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Sample records for 5 10 15

  1. 5,10,15-Triferrocenylcorrole Complexes.

    PubMed

    Pomarico, Giuseppe; Galloni, Pierluca; Mandoj, Federica; Nardis, Sara; Stefanelli, Manuela; Vecchi, Andrea; Lentini, Sara; Cicero, Daniel O; Cui, Yan; Zeng, Lihan; Kadish, Karl M; Paolesse, Roberto

    2015-11-01

    Complexes of 5,10,15-triferrocenylcorrole were synthesized from the crude free-base corrole product obtained by the reaction of ferrocenyl aldehyde and pyrrole. Direct formation of the complex in this manner leads to an increase of the reaction yield by protecting the corrole ring toward oxidative decomposition. The procedure was successful and gave the expected product in the case of the copper and triphenylphosphinecobalt complexes, but an unexpected result was obtained in the case of the nickel derivative, where metal insertion led to a ring opening of the macrocycle at the 5 position, giving as a final product a linear tetrapyrrole nickel complex bearing two ferrocenyl groups. The purified 5,10,15-triferrocenylcorrole complexes have been fully characterized by a combination of spectroscopic methods, electrochemistry, spectroelectrochemistry, and density functional theory calculations. Copper derivatives of 10-monoferrocenyl- and 5,15-diferrocenylcorrole were prepared to investigate how the number and position of the ferrocenyl groups influenced the spectroscopic and electrochemical properties of the resulting complexes. A complete assignment of resonances in the (1)H and (13)C NMR spectra was performed for the cobalt and nickel complexes, and detailed electrochemical characterization was carried out to provide additional insight into the degree of communication between the meso-ferrocenyl groups on the conjugated macrocycle and the central metal ion of the ferrocenylcorrole derivatives. PMID:26460880

  2. 15 CFR 10.5 - Development of a recommended standard.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 1 2010-01-01 2010-01-01 false Development of a recommended standard... DEVELOPMENT OF VOLUNTARY PRODUCT STANDARDS § 10.5 Development of a recommended standard. (a) The Standard... Department or the chairman of this committee. If conducted by the chairman, a report of the vote shall...

  3. 15 CFR 10.5 - Development of a recommended standard.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 1 2011-01-01 2011-01-01 false Development of a recommended standard... DEVELOPMENT OF VOLUNTARY PRODUCT STANDARDS § 10.5 Development of a recommended standard. (a) The Standard... Department or the chairman of this committee. If conducted by the chairman, a report of the vote shall...

  4. β-Nitro-5,10,15-tritolylcorroles

    PubMed Central

    Stefanelli, Manuela; Pomarico, Giuseppe; Tortora, Luca; Nardis, Sara; Fronczek, Frank R.; McCandless, Gregory T.; Smith, Kevin M.; Manowong, Machima; Chen, Ping; Kadish, Karl M.; Rosa, Angela; Ricciardi, Giampaolo; Paolesse, Roberto

    2012-01-01

    Functionalization of the β-pyrrolic positions of the corrole macrocycle with –NO2 groups is limited at present to metallocorrolates due to of the instability exhibited by corrole free bases under oxidizing conditions. A careful choice of the oxidant can limit the transformation of corroles into decomposition products or isocorrole species, preserving the corrole aromaticity, and thus allowing the insertion of nitro groups onto the corrole framework. Here we report results obtained by reacting 5,10,15-tritolylcorrole (TTCorrH3) with the AgNO2/NaNO2 system, to give mono- and di-nitrocorrole derivatives when stoichiometry is carefully controlled. Reactions were found to be regioselective, affording the 3-NO2TTCorrH3 and 3,17-(NO2)2TTCorrH3 isomers as the main products in the case of mono- and di-substitution, in 53 and 20% yields, respectively. In both cases, traces of other mono- and di-substituted isomers were detected, which were structurally characterized by X-ray crystallography. The influence of the β-nitro substituents on the corrole properties is studied in detail by UV-visible, electrochemical, and spectroelectrochemical characterization of these functionalized corroles. Density Functional Theory (DFT) and time-dependent DFT (TDDFT) calculations of the ground and excited state properties of these β-nitrocorrole derivatives also afforded significant information, closely matching the experimental observations. It is found that the β-NO2 substituents conjugate with the π-aromatic system of the macrocycle, which initiates significant changes in both the spectroscopic and redox properties of the so functionalized corroles. This effect is more pronounced when the nitro group is introduced at the 2-position, because in this case the conjugation is, for steric reasons, more efficient than in the 3-nitro isomer. PMID:22668242

  5. 10 CFR 1.5 - Location of principal offices and regional offices.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 10 Energy 1 2011-01-01 2011-01-01 false Location of principal offices and regional offices. 1.5 Section 1.5 Energy NUCLEAR REGULATORY COMMISSION STATEMENT OF ORGANIZATION AND GENERAL INFORMATION Introduction § 1.5 Location of principal offices and regional offices. (a) The principal NRC offices are located in the Washington, DC, area....

  6. 10 CFR 1.5 - Location of principal offices and regional offices.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 10 Energy 1 2013-01-01 2013-01-01 false Location of principal offices and regional offices. 1.5 Section 1.5 Energy NUCLEAR REGULATORY COMMISSION STATEMENT OF ORGANIZATION AND GENERAL INFORMATION Introduction § 1.5 Location of principal offices and regional offices. (a) The principal NRC offices are located in the Washington, DC, area....

  7. The corrole and ferrocene marriage: 5,10,15-triferrocenylcorrolato Cu.

    PubMed

    Pomarico, Giuseppe; Vecchi, Andrea; Mandoj, Federica; Bortolini, Olga; Cicero, Daniel O; Galloni, Pierluca; Paolesse, Roberto

    2014-04-21

    Two synthetic routes have been defined for the preparation of a 5,10,15-triferrocenylcorrole Cu derivative. This complex has been characterized and the preliminary electrochemical investigation shows a strong interaction among the corrole and meso ferrocenyl substituents. The results obtained suggest that peculiar properties are gained by combining the eccentric characteristics of ferrocenyl substitution with the corrole macrocycle. PMID:24616907

  8. Use of the "Mental Health Inventory - 5" with Portuguese 10-15 years old.

    PubMed

    Marques, Susana C; Pais-Ribeiro, José Luis; Lopez, Shane J

    2011-05-01

    The present study describes the psychometric properties of the Portuguese version of the Mental Health Inventory-5 for use with young adolescents. A sample of 367 Portuguese students (aged 10-15 years) completed the Portuguese-language versions of Mental Health Inventory-5 (MHI-5; Berwick et al., 1991), Children's Hope Scale (CHS; Snyder et al., 1997), Students' Life Satisfaction Scale (SLSS; Huebner, 1991a), and Global Self-Worth Sub-scale (Harter, 1985). Analysis of readability, reliability (internal consistency and 1-year stability), factor structure, and criterion-related validity suggested that the MHI-5 can be appropriately used in this age group. Implications of the findings are discussed. PMID:21568203

  9. Combustion synthesis of 5 and 10 mol% YO 1.5 doped ThO 2 powders

    NASA Astrophysics Data System (ADS)

    Purohit, R. D.; Saha, S.; Tyagi, A. K.

    2003-11-01

    Nanocrystalline 5 and 10 mol% YO 1.5 doped ThO 2 powders were prepared by the combustion technique using citric acid as a fuel and nitrates as oxidants. The auto-ignition of the fuel-deficient precursors (prepared by thermal dehydration of the aqueous solutions containing metal nitrates and citric acid in required molar ratio) directly resulted in the well crystalline powders of the desired solid solutions along with traces of carbonaceous material. The as-prepared and calcined powders were characterized by X-ray diffraction (XRD), high-temperature XRD and by their sinterability. The YO 1.5 doped ThO 2 powders when cold-pressed and sintered at 1300 °C for 2 h resulted in ⩾95% of their theoretical densities with nanograin microstructure.

  10. RealGasBrine v1.0 option of TOUGH+ v1.5

    SciTech Connect

    Moridis, George

    2015-02-27

    RealGasBrine v1.0 is a numerical code that for the simulation of the behavior of gas-bearing porous and/fractured geologic media. It is an option of TOUGH+ v1.5 [Moridis, 2014], a successor to the TOUGH2 [Pruess et al., 1999; 2012] family of codes for multi-component, multiphase ?uid and heat ?ow developed at the Lawrence Berkeley National Laboratory. RealGasBrine v1.0 needs the TOUGH+ v1.5 core code in order to compile and execute. It is written in standard FORTRAN 95/2003, and can be run on any computational platform (workstation, PC, Macintosh) for which such compilers are available. RealGasBrine v1.0 describes the non-isothermal two- (for pure water) or three-phase (for brine) flow of an aqueous phase and a real gas mixture in a gas-bearing medium, with a particular focus in ultra-tight (such as tight-sand and shale gas) systems. Up to 12 individual real gases can be tracked, and salt can precipitate as solid halite. The capabilities of the code include coupled flow and thermal effects, real gas behavior, Darcy and non-Darcy flow, several isotherm options of gas sorption onto the grains of the porous media, complex fracture descriptions, gas solubility into water, and geomechanical effects on flow properties. RealGasBrine v1.0 allows the study of flow and transport of fluids and heat over a wide range of time frames and spatial scales not only in gas reservoirs, but also in any problem involving the flow of gases in geologic media, including the geologic storage of greenhouse gas mixtures, the behavior of geothermal reservoirs with multi-component condensable (H2O and CO2) and non-condensable gas mixtures, the transport of water and released H2 in nuclear waste storage applications, etc.

  11. Assessment of agreement between the AMPLICOR HIV-1 MONITOR test versions 1.0 and 1.5.

    PubMed

    Hill, Charles E; Green, Alicia M; Ingersoll, Jessica; Easley, Kirk A; Nolte, Frederick S; Caliendo, Angela M

    2004-01-01

    The agreement of the microwell plate AMPLICOR HIV-1 MONITOR version 1.0 (MWP 1.0), the microwell plate AMPLICOR HIV-1 MONITOR version 1.5 (MWP 1.5), and the COBAS AMPLICOR HIV-1 MONITOR version 1.5 (COBAS 1.5) tests was evaluated using clinical specimens and well-characterized control material. Two hundred patient plasma specimens and a panel of known human immunodeficiency virus type 1 (HIV-1) subtypes were tested. All data were log(10) transformed prior to analysis. The 95% limits of agreement for the three tests at the average of 3.66 log(10) copies/ml were +/- 0.28 log(10), +/- 0.34 log(10), and +/- 0.34 log(10) copies/ml for MWP 1.0-MWP 1.5, MWP 1.0-COBAS 1.5, and MWP 1.5-COBAS 1.5, respectively. Ten specimens (6.1%) had differences exceeding the limits of agreement for the MWP 1.0 and MWP 1.5 tests. Correlation coefficients among the three tests were high (r >or=0.96). The viral-load values obtained with the MWP 1.0 test were only 2.1% higher on average than those measured with the MWP 1.5 test and 1.6% higher than those seen with the COBAS 1.5 test. The MWP 1.5 test values were 0.8% higher than the COBAS 1.5 test values. Overall, there was less agreement among the different tests for viral-load values near the lower limit of quantification. The MWP 1.0 test underquantified subtypes A, E, F, G, and H by 1.0 to 2.0 log(10) copies/ml; this problem was not observed with the MWP 1.5 test. The close agreement among the results obtained with the different test versions and formats suggests that it is not necessary to reestablish a baseline viral load when changing AMPLICOR HIV-1 MONITOR tests, unless the patient is known to be infected with a non-B subtype. PMID:14715766

  12. RealGasBrine v1.0 option of TOUGH+ v1.5

    2015-02-27

    RealGasBrine v1.0 is a numerical code that for the simulation of the behavior of gas-bearing porous and/fractured geologic media. It is an option of TOUGH+ v1.5 [Moridis, 2014], a successor to the TOUGH2 [Pruess et al., 1999; 2012] family of codes for multi-component, multiphase ?uid and heat ?ow developed at the Lawrence Berkeley National Laboratory. RealGasBrine v1.0 needs the TOUGH+ v1.5 core code in order to compile and execute. It is written in standard FORTRANmore » 95/2003, and can be run on any computational platform (workstation, PC, Macintosh) for which such compilers are available. RealGasBrine v1.0 describes the non-isothermal two- (for pure water) or three-phase (for brine) flow of an aqueous phase and a real gas mixture in a gas-bearing medium, with a particular focus in ultra-tight (such as tight-sand and shale gas) systems. Up to 12 individual real gases can be tracked, and salt can precipitate as solid halite. The capabilities of the code include coupled flow and thermal effects, real gas behavior, Darcy and non-Darcy flow, several isotherm options of gas sorption onto the grains of the porous media, complex fracture descriptions, gas solubility into water, and geomechanical effects on flow properties. RealGasBrine v1.0 allows the study of flow and transport of fluids and heat over a wide range of time frames and spatial scales not only in gas reservoirs, but also in any problem involving the flow of gases in geologic media, including the geologic storage of greenhouse gas mixtures, the behavior of geothermal reservoirs with multi-component condensable (H2O and CO2) and non-condensable gas mixtures, the transport of water and released H2 in nuclear waste storage applications, etc.« less

  13. Tailoring the interfacial exchange coupling of perpendicularly magnetized Co/L10-Mn1.5Ga bilayers

    NASA Astrophysics Data System (ADS)

    Xiao, J. X.; Lu, J.; Liu, W. Q.; Zhang, Y. W.; Wang, H. L.; Zhu, L. J.; Deng, H. X.; Wei, D. H.; Xu, Y. B.; Zhao, J. H.

    2016-06-01

    We have studied the magnetic properties of Co (2–12 MLs)/L10-Mn1.5Ga (15 nm) bilayers without and with annealing at 300 °C by a combination of superconducting quantum interference device (SQUID) magnetometry and x-ray magnetic circular dichroism (XMCD). We find that the Co layer can remain perpendicularly magnetized when its thickness is less than six monolayers due to the coupling between Co and L10-Mn1.5Ga layers, which is doubly confirmed by both SQUID and XMCD measurements. Such an exchange coupling between L10-Mn1.5Ga and Co layers changes from ferromagnetic coupling to antiferromagnetic coupling after the annealing process. Furthermore, the magnetic coupling can also be tailored from ferromagnetic to antiferromagnetic by changing the L10-Mn1.5Ga surface from Mn-rich to Ga-rich. The first-principles calculations show that the interfacial coupling type is ferromagnetic for a Mn-terminated L10-Mn1.5Ga bilayer, while antiferromagnetic for a Ga-terminated bilayer. The spin and orbital moments of Co in the Co/L10-Mn1.5Ga bilayers are calculated according to the sum rules and the ratio of the orbital to spin magnetic moments for Co is not enhanced like other perpendicularly magnetized Co-based multilayers such as Co/Pd and Co/Pt.

  14. Synthesis of 21,23-selenium- and tellurium-substituted 5-porphomethenes, 5,10-porphodimethenes, 5,15-porphodimethenes, and porphotrimethenes and their interactions with mercury.

    PubMed

    Ahmad, Sohail; Yadav, Kumar Karitkey; Bhattacharya, Soumee; Chauhan, Prashant; Chauhan, S M S

    2015-04-17

    The 3+1 condensation of symmetrical 16-Selena/telluratripyrranes with symmetrical selenophene-2,5-diols/tellurophene-2,5-diols in the presence of BF3-etheratre or BF3-methanol followed by oxidation with DDQ gave 5,10-porphodimethenes, whereas the process with unsymmetrical selenophene-2,5-diols/tellurophene-2,5-diols gave 5-porphomethenes. In addition, the reaction of unsymmetrical 16-Selena/telluratripyrranes with symmetrical selenophene-2,5-diols/tellurophene-2,5-diols gave the corresponding porphotrimethenes, whereas the process with unsymmetrical selenophene-2,5-diols/tellurophene-2,5-diols gave the 5,15-porphodimethenes. The structures of different products were characterized by IR, (1)H and (13)C NMR, (1)H-(1)H COSY, CHN analysis, and mass spectrometry. The binding of mercury with the calix[4]phyrins mentioned above had been observed in the decreasing order of porphodimethenes > porphomethenes > porphotrimethenes by UV-vis and (1)H NMR spectroscopy. PMID:25803565

  15. Effects of Heating on Proportions of Azaspiracids 1-10 in Mussels (Mytilus edulis) and Identification of Carboxylated Precursors for Azaspiracids 5, 10, 13, and 15.

    PubMed

    Kilcoyne, Jane; McCarron, Pearse; Hess, Philipp; Miles, Christopher O

    2015-12-30

    Azaspiracids (AZAs) are marine biotoxins that induce human illness following the consumption of contaminated shellfish. European Union regulation stipulates that only raw shellfish are tested, yet shellfish are often cooked prior to consumption. Analysis of raw and heat-treated mussels (Mytilus edulis) naturally contaminated with AZAs revealed significant differences (up to 4.6-fold) in AZA1-3 (1-3) and 6 (6) values due to heat-induced chemical conversions. Consistent with previous studies, high levels of 3 and 6 were detected in some samples that were otherwise below the limit of quantitation before heating. Relative to 1, in heat-treated mussels the average (n = 40) levels of 3 (range, 11-502%) and 6 (range, 3-170%) were 62 and 31%, respectively. AZA4 (4) (range, <1-27%), AZA5 (5) (range, 1-21%), and AZA8 (8) (range, 1-27%) were each ∼5%, whereas AZA7 (7), AZA9 (9), and AZA10 (10) (range, <1-8%) were each under 1.5%. Levels of 5, 10, AZA13 (13), and AZA15 (15) increased after heating, leading to the identification of novel carboxylated AZA precursors in raw shellfish extracts, which were shown by deuterium labeling to be precursors for 5, 10, 13, and 15. PMID:26631586

  16. Synthesis of CeFe10.5Mo1.5 with ThMn12-type structure by melt spinning

    SciTech Connect

    Zhou, C; Tessema, M; Meyer, MS; Pinkerton, FE

    2013-06-01

    Rare earth compounds RFe12_xMx with tetragonal ThMn12-type structure are of great research interest for potential applications as permanent magnets. These materials are known to serve as the precursors for nitriding and hydriding processes which in certain conditions can dramatically increase the Curie temperature, spontaneous magnetization, and affect the magnetic anisotropy. In this paper, we report the phase study of CeFe10.5Mo1.5 samples melt spun at various surface wheel speeds vs between 5 m/s and 60 m/s. The results from quantitative Rietveld analysis indicate that the as-spun ribbons are a mixture of primary CeFe10.5Mo1.5 phase with impurity phases such as Ce2Fe17, Fe-Mo alloy and CeFe2. When the wheel speed vs is below 25 m/s, CeFe10.5Mo1.5 phase accounts for greater than 85 wt% in the as-spun ribbons, while the Fe-Mo alloy is the only detectable impurity phase. Above v(s)=25 m/s, as the wheel speed increases, CeFe10.5Mo1.5 phase decreases monotonically to about 60 wt% at v(s)=6O m/s while the amounts of impurity phases increase. Thermogravimetric measurement indicates that the Curie temperature T-c. corresponding to CeFe10.5Mo1.5 phase is 341 K. As a result, the best performing sample melt spun at v(s),=15 m/s only exhibits an energy product BHmax=0.121 MGOe at room temperature. Although such a number is modest for a permanent magnet, further nitriding is expected to greatly enhance the Curie temperature, and hence the magnetic performance. (C) 2013 Elsevier B.V. All rights reserved.

  17. Computational dosimetry in embryos exposed to electromagnetic plane waves over the frequency range of 10 MHz-1.5 GHz.

    PubMed

    Kawai, Hiroki; Nagaoka, Tomoaki; Watanabe, Soichi; Saito, Kazuyuki; Takahashi, Masaharu; Ito, Koichi

    2010-01-01

    This paper presents calculated specific absorption rate (SAR) dosimetry in 4 and 8 week Japanese pregnant-woman models exposed to plane waves over the frequency range of 10 MHz-1.5 GHz. Two types of 2 mm spatial-resolution pregnant-woman models comprised a woman model, which is similar to the average-sized Japanese adult female in height and weight, with a cubic (4 week) embryo or spheroidal (8 week) one. The averaged SAR in the embryos exposed to vertically and horizontally polarized plane waves at four kinds of propagation directions are calculated from 10 MHz to 1.5 GHz. The results indicate that the maximum average SAR in the embryos exposed to plane waves is lower than 0.08 W kg(-1) when the incident power density is at the reference level of ICNIRP guideline for general public environment. PMID:20009180

  18. 21 CFR 73.3118 - N,N′-(9,10-Dihydro-9,10-dioxo-1,5-anthracenediyl) bisbenzamide.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 21 Food and Drugs 1 2012-04-01 2012-04-01 false N,Nâ²-(9,10-Dihydro-9,10-dioxo-1,5-anthracenediyl) bisbenzamide. 73.3118 Section 73.3118 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL LISTING OF COLOR ADDITIVES EXEMPT FROM CERTIFICATION Medical Devices § 73.3118...

  19. 21 CFR 73.3118 - N,N′-(9,10-Dihydro-9,10-dioxo-1,5-anthracenediyl) bisbenzamide.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 21 Food and Drugs 1 2013-04-01 2013-04-01 false N,Nâ²-(9,10-Dihydro-9,10-dioxo-1,5-anthracenediyl) bisbenzamide. 73.3118 Section 73.3118 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL LISTING OF COLOR ADDITIVES EXEMPT FROM CERTIFICATION Medical Devices § 73.3118...

  20. Interaction peculiarities of 5,10,15,20-tetrakis(4-N-methylpyridil) tetra iodide porphyrin with albumin

    NASA Astrophysics Data System (ADS)

    Lebedeva, N. Sh.; Malkova, E. A.; Popova, T. E.; Kutyrev, A. E.; Syrbu, S. A.; Parfenyuk, E. V.; Vyugin, A. I.

    2014-01-01

    In present work interactions of bovine serum albumin with 5,10,15,20-tetrakis(4-N-methylpyridil) tetra iodide porphyrin have been studied by electron absorption and fluorescence spectroscopy. The studies were carried out in aqueous media at different pH and in water-dimethylformamide mixtures containing up to 0.19 M of the organic solvent. It has been demonstrated that the porphyrin forms stable complexes with BSA in which the porphyrin is located subdomains IB and IIA. The stability constants of the complexes is practically independent of pH.

  1. Method of using 5,10,15,20-tetrakis(carboxyphenyl)porphine for detecting cancers of the lung

    DOEpatents

    Cole, D.A.; Moody, D.C. III; Ellinwood, L.E.; Klein, M.G.

    1992-11-10

    A method is described for using tetra-aryl porphyrins for and, in particular, 5,10,15,20-tetrakis(4-carboxyphenyl)porphine as a fluorescent tracer for cancers of the lung, and as a radiotracer therefor as a complex with [sup 67]Cu. The latter complex also provides a source of beta radiation for selective destruction of lung malignancies as well as gamma radiation useful for image analysis of the lungs by single photon emission computed tomography, as an example, both in vivo. Copper-64 may be substituted for the [sup 67]Cu if only radiotracer characteristics are of interest. This lighter isotope of copper is a positron emitter, and positron emission tomography techniques can be used to locate the malignant tissue mass. 1 figure.

  2. Method of using 5,10,15,20-tetrakis(carboxyphenyl)porphine for detecting cancers of the lung

    DOEpatents

    Cole, Dean A.; Moody, III, David C.; Ellinwood, L. Edward; Klein, M. Gerard

    1992-01-01

    Method using tetra-aryl porphyrins for and, in particular, 5,10,15,20-tetrakis(4-carboxyphenyl)porphine as a fluorescent tracer for cancers of the lung, and as a radiotracer therefor as a complex with .sup.67 Cu. The latter complex also provides a source of beta radiation for selective destruction of lung malignancies as well as gamma radiation useful for image analysis of the situs thereof by single photon emission computed tomography, as an example, both in vivo. Copper-64 may be substituted for the .sup.67 Cu if only radiotracer characteristics are of interest. This lighter isotope of copper is a positron emitter, and positron emission tomography techniques cna be used to locate the malignant tissue mass.

  3. Method using 5,10,15,20-tetrakis(4-carboxyphenyl)porphine for treating cancers of the lung

    DOEpatents

    Cole, Dean A.; Moody, III, David C.; Ellinwood, L. Edward; Klein, M. Gerard

    1995-01-01

    Method using tetra-aryl porphyrins for and, in particular, 5,10,15,20-tetrakis(4-carboxyphenyl)porphine as a fluorescent tracer for cancers of the lung, and as a radiotracer therefor as a complex with .sup.67 Cu. The latter complex also provides a source of beta radiation for selective destruction of lung malignancies as well as gamma radiation useful for image analysis of the situs thereof by single photon emission computed tomography, as an example, both in vivo. Copper-64 may be substituted for the .sup.67 Cu if only radiotracer characteristics are of interest. This lighter isotope of copper is a positron emitter, and positron emission tomography techniques can be used to locate the malignant tissue mass.

  4. Operation of NIM5 fountain with 1.5x10-15 uncertainty and design of new NIM6 in NIM

    NASA Astrophysics Data System (ADS)

    Fang, F.; Liu, N.; Liu, K.; Chen, W.; Suo, R.; Li, Tianchu

    2016-06-01

    The cesium fountain primary frequency standard NIM5 started to operate since 2008 and started to report to BIPM since 2014. The major constrains of NIM5 is a relatively large background signal at the detection and microwave leakages due to the Ramsey cavity. A new fountain clock NIM6 is under construction. Besides some improvements on the vacuum system, a new Ramsey cavity and a microwave synthesizer are made to reduce the Type B uncertainty. Another feature of NIM6 is collecting atoms from a MOT loading optical molasses to get more atoms with a more uniform density distribution. With a new frequency synthesizer based on cryogenic sapphire oscillator (CSO), NIM6 is aiming to reach the quantum projection noise, thus leading to a reduced Type A uncertainty compared with NIM5.

  5. Effect of Annealing Time on Microstructural Evolution and Deformation Characteristics in 10Mn1.5Al TRIP Steel

    NASA Astrophysics Data System (ADS)

    Han, Qihang; Zhang, Yulong; Wang, Li

    2015-05-01

    To investigate microstructural evolution and its effects on the deformation behaviors of cold-rolled 10Mn1.5Al TRIP steel, a series of intercritical annealing treatments with various holding times from 3 minutes to 48 hours were conducted. With the increase of the holding time from 3 minutes to 12 hours, the elongation was improved from 15 to 42 pct, while the tensile strength was only reduced from 1210 to 1095 MPa; the strength-ductility combination thus exceeded 45 GPa pct. Austenite was found to coexist with martensite within deformed grains, which reduced the strain concentration at the interface. The austenite transformation fraction, as measured from the {220} peaks, after 3 minutes annealing was half that after 12 hours annealing. This is an indication that the slip systems were more easily activated in the micro-scaled grains compared with nano-scaled grains. Therefore, although the stability of austenite would have increased during annealing, size-induced slip suppression was reduced. Thus, more strain was accommodated in the austenite, facilitating a greater strain-induced transformation and better ductility.

  6. The diagnostic value of 1.5-T diffusion-weighted MR imaging in detecting 5 to 10 mm metastatic cervical lymph nodes of nasopharyngeal carcinoma

    PubMed Central

    Jin, Guan Qiao; Yang, Jun; Liu, Li Dong; Su, Dan Ke; Wang, Duo Ping; Zhao, Sheng Fa; Liao, Zhi Ling

    2016-01-01

    Abstract The aim of the study was to prospectively assess the diagnostic accuracy of 1.5 T diffusion-weighted imaging (DWI) for 5 to 10 mm metastatic cervical lymph nodes of patients with nasopharyngeal carcinoma (NPC). All patients with histopathologically confirmed NPC underwent DWI with 2 b values of 0 and 800 s/mm2 were enrolled. The shortest axial diameter and mean apparent diffusion coefficient (ADC) value were recorded when lymph nodes with a shortest axial diameter from 5 to 10 mm were measured. The correlation between the pathological diagnoses and mean ADC values in the benign and metastatic lymph nodes were compared using the Z test. Receiver operating characteristic (ROC) curve analysis was performed to evaluate the diagnostic performance of DWI. Three hundred fourteen nodes of 52 patients with NPC consisted of 46.5% (146/314) metastatic lymph nodes and 53.5% (168/314) benign lymph nodes. The mean ADC value (×10–3 mm2/s) of benign lymph nodes was (1.110 ± 0.202), which was significantly higher than that of metastatic nodes (0.878 ± 0.159) (P < 0.05). The sensitivity, specificity, positive predictive value, and negative predictive value, accuracy for differentiating metastatic from benign lymph nodes using a cutoff ADC value of 0.924 × 10–3 mm2/s was 83.56%, 82.74%, 80.79%, 85.28%, and 82.80%, respectively. The area under the ROC curve was 0.851 (95% confidence intervals: 0.807–0.889). This study demonstrated that DWI is helpful in detecting 5 to 10 mm metastatic lymph nodes of patients with NPC. PMID:27512841

  7. Systematic Study of Rayleigh-Taylor Growth in Directly Driven Plastic Targets in a Laser-Intensity Range from ~2 x 10^14 to ~1.5 x 10^15 W/cm^2

    SciTech Connect

    Smalyuk, V.A.; Hu, S.X.; Goncharov, V.N.; Meyerhofer, D.D.; Sangster, T.C.; Stoeckl, C.; Yaakobi, B.

    2008-09-05

    Direct-drive, Rayleigh–Taylor (RT) growth experiments were performed using planar plastic targets on the OMEGA Laser Facility [T. R. Boehly et al., Opt. Commun. 133, 495 (1997)] at laser intensities between ~2 x 10^14 and ~1.5 x 10^15 W/cm^2. The primary purpose of the experiments was to test fundamental physics in hydrocodes at the range of drive intensities relevant to ignition designs. The target acceleration was measured with a streak camera using side-on, x-ray radiography, while RT growth was measured with a framing camera using face-on radiography. In a laser-intensity range from 2 to 5 x 10^14 W/cm^2, the measured RT growth agrees well with two-dimensional simulations, based on a local model of thermal-electron transport. The RT growth at drive intensities above ~1.0 x 10^15 W/cm^2 was strongly stabilized compared to the local model predictions. The experiments demonstrate that standard simulations, based on a local model of electron thermal transport, break down at peak intensities of ignition designs, although they work well at lower intensities. These results also imply that direct-drive ignition targets are significantly more stable than previously calculated using local electron-transport models at peak intensities of ignition designs. The preheating effects by nonlocal electron transport and hot electrons were identified as some of the stabilizing mechanisms.

  8. Systematic study of Rayleigh-Taylor growth in directly driven plastic targets in a laser-intensity range from {approx}2x10{sup 14} to {approx}1.5x10{sup 15} W/cm{sup 2}

    SciTech Connect

    Smalyuk, V. A.; Hu, S. X.; Goncharov, V. N.; Meyerhofer, D. D.; Sangster, T. C.; Stoeckl, C.; Yaakobi, B.

    2008-08-15

    Direct-drive, Rayleigh-Taylor (RT) growth experiments were performed using planar plastic targets on the OMEGA Laser Facility [T. R. Boehly et al., Opt. Commun. 133, 495 (1997)] at laser intensities between {approx}2x10{sup 14} and {approx}1.5x10{sup 15} W/cm{sup 2}. The primary purpose of the experiments was to test fundamental physics in hydrocodes at the range of drive intensities relevant to ignition designs. The target acceleration was measured with a streak camera using side-on, x-ray radiography, while RT growth was measured with a framing camera using face-on radiography. In a laser-intensity range from 2 to 5x10{sup 14} W/cm{sup 2}, the measured RT growth agrees well with two-dimensional simulations, based on a local model of thermal-electron transport. The RT growth at drive intensities above {approx}1.0x10{sup 15} W/cm{sup 2} was strongly stabilized compared to the local model predictions. The experiments demonstrate that standard simulations, based on a local model of electron thermal transport, break down at peak intensities of ignition designs, although they work well at lower intensities. These results also imply that direct-drive ignition targets are significantly more stable than previously calculated using local electron-transport models at peak intensities of ignition designs. The preheating effects by nonlocal electron transport and hot electrons were identified as some of the stabilizing mechanisms.

  9. 10 CFR 15.35 - Payments.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... described in 5 U.S.C. 5514 and codified in 10 CFR part 16, all installment payment arrangements must be in... 10 Energy 1 2011-01-01 2011-01-01 false Payments. 15.35 Section 15.35 Energy NUCLEAR REGULATORY COMMISSION DEBT COLLECTION PROCEDURES Administrative Collection of Claims § 15.35 Payments. (a) Payment...

  10. 10 CFR 15.35 - Payments.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... described in 5 U.S.C. 5514 and codified in 10 CFR part 16, all installment payment arrangements must be in... 10 Energy 1 2010-01-01 2010-01-01 false Payments. 15.35 Section 15.35 Energy NUCLEAR REGULATORY COMMISSION DEBT COLLECTION PROCEDURES Administrative Collection of Claims § 15.35 Payments. (a) Payment...

  11. 10 CFR 15.35 - Payments.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... described in 5 U.S.C. 5514 and codified in 10 CFR part 16, all installment payment arrangements must be in... 10 Energy 1 2014-01-01 2014-01-01 false Payments. 15.35 Section 15.35 Energy NUCLEAR REGULATORY COMMISSION DEBT COLLECTION PROCEDURES Administrative Collection of Claims § 15.35 Payments. (a) Payment...

  12. 10 CFR 15.35 - Payments.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... described in 5 U.S.C. 5514 and codified in 10 CFR part 16, all installment payment arrangements must be in... 10 Energy 1 2012-01-01 2012-01-01 false Payments. 15.35 Section 15.35 Energy NUCLEAR REGULATORY COMMISSION DEBT COLLECTION PROCEDURES Administrative Collection of Claims § 15.35 Payments. (a) Payment...

  13. In vitro cytotoxicity assessment of [5,10,15,20-tetra (4-sulfophenyl) porphyrin] on tumor and nontumor cell lines

    NASA Astrophysics Data System (ADS)

    Alexandrova, R.; Sabotinov, O.; Stoykova, Elena V.; Ion, Rodica-Mariana; Shurulinkov, Stanislav; Minchev, Georgi

    2004-06-01

    In this study we evaluate the cytotoxicity of 5,10,15,20- tetra (4-sulfophenyl) porphyrins on a tumor cell line LSCC-SF-Mc29, obtained from a transplantable chicken hepatoma induced by the myelocytomatosis virus Mc29, a timor line LSR-SF-SR, obtained from a transplantable sarcoma in rat induced by Rous sarcoma virus strain Schmidt-Ruppin and for normal mouse cell line (BALB/c-3T3-A31) and bovine kidney cell line (MDBK). The cells were exposed to irradiation from a pulsed CuBr vapor laser system at 510.6 nm and 578.2 nm at fluence rate 50 mW/cm2 and pulse frequency rate 20 kHz. The viability of cells was determined by the neutral red uptake cytotoxicity assay. The light dose-response curves and light exposures that ensure viability drop to 50 % were obtained for each cell line. The cytotoxic effect of TS4PP is most distinguished for LSCC-SF-Mc29. The bovine cell line is more vulnerable than the mouse line, especially at 510.6 nm. The 2-4 times higher viability of the normal cell lines in comparison with the tumor lines has been obtained.

