force for the new emphasis on the development of high saturation, low loss magnets capable of maintaining structural integrity in high stress and high temperature environments. It is this combination of desired material characteristics that is the motivation of this effort to measure, model, and predict the creep behavior of such advanced magnetic materials. Hiperco® Alloy 50HS, manufactured by Carpenter Technology Corporation, is one of the leading candidates for these applications. Material specimens were subjected to a battery of mechanical tests in order to study and characterize their behaviors. Tensile tests provided stress versus strain behaviors that clearly indicated: a yield point, a heterogeneous deformation described as Lüders elongation, the Portevin-LeChatelier effect at elevated temperatures, and most often a section of homogeneous deformation that concluded with necking and fracture. Creep testing indicated three distinct types of behavior. Two types resembled a traditional response with primary, secondary, and tertiary stages; while the third type can be characterized by an abrupt increase in strain rate that acts as a transition from one steady-state behavior to another. The relationships between the tensile and creep responses are discussed. Analyses of the mechanical behavior include double linear regression of empirically modeled data, and constant strain rate testing to bridge the tensile and creep test parameters.

  8. Finite Element Analysis of Plastic Deformation During Impression Creep

    NASA Astrophysics Data System (ADS)

    Naveena; Ganesh Kumar, J.; Mathew, M. D.

    2015-04-01

    Finite element (FE) analysis of plastic deformation associated with impression creep deformation of 316LN stainless steel was carried out. An axisymmetric FE model of 10 × 10 × 10 mm specimen with 1-mm-diameter rigid cylindrical flat punch was developed. FE simulation of impression creep deformation was performed by assuming elastic-plastic-power-law creep deformation behavior. Evolution of the stress with time under the punch during elastic, plastic, and creep processes was analyzed. The onset of plastic deformation was found to occur at a nominal stress about 1.12 times the yield stress of the material. The size of the developed plastic zone was predicted to be about three times the radius of the punch. The material flow behavior and the pile-up on specimen surface have been modeled.

  9. A New Creep Constitutive Model for 7075 Aluminum Alloy Under Elevated Temperatures

    NASA Astrophysics Data System (ADS)

    Lin, Y. C.; Jiang, Yu-Qiang; Zhou, Hua-Min; Liu, Guan

    2014-12-01

    Exposure of aluminum alloy to an elastic loading, during "creep-aging forming" or other manufacturing processes at relatively high temperature, may lead to the lasting creep deformation. The creep behaviors of 7075 aluminum alloy are investigated by uniaxial tensile creep experiments over wide ranges of temperature and external stress. The results show that the creep behaviors of the studied aluminum alloy strongly depend on the creep temperature, external stress, and creep time. With the increase of creep temperature and external stress, the creep strain increases quickly. In order to overcome the shortcomings of the Bailey-Norton law and θ projection method, a new constitutive model is proposed to describe the variations of creep strain with time for the studied aluminum alloy. In the proposed model, the dependences of creep strain on the creep temperature, external stress, and creep time are well taken into account. A good agreement between the predicted and measured creep strains shows that the established creep constitutive model can give an accurate description of the creep behaviors of 7075 aluminum alloy. Meanwhile, the obtained stress exponent indicates that the creep process is controlled by the dislocation glide, which is verified by the microstructural observations.

  10. Experimental investigation of creep crack tip deformation using moire interferometry

    NASA Astrophysics Data System (ADS)

    Kang, B. S.-J.; Zhuang, Y.-N.

    High temperature moire interferometry was applied to obtain full-field creep crack tip displacements of a three-point bend Al 2024-T4 specimen under constant temperature of 200 C up to 720 hr. C* was evaluated by the moire data obtained at discrete time intervals. Test results indicated that under steady-state creep condition, the creep crack tip v-displacement rate agreed with the asymptotic solution based on C*-integral, however, no creeping behavior was observed for the crack tip u-displacement field after t = 276 hr. This discrepancy may be due to the initial large creep crack tip blunting and cavitation damage which alter the creep crack tip singular field such that the C*-integral is no longer applicable to characterize steady-state creep crack tip field. It is suggested that the size and shape of material grain boundaries may play an important role on the creeping behavior of the material.

  11. High-temperature creep of polycrystalline chromium

    NASA Technical Reports Server (NTRS)

    Stephens, J. R.; Klopp, W. D.

    1972-01-01

    The creep properties of high-purity, polycrystalline chromium were determined over the temperature range 0.51 to 0.78 T sub m, where T sub m is the melting temperature. Creep rates determined from step-load creep tests can be represented by the general creep equation; epsilon/D = k((sigma/E) to the nth power) where epsilon is the minimum creep rate, D is the diffusivity, k is the creep rate constant, sigma is the applied stress, E is the modulus, and n is the stress exponent, equal to 4.3 for chromium. This correlation and metallographic observations suggest a dislocation climb mechanism is operative in the creep of chromium over the temperature range investigated.

  12. Effect of Tungsten on Primary Creep Deformation and Minimum Creep Rate of Reduced Activation Ferritic-Martensitic Steel

    NASA Astrophysics Data System (ADS)

    Vanaja, J.; Laha, Kinkar; Mathew, M. D.

    2014-10-01

    Effect of tungsten on transient creep deformation and minimum creep rate of reduced activation ferritic-martensitic (RAFM) steel has been assessed. Tungsten content in the 9Cr-RAFM steel has been varied between 1 and 2 wt pct, and creep tests were carried out over the stress range of 180 and 260 MPa at 823 K (550 °C). The tempered martensitic steel exhibited primary creep followed by tertiary stage of creep deformation with a minimum in creep deformation rate. The primary creep behavior has been assessed based on the Garofalo relationship, , considering minimum creep rate instead of steady-state creep rate . The relationships between (i) rate of exhaustion of transient creep r' with minimum creep rate, (ii) rate of exhaustion of transient creep r' with time to reach minimum creep rate, and (iii) initial creep rate with minimum creep rate revealed that the first-order reaction-rate theory has prevailed throughout the transient region of the RAFM steel having different tungsten contents. The rate of exhaustion of transient creep r' and minimum creep rate decreased, whereas the transient strain ɛ T increased with increase in tungsten content. A master transient creep curve of the steels has been developed considering the variation of with . The effect of tungsten on the variation of minimum creep rate with applied stress has been rationalized by invoking the back-stress concept.

  13. Creep deformation characteristics of ductile discontinuous fiber reinforced composites

    SciTech Connect

    Biner, S.B.

    1993-10-01

    Role of material parameters and geometric parameters of ductile reinforcing phase on the creep deformation behavior of 20% discontinuously reinforced composite was numerically investigated including debonding and pull-out mechanisms. Results indicate that for rigidly bonded interfaces, the creep rate of the composite is not significantly influenced by the material properties and geometric parameters of the ductile reinforcing phase due to development of large hydrostatic stress and constrained deformation in the reinforcement. For debonding interfaces, the geometric parameters of the reinforcing phase are important; however, event with very weak interfacial behavior low composite creep rates can be achieved by suitable selection of the geometric parameters of the ductile reinforcing phase.

  14. Low Temperature Creep of Hot-Extruded Near-Stoichiometric NiTi Shape Memory Alloy. Part I; Isothermal Creep

    NASA Technical Reports Server (NTRS)

    Raj, S. V.; Noebe, R. D.

    2013-01-01

    This two-part paper is the first published report on the long term, low temperature creep of hot-extruded near-stoichiometric NiTi. Constant load tensile creep tests were conducted on hot-extruded near-stoichiometric NiTi at 300, 373 and 473 K under initial applied stresses varying between 200 and 350 MPa as long as 15 months. These temperatures corresponded to the martensitic, two-phase and austenitic phase regions, respectively. Normal primary creep lasting several months was observed under all conditions indicating dislocation activity. Although steady-state creep was not observed under these conditions, the estimated creep rates varied between 10(exp -10) and 10(exp -9)/s. The creep behavior of the two phases showed significant differences. The martensitic phase exhibited a large strain on loading followed by a primary creep region accumulating a small amount of strain over a period of several months. The loading strain was attributed to the detwinning of the martensitic phase whereas the subsequent strain accumulation was attributed to dislocation glide-controlled creep. An "incubation period" was observed before the occurrence of detwinning. In contrast, the austenitic phase exhibited a relatively smaller loading strain followed by a primary creep region, where the creep strain continued to increase over several months. It is concluded that the creep of the austenitic phase occurs by a dislocation glide-controlled creep mechanism as well as by the nucleation and growth of deformation twins.

  15. Threshold Stress Creep Behavior of Alloy 617 at Intermediate Temperatures

    SciTech Connect

    J.K. Benz; L.J. Carroll; J.K. Wright; R.N. Wright; T. Lillo

    2014-06-01

    Creep of Alloy 617, a solid solution Ni-Cr-Mo alloy, was studied in the temperature range of 1023 K to 1273 K (750 °C to 1000 °C). Typical power-law creep behavior with a stress exponent of approximately 5 is observed at temperatures from 1073 K to 1273 K (800 °C to 1000 °C). Creep at 1023 K (750 °C), however, exhibits threshold stress behavior coinciding with the temperature at which a low volume fraction of ordered coherent y' precipitates forms. The threshold stress is determined experimentally to be around 70 MPa at 1023 K (750 °C) and is verified to be near zero at 1173 K (900 °C)—temperatures directly correlating to the formation and dissolution of y' precipitates, respectively. The y' precipitates provide an obstacle to continued dislocation motion and result in the presence of a threshold stress. TEM analysis of specimens crept at 1023 K (750 °C) to various strains, and modeling of stresses necessary for y' precipitate dislocation bypass, suggests that the climb of dislocations around the y' precipitates is the controlling factor for continued deformation at the end of primary creep and into the tertiary creep regime. As creep deformation proceeds at an applied stress of 121 MPa and the precipitates coarsen, the stress required for Orowan bowing is reached and this mechanism becomes active. At the minimum creep rate at an applied stress of 145 MPa, the finer precipitate size results in higher Orowan bowing stresses and the creep deformation is dominated by the climb of dislocations around the y' precipitates.

  16. Features controlling the early stages of creep deformation of Waspaloy

    NASA Technical Reports Server (NTRS)

    Ferrari, A.; Wilson, D. J.

    1974-01-01

    A model has been presented for describing primary and second stage creep. General equations were derived for the amount and time of primary creep. It was shown how the model can be used to extrapolate creep data. Applicability of the model was demonstrated for Waspaloy with gamma prime particle sizes from 75 - 1000 A creep tested in the temperature range 1000 - 1400 F (538 - 760 C). Equations were developed showing the dependence of creep parameters on dislocation mechanism, gamma prime volume fraction and size.

  17. Stress versus temperature dependence of activation energies for creep

    NASA Technical Reports Server (NTRS)

    Freed, A. D.; Raj, S. V.; Walker, K. P.

    1992-01-01

    The activation energy for creep at low stresses and elevated temperatures is associated with lattice diffusion, where the rate controlling mechanism for deformation is dislocation climb. At higher stresses and intermediate temperatures, the rate controlling mechanism changes from dislocation climb to obstacle-controlled dislocation glide. Along with this change in deformation mechanism occurs a change in the activation energy. When the rate controlling mechanism for deformation is obstacle-controlled dislocation glide, it is shown that a temperature-dependent Gibbs free energy does better than a stress-dependent Gibbs free energy in correlating steady-state creep data for both copper and LiF-22mol percent CaF2 hypereutectic salt.

  18. Creep Behavior, Deformation Mechanisms, and Creep Life of Mod.9Cr-1Mo Steel

    NASA Astrophysics Data System (ADS)

    ABE, Fujio

    2015-12-01

    The creep behavior, deformation mechanisms, and the correlation between creep deformation parameters and creep life have been investigated for Mod.9Cr-1Mo steel (Gr.91, 9Cr-1Mo-VNb) by analyzing creep strain data at 723 K to 998 K (450 °C to 725 °C), 40 to 450 MPa, and t r = 11.4 to 68,755 hours in NIMS Creep Data Sheet. The time to rupture t r is reasonably correlated with the minimum creep rate {dot{\\varepsilon }}_{ min } and the acceleration of creep rate by strain in the acceleration region dln {dot{\\varepsilon }} /d ɛ, as t r = 1.5/[ {dot{\\varepsilon }}_{ min } ( dln {dot{\\varepsilon }} /d ɛ)], where {dot{\\varepsilon }}_{ min } and dln {dot{\\varepsilon }} /d ɛ reflect the creep behavior in the transient and acceleration regions, respectively. The {dot{\\varepsilon }}_{ min } is inversely proportional to the time to minimum creep rate t m, while it is proportional to the strain to minimum creep rate ɛ m, as {dot{\\varepsilon }}_{ min } = 0.54 ( ɛ m/ t m). The ɛ m decreases with decreasing stress, suggesting that the creep deformation in the transient region becomes localized in the vicinity of prior austenite grain boundaries with decreasing stress. The duration of acceleration region is proportional to the duration of transient region, while the dln {dot{\\varepsilon }} /d ɛ is inversely proportional to the ɛ m. The t r is also correlated with the t m, as t r = g t m, where g is a constant. The present creep life equations reasonably predict the degradation in creep rupture strength at long times. The downward deviation takes place in the t r vs {dot{\\varepsilon }}_{ min } curves (Monkman-Grant plot). At the same {dot{\\varepsilon }}_{ min } , both the ɛ m and t m change upon the condition of t m ∝ ɛ m. The decrease in ɛ m with decreasing stress, corresponding to decreasing {dot{\\varepsilon }}_{ min } , causes a decrease in t m, indicating the downward deviation of the t r vs {dot{\\varepsilon }}_{ min } curves.

  19. Creep resistant high temperature martensitic steel

    SciTech Connect

    Hawk, Jeffrey A.; Jablonski, Paul D.; Cowen, Christopher J.

    2015-11-13

    The disclosure provides a creep resistant alloy having an overall composition comprised of iron, chromium, molybdenum, carbon, manganese, silicon, nickel, vanadium, niobium, nitrogen, tungsten, cobalt, tantalum, boron, and potentially additional elements. In an embodiment, the creep resistant alloy has a molybdenum equivalent Mo(eq) from 1.475 to 1.700 wt. % and a quantity (C+N) from 0.145 to 0.205. The overall composition ameliorates sources of microstructural instability such as coarsening of M.sub.23C.sub.6 carbides and MX precipitates, and mitigates or eliminates Laves and Z-phase formation. A creep resistant martensitic steel may be fabricated by preparing a melt comprised of the overall composition followed by at least austenizing and tempering. The creep resistant alloy exhibits improved high-temperature creep strength in the temperature environment of around 650.degree. C.

  20. Vertebroplasty reduces progressive ׳creep' deformity of fractured vertebrae.

    PubMed

    Luo, J; Pollintine, P; Annesley-Williams, D J; Dolan, P; Adams, M A

    2016-04-11

    Elderly vertebrae frequently develop an "anterior wedge" deformity as a result of fracture and creep mechanisms. Injecting cement into a damaged vertebral body (vertebroplasty) is known to help restore its shape and stiffness. We now hypothesise that vertebroplasty is also effective in reducing subsequent creep deformations. Twenty-eight spine specimens, comprising three complete vertebrae and the intervening discs, were obtained from cadavers aged 67-92 years. Each specimen was subjected to increasingly-severe compressive loading until one of its vertebrae was fractured, and the damaged vertebral body was then treated by vertebroplasty. Before and after fracture, and again after vertebroplasty, each specimen was subjected to a static compressive force of 1kN for 1h while elastic and creep deformations were measured in the anterior, middle and posterior regions of each adjacent vertebral body cortex, using a 2D MacReflex optical tracking system. After fracture, creep in the anterior and central regions of the vertebral body cortex increased from an average 4513 and 885 microstrains, respectively, to 54,107 and 34,378 microstrains (both increases: P<0.001). Elastic strains increased by a comparable amount. Vertebroplasty reduced creep in the anterior and central cortex by 61% (P=0.006) and 66% (P=0.017) respectively. Elastic strains were reduced by less than half this amount. Results suggest that the beneficial effects of vertebroplasty on the vertebral body continue long after the post-operative radiographs. Injected cement not only helps to restore vertebral shape and elastic properties, but also reduces subsequent creep deformation of the damaged vertebra. PMID:26459490

  1. In Situ Observation of High Temperature Creep Behavior During Annealing of Steel

    NASA Astrophysics Data System (ADS)

    Zhang, X. F.; Terasaki, H.; Komizo, Y.; Murakami, Y.; Yasuda, K.

    2012-12-01

    Previous studies on creep suggested a close relationship between polycrystal grain size, substructure, and creep rate. At present, however, our understanding of the influence of polycrystal grain size, substructure, and thermal stress on creep deformation behavior seems rather insufficient, especially as there is a general lack of in situ data on structural changes during creep. In this study, the effects of thermal stress, austenite grain size, and cooling rate on slip deformations in C-Mn-Al steel during annealing were investigated systematically on the basis of in situ observations using high temperature laser scanning confocal microscopy. Finally, a kinetics model based on thermal expansion anisotropy and temperature difference was developed to explain these interesting experimental results. The in situ investigation of slip deformation during annealing greatly contributes to the understanding of high temperature creep behavior.

  2. Deformation and crack growth response under cyclic creep conditions

    SciTech Connect

    Brust, F.W. Jr.

    1995-12-31

    To increase energy efficiency, new plants must operate at higher and higher temperatures. Moreover, power generation equipment continues to age and is being used far beyond its intended original design life. Some recent failures which unfortunately occurred with serious consequences have clearly illustrated that current methods for insuring safety and reliability of high temperature equipment is inadequate. Because of these concerns, an understanding of the high-temperature crack growth process is very important and has led to the following studies of the high temperature failure process. This effort summarizes the results of some recent studies which investigate the phenomenon of high temperature creep fatigue crack growth. Experimental results which detail the process of creep fatigue, analytical studies which investigate why current methods are ineffective, and finally, a new approach which is based on the T{sup *}-integral and its ability to characterize the creep-fatigue crack growth process are discussed. The potential validity of this new predictive methodology is illustrated.

  3. Elevated temperature deformation of TD-nickel base alloys

    NASA Technical Reports Server (NTRS)

    Petrovic, J. J.; Kane, R. D.; Ebert, L. J.

    1972-01-01

    Sensitivity of the elevated temperature deformation of TD-nickel to grain size and shape was examined in both tension and creep. Elevated temperature strength increased with increasing grain diameter and increasing L/D ratio. Measured activation enthalpies in tension and creep were not the same. In tension, the internal stress was not proportional to the shear modulus. Creep activation enthalpies increased with increasing L/D ratio and increasing grain diameter, to high values compared with that of the self diffusion enthalpy. It has been postulated that two concurrent processes contribute to the elevated temperature deformation of polycrystalline TD-nickel: (1) diffusion controlled grain boundary sliding, and (2) dislocation motion.

  4. Elevated temperature creep-rupture behavior of the single crystal nickel-base superalloy NASAIR 100

    NASA Technical Reports Server (NTRS)

    Nathal, M. V.; Ebert, L. J.

    1985-01-01

    The creep and rupture behavior of 001-line-oriented single crystals of the nickel-base superalloy NASAIR 100 was investigated at temperatures of 925 and 1000 C. In the stress and temperature ranges studied, the steady state creep rate, time to failure, time to the onset of secondary creep, and the time to the onset of tertiary creep all exhibited power law dependencies on the applied stress. The creep rate exponents for this alloy were between seven and eight, and the modulus-corrected activation energy for creep was approximately 350 kjoule/mole, which was comparable to the measured activation energy for Ostwald ripening of the gamma-prime precipitates. Oriented gamma-prime coarsening to form lamellae perpendicular to the applied stress was very prominent during creep. At 1000 C, the formation of a continuous gamma-gamma-prime lamellar structure was completed during the primary creep stage. Shear through the gamma-gamma-prime interface is considerd to be the rate limiting step in the deformation process. Gradual thickening of the lamellae appeared to be the cause of the onset of tertiary creep. At 925 C, the fully developed lamellar structure was not achieved until the secondary or tertiary creep stages. At this temperature, the gamma-gamma-prime lamellar structure did not appear to be as beneficial for creep resistance as at the higher temperature.

  5. A True-Stress Creep Model Based on Deformation Mechanisms for Polycrystalline Materials

    NASA Astrophysics Data System (ADS)

    Wu, Xijia; Williams, Steve; Gong, Diguang

    2012-11-01

    A true-stress creep model has been developed based on well-recognized deformation mechanisms, i.e., dislocation glide, dislocation climb, and grain boundary sliding. The model provides a physics-based description of the entire creep deformation process with regards to the strain-time history (primary, secondary, and tertiary creep), rupture strain and lifetime, which finds good agreement with experimental observations for Waspaloy. A deformation-mechanism map is constructed for Waspaloy, and a creep failure criterion is defined by the dominant deformation mechanisms leading to intergranular/transgranular fracture. Thus, the model is a self-consistent tool for creep life prediction.

  6. Creep Properties and Deformation Mechanisms of a FGH95 Ni-based Superalloy

    NASA Astrophysics Data System (ADS)

    Xie, Jun; Tian, Su-gui; Zhou, Xiao-ming

    2013-07-01

    By means of full heat treatment, microstructure observation, lattice parameters determination, and the measurement of creep curves, an investigation has been conducted into the microstructure and creep mechanisms of FGH95 Ni-based superalloy. Results show that after the alloy is hot isostatically pressed, coarse γ' phase discontinuously distributes along the previous particle boundaries. After solution treatment at high temperature and aging, the grain size has no obvious change, and the amount of coarse γ' phase decreases, and a high volume fraction of fine γ' phase dispersedly precipitates in the γ matrix. Moreover, the granular carbides are found to be precipitated along grain boundaries, which can hinder the grain boundaries' sliding and enhance the creep resistance of the alloy. By x-ray diffraction analysis, it is indicated that the lattice misfit between the γ and γ' phases decreases in the alloy after full heat treatment. In the ranges of experimental temperatures and applied stresses, the creep activation energy of the alloy is measured to be 630.4 kJ/mol. During creep, the deformation mechanisms of the alloy are that dislocations slip in the γ matrix or shear into the γ' phase. Thereinto, the creep dislocations move over the γ' phase by the Orowan mechanism, and the < { 1 10 } rangle super-dislocation shearing into the γ' phase can be decomposed to form the configuration of (1/3) < { 1 12 } rangle super-Shockleys' partials and the stacking fault.

  7. Primary creep of Ni{sub 3}(Al, Ta) single crystals at room temperature

    SciTech Connect

    Uchic, M.D.; Nix, W.D.

    1997-12-31

    This study examines the time-dependent deformation of Ni{sub 3}(Al, Ta) at room temperature. Tension creep experiments have been performed on single crystals with one [111]<101> slip system active at the start of the test, where the applied stress ranged from 66.4 MPa (the measured 0.01% flow stress) to 143 MPa (which produced approximately 9% plastic strain). All creep curves displayed primary creep leading to eventual exhaustion, where the measured creep strain declined at a rate faster than predicted for logarithmic creep. However, no correlation between the applied stress and the form of the declining creep rate can be made at this time. Many creep curves can be obtained from one sample, as the creep curves from both virgin samples and samples with prior deformation history (at the same test stress) were indistinguishable. At the beginning of an incremental creep test, where the stress is increased by a small amount to reinitiate plastic flow in an exhausted sample, a significant retardation of the plastic response of the sample occurred when the stress increment was below 4 MPa. Preliminary TEM studies of a sample strained to 6% suggest that room temperature creep tests may not be ideal for examining the flow of Anti-Phase-Boundary (APB) dissociated dislocations.

  8. Stress versus temperature dependent activation energies in creep

    NASA Technical Reports Server (NTRS)

    Freed, A. D.; Raj, S. V.; Walker, K. P.

    1990-01-01

    The activation energy for creep at low stresses and elevated temperatures is lattice diffusion, where the rate controlling mechanism for deformation is dislocation climb. At higher stresses and intermediate temperatures, the rate controlling mechanism changes from that of dislocation climb to one of obstacle-controlled dislocation glide. Along with this change, there occurs a change in the activation energy. It is shown that a temperature-dependent Gibbs free energy does a good job of correlating steady-state creep data, while a stress-dependent Gibbs free energy does a less desirable job of correlating the same data. Applications are made to copper and a LiF-22 mol. percent CaF2 hypereutectic salt.

  9. High temperature creep behavior of single crystal gamma prime and gamma alloys

    NASA Technical Reports Server (NTRS)

    Nathal, M. V.; Diaz, J. O.; Miner, R. V.

    1989-01-01

    The creep behavior of single crystals of gamma-prime and gamma alloys were investigated and compared to the response of two-phase superalloys tested previously. High temperature deformation in the gamma alloys was characteristic of a climb-controlled mechanism, whereas the gamma-prime based materials exhibited glide-controlled creep behavior. The superalloys were much more creep resistant than their constituent phases, which indicates the importance of the gamma/gamma-prime interface as a barrier for dislocation motion during creep.

  10. Assessment of Tungsten Content on Tertiary Creep Deformation Behavior of Reduced Activation Ferritic-Martensitic Steel

    NASA Astrophysics Data System (ADS)

    Vanaja, J.; Laha, Kinkar

    2015-10-01

    Tertiary creep deformation behavior of reduced activation ferritic-martensitic (RAFM) steels having different tungsten contents has been assessed. Creep tests were carried out at 823 K (550 °C) over a stress range of 180 to 260 MPa on three heats of the RAFM steel (9Cr-W-0.06Ta-0.22V) with tungsten content of 1, 1.4, and 2.0 wt pct. With creep exposure, the steels exhibited minimum in creep rate followed by progressive increase in creep rate until fracture. The minimum creep rate decreased, rupture life increased, and the onset of tertiary stage of creep deformation delayed with the increase in tungsten content. The tertiary creep behavior has been assessed based on the relationship, , considering minimum creep rate () instead of steady-state creep rate. The increase in tungsten content was found to decrease the rate of acceleration of tertiary parameter ` p.' The relationships between (1) tertiary parameter `p' with minimum creep rate and time spent in tertiary creep deformation and (2) the final creep rate with minimum creep rate revealed that the same first-order reaction rate theory prevailed in the minimum creep rate as well as throughout the tertiary creep deformation behavior of the steel. A master tertiary creep curve of the steels has been developed. Scanning electron microscopic investigation revealed enhanced coarsening resistance of carbides in the steel on creep exposure with increase in tungsten content. The decrease in tertiary parameter ` p' with tungsten content with the consequent decrease in minimum creep rate and increase in rupture life has been attributed to the enhanced microstructural stability of the steel.

  11. The creep deformation and elevated temperature microstructural stability of a two-phase TiAl/Ti{sub 3}Al lamellar alloy

    SciTech Connect

    Bartholomeusz, M.F.; Wert, J.A.

    1995-08-01

    Enhanced work hardening of the phases in the lamellar microstructure has been cited as an explanation for the lower minimum creep rates of a two-phase TiAl/Ti{sub 3}Al lamellar alloy compared with the minimum creep rates of the individual TiAl and Ti{sub 3}Al single-phase alloys tested between 980 K and 1,130 K. This proposition is confirmed by TEM observations. Thermal and thermomechanical exposure result in the microstructural evolution, which increases the minimum creep rate ({dot {var_epsilon}}{sub min}) of the lamellar alloy. The effect of microstructural evolution on {dot {var_epsilon}}{sub min} will be discussed in the present paper.

  12. Temperature-dependent transient creep and dynamics of cratonic lithosphere

    NASA Astrophysics Data System (ADS)

    Birger, Boris I.

    2013-11-01

    Large-scale mantle convection forms the upper boundary layer (lithosphere) where the vertical temperature drop is about 1300 K. Theoretical rheology and laboratory experiments with rock samples show that transient creep occurs while creep strains are sufficiently small. The transient creep is described by the temperature-dependent Andrade rheological model. Since plate tectonics allows only small deformations in lithospheric plates, creep of the lithosphere plates is transient whereas steady-state creep, described by non-Newtonian power-law rheological model, takes place in the underlying mantle. The solution of stability problem shows that the lithosphere is stable but small-scale convective oscillations are attenuated very weakly in regions of thickened lithosphere beneath continental cratons (subcratonic roots) where the thickness of the lithosphere is about 200 km. These oscillations create small-scale convective cells (the horizontal dimensions of the cells are of the order of the subcratonic lithosphere thickness). Direction of motion within the cells periodically changes (the period of convective oscillations is of the order of 3 × 108 yr). In this study, the oscillations of cratonic lithosphere caused by initial relief perturbation are considered. This relief perturbation is assumed to be created by overthrusting in orogenic belts surrounding cratons. The perturbation of the Earth's surface relief leads to a fast isothermal process of isostatic recovery. In the presence of vertical temperature gradient, vertical displacements, associated with the recovery process in the lithosphere interior, instantly produce the initial temperature perturbations exciting thermoconvective oscillations in the cratonic lithosphere. These small-amplitude convective oscillations cause oscillatory crustal movements which form sedimentary basins on cratons.

  13. A microstructural study of creep and thermal fatigue deformation in 60Sn-40Pb solder joints

    SciTech Connect

    Tribula, D.

    1990-06-02

    Thermal fatigue failures of solder joints in electronic devices often arise from cyclic shear strains imposed by the mismatched thermal expansion coefficients of the materials that bind the joint as temperature changes are encountered. Increased solder joint reliability demands a fundamental understanding of the metallurigical mechanisms that control the fatigue to design accurate accelerated probative tests and new, more fatigue resistant solder alloys. The high temperatures and slow strain rates that pertain to thermal fatigue imply that creep is an important deformation mode in the thermal fatigue cycle. In this work, the creep behaviour of a solder joint is studied to determine the solder's microstructural response to this type of deformation and to relate this to the more complex problem of thermal fatigue. It is shown that creep failures arise from the inherent inhomogeneity and instability of the solder microstructure and suggest that small compositional changes of the binary near-eutectic Pn-Sn alloy may defeat the observed failure mechanisms. This work presents creep and thermal fatigue data for several near-eutectic Pb-Sn solder compositions and concludes that a 58Sn-40Pb-2In and a 58Sn-40Pb-2Cd alloy show significantly enhanced fatigue resistance over that of the simple binary material. 80 refs., 33 figs., 1 tab.

  14. Motion of a Deformed Sphere with Slip in Creeping Flows

    NASA Astrophysics Data System (ADS)

    Benard, Andre; Jia, Liping; Petty, Charles

    2004-11-01

    An analytical solution for the motion of a slightly deformed sphere in creeping flows with the assumption of slip on the particle surface is presented. Explicit expressions are obtained for the hydrodynamic force and torque exerted by the fluid on the deformed sphere. A perturbation method, based on previous work done by Brenner [1964] and Lamb[1945], is used to solve for the motion of a fluid influenced by the presence of a deformed sphere. Slip is assumed at the surface of the particle. Hydrodynamic force and torque exerted by the fluid on the deformed sphere are expressed explicitly for a translational and rotational deformed sphere. The equation governing the motion and orientation of a spheroid induced by homogenous flows is also presented. This evolution equation for the orientation of the spheroid is similar to the equation derived by Jeffery [1922]. Solutions of this equation show that the period of rotation of the particle with slip is longer than for the same particle without slip. Furthermore, when the slip coefficient is sufficiently low, the particle rotates to a fixed angle that corresponds to a quasi-steady state in the flow. REFERENCES Brenner, H. 1964 The Stokes resistance of a slightly deformed sphere. Chemical Engineering Science 19, 519-539 Jeffery, G.B.1922 The motion of ellipsoidal particles immersed in a viscous fluid. Proc. Soc. Lond. Math., 102, 161-179 Lamb, H. 1945 Hydrodynamics, sixth version, Dover, New York, U.S.A

  15. Creep deformation modeling of a tool steel with a tempered martensitic structure used for extrusion dies

    NASA Astrophysics Data System (ADS)

    Reggiani, Barbara; Donati, Lorenzo; Tomesani, Luca

    2011-05-01

    Aim of an extrusion die is to allow the production of the profile with the required dimension tolerances and quality level. One of the main impediment to achieve this aim could be an excessive die deformation due to the high cyclic loads and temperatures acting on the die during the extrusion process. In order to investigate the mechanisms that influence the die deformation, a physical experiment reproducing the thermo-mechanical conditions of a die was performed on a martensitic tool steel used for extrusion tools (AISI H11). The design of experiment consisted of 4 levels of temperature, 3 levels of stress and 3 types of load, i.e. pure creep, pure fatigue and creep-fatigue. In all cases, the same pattern of the mandrel displacement-time curve was found consisting of 3 stages as those typical of the strain evolution in a standard creep test with a marked primary phase. Thus, with the aim to define an easy-applicable equation to estimate the die deformation, the time hardening creep law was chosen. In order to obtain the temperature gradient within the specimen coupled thermo-electric simulations were previously performed. The nodal temperature have been then imported within the structural model and the mechanical properties assigned to the each element as a function of these values. Coefficients of the time-hardening law were optimized, for each testing condition, on the basis of experimental data starting from values for similar alloys found in literature. The values found were validated against additional experimental data performed with different specimen geometries. A good average agreement was found between experimental and numerical results.

  16. Improved Creep Measurements for Ultra-High Temperature Materials

    NASA Technical Reports Server (NTRS)

    Hyers, Robert W.; Ye, X.; Rogers, Jan R.

