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Sample records for ac conductivity measurements

  1. Studies on the activation energy from the ac conductivity measurements of rubber ferrite composites containing manganese zinc ferrite

    NASA Astrophysics Data System (ADS)

    Hashim, Mohd.; Alimuddin; Kumar, Shalendra; Shirsath, Sagar E.; Mohammed, E. M.; Chung, Hanshik; Kumar, Ravi

    2012-11-01

    Manganese zinc ferrites (MZF) have resistivities between 0.01 and 10 Ω m. Making composite materials of ferrites with either natural rubber or plastics will modify the electrical properties of ferrites. The moldability and flexibility of these composites find wide use in industrial and other scientific applications. Mixed ferrites belonging to the series Mn(1-x)ZnxFe2O4 were synthesized for different ‘x’ values in steps of 0.2, and incorporated in natural rubber matrix (RFC). From the dielectric measurements of the ceramic manganese zinc ferrite and rubber ferrite composites, ac conductivity and activation energy were evaluated. A program was developed with the aid of the LabVIEW package to automate the measurements. The ac conductivity of RFC was then correlated with that of the magnetic filler and matrix by a mixture equation which helps to tailor properties of these composites.

  2. Optical, electrical and ac conductivity measurements of nonlinear optical Dimethylaminomethylphthalimide doped with cadmium chloride single crystal for nano applications

    NASA Astrophysics Data System (ADS)

    Subramani, K.; Joseph, P. S.; Shankar, G.

    2013-07-01

    Single crystals of Dimethylaminomethylphthalimide cadmium chloride (DAMPCC) were grown by a slow evaporation technique. The unit cell parameters and crystal structure were measured by the powder X-ray diffraction analysis. The modes of vibrations of different molecular groups present in the DAMPCC crystal have been identified by FTIR spectral analysis. The UV-vis-NIR spectral analysis is used to study the optical behaviors like absorption and transmission properties of the crystal. The diffuse reflectance spectrum in absorption studies is calculated. The optical band gap of the DAMPCC crystal is calculated to be cut off wavelength 360 nm at photon energy 4.772 eV. The optical conductivity, electrical conductivity and ac conductivity are also calculated. Finally the nonlinear optics (NLO) property of DAMPCC crystal was confirmed by second harmonic generation (SHG) test using the Nd:YAG laser of fundamental wavelength 1064 nm.

  3. Estimation of Density of Localized States in Amorphous Se80Te20 and Se80Te10M10 (M = Cd, In, Sb) Alloys Using AC Conductivity Measurements

    NASA Astrophysics Data System (ADS)

    Chandel, N.; Mehta, N.; Kumar, A.

    2015-08-01

    The ac conductivity of amorphous Se80Te20 (a-Se80Te20) and amorphous Se80Te10M10 (a-Se80Te10M10) alloys has been measured as a function of temperature and frequency in a low-temperature regime. An analysis of the experimental data confirms that ac conductivity is reasonably well interpreted by the Austin-Mott model. The density of localized states was determined in the low-temperature region from 201 K to 280 K. Possible explanations of "metal-induced effects" on the conduction mechanism of a-Se80Te20 alloy are discussed.

  4. A single-shot spatial chirp method for measuring initial AC conductivity evolution of femtosecond laser pulse excited warm dense matter

    SciTech Connect

    Chen, Z.; Hering, P.; Brown, S. B.; Curry, C.; Tsui, Y. Y.; Glenzer, S. H.

    2016-09-19

    To study the rapid evolution of AC conductivity from ultrafast laser excited warm dense matter (WDM), a spatial chirp single-shot method is developed utilizing a crossing angle pump-probe configuration. The pump beam is shaped individually in two spatial dimensions so that it can provide both sufficient laser intensity to excite the material to warm dense matter state and a uniform time window of up to 1 ps with sub-100 fs FWHM temporal resolution. Here, temporal evolution of AC conductivity in laser excited warm dense gold was also measured.

  5. A single-shot spatial chirp method for measuring initial AC conductivity evolution of femtosecond laser pulse excited warm dense matter.

    PubMed

    Chen, Z; Hering, P; Brown, S B; Curry, C; Tsui, Y Y; Glenzer, S H

    2016-11-01

    To study the rapid evolution of AC conductivity from ultrafast laser excited warm dense matter (WDM), a spatial chirp single-shot method is developed utilizing a crossing angle pump-probe configuration. The pump beam is shaped individually in two spatial dimensions so that it can provide both sufficient laser intensity to excite the material to warm dense matter state and a uniform time window of up to 1 ps with sub-100 fs FWHM temporal resolution. Temporal evolution of AC conductivity in laser excited warm dense gold was also measured.

  6. AC resistance measuring instrument

    DOEpatents

    Hof, P.J.

    1983-10-04

    An auto-ranging AC resistance measuring instrument for remote measurement of the resistance of an electrical device or circuit connected to the instrument includes a signal generator which generates an AC excitation signal for application to a load, including the device and the transmission line, a monitoring circuit which provides a digitally encoded signal representing the voltage across the load, and a microprocessor which operates under program control to provide an auto-ranging function by which range resistance is connected in circuit with the load to limit the load voltage to an acceptable range for the instrument, and an auto-compensating function by which compensating capacitance is connected in shunt with the range resistance to compensate for the effects of line capacitance. After the auto-ranging and auto-compensation functions are complete, the microprocessor calculates the resistance of the load from the selected range resistance, the excitation signal, and the load voltage signal, and displays of the measured resistance on a digital display of the instrument. 8 figs.

  7. AC Resistance measuring instrument

    DOEpatents

    Hof, Peter J.

    1983-01-01

    An auto-ranging AC resistance measuring instrument for remote measurement of the resistance of an electrical device or circuit connected to the instrument includes a signal generator which generates an AC excitation signal for application to a load, including the device and the transmission line, a monitoring circuit which provides a digitally encoded signal representing the voltage across the load, and a microprocessor which operates under program control to provide an auto-ranging function by which range resistance is connected in circuit with the load to limit the load voltage to an acceptable range for the instrument, and an auto-compensating function by which compensating capacitance is connected in shunt with the range resistance to compensate for the effects of line capacitance. After the auto-ranging and auto-compensation functions are complete, the microprocessor calculates the resistance of the load from the selected range resistance, the excitation signal, and the load voltage signal, and displays of the measured resistance on a digital display of the instrument.

  8. Automated ac galvanomagnetic measurement system

    NASA Technical Reports Server (NTRS)

    Szofran, F. R.; Espy, P. N.

    1985-01-01

    An automated, ac galvanomagnetic measurement system is described. Hall or van der Pauw measurements in the temperature range 10-300 K can be made at a preselected magnetic field without operator attendance. Procedures to validate sample installation and correct operation of other system functions, such as magnetic field and thermometry, are included. Advantages of ac measurements are discussed.

  9. Evolution of AC conductivity of wet illitic clay during drying

    NASA Astrophysics Data System (ADS)

    Csáki, Š.; Štubňa, I.; Trnovcová, V.; Ondruška, J.; Vozár, L.; Dobroň, P.

    2017-02-01

    The evolution of the AC electrical conductivity during drying as well as the relationship between sample volume and moisture of green illite samples were investigated. The samples were prepared from illitic clay (80 mass % illite, 4 mass % montmorillonite, 12 mass % quartz and 4 mass % of orthoclase) and distilled water with initial moisture content 36 mass % and were freely dried in air. Conductivity was measured by the volt-ampere method with AC power supply of 5 V in the frequency range from 50 Hz to 10 kHz. The AC conductivity steeply increased with increasing moisture, up to 15 mass %. At higher values of the moisture, the AC conductivity was high and almost constant. The volume of samples increased with increasing moisture when the moisture was higher than 8 mass %. Below this value, the dimensions of samples do not significantly change. The dependence of the relative volume change on moisture is presented in a form of the Bigot’s curve.

  10. Impedance, AC conductivity and dielectric behavior Adeninium Trichloromercurate (II)

    NASA Astrophysics Data System (ADS)

    Fersi, M. Amine; Chaabane, I.; Gargouri, M.

    2016-09-01

    In this work, we report the measurements impedance spectroscopy technique for the organic-inorganic hybrid compound (C5H6N5) HgCl3, 11/2H2O measured in the 209 Hz-5 MHz frequency range from 378 to 428 K. Besides, the Cole-Cole (Z″ versus Z‧) plots were well fitted to an equivalent circuit built up by a parallel combination of resistance (R), fractal capacitance (CPE) and capacitance (C). Furthermore, the AC conductivity was investigated as a function of temperature and frequency in the same range. The experiment results indicated that AC conductivityac) was proportional to σdc + A ωS . The obtained results are discussed in terms of the correlated barrier hopping (CBH) model. An agreement between the experimental and theoretical results suggests that the AC conductivity behavior of Adeninium Trichloromercurate (II) can be successfully explained by CBH model. The contribution of single polaron hopping to AC conductivity in a present alloy was also studied.

  11. ac-resistance-measuring instrument

    SciTech Connect

    Hof, P.J.

    1981-04-22

    An auto-ranging ac resistance measuring instrument for remote measurement of the resistance of an electrical device or circuit connected to the instrument includes a signal generator which generates an ac excitation signal for application to a load, including the device and the transmission line, a monitoring circuit which provides a digitally encoded signal representing the voltage across the load, and a microprocessor which operates under program control to provide an auto-ranging function by which range resistance is connected in circuit with the load to limit the load voltage to an acceptable range for the instrument, and an auto-compensating function by which compensating capacitance is connected in shunt with the range resistance to compensate for the effects of line capacitance.

  12. AC Conductivity and Dielectric Properties of Borotellurite Glass

    NASA Astrophysics Data System (ADS)

    Taha, T. A.; Azab, A. A.

    2016-10-01

    Borotellurite glasses with formula 60B2O3-10ZnO-(30 - x)NaF- xTeO2 ( x = 0 mol.%, 5 mol.%, 10 mol.%, and 15 mol.%) have been synthesized by thermal melting. X-ray diffraction (XRD) analysis confirmed that the glasses were amorphous. The glass density ( ρ) was determined by the Archimedes method at room temperature. The density ( ρ) and molar volume ( V m) were found to increase with increasing TeO2 content. The direct-current (DC) conductivity was measured in the temperature range from 473 K to 623 K, in which the electrical activation energy of ionic conduction increased from 0.27 eV to 0.48 eV with increasing TeO2 content from 0 mol.% to 15 mol.%. The dielectric parameters and alternating-current (AC) conductivity ( σ ac) were investigated in the frequency range from 1 kHz to 1 MHz and temperature range from 300 K to 633 K. The AC conductivity and dielectric constant decreased with increasing TeO2 content from 0 mol.% to 15 mol.%.

  13. Study of AC electrical conduction mechanisms in an epoxy polymer

    NASA Astrophysics Data System (ADS)

    Jilani, Wissal; Mzabi, Nissaf; Gallot-Lavallée, Olivier; Fourati, Najla; Zerrouki, Chouki; Zerrouki, Rachida; Guermazi, Hajer

    2015-11-01

    The AC conductivity of an epoxy resin was investigated in the frequency range 10^{-1} - 106 Hz at temperatures ranging from -100 to 120 °C. The frequency dependence of σ_{ac} was described by the law: σ_{ac}=ω \\varepsilon0\\varepsilon^''_{HN}+Aωs. The study of temperature variation of the exponent (s) reveals two conduction models: the AC conduction dependence upon temperature is governed by the small polaron tunneling mechanism (SPTM) at low temperature (-100 -60 °C) and the correlated barrier hopping (CHB) model at high temperature (80-120 °C).

  14. AC conductivity of a niobium thin film in a swept magnetic field.

    PubMed

    Tsindlekht, M I; Genkin, V M; Gazi, S; Chromik, S

    2013-02-27

    We report results of measurements of the ac conductivity of a Nb superconducting thin film in a swept dc magnetic field. In the mixed state the swept dc field creates vortices at the film surface which pass through the film and form the observed ac conductivity. Vortex rate generation does not depend on the value of the dc field and there is a large plateau-like region of dc magnetic fields where the dissipation is approximately constant. A proposed phenomenological model describes quite well the main features of the ac response in these fields, including its dependency on the sweep rate, ac amplitude, frequency, and value of the second and third harmonics.

  15. AC Conductivity Studies of Lithium Based Phospho Vanadate Glasses

    NASA Astrophysics Data System (ADS)

    Nagendra, K.; Babu, G. Satish; Reddy, C. Narayana; Gowda, Veeranna

    2011-07-01

    Glasses in the system xLi2SO4-20Li2O-(80-x) [80P2O5-20V2O5] (5⩾x⩾20 mol%) has been prepared by melt quenching method. Dc and ac conductivity has been studied over a wide range of frequency (10 Hz to 10 MHz) and temperature (298 K-523 K). The dc conductivity found to increase with increase of Li2SO4 concentration. The ac conductivities have been fitted to the Almond-West type single power law equation σ(ω) = σ(0)+Aωs where `s' is the power law exponent. The ac conductivity found to increase with increase of Li2SO4 concentration. An attempt is made to elucidate the enhancement of lithium ion conduction in phosphor-vanadate glasses by considering the expansion of network structure.

  16. AC Conductivity Studies of Lithium Based Phospho Vanadate Glasses

    SciTech Connect

    Nagendra, K.; Babu, G. Satish; Gowda, Veeranna; Reddy, C. Narayana

    2011-07-15

    Glasses in the system xLi{sub 2}SO{sub 4}-20Li{sub 2}O-(80-x) [80P{sub 2}O{sub 5}-20V{sub 2}O{sub 5}](5{>=}x{>=}20 mol%) has been prepared by melt quenching method. Dc and ac conductivity has been studied over a wide range of frequency (10 Hz to 10 MHz) and temperature (298 K-523 K). The dc conductivity found to increase with increase of Li{sub 2}SO{sub 4} concentration. The ac conductivities have been fitted to the Almond-West type single power law equation {sigma}({omega}) = {sigma}(0)+A{omega}{sup s} where 's' is the power law exponent. The ac conductivity found to increase with increase of Li{sub 2}SO{sub 4} concentration. An attempt is made to elucidate the enhancement of lithium ion conduction in phosphor-vanadate glasses by considering the expansion of network structure.

  17. Ocular vestibular evoked myogenic potentials to air conduction (AC oVEMP): useful in clinical practice?

    PubMed

    Walther, L E; Rogowski, M; Hörmann, K; Schaaf, H; Löhler, J

    2011-01-01

    Cervical vestibular-evoked myogenic potential (cVEMP) and ocular VEMP (oVEMP) stimuli can be used to measure otolith function using air (AC) and bone conducted (BC) stimuli. Cervical VEMPs reflect saccular function and can be recorded using air conduction (AC), whereas oVEMPs reflect probably predominantly utricular function. Air- and bone-conducted vibration can be used, because AC oVEMP methodology seems to be fast and simple in clinical practice to measure otolith function. In this study we discuss the advantages and problems of AC oVEMP stimulation. AC oVEMP can be easily and quickly obtained within a few seconds. N10 (first negative peak) and p15 (first positive peak) latencies may be used as parameters for clinical interpretation but amplitude fluctuations are relatively large. For daily clinical use of VEMP visualization in a normogram seems feasible. Especially the AC oVEMP methodology (100 dB nHL, tone burst 500 Hz) is fast and efficient in clinical practice to measure otolith function, predominantly utricular function.

  18. Broadband AC Conductivity of XUV Excited Warm Dense Gold

    NASA Astrophysics Data System (ADS)

    Chen, Z.; Tsui, Y.; Toleikis, S.; Hering, P.; Brown, S.; Curry, C.; Tanikawa, T.; Hoeppner, H.; Levy, M.; Goede, S.; Ziaja-Motyka, B.; Rethfeld, B.; Recoules, Vanina; Ng, A.; Glenzer, S.

    2015-11-01

    The properties of ultrafast laser excited warm dense gold have been extensively studied in the past decade. In those studies, a 400nm ultrashort laser pulse was used to excite the 5 d electrons in gold to 6s/p state. Here we will present our recent study of warm dense gold with 245eV, 70fs pulses to selectively excite 4 f electrons using the XUV-FEL at FLASH. The AC conductivity of the warm dense gold was measured at different wavelengths (485nm, 520nm, 585nm, 640nm and 720nm) to cover the range from 5 d-6 s / p interband transitions to 6 s/ p intraband transitions. Preliminary result suggests that the onset of 5 d-6 s / p band transition shifts from 2.3eV to ~ 2eV, which is in agreement with the study of 400nm laser pulse excited warm dense gold. More detailed analysis of our data will also be presented.

  19. Correction of the power law of ac conductivity in ion-conducting materials due to the electrode polarization effect.

    PubMed

    Khamzin, A A; Popov, I I; Nigmatullin, R R

    2014-03-01

    Based on the supposition related to fractal nature of transport processes in ion-conducting materials, an expression for the low-frequency ac conductivity dependence was derived. This expression for the ac conductivity generalizes the power-law dependence and gives a possibility to take into account the influence of the electrode polarization effect. The ac conductivity expression obtained is in excellent agreement with experimental data for a wide frequency range.

  20. Calibration-free electrical conductivity measurements for highly conductive slags

    SciTech Connect

    MACDONALD,CHRISTOPHER J.; GAO,HUANG; PAL,UDAY B.; VAN DEN AVYLE,JAMES A.; MELGAARD,DAVID K.

    2000-05-01

    This research involves the measurement of the electrical conductivity (K) for the ESR (electroslag remelting) slag (60 wt.% CaF{sub 2} - 20 wt.% CaO - 20 wt.% Al{sub 2}O{sub 3}) used in the decontamination of radioactive stainless steel. The electrical conductivity is measured with an improved high-accuracy-height-differential technique that requires no calibration. This method consists of making continuous AC impedance measurements over several successive depth increments of the coaxial cylindrical electrodes in the ESR slag. The electrical conductivity is then calculated from the slope of the plot of inverse impedance versus the depth of the electrodes in the slag. The improvements on the existing technique include an increased electrochemical cell geometry and the capability of measuring high precision depth increments and the associated impedances. These improvements allow this technique to be used for measuring the electrical conductivity of highly conductive slags such as the ESR slag. The volatilization rate and the volatile species of the ESR slag measured through thermogravimetric (TG) and mass spectroscopy analysis, respectively, reveal that the ESR slag composition essentially remains the same throughout the electrical conductivity experiments.

  1. Dielectric behavior and ac electrical conductivity in samarium substituted Mg-Ni ferrites

    NASA Astrophysics Data System (ADS)

    Melagiriyappa, E.; Veena, M.; Somashekarappa, A.; Shankaramurthy, G. J.; Jayanna, H. S.

    2014-08-01

    Samarium substituted MgNi ferrites with composition Mg1-xNixFe2-ySmyO4 ( x = 0, 0.2, 0.4, 0.6, 0.8, 1.0; y = 0.0, 0.05, 0.1) have been prepared by ceramic method. Dielectric measurements of the samples have been carried out at room temperature as a function of frequency and composition. X-ray diffraction patterns have confirmed the single-phase spinel cubic structure for all the samples. Dielectric constant ( ɛ') and dielectric loss (tan δ) decrease while ac electrical conductivity ( σ ac ) increases with increase in frequency. Dielectric properties have been explained on the basis of Maxwell-Wagner's two layer model. The conduction mechanism in these ferrites is due to electron hopping between Ni2+ and Ni3+ as well as Fe3+ and Fe2+ ions on octahedral sites. Dielectric constant and ac conductivity increases and decreases respectively with nickel content. A significant reduction in the values of dielectric constant and ac electrical conductivity has been observed in Sm3+ ions substituted samples.

  2. ac and dc percolative conductivity of magnetite-cellulose acetate composites

    SciTech Connect

    Chiteme, C.; McLachlan, D. S.; Sauti, G.

    2007-03-01

    ac and dc conductivity results for a percolating system, which consists of a conducting powder (magnetite) combined with an 'insulating' powder (cellulose acetate), are presented. Impedance and modulus spectra are obtained in a percolation system. The temperature dependence of the resistivity of the cellulose acetate is such that at 170 deg. C, it is essentially a conductor at frequencies below 0.059{+-}0.002 Hz, and a dielectric above. The percolation parameters, from the dc conductivity measured at 25 and 170 deg. C, are determined and discussed in relation to the ac results. The experimental results scale as a function of composition, temperature, and frequency. An interesting result is the correlation observed between the scaling parameter (f{sub ce}), obtained from a scaling of the ac measurements, and the peak frequency (f{sub cp}) of the arcs, obtained from impedance spectra, above the critical volume fraction. Scaling at 170 deg. C is not as good as at 25 deg. C, probably indicating a breakdown in scaling at the higher temperature. The modulus plots show the presence of two materials: a conducting phase dominated by the cellulose acetate and the isolated conducting clusters below the critical volume fraction {phi}{sub c}, as well as the interconnected conducting clusters above {phi}{sub c}. These results are confirmed by computer simulations using the two exponent phenomenological percolation equation. These results emphasize the need to analyze ac conductivity results in terms of both impedance and modulus spectra in order to get more insight into the behavior of composite materials.

  3. AC loss measurements of twisted and untwisted BSCCO multifilamentary tapes

    NASA Astrophysics Data System (ADS)

    Jiang, Zhenan; Amemiya, Naoyuki; Nishioka, Takamasa; Oh, Sang-Soo

    2005-01-01

    AC losses in twisted and untwisted BSCCO multifilamentary superconducting tapes with Ag matrix developed in DAPAS program were measured by an electrical method. Magnetization and transport losses were measured by a pick-up coil and by a voltage taps. Total AC loss during simultaneous application of AC transport current and an AC transverse magnetic field was given by the sum of the magnetization and transport losses measured during this simultaneous application. The magnetization loss without transport current of untwisted and twisted tapes was measured first to evaluate the effect of twisting to decouple filaments. Then, the total AC loss of the twisted tape was measured in transverse magnetic fields with various amplitudes and orientations, while the amplitude of the transport current was fixed. The measured total AC loss in a parallel transverse magnetic field was compared with some theoretical models to study the detailed characteristics of the measured total AC loss of the sample.

  4. Measuring Salinity by Conductivity.

    ERIC Educational Resources Information Center

    Lapworth, C. J.

    1981-01-01

    Outlines procedures for constructing an instrument which uses an electrode and calibration methods to measure the salinity of waters in environments close to and affected by a saline estuary. (Author/DC)

  5. Influence of temperature on AC conductivity of nanocrystalline CuAlO2

    NASA Astrophysics Data System (ADS)

    Prakash, T.

    2012-07-01

    Nanocrystalline CuAlO2 was synthesized by mechanical alloying of Cu2O and α-Al2O3 powders in the molar ratio of 1:1 for 20 h in toluene medium with tungsten carbide balls and vials using planetary ball mill. The ball milling was carried out at 300 rpm with a ball to powder weight ratio of 10:1 and then annealed at 1373 K in a platinum crucible for 20 h to get CuAlO2 phase with average crystallite size 45 nm. Complex impedance spectroscopic measurement in the frequency region 1 Hz to 10 MHz between the temperatures 333 to 473 K was carried out for nanocrystalline CuAlO2 sample. The obtained complex impedance data was analyzed for AC conductivities, DC and AC conductivities correlations and crossover frequencies ( f co ). The BNN (Barton, Nakajima and Namikawa) relation was applied to understand the correlation between DC and AC conductivities. The observed experimental results were discussed in the paper.

  6. Measurement of AC electrical characteristics of SSC superconducting dipole magnets

    SciTech Connect

    Smedley, K M; Shafer, R E

    1992-01-01

    Experiments were conducted to measure the AC electrical characteristics of SSC superconducting dipole magnets over the frequency range of 0.1 Hz to 10 kHz. A magnet equivalent circuit representing the magnet DC inductance, eddy current losses, coil-to-ground and turn-to-turn capacitance, was synthesized from the experimental data. This magnet equivalent circuit can be used to predict the current ripple distribution along the superconducting magnet string and can provide dynamic information for the design of the collider current regulation loop.

  7. Random free energy barrier hopping model for ac conduction in chalcogenide glasses

    NASA Astrophysics Data System (ADS)

    Murti, Ram; Tripathi, S. K.; Goyal, Navdeep; Prakash, Satya

    2016-03-01

    The random free energy barrier hopping model is proposed to explain the ac conductivityac) of chalcogenide glasses. The Coulomb correlation is consistently accounted for in the polarizability and defect distribution functions and the relaxation time is augmented to include the overlapping of hopping particle wave functions. It is observed that ac and dc conduction in chalcogenides are due to same mechanism and Meyer-Neldel (MN) rule is the consequence of temperature dependence of hopping barriers. The exponential parameter s is calculated and it is found that s is subjected to sample preparation and measurement conditions and its value can be less than or greater than one. The calculated results for a - Se, As2S3, As2Se3 and As2Te3 are found in close agreement with the experimental data. The bipolaron and single polaron hopping contributions dominates at lower and higher temperatures respectively and in addition to high energy optical phonons, low energy optical and high energy acoustic phonons also contribute to the hopping process. The variations of hopping distance with temperature is also studied. The estimated defect number density and static barrier heights are compared with other existing calculations.

  8. Polaron conductivity mechanism in potassium acid phthalate crystal: AC-conductivity investigation

    NASA Astrophysics Data System (ADS)

    Filipič, Cene; Levstik, Iva; Levstik, Adrijan; Hadži, Dušan

    2016-08-01

    The complex dielectric constant, \\varepsilon *(ν ,T), of potassium acid phthalate monocrystal (KAP) was investigated over the broad frequency and temperature range. While the imaginary part of dielectric constant ε‧‧(ν) increases rapidly with increasing temperature in the studied temperature range, the real part of dielectric constant ε‧(ν) increases only at high temperatures; there is almost no change of ε‧(ν) below 200 K. Both values of ε‧ and ε‧‧ are frequency dependent; the values increase with decreasing frequencies. At temperatures below 450 K the ac electrical conductivity and dielectric constant follow simultaneously the universal dielectric response (UDR). The analysis of the temperature dependence of the UDR parameter s in terms of the theoretical model for small polarons revealed that this mechanism governs the charge transport in KAP crystal in the studied temperature range.

  9. Scaling of the holographic AC conductivity for non-Fermi liquids at criticality

    NASA Astrophysics Data System (ADS)

    Kiritsis, Elias; Peña-Benitez, Francisco

    2015-11-01

    The frequency dependence of the AC conductivity is studied in a holographic model of a non-fermi liquid that is amenable to both analytical and numerical computation. In the regime that dissipation dominates the DC conductivity, the AC conductivity is described well in the IR by a Drude peak despite the absence of quasiparticles. In the regime where pair-production-like processes dominate the conductivity there is no Drude peak. A scaling tail is found for the AC conductivity that is independent of the charge density and momentum dissipation. Evidence is given that this scaling tail σ AC ˜ ω m appears generically in quantum critical holographic systems and the associated scaling exponent m is calculated in terms of the Lifshitz and conduction critical exponents.

  10. Thermal conductivity Measurements of Kaolite

    SciTech Connect

    Wang, H

    2003-02-21

    Testing was performed to determine the thermal conductivity of Kaolite 1600, which primarily consists of Portland cement and vermiculite. The material was made by Thermal Ceramics for refractory applications. Its combination of light weight, low density, low cost, and noncombustibility made it an attractive alternative to the materials currently used in ES-2 container for radioactive materials. Mechanical properties and energy absorption tests of the Kaolite have been conducted at the Y-12 complex. Heat transfer is also an important factor for the application of the material. The Kaolite samples are porous and trap moisture after extended storage. Thermal conductivity changes as a function of moisture content below 100 C. Thermal conductivity of the Kaolite at high temperatures (up to 700 C) are not available in the literature. There are no standard thermal conductivity values for Kaolite because each sample is somewhat different. Therefore, it is necessary to measure thermal conductivity of each type of Kaolite. Thermal conductivity measurements will help the modeling and calculation of temperatures of the ES-2 containers. This report focuses on the thermal conductivity testing effort at ORNL.

  11. Temperature characterization of dielectric permittivity and AC conductivity of nano copper oxide-doped polyaniline composite

    NASA Astrophysics Data System (ADS)

    Shubha, L. N.; Madhusudana Rao, P.

    2016-06-01

    The polyaniline/copper oxide (PANI/CuO) nanocomposite was prepared by mixing solutions of polyaniline and copper oxide nanoparticles in dimethyl sulfoxide (DMSO). The synthesized polymer nanocomposites were characterized by X-ray powder diffraction (XRD), scanning electron microscope (SEM) and UV-visible spectroscopy. The characteristic peaks in XRD and UV-visible spectra confirmed the presence of CuO in the polymer structure. SEM images indicated morphological changes in the composite matrix as compared to the pristine PANI. The DC conductivity measurements were performed using two-probe method for various temperatures. AC conductivity and dielectric response of the composites were investigated in the frequency range of 102-106Hz using LCR meter. Dielectric permittivity ɛ‧(w) and dielectric loss factor ɛ‧‧(w) were investigated. It was observed that ɛ‧(w) and ɛ‧‧(w) decrease with increase in frequency at all temperatures. At a particular frequency it is observed that both ɛ‧(w) and ɛ‧‧(w) increase with increase in temperature. It was also observed that AC conductivity increased with increase in frequency and temperature.

  12. AC motor controller with 180 degree conductive switches

    NASA Technical Reports Server (NTRS)

    Oximberg, Carol A. (Inventor)

    1995-01-01

    An ac motor controller is operated by a modified time-switching scheme where the switches of the inverter are on for electrical-phase-and-rotation intervals of 180.degree. as opposed to the conventional 120.degree.. The motor is provided with three-phase drive windings, a power inverter for power supplied from a dc power source consisting of six switches, and a motor controller which controls the current controlled switches in voltage-fed mode. During full power, each switch is gated continuously for three successive intervals of 60.degree. and modulated for only one of said intervals. Thus, during each 60.degree. interval, the two switches with like signs are on continuously and the switch with the opposite sign is modulated.

  13. Workshop on thin film thermal conductivity measurements

    NASA Astrophysics Data System (ADS)

    Feldman, Albert; Balzaretti, Naira M.; Guenther, Arthur H.

    1998-04-01

    On a subject of considerable import to the laser-induced damage community, a two day workshop on the topic, Thin Film Thermal Conductivity Measurement was held as part of the 13th Symposium on Thermophysical Properties at the University of Colorado in Boulder CO, June 25 and 26, 1997. The Workshop consisted of 4 sessions of 17 oral presentations and two discussion sessions. Two related subjects of interest were covered; 1) methods and problems associated with measuring thermal conductivity ((kappa) ) of thin films, and 2) measuring and (kappa) of chemical vapor deposited (CVD) diamond. On the subject of thin film (kappa) measurement, several recently developed imaginative techniques were reviewed. However, several authors disagreed on how much (kappa) in a film differs from (kappa) in a bulk material of the same nominal composition. A subject of controversy was the definition of an interface. In the first discussion session, several questions were addressed, a principal one being, how do we know that the values of (kappa) we obtain are correct and is there a role for standards in thin film (kappa) measurement. The second discussion session was devoted to a round-robin interlaboratory comparison of (kappa) measurements on a set of CVD diamond specimens and several other specimens of lower thermal conductivity. Large interlaboratory differences obtained in an earlier round robin had been attributed to specimen inhomogeneity. Unfortunately, large differences were also observed in the second round robin even though the specimens were more homogenous. There was good consistency among the DC measurements, however, the AC measurements showed much greater variability. There was positive feedback from most of the attenders regarding the Workshop with nearly all respondents recommending another Workshop in three or fewer years. There was general recognition that thin film thermal conductivity measurements are important for predicting the resistance of optical coating

  14. Structural, dielectric and AC conductivity properties of Co2+ doped mixed alkali zinc borate glasses

    NASA Astrophysics Data System (ADS)

    Madhu, B. J.; Banu, Syed Asma; Harshitha, G. A.; Shilpa, T. M.; Shruthi, B.

    2013-02-01

    The Co2+ doped 19.9ZnO+5Li2CO3+25Na2CO3+50B2O3 (ZLNB) mixed alkali zinc borate glasses have been prepared by a conventional melt quenching method. The structural (XRD & FT-IR), dielectric and a.c. conductivityac) properties have been investigated. Amorphous nature of these glasses has been confirmed from their XRD pattern. The dielectric properties and electrical conductivityac) of these glasses have been studied from 100Hz to 5MHz at the room temperature. Based on the observed trends in the a.c. conductivities, the present glass samples are found to exhibit a non-Debye behavior.

  15. Synthesis, Spectroscopic, ac Conductivity and Thermal Studies on Co(III) Acetylacetonate-Iodine Complex

    NASA Astrophysics Data System (ADS)

    Hashem, H. A.; Refat, M. S.

    A spectrophotometric study of 1:1 donor-acceptor complex, cobalt (III) acetylacetonate (donor) and iodine (σ-acceptor) has been preformed. The equilibrium constants, (K) and the absorpitivity (ɛ) for the formation of the iodine complex have been calculated. The predicted structure of the solid triiodide charge-transfer complex reported in this study is further supported by thermal, far and mid infrared spectroscopic measurements. Electron transfer from Co (acac = 2, 4-pentanedionate)3 to iodine leads to the formation of an organic semiconductor with the formula of [Co(acac)3]_2 I+. I3-. The kinetic parameters (nonisothermal method) for their decomposition have been evaluated by graphical methods using the equations of Freeman-Carroll (FC), Horowitz-Metzger (HM) and Coats-Redfern (CR). The ac conductivity and dielectric properties of [Co(acac)3]_2 I+. I3- have been measured over the frequency 50-106 Hz at temperature 298 K.

  16. Calorimetric method of ac loss measurement in a rotating magnetic field.

    PubMed

    Ghoshal, P K; Coombs, T A; Campbell, A M

    2010-07-01

    A method is described for calorimetric ac-loss measurements of high-T(c) superconductors (HTS) at 80 K. It is based on a technique used at 4.2 K for conventional superconducting wires that allows an easy loss measurement in parallel or perpendicular external field orientation. This paper focuses on ac loss measurement setup and calibration in a rotating magnetic field. This experimental setup is to demonstrate measuring loss using a temperature rise method under the influence of a rotating magnetic field. The slight temperature increase of the sample in an ac-field is used as a measure of losses. The aim is to simulate the loss in rotating machines using HTS. This is a unique technique to measure total ac loss in HTS at power frequencies. The sample is mounted on to a cold finger extended from a liquid nitrogen heat exchanger (HEX). The thermal insulation between the HEX and sample is provided by a material of low thermal conductivity, and low eddy current heating sample holder in vacuum vessel. A temperature sensor and noninductive heater have been incorporated in the sample holder allowing a rapid sample change. The main part of the data is obtained in the calorimetric measurement is used for calibration. The focus is on the accuracy and calibrations required to predict the actual ac losses in HTS. This setup has the advantage of being able to measure the total ac loss under the influence of a continuous moving field as experienced by any rotating machines.

  17. Calorimetric method of ac loss measurement in a rotating magnetic field

    SciTech Connect

    Ghoshal, P. K.; Coombs, T. A.; Campbell, A. M.

    2010-07-15

    A method is described for calorimetric ac-loss measurements of high-T{sub c} superconductors (HTS) at 80 K. It is based on a technique used at 4.2 K for conventional superconducting wires that allows an easy loss measurement in parallel or perpendicular external field orientation. This paper focuses on ac loss measurement setup and calibration in a rotating magnetic field. This experimental setup is to demonstrate measuring loss using a temperature rise method under the influence of a rotating magnetic field. The slight temperature increase of the sample in an ac-field is used as a measure of losses. The aim is to simulate the loss in rotating machines using HTS. This is a unique technique to measure total ac loss in HTS at power frequencies. The sample is mounted on to a cold finger extended from a liquid nitrogen heat exchanger (HEX). The thermal insulation between the HEX and sample is provided by a material of low thermal conductivity, and low eddy current heating sample holder in vacuum vessel. A temperature sensor and noninductive heater have been incorporated in the sample holder allowing a rapid sample change. The main part of the data is obtained in the calorimetric measurement is used for calibration. The focus is on the accuracy and calibrations required to predict the actual ac losses in HTS. This setup has the advantage of being able to measure the total ac loss under the influence of a continuous moving field as experienced by any rotating machines.

  18. Calorimetric method of ac loss measurement in a rotating magnetic field

    NASA Astrophysics Data System (ADS)

    Ghoshal, P. K.; Coombs, T. A.; Campbell, A. M.

    2010-07-01

    A method is described for calorimetric ac-loss measurements of high-Tc superconductors (HTS) at 80 K. It is based on a technique used at 4.2 K for conventional superconducting wires that allows an easy loss measurement in parallel or perpendicular external field orientation. This paper focuses on ac loss measurement setup and calibration in a rotating magnetic field. This experimental setup is to demonstrate measuring loss using a temperature rise method under the influence of a rotating magnetic field. The slight temperature increase of the sample in an ac-field is used as a measure of losses. The aim is to simulate the loss in rotating machines using HTS. This is a unique technique to measure total ac loss in HTS at power frequencies. The sample is mounted on to a cold finger extended from a liquid nitrogen heat exchanger (HEX). The thermal insulation between the HEX and sample is provided by a material of low thermal conductivity, and low eddy current heating sample holder in vacuum vessel. A temperature sensor and noninductive heater have been incorporated in the sample holder allowing a rapid sample change. The main part of the data is obtained in the calorimetric measurement is used for calibration. The focus is on the accuracy and calibrations required to predict the actual ac losses in HTS. This setup has the advantage of being able to measure the total ac loss under the influence of a continuous moving field as experienced by any rotating machines.

  19. Ac-conductivity and dielectric response of new zinc-phosphate glass/metal composites

    NASA Astrophysics Data System (ADS)

    Maaroufi, A.; Oabi, O.; Lucas, B.

    2016-07-01

    The ac-conductivity and dielectric response of new composites based on zinc-phosphate glass with composition 45 mol%ZnO-55 mol%P2O5, filled with metallic powder of nickel (ZP/Ni) were investigated by impedance spectroscopy in the frequency range from 100 Hz to 1 MHz at room temperature. A high percolating jump of seven times has been observed in the conductivity behavior from low volume fraction of filler to the higher fractions, indicating an insulator - semiconductor phase transition. The measured conductivity at higher filler volume fraction is about 10-1 S/cm and is frequency independent, while, the obtained conductivity for low filler volume fraction is around 10-8 S/cm and is frequency dependent. Moreover, the elaborated composites are characterized by high dielectric constants in the range of 105 for conductive composites at low frequencies (100 Hz). In addition, the distribution of the relaxation processes was also evaluated. The Debye, Cole-Cole, Davidson-Cole and Havriliak-Negami models in electric modulus formalism were used to model the observed relaxation phenomena in ZP/Ni composites. The observed relaxation phenomena are fairly simulated by Davidson-Cole model, and an account of the interpretation of results is given.

  20. AC conductivity and structural properties of Mg-doped ZnO ceramic

    NASA Astrophysics Data System (ADS)

    Othman, Zayani Jaafar; Hafef, Olfa; Matoussi, Adel; Rossi, Francesca; Salviati, Giancarlo

    2015-11-01

    Undoped ZnO and Zn1- x Mg x O ceramic pellets were synthesized by the standard sintering method at the temperature of 1200 °C. The influence of Mg doping on the morphological, structural and electrical properties was studied. The scanning electron microscopy images revealed rough surface textured by grain boundaries and compacted grains having different shapes and sizes. Indeed, the X-ray diffraction reveals the alloying of hexagonal ZnMgO phase and the segregation of cubic MgO phase. The crystallite size, strain and stress were studied using Williamson-Hall (W-H) method. The results of mean particle size of Zn1- x Mg x O composites showed an inter-correlation with W-H analysis and Sherrer method. The electrical conductivity of the films was measured from 173 to 373 K in the frequency range of 0.1 Hz-1 MHz to identify the dominant conductivity mechanism. The DC conductivity is thermally activated by electron traps having activation energy of about 0.09 to 0.8 eV. The mechanisms of AC conductivity are controlled by the correlated barrier hopping model for the ZnO sample and the small polaron tunneling (SPT) model for Zn0.64Mg0.36O and Zn0.60Mg0.40O composites.

  1. Hydraulic Conductivity Measurements Barrow 2014

    DOE Data Explorer

    Katie McKnight; Tim Kneafsey; Craig Ulrich; Jil Geller

    2015-02-22

    Six individual ice cores were collected from Barrow Environmental Observatory in Barrow, Alaska, in May of 2013 as part of the Next Generation Ecosystem Experiment (NGEE). Each core was drilled from a different location at varying depths. A few days after drilling, the cores were stored in coolers packed with dry ice and flown to Lawrence Berkeley National Laboratory (LBNL) in Berkeley, CA. 3-dimensional images of the cores were constructed using a medical X-ray computed tomography (CT) scanner at 120kV. Hydraulic conductivity samples were extracted from these cores at LBNL Richmond Field Station in Richmond, CA, in February 2014 by cutting 5 to 8 inch segments using a chop saw. Samples were packed individually and stored at freezing temperatures to minimize any changes in structure or loss of ice content prior to analysis. Hydraulic conductivity was determined through falling head tests using a permeameter [ELE International, Model #: K-770B]. After approximately 12 hours of thaw, initial falling head tests were performed. Two to four measurements were collected on each sample and collection stopped when the applied head load exceeded 25% change from the original load. Analyses were performed between 2 to 3 times for each sample. The final hydraulic conductivity calculations were computed using methodology of Das et al., 1985.

  2. Electron Temperature Measurement by Floating Probe Method Using AC Voltage

    NASA Astrophysics Data System (ADS)

    Satoshi, Nodomi; Shuichi, Sato; Mikio, Ohuchi

    2016-11-01

    This study presents a novel floating probe method to measure electron temperatures using a hollow cathode-type discharge tube. The proposed method detects a shift in the floating potential when an AC voltage is applied to a probe through an intermediary blocking capacitor. The shift in the floating potential is described as a function of the electron temperature and the applied AC voltage. The floating probe method is simpler than the Langmuir probe method because it does not require the measurement of volt-ampere characteristics. As the input AC voltage increases, the electron temperature converges. The electron temperature measured using the floating probe method with an applied sinusoidal voltage shows a value close to the first (tail) electron temperature in the range of the floating potential.

  3. ac conductance in granular insulating Co-ZrO{sub 2} thin films: A universal response

    SciTech Connect

    Konstantinovic, Zorica; Garcia del Muro, Montserrat; Kovylina, Miroslavna; Batlle, Xavier; Labarta, Amilcar

    2009-03-01

    The ac conductance in granular insulating Co-ZrO{sub 2} thin films prepared by pulsed laser deposition is systematically studied as a function of the Co volume content x. An absorption phenomenon at low frequencies that mimics the universal response of disordered dielectric materials is observed in the range of metal content below the Co percolation threshold x{sub p}{approx_equal}0.35 in the so-called dielectric regime. The temperature and frequency dependences of this absorption phenomenon are successfully analyzed in terms of random competing conduction channels between Co particles through thermally assisted tunneling and capacitive conductance. The ac conductance is well correlated with the nanostructure of the samples obtained by the transmission electron microscopy and perfectly matches the calculated ac response for a random resistor-capacitor network. We also show the occurrence of fractional power-law dependences on the frequency of the ac conductance taking place at very low frequencies as compared to the typical ranges at which dispersive behavior is observed in classical-disordered dielectric materials.

  4. Charging in the ac Conductance of a Double Barrier Resonant Tunneling Structure

    NASA Technical Reports Server (NTRS)

    Anantram, M. P.; Saini, Subhash (Technical Monitor)

    1998-01-01

    There have been many studies of the linear response ac conductance of a double barrier resonant tunneling structure (DBRTS), both at zero and finite dc biases. While these studies are important, they fail to self consistently include the effect of the time dependent charge density in the well. In this paper, we calculate the ac conductance at both zero and finite do biases by including the effect of the time dependent charge density in the well in a self consistent manner. The charge density in the well contributes to both the flow of displacement currents in the contacts and the time dependent potential in the well. We find that including these effects can make a significant difference to the ac conductance and the total ac current is not equal to the simple average of the non-selfconsistently calculated conduction currents in the two contacts. This is illustrated by comparing the results obtained with and without the effect of the time dependent charge density included correctly. Some possible experimental scenarios to observe these effects are suggested.

  5. Theoretical analysis on ac susceptibility measurements of superconductor tapes

    NASA Astrophysics Data System (ADS)

    Chen, Du-Xing; Sun, Yue-Ming; Li, Shuo; Fang, Jin

    2017-02-01

    Perpendicular ac susceptibility χ ={χ\\prime}-j{χ\\prime \\prime} of a superconducting long tape defined by magnetic moment and determined inductively by magnetic flux is calculated using Brandt’s technique from a power-law dependence of electric field on sheet current density. The requirements of χ measurements to the experimental setup and procedure are discussed based on the calculation results.

  6. AC Conductivity Studies in Lithium-Borate Glass Containing Gold Nanoparticles

    NASA Astrophysics Data System (ADS)

    Shivaprakash, Y.; Anavekar, R. V.

    2011-07-01

    Gold nanoparticles have been synthesized in a base glass with composition 30Li2O-70B2O3 using gold chloride (HAuCl4.3H2O) as a dopant. The samples are characterized using XRD, ESR, SEM and optical absorption in the visible range. AC conductivity studies have been performed at RT over a frequency range 100 to 10 MHz. The dc conductivity is calculated from the complex impedence plot. The dc conductivity is found to be increasing with the increase of dopant concentration. AC conductivity data is fitted with Almond-West law with power exponent `s'. The values of `s' is found to lie in the range of 0.70-0.73.

  7. Ionic ac and dc conductivities of NaCrP2O7 compound

    NASA Astrophysics Data System (ADS)

    Sassi, M.; Oueslati, A.; Gargouri, M.

    2015-05-01

    The NaCrP2O7 compound was prepared by the solid-state reaction method. The formation of a single-phase material was confirmed by the X-ray diffraction studies and found to be a monoclinic system. The electrical properties of this compound have been measured in the temperature range from 523 to 673 K and the frequency range from 209 Hz to 5 MHz. The Nyquist plots are well fitted to an equivalent circuit consisting of a series of combination of grains and grain boundary elements. The ac conductivity of NaCrP2O7 has been analyzed as a function of temperature and frequency. The scaling behavior of the imaginary part of the complex modulus suggests that the relaxation describes the same mechanism at various temperatures. The conductivity and modulus formalisms provide nearly the same activation energies for electrical relaxation of mobile ions suggesting that the ion transport is probably due to a hopping mechanism dominated by the motion of the monovalent ions Na+ along tunnels presented in the structure of the investigated material.

  8. Measurement of the 225Ac half-life.

    PubMed

    Pommé, S; Marouli, M; Suliman, G; Dikmen, H; Van Ammel, R; Jobbágy, V; Dirican, A; Stroh, H; Paepen, J; Bruchertseifer, F; Apostolidis, C; Morgenstern, A

    2012-11-01

    The (225)Ac half-life was determined by measuring the activity of (225)Ac sources as a function of time, using various detection techniques: α-particle counting with a planar silicon detector at a defined small solid angle and in a nearly-2π geometry, 4πα+β counting with a windowless CsI sandwich spectrometer and with a pressurised proportional counter, gamma-ray spectrometry with a HPGe detector and with a NaI(Tl) well detector. Depending on the technique, the decay was followed for 59-141 d, which is about 6-14 times the (225)Ac half-life. The six measurement results were in good mutual agreement and their mean value is T(1/2)((225)Ac)=9.920 (3)d. This half-life value is more precise and better documented than the currently recommended value of 10.0 d, based on two old measurements lacking uncertainty evaluations.

  9. Gas sensing properties of magnesium doped SnO{sub 2} thin films in relation to AC conduction

    SciTech Connect

    Deepa, S.; Skariah, Benoy Thomas, Boben; Joseph, Anisha

    2014-01-28

    Conducting magnesium doped (0 to 1.5 wt %) tin oxide thin films prepared by Spray Pyrolysis technique achieved detection of 1000 ppm of LPG. The films deposited at 304 °C exhibit an enhanced response at an operating temperature of 350 °C. The microstructural properties are studied by means of X-ray diffraction. AC conductivity measurements are carried out using precision LCR meter to analyze the parameters that affect the variation in sensing. The results are correlated with compositional parameters and the subsequent modification in the charge transport mechanism facilitating an enhanced LPG sensing action.

  10. Gas sensing properties of magnesium doped SnO2 thin films in relation to AC conduction

    NASA Astrophysics Data System (ADS)

    Deepa, S.; Joseph, Anisha; Skariah, Benoy; Thomas, Boben

    2014-01-01

    Conducting magnesium doped (0 to 1.5 wt %) tin oxide thin films prepared by Spray Pyrolysis technique achieved detection of 1000 ppm of LPG. The films deposited at 304 °C exhibit an enhanced response at an operating temperature of 350 °C. The microstructural properties are studied by means of X-ray diffraction. AC conductivity measurements are carried out using precision LCR meter to analyze the parameters that affect the variation in sensing. The results are correlated with compositional parameters and the subsequent modification in the charge transport mechanism facilitating an enhanced LPG sensing action.

  11. Measurements of AC Losses and Current Distribution in Superconducting Cables

    SciTech Connect

    Nguyen, Doan A; Ashworth, Stephen P; Duckworth, Robert C; Carter, Bill; Fleshler, Steven

    2011-01-01

    This paper presents our new experimental facility and techniques to measure ac loss and current distribution between the layers for High Temperature Superconducting (HTS) cables. The facility is powered with a 45 kVA three-phase power supply which can provide three-phase currents up to 5 kA per phase via high current transformers. The system is suitable for measurements at any frequency between 20 and 500 Hz to better understand the ac loss mechanisms in HTS cables. In this paper, we will report techniques and results for ac loss measurements carried out on several HTS cables with and without an HTS shielding layer. For cables without a shielding layer, care must be taken to control the effect of the magnetic fields from return currents on loss measurements. The waveform of the axial magnetic field was also measured by a small pick-up coil placed inside a two-layer cable. The temporal current distribution between the layers can be calculated from the waveform of the axial field.

  12. AC-coupled front-end for biopotential measurements.

    PubMed

    Spinelli, Enrique Mario; Pallàs-Areny, Ramon; Mayosky, Miguel Angel

    2003-03-01

    AC coupling is essential in biopotential measurements. Electrode offset potentials can be several orders of magnitude larger than the amplitudes of the biological signals of interest, thus limiting the admissible gain of a dc-coupled front end to prevent amplifier saturation. A high-gain input stage needs ac input coupling. This can be achieved by series capacitors, but in order to provide a bias path, grounded resistors are usually included, which degrade the common mode rejection ratio (CMRR). This paper proposes a novel balanced input ac-coupling network that provides a bias path without any connection to ground, thus resulting in a high CMRR. The circuit being passive, it does not limit the differential dc input voltage. Furthermore, differential signals are ac coupled, whereas common-mode voltages are dc coupled, thus allowing the closed-loop control of the dc common mode voltage by means of a driven-right-leg circuit. This makes the circuit compatible with common-mode dc shifting strategies intended for single-supply biopotential amplifiers. The proposed circuit allows the implementation of high-gain biopotential amplifiers with a reduced number of parts, thus resulting in low power consumption. An electrocardiogram amplifier built according to the proposed design achieves a CMRR of 123 dB at 50 Hz.

  13. Investigation on the AC loss characteristics of MgB 2 wires by using a conduction cooling device

    NASA Astrophysics Data System (ADS)

    Jin, H. B.; Li, Z.; Ryu, K.

    2011-11-01

    In this study, we have experimentally investigated the AC loss characteristics of MgB2 wires with matrix of Fe and Cu by using a conduction cooling device. We fabricated the conduction cooling device to cool MgB2 wires down to 4 K. We also developed our unique test method, which is called AC pulse technique, to evaluate their AC loss characteristics within few hundred milliseconds. The test results show that the AC loss of the Fe/MgB2 wire is mainly generated in the ferromagnetic Fe matrix. Its AC loss is ten times larger than that of the Cu/MgB2 wire. In this paper, the evaluation technique of AC loss by using the conduction cooling device is described and the test results are discussed.