  14. Microstructure of Hot Rolled 1.0C-1.5Cr Bearing Steel and Subsequent Spheroidization Annealing

    NASA Astrophysics Data System (ADS)

    Li, Zhen-Xing; Li, Chang-Sheng; Zhang, Jian; Li, Bin-Zhou; Pang, Xue-Dong

    2016-04-01

    The effect of final rolling temperature and cooling process on the microstructure of 1.0C-1.5Cr bearing steel was studied, and the relationship between the microstructure parameters and subsequent spheroidization annealing was analyzed. The results indicate that the increase of water-cooling rate after hot rolling and the decrease of final cooling temperature are beneficial to reducing both the pearlite interlamellar spacing and pearlite colony size. Prior austenite grain size can be reduced by decreasing the final rolling temperature and increasing the water-cooling rate. When the final rolling temperature was controlled around 1103 K (830 °C), the subsequent cooling rate was set to 10 K/s and final cooling temperature was 953 K (680 °C), the precipitation of grain boundary cementite was suppressed effectively and lots of rod-like cementite particles were observed in the microstructure. Interrupted quenching was employed to study the dissolution behavior of cementite during the austenitizing at 1073 K (800 °C). The decrease of both pearlite interlamellar spacing and pearlite colony size could facilitate the initial dissolution and fragmentation of cementite lamellae, which could shorten the spheroidization time. The fragmentation of grain boundary cementite tends to form large-size undissolved cementite particles. With the increase of austenitizing time from 20 to 300 minutes, mean diameter of undissolved cementite particles increases, indicating the cementite particle coarsening and cementite dissolution occuring simultaneously. Mean diameter of cementite particles in the final spheroidized microstructure is proportional to the mean diameter of undissolved cementite particles formed during partial austenitizing.

  15. Microstructure of Hot Rolled 1.0C-1.5Cr Bearing Steel and Subsequent Spheroidization Annealing

    NASA Astrophysics Data System (ADS)

    Li, Zhen-Xing; Li, Chang-Sheng; Zhang, Jian; Li, Bin-Zhou; Pang, Xue-Dong

    2016-07-01

    The effect of final rolling temperature and cooling process on the microstructure of 1.0C-1.5Cr bearing steel was studied, and the relationship between the microstructure parameters and subsequent spheroidization annealing was analyzed. The results indicate that the increase of water-cooling rate after hot rolling and the decrease of final cooling temperature are beneficial to reducing both the pearlite interlamellar spacing and pearlite colony size. Prior austenite grain size can be reduced by decreasing the final rolling temperature and increasing the water-cooling rate. When the final rolling temperature was controlled around 1103 K (830 °C), the subsequent cooling rate was set to 10 K/s and final cooling temperature was 953 K (680 °C), the precipitation of grain boundary cementite was suppressed effectively and lots of rod-like cementite particles were observed in the microstructure. Interrupted quenching was employed to study the dissolution behavior of cementite during the austenitizing at 1073 K (800 °C). The decrease of both pearlite interlamellar spacing and pearlite colony size could facilitate the initial dissolution and fragmentation of cementite lamellae, which could shorten the spheroidization time. The fragmentation of grain boundary cementite tends to form large-size undissolved cementite particles. With the increase of austenitizing time from 20 to 300 minutes, mean diameter of undissolved cementite particles increases, indicating the cementite particle coarsening and cementite dissolution occuring simultaneously. Mean diameter of cementite particles in the final spheroidized microstructure is proportional to the mean diameter of undissolved cementite particles formed during partial austenitizing.

  16. Research on fast fault identification method of 10.5 kV/1.5 kA superconducting fault current limiter

    NASA Astrophysics Data System (ADS)

    Zhang, Zhifeng; Sun, Qiang; Xiao, Liye; Liu, Daqian; Qiu, Ming; Qiu, Qinquan; Zhang, Guomin; Dai, Shaotao; Lin, Liangzhen

    2014-09-01

    Superconducting fault current limiter (SFCL) is a prospective electric devices connected in series in power grid to limit short-circuit current. A 10.5 kV/1.5 kA 3-phase SFCL with HTS coil of 6.24 mH was developed at IEECAS in China in 2005, which was operated in a local power grid in Hunan province for more than 11,000 h, and integrated lately in a superconducting power substation in Baiyin city in 2011 and is still running safely and reliably. In order to reduce the fault response time and enhance the performance of the SFCL, we analyzed the structure characteristics of the SFCL and discussed the variation of currents and voltages of the HTS coil and the bridge during the fault time. The simulation and tests results of power system validate the feasibility of the fast fault identification method.

  17. 43 CFR 15.5 - Wrecks.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 43 Public Lands: Interior 1 2013-10-01 2013-10-01 false Wrecks. 15.5 Section 15.5 Public Lands: Interior Office of the Secretary of the Interior KEY LARGO CORAL REEF PRESERVE § 15.5 Wrecks. No person... coral formation....

  18. 43 CFR 15.5 - Wrecks.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 43 Public Lands: Interior 1 2012-10-01 2011-10-01 true Wrecks. 15.5 Section 15.5 Public Lands: Interior Office of the Secretary of the Interior KEY LARGO CORAL REEF PRESERVE § 15.5 Wrecks. No person... coral formation....

  19. 43 CFR 15.5 - Wrecks.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 43 Public Lands: Interior 1 2011-10-01 2011-10-01 false Wrecks. 15.5 Section 15.5 Public Lands: Interior Office of the Secretary of the Interior KEY LARGO CORAL REEF PRESERVE § 15.5 Wrecks. No person... coral formation....

  20. 43 CFR 15.5 - Wrecks.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 43 Public Lands: Interior 1 2014-10-01 2014-10-01 false Wrecks. 15.5 Section 15.5 Public Lands: Interior Office of the Secretary of the Interior KEY LARGO CORAL REEF PRESERVE § 15.5 Wrecks. No person... coral formation....

  1. 46 CFR 5.15 - Investigating Officer.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 1 2010-10-01 2010-10-01 false Investigating Officer. 5.15 Section 5.15 Shipping COAST... REGULATIONS-PERSONNEL ACTION Definitions § 5.15 Investigating Officer. An investigating officer is a Coast... credentials issued by the Coast Guard. An Officer in Charge, Marine Inspection is an investigating...

  2. 46 CFR 196.15-5 - Drafts.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 7 2013-10-01 2013-10-01 false Drafts. 196.15-5 Section 196.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS OPERATIONS Test, Drills, and Inspections § 196.15-5 Drafts. (a) The master of every vessel on an ocean, coastwise, or Great Lakes voyage shall enter the drafts of the...

  3. 46 CFR 196.15-5 - Drafts.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 7 2014-10-01 2014-10-01 false Drafts. 196.15-5 Section 196.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS OPERATIONS Test, Drills, and Inspections § 196.15-5 Drafts. (a) The master of every vessel on an ocean, coastwise, or Great Lakes voyage shall enter the drafts of the...

  4. 10 CFR 15.35 - Payments.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... described in 5 U.S.C. 5514 and codified in 10 CFR part 16, all installment payment arrangements must be in... 10 Energy 1 2013-01-01 2013-01-01 false Payments. 15.35 Section 15.35 Energy NUCLEAR REGULATORY...) Otherwise directed in any other part of this chapter....

  5. Ti12.5Zr21V10Cr8.5MnxCo1.5Ni46.5-x AB2-type metal hydride alloys for electrochemical storage application: Part 1. Structural characteristics

    NASA Astrophysics Data System (ADS)

    Bendersky, L. A.; Wang, K.; Levin, I.; Newbury, D.; Young, K.; Chao, B.; Creuziger, A.

    2012-11-01

    The microstructures of a series of AB2-based metal hydride alloys (Ti12.5Zr21V10Cr8.5MnxCo1.5Ni46.5-x) designed to have different fractions of non-Laves secondary phases were studied by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, energy dispersive X-ray spectrometry, and electron backscatter diffraction. The results indicate that the alloys contain a majority of hydrogen storage Laves phases and a minority of fine-structured non-Laves phases. Formation of the phases is accomplished by dendritic growth of a hexagonal C14 Laves phase. The C14 phase is followed by either a peritectic solidification of a cubic C15 Laves phase (low Mn containing alloys) or a C14 phase of different composition (high Mn containing alloys), and finally a B2 phase formed in the interdendritic regions (IDR). The interdendritic regions may then undergo further solid-state transformation into Zr7Ni10-type, Zr9Ni11-type and TiNi-type phases. As the Mn content in the alloy increases, the fraction of the C14 phase increases, whereas the fraction of C15 decreases. In the IDRs when the alloy's Mn content increases the Zr9Ni11 phases and Zr7Ni10 phase fraction first increases and then decreases, while the TiNi-based phase fraction first increases and then stabilized at 0.02. IDR compositions can be generally expressed as (Ti,Zr,V,Cr,Mn,Co)50Ni50, which accounted for 7-10% of the overall alloy volume fraction.

  6. Beyond y and μ: the shape of the CMB spectral distortions in the intermediate epoch, 1.5 × 10{sup 4}∼10{sup 5}

    SciTech Connect

    Khatri, Rishi; Sunyaev, Rashid A. E-mail: sunyaev@mpa-Garching.mpg.de

    2012-09-01

    We calculate numerical solutions and analytic approximations for the intermediate-type spectral distortions. Detection of a μ-type distortion (saturated comptonization) in the CMB will constrain the time of energy injection to be at a redshift 2 × 10{sup 6}∼>z∼>2 × 10{sup 5}, while a detection of a y-type distortion (minimal comptonization) will mean that there was heating of CMB at redshift z∼<1.5 × 10{sup 4}. We point out that the partially comptonized spectral distortions, generated in the redshift range 1.5 × 10{sup 4}∼10{sup 5}, are much richer in information than the pure y and μ-type distortions. The spectrum created during this period is intermediate between y and μ-type distortions and depends sensitively on the redshift of energy injection. These intermediate-type distortions cannot be mimicked by a mixture of y and μ-type distortions at all frequencies and vice versa. The measurement of these intermediate-type CMB spectral distortions has the possibility to constrain precisely not only the amount of energy release in the early Universe but also the mechanism, for example, particle annihilation and Silk damping can be distinguished from particle decay. The intermediate-type distortion templates and software code using these templates to calculate the CMB spectral distortions for user-defined energy injection rate is made publicly available.

  7. Ti12.5Zr21V10Cr8.5MnxCo1.5Ni46.5-x AB2-type metal hydride alloys for electrochemical storage application: Part 2. Hydrogen storage and electrochemical properties

    NASA Astrophysics Data System (ADS)

    Young, K.; Chao, B.; Bendersky, L. A.; Wang, K.

    2012-11-01

    In Part 2 of this report, the hydrogen gas charging and electrochemical properties of a series of AB2-based metal alloys (Ti12.5Zr21V10Cr8.5MnxCo1.5Ni46.5-x) designed to have different fractions of Zr-Ni-type secondary phases by varying the Mn/Ni-content were studied to establish correlations of these properties with abundances of the secondary phases. In the gas charging, the general trend of pressure-concentration-temperature slope factor and hysteresis is to diminish with increase in the Zr7Ni10 phase abundance; the trend of reversible hydrogen storage capacity is to increase as the TiNi-derived AB phase abundance increases. As for the electrochemical properties, the number of activation cycles needed to achieve a given percentage of capacity and power decreases with increase in the total amount of secondary phases. Trends of changes in both the total and reversible capacities follow that in AB phase abundance; the evolution of high-rate dischargeability, bulk diffusion, and surface exchange current is similar to that of Zr7Ni10 phase abundance - increase in the beginning and decrease afterward as the Mn-content in the alloy increases. Other properties, such as metal-hydrogen bond strength and maximum gaseous phase storage capacity, are predominately dependent on the alloys' composition, i.e. the Mn/Ni ratio.

  8. Body Weight Gain During a Discrete Nursing Episode in Suckling Rats Reared at 1.5-g or 1.5-g Exceeds that of 1.0-g Controls and is Independent of Material Hypergravity Exposure

    NASA Technical Reports Server (NTRS)

    Ronca, April E.; Baer, Lisa A.; Plaut, Karen; Wade, Charles E.; Sun, Sid (Technical Monitor)

    2001-01-01

    We recently reported that body weights of suckling rats reared during 1.5-g centrifugation are approximately 10% lower than those of 1.0-g controls. This finding raises the possibility that hypergravity exposed pups ingest less milk than controls due to either impairments in their ability to acquire milk from the nipple, or to decreased availability or palatability of their mother's milk. In the present study, we analyzed body weight gain in suckling rats reared during a discrete nursing episode following rearing at either 1.75-g, 1.5-g or 1.0-g. On Gestational day (G) 10 of the rats' 22-day pregnancy, time-bred SD rat dams were 1:1 matched based on body weight and assigned to either Hypergravity (HG) or Stationary Yoked Control (SYC) conditions and to either 1.75-g or 1.5-g conditions. Beginning on G11, HG dams and litters were exposed to 26 days of continuous centrifugation with brief daily stops for veterinary inspection and animal maintenance. On the day following birth (Postnatal day), litters were pooled within each condition then randomly re-assigned in equivalent proportions to HG and SYC dams. On P15, HG litters were removed from their mother's and placed in an incubator (33 C). Following a 4hr deprivation period, four neonates were tested from each litter, with two pups placed with either their own dam or the SYC dam; two pups from the yoked mother were paired with the HG pups. Pups were individually weighed, permitted to suckle for 75 min, then re-weighed. At the start of the test, the body weights of HG pups were significantly less than those of SYC pups (p less than 0.05). Relative to SYC pups, BG pups showed significantly greater proportional body weight gain (p less than 0.05), possibly due to augmented post-centrifugation feeding. Pup weight gain was independent of maternal hypergravity exposure. Neither impairments in milk acquisition nor milk availability or palatibility of hypergravity-exposed dams cannot account for reduced body mass of

  9. 46 CFR 193.15-10 - Controls.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... EQUIPMENT Carbon Dioxide and Clean Agent Extinguishing Systems, Details § 193.15-10 Controls. (a) Except as... one hazard, a manifold with normally closed stop valves shall be used to direct the carbon dioxide... § 193.15-5(d) which contain not more than 300 pounds of carbon dioxide. (c) One of the...

  10. Effects of dietary glycerin inclusion at 0, 5, 10, and 15 percent of dry matter on energy metabolism and nutrient balance in finishing beef steers

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Expansion of the biodiesel industry has increased the glycerin (GLY) supply. Glycerin is an energy-dense feed that can be used in ruminant species; however, the energy value of GLY is not known. Therefore, the effects of GLY inclusion at 0%, 5%, 10%, and 15% on energy balance in finishing cattle d...

  11. Effects of dietary glycerin inclusion at 0, 5, 10, and 15% of dry matter on energy metabolism and nutrient balance in finishing beef steers

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Expansion of the biodiesel industry has increased the glycerin (GLY) supply. Glycerin is an energy-dense feed that can be used in ruminant species; however, the energy value of GLY is not known. Therefore, the effects of GLY inclusion at 0%, 5%, 10%, and 15% in dry-rolled corn (DRC)-based diets we...

  12. Cleft Lip/Palate, Short Stature, and Developmental Delay in a Boy with a 5.6-Mb Interstitial Deletion Involving 10p15.3p14

    PubMed Central

    Gamba, Bruno F.; Rosenberg, Carla; Costa, Silvia; Richieri-Costa, Antonio; Ribeiro-Bicudo, Lucilene A.

    2015-01-01

    The chromosome interval 10p15.3p14 harbors about a dozen genes. This region has been implicated in a few well-known human phenotypes, namely HDR syndrome (hypoparathyroidism, sensorineural deafness, and renal dysplasia) and DGS2 (DiGeorge syndrome 2), but a number of variable phenotypes have also been reported. Cleft lip/palate seems to be a very unusual finding within the clinical spectrum of patients with this deletion. Here, we report a male child born with short stature, cleft lip/palate, and feeding problems who was found to have a 5.6-Mb deletion at 10p15.3p14. PMID:25852446

  13. Ultrasonic Characterization of Microstructural Changes in Ti-10V-4.5Fe-1.5Al β-Titanium Alloy

    NASA Astrophysics Data System (ADS)

    Viswanath, A.; Kumar, Anish; Jayakumar, T.; Purnachandra Rao, B.

    2015-08-01

    Ultrasonic measurements have been carried out in Ti-10V-4.5Fe-1.5Al β-titanium alloy specimens subjected to β annealing at 1173 K (900 °C) for 1 hour followed by heat treatment in the temperature range of 823 K to 1173 K (550 °C to 900 °C) at an interval of 50 K (50 °C) for 1 hour, followed by water quenching. Ultrasonic parameters such as ultrasonic longitudinal wave velocity, ultrasonic shear wave velocity, shear anisotropy parameter, ultrasonic attenuation, and normalized nonlinear ultrasonic parameter have been correlated with various microstructural changes to understand the interaction of the propagating ultrasonic wave with microstructural features in the alloy. Simulation studies using JMatPro® software and X-ray diffraction measurements have been carried out to estimate the α-phase volume fraction in the specimens heat treated below the β-transus temperature (BTT). It is found that the α-phase (HCP) volume fraction increases from 0 to 52 pct, with decrease in the temperature from 1073 K to 823 K (800 °C to 550 °C). Ultrasonic longitudinal and shear wave velocities are found to increase with decrease in the heat treatment temperature below the BTT, and they exhibited linear relationships with the α-phase volume fraction. Thickness-independent ultrasonic parameters, Poisson's ratio, and the shear anisotropy parameter exhibited the opposite behavior, i.e., decrease with increase in the α-phase consequent to decrease in the heat treatment temperature from 1073 K to 823 K (800 °C to 550 °C). Ultrasonic attenuation is found to decrease from 0.7 dB/mm for the β-annealed specimen to 0.23 dB/mm in the specimen heat treated at 823 K (550 °C) due to the combined effect of the decrease in the β-phase (BCC) with higher damping characteristics and the reduction in scattering due to randomization of β grains with the precipitation of α-phase. Normalized nonlinear ultrasonic parameter is found to increase with increase in the α-phase volume fraction

  14. Granular superconductivity in polycrystalline ruthenocuprate RuSr2(Gd1.5Ce0.5)Cu2O10-δ: magnetoresistive and magnetization studies

    NASA Astrophysics Data System (ADS)

    Belevtsev, B. I.; Beliayev, E. Yu; Naugle, D. G.; Rathnayaka, K. D. D.; Anatska, M. P.; Felner, I.

    2007-01-01

    Granular superconductivity effects in polycrystalline samples of RuSr2(Gd1.5Ce0.5)Cu2O10-δ, as prepared (by a solid-state reaction method) and annealed (12 h at 845 °C) in pure oxygen at 30 atm, are presented. The resistive transition to the superconducting state of the as-prepared sample is found to be considerably affected by granularity. In particular, an evident kink in the temperature dependence of the resistance R(T) is seen at the temperature, Tc0ap34 K, at which grains become superconducting. The resistive transition depends strongly on the applied current. The family of R(T) curves taken for different transport currents is branched with a branching point at TcJap23.2 K. Below this temperature the intergrain Josephson coupling starts to develop. For low current, R decreases with decreasing temperature below TcJ as expected for the transition to the superconducting state, whereas R(T) curves for higher current form a minimum at Tap17.3 K, showing a quasi-re-entrant behaviour. The influence of the granular structure of the as-prepared sample shows itself also in the temperature behaviour of the magnetization, M(T), in low field. Application of low magnetic field (below 400 Oe) leads to a broadening of the resistive transitions below TcJ, similar to that caused by increasing the current. Both the current and magnetic field depress the Josephson coupling between the grains, producing a dramatically large effect on the resistive transition. The R(T) and M(T) dependences of the annealed sample show a fairly sharp superconducting transition far less affected by granularity. The results obtained imply that oxygen annealing improves the intergranular connection considerably, but it does not exert much influence on the intragrain superconductivity. No indication of intragrain granularity has been found in the samples studied. The influence of ageing (due to deoxidation) of samples for different conditions of storage is considered briefly as well.

  15. Multilayer thin films with compositional PbZr0.52Ti0.48O3/Bi1.5Zn1.0Nb1.5O7 layers for tunable applications.

    PubMed

    Yu, Shihui; Li, Lingxia; Zhang, Weifeng; Sun, Zheng; Dong, Helei

    2015-01-01

    The dielectric properties and tunability of multilayer thin films with compositional PbZr0.52Ti0.48O3/Bi1.5Zn1.0Nb1.5O7 (PZT/BZN) layers (PPBLs) fabricated by pulsed laser deposition on Pt/TiO2/SiO2/Si substrate have been investigated. Dielectric measurements indicate that the PZT/BZN bilayer thin films exhibit medium dielectric constant of about 490, low loss tangent of 0.017, and superior tunable dielectric properties (tunability=49.7% at 500 kV/cm) at a PZT/BZN thickness ratio of 3, while the largest figure of merit is obtained as 51.8. The thickness effect is discussed with a series connection model of bilayer capacitors, and the calculated dielectric constant and loss tangent are obtained. Furthermore, five kinds of thin-film samples comprising single bilayers, two, three, four and five PPBLs were also elaborated with the final same thickness. The four PPBLs show the largest dielectric constant of ~538 and tunability of 53.3% at a maximum applied bias field of 500 kV/cm and the lowest loss tangent of ~0.015, while the largest figure of merit is 65.6. The results indicate that four PPBLs are excellent candidates for applications of tunable devices. PMID:25960043

  16. Multilayer thin films with compositional PbZr0.52Ti0.48O3/Bi1.5Zn1.0Nb1.5O7 layers for tunable applications

    PubMed Central

    Yu, Shihui; Li, Lingxia; Zhang, Weifeng; Sun, Zheng; Dong, Helei

    2015-01-01

    The dielectric properties and tunability of multilayer thin films with compositional PbZr0.52Ti0.48O3/Bi1.5Zn1.0Nb1.5O7 (PZT/BZN) layers (PPBLs) fabricated by pulsed laser deposition on Pt/TiO2/SiO2/Si substrate have been investigated. Dielectric measurements indicate that the PZT/BZN bilayer thin films exhibit medium dielectric constant of about 490, low loss tangent of 0.017, and superior tunable dielectric properties (tunability = 49.7% at 500 kV/cm) at a PZT/BZN thickness ratio of 3, while the largest figure of merit is obtained as 51.8. The thickness effect is discussed with a series connection model of bilayer capacitors, and the calculated dielectric constant and loss tangent are obtained. Furthermore, five kinds of thin–film samples comprising single bilayers, two, three, four and five PPBLs were also elaborated with the final same thickness. The four PPBLs show the largest dielectric constant of ~538 and tunability of 53.3% at a maximum applied bias field of 500 kV/cm and the lowest loss tangent of ~0.015, while the largest figure of merit is 65.6. The results indicate that four PPBLs are excellent candidates for applications of tunable devices. PMID:25960043

  17. Multilayer thin films with compositional PbZr0.52Ti0.48O3/Bi1.5Zn1.0Nb1.5O7 layers for tunable applications

    NASA Astrophysics Data System (ADS)

    Yu, Shihui; Li, Lingxia; Zhang, Weifeng; Sun, Zheng; Dong, Helei

    2015-05-01

    The dielectric properties and tunability of multilayer thin films with compositional PbZr0.52Ti0.48O3/Bi1.5Zn1.0Nb1.5O7 (PZT/BZN) layers (PPBLs) fabricated by pulsed laser deposition on Pt/TiO2/SiO2/Si substrate have been investigated. Dielectric measurements indicate that the PZT/BZN bilayer thin films exhibit medium dielectric constant of about 490, low loss tangent of 0.017, and superior tunable dielectric properties (tunability = 49.7% at 500 kV/cm) at a PZT/BZN thickness ratio of 3, while the largest figure of merit is obtained as 51.8. The thickness effect is discussed with a series connection model of bilayer capacitors, and the calculated dielectric constant and loss tangent are obtained. Furthermore, five kinds of thin-film samples comprising single bilayers, two, three, four and five PPBLs were also elaborated with the final same thickness. The four PPBLs show the largest dielectric constant of ~538 and tunability of 53.3% at a maximum applied bias field of 500 kV/cm and the lowest loss tangent of ~0.015, while the largest figure of merit is 65.6. The results indicate that four PPBLs are excellent candidates for applications of tunable devices.

  18. 43 CFR 15.5 - Wrecks.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 43 Public Lands: Interior 1 2010-10-01 2010-10-01 false Wrecks. 15.5 Section 15.5 Public Lands: Interior Office of the Secretary of the Interior KEY LARGO CORAL REEF PRESERVE § 15.5 Wrecks. No person shall willfully destroy molest, remove, deface, displace, or tamper with any wrecks, parts of wrecks or any cargo pertaining to such wrecks...

  19. 15 CFR 734.10 - Patent applications.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... and Trademark Office, 37 CFR part 5; 1 or 1 Regulations issued by the Patent and Trademark Office in 37 CFR part 5 provide for the export to a foreign country of unclassified technical data in the form... 15 Commerce and Foreign Trade 2 2012-01-01 2012-01-01 false Patent applications. 734.10...

  20. 15 CFR 734.10 - Patent applications.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... and Trademark Office, 37 CFR part 5; 1 or 1 Regulations issued by the Patent and Trademark Office in 37 CFR part 5 provide for the export to a foreign country of unclassified technical data in the form... 15 Commerce and Foreign Trade 2 2011-01-01 2011-01-01 false Patent applications. 734.10...

  1. 15 CFR 734.10 - Patent applications.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... and Trademark Office, 37 CFR part 5; 1 or 1 Regulations issued by the Patent and Trademark Office in 37 CFR part 5 provide for the export to a foreign country of unclassified technical data in the form... 15 Commerce and Foreign Trade 2 2014-01-01 2014-01-01 false Patent applications. 734.10...

  2. 15 CFR 734.10 - Patent applications.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... and Trademark Office, 37 CFR part 5; 1 or 1 Regulations issued by the Patent and Trademark Office in 37 CFR part 5 provide for the export to a foreign country of unclassified technical data in the form... 15 Commerce and Foreign Trade 2 2010-01-01 2010-01-01 false Patent applications. 734.10...

  3. 15 CFR 734.10 - Patent applications.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... and Trademark Office, 37 CFR part 5; 1 or 1 Regulations issued by the Patent and Trademark Office in 37 CFR part 5 provide for the export to a foreign country of unclassified technical data in the form... 15 Commerce and Foreign Trade 2 2013-01-01 2013-01-01 false Patent applications. 734.10...

  4. The Effect of Aging Heat Treatment on the Microstructure and Mechanical Properties of 10Cr20Ni25Mo1.5NbN Austenitic Steel

    NASA Astrophysics Data System (ADS)

    Liang, Zhiyuan; Sha, Wanhua; Zhao, Qinxin; Wang, Chongbin; Wang, Jianyong; Jiang, Weiwei

    2016-01-01

    The effect of aging heat treatment on the microstructure and mechanical properties of 10Cr20Ni25Mo1.5NbN austenitic steel was investigated in this article. The microstructure was characterized by scanning electron microscopy, energy dispersive spectrometry and transmission electron microscopy. Results show that the microstructure of 10Cr20Ni25Mo1.5NbN austenitic is composed of austenite. This steel was strengthened by precipitates of secondary phases that were mainly M23C6 carbides and NbCrN nitrides. As aging treatment time increased, the tensile strength first rose (0-3,000 h) and then fell (3,000-5,000 h) due to the decrease of high density of dislocations. The impact absorbed energy decreased sharply, causing the sulfides to precipitate at the grain boundary. Therefore, the content of sulfur should be strictly controlled in the steelmaking process.

  5. 46 CFR 194.15-5 - Ventilation.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 7 2011-10-01 2011-10-01 false Ventilation. 194.15-5 Section 194.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS HANDLING, USE, AND CONTROL OF EXPLOSIVES AND OTHER HAZARDOUS MATERIALS Chemistry Laboratory and Scientific Laboratory §...

  6. 46 CFR 194.15-5 - Ventilation.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 7 2014-10-01 2014-10-01 false Ventilation. 194.15-5 Section 194.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS HANDLING, USE, AND CONTROL OF EXPLOSIVES AND OTHER HAZARDOUS MATERIALS Chemistry Laboratory and Scientific Laboratory §...

  7. 46 CFR 194.15-5 - Ventilation.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 7 2012-10-01 2012-10-01 false Ventilation. 194.15-5 Section 194.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS HANDLING, USE, AND CONTROL OF EXPLOSIVES AND OTHER HAZARDOUS MATERIALS Chemistry Laboratory and Scientific Laboratory §...

  8. 46 CFR 194.15-5 - Ventilation.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 7 2013-10-01 2013-10-01 false Ventilation. 194.15-5 Section 194.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS HANDLING, USE, AND CONTROL OF EXPLOSIVES AND OTHER HAZARDOUS MATERIALS Chemistry Laboratory and Scientific Laboratory §...

  9. 46 CFR 194.15-5 - Ventilation.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 7 2010-10-01 2010-10-01 false Ventilation. 194.15-5 Section 194.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS HANDLING, USE, AND CONTROL OF EXPLOSIVES AND OTHER HAZARDOUS MATERIALS Chemistry Laboratory and Scientific Laboratory §...

  10. Effect of annealing temperature of Bi1.5Zn1.0Nb1.5O7 gate insulator on performance of ZnO based thin film transistors

    NASA Astrophysics Data System (ADS)

    Wei, Ye; Wei, Ren; Peng, Shi; Zhuangde, Jiang

    2016-07-01

    The bottom-gate structure ZnO based thin film transistors (ZnO-TFTs) using Bi1.5Zn1.0Nb1.5O7 (BZN) thin films as gate insulator were fabricated on Pt/SiO2/Si substrate by radio frequency magnetic sputtering. We investigated the effect of annealing temperature at 300, 400, and 500 °C on the performance of BZN thin films and ZnO-TFTs. XRD measurement confirmed that BZN thin films were amorphous in nature. BZN thin films annealed at 400 °C obtain the high capacitance density of 249 nF/cm2, high dielectric constant of 71, and low leakage current density of 10‑7 A/cm2 on/off current ratio and field effect mobility of ZnO-TFTs annealed at 400 °C are approximately one order of magnitude and two times, respectively higher than that of ZnO-TFTs annealed at 300 °C. When the annealing temperature is 400 °C, the electrical performance of ZnO-TFTs is enhanced remarkably. Devices obtain a low sub-threshold swing of 470 mV/dec and surface states density of 3.21 × 1012cm‑2. Project supported by the National Natural Science Foundation of China (Nos. 51332003, 51202184), the International Science & Technology Cooperation Program of China (Nos. 2010DFB13640, 2011DFA51880), and the “111 Project” of China (No. B14040).

  11. D5h [PhSiO1.5]10 synthesis via F(-) catalyzed rearrangement of [PhSiO1.5]n. An experimental/computational analysis of likely reaction pathways.

    PubMed

    Furgal, Joseph C; Goodson, Theodore; Laine, Richard M

    2016-01-21

    We describe here the synthesis and analysis of the reaction pathways leading to formation of the rare D5h decaphenylsilsesquioxane (SQ) [PhSiO1.5]10via F(-) catalyzed rearrangement of [PhSiO1.5]nn = 8, 12, and oligomers initially synthesized from PhSi(OEt)3. Isolated yields of ∼50% [PhSiO1.5]10 are obtained via rearrangement of all starting materials. The recovered starting materials can be re-equilibrated using catalytic F(-) to generate similar yields in second batches. These yields arise because [PhSiO1.5]10 exhibits higher solubility and better energy stabilization (10 kcal mol(-1) theory) in CH2Cl2 compared to [PhSiO1.5]8 or [PhSiO1.5]12. Reaction intermediates were identified using time dependent (19)F NMR and MALDI-ToF mass spectrometry eventually equilibrating to form the 8 : 10 : 12 cages in a 1 : 3 : 1.3 equilibrium in CH2Cl2. Experimental results coupled with modeling using the Gamess computational package provide multiple reasonable pathways for SQ rearrangements to [RSiO1.5]10, starting from [RSiO1.5]8. Heats of reaction for interconversion of the model intermediates [HSiO1.5]x determined computationally, were used to select the most reasonable reaction pathways. The findings support a mechanism involving activation and cleavage of a T8 cage corner by F(-) attachment, followed by the corners stepwise removal as [i.e. RSi(OH)3], followed thereafter by reinsertion forming [RSiO1.5]9-OH followed by, insertion of another corner to form [RSiO1.5]10-(OH)2 and finally condensation to give [RSiO1.5]10. The most enthalpically favorable path (-24 kcal mol(-1)) involves a hybrid mechanism. PMID:26648403

  12. 46 CFR 193.15-10 - Controls.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 7 2012-10-01 2012-10-01 false Controls. 193.15-10 Section 193.15-10 Shipping COAST... EQUIPMENT Carbon Dioxide and Clean Agent Extinguishing Systems, Details § 193.15-10 Controls. (a) Except as noted in § 193.15-20(b), all controls and valves for the operation of the system shall be outside...

  13. 46 CFR 193.15-10 - Controls.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 7 2013-10-01 2013-10-01 false Controls. 193.15-10 Section 193.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS FIRE PROTECTION EQUIPMENT Carbon Dioxide and Clean Agent Extinguishing Systems, Details § 193.15-10 Controls. (a) Except as noted in § 193.15-20(b), all controls...

  14. Synthesis and unusual properties of the first 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraalkylporphyrin

    SciTech Connect

    NELSON,NORA Y.; MEDFORTH,CRAIG J.; NURCO,DANIEL J.; JIA,SONG-LING; SHELNUTT,JOHN A.; SMITH,KEVIN M.

    2000-03-06

    The new perhalogenated porphyrin 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(trifluoromethyl)porphinato-nickel(II) exhibits several striking features, including an extremely ruffled macrocycle with a very short Ni-N distance, an unusually red-shifted optical spectrum, and, surprisingly, hindered rotation of the meso-trifluoromethyl substituents ({Delta}G{sub 278}{sup +} = 47 kJ/mol).

  15. 15 CFR 5.5 - Vending machines.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 15 Commerce and Foreign Trade 1 2012-01-01 2012-01-01 false Vending machines. 5.5 Section 5.5... machines. (a) The income from any vending machines which are located within reasonable proximity to and are... shall be assigned to the operator of such stand. (b) If a vending machine vends articles of a...

  16. 15 CFR 5.5 - Vending machines.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 15 Commerce and Foreign Trade 1 2013-01-01 2013-01-01 false Vending machines. 5.5 Section 5.5... machines. (a) The income from any vending machines which are located within reasonable proximity to and are... shall be assigned to the operator of such stand. (b) If a vending machine vends articles of a...

  17. 15 CFR 5.5 - Vending machines.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 1 2010-01-01 2010-01-01 false Vending machines. 5.5 Section 5.5... machines. (a) The income from any vending machines which are located within reasonable proximity to and are... shall be assigned to the operator of such stand. (b) If a vending machine vends articles of a...

  18. 15 CFR 5.5 - Vending machines.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 15 Commerce and Foreign Trade 1 2014-01-01 2014-01-01 false Vending machines. 5.5 Section 5.5... machines. (a) The income from any vending machines which are located within reasonable proximity to and are... shall be assigned to the operator of such stand. (b) If a vending machine vends articles of a...

  19. 15 CFR 5.5 - Vending machines.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 1 2011-01-01 2011-01-01 false Vending machines. 5.5 Section 5.5... machines. (a) The income from any vending machines which are located within reasonable proximity to and are... shall be assigned to the operator of such stand. (b) If a vending machine vends articles of a...

  20. Plasmid profiles of drug resistant Shigella boydii types 1-5, 8, 10, 12-14 from Ethiopia (1974-85).

    PubMed Central

    Gebre-Yohannes, A.; Drasar, B. S.

    1997-01-01

    Plasmid profile analysis by agarose gel electrophoresis was performed on 42 drug resistant strains of Shigella boydii serotypes 1-5, 8, 10, 12-14, collected between 1974 and 1985 from endemic cases of shigellosis in Ethiopia, and their Escherichia coli K12 transconjugants. Resistance factors (R factors) were further characterized by incompatibility testing. Patterns of small plasmids, less than 15 kb, were similar within each of the individual S. boydii serotypes. Plasmids of about 3.3-3.7 kb were found in all strains of serotypes 2 and 4. Plasmids of about 4.3-4.6 kb were found in about 86% of strains. Serotypes 1, 2 and 3 were characterized by plasmids of about 5.6-5.7 kb. The 6.4-6.7 kb plasmid was found consistently in serotypes 1, 2, 3, 5, 8, 12 and 13 which were resistant to SSu or had an SSu resistance component in their phenotypes. Large plasmids (155-186 kb) were found in most S. boydii strains. Conjugative drug resistance plasmids, most often coding for three or less drugs, were found in about 26% of drug resistant strains. R-factors, coding for AT resistance (in types 2 and 8), and ASSuT resistance (in type 4), were compatible with all reference plasmids tested. Plasmids belonging to incompatibility groups X and N were found in serotypes 5 and 10, respectively. PMID:9440431

  1. 46 CFR 168.15-10 - Construction.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 7 2012-10-01 2012-10-01 false Construction. 168.15-10 Section 168.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS CIVILIAN NAUTICAL SCHOOL VESSELS Accommodations § 168.15-10 Construction. (a) The accommodations provided must be securely constructed,...