    2010-01-01

    Our team has developed a novel approach to measuring creep at extremely high temperatures using electrostatic levitation (ESL). This method has been demonstrated on niobium up to 2300 C, while ESL has melted tungsten (3400 C). This method has been extended to lower temperatures and higher stresses and applied to new materials, including a niobium-based superalloy, MASC. High-precision machined spheres of the sample are levitated in the NASA MSFC ESL, a national user facility and heated with a laser. The samples are rotated with an induction motor at up to 30,000 revolutions per second. The rapid rotation loads the sample through centripetal acceleration, producing a shear stress of about 60 MPa at the center, causing the sample to deform. The deformation of the sample is captured on high-speed video, which is analyzed by machine-vision software from the University of Massachusetts. The deformations are compared to finite element models to determine the constitutive constants in the creep relation. Furthermore, the non-contact method exploits stress gradients within the sample to determine the stress exponent in a single test.

  17. Analyses of Transient and Tertiary Small Punch Creep Deformation of 316LN Stainless Steel

    NASA Astrophysics Data System (ADS)

    Ganesh Kumar, J.; Ganesan, V.; Laha, K.

    2016-09-01

    Creep deformation behavior of 316LN stainless steel (SS) under small punch creep (SPC) and uniaxial creep test has been assessed and compared at 923 K (650 °C). The transient and tertiary creep deformation behaviors have been analyzed according to the equation proposed for SPC deflection, δ = δ0 + δ_{{T}} \\cdot (1 - {{e}}^{ - κ \\cdot t} ) + dot{δ }_{{s}} t + δ3 {{e}}^{{[ {φ ( {t - t_{{r}} } )} ]}} on the basis of Dobes and Cadek equation for uniaxial creep strain. Trends in the variations of (i) rate of exhaustion of transient creep ( κ) with steady-state deflection rate ( dot{δ }_{{s}} ) (ii) ` κ' with time to attain steady-state deflection rate, and (iii) initial creep deflection rate with steady-state deflection rate implied that transient SPC deformation obeyed first-order reaction rate theory. The rate of exhaustion of transient creep ( r') values that were determined from uniaxial creep tests were correlated with those obtained from SPC tests. Master curves representing transient creep deformation in both SPC and uniaxial creep tests have been derived and their near coincidence brings unique equivalence between both the test techniques. The relationships between (i) rate of acceleration of tertiary creep ( φ) and steady-state deflection rate, (ii) ` φ' and time spent in tertiary stage, and (iii) final creep deflection rate and steady-state deflection rate revealed that first-order reaction rate theory governed SPC deformation throughout the tertiary region also. Interrelationship between the transient, secondary, and tertiary creep parameters indicated that the same mechanism prevailed throughout the SPC deformation.

  18. Analyses of Transient and Tertiary Small Punch Creep Deformation of 316LN Stainless Steel

    NASA Astrophysics Data System (ADS)

    Ganesh Kumar, J.; Ganesan, V.; Laha, K.

    2016-07-01

    Creep deformation behavior of 316LN stainless steel (SS) under small punch creep (SPC) and uniaxial creep test has been assessed and compared at 923 K (650 °C). The transient and tertiary creep deformation behaviors have been analyzed according to the equation proposed for SPC deflection, δ = δ0 + δ_{T} \\cdot (1 - {e}^{ - κ \\cdot t} ) + dot{δ }_{s} t + δ3 {e}^{{[ {φ ( {t - t_{r} } )} ]}} on the basis of Dobes and Cadek equation for uniaxial creep strain. Trends in the variations of (i) rate of exhaustion of transient creep (κ) with steady-state deflection rate ( dot{δ }_{s} ) (ii) `κ' with time to attain steady-state deflection rate, and (iii) initial creep deflection rate with steady-state deflection rate implied that transient SPC deformation obeyed first-order reaction rate theory. The rate of exhaustion of transient creep (r') values that were determined from uniaxial creep tests were correlated with those obtained from SPC tests. Master curves representing transient creep deformation in both SPC and uniaxial creep tests have been derived and their near coincidence brings unique equivalence between both the test techniques. The relationships between (i) rate of acceleration of tertiary creep (φ) and steady-state deflection rate, (ii) `φ' and time spent in tertiary stage, and (iii) final creep deflection rate and steady-state deflection rate revealed that first-order reaction rate theory governed SPC deformation throughout the tertiary region also. Interrelationship between the transient, secondary, and tertiary creep parameters indicated that the same mechanism prevailed throughout the SPC deformation.

  19. Creep and precipitation behaviors of AL6XN austenitic steel at elevated temperatures

    NASA Astrophysics Data System (ADS)

    Meng, L. J.; Sun, J.; Xing, H.

    2012-08-01

    Creep behaviors of the solution-treated AL6XN austenitic stainless steel have been investigated at 873-1023 K and 120-260 MPa. The results showed that the creep stress exponent and activation energy of the AL6XN steel are 5 and 395.4 kJ/mol, respectively in the power-law breakdown regime. TEM observations revealed that dislocations distributed homogenously in grains. The creep deformation mechanism is mainly attributed to viscous dislocation glide. Precipitates in the steel after creep deformation were additionally analyzed by TEM, and the results showed that there are four different types of precipitates, such as M23C6, M6C, σ phase and Laves phase. The M23C6 carbides were observed at grain boundaries in the steel after creep at 873 K. The M6C, σ phase and Laves phase precipitates were found when the creep temperature increases to 923-1023 K. Although the AL6XN steel exhibited low steady state creep rates, a high volume fraction of brittle precipitates of σ and Laves phases reduced the creep lifetime of the steel at elevated temperatures.

  20. Creep deformation and rupture behavior of CLAM steel at 823 K and 873 K

    NASA Astrophysics Data System (ADS)

    Zhong, Boyu; Huang, Bo; Li, Chunjing; Liu, Shaojun; Xu, Gang; Zhao, Yanyun; Huang, Qunying

    2014-12-01

    China Low Activation Martensitic (CLAM) steel is selected as the candidate structural material in Fusion Design Study (FDS) series fusion reactor conceptual designs. The creep property of CLAM steel has been studied in this paper. Creep tests have been carried out at 823 K and 873 K over a stress range of 150-230 MPa. The creep curves showed three creep regimes, primary creep, steady-state creep and tertiary creep. The relationship between minimum creep rate (ε˙min) and the applied stress (σ) could be described by Norton power law, and the stress exponent n was decreased with the increase of the creep temperature. The creep mechanism was analyzed with the fractographes of the rupture specimens which were examined by scanning electron microscopy (SEM). The coarsening of precipitates observed with transmission electron microscope (TEM) indicated the microstructural degradation after creep test.

  1. Non-contact Creep Resistance Measurement for Ultra-High Temperature Materials

    NASA Technical Reports Server (NTRS)

    Lee, J.; Bradshaw, C.; Rogers, J. R.; Rathz, T. J.; Wall, J. J.; Choo, H.; Liaw, P. K.; Hyers, R. W.

    2005-01-01

    Conventional techniques for measuring creep are limited to about 1700 C, so a new technique is required for higher temperatures. This technique is based on electrostatic levitation (ESL) of a spherical sample, which is rotated quickly enough to cause creep deformation by centrifugal acceleration. Creep of samples has been demonstrated at up to 2300 C in the ESL facility at NASA MSFC, while ESL itself has been applied at over 3000 C, and has no theoretical maximum temperature. The preliminary results and future directions of this NASA-funded research collaboration will be presented.

  2. Compressive creep behavior of an electric brush-plated nanocrystalline Cu at room temperature

    NASA Astrophysics Data System (ADS)

    Wang, Guoyong; Lian, Jianshe; Jiang, Zhonghao; Qin, Liyuan; Jiang, Qing

    2009-10-01

    Creep tests were conducted on a nanocrystalline Cu at room temperature. The results at very low strain rates (<4×10-8 s-1) are consistent with Coble creep. An overall view of stress-strain rate behavior of this nanocrystalline Cu indicates that as the strain rate decreases, the deformation mechanism transition from predominantly dislocation activity to diffusion Coble creep, as evidenced by the strain rate sensitivity on stress trending to m =1 and activation volume trending to υ =1.5b3. The typical strain rate sensitivity of m =0.5 for surperplasticity can hardly be obtained at such low homogenous temperature.

  3. Room Temperature Creep Of SiC/SiC Composites

    NASA Technical Reports Server (NTRS)

    Morscher, Gregory N.; Gyekenyesi, Andrew; Levine, Stanley (Technical Monitor)

    2001-01-01

    During a recent experimental study, time dependent deformation was observed for a damaged Hi-Nicalon reinforced, BN interphase, chemically vapor infiltrated SiC matrix composites subjected to static loading at room temperature. The static load curves resembled primary creep curves. In addition, acoustic emission was monitored during the test and significant AE activity was recorded while maintaining a constant load, which suggested matrix cracking or interfacial sliding. For similar composites with carbon interphases, little or no time dependent deformation was observed. Evidently, exposure of the BN interphase to the ambient environment resulted in a reduction in the interfacial mechanical properties, i.e. interfacial shear strength and/or debond energy. These results were in qualitative agreement with observations made by Eldridge of a reduction in interfacial shear stress with time at room temperature as measured by fiber push-in experiments.

  4. Micro-scale strain mapping technique: a tool to quantify strain partitioning during creep deformation

    NASA Astrophysics Data System (ADS)

    Quintanilla-Terminel, Alejandra; Zimmerman, Mark; Evans, Brian; Kohlstedt, David

    2016-04-01

    Several deformation mechanisms interact to accommodate plastic deformation. Quantifying the contribution of each to the total strain is necessary for establishing a better link between observed microstructures and mechanical data, as well as to allow more confident extrapolation from laboratory to natural conditions. In this contribution, we present the experimental and computational technique involved in micro-scale strain mapping (MSSM). The MSSM technique relies on analyzing the relative displacement of initially regularly spaced markers after deformation. We present several microfabrication techniques that permit us to pattern various rocks with micrometric and nanometric metal markers, as well as the challenges faced in working at high temperatures and pressures. A Hough transform algorithm was used to detect the markers and automate as much as possible the strain analysis. The von Mises strain is calculated for a set of n-points and their relative displacements, which allow us to map the strain at different length scales. We applied the MSSM technique to study strain partitioning during deformation creep of Carrara marble and San Carlos olivine at a confining pressure, Pc, of 300 MPa and homologous temperatures of 0.3 to 0.6. We measured the local strain and strain heterogeneity produced during creep deformation of split cylinders of Carrara marble under conventional triaxial loading to inelastic strains of 11 to 36% at a strain rate of 3x10‑5s‑1, Pc = 300 MPa and 400o < T <700oC. We conclude that the evolution of deformation structures in marble takes place over a substantial interval in strain and that the duration of this interval depends on strain rate, temperature, and pressure. Our first results on strain mapping of olivine deformed at T = 1150oC and Pc = 300 MPa demonstrate promise for characterizing intragranular strain and better defining the contribution of grain boundary sliding to the total strain.

  5. Non-contact Creep Resistance Measurement for Ultra-high temperature Materials

    NASA Technical Reports Server (NTRS)

    Hyers, Robert W.; Lee, Jonghuyn; Bradshaw, Richard C.; Rogers, Jan; Rathz, Thomas J.; Wall, James J.; Choo, Hahn; Liaw, Peter K.

    2005-01-01

    Continuing pressures for higher performance and efficiency in propulsion are driving ever more demanding needs for high-temperature materials. Some immediate applications in spaceflight include combustion chambers for advanced chemical rockets and turbomachinery for jet engines and power conversion in nuclear-electric propulsion. In the case of rockets, the combination of high stresses and high temperatures make the characterization of creep properties very important. Creep is even more important in the turbomachinery, where a long service life is an additional constraint. Some very high-temperature materials are being developed, including platinum group metals, carbides, borides, and silicides. But the measurement of creep properties at very high temperatures is itself problematic, because the testing instrument must operate at such high temperatures. Conventional techniques are limited to about 1700 C. A new, containerless technique for measuring creep deformation has been developed. This technique is based on electrostatic levitation (ESL) of a spherical sample, which is heated to the measurement temperature and rotated at a rate such that the centrifugal acceleration causes creep deformation. Creep of samples has been demonstrated at up to 2300 C in the ESL facility at NASA MSFC, while ESL itself has been applied at over 3000 C, and has no theoretical maximum temperature. The preliminary results and future directions of this NASA-funded research collaboration will be presented.

  6. High temperature creep resistant austenitic alloy

    DOEpatents

    Maziasz, Philip J.; Swindeman, Robert W.; Goodwin, Gene M.

    1989-01-01

    An improved austenitic alloy having in wt % 19-21 Cr, 30-35 Ni, 1.5-2.5 Mn, 2-3 Mo, 0.1-0.4 Si, 0.3-0.5 Ti, 0.1-0.3 Nb, 0.1-0.5 V, 0.001-0.005 P, 0.08-0.12 C, 0.01-0.03 N, 0.005-0.01 B and the balance iron that is further improved by annealing for up to 1 hour at 1150.degree.-1200.degree. C. and then cold deforming 5-15 %. The alloy exhibits dramatically improved creep rupture resistance and ductility at 700.degree. C.

  7. Improved high temperature creep resistant austenitic alloy

    DOEpatents

    Maziasz, P.J.; Swindeman, R.W.; Goodwin, G.M.

    1988-05-13

    An improved austenitic alloy having in wt% 19-21 Cr, 30-35 Ni, 1.5-2.5 Mn, 2-3 Mo, 0.1-0.4 Si, 0.3-0.5 Ti, 0.1-0.3 Nb, 0.1-0.5 V, 0.001-0.005 P, 0.08-0.12 C, 0.01-0.03 N, 0.005-0.01 B and the balance iron that is further improved by annealing for up to 1 hour at 1150-1200/degree/C and then cold deforming 5-15%. The alloy exhibits dramatically improved creep rupture resistance and ductility at 700/degree/C. 2 figs.

  8. Fatigue and Creep-Fatigue Deformation of an Ultra-Fine Precipitate Strengthened Advanced Austenitic Alloy

    SciTech Connect

    M.C. Carroll; L.J. Carroll

    2012-10-01

    An advanced austenitic alloy, HT-UPS (high-temperature ultrafine-precipitation-strengthened), has been identified as an ideal candidate material for the structural components of fast reactors and energy-conversion systems. HT-UPS alloys demonstrate improved creep resistance relative to 316 stainless steel (SS) through additions of Ti and Nb, which precipitate to form a widespread dispersion of stable nanoscale metallic carbide (MC) particles in the austenitic matrix. The low-cycle fatigue and creep-fatigue behavior of an HT-UPS alloy have been investigated at 650 °C and a 1.0% total strain, with an R-ratio of -1 and hold times at peak tensile strain as long as 150 min. The cyclic deformation response of HT-UPS is directly compared to that of standard 316 SS. The measured values for total cycles to failure are similar, despite differences in peak stress profiles and in qualitative observations of the deformed microstructures. Crack propagation is primarily transgranular in fatigue and creep-fatigue of both alloys at the investigated conditions. Internal grain boundary damage in the form of fine cracks resulting from the tensile hold is present for hold times of 60 min and longer, and substantially more internal cracks are quantifiable in 316 SS than in HT-UPS. The dislocation substructures observed in the deformed material differ significantly; an equiaxed cellular structure is observed in 316 SS, whereas in HT-UPS the microstructure takes the form of widespread and relatively homogenous tangles of dislocations pinned by the nanoscale MC precipitates. The significant effect of the fine distribution of precipitates on observed fatigue and creep-fatigue response is described in three distinct behavioral regions as it evolves with continued cycling.

  9. Long-term performance of ceramic matrix composites at elevated temperatures: Modelling of creep and creep rupture

    SciTech Connect

    Curtin, W.A.; Fabeny, B.; Ibnabdeljalil, M.; Iyengar, N.; Reifsnider, K.L.

    1996-07-31

    The models developed, contain explicit dependences on constituent material properties and their changes with time, so that composite performance can be predicted. Three critical processes in ceramic composites at elevated temperatures have been modeled: (1) creep deformation of composite vs stress and time-dependent creep of fibers and matrix, and failure of these components; (2) creep deformation of ``interface`` around broken fibers; and (3) lifetime of the composite under conditions of fiber strength loss over time at temperature. In (1), general evolution formulas are derived for relaxation time of matrix stresses and steady-state creep rate of composite; the model is tested against recent data on Ti-MMCs. Calculations on a composite of Hi-Nicalon fibers in a melt-infiltrated SiC matrix are presented. In (2), numerical simulations of composite failure were made to map out time-to-failure vs applied load for several sets of material parameters. In (3), simple approximate relations are obtained between fiber life and composite life that should be useful for fiber developers and testers. Strength degradation data on Hi-Nicalon fibers is used to assess composite lifetime vs fiber lifetime for Hi-Nicalon fiber composites.

  10. Elevated temperature creep properties of the 54Fe-29Ni-17Co "Kovar" alloy.

    SciTech Connect

    Stephens, John Joseph, Jr.; Rejent, Jerome Andrew; Schmale, David T.

    2009-01-22

    The outline of this presentation is: (1) Applications of Kovar Alloy in metal/ceramic brazing; (2) Diffusion bonding of precision-photoetched Kovar parts; (3) Sample composition and annealing conditions; (4) Intermediate temperature creep properties (350-650 C); (5) Power law creep correlations--with and without modulus correction; (6) Compressive stress-strain properties (23-900 C); (7) Effect of creep deformation on grain growth; and (8) Application of the power law creep correlation to the diffusion bonding application. The summary and conclusions are: Elevated temperature creep properties of Kovar from 750-900 C obey a power law creep equation with a stress exponent equal to 4.9, modulus compensated activation energy of 47.96 kcal/mole. Grain growth in Kovar creep samples tested at 750 and 800 C is quite sluggish. Significant grain growth occurs at 850 C and above, this is consistent with isothermal grain growth studies performed on Kovar alloy wires. Finite element analysis of the diffusion bonding of Kovar predict that stresses of 30 MPa and higher are needed for good bonding at 850 C, we believe that 'sintering' effects must be accounted for to allow FEA to be predictive of actual processing conditions. Additional creep tests are planned at 250-650 C.

  11. Experimental and computational simulation studies on creep deformation mechanisms of a novel nanostructured Cu and Cu-10%Sn Alloy

    NASA Astrophysics Data System (ADS)

    Abo-Elsoud, Mohamed A.

    2015-04-01

    This work presents experimental and computational simulation studies on creep deformation mechanisms of a novel nanostructured Cu and Cu-10%Sn alloy that prepared by mechanical alloying (MA) copper with elemental Tin. Mechanical Newtonian creep model is employed for computational simulation of creep deformation mechanism under low stress-high temperature and to justify the experimental findings. The observed behaviors are discussed and compared with the predications of the Nabarro-Herring (N-H) theory of directional diffusion. A simple theory based on the climb controlled generation of dislocations from a fixed density of sources is developed to explain the observed behavior. TEM and SEM investigations are convenient and powerful techniques for characterization of phases and a novel nano-grain structured of the resulting materials. The reduction of grain size to the nanometer scale improves their mechanical properties.

  12. High-Temperature Creep of Fine-Grained Anorthite Aggregate

    NASA Astrophysics Data System (ADS)

    Yabe, K.; Koizumi, S.; Hiraga, T.

    2014-12-01

    Rheology of the lower crust has often been compared to the creep properties of polycrystalline anorthite. Samples that have been used in previous studies (Dimanov et al., 1999; Rybacki and Dresen, 2000) were prepared through crystallization of anorthite glass which can remain in the experiment and also contain some impurities such as absorbed water, TiO2, MgO and Fe2O3. In this study, we synthesized genuinely pure polycrystalline anorthite using the technique that does not allow the contamination of water and glass phase. Also, we prepared anorthite aggregates with glass phase and/or a small amount (1wt%) of MgO to investigate the creep properties of pure and impure anorthite aggregates. Pure anorthite powders were prepared through high temperature reaction of highly pure and nano-sized powders of CaCO3, Al2O3 and SiO2 and then they were vacuum sintered (Koizumi et al., 2010). For MgO doping, we added Mg(OH)2powders at the synthesis of anorthite powders. Glass phase was introduced to the samples by sintering above melting temperature and subsequent quenching. Constant load tests under 1 atmosphere were performed at temperatures ranging from 1150 to 1380˚C and stresses of 10 to 120 MPa. We measured Arithmetic mean grain size of specimens by microstructural observations using scanning electron microscopy (SEM) before and after creep tests. Grain sizes of all the specimens were around 1 μm before and after the creep test. Log stress versus log strain rate showed a linear relationship where its slope gave a stress exponent, n of 1, indicating that all the samples were deformed under diffusion creep. Anorthite containing MgO and glass phase were more than two and one orders of magnitude weaker than genuinely pure anorthite aggregates, respectively. Further, our pure aggregate exhibited three orders of magnitude lager strength compared to the "pure" aggregate used in previous studies. These results indicate that a small amount of glass and/or impurities including water

  13. Elevated temperature creep properties for selected active metal braze alloys

    SciTech Connect

    Stephens, J.J.

    1997-02-01

    Active metal braze alloys reduce the number of processes required for the joining of metal to ceramic components by eliminating the need for metallization and/or Ni plating of the ceramic surfaces. Titanium (Ti), V, and Zr are examples of active element additions which have been used successfully in such braze alloys. Since the braze alloy is expected to accommodate thermal expansion mismatch strains between the metal and ceramic materials, a knowledge of its elevated temperature mechanical properties is important. In particular, the issue of whether or not the creep strength of an active metal braze alloy is increased or decreased relative to its non-activated counterpart is important when designing new brazing processes and alloy systems. This paper presents a survey of high temperature mechanical properties for two pairs of conventional braze alloys and their active metal counterparts: (a) the conventional 72Ag-28Cu (Cusil) alloy, and the active braze alloy 62.2Ag- 36.2Cu-1.6Ti (Cusil ABA), and (b) the 82Au-18Ni (Nioro) alloy and the active braze alloy Mu-15.5M-0.75Mo-1.75V (Nioro ABA). For the case of the Cusil/Cusil ABA pair, the active metal addition contributes to solid solution strengthening of the braze alloy, resulting in a higher creep strength as compared to the non-active alloy. In the case of the Nioro/Nioro ABA pair, the Mo and V additions cause the active braze alloy to have a two-phase microstructure, which results in a reduced creep strength than the conventional braze alloy. The Garofalo sinh equation has been used to quantitatively describe the stress and temperature dependence of the deformation behavior. It will be observed that the effective stress exponent in the Garofalo sinh equation is a function of the instantaneous value of the stress argument.

  14. Creep-strengthening of steel at high temperatures using nano-sized carbonitride dispersions.

    PubMed

    Taneike, Masaki; Abe, Fujio; Sawada, Kota

    2003-07-17

    Creep is a time-dependent mechanism of plastic deformation, which takes place in a range of materials under low stress-that is, under stresses lower than the yield stress. Metals and alloys can be designed to withstand creep at high temperatures, usually by a process called dispersion strengthening, in which fine particles are evenly distributed throughout the matrix. For example, high-temperature creep-resistant ferritic steels achieve optimal creep strength (at 923 K) through the dispersion of yttrium oxide nanoparticles. However, the oxide particles are introduced by complicated mechanical alloying techniques and, as a result, the production of large-scale industrial components is economically unfeasible. Here we report the production of a 9 per cent Cr martensitic steel dispersed with nanometre-scale carbonitride particles using conventional processing techniques. At 923 K, our dispersion-strengthened material exhibits a time-to-rupture that is increased by two orders of magnitude relative to the current strongest creep-resistant steels. This improvement in creep resistance is attributed to a mechanism of boundary pinning by the thermally stable carbonitride precipitates. The material also demonstrates enough fracture toughness. Our results should lead to improved grades of creep-resistant steels and to the economical manufacture of large-scale steel components for high-temperature applications. PMID:12867976

  15. Creep behaviour of Cu-30 percent Zn at intermediate temperatures

    NASA Technical Reports Server (NTRS)

    Raj, S. V.

    1991-01-01

    The present, intermediate-temperature (573-823 K) range investigation of creep properties for single-phase Cu-30 percent Zn alpha-brass observed inverse, linear, and sigmoidal primary-creep transients above 573 K under stresses that yield minimum creep rates in the 10 to the -7th to 2 x 10 to the -4th range; normal primary creep occurred in all other conditions. In conjunction with a review of the pertinent literature, a detailed analysis of these data suggests that no clearly defined, classes M-to-A-to-M transition exists in this alloy notwithstanding the presence of both classes' characteristics under nominally similar stresses and temperatures.

  16. Dislocation decorrelation and relationship to deformation microtwins during creep of a y' precipitate strengthened Ni-based superalloy

    SciTech Connect

    Unocic, R. R.; Zhou, N.; Kovarik, Libor; Shen, C.; Wang, Y.; Mills, M. J.

    2011-11-01

    The evolution of microtwins during high temperature creep deformation in a strengthened Ni-base superalloy has been investigated through a combination of creep testing, TEM characterization, theoretical modeling and computer simulation. Experimentally, microtwin nucleation sources were identified and their evolution was tracked by characterizing the deformation substructure at different stages of the creep deformation. Initially, deformation is highly localized around stress concentrators such as carbides, borides and serrated grain boundaries, which act as sources of a/2<110> matrix type dislocations. Due to microstructural effects such as fine channels between particles and low matrix stacking fault energies, the a/2<110> matrix dislocations dissociate into a/6<112> Shockley partials, which were commonly observed to be decorrelated from one another, creating extended intrinsic stacking faults in the matrix. As deformation progress further, microtwins form via partial dislocations cooperatively shearing both and phases on adjacent {111} glide planes. The TEM observations lead directly to an analysis of dislocation-precipitate interactions. Through phase field simulations and theoretical analysis based on Orowan looping, the important processes of dislocation dissociation and decorrelation are modeled in detail, providing comprehensive insight into the microstructural features and applied stress conditions that favor the microtwinning deformation mode in strengthened Ni-based superalloys.

  17. Creep in solid 4He at temperatures below 1 K

    NASA Astrophysics Data System (ADS)

    Zhuchkov, V. A.; Lisunov, A. A.; Maidanov, V. A.; Neoneta, A. S.; Rubanskyi, V. Yu.; Rubets, S. P.; Rudavskii, E. Ya.; Smirnov, S. N.

    2015-03-01

    Creep in solid 4He at temperatures of ˜100-1000 mK is studied experimentally by detecting the flow of helium through a frozen porous membrane under a constant external force. Creep curves are measured for different temperatures and mechanical stresses. This method has made it possible to detect low creep rates in helium down to the lowest temperatures in these experiments. It is found that throughout this temperature range, creep is thermally activated and the activation energy decreases with falling temperature and increasing mechanical stress. An analysis shows that for temperatures above ≈500 mK, Nabarro-Herring diffusive creep takes place in solid helium with mass transfer by self diffusion of atoms and a counterflow of vacancies. The experimental data have been used to obtain the self-diffusion coefficient as a function of temperature for different stresses. At temperatures below ≈500 mK creep takes place at a very low flow rate (˜10-13 cm/s) and a very low activation energy (˜0.5-0.7 K), while the creep mechanism remains unclear.

  18. Dislocation decorrelation and relationship to deformation microtwins during creep of a precipitate strengthened Ni-based superalloy

    SciTech Connect

    Unocic, Raymond R; Zhou, Ning; Kovarik, Libor; Shen, Chen; Wang, Yunzhi; Mills, Michael J.

    2011-01-01

    The evolution of microtwins during high temperature creep deformation in a strengthened Ni-base superalloy has been investigated through a combination of creep testing, transmission electron microscopy (TEM), theoretical modeling, and computer simulation. Experimentally, microtwin nucleation sources were identified and their evolution was tracked by characterizing the deformation substructure at different stages of creep deformation. Deformation is highly localized around stress concentrators such as carbides, borides and serrated grain boundaries, which act as sources of a/2<110> matrix-type dislocations. Due to fine channels between particles, coupled with the low matrix stacking fault energy, the a/2<110> matrix dislocations dissociate into a/6<112> Shockley partials, which were commonly observed to be decorrelated from one another, creating extended intrinsic stacking faults in the matrix. Microtwins are common and form via Shockley partial dislocations cooperatively shearing both and phases on adjacent {111} glide planes. The TEM observations lead directly to an analysis of dislocation-precipitate interactions. Through phase field simulations and theoretical analyses based on Orowan looping, the important processes of dislocation dissociation and decorrelation are modeled in detail, providing comprehensive insight into the microstructural features and applied stress conditions that favor the microtwinning deformation mode in strengthened Ni-based superalloys.

  19. CREEP-2: Long-term time-dependent rock deformation in a deep-sea observatory.

    NASA Astrophysics Data System (ADS)

    Boon, Steve; Meredith, Philip; Heap, Michael; Berenzoli, Laura; Favali, Paolo

    2010-05-01

    Earthquake rupture and volcanic eruptions are the most spectacular manifestations of dynamic failure of a critically stressed crust. But these are actually rather rare events, and most of the crust spends most of its time in a highly-stressed but sub-critical state. Below a few hundred metres, the crust is saturated, and water-rock chemical reactions lead to time-dependent deformation that allows rocks to fail over extended periods of time at stresses far below their short-term strength by the mechanism of stress corrosion crack growth. This process is highly non-linear and a change in applied stress of around 5% can lead to a change in the time-to-failure of more than an order of magnitude. Theoretical calculations based on reaction rate theory suggest that such cracking may occur down to stresses as low as 20% of the rock strength, implying that time-dependent cracking will be an important deformation mechanism over geological time and at typical tectonic strain rates. A number of theoretical models have been proposed to explain this behaviour. However, it is currently not possible to discriminate between these competing models due to the relatively narrow bandwidth of strain rates that are practicably achievable in conventional laboratory experiments. Ultra-long-term experiments at very low strain rates are clearly essential to address this problem. We have therefore used the stability of the deep-sea environment to conduct ultra-long-term experiments. At depth, the temperature remains constant throughout the year and water pressure also remains essentially constant, especially in the Ionian Sea where the tidal range is minimal. We have successfully conducted a pilot experiment (CREEP-1) in which we used the constant sea-water pressure at depth to provide both a constant confining pressure and a constant deforming stress for our rock samples. Building on that success, we are now building a multi-sample deformation observatory (CREEP-2) to be deployed at

  20. Creep Behavior of High Temperature Alloys for Generation IV Nuclear Energy Systems

    NASA Astrophysics Data System (ADS)

    Wen, Xingshuo

    are believed to be responsible for the monotonically increasing creep rates. Apart from dislocation creep, diffusional creep in existence at low stress level in fine-grained (ASTM 8) material also contributed partly to the creep rates. A reasonable prediction on the long term performance of alloy 617 was also made by extrapolation method using optimized parameters based on creep test data. Furthermore, microstructure characterization was performed utilizing Optical Microscopy (OM), Scanning Electron Microscopy (SEM), Electron Backscattered Diffraction (EBSD), Transmission Electron Microscopy (TEM) and related analytical techniques on samples from both before and after creep, with special attention given to grain size effects, grain boundary type, and dislocation substructures. Evidences for dislocation climb and dislocation glide were found through detailed dislocation analysis by TEM, proving the dislocation climb-glide mechanism. The formation of subgrain boundary, the changes in boundary characters and grain sizes was confirmed by EBSD analysis for dynamic recrystallization. The effects of initial grain size and grain boundary character distribution on the creep behavior and mechanism were also evaluated. Through the results obtained from this experimental study, new insights were provided into how changes in microstructure take place during high temperature creep of alloy 617, creep mechanism at different conditions was identified, and the creep deformation model was discussed. The results will also serve to technological and code case development and design of materials for NGNP.

  1. Circular Functions Based Comprehensive Analysis of Plastic Creep Deformations in the Fiber Reinforced Composites

    NASA Astrophysics Data System (ADS)

    Monfared, Vahid

    2016-06-01

    Analytically based model is presented for behavioral analysis of the plastic deformations in the reinforced materials using the circular (trigonometric) functions. The analytical method is proposed to predict creep behavior of the fibrous composites based on basic and constitutive equations under a tensile axial stress. New insight of the work is to predict some important behaviors of the creeping matrix. In the present model, the prediction of the behaviors is simpler than the available methods. Principal creep strain rate behaviors are very noteworthy for designing the fibrous composites in the creeping composites. Analysis of the mentioned parameter behavior in the reinforced materials is necessary to analyze failure, fracture, and fatigue studies in the creep of the short fiber composites. Shuttles, spaceships, turbine blades and discs, and nozzle guide vanes are commonly subjected to the creep effects. Also, predicting the creep behavior is significant to design the optoelectronic and photonic advanced composites with optical fibers. As a result, the uniform behavior with constant gradient is seen in the principal creep strain rate behavior, and also creep rupture may happen at the fiber end. Finally, good agreements are found through comparing the obtained analytical and FEM results.

  2. Brittle, creep and melt damage mechanics of the lithosphere: is slow creep deformation a key to intraplate volcanic provinces?

    NASA Astrophysics Data System (ADS)

    Liu, J.; Regenauer-Lieb, K.; Karrech, A.; Rosenbaum, G.; Lyakhovsky, V.

    2014-12-01

    We investigate the problem of intraplate melt generation with the aim of understanding spatial and temporal relationships between magmatism and extremely slow intraplate deformation. We present numerical models that consider feedback between melt generation and lithospheric deformation and incorporate three different damage mechanisms: brittle damage, creep damage, and melt damage. Melt conditions are calculated with a Gibbs energy minimization method, and the energy equation solved self-consistently for latent heat and shear heating effects. We use an extremely slowly lithosphere extension model (1-1.5 mm/y) to investigate the mechanics leading to intraplate volcanism in a cold lithosphere (~50mW/m2) such as the Harrat Ash-Shaam volcanic field in NW Arabia. We find that the extremely slow extension is a key to a very potent melt transfer mechanism through the lithosphere. The mechanism relies on multiple feedback mechanisms active in the accommodation of strain in the presence of fluids. These are capable of generating melts in the lithosphere/asthenosphere even in regions of relatively low heat flux. Once low degrees of partial melts are generated, the triple feedback between brittle-creep and melt damage leads to high porosity lithospheric-scale shear zones capable of transferring melts and fluids to the surface. Efficient localization in the weaker ductile domains implies that the final pattern of strain distribution is controlled by slow creep from below rather than by brittle deformation from above. Our model provides an explanation for intraplate volcanic provinces, which appear to rely on slowly deforming lithospheres. A significant finding is that slow extension, rather than fast extension, can localize melt damage more effectively in the deeper creeping section of the lithosphere. This finding may have profound implications to the fundamental dynamic control on intraplate volcanism.