  14. Experimental and theoretical study of AC electrical conduction mechanisms of semicrystalline parylene C thin films.

    PubMed

    Kahouli, Abdelkader; Sylvestre, Alain; Jomni, Fethi; Yangui, Béchir; Legrand, Julien

    2012-01-26

    The electrical conduction mechanisms of semicrystalline thermoplastic parylene C (-H(2)C-C(6)H(3)Cl-CH(2)-)(n) thin films were studied in large temperature and frequency regions. The alternative current (AC) electrical conduction in parylene C is governed by two processes which can be ascribed to a hopping transport mechanism: correlated barrier hopping (CBH) model at low [77-155 K] and high [473-533 K] temperature and the small polaron tunneling mechanism (SPTM) from 193 to 413 K within the framework of the universal law of dielectric response. The conduction mechanism is explained with the help of Elliot's theory, and the Elliot's parameters are determined. From frequency- and temperature-conductivity characteristics, the activation energy is found to be 1.27 eV for direct current (DC) conduction interpreted in terms of ionic conduction mechanism. The power law dependence of AC conductivity is interpreted in terms of electron hopping with a density N(E(F)) (~10(18) eV cm(-3)) over a 0.023-0.03 eV high barrier across a distance of 1.46-1.54 Å.

  15. AC Conductivity and Diffuse Reflectance Studies of Ag-TiO2 Nanoparticles

    NASA Astrophysics Data System (ADS)

    Abdul Gafoor, A. K.; Musthafa, M. M.; Pradyumnan, P. P.

    2012-09-01

    Silver (Ag)-TiO2 nanoparticles synthesized by a low-temperature hydrothermal method in the anatase phase have been investigated by x-ray diffraction. Transmission electron microscopy has been used for morphological studies. Surface areas were studied by the Brunauer-Emmett-Teller method. Alternating-current (AC) conductivity and dielectric properties were studied for various dopant levels of 0.25 wt.%, 0.5 wt.%, and 1.0 wt.% at 300 K in the frequency range from 42 Hz to 5 MHz. AC conductivity and dielectric properties of TiO2 nanoparticles were greatly affected by loading with Ag. At high frequencies, the materials showed high AC conductivity and low dielectric constant. Diffuse reflectance studies were carried out for various dopant levels at 300 K by ultraviolet-visible (UV-Vis) spectroscopy. Considerable absorption of visible light by 0.5 wt.% and 1.0 wt.% Ag-TiO2 nanoparticles was observed due to the decrease of the energy band gap on Ag loading.

  16. Microwave a.c. conductivity of domain walls in ferroelectric thin films

    PubMed Central

    Tselev, Alexander; Yu, Pu; Cao, Ye; Dedon, Liv R.; Martin, Lane W.; Kalinin, Sergei V.; Maksymovych, Petro

    2016-01-01

    Ferroelectric domain walls are of great interest as elementary building blocks for future electronic devices due to their intrinsic few-nanometre width, multifunctional properties and field-controlled topology. To realize the electronic functions, domain walls are required to be electrically conducting and addressable non-destructively. However, these properties have been elusive because conducting walls have to be electrically charged, which makes them unstable and uncommon in ferroelectric materials. Here we reveal that spontaneous and recorded domain walls in thin films of lead zirconate and bismuth ferrite exhibit large conductance at microwave frequencies despite being insulating at d.c. We explain this effect by morphological roughening of the walls and local charges induced by disorder with the overall charge neutrality. a.c. conduction is immune to large contact resistance enabling completely non-destructive walls read-out. This demonstrates a technological potential for harnessing a.c. conduction for oxide electronics and other materials with poor d.c. conduction, particularly at the nanoscale. PMID:27240997

  17. Microwave a.c. conductivity of domain walls in ferroelectric thin films.

    PubMed

    Tselev, Alexander; Yu, Pu; Cao, Ye; Dedon, Liv R; Martin, Lane W; Kalinin, Sergei V; Maksymovych, Petro

    2016-05-31

    Ferroelectric domain walls are of great interest as elementary building blocks for future electronic devices due to their intrinsic few-nanometre width, multifunctional properties and field-controlled topology. To realize the electronic functions, domain walls are required to be electrically conducting and addressable non-destructively. However, these properties have been elusive because conducting walls have to be electrically charged, which makes them unstable and uncommon in ferroelectric materials. Here we reveal that spontaneous and recorded domain walls in thin films of lead zirconate and bismuth ferrite exhibit large conductance at microwave frequencies despite being insulating at d.c. We explain this effect by morphological roughening of the walls and local charges induced by disorder with the overall charge neutrality. a.c. conduction is immune to large contact resistance enabling completely non-destructive walls read-out. This demonstrates a technological potential for harnessing a.c. conduction for oxide electronics and other materials with poor d.c. conduction, particularly at the nanoscale.

  18. Microwave a.c. conductivity of domain walls in ferroelectric thin films

    SciTech Connect

    Tselev, Alexander; Yu, Pu; Cao, Ye; Dedon, Liv R.; Martin, Lane W.; Kalinin, Sergei V.; Maksymovych, Petro

    2016-05-31

    Ferroelectric domain walls are of great interest as elementary building blocks for future electronic devices due to their intrinsic few-nanometre width, multifunctional properties and field-controlled topology. To realize the electronic functions, domain walls are required to be electrically conducting and addressable non-destructively. However, these properties have been elusive because conducting walls have to be electrically charged, which makes them unstable and uncommon in ferroelectric materials. Here we reveal that spontaneous and recorded domain walls in thin films of lead zirconate and bismuth ferrite exhibit large conductance at microwave frequencies despite being insulating at d.c. We explain this effect by morphological roughening of the walls and local charges induced by disorder with the overall charge neutrality. a.c. conduction is immune to large contact resistance enabling completely non-destructive walls read-out. Finally, this demonstrates a technological potential for harnessing a.c. conduction for oxide electronics and other materials with poor d.c. conduction, particularly at the nanoscale.

  19. Microwave a.c. conductivity of domain walls in ferroelectric thin films

    DOE PAGES

    Tselev, Alexander; Yu, Pu; Cao, Ye; ...

    2016-05-31

    Ferroelectric domain walls are of great interest as elementary building blocks for future electronic devices due to their intrinsic few-nanometre width, multifunctional properties and field-controlled topology. To realize the electronic functions, domain walls are required to be electrically conducting and addressable non-destructively. However, these properties have been elusive because conducting walls have to be electrically charged, which makes them unstable and uncommon in ferroelectric materials. Here we reveal that spontaneous and recorded domain walls in thin films of lead zirconate and bismuth ferrite exhibit large conductance at microwave frequencies despite being insulating at d.c. We explain this effect by morphologicalmore » roughening of the walls and local charges induced by disorder with the overall charge neutrality. a.c. conduction is immune to large contact resistance enabling completely non-destructive walls read-out. Finally, this demonstrates a technological potential for harnessing a.c. conduction for oxide electronics and other materials with poor d.c. conduction, particularly at the nanoscale.« less

  20. Temperature and frequency dependence of AC conductivity of new quaternary Se-Te-Bi-Pb chalcogenide glasses

    NASA Astrophysics Data System (ADS)

    Yadav, Preeti; Sharma, Ambika

    2016-05-01

    The aim of the present work is to study the temperature and frequency dependence of ac conductivity of new quaternary Se84-xTe15Bi1.0Pbx chalcogenide glasses. The Se84-xTe15Bi1.0Pbx (x = 2, 6) glassy alloys are prepared by using melt quenching technique. The temperature and frequency dependent behavior of ac conductivity σac(ω) has been carried out in the frequency range 42 Hz to 5 MHz and in the temperature range of 298-323 K below glass transition temperature. The behavior of ac conductivity is described in terms of the power law ωs. The obtained temperature dependence behavior of ac conductivity and frequency component (s) are explained by means of correlated barrier hopping model recommended by Elliot.

  1. Measured losses in superconductor magnets for 60-Hertz ac operation.

    NASA Technical Reports Server (NTRS)

    Hamlet, I. L.; Kilgore, R. A.

    1971-01-01

    Results of an experimental study of electrical losses in superconductor magnets. Preliminary 60-Hz ac loss data are presented for coils constructed of Nb3Sn ribbon, Nb-Ti cable, and multifilament Nb-Ti. Losses have been measured for different size coils up to approximately 20 cm in diameter. Of the conductor types tested, Nb3Sn ribbon has the lowest losses for ac operation. In Nb3Sn-ribbon coils of different sizes, the loss per unit length of conductor is shown to decrease with a decrease in the rate of change of current and to increase, in general, with increase in coil size. An important aspect of the study is the high degree of repeatability of the data.

  2. Instantaneous velocity measurement of AC electroosmotic flows by laser induced fluorescence photobleaching anemometer with high temporal resolution

    NASA Astrophysics Data System (ADS)

    Zhao, Wei; Yang, Fang; Qiao, Rui; Wang, Guiren; Rui Qiao Collaboration

    2015-11-01

    Understanding the instantaneous response of flows to applied AC electric fields may help understand some unsolved issues in induced-charge electrokinetics and enhance performance of microfluidic devices. Since currently available velocimeters have difficulty in measuring velocity fluctuations with frequency higher than 1 kHz, most experimental studies so far focus only on the average velocity measurement in AC electrokinetic flows. Here, we present measurements of AC electroosmotic flow (AC-EOF) response time in microchannels by a novel velocimeter with submicrometer spatial resolution and microsecond temporal resolution, i.e. laser-induced fluorescence photobleaching anemometer (LIFPA). Several parameters affecting the AC-EOF response time to the applied electric signal were investigated, i.e. channel length, transverse position and solution conductivity. The experimental results show that the EOF response time under a pulsed electric field decreases with the reduction of the microchannel length, distance between the detection position to the wall and the conductivity of the solution. This work could provide a new powerful tool to measure AC electrokinetics and enhance our understanding of AC electrokinetic flows.

  3. Effect of nanosilica on optical, electric modulus and AC conductivity of polyvinyl alcohol/polyaniline films

    NASA Astrophysics Data System (ADS)

    El-Sayed, Somyia; Abel-Baset, Tarob; Elfadl, Azza Abou; Hassen, Arafa

    2015-05-01

    Nanosilica (NS) was synthesized by a sol-gel method and mixed with 0.98 polyvinyl alcohol (PVA)/0.02 polyaniline (PANI) in different amounts to produce nanocomposite films. High-resolution transmission electron microscopy (HR-TEM) revealed the average particle size of the NS to be ca. 15 nm. Scanning electron microscopy (SEM) showed that the NS was well-dispersed on the surface of the PVA/PNAI films. The Fourier transform infrared (FTIR) spectra of the samples showed a significant change in the intensity of the characteristic peak of the functional groups in the composite films with the amount of NS added. The absorbance and refractive index (n) of the composites were studied in the UV-vis range, and the optical energy band gap, Eg, and different optical parameters were calculated. The dielectric loss modulus, M″ and ac conductivity, σac, of the samples were studied within 300-425 K and 0.1 kHz-5 MHz, respectively. Two relaxation peaks were observed in the frequency dependence of the dielectric loss modulus, M″. The behavior of σac(f) for the composite films indicated that the conduction mechanism was correlated barrier hopping (CBH). The results of this work are discussed and compared with those of previous studies of similar composites.

  4. Thermal Conductivity Measurement using Thermoelectric Module

    NASA Astrophysics Data System (ADS)

    Ajiwiguna, T. A.; Kim, S. Y.

    2016-11-01

    In this study, thermoelectric module is used as a heater for thermal conductivity measurement of solid materials. Principle of temperature gradient is adopted in this measurement. Stainless steel is utilized as a reference material. Each temperatures are measured by t-type thermocouple and the thermal conductivity is then calculated. The result shows that the thermal conductivity of tested materials is 0.303 W/mK with maximum uncertainty of 3.79%. To assure the result of this measurement, the thermal conductivity of tested material is also measured by laser flash method. The difference result of both measurement is below 5%.

  5. AC impedance spectroscopy and conductivity studies of Dy doped Bi4V2O11 ceramics

    NASA Astrophysics Data System (ADS)

    Bag, Sasmitarani; Das, Parthasarathi; Behera, Banarji

    2017-03-01

    The ac impedance and conductivity properties of Dy doped Bi4V2 - x Dy x O11 (x = 0.05, 0.10, 0.15 and 0.20) ceramics prepared by solid-state reaction technique, in a wide frequency range at different temperatures have been studied. All the samples exhibited β-type phase orthorhombic structure at room temperature. The Nyquist plot confirmed the presence of both grain and grain boundary effects for all Dy doped samples. Double relaxation behavior was also observed. The grain and grain boundary resistance decreases with rise in temperature for all the concentration and exhibits a typical negative temperature co-efficient of resistance (NTCR) behavior. An analysis of the electric modulus suggests the possible hopping mechanism for electrical transport processes of all the materials. The ac conductivity spectrum obeys Jonscher's universal power law. DC conductivity of the materials were also studied and values of the activation energy found to be 0.40, 0.49, 0.73 and 0.78 eV for the compositions x = 0.05, 0.10, 0.15 and 0.20, respectively, at different temperatures (150-375 °C).

  6. AC conductivity studies of Fe doped TiO2 nanotubes

    NASA Astrophysics Data System (ADS)

    Vijayan, P. P.; Thomas, M.; George, K. C.

    2015-02-01

    Fe-doped TiO2 nanotubes are prepared by the combination of sol-gel process with hydrothermal treatment. The morphology and crystalline structure of TiO2 nanotubes are characterized by transmission electron microscopy (TEM), X-ray diffraction respectively (XRD). Fe doping induces a structural transformation from anatase to rutile. The temperature dependence of the ac electrical conductivity is investigated in the temperature range 303-413 K. Positive temperature coefficient of resistance is observed in the Fe doped TiO2 nanotubes. PL spectrum shows the presence of oxygen vacancies and self trapped excitons in Fe doped TiO2 nanotubes and undoped samples.

  7. AC Magnetic Properties of Large Volume of Water — Susceptibility Measurement in Unshielded Environment

    NASA Astrophysics Data System (ADS)

    Tsukada, Keiji; Kiwa, Toshihiko; Masuda, Yuuki

    2006-10-01

    To investigate the effect of low-frequency magnetic-field exposure of a human body, the low-frequency AC magnetic property of a large volume of water was measured by low-frequency magnetic field exposure (from 50 Hz to 1.2 kHz). The results indicate that the AC magnetic property of water is due to diamagnetism in the low-frequency range. The phase between the main magnetic field and the generated magnetic field remained constant at about 180°. Results were not affected by conductivity or pH. Moreover, the magnetic-field strength from water showed a susceptibility frequency dependence proportional to the frequency above approximately 400 Hz. Because of the incremental effects of susceptibility, the magnetic field from water was measured using a conventional magnetic sensor (magnetic resistive; MR) in an unshielded environment.

  8. AC conductivity scaling behavior in grain and grain boundary response regime of fast lithium ionic conductors

    NASA Astrophysics Data System (ADS)

    Mariappan, C. R.

    2014-05-01

    AC conductivity spectra of Li-analogues NASICON-type Li1.5Al0.5Ge1.5P3O12 (LAGP), Li-Al-Ti-P-O (LATP) glass-ceramics and garnet-type Li7La2Ta2O13 (LLTO) ceramic are analyzed by universal power law and Summerfield scaling approaches. The activation energies and pre-exponential factors of total and grain conductivities are following the Meyer-Neldel (M-N) rule for NASICON-type materials. However, the garnet-type LLTO material deviates from the M-N rule line of NASICON-type materials. The frequency- and temperature-dependent conductivity spectra of LAGP and LLTO are superimposed by Summerfield scaling. The scaled conductivity curves of LATP are not superimposed at the grain boundary response region. The superimposed conductivity curves are observed at cross-over frequencies of grain boundary response region for LATP by incorporating the exp ( {{{ - (EAt - EAg )} {{{ - (EAt - EAg )} {kT}}} ) factor along with Summerfield scaling factors on the frequency axis, where EAt and EAg are the activation energies of total and grain conductivities, respectively.

  9. New method for measuring the thermal conductivity.

    PubMed

    Goldratt, E; Greenfield, A J

    1978-11-01

    A new experimental method is presented for measuring the thermal conductivity as a function of temperature. The basic innovation lies in extracting from the measured temperature profile of a sample in vacuo, the thermal conductivity of each individual cross-sectional sample element. The estimated experimental error is +/-1%. Not only is high accuracy achieved, but also a self-checking procedure offers the possibility of avoiding systematic errors. Measurements on two samples of type 304 stainless steel are presented. Three independent sets of measurements give consistent values for the thermal conductivity to well within the estimated error of +/-1%.

  10. AC and DC conductivity of ionic liquid containing polyvinylidene fluoride thin films

    NASA Astrophysics Data System (ADS)

    Frübing, Peter; Wang, Feipeng; Kühle, Till-Friedrich; Gerhard, Reimund

    2016-01-01

    Polarisation processes and charge transport in polyvinylidene fluoride (PVDF) with a small amount (0.01-10 wt%) of the ionic liquid (IL) 1-ethyl-3-methylimidazolium nitrate ({[EMIM]}^+[{NO}_3]^-) are investigated by means of dielectric spectroscopy. The response of PVDF that contains more than 0.01 wt% IL is dominated by a low-frequency relaxation which shows typical signatures of electrode polarisation. Furthermore, the α a relaxation, related to the glass transition, disappears for IL contents of more than 1 wt%, which indicates that the amorphous phase loses its glass-forming properties and undergoes structural changes. The DC conductivity is determined from the low-frequency limit of the AC conductivity and from the dielectric loss peak related to the electrode polarisation. DC conductivities of 10^{-10} to 10^{-2} {S}/{m} are obtained—increasing with IL content and temperature. The dependence of the DC conductivity on the IL content follows a power law with an exponent greater than one, indicating an increase in the ion mobility. The temperature dependence of the DC conductivity shows Vogel-Fulcher-Tammann behaviour, which implies that charge transport is coupled to polymer chain motion. Mobile ion densities and ion mobilities are calculated from the DC conductivity and the dielectric loss related to electrode polarisation, with the results that less than one per cent of the total ion concentration contributes to the conductivity and that the strong increase in conductivity with temperature is mainly caused by a strong increase in ion mobility. This leads to the conclusion that in particular the ion mobility must be reduced in order to decrease the DC conductivity.

  11. Electric properties of carbon nano-onion/polyaniline composites: a combined electric modulus and ac conductivity study

    NASA Astrophysics Data System (ADS)

    Papathanassiou, Anthony N.; Mykhailiv, Olena; Echegoyen, Luis; Sakellis, Ilias; Plonska-Brzezinska, Marta E.

    2016-07-01

    The complex electric modulus and the ac conductivity of carbon nano-onion/polyaniline composites were studied from 1 mHz to 1 MHz at isothermal conditions ranging from 15 K to room temperature. The temperature dependence of the electric modulus and the dc conductivity analyses indicate a couple of hopping mechanisms. The distinction between thermally activated processes and the determination of cross-over temperature were achieved by exploring the temperature dependence of the fractional exponent of the dispersive ac conductivity and the bifurcation of the scaled ac conductivity isotherms. The results are analyzed by combining the granular metal model (inter-grain charge tunneling of extended electron states located within mesoscopic highly conducting polyaniline grains) and a 3D Mott variable range hopping model (phonon assisted tunneling within the carbon nano-onions and clusters).

  12. Phonon effects on the current noise spectra and the ac conductance of a single molecular junction.

    PubMed

    Ding, Guo-Hui; Dong, Bing

    2014-07-30

    By using nonequilibrium Green's functions and the equation of motion method, we formulate a self-consistent field theory for the electron transport through a single-molecule junction (SMJ) coupled with a vibrational mode. We show that the nonequilibrium dynamics of the phonons in a strong electron-phonon coupling regime can be taken into account appropriately in this self-consistent perturbation theory, and the self-energy of the phonons is connected with the current fluctuations in the molecular junction. We calculate the finite-frequency nonsymmetrized noise spectra and the ac conductance, which reveal a wealth of inelastic electron tunneling characteristics on the absorption and emission properties of this SMJ. In the presence of a finite bias voltage and the electron tunneling current, the vibration mode of the molecular junction is heated and driven to an unequilibrated state. The influences of unequilibrated phonons on the current and the noise spectra are investigated.

  13. Phonon effects on the current noise spectra and the ac conductance of a single molecular junction

    NASA Astrophysics Data System (ADS)

    Ding, Guo-Hui; Dong, Bing

    2014-07-01

    By using nonequilibrium Green’s functions and the equation of motion method, we formulate a self-consistent field theory for the electron transport through a single-molecule junction (SMJ) coupled with a vibrational mode. We show that the nonequilibrium dynamics of the phonons in a strong electron-phonon coupling regime can be taken into account appropriately in this self-consistent perturbation theory, and the self-energy of the phonons is connected with the current fluctuations in the molecular junction. We calculate the finite-frequency nonsymmetrized noise spectra and the ac conductance, which reveal a wealth of inelastic electron tunneling characteristics on the absorption and emission properties of this SMJ. In the presence of a finite bias voltage and the electron tunneling current, the vibration mode of the molecular junction is heated and driven to an unequilibrated state. The influences of unequilibrated phonons on the current and the noise spectra are investigated.

  14. AC conductivity and dielectric relaxation of tris(N,N-dimethylanilinium) hexabromidostannate(IV) bromide: (C8H12N)3SnBr6.Br

    NASA Astrophysics Data System (ADS)

    Chouaib, H.; Kamoun, S.

    2015-10-01

    The X-ray powder analysis, thermogravimetric analysis, differential scanning calorimetry analysis and complex impedance spectroscopic data have been carried out on (C8H12N)3SnBr6.Br compound. The results show that this compound exhibits a phase transition at (T=365±2 K) which has been characterized by differential scanning calorimetry (DSC), AC conductivity and dielectric measurements. The AC conductivity, the modulus analysis, the dielectric constants and the polarizability have been studied using impedance in the temperature range from 334 K to 383 K and in the frequency range between 20 Hz and 2 MHz. The temperature dependence of DC conductivity follows the Arrhenius law. Moreover, the frequency dependence of conductivity follows Jonscher's dynamical law with the relation: σ(ω , T) =σDC + B(T)ω s(T) . Relaxation peaks can be observed in the complex modulus analysis and after a transformation of the complex permittivity ε* to the complex polarizability α*.

  15. Absorption and Attenuation Coefficients Using the WET Labs ac-s in the Mid-Atlantic Bight: Field Measurements and Data Analysis

    NASA Technical Reports Server (NTRS)

    Ohi, Nobuaki; Makinen, Carla P.; Mitchell, Richard; Moisan, Tiffany A.

    2008-01-01

    Ocean color algorithms are based on the parameterization of apparent optical properties as a function of inherent optical properties. WET Labs underwater absorption and attenuation meters (ac-9 and ac-s) measure both the spectral beam attenuation [c (lambda)] and absorption coefficient [a (lambda)]. The ac-s reports in a continuous range of 390-750 nm with a band pass of 4 nm, totaling approximately 83 distinct wavelengths, while the ac-9 reports at 9 wavelengths. We performed the ac-s field measurements at nine stations in the Mid-Atlantic Bight from water calibrations to data analysis. Onboard the ship, the ac-s was calibrated daily using Milli Q-water. Corrections for the in situ temperature and salinity effects on optical properties of water were applied. Corrections for incomplete recovery of the scattered light in the ac-s absorption tube were performed. The fine scale of spectral and vertical distributions of c (lambda) and a (lambda) were described from the ac-s. The significant relationships between a (674) and that of spectrophotometric analysis and chlorophyll a concentration of discrete water samples were observed.

  16. AC conductivity and its scaling behavior in MgO-Li2O-B2O3-Bi2O3 glasses

    NASA Astrophysics Data System (ADS)

    Purnima, M.; Bale, Shashidhar; Samee, M. A.; Ahmmad, Shaik Kareem; Rahman, Syed

    2013-02-01

    In the present work, the compositional dependence of density, refractive index and glass transition temperature of xMgO-(25-x)Li2O-50B2O3-25Bi2O3 glasses is studied. Impedance spectroscopy technique is employed on these samples and the data are analyzed using Cole-Cole type impedance response function. The AC conductivity behavior of the present glasses has been investigated in the frequency range from 100 Hz to 1 MHz and as a function of temperature the measured AC data are analyzed using the Jonscher’s universal power law to explain the observed dispersive behavior of the electrical conductivity. The temperature and composition dependence scaling behavior in the AC conductivity are satisfactorily explained by scaling the AC conductivity σ‧(ω) by hopping frequency ωp. The frequency response of dielectric constant ɛ‧ and dielectric loss tanδ as a function of temperature were studied. The tanδ peak shifts to higher frequency with increasing temperature, indicating dipolar relaxation character of dielectric loss in the present glasses.

  17. Conductance measurement circuit with wide dynamic range

    NASA Technical Reports Server (NTRS)

    Mount, Bruce E. (Inventor); Von Esch, Myron (Inventor)

    1994-01-01

    A conductance measurement circuit to measure conductance of a solution under test with an output voltage proportional to conductance over a 5-decade range, i.e., 0.01 uS to 1000 uS or from 0.1 uS to 10,000 uS. An increase in conductance indicates growth, or multiplication, of the bacteria in the test solution. Two circuits are used each for an alternate half-cycle time periods of an alternate squarewave in order to cause alternate and opposite currents to be applied to the test solution. The output of one of the two circuits may be scaled for a different range optimum switching frequency dependent upon the solution conductance and to enable uninterrupted measurement over the complete 5-decade range. This circuitry provides two overlapping ranges of conductance which can be read simultaneously without discontinuity thereby eliminating range switching within the basic circuitry. A VCO is used to automatically change the operating frequency according to the particular value of the conductance being measured, and comparators indicate which range is valid and also facilitate computer-controlled data acquisition. A multiplexer may be used to monitor any number of solutions under test continuously.

  18. Thermal conductivity measurements of Summit polycrystalline silicon.

    SciTech Connect

    Clemens, Rebecca; Kuppers, Jaron D.; Phinney, Leslie Mary

    2006-11-01

    A capability for measuring the thermal conductivity of microelectromechanical systems (MEMS) materials using a steady state resistance technique was developed and used to measure the thermal conductivities of SUMMiT{trademark} V layers. Thermal conductivities were measured over two temperature ranges: 100K to 350K and 293K to 575K in order to generate two data sets. The steady state resistance technique uses surface micromachined bridge structures fabricated using the standard SUMMiT fabrication process. Electrical resistance and resistivity data are reported for poly1-poly2 laminate, poly2, poly3, and poly4 polysilicon structural layers in the SUMMiT process from 83K to 575K. Thermal conductivity measurements for these polysilicon layers demonstrate for the first time that the thermal conductivity is a function of the particular SUMMiT layer. Also, the poly2 layer has a different variation in thermal conductivity as the temperature is decreased than the poly1-poly2 laminate, poly3, and poly4 layers. As the temperature increases above room temperature, the difference in thermal conductivity between the layers decreases.

  19. Local measurement of thermal conductivity and diffusivity

    SciTech Connect

    Hurley, David H.; Schley, Robert S.; Khafizov, Marat; Wendt, Brycen L.

    2015-12-15

    Simultaneous measurement of local thermal diffusivity and conductivity is demonstrated on a range of ceramic samples. This was accomplished by measuring the temperature field spatial profile of samples excited by an amplitude modulated continuous wave laser beam. A thin gold film is applied to the samples to ensure strong optical absorption and to establish a second boundary condition that introduces an expression containing the substrate thermal conductivity. The diffusivity and conductivity are obtained by comparing the measured phase profile of the temperature field to a continuum based model. A sensitivity analysis is used to identify the optimal film thickness for extracting the both substrate conductivity and diffusivity. Proof of principle studies were conducted on a range of samples having thermal properties that are representatives of current and advanced accident tolerant nuclear fuels. It is shown that by including the Kapitza resistance as an additional fitting parameter, the measured conductivity and diffusivity of all the samples considered agreed closely with the literature values. A distinguishing feature of this technique is that it does not require a priori knowledge of the optical spot size which greatly increases measurement reliability and reproducibility.

  20. Local measurement of thermal conductivity and diffusivity

    SciTech Connect

    Hurley, David H.; Schley, Robert S.; Khafizov, Marat; Wendt, Brycen L.

    2015-12-01

    Simultaneous measurement of local thermal diffusivity and conductivity is demonstrated on a range of ceramic samples. This was accomplished by measuring the temperature field spatial profile of samples excited by an amplitude modulated continuous wave laser beam. A thin gold film is applied to the samples to ensure strong optical absorption and to establish a second boundary condition that introduces an expression containing the substrate thermal conductivity. The diffusivity and conductivity are obtained by comparing the measured phase profile of the temperature field to a continuum based model. A sensitivity analysis is used to identify the optimal film thickness for extracting the both substrate conductivity and diffusivity. Proof of principle studies were conducted on a range of samples having thermal properties that are representative of current and advanced accident tolerant nuclear fuels. It is shown that by including the Kapitza resistance as an additional fitting parameter, the measured conductivity and diffusivity of all the samples considered agree closely with literature values. Lastly, a distinguishing feature of this technique is that it does not require a priori knowledge of the optical spot size which greatly increases measurement reliability and reproducibility.

  1. Local measurement of thermal conductivity and diffusivity

    DOE PAGES

    Hurley, David H.; Schley, Robert S.; Khafizov, Marat; ...

    2015-12-01

    Simultaneous measurement of local thermal diffusivity and conductivity is demonstrated on a range of ceramic samples. This was accomplished by measuring the temperature field spatial profile of samples excited by an amplitude modulated continuous wave laser beam. A thin gold film is applied to the samples to ensure strong optical absorption and to establish a second boundary condition that introduces an expression containing the substrate thermal conductivity. The diffusivity and conductivity are obtained by comparing the measured phase profile of the temperature field to a continuum based model. A sensitivity analysis is used to identify the optimal film thickness formore » extracting the both substrate conductivity and diffusivity. Proof of principle studies were conducted on a range of samples having thermal properties that are representative of current and advanced accident tolerant nuclear fuels. It is shown that by including the Kapitza resistance as an additional fitting parameter, the measured conductivity and diffusivity of all the samples considered agree closely with literature values. Lastly, a distinguishing feature of this technique is that it does not require a priori knowledge of the optical spot size which greatly increases measurement reliability and reproducibility.« less

  2. Ac-loss measurement of a DyBCO-Roebel assembled coated conductor cable (RACC)

    NASA Astrophysics Data System (ADS)

    Schuller, S.; Goldacker, W.; Kling, A.; Krempasky, L.; Schmidt, C.

    2007-10-01

    Low ac-loss HTS cables for transport currents well above 1 kA are required for application in transformers and generators and are taken into consideration for future generations of fusion reactor coils. Coated conductors (CC) are suitable candidates for high field application at an operation temperature around 50-77 K, which is a crucial precondition for economical cooling costs. We prepared a short length of a Roebel bar cable made of industrial DyBCO coated conductor (Theva Company, Germany). Meander shaped tapes of 4 mm width with a twist pitch of 122 mm were cut from 10 mm wide CC tapes using a specially designed tool. Eleven of these strands were assembled to a cable. The electrical and mechanical connection of the tapes was achieved using a silver powder filled conductive epoxy resin. Ac-losses of a short sample in an external ac field were measured as a function of frequency and field amplitude in transverse and parallel field orientations. In addition, the coupling current time constant of the sample was directly measured.

  3. Molecular conductance measurements through printed Au nanodots

    NASA Astrophysics Data System (ADS)

    Jiang, W.; Garfunkel, E.; Zhitenev, N.; Abusch-Magder, D.; Tennant, D.; Bao, Z.

    2006-09-01

    Gold pads with ˜100nm diameter are imprinted on self-assembled monolayers of alkane dithiols of different lengths using nanotransfer printing. The pads are contacted by conductive atomic force microscope tips, and electron transport was measured as a function of force. Atomic scale topography at the metal-molecule interface is essential to describe the conductance-stress relationship. A finite force (1-10nN) deforms devices resulting in two competing effects: (a) a larger contact area and (b) deformation of the interfacial bonds and/or tilting of the molecules. The estimated conductance of molecules is significantly smaller than results suggested in previous experiments and calculations.

  4. Ferromagnetic resonance and ac conductivity of a polymer composite of Fe3O4 and Fe3C nanoparticles dispersed in a graphite matrix

    NASA Astrophysics Data System (ADS)

    Guskos, N.; Anagnostakis, E. A.; Likodimos, V.; Bodziony, T.; Typek, J.; Maryniak, M.; Narkiewicz, U.; Kucharewicz, I.; Waplak, S.

    2005-01-01

    Ferromagnetic resonance (FMR) and ac conductivity have been applied to study a polymer composite containing as filler a binary mixture of magnetite (Fe3O4) and cementite (Fe3C) nanoparticles (30-50nm) dispersed in a diamagnetic carbon matrix, which was synthesized by the carburization of nanocrystalline iron. Ac conductivity measurements showed thermally activated behavior involving a range of activation energies and power law frequency dependence at high frequencies similar to conducting polymer composites randomly filled with metal particles. Ferromagnetic resonance measurements revealed a relatively narrow FMR line at high temperatures indicating the presence of ferromagnetic nanoparticles, where thermal fluctuations and interparticle interactions determine the FMR temperature variation. An abrupt change of the FMR spectra was observed at T <81K (ΔT⩽1K) coinciding with a sharp anomaly resolved in the temperature derivative of the ac conductivity. This behavior is attributed to the Verwey transition of Fe3O4 nanoparticles, where the concurrent skin depth variation unveils the FMR of large magnetite conglomerates and thus allows discriminating their contribution from relatively isolated nanoparticles.

  5. Thermal Conductivity Measurements of Caged Structural Superconductors

    NASA Astrophysics Data System (ADS)

    Matsuzaki, H.; Hida, K.; Kase, N.; Nakano, T.; Takeda, N.

    Thermal conductivity of Ca3Rh4Sn13 and Sr3Ir4Sn13 were measured in magnetic fields to reveal superconducting state. From magnetic susceptibility χ(T) and electrical resistivity ρ(T) measurements, superconducting transition temperature Tc of Ca3Rh4Sn13 and Sr3Ir4Sn13 is determined to be 8 and 5 K, respectively. Thermal conductivity κ(T) of Ca3Rh4Sn13 indicates that superconducting state is nodeless s-wave, because residual thermal conductivity κ0/T in zero magnetic field is very small. On the other hand, κ(T) of Sr3Ir4Sn13 in zero magnetic field suggests that superconductivity possesses nodal gap rather than full gap. Whether nodal superconducting gap exists or not still remains to be clarified, because there is a possibility that the achieving temperature is insufficient to discuss superconducting state.

  6. Thermal conductivity measurement of fluids using the 3ω method

    NASA Astrophysics Data System (ADS)

    Lee, Seung-Min

    2009-02-01

    We have developed a procedure to measure the thermal conductivity of dielectric liquids and gases using a steady state ac hot wire method in which a thin metal wire is used as a heater and thermometer. The temperature response of the heater wire was measured in a four-probe geometry using an electronic circuit developed for the conventional 3ω method. The measurements have been performed in the frequency range from 1 mHz to 1 kHz. We devised a method to transform the raw data into well-known linear logarithmic frequency dependence plot. After the transformation, an optimal frequency region of the thermal conductivity data was clearly determined as has been done with the data from thin metal film heater. The method was tested with air, water, ethanol, mono-, and tetraethylene glycol. Volumetric heat capacity of the fluids was also calculated with uncertainty and the capability as a probe for metal-liquid thermal boundary conductance was discussed.

  7. Contact-independent electrical conductance measurement

    DOEpatents

    Mentzel, Tamar S.; MacLean, Kenneth; Kastner, Marc A.; Ray, Nirat

    2017-01-24

    Electrical conductance measurement system including a one-dimensional semiconducting channel, with electrical conductance sensitive to electrostatic fluctuations, in a circuit for measuring channel electrical current. An electrically-conductive element is disposed at a location at which the element is capacitively coupled to the channel; a midpoint of the element aligned with about a midpoint of the channel, and connected to first and second electrically-conductive contact pads that are together in a circuit connected to apply a changing voltage across the element. The electrically-conductive contact pads are laterally spaced from the midpoint of the element by a distance of at least about three times a screening length of the element, given in SI units as (K.di-elect cons..sub.0/e.sup.2D(E.sub.F)).sup.1/2, where K is the static dielectric constant, .di-elect cons..sub.0 is the permittivity of free space, e is electron charge, and D(E.sub.F) is the density of states at the Fermi energy for the element.

  8. Thermal Conductivity Measurement of Synthesized Mantle Minerals

    NASA Astrophysics Data System (ADS)

    Asimow, P. D.; Luo, S.; Mosenfelder, J. L.; Liu, W.; Staneff, G. D.; Ahrens, T. J.; Chen, G.

    2002-12-01

    Direct thermal conductivity (k) measurement of mantle minerals is crucial to constrain the thermal profile of the Earth as well as geodynamic studies of the mantle (e.g., to determine the Rayleigh number). We have embarked on systematic multi-anvil syntheses of dense polycrystalline specimens of mantle phases of adequate size and zero porosity for precise thermal conductivity measurements by the 3ω method (\\textit{Cahill and Pohl, Phys. Rev. B, 1987}) under elevated temperatures (T). Coesite and stishovite (see \\textit{Luo et al., GRL, 2002}) as well as majorite and wadsleyite have been synthesized; ringwoodite and perovskite are scheduled. Preliminary thermal conductivity measurements at ambient pressure on coesite (120 - 300 K, 9.53 Wm-1K-1 at 300 K) are consistent with prior room temperature data (\\textit{Yukutake & Shimada, PEPI, 1978}), while our stishovite data at 300 K appear to be low (1.96 Wm-1K-1). Efforts are being made to extend the measurement to higher temperatures (e.g., above Debye temperature Θ D), thus allowing determination of k(T) relationship (say, k~ T-n); success will depend on the decomposition kinetics of these metastable phases. The pressure dependence of k of these synthesized samples can also be measured (\\textit{e.g., Osako et al., HPMPS-6, 2002; Xu et al., EOS, 2001}). Recent thermal conductivity measurement on LiF and Al2O_3 from shock wave loading (\\textit{Holland & Ahrens, 1998}) is consistent with the modeling on MgO and Al2O_3 (\\textit{Manga & Jeanloz, JGR, 1997}) with classical theories. Thus, k values at modest pressures and T (say, above Θ D) would allow extrapolation of k to appropriate mantle conditions.

  9. Measurement and modeling of unsaturated hydraulic conductivity

    USGS Publications Warehouse

    Perkins, Kim S.; Elango, Lakshmanan

    2011-01-01

    The unsaturated zone plays an extremely important hydrologic role that influences water quality and quantity, ecosystem function and health, the connection between atmospheric and terrestrial processes, nutrient cycling, soil development, and natural hazards such as flooding and landslides. Unsaturated hydraulic conductivity is one of the main properties considered to govern flow; however it is very difficult to measure accurately. Knowledge of the highly nonlinear relationship between unsaturated hydraulic conductivity (K) and volumetric water content is required for widely-used models of water flow and solute transport processes in the unsaturated zone. Measurement of unsaturated hydraulic conductivity of sediments is costly and time consuming, therefore use of models that estimate this property from more easily measured bulk-physical properties is common. In hydrologic studies, calculations based on property-transfer models informed by hydraulic property databases are often used in lieu of measured data from the site of interest. Reliance on database-informed predicted values with the use of neural networks has become increasingly common. Hydraulic properties predicted using databases may be adequate in some applications, but not others. This chapter will discuss, by way of examples, various techniques used to measure and model hydraulic conductivity as a function of water content, K. The parameters that describe the K curve obtained by different methods are used directly in Richards’ equation-based numerical models, which have some degree of sensitivity to those parameters. This chapter will explore the complications of using laboratory measured or estimated properties for field scale investigations to shed light on how adequately the processes are represented. Additionally, some more recent concepts for representing unsaturated-zone flow processes will be discussed.

  10. Anomalous dielectric and AC conductivity behavior of the nanocrystalline Ni-Cu ferrite synthesized via combustion method

    SciTech Connect

    Madhu, B. J.; Rashmi, B. N.; Banu, Arshiya; Seema, G. A.; Shruthi, B.; Jayanna, H. S.

    2013-02-05

    Nanocrystalline Ni-Cu ferrites (Ni{sub 0.5}Cu{sub 0.5}Fe{sub 2}O{sub 4}) were prepared using solution combustion method. The structure of the samples were studied with the X-ray diffraction (XRD) using Cu-K{sub {alpha}} radiation. Frequency and temperature dependence of dielectric and a.c. conductivity studies have been undertaken on the Ni-Cu nanoferrites in the frequency region 100Hz-5MHz. The dielectric constant ({epsilon} Prime ) is found to decrease initially with the frequency and finally reaching a constant value at higher frequencies. Observed trends in the dielectric constant are ascribed to the Maxwell-Wagner type interfacial polarization, which is in agreement with the Koop'fs phenomenological theory. The a.c. conductivity ({sigma}{sub ac}) is found to increase with an increase in the frequency from room temperature up to 300 Degree-Sign C. However, at a temperature of 400 Degree-Sign C, the a.c. conductivity is found to decrease with an increase in the frequency exhibiting an abnormal behavior. The electrical conduction mechanism in the present nano nickel-copper ferrite is found to be in accordance with the electron hopping model.

  11. Anomalous dielectric and AC conductivity behavior of the nanocrystalline Ni-Cu ferrite synthesized via combustion method

    NASA Astrophysics Data System (ADS)

    Madhu, B. J.; Rashmi, B. N.; Banu, Arshiya; Seema, G. A.; Shruthi, B.; Jayanna, H. S.

    2013-02-01

    Nanocrystalline Ni-Cu ferrites (Ni0.5Cu0.5Fe2O4) were prepared using solution combustion method. The structure of the samples were studied with the X-ray diffraction (XRD) using Cu-Kα radiation. Frequency and temperature dependence of dielectric and a.c. conductivity studies have been undertaken on the Ni-Cu nanoferrites in the frequency region 100Hz-5MHz. The dielectric constant (ɛ') is found to decrease initially with the frequency and finally reaching a constant value at higher frequencies. Observed trends in the dielectric constant are ascribed to the Maxwell-Wagner type interfacial polarization, which is in agreement with the Koop'fs phenomenological theory. The a.c. conductivityac) is found to increase with an increase in the frequency from room temperature up to 300 °C. However, at a temperature of 400 °C, the a.c. conductivity is found to decrease with an increase in the frequency exhibiting an abnormal behavior. The electrical conduction mechanism in the present nano nickel-copper ferrite is found to be in accordance with the electron hopping model.

  12. A.c. conductivity and dielectric properties of LiNi 3/5Cu 2/5VO 4 ceramics

    NASA Astrophysics Data System (ADS)

    Ram, Moti

    2010-03-01

    The LiNi 3/5Cu 2/5VO 4 was synthesized using solution-based chemical method whose dielectric and a.c. conductivity properties were investigated using complex impedance spectroscopy (CIS) technique. Variation of dielectric constant ( εr) as a function of frequency at different temperatures indicates low frequency dispersion. A.c conductivity analysis indicates that electrical conduction in the material is a thermally activated process. Frequency dependence of a.c. conductivity at different temperatures obeys Jonscher's universal law: σ ac= σ dc+ A( ω) n.

  13. Validation of conducting wall models using magnetic measurements

    NASA Astrophysics Data System (ADS)

    Hanson, J. M.; Bialek, J.; Turco, F.; Navratil, G. A.; King, J.; Strait, E. J.; Turnbull, A. D.

    2016-10-01

    Comparisons between magnetic measurements of the DIII D wall eddy current response to applied ac, non-axisymmetric fields and MHD stability code predictions favor a fully 3D treatment of the conducting elements in the system. We describe validation studies of the wall models in the MARS-F and VALEN stability codes, using coil-sensor vacuum coupling measurements. The measurements are sensitive to induced wall currents, owing to the close proximities of the sensors and coils to the wall. VALEN treats conducting structures with arbitrary 3D geometries, while MARS-F uses an axisymmetric wall model and spectral decomposition of the problem geometry. Straightforward improvements to the VALEN model, such as refining the wall mesh and sensor geometry, lead to good agreement with single-channel measurements. Comparisons of couplings to multi-coil toroidal mode perturbations to both codes favor the 3D simulation approach, likely because it naturally treats sidebands generated by the coils and wall currents. Work supported by the US Department of Energy under DE-FG02- 04ER54761, DE-FC02-04ER54698, and DE-FG02-95ER54309.

  14. Dielectric and ac conductivity studies of ZnO/Eu3+: Titanosilicate matrix

    NASA Astrophysics Data System (ADS)

    Arun Kumar, K. V.; Sunil, Thomas; Ann Mary, K. A.; Cyriac, Joseph; Biju, P. R.; Unnikrishnan, N. V.

    2014-01-01

    ZnO nanoparticles /Eu3+ doped SiO2-TiO2 matrices were synthesized through sol-gel route. Structural and dielectric properties of ZnO nanocrystallites co-doped with Eu3+ in SiO2-TiO2 matrices were presented. The HRTEM and XRD measurements confirm the presence of ZnO nanocrystallites. The dielectric and electrical conductivity studies of the samples are completed for a frequency of 100 Hz to 2 MHz. The conductivity variation with the ZnO content in the Eu3+ doped SiO2-TiO2 system were explained by correlating the presence of ionic contribution to the electrical conductivity process. From the frequency dependence of dielectric constant and conductivity, the Cole-Cole parameters and power law parameters were evaluated. The dielectric relaxation phenomena were investigated using the dielectric moduli formulation.

  15. AC Hopping Conductance in Nanocomposite Films with Ferromagnetic Alloy Nanoparticles in a PbZrTiO3 Matrix

    NASA Astrophysics Data System (ADS)

    Koltunowicz, T. N.; Zukowski, P.; Boiko, O.; Saad, A.; Fedotova, J. A.; Fedotov, A. K.; Larkin, A. V.; Kasiuk, J.

    2015-07-01

    In this work, the temperature and frequency dependences of the real part of the admittance [ σ( f, T)] of annealed nanocomposite films containing Co45 Fe45Zr10-based nanoparticles covered with native oxides and embedded in a doped PbZrTiO3 ferroelectric matrix were studied. The nanocomposites studied were deposited by ion sputtering a complex target in a mixed Ar/O2 atmosphere followed by a 15-min annealing process (with steps of 25 K) in air in the temperature range of 398 K ≤ T a ≤ 573 K. The σ( f, T) of the annealed samples was measured in the temperature range of 77 K < T p < 373 K at frequencies of 50 Hz < f < 1 MHz. The observed σ( f, T) dependences confirmed that the annealed samples displayed the effects of negative capacitance over the whole frequency and temperature ranges studied because of the pronounced oxidation of the nanoparticles. The σ( f, T) dependences obtained are described using an earlier-developed AC hopping conductance model. Comparisons between experimental and simulation results allow the model parameters to be estimated, such as the activation energies of the hopping conductance and the lifetimes of the electrons in the nanoparticles.

  16. Measuring Contact Thermal Conductances at Low Temperatures

    NASA Technical Reports Server (NTRS)

    Salerno, Louis J.; Kittel, Peter; Brooks, Walter; Spivak, Alan L.; Marks, William G., Jr.

    1987-01-01

    Instrument measures thermal conductance of pressed contacts in liquid helium. Makes measurements automatically as function of force on pairs of brass samples having various surface finishes. Developed as part of effort to determine heat-transfer characteristics of bolted joints on cryogenically cooled focal planes in infrared equipment. Cylindrical chamber hangs from cover plate in bath of liquid helium. Inside chamber rocker arm applies controlled force to samples. Upper sample made slightly wider than lower one so two samples remain in complete contact even under slight lateral misalignment.

  17. Design of Low Temperature AC Susceptibility Measurement Scheme for Molecular Magnets

    NASA Astrophysics Data System (ADS)

    Korenblit, Simcha; Moon, Byoung; Lee, Yoonseok; Sultan, Reza

    2006-03-01

    AC susceptibility is one of the most important physical properties in many materials such as magnetic materials and superconductors. Although there are many commercial AC susceptibility measurement systems which cover a broad range of temperatures, it is still a daunting task to extend their measurement range into the low millikelvins. We are currently developing a low temperature AC susceptometer for the mK range. As a part of this effort, we have developed a versatile low-cost computer controlled coil-winder to make various types of coils. We have designed primary and secondary coils and wound them using the machine, and performed characterization of the AC susceptometer. In this presentation, I will explain the basics of magnetic susceptibility, its measurement, design considerations for building an AC magnetic susceptometer, and discuss the details of an actual apparatus designed and realized by the authors.

  18. Measurement of heat conduction through stacked screens.

    PubMed

    Lewis, M A; Kuriyama, T; Kuriyama, F; Radebaugh, R

    1998-01-01

    This paper describes the experimental apparatus for the measurement of heat conduction through stacked screens as well as some experimental results taken with the apparatus. Screens are stacked in a fiberglass-epoxy cylinder, which is 24.4 mm in diameter and 55 mm in length. The cold end of the stacked screens is cooled by a Gifford-McMahon (GM) cryocooler at cryogenic temperature, and the hot end is maintained at room temperature. Heat conduction through the screens is determined from the temperature gradient in a calibrated heat flow sensor mounted between the cold end of the stacked screens and the GM cryocooler. The samples used for these experiments consisted of 400-mesh stainless steel screens, 400-mesh phosphor bronze screens, and two different porosities of 325-mesh stainless steel screens. The wire diameter of the 400-mesh stainless steel and phosphor bronze screens was 25.4 micrometers and the 325-mesh stainless steel screen wire diameters were 22.9 micrometers and 27.9 micrometers. Standard porosity values were used for the experimental data with additional porosity values used on selected experiments. The experimental results showed that the helium gas between each screen enhanced the heat conduction through the stacked screens by several orders of magnitude compared to that in vacuum. The conduction degradation factor is the ratio of actual heat conduction to the heat conduction where the regenerator material is assumed to be a solid rod of the same cross sectional area as the metal fraction of the screen. This factor was about 0.1 for the stainless steel and 0.022 for the phosphor bronze, and almost constant for the temperature range of 40 to 80 K at the cold end.

  19. Measurement of heat conduction through stacked screens

    NASA Technical Reports Server (NTRS)

    Lewis, M. A.; Kuriyama, T.; Kuriyama, F.; Radebaugh, R.

    1998-01-01

    This paper describes the experimental apparatus for the measurement of heat conduction through stacked screens as well as some experimental results taken with the apparatus. Screens are stacked in a fiberglass-epoxy cylinder, which is 24.4 mm in diameter and 55 mm in length. The cold end of the stacked screens is cooled by a Gifford-McMahon (GM) cryocooler at cryogenic temperature, and the hot end is maintained at room temperature. Heat conduction through the screens is determined from the temperature gradient in a calibrated heat flow sensor mounted between the cold end of the stacked screens and the GM cryocooler. The samples used for these experiments consisted of 400-mesh stainless steel screens, 400-mesh phosphor bronze screens, and two different porosities of 325-mesh stainless steel screens. The wire diameter of the 400-mesh stainless steel and phosphor bronze screens was 25.4 micrometers and the 325-mesh stainless steel screen wire diameters were 22.9 micrometers and 27.9 micrometers. Standard porosity values were used for the experimental data with additional porosity values used on selected experiments. The experimental results showed that the helium gas between each screen enhanced the heat conduction through the stacked screens by several orders of magnitude compared to that in vacuum. The conduction degradation factor is the ratio of actual heat conduction to the heat conduction where the regenerator material is assumed to be a solid rod of the same cross sectional area as the metal fraction of the screen. This factor was about 0.1 for the stainless steel and 0.022 for the phosphor bronze, and almost constant for the temperature range of 40 to 80 K at the cold end.

  20. Thermal Conductivity Measurements on consolidated Soil Analogs

    NASA Astrophysics Data System (ADS)

    Seiferlin, K.; Heimberg, M.; Thomas, N.