  2. 46 CFR 168.15-10 - Construction.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 7 2013-10-01 2013-10-01 false Construction. 168.15-10 Section 168.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS CIVILIAN NAUTICAL SCHOOL VESSELS Accommodations § 168.15-10 Construction. (a) The accommodations provided must be securely constructed,...

  3. 46 CFR 168.15-10 - Construction.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 7 2014-10-01 2014-10-01 false Construction. 168.15-10 Section 168.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS CIVILIAN NAUTICAL SCHOOL VESSELS Accommodations § 168.15-10 Construction. (a) The accommodations provided must be securely constructed,...

  4. 46 CFR 168.15-10 - Construction.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 7 2010-10-01 2010-10-01 false Construction. 168.15-10 Section 168.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS CIVILIAN NAUTICAL SCHOOL VESSELS Accommodations § 168.15-10 Construction. (a) The accommodations provided must be securely constructed,...

  5. 46 CFR 168.15-10 - Construction.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 7 2011-10-01 2011-10-01 false Construction. 168.15-10 Section 168.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS CIVILIAN NAUTICAL SCHOOL VESSELS Accommodations § 168.15-10 Construction. (a) The accommodations provided must be securely constructed,...

  6. 46 CFR 196.15-10 - Sanitation.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 7 2010-10-01 2010-10-01 false Sanitation. 196.15-10 Section 196.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS OPERATIONS Test, Drills, and Inspections § 196.15-10 Sanitation. (a) It shall be the duty of the master and chief engineer to see that the vessel, and, in...

  7. 46 CFR 76.10-15 - Piping.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 3 2010-10-01 2010-10-01 false Piping. 76.10-15 Section 76.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) PASSENGER VESSELS FIRE PROTECTION EQUIPMENT Fire Main System, Details § 76.10-15 Piping. (a) All piping, valves, and fittings shall meet the applicable requirements...

  8. 46 CFR 95.10-15 - Piping.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Piping. 95.10-15 Section 95.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS FIRE PROTECTION EQUIPMENT Fire Main System, Details § 95.10-15 Piping. (a) All piping, valves, and fittings shall meet the...

  9. 46 CFR 193.10-15 - Piping.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 7 2011-10-01 2011-10-01 false Piping. 193.10-15 Section 193.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS FIRE PROTECTION EQUIPMENT Fire Main System, Details § 193.10-15 Piping. (a) All piping, valves, and fittings, shall meet...

  10. 46 CFR 42.15-10 - Doors.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 2 2013-10-01 2013-10-01 false Doors. 42.15-10 Section 42.15-10 Shipping COAST GUARD... Assignment of Freeboard § 42.15-10 Doors. (a) All access openings in bulkheads at ends of enclosed superstructures shall be fitted with doors of steel or other equivalent material, permanently and...

  11. 46 CFR 42.15-10 - Doors.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 2 2014-10-01 2014-10-01 false Doors. 42.15-10 Section 42.15-10 Shipping COAST GUARD... Assignment of Freeboard § 42.15-10 Doors. (a) All access openings in bulkheads at ends of enclosed superstructures shall be fitted with doors of steel or other equivalent material, permanently and...

  12. 46 CFR 42.15-10 - Doors.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 2 2012-10-01 2012-10-01 false Doors. 42.15-10 Section 42.15-10 Shipping COAST GUARD... Assignment of Freeboard § 42.15-10 Doors. (a) All access openings in bulkheads at ends of enclosed superstructures shall be fitted with doors of steel or other equivalent material, permanently and...

  13. 46 CFR 42.15-10 - Doors.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 2 2010-10-01 2010-10-01 false Doors. 42.15-10 Section 42.15-10 Shipping COAST GUARD... Assignment of Freeboard § 42.15-10 Doors. (a) All access openings in bulkheads at ends of enclosed superstructures shall be fitted with doors of steel or other equivalent material, permanently and...

  14. 46 CFR 42.15-10 - Doors.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 2 2011-10-01 2011-10-01 false Doors. 42.15-10 Section 42.15-10 Shipping COAST GUARD... Assignment of Freeboard § 42.15-10 Doors. (a) All access openings in bulkheads at ends of enclosed superstructures shall be fitted with doors of steel or other equivalent material, permanently and...

  15. A direct sensitized fluorimetric determination of 5,10,15,20-tetra(m-hydroxyphenyl)chlorin [m-THPC (Foscan)] in human plasma using a cyclodextrin inclusion complex.

    PubMed

    Desroches, M C; Kasselouri, A; Bourdon, O; Chaminade, P; Blais, J; Prognon, P

    2001-06-01

    The 5,10,15,20-tetra(m-hydroxyphenyl)chlorin (m-THPC) (Foscan) is a photosensitizer used in the photodynamic therapy (PDT) of cancers which is currently under clinical trial. The formation of a m-THPC inclusion complex with dimethyl-beta-cyclodextrin (Me-beta-CD) in solution was demonstrated on the basis of circular dichroism experiments. A 1:2 complex stoichiometry was found and an inclusion constant beta 2 = 2.8(+/- 0.4) x 10(10) M-2 was determined. The formation of such a complex was shown to enhance the m-THPC fluorescence intensity. It could be exploited to improve the sensitivity of the direct m-THPC detection in human plasma. Optimization of the operating conditions shows that the best results were obtained by the addition of 100 microL of a concentrated Me-beta-CD solution (3.2 x 10(-2) M) to 1 mL plasma samples. Compared to the standard conditions, a 90% increase in sensitivity was obtained. The proposed analytical method which showed a linear response function [0-300 ng mL-1 (440 pM)] and a low limit of detection [1.5 ng mL-1 (2 pM) (S/N = 3)] appears, especially due to the absence of metabolism, a simple and specific method suitable for pharmacokinetics studies in patients. PMID:11445963

  16. 46 CFR 151.10-15 - Certificate endorsement.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 5 2012-10-01 2012-10-01 false Certificate endorsement. 151.10-15 Section 151.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CERTAIN BULK DANGEROUS CARGOES BARGES CARRYING BULK LIQUID HAZARDOUS MATERIAL CARGOES Barge Hull Construction Requirements § 151.10-15 Certificate endorsement. (a)-(b) (c)...

  17. Application of an octa-anionic 5,10,15,20-tetra[3,5-(nido-carboranylmethyl)phenyl]porphyrin (H2OCP) as dual sensitizer for BNCT and PDT

    Technology Transfer Automated Retrieval System (TEKTRAN)

    The applications of the octa-anionic 5,10,15,20-tetra[3,5-(nidocarboranylmethyl) phenyl]porphyrin (H2OCP) as a boron delivery agent in boron neutron capture therapy (BNCT) and a photosensitizer in photodynamic therapy (PDT) have been investigated. Using F98 Rat glioma cells, we evaluated the cytotox...

  18. Molecular binding behaviors of pyromellitic and naphthalene diimide derivatives by tetrasulfonated 1,5-dinaphtho-(3n+8)-crown-n (n = 8, 10) in aqueous solution.

    PubMed

    Chen, Ling; Zhang, Ying-Ming; Wang, Li-Hua; Liu, Yu

    2013-06-01

    The highly affinitive and selective binding processes of tetrasulfonated 1,5-dinaphtho-38-crown-10 (1(4-)) and tetrasulfonated 1,5-dinaphtho-32-crown-8 (2(4-)) with pyromellitic diimide and naphthalene diimide derivatives bearing cationic terminal groups (PMDI(2+) and NDI(2+)) are comprehensively investigated in aqueous solution by (1)H NMR and UV/vis experiments, mass spectrometry, microcalorimetric titration, and crystallographic analysis. The binding process of host-guest complexation is thermodynamically driven by the large enthalpic gain and favorable entropic change with the high association constants in the range of 10(4)-10(6) M(-1) order of magnitude. Combined with our previously reported thermodynamic data of ethyl viologen (EV(2+)), it is found that the exclusively selective binding behaviors originate from the size/shape matching effect, as well as the electrostatic interaction between negatively charged hosts and positively charged guests and aromatic π-stacking interrelation between electron-rich donors and electron-deficient acceptors. PMID:23638773

  19. 46 CFR 95.15-10 - Controls.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false Controls. 95.15-10 Section 95.15-10 Shipping COAST GUARD... Dioxide Extinguishing Systems, Details § 95.15-10 Controls. (a) Except as noted in § 95.15-20(b) all controls and valves for the operation of the system shall be outside the space protected, and shall not...

  20. 46 CFR 95.15-10 - Controls.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false Controls. 95.15-10 Section 95.15-10 Shipping COAST GUARD... Dioxide Extinguishing Systems, Details § 95.15-10 Controls. (a) Except as noted in § 95.15-20(b) all controls and valves for the operation of the system shall be outside the space protected, and shall not...

  1. 46 CFR 95.15-10 - Controls.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Controls. 95.15-10 Section 95.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS FIRE PROTECTION EQUIPMENT Carbon Dioxide Extinguishing Systems, Details § 95.15-10 Controls. (a) Except as noted in § 95.15-20(b) all controls and valves for the...

  2. Dichloro (1,10-phenanthroline-5,6-dione) palladium (II) complex supported by mesoporous silica SBA-15 as a photocatalyst for degradation of 2,4-dichlorophenol

    NASA Astrophysics Data System (ADS)

    Abolhosseini Sh., A.; Mahjoub, A. R.; Eslami-Moghadam, M.; Fakhri, H.

    2014-11-01

    A new photocatalyst, dichloro (1,10-phenanthroline-5,6-dione) palladium (II) complex supported on SBA-15 silica was synthesized by ship-in-a-bottle method. The products obtained were characterized by X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), Ultraviolet-Visible spectroscopy (UV-Vis), 1H NMR spectroscopy, N2 adsorption-desorption and inductively coupled plasma atomic emission spectroscopy (ICP-AES). The band gap energy of the complex was determined by the diffuse reflectance spectroscopy (DRS) and density functional theory (DFT) calculation, indicating that it can be considered appropriate candidate for photocatalytic activity in the region of solar spectrum. The results indicated improved photocatalytic efficiency for the complex supported on SBA-15 silica compared to the pure complex. To improve photocatalytic activity, the effect of complex loading and optimal synthesis conditions were investigated.

  3. Advances in Classification Research. Volume 10. Proceedings of the ASIS SIG/CR Classification Research Workshop (10th, Washington, DC, November 1-5, 1999). ASIST Monograph Series.

    ERIC Educational Resources Information Center

    Albrechtsen, Hanne, Ed.; Mai, Jens-Erik, Ed.

    This volume is a compilation of the papers presented at the 10th ASIS (American Society for Information Science) workshop on classification research. Major themes include the social and cultural informatics of classification and coding systems, subject access and indexing theory, genre analysis and the agency of documents in the ordering of…

  4. Early lung cancer detection project: Evaluation of 5, 10, 15, 20 tetrakis (4-carboxyphenyl) porphine (H{sub 2}TCPP). Final report

    SciTech Connect

    Tockman, M.S.

    1998-10-01

    The author evaluated a synthetic porphyrin, 5, 10, 15, 20 tetrakis (4-carboxyphenyl) porphene (H{sub 2}TCPP) as a marker of carcinogenesis. H{sub 2}TCPP was compared with two other carcinogenesis markers evaluated in the laboratory for their ability to detect exfoliated sputum cells undergoing transformation to lung cancer. In the present project the authors first established optimal conditions for cultured neoplastic and non-neoplastic (sputum) cells to take up H{sub 2}TCPP. This was accomplished using spectrofluorimetry and video-enhanced fluorescent microscopy to maximize H{sub 2}TCPP auto-fluorescence across a matrix of substrate conditions, including; reagent concentration, incubation time, temperature, and pH. The second aim was to validate H{sub 2}TCPP on clinical material obtained from subjects monitored in advance of clinical cancer and link those marker results with subsequent histologic confirmation of disease. This was accomplished by applying H{sub 2}TCPP to sputum specimens archived by the Frost Center at Johns Hopkins which maintains a record of the clinical course and long-term follow-up for the patients from whom the specimens were obtained. The authors have used fluorescent immunostaining and flow cytometry to compare uptake of these cytoplasmic Mabs to that of a potential new marker of carcinogenesis, 5, 10, 15, 20 tetrakis (4 carboxyphenyl) porphene (H{sub 2}TCPP). The nuclear uptake of H{sub 2}TCPP was compared to a standard quantitative fluorescent DNA marker (7-AAD).

  5. Photophysical Characterization and in Vitro Phototoxicity Evaluation of 5,10,15,20-Tetra(quinolin-2-yl)porphyrin as a Potential Sensitizer for Photodynamic Therapy.

    PubMed

    Costa, Letícia D; e Silva, Joana de A; Fonseca, Sofia M; Arranja, Cláudia T; Urbano, Ana M; Sobral, Abilio J F N

    2016-01-01

    Photodynamic therapy (PDT) is a selective and minimally invasive therapeutic approach, involving the combination of a light-sensitive compound, called a photosensitizer (PS), visible light and molecular oxygen. The interaction of these per se harmless agents results in the production of reactive species. This triggers a series of cellular events that culminate in the selective destruction of cancer cells, inside which the photosensitizer preferentially accumulates. The search for ideal PDT photosensitizers has been a very active field of research, with a special focus on porphyrins and porphyrin-related macrocycle molecules. The present study describes the photophysical characterization and in vitro phototoxicity evaluation of 5,10,15,20-tetra(quinolin-2-yl)porphyrin (2-TQP) as a potential PDT photosensitizer. Molar absorption coefficients were determined from the corresponding absorption spectrum, the fluorescence quantum yield was calculated using 5,10,15,20-tetraphenylporphyrin (TPP) as a standard and the quantum yield of singlet oxygen generation was determined by direct phosphorescence measurements. Toxicity evaluations (in the presence and absence of irradiation) were performed against HT29 colorectal adenocarcinoma cancer cells. The results from this preliminary study show that the hydrophobic 2-TQP fulfills several critical requirements for a good PDT photosensitizer, namely a high quantum yield of singlet oxygen generation (Φ∆ 0.62), absence of dark toxicity and significant in vitro phototoxicity for concentrations in the micromolar range. PMID:27043519

  6. NiO nanoparticles modified with 5,10,15,20-tetrakis(4-carboxyl pheyl)-porphyrin: promising peroxidase mimetics for H2O2 and glucose detection.

    PubMed

    Liu, Qingyun; Yang, Yanting; Li, Hui; Zhu, Renren; Shao, Qian; Yang, Shanguang; Xu, Jingjing

    2015-02-15

    NiO nanoparticles (NPs) and 5,10,15,20-tetrakis(4-carboxyl pheyl)-porphyrin (H2TCPP) functionalized NiO nanoparticles (H2TCPP-NiO nanocomposites) have been prepared by a facile method and characterized by powder X-ray diffraction (XRD), transmission electron microscope (TEM) and Fourier transform infrared spectra (FTIR), respectively. NiO NPs and H2TCPP-NiO nanocomposites have been proven to function as peroxidase mimetics that can catalyze the reaction of peroxidase substrate 3,3',5,5'-tetramethylbenzidine (TMB) in the presence of H2O2 to produce a blue color reaction. Kinetic analysis indicated that the catalytic behavior was in accord with typical Michaelis-Menten kinetics. And these nanoparticles also exhibited strong affinity for the substrates of 3,3,5,5-tetramethylbiphenyl dihydrochloride (TMB). Experimental results showed that H2TCPP-NiO NPs exhibited a high sensitivity and a low detection limit towards H2O2 (8.0 × 10(-6) M). The H2TCPP-NiO NPs/glucose oxidase (GOx)/TMB system provides a novel colorimetric sensor for glucose and shows good response toward glucose detection over arrange of 0.05-0.50 mM with a limit of detection 2.0 × 10(-5)M. Fluorescence probe experiments demonstrated that the peroxidase-like activity of H2TCPP-NiO NPs originated from the generation of OH radical. Thus it may provide great potential applications in biomedicine, biotechnology and environmental chemistry. PMID:25212068

  7. Synthesis and properties of 5,10,15,20-tetrakis[4-(3-N,N-dimethylaminopropoxy)phenyl] chlorin as potential broad-spectrum antimicrobial photosensitizers.

    PubMed

    Ferreyra, Darío D; Reynoso, Eugenia; Cordero, Paula; Spesia, Mariana B; Alvarez, M Gabriela; Milanesio, M Elisa; Durantini, Edgardo N

    2016-05-01

    A novel 5,10,15,20-tetrakis[4-(3-N,N-dimethylaminopropoxy)phenyl]chlorin (TAPC) was synthesized by reduction of the corresponding porphyrin TAPP with p-toluenesulfonhydrazide, followed by selective oxidation with o-chloranil. Spectroscopic properties and the photodynamic activity of these photosensitizers were compared in N,N-dimethylformamide. An increase in the absorption band at 650nm was found for the chlorin derivative with respect to TAPP. These photosensitizers emit red fluorescence with quantum yields of 0.15. Both compounds were able to photosensitize singlet molecular oxygen with quantum yields of about 0.5. Also, the formation of superoxide anion radical was detected in the presence of TAPC or TAPP and NADH. Photodynamic inactivation was investigated on a Gram-positive bacterium Staphylococcus aureus, a Gram-negative bacterium Escherichia coli and a fungal yeast Candida albicans cells. In vitro experiments showed that TAPC or TAPP were rapidly bound to microbial cells at short incubation periods. These photosensitizers, without intrinsic positive charges, contain four basic amino groups. These substituents can be protonated at physiological pH, increasing the interaction with the cell envelopment. Photosensitized inactivation improved with an increase of both photosensitizer concentrations and irradiation times. After 15min irradiation, a 7 log reduction of S. aureus was found for treated with 1μM photosensitizer. Similar result was obtained with E. coli after using 5μM photosensitizer and 30min irradiation. Also, the last conditions produced a decrease of 5 log in C. albicans cells. Therefore, TAPC was highly effective as a broad-spectrum antimicrobial photosensitizer. PMID:26994333

  8. 46 CFR 97.15-10 - Sanitation.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Sanitation. 97.15-10 Section 97.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS OPERATIONS Tests, Drills, and Inspections § 97.15-10 Sanitation. (a) It shall be the duty of the master and chief engineer to see that the vessel, and, in particular,...

  9. 1.5-μm and 10-Gb s-1 etched mesa buried heterostructure DFB-LD for datacenter networks

    NASA Astrophysics Data System (ADS)

    Kwon, Oh Kee; Lee, Chul Wook; Leem, Young Ahn; Kim, Ki Soo; Oh, Su Hwan; Nam, Eun Soo

    2015-10-01

    We report a 1.5 μm and 10 Gb s-1 etched mesa buried heterostructure λ/4-shifted distributed feedback laser diode (DFB-LD) for the low-cost application of WDM-based datacenter networks. To reduce the threshold current and improve the modulation bandwidth in a conventional p-/n-/p-InP current blocking structure, a thin undoped-InP (u-InP) layer was inserted between the side walls of the active region and the p-InP layer (i.e., a u-/p-/n-/p-InP structure), and the region containing the active region and the current blocking structures was etched in a mesa form (i.e., an etched mesa). From this work, it was found that a 300 μm long anti-reflection (AR)-AR DFB-LD with a mesa width of 8 μm is reduced by about 25% while a side mode suppression ratio is >50 dB and a 3 dB bandwidth is >10 GHz at a current of 40 mA; in addition, it shows a clear eye-opening with a dynamic extinction ratio of >4.5 dB at 10 Gb s-1, and a power penalty of <1 dB after a 2 km transmission.

  10. 10 CFR 10.5 - Definitions.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 10 Energy 1 2014-01-01 2014-01-01 false Definitions. 10.5 Section 10.5 Energy NUCLEAR REGULATORY COMMISSION CRITERIA AND PROCEDURES FOR DETERMINING ELIGIBILITY FOR ACCESS TO RESTRICTED DATA OR NATIONAL SECURITY INFORMATION OR AN EMPLOYMENT CLEARANCE General Provisions § 10.5 Definitions. Access authorization means an administrative...

  11. 10 CFR 10.5 - Definitions.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 10 Energy 1 2011-01-01 2011-01-01 false Definitions. 10.5 Section 10.5 Energy NUCLEAR REGULATORY COMMISSION CRITERIA AND PROCEDURES FOR DETERMINING ELIGIBILITY FOR ACCESS TO RESTRICTED DATA OR NATIONAL SECURITY INFORMATION OR AN EMPLOYMENT CLEARANCE General Provisions § 10.5 Definitions. Access authorization means an administrative...

  12. 10 CFR 10.5 - Definitions.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 1 2012-01-01 2012-01-01 false Definitions. 10.5 Section 10.5 Energy NUCLEAR REGULATORY COMMISSION CRITERIA AND PROCEDURES FOR DETERMINING ELIGIBILITY FOR ACCESS TO RESTRICTED DATA OR NATIONAL SECURITY INFORMATION OR AN EMPLOYMENT CLEARANCE General Provisions § 10.5 Definitions. Access authorization means an administrative...

  13. 10 CFR 10.5 - Definitions.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 1 2010-01-01 2010-01-01 false Definitions. 10.5 Section 10.5 Energy NUCLEAR REGULATORY COMMISSION CRITERIA AND PROCEDURES FOR DETERMINING ELIGIBILITY FOR ACCESS TO RESTRICTED DATA OR NATIONAL SECURITY INFORMATION OR AN EMPLOYMENT CLEARANCE General Provisions § 10.5 Definitions. Access authorization means an administrative...

  14. Study of dependence of fast electron transport on target material using the 10ps, 1.5kJ Omega EP laser

    NASA Astrophysics Data System (ADS)

    Sorokovikova, A.; Wei, M. S.; Stephens, R. B.; Jacquez, J.; Mishra, R.; Sawada, H.; Theobald, W.; Patel, P.; McLean, H.; Sentoku, Y.; Beg, F. N.

    2011-10-01

    Igniting a Fast Ignition (FI) target requires generation of hot electrons inside a cone tip that travel to the compressed fuel through the tip. Its material must withstand the shell implosion. The effect of different materials on electron transport was previously studied at the Titan laser (150 J 0.7ps); emission from a buried fluor characterized the laser-generated electrons transmission through Al, Mo, or Au. Recent experiments using the OMEGA EP (300 J, 1 ps) showed similar effects on transport--going from Al to Au halved the detected electrons and decreased their divergence. We have extended these experiments to 10 ps, 1.5 kJ pulses to study pulse length effects. Experiments are modeled using both collisional and hybrid PIC codes. Detailed results will be presented. Supported by US DOE contracts DE-NA0000870, DE-FG02-05ER54834, DE-FC02-04ER54789.

  15. Demonstration of sub-meter GPS orbit determination and 1.5 parts in 10 to the 8th three-dimensional baseline accuracy

    NASA Technical Reports Server (NTRS)

    Lichten, Stephen M.; Bertiger, Willy I.

    1989-01-01

    Strategies for the estimation of precise GPS orbits and ground baselines, designed to minimize error sources related to the GPS orbit accuracy and the tropospheric delay, are demonstrated. Using GPS data from field experiments conducted in 1985 and 1986, it is shown that, by carefully selecting well-known stations to serve as reference points and by using the GPS data to determine high-accuracy GPS orbits and to solve for wet tropospheric delay fluctuations, the 2000-km baselines in North America can now be estimated with the accuracy better than 1.5 parts in 10 to the 8th. Using these strategies, better than l-m accuracy was achieved for the two best-tracked satellites (of the seven total operational GPS satellites).

  16. 973 nm wavelength stabilized hybrid ns-MOPA diode laser system with 15.5 W peak power and a spectral line width below 10 pm

    NASA Astrophysics Data System (ADS)

    Vu, Thi N.; Klehr, Andreas; Sumpf, Bernd; Wenzel, Hans; Erbert, Götz; Tränkle, Günther

    2014-05-01

    A master oscillator power amplifier (MOPA) system for the generation of ns-pulses with high peak power, narrow spectral line width, and stabilized emission wavelength will be presented. The master oscillator is a distributed feedback (DFB) ridge waveguide (RW) laser. The tapered amplifier consists of one RW section and one flared gain-guided section. The DFB laser is operated in continuous wave mode and emits at 973.5 nm with a spectral line width below 10 pm. The RW section of the amplifier acts as an optical gate. The tapered section amplifies the generated optical pulse. An optical peak power of 15.5 W for a pulse width of 8 ns is obtained. The emission wavelength remains constant at all output power levels of the MOPA system for a fixed current into the DFB laser. The spectral power density of the ASE is 37 dB smaller than the lasing spectral power density. The spectral line width is smaller than 10 pm, limited by the resolution of the optical spectrum analyzer.

  17. 33 CFR 66.10-5-66.10-10 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 33 Navigation and Navigable Waters 1 2012-07-01 2012-07-01 false 66.10-5-66.10-10 Section 66.10-5-66.10-10 Navigation and Navigable Waters COAST GUARD, DEPARTMENT OF HOMELAND SECURITY AIDS TO NAVIGATION PRIVATE AIDS TO NAVIGATION Uniform State Waterway Marking System §§ 66.10-5—66.10-10...

  18. 33 CFR 66.10-5-66.10-10 - [Reserved

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 33 Navigation and Navigable Waters 1 2010-07-01 2010-07-01 false 66.10-5-66.10-10 Section 66.10-5-66.10-10 Navigation and Navigable Waters COAST GUARD, DEPARTMENT OF HOMELAND SECURITY AIDS TO NAVIGATION PRIVATE AIDS TO NAVIGATION Uniform State Waterway Marking System §§ 66.10-5—66.10-10...

  19. Vibrational spectroscopy investigation using ab initio and density functional theory analysis on the structure of 5-chloro-10-oxa-3-thia-tricyclo[5.2.1.0 1,5]dec-8-ene-3,3-dioxide

    NASA Astrophysics Data System (ADS)

    Arslan, Hakan; Demircan, Aydın; Göktürk, Ersen

    2008-01-01

    The IR spectra of 5-chloro-10-oxa-3-thia-tricyclo[5.2.1.0 1,5]dec-8-ene-3,3-dioxide (COTDO) has been recorded in the region 4000-525 cm -1. The optimized molecular geometry, frequency and intensity of the vibrational bands of COTDO in the ground state has been calculated using the Hartree-Fock and density functional using Becke's three-parameter hybrid method with the Lee, Yang, and Parr correlation functional methods with 6-31G(d,p) and 6-311G(d,p) basis sets. The harmonic vibrational frequencies were calculated and the scaled values have been compared with experimental IR spectra. The calculated geometrical parameters and harmonic vibrations are predicted in a very good agreement with the experimental data. The theoretical vibrational spectra of the title compound were interpreted by means of potential energy distributions (PEDs) using VEDA 4 program. With the help of this modern technique we were able to complete the assignment of the vibrational spectra of the title compound.

  20. (2,3,5,6-Tetra­fluoro­phenolato-κO)(5,10,15,20-tetra­phenyl­porphyrinato)iron(III)

    PubMed Central

    Xu, Nan; Powell, Douglas R.; Richter-Addo, George B.

    2013-01-01

    The title compound, [Fe(C44H28N4)(C6HF4O)], is a porphyrin complex with iron(III) in fivefold coordination with a tetra­fluoro­phenolate group as the axial ligand. The Fe atom and the phenolate ligand are disordered across the porphyrin ring with the two phenolates appearing to be roughly related by a center of symmetry. The occupancies of the two phenolate groups refined to 0.788 (3) for the major component and 0.212 (3) for the minor component. The structure shows extraordinary Fe displacements of 0.488 (4) (major) and 0.673 (4) Å (minor) from the 24-atom mean plane of the porphyrin. The Fe—Np distances range from 2.063 (4) to 2.187 (6) Å and the Fe—O distances are 1.903 (5) Å for major component and 1.87 (2) Å for minor component. The four phenyl groups attached to the porphyrin ring form dihedral angles of 63.4 (4), 49.6 (4), 62.4 (4), and 63.3 (4)° (in increasing numerical order) with the three nearest C atoms of the porphyrin ring. The major and minor component phenolate groups form dihedral angles of 24.9 (4)° and 24.8 (4)°, respectively, with the four porphyrin N atoms. The Fe⋯Fe distance between the two iron(III) atoms of adjacent porphyrin mol­ecules is 6.677 (3) Å. No close inter­molecular inter­action was observed. The crystal studied was twinned by inversion, with a major–minor component ratio of 0.53 (3):0.47 (3). PMID:24098188

  1. A true electron-transfer reaction between 5,10,15,20-tetraphenylporphyrinato cadmium(II) and the hexacyanoferrate couple at the nitrobenzene/water interface.

    PubMed

    Osakai, Toshiyuki; Ichikawa, Seiko; Hotta, Hiroki; Nagatani, Hirohisa

    2004-11-01

    The ability of some metal complexes of 5,10,15,20-tetraphenylporphyrin (TPP) to give a voltammetric wave due to the heterogeneous electron transfer (ET) at a nitrobenzene (NB)/water (W) interface has been examined. The previously-proposed, electron-conductor separating oil-water (ECSOW) system has been successfully employed to find that the TPP complex with cadmium(II) added to NB gives a well-defined, reversible wave for the heterogeneous (i.e., "true") ET with the hexacyanoferrate couple in W. A digital simulation analysis has entirely excluded the possibility of the ion-transfer mechanism due to the homogeneous ET in W. The a.c. impedance method has then been used to determine the kinetic parameters including the standard rate constant k0 (= 0.10 cm M(-1) s(-1)) and the transfer coefficient alpha (= 0.53 at the half-wave potential). These values are in good agreement with those predicted from the Marcus theory with the assumption that the heterogeneous ET due to molecular collision occurs at the "sharp" NB/W interface. PMID:15566151

  2. Thermodynamics and kinetics of the formation of the supramolecular complexes bisacetato(5,10,15,20-tetraphenylporphinate)zirconium(IV) with pyridine and imidazole

    NASA Astrophysics Data System (ADS)

    Tyulyaeva, E. Yu.; Lomova, T. N.

    2010-05-01

    The equilibria and rates of step reactions for the formation of the supramolecular complexes of bisacetato(5,10,15,20-tetraphenylporphinate)zirconium(IV) (AcO)2ZrTPP and bioactive bases pyridine (Py) and imidazole (Im) in toluene were studied using UV-Vis and IR spectroscopy. The step stoichiometric mechanism, including the reversible coordination of two Py molecules ( K 1 = 1.8 × 108 l2/mol2), the equilibrium of the displacement of two AcO- into the second coordination sphere by increasing the concentration of the solvent polar component ( K 2 = 2.4), and the coordination of the third and fourth Py molecules in a one step with the formation of [(Py)4ZrTPP]2+ · 2(AcO)- ( K 3 = 2.8 × 104 l2/mol2), was verified. It was established that the spectrophotometric titration is sensible for the two-stage π-π-complexation of [(Py)4ZrTPP]2+ · 2(AcO)- with Py molecules ( K 4 = 29 l/mol and K 5 = 1.8 l/mol). It was shown that the stronger base Im reacts irreversibly with (AcO)2ZrTPP. The thermodynamic and optical characteristics of (AcO)2ZrTPP required for using the complex in the detection of bioactive bases were studied.

  3. Mitochondria and DNA Targeting of 5,10,15,20-Tetrakis(7-sulfonatobenzo[b]thiophene) Porphyrin-Induced Photodynamic Therapy via Intrinsic and Extrinsic Apoptotic Cell Death.

    PubMed

    Rangasamy, Sabarinathan; Ju, Hee; Um, Soohyun; Oh, Dong-Chan; Song, Joon Myong

    2015-09-10

    Photodynamic therapy (PDT) selectively targets subcellular organelles and promises an excellent therapeutic strategy for cancer treatment. Here, we report the synthesis of a new water-soluble photosensitizer, 5,10,15,20-tetrakis (7-sulfonatobenzo[b]thiophene) porphyrin (SBTP). Rational design of the porphyrinic molecule containing benzo[b]thiophene moiety at the meso-position led to selective accumulation in both mitochondria and nucleus of MCF-7 cells. This multitarget ability of SBTP can cause damage to mitochondria as well as DNA simultaneously. FACS analysis showed rapid cellular uptake of SBTP. High-content cell-based assay was executed to concurrently monitor increase of cytosolic Ca(2+) levels, mitochondrial permeability transition (MPT), and caspase-3/7/8 activation in MCF-7 cells under the pathological condition caused by PDT action of SBTP. The study of cell death dynamics showed that PDT action of SBTP caused an increase in the MPT followed by an increase in cytosolic Ca(2+) level. The localization of SBTP in the mitochondria activated the intrinsic apoptotic pathway. Additionally, localization of SBTP in the nucleus led to DNA damage in MCF-7 cells. The DNA fragmentation that occurred by PDT action of SBTP was thought to be responsible for extrinsic apoptosis of MCF-7 cells. SBTP demonstrated effective PDT activity of 5 μM IC50 value to MCF-7 cells by bitargeting mitochondria and DNA. PMID:26295496

  4. 10 CFR 51.15 - Time schedules.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... CFR part 2, the presiding officer, the Atomic Safety and Licensing Board or the Commissioners acting... 10 Energy 2 2012-01-01 2012-01-01 false Time schedules. 51.15 Section 51.15 Energy NUCLEAR... REGULATORY FUNCTIONS National Environmental Policy Act-Regulations Implementing Section 102(2) § 51.15...

  5. 10 CFR 61.15 - Financial information.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 10 Energy 2 2011-01-01 2011-01-01 false Financial information. 61.15 Section 61.15 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) LICENSING REQUIREMENTS FOR LAND DISPOSAL OF RADIOACTIVE WASTE Licenses § 61.15 Financial information. The financial information must be sufficient to demonstrate that...

  6. 10 CFR 15.3 - Communications.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 1 2010-01-01 2010-01-01 false Communications. 15.3 Section 15.3 Energy NUCLEAR REGULATORY COMMISSION DEBT COLLECTION PROCEDURES Application and Coverage § 15.3 Communications. Unless otherwise specified, communications concerning the regulations in this part may be addressed to...

  7. 10 CFR 1017.15 - Review process.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 10 Energy 4 2014-01-01 2014-01-01 false Review process. 1017.15 Section 1017.15 Energy DEPARTMENT... INFORMATION Review of a Document or Material for Unclassified Controlled Nuclear Information § 1017.15 Review... document outside of his or her organization for the review, he or she must mark the front of the...

  8. 10 CFR 51.15 - Time schedules.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... CFR part 2, the presiding officer, the Atomic Safety and Licensing Board or the Commissioners acting... 10 Energy 2 2011-01-01 2011-01-01 false Time schedules. 51.15 Section 51.15 Energy NUCLEAR... REGULATORY FUNCTIONS National Environmental Policy Act-Regulations Implementing Section 102(2) § 51.15...

  9. 10 CFR 51.15 - Time schedules.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... CFR part 2, the presiding officer, the Atomic Safety and Licensing Board or the Commissioners acting... 10 Energy 2 2010-01-01 2010-01-01 false Time schedules. 51.15 Section 51.15 Energy NUCLEAR... REGULATORY FUNCTIONS National Environmental Policy Act-Regulations Implementing Section 102(2) § 51.15...

  10. 10 CFR 61.15 - Financial information.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Financial information. 61.15 Section 61.15 Energy NUCLEAR....15 Financial information. The financial information must be sufficient to demonstrate that the financial qualifications of the applicant are adequate to carry out the activities for which the license...

  11. 10 CFR 61.15 - Financial information.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 2 2012-01-01 2012-01-01 false Financial information. 61.15 Section 61.15 Energy NUCLEAR....15 Financial information. The financial information must be sufficient to demonstrate that the financial qualifications of the applicant are adequate to carry out the activities for which the license...

  12. 10 CFR 15.3 - Communications.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 10 Energy 1 2013-01-01 2013-01-01 false Communications. 15.3 Section 15.3 Energy NUCLEAR REGULATORY COMMISSION DEBT COLLECTION PROCEDURES Application and Coverage § 15.3 Communications. Unless otherwise specified, communications concerning the regulations in this part may be addressed to...