  3. Creep and Environmental Effects on High Temperature Creep-Fatigue Behavior of Alloy 617

    SciTech Connect

    L. J. Carroll; C. Cabet; R. Madland; R. Wright

    2011-06-01

    Alloy 617 is the leading candidate material for Intermediate Heat Exchanger (IHX) of a Very High Temperature Reactor (VHTR), expected to have an outlet temperature as high as 950 C. System start-ups and shut-downs as well as power transients will produce low cycle fatigue (LCF) loadings of components. Acceptance of Alloy 617 in Section III of the ASME Code for nuclear construction requires a detailed understanding of the creep-fatigue behavior in both air and impure helium, representative of the VHTR primary coolant. Strain controlled LCF tests including hold times at maximum tensile strain were conducted at total strain range of 0.3% in air at 950 C. Creep-fatigue testing was also performed in a simulated VHTR impure helium coolant for selected experimental conditions. The fatigue resistance decreased when a hold time was added at peak tensile stress, consistent with the observed change in fracture mode from transgranular to intergranular with introduction of a tensile hold. Increases in the tensile hold time, beyond 180 sec, was not detrimental to the creep-fatigue resistance. Grain boundary damage in the form of grain boundary cracking was present in the bulk of the creep-fatigue specimens. This bulk cracking was quantified and found to be similar for hold times of up to 1800 sec consistent with the saturation in failure lives and rapid stress relaxation observed during the creep portion of the creep-fatigue cycle.

  4. High temperature creep of SiC densified using a transient liquid phase

    SciTech Connect

    Jou, Z.C.; Virkar, A.V. ); Cutler, R.A. )

    1991-09-01

    Silicon carbide-based ceramics can be rapidly densified above approximately 1850 {degree}C due to a transient liquid phase resulting from the reaction between alumina and aluminum oxycarbides. The resulting ceramics are fine-grained, dense, and exhibit high strength at room temperature. SiC hot pressed at 1875 {degree}C for 10 min in Ar was subjected to creep deformation in bending at elevated temperatures between 1500 and 1650 {degree}C in Ar. Creep was thermally activated with an activation energy of 743 kJ/mol. Creep rates at 1575 {degree}C were between 10{sup {minus}9}/s and 10{sup {minus}7}/s at an applied stress between 38 and 200 MPa, respectively, resulting in a stress exponent of {approx}1.7.

  5. Orientation dependence of high temperature creep strength and internal stress in Ni{sub 3}Al alloy single crystals

    SciTech Connect

    Miura, Seiji; Peng, Z.L.; Mishima, Yoshinao

    1997-12-31

    High temperature creep behavior of a nickel-rich Ni{sub 3}(Al,Ta) with the L1{sub 2} structure is investigated in order to clarify the influence of crystallographic orientation with respect to the stress axis. The single crystals with four different orientations are deformed in compressive creep at temperatures ranging from 1,123 to 1,273 K under a constant load, initial shear stress being 35 to 120 MPa for (111)[{bar 1}01] slip system. The results show a distinct orientation dependence of creep strength, although shape of creep curves, stress exponent and the activation energy seem to be independent of the orientation. It is shown, however, the internal stress, being measured by strain transient dip tests, is found to be orientation dependent and the creep behavior is independent on orientation if it is interpreted using the effective stress instead of the applied shear stress.

  6. Phenomenological and microstructural analysis of room temperature creep in titanium alloys

    SciTech Connect

    Neeraj, T.; Hou, D.H.; Daehn, G.S.; Mills, M.J.

    2000-04-03

    Primary creep is the dominant mode of deformation during creep of titanium alloys at room temperature. Based on a study of both Ti-6Al and Ti-6Al-2Sn-4Zr-2Mo, it is shown that the transient creep behavior can be described by a power law of the form {var_epsilon} = At{sup a}, while the strain-rate-sensitive Hollomon law, {sigma} = K{var_epsilon}{sup n}{dot {var_epsilon}}{sup m}, represents the constant strain rate behavior of titanium alloys reasonably well. A simple analytical result is derived to relate these two expressions. Using this solution, the long time creep response has been predicted reasonably well from the constant strain rate results for the two alloys studied. Relative to other metals, it is shown that titanium alloys exhibit exceptionally low values of strain hardening. Optical microscope observations of slip line evolution have been used to relate the deformation mechanisms to the macroscopic behavior. Operative slip systems, as well as dislocation distributions and morphologies, are also presented for the first time following creep of a single-phase {alpha} microstructure in Ti-6Al.

  7. The constitutive representation of high-temperature creep damage

    NASA Technical Reports Server (NTRS)

    Chan, K. S.

    1988-01-01

    The elastic-viscoplastic constitutive equations of Bodner-Partom were applied to modeling creep damage in a high temperature Ni-alloy, B1900 + Hf. Both tertiary creep in bulk materials and creep crack growth in flawed materials were considered. In the latter case, the energy rate line integral was used for characterizing the crack driving force, and the rate of crack extension was computed using a local damage formulation that assumed fracture was controlled by cavitation occurring within the crack-tip process zone. The results of this investigation were used to assess the evolution equation for isotropic damage utilized in the Bodner-Partom constitutive equations.

  8. A model for high temperature creep of single crystal superalloys based on nonlocal damage and viscoplastic material behavior

    NASA Astrophysics Data System (ADS)

    Trinh, B. T.; Hackl, K.

    2014-07-01

    A model for high temperature creep of single crystal superalloys is developed, which includes constitutive laws for nonlocal damage and viscoplasticity. It is based on a variational formulation, employing potentials for free energy, and dissipation originating from plasticity and damage. Evolution equations for plastic strain and damage variables are derived from the well-established minimum principle for the dissipation potential. The model is capable of describing the different stages of creep in a unified way. Plastic deformation in superalloys incorporates the evolution of dislocation densities of the different phases present. It results in a time dependence of the creep rate in primary and secondary creep. Tertiary creep is taken into account by introducing local and nonlocal damage. Herein, the nonlocal one is included in order to model strain localization as well as to remove mesh dependence of finite element calculations. Numerical results and comparisons with experimental data of the single crystal superalloy LEK94 are shown.

  9. The high temperature creep behavior of oxides and oxide fibers

    NASA Technical Reports Server (NTRS)

    Jones, Linda E.; Tressler, Richard E.

    1991-01-01

    A thorough review of the literature was conducted on the high-temperature creep behavior of single and polycrystalline oxides which potentially could serve as fiber reinforcements in ceramics or metal matrix applications. Sapphire when oriented with the basal plane perpendicular to the fiber axis (c-axis oriented) is highly creep resistant at temperatures in excess of 1600 C and applied loads of 100 MPa and higher. Pyramidal slip is preferentially activated in sapphire under these conditions and steady-state creep rates in the range of 10(exp -7) to 10 (exp -8)/s were reported. Data on the creep resistance of polycrystalline beryllia suggest that C-axiz oriented single crystal beryllia may be a viable candidate as a fiber reinforcement material; however, the issure of fabricability and moisture sensitivity must be addressed for this material. Yttrium aluminum garnet (YAG) also appears to be a fiber candidate material having a high resistance to creep which is due to it's complex crystal structure and high Peierl resistance. The high creep resistance of garnet suggests that there may be other complex ternary oxides such as single crystal mullite which may also be candidate materials for fiber reinforcements. Finally, CVD and single crystal SiC, although not oxides, do possess a high resistance to creep in the temperature range between 1550 and 1850 C and under stresses of 110 to 220 MPa. From a review of the literature, it appears that for high creep resistant applications sapphire, silicon carbide, yttrium aluminum garnet, mullite, and beryllia are desirable candidate materials which require further investigation.

  10. Elevated temperature deformation of thoria dispersed nickel-chromium

    NASA Technical Reports Server (NTRS)

    Kane, R. D.; Ebert, L. J.

    1974-01-01

    The deformation behavior of thoria nickel-chromium (TD-NiCr) was examined over the temperature range 593 C (1100 F) to 1260 C (2300 F) in tension and compression and at 1093 C (2000 F) in creep. Major emphasis was placed on: (1) the effects of the material and test related variables (grain size, temperature, stress and strain rate) on the deformation process; and (2) the evaluation of single crystal TD-NiCr material produced by a directional recrystallization process. Elevated temperature yield strength levels and creep activation enthalpies were found to increase with increasing grain size reaching maximum values for the single crystal TD-NiCr. Stress exponent of the steady state creep rate was also significantly higher for the single crystal TD-NiCr as compared to that determined for the polycrystalline materials. The elevated temperature deformation of TD-NiCr was analyzed in terms of two concurrent, parallel processes: diffusion controlled grain boundary sliding, and dislocation motion.

  11. Plastic Deformation of Aluminum Single Crystals at Elevated Temperatures

    NASA Technical Reports Server (NTRS)

    Johnson, R D; Young, A P; Schwope, A D

    1956-01-01

    This report describes the results of a comprehensive study of plastic deformation of aluminum single crystals over a wide range of temperatures. The results of constant-stress creep tests have been reported for the temperature range from 400 degrees to 900 degrees F. For these tests, a new capacitance-type extensometer was designed. This unit has a range of 0.30 inch over which the sensitivity is very nearly linear and can be varied from as low a sensitivity as is desired to a maximum of 20 microinches per millivolt with good stability. Experiments were carried out to investigate the effect of small amounts of prestraining, by two different methods, on the creep and tensile properties of these aluminum single crystals. From observations it has been concluded that plastic deformation takes place predominantly by slip which is accompanied by the mechanisms of kinking and polygonization.

  12. High-Temperature Deformation of Enstatite Aggregates

    NASA Astrophysics Data System (ADS)

    Bystricky, M.; Lawlis, J.; Mackwell, S. J.; Heidelbach, F.; Raterron, P. C.

    2011-12-01

    Although enstatite is a significant component of the upper mantle, its rheology is still poorly understood. We have performed an experimental investigation of the mechanical properties of enstatite at high pressure and temperature in the proto- and ortho-enstatite stability fields. Synthetic enstatite powders were produced by reacting San Carlos olivine powders with lab-grade quartz. Powders were hot-pressed at high PT, and were then baked at 1000°C under controlled oxygen fugacity conditions to remove all hydrous defect species. The polycrystalline enstatite samples were deformed in a Paterson gas-medium apparatus at temperatures of 1200-1300°C, an oxygen fugacity buffered at Ni/NiO, and confining pressures of 300 or 450 MPa. Under these conditions, samples were in the orthoenstatite field at 450 MPa and likely mainly in the protoenstatite field at 300 MPa. At both confining pressures, the mechanical data display a progressive increase of the stress exponent n from 1 to 3 as a function of differential stress, suggesting a transition from diffusional to dislocation creep. Non-linear least-square fits to the high-stress data yielded flow laws with n=3 and activation energies of 600 and 720 kJ/mol for ortho- and proto-enstatite, respectively. The measured strengths are significantly higher than those derived from Raleigh et al. (1971) and Ross and Nielsen (1978), due to the influence of water on the mechanical behavior of their samples. Deformed samples were analysed using optical microscopy, SEM and TEM. Because enstatite reverts to clinoenstatite during quenching, the microstructures present highly twinned grains composed of thin alternating domains of clino- and ortho-pyroxene. Nevertheless, the microstructures show evidence of dislocation processes in the form of undulatory extinction and kink bands. Crystallographic preferred orientations measured by EBSD are axisymmetric and indicate preferential slip on (100)[001]. High resolution TEM indicates that for

  13. Fatigue and creep-fatigue deformation of several nickel-base superalloys at 650 C

    NASA Technical Reports Server (NTRS)

    Miner, R. V.; Gayda, J.; Maier, R. D.

    1982-01-01

    Transmission electron microscopy has been used to study the bulk deformation characteristics of seven nickel-base superalloys tested in fatigue and creep-fatigue at 650 C. The alloys were Waspalloy, HIP Astroloy, H plus F Astroloy, H plus F Rene 95, IN 100, MERL 76, and NASA IIB-7. The amount of bulk deformation observed in all the alloys was low. In tests with inelastic strain amplitudes less than about 0.003, only some grains exhibited yielding and the majority of those had the 110 line near the tensile axis. Deformation occurred on octahedral systems for all of the alloys except MERL 76 which also showed abundant primary cube slip. Creep-fatigue cycling occasionally produced extended faults between partial dislocations, but otherwise deformation was much the same as for fatigue cycling.

  14. Deformation mechanisms responsible for the creep resistance of Ti-Al alloys

    SciTech Connect

    Morris, M.A.; Lipe, T.

    1997-12-31

    Two {gamma}-based Ti-Al alloys with similar grain sizes and, respectively, lamellar and duplex microstructures have been creep tested at 700 C and constant stresses ranging between 280 and 430 MPa. TEM observations have confirmed that the duplex alloy deforms by extensive mechanical twinning whose density increases with applied stress and increasing strain. The new twin interfaces subdivide the {gamma} grains throughout the primary stage of creep. At the onset of the minimum creep rate, the twin interfaces in the duplex alloy behave in the same way as the {gamma}/{gamma} or the {alpha}{sub 2}/{gamma} interfaces in the lamellar alloy. However, single dislocations were also present and it appears that in both alloys the deformation process is controlled by the accumulation and emission of dislocations from the different interfaces.

  15. Analysis of slip activity and heterogeneous deformation in tension and tension-creep of Ti-5Al-2.5Sn (wt %) using in-situ SEM experiments

    NASA Astrophysics Data System (ADS)

    Li, H.; Boehlert, C. J.; Bieler, T. R.; Crimp, M. A.

    2012-08-01

    The deformation behavior of a Ti-5Al-2.5Sn (wt %) near-α alloy was investigated during in-situ deformation inside a scanning electron microscope. Tensile experiments were performed at 296 K and 728 K (≈0.4 T m), while tensile-creep experiments were performed at 728 K and 763 K. Active deformation systems were identified using electron backscattered diffraction-based slip trace analysis. Both basal and prismatic slip systems were active during the tensile experiments. Basal slip was observed for grains clustered around high Schmid factor orientations, while prismatic slip exhibited less dependence on the crystallographic orientation. The tension-creep experiments revealed less slip but more development of grain boundary ledges than in the higher strain rate tensile experiments. Some of the grain boundary ledges evolved into grain boundary cracks, and grain boundaries oriented nearly perpendicular to the tensile axis formed ledges earlier in the deformation process. Grain boundaries with high misorientations also tended to form ledges earlier than those with lower misorientations. Most of the grain boundary cracks formed in association with grains displaying hard orientations, where the c-axis was nearly perpendicular to the tensile direction. For the tension-creep experiments, pronounced basal slip was observed in the lower-stress creep regime and the activity of prismatic slip increased with increasing creep stress and temperature.

  16. Phase boundary mobility in naturally deformed, high-grade quartzofeldspathic rocks: evidence for diffusional creep

    NASA Astrophysics Data System (ADS)

    Gower, Robert J. W.; Simpson, Carol

    1992-03-01

    Grain shape fabrics and optical microstructures of some quartzofeldspathic rocks deformed under upper amphibolite facies conditions in the southwestern Grenville Province, Ontario, Canada, suggest that quartz and feldspar have accommodated intracrystalline plastic strains by both diffusional and dislocation creep. In these rocks, quartz and feldspar form polycrystalline domains separated by gently curved and locally cuspate phase boundaries whose morphology is similar in certain respects to the phase boundary morphology of rocks annealed experimentally under hydrostatic stress conditions. In the naturally deformed rocks, however, phase boundary cusps consistently point along the foliation and parallel to the mineral fibre lineation (i.e. in directions of inferred finite extension) which implies that phase boundary motion and cusp formation occurred during deformation. Optical microstructures in feldspar and crystallographic preferred orientations in quartz are consistent with the accommodation of some intracrystalline plastic strains by dislocation creep. However, the morphology of quartz-feldspar phase boundaries cannot be explained by either dislocation creep or static annealing alone. We propose that phase boundary motion resulted from a diffusion-assisted process involving dissolution at foliation-parallel quartz-feldspar phase boundaries, mass transfer over length scales of the order of feldspar domain size (≈200 μm or greater) and precipitation at quartz-feldspar phase boundary cusps. This study extends the range of natural deformation conditions under which diffusional creep has been identified in quartzofeldspathic rocks. It also has important implications for the natural rheological behavior of the mid- and lower-continental crust.

  17. Correlation of creep rate with microstructural changes during high temperature creep

    NASA Technical Reports Server (NTRS)

    Young, C. T.; Sommers, B. R.; Lytton, J. L.

    1977-01-01

    Creep tests were conducted on Haynes 188 cobalt-base alloy and alpha titanium. The tests on Haynes 188 were conducted at 1600 F and 1800 F for stresses from 3 to 20 ksi, and the as-received, mill-annealed results were compared to specimens given 5%, 10%, and 15% room temperature prestrains and then annealed one hour at 1800 F. The tests on alpha titanium were performed at 7,250 and 10,000 psi at 500 C. One creep test was done at 527 C and 10,000 psi to provide information on kinetics. Results for annealed titanium were compared to specimens given 10% and 20% room temperature prestrains followed by 100 hours recovery at 550 C. Electron microscopy was used to relate dislocation and precipitate structure to the creep behavior of the two materials. The results on Haynes 188 alloy reveal that the time to reach 0.5% creep strain at 1600 F increases with increasing prestrain for exposure times less than 1,000 hours, the increase at 15% prestrain being more than a factor of ten.

  18. Examination of the distribution of the tensile deformation systems in tension and tension-creep of Ti-6Al-4V (wt.%) at 296 K and 728 K

    NASA Astrophysics Data System (ADS)

    Li, H.; Boehlert, C. J.; Bieler, T. R.; Crimp, M. A.

    2015-03-01

    The deformation behaviour of an α + β Ti-6Al-4V (wt.%) alloy was investigated during in situ deformation inside a scanning electron microscopy (SEM). Tensile experiments were performed at 296 and 728 K (~0.4Tm), while a tensile-creep experiment was performed at 728 K and 310 MPa (σ/σys = 0.74). The active deformation systems were identified using electron backscattered diffraction-based slip-trace analysis and SEM images of the specimen surface. The distribution of the active deformation systems varied as a function of temperature. Basal slip deformation played a major role in the tensile deformation behaviour, and the relative activity of basal slip increased with increasing temperature. For the 296 K tension deformation, basal slip was less active than prismatic slip, whereas this was reversed at 728 K. Twinning was observed in both the 296 and 728 K tension experiments; however, no more than 4% of the total deformation systems observed was twins. The tension-creep experiment revealed no slip traces, however grain boundary ledge formation was observed, suggesting that grain boundary sliding was an active deformation mechanism. The results of this work were compared with those from previous studies on commercially pure Ti, Ti-5Al-2.5Sn (wt.%) and Ti-8Al-1Mo-1V (wt.%), and the effects of alloying on the deformation behaviour are discussed. The relative amount of basal slip activity increased with increasing Al content.

  19. Effect of HIP Temperature on Microstructure and Creep Property of FGH95 Alloy

    NASA Astrophysics Data System (ADS)

    Xie, Jun; Tian, Su-Gui; Zhou, Xiao-Ming

    2012-02-01

    By means of hot isostatic pressing (HIP) treatment, microstructure observation and creep properties measurement, the effects of the HIP temperatures on the microstructure and creep properties of FGH95 nickel-base superalloy are investigated. The results show that, when the HIP temperature is lower than solubility of γ' phase, the coarser γ' phase is precipitated in the previous particle boundary (PPB) regions, and the quantity and size of the coarser γ' phase which is distributed in the regions decrease as the HIP temperature increases. No feature of the grain growing up is detected after the alloy is solution treated at 1140 °C. Moreover, there are a few of carbide particles distributing along the grain boundary and in the grain. After HIP treated at 1180 °C and fully heat treated, coarser γ' phase is dissolved in the alloy, and the depleted zone of the fine γ' phase has disappeared. In addition, the grains grow up obviously in the alloy, and the γ' phase and fine carbide particles are dispersedly precipitated in the grains and along boundaries, which can enhance the creep resistance of the alloy. The deformation mechanisms of the alloy are that the dislocations slip in the matrix or shear into γ' phase during creep.

  20. High temperature tensile creep, creep damage and failure under superimposed compressional stress

    NASA Astrophysics Data System (ADS)

    Boček, M.

    1985-04-01

    The paper presents a theoretical examination of the influence of compressional stresses upon the characteristics of high temperature tensile creep. The calculations are based on a phenomenological creep cavitation model, which is adapted for superimposed pressure loading. Therefrom a power law strain rate/stress equation is obtained in which the hydrostatic pressure P enters in the stress function σ1n = ( σ - P) n. However, impeding cavity growth, P has an additional influence upon the strain rate through a variable structure parameter described by the damage function A< σ1>. From A< σ1> the stress rupture lines tf< σ1> for superimposed creep are obtained. The calculations are compared to experimental results from literature. By means of the life fraction rule the lifetime is calculated for load cycling in which tensional and compressional loading phases alternate. The lifetime depends sensitively upon the ratio of the minimum to maximum stress amplitude ( r) and upon a stress factor η characterizing the influence of the stress state upon cavitation damage. The lifetime computations are compared with experimental results obtained on the stainless steel AISI 304. The calculations show that the Monkman-Grant relationship should also be obeyed for superimposed creep.

  1. Creep deformation of a fully lamellar gamma based titanium aluminide alloy

    SciTech Connect

    Herrouin, F.; Bowen, P.; Jones, I.P.

    1997-12-31

    A complex two phase {gamma}-TiAl alloy, Ti-47Al-1Cr-1Mn-2Ta-0.2Si (at.%) in a fully lamellar condition, has been creep tested at a stress of 200 MPa and a temperature of 700 C. This simulates the in-service operating conditions for several potential gas turbine aero engine applications where creep resistance is a design limiting material property. The results indicate that reduction in lamellae thickness and avoidance of feathery type microstructures contribute to improved creep resistance.

  2. Strain localization during high temperature creep of marble: The effect of inclusions

    NASA Astrophysics Data System (ADS)

    Rybacki, E.; Morales, L. F. G.; Naumann, M.; Dresen, G.

    2014-11-01

    The deformation of rocks in the Earth's middle and lower crust is often localized in ductile shear zones. To better understand the initiation and propagation of high-temperature shear zones induced by the presence of structural and material heterogeneities, we performed deformation experiments in the dislocation creep regime on Carrara marble samples containing weak (limestone) or strong (novaculite) second phase inclusions. The samples were mostly deformed in torsion at a bulk shear strain rate of ≈ 1.9 × 10- 4 s- 1 to bulk shear strains γ between 0.02 and 2.9 using a Paterson-type gas deformation apparatus at 900 °C temperature and 400 MPa confining pressure. At low strain, twisted specimens with weak inclusions show minor strain hardening that is replaced by strain weakening at γ > 0.1-0.2. Peak shear stress at the imposed conditions is about 20 MPa, which is ≈ 8% lower than the strength of intact samples. Strain progressively localized within the matrix with increasing bulk strain, but decayed rapidly with increasing distance from the inclusion tip. Microstructural analysis shows twinning and recrystallization within this process zone, with a strong crystallographic preferred orientation, dominated by {r} and (c) slip in < a >. Recrystallization-induced weakening starts at local shear strain of about 1 in the process zone, corresponding to a bulk shear strain of about 0.1. In contrast, torsion of a sample containing strong inclusions deformed at similar stress as inclusion-free samples, but do not show localization. The experiments demonstrate that the presence of weak heterogeneities initiates localized creep at local stress concentrations around the inclusion tips. Recrystallization-induced grain size reduction may only locally promote grain boundary diffusion creep. Accordingly, the bulk strength of the twisted aggregate is close to or slightly below the lower (isostress) strength bound, determined from the flow strength and volume fraction of matrix

  3. Characterization of micro-scale creep deformation of an electro-active paper actuator

    NASA Astrophysics Data System (ADS)

    Lee, Sangwoo; Kim, Joo-Hyung; Kang, Kwangseon; Kim, Jaehwan; Kim, Heung Soo; Yang, Chulho

    2009-09-01

    The creep deformation process of an electro-active paper (EAPap) actuator was investigated by adapting stepwise dead-weight loading. To understand the deformation mechanism of the EAPap film, including morphological and structural changes, various loading conditions below yield strength were applied to cellophane EAPap. From the structural observation, micro-dimples and micro-cracks were detected at applied load lower than 10% of yield strength, while they were not found in higher load conditions. It is hypothesized that only short and random fibers in the amorphous region may respond to the applied stress at the low loading condition, not the fibers in the crystalline area. As a result, deformation energy at the localized spot accumulated and created micro-defects at the surface. Meanwhile, fibers in the crystalline region may sustain most of the loads as creep load increases to a high level. Molecular chains in the fiber may rotate and elongate with high load. Elongated fibers were observed only at a high level of load. From the structural change as a function of applied load, a peak shift of crystal orientation was observed only in high load conditions by wide angle x-ray measurement. This may confirm that creep deformation could give rise to structure changes in EAPap.

  4. Submarine creeping landslide deformation controlled by the presence of gas hydrates: The Tuaheni Landslide Complex, New Zealand

    NASA Astrophysics Data System (ADS)

    Gross, Felix; Mountjoy, Joshu; Crutchle, Garethy; Koch, Stephanie; Bialas, Jörg; Pecher, Ingo; Woelz, Susi; Dannowski, Anke; Carey, Jon; Micallef, Aaron; Böttner, Christoph; Huhn, Katrin; Krastel, Sebastian

    2016-04-01

    Methane hydrate occurrence is bound to a finite pressure/temperature window on continental slopes, known as the gas hydrate stability zone (GHSZ). Hydrates within sediment pore spaces and fractures are recognized to act like a cement, increasing shear strength and stabilizing slopes. However, recent studies show that over longer strain periods methane hydrates can undergo ductile deformation. This combination of short term strengthening and longer term ductile behavior is implicated in the development of slow creeping submarine landforms within the GHSZ. In order to study this phenomenon, a new high-resolution seismic 3D volume was acquired at the Tuaheni Landslide Complex (TLC) at the Hikurangi margin offshore the North Island of New Zealand. Parts of TLC have been interpreted as a slow moving landslide controlled by the gas hydrate system. Two hypotheses for its slow deformation related to the presence of methane hydrates have been proposed: i) Hydrofracturing, driven by gas pressure at the base of the GHSZ, allows pressurized fluids to ascend toward the seafloor, thereby weakening the shallow debris and promoting failure. ii) The mixture of methane hydrates and sediment results in a rheology that behaves in a ductile way under sustained loading, resulting in slow deformation comparable to that of terrestrial and extra-terrestrial rock glaciers. The 3D dataset reveals the distribution of gas and the extend of gas hydrate stability within the deformed debris, as well as deformation fabrics like tectonic-style faulting and a prominent basal décollement, known to be a critical element of terrestrial earth-flows and rock glaciers. Observations from 3D data indicate that the TLC represents the type example of a new submarine landform - an active creeping submarine landslide - which is influenced by the presence of gas hydrates. The morphology, internal structure and deformation of the landslide are comparable with terrestrial- and extra-terrestrial earth flows and

  5. Measurement of Creep Properties of Ultra-High-Temperature Materials by a Novel Non-Contact Technique

    NASA Technical Reports Server (NTRS)

    Hyers, Robert W.; Lee, Jonghyun; Rogers, Jan R.; Liaw, Peter K.

    2007-01-01

    A non-contact technique for measuring the creep properties of materials has been developed and validated as part of a collaboration among the University of Massachusetts, NASA Marshall Space Flight Center Electrostatic Levitation Facility (ESL), and the University of Tennessee. This novel method has several advantages over conventional creep testing. The sample is deformed by the centripetal acceleration from the rapid rotation, and the deformed shapes are analyzed to determine the strain. Since there is no contact with grips, there is no theoretical maximum temperature and no concern about chemical compatibility. Materials may be tested at the service temperature even for extreme environments such as rocket nozzles, or above the service temperature for accelerated testing of materials for applications such as jet engines or turbopumps for liquid-fueled engines. The creep measurements have been demonstrated to 2400 C with niobium, while the test facility, the NASA MSFC ESL, has processed materials up to 3400 C. Furthermore, the ESL creep method employs a distribution of stress to determine the stress exponent from a single test, versus the many tests required by conventional methods. Determination of the stress exponent from the ESL creep tests requires very precise measurement of the surface shape of the deformed sample for comparison to deformations predicted by finite element models for different stress exponents. An error analysis shows that the stress exponent can be determined to about 1% accuracy with the current methods and apparatus. The creep properties of single-crystal niobium at 1985 C showed excellent agreement with conventional tests performed according to ASTM Standard E-139. Tests on other metals, ceramics, and composites relevant to rocket propulsion and turbine engines are underway.

  6. Microstructural behavior of 8Cr-ODS martensitic steels during creep deformation

    NASA Astrophysics Data System (ADS)

    Shinozuka, K.; Esaka, H.; Tamura, M.; Tanigawa, H.

    2011-10-01

    Oxide dispersion strengthened (ODS) steels show a high anisotropy in their creep behavior because of the δ-ferrite grain elongated in the hot-rolled direction and the characteristic formation of creep cavities. In this work, the relationship between the δ-ferrite grain and the growth of creep cavities in 8Cr-ODS steels was investigated. The samples of two ODS steels with different δ-ferrite volume fractions were machined parallel and perpendicular to the hot-rolled direction. Creep rupture tests and interrupted tests were performed at 700 °C and about 197 MPa. Cavities formed in the martensite along δ-ferrite grains during creep deformation. The area fraction of the cavities of all specimens increased in proportion to the cube root of test time. When the volume fraction of δ-ferrite was high and δ-ferrite grains elongated parallel to the load direction, δ-ferrite then obstructed the propagation of cracks. However, when the volume fraction of δ-ferrite was low and δ-ferrite grains elongated perpendicular to the load direction, δ-ferrite grains had little effect on crack propagation.

  7. High-temperature deformation and diffusion in oxides

    SciTech Connect

    Routbort, J.L.

    1992-06-01

    High-temperature, steady-state deformation is usually controlled by diffusion of the slowest moving ion along its fastest diffusion path. Therefore, measurements of steady-state deformation can, in principle, be used to obtain information concerning diffusion. This paper will briefly review the assumptions that relate creep, defect chemistry, and diffusion. Steady-state deformation of the NaCI-structured oxides, Co{sub 1-x}O and Mn{sub l-x}O, and the perovskite-structured high-temperature superconductors YBa{sub 2}Cu{sub 3}0{sub x} and Bi{sub 2}Sr{sub 2}CaCu{sub 2}0{sub x} will be discussed, emphasizing diffusion of the minority defects.

  8. Elevated temperature creep behavior of Inconel alloy 625

    SciTech Connect

    Purohit, A.; Burke, W.F.

    1984-07-01

    Inconel 625 in the solution-annealed condition has been selected as the clad material for the fuel and control rod housing assemblies of the Upgraded Transient Reactor Test Facility (TREAT Upgrade or TU). The clad is expected to be subjected to temperatures up to about 1100/sup 0/C. Creep behavior for the temperature range of 800/sup 0/C to 1100/sup 0/C of Inconel alloy 625, in four distinct heat treated conditions, was experimentally evaluated.

  9. Creep Deformation and Rupture Behavior of Single- and Dual-Pass 316LN Stainless-Steel-Activated TIG Weld Joints

    NASA Astrophysics Data System (ADS)

    Vijayanand, V. D.; Vasudevan, M.; Ganesan, V.; Parameswaran, P.; Laha, K.; Bhaduri, A. K.

    2016-03-01

    Creep deformation and rupture behavior of single-pass and dual-pass 316LN stainless steel (SS) weld joints fabricated by an autogenous activated tungsten inert gas welding process have been assessed by performing metallography, hardness, and conventional and impression creep tests. The fusion zone of the single-pass joint consisted of columnar zones adjacent to base metals with a central equiaxed zone, which have been modified extensively by the thermal cycle of the second pass in the dual-pass joint. The equiaxed zone in the single-pass joint, as well as in the second pass of the dual-pass joint, displayed the lowest hardness in the joints. In the dual-pass joint, the equiaxed zone of the first pass had hardness comparable to the columnar zone. The hardness variations in the joints influenced the creep deformation. The equiaxed and columnar zone in the first pass of the dual-pass joint was more creep resistant than that of the second pass. Both joints possessed lower creep rupture life than the base metal. However, the creep rupture life of the dual-pass joint was about twofolds more than that of the single-pass joint. Creep failure in the single-pass joint occurred in the central equiaxed fusion zone, whereas creep cavitation that originated in the second pass was blocked at the weld pass interface. The additional interface and strength variation between two passes in the dual-pass joint provides more restraint to creep deformation and crack propagation in the fusion zone, resulting in an increase in the creep rupture life of the dual-pass joint over the single-pass joint. Furthermore, the differences in content, morphology, and distribution of delta ferrite in the fusion zone of the joints favors more creep cavitation resistance in the dual-pass joint over the single-pass joint with the enhancement of creep rupture life.

  10. Creep Deformation and Rupture Behavior of Single- and Dual-Pass 316LN Stainless-Steel-Activated TIG Weld Joints

    NASA Astrophysics Data System (ADS)

    Vijayanand, V. D.; Vasudevan, M.; Ganesan, V.; Parameswaran, P.; Laha, K.; Bhaduri, A. K.