    2007-08-01

    Heat transport in porous media such as soils and regolith is significantly reduced compared to the properties of compact samples of the same material. The bottle neck for solid state heat transport is the contact area between adjacent grains. For "dry" and unconsolidated materials the contact areas and thus the thermal conductivity are extremely small. Sintering and cementation are two processes that can increase the cross section of interstitial bonds signifcantly. On Mars, cementation can be caused by condensation of water or carbon dioxide ice from the vapor phase, or from salts and minerals that fall out from aqueous solutions. We produced several artificially cemented samples, using small glass beads of uniform size as soil analog. The cementation is achieved by initially molten wax that is mixed with the glass beads while liqiud. The wax freezes preferably at the contact points between grains, thus minimizing surface energy, and consolidates the samples. The thermal conductivity of these samples is then measured in vacuum. We present the results of these measurements and compare them with theoretical models. The observed range of thermal conductivity values can explain some, but not all of the variations in thermal intertia that can be seen in TES remote sensing data.

  1. System for absolute measurement of electrolytic conductivity in aqueous solutions based on van der Pauw's theory

    NASA Astrophysics Data System (ADS)

    Zhang, Bing; Lin, Zhen; Zhang, Xiao; Yu, Xiang; Wei, Jiali; Wang, Xiaoping

    2014-05-01

    Based on an innovative application of van der Pauw's theory, a system was developed for the absolute measurement of electrolytic conductivity in aqueous solutions. An electrolytic conductivity meter was designed that uses a four-electrode system with an axial-radial two-dimensional adjustment structure coupled to an ac voltage excitation source and signal collecting circuit. The measurement accuracy, resolution and repeatability of the measurement system were examined through a series of experiments. Moreover, the measurement system and a high-precision electrolytic conductivity meter were compared using some actual water samples.

  2. Quantitative Thermal Microscopy Measurement with Thermal Probe Driven by dc+ac Current

    NASA Astrophysics Data System (ADS)

    Bodzenta, Jerzy; Juszczyk, Justyna; Kaźmierczak-Bałata, Anna; Firek, Piotr; Fleming, Austin; Chirtoc, Mihai

    2016-07-01

    Quantitative thermal measurements with spatial resolution allowing the examination of objects of submicron dimensions are still a challenging task. The quantity of methods providing spatial resolution better than 100 nm is very limited. One of them is scanning thermal microscopy (SThM). This method is a variant of atomic force microscopy which uses a probe equipped with a temperature sensor near the apex. Depending on the sensor current, either the temperature or the thermal conductivity distribution at the sample surface can be measured. However, like all microscopy methods, the SThM gives only qualitative information. Quantitative measuring methods using SThM equipment are still under development. In this paper, a method based on simultaneous registration of the static and the dynamic electrical resistances of the probe driven by the sum of dc and ac currents, and examples of its applications are described. Special attention is paid to the investigation of thin films deposited on thick substrates. The influence of substrate thermal properties on the measured signal and its dependence on thin film thermal conductivity and film thickness are analyzed. It is shown that in the case where layer thicknesses are comparable or smaller than the probe-sample contact diameter, a correction procedure is required to obtain actual thermal conductivity of the layer. Experimental results obtained for thin SiO2 and BaTiO_{3 }layers with thicknesses in the range from 11 nm to 100 nm are correctly confirmed with this approach.

  3. Direct measurements of the atmospheric conduction current

    NASA Technical Reports Server (NTRS)

    Burke, H. K.; Few, A. A.

    1978-01-01

    A method of measuring the atmospheric conduction current above the ground has been employed to obtain data for 12 weeks during the first half of 1974. The instrument consists of a split aluminum sphere suspended by insulated wires to a wooden frame. The measuring electronics and the transmitter are enclosed within the spherical structure. The interaction of the instrument with its atmospheric electrical environment is analyzed, and it is shown that in steady state conditions, predictable differences in the instrumentally measured currents and the atmospheric conduction current will be less than 5% and in the nonsteady state situations the difference is less than 20%. Diurnal variations, a probable winter-summer variation, sunrise, and fog effects were observed for the data obtained during fair-weather conditions. Disturbed weather data are interpreted for the effects of low clouds on the atmospheric current. The charge concentrations within overcast clouds sufficient to produce the observed reversed atmospheric currents are estimated to be small in relation to values in thunderclouds.

  4. Centrifugal techniques for measuring saturated hydraulic conductivity

    USGS Publications Warehouse

    Nimmo, John R.; Mello, Karen A.

    1991-01-01

    Centrifugal force is an alternative to large pressure gradients for the measurement of low values of saturated hydraulic conductivity (Ksat). With a head of water above a porous medium in a centrifuge bucket, both constant-head and falling-head measurements are practical at forces up to at least 1800 times normal gravity. Darcy's law applied to the known centrifugal potential leads to simple formulas for Ksat that are analogous to those used in the standard gravity-driven constant- and falling-head methods. Both centrifugal methods were tested on several fine-textured samples of soil and ceramic with Ksat between about 10−10 and 10−9 m/s. The results were compared to falling-head gravity measurements. The comparison shows most measurements agreeing to within 20% for a given sample, much of the variation probably resulting from run-to-run changes in sample structure. The falling-head centrifuge method proved to be especially simple in design and operation and was more accurate than the constant-head method. With modified apparatus, Ksat measurements less than 10−10 m/s should be attainable.

  5. Thermal conductivity measurements of warm dense iron at the LCLS

    NASA Astrophysics Data System (ADS)

    McKelvey, A.; Jiang, S.; Collins, G.; Shepherd, R.; Hau-Riege, S. P.; Hill, M. P.; Brown, C. R. D.; Floyd, E.; Fyrth, J. D.; Skidmore, J. W.; Hua, R.; Beg, F. N.; Kim, M.; Cho, B.; Lee, J.; King, J.; Freeman, R. R.; Lee, H. J.; Galtier, E.; Audebert, P.; Levy, A.; Ping, Y.

    2016-10-01

    Accurate knowledge of conductivity characteristics in the strongly coupled plasma regime is extremely important for ICF processes such as the onset of hydrodynamic instabilities, thermonuclear burn propagation waves, shell mixing, and efficient x-ray conversion of indirect drive schemes. Recently, an experiment was performed at the LCLS at SLAC to measure the thermal conductivity of warm dense iron. The experiment used 6.8 keV x-rays to differentially heat thin bi-layer Au/Fe targets and establish a prompt temperature gradient at the layer interface. We used a SOP and a FDI to measure the rear layer's time-resolved temperature, expansion velocity, and reflectivity. Data from the time-resolved diagnostics for 100 nm Au and 50 to 100 nm Fe targets will be presented along with analysis and comparison with various models in the strongly coupled plasma regime. This work was performed under the auspices of the U.S. Department of Energy by Lawrence Livermore National Laboratory under contract DE-AC52-07NA27344.

  6. Ac Permeability Measurement for Inter- and Intragrain Critical Current Densities in Oxide Superconductors

    NASA Astrophysics Data System (ADS)

    Matsushita, Teruo; Ni, Baorong

    1989-03-01

    A simple measuring method to discriminate between inter- and intragrain current densities in oxide superconductors under given magnetic fields and temperatures is proposed. This is a measurement of the imaginary part of the ac permeability or susceptibility as a function of the ac field amplitude. In this method, the analysis used to derive the penetration depth of the ac field in Campbell’s method or the waveform analysis method is not necessary. This method is useful when the value of the penetration field into the grains and that into the bulk specimen are remarkably different.

  7. Reflectometer distance measurement between parallel conductive plates

    NASA Technical Reports Server (NTRS)

    Hearn, Chase P.; Neece, Robert T.

    1995-01-01

    This report presents an analytic and experimental investigation of the measurement problem in which a reflectometer is used to determine the distance to a target that is a highly conductive surface parallel to the reflectometer antenna ground plane. These parallel surfaces constitute a waveguide (WG) which can contribute parasitic perturbations that seriously degrade the accuracy of the measurements. Two distinct parallel-plate-waveguide (PPWG) phenomena are described, and their effects on both frequency and time-domain reflectometers are considered. The time-domain processing approach was found to be superior to a representative frequency-domain phase-measurement approach because of less susceptibility to perturbations produced by edge reflections and immunity to phase capture. Experimental results are presented which show that a simple radiating system modification can suppress parallel-plate (PP) propagation. The addition of a thin layer of lossy mu-metal 'magnetic absorber' to the antenna ground plane allowed a measurement accuracy of 0.025 cm (0.01 in.) when a vector network analyzer (VNA) is used as a time-domain reflectometer.

  8. AC conductivity of (FeCoZr)x(PZT)(100-x) nanocomposites produced in vacuum chamber

    NASA Astrophysics Data System (ADS)

    Boiko, Oleksandr; Bondariev, Vitalii; Czarnacka, Karolina

    2015-09-01

    In this work, the temperature and frequency dependences of conductivity σ and Arrhenius plots of annealed nanocomposite films containing Fe45Co45Zr10 - based nanoparticles embedded in a doped PbZrTiO3 ferroelectric matrix were studied. The nanocomposites studied were deposited by sputtering with use of argon and oxygen ions in a vacuum chamber. Tested samples were followed by a 15-min annealing process in air in the temperature range of 398 K <= Ta <= 748 K with steps of 25 K. The σ(f,T) dependences of nanocomposite samples was measured in ambient temperature range of 77 K < Tp < 373 K at frequencies of 50 Hz < f < 1MHz. It was established that nanocomposite sample with metallic phase content x = 55.6 at.% demonstrates strong temperature and frequency dependences, which is typical for a percolation systems. Type of conduction in such nanostructure is defined as dielectric, which may be related with the additional oxidation of metallic nanoparticles during the annealing process. For the tested sample with x = 88.4 at.%. we observe metallic type of conduction, when metallic nanoparticles form a permanent conductive channels in dielectric matrix.

  9. Correlation of AC Loss Data from Magnetic Susceptibility Measurements with YBCO Film Quality (Postprint)

    DTIC Science & Technology

    2012-02-01

    excimer laser operating at the KrF, 248 nm , wavelength. Substrates included LaAlO3 ( 100 ) and SrTiO3 ( 100 ) single crystal substrates as well as buffered...AFRL-RZ-WP-TP-2012-0100 CORRELATION OF AC LOSS DATA FROM MAGNETIC SUSCEPTIBILITY MEASUREMENTS WITH YBCO FILM QUALITY (POSTPRINT) Paul N...CORRELATION OF AC LOSS DATA FROM MAGNETIC SUSCEPTIBILITY MEASUREMENTS WITH YBCO FILM QUALITY (POSTPRINT) 5a. CONTRACT NUMBER In-house 5b. GRANT

  10. The change in dielectric constant, AC conductivity and optical band gaps of polymer electrolyte film: Gamma irradiation

    SciTech Connect

    Raghu, S. Subramanya, K. Sharanappa, C. Mini, V. Archana, K. Sanjeev, Ganesh Devendrappa, H.

    2014-04-24

    The effects of gamma (γ) irradiation on dielectric and optical properties of polymer electrolyte film were investigated. The dielectric constant and ac conductivity increases with γ dose. Also optical band gap decreased from 4.23 to 3.78ev after irradiation. A large dependence of the polymer properties on the irradiation dose was noticed. This suggests that there is a possibility of improving polymer electrolyte properties on gamma irradiation.

  11. AC loss measurements in HTS coil assemblies with hybrid coil structures

    NASA Astrophysics Data System (ADS)

    Jiang, Zhenan; Long, Nicholas J.; Staines, Mike; Badcock, Rodney A.; Bumby, Chris W.; Buckley, Robert G.; Amemiya, Naoyuki

    2016-09-01

    Both AC loss and wire cost in coil windings are critical factors for high temperature superconductor (HTS) AC machinery applications. We present AC loss measurement results in three HTS coil assemblies at 77 K and 65 K which have a hybrid coil structure comprising one central winding (CW) and two end windings (EWs) wound with ReBCO and BSCCO wires with different self-field I c values at 77 K. All AC loss results in the coil assemblies are hysteretic and the normalized AC losses in the coil assemblies at different temperatures can be scaled with the I c value of the coil assemblies. The normalised results show that AC loss in a coil assembly with BSCCO CW can be reduced by using EWs wound with high I c ReBCO wires, whilst further AC loss reduction can be achieved by replacing the BSCCO CW with ReBCO CW. The results imply that a flexible hybrid coil structure is possible which considers both AC loss and wire cost in coil assemblies.

  12. AC conductivity and electrochemical studies of PVA/PEG based polymer blend electrolyte films

    NASA Astrophysics Data System (ADS)

    Polu, Anji Reddy; Kumar, Ranveer; Dehariya, Harsha

    2012-06-01

    Polymer blend electrolyte films based on Polyvinyl alcohol(PVA)/Poly(ethylene glycol)(PEG) and magnesium nitrate (Mg(NO3)2) were prepared by solution casting technique. Conductivity in the temperature range 303-373 K and transference number measurements have been employed to investigate the charge transport in this polymer blend electrolyte system. The highest conductivity is found to be 9.63 × 10-5 S/cm at 30°C for sample with 30 weight percent of Mg(NO3)2 in PVA/PEG blend matrix. Transport number data shows that the charge transport in this polymer electrolyte system is predominantly due to ions. Using this electrolyte, an electrochemical cell with configuration Mg/(PVA+PEG+Mg(NO3)2)/(I2+C+electrolyte) was fabricated and its discharge characteristics profile has been studied.

  13. Measuring Thermal Conductivity at LH2 Temperatures

    NASA Technical Reports Server (NTRS)

    Selvidge, Shawn; Watwood, Michael C.

    2004-01-01

    For many years, the National Institute of Standards and Technology (NIST) produced reference materials for materials testing. One such reference material was intended for use with a guarded hot plate apparatus designed to meet the requirements of ASTM C177-97, "Standard Test Method for Steady-State Heat Flux Measurements and Thermal Transmission Properties by Means of the Guarded-Hot-Plate Apparatus." This apparatus can be used to test materials in various gaseous environments from atmospheric pressure to a vacuum. It allows the thermal transmission properties of insulating materials to be measured from just above ambient temperature down to temperatures below liquid hydrogen. However, NIST did not generate data below 77 K temperature for the reference material in question. This paper describes a test method used at NASA's Marshall Space Flight Center (MSFC) to optimize thermal conductivity measurements during the development of thermal protection systems. The test method extends the usability range of this reference material by generating data at temperatures lower than 77 K. Information provided by this test is discussed, as are the capabilities of the MSFC Hydrogen Test Facility, where advanced methods for materials testing are routinely developed and optimized in support of aerospace applications.

  14. THz conductivity measurement of MnSi

    NASA Astrophysics Data System (ADS)

    Mohtashemi, Laleh; Farahani, Amir; Karhu, Eric; Monchesky, Theodore L.; Dodge, J. Steven

    2012-10-01

    We present measurements of the low-frequency optical conductivity of a thin film of MnSi, using time-domain terahertz spectroscopy. At low temperatures and low frequencies, we extract the DC resistivity, scattering life time and plasma frequency from a Drude fit. We obtain a value of φp˜1.0 eV, which can be used to estimate the renormalization coefficient through comparison with band theory. At higher temperatures, a deviation from Drude behavior is observed, suggesting a loss of quasi-particle coherence. In the region of low temperatures and high frequencies, we see evidence for a crossover to the anomalous power law dependence observed by Mena et al.footnotetextF.P. Mena et al. Phys. Rev. B. 67, 241101(R) (2003). As the temperature increases, the anomalous frequency dependence becomes more pronounced, and the plasma frequency inferred from a Drude fit increases dramatically. Above T 50 K, σ2(φ) develops a negative slope that is inconsistent with both a Drude model and the anomalous power law observed earlier, indicating a sharp pseudogap in the conductivity spectrum.

  15. Measurement of the Optical Conductivity of Graphene

    SciTech Connect

    Mak, K.; Sfeir, M; Wu, Y; Lui, C; Misewich, J; Heinz, T

    2008-01-01

    Optical reflectivity and transmission measurements over photon energies between 0.2 and 1.2 eV were performed on single-crystal graphene samples on a SiO2 substrate. For photon energies above 0.5 eV, graphene yielded a spectrally flat optical absorbance of (2.3{+-}0.2)%. This result is in agreement with a constant absorbance of pa, or a sheet conductivity of pe2/2h, predicted within a model of noninteracting massless Dirac fermions. This simple result breaks down at lower photon energies, where both spectral and sample-to-sample variations were observed. This 'nonuniversal' behavior is explained by including the effects of doping and finite temperature, as well as contributions from intraband transitions.

  16. AC CONDUCTION PHENOMENON OF Li2O-WO3-B2O3 GLASSES DOPED WITH V2O5

    NASA Astrophysics Data System (ADS)

    Rao, Linganaboina Srinivasa; Veeraiah, Nalluri; Rao, Tumu Venkatappa

    2013-04-01

    The glass composition 40Li2O-5WO3-(55-x)B2O3: xV2O5 for x = 0.2, 0.4, 0.6 and 0.8 is chosen for the present study. The glass samples were synthesized by conventional melt-quenching technique. The dielectric properties such as constant (ɛ‧), loss (tan δ) and ac conductivityac) are carried out as a function of temperature (30-270°C) and frequency (102-105 Hz). The glass sample (at x = 0.6) exhibited highest ac conductivityac) and spreading factor (β) among all the samples. All glasses exhibited mixed conduction (both electronic and ionic) at high temperatures. The frequency exponent s denotes the ac conduction mechanism is associated with both QMT model (at low temperatures) and CBH model (at high temperatures).

  17. Sensitive bridge circuit measures conductance of low-conductivity electrolyte solutions

    NASA Technical Reports Server (NTRS)

    Schmidt, K.

    1967-01-01

    Compact bridge circuit measures sensitive and accurate conductance of low-conductivity electrolyte solutions. The bridge utilizes a phase sensitive detector to obtain a linear deflection of the null indicator relative to the measured conductance.

  18. A.C. Conductivity of Bi2Cu0.1V0.9O5.35 Films for Fuel Cell Application

    NASA Astrophysics Data System (ADS)

    Nimat, R. K.; Lokare, S. A.; Pawar, S. H.

    2011-07-01

    The A.C. conductivity and dielectric properties of Bi2Cu0.1V0.9O5.35 thin films were studied as a function of frequency and temperature. The A.C. conductivity of Bi2Cu0.1V0.9O5.35 film increases with frequency. The low frequency region corresponds to the D.C. conductivity where the inter-well hopping responsible for D.C. conduction completely dominates over the intra-well hopping associated with pure A.C. conduction. Higher values of A.C. conductivity for films formed on alumina substrates predict their suitability for fuel cell application

  19. Calculation of the ac to dc resistance ratio of conductive nonmagnetic straight conductors by applying FEM simulations

    NASA Astrophysics Data System (ADS)

    Riba, Jordi-Roger

    2015-09-01

    This paper analyzes the skin and proximity effects in different conductive nonmagnetic straight conductor configurations subjected to applied alternating currents and voltages. These effects have important consequences, including a rise of the ac resistance, which in turn increases power loss, thus limiting the rating for the conductor. Alternating current (ac) resistance is important in power conductors and bus bars for line frequency applications, as well as in smaller conductors for high frequency applications. Despite the importance of this topic, it is not usually analyzed in detail in undergraduate and even in graduate studies. To address this, this paper compares the results provided by available exact formulas for simple geometries with those obtained by means of two-dimensional finite element method (FEM) simulations and experimental results. The paper also shows that FEM results are very accurate and more general than those provided by the formulas, since FEM models can be applied in a wide range of electrical frequencies and configurations.

  20. Linear optics measurements and corrections using an AC dipole in RHIC

    SciTech Connect

    Wang, G.; Bai, M.; Yang, L.

    2010-05-23

    We report recent experimental results on linear optics measurements and corrections using ac dipole. In RHIC 2009 run, the concept of the SVD correction algorithm is tested at injection energy for both identifying the artificial gradient errors and correcting it using the trim quadrupoles. The measured phase beatings were reduced by 30% and 40% respectively for two dedicated experiments. In RHIC 2010 run, ac dipole is used to measure {beta}* and chromatic {beta} function. For the 0.65m {beta}* lattice, we observed a factor of 3 discrepancy between model and measured chromatic {beta} function in the yellow ring.

  1. The Wechsler ACS Social Perception Subtest: A Preliminary Comparison with Other Measures of Social Cognition

    ERIC Educational Resources Information Center

    Kandalaft, Michelle R.; Didehbani, Nyaz; Cullum, C. Munro; Krawczyk, Daniel C.; Allen, Tandra T.; Tamminga, Carol A.; Chapman, Sandra B.

    2012-01-01

    Relative to other cognitive areas, there are few clinical measures currently available to assess social perception. A new standardized measure, the Wechsler Advanced Clinical Solutions (ACS) Social Perception subtest, addresses some limitations of existing measures; however, little is known about this new test. The first goal of this investigation…

  2. AC magnetic field-assisted method to develop porous carbon nanotube/conducting polymer composites for application in thermoelectric materials

    NASA Astrophysics Data System (ADS)

    Chuang, Chun-Yu; Yang, Shu-Chian; Chang, Su-Hua; Yang, Ta-I.

    2015-04-01

    Thermoelectric materials are very effective in converting waste heat sources into useful electricity. Researchers are continuing to develop new polymeric thermoelectric materials. The segregated-network carbon nanotube (CNT)- polymer composites are most promising. Thus, the goal of this study is to develop novel porous CNT -polymer composites with improved thermoelectric properties. The research efforts focused on modifying the surface of the CNT with magnetic nanoparticles so that heat was released when subjecting to an AC magnetic field. Subsequently, polymers covered on the surface of the CNT were crosslinked. The porous CNT -polymer composites can be obtained by removing the un-crosslinked polymers. Polydimethylsiloxane polymer was utilized to investigate the effect of porosity and electrical conductivity on the thermoelectric properties of the composites. This AC magnetic field-assisted method to develop porous carbon nanotube/polymer composites for application in thermoelectric materials is introduced for the first time. The advantage of this method is that the electrical conductivity of the composites was high since we can easily to manipulate the CNT to form a conducting path. Another advantage is that the high porosity significantly reduced the thermal conductivity of the composites. These two advantages enable us to realize the polymer composites for thermoelectric applications. We are confident that this research will open a new avenue for developing polymer thermoelectric materials.

  3. Dielectric relaxation and ac conductivity behavior of carboxyl functionalized multiwalled carbon nanotubes/poly (vinyl alcohol) composites

    NASA Astrophysics Data System (ADS)

    Amrin, Sayed; Deshpande, V. D.

    2017-03-01

    We study the dielectric relaxation and ac conductivity behavior of MWCNT-COOH/Polyvinyl alcohol nanocomposite films in the temperature (T) range 303-423 K and in the frequency (f) range 0.1 Hz-1 MHz. The dielectric constant increases with an increase in temperature and also with an increase in MWCNT-COOH loading into the polymer matrix, as a result of interfacial polarization. The permittivity data were found to fit well with the modified Cole-Cole equation. Temperature dependent values of the relaxation times, free charge carrier conductivity and space charge carrier conductivity were extracted from the equation. An observed increment in the ac conductivity for the nanocomposites was analysed by a Jonscher power law which suggests that the correlated barrier hopping is the dominant charge transport mechanism for the nanocomposite films. The electric modulus study revealed deviations from ideal Debye-type behavior which are explained by considering a generalized susceptibility function. XRD and DSC results show an increase in the degree of crystallinity.

  4. Development of the Exams Data Analysis Spreadsheet as a Tool to Help Instructors Conduct Customizable Analyses of Student ACS Exam Data

    ERIC Educational Resources Information Center

    Brandriet, Alexandra; Holme, Thomas

    2015-01-01

    The American Chemical Society Examinations Institute (ACS-EI) has recently developed the Exams Data Analysis Spread (EDAS) as a tool to help instructors conduct customizable analyses of their student data from ACS exams. The EDAS calculations allow instructors to analyze their students' performances both at the total score and individual item…

  5. 21 CFR 882.1550 - Nerve conduction velocity measurement device.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Nerve conduction velocity measurement device. 882... conduction velocity measurement device. (a) Identification. A nerve conduction velocity measurement device is a device which measures nerve conduction time by applying a stimulus, usually to a...

  6. 21 CFR 882.1550 - Nerve conduction velocity measurement device.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Nerve conduction velocity measurement device. 882... conduction velocity measurement device. (a) Identification. A nerve conduction velocity measurement device is a device which measures nerve conduction time by applying a stimulus, usually to a...

  7. 21 CFR 882.1550 - Nerve conduction velocity measurement device.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Nerve conduction velocity measurement device. 882... conduction velocity measurement device. (a) Identification. A nerve conduction velocity measurement device is a device which measures nerve conduction time by applying a stimulus, usually to a...

  8. 21 CFR 882.1550 - Nerve conduction velocity measurement device.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Nerve conduction velocity measurement device. 882... conduction velocity measurement device. (a) Identification. A nerve conduction velocity measurement device is a device which measures nerve conduction time by applying a stimulus, usually to a...

  9. 21 CFR 882.1550 - Nerve conduction velocity measurement device.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Nerve conduction velocity measurement device. 882... conduction velocity measurement device. (a) Identification. A nerve conduction velocity measurement device is a device which measures nerve conduction time by applying a stimulus, usually to a...

  10. Human/Nonhuman Primate AC-PC Ratio - Considerations for Translational Brain Measurements

    PubMed Central

    Fiandaca, Massimo S.; Salegio, Ernesto Aguilar; Yin, Dali; Richardson, R. Mark; Valles, Francisco E.; Larson, Paul S.; Starr, Philip A.; Lonser, Russell R.; Bankiewicz, Krystof S.

    2011-01-01

    This comparative magnetic resonance imaging (MRI) analysis evaluated the ratio of AC-PC (anterior commissure to posterior commissure) distance measures in selected groups of humans and nonhuman primates (NHPs). An understanding of the basis of this ratio between primate species may allow more accurate translation of NHP stereotactic targeting measurements to upcoming human trials. MRI datasets of adult humans [n=21], and juvenile and adult NHPs (Macaca fascicularis [n=40], and Macaca mulatta [n=32]), were evaluated in a mid-sagittal plane to obtain the AC-PC distance measure for each examined subject. Two trained evaluators, blinded to each other’s results, carried out three separate measurements of the AC-PC length for each subject. Each observer carried out measurements of the entire dataset [n=93] before repeating the measurements two additional times. Previous dataset measures were not available for review at the time of subsequent measures. Inter- and intra-observer variabilities were not statistically significant. Minimal intraspecies variation was found in the AC-PC measurement of our human and NHP groups. We found significant interspecies differences, however, more between humans and NHPs, and less between the NHP groups. Regression analysis confirms the strong linear relationship of AC-PC distance based primarily on species in our study groups. Human/NHP AC-PC ratios varied between 2.1 to 2.3 based on the compared NHP species groups. We conclude that the scale differences in brain measurements between NHPs and humans described in this study allows improved translation of stereotactic targeting coordinates in future human clinical trials, which may lead to improved efficacy and safety. PMID:21185868

  11. Measurements of AC Loss In Second-Generation HTS Tapes in a DC Magnetic Field

    NASA Astrophysics Data System (ADS)

    Osofsky, M. S.; Soulen, R. J.; Gubser, D. U.; Datta, T.

    2008-03-01

    The successful application of superconductivity to motors and other power system components depends on the characterization and subsequent minimization of the ac loss in the superconductor used for fabrication of the component. The superconductive component, excited by an ac power source, may be exposed to large dc magnetic fields and/or ac fields. To further complicate the situation, the transport properties of the tapes are strongly dependent on the angle between the applied field and the YBCO c-axis (normal to the tape surface). We report on measurements of the transport ac loss of a YBaCuO tape at 65 K, at several frequencies, in applied dc fields of 1-3 T with the field parallel and perpendicular to the tape normal.

  12. Dielectric properties and study of AC electrical conduction mechanisms by non-overlapping small polaron tunneling model in Bis(4-acetylanilinium) tetrachlorocuprate(II) compound

    NASA Astrophysics Data System (ADS)

    Abkari, A.; Chaabane, I.; Guidara, K.

    2016-09-01

    In the present work, the synthesis and characterization of the Bis(4-acetylanilinium) tetrachlorocuprate(II) compound are presented. The structure of this compound is analyzed by X-ray diffraction which confirms the formation of single phase and is in good agreement the literature. Indeed, the Thermo gravimetric Analysis (TGA) shows that the decomposition of the compound is observed in the range of 420-520 K. However, the differential thermal analysis (DTA) indicates the presence of a phase transition at T=363 k. Furthermore, the dielectric properties and AC conductivity were studied over a temperature range (338-413 K) and frequency range (200 Hz-5 MHz) using complex impedance spectroscopy. Dielectric measurements confirmed such thermal analyses by exhibiting the presence of an anomaly in the temperature range of 358-373 K. The complex impedance plots are analyzed by an electrical equivalent circuit consisting of resistance, constant phase element (CPE) and capacitance. The activation energy values of two distinct regions are obtained from log σT vs 1000/T plot and are found to be E=1.27 eV (T<363 K) and E=1.09 eV (363 Kac conductivity, σac, has been analyzed by Jonscher's universal power law σ(ω)=σdc+Aωs. The value of s is to be temperature-dependent, which has a tendency to increase with temperature and the non-overlapping small polaron tunneling (NSPT) model is the most applicable conduction mechanism in the title compound. Complex impedance spectra of [C8H10NO]2CuCl4 at different temperatures.

  13. AC Inductive Measurement of Intergrain and Intragrain Currents in High-Tc Oxide Superconductors

    NASA Astrophysics Data System (ADS)

    Ni, Baorong; Munakata, Toshiyuki; Matsushita, Teruo; Iwakuma, Masataka; Funaki, Kazuo; Takeo, Masakatsu; Yamafuji, Kaoru

    1988-09-01

    Bulk intergrain current and closed intragrain current in sintered Y-Ba-Cu-O superconductors were measured at 77 K by using an ac inductive method. These currents can be separated because of the large difference in penetrating rates of the magnetic flux into specimens with respect to the ac field amplitude. The obtained intergrain current density agreed approximately with critical current density measured resistively. The closed intragrain current density amounted to 4.3× 108 A/m2 at B{=}0.5 T and decreased gradually with increasing magnetic field. The present results show that the ac inductive measurement is one of the available nondestructive methods to characterize sintered oxide specimens.

  14. Development of Low-Frequency AC Voltage Measurement System Using Single-Junction Thermal Converter

    NASA Astrophysics Data System (ADS)

    Amagai, Yasutaka; Nakamura, Yasuhiro

    Accurate measurement of low-frequency AC voltage using a digital multimeter at frequencies of 4-200Hz is a challenge in the mechanical engineering industry. At the National Metrology Institute of Japan, we developed a low-frequency AC voltage measurement system for calibrating digital multimeters operating at frequencies down to 1 Hz. The system uses a single-junction thermal converter and employs a theoretical model and a three-parameter sine wave fitting algorithm based on the least-square (LS) method. We calibrated the AC voltage down to 1Hz using our measurement system and reduced the measurement time compared with that using thin-film thermal converters. Our measurement results are verified by comparison with those of a digital sampling method using a high-resolution analog-to-digital converter; our data are in agreement to within a few parts in 105. Our proposed method enables us to measure AC voltage with an uncertainty of 25 μV/V (k = 1) at frequencies down to 4 Hz and a voltage of 10 V.

  15. Anomalous three-dimensional bulk ac conduction within the Kondo gap of SmB6 single crystals

    NASA Astrophysics Data System (ADS)

    Laurita, N. J.; Morris, C. M.; Koohpayeh, S. M.; Rosa, P. F. S.; Phelan, W. A.; Fisk, Z.; McQueen, T. M.; Armitage, N. P.

    2016-10-01

    The Kondo insulator SmB6 has long been known to display anomalous transport behavior at low temperatures, T <5 K. In this temperatures range, a plateau is observed in the dc resistivity, contrary to the exponential divergence expected for a gapped system. Recent theoretical calculations suggest that SmB6 may be the first topological Kondo insulator (TKI) and propose that the residual conductivity is due to topological surface states which reside within the Kondo gap. Since the TKI prediction many experiments have claimed to observe high mobility surface states within a perfectly insulating hybridization gap. Here, we investigate the low energy optical conductivity within the hybridization gap of single crystals of SmB6 via time domain terahertz spectroscopy. Samples grown by both optical floating zone and aluminum flux methods are investigated to probe for differences originating from sample growth techniques. We find that both samples display significant three-dimensional bulk conduction originating within the Kondo gap. Although SmB6 may be a bulk dc insulator, it shows significant bulk ac conduction that is many orders of magnitude larger than any known impurity band conduction. The nature of these in-gap states and their coupling with the low energy spin excitons of SmB6 is discussed. Additionally, the well-defined conduction path geometry of our optical experiments allows us to show that any surface states, which lie below our detection threshold if present, must have a sheet resistance of R /square≥ 1000 Ω .

  16. Fiber - Optic Devices as Temperature Sensors for Temperature Measurements in AC Magnetic Fields

    NASA Astrophysics Data System (ADS)

    Rablau, Corneliu; Lafrance, Joseph; Sala, Anca

    2007-10-01

    We report on the investigation of several fiber-optic devices as potential sensors for temperature measurements in AC magnetic fields. Common temperature sensors, such as thermocouples, thermistors or diodes, will create random and/or systematic errors when placed in a magnetic field. A DC magnetic field is susceptible to create a systematic offset to the measurement, while in an AC magnetic field of variable frequency random errors which cannot be corrected for can also be introduced. Fiber-Bragg-gratings and thin film filters have an inherent temperature dependence. Detrimental for their primary applications, the same dependence allows one to use such devices as temperature sensors. In an AC magnetic field, they present the advantage of being immune to electromagnetic interference. Moreover, for fiber-Bragg-gratings, the shape factor and small mass of the bare-fiber device make it convenient for temperature measurements on small samples. We studied several thin-film filters and fiber-Bragg-gratings and compared their temperature measurement capabilities in AC magnetic fields of 0 to 150 Gauss, 0 to 20 KHz to the results provided by off-the-shelf thermocouples and thermistor-based temperature measurement systems.

  17. Crystal structure, NMR study, dielectric relaxation and AC conductivity of a new compound [Cd3(SCN)2Br6(C2H9N2)2]n

    NASA Astrophysics Data System (ADS)

    Saidi, K.; Kamoun, S.; Ayedi, H. Ferid; Arous, M.

    2013-11-01

    The crystal structure, the 13C NMR spectroscopy and the complex impedance have been carried out on [Cd3(SCN)2Br6(C2H9N2)2]n. Crystal structure shows a 2D polymeric network built up of two crystallographically independent cadmium atoms with two different octahedral coordinations. This compound exhibits a phase transition at (T=355±2 K) which has been characterized by differential scanning calorimetry (DSC), X-rays powder diffraction, AC conductivity and dielectric measurements. Examination of 13C CP/MAS line shapes shows indirect spin-spin coupling (14N and 13C) with a dipolar coupling constant of 1339 Hz. The AC conductivity of this compound has been carried out in the temperature range 325-376 K and the frequency range from 10-2 Hz to 10 MHz. The impedance data were well fitted to two equivalent electrical circuits. The results of the modulus study reveal the presence of two distinct relaxation processes. One, at low frequency side, is thermally activated due to the ionic conduction of the crystal and the other, at higher frequency side, gradually disappears when temperature reaches 355 K which is attributed to the localized dipoles in the crystal. Moreover, the temperature dependence of DC-conductivity in both phases follows the Arrhenius law and the frequency dependence of σ(ω,T) follows Jonscher's universal law. The near values of activation energies obtained from the conductivity data and impedance confirm that the transport is through the ion hopping mechanism.

  18. AC impedance analysis of ionic and electronic conductivities in electrode mixture layers for an all-solid-state lithium-ion battery

    NASA Astrophysics Data System (ADS)

    Siroma, Zyun; Sato, Tomohiro; Takeuchi, Tomonari; Nagai, Ryo; Ota, Akira; Ioroi, Tsutomu

    2016-06-01

    The ionic and electronic effective conductivities of an electrode mixture layers for all-solid-state lithium-ion batteries containing Li2Ssbnd P2S5 as a solid electrolyte were investigated by AC impedance measurements and analysis using a transmission-line model (TLM). Samples containing graphite (graphite electrodes) or LiNi0.5Co0.2Mn0.3O2 (NCM electrodes) as the active material were measured under a "substrate | sample | bulk electrolyte | sample | substrate" configuration (ion-electron connection) and a "substrate | sample | substrate" configuration (electron-electron connection). Theoretically, if the electronic resistance is negligibly small, which is the case with our graphite electrodes, measurement with the ion-electron connection should be effective for evaluating ionic conductivity. However, if the electronic resistance is comparable to the ionic resistance, which is the case with our NCM electrodes, the results with the ion-electron connection may contain some inherent inaccuracy. In this report, we theoretically and practically demonstrate the advantage of analyzing the results with the electron-electron connection, which gives both the ionic and electronic conductivities. The similarity of the behavior of ionic conductivity with the graphite and NCM electrodes confirms the reliability of this analysis.

  19. Motor conduction measurement in myelopathy hand

    PubMed Central

    Shibuya, Ryoichi; Wada, Eiji; Iwasaki, Motoki; Yonenobu, Kazuo; Yoshikawa, Hideki

    2014-01-01

    Summary We studied the relationship between intramedullary high signal intensity (IMHSI) on T2-weighted magnetic resonance images and motor conduction in the spinal cords of cervical spondylotic myelopathy (CSM) patients. There was no significant difference between the biceps or triceps central motor conduction times (CMCTs) of the patients who did and did not exhibit IMHSI, whereas the abductor pollicis brevis CMCT was significantly longer in the patients who exhibited IMHSI (p<0.05) than in those who did not. The CMCT of the abductor pollicis brevis is sensitive to the degree of damage in the cervical spinal cord. Hand dysfunction is a characteristic of CSM regardless of the cervical level affected by the condition. The motor fibers innervating the intrinsic muscles of the hand in the long tract of the cervical spinal cord are more sensitive than other motor fibers. For this reason, we consider that myelopathy hand is a characteristic impairment of CSM. Transcranial magnetic stimulation of the hand motor cortex is useful for the evaluation of cervical myelopathy. PMID:25473737

  20. Note: Development of a microfabricated sensor to measure thermal conductivity of picoliter scale liquid samples

    NASA Astrophysics Data System (ADS)

    Park, Byoung Kyoo; Yi, Namwoo; Park, Jaesung; Kim, Dongsik

    2012-10-01

    This paper presents a thermal analysis device, which can measure thermal conductivity of picoliter scale liquid sample. We employ the three omega method with a microfabricated AC thermal sensor with nanometer width heater. The liquid sample is confined by a micro-well structure fabricated on the sensor surface. The performance of the instrument was verified by measuring the thermal conductivity of 27-picoliter samples of de-ionized (DI) water, ethanol, methanol, and DI water-ethanol mixtures with accuracies better than 3%. Furthermore, another analytical scheme allows real-time thermal conductivity measurement with 5% accuracy. To the best of our knowledge, this technique requires the smallest volume of sample to measure thermal property ever.

  1. Note: Development of a microfabricated sensor to measure thermal conductivity of picoliter scale liquid samples.

    PubMed

    Park, Byoung Kyoo; Yi, Namwoo; Park, Jaesung; Kim, Dongsik

    2012-10-01

    This paper presents a thermal analysis device, which can measure thermal conductivity of picoliter scale liquid sample. We employ the three omega method with a microfabricated AC thermal sensor with nanometer width heater. The liquid sample is confined by a micro-well structure fabricated on the sensor surface. The performance of the instrument was verified by measuring the thermal conductivity of 27-picoliter samples of de-ionized (DI) water, ethanol, methanol, and DI water-ethanol mixtures with accuracies better than 3%. Furthermore, another analytical scheme allows real-time thermal conductivity measurement with 5% accuracy. To the best of our knowledge, this technique requires the smallest volume of sample to measure thermal property ever.

  2. Effects of Luttinger leads on the AC conductance of a quantum dot

    NASA Astrophysics Data System (ADS)

    Yang, Kai-Hua; Qin, Chang-Dong; Wang, Huai-Yu; Liu, Kai-Di

    2017-04-01

    We investigate the joint effects of the intralead electron interaction and an external alternating gate voltage on the transport of a quantum dot coupled to two Luttinger liquid leads in the Kondo regime. We find the transferring between two Kondo physics mechanics by investigation of differential conductance. For very weak intralead interaction, the satellite and main Kondo resonant peaks appear in the differential conductance. For moderately strong intralead interaction, all the peaks disappear and evolve into dips, which signifies that a photon-assisted single-channel Kondo (1CK) physics turns into two-channel Kondo (2CK) physics. The 1CK and 2CK mechanisms can coexist within a region of the intralead interaction parameter. The 1CK physics transits to the 2CK one gradually, not suddenly. In the limit of strong interaction, all dips disappear. When the bias voltage is small, there is no photon exchange between the quantum dot and alternative field, and the differential conductance scales as a power law both in bias voltage and in temperature. As the field becomes stronger, the quantum dot will emit and absorb photons.

  3. Synthesis, crystal structure, NMR study and AC conductivity of [(C3H7)4N]2Cd2ClF5 compound

    NASA Astrophysics Data System (ADS)

    Hajji, Rachid; Oueslati, Abderrazak; Body, Monique; Hlel, Faouzi

    2015-08-01

    The [(C3H7)4N]2Cd2ClF5 compound was crystallized in the triclinic system with space group P1. The crystal structure consists of organic-inorganic layers, stacked along direction. The organic part consists of two cations types. The inorganic layer is made up of Cd2ClF5 dimmers composed of two in-equivalent irregular tetrahedra sharing one edge (Cl-F). The MAS NMR spectra showed two, three and five isotropic resonances relative to 111Cd, 13C and 19F nuclei, respectively. DSC measurement disclosed a phase transition at around 380 K. The impedance spectroscopy and AC electrical conductivity measurements of our compound were taken from 209 Hz to 5 MHz over the temperature range of 350-381 K. Nyquist plots ( Z″ vs Z') show semicircle arcs at different temperatures, and an electrical equivalent circuit has been proposed to explain the impedance results. The circuits consist of the parallel combination of bulk resistance ( R), capacitance ( C) and fractal capacitance (CPE). The conductivity σ p follows the Arrhenius relation. The near value of activation energies obtained from the conductivity data and circuit equivalent confirms that the transport is through hopping mechanism. The analysis of the experimental data shows that the reorientation motion of [N(C3H7)4]+ cations and/or [Cd2ClF5]2- anions is probably responsible for the observed conductivity.

  4. Calorimetric AC loss measurement of MgB2 superconducting tape in an alternating transport current and direct magnetic field

    NASA Astrophysics Data System (ADS)

    See, K. W.; Xu, X.; Horvat, J.; Cook, C. D.; Dou, S. X.

    2012-11-01

    Applications of MgB2 superconductors in electrical engineering have been widely reported, and various studies have been made to define their alternating current (AC) losses. However, studies on the transport losses with an applied transverse DC magnetic field have not been conducted, even though this is one of the favored conditions in applications of practical MgB2 tapes. Methods and techniques used to characterize and measure these losses have so far been grouped into ‘electrical’ and ‘calorimetric’ approaches with external conditions set to resemble the application conditions. In this paper, we present a new approach to mounting the sample and employ the calorimetric method to accurately determine the losses in the concurrent application of AC transport current and DC magnetic fields that are likely to be experienced in practical devices such as generators and motors. This technique provides great simplification compared to the pickup coil and lock-in amplifier methods and is applied to a long length (˜10 cm) superconducting tape. The AC loss data at 20 and 30 K will be presented in an applied transport current of 50 Hz under external DC magnetic fields. The results are found to be higher than the theoretical predictions because of the metallic fraction of the tape that contributes quite significantly to the total losses. The data, however, will allow minimization of losses in practical MgB2 coils and will be used in the verification of numerical coil models.

  5. In situ conductance measurements of copper phthalocyanine thin film growth on sapphire [0001].

    PubMed

    Murdey, Richard; Sato, Naoki

    2011-06-21

    The current flowing through a thin film of copper phthalocyanine vacuum deposited on a single crystal sapphire [0001] surface was measured during film growth from 0 to 93 nm. The results, expressed as conductance vs. nominal film thickness, indicate three distinct film growth regions. Conductive material forms below about 5 nm and again above 35 nm, but in the intermediate thicknesses the film conductance was observed to decrease with increasing film thickness. With the aid of ac-AFM topology images taken ex situ, the conductance results are explained based on the Stranski-Krastanov (2D + 3D) film growth mechanism, in which the formation of a thin wetting layer is followed by the growth of discrete islands that eventually coalesce into an interpenetrating, conductive network.

  6. Dielectric and AC-conductivity studies of Dy2O3 doped (K0.5Na0.5)NbO3 ceramics

    NASA Astrophysics Data System (ADS)

    Peddigari, Mahesh; Thota, Subhash; Pamu, Dobbidi

    2014-08-01

    (K0.5Na0.5)NbO3 + x wt.% Dy2O3 (x = 0-1.5) ferroelectric ceramics were prepared by conventional solid state reaction method. XRD patterns revealed that orthorhombic symmetry has transformed into psuedocubic symmetry with increasing the substitution of Dy3+ in the Na+ site. Temperature and frequency dependences of relative dielectric permittivity maximum conforms the transformation from normal ferroelectric to relaxor ferroelectric behaviour. Frequency dependence of the relative dielectric permittivity maximum temperature observed for the samples with x ≥ 1.0 and satisfied the Vogel-Fulcher law. The diffuseness exponent γ (1.27-1.95) estimated from the high temperature slopes of the diffused dielectric permittivity data reveals that the degree of relaxor behavior increases with increasing the amount of Dy2O3. The temperature dependence of AC-conductivity σAC (T) analysis in the range 310 K < T < 470 K reveals the existence of variable range hopping of charge carriers with average hopping length RH and hopping energy EH are in the range 8.5-27 Å and 48-153 meV, respectively. Voltage dependent dielectric constant measurements confirm the ferroelectric nature of KNN+ x wt% Dy2O3 ceramics.

  7. Effective method to measure back emfs and their harmonics of permanent magnet ac motors

    NASA Astrophysics Data System (ADS)

    Jiang, Q.; Bi, C.; Lin, S.

    2006-04-01

    As the HDD spindle motors become smaller and smaller, the back electromotive forces (emfs) measurement faces the new challenges due to their low inertias and small sizes. This article proposes a novel method to measure the back emfs and their harmonic components of PM ac motors only through a freewheeling procedure. To eliminate the influence of the freewheeling deceleration, the phase flux linkages are employed to obtain the back emf amplitudes and phases of the fundamental and harmonic components by using finite Fourier series analysis. The proposed method makes the freewheeling measurement of the back emfs and their harmonics accurate and fast. It is especially useful for the low inertia PM ac motors, such as spindle motors for small form factor HDDs.

  8. Size-dependent conductivity dispersion of gold nanoparticle colloids in a microchip: contactless measurements

    NASA Astrophysics Data System (ADS)

    Khalafalla, M. A. H.; Mesli, A.; Widattallah, H. M.; Sellai, A.; Al-harthi, S.; Al-Lawati, Haider A. J.; Suliman, F. O.

    2014-08-01

    We performed admittance measurements to investigate the particle size dependence of the conductivity of gold nanoparticle (Diameters: 6-100 nm) colloids in electrophoresis microchip in the frequency range of 0.03-1.00 MHz. The admittance was measured with two electrodes capacitively coupled to the colloid contained in a microchip capillary channel. The imaginary and real components of the admittance showed low-frequency dispersion associated with the polarization of the nanoparticles induced by the AC electric field. This was evident from the linear dependence of the process relaxation time as a function of the square of the radius of the nanoparticle.

  9. Non-Contact Electrical Conductivity Measurement Technique for Molten Metals

    NASA Technical Reports Server (NTRS)

    Rhim, W. K.; Ishikawa, T.

    1998-01-01

    A non-contact technique of measuring the electrical conductivity (or resistivity) of conducting liquids while they are levitated by the high temperature electrostatic levitator in a high vacuum is reported.

  10. Thermal-Conductivity Measurement of Thermoelectric Materials Using 3{{\\upomega }} Method

    NASA Astrophysics Data System (ADS)

    Hahtela, O.; Ruoho, M.; Mykkänen, E.; Ojasalo, K.; Nissilä, J.; Manninen, A.; Heinonen, M.

    2015-12-01

    In this work, a measurement system for high-temperature thermal-conductivity measurements has been designed, constructed, and characterized. The system is based on the 3{\\upomega } method which is an ac technique suitable for both bulk and thin-film samples. The thermal-conductivity measurements were performed in a horizontal three-zone tube furnace whose sample space can be evacuated to vacuum or alternatively a protective argon gas environment can be applied to prevent undesired oxidation and contamination of the sample material. The system was tested with several dielectric, semiconductor, and metal bulk samples from room temperature up to 725 K. The test materials were chosen so that the thermal-conductivity values covered a wide range from 0.37 W\\cdot m^{-1}\\cdot K^{-1} to 150 {} \\cdot m^{-1}\\cdot K^{-1}. An uncertainty analysis for the thermal-conductivity measurements was carried out. The measurement accuracy is mainly limited by the determination of the third harmonic of the voltage over the resistive metal heater strip that is used for heating the sample. A typical relative measurement uncertainty in the thermal-conductivity measurements was between 5 % and 8 % (k=2). An extension of the 3{\\upomega } method was also implemented in which the metal heater strip is first deposited on a transferable Kapton foil. Utilizing such a prefabricated sensor allows for faster measurements of the samples as there is no need to deposit a heater strip on each new sample.

  11. Measurement of AC Losses in a Racetrack Superconducting Coil Made from YBCO Coated Conductor

    NASA Astrophysics Data System (ADS)

    Seiler, Eugen; Abrahamsen, Asger B.; Kováč, Ján; Wichmann, Mike; Træholt, Chresten

    We present the results of transport measurements of AC losses in a racetrack shaped superconducting coil made from coated conductor tape. The outer dimensions of the coil are approximately 24 cm × 12 cm and it has 57 turns. The coil is impregnated with epoxy resin and fiberglass tape is used to insulate the individual turns and to improve the mechanical properties of the epoxy when exposed to thermal cycling. The coil is manufactured as a part of the field winding of a small synchronous generator; therefore stainless steel frames are installed on the inner and outer side of the winding to reinforce it. The AC loss is measured versus the transport current Ia with the coil immersed in liquid nitrogen. Measurements at frequencies 21 Hz, 36 Hz and 72 Hz are compared. The AC losses follow Ia2 dependence at low current amplitudes and Ia3 at high amplitudes. After cutting the inner steel frame the low amplitude losses are decreased, their frequency dependence is reduced but their dependence on the current remains unchanged.

  12. Direct Detection of Pure ac Spin Current by X-Ray Pump-Probe Measurements

    NASA Astrophysics Data System (ADS)

    Li, J.; Shelford, L. R.; Shafer, P.; Tan, A.; Deng, J. X.; Keatley, P. S.; Hwang, C.; Arenholz, E.; van der Laan, G.; Hicken, R. J.; Qiu, Z. Q.

    2016-08-01

    Despite recent progress in spin-current research, the detection of spin current has mostly remained indirect. By synchronizing a microwave waveform with synchrotron x-ray pulses, we use the ferromagnetic resonance of the Py (Ni81Fe19 ) layer in a Py /Cu /Cu75Mn25/Cu /Co multilayer to pump a pure ac spin current into the Cu75Mn25 and Co layers, and then directly probe the spin current within the Cu75Mn25 layer and the spin dynamics of the Co layer by x-ray magnetic circular dichroism. This element-resolved pump-probe measurement unambiguously identifies the ac spin current in the Cu75Mn25 layer.

  13. A Method for Measuring the Specific Electrical Conductivity of an Anisotropically Conductive Medium

    NASA Astrophysics Data System (ADS)

    Ašmontas, S.; Kleiza, V.; Kleiza, J.

    2008-06-01

    The paper deals with the ways of finding an electrical conductivity tensor of a plane and anisotropically conductive sample. Application of the Van der Pauw method to investigate the conductivity of anisotropically conductive media makes the basis of research. Several models of distribution of the electric field potential are presented, their merits and demerits are discussed, and the necessary physical measurements are indicated. On the basis of these models, the respective calculation expressions of the specific conductivity tensor are derived and algorithms for their realization and error calculation are developed.