  13. 10 CFR 15.3 - Communications.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 1 2012-01-01 2012-01-01 false Communications. 15.3 Section 15.3 Energy NUCLEAR REGULATORY COMMISSION DEBT COLLECTION PROCEDURES Application and Coverage § 15.3 Communications. Unless otherwise specified, communications concerning the regulations in this part may be addressed to...

  14. 10 CFR 810.15 - Violations.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 4 2012-01-01 2012-01-01 false Violations. 810.15 Section 810.15 Energy DEPARTMENT OF ENERGY ASSISTANCE TO FOREIGN ATOMIC ENERGY ACTIVITIES § 810.15 Violations. (a) The Atomic Energy Act... person from violating any provision of the Atomic Energy Act or its implementing regulations. (2)...

  15. 10 CFR 810.15 - Violations.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 10 Energy 4 2013-01-01 2013-01-01 false Violations. 810.15 Section 810.15 Energy DEPARTMENT OF ENERGY ASSISTANCE TO FOREIGN ATOMIC ENERGY ACTIVITIES § 810.15 Violations. (a) The Atomic Energy Act... person from violating any provision of the Atomic Energy Act or its implementing regulations. (2)...

  16. 10 CFR 810.15 - Violations.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 10 Energy 4 2014-01-01 2014-01-01 false Violations. 810.15 Section 810.15 Energy DEPARTMENT OF ENERGY ASSISTANCE TO FOREIGN ATOMIC ENERGY ACTIVITIES § 810.15 Violations. (a) The Atomic Energy Act... person from violating any provision of the Atomic Energy Act or its implementing regulations. (2)...

  17. 10 CFR 51.15 - Time schedules.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... CFR part 2, the presiding officer, the Atomic Safety and Licensing Board or the Commissioners acting... 10 Energy 2 2014-01-01 2014-01-01 false Time schedules. 51.15 Section 51.15 Energy NUCLEAR... REGULATORY FUNCTIONS National Environmental Policy Act-Regulations Implementing Section 102(2) § 51.15...

  18. 10 CFR 51.15 - Time schedules.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... CFR part 2, the presiding officer, the Atomic Safety and Licensing Board or the Commissioners acting... 10 Energy 2 2013-01-01 2013-01-01 false Time schedules. 51.15 Section 51.15 Energy NUCLEAR... REGULATORY FUNCTIONS National Environmental Policy Act-Regulations Implementing Section 102(2) § 51.15...

  19. 10 CFR 707.15 - Collective bargaining.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 4 2012-01-01 2012-01-01 false Collective bargaining. 707.15 Section 707.15 Energy DEPARTMENT OF ENERGY WORKPLACE SUBSTANCE ABUSE PROGRAMS AT DOE SITES Procedures § 707.15 Collective bargaining. When establishing drug testing programs, contractors who are parties to collective...

  20. 10 CFR 707.15 - Collective bargaining.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 10 Energy 4 2014-01-01 2014-01-01 false Collective bargaining. 707.15 Section 707.15 Energy DEPARTMENT OF ENERGY WORKPLACE SUBSTANCE ABUSE PROGRAMS AT DOE SITES Procedures § 707.15 Collective bargaining. When establishing drug testing programs, contractors who are parties to collective...

  1. 10 CFR 707.15 - Collective bargaining.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 10 Energy 4 2013-01-01 2013-01-01 false Collective bargaining. 707.15 Section 707.15 Energy DEPARTMENT OF ENERGY WORKPLACE SUBSTANCE ABUSE PROGRAMS AT DOE SITES Procedures § 707.15 Collective bargaining. When establishing drug testing programs, contractors who are parties to collective...

  2. 10 CFR 707.15 - Collective bargaining.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 10 Energy 4 2011-01-01 2011-01-01 false Collective bargaining. 707.15 Section 707.15 Energy DEPARTMENT OF ENERGY WORKPLACE SUBSTANCE ABUSE PROGRAMS AT DOE SITES Procedures § 707.15 Collective bargaining. When establishing drug testing programs, contractors who are parties to collective...

  3. 10 CFR 707.15 - Collective bargaining.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 4 2010-01-01 2010-01-01 false Collective bargaining. 707.15 Section 707.15 Energy DEPARTMENT OF ENERGY WORKPLACE SUBSTANCE ABUSE PROGRAMS AT DOE SITES Procedures § 707.15 Collective bargaining. When establishing drug testing programs, contractors who are parties to collective...

  4. 10 CFR 1008.15 - Civil remedies.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 10 Energy 4 2011-01-01 2011-01-01 false Civil remedies. 1008.15 Section 1008.15 Energy DEPARTMENT OF ENERGY (GENERAL PROVISIONS) RECORDS MAINTAINED ON INDIVIDUALS (PRIVACY ACT) Requests for Access or Amendment § 1008.15 Civil remedies. Subsection (g) of the Act provides that an individual may bring...

  5. 10 CFR 1008.15 - Civil remedies.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 10 Energy 4 2013-01-01 2013-01-01 false Civil remedies. 1008.15 Section 1008.15 Energy DEPARTMENT OF ENERGY (GENERAL PROVISIONS) RECORDS MAINTAINED ON INDIVIDUALS (PRIVACY ACT) Requests for Access or Amendment § 1008.15 Civil remedies. Subsection (g) of the Act provides that an individual may bring...

  6. 10 CFR 1008.15 - Civil remedies.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 4 2012-01-01 2012-01-01 false Civil remedies. 1008.15 Section 1008.15 Energy DEPARTMENT OF ENERGY (GENERAL PROVISIONS) RECORDS MAINTAINED ON INDIVIDUALS (PRIVACY ACT) Requests for Access or Amendment § 1008.15 Civil remedies. Subsection (g) of the Act provides that an individual may bring...

  7. 10 CFR 1008.15 - Civil remedies.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 10 Energy 4 2014-01-01 2014-01-01 false Civil remedies. 1008.15 Section 1008.15 Energy DEPARTMENT OF ENERGY (GENERAL PROVISIONS) RECORDS MAINTAINED ON INDIVIDUALS (PRIVACY ACT) Requests for Access or Amendment § 1008.15 Civil remedies. Subsection (g) of the Act provides that an individual may bring...

  8. 10 CFR 60.15 - Site characterization.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Site characterization. 60.15 Section 60.15 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) DISPOSAL OF HIGH-LEVEL RADIOACTIVE WASTES IN GEOLOGIC REPOSITORIES Licenses Preapplication Review § 60.15 Site characterization. (a) Prior to submittal of an application for a license to...

  9. 10 CFR 60.15 - Site characterization.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 2 2012-01-01 2012-01-01 false Site characterization. 60.15 Section 60.15 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) DISPOSAL OF HIGH-LEVEL RADIOACTIVE WASTES IN GEOLOGIC REPOSITORIES Licenses Preapplication Review § 60.15 Site characterization. (a) Prior to submittal of an application for a license to...

  10. 10 CFR 60.15 - Site characterization.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 10 Energy 2 2014-01-01 2014-01-01 false Site characterization. 60.15 Section 60.15 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) DISPOSAL OF HIGH-LEVEL RADIOACTIVE WASTES IN GEOLOGIC REPOSITORIES Licenses Preapplication Review § 60.15 Site characterization. (a) Prior to submittal of an application for a license to...

  11. 10 CFR 60.15 - Site characterization.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 10 Energy 2 2013-01-01 2013-01-01 false Site characterization. 60.15 Section 60.15 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) DISPOSAL OF HIGH-LEVEL RADIOACTIVE WASTES IN GEOLOGIC REPOSITORIES Licenses Preapplication Review § 60.15 Site characterization. (a) Prior to submittal of an application for a license to...

  12. 10 CFR 60.15 - Site characterization.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 10 Energy 2 2011-01-01 2011-01-01 false Site characterization. 60.15 Section 60.15 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) DISPOSAL OF HIGH-LEVEL RADIOACTIVE WASTES IN GEOLOGIC REPOSITORIES Licenses Preapplication Review § 60.15 Site characterization. (a) Prior to submittal of an application for a license to...

  13. 10 CFR 1008.15 - Civil remedies.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 4 2010-01-01 2010-01-01 false Civil remedies. 1008.15 Section 1008.15 Energy DEPARTMENT OF ENERGY (GENERAL PROVISIONS) RECORDS MAINTAINED ON INDIVIDUALS (PRIVACY ACT) Requests for Access or Amendment § 1008.15 Civil remedies. Subsection (g) of the Act provides that an individual may bring...

  14. 10 CFR 54.15 - Specific exemptions.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 2 2010-01-01 2010-01-01 false Specific exemptions. 54.15 Section 54.15 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) REQUIREMENTS FOR RENEWAL OF OPERATING LICENSES FOR NUCLEAR POWER PLANTS... granted by the Commission in accordance with 10 CFR 50.12....

  15. 31 CFR 15.737-10 - Conferences.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... INTEREST Administrative Enforcement Proceedings § 15.737-10 Conferences. (a) In general. The Director may... administrative disciplinary proceeding has been instituted against him/her. If such conference results in a... 31 Money and Finance: Treasury 1 2010-07-01 2010-07-01 false Conferences. 15.737-10 Section...

  16. 15 CFR 719.10 - Discovery.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 15 Commerce and Foreign Trade 2 2014-01-01 2014-01-01 false Discovery. 719.10 Section 719.10... INDUSTRY AND SECURITY, DEPARTMENT OF COMMERCE CHEMICAL WEAPONS CONVENTION REGULATIONS ENFORCEMENT § 719.10... in the request (at least 10 days after service, or within such additional time as the ALJ may...

  17. 15 CFR 719.10 - Discovery.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 15 Commerce and Foreign Trade 2 2013-01-01 2013-01-01 false Discovery. 719.10 Section 719.10... INDUSTRY AND SECURITY, DEPARTMENT OF COMMERCE CHEMICAL WEAPONS CONVENTION REGULATIONS ENFORCEMENT § 719.10... in the request (at least 10 days after service, or within such additional time as the ALJ may...

  18. 15 CFR 719.10 - Discovery.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 2 2010-01-01 2010-01-01 false Discovery. 719.10 Section 719.10... INDUSTRY AND SECURITY, DEPARTMENT OF COMMERCE CHEMICAL WEAPONS CONVENTION REGULATIONS ENFORCEMENT § 719.10... in the request (at least 10 days after service, or within such additional time as the ALJ may...

  19. 15 CFR 719.10 - Discovery.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 15 Commerce and Foreign Trade 2 2012-01-01 2012-01-01 false Discovery. 719.10 Section 719.10... INDUSTRY AND SECURITY, DEPARTMENT OF COMMERCE CHEMICAL WEAPONS CONVENTION REGULATIONS ENFORCEMENT § 719.10... in the request (at least 10 days after service, or within such additional time as the ALJ may...

  20. 15 CFR 719.10 - Discovery.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 2 2011-01-01 2011-01-01 false Discovery. 719.10 Section 719.10... INDUSTRY AND SECURITY, DEPARTMENT OF COMMERCE CHEMICAL WEAPONS CONVENTION REGULATIONS ENFORCEMENT § 719.10... in the request (at least 10 days after service, or within such additional time as the ALJ may...

  1. 10 CFR 15.27 - Contact with debtor's employing agency.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... accomplished in accordance with 5 U.S.C. 5514 and the provisions of 10 CFR part 16. ... 10 Energy 1 2010-01-01 2010-01-01 false Contact with debtor's employing agency. 15.27 Section 15... Claims § 15.27 Contact with debtor's employing agency. If the debtor is employed by the...

  2. Pathways to quiescence: SHARDS view on the star formation histories of massive quiescent galaxies at 1.0 < z < 1.5

    NASA Astrophysics Data System (ADS)

    Domínguez Sánchez, Helena; Pérez-González, Pablo G.; Esquej, Pilar; Eliche-Moral, M. Carmen; Barro, Guillermo; Cava, Antonio; Koekemoer, Anton M.; Alcalde Pampliega, Belén; Alonso Herrero, Almudena; Bruzual, Gustavo; Cardiel, Nicolás; Cenarro, Javier; Ceverino, Daniel; Charlot, Stéphane; Hernán Caballero, Antonio

    2016-04-01

    We present star formation histories (SFHs) for a sample of 104 massive (stellar mass M > 1010 M⊙) quiescent galaxies (MQGs) at z = 1.0-1.5 from the analysis of spectrophotometric data from the Survey for High-z Absorption Red and Dead Sources (SHARDS) and HST/WFC3 G102 and G141 surveys of the GOODS-North field, jointly with broad-band observations from ultraviolet (UV) to far-infrared (far-IR). The sample is constructed on the basis of rest-frame UVJ colours and specific star formation rates (sSFRs = SFR/Mass). The spectral energy distributions (SEDs) of each galaxy are compared to models assuming a delayed exponentially declining SFH. A Monte Carlo algorithm characterizes the degeneracies, which we are able to break taking advantage of the SHARDS data resolution, by measuring indices such as MgUV and D4000. The population of MQGs shows a duality in their properties. The sample is dominated (85 per cent) by galaxies with young mass-weighted ages, overline{t_M} < 2 Gyr, short star formation time-scales, <τ> ˜ 60-200 Myr, and masses log(M/M⊙) ˜ 10.5. There is an older population (15 per cent) with overline{t_M} = 2-4 Gyr, longer star formation time-scales, <τ> ˜ 400 Myr, and larger masses, log(M/M⊙) ˜ 10.7. The SFHs of our MQGs are consistent with the slope and the location of the main sequence of star-forming galaxies at z > 1.0, when our galaxies were 0.5-1.0 Gyr old. According to these SFHs, all the MQGs experienced a luminous infrared galaxy phase that lasts for ˜500 Myr, and half of them an ultraluminous infrared galaxy phase for ˜100 Myr. We find that the MQG population is almost assembled at z ˜ 1, and continues evolving passively with few additions to the population.

  3. Novel nanomaterials based on 5,10,15,20-tetrakis(3,4-dimethoxyphenyl)-21H,23H-porphyrin entrapped in silica matrices

    SciTech Connect

    Fagadar-Cosma, Eugenia; Enache, Corina; Vlascici, Dana; Fagadar-Cosma, Gheorghe; Vasile, Mihaela; Bazylak, Grzegorz

    2009-12-15

    The present study is dealing with the obtaining of transparent hybrid silica materials encapsulating 5,10,15,20-tetrakis(3,4-dimethoxyphenyl)-21H,23H-porphyrin designated for advanced optoelectronic devices. The porphyrin was synthesized by three methods: an Adler-type reaction between pyrrole and 3,4-dimethoxybenzaldehyde in propionic acid medium; by Lindsey condensation of pyrrole with 3,4-dimethoxybenzaldehyde in the presence of BF{sub 3}.OEt{sub 2} and by a multicomponent reaction by simultaneously using of pyrrole and two different aldehydes: 3,4-dimethoxybenzaldehyde and 3-hydroxybenzaldehyde. The 3,4-dimethoxyphenyl substituted porphyrin was characterized by HPLC, TLC, UV-vis, FT-IR, {sup 1}H NMR and {sup 13}C NMR analysis. Excitation and emission spectra were also discussed in terms of pH conditions. The hybrid materials, consisting in the porphyrin encapsulated in silica matrices, have been prepared successfully via the two steps acid-base catalyzed hydrolysis and condensation of tetraethylorthosilicate using different approaches of the sol-gel process: in situ, by impregnation and by sonication. The synthetic conditions and the compositions were monitored and characterized by using spectroscopic methods such as FT-IR, fluorescence and UV-vis. Atomic force microscopy (AFM) has been applied to observe the columnar or pyramidal nanostructures which are formed by the immobilization of porphyrin on the silica matrices.

  4. Mössbauer effect study of tight spin coupling in oxidized chloro-5,10,15,20- tetra(mesityl)porphyrinatoiron(III)

    NASA Astrophysics Data System (ADS)

    Boso, Brian; Lang, George; McMurry, Thomas J.; Groves, John T.

    1983-08-01

    Mössbauer spectra of a polycrystalline form of oxidized chloro-5,10,15,20-tetra(mesityl)porphyrin- atoiron(III) [Fe(TMP)Cl], compound A, were recorded over a range of temperatures (4.2-195 K) and magnetic fields (0-6 T). These spectra of compound A exhibit magnetic features which are markedly different from those of the analogous protein complexes, horse radish peroxidase compound I (HRP-I) and compound ES of cytochrome c peroxidase, even though chemical evidence and optical spectroscopy indicate that compound A is similar to the others in comprising a Fe(IV) complex within a porphyrin cation radical. We interpret the data by employing a spin Hamiltonian model in which the central Fe(IV) complex, with S=1, is tightly coupled to a S=1/2 system of the oxidized porphyrin to yield a net S=3/2 system as suggested by the susceptibility measurements. The theoretical treatment yields information on the d-electron energies which is similar to that more directly available in the peroxidase spectra. The strength of the axial crystal field is found to increase progressively in the series HRP-I, ES, compound A, while the spin coupling in A is the strongest of the three by several orders of magnitude. The good fits to experimental data confirm the efficacy of the theoretical treatment which may be applicable to a variety of other coupled systems.

  5. Surfactant assisted self-assembly of zinc 5,10-bis (4-pyridyl)-15,20-bis (4-octadecyloxyphenyl) porphyrin into supramolecular nanoarchitectures.

    PubMed

    Gautam, Renu; Chauhan, S M S

    2014-10-01

    The surfactant assisted self-assembly (SAS) method has been used in the formation of nanocubes, nanorods and microrods from zinc 5,10-bis (4-pyridyl)-15,20-bis (4-octadecyloxyphenyl) porphyrin. By the dropwise addition of chloroform solution of the zinc porphyrin into an aqueous solution of cetyltrimethylammonium bromide (CTAB), cuboidal nanostructures are formed at the initial stage. The nanocubes are transformed into nanorods and microrods by aging under ambient conditions. The longer nanorods with well defined edges have been formed with lower concentration of porphyrin solution whereas the shorter nanorods have been formed with higher concentration of zinc porphyrin. The synergistic effect of hydrophobic interactions by the long alkyl chains substituted on the peripheral phenyl rings of porphyrin and axial coordination of pyridyl nitrogen atoms with central zinc is mainly responsible for the formation of different nanostructures. The nanostructures were characterized by UV-visible spectra, fluorescence spectroscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM), atomic force microscopy (AFM), IR spectroscopy and X-ray diffraction (XRD) pattern. PMID:25175235

  6. Thermoeconomic modeling and parametric study of hybrid SOFC-gas turbine-steam turbine power plants ranging from 1.5 to 10 MWe

    NASA Astrophysics Data System (ADS)

    Arsalis, Alexandros

    Detailed thermodynamic, kinetic, geometric, and cost models are developed, implemented, and validated for the synthesis/design and operational analysis of hybrid SOFC-gas turbine-steam turbine systems ranging in size from 1.5 to 10 MWe. The fuel cell model used in this research work is based on a tubular Siemens-Westinghouse-type SOFC, which is integrated with a gas turbine and a heat recovery steam generator (HRSG) integrated in turn with a steam turbine cycle. The current work considers the possible benefits of using the exhaust gases in a HRSG in order to produce steam which drives a steam turbine for additional power output. Four different steam turbine cycles are considered in this research work: a single-pressure, a dual-pressure, a triple pressure, and a triple pressure with reheat. The models have been developed to function both at design (full load) and off-design (partial load) conditions. In addition, different solid oxide fuel cell sizes are examined to assure a proper selection of SOFC size based on efficiency or cost. The thermoeconomic analysis includes cost functions developed specifically for the different system and component sizes (capacities) analyzed. A parametric study is used to determine the most viable system/component syntheses/designs based on maximizing total system efficiency or minimizing total system life cycle cost.

  7. Structural, optical and dispersion properties of 5,10,15,20-tetraphenyl-21H,23H-porphyrin zinc thin films

    NASA Astrophysics Data System (ADS)

    Zeyada, Hamdy M.; Makhlouf, Mohamed M.; Ali, Mohamed A.

    2016-02-01

    The thin films of 5,10,15,20-tetraphenyl-21H,23H-porphyrin zinc, ZnTPP, were successfully prepared by the thermal evaporation technique. The structure formation and optical properties of ZnTPP thin films were studied. The surface morphology and structural characteristics of ZnTPP thin films were analyzed by atomic force microscopy (AFM) and X-ray diffraction (XRD) techniques, respectively. The optical constants of ZnTPP films were measured by spectrophotometer measurements of the transmittance and reflectance at a normal incidence of light in the spectral wavelength range from 200 to 2500 nm. The absorption spectrum of ZnTPP films showed four absorption bands, namely, the Q, B, N, and M bands. Anomalous dispersion was observed in the absorption region and normal dispersion occurred in the transparent region of the spectrum. We adopted the multi-oscillator and the single-oscillator models to interpret the results of anomalous and normal dispersion characteristics, respectively. The energy band gap of ZnTPP films was measured and the type of electron transition was determined to be the indirect allowed transition. The annealing process had an obvious effect on the morphology, structure, optical constants, and spectral dispersion parameters of ZnTPP thin films.

  8. SpaceCube Version 1.5

    NASA Technical Reports Server (NTRS)

    Geist, Alessandro; Lin, Michael; Flatley, Tom; Petrick, David

    2013-01-01

    SpaceCube 1.5 is a high-performance and low-power system in a compact form factor. It is a hybrid processing system consisting of CPU (central processing unit), FPGA (field-programmable gate array), and DSP (digital signal processor) processing elements. The primary processing engine is the Virtex- 5 FX100T FPGA, which has two embedded processors. The SpaceCube 1.5 System was a bridge to the SpaceCube 2.0 and SpaceCube 2.0 Mini processing systems. The SpaceCube 1.5 system was the primary avionics in the successful SMART (Small Rocket/Spacecraft Technology) Sounding Rocket mission that was launched in the summer of 2011. For SMART and similar missions, an avionics processor is required that is reconfigurable, has high processing capability, has multi-gigabit interfaces, is low power, and comes in a rugged/compact form factor. The original SpaceCube 1.0 met a number of the criteria, but did not possess the multi-gigabit interfaces that were required and is a higher-cost system. The SpaceCube 1.5 was designed with those mission requirements in mind. The SpaceCube 1.5 features one Xilinx Virtex-5 FX100T FPGA and has excellent size, weight, and power characteristics [4×4×3 in. (approx. = 10×10×8 cm), 3 lb (approx. = 1.4 kg), and 5 to 15 W depending on the application]. The estimated computing power of the two PowerPC 440s in the Virtex-5 FPGA is 1100 DMIPS each. The SpaceCube 1.5 includes two Gigabit Ethernet (1 Gbps) interfaces as well as two SATA-I/II interfaces (1.5 to 3.0 Gbps) for recording to data drives. The SpaceCube 1.5 also features DDR2 SDRAM (double data rate synchronous dynamic random access memory); 4- Gbit Flash for storing application code for the CPU, FPGA, and DSP processing elements; and a Xilinx Platform Flash XL to store FPGA configuration files or application code. The system also incorporates a 12 bit analog to digital converter with the ability to read 32 discrete analog sensor inputs. The SpaceCube 1.5 design also has a built

  9. Mechano-thermal synthesis of nanocrystalline RuSr2Eu1.5Ce0.5Cu2O10-δ materials: Micro-structural, optical and magnetic properties

    NASA Astrophysics Data System (ADS)

    Balamurugan, S.; Hussain, A. K. Jakkir; Parthiban, P.; Satya, A. T.; Janaki, J.

    2016-05-01

    The nanocrystalline RuSr2Eu1.5Ce0.5Cu2O10-δ (referred to as Ru1222Eu) materials were successfully prepared by mechano-thermal route and studied the Ru1222Eu materials by powder XRD, FT-IR, SEM-EDX and ac-susceptibility measurements. The as-milled powder annealed at 950 - 1000°C is crystallized in nearly single tetragonal phase of Ru1222Eu materials with average crystalline size of ~40 nm. Agglomeration of fine particles is seen through SEM micro-images in the Ru1222Eu phase materials. Contrary to magneto-superconductivity, a magnetic ordering is seen at ~60 K for Ru1222Eu phase under low applied field of 0.5 Oe at 10 Hz.

  10. 15 CFR 10.2 - Funding.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 15 Commerce and Foreign Trade 1 2012-01-01 2012-01-01 false Funding. 10.2 Section 10.2 Commerce and Foreign Trade Office of the Secretary of Commerce PROCEDURES FOR THE DEVELOPMENT OF VOLUNTARY PRODUCT STANDARDS § 10.2 Funding. Groups who represent producers, distributors, consumers or users,...

  11. 15 CFR 10.2 - Funding.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 15 Commerce and Foreign Trade 1 2013-01-01 2013-01-01 false Funding. 10.2 Section 10.2 Commerce and Foreign Trade Office of the Secretary of Commerce PROCEDURES FOR THE DEVELOPMENT OF VOLUNTARY PRODUCT STANDARDS § 10.2 Funding. Groups who represent producers, distributors, consumers or users,...

  12. 15 CFR 10.2 - Funding.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 1 2010-01-01 2010-01-01 false Funding. 10.2 Section 10.2 Commerce and Foreign Trade Office of the Secretary of Commerce PROCEDURES FOR THE DEVELOPMENT OF VOLUNTARY PRODUCT STANDARDS § 10.2 Funding. Groups who represent producers, distributors, consumers or users,...

  13. 15 CFR 10.2 - Funding.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 15 Commerce and Foreign Trade 1 2014-01-01 2014-01-01 false Funding. 10.2 Section 10.2 Commerce and Foreign Trade Office of the Secretary of Commerce PROCEDURES FOR THE DEVELOPMENT OF VOLUNTARY PRODUCT STANDARDS § 10.2 Funding. Groups who represent producers, distributors, consumers or users,...

  14. 15 CFR 10.2 - Funding.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 1 2011-01-01 2011-01-01 false Funding. 10.2 Section 10.2 Commerce and Foreign Trade Office of the Secretary of Commerce PROCEDURES FOR THE DEVELOPMENT OF VOLUNTARY PRODUCT STANDARDS § 10.2 Funding. Groups who represent producers, distributors, consumers or users,...

  15. 15 CFR 10.12 - Editorial changes.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 1 2010-01-01 2010-01-01 false Editorial changes. 10.12 Section 10.12... PRODUCT STANDARDS § 10.12 Editorial changes. The Department may, without prior notice, make such editorial or other minor changes as it deems necessary to reduce ambiguity or to improve clarity in...

  16. 15 CFR 10.12 - Editorial changes.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 15 Commerce and Foreign Trade 1 2012-01-01 2012-01-01 false Editorial changes. 10.12 Section 10.12... PRODUCT STANDARDS § 10.12 Editorial changes. The Department may, without prior notice, make such editorial or other minor changes as it deems necessary to reduce ambiguity or to improve clarity in...

  17. 15 CFR 10.12 - Editorial changes.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 1 2011-01-01 2011-01-01 false Editorial changes. 10.12 Section 10.12... PRODUCT STANDARDS § 10.12 Editorial changes. The Department may, without prior notice, make such editorial or other minor changes as it deems necessary to reduce ambiguity or to improve clarity in...

  18. 15 CFR 10.12 - Editorial changes.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 15 Commerce and Foreign Trade 1 2014-01-01 2014-01-01 false Editorial changes. 10.12 Section 10.12... PRODUCT STANDARDS § 10.12 Editorial changes. The Department may, without prior notice, make such editorial or other minor changes as it deems necessary to reduce ambiguity or to improve clarity in...

  19. 15 CFR 10.12 - Editorial changes.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 15 Commerce and Foreign Trade 1 2013-01-01 2013-01-01 false Editorial changes. 10.12 Section 10.12... PRODUCT STANDARDS § 10.12 Editorial changes. The Department may, without prior notice, make such editorial or other minor changes as it deems necessary to reduce ambiguity or to improve clarity in...

  20. 15 CFR 2004.10 - Other charges.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 3 2010-01-01 2010-01-01 false Other charges. 2004.10 Section 2004.10... TRADE REPRESENTATIVE FREEDOM OF INFORMATION POLICIES AND PROCEDURES Costs § 2004.10 Other charges. USTR may apply other charges, including the following: (a) Special charges. USTR shall recover the...

  1. 15 CFR 2004.10 - Other charges.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 3 2011-01-01 2011-01-01 false Other charges. 2004.10 Section 2004.10... TRADE REPRESENTATIVE FREEDOM OF INFORMATION POLICIES AND PROCEDURES Costs § 2004.10 Other charges. USTR may apply other charges, including the following: (a) Special charges. USTR shall recover the...

  2. 15 CFR 8.10 - Investigations.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 1 2010-01-01 2010-01-01 false Investigations. 8.10 Section 8.10... Compliance § 8.10 Investigations. (a) Making the investigation. The responsible Department official or his designee will make a prompt investigation whenever a compliance review, report, complaint, or any...

  3. 15 CFR 8.10 - Investigations.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 1 2011-01-01 2011-01-01 false Investigations. 8.10 Section 8.10... Compliance § 8.10 Investigations. (a) Making the investigation. The responsible Department official or his designee will make a prompt investigation whenever a compliance review, report, complaint, or any...

  4. 15 CFR 10.0 - General.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 1 2011-01-01 2011-01-01 false General. 10.0 Section 10.0 Commerce and Foreign Trade Office of the Secretary of Commerce PROCEDURES FOR THE DEVELOPMENT OF VOLUNTARY PRODUCT STANDARDS § 10.0 General. (a) Introduction. The Department of Commerce (hereinafter referred to...

  5. 15 CFR 10.0 - General.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 15 Commerce and Foreign Trade 1 2012-01-01 2012-01-01 false General. 10.0 Section 10.0 Commerce and Foreign Trade Office of the Secretary of Commerce PROCEDURES FOR THE DEVELOPMENT OF VOLUNTARY PRODUCT STANDARDS § 10.0 General. (a) Introduction. The Department of Commerce (hereinafter referred to...

  6. 15 CFR 10.0 - General.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 15 Commerce and Foreign Trade 1 2013-01-01 2013-01-01 false General. 10.0 Section 10.0 Commerce and Foreign Trade Office of the Secretary of Commerce PROCEDURES FOR THE DEVELOPMENT OF VOLUNTARY PRODUCT STANDARDS § 10.0 General. (a) Introduction. The Department of Commerce (hereinafter referred to...

  7. 15 CFR 990.10 - Purpose.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 15 Commerce and Foreign Trade 3 2014-01-01 2014-01-01 false Purpose. 990.10 Section 990.10 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) NATIONAL OCEANIC AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE OIL POLLUTION ACT REGULATIONS NATURAL RESOURCE DAMAGE ASSESSMENTS Introduction § 990.10...

  8. 1,5-Diamido-9,10-anthraquinone, a Centrosymmetric Redox-Active Bridge with Two Coupled β-Ketiminato Chelate Functions: Symmetric and Asymmetric Diruthenium Complexes.

    PubMed

    Ansari, Mohd Asif; Mandal, Abhishek; Paretzki, Alexa; Beyer, Katharina; Fiedler, Jan; Kaim, Wolfgang; Lahiri, Goutam Kumar

    2016-06-01

    The dinuclear complexes {(μ-H2L)[Ru(bpy)2]2}(ClO4)2 ([3](ClO4)2), {(μ-H2L)[Ru(pap)2]2}(ClO4)2 ([4](ClO4)2), and the asymmetric [(bpy)2Ru(μ-H2L)Ru(pap)2](ClO4)2 ([5](ClO4)2) were synthesized via the mononuclear species [Ru(H3L)(bpy)2]ClO4 ([1]ClO4) and [Ru(H3L)(pap)2]ClO4 ([2]ClO4), where H4L is the centrosymmetric 1,5-diamino-9,10-anthraquinone, bpy is 2,2'-bipyridine, and pap is 2-phenylazopyridine. Electrochemistry of the structurally characterized [1]ClO4, [2]ClO4, [3](ClO4)2, [4](ClO4)2, and [5](ClO4)2 reveals multistep oxidation and reduction processes, which were analyzed by electron paramagnetic resonance (EPR) of paramagnetic intermediates and by UV-vis-NIR spectro-electrochemistry. With support by time-dependent density functional theory (DFT) calculations the redox processes could be assigned. Significant results include the dimetal/bridging ligand mixed spin distribution in 3(3+) versus largely bridge-centered spin in 4(3+)-a result of the presence of Ru(II)-stabilizig pap coligands. In addition to the metal/ligand alternative for electron transfer and spin location, the dinuclear systems allow for the observation of ligand/ligand and metal/metal site differentiation within the multistep redox series. DFT-supported EPR and NIR absorption spectroscopy of the latter case revealed class II mixed-valence behavior of the oxidized asymmetric system 5(3+) with about equal contributions from a radical bridge formulation. In comparison to the analogues with the deprotonated 1,4-diaminoanthraquinone isomer the centrosymmetric H2L(2-) bridge shows anodically shifted redox potentials and weaker electronic coupling between the chelate sites. PMID:27171539

  9. 21 CFR 73.3117 - 16,23-Dihydrodinaphtho[2,3-a:2′,3′-i] naphth [2′,3′:6,7] indolo [2,3-c] carbazole-5,10,15,17,22...

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ..., DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL LISTING OF COLOR ADDITIVES EXEMPT FROM CERTIFICATION Medical Devices § 73.3117 16,23-Dihydrodinaphtho naphth indolo carbazole-5,10,15,17,22,24-hexone. (a)...

  10. 21 CFR 73.3117 - 16,23-Dihydrodinaphtho[2,3-a:2′,3′-i] naphth [2′,3′:6,7] indolo [2,3-c] carbazole-5,10,15,17,22...

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ..., DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL LISTING OF COLOR ADDITIVES EXEMPT FROM CERTIFICATION Medical Devices § 73.3117 16,23-Dihydrodinaphtho naphth indolo carbazole-5,10,15,17,22,24-hexone. (a)...

  11. 46 CFR 12.15-5 - Physical and medical requirements.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 1 2010-10-01 2010-10-01 false Physical and medical requirements. 12.15-5 Section 12.15... REQUIREMENTS FOR RATING ENDORSEMENTS Qualified Member of the Engine Department § 12.15-5 Physical and medical requirements. The physical and medical requirements for an endorsement as QMED are found in § 10.215 of...

  12. 46 CFR 12.15-5 - Physical and medical requirements.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 1 2012-10-01 2012-10-01 false Physical and medical requirements. 12.15-5 Section 12.15... REQUIREMENTS FOR RATING ENDORSEMENTS Qualified Member of the Engine Department § 12.15-5 Physical and medical requirements. The physical and medical requirements for an endorsement as QMED are found in § 10.215 of...

  13. 46 CFR 12.15-5 - Physical and medical requirements.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 1 2011-10-01 2011-10-01 false Physical and medical requirements. 12.15-5 Section 12.15... REQUIREMENTS FOR RATING ENDORSEMENTS Qualified Member of the Engine Department § 12.15-5 Physical and medical requirements. The physical and medical requirements for an endorsement as QMED are found in § 10.215 of...

  14. 10 CFR 1017.15 - Review process.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 10 Energy 4 2013-01-01 2013-01-01 false Review process. 1017.15 Section 1017.15 Energy DEPARTMENT OF ENERGY (GENERAL PROVISIONS) IDENTIFICATION AND PROTECTION OF UNCLASSIFIED CONTROLLED NUCLEAR... process. (a) Reviewing documents for UCNI. Anyone who originates or possesses a document that he or...

  15. 10 CFR 1017.15 - Review process.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 4 2012-01-01 2012-01-01 false Review process. 1017.15 Section 1017.15 Energy DEPARTMENT OF ENERGY (GENERAL PROVISIONS) IDENTIFICATION AND PROTECTION OF UNCLASSIFIED CONTROLLED NUCLEAR... process. (a) Reviewing documents for UCNI. Anyone who originates or possesses a document that he or...

  16. 10 CFR 1017.15 - Review process.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 10 Energy 4 2011-01-01 2011-01-01 false Review process. 1017.15 Section 1017.15 Energy DEPARTMENT OF ENERGY (GENERAL PROVISIONS) IDENTIFICATION AND PROTECTION OF UNCLASSIFIED CONTROLLED NUCLEAR... process. (a) Reviewing documents for UCNI. Anyone who originates or possesses a document that he or...