    2016-06-01

    Creep deformation and rupture behavior of single-pass and dual-pass 316LN stainless steel (SS) weld joints fabricated by an autogenous activated tungsten inert gas welding process have been assessed by performing metallography, hardness, and conventional and impression creep tests. The fusion zone of the single-pass joint consisted of columnar zones adjacent to base metals with a central equiaxed zone, which have been modified extensively by the thermal cycle of the second pass in the dual-pass joint. The equiaxed zone in the single-pass joint, as well as in the second pass of the dual-pass joint, displayed the lowest hardness in the joints. In the dual-pass joint, the equiaxed zone of the first pass had hardness comparable to the columnar zone. The hardness variations in the joints influenced the creep deformation. The equiaxed and columnar zone in the first pass of the dual-pass joint was more creep resistant than that of the second pass. Both joints possessed lower creep rupture life than the base metal. However, the creep rupture life of the dual-pass joint was about twofolds more than that of the single-pass joint. Creep failure in the single-pass joint occurred in the central equiaxed fusion zone, whereas creep cavitation that originated in the second pass was blocked at the weld pass interface. The additional interface and strength variation between two passes in the dual-pass joint provides more restraint to creep deformation and crack propagation in the fusion zone, resulting in an increase in the creep rupture life of the dual-pass joint over the single-pass joint. Furthermore, the differences in content, morphology, and distribution of delta ferrite in the fusion zone of the joints favors more creep cavitation resistance in the dual-pass joint over the single-pass joint with the enhancement of creep rupture life.

  11. Multimechanism-Deformation Parameters of Domal Salts Using Transient Creep Analysis

    SciTech Connect

    MUNSON, DARRELL E

    1999-09-01

    Use of Gulf Coast salt domes for construction of very large storage caverns by solution mining has grown significantly in the last several decades. In fact, among the largest developers of storage caverns along the Gulf Coast is the Strategic Petroleum Reserve (SPR) which has purchased or constructed 62 crude oil storage caverns in four storage sites (domes). Although SPR and commercial caverns have been operated economically for many years, the caverns still exhibit some relatively poorly understood behaviors, especially involving creep closure volume loss and hanging string damage from salt falls. Since it is possible to postulate that some of these behaviors stem from geomechanical or reformational aspects of the salt, a method of correlating the cavern response to mechanical creep behavior as determined in the laboratory could be of considerable value. Recently, detailed study of the creep response of domal salts has cast some insight into the influence of different salt origins on cavern behavior. The study used a simple graphical analysis of limited non-steady state data to establish an approach or bound to steady state, as an estimate of the steady state behavior of a given salt. This permitted analysis of sparse creep databases for domal salts. It appears that a shortcoming of this steady state analysis method is that it obscures some critical differences of the salt material behavior. In an attempt to overcome the steady state analysis shortcomings, a method was developed based on integration of the Multimechanism-Deformation (M-D) creep constitutive model to obtain fits to the transient response. This integration process permits definition of all the material sensitive parameters of the model, while those parameters that are constants or material insensitive parameters are fixed independently. The transient analysis method has proven more sensitive to differences in the creep characteristics and has provided a way of defining different behaviors within a

  12. Influence of flowing sodium on creep deformation and rupture behaviour of 316L(N) austenitic stainless steel

    NASA Astrophysics Data System (ADS)

    Ravi, S.; Laha, K.; Mathew, M. D.; Vijayaraghavan, S.; Shanmugavel, M.; Rajan, K. K.; Jayakumar, T.

    2012-08-01

    The influence of flowing sodium on creep deformation and rupture behaviour of AISI 316L(N) austenitic stainless steel has been investigated at 873 K over a stress range of 235-305 MPa. The results were compared with those obtained from testing in air environment. The steady state creep rates of the material were not influenced appreciably by the testing environments. The time to onset of tertiary stage of creep deformation was delayed in sodium environment. The creep-rupture lives of the material increased in sodium environment, which became more pronounced at lower applied stresses. The increase in rupture life of the material in flowing sodium was accompanied by an increase in rupture ductility. The creep damage on specimen surface as well as inside the specimen was less in specimen tested in sodium. SEM fractographic investigation revealed predominantly transgranular dimple failure for the specimen tested in sodium, whereas predominantly intergranular creep failure was observed in the air tested specimens. Almost no oxidation was observed in the specimens creep tested in the sodium environment. Absence of oxidation and less creep damage cavitation extended the secondary state in liquid sodium tests and lead to increase in creep rupture life and ductility of the material as compared to in air.

  13. Probabilistic material degradation under high temperature, fatigue, and creep

    NASA Technical Reports Server (NTRS)

    Boyce, L.

    1993-01-01

    A methodology has been developed and embodied in two computer codes for quantitatively characterizing the material strength degradation of aerospace propulsion system structural components that are subjected to various random effects over the course of their service lives. The codes, PROMISS and PROMISC, constitute a material-resistance model that is used in the NESSUS aerospace structural-reliability program. NESSUS addresses the service life-reducing effects of high temperature, mechanical fatigue, and creep.

  14. High-Temperature Deformation of Dry Diabase with Application to Tectonics on Venus

    NASA Technical Reports Server (NTRS)

    Mackwell, S. J.; Zimmerman, M. E.; Kohlstedt, D. L.

    1998-01-01

    We have performed an experimental study to quantify the high-temperature creep behavior of natural diabase rocks under dry deformation conditions. Samples of both Maryland diabase and Columbia diabase were investigated to measure the effects of temperature, oxygen fugacity, and plagioclase-to-pyroxene ratio on creep strength. Flow laws determined for creep of these diabases were characterized by an activation energy of Q = 485 +/- 30 kJ/mol and a stress exponent of n = 4.7 +/- 0.6, indicative of deformation dominated by dislocation creep processes. Although n and Q are the same for the two rocks within experimental error, the Maryland diabase, which has the lower plagioclase content, is significantly stronger than the Columbia diabase. Thus the modal abundance of the various minerals plays an important role in defining rock strength. Within the s ample-to-sample variation, no clear influence of oxygen fugacity on creep strength could be discerned for either rock. The dry creep strengths of both rocks are significantly greater than values previously measured on diabase under "as-received" or wet conditions. Application of these results to the present conditions in the lithosphere on Venus predicts a high viscosity crust with strong dynamic coupling between mantle convection and crustal deformation, consistent with measurements of topography and gravity for that planet.

  15. Understanding creep in sandstone reservoirs - theoretical deformation mechanism maps for pressure solution in granular materials

    NASA Astrophysics Data System (ADS)

    Hangx, Suzanne; Spiers, Christopher

    2014-05-01

    Subsurface exploitation of the Earth's natural resources removes the natural system from its chemical and physical equilibrium. As such, groundwater extraction and hydrocarbon production from subsurface reservoirs frequently causes surface subsidence and induces (micro)seismicity. These effects are not only a problem in onshore (e.g. Groningen, the Netherlands) and offshore hydrocarbon fields (e.g. Ekofisk, Norway), but also in urban areas with extensive groundwater pumping (e.g. Venice, Italy). It is known that fluid extraction inevitably leads to (poro)elastic compaction of reservoirs, hence subsidence and occasional fault reactivation, and causes significant technical, economic and ecological impact. However, such effects often exceed what is expected from purely elastic reservoir behaviour and may continue long after exploitation has ceased. This is most likely due to time-dependent compaction, or 'creep deformation', of such reservoirs, driven by the reduction in pore fluid pressure compared with the rock overburden. Given the societal and ecological impact of surface subsidence, as well as the current interest in developing geothermal energy and unconventional gas resources in densely populated areas, there is much need for obtaining better quantitative understanding of creep in sediments to improve the predictability of the impact of geo-energy and groundwater production. The key problem in developing a reliable, quantitative description of the creep behaviour of sediments, such as sands and sandstones, is that the operative deformation mechanisms are poorly known and poorly quantified. While grain-scale brittle fracturing plus intergranular sliding play an important role in the early stages of compaction, these time-independent, brittle-frictional processes give way to compaction creep on longer time-scales. Thermally-activated mass transfer processes, like pressure solution, can cause creep via dissolution of material at stressed grain contacts, grain

  16. Intragranular deformation heterogeneities during the creep of ice polycrystals: experimental measurements vs. modeling

    NASA Astrophysics Data System (ADS)

    Grennerat, F.; Montagnat, M.; Castelnau, O.; Vacher, P.; Suquet, P.; Moulinec, H.; Duval, P.

    2011-12-01

    Similarly as minerals from the Earth mantle, ice exhibits a strongly anisotropic rheology resulting from the small number of independent slip systems for dislocations. Therefore, a significant heterogeneity of stress and strain distributions is expected at the inter- and intra-granular scale during polycrystal deformation, owing to the mechanical interaction between adjacent grains. A Digital Image Correlation (DIC) technique has been adapted to polycrystalline ice specimens in order to characterize the development of strain heterogeneities at an intragranular scale during transient creep deformation. Specimens exhibit a columnar microstructure so that plastic deformation is essentially 2-D with no in-depth gradients, and therefore surface DIC analyses are representative for the whole specimen volume. Local misorientations at the intragranular scale were also extracted from microstructure analyses carried out with an automatic texture analyzer before and after deformation. Highly localized strain patterns are evidenced by the DIC technique. Local equivalent strain can reach values as high as one order of magnitude larger than the macroscopic average. The structure of the strain pattern does not evolve with strain in the transient creep regime. Almost no correlation between the measured local strain and the Schmid factor of the slip plane of the underlying grain is observed, highlighting the importance of the mechanical interactions between neighboring grains resulting from the very large viscoplastic anisotropy of ice crystals. Finally, the experimental microstructure was introduced in a full-field FFT polycrystal model; simulated strain fields are in good match with experimental ones.

  17. High Precision Measurements of Temperature Dependence of Creep Rate of Polycrystalline Forsterite

    NASA Astrophysics Data System (ADS)

    Nakakoji, T.; Hiraga, T.

    2014-12-01

    Obtaining temperature dependence of creep rate, that is, activation energy for the creep is critical in geophysics, since its value can indicate deformation mechanism and also allows to extrapolate the creep rate measured in the room experiments to geological conditions when the creep mechanism is identical in both cases. Although numerous experimental results have been obtained so far, the obtained activation energy often contains error range of >50 kJ/mol, which often causes large uncertainties in strain rate at applied geological conditions. To minimize this error, it is important to collect strain rates at many different temperatures with high accuracy. We conducted high temperature compression experiments on synthetic forsterite (90%vol) and enstatite (10vol %) aggregates under increasing and decreasing temperatures. We applied a constant load of ~20 MPa using uniaxial testing machine (Shimadzu AG-X 50kN). The temperature was changed from 1360°C to 1240°C by furnace attached to the machine. Prior to the applying the load to the samples the grain size was saturated at 1360°C for 24 hours to minimize grain growth during the test. Decreasing-rate of temperature was 0.11min/°C and 0.02min/°C at temperature ranges of 1360 to 1300 and 1300 to 1240 respectively. The increasing-rate of the temperature was the same as the decreasing-rate. Strain rates from every 1 degree were obtained successfully. After the experiment, we analyzed the microstructure of the sample with scanning electron microscopy to measure the grain diameter. Arrhenius plots of strain rate demonstrate very linear distribution at > 1300 °C giving an activation energy of 649 ± 14 kJ/mol, whereas weak transition to lower activation energy 550 ± 23 kJ/mol below 1300°C was observed. Tasaka et al. (2013) obtained the activation energy of 370 ± 50 kJ/mol from similar temperature ranges used in our study but finer-grained samples. Combining these results, we interpret our results of high activation

  18. Cell structure in cold worked and creep deformed phosphorus alloyed copper

    SciTech Connect

    Wu, Rui; Pettersson, Niklas; Martinsson, Åsa; Sandström, Rolf

    2014-04-01

    Transmission electron microscopy (TEM) examinations on as-received, cold worked, as well as cold worked and creep tested phosphorus-alloyed oxygen-free copper (Cu-OFP) have been carried out to study the role of the cell structure. The cell size decreased linearly with increasing plastic deformation in tension. The flow stress in the tests could also be correlated to the cell size. The observed relation between the flow stress and the cell size was in excellent agreement with previously published results. The dense dislocation walls that appeared after cold work in tension is likely to be the main reason for the dramatic increase in creep strength. The dense dislocation walls act as barriers against dislocation motion and their presence also reduces the recovery rate due to an unbalanced dislocation content.

  19. Developing Dislocation Subgrain Structures and Cyclic Softening During High-Temperature Creep-Fatigue of a Nickel Alloy

    NASA Astrophysics Data System (ADS)

    Carroll, M. C.; Carroll, L. J.

    2013-08-01

    The complex cyclic deformation response of Alloy 617 under creep-fatigue conditions is of practical interest both in terms of the observed detriment in failure life and the considerable cyclic softening that occurs. At the low strain ranges investigated, the inelastic strain is the sole predictor of the failure life without taking into consideration a potentially significant environmental influence. The tensile-hold creep-fatigue peak stress response can be directly correlated to the evolving dislocation substructure, which consists of a relatively homogenous distribution of subgrains. Progressive high-temperature cycling with a static hold allows for the rearrangement of loose tangles of dislocations into well-ordered hexagonal dislocation networks. The cyclic softening during tensile-hold creep-fatigue deformation is attributable to two factors: the rearrangement of dislocation substructures into lower-energy configurations, which includes a decreasing dislocation density in subgrain interiors through integration into the subgrain boundaries, and the formation of surface grain boundary cracks and cavity formation or separation at interior grain boundaries, which occurs perpendicular to the stress axis. Effects attributable to the tensile character of the hold cycle are further analyzed through variations in the creep-fatigue waveform and illuminate the effects of the hold-time character on the overall creep-fatigue behavior and evolution of the dislocation substructure.

  20. High-precision Non-Contact Measurement of Creep of Ultra-High Temperature Materials for Aerospace

    NASA Technical Reports Server (NTRS)

    Rogers, Jan R.; Hyers, Robert

    2008-01-01

    For high-temperature applications (greater than 2,000 C) such as solid rocket motors, hypersonic aircraft, nuclear electric/thermal propulsion for spacecraft, and more efficient jet engines, creep becomes one of the most important design factors to be considered. Conventional creep-testing methods, where the specimen and test apparatus are in contact with each other, are limited to temperatures approximately 1,700 C. Development of alloys for higher-temperature applications is limited by the availability of testing methods at temperatures above 2000 C. Development of alloys for applications requiring a long service life at temperatures as low as 1500 C, such as the next generation of jet turbine superalloys, is limited by the difficulty of accelerated testing at temperatures above 1700 C. For these reasons, a new, non-contact creep-measurement technique is needed for higher temperature applications. A new non-contact method for creep measurements of ultra-high-temperature metals and ceramics has been developed and validated. Using the electrostatic levitation (ESL) facility at NASA Marshall Space Flight Center, a spherical sample is rotated quickly enough to cause creep deformation due to centrifugal acceleration. Very accurate measurement of the deformed shape through digital image analysis allows the stress exponent n to be determined very precisely from a single test, rather than from numerous conventional tests. Validation tests on single-crystal niobium spheres showed excellent agreement with conventional tests at 1985 C; however the non-contact method provides much greater precision while using only about 40 milligrams of material. This method is being applied to materials including metals and ceramics for non-eroding throats in solid rockets and next-generation superalloys for turbine engines. Recent advances in the method and the current state of these new measurements will be presented.

  1. Modeling of high homologous temperature deformation behavior for stress and life-time analyses

    SciTech Connect

    Krempl, E.

    1997-12-31

    Stress and lifetime analyses need realistic and accurate constitutive models for the inelastic deformation behavior of engineering alloys at low and high temperatures. Conventional creep and plasticity models have fundamental difficulties in reproducing high homologous temperature behavior. To improve the modeling capabilities {open_quotes}unified{close_quotes} state variable theories were conceived. They consider all inelastic deformation rate-dependent and do not have separate repositories for creep and plasticity. The viscoplasticity theory based on overstress (VBO), one of the unified theories, is introduced and its properties are delineated. At high homologous temperature where secondary and tertiary creep are observed modeling is primarily accomplished by a static recovery term and a softening isotropic stress. At low temperatures creep is merely a manifestation of rate dependence. The primary creep modeled at low homologous temperature is due to the rate dependence of the flow law. The model is unaltered in the transition from low to high temperature except that the softening of the isotropic stress and the influence of the static recovery term increase with an increase of the temperature.

  2. Dissolution and Replacement Creep:A Significant Deformation Mechanism in Mid-crustal Rocks

    NASA Astrophysics Data System (ADS)

    Wintsch, R. P.

    2001-12-01

    Zoning patterns and zoning truncations in metamorphic minerals in a granodioritic orthogneiss from the Bronson Hill terrane, New England indicate that strain and S-C fabrics in these rocks were produced by dissolution, precipitation, and replacement processes, even at epidote-amphibolite facies metamorphic conditions. The metamorphic fabric is defined by alternating layers and folia dominated by quartz, feldspars, and biotite + epidote. Zoning patterns in most metamorphic plagioclase, orthoclase, epidote, and sphene are truncated at boundaries normal to the shortening direction, suggesting dissolution. Interfaces of relict igneous orthoclase phenocrysts that face the shortening direction are embayed and replaced by biotite, epidote and myrmekitic intergrowths of plagioclase and quartz. Metamorphic plagioclase grains are also replaced by epidote. We interpret these microstructures to reflect strain-enhanced dissolution. The cores of many grains show asymmetric overgrowths with at least two generations of beards, all oriented on the ends of grains that face the extension direction. We interpret these textures to reflect precipitation of components dissolved by deformation enhanced dissolution. While biotite and quartz probably deformed by dislocation creep, the overall deformation was accommodated by dissolution perpendicular to the shortening direction, and precipitation parallel to it. These chemical processes must have been activated at lower stresses than the dislocation creep predicted from extrapolations of data from experiments in dry rocks. Thus wet crust is likely to be weaker than calculated from these experimental studies. Where such processes dominate, stress may not be high enough to reach brittle failure.

  3. Dissolution and replacement creep: a significant deformation mechanism in mid-crustal rocks

    NASA Astrophysics Data System (ADS)

    Wintsch, R. P.; Yi, Keewook

    2002-07-01

    Zoning patterns and zoning truncations in metamorphic minerals in a granodioritic orthogneiss indicate that strain and S- C fabrics in these rocks were produced by dissolution, precipitation, and replacement processes, even at epidote-amphibolite facies metamorphic conditions. The metamorphic fabric is defined by alternating layers and folia dominated by quartz, feldspars, and biotite+epidote. Zoning patterns in most metamorphic plagioclase, orthoclase, epidote, and sphene are truncated at boundaries normal to the shortening direction, suggesting dissolution. Interfaces of relict igneous orthoclase phenocrysts that face the shortening direction are embayed and replaced by biotite, epidote, and myrmekitic intergrowths of plagioclase and quartz. Metamorphic plagioclase grains are also replaced by epidote. We interpret these microstructures to reflect strain-enhanced dissolution. The cores of many grains show asymmetric overgrowths with at least two generations of beards, all oriented on the ends of grains that face the extension direction. We interpret these textures to reflect precipitation of components dissolved by deformation-enhanced dissolution. While biotite and quartz probably deformed by dislocation creep, the overall deformation was accommodated by dissolution perpendicular to the shortening direction, and precipitation parallel to it. These chemical processes must have been activated at lower stresses than the dislocation creep predicted from extrapolations of data from experiments in dry rocks. Thus wet crust is likely to be weaker than calculated from these experimental studies.

  4. An experimental study of uniaxial creep, cyclic creep and relaxation of aisi type 304 stainless steel at room temperature

    NASA Astrophysics Data System (ADS)

    Kujawski, D.; Kallianpur, V.; Krempl, E.

    1980-04-01

    FOLLOWING previous work ( KREMPL, 1979), a servocontrolled testing machine and strain measurement at the gage length were used to study the uniaxial rate(time)-dependent behavior of AISI Type 304 stainless steel at room temperature. The test results show that the creep strain accumulated in a given period of time depends strongly on the stress-rate preceding the creep test. In constant stress-rate zero-to-tension loading the creep strain accumulated in a fixed time-period at a given stress level is always higher during loading than during unloading. Continued cycling causes an exhaustion of creep ratchetting which depends on the stress-rate. Periods of creep and relaxation introduced during completely reversed plastic cycling show that the curved portions of the hysteresis loop exhibit most of the inelasticity. In the straight portions, creep and relaxation are small and there exists a region commencing after unloading where the behavior is similar to that at the origin for virgin materials. This region does not extend to zero stress. The results are at variance with creep theory and with viscoplasticity theories which assume that the yield surface expands with the stress. They support the theory of viscoplasticity based on total strain and overstress.

  5. Ambient-temperature creep failure of silver-aided diffusion bonds between steel

    SciTech Connect

    Henshall, G.A.; Kassner, M.E.; Rosen, R.S.

    1990-01-15

    It has long been known that thin (e.g., 1 {mu}m {minus} 1 mm) interlayer bonds between higher strength base materials may have high ultimate tensile or rupture strengths despite the relatively low strength of the filler metal. The high strength of the joint is due to the mechanical constraint provided by the stronger base metals which restricts transverse contraction of the interlayer. The constraint produces a triaxial state or stress and reduces the effective stress, thus reducing the tendency for the interlayer to plastically deform. Plasticity of the base metal reduces the constraint and decreases the strength of the bond. The purpose of this work was twofold. First, the validity of the base-metal- accelerated'' delayed-failure theory for bonds utilizing plastic base metals was checked. Creep-rupture tests were performed on diffusion-bonded specimens using silver interlayers deposited by planar-magnetron sputtering (PMS), a physical vapor-deposition process. The PMS process was preferred because of the superior quality and strength of the bond and because this modern low-temperature joining process is increasingly utilized for joining ceramic and composite materials. The role of plastic base metals in the fracture process was further investigated by conducting tensile-rupture tests of diffusion bonds made with stainless steel base metals of different yield strengths, and therefore different creep rates. The second purpose was to determine whether delayed failure occurs in interlayer bonds between elastic base metals, which do not creep over the range of applied stresses. This question is particularly relevant since many alloys, ceramics and composites fall within this category. Again, ambient and near-ambient temperature creep-rupture tests were performed at a variety of stresses below the UTS of the bond. 25 refs., 7 figs.

  6. Elevated temperature creep properties of NiAl cryomilled with and without Y2O3

    NASA Technical Reports Server (NTRS)

    Whittenberger, J. Daniel; Luton, Michael J.

    1995-01-01

    The creep properties of lots of NiAl cryomilled with and without Y2O3 have been determined in compression and tension. Although identical cryomilling procedures were used, differences in composition were found between the lot ground with 0.5 vol% yttria and the lot ground without Y2O3. Compression testing between 1000 and 1300 K yielded similar creep strengths for both materials, while tensile creep rupture testing indicated that the yttria-containing alloy was slightly stronger than the Y2O3-free version. Both compression and tensile testing showed two deformation regimes; whereas the stress state did not affect the high stress exponent (n approximately equals 10) mechanism, the low stress exponent regime n was approximately 6 in tension and approximately 2 in compression. The strengths in tension were somewhat less than those measured in compression, but the estimated activation energies (Q) of approximately 600 kJ/mol for tensile testing were closer to the previously measured values (approximately 700 kJ/mol) for NiAl-AlN and very different from the Q's of 400 and 200 kJ/mol for compression tests in the high and low stress exponent regimes, respectively. A Larson-Miller comparison indicated that cryomilling can produce an alloy with long-term, high-temperature strength at least equal to conventional superalloys.

  7. High temperature tensile deformation behavior of Grade 92 steel

    NASA Astrophysics Data System (ADS)

    Alsagabi, Sultan; Shrestha, Triratna; Charit, Indrajit

    2014-10-01

    Candidate structural materials for advanced reactors need to have superior high temperature strength and creep-rupture properties among other characteristics. The ferritic-martensitic Grade 92 steel (Fe-9Cr-2W-0.5Mo, wt.%) is considered such a candidate structural material. Tensile tests were performed at temperatures of 600, 650 and 700 °C in the strain rate range of 10-5-10-3 s-1. After analyzing the tensile results using the Bird-Mukherjee-Dorn (BMD) equation, a stress exponent of about 9.5 and an activation energy of about 646 kJ/mol were obtained. In the light of high values of the stress exponent and activation energy, the threshold stress concept was used to elucidate the operating high temperature deformation mechanism. As a result of this modification, the true activation energy and stress exponent of the high temperature deformation in Grade 92 steel were found to be about 245 kJ/mol and 5, respectively. Thus, the dominant high temperature deformation mechanism was identified as the high temperature climb of edge dislocations and the appropriate constitutive equation was developed.

  8. Monotonic and transient creep experiments for single phase gamma TiAl at intermediate temperatures

    SciTech Connect

    Lu, M.; Hemker, K.J.

    1997-12-31

    Monotonic creep experiments (constant stress and constant temperature) of a single phase {gamma} Ti{sub 47}Al{sub 51}Mn{sub 2} were conducted within a temperature region where the yield stress anomaly is observed (500 C--600 C). The creep strength was found to have a normal temperature dependence. In addition to the monotonic creep experiments, temperature change experiments were performed. The creep activation energy obtained by the transient experiments was found to be significantly lower than that obtained from the monotonic experiments. TEM observations indicate that the microstructure evolves throughout creep, and no evidence of the formation of subgrains was observed. Instead, the mobility and the multiplication of ordinary dislocations were found to play a dominant role in intermediate temperature creep of single phase {gamma}TiAl.

  9. Creep deformation and fracture behaviour of a nitrogen-bearing type 316 stainless steel weld metal

    NASA Astrophysics Data System (ADS)

    Sasikala, G.; Mathew, M. D.; Bhanu Sankara Rao, K.; Mannan, S. L.

    1999-08-01

    Creep properties of a nuclear grade type 316 stainless steel (SS) weld metal containing ˜0.08 wt% of nitrogen were studied at 873 and 923 K. These properties were compared with those of a type 316 SS weld metal without nitrogen. In general, the nitrogen-bearing weld metal exhibited better creep and rupture properties. The rupture strengths of the nitrogen-containing weld metal was ˜40% higher than that for the type 316 SS weld metal at both the temperatures. The steady-state (minimum) creep rates were up to two orders of magnitude lower for the nitrogen-containing weld metal compared to 316 SS weld metal. Rupture ductility of nitrogen-containing weld metal was lower at all the test conditions; the long-term ductility at 923 K was below 5%. The differences in creep behaviour of the two weld metals are discussed with respect to the influence of nitrogen on microstructural evolution in the two weld metals.

  10. Transient creep, aseismic damage and slow failure in Carrara marble deformed across the brittle-ductile transition

    NASA Astrophysics Data System (ADS)

    Schubnel, A.; Walker, E.; Thompson, B. D.; Fortin, J.; Guéguen, Y.; Young, R. P.

    2006-09-01

    Two triaxial compression experiments were performed on Carrara marble at high confining pressure, in creep conditions across the brittle-ductile transition. During cataclastic deformation, elastic wave velocity decrease demonstrated damage accumulation (microcracks). Keeping differential stress constant and reducing normal stress induced transient creep events (i.e., fast accelerations in strain) due to the sudden increase of microcrack growth. Tertiary creep and brittle failure followed as damage came close to criticality. Coalescence and rupture propagation were slow (60-200 seconds with ~150 MPa stress drops and millimetric slips) and radiated little energy in the experimental frequency range (0.1-1 MHz). Microstructural analysis pointed out strong interactions between intra-crystalline plastic deformation (twinning and dislocation glide) and brittle deformation (microcracking) at the macroscopic level. Our observations highlight the dependence of acoustic efficiency on the material's rheology, at least in the ultrasonic frequency range, and the role played by pore fluid diffusion as an incubation process for delayed failure triggering.

  11. Creep of 304 LN and 316 L stainless steels at cryogenic temperatures

    SciTech Connect

    Roth, L.D.; Manhardt, A.E.; Dalder, E.N.C.; Kershaw, R.P. Jr.

    1985-08-07

    Creep behavior of Type 304 LN plate and 316 L shielded-metal-arc (SMA)-deposited stainless weld metal was investigated at 4/sup 0/K. Testing was performed at constant load in a creep machine with a cryostat designed for long-term stability. Both transient and steady-state creep were observed during tests lasting over 2000 hours. Steady-state creep rates were much greater than expected from extrapolations of 300-K creep data. Creep rates on the order of 10/sup -10/ s/sup -1/ were observed at stresses around the yield stress for both materials. The stress exponent under these conditions if approx.2.3. Possible creep mechanisms at this temperature and the impact of these results on the design of engineering structures for long-term structural stability at cryogenic temperatures are discussed.

  12. Analytical, Numerical, and Experimental Investigation on a Non-Contact Method for the Measurements of Creep Properties of Ultra-High-Temperature Materials

    NASA Technical Reports Server (NTRS)

    Lee, Jonghyun; Hyers, Robert W.; Rogers, Jan R.; Rathz, Thomas J.; Choo, Hahn; Liaw, Peter

    2006-01-01

    Responsive access to space requires re-use of components such as rocket nozzles that operate at extremely high temperatures. For such applications, new ultra-hightemperature materials that can operate over 2,000 C are required. At the temperatures higher than the fifty percent of the melting temperature, the characterization of creep properties is indispensable. Since conventional methods for the measurement of creep is limited below 1,700 C, a new technique that can be applied at higher temperatures is strongly demanded. This research develops a non-contact method for the measurement of creep at the temperatures over 2,300 C. Using the electrostatic levitator in NASA MSFC, a spherical sample was rotated to cause creep deformation by centrifugal acceleration. The deforming sample was captured with a digital camera and analyzed to measure creep deformation. Numerical and analytical analyses have also been conducted to compare the experimental results. Analytical, numerical, and experimental results showed a good agreement with one another.

  13. Deterministic Multiaxial Creep and Creep Rupture Enhancements for CARES/Creep Integrated Design Code

    NASA Technical Reports Server (NTRS)

    Jadaan, Osama M.

    1998-01-01

    High temperature and long duration applications of monolithic ceramics can place their failure mode in the creep rupture regime. A previous model advanced by the authors described a methodology by which the creep rupture life of a loaded component can be predicted. That model was based on the life fraction damage accumulation rule in association with the modified Monkman-Grant creep rupture criterion. However, that model did not take into account the deteriorating state of the material due to creep damage (e.g., cavitation) as time elapsed. In addition, the material creep parameters used in that life prediction methodology, were based on uniaxial creep curves displaying primary and secondary creep behavior, with no tertiary regime. The objective of this paper is to present a creep life prediction methodology based on a modified form of the Kachanov-Rabotnov continuum damage mechanics (CDM) theory. In this theory, the uniaxial creep rate is described in terms of sum, temperature, time, and the current state of material damage. This scalar damage state parameter is basically an abstract measure of the current state of material damage due to creep deformation. The damage rate is assumed to vary with stress, temperature, time, and the current state of damage itself. Multiaxial creep and creep rupture formulations of the CDM approach are presented in this paper. Parameter estimation methodologies based on nonlinear regression analysis are also described for both, isothermal constant stress states and anisothermal variable stress conditions This creep life prediction methodology was preliminarily added to the integrated design code CARES/Creep (Ceramics Analysis and Reliability Evaluation of Structures/Creep), which is a postprocessor program to commercially available finite element analysis (FEA) packages. Two examples, showing comparisons between experimental and predicted creep lives of ceramic specimens, are used to demonstrate the viability of Ns methodology and the

  14. Modeling creep deformation of a two-phase TiAl/Ti[sub 3]Al alloy with a lamellar microstructure

    SciTech Connect

    Bartholomeusz, M.F. ); Wert, J.A. . Dept. of Materials Science and Engineering)

    1994-10-01

    A two-phase TiAl/Ti[sub 3]Al alloy with a lamellar microstructure has been previously shown to exhibit a lower minimum creep rate than the minimum creep rates of the constituent TiAl and Ti[sub 3]Al single-phase alloys. Fiducial-line experiments described in the present article demonstrate that the creep rates of the constituent phases within the two-phase TiAl/Ti[sub 3]Al lamellar alloy tested in compression are more than an order of magnitude lower than the creep rates of single-phase TiAl and Ti[sub 3]Al alloys tested in compression at the same stress and temperature. Additionally, the fiducial-line experiments show that no interfacial sliding of the phases in the TiAl/Ti[sub 3]Al lamellar alloy occurs during creep. The lower creep rate of the lamellar alloy is attributed to enhanced hardening of the constituent phases within the lamellar microstructure. A composite-strength model has been formulated to predict the creep rate of the lamellar alloy, taking into account the lower creep rates of the constituent phases within the lamellar microstructure. Application of the model yields a very good correlation between the predicted an experimentally observed minimum creep rates over moderate stress and temperature ranges.

  15. Modeling creep deformation of a two-phase TiAI/Ti3Al alloy with a lamellar microstructure

    NASA Astrophysics Data System (ADS)

    Bartholomeusz, Michael F.; Wert, John A.

    1994-10-01

    A two-phase TiAl/Ti3Al alloy with a lamellar microstructure has been previously shown to exhibit a lower minimum creep rate than the minimum creep rates of the constituent TiAl and Ti3Al single-phase alloys. Fiducial-line experiments described in the present article demonstrate that the creep rates of the constituent phases within the two-phase TiAl/Ti3Al lamellar alloy tested in compression are more than an order of magnitude lower than the creep rates of single-phase TiAl and Ti3Al alloys tested in compression at the same stress and temperature. Additionally, the fiducial-line experiments show that no interfacial sliding of the phases in the TiAl/Ti3Al lamellar alloy occurs during creep. The lower creep rate of the lamellar alloy is attributed to enhanced hardening of the constituent phases within the lamellar microstructure. A composite-strength model has been formulated to predict the creep rate of the lamellar alloy, taking into account the lower creep rates of the constituent phases within the lamellar micro-structure. Application of the model yields a very good correlation between predicted and experimentally observed minimum creep rates over moderate stress and temperature ranges.