  14. Broadband Interferometer for Measuring Transmitted Wavefronts of Optical Bandpass Filters for HST (ACS)

    NASA Technical Reports Server (NTRS)

    Boucarut, R. A.; Leviton, D. B.

    1998-01-01

    The transmitted wavefronts of optical filters for the Hubble Space Telescope (HST) Advanced Camera for Surveys (ACS) are characterized using the Wildly and Openly Modified Broadband Achromatic Twyman Green (WOMBAT) Interferometer developed in the NASA/GSFC Optics Branch's Diffraction Grating Evaluation Facility (DGEF). Because only four of thirty-three of ACS's optical bandpass filters transmit the 633 nm light of most commercial interferometers, a broadband interferometer is required to verify specified transmitted wavefront of ACS filters. WOMBAT's design is a hybrid of the BAT interferometer developed by JPL used for HST Wide Field and Planetary Camera 2 (WFPC-2) filters and a WYKO 400 phase shifting interferometer. It includes a broadband light source, monochromator, off-axis, parabolic collimating and camera mirrors, an aluminum-coated fused silica beam splitter, flat retroreflecting mirrors for the test and reference arms, and a LTV-sensitive CCD camera. An outboarded, piezo-electric phase shifter holds the flat mirror in the interferometer's reference arm. The interferometer is calibrated through interaction between the WYKO system's software and WONMAT hardware for the test wavelength of light entering the beam splitter. Phase-shifted interferograms of the filter mounted in the test arm are analyzed using WYKO's Vision' software. Filters as large as 90 mm in diameter have been measured over a wavelength range from 200 to 1100 nm with a sensitivity of lambda/200 rms at lambda = 633 nm. Results of transmitted wavefront measurements are shown for ACS fixed band pass and spatially-variable bandpass filters for a variety of wavelengths.

  15. Electrical conductivity measurements of nanofluids and development of new correlations.

    PubMed

    Konakanchi, Hanumantharao; Vajjha, Ravikanth; Misra, Debasmita; Das, Debendra

    2011-08-01

    In this study the electrical conductivity of aluminum oxide (Al2O3), silicon dioxide (SiO2) and zinc oxide (ZnO) nanoparticles dispersed in propylene glycol and water mixture were measured in the temperature range of 0 degrees C to 90 degrees C. The volumetric concentration of nanoparticles in these fluids ranged from 0 to 10% for different nanofluids. The particle sizes considered were from 20 nm to 70 nm. The electrical conductivity measuring apparatus and the measurement procedure were validated by measuring the electrical conductivity of a calibration fluid, whose properties are known accurately. The measured electrical conductivity values agreed within +/- 1% with the published data reported by the manufacturer. Following the validation, the electrical conductivities of different nanofluids were measured. The measurements showed that electrical conductivity of nanofluids increased with an increase in temperature and also with an increase in particle volumetric concentration. For the same nanofluid at a fixed volumetric concentration, the electrical conductivity was found to be higher for smaller particle sizes. From the experimental data, empirical models were developed for three nanofluids to express the electrical conductivity as functions of temperature, volumetric concentration and the size of the nanoparticles.

  16. Measuring the local electrical conductivity of human brain tissue

    NASA Astrophysics Data System (ADS)

    Akhtari, M.; Emin, D.; Ellingson, B. M.; Woodworth, D.; Frew, A.; Mathern, G. W.

    2016-02-01

    The electrical conductivities of freshly excised brain tissues from 24 patients were measured. The diffusion-MRI of the hydrogen nuclei of water molecules from regions that were subsequently excised was also measured. Analysis of these measurements indicates that differences between samples' conductivities are primarily due to differences of their densities of solvated sodium cations. Concomitantly, the sample-to-sample variations of their diffusion constants are relatively small. This finding suggests that non-invasive in-vivo measurements of brain tissues' local sodium-cation density can be utilized to estimate its local electrical conductivity.

  17. Influence of n-type nickel ferrite in enhancing the AC conductivity of optimized polyaniline-nickel ferrite nanocomposite

    NASA Astrophysics Data System (ADS)

    Megha, R.; Ravikiran, Y. T.; Vijaya Kumari, S. C.; Thomas, S.

    2017-04-01

    In the present work, n-type nickel ferrite (NF) particles prepared by sol gel autocombustion method were used to synthesize optimized polyaniline-nickel ferrite (PANI-NF) nanocomposite by in situ polymerization method. Then, NF, PANI and the composite were structurally characterized using Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD) and scanning electron microscopy (SEM) techniques. Improved π-electron delocalization in PANI-NF composite as compared to that in PANI was confirmed from FTIR analysis. Interfacial interaction between PANI and NF was confirmed from XRD studies. Highly agglomerated, more densely packed particles of the composite facilitating easier charge transport were confirmed from SEM image. Transmission electron microscopy (TEM) image was analysed to calculate accurate average particle size of the composite by fitting the data to log-normal distribution function. Crystalline nature of the composite was confirmed from selected area electron diffraction (SAED) analysis. Remarkable increase in AC conductivity of the PANI-NF composite as compared to that of PANI due mainly to the formation of interfacial heterojunction barrier between p-type PANI and n-type NF was confirmed experimentally and well supported theoretically by calculating binding energy, hopping distance and density of states at Fermi level as per correlated barrier hopping (CBH) model.

  18. Recent Advances in AC-DC Transfer Measurements Using Thin-Film Thermal Converters

    SciTech Connect

    WUNSCH,THOMAS F.; KINARD,JOSEPH R.; MANGINELL,RONALD P.; LIPE,THOMAS E.; SOLOMON JR.,OTIS M.; JUNGLING,KENNETH C.

    2000-12-08

    New standards for ac current and voltage measurements, thin-film multifunction thermal converters (MJTCS), have been fabricated using thin-film and micro-electro-mechanical systems (MEMS) technology. Improved sensitivity and accuracy over single-junction thermoelements and targeted performance will allow new measurement approaches in traditionally troublesome areas such as the low frequency and high current regimes. A review is presented of new microfabrication techniques and packaging methods that have resulted from a collaborative effort at Sandia National Laboratories and the National Institute of Standards and Technology (MHZ).

  19. Low-temperature AC conductivity of Bi 2Sr 2CaCu 2O 8+ δ

    NASA Astrophysics Data System (ADS)

    Corson, J.; Orenstein, J.; Eckstein, J. N.; Bozovic, I.

    2000-05-01

    We report measurements of anamolously large dissipative conductivities, σ1, in Bi 2Sr 2CaCu 2O 8+ δ at low temperatures. We have measured the complex conductivity of Bi 2Sr 2CaCu 2O 8+ δ thin films at 100-600 GHz as a function of doping from the underdoped to the overdoped state. At low temperatures there exists a residual σ1 which scales with the T=0 superfluid density as the doping is varied. This residual σ1 is larger than the possible contribution to σ1 from a thermal population of quasiparticles (QP) at the d-wave gap nodes.

  20. ac conduction in disordered solids: Comparison of effective-medium and distributed-transition-rate-response models

    NASA Astrophysics Data System (ADS)

    MacDonald, J. Ross

    1994-04-01

    Dyre has proposed that in the low-temperature limit an effective medium approximation, termed the Bryksin equation here (the BEM), predicts a universal frequency dependence for the normalized small-signal ac frequency relaxation response of nonmetallic disordered solids. This response has been claimed to be practically identical to that found for an exponential distribution of transition rates (EDTR) in the particular limiting uniform-energy-barrier-distribution case, but comparison of the two responses has been inadequate so far. Although it is shown here that they can be well differentiated, the question of which or either is universal still requires further comparisons with experiment for its answer. A generalization of the limiting low-temperature BEM equation applicable for nonzero temperatures, the GBEM, is developed and used to evaluate the temperature and frequency ranges for which the BEM is still adequate. It is found that GBEM response can be well approximated by the important EDTR solution and leads to a frequency exponent with the same temperature dependence as the latter. An expression derived herein for the dc conductivity predicted by the GBEM involves 1/3 of the maximum thermal activation energy (i.e., the effective percolation energy), however, rather than the energy itself. Further, unlike the BEM, the GBEM predicts the presence of an intrinsic temperature-independent high-frequency-limiting conductivity whose magnitude is evaluated. The combination of conductive- and dielectric-system response, always experimentally present for a conductive system, is evaluated for the GBEM, and in the frequency range where the GBEM and BEM are indistinguishable it leads to frequency and temperature response remarkably similar to that observed for most disordered materials. Finally, it is suggested that Dyre's macroscopic simulations of the relaxation problem do not seem fully relevant to physical situations of interest and thus should not be taken to confirm

  1. Computer-assisted system for measuring capacitance and conductance of a diode using a phase sensitive technique

    NASA Astrophysics Data System (ADS)

    Ketelsen, L. J. P.; Serway, R. A.

    1981-12-01

    This paper describes a system for making accurate and reliable ac measurements of capacitance as a function of frequency, bias voltage, and temperature. The experimental apparatus consists of the basic capacitance measuring circuit and an information gathering device. The basic circuit includes a constant ac voltage source in series with the cell, a dc source for biasing the cell, an ac current amplifier in series with the cell for monitoring the current, and a lock-in amplifier to measure the ac current. The capacitance device is interfaced with a microcomputer to facilitate handling large quantities of data in a short time. The computer is also used to increment the bias voltage for C-V measurements. The system has the capability of measuring capacitance to an accuracy of about 5 digits. We have used this system to study deep impurity levels in thin-film, polycrystalline CdS/CuxS solar cells. The deep traps appear as anomalies in the otherwise linear l/C2 versus V plots. These levels play an important role in determining cell characteristics and may also influence the cell's efficiency. The advantages of the capacitance-conductance system described in this paper are: (1) simple construction; (2) accurate calibration procedure; (3) ability to take data with 4 1/2 stable digits; (4) the admittance can be measured as a function of bias voltage, frequency, and temperature; (5) automation, i.e., computer controlled, and (6) the ability to accurately provide information on unstable samples.

  2. Optical transmission versus ac magnetization measurements for monitoring colloidal Ni nanorod rotational dynamics

    NASA Astrophysics Data System (ADS)

    Gratz, M.; Tschöpe, A.

    2017-01-01

    Ni nanorods with an average length < 250 nm and diameter < 30 nm were synthesized using the AAO template method. The magnetization and optical transmission of nanorod colloidal dispersions in alternating magnetic fields were measured and analyzed with the objective of comparing the intrinsic Brownian relaxation times obtained with the two methods. The different physical origin of the measured signal, related to different moments of the orientation distribution function, and the non-linear effects expected for the large magnetic moments of the Ni nanorods at common field amplitudes required a comprehensive modelling. The time-dependent magnetization and optical transmission in ac magnetic fields was derived by numerical solution of the Fokker-Planck equation. The simulated time-dependent magnetization and optical transmission at a given frequency and field amplitude were analyzed analogous to experimental data to determine characteristic relaxation frequencies. Empirical relationships were derived which enabled extraction of the intrinsic Brownian relaxation time from the characteristic frequencies measured in the non-linear regime. Despite large differences in the characteristic frequencies obtained from magnetization and optical transmission measurements, the retrieved intrinsic Brownian relaxation times were found to agree well. The potential of ac magnetic field-dependent optical transmission for biosensing applications was demonstrated by monitoring the adsorption of the protein gelatine on the nanorod labels.

  3. Contactless electrical conductivity measurement of electromagnetically levitated metallic melts

    SciTech Connect

    Richardsen, T.; Lohoefer, G.

    1999-07-01

    The electrical conductivity {sigma} of metallic liquids is of obvious importance to many liquid metal processing operations, because it controls the melt flow under the influence of electromagnetic fields, e.g. during casting processes, or in crystal growth furnaces. A facility for noninvasive measurements of the electrical conductivity of liquid metals above and below the melting temperature is presented. It combines the containerless positioning method of electromagnetic levitation with the contactless technique of inductive conductivity measurement. Contrary to the conventional measurement method, the sample is freely suspended within the measuring field and, thus, has no exactly predefined shape. This made a new theoretical basis necessary with implications on the measurement and levitation fields. Furthermore, the problem of the mutual inductive interactions between the levitation and the measuring coils had to be solved.

  4. Mutation Glu82Lys in lamin A/C gene is associated with cardiomyopathy and conduction defect

    SciTech Connect

    Wang Hu; Wang Jizheng; Zheng Weiyue; Wang Xiaojian; Wang Shuxia; Song Lei; Zou Yubao; Yao Yan; Hui Rutai . E-mail: huirutai@sglab.org

    2006-05-26

    Dilated cardiomyopathy is a form of heart muscle disease characterized by impaired systolic function and ventricular dilation. The mutations in lamin A/C gene have been linked to dilated cardiomyopathy. We screened genetic mutations in a large Chinese family of 50 members including members with dilated cardiomyopathy and found a Glu82Lys substitution mutation in the rod domain of the lamin A/C protein in eight family members, three of them have been diagnosed as dilated cardiomyopathy, one presented with heart dilation. The pathogenic mechanism of lamin A/C gene defect is poorly understood. Glu82Lys mutated lamin A/C and wild type protein was transfected into HEK293 cells. The mutated protein was not properly localized at the inner nuclear membrane and the emerin protein, which interacts with lamin A/C, was also aberrantly distributed. The nuclear membrane structure was disrupted and heterochromatin was aggregated aberrantly in the nucleus of the HEK293 cells stably transfected with mutated lamin A/C gene as determined by transmission electron microscopy.

  5. Electrical resistivity and AC-calorimetric measurements of PrRu 4P 12 under pressure

    NASA Astrophysics Data System (ADS)

    Miyake, A.; Holmes, A. T.; Kagayama, T.; Shimizu, K.; Sekine, C.; Shirotani, I.; Kikuchi, D.; Sugawara, H.; Sato, H.

    2008-04-01

    We have studied the effect of pressure in the filled skutterudite PrRu 4P 12, which shows a metal-insulator (MI) transition at TMI=63 K, via simultaneous measurements of electrical resistivity ( ρ) and AC-calorimetry ( CAC). Schottky-like anomalies in CAC disappear under pressure, suggesting a change of the ground state. The resistivity below TMI is strongly suppressed with increasing pressure, in contrast to the weak pressure dependence of TMI. Above 10 GPa, ρ(T) shows metallic behavior with small anomalies at TMI. We discuss the likely change of ground state in PrRu 4P 12 with pressure from triplet to singlet.

  6. In situ measurement of conductivity during nanocomposite film deposition

    NASA Astrophysics Data System (ADS)

    Blattmann, Christoph O.; Pratsinis, Sotiris E.

    2016-05-01

    Flexible and electrically conductive nanocomposite films are essential for small, portable and even implantable electronic devices. Typically, such film synthesis and conductivity measurement are carried out sequentially. As a result, optimization of filler loading and size/morphology characteristics with respect to film conductivity is rather tedious and costly. Here, freshly-made Ag nanoparticles (nanosilver) are made by scalable flame aerosol technology and directly deposited onto polymeric (polystyrene and poly(methyl methacrylate)) films during which the resistance of the resulting nanocomposite is measured in situ. The formation and gas-phase growth of such flame-made nanosilver, just before incorporation onto the polymer film, is measured by thermophoretic sampling and microscopy. Monitoring the nanocomposite resistance in situ reveals the onset of conductive network formation by the deposited nanosilver growth and sinternecking. The in situ measurement is much faster and more accurate than conventional ex situ four-point resistance measurements since an electrically percolating network is detected upon its formation by the in situ technique. Nevertheless, general resistance trends with respect to filler loading and host polymer composition are consistent for both in situ and ex situ measurements. The time lag for the onset of a conductive network (i.e., percolation) depends linearly on the glass transition temperature (Tg) of the host polymer. This is attributed to the increased nanoparticle-polymer interaction with decreasing Tg. Proper selection of the host polymer in combination with in situ resistance monitoring therefore enable the optimal preparation of conductive nanocomposite films.

  7. Measurements of prompt radiation induced conductivity of Kapton.

    SciTech Connect

    Preston, Eric F.; Zarick, Thomas Andrew; Sheridan, Timothy J.; Hartman, E. Frederick; Stringer, Thomas Arthur

    2010-10-01

    We performed measurements of the prompt radiation induced conductivity in thin samples of Kapton (polyimide) at the Little Mountain Medusa LINAC facility in Ogden, UT. Three mil samples were irradiated with a 0.5 {mu}s pulse of 20 MeV electrons, yielding dose rates of 1E9 to 1E10 rad/s. We applied variable potentials up to 2 kV across the samples and measured the prompt conduction current. Analysis rendered prompt conductivity coefficients between 6E-17 and 2E-16 mhos/m per rad/s, depending on the dose rate and the pulse width.

  8. Indirect measurement of thermal conductivity in silicon nanowires

    SciTech Connect

    Pennelli, Giovanni Nannini, Andrea; Macucci, Massimo

    2014-02-28

    We report indirect measurements of thermal conductivity in silicon nanostructures. We have exploited a measurement technique based on the Joule self-heating of silicon nanowires. A standard model for the electron mobility has been used to determine the temperature through the accurate measurement of the nanowire resistance. We have applied this technique to devices fabricated with a top-down process that yields nanowires together with large silicon areas used both as electrical and as thermal contacts. As there is crystalline continuity between the nanowires and the large contact areas, our thermal conductivity measurements are not affected by any temperature drop due to the contact thermal resistance. Our results confirm the observed reduction of thermal conductivity in nanostructures and are comparable with those previously reported in the literature, achieved with more complex measurement techniques.

  9. Non-Contact Conductivity Measurement for Automated Sample Processing Systems

    NASA Technical Reports Server (NTRS)

    Beegle, Luther W.; Kirby, James P.

    2012-01-01

    A new method has been developed for monitoring and control of automated sample processing and preparation especially focusing on desalting of samples before analytical analysis (described in more detail in Automated Desalting Apparatus, (NPO-45428), NASA Tech Briefs, Vol. 34, No. 8 (August 2010), page 44). The use of non-contact conductivity probes, one at the inlet and one at the outlet of the solid phase sample preparation media, allows monitoring of the process, and acts as a trigger for the start of the next step in the sequence (see figure). At each step of the muti-step process, the system is flushed with low-conductivity water, which sets the system back to an overall low-conductivity state. This measurement then triggers the next stage of sample processing protocols, and greatly minimizes use of consumables. In the case of amino acid sample preparation for desalting, the conductivity measurement will define three key conditions for the sample preparation process. First, when the system is neutralized (low conductivity, by washing with excess de-ionized water); second, when the system is acidified, by washing with a strong acid (high conductivity); and third, when the system is at a basic condition of high pH (high conductivity). Taken together, this non-contact conductivity measurement for monitoring sample preparation will not only facilitate automation of the sample preparation and processing, but will also act as a way to optimize the operational time and use of consumables

  10. Thermal conductivity measurements in unsaturated hydrate-bearing sediments

    NASA Astrophysics Data System (ADS)

    Dai, Sheng; Cha, Jong-Ho; Rosenbaum, Eilis J.; Zhang, Wu; Seol, Yongkoo

    2015-08-01

    Current database on the thermal properties of hydrate-bearing sediments remains limited and has not been able to capture their consequential changes during gas production where vigorous phase changes occur in this unsaturated system. This study uses the transient plane source (TPS) technique to measure the thermal conductivity of methane hydrate-bearing sediments with various hydrate/water/gas saturations. We propose a simplified method to obtain thermal properties from single-sided TPS signatures. Results reveal that both volume fraction and distribution of the pore constituents govern the thermal conductivity of unsaturated specimens. Thermal conductivity hysteresis is observed due to water redistribution and fabric change caused by hydrate formation and dissociation. Measured thermal conductivity increases evidently when hydrate saturation Sh > 30-40%, shifting upward from the geometric mean model prediction to a Pythagorean mixing model. These observations envisage a significant drop in sediment thermal conductivity when residual hydrate/water saturation falls below ~40%, hindering further gas production.

  11. Redesign of an AC Magnetic Susceptometer for Measurements in Smaller Samples

    NASA Astrophysics Data System (ADS)

    Vargas, Andres; Fukuda, Ryan; Sunny, Smitha; Ho, Pei-Chun

    2013-03-01

    A new AC magnetic susceptometer was created for the purpose of measuring the magnetic properties of smaller samples, such as nanoparticles that are currently being synthesized in our lab. The susceptometer consists of a primary coil, a secondary coil, and a sample holder. The primary coil is the outer component of the susceptometer, which provides a magnetic field when current is applied due to Ampere's Law. Inside of the primary coil lies the secondary coil, which has two oppositely wound solenoids; they are oppositely wound to reduce background signal. The sample holder lies inside of the secondary coil with the sample. All of these go inside of a beryllium copper casing for protection. We tested the susceptometer by looking for the ferromagnetic phase transition of an 11 mg Gd sample. A ~ 100 μ A AC current was applied to the primary coil, which created a magnetic field that polarized the magnetic moments in the sample. This induced a voltage on the secondary coil, which is proportional to the magnetic susceptibility. We measured the temperature dependency of the induced voltage from 10 K to 300 K. The results showed a sharp increase in the induced voltage around 293K, which agrees with the known ferromagnetic transition of Gd. Research at CSU-Fresno is supported by NSF DMR-1104544. Felipe Vargas is also supported by Undergraduate Research Grant and Faculty-Sponsored Student Research Award at CSU Fresno.

  12. pH measurement of low-conductivity waters

    USGS Publications Warehouse

    Busenberg, Eurybiades; Plummer, L.N.

    1987-01-01

    pH is an important and commonly measured parameter of precipitation and other natural waters. The various sources of errors in pH measurement were analyzed and procedures for improving the accuracy and precision of pH measurements in natural waters with conductivities of < 100 uS/cm at 25 C are suggested. Detailed procedures are given for the preparation of dilute sulfuric acid standards to evaluate the performance of pH electrodes in low conductivity waters. A daily check of the pH of dilute sulfuric acid standards and deionized water saturated with a gas mixture of low carbon dioxide at partial pressure (air) prior to the measurement of the pH of low conductivity waters is suggested. (Author 's abstract)

  13. Noninvasive measurement of conductivity anisotropy at larmor frequency using MRI.

    PubMed

    Lee, Joonsung; Song, Yizhuang; Choi, Narae; Cho, Sungmin; Seo, Jin Keun; Kim, Dong-Hyun

    2013-01-01

    Anisotropic electrical properties can be found in biological tissues such as muscles and nerves. Conductivity tensor is a simplified model to express the effective electrical anisotropic information and depends on the imaging resolution. The determination of the conductivity tensor should be based on Ohm's law. In other words, the measurement of partial information of current density and the electric fields should be made. Since the direct measurements of the electric field and the current density are difficult, we use MRI to measure their partial information such as B1 map; it measures circulating current density and circulating electric field. In this work, the ratio of the two circulating fields, termed circulating admittivity, is proposed as measures of the conductivity anisotropy at Larmor frequency. Given eigenvectors of the conductivity tensor, quantitative measurement of the eigenvalues can be achieved from circulating admittivity for special tissue models. Without eigenvectors, qualitative information of anisotropy still can be acquired from circulating admittivity. The limitation of the circulating admittivity is that at least two components of the magnetic fields should be measured to capture anisotropic information.

  14. Simultaneous Rheoelectric Measurements of Strongly Conductive Complex Fluids

    NASA Astrophysics Data System (ADS)

    Helal, Ahmed; Divoux, Thibaut; McKinley, Gareth H.

    2016-12-01

    We introduce an modular fixture designed for stress-controlled rheometers to perform simultaneous rheological and electrical measurements on strongly conductive complex fluids under shear. By means of a nontoxic liquid metal at room temperature, the electrical connection to the rotating shaft is completed with minimal additional mechanical friction, allowing for simultaneous stress measurements at values as low as 1 Pa. Motivated by applications such as flow batteries, we use the capabilities of this design to perform an extensive set of rheoelectric experiments on gels formulated from attractive carbon-black particles, at concentrations ranging from 4 to 15 wt %. First, experiments on gels at rest prepared with different shear histories show a robust power-law scaling between the elastic modulus G0' and the conductivity σ0 of the gels—i.e., G0'˜σ0α, with α =1.65 ±0.04 , regardless of the gel concentration. Second, we report conductivity measurements performed simultaneously with creep experiments. Changes in conductivity in the early stage of the experiments, also known as the Andrade-creep regime, reveal for the first time that plastic events take place in the bulk, while the shear rate γ ˙ decreases as a weak power law of time. The subsequent evolution of the conductivity and the shear rate allows us to propose a local yielding scenario that is in agreement with previous velocimetry measurements. Finally, to establish a set of benchmark data, we determine the constitutive rheological and electrical behavior of carbon-black gels. Corrections first introduced for mechanical measurements regarding shear inhomogeneity and wall slip are carefully extended to electrical measurements to accurately distinguish between bulk and surface contributions to the conductivity. As an illustrative example, we examine the constitutive rheoelectric properties of five different grades of carbon-black gels and we demonstrate the relevance of this rheoelectric apparatus as a

  15. Novel multijunction thermal converter in planar technique for AC current, voltage, power and optical radiation measurement

    NASA Astrophysics Data System (ADS)

    Klonz, M.; Weimann, T.

    1990-05-01

    A new planar thin film design of multijunction thermocouples on a silicon chip containing a window with a SiO2-membrane for low heat conductance underneath of the thermocouples is described. It is used as the sensor for the temperature difference in a multijunction thermal converter for ac-dc transfer of electrical quantities like voltage, current and power via Joule heat in a thin film resistor. By coating the heater with an optically absorbing layer it is used as a highly sensitive radiometer transferring absorbed energy to Joule heat in the resistor. The design can easily be optimized for all different frequency applications. It offers the possibility of the mass production of transfer standards at highest level of accuracy.

  16. Wet method for measuring starch gelatinization temperature using electrical conductivity.

    PubMed

    Morales-Sanchez, E; Figueroa, J D C; Gaytan-Martínez, M

    2009-09-01

    The objective of the present study was to develop a method for obtaining the gelatinization temperature of starches by using electrical conductivity. Native starches from corn, rice, potato, and wheat were prepared with different proportions of water and heated from room temperature to 90 degrees C, in a device especially designed for monitoring the electrical conductivity as a function of temperature. The results showed a linear trend of the electrical conductivity with the temperature until it reaches the onset gelatinization temperature. After that point, the electrical conductivity presented an increment or decrement depending on the water content in the sample and it was related to starch swelling and gelatinization phenomena. At the end gelatinization temperature, the conductivity becomes stable and linear, indicating that there are no more changes of phase. The starch gelatinization parameter, which was evaluated in the 4 types of starches using the electrical conductivity, was compared with those obtained by using differential scanning calorimeter (DSC). The onset temperature at which the electrical conductivity increased or decreased was found to be similar to that obtained by DSC. Also, the final temperature at which the electrical conductivity returned to linearity matched the end gelatinization temperature of the DSC. Further, a wet method for measuring the onset, peak, and end gelatinization temperatures as a function of temperature using the electrical conductivity curves is presented for a starch-water suspension.

  17. AC photovoltaic module magnetic fields

    SciTech Connect

    Jennings, C.; Chang, G.J.; Reyes, A.B.; Whitaker, C.M.

    1997-12-31

    Implementation of alternating current (AC) photovoltaic (PV) modules, particularly for distributed applications such as PV rooftops and facades, may be slowed by public concern about electric and magnetic fields (EMF). This paper documents magnetic field measurements on an AC PV module, complementing EMF research on direct-current PV modules conducted by PG and E in 1993. Although not comprehensive, the PV EMF data indicate that 60 Hz magnetic fields (the EMF type of greatest public concern) from PV modules are comparable to, or significantly less than, those from household appliances. Given the present EMF research knowledge, AC PV module EMF may not merit considerable concern.

  18. Analytical estimation of skeleton thermal conductivity of a geopolymer foam from thermal conductivity measurements

    NASA Astrophysics Data System (ADS)

    Henon, J.; Alzina, A.; Absi, J.; Smith, D. S.; Rossignol, S.

    2015-07-01

    The geopolymers are alumino-silicate binders. The addition of a high pores volume fraction, gives them a thermal insulation character desired in the building industry. In this work, potassium geopolymer foams were prepared at room temperature (< 70 ∘C) by a process of in situ gas release. The porosity distribution shows a multiscale character. However, the thermal conductivity measurements gave values from 0.35 to 0.12 Wm-1.K-1 for a pore volume fraction values between 65 and 85%. In the aim to predict the thermal properties of these foams and focus on the relationship "thermal-conductivity/microstructure", knowledge of the thermal conductivity of their solid skeleton (λ s ) is paramount. However, there is rare work on the determination of this value depending on the initial composition. By the formulation used, the foaming agent contributes to the final network, and it is not possible to obtain a dense material designate to make a direct measurement of λ s . The objective of this work is to use inverse analytical methods to identify the value of λ s . Measurements of thermal conductivity by the fluxmetre technique were performed. The obtained value of the solid skeleton thermal conductivity by the inverse numerical technique is situated in a framework between 0.95 and 1.35 Wm-1.K-1 and is in agreement with one issue from the literature.

  19. Thermal and Electrical Conductivity Measurements of CDA 510 Phosphor Bronze

    NASA Technical Reports Server (NTRS)

    Tuttle, James E.; Canavan, Edgar; DiPirro, Michael

    2009-01-01

    Many cryogenic systems use electrical cables containing phosphor bronze wire. While phosphor bronze's electrical and thermal conductivity values have been published, there is significant variation among different phosphor bronze formulations. The James Webb Space Telescope (JWST) will use several phosphor bronze wire harnesses containing a specific formulation (CDA 510, annealed temper). The heat conducted into the JWST instrument stage is dominated by these harnesses, and approximately half of the harness conductance is due to the phosphor bronze wires. Since the JWST radiators are expected to just keep the instruments at their operating temperature with limited cooling margin, it is important to know the thermal conductivity of the actual alloy being used. We describe an experiment which measured the electrical and thermal conductivity of this material between 4 and 295 Kelvin.

  20. Thermal and Electrical Conductivity Measurements of Cda 510 Phosphor Bronze

    NASA Astrophysics Data System (ADS)

    Tuttle, J.; Canavan, E.; DiPirro, M.

    2010-04-01

    Many cryogenic systems use electrical cables containing phosphor bronze wire. While phosphor bronze's electrical and thermal conductivity values have been published, results vary among different phosphor bronze formulations. The James Webb Space Telescope (JWST) will use several phosphor bronze wire harnesses containing a specific formulation (CDA 510, annealed temper). These harnesses dominate the heat conducted into the JWST instrument stage, and approximately half of the harness conductance is due to the phosphor bronze wires. Since the JWST radiators are expected to keep the instruments at their operating temperature with limited cooling margin, it is important to know the thermal conductivity of the actual alloy being used. We describe an experiment that measured its electrical and thermal conductivity between 4 and 295 Kelvin.

  1. Spectral response of atmospheric electric field measurements near AC high voltage power lines

    NASA Astrophysics Data System (ADS)

    Silva, H. G.; Matthews, J. C.; Wright, M. D.; Shallcross, D. E.

    2015-10-01

    To understand the influence of corona ion emission on the atmospheric electrical field, measurements were made near to two AC high voltage power lines. A JCI 131 field-mill recorded the atmospheric electric field over one year. Meteorological measurements were also taken. The data series is divided in four zones (dependent on wind direction): whole zones, Z0; zone 1, Z1; zone 2, Z2; zone 3, Z3. Z3 is the least affected by corona ion emission and for that reason it is used as a reference against Z1 and Z2, which are strongly influenced by this phenomena. Analysis was undertaken for all weather days and dry days only. The Lomb-Scargle strategy developed for unevenly spaced time-series is used to calculate the spectral response of the aforementioned zones. Only frequencies above 1 minute are considered.

  2. Conductivity As A Measure Of Degree Of Polymerization

    NASA Technical Reports Server (NTRS)

    Dean, David L.; Walsh, Robert K.

    1993-01-01

    In improved method of dielectric monitoring of process of polymerization of mixed ingredients of polymeric material, emphasis placed on measurement of conductivity rather than permittivity. Conductivity tends to change more during curing process than permittivity does, is less dependent on frequency, and more-sensitive and more-reliable indicator of progress of cure. Conductivity used to compute quantity called "ion viscosity," which relates to classical viscosity of fluid. During cure of typical polymer, ion viscosity varies over wide range, eventually rising to plateau toward end of cure.

  3. In-Pile Thermal Conductivity Measurement Method for Nuclear Fuels

    SciTech Connect

    Joy L. Rempe; Brandon Fox; Heng Ban; Joshua E. Daw; Darrell L. Knudson; Keith G. Condie

    2009-08-01

    Thermophysical properties of advanced nuclear fuels and materials during irradiation must be known prior to their use in existing, advanced, or next generation reactors. Thermal conductivity is one of the most important properties for predicting fuel and material performance. A joint Utah State University (USU) / Idaho National Laboratory (INL) project, which is being conducted with assistance from the Institute for Energy Technology at the Norway Halden Reactor Project, is investigating in-pile fuel thermal conductivity measurement methods. This paper focuses on one of these methods – a multiple thermocouple method. This two-thermocouple method uses a surrogate fuel rod with Joule heating to simulate volumetric heat generation to gain insights about in-pile detection of thermal conductivity. Preliminary results indicated that this method can measure thermal conductivity over a specific temperature range. This paper reports the thermal conductivity values obtained by this technique and compares these values with thermal property data obtained from standard thermal property measurement techniques available at INL’s High Test Temperature Laboratory. Experimental results and material properties data are also compared to finite element analysis results.

  4. Thermal conductivity measurement of thin films by a dc method.

    PubMed

    Yang, Junyou; Zhang, Jiansheng; Zhang, Hui; Zhu, Yunfeng

    2010-11-01

    A dc method, which needs no complex numerical calculation and expensive hardware configuration, was developed to measure the cross-plane thermal conductivity of thin films in this paper. Two parallel metallic heaters, which were deposited on different parts of the sample, serve simultaneously as the heaters and temperature sensors during the measurement. A direct current was flowed through the same two metallic strips to heat the thin-film sample. The heating power and the heater's temperature were obtained by a data acquisition device, and the thermal conductivity of thin film was calculated. To verify the validity of the dc method, several SiO(2) films with different thicknesses were deposited on Si wafers, respectively, and their thermal conductivities were measured by both the dc method and 3ω method. The results of two methods are in good agreement within an acceptable error, and they are also inconsistent with some of previously published data.

  5. Method for Measuring Thermal Conductivity of Small Samples Having Very Low Thermal Conductivity

    NASA Technical Reports Server (NTRS)

    Miller, Robert A.; Kuczmarski, Maria a.

    2009-01-01

    This paper describes the development of a hot plate method capable of using air as a standard reference material for the steady-state measurement of the thermal conductivity of very small test samples having thermal conductivity on the order of air. As with other approaches, care is taken to ensure that the heat flow through the test sample is essentially one-dimensional. However, unlike other approaches, no attempt is made to use heated guards to block the flow of heat from the hot plate to the surroundings. It is argued that since large correction factors must be applied to account for guard imperfections when sample dimensions are small, it may be preferable to simply measure and correct for the heat that flows from the heater disc to directions other than into the sample. Experimental measurements taken in a prototype apparatus, combined with extensive computational modeling of the heat transfer in the apparatus, show that sufficiently accurate measurements can be obtained to allow determination of the thermal conductivity of low thermal conductivity materials. Suggestions are made for further improvements in the method based on results from regression analyses of the generated data.

  6. The thermal conductivity of meteorites: New measurements and analysis

    NASA Astrophysics Data System (ADS)

    Opeil, C. P.; Consolmagno, G. J.; Britt, D. T.

    2010-07-01

    We have measured the thermal conductivity at low temperatures (5-300 K) of six meteorites representing a range of compositions, including the ordinary chondrites Cronstad (H5) and Lumpkin (L6), the enstatite chondrite Abee (E4), the carbonaceous chondrites NWA 5515 (CK4 find) and Cold Bokkeveld (CM2), and the iron meteorite Campo del Cielo (IAB find). All measurements were made using a Quantum Design Physical Properties Measurement System, Thermal Transport Option (TTO) on samples cut into regular parallelepipeds of ˜2-6 mm dimension. The iron meteorite conductivity increases roughly linearly from 15 W m -1 K -1 at 100 K to 27 W m -1 K -1 at 300 K, comparable to typical values for metallic iron. By contrast, the conductivities of all the stony samples except Abee appear to be controlled by the inhomogeneous nature of the meteorite fabric, resulting in values that are much lower than those of pure minerals and which vary only slightly with temperature above 100 K. The L and CK sample conductivities above 100 K are both about 1.5 W m -1 K -1, that of the H is 1.9 W m -1 K -1, and that of the CM sample is 0.5 W m -1 K -1; by contrast the literature value at 300 K for serpentine is 2.5 W m -1 K -1 and those of enstatite and olivine range from 4.5 to 5 W m -1 K -1 (which is comparable to the Abee value). These measurements are among the first direct measurements of thermal conductivity for meteorites. The results compare well with previous estimates for meteorites, where conductivity was derived from diffusivity measurements and modeled heat capacities; our new values are of a higher precision and cover a wider range of temperatures and meteorite types. If the rocky material that makes up asteroids and provides the dust to comets, Kuiper Belt objects, and icy satellites has the same low thermal conductivities as the ordinary and carbonaceous chondrites measured here, this would significantly change models of their thermal evolution. These values would also lower their

  7. Spectral Measurements from the Optical Emission of the A.C. Plasma Anemometer

    NASA Astrophysics Data System (ADS)

    Matlis, Eric; Marshall, Curtis; Corke, Thomas; Gogineni, Sivaram

    2015-11-01

    The optical emission properties of a new class of AC-driven flow sensors based on a glow discharge (plasma) is presented. These results extend the utility of the plasma sensor that has recently been developed for measurements in high-enthalpy flows. The plasma sensor utilizes a high frequency (1MHz) AC discharge between two electrodes as the main sensing element. The voltage drop across the discharge correlates to changes in the external flow which can be calibrated for mass-flux (ρU) or pressure depending on the design of the electrodes and orientation relative to the free-stream flow direction. Recent experiments examine the potential for spectral analysis of the optical emission of the discharge to provide additional insight to the flow field. These experiments compare the optical emission of the plasma to emission from breakdown due to an ND:YAG laser. The oxygen 777.3 nm band in particular is a focus of interest as a marker for the determination of gas density.

  8. Resistivity and AC calorimetry measurements on CeNiGe2 under pressure

    NASA Astrophysics Data System (ADS)

    Holmes, A. T.; Muramatsu, T.; Miyake, A.; Kaczorowski, D.; Bukowski, Z.; Kagayama, T.; Shimizu, K.

    2007-03-01

    We present resistivity and AC calorimetry measurements of single crystalline CeNiGe2 under high pressure and low temperature in a diamond anvil cell. CeNiGe2 is a highly anisotropic, antiferromagnetic Kondo system at ambient pressure, located close to the boundary with non-magnetic systems. It has two ordering temperatures, T=3.9 K and T=3.2 K, which are suppressed under pressure. Between 0.7 and 1.4 GPa only a single transition was identified, with TN reaching 1.9 K by 1.4 GPa. At 1.9 GPa two transitions could again be seen by AC calorimetry at 2.0 and 1.3 K, accompanied by a qualitative change in the behaviour of the resistivity. The Sommerfeld coefficient showed a maximum of 755 mJ mol-1 K-2 at 1.4 GPa, up from 448 mJ mol-1 K-2 at close to ambient pressure. The residual resistivity was found to decrease sharply above 1.4 GPa after an initial increase with pressure.

  9. Measurements of prompt radiation induced conductivity in Teflon (PTFE).

    SciTech Connect

    Hartman, E. Frederick; Zarick, Thomas Andrew; Sheridan, Timothy J.; Preston, E.

    2013-05-01

    We performed measurements of the prompt radiation induced conductivity (RIC) in thin samples of Teflon (PTFE) at the Little Mountain Medusa LINAC facility in Ogden, UT. Three mil (76.2 microns) samples were irradiated with a 0.5 %CE%BCs pulse of 20 MeV electrons, yielding dose rates of 1E9 to 1E11 rad/s. We applied variable potentials up to 2 kV across the samples and measured the prompt conduction current. Details of the experimental apparatus and analysis are reported in this report on prompt RIC in Teflon.

  10. VALIDATION OF A THERMAL CONDUCTIVITY MEASUREMENT SYSTEM FOR FUEL COMPACTS

    SciTech Connect

    Jeff Phillips; Colby Jensen; Changhu Xing; Heng Ban

    2011-03-01

    A high temperature guarded-comparative-longitudinal heat flow measurement system has been built to measure the thermal conductivity of a composite nuclear fuel compact. It is a steady-state measurement device designed to operate over a temperature range of 300 K to 1200 K. No existing apparatus is currently available for obtaining the thermal conductivity of the composite fuel in a non-destructive manner due to the compact’s unique geometry and composite nature. The current system design has been adapted from ASTM E 1225. As a way to simplify the design and operation of the system, it uses a unique radiative heat sink to conduct heat away from the sample column. A finite element analysis was performed on the measurement system to analyze the associated error for various operating conditions. Optimal operational conditions have been discovered through this analysis and results are presented. Several materials have been measured by the system and results are presented for stainless steel 304, inconel 625, and 99.95% pure iron covering a range of thermal conductivities of 10 W/m*K to 70 W/m*K. A comparison of the results has been made to data from existing literature.

  11. Simultaneous specific heat and thermal conductivity measurement of individual nanostructures

    NASA Astrophysics Data System (ADS)

    Zheng, Jianlin; Wingert, Matthew C.; Moon, Jaeyun; Chen, Renkun

    2016-08-01

    Fundamental phonon transport properties in semiconductor nanostructures are important for their applications in energy conversion and storage, such as thermoelectrics and photovoltaics. Thermal conductivity measurements of semiconductor nanostructures have been extensively pursued and have enhanced our understanding of phonon transport physics. Specific heat of individual nanostructures, despite being an important thermophysical parameter that reflects the thermodynamics of solids, has remained difficult to characterize. Prior measurements were limited to ensembles of nanostructures in which coupling and sample inhomogeneity could play a role. Herein we report the first simultaneous specific heat and thermal conductivity measurements of individual rod-like nanostructures such as nanowires and nanofibers. This technique is demonstrated by measuring the specific heat and thermal conductivity of single ˜600-700 nm diameter Nylon-11 nanofibers (NFs). The results show that the thermal conductivity of the NF is increased by 50% over the bulk value, while the specific heat of the NFs exhibits bulk-like behavior. We find that the thermal diffusivity obtained from the measurement, which is related to the phonon mean free path (MFP), decreases with temperature, indicating that the intrinsic phonon Umklapp scattering plays a role in the NFs. This platform can also be applied to one- and two- dimensional semiconductor nanostructures to probe size effects on the phonon spectra and other transport physics.

  12. Simple uniaxial pressure device for ac-susceptibility measurements suitable for closed cycle refrigerator system.

    PubMed

    Arumugam, S; Manivannan, N; Murugeswari, A

    2007-06-01

    A simple design of the uniaxial pressure device for the measurement of ac-susceptibility at low temperatures using closed cycle refrigerator system is presented for the first time. This device consists of disc micrometer, spring holder attachment, uniaxial pressure cell, and the ac-susceptibility coil wound on stycast bobbin. It can work under pressure till 0.5 GPa and at the temperature range of 30-300 K. The performance of the system at ambient pressure is tested and calibrated with standard paramagnetic salts [Gd(2)O(3), Er(2)O(3), and Fe(NH(4)SO(4))(2)6H(2)O], Fe(3)O(4), Gd metal, Dy metal, superconductor (YBa(2)Cu(3)O(7)), manganite (La(1.85)Ba(0.15)MnO(3)), and spin glass material (Pr(0.8)Sr(0.2)MnO(3)). The performance of the uniaxial pressure device is demonstrated by investigating the uniaxial pressure dependence of La(1.85)Ba(0.15)MnO(3) single crystal with P||c axis. The Curie temperature (T(c)) decreases as a function of pressure with P||c axis (dT(c)dP(||c axis)=-11.65 KGPa) up to 46 MPa. The design is simple, is user friendly, and does not require pressure calibration. Measurement can even be made on thin and small size oriented crystals. The failure of the coil is remote under uniaxial pressure. The present setup can be used as a multipurpose uniaxial pressure device for the measurement of Hall effect and thermoelectric power with a small modification in the pressure cell.

  13. Simple uniaxial pressure device for ac-susceptibility measurements suitable for closed cycle refrigerator system

    NASA Astrophysics Data System (ADS)

    Arumugam, S.; Manivannan, N.; Murugeswari, A.

    2007-06-01

    A simple design of the uniaxial pressure device for the measurement of ac-susceptibility at low temperatures using closed cycle refrigerator system is presented for the first time. This device consists of disc micrometer, spring holder attachment, uniaxial pressure cell, and the ac-susceptibility coil wound on stycast bobbin. It can work under pressure till 0.5GPa and at the temperature range of 30-300K. The performance of the system at ambient pressure is tested and calibrated with standard paramagnetic salts [Gd2O3, Er2O3, and Fe(NH4SO4)26H2O], Fe3O4, Gd metal, Dy metal, superconductor (YBa2Cu3O7), manganite (La1.85Ba0.15MnO3), and spin glass material (Pr0.8Sr0.2MnO3). The performance of the uniaxial pressure device is demonstrated by investigating the uniaxial pressure dependence of La1.85Ba0.15MnO3 single crystal with P ‖c axis. The Curie temperature (Tc) decreases as a function of pressure with P ‖c axis (dTc/dP‖caxis=-11.65K/GPa) up to 46MPa. The design is simple, is user friendly, and does not require pressure calibration. Measurement can even be made on thin and small size oriented crystals. The failure of the coil is remote under uniaxial pressure. The present setup can be used as a multipurpose uniaxial pressure device for the measurement of Hall effect and thermoelectric power with a small modification in the pressure cell.

  14. Measurement of the anisotropic thermal conductivity of the porcine cornea.

    PubMed

    Barton, Michael D; Trembly, B Stuart

    2013-10-01

    Accurate thermal models for the cornea of the eye support the development of thermal techniques for reshaping the cornea and other scientific purposes. Heat transfer in the cornea must be quantified accurately so that a thermal treatment does not destroy the endothelial layer, which cannot regenerate, and yet is responsible for maintaining corneal transparency. We developed a custom apparatus to measure the thermal conductivity of ex vivo porcine corneas perpendicular to the surface and applied a commercial apparatus to measure thermal conductivity parallel to the surface. We found that corneal thermal conductivity is 14% anisotropic at the normal state of corneal hydration. Small numbers of ex vivo feline and human corneas had a thermal conductivity perpendicular to the surface that was indistinguishable from the porcine corneas. Aqueous humor from ex vivo porcine, feline, and human eyes had a thermal conductivity nearly equal to that of water. Including the anisotropy of corneal thermal conductivity will improve the predictive power of thermal models of the eye.

  15. DC and AC Electric Field Measurements by Spin-Plane Double Probes Onboard MMS

    NASA Astrophysics Data System (ADS)

    Lindqvist, P. A.; Marklund, G. T.; Khotyaintsev, Y. V.; Ergun, R. E.; Goodrich, K.; Torbert, R. B.; Argall, M. R.; Nakamura, R.

    2015-12-01

    The four spacecraft of the NASA Magnetospheric Multiscale mission (MMS) were launched on 12 March 2015 into a 1.2 x 12 Re equatorial orbit to study energy conversion processes in Earth's magnetosphere. After a 5-month commissioning period the first scientific phase starts on 1 September as the orbit enters the dusk magnetopause region. The Spin-plane Double Probe electric field instrument (SDP), part of the electric and magnetic fields instrument suite FIELDS, measures the electric field in the range 0.3 - 500 mV/m with a continuous time resolution up to 8192 samples/s. The instrument features adjustable bias currents and guard voltages to optimize the measurement performance. SDP also measures the spacecraft potential, which can be controlled by the Active Spacecraft Potential Control (ASPOC) ion emitter, and under certain conditions can be used to determine plasma density. We present observations of DC and AC electric fields in different plasma regions covered by MMS since launch including the night side flow braking region, reconnection regions at the dusk and dayside magnetopause, and in the magnetosheath. We compare the electric field measurements by SDP to other, independent determinations of the electric field, in particular by the Electron Drift Instrument (EDI), in order to assess the accuracy of the electric field measurement under different plasma conditions. We also study the influence of the currents emitted by ASPOC and EDI on the SDP measurements.

  16. The investigation of dielectric properties and ac conductivity of new ceramic diphosphate Ag0.6Na0.4FeP2O7 using impedance spectroscopy method

    NASA Astrophysics Data System (ADS)

    Nasri, S.; Megdiche, M.; Gargouri, M.

    2016-10-01

    In this paper, Ag0.6Na0.4FeP2O7 has been synthesized by solid state reaction method. The ceramic compound was characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), vibrational spectroscopy and impedance measurements. In fact, the investigated sample has shown single phase type monoclinic structure with P21/C space group. The frequency-dependent electrical data are analyzed in the frame-work of conductivity and electric modulus formalisms. The real and imaginary parts of complex impedance are well fitted to equivalent circuit model based on the Z-View-software. Besides, the observed frequency dependence of conductivity is found to obey Jonscher's universal law. The temperature dependence of both ac conductivity and the parameter s is reasonably well interpreted by the correlated barrier hopping (CBH). The theoretical fitting between the proposed model and the experimental data showed good agreement. The contribution of single polaron and bipolaron hopping to a.c. conductivity in present compound is also studied. The ionic conductivity is discussed on the basis of the structural characteristics of the sample.

  17. Aqueous solubilities of phenol derivatives by conductivity measurements

    SciTech Connect

    Achard, C.; Jaoui, M.; Schwing, M.; Rogalski, M.

    1996-05-01

    The aqueous solubilities of five chlorophenols and three nitrophenols were measured by conductimetry at temperatures between 15 and 48C. The solubilities of 2-chlorophenol, 4-chlorophenol, 2,4-dichlorophenol, 2,4,6-trichlorophenol, pentachlorophenol, 2-nitrophenol, 4-nitrophenol, and 2,4-dinitrophenol were studied. Automatic conductivity measurements allow the determination of the solute concentration and, hence, the determination of the solubility. Emulsion formation can also be followed. Results obtained are in good agreement with literature values.

  18. Surface Roughness Influence on Eddy Current Electrical Conductivity Measurements

    DTIC Science & Technology

    2003-01-01

    presented on shot peened pure ( C11000 ) copper , in which the effect is particularly stro n g and readily measurable because of the low penetration depth...electri- cal conductivity measurements were carried out on each fully relaxed shot peened copper specimen over a wide frequency range from 1 kHz to...residual stress is created over a shallow surface layer. Shot peening is performed on a wide range of materials, including gas turbine engine components

  19. Measurement of soil hydraulic conductivity in relation with vegetation

    NASA Astrophysics Data System (ADS)

    Chen, Xi; Cheng, Qinbo

    2010-05-01

    Hydraulic conductivity is a key parameter which influences hydrological processes of infiltration, surface and subsurface runoff. Vegetation alters surface characteristics (e.g., surface roughness, litter absorption) or subsurface characteristics (e.g. hydraulic conductivity). Field infiltration experiment of a single ring permeameter is widely used for measuring soil hydraulic conductivity. Measurement equipment is a simple single-ring falling head permeameter which consists of a hollow cylinder that is simply inserted into the top soil. An optimization method on the basis of objective of minimum error between the measured and simulated water depths in the single-ring is developed for determination of the soil hydraulic parameters. Using the single ring permeameter, we measured saturated hydraulic conductivities (Ks) of the red loam soil with and without vegetation covers on five hillslopes at Taoyuan Agro-Ecology Experimental Station, Hunan Province of China. For the measurement plots without vegetation roots, Ks value of the soil at 25cm depth is much smaller than that of surface soil (1.52×10-4 vs. 1.10×10-5 m/s). For the measurement plots with vegetation cover, plant roots significantly increase Ks of the lower layer soil but this increase is not significant for the shallow soil. Moreover, influences of vegetation root on Ks depend on vegetation species and ages. Ks value of the Camellia is about three times larger than that of seeding of Camphor (2.62×10-4 vs. 9.82×10-5 m/s). Ks value of the matured Camellia is 2.72×10-4 m/s while Ks value of the young Camellia is only 2.17×10-4 m/s. Key words: single ring permeameter; soil hydraulic conductivity; vegetation

  20. Measurement of Electrical Conductivity for a Biomass Fire

    PubMed Central

    Mphale, Kgakgamatso; Heron, Mal

    2008-01-01

    A controlled fire burner was constructed where various natural vegetation species could be used as fuel. The burner was equipped with thermocouples to measure fuel surface temperature and used as a cavity for microwaves with a laboratory quality 2-port vector network analyzer to determine electrical conductivity from S-parameters. Electrical conductivity for vegetation material flames is important for numerical prediction of flashover in high voltage power transmission faults research. Vegetation fires that burn under high voltage transmission lines reduce flashover voltage by increasing air electrical conductivity and temperature. Analyzer determined electrical conductivity ranged from 0.0058 - 0.0079 mho/m for a fire with a maximum temperature of 1240 K. PMID:19325812

  1. Measurements of prompt radiation induced conductivity of alumina and sapphire

    SciTech Connect

    Hartman, E. Frederick; Zarick, Thomas Andrew; Sheridan, Timothy J.; Preston, Eric F.