  17. Aqua­(9,10-dioxoanthracene-1,5-disul­fonato-κO 1)bis­(1,10-phenanthroline-κ2 N,N′)nickel(II)

    PubMed Central

    Cao, Ying-Yu

    2010-01-01

    In the mononuclear title complex, [Ni(C14H6O8S2)(C12H8N2)2(H2O)], the NiII atom is in a distorted octa­hedral coordination formed by four N atoms from two chelating 1,10-phenanthroline ligands and by two O atoms, one from a 9,10-dioxoanthracene-1,5-disulfonate ligand and the other from a water mol­ecule. An intra­molecular O—H⋯O hydrogen bond occurs. In the crystal, inter­molecular O—H⋯O hydrogen bonds link the mononuclear complexes into chains extending parallel to [010]. Furthermore, π–π stacking inter­actions [centroid–centroid distance = 3.5696 (6) Å] stabilize the crystal structuure. PMID:21587353

  18. 46 CFR 72.15-5 - Structural fire protection.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 3 2010-10-01 2010-10-01 false Structural fire protection. 72.15-5 Section 72.15-5... ARRANGEMENT Ventilation § 72.15-5 Structural fire protection. See § 72.05-50 for ventilation requirements pertaining to structural fire protection....

  19. 46 CFR 188.15-5 - Design of vessels.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 7 2013-10-01 2013-10-01 false Design of vessels. 188.15-5 Section 188.15-5 Shipping... PROVISIONS Equivalents § 188.15-5 Design of vessels. (a) In order not to inhibit design and application the Commandant may accept vessels of unusual, unique, special, or exotic design, both new and for...

  20. 46 CFR 188.15-5 - Design of vessels.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 7 2012-10-01 2012-10-01 false Design of vessels. 188.15-5 Section 188.15-5 Shipping... PROVISIONS Equivalents § 188.15-5 Design of vessels. (a) In order not to inhibit design and application the Commandant may accept vessels of unusual, unique, special, or exotic design, both new and for...

  1. 46 CFR 188.15-5 - Design of vessels.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 7 2014-10-01 2014-10-01 false Design of vessels. 188.15-5 Section 188.15-5 Shipping... PROVISIONS Equivalents § 188.15-5 Design of vessels. (a) In order not to inhibit design and application the Commandant may accept vessels of unusual, unique, special, or exotic design, both new and for...

  2. 46 CFR 168.15-5 - Location of crew spaces.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 7 2010-10-01 2010-10-01 false Location of crew spaces. 168.15-5 Section 168.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS CIVILIAN NAUTICAL SCHOOL VESSELS Accommodations § 168.15-5 Location of crew spaces. (a) Quarters must be located so that...

  3. 46 CFR 61.15-5 - Steam piping.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 2 2011-10-01 2011-10-01 false Steam piping. 61.15-5 Section 61.15-5 Shipping COAST... Periodic Tests of Piping Systems § 61.15-5 Steam piping. (a) Main steam piping shall be subjected to a... removed and the piping thoroughly examined. (b) All steam piping subject to pressure from the main...

  4. 46 CFR 61.15-5 - Steam piping.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 2 2014-10-01 2014-10-01 false Steam piping. 61.15-5 Section 61.15-5 Shipping COAST... Periodic Tests of Piping Systems § 61.15-5 Steam piping. (a) Main steam piping shall be subjected to a... removed and the piping thoroughly examined. (b) All steam piping subject to pressure from the main...

  5. 46 CFR 61.15-5 - Steam piping.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 2 2013-10-01 2013-10-01 false Steam piping. 61.15-5 Section 61.15-5 Shipping COAST... Periodic Tests of Piping Systems § 61.15-5 Steam piping. (a) Main steam piping shall be subjected to a... removed and the piping thoroughly examined. (b) All steam piping subject to pressure from the main...

  6. 46 CFR 61.15-5 - Steam piping.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 2 2010-10-01 2010-10-01 false Steam piping. 61.15-5 Section 61.15-5 Shipping COAST... Periodic Tests of Piping Systems § 61.15-5 Steam piping. (a) Main steam piping shall be subjected to a... removed and the piping thoroughly examined. (b) All steam piping subject to pressure from the main...

  7. 46 CFR 61.15-5 - Steam piping.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 2 2012-10-01 2012-10-01 false Steam piping. 61.15-5 Section 61.15-5 Shipping COAST... Periodic Tests of Piping Systems § 61.15-5 Steam piping. (a) Main steam piping shall be subjected to a... removed and the piping thoroughly examined. (b) All steam piping subject to pressure from the main...

  8. 43 CFR 1.5 - Signature to constitute certificate.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 43 Public Lands: Interior 1 2010-10-01 2010-10-01 false Signature to constitute certificate. 1.5 Section 1.5 Public Lands: Interior Office of the Secretary of the Interior PRACTICES BEFORE THE DEPARTMENT OF THE INTERIOR § 1.5 Signature to constitute certificate. When an individual who appears in a representative capacity signs a paper in...

  9. 46 CFR 46.15-5 - Engineering requirements.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 2 2011-10-01 2011-10-01 false Engineering requirements. 46.15-5 Section 46.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) LOAD LINES SUBDIVISION LOAD LINES FOR PASSENGER VESSELS Subdivision Load Lines for Passenger Vessels Engaged in Foreign, Coastwise, and Great Lakes Voyages § 46.15-5 Engineering...

  10. 46 CFR 46.15-5 - Engineering requirements.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 2 2014-10-01 2014-10-01 false Engineering requirements. 46.15-5 Section 46.15-5... Lakes Voyages § 46.15-5 Engineering requirements. (a) Bilge and ballast systems, piping, inlets and... subchapter F (Marine Engineering) of this chapter....

  11. 46 CFR 46.15-5 - Engineering requirements.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 2 2012-10-01 2012-10-01 false Engineering requirements. 46.15-5 Section 46.15-5... Lakes Voyages § 46.15-5 Engineering requirements. (a) Bilge and ballast systems, piping, inlets and... subchapter F (Marine Engineering) of this chapter....

  12. 46 CFR 46.15-5 - Engineering requirements.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 2 2013-10-01 2013-10-01 false Engineering requirements. 46.15-5 Section 46.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) LOAD LINES SUBDIVISION LOAD LINES FOR PASSENGER VESSELS Subdivision Load Lines for Passenger Vessels Engaged in Foreign, Coastwise, and Great Lakes Voyages § 46.15-5 Engineering...

  13. 47 CFR 15.5 - General conditions of operation.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 1 2012-10-01 2012-10-01 false General conditions of operation. 15.5 Section 15.5 Telecommunication FEDERAL COMMUNICATIONS COMMISSION GENERAL RADIO FREQUENCY DEVICES General § 15.5 General conditions of operation. (a) Persons operating intentional or unintentional radiators shall not be deemed to have any vested...

  14. 47 CFR 15.5 - General conditions of operation.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 1 2011-10-01 2011-10-01 false General conditions of operation. 15.5 Section 15.5 Telecommunication FEDERAL COMMUNICATIONS COMMISSION GENERAL RADIO FREQUENCY DEVICES General § 15.5 General conditions of operation. (a) Persons operating intentional or unintentional radiators shall not be deemed to have any vested...

  15. 46 CFR 46.15-5 - Engineering requirements.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 2 2010-10-01 2010-10-01 false Engineering requirements. 46.15-5 Section 46.15-5... Lakes Voyages § 46.15-5 Engineering requirements. (a) Bilge and ballast systems, piping, inlets and... subchapter F (Marine Engineering) of this chapter....

  16. 46 CFR 167.15-5 - Authority of marine inspectors.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 7 2010-10-01 2010-10-01 false Authority of marine inspectors. 167.15-5 Section 167.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS PUBLIC NAUTICAL SCHOOL SHIPS Inspections § 167.15-5 Authority of marine inspectors. Marine inspectors may at any...

  17. 46 CFR 91.15-5 - Alternate compliance.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... CFR 8.110(b). ... 46 Shipping 4 2013-10-01 2013-10-01 false Alternate compliance. 91.15-5 Section 91.15-5 Shipping... CERTIFICATION Inspection of Vessels § 91.15-5 Alternate compliance. (a) In place of compliance with...

  18. 46 CFR 72.15-5 - Structural fire protection.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 3 2013-10-01 2013-10-01 false Structural fire protection. 72.15-5 Section 72.15-5... ARRANGEMENT Ventilation § 72.15-5 Structural fire protection. See § 72.05-50 for ventilation requirements pertaining to structural fire protection....

  19. 46 CFR 72.15-5 - Structural fire protection.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 3 2011-10-01 2011-10-01 false Structural fire protection. 72.15-5 Section 72.15-5... ARRANGEMENT Ventilation § 72.15-5 Structural fire protection. See § 72.05-50 for ventilation requirements pertaining to structural fire protection....

  20. 46 CFR 167.15-5 - Authority of marine inspectors.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 7 2011-10-01 2011-10-01 false Authority of marine inspectors. 167.15-5 Section 167.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS PUBLIC NAUTICAL SCHOOL SHIPS Inspections § 167.15-5 Authority of marine inspectors. Marine inspectors may at any...

  1. 46 CFR 167.15-5 - Authority of marine inspectors.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 7 2012-10-01 2012-10-01 false Authority of marine inspectors. 167.15-5 Section 167.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS PUBLIC NAUTICAL SCHOOL SHIPS Inspections § 167.15-5 Authority of marine inspectors. Marine inspectors may at any...

  2. 46 CFR 167.15-5 - Authority of marine inspectors.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 7 2013-10-01 2013-10-01 false Authority of marine inspectors. 167.15-5 Section 167.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS PUBLIC NAUTICAL SCHOOL SHIPS Inspections § 167.15-5 Authority of marine inspectors. Marine inspectors may at any...

  3. 46 CFR 167.15-5 - Authority of marine inspectors.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 7 2014-10-01 2014-10-01 false Authority of marine inspectors. 167.15-5 Section 167.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS PUBLIC NAUTICAL SCHOOL SHIPS Inspections § 167.15-5 Authority of marine inspectors. Marine inspectors may at any...

  4. 46 CFR 188.15-5 - Design of vessels.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 7 2010-10-01 2010-10-01 false Design of vessels. 188.15-5 Section 188.15-5 Shipping... PROVISIONS Equivalents § 188.15-5 Design of vessels. (a) In order not to inhibit design and application the Commandant may accept vessels of unusual, unique, special, or exotic design, both new and for...

  5. 46 CFR 168.15-5 - Location of crew spaces.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 7 2012-10-01 2012-10-01 false Location of crew spaces. 168.15-5 Section 168.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS CIVILIAN NAUTICAL SCHOOL VESSELS Accommodations § 168.15-5 Location of crew spaces. (a) Quarters must be located so that...

  6. 46 CFR 168.15-5 - Location of crew spaces.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 7 2014-10-01 2014-10-01 false Location of crew spaces. 168.15-5 Section 168.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS CIVILIAN NAUTICAL SCHOOL VESSELS Accommodations § 168.15-5 Location of crew spaces. (a) Quarters must be located so that...

  7. 46 CFR 168.15-5 - Location of crew spaces.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 7 2013-10-01 2013-10-01 false Location of crew spaces. 168.15-5 Section 168.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS CIVILIAN NAUTICAL SCHOOL VESSELS Accommodations § 168.15-5 Location of crew spaces. (a) Quarters must be located so that...

  8. 46 CFR 111.15-5 - Battery installation.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false Battery installation. 111.15-5 Section 111.15-5 Shipping... REQUIREMENTS Storage Batteries and Battery Chargers: Construction and Installation § 111.15-5 Battery installation. (a) Large batteries. Each large battery installation must be in a room that is only for...

  9. 46 CFR 111.15-5 - Battery installation.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Battery installation. 111.15-5 Section 111.15-5 Shipping... REQUIREMENTS Storage Batteries and Battery Chargers: Construction and Installation § 111.15-5 Battery installation. (a) Large batteries. Each large battery installation must be in a room that is only for...

  10. 46 CFR 111.15-5 - Battery installation.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false Battery installation. 111.15-5 Section 111.15-5 Shipping... REQUIREMENTS Storage Batteries and Battery Chargers: Construction and Installation § 111.15-5 Battery installation. (a) Large batteries. Each large battery installation must be in a room that is only for...

  11. 46 CFR 111.15-5 - Battery installation.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Battery installation. 111.15-5 Section 111.15-5 Shipping... REQUIREMENTS Storage Batteries and Battery Chargers: Construction and Installation § 111.15-5 Battery installation. (a) Large batteries. Each large battery installation must be in a room that is only for...

  12. 46 CFR 111.15-5 - Battery installation.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false Battery installation. 111.15-5 Section 111.15-5 Shipping... REQUIREMENTS Storage Batteries and Battery Chargers: Construction and Installation § 111.15-5 Battery installation. (a) Large batteries. Each large battery installation must be in a room that is only for...

  13. 46 CFR 42.15-5 - Superstructure end bulkheads.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 2 2010-10-01 2010-10-01 false Superstructure end bulkheads. 42.15-5 Section 42.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) LOAD LINES DOMESTIC AND FOREIGN VOYAGES BY SEA Conditions of Assignment of Freeboard § 42.15-5 Superstructure end bulkheads. (a) Bulkheads at exposed ends of enclosed...

  14. 46 CFR 71.15-5 - Alternate compliance.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... rules and supplements are incorporated by reference into 46 CFR 8.110(b). ... 46 Shipping 3 2010-10-01 2010-10-01 false Alternate compliance. 71.15-5 Section 71.15-5 Shipping... Inspection of Vessels § 71.15-5 Alternate compliance. (a) In place of compliance with other...

  15. 46 CFR 71.15-5 - Alternate compliance.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... rules and supplements are incorporated by reference into 46 CFR 8.110(b). ... 46 Shipping 3 2012-10-01 2012-10-01 false Alternate compliance. 71.15-5 Section 71.15-5 Shipping... Inspection of Vessels § 71.15-5 Alternate compliance. (a) In place of compliance with other...

  16. 46 CFR 91.15-5 - Alternate compliance.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    .... Approved classification society rules and supplements are incorporated by reference into 46 CFR 8.110(b). ... 46 Shipping 4 2012-10-01 2012-10-01 false Alternate compliance. 91.15-5 Section 91.15-5 Shipping... CERTIFICATION Inspection of Vessels § 91.15-5 Alternate compliance. (a) In place of compliance with...

  17. 46 CFR 91.15-5 - Alternate compliance.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    .... Approved classification society rules and supplements are incorporated by reference into 46 CFR 8.110(b). ... 46 Shipping 4 2011-10-01 2011-10-01 false Alternate compliance. 91.15-5 Section 91.15-5 Shipping... CERTIFICATION Inspection of Vessels § 91.15-5 Alternate compliance. (a) In place of compliance with...

  18. 46 CFR 91.15-5 - Alternate compliance.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    .... Approved classification society rules and supplements are incorporated by reference into 46 CFR 8.110(b). ... 46 Shipping 4 2010-10-01 2010-10-01 false Alternate compliance. 91.15-5 Section 91.15-5 Shipping... CERTIFICATION Inspection of Vessels § 91.15-5 Alternate compliance. (a) In place of compliance with...

  19. 46 CFR 71.15-5 - Alternate compliance.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... rules and supplements are incorporated by reference into 46 CFR 8.110(b). ... 46 Shipping 3 2011-10-01 2011-10-01 false Alternate compliance. 71.15-5 Section 71.15-5 Shipping... Inspection of Vessels § 71.15-5 Alternate compliance. (a) In place of compliance with other...

  20. 46 CFR 168.15-5 - Location of crew spaces.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 7 2011-10-01 2011-10-01 false Location of crew spaces. 168.15-5 Section 168.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) NAUTICAL SCHOOLS CIVILIAN NAUTICAL SCHOOL VESSELS Accommodations § 168.15-5 Location of crew spaces. (a) Quarters must be located so that...

  1. Manganese [III] Tetrakis [5,10,15,20]-Benzoic Acid Porphyrin Reduces Adiposity and Improves Insulin Action in Mice with Pre-Existing Obesity

    PubMed Central

    Brestoff, Jonathan R.; Brodsky, Tim; Sosinsky, Alexandra Z.; McLoughlin, Ryan; Stansky, Elena; Fussell, Leila; Sheppard, Aaron; DiSanto-Rose, Maria; Kershaw, Erin E.; Reynolds, Thomas H.

    2015-01-01

    The superoxide dismutase mimetic manganese [III] tetrakis [5,10,15,20]-benzoic acid porphyrin (MnTBAP) is a potent antioxidant compound that has been shown to limit weight gain during short-term high fat feeding without preventing insulin resistance. However, whether MnTBAP has therapeutic potential to treat pre-existing obesity and insulin resistance remains unknown. To investigate this, mice were treated with MnTBAP or vehicle during the last five weeks of a 24-week high fat diet (HFD) regimen. MnTBAP treatment significantly decreased body weight and reduced white adipose tissue (WAT) mass in mice fed a HFD and a low fat diet (LFD). The reduction in adiposity was associated with decreased caloric intake without significantly altering energy expenditure, indicating that MnTBAP decreases adiposity in part by modulating energy balance. MnTBAP treatment also improved insulin action in HFD-fed mice, a physiologic response that was associated with increased protein kinase B (PKB) phosphorylation and expression in muscle and WAT. Since MnTBAP is a metalloporphyrin molecule, we hypothesized that its ability to promote weight loss and improve insulin sensitivity was regulated by heme oxygenase-1 (HO-1), in a similar fashion as cobalt protoporphyrins. Despite MnTBAP treatment increasing HO-1 expression, administration of the potent HO-1 inhibitor tin mesoporphyrin (SnMP) did not block the ability of MnTBAP to alter caloric intake, adiposity, or insulin action, suggesting that MnTBAP influences these metabolic processes independent of HO-1. These data demonstrate that MnTBAP can ameliorate pre-existing obesity and improve insulin action by reducing caloric intake and increasing PKB phosphorylation and expression. PMID:26397111

  2. Manganese [III] Tetrakis [5,10,15,20]-Benzoic Acid Porphyrin Reduces Adiposity and Improves Insulin Action in Mice with Pre-Existing Obesity.

    PubMed

    Brestoff, Jonathan R; Brodsky, Tim; Sosinsky, Alexandra Z; McLoughlin, Ryan; Stansky, Elena; Fussell, Leila; Sheppard, Aaron; DiSanto-Rose, Maria; Kershaw, Erin E; Reynolds, Thomas H

    2015-01-01

    The superoxide dismutase mimetic manganese [III] tetrakis [5,10,15,20]-benzoic acid porphyrin (MnTBAP) is a potent antioxidant compound that has been shown to limit weight gain during short-term high fat feeding without preventing insulin resistance. However, whether MnTBAP has therapeutic potential to treat pre-existing obesity and insulin resistance remains unknown. To investigate this, mice were treated with MnTBAP or vehicle during the last five weeks of a 24-week high fat diet (HFD) regimen. MnTBAP treatment significantly decreased body weight and reduced white adipose tissue (WAT) mass in mice fed a HFD and a low fat diet (LFD). The reduction in adiposity was associated with decreased caloric intake without significantly altering energy expenditure, indicating that MnTBAP decreases adiposity in part by modulating energy balance. MnTBAP treatment also improved insulin action in HFD-fed mice, a physiologic response that was associated with increased protein kinase B (PKB) phosphorylation and expression in muscle and WAT. Since MnTBAP is a metalloporphyrin molecule, we hypothesized that its ability to promote weight loss and improve insulin sensitivity was regulated by heme oxygenase-1 (HO-1), in a similar fashion as cobalt protoporphyrins. Despite MnTBAP treatment increasing HO-1 expression, administration of the potent HO-1 inhibitor tin mesoporphyrin (SnMP) did not block the ability of MnTBAP to alter caloric intake, adiposity, or insulin action, suggesting that MnTBAP influences these metabolic processes independent of HO-1. These data demonstrate that MnTBAP can ameliorate pre-existing obesity and improve insulin action by reducing caloric intake and increasing PKB phosphorylation and expression. PMID:26397111

  3. High accuracy {sup 18}O(p,{alpha}){sup 15}N reaction rate in the 8{center_dot}10{sup 6}-5{center_dot}10{sup 9} K temperature range

    SciTech Connect

    La Cognata, M.; Spitaleri, C.; Cherubini, S.; Crucilla, V.; Gulino, M.; Kiss, G. G.; Lamia, L.; Pizzone, R. G.; Puglia, S. M. R.; Rapisarda, G. G.; Romano, S.; Sergi, M. L.; Mukhamedzhanov, A.; Banu, A.; Goldberg, V.; Tabacaru, G.; Trache, L.; Tribble, R. E.; Coc, A.

    2011-10-28

    The {sup 18}O(p,{alpha}){sup 15}N reaction is of great importance in several astrophysical scenarios, as it influences the production of key isotopes such as {sup 19}F, {sup 18}O and {sup 15}N. In this work, a high accuracy {sup 18}O(p,{alpha}){sup 15}N reaction rate is proposed, based on the simultaneous fit of direct measurements and of the results of a new Trojan Horse experiment. In particular, we have focused on the study of the broad 660 keV 1/2{sup +} resonance. Since {Gamma}{approx}100-300 keV, it strongly influences the nearly-zero-energy region of the cross section by means of the low-energy tail of the resonant contribution and dominates the cross section at higher energies. Here we provide a factor of 2 larger reaction rate above T{approx}0.5 10{sup 9} K based over our new improved determination of its resonance parameters.

  4. 15 CFR 923.10 - General.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 3 2010-01-01 2010-01-01 false General. 923.10 Section 923.10 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) NATIONAL OCEANIC AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE OCEAN AND COASTAL RESOURCE MANAGEMENT COASTAL ZONE MANAGEMENT PROGRAM REGULATIONS Uses...

  5. 15 CFR 922.10 - General.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 3 2011-01-01 2011-01-01 false General. 922.10 Section 922.10 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) NATIONAL OCEANIC AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE OCEAN AND COASTAL RESOURCE MANAGEMENT NATIONAL MARINE SANCTUARY PROGRAM REGULATIONS...

  6. 15 CFR 923.10 - General.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 15 Commerce and Foreign Trade 3 2012-01-01 2012-01-01 false General. 923.10 Section 923.10 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) NATIONAL OCEANIC AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE OCEAN AND COASTAL RESOURCE MANAGEMENT COASTAL ZONE MANAGEMENT PROGRAM REGULATIONS Uses...

  7. 15 CFR 2008.10 - Declassification authority.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 15 Commerce and Foreign Trade 3 2014-01-01 2014-01-01 false Declassification authority. 2008.10 Section 2008.10 Commerce and Foreign Trade Regulations Relating to Foreign Trade Agreements OFFICE OF THE UNITED STATES TRADE REPRESENTATIVE REGULATIONS TO IMPLEMENT E.O. 12065; OFFICE OF THE UNITED STATES...

  8. 15 CFR 2008.10 - Declassification authority.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 3 2011-01-01 2011-01-01 false Declassification authority. 2008.10 Section 2008.10 Commerce and Foreign Trade Regulations Relating to Foreign Trade Agreements OFFICE OF THE UNITED STATES TRADE REPRESENTATIVE REGULATIONS TO IMPLEMENT E.O. 12065; OFFICE OF THE UNITED STATES...

  9. 15 CFR 2008.10 - Declassification authority.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 15 Commerce and Foreign Trade 3 2012-01-01 2012-01-01 false Declassification authority. 2008.10 Section 2008.10 Commerce and Foreign Trade Regulations Relating to Foreign Trade Agreements OFFICE OF THE UNITED STATES TRADE REPRESENTATIVE REGULATIONS TO IMPLEMENT E.O. 12065; OFFICE OF THE UNITED STATES...

  10. 15 CFR 2008.10 - Declassification authority.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 3 2010-01-01 2010-01-01 false Declassification authority. 2008.10 Section 2008.10 Commerce and Foreign Trade Regulations Relating to Foreign Trade Agreements OFFICE OF THE UNITED STATES TRADE REPRESENTATIVE REGULATIONS TO IMPLEMENT E.O. 12065; OFFICE OF THE UNITED STATES...

  11. 15 CFR 2008.10 - Declassification authority.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 15 Commerce and Foreign Trade 3 2013-01-01 2013-01-01 false Declassification authority. 2008.10 Section 2008.10 Commerce and Foreign Trade Regulations Relating to Foreign Trade Agreements OFFICE OF THE UNITED STATES TRADE REPRESENTATIVE REGULATIONS TO IMPLEMENT E.O. 12065; OFFICE OF THE UNITED STATES...

  12. 10 CFR 810.15 - Violations.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... ENERGY ASSISTANCE TO FOREIGN ATOMIC ENERGY ACTIVITIES § 810.15 Violations. (a) The Atomic Energy Act... person from violating any provision of the Atomic Energy Act or its implementing regulations. (2) Any... Atomic Energy Act may be fined up to $10,000 or imprisoned up to 10 years, or both. If the offense...

  13. 10 CFR 810.15 - Violations.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... ENERGY ASSISTANCE TO FOREIGN ATOMIC ENERGY ACTIVITIES § 810.15 Violations. (a) The Atomic Energy Act... person from violating any provision of the Atomic Energy Act or its implementing regulations. (2) Any... Atomic Energy Act may be fined up to $10,000 or imprisoned up to 10 years, or both. If the offense...

  14. 15 CFR 14.10 - Purpose.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 1 2010-01-01 2010-01-01 false Purpose. 14.10 Section 14.10 Commerce and Foreign Trade Office of the Secretary of Commerce UNIFORM ADMINISTRATIVE REQUIREMENTS FOR GRANTS AND AGREEMENTS WITH INSTITUTIONS OF HIGHER EDUCATION, HOSPITALS, OTHER NON-PROFIT, AND COMMERCIAL ORGANIZATIONS Pre-Award Requirements §...

  15. 15 CFR 20.10 - Compliance reviews.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 15 Commerce and Foreign Trade 1 2013-01-01 2013-01-01 false Compliance reviews. 20.10 Section 20... AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 20.10 Compliance reviews. (a) DOC may conduct compliance reviews and...

  16. 15 CFR 20.10 - Compliance reviews.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 15 Commerce and Foreign Trade 1 2012-01-01 2012-01-01 false Compliance reviews. 20.10 Section 20... AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 20.10 Compliance reviews. (a) DOC may conduct compliance reviews and...

  17. 15 CFR 20.10 - Compliance reviews.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 1 2010-01-01 2010-01-01 false Compliance reviews. 20.10 Section 20... AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 20.10 Compliance reviews. (a) DOC may conduct compliance reviews and...

  18. 15 CFR 20.10 - Compliance reviews.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 15 Commerce and Foreign Trade 1 2014-01-01 2014-01-01 false Compliance reviews. 20.10 Section 20... AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 20.10 Compliance reviews. (a) DOC may conduct compliance reviews and...

  19. 15 CFR 20.10 - Compliance reviews.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 1 2011-01-01 2011-01-01 false Compliance reviews. 20.10 Section 20... AGE IN PROGRAMS OR ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE Investigation, Conciliation, and Enforcement Procedures § 20.10 Compliance reviews. (a) DOC may conduct compliance reviews and...

  20. 15 CFR 923.10 - General.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 3 2011-01-01 2011-01-01 false General. 923.10 Section 923.10 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) NATIONAL OCEANIC AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE OCEAN AND COASTAL RESOURCE MANAGEMENT COASTAL ZONE MANAGEMENT PROGRAM REGULATIONS Uses...

  1. 15 CFR 923.10 - General.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 15 Commerce and Foreign Trade 3 2013-01-01 2013-01-01 false General. 923.10 Section 923.10 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) NATIONAL OCEANIC AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE OCEAN AND COASTAL RESOURCE MANAGEMENT COASTAL ZONE MANAGEMENT PROGRAM REGULATIONS Uses...

  2. 10. "TEST STAND 15, AIR FORCE FLIGHT TEST CENTER." ca. ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    10. "TEST STAND 1-5, AIR FORCE FLIGHT TEST CENTER." ca. 1958. Test Area 1-115. Original is a color print, showing Test Stand 1-5 from below, also showing the superstructure of TS1-4 at left. - Edwards Air Force Base, Air Force Rocket Propulsion Laboratory, Leuhman Ridge near Highways 58 & 395, Boron, Kern County, CA

  3. 46 CFR 105.15-5 - Authority of marine inspectors.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Authority of marine inspectors. 105.15-5 Section 105.15... COMMERCIAL FISHING VESSELS DISPENSING PETROLEUM PRODUCTS Inspection Required § 105.15-5 Authority of marine inspectors. (a) Marine inspectors may at any time lawfully inspect any vessel subject to the requirements...

  4. 46 CFR 105.15-5 - Authority of marine inspectors.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false Authority of marine inspectors. 105.15-5 Section 105.15... COMMERCIAL FISHING VESSELS DISPENSING PETROLEUM PRODUCTS Inspection Required § 105.15-5 Authority of marine inspectors. (a) Marine inspectors may at any time lawfully inspect any vessel subject to the requirements...

  5. 46 CFR 105.15-5 - Authority of marine inspectors.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false Authority of marine inspectors. 105.15-5 Section 105.15... COMMERCIAL FISHING VESSELS DISPENSING PETROLEUM PRODUCTS Inspection Required § 105.15-5 Authority of marine inspectors. (a) Marine inspectors may at any time lawfully inspect any vessel subject to the requirements...

  6. 46 CFR 105.15-5 - Authority of marine inspectors.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Authority of marine inspectors. 105.15-5 Section 105.15... COMMERCIAL FISHING VESSELS DISPENSING PETROLEUM PRODUCTS Inspection Required § 105.15-5 Authority of marine inspectors. (a) Marine inspectors may at any time lawfully inspect any vessel subject to the requirements...

  7. 46 CFR 105.15-5 - Authority of marine inspectors.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false Authority of marine inspectors. 105.15-5 Section 105.15... COMMERCIAL FISHING VESSELS DISPENSING PETROLEUM PRODUCTS Inspection Required § 105.15-5 Authority of marine inspectors. (a) Marine inspectors may at any time lawfully inspect any vessel subject to the requirements...

  8. Low frequency noise in magnetic tunneling junctions with Co40Fe40B20/Co70.5Fe4.5Si15B10 composite free layer

    NASA Astrophysics Data System (ADS)

    Yuan, Z. H.; Feng, J. F.; Guo, Peng; Wan, C. H.; Wei, H. X.; Ali, S. S.; Han, X. F.; Nakano, T.; Naganuma, H.; Ando, Y.

    2016-01-01

    Magnetic tunneling junctions with Co40Fe40B20/Co70.5Fe4.5Si15B10 composite free layer have been fabricated and annealed at different temperatures to obtain the highest tunneling magnetoresistance. The field and temperature dependences of the low frequency noise have been measured to understand the origin of noise. The random telegraph noise has been observed at low magnetic field, and the corresponding fluctuating moment is estimated to be 4.8×105 μB with an effective area of 240 nm2. The dependence of noise on temperature was coincident with the thermally activated kinetics model above 30 K while it deviated from this model below 30 K. Studying the origin of the low frequency noise is helpful to reduce the noise level in MTJs.

  9. 46 CFR 188.10-15 - Coastwise.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS GENERAL PROVISIONS Definition of Terms Used in This Subchapter § 188.10-15 Coastwise. Under this designation shall be included all vessels normally navigating the waters of any ocean or the Gulf of Mexico 20 nautical miles...

  10. 46 CFR 193.15-10 - Controls.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... EQUIPMENT Carbon Dioxide Extinguishing Systems, Details § 193.15-10 Controls. (a) Except as noted in § 193..., a manifold with normally closed stop valves shall be used to direct the carbon dioxide into the...) which contain not more than 300 pounds of carbon dioxide. (c) One of the stations controlling the...

  11. 46 CFR 193.15-10 - Controls.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... EQUIPMENT Carbon Dioxide Extinguishing Systems, Details § 193.15-10 Controls. (a) Except as noted in § 193..., a manifold with normally closed stop valves shall be used to direct the carbon dioxide into the...) which contain not more than 300 pounds of carbon dioxide. (c) One of the stations controlling the...

  12. 46 CFR 111.15-10 - Ventilation.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... REQUIREMENTS Storage Batteries and Battery Chargers: Construction and Installation § 111.15-10 Ventilation. (a) General. Each room, locker, and box for storage batteries must be arranged or ventilated to prevent... with the battery charger so that the battery cannot be charged without ventilation. (c) Large...

  13. 46 CFR 111.15-10 - Ventilation.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... REQUIREMENTS Storage Batteries and Battery Chargers: Construction and Installation § 111.15-10 Ventilation. (a) General. Each room, locker, and box for storage batteries must be arranged or ventilated to prevent... with the battery charger so that the battery cannot be charged without ventilation. (c) Large...

  14. 46 CFR 111.15-10 - Ventilation.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... REQUIREMENTS Storage Batteries and Battery Chargers: Construction and Installation § 111.15-10 Ventilation. (a) General. Each room, locker, and box for storage batteries must be arranged or ventilated to prevent... with the battery charger so that the battery cannot be charged without ventilation. (c) Large...

  15. 46 CFR 111.15-10 - Ventilation.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... REQUIREMENTS Storage Batteries and Battery Chargers: Construction and Installation § 111.15-10 Ventilation. (a) General. Each room, locker, and box for storage batteries must be arranged or ventilated to prevent... with the battery charger so that the battery cannot be charged without ventilation. (c) Large...

  16. 46 CFR 111.15-10 - Ventilation.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... REQUIREMENTS Storage Batteries and Battery Chargers: Construction and Installation § 111.15-10 Ventilation. (a) General. Each room, locker, and box for storage batteries must be arranged or ventilated to prevent... with the battery charger so that the battery cannot be charged without ventilation. (c) Large...

  17. 46 CFR 188.10-15 - Coastwise.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS GENERAL PROVISIONS Definition of Terms Used in This Subchapter § 188.10-15 Coastwise. Under this designation shall be included all vessels normally navigating the waters of any ocean or the Gulf of Mexico 20 nautical miles...

  18. 46 CFR 188.10-15 - Coastwise.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS GENERAL PROVISIONS Definition of Terms Used in This Subchapter § 188.10-15 Coastwise. Under this designation shall be included all vessels normally navigating the waters of any ocean or the Gulf of Mexico 20 nautical miles...

  19. 34 CFR 5.15 - Creation of records.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false Creation of records. 5.15 Section 5.15 Education Office of the Secretary, Department of Education AVAILABILITY OF INFORMATION TO THE PUBLIC PURSUANT TO PUB. L. 90-23 (Eff. until 7-14-10) What Records Are Available § 5.15 Creation of records. Records are...

  20. Sol-gel synthesis of quaternary (P2O5)55-(CaO)25-(Na2O)(20-x)-(TiO2) x bioresorbable glasses for bone tissue engineering applications (x = 0, 5, 10, or 15).

    PubMed

    Foroutan, Farzad; Walters, Nick J; Owens, Gareth J; Mordan, Nicola J; Kim, Hae-Won; de Leeuw, Nora H; Knowles, Jonathan C

    2015-08-01

    In the present study, we report a new and facile sol-gel synthesis of phosphate-based glasses with the general formula of (P2O5)55-(CaO)25-(Na2O)(20-x)-(TiO2) x , where x = 0, 5, 10 or 15, for bone tissue engineering applications. The sol-gel synthesis method allows greater control over glass morphology at relatively low processing temperature (200 °C) in comparison with phosphate-based melt-derived glasses (~1000 °C). The glasses were analyzed using several characterization techniques, including x-ray diffraction (XRD), (31)P magic angle spinning nuclear magnetic resonance ((31)P MAS-NMR), Fourier transform infrared (FTIR) spectroscopy and energy-dispersive x-ray (EDX) spectroscopy, which confirmed the amorphous and glassy nature of the prepared samples. Degradation was assessed by measuring the ion release and pH change of the storage medium. Cytocompatibility was also confirmed by culturing osteoblast-like osteosarcoma cell line MG-63 on the glass microparticles over a seven-day period. Cell attachment to the particles was imaged using scanning electron microscopy (SEM) and confocal laser scanning microscopy (CLSM). The results revealed the potential of phosphate-based sol-gel derived glasses containing 5 or 10 mol% TiO2, with high surface area, ideal dissolution rate for cell attachment and easily metabolized dissolution products, for bone tissue engineering applications. PMID:26306553

  1. 16 CFR 1.5 - Purpose.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 16 Commercial Practices 1 2012-01-01 2012-01-01 false Purpose. 1.5 Section 1.5 Commercial Practices FEDERAL TRADE COMMISSION ORGANIZATION, PROCEDURES AND RULES OF PRACTICE GENERAL PROCEDURES Industry Guidance Industry Guides § 1.5 Purpose. Industry guides are administrative interpretations of...