  16. Creep-fatigue interaction at high temperature; Proceedings of the Symposium, 112th ASME Winter Annual Meeting, Atlanta, GA, Dec. 1-6, 1991

    SciTech Connect

    Haritos, G.K.; Ochoa, O.O.

    1991-01-01

    Various papers on creep-fatigue interaction at high temperature are presented. Individual topics addressed include: analysis of elevated temperature fatigue crack growth mechanisms in Alloy 718, physically based microcrack propagation laws for creep-fatigue-environment interaction, in situ SEM observation of short fatigue crack growth in Waspaloy at 700 C under cyclic and dwell conditions, evolution of creep-fatigue life prediction models, TMF design considerations in turbine airfoils of advanced turbine engines. Also discussed are: high temperature fatigue life prediction computer code based on the total strain version of strainrange partitioning, atomic theory of thermodynamics of internal variables, geometrically nonlinear analysis of interlaminar stresses in unsymmetrically laminated plates subjected to uniform thermal loading, experimental investigation of creep crack tip deformation using moire interferometry.

  17. Creep-fatigue interaction at high temperature; Proceedings of the Symposium, 112th ASME Winter Annual Meeting, Atlanta, GA, Dec. 1-6, 1991

    NASA Astrophysics Data System (ADS)

    Haritos, George K.; Ochoa, O. O.

    Various papers on creep-fatigue interaction at high temperature are presented. Individual topics addressed include: analysis of elevated temperature fatigue crack growth mechanisms in Alloy 718, physically based microcrack propagation laws for creep-fatigue-environment interaction, in situ SEM observation of short fatigue crack growth in Waspaloy at 700 C under cyclic and dwell conditions, evolution of creep-fatigue life prediction models, TMF design considerations in turbine airfoils of advanced turbine engines. Also discussed are: high temperature fatigue life prediction computer code based on the total strain version of strainrange partitioning, atomic theory of thermodynamics of internal variables, geometrically nonlinear analysis of interlaminar stresses in unsymmetrically laminated plates subjected to uniform thermal loading, experimental investigation of creep crack tip deformation using moire interferometry. (For individual items see A93-31336 to A93-31344)

  18. Constitutive Modeling of High Temperature Uniaxial Creep-Fatigue and Creep-Ratcheting Responses of Alloy 617

    SciTech Connect

    P.G. Pritchard; L.J. Carroll; T. Hassan

    2013-07-01

    Inconel Alloy 617 is a high temperature creep and corrosion resistant alloy and is a leading candidate for use in Intermediate Heat Exchangers (IHX) of the Next Generation Nuclear Plants (NGNP). The IHX of the NGNP is expected to experience operating temperatures in the range of 800 degrees - 950 degrees C, which is in the creep regime of Alloy 617. A broad set of uniaxial, low-cycle fatigue, fatigue-creep, ratcheting, and ratcheting-creep experiments are conducted in order to study the fatigue and ratcheting responses, and their interactions with the creep response at high temperatures. A unified constitutive model developed at North Carolina State University is used to simulate these experimental responses. The model is developed based on the Chaboche viscoplastic model framework. It includes cyclic hardening/softening, strain rate dependence, strain range dependence, static and dynamic recovery modeling features. For simulation of the alloy 617 responses, new techniques of model parameter determination are developed for optimized simulations. This paper compares the experimental responses and model simulations for demonstrating the strengths and shortcomings of the model.

  19. Experimental characterization of crack tip deformation fields in Alloy 718 at high temperatures

    SciTech Connect

    Liu, J.; Lyons, J.; Sutton, M.; Reynolds, A.

    1998-01-01

    A series of fracture mechanics tests were conducted at temperatures of 650 C and 704 C in air, using Inconel 719. A noncontacting measurement technique, based on computer vision and digital image correlation, was applied to directly measure surface displacements and strains prior to and during creep crack growth. For the first time, quantitative comparisons at elevated temperatures are presented between experimentally measured near-crack-tip deformation fields and theoretical linear elastic and viscoelastic fracture mechanics solutions. The results establish that linear elastic conditions dominate the near-crack-tip displacements and strains at 650 C during crack growth, and confirm that K{sub 1} is a viable continuum-based fracture parameter for creep crack growth characterization. Postmortem fractographic analyses indicate that grain boundary embrittlement leads to crack extension before a significant amount of creep occurs at this temperature. At higher temperatures, however, no crack growth was observed due to crack tip blunting and concurrent stress reduction after load application.

  20. Elevated temperature flow strength, creep resistance and diffusion welding characteristics of Ti-6Al-2Nb-1Ta-0.8Mo

    NASA Technical Reports Server (NTRS)

    Whittenberger, J. D.; Moore, T. J.

    1979-01-01

    A study of the flow strength, creep resistance and diffusion welding characteristics of the titanium alloy Ti-6Al-2Nb-1Ta-0.8Mo has been conducted. Two mill-processed forms of this alloy were examined. The forged material had been processed above the beta transus (approximately 1275 K) while the rolled form had been subjected to work below the beta transus. Between 1150 and 1250 K, the forged material was stronger and more creep resistant than the rolled alloy. Both forms exhibit superplastic characteristics in this temperature range. Strain measurements during diffusion welding experiments at 1200 K reveal that weld interfaces have no measurable effect on the overall creep deformation. Significant deformation appears to be necessary to produce a quality diffusion weld between superplastic materials. A 'soft' interlayer inserted between faying surfaces would seemingly allow manufacture of quality diffusion welds with little overall deformation.

  1. Elevated-temperature flow strength, creep resistance and diffusion welding characteristics of Ti-gAl-2Nb-1Ta-0.8Mo

    NASA Technical Reports Server (NTRS)

    Whittenberger, J. D.; Moore, T. J.

    1977-01-01

    A study of the flow strength, creep resistance and diffusion welding characteristics of the titanium alloy Ti-6Al-2Nb-1Ta-0.8Mo was conducted. Two mill-processed forms of this alloy were examined. The forged material was essentially processed above the beta transus while the rolled form was subjected to considerable work below the beta transus. Between 1150 and 1250 K, the forged material was stronger and more creep resistant than the rolled alloy. Both forms exhibit superplastic characteristics in this temperature range. Strain measurements during diffusion welding experiments at 1200 K reveal that weld interfaces have no measurable effect on the overall creep deformation. Significant deformation appears to be necessary to produce a quality diffusion weld between superplastic materials. A 'soft' interlayer inserted between faying surfaces would seemingly allow manufacture of quality diffusion welds with little overall deformation.

  2. In-situ scanning electron microscopy (sem) observations of the tensile and tensile-creep deformation of Titanium-8Aluminum-1mo-1v (wt.%) alloy

    NASA Astrophysics Data System (ADS)

    Ghosh Dastidar, Indraroop

    Titanium (Ti) and titanium alloys (Ti alloys) are attractive for structural applications, such as in the aerospace and automotive industries due to their high specific strength, excellent corrosion resistance and good ability to withstand elevated temperatures. To develop Ti alloys with better mechanical properties, it is necessary to comprehend the deformation behavior of available Ti alloys. Previous studies performed by another graduate student, Dr. Hongmei Li, involved investigation of the deformation behavior of commercially pure (CP) Ti, Ti-5Al-2.5Sn (wt.%), Ti-3Al-2.5V (wt.%) and Ti-6Al-4V (wt.%) alloys. The current thesis focused on investigating the deformation behavior of Ti-8Al-1Mo-1V (wt.%). In-situ tensile and tensile-creep experiments were performed at temperatures ranging from room temperature (RT) to 650OC inside a scanning electron microscope (SEM), which allowed for the observation of the surface deformation evolution. Electron Back Scattered Diffraction (EBSD) was used to identify the distribution of the active deformation systems. In this thesis efforts were made to characterize the various deformation modes of the Ti-8Al-1Mo-1V (wt.%) alloy as a function of the testing conditions (stress and temperature). It was observed that prismatic slip made up the majority of the observed slip systems during the RT tensile deformation, while basal and prismatic slip were almost equally active during the 455OC tensile deformation. Grain boundary ledges were observed during the elevated temperature tensile-creep deformation and from this observation it was suggested that grain boundary sliding was an active deformation mode. This work also involved estimating the Critical Resolved Shear Stress (CRSS) ratios of the alpha-phase deformation modes. The CRSS ratios were compared with the CRSS ratios of CP Ti and other Ti alloys. Overall, this work was intended to add more data to the scientific literature of Ti alloys in order to better comprehend their

  3. Correlation of creep rate with microstructural changes during high temperature creep

    NASA Technical Reports Server (NTRS)

    Young, C. T.; Hochella, W. A.; Lytton, J. L.

    1973-01-01

    The techniques of electron microscopy were used to examine the microstructural changes which occur during primary creep for two important types of engineering alloys: (1) alloys strengthened by solid-solution additions, and (2) dispersion-strengthened alloys. The metals chosen for study are unalloyed titanium, Ti-6Al-4V, and the cobalt-base alloy, Haynes 188. Results to date on NGR 47-004-108 show that development of prior dislocation substructure in Haynes 188 by 10% prestrain and annealing for one hour at 1800 F increases the time to reach 0.5% creep strain at 1600 F by more than an order of magnitude for creep stresses from 3 to 20 ksi. For creep at 1800 F, similar results were obtaind for stresses above 7 ksi, but the prior substructure decreases creep resistance below 7 ksi. This effect appears to be related to instability of grain structure at 1800 F in prestrained material.

  4. Effect of inclusions on strain localization during high temperature creep of marble

    NASA Astrophysics Data System (ADS)

    Rybacki, E.; Morales, L. G.; Naumann, M.; Dresen, G. H.

    2013-12-01

    The deformation of rocks in the Earth's lower crust is often localized in ductile shear zones. Strain localization in rocks deforming at high temperature and pressures may be induced by various physical, chemical, or structurally-related mechanisms. Here, we studied the initiation and propagation of localized deformation in the ductile deformation regime by high temperature deformation experiments on marble with weak or strong inclusions. As starting material we used samples of coarse-grained Carrara marble containing one or two thin artificially prepared sheets of fine-grained Solnhofen limestone or Arkansas novaculite, which act under the applied experimental conditions as soft or strong material heterogeneities, respectively. Samples were deformed in the dislocation creep regime using a Paterson-type gas deformation apparatus at 900°C temperature and confining pressures of 300-400 MPa. Torsion experiments were performed on hollow cylinder samples at a bulk shear strain rate of ≈1.9 x 10-4 s-1 to shear strains γ between 0.02 and 2.9. At low strain, twisted specimens with weak inclusions show minor strain hardening that is replaced by strain weakening at shear strains in excess of ≈0.1- 0.2. Peak shear stress at the imposed condition is about 20MPa, which is ≈8% lower than the strength of inclusion-free samples. Strain progressively localized within the weak inclusions with increasing bulk strain, approaching at γ ≈ 1 a strain ratio of ≈24 with respect to the adjacent matrix strain. This ratio is about half of the strain ratio that is expected from the creep strength contrast between pure marble and limestone at the measured bulk stress. The localization of strain extended into narrow bands in front of the inclusions, where the degree of localization decays exponentially with increasing distance from the tip of the inclusion. Microstructural analysis shows twinning, recrystallization and the development of a strong crystallographic preferred

  5. Generation of long time creep data on refractory alloys at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Sheffler, K. D.; Ebert, R. R.

    1971-01-01

    Ultrahigh vacuum creep tests were conducted on tantalum, tungsten, and molybdenum alloys to develop creep data and to evaluate the influence of liquid lithium exposure on the creep behavior of the tantalum alloy T-111. Test conditions were generally selected to provide 1% creep in 1000 to 10,000 hours, with test temperatures ranging from 1600 to 2912 F (1144 to 1873 K). Tests on T-111 specimens exposed to vacuum and to liquid lithium for various times and temperatures showed large reductions in creep strength for exposures in the 1800 to 1900 F (1255 to 1310 K) range. Tests on the ASTAR 811c showed a significant influence of grain size on the creep strength of this material, with larger grain size specimens being significantly stronger above the equicohesive temperature of 2000 F (1366 K).

  6. The role of interfacial dislocation networks in high temperature creep of superalloys

    NASA Technical Reports Server (NTRS)

    Gabb, T. P.; Draper, S. L.; Hull, D. R.; Mackay, R. A.; Nathal, M. V.

    1989-01-01

    The dislocation networks generated during high-temperature creep of several single-crystal nickel-based superalloys are analyzed. The networks continually evolve during creep at relatively low temperatures or eventually reach a more stable configuration at high temperatures. Specifically, the role of these networks in directional coarsening processes are studied, along with their formation kinetics, characteristics, and stability during creep. The results of this study combined with previous findings suggest that the directional coarsening process is strongly influenced by elastic strain energy. The dislocation networks formed during primary creep are found to be stable during all subsequent creep stages. Aspects of these dislocation networks are determined to be a product of both the applied creep stress and coherency strains.

  7. Generation of long time creep data on refractory alloys at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Sheffler, K. D.

    1971-01-01

    Ultrahigh vacuum creep tests were performed on tungsten, molybdenum, and tantalum alloys to develop design creep data and to evaluate the influence of liquid lithium exposure on the creep resistance of a tantalum alloy. Test conditions were generally selected to provide 1% creep in 1000 to 10,000 hours, with the test temperatures ranging between 1600 and 2900 F (1144 K and 1866 K). One percent creep life data from a tantalum-base T-111 alloy (Ta-8%W-2%Hf) were analyzed using a station function method to provide an improved parametric representation of the T-111 data. In addition, the minimum creep rate data from an ASTAR 811C alloy (Ta-8%W-1%Re-0.7%Hf0.025%C) were analyzed to determine the stress and temperature dependence of creep rate. Results of this analysis indicated that the activation energy for creep decreased from about 150 Kcal/mole (5130 J/mole) above 2400 F (1589 K) to about 110 Kcal/mole (3760 J/mole) below 2000 F (1361 K). This temperature range corresponds to the range where the creep mechanism changes from grain boundary sliding to intragranular creep.

  8. Application of an Uncoupled Elastic-plastic-creep Constitutive Model to Metals at High Temperature

    NASA Technical Reports Server (NTRS)

    Haisler, W. E.

    1983-01-01

    A uniaxial, uncoupled constitutive model to predict the response of thermal and rate dependent elastic-plastic material behavior is presented. The model is based on an incremental classicial plasticity theory extended to account for thermal, creep, and transient temperature conditions. Revisions to he combined hardening rule of the theory allow for better representation of cyclic phenomenon including the high rate of strain hardening upon cyclic reyield and cyclic saturation. An alternative approach is taken to model the rate dependent inelastic deformation which utilizes hysteresis loops and stress relaxation test data at various temperatures. The model is evaluated and compared to experiments which involve various thermal and mechanical load histories on 5086 aluminum alloy, 304 stainless steel and Hastelloy-X.

  9. Mechanisms of High Temperature/Low Stress Creep of Ni-Based Superalloy Single Crystals

    SciTech Connect

    Michael J. Mills

    2009-03-05

    Cast nickel-based superalloys are used for blades in land-based, energy conversion and powerplant applications, as well as in aircraft gas turbines operating at temperatures up to 1100 C, where creep is one of the life-limiting factors. Creep of superalloy single crystals has been extensively studied over the last several decades. Surprisingly, only recently has work focused specifically on the dislocation mechanisms that govern high temperature and low stress creep. Nevertheless, the perpetual goal of better engine efficiency demands that the creep mechanisms operative in this regime be fully understood in order to develop alloys and microstructures with improved high temperature capability. At present, the micro-mechanisms controlling creep before and after rafting (the microstructure evolution typical of high temperature creep) has occurred have yet to be identified and modeled, particularly for [001] oriented single crystals. This crystal orientation is most interesting technologically since it exhibits the highest creep strength. The major goal of the program entitled ''Mechanisms of High Temperature/Low Stress Creep of Ni-Based Superalloy Single Crystals'' (DOE Grant DE-FG02-04ER46137) has been to elucidate these creep mechanisms in cast nickel-based superalloys. We have utilized a combination of detailed microstructure and dislocation substructure analysis combined with the development of a novel phase-field model for microstructure evolution.

  10. Implications of Microstructural Studies of the SAFOD Gouge for the Strength and Deformation Mechanisms in the Creeping Segment of the San Andreas Fault

    NASA Astrophysics Data System (ADS)

    Hadizadeh, J.; Gratier, J. L.; Mittempergher, S.; Renard, F.; Richard, J.; di Toro, G.; Babaie, H. A.

    2010-12-01

    The San Andreas Fault zone (SAF) in the vicinity of the San Andreas Fault Observatory at Depth (SAFOD)in central California is characterized by an average 21 mm/year aseismic creep and strain release through repeating M<3 earthquakes. Seismic inversion studies indicate that the ruptures occur on clusters of stationary patches making up 1% or less of the total fault surface area. The existence of these so-called asperity patches, although not critical in determining the fault strength, suggests interaction of different deformation mechanisms. What are the deformation mechanisms, and how do the mechanisms couple and factor into the current strength models for the SAF? The SAFOD provides core samples and geophysical data including cores from two shear zones where the main borehole casing is deforming. The studies so far show a weak fault zone with about 200m of low-permeability damage zone without anomalous temperature or high fluid pressure (Zoback et al. EOS 2010). To answer the above questions, we studied core samples and thin sections ranging in measured depths (MD) from 3059m to 3991m including gouge from borehole casing deformation zones. The methods of study included high resolution scanning and transmission electron microscopy, cathodoluminescence imaging, X-ray fluorescence mapping, and energy dispersive X-ray spectroscopy. The microstructural and analytical data suggest that deformation is by a coupling of cataclastic flow and pressure solution accompanied by widespread alteration of feldspar to clay minerals and other neomineralizations. The clay contents of the gouge and streaks of serpentinite are not uniformly distributed, but weakness of the creeping segment is likely to be due to intrinsically low frictional strength of the fault material. This conclusion, which is based on the overall ratio of clay/non-clay constituents and the presence of talc in the actively deforming zones, is consistent with the 0.3-0.45 coefficient of friction for the drill

  11. Creep of CMSX-4 superalloy single crystals: Effects of rafting at high temperature

    SciTech Connect

    Reed, R.C.; Matan, N.; Cox, D.C.; Rist, M.A.; Rae, C.M.F.

    1999-09-29

    The creep performance of (001)-orientated CMSX-4 superalloy single crystals at temperatures beyond 1000 C is analyzed. Rafting of the {gamma}{prime} structure occurs rapidly, e.g., for the 1150 C/100 MPa tests rafting is completed within the first 10 h. At this stage and for a considerable time thereafter the creep strain rate decreases with increasing strain, implying a creep hardening effect which is absent at lower temperatures when the kinetics of rafting is less rapid. Once a critical strain {epsilon}* of (0.7 {+-} 0.3)% is reached, the creep strain increases dramatically and failure occurs within a few tens of hours. It is demonstrated that methods of interpretation which, assume a proportionality between the creep strain rate and creep strain, are unable to account for creep hardening which occurs as a consequence of rafting. A modification is proposed which accounts for the blocking of the glide/climb of {l{underscore}brace}111{r{underscore}brace}{l{underscore}angle}1{bar 1}0{r{underscore}angle} creep dislocations which occurs as the number of vertical {gamma} channels is reduced and cellular dislocation networks become stabilized. Consequently, failure must be taken to be associated with creep cavitation, which occurs predominantly around casting porosity. It is emphasized that more work is required to quantify the interaction between the various creep damage mechanisms.

  12. Nonlinear deformation and localized failure of bacterial streamers in creeping flows

    PubMed Central

    Biswas, Ishita; Ghosh, Ranajay; Sadrzadeh, Mohtada; Kumar, Aloke

    2016-01-01

    We investigate the failure of bacterial floc mediated streamers in a microfluidic device in a creeping flow regime using both experimental observations and analytical modeling. The quantification of streamer deformation and failure behavior is possible due to the use of 200 nm fluorescent polystyrene beads which firmly embed in the extracellular polymeric substance (EPS) and act as tracers. The streamers, which form soon after the commencement of flow begin to deviate from an apparently quiescent fully formed state in spite of steady background flow and limited mass accretion indicating significant mechanical nonlinearity. This nonlinear behavior shows distinct phases of deformation with mutually different characteristic times and comes to an end with a distinct localized failure of the streamer far from the walls. We investigate this deformation and failure behavior for two separate bacterial strains and develop a simplified but nonlinear analytical model describing the experimentally observed instability phenomena assuming a necking route to instability. Our model leads to a power law relation between the critical strain at failure and the fluid velocity scale exhibiting excellent qualitative and quantitative agreeing with the experimental rupture behavior. PMID:27558511

  13. Nonlinear deformation and localized failure of bacterial streamers in creeping flows.

    PubMed

    Biswas, Ishita; Ghosh, Ranajay; Sadrzadeh, Mohtada; Kumar, Aloke

    2016-01-01

    We investigate the failure of bacterial floc mediated streamers in a microfluidic device in a creeping flow regime using both experimental observations and analytical modeling. The quantification of streamer deformation and failure behavior is possible due to the use of 200 nm fluorescent polystyrene beads which firmly embed in the extracellular polymeric substance (EPS) and act as tracers. The streamers, which form soon after the commencement of flow begin to deviate from an apparently quiescent fully formed state in spite of steady background flow and limited mass accretion indicating significant mechanical nonlinearity. This nonlinear behavior shows distinct phases of deformation with mutually different characteristic times and comes to an end with a distinct localized failure of the streamer far from the walls. We investigate this deformation and failure behavior for two separate bacterial strains and develop a simplified but nonlinear analytical model describing the experimentally observed instability phenomena assuming a necking route to instability. Our model leads to a power law relation between the critical strain at failure and the fluid velocity scale exhibiting excellent qualitative and quantitative agreeing with the experimental rupture behavior. PMID:27558511

  14. Creep deformation and mechanisms in Haynes 230 at 800 °C and 900 °C

    NASA Astrophysics Data System (ADS)

    Pataky, Garrett J.; Sehitoglu, Huseyin; Maier, Hans J.

    2013-11-01

    Creep was studied in Haynes 230, a material candidate for the very high temperature reactor's intermediate heat exchanger, at 800 °C and 900 °C. This study focused on the differences between the behavior at the two elevated temperature, and using the microstructure, grain boundary serrations and triple junction strain concentrations were quantitatively identified. There was significant damage in the 900 °C samples and the creep was almost entirely tertiary. In contrast, the 800 °C sample exhibited secondary creep. Using an Arrhenius equation, the minimum creep rate exponents were found to be n ≈ 3 and n ≈ 5 for 900 °C and 800 °C, respectively. The creep mechanisms were identified as solute drag for n ≈ 3 and dislocation climb for n ≈ 5. Strain concentrations were identified at triple junctions and grain boundary serrations using high resolution digital image correlation overlaid on the microstructure. The grain boundary serrations restrict grain boundary sliding which may reduce the creep damage at triple junctions and extend the creep life of Haynes 230 at elevated temperatures.

  15. Quantitative analysis of microstructure deformation in creep fenomena of ferritic SA-213 T22 and austenitic SA-213 TP304H material

    NASA Astrophysics Data System (ADS)

    Mulyana, Cukup; Taufik, Ahmad; Gunawan, Agus Yodi; Siregar, Rustam Efendi

    2013-09-01

    The failure of critical component of fossil fired power plant that operated in creep range (high stress, high temperature and in the long term) depends on its microstructure characteristics. Ferritic low carbon steel (2.25Cr-1Mo) and Austenitic stainless alloy (18Cr-8Ni) are used as a boiler tube in the secondary superheater outlet header to deliver steam before entering the turbin. The tube failure is occurred in a form of rupture, resulting trip that disrupts the continuity of the electrical generation. The research in quantification of the microstructure deformation has been done in predicting the remaining life of the tube through interrupted accelerated creep test. For Austenitic Stainless Alloy (18Cr-8Ni), creep test was done in 550°C with the stress 424.5 MPa and for Ferritic Low Carbon Steel (2.25Cr-1Mo) in 570°C with the stress 189 MPa. The interrupted accelerated creep test was done by stopping the observation in condition 60%, 70%, 80% and 90% of remaining life, the creep test fracture was done before. Then the micro hardness test, photo micro, SEM and EDS were obtained from those samples. Refer to ASTM E122, microstructure parameters were calculated. The results indicated that there are a consistency of decreasing their grain diameters, increasing their grain size numbers, micro hardness, and the length of crack or void number per unit area with the decreasing of remaining life. While morphology of grain (stated in parameter α=LV/LH) relatively constant for austenitic. However, for ferritic the change of morphology revealed significantly. Fracture mode propagation of ferritic material is growth with voids transgranular and intergranular crack, and for austenitic material the fracture growth with intergranular creep fracture void and wedge crack. In this research, it was proposed a formulation of mathematical model for creep behavior corresponding their curve fitting resulted for the primary, secondary and tertiary in accelerated creep test. In

  16. Creep deformation behavior of Sn-3.5Ag solder/Cu couple at small length scales

    SciTech Connect

    Kerr, M.; Chawla, N

    2004-09-06

    In order to adequately characterize the behavior of solder balls in electronic devices, the mechanical behavior of solder joints needs to be studied at small length scales. The creep behavior of single solder ball Sn-Ag/Cu solder joints was studied in shear, at 25, 60, 95, and 130 deg. C, using a microforce testing system. A change in the creep stress exponent with increasing stress was observed and explained in terms of a threshold stress for bypass of Ag{sub 3}Sn particles by dislocations. The stress exponent was also temperature dependent, exhibiting an increase in exponent of two from lower to higher temperature. The activation energy for creep was found to be temperature dependant, correlating with self-diffusion of pure Sn at high temperatures, and dislocation core diffusion of pure Sn at lower temperatures. Normalizing the creep rate for activation energy and the temperature-dependence of shear modulus allowed for unification of the creep data. Microstructure characterization, including preliminary TEM analysis, and fractographic analysis were conducted in order to fully describe the creep behavior of the material.

  17. Creep rupture analysis of a beam resting on high temperature foundation

    NASA Technical Reports Server (NTRS)

    Gu, Randy J.; Cozzarelli, Francis A.

    1988-01-01

    A simplified uniaxial strain controlled creep damage law is deduced with the use of experimental observation from a more complex strain dependent law. This creep damage law correlates the creep damage, which is interpreted as the density variation in the material, directly with the accumulated creep strain. Based on the deduced uniaxial strain controlled creep damage law, a continuum mechanical creep rupture analysis is carried out for a beam resting on a high temperature elastic (Winkler) foundation. The analysis includes the determination of the nondimensional time for initial rupture, the propagation of the rupture front with the associated thinning of the beam, and the influence of creep damage on the deflection of the beam. Creep damage starts accumulating in the beam as soon as the load is applied, and a creep rupture front develops at and propagates from the point at which the creep damage first reaches its critical value. By introducing a series of fundamental assumptions within the framework of technical Euler-Bernoulli type beam theory, a governing set of integro-differential equations is derived in terms of the nondimensional bending moment and the deflection. These governing equations are subjected to a set of interface conditions at the propagating rupture front. A numerical technique is developed to solve the governing equations together with the interface equations, and the computed results are presented and discussed in detail.

  18. High temperature deformation mechanisms of L12-containing Co-based superalloys

    NASA Astrophysics Data System (ADS)

    Titus, Michael Shaw

    Ni-based superalloys have been used as the structural material of choice for high temperature applications in gas turbine engines since the 1940s, but their operating temperature is becoming limited by their melting temperature (Tm =1300degrees C). Despite decades of research, no viable alternatives to Ni-based superalloys have been discovered and developed. However, in 2006, a ternary gamma' phase was discovered in the Co-Al-W system that enabled a new class of Co-based superalloys to be developed. These new Co-based superalloys possess a gamma-gamma' microstructure that is nearly identical to Ni-based superalloys, which enables these superalloys to achieve extraordinary high temperature mechanical properties. Furthermore, Co-based alloys possess the added benefit of exhibiting a melting temperature of at least 100degrees C higher than commercial Ni-based superalloys. Superalloys used as the structural materials in high pressure turbine blades must withstand large thermomechanical stresses imparted from the rotating disk and hot, corrosive gases present. These stresses induce time-dependent plastic deformation, which is commonly known as creep, and new superalloys must possess adequate creep resistance over a broad range of temperature in order to be used as the structural materials for high pressure turbine blades. For these reasons, this research focuses on quantifying high temperature creep properties of new gamma'-containing Co-based superalloys and identifying the high temperature creep deformation mechanisms. The high temperature creep properties of new Co- and CoNi-based alloys were found to be comparable to Ni-based superalloys with respect to minimum creep rates and creep-rupture lives at 900degrees C up to the solvus temperature of the gamma' phase. Co-based alloys exhibited a propensity for extended superlattice stacking fault formation in the gamma' precipitates resulting from dislocation shearing events. When Ni was added to the Co-based compositions

  19. Creep and creep-rupture behavior of Alloy 718

    SciTech Connect

    Brinkman, C.R.; Booker, M.K.; Ding, J.L.

    1991-01-01

    Data obtained from creep and creep-rupture tests conducted on 18 heats of Alloy 718 were used to formulate models for predicting high temperature time dependent behavior of this alloy. Creep tests were conducted on specimens taken from a number of commercial product forms including plate, bar, and forgoing material that had been procured and heat treated in accordance with ASTM specifications B-670 or B-637. Data were obtained over the temperature range of 427 to 760{degree}C ad at test times to about 87,000 h. Comparisons are given between experimental data and the analytical models. The analytical models for creep-rupture included one based on lot-centering regression analysis and two based on the Minimum Commitment Method. A master'' curve approach was used to develop and equation for estimating creep deformation up to the onset of tertiary creep. 11 refs., 13 figs.

  20. Mechanisms Governing the Creep Behavior of High Temperature Alloys for Generation IV Nuclear Energy Systems

    SciTech Connect

    Vasudevan, Vijay; Carroll, Laura; Sham, Sam

    2015-04-06

    This research project, which includes collaborators from INL and ORNL, focuses on the study of alloy 617 and alloy 800H that are candidates for applications as intermediate heat exchangers in GEN IV nuclear reactors, with an emphasis on the effects of grain size, grain boundaries and second phases on the creep properties; the mechanisms of dislocation creep, diffusional creep and cavitation; the onset of tertiary creep; and theoretical modeling for long-term predictions of materials behavior and for high temperature alloy design.

  1. Time-dependent deformation at elevated temperatures in basalt from El Hierro, Stromboli and Teide volcanoes

    NASA Astrophysics Data System (ADS)

    Benson, P. M.; Fahrner, D.; Harnett, C. E.; Fazio, M.

    2014-12-01

    Time dependent deformation describes the process whereby brittle materials deform at a stress level below their short-term material strength (Ss), but over an extended time frame. Although generally well understood in engineering (where it is known as static fatigue or "creep"), knowledge of how rocks creep and fail has wide ramifications in areas as diverse as mine tunnel supports and the long term stability of critically loaded rock slopes. A particular hazard relates to the instability of volcano flanks. A large number of flank collapses are known such as Stromboli (Aeolian islands), Teide, and El Hierro (Canary Islands). Collapses on volcanic islands are especially complex as they necessarily involve the combination of active tectonics, heat, and fluids. Not only does the volcanic system generate stresses that reach close to the failure strength of the rocks involved, but when combined with active pore fluid the process of stress corrosion allows the rock mass to deform and creep at stresses far lower than Ss. Despite the obvious geological hazard that edifice failure poses, the phenomenon of creep in volcanic rocks at elevated temperatures has yet to be thoroughly investigated in a well controlled laboratory setting. We present new data using rocks taken from Stromboli, El Heirro and Teide volcanoes in order to better understand the interplay between the fundamental rock mechanics of these basalts and the effects of elevated temperature fluids (activating stress corrosion mechanisms). Experiments were conducted over short (30-60 minute) and long (8-10 hour) time scales. For this, we use the method of Heap et al., (2011) to impose a constant stress (creep) domain deformation monitored via non-contact axial displacement transducers. This is achieved via a conventional triaxial cell to impose shallow conditions of pressure (<25 MPa) and temperature (<200 °C), and equipped with a 3D laboratory seismicity array (known as acoustic emission, AE) to monitor the micro

  2. High-Temperature Creep Behavior Of Fiber-Reinforced Niobium

    NASA Technical Reports Server (NTRS)

    Petrasek, Donald W.; Titran, Robert H.

    1990-01-01

    Study conducted to determine feasibility of using composite materials in advanced space power systems, described in 22-page report. Tungsten fibers reduce creep and mass in advanced power systems. Reinforcing niobium alloys with tungsten fibers increases their resistances to creep by factors of as much as 10.