    2011-04-01

    We performed measurements of the prompt radiation induced conductivity in thin samples of Alumina and Sapphire at the Little Mountain Medusa LINAC facility in Ogden, UT. Five mil thick samples were irradiated with pulses of 20 MeV electrons, yielding dose rates of 1E7 to 1E9 rad/s. We applied variable potentials up to 1 kV across the samples and measured the prompt conduction current. Analysis rendered prompt conductivity coefficients between 1E10 and 1E9 mho/m/(rad/s), depending on the dose rate and the pulse width for Alumina and 1E7 to 6E7 mho/m/(rad/s) for Sapphire.

  2. Thermal Conductivity of Ionic Liquids: Measurement and Prediction

    NASA Astrophysics Data System (ADS)

    Fröba, A. P.; Rausch, M. H.; Krzeminski, K.; Assenbaum, D.; Wasserscheid, P.; Leipertz, A.

    2010-12-01

    This study reports thermal-conductivity data for a series of [EMIM] (1-ethyl-3-methylimidazolium)-based ionic liquids (ILs) having the anions [NTf2] (bis(trifluoromethylsulfonyl)imide), [OAc] (acetate), [N(CN)2] (dicyanimide), [C(CN)3] (tricyanomethide), [MeOHPO2] (methylphosphonate), [EtSO4] (ethylsulfate), or [OcSO4] (octylsulfate), and in addition for ILs with the [NTf2]-anion having the cations [HMIM] (1-hexyl-3-methylimidazolium), [OMA] (methyltrioctylammonium), or [BBIM] (1,3-dibutylimidazolium). Measurements were performed in the temperature range between (273.15 and 333.15) K by a stationary guarded parallel-plate instrument with a total measurement uncertainty of 3 % ( k = 2). For all ILs, the temperature dependence of the thermal conductivity can well be represented by a linear equation. While for the [NTf2]-based ILs, a slight increase of the thermal conductivity with increasing molar mass of the cation is found at a given temperature, the [EMIM]-based ILs show a pronounced, approximately linear decrease with increasing molar mass of the different probed anions. Based on the experimental data obtained in this study, a simple relationship between the thermal conductivity, molar mass, and density is proposed for the prediction of the thermal-conductivity data of ILs. For this, also densities were measured for [EMIM][OAc], [EMIM][C(CN)3], and [HMIM][NTf2]. The mean absolute percentage deviation of all thermal-conductivity data for ILs found in the literature from the proposed prediction is about 7 %. This result represents a convenient simplification in the acquisition of thermal conductivity information for the enormous amount of structurally different IL cation/anion combinations available.

  3. Fabrication of setup for high temperature thermal conductivity measurement

    NASA Astrophysics Data System (ADS)

    Patel, Ashutosh; Pandey, Sudhir K.

    2017-01-01

    In this work, we report the fabrication of an experimental setup for high temperature thermal conductivity (κ) measurement. It can characterize samples with various dimensions and shapes. Steady state based axial heat flow technique is used for κ measurement. Heat loss is measured using parallel thermal conductance technique. Simple design, lightweight, and small size sample holder is developed by using a thin heater and limited components. Low heat loss value is achieved by using very low thermal conductive insulator block with small cross-sectional area. Power delivered to the heater is measured accurately by using 4-wire technique and for this, the heater is developed with 4 wires. This setup is validated by using Bi0.36Sb1.45Te3, polycrystalline bismuth, gadolinium, and alumina samples. The data obtained for these samples are found to be in good agreement with the reported data. The maximum deviation of 6% in the value κ is observed. This maximum deviation is observed with the gadolinium sample. We also report the thermal conductivity of polycrystalline tellurium from 320 K to 550 K and the nonmonotonous behavior of κ with temperature is observed.

  4. Measuring Impulsivity in Adolescents with Serious Substance and Conduct Problems

    ERIC Educational Resources Information Center

    Thompson, Laetitia L.; Whitmore, Elizabeth A.; Raymond, Kristen M.; Crowley, Thomas J.

    2006-01-01

    Adolescents with substance use and conduct disorders have high rates of aggression and attention deficit hyperactivity disorder (ADHD), all of which have been characterized in part by impulsivity. Developing measures that capture impulsivity behaviorally and correlate with self-reported impulsivity has been difficult. One promising behavioral…

  5. In situ thermal conductivity measurements of Titan's lower atmosphere

    NASA Astrophysics Data System (ADS)

    Hathi, B.; Ball, A. J.; Banaszkiewicz, M.; Daniell, P. M.; Garry, J. R. C.; Hagermann, A.; Leese, M. R.; Lorenz, R. D.; Rosenberg, P. D.; Towner, M. C.; Zarnecki, J. C.

    2008-10-01

    Thermal conductivity measurements, presented in this paper (Fig. 3), were made during the descent of the Huygens probe through the atmosphere of Titan below the altitude of 30 km. The measurements are broadly consistent with reference values derived from the composition, pressure and temperature profiles of the atmosphere; except in narrow altitude regions around 19 km and 11 km, where the measured thermal conductivity is lower than the reference by 1% and 2%, respectively. Only single data point exists at each of the two altitudes mentioned above; if true however, the result supports the case for existence for molecules heavier than nitrogen in these regions (such as: ethane, other primordial noble gases, carbon dioxide, and other hydrocarbon derivatives). The increasing thermal conductivity observed below 7 km altitude could be due to some liquid deposition during the descent; either due to condensation and/or due to passing through layers of fog/cloud containing liquid nitrogen-methane. Thermal conductivity measurements do not allow conclusions to be drawn about how such liquid may have entered the sensor, but an estimate of the cumulative liquid content encountered in the last 7 km is 0.6% by volume of the Titan's atmosphere sampled during descent.

  6. Apparatus measures thermal conductivity of honeycomb-core panels

    NASA Technical Reports Server (NTRS)

    1966-01-01

    Overall thermal conductivity of honeycomb-core panels at elevated temperatures is measured by an apparatus with a heater assembly and a calibrated heat-rate transducer. The apparatus has space between the heater and transducer for insertion of a test panel and insulation.

  7. An AC phase measuring interferometer for measuring dn/dT of fused silica and calcium fluoride at 193 nm

    SciTech Connect

    Shagam, R.N.

    1998-09-01

    A novel method for the measurement of the change in index of refraction vs. temperature (dn/dT) of fused silica and calcium fluoride at the 193 nm wavelength has been developed in support of thermal modeling efforts for the development of 193 nm-based photolithographic exposure tools. The method, based upon grating lateral shear interferometry, uses a transmissive linear grating to divide a 193 nm laser beam into several beam paths by diffraction which propagate through separate identical material samples. One diffracted order passing through one sample overlaps the undiffracted beam from a second sample and forms interference fringes dependent upon the optical path difference between the two samples. Optical phase delay due to an index change from heating one of the samples causes the interference fringes to change sinusoidally with phase. The interferometer also makes use of AC phase measurement techniques through lateral translation of the grating. Results for several samples of fused silica and calcium fluoride are demonstrated.

  8. Comparison of different methods for measuring thermal conductivities

    SciTech Connect

    Hartung, D.; Gather, F.; Klar, P. J.

    2012-06-26

    Two different methods for the measurement of the thermal conductivity have been applied to a glass (borosilicate) bulk sample. The first method was in the steady-state using an arrangement of gold wires on the sample to create a thermal gradient and to measure the temperatures locally. This allows one to calculate the in-plane thermal conductivity of the sample. The same wire arrangement was also used for a 3{omega}-measurement of the direction-independent bulk thermal conductivity. The 3{omega}-approach is based on periodical heating and a frequency dependent analysis of the temperature response. The results of both methods are in good agreement with each other for this isotropic material, if thermal and radiative losses are accounted for. Our results demonstrate that especially in the case of thin-film measurements, finite element analysis has to be applied to correct for heat losses due to geometry and radiation. In this fashion, the wire positions can be optimized in order to minimize measurement errors.

  9. Electrical Conductivity Measurements in Strongly Coupled Metal Plasmas

    NASA Astrophysics Data System (ADS)

    Desilva, Alan; Katsouros, Joseph

    1999-11-01

    We measure the electrical conductivity of strongly coupled plasmas of various metals, including aluminum, iron, copper, and tungsten, in the temperature range 6-30 kK, in a density range from about 1/2 solid density down to about 10-3 times solid density. These plasmas may have coupling parameters (ratio of mean interparticle Coulomb energy to mean kinetic energy) ranging from as high as 50 down to unity. Plasmas are created by rapid vaporization of metal wire in a water bath which act as a tamper. Streak photography serves to determine the growth of the plasma radius in time, allowing determination of mean density. Temperature is deduced from the measured energy input in conjunction with an equation of state from the LANL SESAME database [1], and a brightness temperature may be obtained from radiation measurements. The column resistance is determined from time-resolved voltage and current measurements. Results of conductivity measurements will be shown and compared with the predictions of conductivity theories. 1.SESAME: The Los Alamos National Laboratory Equation of State Database, Report LA-UR-92-3407, ed. S. P. Lyon and J. D. Johnson, Group T-1.

  10. Improved apparatus for measuring hydraulic conductivity at low water content

    USGS Publications Warehouse

    Nimmo, J.R.; Akstin, K.C.; Mello, K.A.

    1992-01-01

    A modification of the steady-state centrifuge method for unsaturated hydraulic conductivity (K) measurement improves the range and adjustability of this method. The modified apparatus allows mechanical adjustment to vary the measured K by a factor of 360. In addition, the use of different flow-regulation ceramic materials can give a total K range covering about six orders of magnitude. The range extension afforded has led to the lowest steady-state K measurement to date, for a sandy soil of the Delhi series (Typic Xeropsamment). -from Authors

  11. Error and uncertainty in Raman thermal conductivity measurements

    DOE PAGES

    Thomas Edwin Beechem; Yates, Luke; Graham, Samuel

    2015-04-22

    We investigated error and uncertainty in Raman thermal conductivity measurements via finite element based numerical simulation of two geometries often employed -- Joule-heating of a wire and laser-heating of a suspended wafer. Using this methodology, the accuracy and precision of the Raman-derived thermal conductivity are shown to depend on (1) assumptions within the analytical model used in the deduction of thermal conductivity, (2) uncertainty in the quantification of heat flux and temperature, and (3) the evolution of thermomechanical stress during testing. Apart from the influence of stress, errors of 5% coupled with uncertainties of ±15% are achievable for most materialsmore » under conditions typical of Raman thermometry experiments. Error can increase to >20%, however, for materials having highly temperature dependent thermal conductivities or, in some materials, when thermomechanical stress develops concurrent with the heating. A dimensionless parameter -- termed the Raman stress factor -- is derived to identify when stress effects will induce large levels of error. Together, the results compare the utility of Raman based conductivity measurements relative to more established techniques while at the same time identifying situations where its use is most efficacious.« less

  12. Error and uncertainty in Raman thermal conductivity measurements

    SciTech Connect

    Thomas Edwin Beechem; Yates, Luke; Graham, Samuel

    2015-04-22

    We investigated error and uncertainty in Raman thermal conductivity measurements via finite element based numerical simulation of two geometries often employed -- Joule-heating of a wire and laser-heating of a suspended wafer. Using this methodology, the accuracy and precision of the Raman-derived thermal conductivity are shown to depend on (1) assumptions within the analytical model used in the deduction of thermal conductivity, (2) uncertainty in the quantification of heat flux and temperature, and (3) the evolution of thermomechanical stress during testing. Apart from the influence of stress, errors of 5% coupled with uncertainties of ±15% are achievable for most materials under conditions typical of Raman thermometry experiments. Error can increase to >20%, however, for materials having highly temperature dependent thermal conductivities or, in some materials, when thermomechanical stress develops concurrent with the heating. A dimensionless parameter -- termed the Raman stress factor -- is derived to identify when stress effects will induce large levels of error. Together, the results compare the utility of Raman based conductivity measurements relative to more established techniques while at the same time identifying situations where its use is most efficacious.

  13. Device and method for measuring thermal conductivity of thin films

    NASA Technical Reports Server (NTRS)

    Amer, Tahani R. (Inventor); Subramanian, Chelakara (Inventor); Upchurch, Billy T. (Inventor); Alderfer, David W. (Inventor); Sealey, Bradley S. (Inventor); Burkett, Jr., Cecil G. (Inventor)

    2001-01-01

    A device and method are provided for measuring the thermal conductivity of rigid or flexible, homogeneous or heterogeneous, thin films between 50 .mu.m and 150 .mu.m thick with relative standard deviations of less than five percent. The specimen is sandwiched between like material, highly conductive upper and lower slabs. Each slab is instrumented with six thermocouples embedded within the slab and flush with their corresponding surfaces. A heat source heats the lower slab and a heat sink cools the upper slab. The heat sink also provides sufficient contact pressure onto the specimen. Testing is performed within a vacuum environment (bell-jar) between 10.sup.-3 to 10.sup.-6 Torr. An anti-radiant shield on the interior surface of the bell-jar is used to avoid radiation heat losses. Insulation is placed adjacent to the heat source and adjacent to the heat sink to prevent conduction losses. A temperature controlled water circulator circulates water from a constant temperature bath through the heat sink. Fourier's one-dimensional law of heat conduction is the governing equation. Data, including temperatures, are measured with a multi-channel data acquisition system. On-line computer processing is used for thermal conductivity calculations.

  14. Developing Test Apparatus and Measurements of AC Loss of High Temperature Superconductors

    DTIC Science & Technology

    2012-11-01

    superconducting wires can be very effectively reduced in proportion of the number of filaments. The oxygen annealing eliminates the residual coupling losses by...made out of YBCO superconducting wires were studied, confirming the simulation method used to calculate and predict AC loss and hysteretic effects of... oxygen annealing were tested in order to determine their effect on AC loss reduction. Results showed that the AC loss in multifilament

  15. New Thermal Conductivity Measurements of Meteorites: Implications for Asteroid Models

    NASA Astrophysics Data System (ADS)

    Consolmagno, Guy; Opeil, C. P.; Britt, D. T.

    2009-09-01

    We have measured the thermal conductivity at low temperatures (5K to 300 K) of meteorites representing a range of compositions, including the ordinary chondrites Chronstad (H5) and Lumpkin (L6), the enstatite chondrite Abee (E4), the carbonaceous chondrites NWA 5515 (CK4 find) and Cold Bokkeveld (CM2), and the iron meteorite Campo del Cielo (IAB find). All measurements were made using a Quantum Design P670 TTO on samples cut into 0.5 - 1 cm prisms. The iron meteorite conductivity increases roughly linearly from 17 W/mK at 100K to 27 W/mK at 300 K. The conductivities of all the stony samples except Abee appear to be controlled by the inhomogeneous nature of the meteorite fabric, resulting in values that are much lower than those of pure minerals and essentially independent of temperature above 100K. The L and CK sample conductivities above 100 K are both 1.5 W/mK, that of the H is 1.9 W/mK, and that of the CM sample is 0.5 W/mK; by contrast the literature value at 300 K for serpentine is 2.5 W/mK and that of enstatite and olivine is 4.5 to 5 W/mK (comparable to our Abee value). Below 100 K all materials' conductivities drop sharply. These low thermal conductivities will have significant effects on the thermal evolution of asteroids and other small solar system bodies where the rocky component is assumed to be meteoritic. These values would indicate lower thermal inertias, potentially affecting the YORP and Yarkovsky spin/orbital evolution of small meteoroids. However, for most asteroids, thermal inertia is dominated by the dusty nature of the regolith rather than the conductivity of the material itself.

  16. A Comparative Study on Pre-Standardization of Total AC Loss Measurements for Oxide-Superconducting Tapes in Japan

    NASA Astrophysics Data System (ADS)

    Funaki, Kazuo; Tanaka, Yasuzo; Osamura, Kozo

    2006-06-01

    We have been considering about standard methods to estimate total AC loss in oxide-superconducting tapes under practical electromagnetic conditions in future power devices. We adopt 4 candidates of the standard methods to measure the AC loss in superconducting wires exposed to AC transverse magnetic field and alternating transport current. We also introduce two pickup coil methods for comparative references of external magnetic field loss. The specimen is a Bi-2223 Ag-alloy-sheathed multifilamentary tape without twisting. 60-100 mm short pieces of specimen were cut from a terminal of a 50 m long specimen for 4 in 6 methods. A double-layer non-inductive coiled specimen was also prepared from the long specimen for the other 2 methods. The scattering in AC loss property among the short specimens prepared is less than 1% in the perpendicular field with the amplitude from 0.01 to 0.1 T at 10 Hz. The scattering in repeated measurements of the loss during 3 heat cycles is within 2-3%, which almost corresponds to that of the critical current in the long specimen. We processed the results measured by each method for the external field loss and total AC loss, summarized dispersion among the observed results of all methods and discussed about the candidates of the standard methods.

  17. Assembly for electrical conductivity measurements in the piston cylinder device

    DOEpatents

    Watson, Heather Christine [Dublin, CA; Roberts, Jeffrey James [Livermore, CA

    2012-06-05

    An assembly apparatus for measurement of electrical conductivity or other properties of a sample in a piston cylinder device wherein pressure and heat are applied to the sample by the piston cylinder device. The assembly apparatus includes a body, a first electrode in the body, the first electrode operatively connected to the sample, a first electrical conductor connected to the first electrode, a washer constructed of a hard conducting material, the washer surrounding the first electrical conductor in the body, a second electrode in the body, the second electrode operatively connected to the sample, and a second electrical conductor connected to the second electrode.

  18. Method of simultaneous measurement of radiative and lattice thermal conductivity.

    NASA Technical Reports Server (NTRS)

    Schatz, J. F.; Simmons, G.

    1972-01-01

    A new technique of high-temperature thermal-conductivity measurement is described. A CO2 gas laser is used to generate a low-frequency temperature wave at one face of a small disk-shaped sample, and an infrared detector views the opposite face to detect the phase of the emerging radiation. A mathematical expression is derived which enables phase data at several frequencies to be used for the simultaneous determination of thermal diffusivity and mean extinction coefficient. Lattice and radiative thermal conductivities are then calculated. Test results for sintered aluminum oxide at temperatures from 530 to 1924 K are within the range of error of previously existing data.

  19. System to Measure Thermal Conductivity and Seebeck Coefficient for Thermoelectrics

    NASA Technical Reports Server (NTRS)

    Kim, Hyun-Jung; Skuza, Jonathan R.; Park, Yeonjoon; King, Glen C.; Choi, Sang H.; Nagavalli, Anita

    2012-01-01

    The Seebeck coefficient, when combined with thermal and electrical conductivity, is an essential property measurement for evaluating the potential performance of novel thermoelectric materials. However, there is some question as to which measurement technique(s) provides the most accurate determination of the Seebeck coefficient at elevated temperatures. This has led to the implementation of nonstandardized practices that have further complicated the confirmation of reported high ZT materials. The major objective of the procedure described is for the simultaneous measurement of the Seebeck coefficient and thermal diffusivity within a given temperature range. These thermoelectric measurements must be precise, accurate, and reproducible to ensure meaningful interlaboratory comparison of data. The custom-built thermal characterization system described in this NASA-TM is specifically designed to measure the inplane thermal diffusivity, and the Seebeck coefficient for materials in the ranging from 73 K through 373 K.

  20. Measurement of Thermal Conductivity of Liquids at High Temperature

    NASA Astrophysics Data System (ADS)

    Schick, V.; Remy, B.; Degiovanni, A.; Demeurie, F.; Meulemans, J.; Lombard, P.

    2012-11-01

    The goal purchased in this paper is to implement a pulse method to measure the thermal conductivity of liquid silica glass above 1200°C until 1600°C. A heat flux stimulation controlled in energy and in time is generated on the front face of an experimental cell. The temperature rise is measured on the rear face of this cell face by using a fast cooled infrared camera. The choice of the measurement cell geometry is fundamental to be able to estimate at the same time the thermal diffusivity and the specific heat of the liquid by an inverse technique. The parameters estimation problem takes into account the optimization of the cell wall thickness. The theoretical model used for the inversion takes into account the coupled heat transfer modes (conduction, convection and radiation) that can occur during the experiment, particularly the thermal conductive short-cut through metallic lateral walls of the cell and radiative transfer within the semi-transparent and participating medium. First measurements are performed on a cell filled with water at ambient temperature in order to validate the parameters estimation procedure.

  1. Thermal conductivity measurements of particulate materials under Martian conditions

    NASA Technical Reports Server (NTRS)

    Presley, M. A.; Christensen, P. R.

    1993-01-01

    The mean particle diameter of surficial units on Mars has been approximated by applying thermal inertia determinations from the Mariner 9 Infrared Radiometer and the Viking Infrared Thermal Mapper data together with thermal conductivity measurement. Several studies have used this approximation to characterize surficial units and infer their nature and possible origin. Such interpretations are possible because previous measurements of the thermal conductivity of particulate materials have shown that particle size significantly affects thermal conductivity under martian atmospheric pressures. The transfer of thermal energy due to collisions of gas molecules is the predominant mechanism of thermal conductivity in porous systems for gas pressures above about 0.01 torr. At martian atmospheric pressures the mean free path of the gas molecules becomes greater than the effective distance over which conduction takes place between the particles. Gas particles are then more likely to collide with the solid particles than they are with each other. The average heat transfer distance between particles, which is related to particle size, shape and packing, thus determines how fast heat will flow through a particulate material.The derived one-to-one correspondence of thermal inertia to mean particle diameter implies a certain homogeneity in the materials analyzed. Yet the samples used were often characterized by fairly wide ranges of particle sizes with little information about the possible distribution of sizes within those ranges. Interpretation of thermal inertia data is further limited by the lack of data on other effects on the interparticle spacing relative to particle size, such as particle shape, bimodal or polymodal mixtures of grain sizes and formation of salt cements between grains. To address these limitations and to provide a more comprehensive set of thermal conductivities vs. particle size a linear heat source apparatus, similar to that of Cremers, was assembled to

  2. AC conductivity and dielectric relaxation in Ba(Sm 1/2Nb 1/2)O 3 ceramic

    NASA Astrophysics Data System (ADS)

    Kumar, Pritam; Singh, B. P.; Sinha, T. P.; Singh, N. K.

    2011-01-01

    The complex perovskite oxide a barium samarium niobate (BSN) synthesized by solid-state reaction technique has single phase with cubic structure. The scanning electron micrograph of the sample shows the average grain size of BSN∼1.22 μm. The field dependence of dielectric response and loss tangent were measured in the temperature range from 323 to 463 K and in the frequency range from 50 Hz to 1 MHz. The complex plane impedance plots show the grain boundary contribution for higher value of dielectric constant in the low frequency region. An analysis of the dielectric constant ( ε‧) and loss tangent (tan δ) with frequency was performed assuming a distribution of relaxation times as confirmed by the scaling behaviour of electric modulus spectra. The low frequency dielectric dispersion corresponds to DC conductivity. The logarithmic angular frequency dependence of the loss peak is found to obey the Arrhenius law with an activation energy of 0.71 eV. The frequency dependence of electrical data is also analyzed in the framework of conductivity and electric modulus formalisms. Both these formalisms show qualitative similarities in relaxation times. The scaling behaviour of imaginary part of electric modulus M″ and dielectric loss spectra suggest that the relaxation describes the same mechanism at various temperatures in BSN. All the observations indicate the polydispersive relaxation in BSN.

  3. Thermal conductivity measurements of proton-heated warm dense matter

    NASA Astrophysics Data System (ADS)

    McKelvey, A.; Fernandez-Panella, A.; Hua, R.; Kim, J.; King, J.; Sio, H.; McGuffey, C.; Kemp, G. E.; Freeman, R. R.; Beg, F. N.; Shepherd, R.; Ping, Y.

    2015-06-01

    Accurate knowledge of conductivity characteristics in the strongly coupled plasma regime is extremely important for ICF processes such as the onset of hydrodynamic instabilities, thermonuclear burn propagation waves, shell mixing, and efficient x-ray conversion of indirect drive schemes. Recently, an experiment was performed on the Titan laser platform at the Jupiter Laser Facility to measure the thermal conductivity of proton-heated warm dense matter. In the experiment, proton beams generated via target normal sheath acceleration were used to heat bi-layer targets with high-Z front layers and lower-Z back layers. The stopping power of a material is approximately proportional to Z2 so a sharp temperature gradient is established between the two materials. The subsequent thermal conduction from the higher-Z material to the lower-Z was measured with time resolved streaked optical pyrometry (SOP) and Fourier domain interferometry (FDI) of the rear surface. Results will be used to compare predictions from the thermal conduction equation and the Wiedemann-Franz Law in the warm dense matter regime. Data from the time resolved diagnostics for Au/Al and Au/C Targets of 20-200 nm thickness will be presented.

  4. Thermal Conductivity Based on Modified Laser Flash Measurement

    NASA Technical Reports Server (NTRS)

    Lin, Bochuan; Ban, Heng; Li, Chao; Scripa, Rosalia N.; Su, Ching-Hua; Lehoczky, Sandor L.

    2005-01-01

    The laser flash method is a standard method for thermal diffusivity measurement. It employs single-pulse heating of one side of a thin specimen and measures the temperature response of the other side. The thermal diffusivity of the specimen can be obtained based on a one-dimensional transient heat transfer analysis. This paper reports the development of a theory that includes a transparent reference layer with known thermal property attached to the back of sample. With the inclusion of heat conduction from the sample to the reference layer in the theoretical analysis, the thermal conductivity and thermal diffusivity of sample can be extracted from the temperature response data. Furthermore, a procedure is established to select two points from the data to calculate these properties. The uncertainty analysis indicates that this method can be used with acceptable levels of uncertainty.

  5. AC Electrical Conduction of Cr-Doped SrTiO3 Thin Films with an Oxygen-Deficient Interface Layer

    NASA Astrophysics Data System (ADS)

    Phan, Bach Thang; Eom, Ki Tae; Lee, Jaichan

    2017-01-01

    The ac electrical conduction of Cr-doped SrTiO3 thin films with an oxygen-deficient interface layer was investigated as a function of temperature and frequency. The Cr-doped SrTiO3 (Cr-STO) thin films with an ultra-thin (˜2 nm) oxygen-deficient layer inserted between the top electrode and the Cr-STO layer exhibited two ac conduction mechanisms, i.e., variable-range hopping and small-polaron hopping conduction, accompanied by a relaxation process. Since high oxygen deficiency induces large lattice distortion in the depletion layer, the first relaxation process occurs at low frequencies in the thin oxygen depletion layer Cr-SrTiO3-δ , and the corresponding conduction behavior follows the small-polaron tunneling model. In the high frequency range, an additional relaxation process is involved and is associated with the variable-range hopping between the localized states in the band gap of the thick Cr-SrTiO3 layer.

  6. Measurement and modeling of unsaturated hydraulic conductivity: Chapter 21

    USGS Publications Warehouse

    Perkins, Kim S.; Elango, Lakshmanan

    2011-01-01

    This chapter will discuss, by way of examples, various techniques used to measure and model hydraulic conductivity as a function of water content, K(). The parameters that describe the K() curve obtained by different methods are used directly in Richards’ equation-based numerical models, which have some degree of sensitivity to those parameters. This chapter will explore the complications of using laboratory measured or estimated properties for field scale investigations to shed light on how adequately the processes are represented. Additionally, some more recent concepts for representing unsaturated-zone flow processes will be discussed.

  7. The role of probe oxide in local surface conductivity measurements

    SciTech Connect

    Barnett, C. J.; Kryvchenkova, O.; Wilson, L. S. J.; Maffeis, T. G. G.; Cobley, R. J.; Kalna, K.

    2015-05-07

    Local probe methods can be used to measure nanoscale surface conductivity, but some techniques including nanoscale four point probe rely on at least two of the probes forming the same low resistivity non-rectifying contact to the sample. Here, the role of probe shank oxide has been examined by carrying out contact and non-contact I V measurements on GaAs when the probe oxide has been controllably reduced, both experimentally and in simulation. In contact, the barrier height is pinned but the barrier shape changes with probe shank oxide dimensions. In non-contact measurements, the oxide modifies the electrostatic interaction inducing a quantum dot that alters the tunneling behavior. For both, the contact resistance change is dependent on polarity, which violates the assumption required for four point probe to remove probe contact resistance from the measured conductivity. This has implications for all nanoscale surface probe measurements and macroscopic four point probe, both in air and vacuum, where the role of probe oxide contamination is not well understood.

  8. Heat conduction nanocalorimeter for pl-scale single cell measurements

    NASA Astrophysics Data System (ADS)

    Johannessen, E. A.; Weaver, J. M. R.; Cobbold, P. H.; Cooper, J. M.

    2002-03-01

    An ultrasensitive nanocalorimeter for use with pl-scale biological samples using silicon microfabrication technology has been developed in which a 720 pl reaction vessel, a calibration heater, and a thermoelectric transducer of 125 μK sensitivity were integrated into a single multilayer thin-film configuration. The resolution of the system ranged from 10 to 25 nW depending on the heat capacity, conductance and power density of the samples studied. The device has been used in heat conduction measurements of the energy released from the enzyme catalyzed hydrolysis of hydrogen peroxide using purified catalase, and for the determination of the catalase activity within a single mouse hepatocyte. The nanocalorimeter has the potential for integration in a high-density array format, where the change in temperature from ultralow volume cellular assays could be used as a generic analytical tool for high throughput screening of bioactive compounds.

  9. Thermal conductivity and emissivity measurements of uranium carbides

    NASA Astrophysics Data System (ADS)

    Corradetti, S.; Manzolaro, M.; Andrighetto, A.; Zanonato, P.; Tusseau-Nenez, S.

    2015-10-01

    Thermal conductivity and emissivity measurements on different types of uranium carbide are presented, in the context of the ActiLab Work Package in ENSAR, a project within the 7th Framework Program of the European Commission. Two specific techniques were used to carry out the measurements, both taking place in a laboratory dedicated to the research and development of materials for the SPES (Selective Production of Exotic Species) target. In the case of thermal conductivity, estimation of the dependence of this property on temperature was obtained using the inverse parameter estimation method, taking as a reference temperature and emissivity measurements. Emissivity at different temperatures was obtained for several types of uranium carbide using a dual frequency infrared pyrometer. Differences between the analyzed materials are discussed according to their compositional and microstructural properties. The obtainment of this type of information can help to carefully design materials to be capable of working under extreme conditions in next-generation ISOL (Isotope Separation On-Line) facilities for the generation of radioactive ion beams.

  10. Evaluation of DC electric field distribution of PPLP specimen based on the measurement of electrical conductivity in LN2

    NASA Astrophysics Data System (ADS)

    Hwang, Jae-Sang; Seong, Jae-Kyu; Shin, Woo-Ju; Lee, Jong-Geon; Cho, Jeon-Wook; Ryoo, Hee-Suk; Lee, Bang-Wook

    2013-11-01

    High temperature superconducting (HTS) cable has been paid much attention due to its high efficiency and high current transportation capability, and it is also regarded as eco-friendly power cable for the next generation. Especially for DC HTS cable, it has more sustainable and stable properties compared to AC HTS cable due to the absence of AC loss in DC HTS cable. Recently, DC HTS cable has been investigated competitively all over the world, and one of the key components of DC HTS cable to be developed is a cable joint box considering HVDC environment. In order to achieve the optimum insulation design of the joint box, analysis of DC electric field distribution of the joint box is a fundamental process to develop DC HTS cable. Generally, AC electric field distribution depends on relative permittivity of dielectric materials but in case of DC, electrical conductivity of dielectric material is a dominant factor which determines electric field distribution. In this study, in order to evaluate DC electric field characteristics of the joint box for DC HTS cable, polypropylene laminated paper (PPLP) specimen has been prepared and its DC electric field distribution was analyzed based on the measurement of electrical conductivity of PPLP in liquid nitrogen (LN2). Electrical conductivity of PPLP in LN2 has not been reported yet but it should be measured for DC electric field analysis. The experimental works for measuring electrical conductivity of PPLP in LN2 were presented in this paper. Based on the experimental works, DC electric field distribution of PPLP specimen was fully analyzed considering the steady state and the transient state of DC. Consequently, it was possible to determine the electric field distribution characteristics considering different DC applying stages including DC switching on, DC switching off and polarity reversal conditions.

  11. Using Atmospheric Measurements of Carbonyl Sulfide to Constrain Conductance

    NASA Astrophysics Data System (ADS)

    Berry, J. A.; Campbell, J. E.; Baker, I. T.; Montzka, S. A.; Kawa, S. R.

    2009-12-01

    Stomata play a key role in controlling the carbon and water cycles and can influence regional climate. We currently use empirical models calibrated from laboratory experiments to model stomata in natural canopies, and we test these models against measurements of latent heat and carbon dioxide fluxes from forests and fields. In many systems net radiation becomes a dominant control on transpiration, and the measured fluxes are actually rather insensitive to conductance providing a poor test of the models. Nevertheless, stomata and especially the responses of stomata to increasing CO2 can have subtle effects the surface energy budget in these densely vegetated systems - with significant impacts on climate. This is the so called “physiological forcing”. We are exploring the use of carbonyl sulfide, OCS an atmospheric trace gas that is taken up through the stomata, as reporter of stomatal conductance at the ecosystem to regional scale. Background concentrations of OCS in the atmosphere are relatively stable; it is produced over the oceans, and it is consumed over land by leaves and soils. Industrial and biomass burning sources, while locally important, have little impact on the large-scale draw-down of OCS concentration in the atmospheric boundary layer over the continents. Uptake by leaves follows the same path as water out of (and CO2 into) leaves and most of the OCS that enters the leaf is consumed. Hence, measurements of OCS concentration and surface flux could be used to provide an independent estimate of canopy conductances to CO2 and water vapor. Soil uptake of OCS which is generally (0.2-0.4) fraction of the total surface uptake also needs to be quantified.

  12. Thermal conductivity measurements of CH and Be by refraction-enhanced x-ray radiography

    NASA Astrophysics Data System (ADS)

    Ping, Yuan; King, Jim; Landen, Otto; Whitley, Heather; London, Rich; Hamel, Sebastien; Sterne, Phil; Panella, Amalia; Freeman, Rick; Collins, Gilbert

    2015-06-01

    Transport properties of warm dense matter are important for modeling the growth of hydrodynamic instabilities near the fuel-ablator interface in an ICF capsule, which determines the mix level in the fuel and thus is critical for successful ignition. A novel technique, time-resolved refraction-enhanced x-ray radiography, has been developed to study thermal conductivity at an interface. Experiments using OMEGA laser have been carried out for CH/Be targets isochorically heated by x-rays to measure the evolution of the density gradient at the interface due to thermal conduction. The sensitivity of this radiographic technique to discontinuities enabled observation of shock/rarefraction waves propagating away from the interface. The radiographs provide enough constraints on the temperatures, densities and scale lengths in CH and Be, respectively. Preliminary data analysis suggests that the thermal conductivities of CH and Be at near solid density and a few eV temperature are higher than predictions by the commonly used Lee-More model. Detailed analysis and comparison with various models will be presented. The work was performed under the auspices of the U.S. Department of Energy by Lawrence Livermore National Security, LLC, Lawrence Livermore National Laboratory under Contract DE-AC52-07NA27344.

  13. Experimental measurements of the thermal conductivity of ash deposits: Part 1. Measurement technique

    SciTech Connect

    A. L. Robinson; S. G. Buckley; N. Yang; L. L. Baxter

    2000-04-01

    This paper describes a technique developed to make in situ, time-resolved measurements of the effective thermal conductivity of ash deposits formed under conditions that closely replicate those found in the convective pass of a commercial boiler. Since ash deposit thermal conductivity is thought to be strongly dependent on deposit microstructure, the technique is designed to minimize the disturbance of the natural deposit microstructure. Traditional techniques for measuring deposit thermal conductivity generally do not preserve the sample microstructure. Experiments are described that demonstrate the technique, quantify experimental uncertainty, and determine the thermal conductivity of highly porous, unsintered deposits. The average measured conductivity of loose, unsintered deposits is 0.14 {+-} 0.03 W/(m K), approximately midway between rational theoretical limits for deposit thermal conductivity.

  14. Apparent thermal conductivity measurements by an unguarded technique

    NASA Astrophysics Data System (ADS)

    Graves, R. S.; Yarbrough, D. W.; McElroy, D. L.

    An unguarded longitudinal heat flow apparatus for measuring the apparent thermal conductivity (lambda/sub a) of insulations was tested. Heat flow is provided by a horizontal electrically heated Nichrome screen sandwiched between test samples that are bounded by temperature controlled copper plates and 9 cm of mineral fiber insulation. A determinate error analysis shows lambda/sub a/ measurement uncertainty to be less than + or - 1.7% for insulating materials as thin as 3 cm. Three-dimensional thermal modeling indicates negligible error in lambda/sub a/ due to edge loss for insulations up to 7.62 cm thick when the temperature difference across the sample is measured at the screen center. System repeatability and reproducibility were determined to be + or - 0.2%. Differences of lambda/sub a/ results from the screen tester and results from the National Bureau of Standards were 0.1% for a 10-kg/m(3) Calibration Transfer Standard and 0.9% for 127-kg/m(3) fibrous glass board (SRM 1450b). Measurements on fiberglass and rock wool batt insulations showed the dependence of lambda/sub a/ on density, temperature, temperature difference, plate emittance, and heat flow direction. Results obtained for lambda/sub a/ as a function of density at 240C differed by less than 2% from values obtained with a guarded hot plate. It is demonstrated that this simple technique has the accuracy and sensitivity needed for useful lambda/sub a/ measurements on thermal insulating materials.

  15. High-Resolution ac Measurements of the Hall Effect in Organic Field-Effect Transistors

    NASA Astrophysics Data System (ADS)

    Chen, Y.; Yi, H. T.; Podzorov, V.

    2016-03-01

    We describe a high resolving power technique for Hall-effect measurements, efficient in determining Hall mobility and carrier density in organic field-effect transistors and other low-mobility systems. We utilize a small low-frequency ac magnetic field (Brms<0.25 T ) and a phase-sensitive (lock-in) detection of Hall voltage, with the necessary corrections for Faraday induction. This method significantly enhances the signal-to-noise ratio and eliminates the necessity of using high magnetic fields in Hall-effect studies. With the help of this method, we are able to obtain the Hall mobility and carrier density in organic transistors with a mobility as low as μ ˜0.3 cm2 V-1 s-1 by using a compact desktop apparatus and low magnetic fields. We find a good agreement between Hall-effect and electric-field-effect measurements, indicating that, contrary to the common belief, certain organic semiconductors with mobilities below 1 cm2 V-1 s-1 can still exhibit a fully developed, band-semiconductor-like Hall effect, with the Hall mobility and carrier density matching those obtained in longitudinal transistor measurements. This suggests that, even when μ <1 cm2 V-1 s-1 , charges in organic semiconductors can still behave as delocalized coherent carriers. This technique paves the way to ubiquitous Hall-effect studies in a wide range of low-mobility materials and devices, where it is typically very difficult to resolve the Hall effect even in very high dc magnetic fields.

  16. Simultaneous measurements of somatosensory evoked AC and near-DC MEG signals.

    PubMed

    Körber, Rainer; Curio, Gabriel; Hartwig, Stefan; Hilschenz, Ingo; Höfner, Nora; Scheer, Hans-Jürgen; Trahms, Lutz; Voigt, Jens; Burghoff, Martin

    2011-04-01

    Magnetoencephalography measurements of somatosensory evoked brain activity taken inside an extremely magnetically shielded room are reported. The massive low frequency shielding in combination with a high sampling rate enabled the simultaneous observation of AC and near-DC effects. Neuronal activation was achieved by repetitive electrostimulation of the right median nerve above motor threshold using repetition rates from 3 Hz to 12 Hz. Stimulation sequences lasted for 10 s and were interspersed with periods of rest of equal length. The recorded magnetic fields, inferred for the N20m and a sustained near-DC component, revealed mainly dipolar patterns with mutually rotated orientations with angles of rotation of 30° and 75°. At the start of the stimulation we observed a fast rise within 100 ms in the evoked magnetic near-DC fields for which a maximum equivalent current dipole strength of 65 nAm was obtained. The sustained fields decayed by a factor of ∼4 to a lower DC-level B(γ) with a time constant τ of order of seconds. For 12 Hz repetition rate B(γ) was decreased. We suggest that the sustained neuronal activity evoked by repetitive electrostimulation could provide a suitable scheme to realize the direct detection of DC effects of neuronal currents via low field magnetic resonance.

  17. Frequency and voltage dependence dielectric properties, ac electrical conductivity and electric modulus profiles in Al/Co3O4-PVA/p-Si structures

    NASA Astrophysics Data System (ADS)

    Bilkan, Çiğdem; Azizian-Kalandaragh, Yashar; Altındal, Şemsettin; Shokrani-Havigh, Roya

    2016-11-01

    In this research a simple microwave-assisted method have been used for preparation of cobalt oxide nanostructures. The as-prepared sample has been investigated by UV-vis spectroscopy, X-ray diffraction (XRD), scanning electron microscopy (SEM). On the other hand, frequency and voltage dependence of both the real and imaginary parts of dielectric constants (ε‧, ε″) and electric modulus (M‧ and M″), loss tangent (tanδ), and ac electrical conductivityac) values of Al/Co3O4-PVA/p-Si structures were obtained in the wide range of frequency and voltage using capacitance (C) and conductance (G/ω) data at room temperature. The values of ε‧, ε″ and tanδ were found to decrease with increasing frequency almost for each applied bias voltage, but the changes in these parameters become more effective in the depletion region at low frequencies due to the charges at surface states and their relaxation time and polarization effect. While the value of σ is almost constant at low frequency, increases almost as exponentially at high frequency which are corresponding to σdc and σac, respectively. The M‧ and M″ have low values at low frequencies region and then an increase with frequency due to short-range mobility of charge carriers. While the value of M‧ increase with increasing frequency, the value of M″ shows two peak and the peaks positions shifts to higher frequency with increasing applied voltage due to the decrease of the polarization and Nss effects with increasing frequency.

  18. Electrical Conductivity Measurements in Strongly Coupled Metal Plasmas

    NASA Astrophysics Data System (ADS)

    Desilva, Alan

    1998-11-01

    The coupling parameter Γ=e^2/akT, where a is the mean ion-ion separation, expresses the ratio of the mean potential energy of ions in a plasma to their mean kinetic energy. Plasma is said to be strongly coupled when Γ is greater than unity. Transport properties of strongly coupled plasmas are of interest in the study of the structure of dense astrophysical objects and gaseous planetary interiors, as well as in arcs and laser-produced plasmas. We are attempting to measure the electrical conductivity of strongly coupled metal plasmas (copper, tungsten and aluminum) in the temperature range 8-30 kK, in a density range from about 1/2 solid density down to about 10-3 times solid density. They may have coupling parameters Γ ranging from as high as 100 down to unity Plasmas are created by rapid vaporization of metal wire in a glass capillary or in a water bath which act as a tamper, slowing the expansion rate. The effect of the tamper is to force the interior pressure of the plasma to be fairly uniform. Streak photography serves to determine the growth of the plasma radius in time, allowing determination of mean density. Temperature is deduced from the measured energy input in conjunction with an equation of state from the LANL sesame database(SESAME: The Los Alamos National Laboratory Equation of State Database, Report No. LA-UR-92-3407, Ed. S. P. Lyon and J. D. Johnson, Group T-1 (unpublished)), and a brightness temperature may be obtained from radiation measurements. The column resistance is simply determined from time-resolved voltage and current measurements. For temperatures less than about 14,000K, as density decreases from the highest values measured, the conductivity falls roughly as the cube of density, reaches a minimum, and subsequently rises to approach the Spitzer prediction at low density. The rate of change of conductivity with density becomes less rapid as temperature increases, and the minimum becomes less pronounced, disappearing altogether above

  19. DNA sequencing using electrical conductance measurements of a DNA polymerase

    NASA Astrophysics Data System (ADS)

    Chen, Yu-Shiun; Lee, Chia-Hui; Hung, Meng-Yen; Pan, Hsu-An; Chiou, Jin-Chern; Huang, G. Steven

    2013-06-01

    The development of personalized medicine--in which medical treatment is customized to an individual on the basis of genetic information--requires techniques that can sequence DNA quickly and cheaply. Single-molecule sequencing technologies, such as nanopores, can potentially be used to sequence long strands of DNA without labels or amplification, but a viable technique has yet to be established. Here, we show that single DNA molecules can be sequenced by monitoring the electrical conductance of a phi29 DNA polymerase as it incorporates unlabelled nucleotides into a template strand of DNA. The conductance of the polymerase is measured by attaching it to a protein transistor that consists of an antibody molecule (immunoglobulin G) bound to two gold nanoparticles, which are in turn connected to source and drain electrodes. The electrical conductance of the DNA polymerase exhibits well-separated plateaux that are ~3 pA in height. Each plateau corresponds to an individual base and is formed at a rate of ~22 nucleotides per second. Additional spikes appear on top of the plateaux and can be used to discriminate between the four different nucleotides. We also show that the sequencing platform works with a variety of DNA polymerases and can sequence difficult templates such as homopolymers.

  20. Computerized measurement of pulmonary conductance and elastic recoil.

    PubMed

    Colebatch, H J; Nail, B S; Ng, C K

    1978-04-01

    A system devloped for on-line measurement of transpulmonary pressure, gas flow at the mouth, change in expired volume and plethysmograph volume uses a minicomputer to control a multiplexed analog to digital converter. The computer identified samples as static or dynamic values by monitoring a voltage activating a solenoid valve, used to close the airway. Analysis of these samples by other task-specific programs yielded the static deflation pressure-volume (PV) curve, the conductance-recoil pressure, GL-Pst(L), relationship and the maximum expiratory flow-volume (MEFV) curve; the MEF-Pst(L) curve and conductance upstream from the equal pressure point were derived. The PV relationship was represented by a fourth-order polynomial and the GL-Pst(L) relationship by linear regression. In 11 subjects the results obtained using on-line data collection, compared with manual analysis of oscillograph recordings, showed small differences in static compliance and in the maximum Pst(L); but overall the two methods showed excellent agreement. Besides advantages of speed and objectivity, this system facilitates a more rigorous analytical treatment of elastic recoil and conductance.