  2. 7 CFR 15b.5 - Assurances required.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 1 2010-01-01 2010-01-01 false Assurances required. 15b.5 Section 15b.5 Agriculture... ACTIVITIES RECEIVING FEDERAL FINANCIAL ASSISTANCE General Provisions § 15b.5 Assurances required. (a) Assurances. An applicant for Federal financial assistance to which this part applies shall submit...

  3. 30 CFR 15.5 - Test samples.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 30 Mineral Resources 1 2010-07-01 2010-07-01 false Test samples. 15.5 Section 15.5 Mineral... § 15.5 Test samples. (a) Submission of test samples. (1) The applicant shall not submit explosives or... magazine for at least 30 days before gallery tests are conducted....

  4. 30 CFR 15.5 - Test samples.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 30 Mineral Resources 1 2011-07-01 2011-07-01 false Test samples. 15.5 Section 15.5 Mineral... § 15.5 Test samples. (a) Submission of test samples. (1) The applicant shall not submit explosives or... magazine for at least 30 days before gallery tests are conducted....

  5. 30 CFR 15.5 - Test samples.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 30 Mineral Resources 1 2013-07-01 2013-07-01 false Test samples. 15.5 Section 15.5 Mineral... § 15.5 Test samples. (a) Submission of test samples. (1) The applicant shall not submit explosives or... magazine for at least 30 days before gallery tests are conducted....

  6. 7 CFR 15.5 - Compliance.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... financial assistance to any other recipient, such other recipient shall also submit such compliance reports... 7 Agriculture 1 2010-01-01 2010-01-01 false Compliance. 15.5 Section 15.5 Agriculture Office of... Department of Agriculture-Effectuation of Title VI of the Civil Rights Act of 1964 § 15.5 Compliance....

  7. 7 CFR 15.5 - Compliance.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... financial assistance to any other recipient, such other recipient shall also submit such compliance reports... 7 Agriculture 1 2013-01-01 2013-01-01 false Compliance. 15.5 Section 15.5 Agriculture Office of... Department of Agriculture-Effectuation of Title VI of the Civil Rights Act of 1964 § 15.5 Compliance....

  8. 7 CFR 15.5 - Compliance.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... financial assistance to any other recipient, such other recipient shall also submit such compliance reports... 7 Agriculture 1 2014-01-01 2014-01-01 false Compliance. 15.5 Section 15.5 Agriculture Office of... Department of Agriculture-Effectuation of Title VI of the Civil Rights Act of 1964 § 15.5 Compliance....

  9. 7 CFR 15.5 - Compliance.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 1 2011-01-01 2011-01-01 false Compliance. 15.5 Section 15.5 Agriculture Office of the Secretary of Agriculture NONDISCRIMINATION Nondiscrimination in Federally-Assisted Programs of the Department of Agriculture-Effectuation of Title VI of the Civil Rights Act of 1964 § 15.5 Compliance. (a) Cooperation and assistance. Each...

  10. 7 CFR 15.5 - Compliance.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... financial assistance to any other recipient, such other recipient shall also submit such compliance reports... 7 Agriculture 1 2012-01-01 2012-01-01 false Compliance. 15.5 Section 15.5 Agriculture Office of... Department of Agriculture-Effectuation of Title VI of the Civil Rights Act of 1964 § 15.5 Compliance....

  11. Hole transporting material 5, 10, 15-tribenzyl-5H-diindolo[3, 2-a:3‧, 2‧-c]-carbazole for efficient optoelectronic applications as an active layer

    NASA Astrophysics Data System (ADS)

    Zheng, Yan-Qiong; J. Potscavage, William, Jr.; Zhang, Jian-Hua; Wei, Bin; Huang, Rong-Juan

    2015-02-01

    In order to explore the novel application of the transparent hole-transporting material 5,10,15-tribenzyl-5H-diindolo[3,2-a:3‧,2‧-c]-carbazole (TBDI), in this article TBDI is used as an active layer but not a buffer layer in a photodetector (PD), organic light-emitting diode (OLED), and organic photovoltaic cell (OPV) for the first time. Firstly, the absorption and emission spectra of a blend layer comprised of TBDI and electron-transporting material bis-(2-methyl-8-quinolinate) 4-phenylphenolate (BAlq) are investigated. Based on the absorption properties, an organic PD with a peak absorption at 320 nm is fabricated, and a relatively-high detectivity of 2.44 × 1011 cm·Hz1/2/W under 320-nm illumination is obtained. The TBDI/tris (8-hydroxyquinoline) aluminum (Alq3) OLED device exhibits a comparable external quantum efficiency and current efficiency to a traditional 4, 4-bis[N-(1-naphthyl)-N-phenyl-amino]biphenyl (α-NPD)/Alq3 OLED. A C70-based Schottky junction with 5 wt%-TBDI yields a power conversion efficiency of 5.0%, which is much higher than 1.7% for an α-NPD-based junction in the same configuration. These results suggest that TBDI has some promising properties which are in favor of the hole-transporting in Schottky junctions with a low-concentration donor. Project supported by the Funding Program for World-Leading Innovative R & D on Science and Technology (FIRST) from JSPS, the Fund from the Science and Technology Commission of Shanghai Municipality, China (Grant Nos. 14DZ2280900 and 14XD1401800), and the Natural Science Foundation of Shanghai (Grant No. 15ZR1416600).

  12. 5 CFR 1205.15 - Denying access.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... under Exemption (b)(7) of the Freedom of Information Act. (b) Form. All denials of access under this... 5 Administrative Personnel 3 2010-01-01 2010-01-01 false Denying access. 1205.15 Section 1205.15... Procedures for Obtaining Records § 1205.15 Denying access. (a) Basis. In accordance with 5 U.S.C....

  13. 5 CFR 1205.15 - Denying access.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... under Exemption (b)(7) of the Freedom of Information Act. (b) Form. All denials of access under this... 5 Administrative Personnel 3 2011-01-01 2011-01-01 false Denying access. 1205.15 Section 1205.15... Procedures for Obtaining Records § 1205.15 Denying access. (a) Basis. In accordance with 5 U.S.C....

  14. 5 CFR 1630.15 - Exemptions.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 5 Administrative Personnel 3 2010-01-01 2010-01-01 false Exemptions. 1630.15 Section 1630.15 Administrative Personnel FEDERAL RETIREMENT THRIFT INVESTMENT BOARD PRIVACY ACT REGULATIONS § 1630.15 Exemptions. (a) Pursuant to subsection (k) of the Privacy Act, 5 U.S.C. 552a, the Board may exempt...

  15. 10 CFR 431.15 - Materials incorporated by reference.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... with 5 U.S.C. 552(a) and 1 CFR 51. Any subsequent amendment to a standard by the standard-setting... 10 Energy 3 2012-01-01 2012-01-01 false Materials incorporated by reference. 431.15 Section 431.15 Energy DEPARTMENT OF ENERGY ENERGY CONSERVATION ENERGY EFFICIENCY PROGRAM FOR CERTAIN COMMERCIAL...

  16. Micro-structural, thermal, optical and physical properties nanocrystalline NbSr2Pr1.5Ce0.5Cu2O10-δ material synthesized by mechano-thermal method

    NASA Astrophysics Data System (ADS)

    Parthiban, P.; Balamurugan, S.; Satya, A. T.; Janaki, J.

    2015-06-01

    We have prepared nanocrystalline NbSr2Pr1.5Ce0.5Cu2O10-δ (Nb1222Pr) material by annealing the ball milled powder at 1000°C for 24h and studied by various characterization techniques such as TG-DTA, XRD, FT-IR, NIR, SEM-EDX, magnetization and electrical resistivity. Significant difference is seen in the TG-DTA curves of the as-milled powder due to ball milling. The annealed Nb1222Pr material is crystallized in tetragonal symmetry with lattice parameters, a = 0.3887(3) nm and c = 2.878(2) nm with reduced average particle size of ˜42.67 nm. Agglomeration of fine spherical particle sizes in the range of ˜180 - 280 nm is seen through SEM micro-image. The variation in the crystalline sizes of the Nb1222Pr phase obtained from XRD and SEM image indicate the polycrystalline characteristic of fine nanocrystalline particles. Neither superconductivity nor magnetic ordering is seen for the Nb1222Pr phase down to 5 K under 100 Oe. The four probe resistivity measurement reveals the semiconducting behavior of the Nb1222Pr phase.

  17. 49 CFR 172.524 - EXPLOSIVES 1.5 placard.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 49 Transportation 2 2012-10-01 2012-10-01 false EXPLOSIVES 1.5 placard. 172.524 Section 172.524... SECURITY PLANS Placarding § 172.524 EXPLOSIVES 1.5 placard. (a) Except for size and color, the EXPLOSIVES 1... subpart, the background color on EXPLOSIVES 1.5 placard must be orange. The “*” shall be replaced,...

  18. 49 CFR 172.524 - EXPLOSIVES 1.5 placard.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 49 Transportation 2 2010-10-01 2010-10-01 false EXPLOSIVES 1.5 placard. 172.524 Section 172.524... SECURITY PLANS Placarding § 172.524 EXPLOSIVES 1.5 placard. (a) Except for size and color, the EXPLOSIVES 1... subpart, the background color on EXPLOSIVES 1.5 placard must be orange. The “*” shall be replaced,...

  19. 49 CFR 172.524 - EXPLOSIVES 1.5 placard.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 49 Transportation 2 2013-10-01 2013-10-01 false EXPLOSIVES 1.5 placard. 172.524 Section 172.524... SECURITY PLANS Placarding § 172.524 EXPLOSIVES 1.5 placard. (a) Except for size and color, the EXPLOSIVES 1... subpart, the background color on EXPLOSIVES 1.5 placard must be orange. The “*” shall be replaced,...

  20. 49 CFR 172.524 - EXPLOSIVES 1.5 placard.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 49 Transportation 2 2011-10-01 2011-10-01 false EXPLOSIVES 1.5 placard. 172.524 Section 172.524... SECURITY PLANS Placarding § 172.524 EXPLOSIVES 1.5 placard. (a) Except for size and color, the EXPLOSIVES 1... subpart, the background color on EXPLOSIVES 1.5 placard must be orange. The “*” shall be replaced,...

  1. 49 CFR 172.524 - EXPLOSIVES 1.5 placard.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 49 Transportation 2 2014-10-01 2014-10-01 false EXPLOSIVES 1.5 placard. 172.524 Section 172.524... SECURITY PLANS Placarding § 172.524 EXPLOSIVES 1.5 placard. (a) Except for size and color, the EXPLOSIVES 1... subpart, the background color on EXPLOSIVES 1.5 placard must be orange. The “*” shall be replaced,...

  2. 46 CFR 32.15-5 - Whistles-T/ALL.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 1 2011-10-01 2011-10-01 false Whistles-T/ALL. 32.15-5 Section 32.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY TANK VESSELS SPECIAL EQUIPMENT, MACHINERY, AND HULL REQUIREMENTS Navigation Equipment § 32.15-5 Whistles—T/ALL. (a) (b) On tankships contracted for on and after November 19, 1955 means shall be provided...

  3. 46 CFR 32.15-5 - Whistles-T/ALL.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 1 2012-10-01 2012-10-01 false Whistles-T/ALL. 32.15-5 Section 32.15-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY TANK VESSELS SPECIAL EQUIPMENT, MACHINERY, AND HULL REQUIREMENTS Navigation Equipment § 32.15-5 Whistles—T/ALL. (a) (b) On tankships contracted for on and after November 19, 1955 means shall be provided...

  4. 48 CFR 15.407-5 - Estimating systems.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 48 Federal Acquisition Regulations System 1 2011-10-01 2011-10-01 false Estimating systems. 15.407-5 Section 15.407-5 Federal Acquisition Regulations System FEDERAL ACQUISITION REGULATION CONTRACTING...) Using an acceptable estimating system for proposal preparation benefits both the Government and...

  5. 46 CFR 189.15-5 - Alternate compliance.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... with the Alternate Compliance Program provisions of 46 CFR part 8. (b) For the purposes of this section... rules and supplements are incorporated by reference into 46 CFR 8.110(b). ... 46 Shipping 7 2012-10-01 2012-10-01 false Alternate compliance. 189.15-5 Section 189.15-5...

  6. 46 CFR 189.15-5 - Alternate compliance.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... with the Alternate Compliance Program provisions of 46 CFR part 8. (b) For the purposes of this section... rules and supplements are incorporated by reference into 46 CFR 8.110(b). ... 46 Shipping 7 2011-10-01 2011-10-01 false Alternate compliance. 189.15-5 Section 189.15-5...

  7. 46 CFR 189.15-5 - Alternate compliance.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... with the Alternate Compliance Program provisions of 46 CFR part 8. (b) For the purposes of this section... rules and supplements are incorporated by reference into 46 CFR 8.110(b). ... 46 Shipping 7 2010-10-01 2010-10-01 false Alternate compliance. 189.15-5 Section 189.15-5...

  8. Reversible thermally induced phase transition in ordered domains of Co(II)-5,10,15,20-tetrakis-(3,5-di-tert-butylphenyl)-porphyrin on Cu(111)

    NASA Astrophysics Data System (ADS)

    Stark, Michael; Ditze, Stefanie; Thomann, Michael; Lungerich, Dominik; Jux, Norbert; Steinrück, Hans-Peter; Marbach, Hubertus

    2016-08-01

    We investigated the adsorption behavior of Co(II)-5,10,15,20-tetrakis-(3,5-di-tert-butylphenyl)-porphyrin (CoTTBPP) on Cu(111) by scanning tunneling microscopy (STM). At room temperature (RT), the coverage dependent adsorption behavior follows an expected scheme: at low coverage step decoration is found, which evolves into supramolecular domains with a hexagonal order at higher coverage. Interestingly, upon cooling the sample to 180 K the occurrence of a clearly distinguishable coexisting herringbone phase is observed. Upon heating to RT again, the herringbone phase vanishes. Thus a temperature dependent, fully reversible phase transition was observed. High resolution STM micrographs allow for the determination of the intramolecular conformations which are different for the two supramolecular arrangements. In addition, we studied the bias voltage dependent appearance of the molecule in STM and assigned a dominant contribution of the central Co at negative bias voltages close to the Fermi edge to the occupied dz2 orbital. Interestingly, the herringbone phase, which dominates at 180 K, exhibits a significantly higher molecular density than the monomodal hexagonal arrangement at RT, which is in line with the "normal" behavior of freezing substances.

  9. Effective exciton blocking by the hole-transporting material 5,10,15-tribenzyl-5H-diindolo[3,2-a:3‧,2‧-c]-carbazole (TBDI) in the tetraphenyldibenzoperiflanthene (DBP) based organic photovoltaic cells

    NASA Astrophysics Data System (ADS)

    Zhang, Jing; Yang, Fang; Zheng, Yanqiong; Wei, Bin; Zhang, Xiaowen; Zhang, Jianhua; Wang, Zixing; Pu, Wenhong; Yang, Changzhu

    2015-12-01

    To explore the novel application of the hole-transporting material (HTM) as exciton blocking layer (EBL) in small molecule organic photovoltaic (OPV) cells, we introduce a recently reported HTM, 5,10,15-tribenzyl-5H-diindolo[3,2-a:3‧,2‧-c]-carbazole (TBDI), and the other two traditional HTMs, N,N‧-diphenyl-N,N‧-bis(1-naphthyl)-1,1‧-biphenyl-4,4‧-diamine (NPB) and 1,1‧-bis(di-4-tolylaminophenyl) cyclohexane (TAPC), to serve as EBLs in the tetraphenyldibenzoperiflanthene (DBP) based planar heterojunction cells. Due to the large band gap of these materials, the EBLs successfully block the misdirected electrons. The optimized devices including the EBLs of TBDI, NPB and TAPC achieve power conversion efficiency (ηPCE) of 1.70%, 1.33%, and 1.33%, respectively, whereas the control device without any EBL shows a ηPCE of only 1.25%. The optical simulation indicates that the maximum optical electric fields for the PHJs including 10-nm EBLs at the wavelength of 610 nm are significantly enhanced relative to that for the 20-nm DBP based control device. By impedance spectroscopy measurement, the device with TBDI EBL shows lower series resistance and total resistance than the device without TBDI, suggesting fast internal carrier mobility and smaller carrier recombination. The novel HTM TBDI better contributes to the device performance relative to the other two HTMs, stemming from its shallower lowest unoccupied molecule orbits (LUMO) level, stronger prevention of exciton quenching, and a smoother TBDI/DBP surface. These results suggest that TBDI is an excellent candidate as EBL for the DBP based OPVs. The overall ηPCE is further enhanced via optimizing the cathode buffer.

  10. 46 CFR 76.10-15 - Piping.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ..., DEPARTMENT OF HOMELAND SECURITY (CONTINUED) PASSENGER VESSELS FIRE PROTECTION EQUIPMENT Fire Main System... fire main shall be sufficient for the effective distribution of the maximum required discharge from two fire pumps operating simultaneously. This is in addition to § 76.10-5(c). The discharge of...

  11. 46 CFR 76.10-15 - Piping.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ..., DEPARTMENT OF HOMELAND SECURITY (CONTINUED) PASSENGER VESSELS FIRE PROTECTION EQUIPMENT Fire Main System... fire main shall be sufficient for the effective distribution of the maximum required discharge from two fire pumps operating simultaneously. This is in addition to § 76.10-5(c). The discharge of...

  12. 46 CFR 76.10-15 - Piping.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ..., DEPARTMENT OF HOMELAND SECURITY (CONTINUED) PASSENGER VESSELS FIRE PROTECTION EQUIPMENT Fire Main System... fire main shall be sufficient for the effective distribution of the maximum required discharge from two fire pumps operating simultaneously. This is in addition to § 76.10-5(c). The discharge of...

  13. 46 CFR 95.10-15 - Piping.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ..., DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS FIRE PROTECTION EQUIPMENT Fire... diameter of the fire main shall be sufficient for the effective distribution of the maximum required discharge from two fire pumps operating simultaneously. This requirement is in addition to § 95.10-5(c)....

  14. 46 CFR 76.10-15 - Piping.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ..., DEPARTMENT OF HOMELAND SECURITY (CONTINUED) PASSENGER VESSELS FIRE PROTECTION EQUIPMENT Fire Main System... fire main shall be sufficient for the effective distribution of the maximum required discharge from two fire pumps operating simultaneously. This is in addition to § 76.10-5(c). The discharge of...

  15. 46 CFR 95.10-15 - Piping.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ..., DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS FIRE PROTECTION EQUIPMENT Fire... diameter of the fire main shall be sufficient for the effective distribution of the maximum required discharge from two fire pumps operating simultaneously. This requirement is in addition to § 95.10-5(c)....

  16. 5 CFR 2421.15 - Secret ballot.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 5 Administrative Personnel 3 2010-01-01 2010-01-01 false Secret ballot. 2421.15 Section 2421.15... FEDERAL LABOR RELATIONS AUTHORITY MEANING OF TERMS AS USED IN THIS SUBCHAPTER § 2421.15 Secret ballot. Secret ballot means the expression by ballot, voting machine or otherwise, but in no event by proxy, of...

  17. 5 CFR 2421.15 - Secret ballot.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 5 Administrative Personnel 3 2011-01-01 2011-01-01 false Secret ballot. 2421.15 Section 2421.15... FEDERAL LABOR RELATIONS AUTHORITY MEANING OF TERMS AS USED IN THIS SUBCHAPTER § 2421.15 Secret ballot. Secret ballot means the expression by ballot, voting machine or otherwise, but in no event by proxy, of...

  18. 5 CFR 2421.15 - Secret ballot.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 5 Administrative Personnel 3 2014-01-01 2014-01-01 false Secret ballot. 2421.15 Section 2421.15... FEDERAL LABOR RELATIONS AUTHORITY MEANING OF TERMS AS USED IN THIS SUBCHAPTER § 2421.15 Secret ballot. Secret ballot means the expression by ballot, voting machine or otherwise, but in no event by proxy, of...

  19. 5 CFR 2421.15 - Secret ballot.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 5 Administrative Personnel 3 2013-01-01 2013-01-01 false Secret ballot. 2421.15 Section 2421.15... FEDERAL LABOR RELATIONS AUTHORITY MEANING OF TERMS AS USED IN THIS SUBCHAPTER § 2421.15 Secret ballot. Secret ballot means the expression by ballot, voting machine or otherwise, but in no event by proxy, of...

  20. 5 CFR 2421.15 - Secret ballot.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 5 Administrative Personnel 3 2012-01-01 2012-01-01 false Secret ballot. 2421.15 Section 2421.15... FEDERAL LABOR RELATIONS AUTHORITY MEANING OF TERMS AS USED IN THIS SUBCHAPTER § 2421.15 Secret ballot. Secret ballot means the expression by ballot, voting machine or otherwise, but in no event by proxy, of...

  1. 5 CFR 1315.15 - Grant recipients.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 5 Administrative Personnel 3 2011-01-01 2011-01-01 false Grant recipients. 1315.15 Section 1315.15 Administrative Personnel OFFICE OF MANAGEMENT AND BUDGET OMB DIRECTIVES PROMPT PAYMENT § 1315.15 Grant recipients. Recipients of Federal assistance may pay interest penalties if so specified in their contracts...

  2. 5 CFR 1315.15 - Grant recipients.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 5 Administrative Personnel 3 2012-01-01 2012-01-01 false Grant recipients. 1315.15 Section 1315.15 Administrative Personnel OFFICE OF MANAGEMENT AND BUDGET OMB DIRECTIVES PROMPT PAYMENT § 1315.15 Grant recipients. Recipients of Federal assistance may pay interest penalties if so specified in their contracts...

  3. 5 CFR 1315.15 - Grant recipients.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 5 Administrative Personnel 3 2014-01-01 2014-01-01 false Grant recipients. 1315.15 Section 1315.15 Administrative Personnel OFFICE OF MANAGEMENT AND BUDGET OMB DIRECTIVES PROMPT PAYMENT § 1315.15 Grant recipients. Recipients of Federal assistance may pay interest penalties if so specified in their contracts...

  4. 5 CFR 1315.15 - Grant recipients.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 5 Administrative Personnel 3 2010-01-01 2010-01-01 false Grant recipients. 1315.15 Section 1315.15 Administrative Personnel OFFICE OF MANAGEMENT AND BUDGET OMB DIRECTIVES PROMPT PAYMENT § 1315.15 Grant recipients. Recipients of Federal assistance may pay interest penalties if so specified in their contracts...

  5. 5 CFR 1653.15 - Payment.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 5 Administrative Personnel 3 2011-01-01 2011-01-01 false Payment. 1653.15 Section 1653.15 Administrative Personnel FEDERAL RETIREMENT THRIFT INVESTMENT BOARD COURT ORDERS AND LEGAL PROCESSES AFFECTING... Pay Child Support or Alimony Currently § 1653.15 Payment. Payment pursuant to a qualifying...

  6. 5 CFR 1653.15 - Payment.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 5 Administrative Personnel 3 2012-01-01 2012-01-01 false Payment. 1653.15 Section 1653.15 Administrative Personnel FEDERAL RETIREMENT THRIFT INVESTMENT BOARD COURT ORDERS AND LEGAL PROCESSES AFFECTING... Pay Child Support or Alimony Currently § 1653.15 Payment. Payment pursuant to a qualifying...

  7. 5 CFR 1653.15 - Payment.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 5 Administrative Personnel 3 2013-01-01 2013-01-01 false Payment. 1653.15 Section 1653.15 Administrative Personnel FEDERAL RETIREMENT THRIFT INVESTMENT BOARD COURT ORDERS AND LEGAL PROCESSES AFFECTING... Pay Child Support or Alimony Currently § 1653.15 Payment. Payment pursuant to a qualifying...

  8. 24 CFR 1.5 - Assurances required.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 24 Housing and Urban Development 1 2010-04-01 2010-04-01 false Assurances required. 1.5 Section 1... TITLE VI OF THE CIVIL RIGHTS ACT OF 1964 § 1.5 Assurances required. (a) General. (1) Every contract for... assistance pursuant to such contract or application, contain or be accompanied by an assurance that...

  9. 5 CFR 1653.15 - Payment.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 5 Administrative Personnel 3 2010-01-01 2010-01-01 false Payment. 1653.15 Section 1653.15... THRIFT SAVINGS PLAN ACCOUNTS Legal Process for the Enforcement of a Participant's Legal Obligations To... process will be made in accordance with § 1653.5....

  10. 47 CFR 15.240 - Operation in the band 433.5-434.5 MHz.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 1 2010-10-01 2010-10-01 false Operation in the band 433.5-434.5 MHz. 15.240 Section 15.240 Telecommunication FEDERAL COMMUNICATIONS COMMISSION GENERAL RADIO FREQUENCY DEVICES Intentional Radiators Radiated Emission Limits, Additional Provisions § 15.240 Operation in the band...

  11. 47 CFR 15.240 - Operation in the band 433.5-434.5 MHz.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 1 2012-10-01 2012-10-01 false Operation in the band 433.5-434.5 MHz. 15.240 Section 15.240 Telecommunication FEDERAL COMMUNICATIONS COMMISSION GENERAL RADIO FREQUENCY DEVICES Intentional Radiators Radiated Emission Limits, Additional Provisions § 15.240 Operation in the band...

  12. 47 CFR 15.240 - Operation in the band 433.5-434.5 MHz.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 1 2014-10-01 2014-10-01 false Operation in the band 433.5-434.5 MHz. 15.240 Section 15.240 Telecommunication FEDERAL COMMUNICATIONS COMMISSION GENERAL RADIO FREQUENCY DEVICES Intentional Radiators Radiated Emission Limits, Additional Provisions § 15.240 Operation in the band...

  13. 47 CFR 15.240 - Operation in the band 433.5-434.5 MHz.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 1 2013-10-01 2013-10-01 false Operation in the band 433.5-434.5 MHz. 15.240 Section 15.240 Telecommunication FEDERAL COMMUNICATIONS COMMISSION GENERAL RADIO FREQUENCY DEVICES Intentional Radiators Radiated Emission Limits, Additional Provisions § 15.240 Operation in the band...

  14. 47 CFR 15.240 - Operation in the band 433.5-434.5 MHz.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 1 2011-10-01 2011-10-01 false Operation in the band 433.5-434.5 MHz. 15.240 Section 15.240 Telecommunication FEDERAL COMMUNICATIONS COMMISSION GENERAL RADIO FREQUENCY DEVICES Intentional Radiators Radiated Emission Limits, Additional Provisions § 15.240 Operation in the band...

  15. 10. "TEST STANDS NOS. 11, 13, & 15; CONCRETE STRUCTURAL ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    10. "TEST STANDS NOS. 1-1, 1-3, & 1-5; CONCRETE STRUCTURAL SECTIONS AND DETAILS." Specifications No. OC12-50-10; Drawing No. 60-09-04; no sheet number within title block. D.O. SERIES 1109/14, Rev. B. Stamped: RECORD DRAWING - AS CONSTRUCTED. Below stamp: Contract DA-04353 Eng. 177, Rev. B; Date: 21 Dec. 1951. - Edwards Air Force Base, Air Force Rocket Propulsion Laboratory, Test Stand 1-5, Test Area 1-115, northwest end of Saturn Boulevard, Boron, Kern County, CA

  16. 48 CFR 15.407-5 - Estimating systems.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 48 Federal Acquisition Regulations System 1 2010-10-01 2010-10-01 false Estimating systems. 15.407... METHODS AND CONTRACT TYPES CONTRACTING BY NEGOTIATION Contract Pricing 15.407-5 Estimating systems. (a) Using an acceptable estimating system for proposal preparation benefits both the Government and...

  17. A comparison of dedicated 1.0 T extremity MRI vs. large-bore 1.5 T MRI for semiquantitative whole organ assessment of osteoarthritis: the MOST study

    PubMed Central

    Roemer, F.W.; Lynch, J.A.; Niu, J.; Zhang, Y.; Crema, M.D.; Tolstykh, I.; El-Khoury, G.Y.; Felson, D.T.; Lewis, C.E.; Nevitt, M.C.; Guermazi, A.

    2009-01-01

    Objective To date semiquantitative whole-organ scoring of knee osteoarthritis (OA) relies on 1.5 T MRI systems. Less costly 1.0 T extremity systems have been introduced that offer superior patient comfort, but may have limitations concerning field-of-view and image quality. The aim of this study was to compare SQ scoring on a 1.0 T system using 1.5 T MRI as the standard of reference. Methods The Multicenter Osteoarthritis (MOST) Study is a longitudinal study of individuals who have or are at high risk for knee OA. A sample of 53 knees was selected in which MRI was performed on a 1.0 T extremity system as well as on a 1.5 T scanner applying a comparable sequence protocol. MRIs were read according to the Whole Organ Magnetic Resonance Imaging Score (WORMS) score. Agreement was determined using weighted kappa statistics. Sensitivity, specificity and accuracy were assessed using the 1.5 T readings as the reference standard. In addition the number of non-readable features was assessed. Results Agreement (w-kappa) for 7 main WORMS features (cartilage, bone marrow lesions, osteophytes, meniscal damage and extrusion, synovitis, effusion) ranged between 0.54 (synovitis) and 0.75 (cartilage). Sensitivity ranged between 68.1% (meniscal damage) and 88.1% (effusion). Specificity ranged between 63.6% (effusion) and 96.4% (bone marrow lesions). Although the overall rate of non-readable features was very low, it was higher for the 1.0 T system (1.9% vs 0.2%). Conclusions Semiquantitative whole organ scoring can be performed using a 1.0 T peripheral scanner with a moderate to high degree of agreement and accuracy compared to SQ assessment using a 1.5 T whole body scanner. Our results are comparable to the published inter- and intra observer exercises obtained from 1.5 T systems. Sensitivity to change of longitudinal scoring was not evaluated in this cross-sectional design and should be investigated in future validation studies. PMID:19766580

  18. 5 CFR 9800.15 - Fees.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 5 Administrative Personnel 3 2013-01-01 2013-01-01 false Fees. 9800.15 Section 9800.15... requesters, educational and non-commercial scientific institutions; representatives of the news media; and... conducting scientific research. (e) For requesters who are representatives of the news media, fees will...

  19. 15 CFR 1150.5 - Preemption.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 3 2010-01-01 2010-01-01 false Preemption. 1150.5 Section 1150.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) TECHNOLOGY ADMINISTRATION, DEPARTMENT OF COMMERCE MARKING OF TOY, LOOK-ALIKE AND IMITATION FIREARMS § 1150.5 Preemption....

  20. 15 CFR 5.7 - Reports.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 1 2011-01-01 2011-01-01 false Reports. 5.7 Section 5.7 Commerce and Foreign Trade Office of the Secretary of Commerce OPERATION OF VENDING STANDS § 5.7 Reports. No later than... forward to the Director, Office of Administrative Services a report on activities under this order....

  1. 15 CFR 5.7 - Reports.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 15 Commerce and Foreign Trade 1 2014-01-01 2014-01-01 false Reports. 5.7 Section 5.7 Commerce and Foreign Trade Office of the Secretary of Commerce OPERATION OF VENDING STANDS § 5.7 Reports. No later than... forward to the Director, Office of Administrative Services a report on activities under this order....

  2. 5 CFR 1655.15 - Taxable distributions.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... to be false; (5) With the exception of a loan described in 5 CFR 1620.45, the loan is not repaid in... 5 Administrative Personnel 3 2010-01-01 2010-01-01 false Taxable distributions. 1655.15 Section... Taxable distributions. (a) The Board may declare any unpaid loan principal, plus unpaid interest, to be...

  3. 5 CFR 1655.15 - Taxable distributions.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... to be false; (5) With the exception of a loan described in 5 CFR 1620.45, the loan is not repaid in... 5 Administrative Personnel 3 2011-01-01 2011-01-01 false Taxable distributions. 1655.15 Section... Taxable distributions. (a) The Board may declare any unpaid loan principal, plus unpaid interest, to be...

  4. 15 CFR 5.2 - Policy.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 1 2010-01-01 2010-01-01 false Policy. 5.2 Section 5.2 Commerce and Foreign Trade Office of the Secretary of Commerce OPERATION OF VENDING STANDS § 5.2 Policy. (a) The... its continuance. (e) Disagreements concerning the denial, revocation, or modification of a permit...

  5. 15 CFR 336.5 - Licenses.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 2 2010-01-01 2010-01-01 false Licenses. 336.5 Section 336.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) INTERNATIONAL TRADE ADMINISTRATION, DEPARTMENT OF COMMERCE MISCELLANEOUS REGULATIONS IMPORTS OF COTTON WOVEN FABRIC § 336.5...

  6. 15 CFR 335.5 - Licenses.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 2 2010-01-01 2010-01-01 false Licenses. 335.5 Section 335.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) INTERNATIONAL TRADE ADMINISTRATION, DEPARTMENT OF COMMERCE MISCELLANEOUS REGULATIONS IMPORTS OF WORSTED WOOL FABRIC § 335.5...

  7. 15 CFR 806.5 - Confidentiality.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 3 2011-01-01 2011-01-01 false Confidentiality. 806.5 Section 806.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) BUREAU OF ECONOMIC ANALYSIS, DEPARTMENT OF COMMERCE DIRECT INVESTMENT SURVEYS § 806.5 Confidentiality....

  8. 15 CFR 1400.5 - Decision.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 3 2010-01-01 2010-01-01 false Decision. 1400.5 Section 1400.5... DEVELOPMENT AGENCY DETERMINATION OF GROUP ELIGIBILITY FOR MBDA ASSISTANCE § 1400.5 Decision. (a) Procedure... information which it wishes considered in its request for a determination of group eligibility. (b)...

  9. 15 CFR 2301.5 - Special consideration.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... consideration element is provided as one of several evaluation criteria contained in the regulations at 15 CFR... 2301.5 Commerce and Foreign Trade Regulations Relating to Telecommunications and Information NATIONAL TELECOMMUNICATIONS AND INFORMATION ADMINISTRATION, DEPARTMENT OF COMMERCE PUBLIC TELECOMMUNICATIONS...

  10. Enhanced negative thermal expansion in La(1-x)Pr(x)Fe10.7Co0.8Si1.5 compounds by doping the magnetic rare-earth element praseodymium.

    PubMed

    Li, Wen; Huang, Rongjin; Wang, Wei; Tan, Jie; Zhao, Yuqiang; Li, Shaopeng; Huang, Chuanjun; Shen, Jun; Li, Laifeng

    2014-06-01

    Experiments have been performed to enhance negative thermal expansion (NTE) in the La(Fe,Co,Si)13-based compounds by optimizing the chemical composition, i.e., proper substitution of La by magnetic element Pr. It is found that increasing the absolute value of the average coefficient of thermal expansion (CTE) in the NTE temperature region (200-300 K) attributes to enhancement of the spontaneous magnetization and its growth rate with increasing Pr content. Typically, the average CTE of La(1-x)Pr(x)Fe10.7Co0.8Si1.5 with x = 0.5 reaches as large as -38.5 × 10(-6) K(-1) between 200 and 300 K (ΔT = 100 K), which is 18.5% larger than that of x = 0. The present results highlight the potential applications of La(Fe,Co,Si)13-based compounds with a larger NTE coefficient. PMID:24848739

  11. Tri-μ-oxido-bis­[(5,10,15,20-tetra­phenyl­porphyrinato-κ4 N)niobium(V)

    PubMed Central

    Soury, Raoudha; Belkhiria, Mohamed Salah; Daran, Jean-Claude; Nasri, Habib

    2011-01-01

    In the title dinuclear NbV compound, [Nb2(C44H28N4)2O3], each Nb atom is seven-coordinated with three bridging O atoms and four N atoms from a chelating tetra­phenyl­porphyrinate anion. The Nb—O bond lengths range from 1.757 (6) to 2.331 (6) Å, and the average (niobium–pyrrole N atom) distance is 2.239 Å. In the dinuclear mol­ecule, the Nb⋯Nb separation is 2.8200 (8) Å, and the dihedral angle between the two porphyrinate mean planes is 5.4 (1)°. Weak inter­molecular C—H⋯π inter­actions are present in the crystal structure. PMID:21836860

  12. Kinetics of the chemical oxidation of (5,10,15,20-tetraphenyl-21H,23H-porphinato)(chloro)(aqua)iridium(III)

    NASA Astrophysics Data System (ADS)

    Tyulyaeva, E. Yu.; Bichan, N. G.; Mozhzhukhina, E. G.; Lomova, T. N.