  3. Creep Deformation, Rupture Analysis, Heat Treatment and Residual Stress Measurement of Monolithic and Welded Grade 91 Steel for Power Plant Components

    NASA Astrophysics Data System (ADS)

    Shrestha, Triratna

    Modified 9Cr-1 Mo (Grade 91) steel is currently considered as a candidate material for reactor pressure vessels (RPVs) and reactor internals for the Very High Temperature Reactor (VHTR), and in fossil-fuel fired power plants at higher temperatures and stresses. The tensile creep behavior of Grade 91 steel was studied in the temperature range of 600°C to 750°C and stresses between 35 MPa and 350 MPa. Heat treatment of Grade 91 steel was studied by normalizing and tempering the steel at various temperatures and times. Moreover, Thermo-Ca1c(TM) calculation was used to predict the precipitate stability and their evolution, and construct carbon isopleths of Grade 91 steel. Residual stress distribution across gas tungsten arc welds (GTAW) in Grade 91 steel was measured by the time-of-flight neutron diffraction using the Spectrometer for Materials Research at Temperature and Stress (SMARTS) diffractometer at Lujan Neutron Scattering Center, Los Alamos National Laboratory, Los Alamos, NM, USA. Analysis of creep results yielded stress exponents of ˜9-11 in the higher stress regime and ˜1 in the lower stress regime. The creep behavior of Grade 91 steel was described by the modified Bird-Mukherjee-Dorn relation. The rate-controlling creep deformation mechanism in the high stress regime was identified as the edge dislocation climb with a stress exponent of n = 5. On the other hand, the deformation mechanism in the Newtonian viscous creep regime (n = 1) was identified as the Nabarro-Herring creep. Creep rupture data were analyzed in terms of Monkman-Grant relation and Larson-Miller parameter. Creep damage tolerance factor and stress exponent were used to identify the cause of creep damage. The fracture surface morphology of the ruptured specimens was studied by scanning electron microscopy to elucidate the failure mechanisms. Fracture mechanism map for Grade 91 steel was developed based on the available material parameters and experimental observations. The microstructural

  4. ACCEPT: a three-dimensional finite element program for large deformation elastic-plastic-creep analysis of pressurized tubes (LWBR/AWBA Development Program)

    SciTech Connect

    Hutula, D.N.; Wiancko, B.E.

    1980-03-01

    ACCEPT is a three-dimensional finite element computer program for analysis of large-deformation elastic-plastic-creep response of Zircaloy tubes subjected to temperature, surface pressures, and axial force. A twenty-mode, tri-quadratic, isoparametric element is used along with a Zircaloy materials model. A linear time-incremental procedure with residual force correction is used to solve for the time-dependent response. The program features an algorithm which automatically chooses the time step sizes to control the accuracy and numerical stability of the solution. A contact-separation capability allows modeling of interaction of reactor fuel rod cladding with fuel pellets or external supports.

  5. Fatigue and creep-fatigue deformation of several nickel-base superalloys at 650 °c

    NASA Astrophysics Data System (ADS)

    Miner, R. V.; Gayda, J.; Maier, R. D.

    1982-10-01

    Specimens of seven nickel-base superalloys for gas turbine disk application that had been failed in fatigue and creep-fatigue at 650 °C were examined by transmission electron microscopy to observe the effects of composition and microstructure on the deformation characteristics of the alloys. The alloys were Waspaloy, HIP Astroloy, H+F Astroloy, H+F René 95, IN 100, MERL 76, and NASA IIB-7. The amount of bulk deformation observed in all the alloys was low. At inelastic strain amplitudes less than about 10-3 only favorably oriented grains exhibited yielding, and the majority of those had <110> near the tensile axis. Deformation occurred on octahedral systems for all the alloys except MERL 76, which also exhibited primary cube slip. The difference in slip behavior between MERL 76 and its parent composition, IN 100, was attributed to the addition of Nb. Deformation occurred in well-defined slip bands in the alloys that contained only fine aging γ', 0.01 to 0.06 μm in size. Alloys which also contained a population of larger aging γ' particles, 0.1 to 0.3 μm, exhibited more homogeneous deformation. Deformation in the creep-fatigue cycle, which employed a 15 minute dwell at the maximum tensile strain of the cycle, was not greatly different from fatigue deformation except that a few extended faults were formed.

  6. Creep deformation of grain boundary in a highly crystalline SiC fibre.

    PubMed

    Shibayama, Tamaki; Yoshida, Yutaka; Yano, Yasuhide; Takahashi, Heishichiro

    2003-01-01

    Silicon carbide (SiC) matrix composites reinforced by SiC fibres (SiC/SiC composites) are currently being considered as alternative materials in high Ni alloys for high-temperature applications, such as aerospace components, gas-turbine energy-conversion systems and nuclear fusion reactors, because of their high specific strength and fracture toughness at elevated temperatures compared with monolithic SiC ceramics. It is important to evaluate the creep properties of SiC fibres under tensile loading in order to determine their usefulness as structural components. However, it would be hard to evaluate creep properties by monoaxial tensile properties when we have little knowledge on the microstructure of crept specimens, especially at the grain boundary. Recently, a simple fibre bend stress relaxation (BSR) test was introduced by Morscher and DiCarlo to address this problem. Interpretation of the fracture mechanism at the grain boundary is also essential to allow improvement of the mechanical properties. In this paper, effects of stress applied by BSR test on microstructural evolution in advanced SiC fibres, such as Tyranno-SA including small amounts of Al, are described and discussed along with the results of microstructure analysis on an atomic scale by using advanced microscopy. PMID:12741492

  7. High temperature inelastic deformation under uniaxial loading - Theory and experiment

    NASA Technical Reports Server (NTRS)

    Chan, K. S.; Lindholm, U. S.; Bodner, S. R.; Walker, K. P.

    1989-01-01

    The elevated-temperature uniaxial inelastic deformation behavior of an Ni-base alloy, B1900 + Hf, is investigated by performing isothermal tensile, creep, cyclic, stress relaxation, and thermomechanical fatigue tests. The range of strain rates examined is from 10 to the -7th to 100 per sec, while the test temperatures range from 25 to 1093 C. This extensive constitutive data base has been used for evaluating the unified constitutive models of Bodner and Partom (1972) and of Walker (1972) which apply for the small-strain regime. Comparison of test results with independent model predictions indicates good agreement over a broad range of loading conditions, demonstrating the applicability of the unified-constitutive-equation approach for describing the strongly nonlinear and temperature-dependent response of meals under a wide range of deformation and thermal histories. Thus the results give confidence that the unified approach is an effective and efficient approach in which complex history-dependent thermoviscoplastic flow can be represented within a single inelastic strain-rate term.

  8. Influence of deformation behavior, oxydation, and temperature on the long time cyclic stress behavior of high temperature steels

    NASA Technical Reports Server (NTRS)

    Maile, K.

    1982-01-01

    The influence of different parameters on the creep-fatigue behavior of several steel alloys was investigated. The higher the temperature the lower the crack initiation value. Pauses during the cycle reduce the damage. Oxidation reduces and protective gas increases the lifetime. Prior loading and prior deformation reduce the lifetime. Short annealing slightly affects the cycle stress behavior. The test results do not satisfactorily agree with methods of extrapolation and damage accumulation.

  9. Tensile and creep rupture properties of (16) uncoated and (2) coated engineering alloys at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Fritz, L. J.; Koster, W. P.

    1977-01-01

    Sixteen test materials were supplied by NASA-Lewis Research Center as wrought bar or cast remelt stock. The cast remelt stock was cast into test blanks with two such materials being also evaluated after Jocoat coating was applied. Mechanical properties evaluated included tensile, modulus of elasticity, Poisson's Ratio, creep properties and creep rupture strength. Tests were conducted at temperatures applicable to the service temperature of the various alloys. This range extended from room temperature to 1000 C.

  10. Parameter correlation of high-temperature creep constitutive equation for RPV metallic materials

    NASA Astrophysics Data System (ADS)

    Xie, Lin-Jun; Ren, Xin; Shen, Ming-Xue; Tu, Li-Qun

    2015-10-01

    Constant-temperature and constant-load creep tests of SA-508 stainless steel were performed at six temperatures, and the creep behavior and properties of this material were determined. Constitutive models were established based on an isothermal creep method to describe the high-temperature creep behavior of SA-508. Material parameter k, stress exponent nσ, and temperature exponent nt of the established constitutive models were determined through experimental data via numerical optimization techniques. The relationship of k, nσ, and nt was evaluated, and a new coefficient model of k-T, nσ-T, nt-T, and nt-nσ was formulated through the parameters of the isothermal creep equation. Moreover, the isothermal creep equation for this material at every temperature point from 450 °C to 1000 °C was obtained from the models. This method can serve as a reference for isothermal creep analysis and provide a way for the safety assessment of components of reactor pressure vessels.

  11. Processing, Microstructure and Creep Behavior of Mo-Si-B-Based Intermetallic Alloys for Very High Temperature Structural Applications

    SciTech Connect

    Vijay Vasudevan

    2008-03-31

    This research project is concerned with developing a fundamental understanding of the effects of processing and microstructure on the creep behavior of refractory intermetallic alloys based on the Mo-Si-B system. In the first part of this project, the compression creep behavior of a Mo-8.9Si-7.71B (in at.%) alloy, at 1100 and 1200 C was studied, whereas in the second part of the project, the constant strain rate compression behavior at 1200, 1300 and 1400 C of a nominally Mo-20Si-10B (in at.%) alloy, processed such as to yield five different {alpha}-Mo volume fractions ranging from 5 to 46%, was studied. In order to determine the deformation and damage mechanisms and rationalize the creep/high temperature deformation data and parameters, the microstructure of both undeformed and deformed samples was characterized in detail using x-ray diffraction, scanning electron microscopy (SEM) with back scattered electron imaging (BSE) and energy dispersive x-ray spectroscopy (EDS), electron back scattered diffraction (EBSD)/orientation electron microscopy in the SEM and transmission electron microscopy (TEM). The microstructure of both alloys was three-phase, being composed of {alpha}-Mo, Mo{sub 3}Si and T2-Mo{sub 5}SiB{sub 2} phases. The values of stress exponents and activation energies, and their dependence on microstructure were determined. The data suggested the operation of both dislocation as well as diffusional mechanisms, depending on alloy, test temperature, stress level and microstructure. Microstructural observations of post-crept/deformed samples indicated the presence of many voids in the {alpha}-Mo grains and few cracks in the intermetallic particles and along their interfaces with the {alpha}-Mo matrix. TEM observations revealed the presence of recrystallized {alpha}-Mo grains and sub-grain boundaries composed of dislocation arrays within the grains (in Mo-8.9Si-7.71B) or fine sub-grains with a high density of b = 1/2<111> dislocations (in Mo-20Si-10B), which

  12. Generation of long time creep data on refractory alloys at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Sheffler, K. D.; Ebert, R. R.

    1973-01-01

    Four separate studies of various aspects of the vacuum creep behavior of two tantalum alloys (T-111 and ASTAR 811C) and of pure CVD tungsten are reported. The first part of the program involved a study of the influence of high temperature pre-exposure to vacuum or to liquid lithium on the subsequent creep behavior T-111 alloy. Results of this study revealed significant effects of pre-exposure on the 1% creep life of T-111, with life reductions of about 3 orders of magnitude being observed in extreme cases. The second part of this study involved an investigation of the creep behavior of T-111 under conditions of continuously increasing stress and decreasing temperature which simulated the conditions anticipated in radioisotope capsule service. Results of this study showed that such test conditions produced a creep curve having a very unusual shape, and led to the identification of a new creep design parameter for this type of service. The third area of investigation was a study of the influence of heat treatment on the microstructure and creep behavior of ASTAR 811C. The fourth part of the program was directed toward a preliminary characterization of the 1% creep life of CVD tungsten as obtained from two different sources.

  13. Creep deformation and fracture behavior of types 316 and 316L(N) stainless steels and their weld metals

    SciTech Connect

    Sasikala, G.; Mathew, M.D.; Bhanu Sankara Rao, K.; Mannan, S.L.

    2000-04-01

    The creep properties of a nuclear-grade type 316(L) stainless steel (SS) alloyed with nitrogen (316L(N)SS) and its weld metal were studied at 873 and 923 K in the range of applied stresses from 100 to 335 MPa. The results were compared with those obtained on a nuclear-grade type 316 SS, which is lean in nitrogen. The creep rupture lives of the weld metals were found to be lower than those of the respective base metals by a factor of 5 to 10. Both the base and weld metals of 314L(N)SS exhibited better resistance to creep deformation compared to their 316SS counterparts at identical test conditions. A power-law relationship between the minimum creep rate and applied stress was found to be obeyed for both the base and weld metals. Both the weld metals generally exhibited lower rupture elongation than the respective base metals; however, at 873 K, the 316 SS base and weld metals had similar rupture elongation at identical applied stresses. Comparison of the rupture lives of the two steels to the ASME curves for the expected minimum stress to rupture for 316 Ss base and weld metals showed that, for 316L(N) SS, the specifications for maximum allowable stresses based on data for 316 SS could prove overconservative. The influence of nitrogen on the creep deformation and fracture behavior, especially in terms of its modifying the precipitation kinetics, is discussed in light of the microstructural observations. In welds containing {delta} ferrite, the kinetics of its transformation and the nature of the transformation products control the deformation and fracture behavior. The influence of nitrogen on the {delta} ferrite transformation behavior and coarsening kinetics is also discussed, on the basis of extensive characterization by metallographic techniques.

  14. Creep deformation and fracture behavior of types 316 and 316L(N) stainless steels and their weld metals

    NASA Astrophysics Data System (ADS)

    Sasikala, G.; Mannan, S. L.; Mathew, M. D.; Rao, K. Bhanu

    2000-04-01

    The creep properties of a nuclear-grade type 316(L) stainless steel (SS) alloyed with nitrogen (316L(N) SS) and its weld metal were studied at 873 and 923 K in the range of applied stresses from 100 to 335 MPa. The results were compared with those obtained on a nuclear-grade type 316 SS, which is lean in nitrogen. The creep rupture lives of the weld metals were found to be lower than those of the respective base metals by a factor of 5 to 10. Both the base and weld metals of 316L(N) SS exhibited better resistance to creep deformation compared to their 316 SS counterparts at identical test conditions. A power-law relationship between the minimum creep rate and applied stress was found to be obeyed for both the base and weld metals. Both the weld metals generally exhibited lower rupture elongation than the respective base metals; however, at 873 K, the 316 SS base and weld metals had similar rupture elongation at identical applied stresses. Comparison of the rupture lives of the two steels to the ASME curves for the expected minimum stress to rupture for 316 SS base and weld metals showed that, for 316L(N) SS, the specifications for maximum allowable stresses based on data for 316 SS could prove overconservative. The influence of nitrogen on the creep deformation and fracture behavior, especially in terms of its modifying the precipitation kinetics, is discussed in light of the microstructural observations. In welds containing δ ferrite, the kinetics of its transformation and the nature of the transformation products control the deformation and fracture behavior. The influence of nitrogen on the δ ferrite transformation behavior and coarsening kinetics is also discussed, on the basis of extensive characterization by metallographic techniques.

  15. An investigation of the deformation mechanism in grain size-sensitive Newtonian creep

    SciTech Connect

    Wang, J.N.

    2000-04-19

    Creep of polycrystalline materials at low stresses often shows a linear relationship between strain rate and stress, and an inverse dependence on grain size squared or cubed. Attribution of this behavior to diffusional creep or grain boundary sliding (GBS) has evoked much confusion and controversy in the literature. A model is proposed to unify these two creep mechanisms. The model predicts a change in dominant mechanism from diffusional creep to GBS accommodated mainly by diffusion or by GBS itself as the amount of matter moved by diffusion decreases. Corresponding to this change, the model also predicts a spectrum of creep rate with the absolute value being dependent upon the extent of diffusion accommodation. Although experimental data exhibit scattering, most of them are in very good agreement with the prediction of the GBS model. Therefore, it is suggested that the Newtonian creep behavior with grain size dependence be induced by GBS rather than by conventional diffusion creep as believed before.

  16. Theory of collective flux creep. [in high temperature superconductors

    NASA Technical Reports Server (NTRS)

    Feigel'man, M. V.; Geshkenbein, V. B.; Larkin, A. I.; Vinokur, V. M.

    1989-01-01

    The nature of flux-creep phenomena in the case of collective pinning by weak disorder is discussed. The Anderson concept of flux bundle is explored and developed. The dependence of the bundle activation barrier U on current j is studied and is shown to be of power-law type: U(j) is proportional to j exp -alpha. The values of exponent alpha for the different regimes of collective creep are found.

  17. Temperature dependence of creep compliance of highly cross-linked epoxy: A molecular simulation study

    SciTech Connect

    Khabaz, Fardin Khare, Ketan S. Khare, Rajesh

    2014-05-15

    We have used molecular dynamics (MD) simulations to study the effect of temperature on the creep compliance of neat cross-linked epoxy. Experimental studies of mechanical behavior of cross-linked epoxy in literature commonly report creep compliance values, whereas molecular simulations of these systems have primarily focused on the Young’s modulus. In this work, in order to obtain a more direct comparison between experiments and simulations, atomistically detailed models of the cross-linked epoxy are used to study their creep compliance as a function of temperature using MD simulations. The creep tests are performed by applying a constant tensile stress and monitoring the resulting strain in the system. Our results show that simulated values of creep compliance increase with an increase in both time and temperature. We believe that such calculations of the creep compliance, along with the use of time temperature superposition, hold great promise in connecting the molecular insight obtained from molecular simulation at small length- and time-scales with the experimental behavior of such materials. To the best of our knowledge, this work is the first reported effort that investigates the creep compliance behavior of cross-linked epoxy using MD simulations.

  18. High temperature tensile and creep behaviour of low pressure plasma-sprayed Ni-Co-Cr-Al-Y coating alloy

    NASA Technical Reports Server (NTRS)

    Hebsur, M. G.; Miner, R. V.

    1986-01-01

    The high temperature tensile and creep behavior of low pressure plasma-sprayed plates of a typical Ni-Co-Cr-Al-Y alloy has been studied. From room temperature to 800 K, the Ni-Co-Cr-Al-Y alloy studied has nearly a constant low ductility and a high strength. At higher temperatures, it becomes weak and highly ductile. At and above 1123 K, the behavior is highly dependent on strain rate and exhibits classic superplastic characteristics with a high ductility at intermediate strain rates and a strain rate sensitivity of about 0.5. At either higher or lower strain rates, the ductility decreases and the strain rate sensitivities are about 0.2. In the superplastic deformation range, the activation energy for creep is 120 + or - 20 kJ/mol, suggesting a diffusion-aided grain boundary sliding mechanism. Outside the superplastic range, the activation energy for creep is calculated to be 290 + or - 20 kJ/mol.

  19. Creep deformation and buttressing capacity of damaged ice shelves: theory and application to Larsen C ice shelf

    NASA Astrophysics Data System (ADS)

    Borstad, C. P.; Rignot, E.; Mouginot, J.; Schodlok, M. P.

    2013-07-01

    Around the perimeter of Antarctica, much of the ice sheet discharges to the ocean through floating ice shelves. The buttressing provided by ice shelves is critical for modulating the flux of ice into the ocean, and the presently observed thinning of ice shelves is believed to be reducing their buttressing capacity and contributing to the acceleration and thinning of the grounded ice sheet. However, relatively little attention has been paid to the role that fractures play in the flow and stability of ice shelves and their capacity to buttress the flow of grounded ice. Here, we develop an analytical framework for describing the role that fractures play in the creep deformation and buttressing capacity of ice shelves. We apply principles of continuum damage mechanics to derive a new analytical relation for the creep of an ice shelf as a function of ice thickness, temperature, material properties, resistive backstress and damage. By combining this analytical theory with an inverse method solution for the spatial rheology of an ice shelf, both backstress and damage can be calculated. We demonstrate the applicability of this new theory using satellite remote sensing and Operation IceBridge data for the Larsen C ice shelf, finding damage associated with known crevasses and rifts. We find that increasing thickness of mélange between rift flanks correlates with decreasing damage, with some rifts deforming coherently with the ice shelf as if completely healed. We quantify the stabilizing backstress caused by ice rises and lateral confinement, finding high backstress associated with two ice rises that likely stabilize the ice front in its current configuration. Though overall the ice shelf appears stable at present, the ice in contact with the Bawden ice rise is weakened by fractures, and additional damage or thinning in this area could portend significant change for the shelf. Using this new approach, field and remote sensing data can be utilized to monitor the structural

  20. Creep deformation and buttressing capacity of damaged ice shelves: theory and application to Larsen C ice shelf

    NASA Astrophysics Data System (ADS)

    Borstad, C. P.; Rignot, E.; Mouginot, J.; Schodlok, M. P.

    2013-12-01

    Around the perimeter of Antarctica, much of the ice sheet discharges to the ocean through floating ice shelves. The buttressing provided by ice shelves is critical for modulating the flux of ice into the ocean, and the presently observed thinning of ice shelves is believed to be reducing their buttressing capacity and contributing to the acceleration and thinning of the grounded ice sheet. However, relatively little attention has been paid to the role that fractures play in the ability of ice shelves to sustain and transmit buttressing stresses. Here, we present a new framework for quantifying the role that fractures play in the creep deformation and buttressing capacity of ice shelves. We apply principles of continuum damage mechanics to derive a new analytical relation for the creep of an ice shelf that accounts for the softening influence of fractures on longitudinal deformation using a state damage variable. We use this new analytical relation, combined with a temperature calculation for the ice, to partition an inverse method solution for ice shelf rigidity into independent solutions for softening damage and stabilizing backstress. Using this new approach, field and remote sensing data can be utilized to monitor the structural integrity of ice shelves, their ability to buttress the flow of ice at the grounding line, and thus their indirect contribution to ice sheet mass balance and global sea level. We apply this technique to the Larsen C ice shelf using remote sensing and Operation IceBridge data, finding damage in areas with known crevasses and rifts. Backstress is highest near the grounding line and upstream of ice rises, in agreement with patterns observed on other ice shelves. The ice in contact with the Bawden ice rise is weakened by fractures, and additional damage or thinning in this area could diminish the backstress transmitted upstream. We model the consequences for the ice shelf if it loses contact with this small ice rise, finding that flow speeds

  1. Generation of long time creep data on refractory alloys at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Sheffler, K. D.

    1970-01-01

    Creep tests were conducted on two tantalum alloys (ASTAR 811C and T-111 alloy), on a molybdenum alloy (TZM), and on CVD tungsten. The T-111 alloy 1% creep life data have been subjected to Manson's station function analysis, and the progress on this analysis is described. In another test program, the behavior of T-111 alloy with continuously varying temperatures and stresses has been studied. The results indicated that the previously described analysis predicts the observed creep behavior with reasonable accuracy. In addition to the T-111 test program, conventional 1% creep life data have been obtained for ASTAR 811C alloy. Previously observed effects of heat treatment on the creep strength of this material have been discussed and a model involving carbide strengthening primarily at the grain boundaries, rather than in a classical dispersion hardening mechanism, has been proposed to explain the observed results.

  2. Deterministic and Probabilistic Creep and Creep Rupture Enhancement to CARES/Creep: Multiaxial Creep Life Prediction of Ceramic Structures Using Continuum Damage Mechanics and the Finite Element Method

    NASA Technical Reports Server (NTRS)

    Jadaan, Osama M.; Powers, Lynn M.; Gyekenyesi, John P.

    1998-01-01

    High temperature and long duration applications of monolithic ceramics can place their failure mode in the creep rupture regime. A previous model advanced by the authors described a methodology by which the creep rupture life of a loaded component can be predicted. That model was based on the life fraction damage accumulation rule in association with the modified Monkman-Grant creep ripture criterion However, that model did not take into account the deteriorating state of the material due to creep damage (e.g., cavitation) as time elapsed. In addition, the material creep parameters used in that life prediction methodology, were based on uniaxial creep curves displaying primary and secondary creep behavior, with no tertiary regime. The objective of this paper is to present a creep life prediction methodology based on a modified form of the Kachanov-Rabotnov continuum damage mechanics (CDM) theory. In this theory, the uniaxial creep rate is described in terms of stress, temperature, time, and the current state of material damage. This scalar damage state parameter is basically an abstract measure of the current state of material damage due to creep deformation. The damage rate is assumed to vary with stress, temperature, time, and the current state of damage itself. Multiaxial creep and creep rupture formulations of the CDM approach are presented in this paper. Parameter estimation methodologies based on nonlinear regression analysis are also described for both, isothermal constant stress states and anisothermal variable stress conditions This creep life prediction methodology was preliminarily added to the integrated design code CARES/Creep (Ceramics Analysis and Reliability Evaluation of Structures/Creep), which is a postprocessor program to commercially available finite element analysis (FEA) packages. Two examples, showing comparisons between experimental and predicted creep lives of ceramic specimens, are used to demonstrate the viability of this methodology and

  3. Assessment of the deformation of the Bateman bipolar hip prosthesis inner bearing due to moisture absorption and creep.

    PubMed

    Lockie, K; Binns, M; Fisher, J; Jobbins, B

    1992-01-01

    The mechanism of inner bearing stiffness of bipolar hip prostheses has been investigated. The Ultra-high Molecular Weight Polyethylene (UHMWPE) component of the Bateman bipolar hip prosthesis has been subjected to a series of static and dynamic tests to assess water absorption and creep. Although deformation of the UHMWPE occurred, this did not produce an increased resistance to movement in the inner bearing. PMID:1572706

  4. Investigation of the rate-controlling mechanism(s) for high temperature creep and the relationship between creep and melting by use of high pressure as a variable

    SciTech Connect

    Not Available

    1991-01-01

    Using high pressure as a variable, the rate-controlling mechanism for high temperature creep and the relationship between creep and melting is investigated for silicon and nickel. An apparatus is used in which the samples are heated to melting point and subjected to 1 to 3 GigaPascal pressure. The stress behavior of the materials are then studied.

  5. Creeping Deformation by the Precise Leveling Survey at the central part of the Longitudinal valley fault, Southeast Taiwan

    NASA Astrophysics Data System (ADS)

    Matta, N.; Murase, M.; Ishiguro, S.; Ozawa, K.; Lin, J.; Chen, W.; Lin, C.

    2011-12-01

    We would like to know the distributed asperity for seismic hazard and forecast. It is closely related to slip distribution on the fault in interseismic. We focused on the accumulating process of the stress at the boundary between the creeping and the locking zone, to clear the behavior on the fault. The Longitudinal Valley Fault (LVF), 150 km long and NNE-SSW striking, passes through the eastern Taiwan, and represents the obvious surface expression of the collision boundary between the Philippine Sea plate and the Eurasian continental plate. Owing to such a high deformation rate, many earthquakes have occurred along the LVF. The 1951 earthquake sequence represents a good example. The southern of LVF segment is observed to be high speed creeping based on the creep meter and leveling survey etc. The northern of LVF segment is not observed to be creeping and are found huge earthquakes evidence by paleo-seismology study in the trench. Yuili fault is one of the active segments of the longitudinal valley faults, is located around the boundary between creeping and locking area. It is reverse fault with east dip. We established about 30km leveling route from Yuli to Changbin to detect the vertical deformation in detail. Murase et al. (2009, 2010, and 2011) established about 30 km densely leveling route from Yuli to Changbin to detect the vertical deformation across the LVF for two years. As a result, the vertical displacement is 1.7 cm in 200 m across the LVF and 2.7 cm in 1000 m, referred to the west end of our route. In addition, a synclinal deformation is detected on the hanging wall side of the fault. This result is caused by the geometry of and the slipping distribution on the fault. The deformation detected in the period from 2009 to 2010 denotes the same tendency and rate of that from 2008 to 2009. We compared to the airphotographs which are taken by Taiwanese government at different age (1978 and 2007). If the creeping on the fault has continued for 30 years, the

  6. Creep behavior of uranium carbide-based alloys

    NASA Technical Reports Server (NTRS)

    Seltzer, M. S.; Wright, T. R.; Moak, D. P.

    1975-01-01

    The present work gives the results of experiments on the influence of zirconium carbide and tungsten on the creep properties of uranium carbide. The creep behavior of high-density UC samples follows the classical time-dependence pattern of (1) an instantaneous deformation, (2) a primary creep region, and (3) a period of steady-state creep. Creep rates for unalloyed UC-1.01 and UC-1.05 are several orders of magnitude greater than those measured for carbide alloys containing a Zr-C and/or W dispersoid. The difference in creep strength between alloyed and unalloyed materials varies with temperature and applied stress.

  7. Effect of creep in titanium alloy Ti-6Al-4V at elevated temperature on aircraft design and flight test

    NASA Technical Reports Server (NTRS)

    Jenkins, J. M.

    1984-01-01

    Short-term compressive creep tests were conducted on three titanium alloy Ti-6Al-4V coupons at three different stress levels at a temperature of 714 K (825 F). The test data were compared to several creep laws developed from tensile creep tests of available literature. The short-term creep test data did not correlate well with any of the creep laws obtained from available literature. The creep laws themselves did not correlate well with each other. Short-term creep does not appear to be very predictable for titanium alloy Ti-6Al-4V. Aircraft events that result in extreme, but short-term temperature and stress excursions for this alloy should be approached cautiously. Extrapolations of test data and creep laws suggest a convergence toward predictability in the longer-term situation.

  8. Phase Transformation and Creep Behavior in Ti50Pd30Ni20 High Temperature Shape Memory Alloy in Compression

    NASA Technical Reports Server (NTRS)

    Kumar, Parikshith K.; Desai, Uri; Monroe, James; Lagoudas, Dimitris C.; Karaman, Ibrahim; Noebe, Ron; Bigelow, Glenn

    2010-01-01

    The creep behavior and the phase transformation of Ti50Pd30Ni20 High Temperature Shape Memory Alloy (HTSMA) is investigated by standard creep tests and thermomechanical tests. Ingots of the alloy are induction melted, extruded at high temperature, from which cylindrical specimens are cut and surface polished. A custom high temperature test setup is assembled to conduct the thermomechanical tests. Following preliminary monotonic tests, standard creep tests and thermally induced phase transformation tests are conducted on the specimen. The creep test results suggest that over the operating temperatures and stresses of this alloy, the microstructural mechanisms responsible for creep change. At lower stresses and temperatures, the primary creep mechanism is a mixture of dislocation glide and dislocation creep. As the stress and temperature increase, the mechanism shifts to predominantly dislocation creep. If the operational stress or temperature is raised even further, the mechanism shifts to diffusion creep. The thermally induced phase transformation tests show that actuator performance can be affected by rate independent irrecoverable strain (transformation induced plasticity + retained martensite) as well as creep. The rate of heating and cooling can adversely impact the actuators performance. While the rate independent irrecoverable strain is readily apparent early in the actuators life, viscoplastic strain continues to accumulate over the lifespan of the HTSMA. Thus, in order to get full actuation out of the HTSMA, the heating and cooling rates must be sufficiently high enough to avoid creep.

  9. 1/2 CREEP FRACTURE IN CERAMIC POLYCRYSTALS I. CREEP CAVITATION EFFECTS IN POLYCRYSTALLINE ALUMINA

    SciTech Connect

    Porter, J. R.; Blumenthal, W.; Evans, A. G.

    1980-09-01

    Fine grained polycrystalline alumina has been deformed in creep at high temperatures, to examine the evolution of cavities at grain boundaries. Cavities with equilibrium and crack-like morphologies have been observed, distributed non-uniformly throughout the material. The role of cavities during creep has been described. A transition from equilibrium to crack-like morphology has been observed and correlated with a model based on the influence of the surface to boundary diffusivity ratio and the local tensile stress. The contribution of cavitation to the creep rate and total creep strain has been analyzed and excluded as the principal cause of the observed non-linear creep rate,

  10. The effect of environment on the creep deformation of ultra-high purity nickel-chromium-iron alloys at 360 degrees Celcius

    NASA Astrophysics Data System (ADS)

    Paraventi, Denise Jean

    2000-10-01

    Steam generators in pressurized water nuclear power plants have experienced significant problems with intergranular stress corrosion cracking (IGSCC) on the inner diameter of steam generator tubing for over 25 years. In the course of research to understand IGSCC, it has been shown that creep deformation may play a significant role in the cracking of commercial Alloy 600 (Ni-16Cr-9Fe-0.03C). The primary water environment can cause decreases in creep resistance (i.e., faster creep rates, shorter time to failure, and higher creep strains). During corrosion under the conditions of interest, both hydrogen reduction and metal dissolution occur. One or both may contribute to the enhancement of creep. The purpose of this work was to isolate the mechanism by which the water environment causes the creep deformation to increase. Activation area and activation enthalpy for glide were measured in argon and primary water on high purity Ni-16Cr-9Fe alloys. The results indicated that the activation area was reduced by primary water, consistent with a hydrogen enhanced plasticity mechanism for enhanced creep. The stress dependence of creep was also examined in argon and primary water. The results indicated that the internal stress of the alloy is reduced by the primary water environment. Lower internal stress is consistent with both a hydrogen model as well as a vacancy-aided climb model for enhanced creep. To isolate the effect of hydrogen on the creep of the alloy, experiments were conducted in a dissociated hydrogen environment. The results indicated that hydrogen would only increase the steady state creep rate if present before loading of the samples. However, if the sample was already in steady state creep and hydrogen introduced, a transient in the creep strain was observed. The creep rate returned to the original steady state rate in a short time. The results indicate that while hydrogen does affect the steady state creep to an extent, hydrogen cannot completely account for

  11. Creep strength and microstructure of F82H steels near tempering temperature

    NASA Astrophysics Data System (ADS)

    Shinozuka, K.; Esaka, H.; Sakasegawa, H.; Tanigawa, H.

    2015-09-01

    Creep rupture tests near the tempering temperature were performed, and the creep behavior at high temperatures and the structures of fracture specimens were investigated. Three kinds of F82H test specimens were used: IEA-heat, mod.3, and BA07. The time-to-rupture of the BA07 specimens was the longest under all the test conditions. This was because the minimum creep rates of BA07 were smallest, and a large quantity of fine precipitates of MX from the ESR treatment were considered to be effective in providing creep resistance. Although mod.3 specimens showed a high creep resistance under high stress, the time-to-rupture of mod.3 and IEA-heat were almost the same at low stress. This was because the fine tempered martensitic structure was weakened by being subjected to a high temperature for a long period. Therefore, it is considered that a large quantity of fine MX precipitates are effective for creep resistance near the tempering temperature.