  1. Quantitative measurements of root water uptake and root hydraulic conductivities

    NASA Astrophysics Data System (ADS)

    Zarebanadkouki, Mohsen; Javaux, Mathieu; Meunier, Felicien; Couvreur, Valentin; Carminati, Andrea

    2016-04-01

    How is root water uptake distributed along the root system and what root properties control this distribution? Here we present a method to: 1) measure root water uptake and 2) inversely estimate the root hydraulic conductivities. The experimental method consists in using neutron radiography to trace deuterated water (D2O) in soil and roots. The method was applied to lupines grown aluminium containers filled with a sandy soil. When the lupines were 4 weeks old, D2O was locally injected in a selected soil regions and its transport was monitored in soil and roots using time-series neutron radiography. By image processing, we quantified the concentration of D2O in soil and roots. We simulated the transport of D2O into roots using a diffusion-convection numerical model. The diffusivity of the roots tissue was inversely estimated by simulating the transport of D2O into the roots during night. The convective fluxes (i.e. root water uptake) were inversely estimating by fitting the experiments during day, when plants were transpiring, and assuming that root diffusivity did not change. The results showed that root water uptake was not uniform along the roots. Water uptake was higher at the proximal parts of the lateral roots and it decreased by a factor of 10 towards the distal parts. We used the data of water fluxes to inversely estimate the profile of hydraulic conductivities along the roots of transpiring plants growing in soil. The water fluxes in the lupine roots were simulated using the Hydraulic Tree Model by Doussan et al. (1998). The fitting parameters to be adjusted were the radial and axial hydraulic conductivities of the roots. The results showed that by using the root architectural model of Doussan et al. (1998) and detailed information of water fluxes into different root segments we could estimate the profile of hydraulic conductivities along the roots. We also found that: 1) in a tap-rooted plant like lupine water is mostly taken up by lateral roots; (2) water

  2. Measurement of the direct C P -violating parameter AC P in the decay D+→K-π+π+

    NASA Astrophysics Data System (ADS)

    Abazov, V. M.; Abbott, B.; Acharya, B. S.; Adams, M.; Adams, T.; Agnew, J. P.; Alexeev, G. D.; Alkhazov, G.; Alton, A.; Askew, A.; Atkins, S.; Augsten, K.; Avila, C.; Badaud, F.; Bagby, L.; Baldin, B.; Bandurin, D. V.; Banerjee, S.; Barberis, E.; Baringer, P.; Bartlett, J. F.; Bassler, U.; Bazterra, V.; Bean, A.; Begalli, M.; Bellantoni, L.; Beri, S. B.; Bernardi, G.; Bernhard, R.; Bertram, I.; Besançon, M.; Beuselinck, R.; Bhat, P. C.; Bhatia, S.; Bhatnagar, V.; Blazey, G.; Blessing, S.; Bloom, K.; Boehnlein, A.; Boline, D.; Boos, E. E.; Borissov, G.; Borysova, M.; Brandt, A.; Brandt, O.; Brock, R.; Bross, A.; Brown, D.; Bu, X. B.; Buehler, M.; Buescher, V.; Bunichev, V.; Burdin, S.; Buszello, C. P.; Camacho-Pérez, E.; Casey, B. C. K.; Castilla-Valdez, H.; Caughron, S.; Chakrabarti, S.; Chan, K. M.; Chandra, A.; Chapon, E.; Chen, G.; Cho, S. W.; Choi, S.; Choudhary, B.; Cihangir, S.; Claes, D.; Clutter, J.; Cooke, M.; Cooper, W. E.; Corcoran, M.; Couderc, F.; Cousinou, M.-C.; Cutts, D.; Das, A.; Davies, G.; de Jong, S. J.; De La Cruz-Burelo, E.; Déliot, F.; Demina, R.; Denisov, D.; Denisov, S. P.; Desai, S.; Deterre, C.; DeVaughan, K.; Diehl, H. T.; Diesburg, M.; Ding, P. F.; Dominguez, A.; Dubey, A.; Dudko, L. V.; Duperrin, A.; Dutt, S.; Eads, M.; Edmunds, D.; Ellison, J.; Elvira, V. D.; Enari, Y.; Evans, H.; Evdokimov, V. N.; Fauré, A.; Feng, L.; Ferbel, T.; Fiedler, F.; Filthaut, F.; Fisher, W.; Fisk, H. E.; Fortner, M.; Fox, H.; Fuess, S.; Garbincius, P. H.; Garcia-Bellido, A.; García-González, J. A.; Gavrilov, V.; Geng, W.; Gerber, C. E.; Gershtein, Y.; Ginther, G.; Gogota, O.; Golovanov, G.; Grannis, P. D.; Greder, S.; Greenlee, H.; Grenier, G.; Gris, Ph.; Grivaz, J.-F.; Grohsjean, A.; Grünendahl, S.; Grünewald, M. W.; Guillemin, T.; Gutierrez, G.; Gutierrez, P.; Haley, J.; Han, L.; Harder, K.; Harel, A.; Hauptman, J. M.; Hays, J.; Head, T.; Hebbeker, T.; Hedin, D.; Hegab, H.; Heinson, A. P.; Heintz, U.; Hensel, C.; Heredia-De La Cruz, I.; Herner, K.; Hesketh, G.; Hildreth, M. D.; Hirosky, R.; Hoang, T.; Hobbs, J. D.; Hoeneisen, B.; Hogan, J.; Hohlfeld, M.; Holzbauer, J. L.; Howley, I.; Hubacek, Z.; Hynek, V.; Iashvili, I.; Ilchenko, Y.; Illingworth, R.; Ito, A. S.; Jabeen, S.; Jaffré, M.; Jayasinghe, A.; Jeong, M. S.; Jesik, R.; Jiang, P.; Johns, K.; Johnson, E.; Johnson, M.; Jonckheere, A.; Jonsson, P.; Joshi, J.; Jung, A. W.; Juste, A.; Kajfasz, E.; Karmanov, D.; Katsanos, I.; Kaur, M.; Kehoe, R.; Kermiche, S.; Khalatyan, N.; Khanov, A.; Kharchilava, A.; Kharzheev, Y. N.; Kiselevich, I.; Kohli, J. M.; Kozelov, A. V.; Kraus, J.; Kumar, A.; Kupco, A.; Kurča, T.; Kuzmin, V. A.; Lammers, S.; Lebrun, P.; Lee, H. S.; Lee, S. W.; Lee, W. M.; Lei, X.; Lellouch, J.; Li, D.; Li, H.; Li, L.; Li, Q. Z.; Lim, J. K.; Lincoln, D.; Linnemann, J.; Lipaev, V. V.; Lipton, R.; Liu, H.; Liu, Y.; Lobodenko, A.; Lokajicek, M.; Lopes de Sa, R.; Luna-Garcia, R.; Lyon, A. L.; Maciel, A. K. A.; Madar, R.; Magaña-Villalba, R.; Malik, S.; Malyshev, V. L.; Mansour, J.; Martínez-Ortega, J.; McCarthy, R.; McGivern, C. L.; Meijer, M. M.; Melnitchouk, A.; Menezes, D.; Mercadante, P. G.; Merkin, M.; Meyer, A.; Meyer, J.; Miconi, F.; Mondal, N. K.; Mulhearn, M.; Nagy, E.; Narain, M.; Nayyar, R.; Neal, H. A.; Negret, J. P.; Neustroev, P.; Nguyen, H. T.; Nunnemann, T.; Orduna, J.; Osman, N.; Osta, J.; Pal, A.; Parashar, N.; Parihar, V.; Park, S. K.; Partridge, R.; Parua, N.; Patwa, A.; Penning, B.; Perfilov, M.; Peters, Y.; Petridis, K.; Petrillo, G.; Pétroff, P.; Pleier, M.-A.; Podstavkov, V. M.; Popov, A. V.; Prewitt, M.; Price, D.; Prokopenko, N.; Qian, J.; Quadt, A.; Quinn, B.; Ratoff, P. N.; Razumov, I.; Ripp-Baudot, I.; Rizatdinova, F.; Rominsky, M.; Ross, A.; Royon, C.; Rubinov, P.; Ruchti, R.; Sajot, G.; Sánchez-Hernández, A.; Sanders, M. P.; Santos, A. S.; Savage, G.; Savitskyi, M.; Sawyer, L.; Scanlon, T.; Schamberger, R. D.; Scheglov, Y.; Schellman, H.; Schwanenberger, C.; Schwienhorst, R.; Sekaric, J.; Severini, H.; Shabalina, E.; Shary, V.; Shaw, S.; Shchukin, A. A.; Simak, V.; Skubic, P.; Slattery, P.; Smirnov, D.; Snow, G. R.; Snow, J.; Snyder, S.; Söldner-Rembold, S.; Sonnenschein, L.; Soustruznik, K.; Stark, J.; Stoyanova, D. A.; Strauss, M.; Suter, L.; Svoisky, P.; Titov, M.; Tokmenin, V. V.; Tsai, Y.-T.; Tsybychev, D.; Tuchming, B.; Tully, C.; Uvarov, L.; Uvarov, S.; Uzunyan, S.; Van Kooten, R.; van Leeuwen, W. M.; Varelas, N.; Varnes, E. W.; Vasilyev, I. A.; Verkheev, A. Y.; Vertogradov, L. S.; Verzocchi, M.; Vesterinen, M.; Vilanova, D.; Vokac, P.; Wahl, H. D.; Wang, M. H. L. S.; Warchol, J.; Watts, G.; Wayne, M.; Weichert, J.; Welty-Rieger, L.; Williams, M. R. J.; Wilson, G. W.; Wobisch, M.; Wood, D. R.; Wyatt, T. R.; Xie, Y.; Yamada, R.; Yang, S.; Yasuda, T.; Yatsunenko, Y. A.; Ye, W.; Ye, Z.; Yin, H.; Yip, K.; Youn, S. W.; Yu, J. M.; Zennamo, J.; Zhao, T. G.; Zhou, B.; Zhu, J.; Zielinski, M.; Zieminska, D.; Zivkovic, L.; D0 Collaboration

    2014-12-01

    We measure the direct C P -violating parameter AC P for the decay of the charged charm meson, D+→K-π+π+ (and charge conjugate), using the full 10.4 fb-1 sample of p p ¯ collisions at √{s }=1.96 TeV collected by the D0 detector at the Fermilab Tevatron collider. We extract the raw reconstructed charge asymmetry by fitting the invariant mass distributions for the sum and difference of charge-specific samples. This quantity is then corrected for detector-related asymmetries using data-driven methods and for possible physics asymmetries (from B →D processes) using input from Monte Carlo simulation. We measure AC P=[-0.16 ±0.15 (stat)±0.09 (syst)]% , which is consistent with zero, as expected from the standard model prediction of C P conservation, and is the most precise measurement of this quantity to date.

  3. AC conductivity and dielectric properties of 2-(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1 H-pyrazol-4-ylimino)-2-(4-nitrophenyl)acetonitrile thin films

    NASA Astrophysics Data System (ADS)

    El-Menyawy, E. M.; Zeyada, H. M.; El-Nahass, M. M.

    2010-12-01

    The dark AC conductivity and dielectric properties of thermally evaporated 2-(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1 H-pyrazol-4-ylimino)-2-(4-nitrophenyl)acetonitrile (DOPNA) thin films in sandwich structure employing symmetrical gold ohmic contacts have been investigated as function of temperature (303-443 K) and frequency (100 Hz-5 MHz). The AC conductivity, σAC( ω), is found to obey Jonscher's universal power law, σAC( ω)= Aω s ( ω is the angular frequency). The AC conductivity of DOPNA thin films has been analyzed with reference to various theoretical models. The correlated barrier hopping is found to be the dominant conduction mechanism for charge carrier transport; the maximum barrier height, hopping length and the density of localized states are estimated. The temperature dependence of the AC conductivity shows Arrhenius type with two thermal activation energies. The activation energies are determined as a function of frequency. The behavior of the real and imaginary parts of the dielectric constant as a function of both temperature and frequency is discussed.

  4. Contactless electrical conductivity measurement of metallic submicron-grain material: Application to the study of aluminum with severe plastic deformation.

    PubMed

    Mito, M; Matsui, H; Yoshida, T; Anami, T; Tsuruta, K; Deguchi, H; Iwamoto, T; Terada, D; Miyajima, Y; Tsuji, N

    2016-05-01

    We measured the electrical conductivity σ of aluminum specimen consisting of submicron-grains by observing the AC magnetic susceptibility resulting from the eddy current. By using a commercial platform for magnetic measurement, contactless measurement of the relative electrical conductivity σn of a nonmagnetic metal is possible over a wide temperature (T) range. By referring to σ at room temperature, obtained by the four-terminal method, σn(T) was transformed into σ(T). This approach is useful for cylinder specimens, in which the estimation of the radius and/or volume is difficult. An experiment in which aluminum underwent accumulative roll bonding, which is a severe plastic deformation process, validated this method of evaluating σ as a function of the fraction of high-angle grain boundaries.

  5. Structural characterization, thermal, ac conductivity and dielectric properties of (C7H12N2)2[SnCl6]Cl2.1.5H2O

    NASA Astrophysics Data System (ADS)

    Hajji, Rachid; Oueslati, Abderrazek; Hajlaoui, Fadhel; Bulou, Alain; Hlel, Faouzi

    2016-05-01

    (C7H12N2)2[SnCl6]Cl2.1.5H2O is crystallized at room temperature in the monoclinic system (space group P21/n). The isolated molecules form organic and inorganic layers parallel to the (a, b) plane and alternate along the c-axis. The inorganic layer is built up by isolated SnCl6 octahedrons. Besides, the organic layer is formed by 2,4-diammonium toluene cations, between which the spaces are filled with free Cl- ions and water molecules. The crystal packing is governed by means of the ionic N-H...Cl and Ow-H...Cl hydrogen bonds, forming a three-dimensional network. The thermal study of this compound is reported, revealing two phase transitions around 360(±3) and 412(±3) K. The electrical and dielectric measurements were reported, confirming the transition temperatures detected in the differential scanning calorimetry (DSC). The frequency dependence of ac conductivity at different temperatures indicates that the correlated barrier hopping (CBH) model is the probable mechanism for the ac conduction behavior.

  6. Measurement of interfacial thermal conductance in Lithium ion batteries

    NASA Astrophysics Data System (ADS)

    Gaitonde, Aalok; Nimmagadda, Amulya; Marconnet, Amy

    2017-03-01

    Increasing usage and recent accidents due to Lithium ion (Li-ion) batteries exploding or catching on fire has inspired research on the thermal management of these batteries. In cylindrical 18650 cells, heat generated during the charge/discharge cycle must dissipate to the surrounding through its metallic case due to the poor thermal conductivity of the jelly roll, which is spirally wound with many interfaces between electrodes and the polymeric separator. This work develops a technique to measure the thermal resistance across the case-separator interface, which ultimately limits heat transfer out of the jelly roll. Commercial 18650 batteries are discharged and opened using a battery disassembly tool, and the 25 μm thick separator and the 200 μm thick metallic case are harvested to make samples. A miniaturized version of the conventional reference bar method

  7. Thermal Conductance Measurement of Metal-CNT Composites using Micro-Sized Suspended Structure

    NASA Astrophysics Data System (ADS)

    Suh, Ki Sung; Bak, Jung Hoon; Lee, Byung Yang; Hong, Seunghun; Park, Yun Daniel

    2008-03-01

    As CNTs have a unique structure and remarkable physical properties, CNT composites have attracted much attention from many researchers. Especially the thermal properties of CNTs and their composite materials have been studied intensively, because CNT has very good thermal transport properties [1-5]. For example, thermal conductivity of CNT is known to be much larger than that of metals such as Ag, Au, Cu and Al. To study the thermal conductance of metal-CNT composites, we have fabricated the micro-sized suspended structures. By using e-beam lithography and metallization, two thermometers have been patterned on the GaAs substrates. Thermal links made of metal or metal-CNT composite also have been patterned between the two thermometers. Then GaAs substrate has been under-etched to form suspended structures. We will show the fabrication methods and measurement scheme using these microstructures. ^* parkyd@phya.snu.ac.kr [1] J.A. Eastman et al., Appl. Phys. Lett. 78, 718 (2001). [2] S.U.S. Choi et al., Appl. Phys. Lett. 79, 2252 (2001). [3] M.J. Biercuk et al., Appl. Phys. Lett. 80, 2767 (2002). [4] R. Ramasubramaniam et al., Appl. Phys. Lett. 80, 4647 (2003). [5] H.Q. Xia et al., Appl. Phys. Lett. 94, 4967 (2003).

  8. Scanning Ion Conductance Microscopy for living cell membrane potential measurement

    NASA Astrophysics Data System (ADS)

    Panday, Namuna

    Recently, the existence of multiple micro-domains of extracellular potential around individual cells have been revealed by voltage reporter dye using fluorescence microscopy. One hypothesis is that these long lasting potential patterns play a vital role in regulating important cell activities such as embryonic patterning, regenerative repair and reduction of cancerous disorganization. We used multifunctional Scanning Ion Conductance Microscopy (SICM) to study these extracellular potential patterns of single cell with higher spatial resolution. To validate this novel technique, we compared the extracellular potential distribution on the fixed HeLa cell surface and Polydimethylsiloxane (PDMS) surface and found significant difference. We then measured the extracellular potential distributions of living melanocytes and melanoma cells and found both the mean magnitude and spatial variation of extracellular potential of the melanoma cells are bigger than those of melanocytes. As compared to the voltage reporter dye based fluorescence microscope method, SICM can achieve quantitative potential measurements of non-labeled living cell membranes with higher spatial resolution.

  9. Electrical conductivity measurements of bacterial nanowires from Pseudomonas aeruginosa

    NASA Astrophysics Data System (ADS)

    Maruthupandy, Muthusamy; Anand, Muthusamy; Maduraiveeran, Govindhan; Sait Hameedha Beevi, Akbar; Jeeva Priya, Radhakrishnan

    2015-12-01

    The extracellular appendages of bacteria (flagella) that transfer electrons to electrodes are called bacterial nanowires. This study focuses on the isolation and separation of nanowires that are attached via Pseudomonas aeruginosa bacterial culture. The size and roughness of separated nanowires were measured using transmission electron microscopy (TEM) and atomic force microscopy (AFM), respectively. The obtained bacterial nanowires indicated a clear image of bacterial nanowires measuring 16 nm in diameter. The formation of bacterial nanowires was confirmed by microscopic studies (AFM and TEM) and the conductivity nature of bacterial nanowire was investigated by electrochemical techniques. Cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS), which are nondestructive voltammetry techniques, suggest that bacterial nanowires could be the source of electrons—which may be used in various applications, for example, microbial fuel cells, biosensors, organic solar cells, and bioelectronic devices. Routine analysis of electron transfer between bacterial nanowires and the electrode was performed, providing insight into the extracellular electron transfer (EET) to the electrode. CV revealed the catalytic electron transferability of bacterial nanowires and electrodes and showed excellent redox activities. CV and EIS studies showed that bacterial nanowires can charge the surface by producing and storing sufficient electrons, behave as a capacitor, and have features consistent with EET. Finally, electrochemical studies confirmed the development of bacterial nanowires with EET. This study suggests that bacterial nanowires can be used to fabricate biomolecular sensors and nanoelectronic devices.

  10. Nonequilibrium temperature measurement in a thermal conduction process

    NASA Astrophysics Data System (ADS)

    Patra, Puneet Kumar; Batra, Romesh C.

    2017-01-01

    We identify the temperature being measured by a thermometer in a nonequilibrium scenario by studying heat conduction in a three-dimensional Lennard-Jones (LJ) system whose two ends are kept at different temperatures. It is accomplished by modeling the thermometer particles also with the LJ potential but with added tethers to prevent their rigid body motion. These models of the system and the thermometer mimic a real scenario in which a mechanical thermometer is "inserted" into a system and kept there long enough for the temperature to reach a steady value. The system is divided into five strips, and for each strip the temperature is measured using an embedded thermometer. Unlike previous works, these thermometers are small enough not to alter the steady state of the nonequilibrium system. After showing initial transients, the thermometers eventually show steady-state conditions with the subregions of the system and provide values of the different temperature definitions—kinetic, configurational, dynamical, and higher-order configurational. It is found that their kinetic and the configurational temperatures are close to the system's kinetic temperature except in the two thermostatted regions. In the thermostatted regions, where the system's kinetic and the configurational temperatures are significantly different, the thermometers register a temperature substantially different from either of these two values. With a decrease in the system density and size, these differences between the kinetic and the configurational temperatures of the thermometer become more pronounced.

  11. High Resolution Thermal Conductivity Measurements of Wide Gap Semiconductors

    NASA Astrophysics Data System (ADS)

    Pollak, Fred

    2002-03-01

    Despite the considerable amount of work on the electronic, optical, and structural properties of wide gap semiconductors (e.g. GaN, AlN, SiC, ZnO) relatively few thermal conductivity (κ)results have been reported. κ is a function of both intrinsic (anharmonic phonon-phonon scattering) and extrinsic (phonon scattering by dislocations, imputities, process-induced damage). Thus κ provides a measure of a material's quality and hence is important from both applied (device heat management, sample quality) and fundamental perspectives. κ can be evaluated by a number of methods including steady-state longitudinal heat flow, modified Angstrom's method, optical pump-probe, laser flash, third harmonic, and scanning thermal microscopy (SThM). With the exception of SThM these approaches require either contacts (destructive) and/or samples thicker than about 100 microns. SThM is essentially nondestructive. flexible, and has a spatial/depth resolution of 2-3 microns. The latter is important for examining low-defect techniques such as LEO in addition to mapping variations in κ across a wafer. This talk will review recent SThM thermal conductivity results on (0001) GaN [LEO (2.0-2.1 W/cm-K), for OMCVD materials sample thickness, n-type doping, grain boundaries, process-induced effects], thick free standing films of (0001) AlN (3.0-3.3 W/cm-K), (0001) SiC wafers including mapping (3.8-3.9 W/cm-K), and the Zn (1.16 W/cm-K) and O (1.02 W/cm-K) faces of bulk (0001) ZnO. Work supported by ONR contract N00014-99-C-0663 administered by Dr. Colin Wood

  12. Vertical hydraulic conductivity measurements in the Denver Basin, Colorado

    USGS Publications Warehouse

    Barkmann, P.E.

    2004-01-01

    The Denver Basin is a structural basin on the eastern flank of the Rocky Mountain Front Range, Colorado, containing approximately 3000 ft of sediments that hold a critical groundwater resource supplying many thousands of households with water. Managing this groundwater resource requires understanding how water gets into and moves through water-bearing layers in a complex multiple-layered sedimentary sequence. The Denver Basin aquifer system consists of permeable sandstone interbedded with impermeable shale that has been subdivided into four principle aquifers named, in ascending order, the Laramie-Fox Hills, Arapahoe, Denver, and Dawson aquifers. Although shale can dominate the stratigraphic interval containing the aquifers, there is very little empirical data regarding the hydrogeologic properties of the shale layers that control groundwater flow in the basin. The amount of water that flows vertically within the basin is limited by the vertical hydraulic conductivity through the confining shale layers. Low vertical flow volumes translate to low natural recharge rates and can have a profound negative impact on long-term well yields and the economic viability of utilizing the resource. To date, direct measurements of vertical hydraulic conductivity from cores of fine-grained sediments have been published from only five locations; and the data span a wide range from 1??10-3 to 1??10-11 cm/sec. This range may be attributable, in part, to differences in sample handling and analytical methods; however, it may also reflect subtle differences in the lithologic characteristics of the fine-grained sediments such as grain-size, clay mineralogy, and compaction that relate to position in the basin. These limited data certainly call for the collection of additional data.

  13. Incorporating residential AC load control into ancillary service markets: Measurement and settlement

    SciTech Connect

    Bode, Josh L.; Sullivan, Michael J.; Berghman, Dries; Eto, Joseph H.

    2013-05-01

    Many pre-existing air conditioner load control programs can provide valuable operational flexibility but have not been incorporated into electricity ancillary service markets or grid operations. Multiple demonstrations have shown that residential air conditioner (AC) response can deliver resources quickly and can provide contingency reserves. A key policy hurdle to be overcome before AC load control can be fully incorporated into markets is how to balance the accuracy, cost, and complexity of methods available for the settlement of load curtailment. Overcoming this hurdle requires a means for assessing the accuracy of shorter-term AC load control demand reduction estimation approaches in an unbiased manner. This paper applies such a method to compare the accuracy of approaches varying in cost and complexity ? including regression analysis, load matching and control group approaches ? using feeder data, household data and AC end-use data. We recommend a practical approach for settlement, relying on an annually updated set of tables, with pre-calculated reduction estimates. These tables allow users to look up the demand reduction per device based on daily maximum temperature, geographic region and hour of day, simplifying settlement and providing a solution to the policy problem presented in this paper.

  14. Electrical-Impedance Tomography for Measuring Material Distributions of Multiphase Flows in Conducting Vessels

    NASA Astrophysics Data System (ADS)

    Liter, S. G.; Torczynski, J. R.; Shollenberger, K. A.; Ceccio, S. L.

    2001-11-01

    An implementation of resistive electrical-impedance tomography (EIT) for measuring material distributions of two-phase flows in vessels with electrically conducting walls is presented. A thin nonconducting rod, with N-1 ring electrodes wrapped around its exterior at equally-spaced axial positions, is inserted into the vessel (i.e., into the interior of the flow). The vessel wall is grounded and serves as the N-th electrode. Current is injected from a ring electrode and exits to the vessel wall, and the resulting voltages at all ring electrodes are recorded. Each ring electrode is used in turn for current injection, and the collection of all measured voltages comprises a data set. Multiple data sets are used to numerically reconstruct the time-averaged impedance distribution within the vessel, from which the material distribution is inferred. Design issues, including the size, spacing, and number of the ring electrodes, are considered. An experiment in which the rod is inserted coaxially into a vertical pipe is presented, and bubble-column applications are discussed. *Sandia is a multiprogram laboratory operated by Sandia Corporation, a Lockheed Martin Company, for the United States Department of Energy under Contract DE-AC04-94AL85000.

  15. AC conductivity and relaxation mechanism in (Nd1/2Li1/2)(Fe1/2V1/2)O3 ceramics

    NASA Astrophysics Data System (ADS)

    Nath, Susmita; Barik, Subrat Kumar; Choudhary, R. N. P.

    2016-05-01

    In the present study we have synthesized polycrystalline sample of (Nd1/2Li1/2)(Fe1/2V1/2)O3 ceramic by a standard high-temperature solid-state reaction technique. Studies of dielectric and electrical properties of the compound have been carried out in a wide range of temperature (RT - 400 °C) and frequency (1kHz - 1MHz) using complex impedance spectroscopic technique. The imaginary vs. real component of the complex impedance plot (Nyquist plot) of the prepared sample exhibits the existence of grain, grain boundary contributions in the complex electrical parameters and negative temperature coefficient of resistance (NTCR) type behavior like semiconductor. Details study of ac conductivity plot reveals that the material obeys universal Jonscher's power law.

  16. Synthesis and characterization of cancrinite-type zeolite, and its ionic conductivity study by AC impedance analysis

    NASA Astrophysics Data System (ADS)

    Kriaa, A.; Ben Saad, K.; Hamzaoui, A. H.

    2012-12-01

    The synthesis of cancrinite in the system NaOH-SiO2-Al2O3-NaHCO3-H2O was performed, according to methods described in the literature, in an autoclave under hydrothermal conditions at T = 473 K. The electrical properties of cancrinite-type zeolite pellets were investigated by complex impedance spectroscopy in the temperature range 465-800°C. The effect of temperature on impedance parameters was studied using an impedance analyzer in a wide frequency range (1 Hz to 13 MHz). The real and imaginary parts of complex impedance trace semicircles in the complex plane are plotted. The bulk resistance of the material decreases with rise in temperature. This exhibits a typical negative temperature coefficient of resistance (NTCR) behavior of the material. The results of bulk electrical conductivity and its activation energy are presented. The modulus analysis suggests that the electrical transport processes in the material are very likely to be of electronic nature. Relaxation frequencies follow an Arrhenius behavior with activation energy values not comparable to those found for the electrical conductivity.

  17. AC losses in high pressure synthesized MgB2 bulk rings measured by a transformer method

    NASA Astrophysics Data System (ADS)

    Meerovich, V.; Sokolovsky, V.; Prikhna, T.; Gawalek, W.; Habisreuther, T.

    2013-03-01

    Recently developed manufacturing technologies use high pressure and various doping additions to prepare bulk MgB2-based materials with a high critical current density measured by the magnetization method. We use a contactless transformer method, which is based on studying the superconductor response to an induced transport current, to measure AC losses in bulk MgB2 rings synthesized under high pressure. The obtained dependence of the losses on the primary current (applied magnetic field) is fitted by a power law with an exponent of ˜2.1 instead of the cubic dependence predicted by Bean’s model and power law electric field-current density (E-J) characteristics with a large exponent. An unusually strong dependence of the AC losses on the frequency is also observed. It is shown that the E-J characteristic of bulk MgB2 is well fitted by the dependence used in the extended critical state model based on account of the viscous vortex motion in the flux flow regime. Numerical simulation using this E-J characteristic gives current and frequency AC loss dependences that agree well with the experimental results.

  18. Steady heat conduction-based thermal conductivity measurement of single walled carbon nanotubes thin film using a micropipette thermal sensor

    PubMed Central

    Shrestha, R.; Lee, K. M.; Chang, W. S.; Kim, D. S.; Rhee, G. H.; Choi, T. Y.

    2013-01-01

    In this paper, we describe the thermal conductivity measurement of single-walled carbon nanotubes thin film using a laser point source-based steady state heat conduction method. A high precision micropipette thermal sensor fabricated with a sensing tip size varying from 2 μm to 5 μm and capable of measuring thermal fluctuation with resolution of ±0.01 K was used to measure the temperature gradient across the suspended carbon nanotubes (CNT) film with a thickness of 100 nm. We used a steady heat conduction model to correlate the temperature gradient to the thermal conductivity of the film. We measured the average thermal conductivity of CNT film as 74.3 ± 7.9 W m−1 K−1 at room temperature. PMID:23556837

  19. Steady heat conduction-based thermal conductivity measurement of single walled carbon nanotubes thin film using a micropipette thermal sensor.

    PubMed

    Shrestha, R; Lee, K M; Chang, W S; Kim, D S; Rhee, G H; Choi, T Y

    2013-03-01

    In this paper, we describe the thermal conductivity measurement of single-walled carbon nanotubes thin film using a laser point source-based steady state heat conduction method. A high precision micropipette thermal sensor fabricated with a sensing tip size varying from 2 μm to 5 μm and capable of measuring thermal fluctuation with resolution of ±0.01 K was used to measure the temperature gradient across the suspended carbon nanotubes (CNT) film with a thickness of 100 nm. We used a steady heat conduction model to correlate the temperature gradient to the thermal conductivity of the film. We measured the average thermal conductivity of CNT film as 74.3 ± 7.9 W m(-1) K(-1) at room temperature.

  20. New measurement of exotic decay of 225Ac by 14C emission

    NASA Astrophysics Data System (ADS)

    Guglielmetti, A.; Bonetti, R.; Ardisson, G.; Barci, V.; Giles, T.; Hussonnois, M.; Le Du, J. F.; Le Naour, C.; Mikheev, V. L.; Pasinetti, A. L.; Ravn, H. L.; Tretyakova, S. P.; Trubert, D.

    The branching ratio of 225Ac decay by emission of 14C was remeasured under improved experimental conditions by using a radioactive source produced at the ISOLDE mass-separator at CERN and a nuclear track detector technique. The result, B = λ14C/λα = (4.5+/-1.4)10-12, is consistent with the anomalously high value obtained in the 1993 experiment, thus confirming the importance of nuclear-structure effects in this exotic decay.

  1. SPHINX Measurements of Radiation Induced Conductivity of Foam

    SciTech Connect

    Ballard, W.P.; Beutler, D.E.; Burt, M.; Dudley, K.J.; Stringer, T.A.

    1998-12-14

    Experiments on the SPHINX accelerator studying radiation-induced conductivity (RIC) in foam indicate that a field-exclusion boundary layer model better describes foam than a Maxwell-Garnett model that treats the conducting gas bubbles in the foam as modifying the dielectric constant. In both cases, wall attachment effects could be important but were neglected.

  2. Reconstruction from boundary measurements for less regular conductivities

    NASA Astrophysics Data System (ADS)

    García, Andoni; Zhang, Guo

    2016-11-01

    In this paper, following Nachman’s idea (1988 Ann. Math. 128 531-76) and Haberman and Tataru’s idea (2013 Duke Math. J. 162 497-516), we reconstruct C 1 conductivity γ or Lipchitz conductivity γ with small enough value of | {{\

  3. Electroanalytical measurements without electrolytes: conducting polymers as probes for redox titration in non-conductive organic media.

    PubMed

    Lange, Ulrich; Mirsky, Vladimir M

    2012-09-26

    Electroanalytical methods have been applied only in conducting media. An application of conducting polymers allows to overcome this limitation. If such material is in electrochemical equilibrium with dissolved redox active species, its electrical conductivity depends on the redox potential of these species. Therefore, conductometric measurements with conducting polymers can provide about the same information as classical redox electrodes. The approach was applied for redox titration. Equivalent points obtained by this titration in aqueous and organic electrolytes were identical. Then the approach was applied for determination of bromine number by redox titration in non-conducting organic phase.

  4. Experimental and theoretical study of AC electrical conduction mechanisms of Organic-inorganic hybrid compound Bis (4-acetylanilinium) tetrachlorocadmiate (II)

    NASA Astrophysics Data System (ADS)

    Jellibi, A.; Chaabane, I.; Guidara, K.

    2016-06-01

    A new organic-inorganic bis (4-acetylaniline) tetrachlorocadmate [C8H10NO]2[CdCl4] can be obtained by slow evaporation at room temperature and characterized by X-ray powder diffraction. It crystallized in an orthorhombic system (Cmca space group). The material electrical properties were characterized by impedance spectroscopy technique in the frequency range from 209 Hz-5 MHz and temperature 413 to 460 K. Besides, the impedance plots show semicircle arcs at different temperatures and an electrical equivalent circuit has been proposed to interpret the impedance results. The circuits consist of the parallel combination of a resistance (R), capacitance (C) and fractal capacitance (CPE). The variation of the exponent s as a function of temperature suggested that the conduction mechanism in Bis (4-acetylanilinium) tetrachlorocadmiate compound is governed by two processes which can be ascribed to a hopping transport mechanism: correlated barrier hopping (CBH) model below 443 K and the small polaron tunneling (SPT) model above 443 K.

  5. In vivo measurements of electrical conductivity of porcine organs at low frequency: new method of measurement.

    PubMed

    Spottorno, J; Multigner, M; Rivero, G; Alvarez, L; de la Venta, J; Santos, M

    2012-10-01

    Calculations of the induced currents created in the human body by external electromagnetic fields would be more accurate provided that more realistic experimental values of the electrical properties of the body were available. The purpose of this work is to experimentally obtain values for the conductivity of living organs in conditions close to the real situation. Two-electrode in vivo measurements of the bioimpedance of some porcine organs have been performed. From these measurements and taking into account geometrical considerations, the electrical conductivity for the kidney, liver, heart, and spinal cord has been obtained and were found to be higher than the values reported in the literature. Furthermore, a new experimental procedure is proposed where the conductivity is determined from the values of the electrical potential and currents that are induced by an external electromagnetic field created by a coil placed close to the organ under study.

  6. Ground level measurements of air conductivities under Florida thunderstorms

    NASA Technical Reports Server (NTRS)

    Blakeslee, Richard J.; Krider, E. P.

    1992-01-01

    Values of the positive and negative polar conductivities under summer thunderstorms in Florida are highly variable and exhibit a significant electrode effect, but the total conductivity usually remains close to values found in fair weather, 0.4 to 1.8 x 10 exp -14 S/m. With these values a method proposed by Krider and Musser (1982) for estimating the total conductivity from changes in the slope of the electric field recovery following a lightning discharge will be extremely sensitive to small time variations in the local Maxwell current density and must be modified to include these effects.

  7. A transient hot-wire instrument for thermal conductivity measurements in electrically conducting liquids at elevated temperatures

    NASA Astrophysics Data System (ADS)

    Alloush, A.; Gosney, W. B.; Wakeham, W. A.

    1982-09-01

    This paper describes a novel type of transient hot-wire cell for thermal conductivity measurements on electrically conducting liquids. A tantalum wire of 25 μm. diameter is used as the sensing element in the cell, and it is insulated from the conducting liquids by an anodic film of tantalum pentoxide, 70 nm thick. The cell is suitable for measurements on conducting liquids at elevated temperatures. The results of test measurements on liquid water at its saturation vapor pressure are reported in order to confirm the correct operation of the thermal conductivity cell. The data, which have an estimated accuracy of ±3%, depart by less than ±1.8% from the correlation proposed by the International Association for the Properties of Steam. Results are also presented for concentrated aqueous solutions of lithium bromide, which are frequently used in absorption refrigerator cycles.

  8. Developing passive MEMS DC/AC current sensor applicable to two-wire appliances with high measurement accuracy

    NASA Astrophysics Data System (ADS)

    Wang, Dong F.; Li, Xiaodong; Xian, Weikang; Liu, Huan; Liu, Xin

    2016-10-01

    A passive MEMS DC/AC current sensor with high measurement accuracy, accomplished by the methodology combining both the "stress-equilibrium" solution and the "position-free" solution, was proposed for measuring electricity consumption of household equipment and Information and Communication Technology devices. For the "stress-equilibrium" solution, slots between two adjacent piezoelectric plates are implemented to minimize the distribution difference of the uneven stress close to the fixed end. The measurement error caused by the uneven stress distribution is decreased from 9% to 4% for ten-piezoelectric-plates and from 8% to 0.5% for three-piezoelectric-plates, respectively. For the "position-free" consideration, an array comprised of four piezoelectric cantilevers is proposed to eliminate the positional error resulted by the uneven magnetic field distribution generated by the test object of electric currents. And the solution is proofed to be an effective method to eliminate the positional error by theoretical and simulation analysis. In light of the above preliminary results, the passive MEMS DC/AC current sensor is believed to be useful to achieve high measurement accuracy via integrating the "stress-equilibrium" and the "position-free" designs. The newly proposed current sensor with high measurement accuracy is applicable to two-wire appliance cord without using any cord separator like that used in Hall-effect based sensor.

  9. Impedance and AC conductivity study of nano crystalline, fine grained multiferroic bismuth ferrite (BiFeO3), synthesized by microwave sintering

    NASA Astrophysics Data System (ADS)

    Kolte, Jayant; Salame, Paresh H.; Daryapurkar, A. S.; Gopalan, P.

    2015-09-01

    In this paper, major reduction in sintering time,temperautre and significant improvement over final density of sitnered sample is reported for the microwave sintered nanocrystalline BiFeO3 (BFO) ceramic. Also, different sintering time and temperatures have been used to tailor the grain size and the final density of the resulting BFO ceramics synthesized from phase pure BFO nanoparticles ( d ¯ ≈ 10 n m ). Microwave sintering resulted in reducing the sintering time substantially (by 1h), and has resulted in submicron sized grains and high resistivity ˜1.8 GΩ-cm. The AC conductivity is seen to follow the Jonscher's power law behavior, suggesting correlated barrier hopping (CBH) mechanism in the sample. The role of oxygen vacancies at high temperature, due to volatility of bismuth, in dielectric and conductivity behavior is also discussed. Further, the sample displayed dielectric anomaly near magnetic transition temperature (˜180 °C) indicating bearing of magnetic moments on the dielectric properties. Using Impedance Spectroscopy (IS) we have established, the electrical heterogeneity of the ceramic BFO reavealing semiconducting nature of grains and insulating nature of grain boundary. This, formation of network of insulating grain boundaries and semiconducting grains could lead to formation of internal barrier layer capacitance (IBLC) leading to high dielectric constant in microwave sintered BFO.

  10. Microtubule alignment and manipulation using AC electrokinetics.

    PubMed

    Uppalapati, Maruti; Huang, Ying-Ming; Jackson, Thomas N; Hancock, William O

    2008-09-01

    The kinesin-microtubule system plays an important role in intracellular transport and is a model system for integrating biomotor-driven transport into microengineered devices. AC electrokinetics provides a novel tool for manipulating and organizing microtubules in solution, enabling new experimental geometries for investigating and controlling the interactions of microtubules and microtubule motors in vitro. By fabricating microelectrodes on glass substrates and generating AC electric fields across solutions of microtubules in low-ionic-strength buffers, bundles of microtubules are collected and aligned and the electrical properties of microtubules in solution are measured. The AC electric fields result in electro-osmotic flow, electrothermal flow, and dielectrophoresis of microtubules, which can be controlled by varying the solution conductivity, AC frequency, and electrode geometry. By mapping the solution conductivity and AC frequency over which positive dielectrophoresis occurs, the apparent conductivity of taxol-stabilized bovine-brain microtubules in PIPES buffer is measured to be 250 mS m(-1). By maximizing dielectrophoretic forces and minimizing electro-osmotic and electrothermal flow, microtubules are assembled into opposed asters. These experiments demonstrate that AC electrokinetics provides a powerful new tool for kinesin-driven transport applications and for investigating the role of microtubule motors in development and maintenance of the mitotic spindle.

  11. Molecular conductance measurements through printed Au nano-dots.

    NASA Astrophysics Data System (ADS)

    Jiang, Weirong; Zhitenev, Nikolai; Bao, Zhenan; Abusch-Magder, David; Tennant, Don; Garfunkel, Eric

    2006-03-01

    Gold pads with ˜100 nm diameter are imprinted on self-assembled monolayers of alkane dithiols of different lengths using nano-transfer technique. The fabrication technique ensures formation of chemical bonds at both ends of molecules while minimizes defect creations compared to other metallization methods. The pads are contacted by conductive atomic force microscope (CAFM) to study electron transport through the SAM as a function of contact force. We found that atomic scale topography at the metal-molecules interface is essential to describe the conductance-stress relationship. In as-fabricated devices, only small percentage of molecules (below 1%) is wired to both contacts. A finite force (1-10 nN) deforms devices resulting in two competing effects: (a) contacting larger number of molecules leading; (b) deforming interfacial bonds and/or tilting the molecules. The estimated conductance of molecules is significantly smaller than in previous CAFM experiments and calculations.

  12. Contactless measurement of alternating current conductance in quantum Hall structures

    SciTech Connect

    Drichko, I. L.; Diakonov, A. M.; Malysh, V. A.; Smirnov, I. Yu.; Ilyinskaya, N. D.; Usikova, A. A.; Galperin, Y. M.; Kummer, M.; Känel, H. von

    2014-10-21

    We report a procedure to determine the frequency-dependent conductance of quantum Hall structures in a broad frequency domain. The procedure is based on the combination of two known probeless methods—acoustic spectroscopy and microwave spectroscopy. By using the acoustic spectroscopy, we study the low-frequency attenuation and phase shift of a surface acoustic wave in a piezoelectric crystal in the vicinity of the electron (hole) layer. The electronic contribution is resolved using its dependence on a transverse magnetic field. At high frequencies, we study the attenuation of an electromagnetic wave in a coplanar waveguide. To quantitatively calibrate these data, we use the fact that in the quantum-Hall-effect regime the conductance at the maxima of its magnetic field dependence is determined by extended states. Therefore, it should be frequency independent in a broad frequency domain. The procedure is verified by studies of a well-characterized p-SiGe/Ge/SiGe heterostructure.

  13. Determining Conductivity by Boundary Measurements: Some Numerical Results

    DTIC Science & Technology

    1988-05-01

    continuous, then -:Let B, ~ - 71iAl. If, 71i and 7y2 are Lipschitz continuous, and for some /3, V-yJ ,3 for i =1, 2, then JIB, - B2111/2,..1/2 <C 3jj1h...case of anisotropic conductors we face a problem of nonuniqueness . One way to avoid the nonuniqueness issue is to convert the matrix conductivity to an

  14. Astronaut Mike Fincke Conducts Fluid Merging Viscosity Measurement (FMVM) Experiment

    NASA Technical Reports Server (NTRS)

    2004-01-01

    Astronaut Mike Fincke places droplets of honey onto the strings for the Fluid Merging Viscosity Measurement (FMVM) investigation onboard the International Space Station (ISS). The FMVM experiment measures the time it takes for two individual highly viscous fluid droplets to coalesce or merge into one droplet. Different fluids and droplet size combinations were tested in the series of experiments. By using the microgravity environment, researchers can measure the viscosity or 'thickness' of fluids without the influence of containers and gravity using this new technique. Understanding viscosity could help scientists understand industrially important materials such as paints, emulsions, polymer melts and even foams used to produce pharmaceutical, food, and cosmetic products.

  15. Reduction of Common-Mode Conducted Noise Emissions in PWM Inverter-fed AC Motor Drive Systems using Optimized Passive EMI Filter

    NASA Astrophysics Data System (ADS)

    Jettanasen, C.; Ngaopitakkul, A.

    2010-10-01

    Conducted electromagnetic interference (EMI) generated by PWM inverter-fed induction motor drive systems, which are currently widely used in many industrial and/or avionic applications, causes severe parasitic current problems, especially at high frequencies (HF). These restrict power electronic drive's evolution. In order to reduce or minimize these EMI problems, several techniques can be applied. In this paper, insertion of an optimized passive EMI filter is proposed. This filter is optimized by taking into account real impedances of each part of a considered AC motor drive system contrarily to commercial EMI filters designed by considering internal impedance of disturbance source and load, equal to 50Ω. Employing the latter EMI filter would make EMI minimization less effective. The proposed EMI filter optimization is mainly dedicated to minimize common mode (CM) currents due to its most dominant effects in this kind of system. The efficiency of the proposed optimization method using two-port network approach is deduced by comparing the minimized CM current spectra to an applied normative level (ex. DO-160D in aeronautics).

  16. Influence of temperature on the electric, dielectric and AC conductivity properties of nano-crystalline zinc substituted cobalt ferrite synthesized by solution combustion technique

    NASA Astrophysics Data System (ADS)

    Rani, Ritu; Kumar, Gagan; Batoo, Khalid M.; Singh, M.

    2014-06-01

    Cobalt-zinc nanoferrites with formulae Co ZnFeO, where x = 0.0, 0.1, 0.2 and 0.3, have been synthesized by solution combustion technique. The variation of DC resistivity with temperature shows the semiconducting behavior of all nanoferrites. The dielectric properties such as dielectric constant (') and dielectric loss tangent (tan are investigated as a function of temperature and frequency. Dielectric constant and loss tangent are found to be increasing with an increase in temperature while with an increase in frequency both, ' and tan , are found to be decreasing. The dielectric properties have been explained on the basis of space charge polarization according to Maxwell-Wagner's two-layer model and the hopping of charge between Fe and Fe. Further, a very high value of dielectric constant and a low value of tan are the prime achievements of the present work. The AC electrical conductivity ( is studied as a function of temperature as well as frequency and is observed to be increasing with the increase in temperature and frequency.

  17. Instrument for Measuring Thermal Conductivity of Materials at Low Temperatures

    NASA Technical Reports Server (NTRS)

    Fesmire, James; Sass, Jared; Johnson, Wesley

    2010-01-01

    With the advance of polymer and other non-metallic material sciences, whole new series of polymeric materials and composites are being created. These materials are being optimized for many different applications including cryogenic and low-temperature industrial processes. Engineers need these data to perform detailed system designs and enable new design possibilities for improved control, reliability, and efficiency in specific applications. One main area of interest is cryogenic structural elements and fluid handling components and other parts, films, and coatings for low-temperature application. An important thermal property of these new materials is the apparent thermal conductivity (k-value).

  18. Nanoscale Electromechanics To Measure Thermal Conductivity, Expansion, and Interfacial Losses.

    PubMed

    Mathew, John P; Patel, Raj; Borah, Abhinandan; Maliakkal, Carina B; Abhilash, T S; Deshmukh, Mandar M

    2015-11-11

    We study the effect of localized Joule heating on the mechanical properties of doubly clamped nanowires under tensile stress. Local heating results in systematic variation of the resonant frequency; these frequency changes result from thermal stresses that depend on temperature dependent thermal conductivity and expansion coefficient. The change in sign of the linear expansion coefficient of InAs is reflected in the resonant response of the system near a bath temperature of 20 K. Using finite element simulations to model the experimentally observed frequency shifts, we show that the thermal conductivity of a nanowire can be approximated in the 10-60 K temperature range by the empirical form κ = bT W/mK, where the value of b for a nanowire was found to be b = 0.035 W/mK(2), significantly lower than bulk values. Also, local heating allows us to independently vary the temperature of the nanowire relative to the clamping points pinned to the bath temperature. We suggest a loss mechanism (dissipation ~10(-4)-10(-5)) originating from the interfacial clamping losses between the metal and the semiconductor nanostructure.

  19. Thermal conductivity of silver loaded conductive epoxy from cryogenic to ambient temperature and its application for precision cryogenic noise measurements

    NASA Astrophysics Data System (ADS)

    Amils, Ricardo I.; Gallego, Juan Daniel; Sebastián, José Luis; Muñoz, Sagrario; Martín, Agustín; Leuther, Arnulf

    2016-06-01

    The pressure to increase the sensitivity of instrumentation has pushed the use of cryogenic Low Noise Amplifier (LNA) technology into a growing number of fields. These areas range from radio astronomy and deep space communications to fundamental physics. In this context manufacturing for cryogenic environments requires a proper thermal knowledge of the materials to be able to achieve adequate design behavior. In this work, we present experimental measurements of the thermal conductivity of a silver filled conductive epoxy (EPO-TEK H20E) which is widely used in cryogenic electronics applications. The characterization has been made using a sample preparation which mimics the practical use of this adhesive in the fabrication of cryogenic devices. We apply the data obtained to a detailed analysis of the effects of the conductive epoxy in a monolithic thermal noise source used for high accuracy cryogenic microwave noise measurements. In this application the epoxy plays a fundamental role since its limited thermal conductivity allows heating the chip with relatively low power. To our knowledge, the cryogenic thermal conductivity data of this epoxy has not been reported before in the literature in the 4-300 K temperature range. A second non-conductive epoxy (Gray Scotch-Weld 2216 B/A), also widely used in cryogenic applications, has been measured in order to validate the method by comparing with previous published data.

  20. Conducting Art Therapy Research Using Quantitative EEG Measures

    ERIC Educational Resources Information Center

    Belkofer, Christopher M.; Konopka, Lukasz M.

    2008-01-01

    This study presents a modified, single subject design that measured the patterns of electrical activity of a participant's brain following an hour spent painting and drawing. Paired t tests were used to compare pre and post art-making electroencephalograph (EEG) data. The results indicated that neurobiological activity after drawing and painting…

  1. MEASUREMENT OF HYDRAULIC CONDUCTIVITY DISTRIBUTIONS: A MANUAL OF PRACTICE

    EPA Science Inventory

    The ability of hydrologists to perform field measurements of aquifer hydraulic properties must be enhanced in order to significantly improve the capacity to solve groundwater contamination problems at Superfund and other sites. The primary purpose of this manual is to provide ne...

  2. Measurements Conducted on an Unknown Object Labeled Pu-239

    SciTech Connect

    Hoteling, Nathan

    2013-11-18

    Measurements were carried out on 12 November 2013 to determine whether Pu-239 was present on an object discovered in a plastic bag with label “Pu-­239 6 uCi.” Following initial survey measurements to verify that the object was not leaking or contaminated, spectra were collected with a High Purity Germanium (HPGe) detector with object positioned in two different configurations. Analysis of the spectra did not yield any direct evidence of Pu-­239. From the measured spectra, minimum detectable activity (MDA) was determined to be approximately 2 uCi for the gamma-­ray measurements. Although there was no direct evidence of Pu-239, a peak at 60 keV characteristic of Am-­241 decay was observed. Since it is very likely that Am-­241 would be present in aged plutonium samples, this was interpreted as indirect evidence for the presence of plutonium on the object. Analysis of this peak led to an estimated Pu-­239 activity of 0.02–0.04 uCi, or <1x10-6 grams.

  3. Measuring Thermal Conductivity of a Small Insulation Sample

    NASA Technical Reports Server (NTRS)

    Miller, Robert A.; Kuczmarski, Maria A.

    2009-01-01

    A multiple-throat venturi system has been invented for measuring laminar flow of air or other gas at low speed (1 to 30 cm/s) in a duct while preserving the laminar nature of the flow and keeping the velocity profile across the duct as nearly flat as possible. While means for measuring flows at higher speeds are well established, heretofore, there have been no reliable means for making consistent, accurate measurements in this speed range. In the original application for which this system was invented, the duct leads into the test section of a low-speed wind tunnel wherein uniform, low-speed, laminar flow is required for scientific experiments. The system could also be used to monitor a slow flow of gas in an industrial process like chemical vapor deposition. In the original application, the multiple- throat venturi system is mounted at the inlet end of the duct having a rectangular cross section of 19 by 14 cm, just upstream of an assembly of inlet screens and flow straighteners that help to suppress undesired flow fluctuations (see Figure 1). The basic venturi measurement principle is well established: One measures the difference in pressure between (1) a point just outside the inlet, where the pressure is highest and the kinetic energy lowest; and (2) the narrowest part (the throat) of the venturi passage, where the kinetic energy is highest and the pressure is lowest. Then by use of Bernoulli s equation for the relationship between pressure and kinetic energy, the volumetric flow speed in the duct can be calculated from the pressure difference and the inlet and throat widths. The design of this system represents a compromise among length, pressure recovery, uniformity of flow, and complexity of assembly. Traditionally, venturis are used to measure faster flows in narrower cross sections, with longer upstream and downstream passages to maintain accuracy. The dimensions of the passages of the present venturi system are sized to provide a readily measurable

  4. Thermal conductivity of silica nanoparticle powder: Measurement and theoretical analysis

    NASA Astrophysics Data System (ADS)

    Huang, Congliang; Lin, Zizhen; Feng, Yanhui; Zhang, Xinxin; Wang, Ge

    2015-12-01

    The hot-wire method was applied to experimentally determine the thermal conductivity (TC) of a silica nanoparticle powder. A fitting model was further employed to analyze the experimental results and to predict the TC over a wider porosity scale. Results show that the effective TC of the silica-nanoparticle powder can be less than that of free air because of the low TC of both the silica nanoparticles and the air confined in the pore spaces; the relative contribution of the nanoparticle TC, the confined air TC, and the radiation heat transfer coefficient to the effective TC will significantly affect at which porosity the extreme value of the effective TC occurs; the porosity obtained when the contribution to the effective TC of the confined air equals that of the nanoparticles is the most favorable for constructing thermal insulation materials.

  5. Electrical Effect in Silver-Point Realization Due to Cell Structure and Bias Voltage Based on Resistance Measurement Using AC and DC Bridges

    NASA Astrophysics Data System (ADS)

    Widiatmo, J. V.; Harada, K.; Yamazawa, K.; Tamba, J.; Arai, M.

    2015-08-01

    Electrical effects related to insulating leakage represent one of the major factors contributing to uncertainties in measurements using high-temperature standard platinum resistance thermometers (HTSPRTs), especially during the realization of the silver freezing point (). This work is focused on the evaluation of the differences in resistance measurements observed when using AC resistance bridges and DC resistance bridges, hereafter, termed the AC-DC differences, as the result of various electrical effects. The magnitude of the AC-DC difference in several silver-point cells is demonstrated with several HTSPRTs. The effect of the cell structure on the AC-DC difference is evaluated by exchanging some components, part by part, within a silver-point cell. Then, the effect of the bias voltage applied to the heat pipe within the silver-point furnace is evaluated. Through the analysis of the experimental results and comparison with the reports in the literature, the importance of evaluating the AC-DC difference as a means to characterize the underlying electrical effects is discussed, considering that applying a negative bias condition to the furnace with respect to the high-temperature SPRT can minimize the AC-DC difference. Concluding recommendations are proposed on the components used in silver-point cells and the application of a bias voltage to the measurement circuit to minimize the effects of the electrical leakage.

  6. Analyses of temperature-dependent interface states, series resistances, and AC electrical conductivities of Al/p—Si and Al/Bi4Ti3O12/p—Si structures by using the admittance spectroscopy method

    NASA Astrophysics Data System (ADS)

    Mert, Yıldırım; Perihan, Durmuş; Şemsettin, Altındal

    2013-10-01

    In this study, Al/p—Si and Al/Bi4Ti3O12/p—Si structures are fabricated and their interface states (Nss), the values of series resistance (Rs), and AC electrical conductivityac) are obtained each as a function of temperature using admittance spectroscopy method which includes capacitance—voltage (C—V) and conductance—voltage (G—V) measurements. In addition, the effect of interfacial Bi4Ti3O12 (BTO) layer on the performance of the structure is investigated. The voltage-dependent profiles of Nss and Rs are obtained from the high-low frequency capacitance method and the Nicollian method, respectively. Experimental results show that Nss and Rs, as strong functions of temperature and applied bias voltage, each exhibit a peak, whose position shifts towards the reverse bias region, in the depletion region. Such a peak behavior is attributed to the particular distribution of Nss and the reordering and restructuring of Nss under the effect of temperature. The values of activation energy (Ea), obtained from the slope of the Arrhenius plot, of both structures are obtained to be bias voltage-independent, and the Ea of the metal-ferroelectric-semiconductor (MFS) structure is found to be half that of the metal—semiconductor (MS) structure. Furthermore, other main electrical parameters, such as carrier concentration of acceptor atoms (NA), built-in potential (Vbi), Fermi energy (EF), image force barrier lowering (Δ Φb), and barrier height (Φb), are extracted using reverse bias C-2—V characteristics as a function of temperature.