    2016-01-01

    The oxidation of (Cl)(H2O)IrTPP with atmospheric oxygen in the presence of concentrated H2SO4 accompanied by coordination of molecular O2 and substitution of axial ligands was studied spectrophotometrically. In 16.785-18.09 MH2SO4 at 298-318 K, (Cl)(H2O)IrTPP experienced two single-electron oxidations in sequence: with an increase in the oxidation state of the iridium cation and with formation of the π-radical cation form (HSO4)IrIVTPP•+ oxidized at the aromatic ligand ( k 298 = 7.2 × 10-6 mol-1 L s-1). Referring to the literature data on the oxidation of (Cl)(H2O)IrTPP in AcOH and CF3COOH, it was shown that the medium acidity and the nature of the axial ligands affect the electron removal site in the chemical oxidation of (Cl)(H2O)IrTPP with atmospheric oxygen in proton-donor solvents.

  13. 15 CFR 1180.5 - Timeliness.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 3 2010-01-01 2010-01-01 false Timeliness. 1180.5 Section 1180.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) TECHNOLOGY ADMINISTRATION, DEPARTMENT OF COMMERCE TRANSFER BY FEDERAL AGENCIES OF SCIENTIFIC, TECHNICAL AND...

  14. 15 CFR 1180.5 - Timeliness.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 3 2011-01-01 2011-01-01 false Timeliness. 1180.5 Section 1180.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) TECHNOLOGY ADMINISTRATION, DEPARTMENT OF COMMERCE TRANSFER BY FEDERAL AGENCIES OF SCIENTIFIC, TECHNICAL AND...

  15. 15 CFR 1180.5 - Timeliness.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 15 Commerce and Foreign Trade 3 2012-01-01 2012-01-01 false Timeliness. 1180.5 Section 1180.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) TECHNOLOGY ADMINISTRATION, DEPARTMENT OF COMMERCE TRANSFER BY FEDERAL AGENCIES OF SCIENTIFIC, TECHNICAL AND...

  16. 15 CFR 1180.5 - Timeliness.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 15 Commerce and Foreign Trade 3 2013-01-01 2013-01-01 false Timeliness. 1180.5 Section 1180.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) TECHNOLOGY ADMINISTRATION, DEPARTMENT OF COMMERCE TRANSFER BY FEDERAL AGENCIES OF SCIENTIFIC, TECHNICAL AND...

  17. 15 CFR 241.5 - Standard dimensions.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 1 2011-01-01 2011-01-01 false Standard dimensions. 241.5 Section 241..., VEGETABLES AND OTHER DRY COMMODITIES, AND FOR CRANBERRIES § 241.5 Standard dimensions. Whenever in the rules and regulations in this part the error on a dimension is mentioned, this error shall be determined...

  18. 15 CFR 241.5 - Standard dimensions.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 1 2010-01-01 2010-01-01 false Standard dimensions. 241.5 Section 241..., VEGETABLES AND OTHER DRY COMMODITIES, AND FOR CRANBERRIES § 241.5 Standard dimensions. Whenever in the rules and regulations in this part the error on a dimension is mentioned, this error shall be determined...

  19. 15 CFR 742.5 - Missile technology.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 2 2011-01-01 2011-01-01 false Missile technology. 742.5 Section 742... BASED CONTROLS § 742.5 Missile technology. (a) License requirements. (1) In support of U.S. foreign... establish the existence of a contract. (d) Missile Technology Control Regime. Missile Technology...

  20. 15 CFR 255.5 - Progress reports.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 1 2010-01-01 2010-01-01 false Progress reports. 255.5 Section 255.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY, DEPARTMENT OF COMMERCE FELLOWSHIPS AND RESEARCH ASSOCIATES FELLOWSHIPS IN LABORATORY STANDARDIZATION AND TESTING...

  1. 15 CFR 760.5 - Reporting requirements.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 2 2011-01-01 2011-01-01 false Reporting requirements. 760.5 Section 760.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) BUREAU... comply with Y's boycott. (xv) Same as (xiv), except that A is asked by U.S. exporter B to assume...

  2. 5 CFR 1208.15 - Remedies.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... APPEALS UNDER THE UNIFORMED SERVICES EMPLOYMENT AND REEMPLOYMENT RIGHTS ACT AND THE VETERANS EMPLOYMENT OPPORTUNITIES ACT USERRA Appeals § 1208.15 Remedies. (a) Order for compliance. If the Board determines that a... of a judge under 5 CFR 1201.111 or a final Board decision under 5 CFR 1201.117) will order...

  3. 15 CFR 785.5 - Representation.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 2 2010-01-01 2010-01-01 false Representation. 785.5 Section 785.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) BUREAU OF INDUSTRY AND SECURITY, DEPARTMENT OF COMMERCE ADDITIONAL PROTOCOL REGULATIONS ENFORCEMENT §...

  4. 15 CFR 784.5 - Subsidiary arrangements.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 15 Commerce and Foreign Trade 2 2014-01-01 2014-01-01 false Subsidiary arrangements. 784.5 Section 784.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) BUREAU OF INDUSTRY AND SECURITY, DEPARTMENT OF COMMERCE ADDITIONAL PROTOCOL REGULATIONS COMPLEMENTARY...

  5. 15 CFR 8b.5 - Assurances required.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 1 2010-01-01 2010-01-01 false Assurances required. 8b.5 Section 8b.5... Assurances required. (a) Assurances. An applicant for Federal financial assistance to which this part applies shall submit an assurance, on a form specified by the Secretary, that the program or activity will...

  6. 15 CFR 742.5 - Missile technology.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 15 Commerce and Foreign Trade 2 2013-01-01 2013-01-01 false Missile technology. 742.5 Section 742... BASED CONTROLS § 742.5 Missile technology. (a) License requirements. (1) In support of U.S. foreign... establish the existence of a contract. (d) Missile Technology Control Regime. Missile Technology...

  7. 15 CFR 742.5 - Missile technology.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 15 Commerce and Foreign Trade 2 2014-01-01 2014-01-01 false Missile technology. 742.5 Section 742... BASED CONTROLS § 742.5 Missile technology. (a) License requirements. (1) In support of U.S. foreign... establish the existence of a contract. (d) Missile Technology Control Regime. Missile Technology...

  8. 15 CFR 742.5 - Missile technology.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 15 Commerce and Foreign Trade 2 2012-01-01 2012-01-01 false Missile technology. 742.5 Section 742... BASED CONTROLS § 742.5 Missile technology. (a) License requirements. (1) In support of U.S. foreign... establish the existence of a contract. (d) Missile Technology Control Regime. Missile Technology...

  9. 15 CFR 701.5 - Confidentiality.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 2 2010-01-01 2010-01-01 false Confidentiality. 701.5 Section 701.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) BUREAU OF INDUSTRY AND SECURITY, DEPARTMENT OF COMMERCE NATIONAL SECURITY INDUSTRIAL BASE REGULATIONS REPORTING...

  10. 15 CFR 742.5 - Missile technology.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 2 2010-01-01 2010-01-01 false Missile technology. 742.5 Section 742... BASED CONTROLS § 742.5 Missile technology. (a) License requirements. (1) In support of U.S. foreign... establish the existence of a contract. (d) Missile Technology Control Regime. Missile Technology...

  11. 15 CFR 905.5 - Exceptions.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 3 2010-01-01 2010-01-01 false Exceptions. 905.5 Section 905.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) NATIONAL OCEANIC AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE GENERAL REGULATIONS USE IN ENFORCEMENT PROCEEDINGS OF INFORMATION COLLECTED BY...

  12. 15 CFR 710.5 - Authority.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 15 Commerce and Foreign Trade 2 2013-01-01 2013-01-01 false Authority. 710.5 Section 710.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) BUREAU OF INDUSTRY AND SECURITY, DEPARTMENT OF COMMERCE CHEMICAL WEAPONS CONVENTION REGULATIONS GENERAL INFORMATION AND OVERVIEW OF THE CHEMICAL WEAPONS...

  13. 15 CFR 801.5 - Confidentiality.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 3 2010-01-01 2010-01-01 false Confidentiality. 801.5 Section 801.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) BUREAU OF ECONOMIC ANALYSIS, DEPARTMENT OF COMMERCE SURVEY OF INTERNATIONAL TRADE IN SERVICES BETWEEN U.S....

  14. 15 CFR 908.5 - Interim reports.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 15 Commerce and Foreign Trade 3 2012-01-01 2012-01-01 false Interim reports. 908.5 Section 908.5 Commerce and Foreign Trade Regulations Relating to Commerce and Foreign Trade (Continued) NATIONAL OCEANIC AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE GENERAL REGULATIONS MAINTAINING REC- ORDS AND SUBMITTING REPORTS ON WEATHER...

  15. 46 CFR 194.10-15 - Magazine van construction.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 7 2014-10-01 2014-10-01 false Magazine van construction. 194.10-15 Section 194.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS HANDLING, USE, AND CONTROL OF EXPLOSIVES AND OTHER HAZARDOUS MATERIALS Magazines § 194.10-15 Magazine...

  16. 46 CFR 194.10-15 - Magazine van construction.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 7 2013-10-01 2013-10-01 false Magazine van construction. 194.10-15 Section 194.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS HANDLING, USE, AND CONTROL OF EXPLOSIVES AND OTHER HAZARDOUS MATERIALS Magazines § 194.10-15 Magazine...

  17. 46 CFR 194.10-15 - Magazine van construction.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 7 2011-10-01 2011-10-01 false Magazine van construction. 194.10-15 Section 194.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS HANDLING, USE, AND CONTROL OF EXPLOSIVES AND OTHER HAZARDOUS MATERIALS Magazines § 194.10-15 Magazine...

  18. 46 CFR 194.10-15 - Magazine van construction.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 7 2012-10-01 2012-10-01 false Magazine van construction. 194.10-15 Section 194.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS HANDLING, USE, AND CONTROL OF EXPLOSIVES AND OTHER HAZARDOUS MATERIALS Magazines § 194.10-15 Magazine...

  19. 46 CFR 90.10-15 - Industrial personnel.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false Industrial personnel. 90.10-15 Section 90.10-15 Shipping... PROVISIONS Definition of Terms Used in This Subchapter § 90.10-15 Industrial personnel. This term means every person carried on board an industrial vessel for the sole purpose of carrying out the industrial...

  20. 46 CFR 90.10-15 - Industrial personnel.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false Industrial personnel. 90.10-15 Section 90.10-15 Shipping... PROVISIONS Definition of Terms Used in This Subchapter § 90.10-15 Industrial personnel. This term means every person carried on board an industrial vessel for the sole purpose of carrying out the industrial...

  1. 46 CFR 90.10-15 - Industrial personnel.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false Industrial personnel. 90.10-15 Section 90.10-15 Shipping... PROVISIONS Definition of Terms Used in This Subchapter § 90.10-15 Industrial personnel. This term means every person carried on board an industrial vessel for the sole purpose of carrying out the industrial...

  2. 46 CFR 90.10-15 - Industrial personnel.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Industrial personnel. 90.10-15 Section 90.10-15 Shipping... PROVISIONS Definition of Terms Used in This Subchapter § 90.10-15 Industrial personnel. This term means every person carried on board an industrial vessel for the sole purpose of carrying out the industrial...

  3. 46 CFR 90.10-15 - Industrial personnel.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Industrial personnel. 90.10-15 Section 90.10-15 Shipping... PROVISIONS Definition of Terms Used in This Subchapter § 90.10-15 Industrial personnel. This term means every person carried on board an industrial vessel for the sole purpose of carrying out the industrial...

  4. 46 CFR 105.10-15 - Flammable liquid.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Flammable liquid. 105.10-15 Section 105.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS COMMERCIAL FISHING VESSELS DISPENSING PETROLEUM PRODUCTS Definition of Terms Used in This Part § 105.10-15 Flammable liquid. (a) The term flammable liquid...

  5. 46 CFR 105.10-15 - Flammable liquid.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false Flammable liquid. 105.10-15 Section 105.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS COMMERCIAL FISHING VESSELS DISPENSING PETROLEUM PRODUCTS Definition of Terms Used in This Part § 105.10-15 Flammable liquid. (a) The term flammable liquid...

  6. 46 CFR 34.10-15 - Piping-T/ALL.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 1 2010-10-01 2010-10-01 false Piping-T/ALL. 34.10-15 Section 34.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY TANK VESSELS FIREFIGHTING EQUIPMENT Fire Main System, Details § 34.10-15 Piping—T/ALL. (a) All piping, valves and fittings shall meet the applicable requirements...

  7. 49 CFR 10.15 - Protection of records.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 49 Transportation 1 2013-10-01 2013-10-01 false Protection of records. 10.15 Section 10.15... INDIVIDUALS General § 10.15 Protection of records. (a) No person may, without permission, remove any record... authority, sells, conveys or disposes of any record * * * or thing of value of the United States or of...

  8. 49 CFR 10.15 - Protection of records.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 49 Transportation 1 2012-10-01 2012-10-01 false Protection of records. 10.15 Section 10.15... INDIVIDUALS General § 10.15 Protection of records. (a) No person may, without permission, remove any record... authority, sells, conveys or disposes of any record * * * or thing of value of the United States or of...

  9. 49 CFR 10.15 - Protection of records.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 49 Transportation 1 2010-10-01 2010-10-01 false Protection of records. 10.15 Section 10.15... INDIVIDUALS General § 10.15 Protection of records. (a) No person may, without permission, remove any record... authority, sells, conveys or disposes of any record * * * or thing of value of the United States or of...

  10. 49 CFR 10.15 - Protection of records.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 49 Transportation 1 2014-10-01 2014-10-01 false Protection of records. 10.15 Section 10.15... INDIVIDUALS General § 10.15 Protection of records. (a) No person may, without permission, remove any record... authority, sells, conveys or disposes of any record * * * or thing of value of the United States or of...

  11. 49 CFR 10.15 - Protection of records.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 49 Transportation 1 2011-10-01 2011-10-01 false Protection of records. 10.15 Section 10.15... INDIVIDUALS General § 10.15 Protection of records. (a) No person may, without permission, remove any record... authority, sells, conveys or disposes of any record * * * or thing of value of the United States or of...

  12. 46 CFR 92.15-10 - Ventilation for closed spaces.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Ventilation for closed spaces. 92.15-10 Section 92.15-10... CONSTRUCTION AND ARRANGEMENT Ventilation § 92.15-10 Ventilation for closed spaces. (a) Except as noted in paragraph (c) of this section, all enclosed spaces within the vessel shall be properly vented or...

  13. 46 CFR 50.10-15 - Marine inspector or inspector.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 2 2010-10-01 2010-10-01 false Marine inspector or inspector. 50.10-15 Section 50.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING GENERAL PROVISIONS Definition of Terms Used in This Subchapter § 50.10-15 Marine inspector or inspector. The term...

  14. 46 CFR 50.10-15 - Marine inspector or inspector.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 2 2012-10-01 2012-10-01 false Marine inspector or inspector. 50.10-15 Section 50.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING GENERAL PROVISIONS Definition of Terms Used in This Subchapter § 50.10-15 Marine inspector or inspector. The term...

  15. 46 CFR 50.10-15 - Marine inspector or inspector.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 2 2011-10-01 2011-10-01 false Marine inspector or inspector. 50.10-15 Section 50.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING GENERAL PROVISIONS Definition of Terms Used in This Subchapter § 50.10-15 Marine inspector or inspector. The term...

  16. 46 CFR 50.10-15 - Marine inspector or inspector.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 2 2013-10-01 2013-10-01 false Marine inspector or inspector. 50.10-15 Section 50.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING GENERAL PROVISIONS Definition of Terms Used in This Subchapter § 50.10-15 Marine inspector or inspector. The term...

  17. 46 CFR 50.10-15 - Marine inspector or inspector.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 2 2014-10-01 2014-10-01 false Marine inspector or inspector. 50.10-15 Section 50.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING GENERAL PROVISIONS Definition of Terms Used in This Subchapter § 50.10-15 Marine inspector or inspector. The term...

  18. 46 CFR 59.10-15 - Rivets and staybolts.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 2 2011-10-01 2011-10-01 false Rivets and staybolts. 59.10-15 Section 59.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING REPAIRS TO BOILERS, PRESSURE VESSELS AND APPURTENANCES Welding Repairs to Boilers and Pressure Vessels in -Service § 59.10-15...

  19. 46 CFR 59.10-15 - Rivets and staybolts.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 2 2010-10-01 2010-10-01 false Rivets and staybolts. 59.10-15 Section 59.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING REPAIRS TO BOILERS, PRESSURE VESSELS AND APPURTENANCES Welding Repairs to Boilers and Pressure Vessels in -Service § 59.10-15...

  20. 46 CFR 92.15-10 - Ventilation for closed spaces.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false Ventilation for closed spaces. 92.15-10 Section 92.15-10... CONSTRUCTION AND ARRANGEMENT Ventilation § 92.15-10 Ventilation for closed spaces. (a) Except as noted in paragraph (c) of this section, all enclosed spaces within the vessel shall be properly vented or...

  1. 46 CFR 92.15-10 - Ventilation for closed spaces.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false Ventilation for closed spaces. 92.15-10 Section 92.15-10... CONSTRUCTION AND ARRANGEMENT Ventilation § 92.15-10 Ventilation for closed spaces. (a) Except as noted in paragraph (c) of this section, all enclosed spaces within the vessel shall be properly vented or...

  2. 46 CFR 92.15-10 - Ventilation for closed spaces.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false Ventilation for closed spaces. 92.15-10 Section 92.15-10... CONSTRUCTION AND ARRANGEMENT Ventilation § 92.15-10 Ventilation for closed spaces. (a) Except as noted in paragraph (c) of this section, all enclosed spaces within the vessel shall be properly vented or...

  3. 46 CFR 190.10-15 - Vertical ladders not accepted.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 7 2011-10-01 2011-10-01 false Vertical ladders not accepted. 190.10-15 Section 190.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS CONSTRUCTION AND ARRANGEMENT Means of Escape § 190.10-15 Vertical ladders not accepted. (a) Vertical...

  4. 46 CFR 190.10-15 - Vertical ladders not accepted.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 7 2010-10-01 2010-10-01 false Vertical ladders not accepted. 190.10-15 Section 190.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) OCEANOGRAPHIC RESEARCH VESSELS CONSTRUCTION AND ARRANGEMENT Means of Escape § 190.10-15 Vertical ladders not accepted. (a) Vertical ladders and deck scuttles shall not in general...

  5. 46 CFR 92.15-10 - Ventilation for closed spaces.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Ventilation for closed spaces. 92.15-10 Section 92.15-10... CONSTRUCTION AND ARRANGEMENT Ventilation § 92.15-10 Ventilation for closed spaces. (a) Except as noted in paragraph (c) of this section, all enclosed spaces within the vessel shall be properly vented or...

  6. 10 CFR 1022.15 - Timing.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... ENERGY (GENERAL PROVISIONS) COMPLIANCE WITH FLOODPLAIN AND WETLAND ENVIRONMENTAL REVIEW REQUIREMENTS Procedures for Floodplain and Wetland Reviews § 1022.15 Timing. (a) For a proposed floodplain action, DOE shall allow 15 days for public comment following issuance of a notice of proposed floodplain...

  7. 10 CFR 1022.15 - Timing.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... ENERGY (GENERAL PROVISIONS) COMPLIANCE WITH FLOODPLAIN AND WETLAND ENVIRONMENTAL REVIEW REQUIREMENTS Procedures for Floodplain and Wetland Reviews § 1022.15 Timing. (a) For a proposed floodplain action, DOE shall allow 15 days for public comment following issuance of a notice of proposed floodplain...

  8. 10 CFR 1022.15 - Timing.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... ENERGY (GENERAL PROVISIONS) COMPLIANCE WITH FLOODPLAIN AND WETLAND ENVIRONMENTAL REVIEW REQUIREMENTS Procedures for Floodplain and Wetland Reviews § 1022.15 Timing. (a) For a proposed floodplain action, DOE shall allow 15 days for public comment following issuance of a notice of proposed floodplain...

  9. 10 CFR 1022.15 - Timing.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... ENERGY (GENERAL PROVISIONS) COMPLIANCE WITH FLOODPLAIN AND WETLAND ENVIRONMENTAL REVIEW REQUIREMENTS Procedures for Floodplain and Wetland Reviews § 1022.15 Timing. (a) For a proposed floodplain action, DOE shall allow 15 days for public comment following issuance of a notice of proposed floodplain...

  10. 10 CFR 1022.15 - Timing.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... ENERGY (GENERAL PROVISIONS) COMPLIANCE WITH FLOODPLAIN AND WETLAND ENVIRONMENTAL REVIEW REQUIREMENTS Procedures for Floodplain and Wetland Reviews § 1022.15 Timing. (a) For a proposed floodplain action, DOE shall allow 15 days for public comment following issuance of a notice of proposed floodplain...

  11. An electrochemical investigation of the effect of macrocycle ring size on the binding of di- and trivalent lanthanide cations by 12-crown-4,4-tert-butylbenzo-15-crown-5, and dibenzo-30-crown-10 in propylene carbonate

    SciTech Connect

    Massaux, J.; Desreux, J.F.

    1982-06-02

    The complexation in anhydrous proplene carbonate of the lanthanide ions by various macrocylic polyethers featuring from four to ten oxygen atoms has been investigated by a competitive potentiometric technique with lead(II) or thallium(I) as auxilliary ions. The stability of the complexes appears to depend primarily on the relative sizes of the metal ions and of the internal cavity of each macrocycle. It depends also on the rigidity of the ligands and is influenced by solvation effects. The small ligands 12-crown-4 (1) and 15-crown-5 (2) exhibit a similar behavior: they form 1:2 lanthanide complexes, the stability of which decreases with decreasing ionic radius despite the higher charge density of the metal ions. The presence of an electron-withdrawing phenyl group, as in 4-tert-butylbenzo-15-crown-5 (3), leads to a strong reduction of the stability constants. A maximum stability of 1:1 complexes of 3 is found at Nd(III) while a marked minimum is observed at Gd(III) in the complexation curve of dibenzo-30-crown-10 (5). Divalent samarium and ytterbium are more strongly coordinated than the corresponding trivalent ions by the crown ethers 1-5. The larger divalent ions fit better into the internal cavity of 5 and they form stable 1:2 sandwich complexes with 1 and 3. The properties of the complexes described in the present work are completely different from those reported so far in the case of noncylic ligands.

  12. 3,7,10,14,15-pentaacetyl-5-butanoyl-13,17-epoxy-8-myrsinene a novel compound isolated from Pycnocycla spinosa extract with potent anti-spasmodic and antidiarrheal properties

    PubMed Central

    Sadraei, H.; Ghanadian, M.; Asghari, G.; Sharifian, R.

    2015-01-01

    Bioassay monitoring of hydroalcoholic extract from the aerial part of Pyconcycla spinosa revealed that it contains components with spasmolytic activity in vitro. In addition, P. spinosa extract at oral dose of 1-5 mg/kg inhibits diarrhoea in animal models. Pharmacological screening of pure compounds isolated from P. spinosa hydroalcoholic extract led to the identification of 3,7,10,14,15-pentaacetyl-5-butanoyl-13,17-epoxy-8-myrsinene (PABEM) which is a new diterpene. In this research, we have investigated antispasmodic and antidiarrheal effects of PABEM for comparison with P. spinosa extract. Aerial parts of P. spinosa were extracted with ethanol. For antispasmodic studies, rat isolated ileum was suspended in Tyrode's solution in an organ bath. The ileum was contracted by acetylcholine (ACh, 0.5 μM), serotonin (5-HT, 5 μM) or electrical field stimulation (EFS). P. spinosa extract in a concentration dependent manner (10-640 μg/ml) inhibited ileum contractions induced by ACh, 5-HT or EFS. The new compound isolated form P. spinosa extract “PABEM” in a similar manner inhibited the contractile response to ACh, 5-HT and EFS. However, the inhibitory effects of PABEM were observed at much lower bath concentrations. The relaxation effect of PABEM was started at 40 ng/ml bath concentration and with 2.5 μg/ml PABEM in the bath, the contractile responses of ileum were completely abolished. Both hydroalcoholic extract of P. spinosa and PABEM reduced intestinal meal transit and castor oil and MgSO4 induced diarrhoea in mice. However, PABEM was about 10 times more potent than its parent extract. This research shows that PABEM is probably the main component responsible for antispasmodic and antidiarrheal actions of P. spinosa extract. PMID:26430457

  13. Synthesis and crystal structure of [C 6N 2H 14]ṡ(Zr 2F 10)ṡ1.5H 2O A new one-dimensional zirconium fluoride templated with DABCO

    NASA Astrophysics Data System (ADS)

    Saada, M. A.; Maisonneuve, V.; Leblanc, M.; Hémon-Ribaud, A.

    2006-01-01

    A new organic-inorganic zirconium (IV) fluoride, [C 6N 2H 14]ṡ(Zr 2F 10)ṡ1.5H 2O, is prepared by slow evaporation at 45 °C from a solution of Zr 4+ and of 1,4-diazabicyclo[2.2.2]-octane (DABCO) in 40% aqueous HF. The structure, determined from single-crystal X-ray diffraction, is monoclinic, space group C2/m, a=19.598(8) Å, b=6.658(3) Å, c=10.891(3) Å, β=101.25(4)° and Z=4. Previously unknown ∞(Zr 2F 10) 2- double chains, built up from edge-sharing ZrF 7 pentagonal bipyramids and ZrF 8 trigonal dodecahedra, are observed. The diprotonated organic cations, water molecules and the ∞(Zr 2F 10) 2- chains are linked by hydrogen bonds.

  14. Synthesis of 5,15-Diaryltetrabenzoporphyrins

    PubMed Central

    Filatov, Mikhail A.; Lebedev, Artem Y.; Vinogradov, Sergei A.; Cheprakov, Andrei V.

    2008-01-01

    A general method of synthesis of 5,15-diaryltetrabenzoporphyrins (Ar2TBPs) has been developed, based on 2 + 2 condensation of dipyrromethanes followed by oxidative aromatization. Two pathways to Ar2TBPs were investigated: the tetrahydroisoindole pathway and the dihydroisoindole pathway. In the tetrahydroisoindole pathway, precursor 5,15-diaryltetracyclohexenoporphyrins (5,15-Ar2TCHPs) were assembled from cyclohexeno-fused meso-unsubstituted dipyrromethanes and aromatic aldehydes or, alternatively, by way of the classical MacDonald synthesis. In the first case, scrambling was observed. Aromatization by tetracyclone was more effective than aromatization by DDQ but failed in the cases of porphyrins with electron-withdrawing substituents in the meso-aryl rings. The dihydroisoindole pathway was found to be much superior to the tetrahydroisoindole pathway, and it was developed into a general preparative method, consisting of (1) the synthesis of 4,7-dihydroisoindole and its transformation into meso-unsubstituted dipyrromethanes, (2) the synthesis of 5,15-diaryloctahydrotetrabenzoporphyrins (5,15-Ar2OHTBPs), and (3) their subsequent aromatization by DDQ. Ar2TBP free bases exhibit optical absorption spectra similar to those of meso-unsubstituted tetrabenzoporphyrins and fluoresce with high quantum yields. Pd complex of Ph2TBP was found to be highly phosphorescent at room temperature. PMID:18452337

  15. 10 CFR 63.15 - Site characterization.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... MOUNTAIN, NEVADA Licenses Preapplication Review § 63.15 Site characterization. (a) DOE shall conduct a program of site characterization with respect to the Yucca Mountain site before it submits an application... repository at Yucca Mountain to the extent practical....

  16. 10 CFR 63.15 - Site characterization.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... MOUNTAIN, NEVADA Licenses Preapplication Review § 63.15 Site characterization. (a) DOE shall conduct a program of site characterization with respect to the Yucca Mountain site before it submits an application... repository at Yucca Mountain to the extent practical....

  17. 10 CFR 63.15 - Site characterization.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... MOUNTAIN, NEVADA Licenses Preapplication Review § 63.15 Site characterization. (a) DOE shall conduct a program of site characterization with respect to the Yucca Mountain site before it submits an application... repository at Yucca Mountain to the extent practical....

  18. 10 CFR 63.15 - Site characterization.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... MOUNTAIN, NEVADA Licenses Preapplication Review § 63.15 Site characterization. (a) DOE shall conduct a program of site characterization with respect to the Yucca Mountain site before it submits an application... repository at Yucca Mountain to the extent practical....

  19. 10 CFR 63.15 - Site characterization.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... MOUNTAIN, NEVADA Licenses Preapplication Review § 63.15 Site characterization. (a) DOE shall conduct a program of site characterization with respect to the Yucca Mountain site before it submits an application... repository at Yucca Mountain to the extent practical....

  20. 10 CFR 75.15 - Facility attachments.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... Accounting and Control for Facilities § 75.15 Facility attachments. (a) The Facility Attachment or... under Article 39(b) of the main text of the Safeguards Agreement, do not have Facility Attachments...

  1. 46 CFR 190.15-10 - Ventilation for closed spaces.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 7 2010-10-01 2010-10-01 false Ventilation for closed spaces. 190.15-10 Section 190.15... CONSTRUCTION AND ARRANGEMENT Ventilation § 190.15-10 Ventilation for closed spaces. (a) All enclosed spaces... chemical laboratories, scientific laboratories, chemical storerooms, and machinery spaces and for...

  2. 43 CFR 15.10 - Operation of watercraft.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 43 Public Lands: Interior 1 2011-10-01 2011-10-01 false Operation of watercraft. 15.10 Section 15.10 Public Lands: Interior Office of the Secretary of the Interior KEY LARGO CORAL REEF PRESERVE § 15... or property, no anchor shall be cast or dragged in such a way as to damage any reef structure....

  3. 43 CFR 15.10 - Operation of watercraft.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 43 Public Lands: Interior 1 2010-10-01 2010-10-01 false Operation of watercraft. 15.10 Section 15.10 Public Lands: Interior Office of the Secretary of the Interior KEY LARGO CORAL REEF PRESERVE § 15... or property, no anchor shall be cast or dragged in such a way as to damage any reef structure....

  4. 43 CFR 15.10 - Operation of watercraft.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 43 Public Lands: Interior 1 2013-10-01 2013-10-01 false Operation of watercraft. 15.10 Section 15.10 Public Lands: Interior Office of the Secretary of the Interior KEY LARGO CORAL REEF PRESERVE § 15... or property, no anchor shall be cast or dragged in such a way as to damage any reef structure....

  5. 43 CFR 15.10 - Operation of watercraft.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 43 Public Lands: Interior 1 2012-10-01 2011-10-01 true Operation of watercraft. 15.10 Section 15.10 Public Lands: Interior Office of the Secretary of the Interior KEY LARGO CORAL REEF PRESERVE § 15... or property, no anchor shall be cast or dragged in such a way as to damage any reef structure....

  6. 43 CFR 15.10 - Operation of watercraft.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 43 Public Lands: Interior 1 2014-10-01 2014-10-01 false Operation of watercraft. 15.10 Section 15.10 Public Lands: Interior Office of the Secretary of the Interior KEY LARGO CORAL REEF PRESERVE § 15... or property, no anchor shall be cast or dragged in such a way as to damage any reef structure....

  7. 46 CFR 190.15-10 - Ventilation for closed spaces.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 7 2013-10-01 2013-10-01 false Ventilation for closed spaces. 190.15-10 Section 190.15... CONSTRUCTION AND ARRANGEMENT Ventilation § 190.15-10 Ventilation for closed spaces. (a) All enclosed spaces... chemical laboratories, scientific laboratories, chemical storerooms, and machinery spaces and for...

  8. 46 CFR 190.15-10 - Ventilation for closed spaces.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 7 2014-10-01 2014-10-01 false Ventilation for closed spaces. 190.15-10 Section 190.15... CONSTRUCTION AND ARRANGEMENT Ventilation § 190.15-10 Ventilation for closed spaces. (a) All enclosed spaces... chemical laboratories, scientific laboratories, chemical storerooms, and machinery spaces and for...

  9. 46 CFR 190.15-10 - Ventilation for closed spaces.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 7 2012-10-01 2012-10-01 false Ventilation for closed spaces. 190.15-10 Section 190.15... CONSTRUCTION AND ARRANGEMENT Ventilation § 190.15-10 Ventilation for closed spaces. (a) All enclosed spaces... chemical laboratories, scientific laboratories, chemical storerooms, and machinery spaces and for...

  10. 46 CFR 190.15-10 - Ventilation for closed spaces.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 7 2011-10-01 2011-10-01 false Ventilation for closed spaces. 190.15-10 Section 190.15... CONSTRUCTION AND ARRANGEMENT Ventilation § 190.15-10 Ventilation for closed spaces. (a) All enclosed spaces... chemical laboratories, scientific laboratories, chemical storerooms, and machinery spaces and for...

  11. 15 CFR 286.10 - Appeal.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... AND TECHNOLOGY, DEPARTMENT OF COMMERCE ACCREDITATION AND ASSESSMENT PROGRAMS NATIONAL VOLUNTARY CONFORMITY ASSESSMENT SYSTEM EVALUATION (NVCASE) PROGRAM § 286.10 Appeal. Any applicant or other...

  12. 15 CFR 286.10 - Appeal.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... AND TECHNOLOGY, DEPARTMENT OF COMMERCE ACCREDITATION AND ASSESSMENT PROGRAMS NATIONAL VOLUNTARY CONFORMITY ASSESSMENT SYSTEM EVALUATION (NVCASE) PROGRAM § 286.10 Appeal. Any applicant or other...

  13. 15 CFR 286.10 - Appeal.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... AND TECHNOLOGY, DEPARTMENT OF COMMERCE ACCREDITATION AND ASSESSMENT PROGRAMS NATIONAL VOLUNTARY CONFORMITY ASSESSMENT SYSTEM EVALUATION (NVCASE) PROGRAM § 286.10 Appeal. Any applicant or other...

  14. 15 CFR 286.10 - Appeal.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... AND TECHNOLOGY, DEPARTMENT OF COMMERCE ACCREDITATION AND ASSESSMENT PROGRAMS NATIONAL VOLUNTARY CONFORMITY ASSESSMENT SYSTEM EVALUATION (NVCASE) PROGRAM § 286.10 Appeal. Any applicant or other...

  15. 15 CFR 286.10 - Appeal.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... AND TECHNOLOGY, DEPARTMENT OF COMMERCE ACCREDITATION AND ASSESSMENT PROGRAMS NATIONAL VOLUNTARY CONFORMITY ASSESSMENT SYSTEM EVALUATION (NVCASE) PROGRAM § 286.10 Appeal. Any applicant or other...

  16. 10 CFR 440.15 - Subgrantees.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... ENERGY ENERGY CONSERVATION WEATHERIZATION ASSISTANCE FOR LOW-INCOME PERSONS § 440.15 Subgrantees. (a) The... weatherization or housing renovation activities; (ii) The subgrantee's experience in assisting low-income persons... relative need for a weatherization project by low-income persons. (c) If DOE finds that a...

  17. 14 CFR 1-5 - Records.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... with 14 CFR part 249 for the preservation of records. ... Aeronautics and Space OFFICE OF THE SECRETARY, DEPARTMENT OF TRANSPORTATION (AVIATION PROCEEDINGS) ECONOMIC... Provisions Sec. 1-5 Records. (a) The general books of account and all books, records, and memoranda...