  12. Low Temperature Creep of a Titanium Alloy Ti-6Al-2Cb-1Ta-0.8Mo

    NASA Technical Reports Server (NTRS)

    Chu, H. P.

    1997-01-01

    This paper presents a methodology for the analysis of low temperature creep of titanium alloys in order to establish design limitations due to the effect of creep. The creep data on a titanium Ti-6Al-2Cb-1Ta-0.8Mo are used in the analysis. A creep equation is formulated to determine the allowable stresses so that creep at ambient temperatures can be kept within an acceptable limit during the service life of engineering structures or instruments. Microcreep which is important to design of precision instruments is included in the discussion also.

  13. Effects of cold rolling deformation on microstructure, hardness, and creep behavior of high nitrogen austenitic stainless steel

    NASA Astrophysics Data System (ADS)

    Sun, Shi-Cheng; Sun, Gui-Xun; Jiang, Zhong-Hao; Ji, Chang-Tao; Liu, Jia-An; Lian, Jian-She

    2014-02-01

    Effects of cold rolling deformation on the microstructure, hardness, and creep behavior of high nitrogen austenitic stainless steel (HNASS) are investigated. Microstructure characterization shows that 70% cold rolling deformation results in significant refinement of the microstructure of this steel, with its average twin thickness reducing from 6.4 μm to 14 nm. Nanoindentation tests at different strain rates demonstrate that the hardness of the steel with nano-scale twins (nt-HNASS) is about 2 times as high as that of steel with micro-scale twins (mt-HNASS). The hardness of nt-HNASS exhibits a pronounced strain rate dependence with a strain rate sensitivity (m value) of 0.0319, which is far higher than that of mt-HNASS (m = 0.0029). nt-HNASS shows more significant load plateaus and a higher creep rate than mt-HNASS. Analysis reveals that higher hardness and larger m value of nt-HNASS arise from stronger strain hardening role, which is caused by the higher storage rate of dislocations and the interactions between dislocations and high density twins. The more significant load plateaus and higher creep rates of nt-HNASS are due to the rapid relaxation of the dislocation structures generated during loading.

  14. Creep of dry clinopyroxene aggregates

    NASA Astrophysics Data System (ADS)

    Bystricky, Misha; Mackwell, Stephen

    2001-01-01

    We have determined diffusional and dislocation creep rheologies for clinopyroxenite Ca1.0Mg0.8Fe0.2Si2O6 under dry conditions by deforming natural and hot-pressed samples at confining pressures of 300-430 MPa and temperatures of 1100°-1250°C with the oxygen fugacity buffered by either nickel-nickel oxide or iron-wüstite powders. The coarse-grained natural Sleaford Bay clinopyroxenite yielded a stress exponent of n = 4.7 ± 0.2 and an activation energy for creep of Q = 760 ± 40 kJ mol-1, consistent with deformation in the dislocation creep regime. The strength of the natural clinopyroxenite is consistent with previous high-temperature measurements of dislocation creep behavior of Sleaford Bay clinopyroxenite by Kirby and Kronenberg [1984] and Boland and Tullis [1986]. Fine-grained clinopyroxenite was prepared from ground powders of the natural clinopyroxenite. Hot-pressed samples were deformed under similar conditions to the natural samples. Mixed-mode deformation behavior was observed, with diffusional creep (n = 1) at lower differential stresses and dislocation creep (with n and Q similar to those of the natural samples) at higher differential stresses. Within the dislocation creep field the predried hot-pressed samples generally yielded creep rates that were about an order of magnitude faster than the natural samples. Thus, even at the highest differential stresses, a component of strain accommodation by grain boundary diffusion was present in the hot-pressed samples. Optical and electron microscope investigations of the deformation microstructures of the natural and hot-pressed samples show evidence for mechanical twinning and activation of dislocation slip systems. When extrapolated to geological conditions expected in the deep crust and upper mantle on Earth and other terrestrial planets, the strength of dry single-phase clinopyroxene aggregates is very high, exceeding that of dry olivine-rich rocks.

  15. Static tensile and tensile creep testing of four boron nitride coated ceramic fibers at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Coguill, Scott L.; Adams, Donald F.; Zimmerman, Richard S.

    1989-01-01

    Six types of uncoated ceramic fibers were static tensile and tensile creep tested at various elevated temperatures. Three types of boron nitride coated fibers were also tested. Room temperature static tensile tests were initially performed on all fibers, at gage lengths of 1, 2, and 4 inches, to determine the magnitude of end effects from the gripping system used. Tests at one elevated temperature, at gage lengths of 8 and 10 inches, were also conducted, to determine end effects at elevated temperatures. Fiber cross sectional shapes and areas were determined using scanning electron microscopy. Creep testing was typically performed for 4 hours, in an air atmosphere.

  16. Creep-fatigue interaction in aircraft gas turbine components by simulation and testing at scaled temperatures

    NASA Astrophysics Data System (ADS)

    Sabour, Mohammad Hossein

    Advanced gas turbine engines, which use hot section airfoil cooling, present a wide range of design problems. The frequencies of applied loads and the natural frequencies of the blade also are important since they have significant effects on failure of the component due to fatigue phenomenon. Due to high temperature environment the thermal creep and fatigue are quite severe. One-dimensional creep model, using ANSYS has been formulated in order to predict the creep life of a gas turbine engine blade. Innovative mathematical models for the prediction of the operating life of aircraft components, specifically gas turbine blades, which are subjected to creep-fatigue at high temperatures, are proposed. The components are modeled by FEM, mathematically, and using similitude principles. Three models have been suggested and evaluated numerically and experimentally. Using FEM method for natural frequencies causes phenomena such as curve veering which is studied in more detail. The simulation studies on the life-limiting modes of failure, as well as estimating the expected lifetime of the blade, using the proposed models have been carried out. Although the scale model approach has been used for quite some time, the thermal scaling has been used in this study for the first time. The only thermal studies in literature using scaling for structures is by NASA in which materials of both the prototype and the model are the same, but in the present study materials also are different. The finite element method is employed to model the structure. Because of stress redistribution due to the creep process, it is necessary to include a full inelastic creep step in the finite element formulation. Otherwise over-conservative creep life predictions will be estimated if only the initial elastic stresses are considered. The experimental investigations are carried out in order to validate the models. The main contributions in the thesis are: (1) Using similitude theory for life prediction of

  17. Static tensile and tensile creep testing of five ceramic fibers at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Zimmerman, Richard S.; Adams, Donald F.

    1989-01-01

    Static tensile and tensile creep testing of five ceramic fibers at elevated temperature was performed. J.P. Stevens, Co., Astroquartz 9288 glass fiber; Nippon Carbon, Ltd., (Dow Corning) nicalon NLM-102 silicon carbide fiber; and 3M Company Nextel 312, 380, and 480 alumina/silica/boria fibers were supplied in unsized tows. Single fibers were separated from the tows and tested in static tension and tensile creep. Elevated test temperatures ranged from 400 C to 1300 C and varied for each fiber. Room temperature static tension was also performed. Computer software was written to reduce all single fiber test data into engineering constants using ASTM Standard Test Method D3379-75 as a reference. A high temperature furnace was designed and built to perform the single fiber elevated temperature testing up to 1300 C. A computerized single fiber creep apparatus was designed and constructed to perform four fiber creep tests simultaneously at temperatures up to 1300 C. Computer software was written to acquire and reduce all creep data.

  18. Static tensile and tensile creep testing of five ceramic fibers at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Zimmerman, Richard S.; Adams, Donald F.

    1988-01-01

    Static tensile and tensile creep testing of five ceramic fibers at elevated temperature was performed. J.P. Stevens, Co., Astroquartz 9288 glass fiber, Nippon Carbon, Ltd., (Dow Corning) Nicalon NLM-102 silicon carbide fiber, and 3M Company Nextel 312, 380, and 480 alumina/silica/boria fibers were supplied in unsized tows. Single fibers were separated from the tows and tested in static tension and tensile creep. Elevated test temperatures ranged from 400 to 1300 C and varied for each fiber. Room temperature static tension was also performed. Computer software was written to reduce all single fiber test data into engineering constants using ASTM Standard Test Method D3379-75 as a reference. A high temperature furnace was designed and built to perform the single fiber elevated temperature testing up to 1300 C. A computerized single fiber creep apparatus was designed and constructed to perform four fiber creep tests simultaneously at temperatures up to 1300 C. Computer software was written to acquire and reduce all creep data.

  19. Creep Mechanisms of a Ni-Co-Based-Wrought Superalloy with Low Stacking Fault Energy

    NASA Astrophysics Data System (ADS)

    Tian, Chenggang; Xu, Ling; Cui, Chuanyong; Sun, Xiaofeng

    2015-10-01

    In order to study the influences of stress and temperature on the creep deformation mechanisms of a newly developed Ni-Co-based superalloy with low stacking fault energy, creep experiments were carried out under a stress range of 345 to 840 MPa and a temperature range of 923 K to 1088 K (650 °C to 815 °C). The mechanisms operated under the various creep conditions were identified and the reasons for their transformation were well discussed. A deformation mechanism map under different creep conditions was summarized, which provides a qualitative representation of the operative creep mechanisms as a function of stress and temperature.

  20. Irradiation creep in structural materials at ITER operating conditions

    SciTech Connect

    Grossbeck, M.L.

    1994-09-01

    Irradiation creep is plastic deformation of a material under the influence of irradiation and stress. Below the regime of thermal creep, there remains a deformation mechanism under irradiation that is weakly temperature dependent and clearly different from thermal creep. This is irradiation creep. Both stress and irradiation are required for irradiation creep. Irradiation creep studies for applications in the past focused mostly on liquid metal fast breeder reactors where temperatures are usually above 400{degrees}C. Fusion reactors, especially nearterm devices such as the ITER will have components operating at temperatures as low as 100{degrees}C exposed to high neutron fluxes. Theories of irradiation creep based on steady-state point defect concentrations do not predict significant irradiation creep deformation at these temperatures; however, data from research reactors show that irradiation creep strains at 60{degrees}C are as high or higher than at temperatures above 300{degrees}C for austenitic stainless steels. Irradiation creep of nickel has also been observed at cryogenic temperatures.

  1. High temperature deformation behavior of Inconel 718 at temperatures reaching into the mushy zone

    NASA Astrophysics Data System (ADS)

    Lewandowski, Michael Stanley

    2000-10-01

    The mechanical response of Inconel 718 with various microstructures (cast directionally-solidified, cast random dendritic, and equiaxed non-dendritic) in the solid and semi-solid state has been characterized. The activation energy for plastic flow in the solid phase was in good agreement with the activation energies for self diffusion and creep in pure nickel and pure iron. When the dendrites were aligned along the compression axis, the directionally solidified materials exhibited a similar activation energy for plastic flow, even at temperatures within the mushy zone. However, in samples containing either the random dendritic or equiaxed non-dendritic microstructures in the semi-solid state, the deformation exhibited a greater dependence on temperature. A simple analysis indicates that this greater temperature dependence is simply a consequence of the transition from plastic flow in the solid to viscous flow in the liquid as the fraction liquid increases (i.e., lubricated flow of the grains due to intergranular liquid in the mushy zone). The deformation behavior is compared against a number of investigations from the literature and a general constitutive equation relating peak now stress versus temperature compensated strain rate is presented. The temperature compensated strain rate is often termed the Zener-Holloman parameter, Z=ėexp (QRT) , where ė is the strain rate, T is the temperature, R is the gas constant, and Q is the activation energy for plastic flow. The results obtained in this investigation for solid state deformation were in good agreement with published literature values and extended the experimental range to higher temperatures and lower strain rates.

  2. Elevated-temperature tensile and creep properties of several ferritic stainless steels

    NASA Technical Reports Server (NTRS)

    Whittenberger, J. D.

    1977-01-01

    The elevated-temperature mechanical properties of several ferritic stainless steels were determined. The alloys evaluated included Armco 18SR, GE 1541, and NASA-18T-A. Tensile and creep strength properties at 1073 and 1273 K and residual room temperature tensile properties after creep testing were measured. In addition, 1273 K tensile and creep tests and residual property testing were conducted with Armco 18SR and GE 1541 which were exposed for 200 hours to a severe oxidizing environment in automotive thermal reactors. Aside from the residual tensile properties for Armco 18SR, prior exposure did not affect the mechanical properties of either alloy. The 1273 K creep strength parallel to the sheet-rolling direction was similar for all three alloys. At 1073 K, NASA-18T-A had better creep strength than either Armco 18SR or GE 1541. NASA-18T-A possesses better residual properties after creep testing than either Armco 18SR or Ge 1541.

  3. Preliminary study of creep thresholds and thermomechanical response in Haynes 188 at temperatures in the range 649 to 871 C

    NASA Technical Reports Server (NTRS)

    Ellis, J. R.; Bartolotta, P. A.; Mladsi, S. W.

    1987-01-01

    The following conclusions were drawn from this study of creep thresholds and thermomechanical response: (1) creep threshold can be determined using the latest electrohydraulic test equipment, providing that test durations are short and relatively large accumulations of creep strain are used in defining the threshold; (2) significant creep strains were measured under monotonic loading as stress levels as low as 4 ksi at temperatures predicted for solar receiver service; and (3) the material exhibited creep ratchetting during simulated service cycles, a result not predicted by analysis using current constitutive models for Haynes 188.

  4. The Creep of Single Crystals of Aluminum

    NASA Technical Reports Server (NTRS)

    Johnson, R D; Shober, F R; Schwope, A D

    1953-01-01

    The creep of single crystals of high-purity aluminum was investigated in the range of temperatures from room temperature to 400 F and at resolved-shear-stress levels of 200, 300, and 400 psi. The tests were designed in an attempt to produce data regarding the relation between the rate of strain and the mechanism of deformation. The creep data are analyzed in terms of shear strain rate and the results are discussed with regard to existing creep theories. Stress-strain curves were determined for the crystals in tinsel and constant-load-rate tests in the same temperature range to supplement the study of plastic deformation by creep with information regarding the part played by crystal orientation, differences in strain markings, and other variables in plastic deformation.

  5. Temperature effects on the strainrange partitioning approach for creep-fatigue analysis.

    NASA Technical Reports Server (NTRS)

    Halford, G. R.; Hirschberg, M. H.; Manson, S. S.

    1972-01-01

    Examination is made of the influence of temperature on the strain-range partitioning approach to creep-fatigue. Results for 2.5Cr-1Mo steel and Type 316 stainless steel show the four partitioned strain range-life relationships to be temperature insensitive to within a factor of two on cyclic life. Monotonic creep and tensile ductilities were also found to be temperature insensitive to within a factor of two. The approach provides bounds on cyclic life that can be readily established for any type of inelastic strain cycle.

  6. The influence of cavitation damage upon high temperature creep under stationary and non-stationary loading conditions. Part III: Creep at steady increasing load and true stress

    NASA Astrophysics Data System (ADS)

    Boček, M.; Hoffmann, M.

    1984-11-01

    In this paper for ideally plastic materials the influence of high temperature cavitation damage upon creep at steady increasing loads is investigated. The damage function A(t) enters a constitutive equation for plastíc flow through an effective stress σ e. For given loading conditions the latter is derived from the solution of Hart's tensile test equation. In the present paper the case of time linear increase in load ( F = constant) and in true stress ( /.s = constant) is investigated. The creep equations for cavitating as well as for non-cavitating materials are derived and the volume change during creep at /.F = constant are calculated.

  7. Investigation of the Compressive Strength and Creep Lifetime of 2024-T3 Aluminum-Alloy Plates at Elevated Temperatures

    NASA Technical Reports Server (NTRS)

    Mathauser, Eldon E; Deveikis, William D

    1957-01-01

    The results of elevated-temperature compressive strength and creep tests of 2024-t3 (formerly 24s-t3) aluminum alloy plates supported in v-grooves are presented. The strength-test results indicate that a relation previously developed for predicting plate compressive strength for plates of all materials at room temperature is also satisfactory for determining elevated-temperature strength. Creep-lifetime results are presented for plates in the form of master creep-lifetime curves by using a time-temperature parameter that is convenient for summarizing tensile creep-rupture data. A comparison is made between tensile and compressive creep lifetime for the plates and a method that made use of isochronous stress-strain curves for predicting plate-creep failure stresses is investigated.

  8. Damage Susceptibility of Grain Boundaries in HT9 Steel Subjected to High-Temperature Creep

    NASA Astrophysics Data System (ADS)

    Leng, Zhe; Field, David P.

    2012-10-01

    HT9 steel is an attractive ferritic/martensitic steel that is used in components of nuclear and fossil power plants because of its high strength and good swelling resistance. Specific phenomena (such as segregation, voiding, cracking, etc.) are prevalent along grain boundaries since these interfaces act as efficient sources for vacancies. The accumulation of vacancies in grain boundaries may result in intergranular fracture. In this study, HT9 steel was subjected to creep tests at elevated temperature (about 0.5 T m) and two different creep conditions (where creep lifetimes were about 100 and about 1000 hours, respectively). The grain boundaries in HT9 steel after creep tests were studied by the use of scanning electron microscopy in order to establish the relationship between the grain boundary structure and creep damage. Images and data obtained using electron backscatter diffraction reveal a high susceptibility of high-angle boundaries to creep cavitation, as expected. In addition, the Σ3 boundaries are also susceptible to damage under these conditions at a similar or even higher rate as compared with random high-angle boundaries.

  9. Fiber creep rate and high-temperature properties of SiC/SiC composites

    SciTech Connect

    Lewinsohn, C.A.; Jones, R.H.; Youngblood, G.E.; Henager, C.H. Jr.

    1998-03-01

    Results of studies aimed at relating the fiber creep rate to the subcritical crack growth rate and fracture properties of SiC/SiC composites have demonstrated that the crack growth rate in a bulk composite is controlled by the fiber creep rate. This result was demonstrated for Nicalon-CG and Hi-Nicalon fiber reinforced material where a 50--75 c shift in the creep strength of the fiber resulted in a similar shift in the crack growth rate of the composite. Irradiation enhanced creep of SiC fibers and matrix must also be considered in the performance assessment of SiC/SiC composites. The shape of the displacement versus time curve for composites containing Hi-Nicalon fibers were similar to those of the previously tested materials, containing Ceramic-grade fibers, that exhibited subcritical crack growth controlled by time-dependent relaxation of the fiber-bridging stresses due to fiber creep. The crack velocity in the CG-C composites at 1100 C in argon was very close to that of the Hi-C materials at 1150--1175 C, this roughly corresponds to the temperature differential shown by DiCarlo et al. to obtain the same relaxation in 1 hour bend stress relaxation (BSR) tests in the two fibers. This supports the hypothesis that subcritical crack growth in SiC/SiC composites is controlled by fiber creep.

  10. Effect of unloading time on interrupted creep in copper

    SciTech Connect

    Chandler, H.D. . School of Mechanical Engineering)

    1994-06-01

    The effect of unloading time on the interrupted creep behavior of polycrystalline copper specimens was investigated over the temperature range 298--773 K. Up to 553 K, cyclic creep acceleration could be explained in terms of deformation and hardening using a dislocation glide model with recovery during unloading being due to dislocation climb. At higher temperatures, recrystallization effects probably influence behavior.

  11. Irradiation creep of nano-powder sintered silicon carbide at low neutron fluences

    SciTech Connect

    Koyanagi, Takaaki; Shimoda, Kazuya; Kondo, Sosuke; Hinoki, Tatsuya; Ozawa, Kazumi; Katoh, Yutai

    2014-12-01

    The irradiation creep behavior of nano-powder sintered silicon carbide was investigated using the bend stress relaxation method under neutron irradiation up to 1.9 dpa. The creep deformation was observed at all temperatures ranging from 380 to 1180 °C mainly from the irradiation creep but with the increasing contributions from the thermal creep at higher temperatures. Microstructural observation and data analysis were performed.

  12. Low Cycle Fatigue and Creep-Fatigue Behavior of Alloy 617 at High Temperature

    SciTech Connect

    Cabet, Celine; Carroll, Laura; Wright, Richard

    2013-10-01

    Alloy 617 is the leading candidate material for an intermediate heat exchanger (IHX) application of the Very High Temperature Nuclear Reactor (VHTR), expected to have an outlet temperature as high as 950 degrees C. Acceptance of Alloy 617 in Section III of the ASME Code for nuclear construction requires a detailed understanding of the creep-fatigue behavior. Initial creep-fatigue work on Alloy 617 suggests a more dominant role of environment with increasing temperature and/or hold times evidenced through changes in creep-fatigue crack growth mechanism/s and failure life. Continuous cycle fatigue and creep-fatigue testing of Alloy 617 was conducted at 950 degrees C and 0.3% and 0.6% total strain in air to simulate damage modes expected in a VHTR application. Continuous cycle specimens exhibited transgranular cracking. Intergranular cracking was observed in the creep-fatigue specimens, although evidence of grain boundary cavitation was not observed. Despite the absence of grain boundary cavitation to accelerate crack propagation, the addition of a hold time at peak tensile strain was detrimental to cycle life. This suggests that creepfatigue interaction may occur by a different mechanism or that the environment may be partially responsible for accelerating failure.

  13. High temperature deformation behavior of a fine-grained tetragonal zirconia

    SciTech Connect

    Morita, K.; Hiraga, K.

    1999-12-31

    The stress exponent, n, defined in the following creep equation has often been regarded as a primary parameter to characterize superplastic deformation in fine-grained tetragonal zirconia containing 2.5 {approximately} 4 mol% yttria (Y-TZP): {var_epsilon} = A{sigma}{sup n}/d{sup p} where {var_epsilon} is the strain rate, {sigma} is the stress, d is the grain size, n is the stress exponent, p is the grain size exponent and A is a material constant. Recent studies have noted that the stress exponents of high-purity Y-TZP can be divided into two categories: n {approximately} 3 at low stresses and n {approximately} 2 at high stresses, where the stress dividing the deformation regions depends on both temperature and grain size. To argue the origins of such regions and relating mechanisms, however, some additional examination seems to be necessary for confirming that the regions characterized with n {approximately} 2 and {approximately} 3 are the genuine ones. This is because experimental limitations have tended to prevent the examination of deformation behavior by Eq. (1) in a strict sense. For example, the n-values have been derived from the overall strain rates that may indispensably include the effects of deformation around the grips of tensile specimens or those of constrained deformation near both sides of compression specimens. Furthermore, the data were obtained under an assumption that the effects of grain growth on the strain rate is negligible in Y-TZP. There seems to be rather little assurance, however, that these situations did not affect the evaluation of the stress exponent. From this point of view, the present study was conducted (1) to examine the effects of grain growth and some other experimental factors on creep behavior and (2) to evaluate the stress exponent from creep strain-rate curves corrected for both instantaneous stress and strain in a high purity Y-TZP.

  14. Temperature dependence of optically induced cell deformations

    NASA Astrophysics Data System (ADS)

    Fritsch, Anatol; Kiessling, Tobias R.; Stange, Roland; Kaes, Josef A.

    2012-02-01

    The mechanical properties of any material change with temperature, hence this must be true for cellular material. In biology many functions are known to undergo modulations with temperature, like myosin motor activity, mechanical properties of actin filament solutions, CO2 uptake of cultured cells or sex determination of several species. As mechanical properties of living cells are considered to play an important role in many cell functions it is surprising that only little is known on how the rheology of single cells is affected by temperature. We report the systematic temperature dependence of single cell deformations in Optical Stretcher (OS) measurements. The temperature is changed on a scale of about 20 minutes up to hours and compared to defined temperature shocks in the range of milliseconds. Thereby, a strong temperature dependence of the mechanics of single suspended cells is revealed. We conclude that the observable differences arise rather from viscosity changes of the cytosol than from structural changes of the cytoskeleton. These findings have implications for the interpretation of many rheological measurements, especially for laser based approaches in biological studies.

  15. Optimization of High Temperature Hoop Creep Response in ODS-Fe3Al Tubes

    SciTech Connect

    Kad, B.K.; Heatherington, J.H.; McKamey, C.; Wright, I.; Sikka, V.; Judkins, R.

    2003-04-22

    Oxide dispersion strengthened (ODS) Fe3Al alloys are currently being developed for heat-exchanger tubes for eventual use at operating temperatures of up to 1100 C in the power generation industry. The development challenges include (a) efforts to produce thin walled ODS-Fe3Al tubes, employing powder extrusion methodologies, with (b) adequate increased strength for service at operating temperatures to (c) mitigate creep failures by enhancing the as-processed grain size. A detailed and comprehensive research and development methodology is prescribed to produce ODS-Fe3Al thin walled tubes. Current single step extrusion consolidation methodologies typically yield 8ft. lengths of 1-3/8 inch diameter, 1/8 inch wall thickness ODS-Fe3Al tubes. The process parameters for such consolidation methodologies have been prescribed and evaluated as being routinely reproducible. Recrystallization treatments at 1200 C produce elongated grains (with their long axis parallel to the extrusion axis), typically 200-2000 {micro}m in diameter, and several millimeters long. The dispersion distribution is unaltered on a micro scale by recrystallization, but the high aspect ratio grain shape typically obtained limits grain spacing and consequently the hoop creep response. Improving hoop creep in ODS-alloys requires an understanding and manipulating the factors that control grain alignment and recrystallization behavior. Current efforts are focused on examining the processing dependent longitudinal vs. transverse creep anisotropy, and exploring post-extrusion methods to improve hoop creep response in ODS-Fe3Al alloy tubes. In this report we examine the mechanisms of hoop creep failure and describe our efforts to improve creep performance via variations in thermal-mechanical treatments.

  16. Low-temperature irradiation creep of fusion reactor structural materials*1

    NASA Astrophysics Data System (ADS)

    Grossbeck, M. L.; Mansur, L. K.

    1991-03-01

    Irradiation creep has been investigated in the Oak Ridge Research Reactor in an assembly spectrally tailored to achieve a He : dpa ratio of 12-14:1 appm/dpa in austenitic stainless steels. Temperatures of 60-400°C were investigated to address the requirements of near term fusion devices. It was found that austenitic alloys, especially PCA, have higher creep rates at 60°C than at 330 and 400°C. Since this phenomenon could not be explained by existing theoretical models, a new mechanism was proposed and a corresponding theoretical model was developed. Since vacancy migration times can be a few orders of magnitude longer than the irradiation times in this temperature regime, the immobile vacancies do not cancel climb produced by mobile interstitials absorbed at dislocations. The result is a high climb rate independent of stress-induced preferred absorption (SIPA) mechanisms. Preliminary calculations indicate that this mechanism coupled with preferred-absorption-driven glide at higher temperatures predicts a high creep rate at low temperatures and a weak temperature dependence of irradiation creep over the entire temperature range investigated.

  17. Experimental Deformation of Olivine Single Crystals at Mantle Pressures and Temperatures

    SciTech Connect

    Raterron, P.; Amiguet, E; Chen, J; Li, L; Cordier, P

    2008-01-01

    Deformation experiments were carried out in a deformation-DIA high-pressure apparatus (D-DIA) on oriented San Carlos olivine single crystals, at pressure (P) ranging from 3.5 to 8.5 GPa, temperature (T) from 1373 to 1673 K, and in poor water condition. Oxygen fugacity (fO2) was maintained within the olivine stability field and contact with enstatite powder ensured an orthopyroxene activity aopx = 1. Two compression directions were tested, promoting either [1 0 0] slip alone or [0 0 1] slip alone in (0 1 0) crystallographic plane, here called, respectively, a-slip and c-slip. Constant applied stress (s) and specimen strain rates ({bar {var_epsilon}}) were monitored in situ using time-resolved X-ray synchrotron diffraction and radiography, respectively. Transmission electron microscopy (TEM) investigation of run products revealed that dislocation creep was responsible for sample deformation. Comparison of the obtained high-P deformation data with the data obtained at room-P by Bai et al. [Bai, Q., Mackwell, S.L., Kohlstedt D.L., 1991, High-temperature creep of olivine single crystals. 1. Mechanical results for buffered samples, Journal of Geophysical Research, 96, 2441-2463] - on identical materials deformed at comparable T-sefO2-aopx conditions - allowed quantifying the P effect on a-slip and c-slip rheological laws. A slip transition with increasing pressure, from dominant a-slip to dominant c-slip, is documented. a-slip appears sensitive to pressure, which translates into the high activation volume V*{sub a} = 12 {+-} 4 cm{sup 3}/mol in the corresponding rheological law, while pressure has little effect on c-slip with V*{sub c} = 3 {+-} 4 cm{sup 3}/mol. These results may explain the discrepancy between olivine low-P and high-P deformation data which has been debated in the literature for more than a decade.

  18. Nanogranular origin of concrete creep.

    PubMed

    Vandamme, Matthieu; Ulm, Franz-Josef

    2009-06-30

    Concrete, the solid that forms at room temperature from mixing Portland cement with water, sand, and aggregates, suffers from time-dependent deformation under load. This creep occurs at a rate that deteriorates the durability and truncates the lifespan of concrete structures. However, despite decades of research, the origin of concrete creep remains unknown. Here, we measure the in situ creep behavior of calcium-silicate-hydrates (C-S-H), the nano-meter sized particles that form the fundamental building block of Portland cement concrete. We show that C-S-H exhibits a logarithmic creep that depends only on the packing of 3 structurally distinct but compositionally similar C-S-H forms: low density, high density, ultra-high density. We demonstrate that the creep rate ( approximately 1/t) is likely due to the rearrangement of nanoscale particles around limit packing densities following the free-volume dynamics theory of granular physics. These findings could lead to a new basis for nanoengineering concrete materials and structures with minimal creep rates monitored by packing density distributions of nanoscale particles, and predicted by nanoscale creep measurements in some minute time, which are as exact as macroscopic creep tests carried out over years. PMID:19541652

  19. Nanogranular origin of concrete creep

    PubMed Central

    Vandamme, Matthieu; Ulm, Franz-Josef

    2009-01-01

    Concrete, the solid that forms at room temperature from mixing Portland cement with water, sand, and aggregates, suffers from time-dependent deformation under load. This creep occurs at a rate that deteriorates the durability and truncates the lifespan of concrete structures. However, despite decades of research, the origin of concrete creep remains unknown. Here, we measure the in situ creep behavior of calcium–silicate–hydrates (C–S–H), the nano-meter sized particles that form the fundamental building block of Portland cement concrete. We show that C–S–H exhibits a logarithmic creep that depends only on the packing of 3 structurally distinct but compositionally similar C–S–H forms: low density, high density, ultra-high density. We demonstrate that the creep rate (≈1/t) is likely due to the rearrangement of nanoscale particles around limit packing densities following the free-volume dynamics theory of granular physics. These findings could lead to a new basis for nanoengineering concrete materials and structures with minimal creep rates monitored by packing density distributions of nanoscale particles, and predicted by nanoscale creep measurements in some minute time, which are as exact as macroscopic creep tests carried out over years. PMID:19541652

  20. Copper modified austenitic stainless steel alloys with improved high temperature creep resistance

    DOEpatents

    Swindeman, R.W.; Maziasz, P.J.

    1987-04-28

    An improved austenitic stainless steel that incorporates copper into a base Fe-Ni-Cr alloy having minor alloying substituents of Mo, Mn, Si, T, Nb, V, C, N, P, B which exhibits significant improvement in high temperature creep resistance over previous steels. 3 figs.

  1. Creep testing of foil-gage metals at elevated temperature using an automated data acquisition system

    NASA Technical Reports Server (NTRS)

    Blackburn, L. B.

    1983-01-01

    A method is being developed to obtain creep data on foil gage metals at elevated temperatures using an automated data acquisition system in conjunction with a mechanically counter balanced extensometer. The automated system components include the Hewlett-Packard (HP) 9845A desktop computer, the HP 3455A digital voltmeter and the HP 3495A scanner. Software for test monitoring and data collection was developed; data manipulation, including curve plotting was done with a HP regression analysis software package. Initial creep tests were conducted on .003 in. thick foil specimens of Ti-6A1-4V at temperatures of 800 F and 1000 F and at stress levels of 25 ksi and 45 ksi. For comparison, duplicate tests were run on .049 in. thick specimens sheet of the same alloy. During testing, the furnace and specimen temperature, bridge voltage, strain and load output were automatically monitored and recorded at predetermined intervals. Using the HP regression analysis program, recorded strain output was plotted as a function of time. These resultant creep curves indicate that, under similar conditions of temperature and stress, foil gage specimens exhibit a higher creep rate than sheet specimens.

  2. Effect of temperature on tensile and creep characteristics of PRD49 fiber/epoxy composites

    NASA Technical Reports Server (NTRS)

    Hanson, M. P.

    1972-01-01

    Tensile and creep data of PRD49-1 and 3 fiber/epoxy-resin composites are presented. Tensile data were obtained from 20 to 477 K (-423 to 400 F). Tensile strengths and moduli were determined at selected temperatures. Creep data are presented for fiber composites at 297, 422 and 450 K (75, 300, and 350 F) for as long as 1000 hours at stress levels of approximately 50 and 80 percent of the ultimate tensile strength at 297 K (75 F). Details of tensile specimens and test procedures used in the investigation are presented.

  3. Effect of temperature on the formation of creep substructure in sodium chloride single crystals

    NASA Technical Reports Server (NTRS)

    Raj, Sai V.; Pharr, George M.

    1992-01-01

    The effect of temperature on the substructure morphology and the cell and subgrain size was investigated experimentally in NaCl single crystals under creep in the temperature range 573-873 K. It is found that the effect of temperature on the cell and subgrain sizes is weak in comparison with the effect of stress. However, there was a qualitative change in the substructure morphology with temperature, with the cells and subgrains better defined at higher temperatures. The volume fraction of the cell boundaries decreased with increasing temperature, thereby indicating a refinement of the microstructure at higher temperatures.