  7. Distance-Dependent Measurements of the Conductance of Porphyrin Nanorods Studied with Conductive Probe Atomic Force Microscopy.

    PubMed

    Zhai, Xianglin; Alexander, Denzel; Derosa, Pedro; Garno, Jayne C

    2017-02-07

    Protocols for nanopatterning porphyrins on Au(111) were developed based on immersion particle lithography. Porphyrins with and without a central metal ion, 5,10,15,20-tetraphenyl-21H,23H-porphyrin (TPP) and 5,10,15,20-tetraphenyl-21H,23H-porphyrin cobalt(II) (CoTPP), were selected for study, which spontaneously formed nanorod geometries depending on concentration parameters. The elongated shapes of the nanorods offers an opportunity for successive distance-dependent conductive probe atomic force microscopy (CP-AFM) measurements along the length of the nanorods. To prepare patterns of TPP and CoTPP nanorods, a mask of silica mesospheres was placed on gold substrates to generate nanoholes within an alkanethiol matrix film. The nanoholes prepared by particle lithography with an immersion step were backfilled with porphyrins by a second immersion step. By controlling the concentration and immersion interval, nanorods of porphyrins were generated with one end of the nanostructure attached to gold within a nanohole. The porphyrin nanorods exhibited slight differences in dimensions at the nanoscale to enable size-dependent measurements of conductive properties. The conductivity along the horizontal direction of the nanorods was evaluated with CP-AFM studies. Changes in conductivity were measured along the long axis of TPP and CoTPP nanorods. The TPP nanorods exhibited conductive profiles of an insulating material, and the CoTPP nanorods exhibited profiles of a semiconductor. The experiments demonstrate the applicability of particle lithography for preparing unique and functional surface platforms of porphyrins to measure distance-dependent conductive properties on gold.

  8. Evaluation of the electrode performance for PAFC by using acid absorption, acceleration and ac-impedance measurement

    SciTech Connect

    Kim, Chang-Soo; Song, Rak-Hyun; Choi, Byung-Woo

    1996-12-31

    In PAFC, the degradation on cathode electrode caused by carbon corrosion, platinum dissolution and growth is especially severe. An acceleration test is a good technique for evaluating the degradation of electrode performance, because it does not need long time. Coleman et al used thermal cycling and on-off cycling as an acceleration test. Song et al showed that hydrogen shortage decreased the electrode performance more rapidly than that of air shortage in gas shortage test. Honji et al reported that the rate of coarsening of Pt particle is rapid in open circuit potential and this is one of major causes on the performance degradation of electrode. The cathode performance has been studied by using acid absorption, acceleration and ac-impedance measurements as functions of the polytetrafluoroethylene (PTFE) contents and sintering temperatures of the electrode.

  9. Deuterium isotope effects on the ionization constant of acetic acid in H2O and D2O by AC conductance from 368 to 548 K at 20 MPa.

    PubMed

    Erickson, K M; Arcis, H; Raffa, D; Zimmerman, G H; Tremaine, P R

    2011-03-31

    Values of the ionization constant of acetic acid in H(2)O and D(2)O (K(HAc) and K(DAc)) and the deuterium isotope effect, ΔpK = pK(DAc) - pK(HAc), have been determined from T = 368 K to T = 548 K at p = 20 MPa, using a flow-through ac conductance cell built at the University of Delaware. Measurements were made on dilute (ionic strength ∼ 10(-4) mol·kg(-1)) solutions of acetic acid, sodium acetate, hydrochloric acid, and sodium chloride in H(2)O and D(2)O, injected in sequence at each temperature and pressure, so that systematic errors in the measured conductance of each solution would cancel. Experimental values for the molar conductivity, Λ, of the strong electrolytes were used to calculate the molar conductivity at infinite dilution, Λ°, using the Fuoss-Hsia-Fernández-Prini (FHFP) equation. These were used to calculate the molar conductivity at infinite dilution for acetic acid which was in turn used to calculate the degree of dissociation and finally the ionization constants of acetic acid. This same procedure was done for the pertinent deuterated solutes in D(2)O. Measured values of log K(HAc), log K(DAc), and ΔpK were obtained to a precision of ±0.008. The present results are in agreement with the only other accurate study at high temperatures and pressures (Mesmer, R. E.; Herting, D. L. J. Solution Chem.1978, 7, 901-913). The deuterium isotope effects, ΔpK, become independent of temperature above ∼420 K, at a value approximately 0.1 unit lower than that at 298 K. These values are ΔpK = 0.43 ± 0.01 and ΔpK = 0.51 ± 0.01, respectively. The temperature dependence of the Walden product ratio, (λ°η)(D(2)O)/(λ°η)(H(2)O), indicates a change in the relative hydration behavior of ions, whereby the effective Stokes radii of the sodium, chloride, and acetate ions in D(2)O relative to H(2)O reverse above ∼423 K. The results also suggest that the greater efficiency of the well-established proton-hopping transport mechanisms for OH(-) and H(3)O

  10. Measurement and Prediction of Effective Thermal Conductivity for Woven Fabric Composites

    NASA Astrophysics Data System (ADS)

    Goo, Nam Seo; Woo, Kyeongsik

    The current paper deals with the measurement and prediction of thermal conductivities for plain weave fabric composites. An experimental apparatus was setup to measure the temperature gradients from which the thermal conductivities were obtained. The thermal conductivities were also calculated using finite element analyses for plain weave unit cell models and then compared with experimental results. In addition, the effect of a phase shift and the fiber volume fraction in the tow on the thermal conductivities was addressed.

  11. Microfabricated AC impedance sensor

    DOEpatents

    Krulevitch, Peter; Ackler, Harold D.; Becker, Frederick; Boser, Bernhard E.; Eldredge, Adam B.; Fuller, Christopher K.; Gascoyne, Peter R. C.; Hamilton, Julie K.; Swierkowski, Stefan P.; Wang, Xiao-Bo

    2002-01-01

    A microfabricated instrument for detecting and identifying cells and other particles based on alternating current (AC) impedance measurements. The microfabricated AC impedance sensor includes two critical elements: 1) a microfluidic chip, preferably of glass substrates, having at least one microchannel therein and with electrodes patterned on both substrates, and 2) electrical circuits that connect to the electrodes on the microfluidic chip and detect signals associated with particles traveling down the microchannels. These circuits enable multiple AC impedance measurements of individual particles at high throughput rates with sufficient resolution to identify different particle and cell types as appropriate for environmental detection and clinical diagnostic applications.

  12. Spatially localized measurement of thermal conductivity using a hybrid photothermal technique

    SciTech Connect

    David H Hurley; Marat Khafizov; Zilong Hua; Rory Kennedy; Heng Ban

    2012-05-01

    A photothermal technique capable of measuring thermal conductivity with micrometer lateral resolution is presented. This technique involves measuring separately the thermal diffusivity, D, and thermal effusivity, e, to extract the thermal conductivity, k=(e2/D)1/2. To generalize this approach, sensitivity analysis was conducted for materials having a range of thermal conductivities. Experimental validation was sought using two substrate materials, SiO2 and CaF2, both coated with thin titanium films. The measured conductivities compare favorably with literature values.

  13. Measurement of Electrical Conductivity into Tomato Cultivation Beds using Small Insertion Type Electrical Conductivity Sensor Designed for Agriculture

    NASA Astrophysics Data System (ADS)

    Kawashima, Kazuko; Futagawa, Masato; Ban, Yoshihiro; Asano, Yoshiyuki; Sawada, Kazuaki

    Our group has studied on-site monitoring sensor for agricultural field. An electrical conductivity (EC) sensor had been fabricated using Si integrated circuit technology. EC information of solutions shows ion concentrations dissolving in water, and can be used as the index of nutrient concentration for plants. So, it is important to measure EC in real time and on site. Because our EC sensor (5mm×5mm in size) is smaller than other commercial ones (several centimeters), it is easy to insert and achieve measurement in rock wool. In this study, our sensor measured long term EC values in tomato cultivation soil and rock wool medium. At first, we calibrated a relationship between output voltages and EC values on the sensor. The sensor was confirmed about enough EC measurement range from 8 to 969mS/m. In long period measurement, the sensor was confirmed about continuous operation for over five months, and intermittent measurement for over a year. In measurement in the cultivation soil, the sensor indicated that water was kept and diffused in the soil. In contrast, it was found that water diffused without keeping in it in rock wool medium. We confirmed our small EC sensor is useful for on-site monitoring and analysis of solution concentration distribution in several kinds of cultivation bed in real time.

  14. Analysis of variance on thickness and electrical conductivity measurements of carbon nanotube thin films

    NASA Astrophysics Data System (ADS)

    Li, Min-Yang; Yang, Mingchia; Vargas, Emily; Neff, Kyle; Vanli, Arda; Liang, Richard

    2016-09-01

    One of the major challenges towards controlling the transfer of electrical and mechanical properties of nanotubes into nanocomposites is the lack of adequate measurement systems to quantify the variations in bulk properties while the nanotubes were used as the reinforcement material. In this study, we conducted one-way analysis of variance (ANOVA) on thickness and conductivity measurements. By analyzing the data collected from both experienced and inexperienced operators, we found some operation details users might overlook that resulted in variations, since conductivity measurements of CNT thin films are very sensitive to thickness measurements. In addition, we demonstrated how issues in measurements damaged samples and limited the number of replications resulting in large variations in the electrical conductivity measurement results. Based on this study, we proposed a faster, more reliable approach to measure the thickness of CNT thin films that operators can follow to make these measurement processes less dependent on operator skills.

  15. Use of tandem circulation wells to measure hydraulic conductivity without groundwater extraction.

    PubMed

    Goltz, Mark N; Huang, Junqi; Close, Murray E; Flintoft, Mark J; Pang, Liping

    2008-09-10

    Conventional methods to measure the hydraulic conductivity of an aquifer on a relatively large scale (10-100 m) require extraction of significant quantities of groundwater. This can be expensive, and otherwise problematic, when investigating a contaminated aquifer. In this study, innovative approaches that make use of tandem circulation wells to measure hydraulic conductivity are proposed. These approaches measure conductivity on a relatively large scale, but do not require extraction of groundwater. Two basic approaches for using circulation wells to measure hydraulic conductivity are presented; one approach is based upon the dipole-flow test method, while the other approach relies on a tracer test to measure the flow of water between two recirculating wells. The approaches are tested in a relatively homogeneous and isotropic artificial aquifer, where the conductivities measured by both approaches are compared to each other and to the previously measured hydraulic conductivity of the aquifer. It was shown that both approaches have the potential to accurately measure horizontal and vertical hydraulic conductivity for a relatively large subsurface volume without the need to pump groundwater to the surface. Future work is recommended to evaluate the ability of these tandem circulation wells to accurately measure hydraulic conductivity when anisotropy and heterogeneity are greater than in the artificial aquifer used for these studies.

  16. AC heat capacities of κ-(BEDT-TTF)2Cu2(CN)3 measured by microchip calorimeter

    NASA Astrophysics Data System (ADS)

    Muraoka, Y.; Yamashita, S.; Yamamoto, T.; Nakazawa, Y.

    2011-09-01

    Thermodynamic measurements of an organic spin liquid compound of κ-(BEDT-TTF)2Cu2(CN)3 where BEDT-TTF is bis(ethylenedithio)tetrathiafulvalene were performed by the ac calorimetry technique using a microchip device of TCG3880. This technique is effective to measure relative temperature and magnetic-field dependences of heat capacity for tiny single crystal samples less than 1μg. Broad hump structures in Cp vs T which are known as so-called 6 K anomaly were observed in κ-(BEDT-TTF)2Cu2(CN)3 and its deuterated compound. The hump temperatures are evaluated as 5.7 K in both compounds. This result demonstrates that the TCG3880 is useful for performing thermodynamic investigations of such kind of organic charge transfer complexes with much reduced sample quantity than the conventional techniques and that the existence of hump structure is intrinsic for κ-(BEDT-TTF)2Cu2(CN)3. The in-plane angular dependence of the magnetic field of 7 T applied parallel to the two dimensional layer is also studied and absence of in-plane anisotropy of the hump structure is discussed in both pristine and deuterated compounds.

  17. Apparatus and method for detecting and/or measuring flaws in conductive material

    DOEpatents

    Hockey, Ronald L.; Riechers, Douglas M.

    2000-01-01

    The present invention uses a magnet and sensor coil unilaterial and in relative motion to a conductive material, to measure perturbation or variation in the magnetic field in the presence of a flaw. A liftoff compensator measures a distance between the conductive material and the magnet.

  18. A Novel Method for Measuring Electrical Conductivity of High Insulating Oil Using Charge Decay

    NASA Astrophysics Data System (ADS)

    Wang, Z. Q.; Qi, P.; Wang, D. S.; Wang, Y. D.; Zhou, W.

    2016-05-01

    For the high insulating oil, it is difficult to measure the conductivity precisely using voltammetry method. A high-precision measurementis proposed for measuring bulk electrical conductivity of high insulating oils (about 10-9--10-15S/m) using charge decay. The oil is insulated and charged firstly, and then grounded fully. During the experimental procedure, charge decay is observed to show an exponential law according to "Ohm" theory. The data of time dependence of charge density is automatically recorded using an ADAS and a computer. Relaxation time constant is fitted from the data using Gnuplot software. The electrical conductivity is calculated using relaxation time constant and dielectric permittivity. Charge density is substituted by electric potential, considering charge density is difficult to measure. The conductivity of five kinds of oils is measured. Using this method, the conductivity of diesel oil is easily measured to beas low as 0.961 pS/m, as shown in Fig. 5.

  19. Studies on structural, thermal and AC conductivity scaling of PEO-LiPF6 polymer electrolyte with added ionic liquid [BMIMPF6

    NASA Astrophysics Data System (ADS)

    Chaurasia, S. K.; Saroj, A. L.; Shalu, Singh, V. K.; Tripathi, A. K.; Gupta, A. K.; Verma, Y. L.; Singh, R. K.

    2015-07-01

    Preparation and characterization of polymer electrolyte films of PEO+10wt.% LiPF6 + xwt.% BMIMPF6 (1-butyl-3-methylimidazolium hexafluorophosphate) containing dopant salt lithium hexafluorophosphate (LiPF6) and ionic liquid (BMIMPF6) having common anion PF6 - are reported. The ionic conductivity of the polymer electrolyte films has been found to increase with increasing concentration of BMIMPF6 in PEO+10 wt.% LiPF6 due to the plasticization effect of ionic liquid. DSC and XRD results show that the crystallinity of polymer electrolyte decreases with BMIMPF6 concentration which, in turn, is responsible for the increase in ionic conductivity. FTIR spectroscopic study shows the complexation of salt and/or ionic liquid cations with the polymer backbone. Ion dynamics behavior of PEO+LiPF6 as well as PEO+LiPF6 + BMIMPF6 polymer electrolytes was studied by frequency dependent conductivity, σ(f) measurements. The values σ(f) at various temperatures have been analyzed in terms of Jonscher power law (JPL) and scaled with respect to frequency which shows universal power law characteristics at all temperatures.

  20. Sodium concentration measurement during hemodialysis through ion-exchange resin and conductivity measure approach: in vitro experiments.

    PubMed

    Tura, Andrea; Sbrignadello, Stefano; Mambelli, Emanuele; Ravazzani, Paolo; Santoro, Antonio; Pacini, Giovanni

    2013-01-01

    Sodium measurement during hemodialysis treatment is important to preserve the patient from clinical events related to hypo- or hyper-natremia Usually, sodium measurement is performed through laboratory equipment which is typically expensive, and requires manual intervention. We propose a new method, based on conductivity measurement after treatment of dialysate solution through ion-exchange resin. To test this method, we performed in vitro experiments. We prepared 40 ml sodium chloride (NaCl) samples at 280, 140, 70, 35, 17.5, 8.75, 4.375 mEq/l, and some "mixed samples", i.e., with added potassium chloride (KCl) at different concentrations (4.375-17.5 mEq/l), to simulate the confounding factors in a conductivity-based sodium measurement. We measured the conductivity of all samples. Afterwards, each sample was treated for 1 min with 1 g of Dowex G-26 resin, and conductivity was measured again. On average, the difference in the conductivity between mixed samples and corresponding pure NaCl samples (at the same NaCl concentration) was 20.9%. After treatment with the exchange resin, it was 14.7%, i.e., 42% lower. Similar experiments were performed with calcium chloride and magnesium chloride as confounding factors, with similar results. We also performed some experiments on actual dialysate solution during hemodialysis sessions in 15 patients, and found that the correlation between conductivity measures and sodium concentration improved after resin treatment (R=0.839 before treatment, R=0.924 after treatment, P<0.0001). We conclude that ion-exchange resin treatment coupled with conductivity measures may improve the measurement of sodium compared to conductivity measures alone, and may become a possible simple approach for continuous and automatic sodium measurement during hemodialysis.

  1. Sodium Concentration Measurement during Hemodialysis through Ion-Exchange Resin and Conductivity Measure Approach: In Vitro Experiments

    PubMed Central

    Tura, Andrea; Sbrignadello, Stefano; Mambelli, Emanuele; Ravazzani, Paolo; Santoro, Antonio; Pacini, Giovanni

    2013-01-01

    Sodium measurement during hemodialysis treatment is important to preserve the patient from clinical events related to hypo- or hyper-natremia Usually, sodium measurement is performed through laboratory equipment which is typically expensive, and requires manual intervention. We propose a new method, based on conductivity measurement after treatment of dialysate solution through ion-exchange resin. To test this method, we performed in vitro experiments. We prepared 40 ml sodium chloride (NaCl) samples at 280, 140, 70, 35, 17.5, 8.75, 4.375 mEq/l, and some “mixed samples”, i.e., with added potassium chloride (KCl) at different concentrations (4.375-17.5 mEq/l), to simulate the confounding factors in a conductivity-based sodium measurement. We measured the conductivity of all samples. Afterwards, each sample was treated for 1 min with 1 g of Dowex G-26 resin, and conductivity was measured again. On average, the difference in the conductivity between mixed samples and corresponding pure NaCl samples (at the same NaCl concentration) was 20.9%. After treatment with the exchange resin, it was 14.7%, i.e., 42% lower. Similar experiments were performed with calcium chloride and magnesium chloride as confounding factors, with similar results. We also performed some experiments on actual dialysate solution during hemodialysis sessions in 15 patients, and found that the correlation between conductivity measures and sodium concentration improved after resin treatment (R=0.839 before treatment, R=0.924 after treatment, P<0.0001). We conclude that ion-exchange resin treatment coupled with conductivity measures may improve the measurement of sodium compared to conductivity measures alone, and may become a possible simple approach for continuous and automatic sodium measurement during hemodialysis. PMID:23844253

  2. Measurement of Thermal Conductivity of Suspension for Ice Storage by Transient Hot Wire Method

    NASA Astrophysics Data System (ADS)

    Matsumoto, Koji; Obara, Keisuke; Okada, Masashi; Kawagoe, Tetsuo; Kang, Chaedong

    We have been studying on a suspension as a new thermal storage material. The suspension is made from silicone oil-water mixture with some additive or water with that by cooling with stirring. When designing the ice storage system using this suspension, the thermal conductivity of the suspension is essential. The purpose of this study is to measure a thermal conductivity of the ice-oil or ice-water suspension with good fluidity. The thermal conductivity was measured by at ransient hot wire method. In this study, the relationship between thermal conductivity and IPF was clarified, and thermal conductivity was expressed as a function of IPF. Moreover, the uncertainty of measurement of the thermal conductivity was estimated.

  3. Conductivity of individual particles measured by a microscopic four-point-probe method

    PubMed Central

    Sun, Ling; Wang, Jianjun; Bonaccurso, Elmar

    2013-01-01

    We introduce a technique for measuring the conductivity of individual hybrid metal, semiconducting core-shell and full-metal conducting particles by a microscopic four-point probe (μ-4PP) method. The four-point probe geometry allows for minimizing contact resistances between electrodes and particles. By using a focused ion beam we fabricate platinum nanoleads between four microelectrodes on a silicon chip and an individual particle, and determine the particle's conductivity via sensitive current and voltage measurements. Up to sixteen particles can be taken up by each chip, which allows for multiple conductivity measurements by simply multiplexing the electric contacts connected to a multimeter. Although, for demonstration, we used full Au (conducting) and Ag-coated latex particles (semiconducting) of a few micrometers in diameter, the method can be applied to other types of conducting or semiconducting particles of different diameters. PMID:23771149

  4. Development of an in situ thermal conductivity measurement system for exploration of the shallow subsurface

    NASA Astrophysics Data System (ADS)

    Chirila, Marian Andrei; Christoph, Benjamin; Vienken, Thomas; Dietrich, Peter; Bumberger, Jan

    2016-06-01

    In this study, we attempted to develop an in situ thermal conductivity measurement system that can be used for subsurface thermal exploration. A new thermal probe was developed for mapping both the spatial and temporal variability of thermal conductivity, via direct push methods in the unconsolidated shallow subsurface. A robust, hollow cylindrical probe was constructed and its performance was tested by carrying out thermal conductivity measurements on materials with known properties. The thermal conductivity of the investigated materials can be worked out by measuring the active power consumption (in alternating current system) and temperature of the probe over fixed time intervals. A calibration method was used to eliminate any undesired thermal effects regarding the size of the probe, based on mobile thermal analyzer thermal conductivity values. Using the hollow cylindrical probe, the thermal conductivity results obtained had an error of less than 2.5% for solid samples (such as Teflon, Agar Jelly and Nylatron).

  5. Measurement of electrical conduction properties of intact embryonic murine hearts by extracellular microelectrode arrays.

    PubMed

    Taylor, David G; Natarajan, Anupama

    2012-01-01

    The study of the embryonic development of the cardiac conduction system and its congenital and toxicological defects requires protocols to measure electrical conduction through the myocardium. However, available methods either lack spatial information, necessitate the hearts to be sliced and mounted, or require specialized equipment. Microelectrode arrays (MEAs) are plates with embedded surface electrodes to measure localized extracellular ionic currents (field potentials) created by the depolarization and repolarization of cultured cells and tissue slices. Here we describe a protocol using MEAs to examine electrical conduction through intact and beating cultured hearts isolated from mouse embryos at 10.5 days postcoitus. This method allows measurements of conduction time, estimates of conduction velocity, atrioventricular conduction delay and block, and heart rate and rhythmicity.

  6. Thermal-Conductivity Apparatus for Steady-State, Comparative Measurement of Ceramic Coatings.

    PubMed

    Slifka, A J

    2000-01-01

    An apparatus has been developed to measure the thermal conductivity of ceramic coatings. Since the method uses an infrared microscope for temperature measurement, coatings as thin as 20 μm can, in principle, be measured using this technique. This steady-state, comparative measurement method uses the known thermal conductivity of the substrate material as the reference material for heat-flow measurement. The experimental method is validated by measuring a plasma-sprayed coating that has been previously measured using an absolute, steady-state measurement method. The new measurement method has a relative standard uncertainty of about 10 %. The measurement of the plasma-sprayed coating gives 0.58 W·m(-1)·K(-l) which compares well with the 0.62 W·m(-1)·K(-l) measured using the absolute method.

  7. Thermal-Conductivity Apparatus for Steady-State, Comparative Measurement of Ceramic Coatings

    PubMed Central

    Slifka, A. J.

    2000-01-01

    An apparatus has been developed to measure the thermal conductivity of ceramic coatings. Since the method uses an infrared microscope for temperature measurement, coatings as thin as 20 μm can, in principle, be measured using this technique. This steady-state, comparative measurement method uses the known thermal conductivity of the substrate material as the reference material for heat-flow measurement. The experimental method is validated by measuring a plasma-sprayed coating that has been previously measured using an absolute, steady-state measurement method. The new measurement method has a relative standard uncertainty of about 10 %. The measurement of the plasma-sprayed coating gives 0.58 W·m−1·K−l which compares well with the 0.62 W·m−1·K−l measured using the absolute method. PMID:27551628

  8. A simple AC calorimeter for specific heat measurement of liquids confined in porous materials: A study of hydrated Vycor

    NASA Astrophysics Data System (ADS)

    Bonetti, Marco; Zanotti, Jean-Marc

    2016-09-01

    Nanometric confinement of fluids in porous media is a classical way to stabilize metastable states. Calorimetric studies give insight on the behavior of confined liquids compared to bulk liquids. We have developed and built a simple quasi-adiabatic AC calorimeter for heat capacity measurement of confined liquids in porous media in a temperature range between 150 K and 360 K. Taking the fully hydrated porous medium as a reference, we address the thermal behavior of water as a monolayer on the surface of a porous silica glass (Vycor). For temperature ranging between 160 K and 325 K, this interfacial water shows a surprisingly large heat capacity. We describe the interfacial Hbond network in the framework of a mean field percolation model, to show that at 160 K interfacial water experiences a transformation from low density amorphous ice to a heterogeneous system where transient low and high density water patches coexist. The fraction of each species is controlled by the temperature. We identify the large entropy of the interfacial water molecules as the cause of this behaviour.

  9. Evaluation of modern IGBT-modules for hard-switched AC/DC/AC converters

    SciTech Connect

    Blaabjerg, F.; Pedersen, J.K.; Jaeger, U.

    1995-12-31

    The development of IGBT devices is still producing faster devices with lower losses. The applications become more advanced like a complete hard-switched AC/DC/AC converter with almost clean input current and regenerating capabilities. This paper will first focus on a detailed characterization and comparison of eight different IGBT-modules representing state-of-the-art for both PT and NPT technologies. The voltage level of the devices is 1,200V and 1,600V/1,700V. The characterization is done on an advanced measurement system which is briefly described. The characterization is based on static and dynamic tests for both IGBT and the diodes in the IGBT-modules at a junction temperature at 125 C. The comparison is first done directly based on conduction losses and switching losses, and later the measurements are used in a loss model for a complete AC/DC/AC converter application. In the AC/DC/AC converter the power losses are modelled, and different operating conditions are compared like different voltage levels in the DC-link. It is concluded dependent on operation conditions different devices will be preferable, but the high voltage devices have the highest losses even at a high operating voltage.

  10. Length Dependent Thermal Conductivity Measurements Yield Phonon Mean Free Path Spectra in Nanostructures

    PubMed Central

    Zhang, Hang; Hua, Chengyun; Ding, Ding; Minnich, Austin J.

    2015-01-01

    Thermal conductivity measurements over variable lengths on nanostructures such as nanowires provide important information about the mean free paths (MFPs) of the phonons responsible for heat conduction. However, nearly all of these measurements have been interpreted using an average MFP even though phonons in many crystals possess a broad MFP spectrum. Here, we present a reconstruction method to obtain MFP spectra of nanostructures from variable-length thermal conductivity measurements. Using this method, we investigate recently reported length-dependent thermal conductivity measurements on SiGe alloy nanowires and suspended graphene ribbons. We find that the recent measurements on graphene imply that 70% of the heat in graphene is carried by phonons with MFPs longer than 1 micron. PMID:25764977

  11. Absolute Steady-State Thermal Conductivity Measurements by Use of a Transient Hot-Wire System.

    PubMed

    Roder, H M; Perkins, R A; Laesecke, A; Nieto de Castro, C A

    2000-01-01

    A transient hot-wire apparatus was used to measure the thermal conductivity of argon with both steady-state and transient methods. The effects of wire diameter, eccentricity of the wire in the cavity, axial conduction, and natural convection were accounted for in the analysis of the steady-state measurements. Based on measurements on argon, the relative uncertainty at the 95 % level of confidence of the new steady-state measurements is 2 % at low densities. Using the same hot wires, the relative uncertainty of the transient measurements is 1 % at the 95 % level of confidence. This is the first report of thermal conductivity measurements made by two different methods in the same apparatus. The steady-state method is shown to complement normal transient measurements at low densities, particularly for fluids where the thermophysical properties at low densities are not known with high accuracy.

  12. Thermal conductivity measurements of particulate materials: 5. Effect of bulk density and particle shape

    NASA Astrophysics Data System (ADS)

    Presley, Marsha A.; Christensen, Philip R.

    2010-07-01

    Thermal conductivities were measured with a line-heat source for three particulate materials with different particle shapes under low pressures of a carbon dioxide atmosphere and various bulk densities. Less than 2 μm kaolinite exhibited a general decrease in thermal conductivity with increasing bulk density. For the range of atmospheric pressures appropriate for Mars, a reduction in porosity of 24% decreased the thermal conductivity by 24%. Kaolinite manifests considerable anisotropy with respect to thermal conductivity. As the particles align the bulk thermal conductivity measured increasingly reflects the thermal conductivity of the short axis. When kyanite is crushed, it forms blady particles that will also tend to align with increasing bulk density. Without any intrinsic anisotropy, however, kyanite particles, like other particulates exhibit an increase in thermal conductivity with increasing bulk density. Under Martian atmospheric pressures, a reduction in porosity of 30% produces a 30% increase in thermal conductivity. Diatomaceous earth maintains a very low bulk density due to the highly irregular shape of the individual particles. A decrease in porosity of 17% produces an increase in thermal conductivity of 27%. The trends in thermal conductivity with bulk density, whether increasing or decreasing, are often not smooth. Whether oscillations in the trends presented in this paper and elsewhere have any physical significance or whether they are merely artifacts of the precision error is unclear. Clarification of this question may not be possible without higher-precision measurements from future laboratories and further development of theoretical modeling.

  13. Influence of the sample mounting on thermal conductance measurements using PPMS TTO option

    NASA Astrophysics Data System (ADS)

    Sebek, J.; Santava, E.

    2009-02-01

    We discuss the performance of the automated heat conductivity measurement system manufactured by the Quantum Design, Inc. The Thermal Transport Option implemented into the Physical Properties Measurement System (PPMS) measures the thermal transport properties of materials (thermal conductivity, Seebeck coefficient and electrical resistivity simultaneously) in the temperature range 1.8 - 395 K and in magnetic fields generated by the installed superconducting solenoid. Recently, discrepancies up to 30% in measured quantities at 390 K have been reported. We critically analyze the experimental method used to measure the above mentioned quantities and show possible sources of problems.

  14. Thickness measurement of multi-layer conductive coatings using multifrequency eddy current techniques

    NASA Astrophysics Data System (ADS)

    Zhang, Dejun; Yu, Yating; Lai, Chao; Tian, Guiyun

    2016-07-01

    To ensure the key structural performance in high-temperature and high-stress environments, thermal barrier coatings (TBCs) are often adopted in engineering. The thickness of these multi-layer conductive coatings is an important quality indicator. In order to measure the thickness of multi-layer conductive coatings, a new measurement approach is presented using eddy current testing techniques, and then, an inversion algorithm is proposed and proved efficient and applicable, of which the maximum experimental relative error is within 10%. Therefore, the new approach can be effectively applied to thickness measurement of multi-layer conductive coatings such as TBCs.

  15. Differential heating: A versatile method for thermal conductivity measurements in high-energy-density matter

    NASA Astrophysics Data System (ADS)

    Ping, Y.; Fernandez-Panella, A.; Sio, H.; Correa, A.; Shepherd, R.; Landen, O.; London, R. A.; Sterne, P. A.; Whitley, H. D.; Fratanduono, D.; Boehly, T. R.; Collins, G. W.

    2015-09-01

    We propose a method for thermal conductivity measurements of high energy density matter based on differential heating. A temperature gradient is created either by surface heating of one material or at an interface between two materials by different energy deposition. The subsequent heat conduction across the temperature gradient is observed by various time-resolved probing techniques. Conceptual designs of such measurements using laser heating, proton heating, and x-ray heating are presented. The sensitivity of the measurements to thermal conductivity is confirmed by simulations.

  16. Differential heating: A versatile method for thermal conductivity measurements in high-energy-density matter

    DOE PAGES

    Ping, Y.; Fernandez-Panella, A.; Sio, H.; ...

    2015-09-04

    We propose a method for thermal conductivity measurements of high energy density matter based on differential heating. A temperature gradient is created either by surface heating of one material or at an interface between two materials by different energy deposition. The subsequent heat conduction across the temperature gradient is observed by various time-resolved probing techniques. Conceptual designs of such measurements using laser heating, proton heating, and x-ray heating are presented. As a result, the sensitivity of the measurements to thermal conductivity is confirmed by simulations.

  17. Differential heating: A versatile method for thermal conductivity measurements in high-energy-density matter

    SciTech Connect

    Ping, Y.; Fernandez-Panella, A.; Correa, A.; Shepherd, R.; Landen, O.; London, R. A.; Sterne, P. A.; Whitley, H. D.; Fratanduono, D.; Collins, G. W.; Sio, H.; Boehly, T. R.

    2015-09-15

    We propose a method for thermal conductivity measurements of high energy density matter based on differential heating. A temperature gradient is created either by surface heating of one material or at an interface between two materials by different energy deposition. The subsequent heat conduction across the temperature gradient is observed by various time-resolved probing techniques. Conceptual designs of such measurements using laser heating, proton heating, and x-ray heating are presented. The sensitivity of the measurements to thermal conductivity is confirmed by simulations.

  18. Evaluation of DLVO theory with disjoining-pressure and film-conductance measurements of common-black films stabilized with sodium dodecyl sulfate.

    PubMed

    Yaros, Heather D; Newman, John; Radke, C J

    2003-06-15

    We develop a unique film holder combining a thin-film balance with AC impedance spectroscopy to measure disjoining pressure, film conductance, and film thickness simultaneously. Foam films stabilized by sodium dodecyl sulfate (SDS) are investigated with and without added sodium chloride (NaCl) electrolyte. Classical colloidal theory, Derjaguin, Landau, Verwey, and Overbeek (DLVO) theory, is tested rigorously over a wide range of solution conditions by comparing the surface charge densities fit to disjoining-pressure isotherms with those estimated independently from film-conductance and surface-tension data. Film-conductance measurements strongly suggest that the adsorbed anionic surfactant is partially complexed with counterions. Therefore, to reconcile the different values of charge densities calculated from surface tension and film conductance with those from disjoining pressure, we propose a simple ion-binding electrostatic model. The ion-complexation framework predicts increased ion complexing with increasing solution ionic strength, in agreement with surface-tension and film-conductance data. Unfortunately, it is not possible to describe similarly the trends of the measured disjoining-pressure isotherms because the diffuse-layer charge density increases, or equivalently, the ion complexation decreases with increasing ionic strength. Accordingly, the ion-binding extension of classical DLVO theory does not permit agreement between theory and independent experimental data from surface tension, disjoining pressure, and film conductance.

  19. On the van der Pauw's method applied to the measurement of low thermal conductivity materials.

    PubMed

    Morales, C; Flores, E; Bodega, J; Leardini, F; Ferrer, I J; Ares, J R; Sánchez, C

    2016-08-01

    The electrical van der Pauw's method has recently been extended to measure the thermal conductivity of different elements and compounds. This technique provides an easy way to determine the sample in-plane thermal conductivity by avoiding the influence of the thermal contact resistances. However, the reported calculated error values appear to be underestimated when dealing with the materials with low thermal conductivity (<5 W/Km) at room temperature. The causes of this underestimation are investigated in this communication and it has been found that they are due to the drastic influence of conduction heat losses through the thermo-resistance wires as well as the resulting modification of the sample temperature map. Both phenomena lead to experimental values of the sample thermal conductivity, which are systematically higher than the tabulated ones. The magnitude of this systematic error is ∼100% dealing with the samples of macroscopic dimensions, and low thermal conductivity indicated that the obtained accurate measurements can be quite challenging.

  20. On the van der Pauw's method applied to the measurement of low thermal conductivity materials

    NASA Astrophysics Data System (ADS)

    Morales, C.; Flores, E.; Bodega, J.; Leardini, F.; Ferrer, I. J.; Ares, J. R.; Sánchez, C.

    2016-08-01

    The electrical van der Pauw's method has recently been extended to measure the thermal conductivity of different elements and compounds. This technique provides an easy way to determine the sample in-plane thermal conductivity by avoiding the influence of the thermal contact resistances. However, the reported calculated error values appear to be underestimated when dealing with the materials with low thermal conductivity (<5 W/Km) at room temperature. The causes of this underestimation are investigated in this communication and it has been found that they are due to the drastic influence of conduction heat losses through the thermo-resistance wires as well as the resulting modification of the sample temperature map. Both phenomena lead to experimental values of the sample thermal conductivity, which are systematically higher than the tabulated ones. The magnitude of this systematic error is ˜100% dealing with the samples of macroscopic dimensions, and low thermal conductivity indicated that the obtained accurate measurements can be quite challenging.

  1. Measurements of Electrical and Thermal Conductivity of Iron Under Earth's Core Conditions

    NASA Astrophysics Data System (ADS)

    Ohta, K.; Kuwayama, Y.; Shimizu, K.; Yagi, T.; Hirose, K.; Ohishi, Y.

    2014-12-01

    Secular cooling of the Earth's core induces the convection of the conductive liquid outer core, which generates the geomagnetic field, and the growth of the solid inner core. Since iron is the primary component of the Earth's core, the electrical and thermal conductivity of iron in both solid and liquid states are key pieces of information for estimating the transport properties of the core. We performed electrical and thermal conductivity measurements on iron under core conditions in a laser-heated diamond anvil cell. Our electrical conductivity measurements on iron clearly show resistivity saturation phenomena in iron under high pressure and high temperature conditions as predicted in a recent laboratory-based model for the core conductivity (Gomi et al., 2013). Direct measurements of thermal diffusivity of iron have been also preformed at high pressures by using the pulsed light heating thermoreflectance technique, which enable us to confirm the validity of the Wiedemann-Franz law toward transition metal under high pressure.

  2. Microstructure, AC impedance and DC electrical conductivity characteristics of NiFe2-xGdxO4 (x = 0, 0.05 and 0.075)

    NASA Astrophysics Data System (ADS)

    Kamala Bharathi, K.; Markandeyulu, G.; Ramana, C. V.

    2012-03-01

    The structure and electrical characteristics of Gd doped Ni ferrite materials, namely NiFe1.95Gd0.05O4 and NiFe1.925Gd0.075O4, are reported to demonstrate their improved electrical properties compared to that of pure NiFe2O4. NiFe1.95Gd0.05O4 and NiFe1.925Gd0.075O4 compounds crystallize in the cubic inverse spinel phase with a very small amount of GdFeO3 additional phase while pure NiFe2O4 crystallize in inverse spinel phase without any impurity phase. The back scattered electron imaging analysis indicate the primary and secondary formation in NiFe1.95Gd0.05O4 and NiFe1.925Gd0.075O4 compounds. Atomic force microscopy measurements indicate that the bulk grains are ˜2-5 micron size while the grain boundaries are thin compared to bulk grains. Impedance spectroscopic analysis at different temperature indicates the different relaxation mechanisms and their variation with temperature, bulk grain and grain-boundary contributions to the electrical conductivity (Rg) and capacitance (Cg) of these materials. The conductivity in pure NiFeO4 is found to be predominantly due to intrinsic bulk contribution (Rg=213 kΩ and Cg=4.5 x 10-8 F). In the case of NiFe1.95Gd0.05O4 and NiFe1.925Gd0.075O4 compounds, grain and grain-boundary contributions to the conductivity are clearly observed. The DC conductivity values (at 300 K) of NiFe2O4, NiFe1.95Gd0.05O4 and NiFe1.925Gd0.075O4 compounds are found to be 1.06 x 10-7 Ω-1 cm-1, 5.73 x 10-8 Ω-1 cm-1 and 1.28 x 10-8 Ω-1 cm-1 respectively.

  3. Thermal conductivity measurement of the He-ion implanted layer of W using transient thermoreflectance technique

    NASA Astrophysics Data System (ADS)

    Qu, Shilian; Li, Yuanfei; Wang, Zhigang; Jia, Yuzhen; Li, Chun; Xu, Ben; Chen, Wanqi; Bai, Suyuan; Huang, Zhengxing; Tang, Zhenan; Liu, Wei

    2017-02-01

    Transient thermoreflectance method was applied on the thermal conductivity measurement of the surface damaged layer of He-implanted tungsten. Uniform damages tungsten surface layer was produced by multi-energy He-ion implantation with thickness of 450 nm. Result shows that the thermal conductivity is reduced by 90%. This technique was further applied on sample with holes on the surface, which was produced by the He-implanted at 2953 K. The thermal conductivity decreases to 3% from the bulk value.

  4. Molecular origins of conduction channels observed in shot-noise measurements.

    PubMed

    Solomon, Gemma C; Gagliardi, Alessio; Pecchia, Alessandro; Frauenheim, Thomas; Di Carlo, Aldo; Reimers, Jeffrey R; Hush, Noel S

    2006-11-01

    Measurements of shot noise from single molecules have indicated the presence of various conduction channels. We present three descriptions of these channels in molecular terms showing that the number of conduction channels is limited by bottlenecks in the molecule and that the channels can be linked to transmission through different junction states. We introduce molecular-conductance orbitals, which allow the transmission to be separated into contributions from individual orbitals and contributions from interference between pairs of orbitals.

  5. 3ω slope comparative method for fluid and powder thermal conductivity measurements

    NASA Astrophysics Data System (ADS)

    Zheng, X. H.; Qiu, L.; Yue, P.; Wang, G.; Tang, D. W.

    2016-09-01

    By analyzing the relationship among the heat penetration depth, measurement frequency and detector characteristic parameters, a simple and practical 3ω slope comparative method has been proposed. The corresponding measurement system for measuring the thermal properties of fluids and powder materials was established and verified using several specimens with known thermophysical parameters, such as alcohol, distilled water, and air. Compared to the two-dimensional model, the data processing of the method is relatively simple and quick. Due to the elimination of errors introduced by the detector parameter measurement, the measurement accuracy of the method is higher than the conventional one-dimensional model. By using an appropriate frequency range, the new method is time saving and convenient for measuring the thermal conductivity of fluids and powders with low thermal conductivity. Based on the analysis, the effective thermal conductivity of nano-SiO2 powder is accurately determined.

  6. IN SITU APPARENT CONDUCTIVITY MEASUREMENTS AND MICROBIAL POPULATION DISTRIBUTION AT A HYDROCARBON CONTAMINATED SITE

    EPA Science Inventory

    We investigated the bulk electrical conductivity and microbial population distribution in sediments at a site contaminated with light non-aqueous phase liquid (LNAPL). The bulk conductivity was measured using in situ vertical resistivity probes, while the most probable number met...

  7. MEASURING VERTICAL PROFILES OF HYDRAULIC CONDUCTIVITY WITH IN SITU DIRECT-PUSH METHODS

    EPA Science Inventory

    U.S. EPA (Environmental Protection Agency) staff developed a field procedure to measure hydraulic conductivity using a direct-push system to obtain vertical profiles of hydraulic conductivity. Vertical profiles were obtained using an in situ field device-composed of a
    Geopr...

  8. The Thermal Conductivity Measurements of Solid Samples by Heat Flux Differantial Scanning Calorimetry

    NASA Astrophysics Data System (ADS)

    Kök, M.; Aydoǧdu, Y.

    2007-04-01

    The thermal conductivity of polyvinylchloride (PVC), polysytrene (PS) and polypropylene (PP) were measured by heat flux DSC. Our results are in good agreement with the results observed by different methods.

  9. Measuring the sedimentation rate in a magnetorheological fluid column via thermal conductivity monitoring

    NASA Astrophysics Data System (ADS)

    Cheng, Haibin; Zhang, Xiaopeng; Liu, Guizhen; Ma, Wentao; Wereley, Norman M.

    2016-05-01

    Measuring sedimentation rate of magnetorheological fluids (MRFs) is of great importance when designing and synthesizing MRFs for engineering applications. A method of characterizing sedimentation rate in an MRF column is proposed utilizing thermal conductivity correlated with particle concentration. A series of MRF samples composed of carbonyl iron particles suspended in silicone oil were prepared, and their concentrations (measured as volume fraction, ∅) and thermal conductivities, k, were tested. A calibration curve was developed to relate particle concentration, ∅, to thermal conductivity, k, using this set of MRF samples with known concentration. The particle concentration, ∅, in the MRF column was then monitored by measuring thermal conductivities (k) at a fixed location and using this calibration relationship. Finally, sedimentation rate in the MRF column was determined by examining how particle concentration varied with time. The sedimentation rate measured in the MRF column was validated using visual observation of mudline (boundary between the topmost clarified fluid zone and MRF below).

  10. Electronic energy gap of molecular hydrogen from electrical conductivity measurements at high shock pressures

    NASA Technical Reports Server (NTRS)

    Nellis, W. J.; Mitchell, A. C.; Mccandless, P. C.; Erskine, D. J.; Weir, S. T.

    1992-01-01

    Electrical conductivities were measured for liquid D2 and H2 shock compressed to pressures of 10-20 GPa (100-200 kbar), molar volumes near 8 cu cm/mol, and calculated temperatures of 2900-4600 K. The semiconducting energy gap derived from the conductivities is 12 eV, in good agreement with recent quasi-particle calculations and with oscillator frequencies measured in diamond-anvil cells.

  11. Thermal Conductivity Measurement Setup for Low Temperature Characterization of Laser Materials

    DTIC Science & Technology

    2014-09-01

    supplied to the lower heater . ............................7 Fig. 5 Our experimental results for thermal conductivity of undoped single-crystal YAG as...lower heater at each test temperature and the steady-state thermal gradient between the two copper plates was measured. With these results, we were able... Thermal Conductivity Measurement Setup for Low Temperature Characterization of Laser Materials by Zachary D Fleischman and Tigran Sanamyan

  12. System to measure accurate temperature dependence of electric conductivity down to 20 K in ultrahigh vacuum.

    PubMed

    Sakai, C; Takeda, S N; Daimon, H

    2013-07-01

    We have developed the new in situ electrical-conductivity measurement system which can be operated in ultrahigh vacuum (UHV) with accurate temperature measurement down to 20 K. This system is mainly composed of a new sample-holder fixing mechanism, a new movable conductivity-measurement mechanism, a cryostat, and two receptors for sample- and four-probe holders. Sample-holder is pushed strongly against the receptor, which is connected to a cryostat, by using this new sample-holder fixing mechanism to obtain high thermal conductivity. Test pieces on the sample-holders have been cooled down to about 20 K using this fixing mechanism, although they were cooled down to only about 60 K without this mechanism. Four probes are able to be touched to a sample surface using this new movable conductivity-measurement mechanism for measuring electrical conductivity after making film on substrates or obtaining clean surfaces by cleavage, flashing, and so on. Accurate temperature measurement is possible since the sample can be transferred with a thermocouple and∕or diode being attached directly to the sample. A single crystal of Bi-based copper oxide high-Tc superconductor (HTSC) was cleaved in UHV to obtain clean surface, and its superconducting critical temperature has been successfully measured in situ. The importance of in situ measurement of resistance in UHV was demonstrated for this HTSC before and after cesium (Cs) adsorption on its surface. The Tc onset increase and the Tc offset decrease by Cs adsorption were observed.

  13. Magnetic resonance electrical impedance tomography for measuring electrical conductivity during electroporation.

    PubMed

    Kranjc, M; Bajd, F; Serša, I; Miklavčič, D

    2014-06-01

    The electroporation effect on tissue can be assessed by measurement of electrical properties of the tissue undergoing electroporation. The most prominent techniques for measuring electrical properties of electroporated tissues have been voltage-current measurement of applied pulses and electrical impedance tomography (EIT). However, the electrical conductivity of tissue assessed by means of voltage-current measurement was lacking in information on tissue heterogeneity, while EIT requires numerous additional electrodes and produces results with low spatial resolution and high noise. Magnetic resonance EIT (MREIT) is similar to EIT, as it is also used for reconstruction of conductivity images, though voltage and current measurements are not limited to the boundaries in MREIT, hence it yields conductivity images with better spatial resolution. The aim of this study was to investigate and demonstrate the feasibility of the MREIT technique for assessment of conductivity images of tissues undergoing electroporation. Two objects were investigated: agar phantoms and ex vivo liver tissue. As expected, no significant change of electrical conductivity was detected in agar phantoms exposed to pulses of all used amplitudes, while a considerable increase of conductivity was measured in liver tissue exposed to pulses of different amplitudes.

  14. Design and Use of a Novel Apparatus for Measuring Capsule Fill Hole Conductance

    SciTech Connect

    Seugling, R M; Nederbragt, W W; Klingmann, J L; Edson, S; Reynolds, J; Cook, R

    2006-11-27

    Description and results of a novel apparatus for determining the flow conductance through a laser drilled hole in a spherical shell for inertial confinement fusion experiments are described. The instrument monitors the pressure of an enclosed volume containing the laser pressure drilled capsule as air bleeds through the hole into the shell. From these measurements one obtains the conductance of the fill hole. This system has proven to be a valuable tool for verifying the conduct conductance into the capsule in a timely and nondestructive manner.

  15. Uncertainty Of The Measurement Of DC Conductivity Of Eramics At Elevated Temperatures

    NASA Astrophysics Data System (ADS)

    Štubňa, Igor; Trnovcová, Viera; Vozár, Libor; Csáki, Štefan

    2015-01-01

    The electrical DC conductivity is measured at room and elevated temperatures on green ceramic samples prepared from kaolin. The arrangement of the sample, with two platinum wire electrodes inserted in the kaolin prism that was used is suitable for measurements of temperature dependences of the DC conductivity from 20 °C to 1100 °C in the air. The uncertainty analysis taking into account thermal expansion of the sample, homogeneity of the temperature field, measurement regime, corrosion of the electrodes, and overlapping of the electrodes is done for 1000 °C. Uncertainties connected with current and voltage measurements and uncertainties connected with the instruments that were used are also considered. The sum of all the partial uncertainties gives an expanded uncertainty of the conductivity measurement. The uncertainty varies with temperature and reaches the value of ˜ 6.5% at 1000 °C.

  16. Measurements of interfacial thermal contact conductance between pressed alloys at low temperatures

    NASA Astrophysics Data System (ADS)

    Zheng, Jiang; Li, Yanzhong; Chen, Pengwei; Yin, Geyuan; Luo, Huaihua

    2016-12-01

    Interfacial thermal contact conductance is the primary factor limiting the heat transfer in many cryogenic engineering applications. This paper presents an experimental apparatus to measure interfacial thermal contact conductance between pressed alloys in a vacuum environment at low temperatures. The measurements of thermal contact conductance between pressed alloys are conducted by using the developed apparatus. The results show that the contact conductance increases with the decrease of surface roughness, the increase of interface temperature and contact pressure. The temperature dependence of thermal conductivity and mechanical properties is analyzed to explain the results. Thermal contact conductance of a pair of stainless steel specimens is obtained in the interface temperature range of 135-245 K and in the contact pressure range of 1-9 MPa. The results are regressed as a power function of temperature and load. Thermal conductance is also obtained between aluminums as well as between stainless steel and aluminum. The load exponents of the regressed relations for different contacts are compared. Existing theoretical models (the Cooper-Mikic-Yovanovich plastic model, the Mikic elastic model and the improved Kimura model) are reviewed and compared with the experimental results. The Cooper-Mikic-Yovanovich model predictions are found to be in good agreement with experimental results, especially with measurements between aluminums.