  18. Eu3Ir2In15: A mixed-valent and vacancy-filled variant of the Sc5Co4Si10 structure type with anomalous magnetic properties

    DOE PAGESBeta

    Sarkar, Sumanta; Jana, Rajkumar; Siva, Ramesh; Banerjee, Swastika; Pati, Swapan K.; Balasubramanian, Mahalingam; Peter, Sebastian C.

    2015-10-27

    Here, a new compound, Eu3Ir2In15 has been synthesized using indium as an active metal flux. The compound crystallizes in tetragonal P4/mbm space group with lattice parameters, a = 14.8580(4) Å, b = 14.8580(4) Å, c = 4.3901(2) Å. It was further characterized by SEM-EDX studies. The temperature dependent magnetic susceptibility suggests that Eu in this compound is exclusively in divalent state. The effective magnetic moment (μeff) of this compound is 7.35 μB/Eu ion with paramagnetic Curie temperature (θp) of -28 K suggesting antiferromagnetic interaction. The mixed valent nature of Eu observed in magnetic measurements was confirmed by XANES measurements. Themore » compound undergoes demagnetization at a low magnetic field (10 Oe), which is quite unusual for Eu based intermetallic compounds. Temperature dependent resistivity studies reveal that the compound is metallic in nature. A comparative study was made between Eu3Ir2In15 and hypothetical vacancy variant Eu5Ir4In10 which also crystallizes in the same crystal structure However our computational studies along with control experiments suggest that the latter is thermodynamically less feasible compared to the former and hence we proposed that it is highly unlikely that a RE5T4X10 would exist with X as a group 13 elements.« less

  19. 10 CFR 712.15 - Management evaluation.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... drugs, as required by this part. Testing must be conducted in accordance with 10 CFR part 707, the... by a certified breath alcohol technician and conform to the DOT procedures (49 CFR part 40... the DOE policies implementing Executive Order 12564, and 10 CFR part 707 or DOE Order 3792.3,...

  20. 10 CFR 712.15 - Management evaluation.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... drugs, as required by this part. Testing must be conducted in accordance with 10 CFR part 707, the... by a certified breath alcohol technician and conform to the DOT procedures (49 CFR part 40... the DOE policies implementing Executive Order 12564, and 10 CFR part 707 or DOE Order 3792.3,...

  1. 10 CFR 712.15 - Management evaluation.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... drugs, as required by this part. Testing must be conducted in accordance with 10 CFR part 707, the... by a certified breath alcohol technician and conform to the DOT procedures (49 CFR part 40... the DOE policies implementing Executive Order 12564, and 10 CFR part 707 or DOE Order 3792.3,...

  2. 10 CFR 712.15 - Management evaluation.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... drugs, as required by this part. Testing must be conducted in accordance with 10 CFR part 707, the... by a certified breath alcohol technician and conform to the DOT procedures (49 CFR part 40... the DOE policies implementing Executive Order 12564, and 10 CFR part 707 or DOE Order 3792.3,...

  3. 10 CFR 712.15 - Management evaluation.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... drugs, as required by this part. Testing must be conducted in accordance with 10 CFR part 707, the... by a certified breath alcohol technician and conform to the DOT procedures (49 CFR part 40... the DOE policies implementing Executive Order 12564, and 10 CFR part 707 or DOE Order 3792.3,...

  4. 10 CFR 605.15 - Fee.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    .... (a) Notwithstanding 10 CFR part 600, a fee may be paid, in appropriate circumstances, to a recipient which is a small business concern as qualified under the criteria and size standards of 13 CFR part 121... be paid to other entities except as a deviation from 10 CFR part 600, nor shall fees be paid...

  5. 10 CFR 605.15 - Fee.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    .... (a) Notwithstanding 10 CFR part 600, a fee may be paid, in appropriate circumstances, to a recipient which is a small business concern as qualified under the criteria and size standards of 13 CFR part 121... be paid to other entities except as a deviation from 10 CFR part 600, nor shall fees be paid...

  6. 10 CFR 605.15 - Fee.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    .... (a) Notwithstanding 10 CFR part 600, a fee may be paid, in appropriate circumstances, to a recipient which is a small business concern as qualified under the criteria and size standards of 13 CFR part 121... be paid to other entities except as a deviation from 10 CFR part 600, nor shall fees be paid...

  7. 10 CFR 605.15 - Fee.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    .... (a) Notwithstanding 10 CFR part 600, a fee may be paid, in appropriate circumstances, to a recipient which is a small business concern as qualified under the criteria and size standards of 13 CFR part 121... be paid to other entities except as a deviation from 10 CFR part 600, nor shall fees be paid...

  8. Synthesis and photophysical properties of the photoactivatable cationic porphyrin 5-(4-N-dodecylpyridyl)-10,15,20-tri(4-N-methylpyridyl)-21H,23H-porphyrin tetraiodide for anti-malaria PDT.

    PubMed

    Stallivieri, Aurélie; Le Guern, Florent; Vanderesse, Régis; Meledje, Esme; Jori, Giulio; Frochot, Céline; Acherar, Samir

    2015-07-01

    This article describes a new synthetic method for obtaining three water soluble porphyrins. The more sophisticated porphyrin [5-(4-N-dodecylpyridyl)-10,15,20-tri(4-N-methylpyridyl)-21H,23H-porphyrin tetraiodide], also named C12 porphyrin, was obtained through a three step methodology. The improvements, compared to syntheses described in the literature, mostly concern the purification procedures. The photophysical properties of the three porphyrins are described and the C12 porphyrin presents a very good (1)O2 yield compared to its chemical intermediates. This porphyrin seems to be a very promising candidate for PDT applications. PMID:26066986

  9. 30 CFR 15.10 - Post-approval product audit.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... regulations (See 30 CFR part 15, 1987 edition). ... 30 Mineral Resources 1 2013-07-01 2013-07-01 false Post-approval product audit. 15.10 Section 15... General Provisions § 15.10 Post-approval product audit. (a) Approved explosives and sheathed...

  10. 30 CFR 15.10 - Post-approval product audit.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... regulations (See 30 CFR part 15, 1987 edition). ... 30 Mineral Resources 1 2014-07-01 2014-07-01 false Post-approval product audit. 15.10 Section 15... General Provisions § 15.10 Post-approval product audit. (a) Approved explosives and sheathed...

  11. 30 CFR 15.10 - Post-approval product audit.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... regulations (See 30 CFR part 15, 1987 edition). ... 30 Mineral Resources 1 2012-07-01 2012-07-01 false Post-approval product audit. 15.10 Section 15... General Provisions § 15.10 Post-approval product audit. (a) Approved explosives and sheathed...

  12. 30 CFR 15.10 - Post-approval product audit.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... regulations (See 30 CFR part 15, 1987 edition). ... 30 Mineral Resources 1 2011-07-01 2011-07-01 false Post-approval product audit. 15.10 Section 15... General Provisions § 15.10 Post-approval product audit. (a) Approved explosives and sheathed...

  13. 15 CFR 946.10 - Liaison officer.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE REGULATIONS OF THE NATIONAL WEATHER SERVICE MODERNIZATION OF THE NATIONAL WEATHER SERVICE § 946.10 Liaison officer. Prior to restructuring a field office... the provision of timely weather warnings and forecasts....

  14. 15 CFR 946.10 - Liaison officer.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE REGULATIONS OF THE NATIONAL WEATHER SERVICE MODERNIZATION OF THE NATIONAL WEATHER SERVICE § 946.10 Liaison officer. Prior to restructuring a field office... the provision of timely weather warnings and forecasts....

  15. 15 CFR 946.10 - Liaison officer.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE REGULATIONS OF THE NATIONAL WEATHER SERVICE MODERNIZATION OF THE NATIONAL WEATHER SERVICE § 946.10 Liaison officer. Prior to restructuring a field office... the provision of timely weather warnings and forecasts....

  16. 15 CFR 946.10 - Liaison officer.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE REGULATIONS OF THE NATIONAL WEATHER SERVICE MODERNIZATION OF THE NATIONAL WEATHER SERVICE § 946.10 Liaison officer. Prior to restructuring a field office... the provision of timely weather warnings and forecasts....

  17. 15 CFR 946.10 - Liaison officer.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE REGULATIONS OF THE NATIONAL WEATHER SERVICE MODERNIZATION OF THE NATIONAL WEATHER SERVICE § 946.10 Liaison officer. Prior to restructuring a field office... the provision of timely weather warnings and forecasts....

  18. Structure and magnetic properties of Ba{sub 5}Ce{sub 1.25}Mn{sub 3.75}O{sub 15}, a new 10H-polytype in the Ba-Ce-Mn-O system

    SciTech Connect

    Macias, Mario A.; Mentre, Olivier; Cuello, Gabriel J.; Gauthier, Gilles H.

    2013-02-15

    Based on the peculiar magnetic properties that are observed in pseudo one-dimensional manganites, we decided to synthesize the new Ba{sub 5}Ce{sub 1.25}Mn{sub 3.75}O{sub 15} compound. The preparation was performed by solid state reaction in air at about 1350 Degree-Sign C, for which we found that the compound crystallizes in a hexagonal symmetry with space group P6{sub 3}/mmc (No-194) and cell parameters a=b=5.7861(2) A and c=23.902(1) A. The structural description was correlated with neutron diffraction and bond valence calculations, confirming the presence of Ce{sup 4+} and Mn{sup 4+} segregated in the different crystallographic positions. Ba{sub 5}Ce{sub 1.25}Mn{sub 3.75}O{sub 15} displays evidence for strong AFM couplings already set at room temperature. The main arrangement of Mn{sup 4+} in magnetically isolated tetramers of face-sharing octahedra is responsible for a metamagnetic-like transition around 50 K. - Graphical abstract: The new Ba{sub 5}Ce{sub 1.25}Mn{sub 3.75}O{sub 15} polytype shows strong AFM couplings in magnetically isolated [Ce{sub 0.25}Mn{sub 3.75}O{sub 15}] tetramers of face-sharing octahedral, resulting in a metamagnetic-like transition around 50 K. Highlights: Black-Right-Pointing-Pointer Ba{sub 5}Ce{sub 1.25}Mn{sub 3.75}O{sub 15}, a new 10H polytype, has been prepared in the Ba-Ce-Mn-O system. Black-Right-Pointing-Pointer The compound crystallizes in the P6{sub 3}/mmc space group with (cchhh){sub 2} stacking sequence. Black-Right-Pointing-Pointer [Ce{sub 0.25}Mn{sub 3.75}O{sub 15}] tetramers are separated by [CeO{sub 6}] octahedra in the structure. Black-Right-Pointing-Pointer Instead of robust AFM ordering, a metamagnetic-like transition is found around 50 K.

  19. Synthesis and structure of 15-(1-benzyl-1 H-imidazol-5-yl)-9,10-dimethoxy-12,13-dihydro-7 aH,15 H-naphto[1',2':5,6][1,3]oxazino[2,3- a]isoquinoline

    NASA Astrophysics Data System (ADS)

    Osyanin, V. A.; Ivleva, E. A.; Rybakov, V. B.; Klimochkin, Yu. N.

    2015-01-01

    The synthesis and X-ray diffraction study of 15-(1-benzyl-1 H-imidazol-5-yl)-9,10-dimethoxy-12,13-dihydro-7 aH,15 H-naphto[1',2':5,6][1,3]oxazino[2,3- a]isoquinoline C32H29N3O3 are performed: triclinic crystal system, space group , a = 7.0319(2) Å, b = 12.2989(6) Å, c = 14.8284(7) Å, α = 84.606(4)°, β = 88.741(3)°, and γ = 86.227(3)°, Z = 2, V = 1273.82(9) Å3, ρcalcd = 1.313 g/cm3 [ T = 100(2) K]. In the molecule, the oxazine ring adopts a half-chair conformation. The positions of two tertiary hydrogen atoms are found, and it is shown that the compound is a trans isomer. The bond lengths and angles in the molecule are standard for this class of compounds.

  20. 33 CFR 66.10-15 - Aids to navigation.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 33 Navigation and Navigable Waters 1 2010-07-01 2010-07-01 false Aids to navigation. 66.10-15 Section 66.10-15 Navigation and Navigable Waters COAST GUARD, DEPARTMENT OF HOMELAND SECURITY AIDS TO NAVIGATION PRIVATE AIDS TO NAVIGATION Uniform State Waterway Marking System § 66.10-15 Aids to navigation....

  1. 33 CFR 66.10-15 - Aids to navigation.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 33 Navigation and Navigable Waters 1 2012-07-01 2012-07-01 false Aids to navigation. 66.10-15 Section 66.10-15 Navigation and Navigable Waters COAST GUARD, DEPARTMENT OF HOMELAND SECURITY AIDS TO NAVIGATION PRIVATE AIDS TO NAVIGATION Uniform State Waterway Marking System § 66.10-15 Aids to navigation....

  2. 33 CFR 66.10-15 - Aids to navigation.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 33 Navigation and Navigable Waters 1 2013-07-01 2013-07-01 false Aids to navigation. 66.10-15 Section 66.10-15 Navigation and Navigable Waters COAST GUARD, DEPARTMENT OF HOMELAND SECURITY AIDS TO NAVIGATION PRIVATE AIDS TO NAVIGATION Uniform State Waterway Marking System § 66.10-15 Aids to navigation....

  3. 33 CFR 66.10-15 - Aids to navigation.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 33 Navigation and Navigable Waters 1 2011-07-01 2011-07-01 false Aids to navigation. 66.10-15 Section 66.10-15 Navigation and Navigable Waters COAST GUARD, DEPARTMENT OF HOMELAND SECURITY AIDS TO NAVIGATION PRIVATE AIDS TO NAVIGATION Uniform State Waterway Marking System § 66.10-15 Aids to navigation....

  4. 33 CFR 66.10-15 - Aids to navigation.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 33 Navigation and Navigable Waters 1 2014-07-01 2014-07-01 false Aids to navigation. 66.10-15 Section 66.10-15 Navigation and Navigable Waters COAST GUARD, DEPARTMENT OF HOMELAND SECURITY AIDS TO NAVIGATION PRIVATE AIDS TO NAVIGATION Uniform State Waterway Marking System § 66.10-15 Aids to navigation....

  5. 15 CFR 990.10 - Purpose.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... AND ATMOSPHERIC ADMINISTRATION, DEPARTMENT OF COMMERCE OIL POLLUTION ACT REGULATIONS NATURAL RESOURCE DAMAGE ASSESSMENTS Introduction § 990.10 Purpose. The goal of the Oil Pollution Act of 1990 (OPA), 33 U.S... services resulting from an incident involving a discharge or substantial threat of a discharge of...

  6. 15 CFR 10.14 - Appeals.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... PRODUCT STANDARDS § 10.14 Appeals. (a) Any person directly affected by a procedural action taken by NIST... hearing the appeal will develop a recommendation to the Committee concerning the resolution of the appeal. NIST will review the recommendation and if found acceptable will subject it to a letter ballot of...

  7. 15 CFR 10.8 - Standing Committee.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... PRODUCT STANDARDS § 10.8 Standing Committee. (a) The Department shall establish and appoint the members of..., distributors, and users or consumers of the product covered by the standard, and representatives of appropriate...) The product or products covered by the standard; (2) The standard itself; and (3) Industry and...

  8. 15 CFR 922.10 - General.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... MARINE SANCTUARY PROGRAM REGULATIONS Site Evaluation List (SEL) § 922.10 General. (a) The Site Evaluation List (SEL) was established as a comprehensive list of marine sites with high natural resource values... site on the SEL, or selection of a site from the SEL as an active candidate for designation as...

  9. 15 CFR 922.10 - General.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... MARINE SANCTUARY PROGRAM REGULATIONS Site Evaluation List (SEL) § 922.10 General. (a) The Site Evaluation List (SEL) was established as a comprehensive list of marine sites with high natural resource values... site on the SEL, or selection of a site from the SEL as an active candidate for designation as...

  10. 15 CFR 922.10 - General.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... MARINE SANCTUARY PROGRAM REGULATIONS Site Evaluation List (SEL) § 922.10 General. (a) The Site Evaluation List (SEL) was established as a comprehensive list of marine sites with high natural resource values... site on the SEL, or selection of a site from the SEL as an active candidate for designation as...

  11. 15 CFR 922.10 - General.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... MARINE SANCTUARY PROGRAM REGULATIONS Site Evaluation List (SEL) § 922.10 General. (a) The Site Evaluation List (SEL) was established as a comprehensive list of marine sites with high natural resource values... site on the SEL, or selection of a site from the SEL as an active candidate for designation as...

  12. 15 CFR 10.10 - Review of published standards.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... DEVELOPMENT OF VOLUNTARY PRODUCT STANDARDS § 10.10 Review of published standards. (a) Each standard published... transferring sponsorship to a private standards-writing organization. While the Department encourages the development of standards to replace Voluntary Product Standards by private standards-writing...

  13. Synthesis, structure, electronic spectroscopy, photophysics, electrochemistry, and X-ray photoelectron spectroscopy of highly-electron-deficient [5,10,15,20-tetrakis(perfluoroalkyl)porphinato]zinc(II ) complexes and their free base derivatives

    SciTech Connect

    Goll, J.G.; Moore, K.T.; Therien, M.J.; Ghosh, A.

    1996-09-04

    The synthesis, optical spectroscopy, photophysical properties, electrochemistry, and X-ray photoelectron spectroscopy of a series of [5,10,15,20-tetrakis(perfluoroalkyl)porphinato]zinc(II ) complexes and their free base analogs are reported. The title compounds were prepared by a condensation methodology that utilizes perfluoro-1-(2`-pyrrolyl)-1-alkanol precursors and employs continuous water removal throughout the course of the reaction to yield the meso perfluorocarbon-substituted porphyrins. The nature of the porphyrin-pendant meso-perfluoroalkyl group exerts considerable influence over the macrocycle`s solubility properties. The structure of the monopyridyl adduct of [5,10,15,20-tetrakis(heptafluoropropyl)porphinato] zinc(II) features an S{sub 4}-distorted porphyrin core; X-ray data are given. Electrochemical studies carried out on these porphyrin and (porphinato)zinc(II) complexes indicate that meso-perfluoroalkylporphyrins are among the most electron-deficient porphyrinic species known. X-ray photoelectron spectroscopy experiments corroborate the electron poor nature of these systems and evince extreme stabilization of the nitrogen ls orbitals, consonant with particularly effective removal of electron density from the macrocycle by the meso-perfluoroalkyl moieties that is modulated by {sigma}-symmetry orbitals. 27 refs., 8 figs., 6 tabs.

  14. 46 CFR 53.10-15 - Manufacturers' data report forms.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... Vessel Code (incorporated by reference; see 46 CFR 53.01-1) must be made available to the marine... 46 Shipping 2 2013-10-01 2013-10-01 false Manufacturers' data report forms. 53.10-15 Section 53.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING...

  15. 46 CFR 53.10-15 - Manufacturers' data report forms.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... Vessel Code (incorporated by reference; see 46 CFR 53.01-1) must be made available to the marine... 46 Shipping 2 2011-10-01 2011-10-01 false Manufacturers' data report forms. 53.10-15 Section 53.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING...

  16. 46 CFR 53.10-15 - Manufacturers' data report forms.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... Vessel Code (incorporated by reference; see 46 CFR 53.01-1) must be made available to the marine... 46 Shipping 2 2014-10-01 2014-10-01 false Manufacturers' data report forms. 53.10-15 Section 53.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING...

  17. 46 CFR 53.10-15 - Manufacturers' data report forms.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... Vessel Code (incorporated by reference; see 46 CFR 53.01-1) must be made available to the marine... 46 Shipping 2 2012-10-01 2012-10-01 false Manufacturers' data report forms. 53.10-15 Section 53.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING...

  18. 46 CFR 53.10-15 - Manufacturers' data report forms.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... Vessel Code (incorporated by reference; see 46 CFR 53.01-1) must be made available to the marine... 46 Shipping 2 2010-10-01 2010-10-01 false Manufacturers' data report forms. 53.10-15 Section 53.10-15 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING...

  19. 10 CFR 470.15 - Allocation of funds.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 10 Energy 3 2010-01-01 2010-01-01 false Allocation of funds. 470.15 Section 470.15 Energy DEPARTMENT OF ENERGY ENERGY CONSERVATION APPROPRIATE TECHNOLOGY SMALL GRANTS PROGRAM § 470.15 Allocation of funds. (a) DOE shall annually allocate fiscal year funds available for support among the 10...

  20. Registration of cotton germplasm line md 10-5

    Technology Transfer Automated Retrieval System (TEKTRAN)

    MD 10-5 (Reg. No. ______, PI 675077) is a noncommercial breeding line of cotton (Gossypium hirsutum L.) released by the USDA-ARS at Stoneville, MS in 2015. MD 10-5 was selected in F4 progenies from a cross between MD 15 (PI 642769) and JJ 1145ne. MD 10-5 has a desirable combination between lint yi...

  1. Synthesis, FT-IR characterization and crystal structure of aqua-(5,10,15,20-tetra-phenyl-porphyrinato-κ(4) N)manganese(III) tri-fluoro-methane-sulfonate.

    PubMed

    Harhouri, Wafa; Mchiri, Chadlia; Najmudin, Shabir; Bonifácio, Cecilia; Nasri, Habib

    2016-05-01

    In the title salt, [Mn(C44H28N4)(H2O)](CF3SO3) or [Mn(III)(TPP)(H2O)](CF3SO3) (where TPP is the dianion of 5,10,15,20-tetra-phenyl-porphyrin), the Mn(III) cation is chelated by the four pyrrole N atoms of the porphyrinate anion and additionally coordinated by an aqua ligand in an apical site, completing the distorted square-pyramidal coordination environment. The average Mn-N(pyrrole) bond length is 1.998 (9) Å and the Mn-O(aqua) bond length is 2.1057 (15) Å. The central Mn(III) ion is displaced by 0.1575 (5) Å from the N4C20 mean plane of the porphyrinate anion towards the apical aqua ligand. The porphyrinate macrocycle exhibits a moderate ruffling and strong saddle deformations. In the crystal lattice, the [Mn(III)(TPP)(H2O)](+) cation and the tri-fluoro-methane-sulfonate counter-ions are arranged in alternating planes packed along [001]. The components are linked together through O-H⋯O hydrogen bonds and much weaker C-H⋯O and C-H⋯F inter-actions. The crystal packing is further stabilized by weak C-H⋯π inter-actions involving the pyrrole and phenyl rings of the porphyrin moieties. PMID:27308027

  2. Synthesis, FT–IR characterization and crystal structure of aqua­(5,10,15,20-tetra­phenyl­porphyrinato-κ4 N)manganese(III) tri­fluoro­methane­sulfonate

    PubMed Central

    Harhouri, Wafa; Mchiri, Chadlia; Najmudin, Shabir; Bonifácio, Cecilia; Nasri, Habib

    2016-01-01

    In the title salt, [Mn(C44H28N4)(H2O)](CF3SO3) or [MnIII(TPP)(H2O)](CF3SO3) (where TPP is the dianion of 5,10,15,20-tetra­phenyl­porphyrin), the MnIII cation is chelated by the four pyrrole N atoms of the porphyrinate anion and additionally coordinated by an aqua ligand in an apical site, completing the distorted square-pyramidal coordination environment. The average Mn—N(pyrrole) bond length is 1.998 (9) Å and the Mn—O(aqua) bond length is 2.1057 (15) Å. The central MnIII ion is displaced by 0.1575 (5) Å from the N4C20 mean plane of the porphyrinate anion towards the apical aqua ligand. The porphyrinate macrocycle exhibits a moderate ruffling and strong saddle deformations. In the crystal lattice, the [MnIII(TPP)(H2O)]+ cation and the tri­fluoro­methane­sulfonate counter-ions are arranged in alternating planes packed along [001]. The components are linked together through O—H⋯O hydrogen bonds and much weaker C—H⋯O and C—H⋯F inter­actions. The crystal packing is further stabilized by weak C—H⋯π inter­actions involving the pyrrole and phenyl rings of the porphyrin moieties. PMID:27308027

  3. TOUGH+ v1.5 Core Code

    2015-08-27

    TOUGH+ v1.5 is a numerical code for the simulation of multi-phase, multi-component flow and transport of mass and heat through porous and fractured media, and represents the third update of the code since its first release [Moridis et al., 2008]. TOUGH+ is a successor to the TOUGH2 [Pruess et al., 1991; 2012] family of codes for multi-component, multiphase fluid and heat flow developed at the Lawrence Berkeley National Laboratory. It is written in standard FORTRANmore » 95/2003, and can be run on any computational platform (workstations, PC, Macintosh). TOUGH+ v1.5 employs dynamic memory allocation, thus minimizing storage requirements. It has a completely modular structure, follows the tenets of Object-Oriented Programming (OOP), and involves the advanced features of FORTRAN 95/2003, i.e., modules, derived data types, the use of pointers, lists and trees, data encapsulation, defined operators and assignments, operator extension and overloading, use of generic procedures, and maximum use of the powerful intrinsic vector and matrix processing operations. TOUGH+ v1.5 is the core code for its family of applications, i.e., the part of the code that is common to all its applications. It provides a description of the underlying physics and thermodynamics of non-isothermal flow, of the mathematical and numerical approaches, as well as a detailed explanation of the general (common to all applications) input requirements, options, capabilities and output specifications. The core code cannot run by itself: it needs to be coupled with the code for the specific TOUGH+ application option that describes a particular type of problem. The additional input requirements specific to a particular TOUGH+ application options and related illustrative examples can be found in the corresponding User’s Manual.« less

  4. TOUGH+ v1.5 Core Code

    SciTech Connect

    Moridis, George J.

    2015-08-27

    TOUGH+ v1.5 is a numerical code for the simulation of multi-phase, multi-component flow and transport of mass and heat through porous and fractured media, and represents the third update of the code since its first release [Moridis et al., 2008]. TOUGH+ is a successor to the TOUGH2 [Pruess et al., 1991; 2012] family of codes for multi-component, multiphase fluid and heat flow developed at the Lawrence Berkeley National Laboratory. It is written in standard FORTRAN 95/2003, and can be run on any computational platform (workstations, PC, Macintosh). TOUGH+ v1.5 employs dynamic memory allocation, thus minimizing storage requirements. It has a completely modular structure, follows the tenets of Object-Oriented Programming (OOP), and involves the advanced features of FORTRAN 95/2003, i.e., modules, derived data types, the use of pointers, lists and trees, data encapsulation, defined operators and assignments, operator extension and overloading, use of generic procedures, and maximum use of the powerful intrinsic vector and matrix processing operations. TOUGH+ v1.5 is the core code for its family of applications, i.e., the part of the code that is common to all its applications. It provides a description of the underlying physics and thermodynamics of non-isothermal flow, of the mathematical and numerical approaches, as well as a detailed explanation of the general (common to all applications) input requirements, options, capabilities and output specifications. The core code cannot run by itself: it needs to be coupled with the code for the specific TOUGH+ application option that describes a particular type of problem. The additional input requirements specific to a particular TOUGH+ application options and related illustrative examples can be found in the corresponding User’s Manual.

  5. Crystal structure of chlorido­{5,10,15,20-tetra­kis­[2-(2,2-di­methyl­propanamido)­phen­yl]porphyrinato-κ4 N}iron(III)

    PubMed Central

    Awasabisah, Dennis; Powell, Douglas R.; Richter-Addo, George B.

    2015-01-01

    The title compound, [Fe(C64H64N8O4)Cl], is a five-coordinate square-pyramidal porphyrin complex with a chloride ion in the axial position, being coordinated from the protected side of the porphyrin; the FeIII atom is displaced by 0.474 (5) Å from the 24-atom mean plane of the porphyrin core towards the chloride. The porphyrin moiety is a ‘picket-fence’ 5,10,15,20-tetra­kis­[2-(2,2-di­methyl­propanamido)­phen­yl]porph­yrinate (por) group. The Fe—Cl bond length is 2.221 (2) Å and the Fe—N(por) bond lengths are in the range 2.043 (5)–2.063 (5) Å. The supra­molecular architecture of the crystal is sustained by C—H⋯O inter­actions between the pyrrolic and phenyl H atoms of one mol­ecule and the carbonyl O atoms of the 2,2-di­methyl­propanamido groups of adjacent mol­ecules. The methyl groups of three of the four tert-butyl substituents exhibited rotational disorder over two positions. The investigated crystal was twinned by a twofold rotation about the (001) axis with a refined twin ratio of 0.4086 (16). PMID:25878847

  6. Crystal structure of chlorido-{5,10,15,20-tetra-kis-[2-(2,2-di-methyl-propanamido)-phen-yl]porphyrinato-κ(4) N}iron(III).

    PubMed

    Awasabisah, Dennis; Powell, Douglas R; Richter-Addo, George B

    2015-02-01

    The title compound, [Fe(C64H64N8O4)Cl], is a five-coordinate square-pyramidal porphyrin complex with a chloride ion in the axial position, being coordinated from the protected side of the porphyrin; the Fe(III) atom is displaced by 0.474 (5) Å from the 24-atom mean plane of the porphyrin core towards the chloride. The porphyrin moiety is a 'picket-fence' 5,10,15,20-tetra-kis-[2-(2,2-di-methyl-propanamido)-phen-yl]porph-yrinate (por) group. The Fe-Cl bond length is 2.221 (2) Å and the Fe-N(por) bond lengths are in the range 2.043 (5)-2.063 (5) Å. The supra-molecular architecture of the crystal is sustained by C-H⋯O inter-actions between the pyrrolic and phenyl H atoms of one mol-ecule and the carbonyl O atoms of the 2,2-di-methyl-propanamido groups of adjacent mol-ecules. The methyl groups of three of the four tert-butyl substituents exhibited rotational disorder over two positions. The investigated crystal was twinned by a twofold rotation about the (001) axis with a refined twin ratio of 0.4086 (16). PMID:25878847

  7. Synthesis and characterization of particulate reinforced Zr[sub 57]Nb[sub 5]Al[sub 10]Cu[sub 15. 4]Ni[sub 12. 6] bulk metallic glass composites

    SciTech Connect

    Choi-Yim, H.; Busch, R.; Johnson, W.L. . W.M. Keck Lab. of Engineering Materials); Koester, U. . Dept. of Chemical Engineering)

    1999-06-22

    The Zr[sub 57]Nb[sub 5]Al[sub 10]Cu[sub 15.4]Ni[sub 12.6] bulk metallic glass forming liquid is reinforced with WC, SiC, W, or Ta particles. Structure, microstructure and thermal stability of the composites are studied by X-ray diffraction, optical microscopy and differential scanning calorimetry. The metallic glass matrix remains amorphous after adding up to 20 vol.% of particles. The reactions at the interfaces between the matrix and the different reinforcing materials are investigated with scanning electron microscopy, transmission electron microscopy and electron microprobe. The mechanical properties of the composites are studied in compression and tension. The influence of the introduced particles on the thermal stability of the matrix as well as on the mechanical properties is discussed.

  8. 46 CFR 59.10-5 - Cracks.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 2 2012-10-01 2012-10-01 false Cracks. 59.10-5 Section 59.10-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING REPAIRS TO BOILERS, PRESSURE VESSELS AND APPURTENANCES Welding Repairs to Boilers and Pressure Vessels in -Service § 59.10-5 Cracks. (a) Cracks extending from the calking edge of plates...

  9. 46 CFR 2.10-5 - Exemptions.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 1 2010-10-01 2010-10-01 false Exemptions. 2.10-5 Section 2.10-5 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY PROCEDURES APPLICABLE TO THE PUBLIC VESSEL INSPECTIONS Fees § 2.10-5 Exemptions. (a) Vessels owned or operated by a non-profit organization may be exempted from payment of...

  10. 49 CFR 10.5 - Definitions.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... its own Privacy Act regulations (49 CFR Part 1007), except to the extent that any system of records... 49 Transportation 1 2011-10-01 2011-10-01 false Definitions. 10.5 Section 10.5 Transportation... Applicability and Policy § 10.5 Definitions. Unless the context requires otherwise, the following...

  11. 49 CFR 10.5 - Definitions.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... its own Privacy Act regulations (49 CFR Part 1007), except to the extent that any system of records... 49 Transportation 1 2014-10-01 2014-10-01 false Definitions. 10.5 Section 10.5 Transportation... Applicability and Policy § 10.5 Definitions. Unless the context requires otherwise, the following...

  12. 49 CFR 10.5 - Definitions.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... its own Privacy Act regulations (49 CFR Part 1007), except to the extent that any system of records... 49 Transportation 1 2013-10-01 2013-10-01 false Definitions. 10.5 Section 10.5 Transportation... Applicability and Policy § 10.5 Definitions. Unless the context requires otherwise, the following...

  13. 49 CFR 10.5 - Definitions.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... its own Privacy Act regulations (49 CFR Part 1007), except to the extent that any system of records... 49 Transportation 1 2012-10-01 2012-10-01 false Definitions. 10.5 Section 10.5 Transportation... Applicability and Policy § 10.5 Definitions. Unless the context requires otherwise, the following...

  14. 49 CFR 10.5 - Definitions.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... its own Privacy Act regulations (49 CFR Part 1007), except to the extent that any system of records... 49 Transportation 1 2010-10-01 2010-10-01 false Definitions. 10.5 Section 10.5 Transportation... Applicability and Policy § 10.5 Definitions. Unless the context requires otherwise, the following...

  15. 15 CFR 0.735-10a-0.735-15 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 15 Commerce and Foreign Trade 1 2014-01-01 2014-01-01 false 0.735-10a-0.735-15 Section 0.735-10a-0.735-15 Commerce and Foreign Trade Office of the Secretary of Commerce EMPLOYEE RESPONSIBILITIES AND CONDUCT Regulatory Limitations Upon Employee Conduct §§ 0.735-10a—0.735-15...

  16. 15 CFR 0.735-10a-0.735-15 - [Reserved

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 15 Commerce and Foreign Trade 1 2010-01-01 2010-01-01 false 0.735-10a-0.735-15 Section 0.735-10a-0.735-15 Commerce and Foreign Trade Office of the Secretary of Commerce EMPLOYEE RESPONSIBILITIES AND CONDUCT Regulatory Limitations Upon Employee Conduct §§ 0.735-10a—0.735-15...

  17. 15 CFR 0.735-10a-0.735-15 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 15 Commerce and Foreign Trade 1 2013-01-01 2013-01-01 false 0.735-10a-0.735-15 Section 0.735-10a-0.735-15 Commerce and Foreign Trade Office of the Secretary of Commerce EMPLOYEE RESPONSIBILITIES AND CONDUCT Regulatory Limitations Upon Employee Conduct §§ 0.735-10a—0.735-15...

  18. 15 CFR 0.735-10a-0.735-15 - [Reserved

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 15 Commerce and Foreign Trade 1 2011-01-01 2011-01-01 false 0.735-10a-0.735-15 Section 0.735-10a-0.735-15 Commerce and Foreign Trade Office of the Secretary of Commerce EMPLOYEE RESPONSIBILITIES AND CONDUCT Regulatory Limitations Upon Employee Conduct §§ 0.735-10a—0.735-15...

  19. 15 CFR 0.735-10a-0.735-15 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 15 Commerce and Foreign Trade 1 2012-01-01 2012-01-01 false 0.735-10a-0.735-15 Section 0.735-10a-0.735-15 Commerce and Foreign Trade Office of the Secretary of Commerce EMPLOYEE RESPONSIBILITIES AND CONDUCT Regulatory Limitations Upon Employee Conduct §§ 0.735-10a—0.735-15...

  20. Core structure of EAS in 10(15) to 10(17) eV

    NASA Technical Reports Server (NTRS)

    Hara, T.; Hatano, Y.; Hayashida, N.; Kifune, T.; Nagano, M.; Tanahashi, G.

    1985-01-01

    With the use of Akeno calorimeter, the attenuation of particles in concrete is analyzed as the function of the shower size of 10 to the 5th power to 10 to the 7th power. The attenuation length does not depend much on the shower size but depends a little on the shower age. The average value is approx. 150 g/sq cm for s = 0.5 to 0.85 and approx. 40 g/sq cm for s = 0.85 to 1.15. These values and their fluctuations are consistent with the equi-intensity curves of extensive air showers (EAS).