  4. Creep Testing of High-Temperature Cu-8 Cr-4 Nb Alloy Completed

    NASA Technical Reports Server (NTRS)

    1995-01-01

    A Cu-8 at.% Cr-4 at.% Nb (Cu-8 Cr-4 Nb) alloy is under development for high-temperature, high heatflux applications, such as actively cooled, hypersonic vehicle heat exchangers and rocket engine combustion chambers. Cu-8 Cr-4 Nb offers a superior combination of strength and conductivity. It has also shown exceptional low-cycle fatigue properties. Following preliminary testing to determine the best processing route, a more detailed testing program was initiated to determine the creep lives and creep rates of Cu-8 Cr-4 Nb alloy specimens produced by extrusion. Testing was conducted at the NASA Lewis Research Center with constant-load vacuum creep units. Considering expected operating temperatures and mission lives, we developed a test matrix to accurately determine the creep properties of Cu-8 Cr-4 Nb between 500 and 800 C. Six bars of Cu-8 Cr-4 Nb were extruded. From these bars, 54 creep samples were machined and tested. The figure on the left shows the steady-state, or second-stage, creep rates for the samples. Comparison data for NARloy-Z (Cu-3 wt % Ag-0.5 wt % Zr), the alloy currently used in combustion chamber liners, were not unavailable. Therefore the steady-state creep rates for Cu at similar temperatures are presented. As expected, in comparison to pure Cu, the creep rates for Cu-8 Cr-4 Nb are much lower. The lives of the samples are presented in the figure on the right. As shown, Cu-8 Cr-4 Nb at 800 C is comparable to NARloy-Z at 648 C. At equivalent temperatures, Cu-8 Cr-4 Nb enjoys a 20 to 50 percent advantage in stress for a given life and 1 to 3 orders of magnitude greater life at a given stress. The improved properties allow for design tradeoffs and improvements in new and existing heat exchangers such as the next generation of combustion chamber liners. Average creep rates for Cu-8 Cr-4 Nb and pure Cu are shown. Average creep lives for Cu-8 Cr- 4 Nb and NARloy-Z are also shown. Currently, two companies are interested in the commercial usage of the Cu

  5. Deformation behavior of a Ni-30Al-20Fe-0.05Zr intermetallic alloy in the temperature range 300 to 1300 K

    NASA Technical Reports Server (NTRS)

    Raj, S. V.; Locci, I. E.; Noebe, R. D.

    1992-01-01

    The deformation properties of an extruded Ni-30Al-20Fe-0.05Zr (at. pct) alloy in the temperature range 300-1300 K were investigated under initial tensile strain rates that varied between 10 exp -6 and 10 exp -3/sec and in constant load compression creep between 1073 and 1300 K. Three deformation regimes were observed: region I, occurring between 400 and 673 K, which consisted of an athermal regime of less than 0.3 percent tensile ductility; region II, between 673 and 1073, where exponential creep was dominant; and region III, between 1073 and 1300 K, where a significant improvement in tensile ductility was observed.

  6. Temperature effects on the strainrange partitioning approach for creep-fatigue analysis

    NASA Technical Reports Server (NTRS)

    Halford, G. R.; Hirschberg, M. H.; Manson, S. S.

    1972-01-01

    Examination is made of the influence of temperature on the strainrange partitioning approach to creep-fatigue. Results for Cr-Mo steel and Type 316 stainless steel show the four partitioned strainrange-life relationships to be temperature insensitive to within a factor of two on cyclic life. Monotonic creep and tensile ductilities were also found to be temperature insensitive to within a factor of two. The approach provides bounds on cyclic life that can be readily established for any type of inelastic strain cycle. Continuous strain cycling results obtained over a broad range of high temperatures and frequencies are in excellent agreement with bounds provided by the approach. The observed transition from one bound to the other is also in good agreement with the approach.

  7. The effects of physical aging at elevated temperatures on the viscoelastic creep on IM7/K3B

    NASA Technical Reports Server (NTRS)

    Gates, Thomas S.; Feldman, Mark

    1994-01-01

    Physical aging at elevated temperature of the advanced composite IM7/K3B was investigated through the use of creep compliance tests. Testing consisted of short term isothermal, creep/recovery with the creep segments performed at constant load. The matrix dominated transverse tensile and in-plane shear behavior were measured at temperatures ranging from 200 to 230 C. Through the use of time based shifting procedures, the aging shift factors, shift rates and momentary master curve parameters were found at each temperature. These material parameters were used as input to a predictive methodology, which was based upon effective time theory and linear viscoelasticity combined with classical lamination theory. Long term creep compliance test data was compared to predictions to verify the method. The model was then used to predict the long term creep behavior for several general laminates.

  8. Steady-state creep of bent reinforced metal-composite plates with consideration of their reduced resistance to transverse shear. 1. Deformation model

    NASA Astrophysics Data System (ADS)

    Yankovskii, A. P.

    2014-05-01

    The problem of deformation of reinforced metal-composite plates is formulated in rectangular Cartesian coordinates using the second version of Timoshenko theory and taking into account the reduced transverse shear resistance of the plates under steady-state creep conditions. A similar model problem of axisymmetric bending of reinforced plates is considered in polar coordinates.

  9. In-situ Creep Testing Capability Development for Advanced Test Reactor

    SciTech Connect

    B. G. Kim; J. L. Rempe; D. L. Knudson; K. G. Condie; B. H. Sencer

    2010-08-01

    Creep is the slow, time-dependent strain that occurs in a material under a constant strees (or load) at high temperature. High temperature is a relative term, dependent on the materials being evaluated. A typical creep curve is shown in Figure 1-1. In a creep test, a constant load is applied to a tensile specimen maintained at a constant temperature. Strain is then measured over a period of time. The slope of the curve, identified in the figure below, is the strain rate of the test during Stage II or the creep rate of the material. Primary creep, Stage I, is a period of decreasing creep rate due to work hardening of the material. Primary creep is a period of primarily transient creep. During this period, deformation takes place and the resistance to creep increases until Stage II, Secondary creep. Stage II creep is a period with a roughly constant creep rate. Stage II is referred to as steady-state creep because a balance is achieved between the work hardening and annealing (thermal softening) processes. Tertiary creep, Stage III, occurs when there is a reduction in cross sectional area due to necking or effective reduction in area due to internal void formation; that is, the creep rate increases due to necking of the specimen and the associated increase in local stress.

  10. Plastic Deformation of Micromachined Silicon Diaphragms with a Sealed Cavity at High Temperatures

    PubMed Central

    Ren, Juan; Ward, Michael; Kinnell, Peter; Craddock, Russell; Wei, Xueyong

    2016-01-01

    Single crystal silicon (SCS) diaphragms are widely used as pressure sensitive elements in micromachined pressure sensors. However, for harsh environments applications, pure silicon diaphragms are hardly used because of the deterioration of SCS in both electrical and mechanical properties. To survive at the elevated temperature, the silicon structures must work in combination with other advanced materials, such as silicon carbide (SiC) or silicon on insulator (SOI), for improved performance and reduced cost. Hence, in order to extend the operating temperatures of existing SCS microstructures, this work investigates the mechanical behavior of pressurized SCS diaphragms at high temperatures. A model was developed to predict the plastic deformation of SCS diaphragms and was verified by the experiments. The evolution of the deformation was obtained by studying the surface profiles at different anneal stages. The slow continuous deformation was considered as creep for the diaphragms with a radius of 2.5 mm at 600 °C. The occurrence of plastic deformation was successfully predicted by the model and was observed at the operating temperature of 800 °C and 900 °C, respectively. PMID:26861332

  11. Plastic Deformation of Micromachined Silicon Diaphragms with a Sealed Cavity at High Temperatures.

    PubMed

    Ren, Juan; Ward, Michael; Kinnell, Peter; Craddock, Russell; Wei, Xueyong

    2016-01-01

    Single crystal silicon (SCS) diaphragms are widely used as pressure sensitive elements in micromachined pressure sensors. However, for harsh environments applications, pure silicon diaphragms are hardly used because of the deterioration of SCS in both electrical and mechanical properties. To survive at the elevated temperature, the silicon structures must work in combination with other advanced materials, such as silicon carbide (SiC) or silicon on insulator (SOI), for improved performance and reduced cost. Hence, in order to extend the operating temperatures of existing SCS microstructures, this work investigates the mechanical behavior of pressurized SCS diaphragms at high temperatures. A model was developed to predict the plastic deformation of SCS diaphragms and was verified by the experiments. The evolution of the deformation was obtained by studying the surface profiles at different anneal stages. The slow continuous deformation was considered as creep for the diaphragms with a radius of 2.5 mm at 600 °C. The occurrence of plastic deformation was successfully predicted by the model and was observed at the operating temperature of 800 °C and 900 °C, respectively. PMID:26861332

  12. Evaluation of Permanent Deformation of CRM-Reinforced SMA and Its Correlation with Dynamic Stiffness and Dynamic Creep

    PubMed Central

    Mashaan, Nuha Salim; Karim, Mohamed Rehan

    2013-01-01

    Today, rapid economic and industrial growth generates increasing amounts of waste materials such as waste tyre rubber. Attempts to inspire a green technology which is more environmentally friendly that can produce economic value are a major consideration in the utilization of waste materials. The aim of this study is to evaluate the effect of waste tyre rubber (crumb rubber modifier (CRM)), in stone mastic asphalt (SMA 20) performance. The virgin bitumen (80/100) penetration grade was used, modified with crumb rubber at four different modification levels, namely, 6%, 12%, 16%, and 20% by weight of the bitumen. The testing undertaken on the asphalt mix comprises the indirect tensile (dynamic stiffness), dynamic creep, and wheel tracking tests. By the experimentation, the appropriate amount of CRM was found to be 16% by weight of bitumen. The results show that the addition of CRM into the mixture has an obvious significant effect on the performance properties of SMA which could improve the mixture's resistance against permanent deformation. Further, higher correlation coefficient was obtained between the rut depth and permanent strain as compared to resilient modulus; thus dynamic creep test might be a more reliable test in evaluating the rut resistance of asphalt mixture. PMID:24302883

  13. Evaluation of permanent deformation of CRM-reinforced SMA and its correlation with dynamic stiffness and dynamic creep.

    PubMed

    Mashaan, Nuha Salim; Karim, Mohamed Rehan

    2013-01-01

    Today, rapid economic and industrial growth generates increasing amounts of waste materials such as waste tyre rubber. Attempts to inspire a green technology which is more environmentally friendly that can produce economic value are a major consideration in the utilization of waste materials. The aim of this study is to evaluate the effect of waste tyre rubber (crumb rubber modifier (CRM)), in stone mastic asphalt (SMA 20) performance. The virgin bitumen (80/100) penetration grade was used, modified with crumb rubber at four different modification levels, namely, 6%, 12%, 16%, and 20% by weight of the bitumen. The testing undertaken on the asphalt mix comprises the indirect tensile (dynamic stiffness), dynamic creep, and wheel tracking tests. By the experimentation, the appropriate amount of CRM was found to be 16% by weight of bitumen. The results show that the addition of CRM into the mixture has an obvious significant effect on the performance properties of SMA which could improve the mixture's resistance against permanent deformation. Further, higher correlation coefficient was obtained between the rut depth and permanent strain as compared to resilient modulus; thus dynamic creep test might be a more reliable test in evaluating the rut resistance of asphalt mixture. PMID:24302883

  14. Creep-fatigue of High Temperature Materials for VHTR: Effect of Cyclic Loading and Environment

    SciTech Connect

    Celine Cabet; L. Carroll; R. Wright; R. Madland

    2011-05-01

    Alloy 617 is the one of the leading candidate materials for Intermediate Heat eXchangers (IHX) of a Very High Temperature Reactor (VHTR). System start-ups and shut-downs as well as power transients will produce low cycle fatigue (LCF) loadings of components. Furthermore, the anticipated IHX operating temperature, up to 950°C, is in the range of creep so that creep-fatigue interaction, which can significantly increase the fatigue crack growth, may be one of the primary IHX damage modes. To address the needs for Alloy 617 codification and licensing, a significant creep-fatigue testing program is underway at Idaho National Laboratory. Strain controlled LCF tests including hold times up to 1800s at maximum tensile strain were conducted at total strain range of 0.3% and 0.6% in air at 950°C. Creep-fatigue testing was also performed in a simulated VHTR impure helium coolant for selected experimental conditions. The creep-fatigue tests resulted in failure times up to 1000 hrs. Fatigue resistance was significantly decreased when a hold time was added at peak stress and when the total strain was increased. The fracture mode also changed from transgranular to intergranular with introduction of a tensile hold. Changes in the microstructure were methodically characterized. A combined effect of temperature, cyclic and static loading and environment was evidenced in the targeted operating conditions of the IHX. This paper This paper reviews the data previously published by Carroll and co-workers in references 10 and 11 focusing on the role of inelastic strain accumulation and of oxidation in the initiation and propagation of surface fatigue cracks.

  15. High temperature creep behaviour of Al-rich Ti-Al alloys

    NASA Astrophysics Data System (ADS)

    Sturm, D.; Heilmaier, M.; Saage, H.; Aguilar, J.; Schmitz, G. J.; Drevermann, A.; Palm, M.; Stein, F.; Engberding, N.; Kelm, K.; Irsen, S.

    2010-07-01

    Compared to Ti-rich γ-TiAl-based alloys Al-rich Ti-Al alloys offer an additional reduction of in density and a better oxidation resistance which are both due to the increased Al content. Polycrystalline material was manufactured by centrifugal casting. Microstructural characterization was carried out employing light-optical, scanning and transmission electron microscopy and XRD analyses. The high temperature creep of two binary alloys, namely Al60Ti40 and Al62Ti38 was comparatively assessed with compression tests at constant true stress in a temperature range between 1173 and 1323 K in air. The alloys were tested in the cast condition (containing various amounts of the metastable phases Al5Ti3 and h-Al2Ti) and after annealing at 1223 K for 200 h which produced (thermodynamically stable) lamellar γ-TiAl + r-Al2Ti microstructures. In general, already the as-cast alloys exhibit a reasonable creep resistance at 1173 K. Compared with Al60Ti40, both, the as-cast and the annealed Al62Ti38 alloy exhibit better creep resistance up to 1323 K which can be rationalized by the reduced lamella spacing. The assessment of creep tests conducted at identical stress levels and varying temperatures yielded apparent activation energies for creep of Q = 430 kJ/mol for the annealed Al60Ti40 alloy and of Q = 383 kJ/mol for the annealed Al62Ti38 material. The latter coincides well with that of Al diffusion in γ-TiAl, whereas the former can be rationalized by the instability of the microstructure containing metastable phases.

  16. Low Temperature Creep of Hot-Extruded Near-Stoichiometric NiTi Shape Memory Alloy. Part 2; Effect of Thermal Cycling

    NASA Technical Reports Server (NTRS)

    Raj, S. V.; Noebe, R. D.

    2013-01-01

    This paper is the first report on the effect prior low temperature creep on the thermal cycling behavior of NiTi. The isothermal low temperature creep behavior of near-stoichiometric NiTi between 300 and 473 K was discussed in Part I. The effect of temperature cycling on its creep behavior is reported in the present paper (Part II). Temperature cycling tests were conducted between either 300 or 373 K and 473 K under a constant applied stress of either 250 or 350 MPa with hold times lasting at each temperature varying between 300 and 700 h. Each specimen was pre-crept either at 300 or at 473 K for several months under an identical applied stress as that used in the subsequent thermal cycling tests. Irrespective of the initial pre-crept microstructures, the specimens exhibited a considerable increase in strain with each thermal cycle so that the total strain continued to build-up to 15 to 20 percent after only 5 cycles. Creep strains were immeasurably small during the hold periods. It is demonstrated that the strains in the austenite and martensite are linearly correlated. Interestingly, the differential irrecoverable strain, in the material measured in either phase decreases with increasing number of cycles, similar to the well-known Manson-Coffin relation in low cycle fatigue. Both phases are shown to undergo strain hardening due to the development of residual stresses. Plots of true creep rate against absolute temperature showed distinct peaks and valleys during the cool-down and heat-up portions of the thermal cycles, respectively. Transformation temperatures determined from the creep data revealed that the austenitic start and finish temperatures were more sensitive to the pre-crept martensitic phase than to the pre-crept austenitic phase. The results are discussed in terms of a phenomenological model, where it is suggested that thermal cycling between the austenitic and martensitic phase temperatures or vice versa results in the deformation of the austenite and

  17. Deformation of granite at elevated temperature and pressure. Final report, 1 March 1984-28 February 1985

    SciTech Connect

    Carter, N.L.

    1985-03-15

    The purpose was to determine the evolution of substructure and mechanical behavior of westerly granite, deformed under both wet and dry conditions, from the initial stages of transient creep well into the steady-state. Following calibration of the 10 kb gas apparatus at elevated temperature and pressure, the main pressure vessel burst. As a consequence, other studies were pursued. These include: (1) analysis of olivine fabrics of ophiolites; (2) upper mantle deformation in collision zones; (3) flow properties of continental lithosphere; and (4) mechanical behavior of oceanic layer 2 basalts. (ACR)

  18. Creep-rupture in powder metallurgical nickel-base superalloys at intermediate temperatures

    NASA Astrophysics Data System (ADS)

    Law, C. C.; Blackburn, M. J.

    1980-03-01

    To gain insight into the factors which control the creep-rupture properties of powder metallurgical nickel-base superalloys at intermediate temperatures (650 to 775°C), a comparative study was conducted on the alloys AF115, modified MAR-M432 (B6) and modified IN100 (MERL76). Creep-rupture properties in these alloys were characterized in terms of the stress and temperature dependence of the secondary creep rate, ɛS, andrupture time, t R . Within the limited stress ranges used, the stress dependence of both ɛS and t R at 704°C can be represented by power laws ɛS and C n and t R = Mσ -p ; where C, M, n, and p are constants. The stress exponents n and p are approximately equal for both AF115 and B6 with values of 16 and 7, respectively. In the case of MERL76, n and p are different, with values of 15 and 5, respectively. The apparent activation energies, Q, are 700, 370 and 520 KJ mol-1 for AF115, B6 and MERL76, respectively. For these alloys, long creep-rupture lives are associated with large values of n and Q. The sig-nificant differences in n and Q values between AF115 and B6 were related to creep re-covery processes for which the lattice misfit between the gamma and the gamma prime was identified to be an important parameter. However, the unequal n and p values in MERL76 compared with those in AF115 and B6, were traced to differences in fracture mode. Failures in AF115 and B6 were initiated at carbide particles at grain boundaries. In contrast, fracture in MERL76 was initiated at grain boundary triple junctions. The rupture lives of AF115 and B6 can be modeled reasonably well by the growth of cavities during secondary creep and propagation of a surface-nucleated crack during the tertiary creep.

  19. Compressive Creep Performance and High Temperature Dimensional Stability of Conventional Silica Refractories

    SciTech Connect

    Karakus, M.; Kirkland, T.P.; Liu, K.C.; Moore, R.E.; Pint, B.A.; Wereszczak, A.A.

    1999-03-01

    Furnace designers and refractory engineers recognize that optimized furnace superstructure design and refractory selection are needed as glass production furnaces are continually striving toward greater output and efficiencies. Harsher operating conditions test refractories to the limit, while changing production technology (such as the conversion to oxy-fuel from traditional air-fuel firing) can alter the way the materials perform. Refractories for both oxy- and air-fuel fired furnace superstructures are subjected to high temperatures during service that may cause them to excessively creep or subside if the refractory material is not creep resistant, or if it is subjected to high stress, or both. Furnace designers can ensure that superstructure structural integrity is maintained if the creep behavior of the refractory material is well understood and well represented by appropriate engineering creep models. Several issues limit the abilities of furnace designers to (1) choose the optimum refractory for their applications, (2) optimize the engineering design, or (3) predict the service mechanical integrity of their furnace superstructures. Published engineering creep data are essentially non-existent for almost all commercially available refractories used for glass furnace superstructures. The limited data that do exist are supplied by the various refractory suppliers. Unfortunately, these suppliers generally have different ways of conducting their mechanical testing and they also interpret and report their data differently; this makes it hard for furnace designers to draw fair comparisons between competing grades of candidate refractories. Furthermore, the refractory supplier's data are often not available in a form that can be readily used for furnace design and for the prediction and design of long-term structural integrity of furnace superstructures. With the aim of providing such comparable data, the US DOE's Office of Industrial Technology and its Advanced

  20. PROCESSING, MICROSTRUCTURE AND CREEP BEHAVIOR OF Mo-Si-B-BASED INTERMETALLIC ALLOYS FOR VERY HIGH TEMPERATURE STRUCTURAL APPLICATIONS

    SciTech Connect

    Vijay K. Vasudevan

    2005-12-21

    This research project is concerned with developing a fundamental understanding of the effects of processing and microstructure on the creep behavior of refractory intermetallic alloys based on the Mo-Si-B system. During this year, the compressive creep behavior of a Mo-3Si-1B (in wt.%) alloy at 1100 and 1200 C were studied and related to the deformation mechanisms through electron microscopy observations of microstructural changes and deformation structures. The microstructure of this alloy was three-phase, being composed of {alpha}-Mo, Mo{sub 3}Si and T2-Mo{sub 5}SiB{sub 2} phases. Results of compressive creep tests at 1200 and 1100 C showed that the creep rates were quite high at stress levels between 250 and 500 MPa, Two minima in the creep strain rate versus strain data were noted, one at small strain values and the second at much larger strains. A stress exponent of 4.26 was obtained upon plotting the strain rate corresponding to the first minima versus stress, which suggests that dislocation climb and glide dominate the creep process in the early stages. On the other hand, the large strain, minimum creep rate versus stress data gave a stress exponent of {approx}1.18, which indicates diffusional mechanisms and recrystallization dominate the later stages of the creep process. At 1100 C, a stress exponent of 2.26 was obtained, which suggests that both diffusional and dislocation mechanisms contribute to the creep strain. Based on the minimum creep rate data at 1100 C and 1200 C, the activation energy for creep was determined to be 525 kJ/mole, which is somewhat higher than that reported for self diffusion in {alpha}-Mo. Microstructural observations of post-crept samples indicated the presence of many voids in the {alpha}-Mo grains and few cracks in the intermetallic particles and along their interfaces with the {alpha}-Mo matrix. In addition, TEM observations revealed the presence of recrystallized grains and sub-grain boundaries composed of dislocation arrays

  1. The solid-solution alloying effects of Ti on the high-temperature deformation behavior of NiAl single crystals

    SciTech Connect

    Kitabjian, P.H.; Nix, W.D.; Garg, A.; Noebe, R.

    1997-12-31

    The authors have investigated the high-temperature deformation behavior of the solid-solution strengthened alloy Ni-47.5Al-2.5Ti. Single crystals were deformed in compression in the hard <001> and soft <111> orientations, at temperatures between 900 C and 1,200 C. The results show that Ti has a very powerful solute strengthening effect in NiAl. The creep rates for the solid-solution alloy were observed to be three to four orders of magnitude lower than for the stoichiometric material. They discuss the efforts to understand this solid-solution strengthening effect. They have studied high-temperature deformation transients in an effort to determine whether solute drag effects contribute to the creep resistance of this solid solution. In addition, they have examined the solute size effect of Ti as it replaces Al on the Al sub-lattice. They discuss the probable mechanism of creep of this alloy in light of TEM observations of the dislocation structures in creep-deformed crystals.

  2. Temperature-dependent elastic anisotropy and mesoscale deformation in a nanostructured ferritic alloy

    SciTech Connect

    Stoica, G. M.; Stoica, A. D.; Miller, M. K.; Ma, D.

    2014-10-10

    Nanostructured ferritic alloys (NFA) are a new class of ultrafine-grained oxide dispersion-strengthened steels, promising for service in extreme environments of high temperature and high irradiation in the next-generation of nuclear reactors. This is owing to the remarkable stability of their complex microstructures containing a high density of Y-Ti-O nanoclusters within grains and along the grain boundaries. While nanoclusters have been recognized to be the primary contributor to the exceptional resistance to irradiation and high-temperature creep, very little is known about the mechanical roles of the polycrystalline grains that constitute the bulk ferritic matrix. Here we report the mesoscale characterization of anisotropic responses of the ultrafine NFA grains to tensile stresses at various temperatures using the state-of-the-art in situ neutron diffraction. We show the first experimental determination of temperature-dependent single-crystal elastic constants for the NFA, and reveal a strong temperature-dependent elastic anisotropy due to a sharp decrease in the shear stiffness constant [c'=(c_11-c_12)/2] when a critical temperature ( T_c ) is approached, indicative of elastic softening and instability of the ferritic matrix. We also show, from anisotropy-induced intergranular strain/stress accumulations, that a common dislocation slip mechanism operates at the onset of yielding for low temperatures, while there is a deformation crossover from low-temperature lattice hardening to high temperature lattice softening in response to extensive plastic deformation.

  3. Temperature-dependent elastic anisotropy and mesoscale deformation in a nanostructured ferritic alloy

    DOE PAGESBeta

    Stoica, G. M.; Stoica, A. D.; Miller, M. K.; Ma, D.

    2014-10-10

    Nanostructured ferritic alloys (NFA) are a new class of ultrafine-grained oxide dispersion-strengthened steels, promising for service in extreme environments of high temperature and high irradiation in the next-generation of nuclear reactors. This is owing to the remarkable stability of their complex microstructures containing a high density of Y-Ti-O nanoclusters within grains and along the grain boundaries. While nanoclusters have been recognized to be the primary contributor to the exceptional resistance to irradiation and high-temperature creep, very little is known about the mechanical roles of the polycrystalline grains that constitute the bulk ferritic matrix. Here we report the mesoscale characterization ofmore » anisotropic responses of the ultrafine NFA grains to tensile stresses at various temperatures using the state-of-the-art in situ neutron diffraction. We show the first experimental determination of temperature-dependent single-crystal elastic constants for the NFA, and reveal a strong temperature-dependent elastic anisotropy due to a sharp decrease in the shear stiffness constant [c'=(c_11-c_12)/2] when a critical temperature ( T_c ) is approached, indicative of elastic softening and instability of the ferritic matrix. We also show, from anisotropy-induced intergranular strain/stress accumulations, that a common dislocation slip mechanism operates at the onset of yielding for low temperatures, while there is a deformation crossover from low-temperature lattice hardening to high temperature lattice softening in response to extensive plastic deformation.« less

  4. In situ proton irradiation-induced creep at very high temperature

    NASA Astrophysics Data System (ADS)

    Campbell, Anne A.; Was, Gary S.

    2013-02-01

    This objective of this work was to develop an experimental facility that can perform in situ high temperature proton irradiation-induced creep experiments on a range of materials. This was achieved by designing an irradiation chamber and stage that allows for load application and removal, provides a method for controlling and monitoring temperature and proton flux, and a means to make in situ measurement of dimensional change of the samples during the experiment. Initial experiments on POCO Graphite Inc. ZXF-5Q grade ultra-fine grain samples irradiated at 1000 °C at a damage rate of 1.15 × 10-6 dpa/s exhibited a linear dependence of measured creep rate on applied stress over a range of stresses from 10 MPa to 40 MPa.

  5. Quantification of uncertainties in coupled material degradation processes - High temperature, fatigue and creep

    NASA Technical Reports Server (NTRS)

    Boyce, L.; Chamis, C. C.

    1991-01-01

    This paper describes the development of methodology that provides for quantification of uncertainties in lifetime strength of aerospace materials subjected to a number of diverse effects. A probabilistic material degradation model, in the form of a randomized multifactor interaction equation, has been postulated for lifetime strength degradation of structural components of aerospace propulsion systems. The model includes effects that typically reduce lifetime strength and may include temperature, mechanical fatigue, creep and others. The paper also includes the analysis of experimental data from the open literature for Inconel 718. These data are used to provide an initial check for model validity, as well as for calibration of the model's empirical material constants. The model validity check and calibration is carried out for three effects, namely, high temperature, mechanical fatigue and creep.

  6. Effect of carbide precipitation on the creep behavior of alloy 800HT in the temperature range 700 C to 900 C

    SciTech Connect

    El-Magd, E.; Nicolini, G.; Farag, M.

    1996-03-01

    The creep behavior of alloy 800HT was studied at 700 C, 800 C, and 900 C under stresses ranging from 30 to 170 MPa. Samples that were tested in the as-quenched condition after solution treatment exhibited longer creep life than those that were over aged before testing. This difference in creep life was found to increase at lower creep stresses at a given temperature. This phenomenon is attributed to the precipitation of M{sub 23}C{sub 6} carbides during the early stages of creep, which strengthen the material by exerting threshold stresses on moving dislocations and thereby reducing the creep rate. A model is developed to describe the influence of carbide precipitation during creep on the behavior of the material under different creep temperatures and stresses. Comparison with the experimental results shows that the model gives accurate predictions of the creep behavior of the material in the range of stresses and temperatures used in the present study. In addition to its predictive value, the model is useful in understanding the factors that affect the creep behavior of materials when precipitation of hard phases is taking place during creep. The strengthening effect of particle precipitation during creep, as represented by the value of the threshold stress, is shown to be a complex function of the supersaturation of the matrix, the applied creep stress, and the test temperature.

  7. Effect of carbide precipitation on the creep behavior of Alloy 800HT in the Temperature Range 700 ° to 900 °

    NASA Astrophysics Data System (ADS)

    El-Magd, E.; Nicolini, G.; Farag, M.

    1996-03-01

    The creep behavior of alloy 800HT was studied at 700 °, 800 °, and 900 ° under stresses ranging from 30 to 170 MPa. Samples that were tested in the as-quenched condition after solution treatment exhibited longer creep life than those that were overaged before testing. This difference in creep life was found to increase at lower creep stresses at a given temperature. This phenomenon is attributed to the precipitation of M23C6carbides during the early stages of creep, which strengthen the material by exerting threshold stresses on moving dislocations and thereby reducing the creep rate. A model is developed to describe the influence of carbide precipitation during creep on the behavior of the material under different creep temperatures and stresses. Comparison with the experimental results shows that the model gives accurate predictions of the creep behavior of the material in the range of stresses and temperatures used in the present study. In addition to its predictive value, the model is useful in understanding the factors that affect the creep behavior of materials when precipitation of hard phases is taking place during creep. The strengthening effect of particle precipitation during creep, as represented by the value of the threshold stress, is shown to be a complex function of the supersaturation of the matrix, the applied creep stress, and the test temperature.

  8. Creep deformation and rupture behavior of 2.25Cr-1Mo steel weldments and its constituents (base metal, weld metal and simulated heat affected zones)

    SciTech Connect

    Laha, K.; Chandravathi, K.S.; Rao, K.B.S.; Mannan, S.L.

    1995-12-31

    Microstructure across a weldment base metal through transformed heat-affected zone (HAZ) to cast weld metal. HAZ of 2.25Cr-1Mo weldment consists of coarse-grain bainite, fine-grain bainite and intercritical region. These HAZ microstructures were simulated by isothermal heat-treatments. Creep tests were carried out on base metal, weld metal, weldment and the simulated HAZ structures. Creep deformation and fracture behavior of 2.25Cr-1Mo weldments has been assessed based on the properties of its constituents. Coarse-grain bainite with low ductility and intercritical structure with low strength are the critical components of HAZ determining performance of the weldments.

  9. Thermocouples with improved high-temperature creep property by oxide dispersion strengthening

    NASA Astrophysics Data System (ADS)

    Hamada, T.; Yamasaki, H.; Kodama, T.

    2013-09-01

    Platinum-based thermocouples, especially type R and S, whose negative branch is made of pure platinum, often rupture during high-temperature operation. The phenomenon occurs because high-temperature creep strength of pure platinum is very low. In order to avoid this rupture, oxide dispersion strengthened (O.D.S.) platinum was applied to construct high-temperature thermometers for the first time. The W(Ga) value of the O.D.S. platinum was found to be 1.11790, which is not high enough for use as standard platinum resistance thermometer. On the other hand, its purity was found sufficiently high for constituting the negative branch of type R and S thermocouples. Type R thermocouple was prepared with the O.D.S. platinum and was calibrated at the fixed points of tin, zinc, aluminum, silver, gold and palladium and the measured E.M.F. satisfied the IEC class 1 tolerance. The production process for the thermocouple material is similar to that of our original O.D.S. alloy, modified to avoid the contamination from the production process. The observed cross-section microstructure of the developed material was highly elongated, which is typical for O.D.S. platinum and creep rupture strength was almost similar to our original O.D.S. platinum, i.e. the initial stress of the creep rupture was several times higher than that of normal pure platinum when comparing with same rupture time.

  10. Effect of prior creep at 1365 K on the room temperature tensile properties of several oxide dispersion strengthened alloys

    NASA Technical Reports Server (NTRS)

    Whittenberger, J. D.

    1977-01-01

    An experimental study was conducted to determine whether oxide dispersion-strengthened (ODS) Ni-base alloys in wrought bar form are subject to creep degradation effects similar to those found in thin-gage sheet. The bar products evaluated included ODS-Ni, ODS-NiCr, and advanced ODS-NiCrAl types; the alloys included microstructures ranging from an essentially perfect single crystal to a structure consisting of very small elongated grains. Tensile test specimens were exposed to creep at various stress levels at 1365 K and then tensile tested at room temperature. Low residual tensile properties, change in fracture mode, appearance of dispersoid free bands, grain boundary cavitation, and/or internal oxidation are interpreted as creep degradation effects. The amount of degradation depends on creep strain, and degradation appears to be due to diffusional creep which produces dispersoid free bands around grain boundaries acting as vacancy sources.