  17. Examination of Humidity Effects on Measured Thickness and Interfacial Phenomena of Exfoliated Graphene on SiO2 via AC-AFM

    NASA Astrophysics Data System (ADS)

    Jinkins, Katherine; Camacho, Jorge; Farina, Lee; Wu, Yan

    2015-03-01

    Tapping (AC) mode Atomic Force Microscopy (AFM) is commonly used to determine the thickness of graphene samples. However, AFM measurements have been shown to be sensitive to environmental conditions such as adsorbed water, in turn dependent on relative humidity (RH). In the present study, AC-AFM is used to measure the thickness and loss tangent of exfoliated graphene on silicon dioxide (SiO2) as RH is increased from 10% to 80%. We show that the measured thickness of graphene is dependent on RH. Loss tangent is an AFM imaging technique that interprets the phase information as a relationship between the stored and dissipated energy in the tip-sample interaction. This study demonstrates the loss tangent of the graphene and oxide regions are both affected by humidity, with generally higher loss tangent for graphene than SiO2. As RH increases, we observe the loss tangent of both materials approaches the same value. We hypothesize that there is a layer of water trapped between the graphene and SiO2 substrate to explain this observation. Using this interpretation, the loss tangent images also indicate movement and change in this trapped water layer as RH increases, which impacts the measured thickness of graphene using AC-AFM.

  18. Thermal conductivity measurements using hot-wires at small Peclet number

    NASA Astrophysics Data System (ADS)

    Arwatz, Gilad; Fan, Yuyang; Hultmark, Marcus

    2015-11-01

    The feasibility of using hot-wires to measure gas thermal conductivity is investigated. When the local Peclet number of a hot-wire is small (Pe<<1), molecular diffusion dominates the heat transport, and the wire becomes less sensitive to velocity. This phenomenon can be utilized to measure the thermal conductivity of the gas. To investigate the viability of the principle of operation, a lumped capacitance model is proposed, capturing the effects of both convection and conduction on heat transfer from the wire. By investigating the sensitivity of the model to velocity, temperature and conduction, it is shown that as wire dimension decreases, the sensor becomes less sensitive to both velocity and temperature and more sensitive to conduction. The model also captures the effect of varying wire dimension as well as overheat ratio.

  19. Perceptions of breath alcohol concentration (BrAC) levels among a sample of bar patrons with BrAC values of 0.08% or higher.

    PubMed

    Martin, Ryan J; Chaney, Beth H; Cremeens-Matthews, Jennifer; Vail-Smith, Karen

    2016-09-01

    Breath alcohol concentration (BrAC) is a commonly used measure of alcohol intoxication. Because of the potential negative consequences of excessive alcohol consumption, it is important to examine how accurately intoxicated individuals can estimate their BrAC values, especially individuals over the legal BrAC driving threshold (i.e., 0.08%). To better understand perceptions of BrAC values among intoxicated individuals, this field study examined actual BrAC values and BrAC range estimates (0.08% and above, 0.02-0.07%, less than 0.02%) among a sample of bar patrons (N = 454) with BrAC levels at 0.08% or higher. Bivariate and multivariate analyses were conducted to examine the relationship between actual BrAC values and perceived BrAC levels. We also examined whether the following demographic and drinking variables were associated with underestimating BrAC in this sample: gender, age, race, college student status, plans to get home, and hazardous drinking. Results indicated that the majority (60.4%) of participants underestimated their BrAC (i.e., less than 0.08%) and lower BrAC values correlated with underestimating BrAC ranges (p < .001, 95% CI[0.2, 0.6]). Further, females (p = .001, 95% CI[1.3, 3.3]) and participants under 21 (p = .039, 95% CI = 1.0, 2.6) were significantly more likely to estimate their BrAC to be less than 0.08%, which is concerning given that young (less than 21) intoxicated females are a group at high risk for sexual assault on college campuses. (PsycINFO Database Record

  20. Ultra-sensitive thermal conductance measurement of one-dimensional nanostructures enhanced by differential bridge.

    PubMed

    Wingert, Matthew C; Chen, Zack C Y; Kwon, Shooshin; Xiang, Jie; Chen, Renkun

    2012-02-01

    Thermal conductivity of one-dimensional nanostructures, such as nanowires, nanotubes, and polymer chains, is of significant interest for understanding nanoscale thermal transport phenomena as well as for practical applications in nanoelectronics, energy conversion, and thermal management. Various techniques have been developed during the past decade for measuring this fundamental quantity at the individual nanostructure level. However, the sensitivity of these techniques is generally limited to 1 × 10(-9) W∕K, which is inadequate for small diameter nanostructures that potentially possess thermal conductance ranging between 10(-11) and 10(-10) W∕K. In this paper, we demonstrate an experimental technique which is capable of measuring thermal conductance of ∼10(-11) W∕K. The improved sensitivity is achieved by using an on-chip Wheatstone bridge circuit that overcomes several instrumentation issues. It provides a more effective method of characterizing the thermal properties of smaller and less conductive one-dimensional nanostructures. The best sensitivity experimentally achieved experienced a noise equivalent temperature below 0.5 mK and a minimum conductance measurement of 1 × 10(-11) W∕K. Measuring the temperature fluctuation of both the four-point and bridge measurements over a 4 h time period shows a reduction in measured temperature fluctuation from 100 mK to 0.6 mK. Measurement of a 15 nm Ge nanowire and background conductance signal with no wire present demonstrates the increased sensitivity of the bridge method over the traditional four-point I-V measurement. This ultra-sensitive measurement platform allows for thermal measurements of materials at new size scales and will improve our understanding of thermal transport in nanoscale structures.

  1. Thermal Conductivity Measurement of an Electron-Beam Physical-Vapor-Deposition Coating.

    PubMed

    Slifka, A J; Filla, B J

    2003-01-01

    An industrial ceramic thermal-barrier coating designated PWA 266, processed by electron-beam physical-vapor deposition, was measured using a steady-state thermal conductivity technique. The thermal conductivity of the mass fraction 7 % yttria-stabilized zirconia coating was measured from 100 °C to 900 °C. Measurements on three thicknesses of coatings, 170 μm, 350 μm, and 510 μm resulted in thermal conductivity in the range from 1.5 W/(m·K) to 1.7 W/(m·K) with a combined relative standard uncertainty of 20 %. The thermal conductivity is not significantly dependent on temperature.

  2. Measurement of the across-plane conductivity of YSZ thin films on silicon

    PubMed Central

    Navickas, E.; Gerstl, M.; Friedbacher, G.; Kubel, F.; Fleig, J.

    2012-01-01

    Across-plane conductivity measurements on ion conducting thin films of a few ten nanometers thickness are challenging due to frequently occurring short-circuits through pinholes in the layer. In this contribution, a method is proposed which allowed across-plane conductivity measurements on yttria stabilized zirconia (YSZ) layers with thicknesses as low as 20 nm. YSZ layers were prepared onto silicon substrates with a thin native silica interlayer and the across-plane conductivity was measured on circular microelectrodes by impedance spectroscopy. The silica interlayer exhibits strongly blocking behavior, which helps to avoid short-circuits through pinholes. Different relaxation frequencies of YSZ and silica make separation of these layers possible. An equivalent circuit is suggested, which allows extraction of YSZ properties, and its validity is proven by varying microelectrodes size and layer thickness. All parameters yield the expected behavior. PMID:27570328

  3. Measurement of the Thermal-Conductivity Coefficient of Nanofluids by the Hot-Wire Method

    NASA Astrophysics Data System (ADS)

    Minakov, A. V.; Rudyak, V. Ya.; Guzei, D. V.; Pryazhnikov, M. I.; Lobasov, A. S.

    2015-01-01

    In this work, the authors present results of adaptation and testing of the hot-wire method for determination for the thermal-conductivity coefficient of nanofluids. A mathematical model of heat transfer with allowance for free convection has been constructed to elucidate the parameters of an experimental setup and the range of its applicability. The experimental procedure has been tested on measurements of the thermal conductivities of water and ethylene glycol. The thermal-conductivity coefficient of a nanofluid has been measured at room temperature. The nanofluid under study was prepared on the basis of ethylene glycol and alumina nanoparticles. The concentrations of the nanoparticles ranged from 0.5% to 2% by volume. Good agreement has been obtained between the measured values of the thermal-conductivity coefficient and the data of other authors.

  4. Bulk conductivity measurement of paper by a new in situ pressure cell

    NASA Astrophysics Data System (ADS)

    Josefowicz, Jack Y.; Anczurowski, Edward; Jones, Arthur Y.; Deslandes, Yves

    1981-06-01

    In this report a new bulk conductivity cell design is described which can be used to characterize both conductivized and nonconductive paper. By the use of optically flat stainless steel electrodes under a pressure of 115 bars during the conductivity measurement, it is shown that the contact resistance between the paper sample and the electrodes is reduced to negligible proportions. The effect of paper surface morphology on the contact resistance during the measurement of bulk conductivity was studied by a comparison between the polished stainless steel electrodes and electrodes composed of liquid Galium Indium, which make intimate contact with the paper surface. Bulk conductivity measurements were determined for paper samples having different basis weights and different degrees of calendering. The results obtained with the pressurized stainless steel electrodes for these paper samples indicate that the contact resistance is essentially eliminated for all the papers studied by using an applied pressure of 115 bars.

  5. Thermal conductivity and diffusivity of biomaterials measured with self-heated thermistors

    NASA Astrophysics Data System (ADS)

    Valvano, J. W.; Cochran, J. R.; Diller, K. R.

    1985-05-01

    This paper presents an experimental method to measure the thermal conductivity and thermal diffusivity of biomaterials. Self-heated thermistor probes, inserted into the tissue of interest, are used to deliver heat as well as to monitor the rate of heat removal. An empirical calibration procedure allows accurate thermal-property measurements over a wide range of tissue temperatures. Operation of the instrument in three media with known thermal properties shows the uncertainty of measurements to be about 2%. The reproducibility is 0.5% for the thermal-conductivity measurements and 2% for the thermal-diffusivity measurements. Thermal properties were measured in dog, pig, rabbit, and human tissues. The tissues included kidney, spleen, liver, brain, heart, lung, pancreas, colon cancer, and breast cancer. Thermal properties were measured for 65 separate tissue samples at 3, 10, 17, 23, 30, 37, and 45°C. The results show that the temperature coefficient of biomaterials approximates that of water.

  6. Improvements of conductivity measurements of electrolyte solutions using a new conductometric cell design.

    PubMed

    Merclin, Nadia; Beronius, Per

    2002-06-20

    A new conductometric cell design, for precise conductance measurements, has been developed and tested using aqueous lidocaine hydrochloride as a model system. A small portion of a stock solution in the conductivity cell is diluted stepwise by pure solvent. The resistance of the cell is measured by means of a precision conductance bridge. Contrary to conventional technique in precision conductometry, the temperature is allowed to change during the measurements and corrected to the desired standard temperature. The temperature is determined using a thermistor immersed in the cell solution, which is agitated during the entire experiment. Using this new approach, significant improvements over conventional conductivity technique were observed. The time required for the measurements was considerably reduced, by a factor of at least ten. The amounts, especially of costly drugs, required in the measurements are also reduced. The pK(a) value obtained, 7.28, is close to the previously reported conductometrically determined average, 7.18. The precision of the single conductivity value is equally high, if not higher, as that obtained using conventional conductivity technique.

  7. Laboratory measurements of electrical conductivities of hydrous and dry Mount Vesuvius melts under pressure

    NASA Astrophysics Data System (ADS)

    Pommier, A.; Gaillard, F.; Pichavant, M.; Scaillet, B.

    2008-05-01

    Quantitative interpretation of MT anomalies in volcanic regions requires laboratory measurements of electrical conductivities of natural magma compositions. The electrical conductivities of three lava compositions from Mount Vesuvius (Italy) have been measured using an impedance spectrometer. Experiments were conducted on both glasses and melts between 400 and 1300°C, at both ambient pressure in air and high pressures (up to 400 MPa). Both dry and hydrous (up to 5.6 wt % H2O) melt compositions were investigated. A change of the conduction mechanism corresponding to the glass transition was systematically observed. The conductivity data were fitted by sample-specific Arrhenius laws on either side of Tg. The electrical conductivity increases with temperature and is higher in the order tephrite, phonotephrite to phonolite. For the three investigated compositions, increasing pressure decreases the conductivity, although the effect of pressure is relatively small. The three investigated compositions have similar activation volumes (ΔV = 16-24 cm3 mol-1). Increasing the water content of the melt increases the conductivity. Comparison of activation energies (Ea) from conductivity and sodium diffusion and use of the Nernst-Einstein relation allow sodium to be identified as the main charge carrier in our melts and presumably also in the corresponding glasses. Our data and those of previous studies highlight the correlation between the Arrhenius parameters Ea and σ0. A semiempirical method allowing the determination of the electrical conductivity of natural magmatic liquids is proposed, in which the activation energy is modeled on the basis of the Anderson-Stuart model, σ0 being obtained from the compensation law and ΔV being fitted from our experimental data. The model enables the electrical conductivity to be calculated for the entire range of melt compositions at Mount Vesuvius and also satisfactorily predicts the electrical response of other melt compositions

  8. Predicting Ratings of Counselor Trainee Empathy with Self-Report Anxiety Measures and Skin Conductance.

    ERIC Educational Resources Information Center

    Bowman, James T.; Giesen, J. Martin

    1982-01-01

    Investigated the degree of relationship between clients' and judges' ratings of counselor trainee (N=29) empathy and self-report anxiety and skin conductance measures. Results indicated the usefulness of anxiety measures to predict counselor empathy is predicated on the criterion for rating counselor empathy. (RC)

  9. Thermal conductivity of particulate materials: A summary of measurements taken at the Marshall Space Flight Center

    NASA Technical Reports Server (NTRS)

    Fountain, J. A.

    1973-01-01

    Thermal conductivity measurements of particulate materials in vacuum are presented in summary. Particulate basalt and soda lime glass beads of various size ranges were used as samples. The differentiated line heat source method was used for the measurements. A comprehensive table is shown giving all pertinent experimental conditions. Least-squares curve fits to the data are presented.

  10. Development of a Handmade Conductivity Measurement Apparatus and Application to Vegetables and Fruits

    ERIC Educational Resources Information Center

    Set, Seng; Kita, Masakazu

    2014-01-01

    This paper describes the development of a simple handmade conductivity measurement apparatus based on a Kohlrausch bridge with inexpensive materials. We have examined the reliability of this apparatus with standard solutions and then measured juices of vegetables and fruits as well as a sports drink. Comparisons to total alkali content as…

  11. Calibration of EMI derived apparent electrical conductivity based on ERT measurements

    NASA Astrophysics Data System (ADS)

    Rudolph, S.; Mester, A.; van der Kruk, J.; Weihermüller, L.; Zimmermann, E.; Vereecken, H.

    2012-04-01

    Soil electrical conductivity (ECa) is an indirect measure for various soil physical and chemical parameters. Among non-invasive geophysical methods, electromagnetic induction (EMI) appears to be the most efficient one that is able to measure ECa over large areas in short time. However, this method currently does not provide quantitative values of ECa due to calibration problems. In the calibration approach of Lavoué et al. (2010) inverted electrical conductivity data from a 120 m long ERT (electrical resistivity tomography) calibration transect were used as input parameter for an electromagnetic forward model to predict ECa measured with EMI. To further improve this calibration method we conducted a field survey within an agricultural field for crop breeding studies. The entire field (60x100 m) was mapped with the EM38-MK2 (Geonics, Ontario, Canada), an EMI system with multiple coil spacing which measures the weighted average of ECa over four depth ranges, immediately after the harvest of sugar beet. On the basis of high-resolution ECa distribution maps, an area with high contrast in ECa was selected for calibrating the EMI sensor with ERT. Along a 30 m long transect EMI measurements with two different internal calibration settings were carried out. A Syscal Pro System (IRIS Instruments, Orleans France) and 120 electrodes with an electrode spacing of 0.25 m were used to measure the apparent resistivity of soil. Post processed ERT measurements were inverted using the robust inversion method of the RES2DINV software. Quantitative EM inductions measurements were derived by linear regression between measured and predicted ECa measurements. The observed offset between the repeated EMI measurements could be removed successfully. Furthermore, shortening and focusing the ERT measurements to a specific area of interest could reduce the measurement time for calibration significantly. Prospectively, the application of a quantitative multi-layer inversion of multi

  12. The thermal conductivity of rock under hydrothermal conditions: measurements and applications

    SciTech Connect

    Williams, Colin F.; Sass, John H.

    1996-01-24

    The thermal conductivities of most major rock-forming minerals vary with both temperature and confining pressure, leading to substantial changes in the thermal properties of some rocks at the high temperatures characteristic of geothermal systems. In areas with large geothermal gradients, the successful use of near-surface heat flow measurements to predict temperatures at depth depends upon accurate corrections for varying thermal conductivity. Previous measurements of the thermal conductivity of dry rock samples as a function of temperature were inadequate for porous rocks and susceptible to thermal cracking effects in nonporous rocks. We have developed an instrument for measuring the thermal conductivity of water-saturated rocks at temperatures from 20 to 350 °C and confining pressures up to 100 MPa. A transient line-source of heat is applied through a needle probe centered within the rock sample, which in turn is enclosed within a heated pressure vessel with independent controls on pore and confining pressure. Application of this technique to samples of Franciscan graywacke from The Geysers reveals a significant change in thermal conductivity with temperature. At reservoir-equivalent temperatures of 250 °C, the conductivity of the graywacke decreases by approximately 25% relative to the room temperature value. Where heat flow is constant with depth within the caprock overlying the reservoir, this reduction in conductivity with temperature leads to a corresponding increase in the geothermal gradient. Consequently, reservoir temperature are encountered at depths significantly shallower than those predicted by assuming a constant temperature gradient with depth. We have derived general equations for estimating the thermal conductivity of most metamorphic and igneous rocks and some sedimentary rocks at elevated temperature from knowledge of the room temperature thermal conductivity. Application of these equations to geothermal exploration should improve estimates

  13. Conductivity Measurements of Synthesized Heteropoly Acid Membranes for Proton Exchange Membrane Fuel Cells

    SciTech Connect

    Record, K.A.; Haley, B.T.; Turner, J.

    2006-01-01

    Fuel cell technology is receiving attention due to its potential to be a pollution free method of electricity production when using renewably produced hydrogen as fuel. In a Proton Exchange Membrane (PEM) fuel cell H2 and O2 react at separate electrodes, producing electricity, thermal energy, and water. A key component of the PEM fuel cell is the membrane that separates the electrodes. DuPont’s Nafion® is the most commonly used membrane in PEM fuel cells; however, fuel cell dehydration at temperatures near 100°C, resulting in poor conductivity, is a major hindrance to fuel cell performance. Recent studies incorporating heteropoly acids (HPAs) into membranes have shown an increase in conductivity and thus improvement in performance. HPAs are inorganic materials with known high proton conductivities. The primary objective of this work is to measure the conductivity of Nafion, X-Ionomer membranes, and National Renewable Energy Laboratory (NREL) Developed Membranes that are doped with different HPAs at different concentrations. Four-point conductivity measurements using a third generation BekkTech conductivity test cell are used to determine membrane conductivity. The effect of multiple temperature and humidification levels is also examined. While the classic commercial membrane, Nafion, has a conductivity of approximately 0.10 S/cm, measurements for membranes in this study range from 0.0030 – 0.58 S/cm, depending on membrane type, structure of the HPA, and the relative humidity. In general, the X-ionomer with H6P2W21O71 HPA gave the highest conductivity and the Nafion with the 12-phosphotungstic (PW12) HPA gave the lowest. The NREL composite membranes had conductivities on the order of 0.0013 – 0.025 S/cm.

  14. Specific conductance measurements in central and western New York streams - A retrospective characterization

    USGS Publications Warehouse

    Kappel, William M.; Sinclair, Gaylen J.; Reddy, James E.; Eckhardt, David A.; deVries, M. Peter; Phillips, Margaret E.

    2012-01-01

    U.S. Geological Survey (USGS) Data Rescue Program funds were used to recover data from paper records for 139 streamgages across central and western New York State; 6,133 different streamflow measurement forms, collected between 1970-80, contained field water-quality measurements. The water-quality data were entered, reviewed, and uploaded into the USGS National Water Information System. In total, 4,285 unique site visits were added to the database. The new values represent baseline water quality from which to measure change and will lead to a comparison of water-quality change over the last 40 years and into the future. Specific conductance was one of the measured properties and represents a simple way to determine if ambient inorganic water quality has been altered by anthropogenic (road salt runoff, wastewater discharges, or natural gas development) or natural sources. The objective of this report is to describe ambient specific conductance characteristics of surface water across the central and western part of New York. This report presents median specific conductance of stream discharge for the period 1970-80 and a description of the relation between specific conductance and concentrations of total dissolved solids (TDS) retrieved from the USGS National Water Information System (NWIS) database from 1955 to present. The data descriptions provide a baseline of surface-water specific conductance data that can used for comparison to current and future measurements in New York streams.

  15. Liquid helium boil-off measurements of heat leakage from sinter-forged BSCCO current leads under DC and AC conditions

    NASA Astrophysics Data System (ADS)

    Cha, Y. S.; Niemann, R. C.; Hull, J. R.; Youngdahl, C. A.; Lanagan, M. T.; Nakade, M.; Hara, T.

    1995-06-01

    Liquid helium boil-off experiments are conducted to determine the heat leakage rate of a pair of BSCCO 2223 high-temperature superconductor current leads made by sinter forging. The experiments are carried out in both DC and AC conditions and with and without an intermediate heat intercept. Current ranges are from 0-500 A for DC tests and 0-1,000 A(sub rms) for AC tests. The leads are self-cooled. Results show that magnetic hysteresis (AC) losses for both the BSCCO leads and the low-temperature superconductor current jumper are small for the current range. It is shown that significant reduction in heat leakage rate (liquid helium boil-off rate) is realized by using the BSCCO superconductor leads. At 100 A, the heat leakage rate of the BSCCO/copper binary lead is approximately 29% of that of the conventional copper lead. Further reduction in liquid helium boil-off rate can be achieved by using an intermediate heat intercept. For example, at 500 K, the heat leakage rate of the BSCCO/copper binary lead is only 7% of that of the conventional copper lead when an intermediate heat intercept is used.

  16. Liquid helium boil-off measurements of heat leakage from sinter-forged BSCCO current leads under DC and AC conditions

    SciTech Connect

    Cha, Y.S.; Niemann, R.C.; Hull, J.R.; Youngdahl, C.A.; Lanagan, M.T.; Nakade, M.; Hara, T.

    1995-06-01

    Liquid helium boil-off experiments are conducted to determine the heat leakage rate of a pair of BSCCO 2223 high-temperature superconductor current leads made by sinter forging. The experiments are carried out in both DC and AC conditions and with and without an intermediate heat intercept. Current ranges are from 0-500 A for DC tests and 0-1,000 A{sub rms} for AC tests. The leads are self-cooled. Results show that magnetic hysteresis (AC) losses for both the BSCCO leads and the low-temperature superconductor current jumper are small for the current range. It is shown that significant reduction in heat leakage rate (liquid helium boil-off rate) is realized by using the BSCCO superconductor leads. At 100 A, the heat leakage rate of the BSCCO/copper binary lead is approximately 29% of that of the conventional copper lead. Further reduction in liquid helium boil-off rate can be achieved by using an intermediate heat intercept. For example, at 500 K, the heat leakage rate of the BSCCO/copper binary lead is only 7% of that of the conventional copper lead when an intermediate heat intercept is used.

  17. Experimental measurement of the plasma conductivity of Z93 and Z93P thermal control paint

    NASA Technical Reports Server (NTRS)

    Hillard, G. Barry

    1993-01-01

    Two samples each of Z93 and Z93P thermal control paint were exposed to a simulated space environment in a plasma chamber. The samples were biased through a series of voltages ranging from -200 volts to +300 volts and electron and ion currents measured. By comparing the currents to those of pure metal samples of the same size and shape, the conductivity of the samples was calculated. Measured conductivity was dependent on the bias potential in all cases. For Z93P, conductivity was approximately constant over much of the bias range and we find a value of 0.5 micro-mhos per square meter for both electron and ion current. For Z93, the dependence on bias was much more pronounced but conductivity can be said to be approximately one order of magnitude larger. In addition to presenting these results, this report documents all of the experimental data as well as the statistical analyses performed.

  18. Experimental Measurement and Numerical Modeling of the Effective Thermal Conductivity of TRISO Fuel Compacts

    SciTech Connect

    Folsom, Charles; Xing, Changhu; Jensen, Colby; Ban, Heng; Marshall, Douglas W.

    2015-03-01

    Accurate modeling capability of thermal conductivity of tristructural-isotropic (TRISO) fuel compacts is important to fuel performance modeling and safety of Generation IV reactors. To date, the effective thermal conductivity (ETC) of tristructural-isotropic (TRISO) fuel compacts has not been measured directly. The composite fuel is a complicated structure comprised of layered particles in a graphite matrix. In this work, finite element modeling is used to validate an analytic ETC model for application to the composite fuel material for particle-volume fractions up to 40%. The effect of each individual layer of a TRISO particle is analyzed showing that the overall ETC of the compact is most sensitive to the outer layer constituent. In conjunction with the modeling results, the thermal conductivity of matrix-graphite compacts and the ETC of surrogate TRISO fuel compacts have been successfully measured using a previously developed measurement system. The ETC of the surrogate fuel compacts varies between 50 and 30 W m-1 K-1 over a temperature range of 50-600°C. As a result of the numerical modeling and experimental measurements of the fuel compacts, a new model and approach for analyzing the effect of compact constituent materials on ETC is proposed that can estimate the fuel compact ETC with approximately 15-20% more accuracy than the old method. Using the ETC model with measured thermal conductivity of the graphite matrix-only material indicate that, in the composite form, the matrix material has a much greater thermal conductivity, which is attributed to the high anisotropy of graphite thermal conductivity. Therefore, simpler measurements of individual TRISO compact constituents combined with an analytic ETC model, will not provide accurate predictions of overall ETC of the compacts emphasizing the need for measurements of composite, surrogate compacts.

  19. Measuring the thermal conductivity of porous media under low atmospheric pressures

    NASA Astrophysics Data System (ADS)

    Uhlmann, Steffen; Knollenberg, Jörg; Grott, Matthias; Hütter, Erika

    2010-05-01

    Upcoming and planned space missions will carry experiments to measure the thermophysical properties of cometary and planetary materials. In order to evaluate and interpret these measurements, reliable laboratory data for the thermal conductivity of porous and granular media under low atmospheric pressure conditions need to be collected. The low thermal conductivity of these materials (~0.1 to 0.001 W/mK) and the large contact resistance between the material and any thermal conductivity sensor makes these measurements extremely challenging. In order to obtain reliable results, a material exchange project involving several laboratories (DLR, Austrian Academy of Science, open for further participation) has been initiated. All labs will carry out thermal conductivity measurements on identical specimen under defined conditions and results will then be compared to gain confidence in the obtained results. At DLR, thermal conductivity measurements will be carried out using the Transient Hot Strip (THS) method, as transient methods suffer less from contact resistance problems than steady state methods such as, e.g., the Guarded Hot Plate method. The employed THS heater/sensor consists of a thin Ni-Fe circuit on a Kapton base layer and is energized with a constant power to determine the self-heating curve as a function of time, which can then be inverted to give the thermal conductivity and diffusivity of the ambient medium. The applied sensor layout minimizes axial heat losses and small diameter (low thermal conductance) electrical connections to the measurement electronics are applied. Furthermore, the thin-film Ni-Fe circuit and Kapton foil ensure a low thermal capacity of the setup. First results using this setup and the certified fibre-glass reference material IRMM440, which has a thermal conductivity of 0.032 W/m, indicate that this method is capable of measuring even low thermal conductivities with an accuracy of 11% and a precision of 1.5%. The method can probably be

  20. In situ electrical conductivity measurements of H2O under static pressure up to 28 GPa

    NASA Astrophysics Data System (ADS)

    Liu, Bao; Gao, Yang; Han, Yonghao; Ma, Yanzhang; Gao, Chunxiao

    2016-08-01

    The in situ electrical conductivity measurements on water in both solid state and liquid state were performed under pressure up to 28 GPa and temperature from 77 K to 300 K using a microcircuit fabricated on a diamond anvil cell (DAC). Water chemically ionization mainly contributes to electrical conduction in liquid state, which is in accord with the results obtained under dynamic pressure. Energy band theory of liquid water was used to understand effect of static pressure on electrical conduction of water. The electric conductivity of H2O decreased discontinuously by four orders of magnitude at 0.7-0.96 GPa, indicating water frozen at this P-T condition. Correspondingly, the conduction of H2O in solid state is determined by arrangement and bending of H-bond in ice VI and ice VII. Based on Jaccard theory, we have concluded that the charge carriers of ice are already existing ions and Bjerrum defects.

  1. Measuring and modeling the thermal conductivities of three-dimensionally woven fabric composites

    NASA Astrophysics Data System (ADS)

    Schuster, J.; Heider, D.; Sharp, K.; Glowania, M.

    2009-03-01

    The effect of a three-dimensional fiber reinforcement on the out-of-plane thermal conductivity of composite materials is investigated. Composite preforms with different fibers in the thickness direction were fabricated. After in fusion by using a vacuum-assisted resin transfer molding process, their through-thickness thermal conductivities were evaluated. The measured thermal conductivities showed a significant increase compared with those of a typical laminated composite. Although the through-thickness thermal conductivity of the samples increased with through-thickness fiber volume fraction, its values did not match those predicted by the simple rule of mixtures. By using finite-element models to better under stand the behavior of the composite material, improvements in an existing analytical model were performed to predict the effective thermal conductivity as a function of material properties and in-contact thermal properties of the composite.

  2. Rolling ball algorithm as a multitask filter for terrain conductivity measurements

    NASA Astrophysics Data System (ADS)

    Rashed, Mohamed

    2016-09-01

    Portable frequency domain electromagnetic devices, commonly known as terrain conductivity meters, have become increasingly popular in recent years, especially in locating underground utilities. Data collected using these devices, however, usually suffer from major problems such as complexity and interference of apparent conductivity anomalies, near edge local spikes, and fading of conductivity contrast between a utility and the surrounding soil. This study presents the experience of adopting the rolling ball algorithm, originally designed to remove background from medical images, to treat these major problems in terrain conductivity measurements. Applying the proposed procedure to data collected using different terrain conductivity meters at different locations and conditions proves the capability of the rolling ball algorithm to treat these data both efficiently and quickly.

  3. The thermal conductivity of rock under hydrothermal conditions: Measurements and applications

    SciTech Connect

    Williams, C.F.; Sass, J.H.

    1996-12-31

    The thermal conductivities of most major rock-forming minerals vary with both temperature and confining pressure, leading to substantial changes in the thermal properties of some rocks at the high temperatures characteristic of geothermal systems. In areas with large geothermal gradients, the successful use of near-surface heat flow measurements to predict temperatures at depth depends upon accurate corrections for varying thermal conductivity. Previous measurements of the thermal conductivity of dry rock samples as a function of temperature were inadequate for porous rocks and susceptible to thermal cracking effects m nonporous rocks. We have developed an instrument for measuring the thermal conductivity of water-saturated rocks at temperatures from 20 to 350{degrees}C and confining pressures up to 100 MPa. A transient line-source of heat is applied through a needle probe centered within the rock sample, which in turn is enclosed within a heated pressure vessel with independent controls on pore and confining pressure. Application of this technique to samples of Franciscan graywacke from The Geysers reveals a significant change in thermal conductivity with temperature. At reservoir-equivalent temperatures of 250{degrees}C, the conductivity of the graywacke decreases by approximately 25 % relative to the room temperature value. Where heat how is constant with depth within the caprock overlying the reservoir, this reduction in conductivity with temperature leads to a corresponding increase in the geothermal gradient. Consequently, reservoir temperatures are encountered at depths significantly shallower than those predicted by assuming a constant temperature gradient with depth. We have derived general equations for estimating the thermal conductivity of most metamorphic and igneous rocks and some sedimentary rocks at elevated temperature from knowledge of the room temperature thermal conductivity.

  4. Influence of probe geometry on measurement results of non-ideal thermal conductivity sensors

    NASA Astrophysics Data System (ADS)

    Tiefenbacher, Patrick; Kömle, Norbert I.; Macher, Wolfgang; Kargl, Günter

    2016-09-01

    The thermal properties of the surface and subsurface layers of planets and planetary objects yield important information that allows us to better understand the thermal evolution of the body itself and its interactions with the environment. Various planetary bodies of our Solar System are covered by so-called regolith, a granular and porous material. On such planetary bodies the dominant heat transfer mechanism is heat conduction via IR radiation and contact points between particles. In this case the energy balance is mainly controlled by the effective thermal conductivity of the top surface layers, which can be directly measured by thermal conductivity probes. A traditionally used method for measuring the thermal conductivity of solid materials is the needle-probe method. Such probes consist of thin steel needles with an embedded heating wire and temperature sensors. For the evaluation of the thermal conductivity of a specific material the temperature change with time is determined by heating a resistance wire with a well-defined electrical current flowing through it and simultaneously measuring the temperature increase inside the probe over a certain time. For thin needle probes with a large length-to-diameter ratio it is mathematically easy to derive the thermal conductivity, while this is not so straightforward for more rugged probes with a larger diameter and thus a smaller length-to-diameter ratio. Due to the geometry of the standard thin needle probes they are mechanically weak and subject to bending when driven into a soil. Therefore, using them for planetary missions can be problematic. In this paper the thermal conductivity values determined by measurements with two non-ideal, ruggedized thermal conductivity sensors, which only differ in length, are compared to each other. Since the theory describing the temperature response of non-ideal sensors is highly complicated, those sensors were calibrated with an ideal reference sensor in various solid and

  5. Recognition tunneling measurement of the conductance of DNA bases embedded in self-assembled monolayers.

    PubMed

    Huang, Shuo; Chang, Shuai; He, Jin; Zhang, Peiming; Liang, Feng; Tuchband, Michael; Li, Shengqing; Lindsay, Stuart

    2010-12-09

    The DNA bases interact strongly with gold electrodes, complicating efforts to measure the tunneling conductance through hydrogen-bonded Watson Crick base pairs. When bases are embedded in a self-assembled alkane-thiol monolayer to minimize these interactions, new features appear in the tunneling data. These new features track the predictions of density-functional calculations quite well, suggesting that they reflect tunnel conductance through hydrogen-bonded base pairs.

  6. Thermal conductivity measurement in clay dominant consolidated material by Transient Hot-Wire method.

    NASA Astrophysics Data System (ADS)

    Garnier, J. P.; Gallier, J.; Mercx, B.; Dudoignon, P.; Milcent, D.

    2010-06-01

    The transient hot-wire (THW) technique is widely used for measurements of the thermal-conductivity of most fluids and some attempts have also been carried out for simultaneous measurements of the thermal-diffusivity with the same hot wire. This technique was also tried to determine thermal properties of soils by the mean of probes which can be considered as wire with some assumptions. The purpose of this paper is to validate the thermal conductivity measurement by the THW technique in geomaterials, composed of compacted sand + clay mineral that can be used for earth construction (Compacted Earth Brick). The thermal transfer behaviors are mainly governed by the texture and moisture of the geomaterials. Thus the investigations were performed (1) in media made of glass beads of different diameters in dry and saturated state in order to observe the role of grain sizes and saturation state on the wire temperature (Δt) measurements and (2) in the compacted clay-geomaterial at different moisture states. The Δt / ln(t) diagrams allow the calculation of two thermal conductivities. The first one, measured in the short time acquisition (< 1s), characterizes the microtexture of the material and its hydrated state. The second one, measured for longer time acquisitions, characterizes the mean thermal conductivity of the material.

  7. Pulse-power integrated-decay technique for the measurement of thermal conductivity

    NASA Astrophysics Data System (ADS)

    Kharalkar, Nachiket M.; Hayes, Linda J.; Valvano, Jonathan W.

    2008-07-01

    A pulse-power integrated-decay technique for the measurement of thermal conductivity of biological tissues is presented. A self-heated thermistor probe is used to deliver heat and also to measure the temperature response. Three-dimensional finite element analyses are used in this paper to design and optimize the technique. The thermal conductivity measurements from the computer simulations were in close accordance with the experimental data. An empirical calibration process, performed in glycerol and agar-gelled water, provides accurate thermal conductivity measurements. An accuracy analysis evaluated multiple experimental protocols using three solutions of known thermal properties. The results indicate that the thermal decay technique protocol had better accuracy than the constant temperature heating techniques. In vitro measurements demonstrate the variability of tissue thermal conductivity, and the need to perform direct measurements for tissues of interest. The factors that may introduce error in the experimental data are (i) poor thermal/physical contact between the thermistor probe and tissue sample, (ii) water loss from tissue during the course of experimentation and (iii) temperature stability.

  8. Thermal conductivity measurements in Porous mixtures of methane hydrate and quartz sand

    USGS Publications Warehouse

    Waite, W.F.; deMartin, B.J.; Kirby, S.H.; Pinkston, J.; Ruppel, C.D.

    2002-01-01

    Using von Herzen and Maxwell's needle probe method, we measured thermal conductivity in four porous mixtures of quartz sand and methane gas hydrate, with hydrate composing 0, 33, 67 and 100% of the solid volume. Thermal conductivities were measured at a constant methane pore pressure of 24.8 MPa between -20 and +15??C, and at a constant temperature of -10??C between 3.5 and 27.6 MPa methane pore pressure. Thermal conductivity decreased with increasing temperature and increased with increasing methane pore pressure. Both dependencies weakened with increasing hydrate content. Despite the high thermal conductivity of quartz relative to methane hydrate, the largest thermal conductivity was measured in the mixture containing 33% hydrate rather than in hydrate-free sand. This suggests gas hydrate enhanced grain-to-grain heat transfer, perhaps due to intergranular contact growth during hydrate synthesis. These results for gas-filled porous mixtures can help constrain thermal conductivity estimates in porous, gas hydrate-bearing systems.

  9. Thermal Conductivity Measurements of Bulk Thermoelectric Materials (Prop. 2004-067)

    SciTech Connect

    Wang, Hsin; Porter, Wallace D; Sharp, J

    2006-01-01

    Thermal conductivity is an important material property of the bulk thermoelectrics. To improve ZT a reduced thermal conductivity is always desired. However, there is no standard material for thermoelectrics and the test results, even on the same material, often show significant scatter. The scatter in thermal conductivity made reported ZT values uncertain and sometime unrepeatable. One of the reasons for the uncertainty is due to the microstructure differences resulting from sintering, heat treatment and other processing parameters. They selected commonly used bulk thermoelectric materials and conducted thermal conductivity measurements using the laser flash diffusivity and differential scanning calorimeter (DSC) systems. Thermal conductivity was measured as a function of temperature of temperature from room temperature to 500 K and back to room temperature. The effect of thermal cycling on the bulk thermoelectric was studied. Comnbined with measurements on electrical resistivity and Seebeck coefficient, they show the use of a ZT map in selecting thermoelectrics. The commercial bulk material showed very good consistency and reliability compared to other bulk materials. The goal is to develop a thermal transport properties database for the bulk thermoelectrics and make the information available to the research community and industry.

  10. Mutual-induction measurement of the AC penetration depth in HTSC's theory of calibration function for flat samples under axial symmetry

    NASA Astrophysics Data System (ADS)

    Klupsch, Th.; Zeisberger, M.

    1995-02-01

    A contribution to find optimum mutual-induction arrangements for investigating the linear AC response properties of the pinned vortices in the mixed state of HTSC is given. In particular, the complex calibration function (mutual-induction coefficient L12 as a function of the complex AC penetration depth λ) is analyzed, strictly axial symmetry and flat sample geometries provided (finite disk and its limiting case of infinite platelet) assuming the radius of at least one induction coil is smaller than the sample radius. Because the sample is positioned transverse to the AC induction B, the mutual inductance becomes, in general, strongly modified by distortions of B around the sample, which results in a strong dependence of L12(λ) upon certain geometry parameters and an enhanced sensitivity to λ for selected |λ| intervals. The analysis is based upon powerful analytic approximation formulae for elementary arrangements derived in a separate paper. Also, formulae to estimate the errors from irregular (eccentric) sample shapes, from the field enhancement near the disk edges as well as from treating the finite-disk problem in the limit of an infinite platelet are given. Except for ultrathin films with thickness much smaller than |λ|, arrangements with both the coils at the same sample side and with the loop radii sufficiently smaller than the disk radius are favored for measurements of small λ with |D/λ| ≳ 1 ( D is the sample thickness), which also includes the possibility of a λ measurement in the bulk limit | D/λ| → ∞.

  11. Microengineered Conductive Elastomeric Electrodes for Long-Term Electrophysiological Measurements with Consistent Impedance under Stretch.

    PubMed

    Hu, Dinglong; Cheng, Tin Kei; Xie, Kai; Lam, Raymond H W

    2015-10-23

    In this research, we develop a micro-engineered conductive elastomeric electrode for measurements of human bio-potentials with the absence of conductive pastes. Mixing the biocompatible polydimethylsiloxane (PDMS) silicone with other biocompatible conductive nano-particles further provides the material with an electrical conductivity. We apply micro-replica mold casting for the micro-structures, which are arrays of micro-pillars embedded between two bulk conductive-PDMS layers. These micro-structures can reduce the micro-structural deformations along the direction of signal transmission; therefore the corresponding electrical impedance under the physical stretch by the movement of the human body can be maintained. Additionally, we conduct experiments to compare the electrical properties between the bulk conductive-PDMS material and the microengineered electrodes under stretch. We also demonstrate the working performance of these micro-engineered electrodes in the acquisition of the 12-lead electrocardiographs (ECG) of a healthy subject. Together, the presented gel-less microengineered electrodes can provide a more convenient and stable bio-potential measurement platform, making tele-medical care more achievable with reduced technical barriers for instrument installation performed by patients/users themselves.

  12. Microengineered Conductive Elastomeric Electrodes for Long-Term Electrophysiological Measurements with Consistent Impedance under Stretch

    PubMed Central

    Hu, Dinglong; Cheng, Tin Kei; Xie, Kai; Lam, Raymond H. W.

    2015-01-01

    In this research, we develop a micro-engineered conductive elastomeric electrode for measurements of human bio-potentials with the absence of conductive pastes. Mixing the biocompatible polydimethylsiloxane (PDMS) silicone with other biocompatible conductive nano-particles further provides the material with an electrical conductivity. We apply micro-replica mold casting for the micro-structures, which are arrays of micro-pillars embedded between two bulk conductive-PDMS layers. These micro-structures can reduce the micro-structural deformations along the direction of signal transmission; therefore the corresponding electrical impedance under the physical stretch by the movement of the human body can be maintained. Additionally, we conduct experiments to compare the electrical properties between the bulk conductive-PDMS material and the microengineered electrodes under stretch. We also demonstrate the working performance of these micro-engineered electrodes in the acquisition of the 12-lead electrocardiographs (ECG) of a healthy subject. Together, the presented gel-less microengineered electrodes can provide a more convenient and stable bio-potential measurement platform, making tele-medical care more achievable with reduced technical barriers for instrument installation performed by patients/users themselves. PMID:26512662

  13. A New Guarded Hot Plate Designed for Thermal-Conductivity Measurements at High Temperature

    NASA Astrophysics Data System (ADS)

    Scoarnec, V.; Hameury, J.; Hay, B.

    2015-03-01

    The Laboratoire National de Métrologie et d'Essais has developed a new guarded hot-plate apparatus operating from to in the thermal-conductivity range from to . This facility has been specifically designed for measuring medium thermal-conductivity materials at high temperature on square specimens (100 mm side), which are easier to machine than circular ones. The hot plate and cold plates are similar with a metering section independent from the guard ring. The specimens are laterally isolated by an air gap of 4 mm width and can be instrumented by temperature sensors in order to reduce effects of thermal contact resistances between the specimens and the heating plates. Measurements have been performed on certified reference materials and on "calibrated" materials. Relative deviations between thermal conductivities measured and reference values are less than 5 % in the operating range.

  14. Correlation of Conductance Measurements from a Quantum Dot with Three Terminals

    NASA Astrophysics Data System (ADS)

    Toonen, Ryan; Prada, Marta; Qin, Hua; Huettel, Andreas; Goswami, Srijit; Blick, Robert; Eberl, Karl

    2005-03-01

    We have measured the differential conductance of a quantum dot coupled by three tunable tunneling barriers to three terminals. The quantum dot is formed by laterally constricting a two-dimensional electron gas (2DEG) in an AlxGa1-xAs/GaAs heterostructure with Schottky split-gates. The advantage to performing conductance measurements on a quantum dot with three leads is that we are able to directly measure information about the individual tunneling barriers and determine how the states interact with the leads. At a base temperature of 250mK, we have observed new phenomena not previously reported from three-terminal, mesoscopic experiments. These effects include conductance peak suppression in the nonlinear bias regime and the simultaneous coupling of two different states to two separate leads.

  15. BRINE Distribution in Harite Rocks-Inference from Measured Electrical CONDUCTIVITY-

    NASA Astrophysics Data System (ADS)

    Kitano, M.; Watanabe, T.

    2013-12-01

    Intercrystalline fluid can significantly affect rheological and transport properties of rocks. Its influences are strongly depended on its distribution. The dihedral angle between solid and liquid phases has been widely accepted as a key parameter that controls solid-liquid textures. The liquid phase is not expected to be interconnected if the dihedral angle is larger than 60°. However, observations contradictory to dihedral angle values have been reported. Watanabe (2010) suggested that the grain boundary fluid coexist with a positive dihedral angle. Similar thin fluid films might exist in grain boundaries of crustal rocks, and play important roles in crustal processes. In order to understand the nature of this fluid, we have studied the distribution of brine in halite rocks through measurements of conductivity. A sample was prepared by cold-pressing (the axial stress of 140MPa, 40minutes) and annealing (the temperature of 160°C and 180MPa confining pressure for about 160hours) of wet NaCl powder. During annealing, conductivity of a sample was monitored (2-electrode method) to reach a quasi-stationary value. The volume fraction of water is estimated to be 0.1×0.01% based on the FTIR measurement. Grains are polygonal and their diameters are ~100 μm. The cylindrical (D=9mm, L=3mm) surface of an annealed sample was weakly dried and coated with RTV rubber to suppress the conduction on the surface. Conductivity measurements were made at various pressure and temperature conditions(P<180 MPa, T<180°C). The dihedral angle of NaCl-water system is 66° at P=30MPa and T=30°C, and it becomes smaller than 60° at high pressure and temperature conditions(Holness & Lewis, 1997). Measured conductivity was of the order of 10-7~10-9 (S/m). When the temperature was fixed, a lower conductivity was observed for a higher pressure. The decrease in conductivity was typically 50% for the increase in pressure of 30MPa. For a given pressure, the conductivity increased with increasing

  16. New portable instrument for the measurement of thermal conductivity in gas process conditions

    NASA Astrophysics Data System (ADS)

    Queirós, C. S. G. P.; Lourenço, M. J. V.; Vieira, S. I.; Serra, J. M.; Nieto de Castro, C. A.

    2016-06-01

    The development of high temperature gas sensors for the monitoring and determination of thermophysical properties of complex process mixtures at high temperatures faces several problems, related with the materials compatibility, active sensing parts sensitivity, and lifetime. Ceramic/thin metal films based sensors, previously developed for the determination of thermal conductivity of molten materials up to 1200 °C, were redesigned, constructed, and applied for thermal conductivity measuring sensors. Platinum resistance thermometers were also developed using the same technology, to be used in the temperature measurement, which were also constructed and tested. A new data acquisition system for the thermal conductivity sensors, based on a linearization of the transient hot-strip model, including a portable electronic bridge for the measurement of the thermal conductivity in gas process conditions was also developed. The equipment is capable of measuring the thermal conductivity of gaseous phases with an accuracy of 2%-5% up to 840 °C (95% confidence level). The development of sensors up to 1200 °C, present at the core of the combustion chambers, will be done in a near future.

  17. An affordable and accurate conductivity probe for density measurements in stratified flows

    NASA Astrophysics Data System (ADS)

    Carminati, Marco; Luzzatto-Fegiz, Paolo

    2015-11-01

    In stratified flow experiments, conductivity (combined with temperature) is often used to measure density. The probes typically used can provide very fine spatial scales, but can be fragile, expensive to replace, and sensitive to environmental noise. A complementary instrument, comprising a low-cost conductivity probe, would prove valuable in a wide range of applications where resolving extremely small spatial scales is not needed. We propose using micro-USB cables as the actual conductivity sensors. By removing the metallic shield from a micro-B connector, 5 gold-plated microelectrodes are exposed and available for 4-wire measurements. These have a cell constant ~550m-1, an intrinsic thermal noise of at most 30pA/Hz1/2, as well as sub-millisecond time response, making them highly suitable for many stratified flow measurements. In addition, we present the design of a custom electronic board (Arduino-based and Matlab-controlled) for simultaneous acquisition from 4 sensors, with resolution (in conductivity, and resulting density) exceeding the performance of typical existing probes. We illustrate the use of our conductivity-measuring system through stratified flow experiments, and describe plans to release simple instructions to construct our complete system for around 200.

  18. Scanning electrochemical microscopy, 52. Bipolar conductance technique at ultramicroelectrodes for resistance measurements.

    PubMed

    LeSuer, Robert J; Fan, Fu-Ren F; Bard, Allen J

    2004-12-01

    The bipolar conductance, BICON, technique for the measurement of solution resistance, based on the application of microsecond current pulses, as originally described by Enke and co-workers for measurements with conventional electrodes, was extended for use with ultramicroelectrodes, with a focus on its application in scanning electrochemical microscopy (SECM). When the plateau time used to make the measurement lies within the BICON conditions, the solution conductance can be obtained directly from the output without the need for calibration curves. However, decreasing the size of the ultramicroelectrode decreases the range of values that satisfy these conditions, and one must resort to calibration curves to obtain solution conductance from the measured current, which was nevertheless found to be proportional to electrolyte concentration with electrodes as small as 5 mum in diameter. BICON/SECM approach curves over insulating substrates followed SECM negative feedback theory and approach curves in the presence of low (micromolar) or no added electrolyte are possible once the background conductivity is taken into account. Approach curves to a conducting substrate at open circuit potential are influenced by the solution time constant (solution resistance at the electrode tip x electrode double layer capacitance), which is a function of the tip/substrate distance, as well as the substrate size.

  19. Direct measurement of thermal conductivity in solid iron at planetary core conditions

    NASA Astrophysics Data System (ADS)

    Konôpková, Zuzana; McWilliams, R. Stewart; Gómez-Pérez, Natalia; Goncharov, Alexander F.

    2016-06-01

    The conduction of heat through minerals and melts at extreme pressures and temperatures is of central importance to the evolution and dynamics of planets. In the cooling Earth’s core, the thermal conductivity of iron alloys defines the adiabatic heat flux and therefore the thermal and compositional energy available to support the production of Earth’s magnetic field via dynamo action. Attempts to describe thermal transport in Earth’s core have been problematic, with predictions of high thermal conductivity at odds with traditional geophysical models and direct evidence for a primordial magnetic field in the rock record. Measurements of core heat transport are needed to resolve this difference. Here we present direct measurements of the thermal conductivity of solid iron at pressure and temperature conditions relevant to the cores of Mercury-sized to Earth-sized planets, using a dynamically laser-heated diamond-anvil cell. Our measurements place the thermal conductivity of Earth’s core near the low end of previous estimates, at 18-44 watts per metre per kelvin. The result is in agreement with palaeomagnetic measurements indicating that Earth’s geodynamo has persisted since the beginning of Earth’s history, and allows for a solid inner core as old as the dynamo.

  20. New portable instrument for the measurement of thermal conductivity in gas process conditions.

    PubMed

    Queirós, C S G P; Lourenço, M J V; Vieira, S I; Serra, J M; Nieto de Castro, C A

    2016-06-01

    The development of high temperature gas sensors for the monitoring and determination of thermophysical properties of complex process mixtures at high temperatures faces several problems, related with the materials compatibility, active sensing parts sensitivity, and lifetime. Ceramic/thin metal films based sensors, previously developed for the determination of thermal conductivity of molten materials up to 1200 °C, were redesigned, constructed, and applied for thermal conductivity measuring sensors. Platinum resistance thermometers were also developed using the same technology, to be used in the temperature measurement, which were also constructed and tested. A new data acquisition system for the thermal conductivity sensors, based on a linearization of the transient hot-strip model, including a portable electronic bridge for the measurement of the thermal conductivity in gas process conditions was also developed. The equipment is capable of measuring the thermal conductivity of gaseous phases with an accuracy of 2%-5% up to 840 °C (95% confidence level). The development of sensors up to 1200 °C, present at the core of the combustion chambers, will be done in a near future.

  1. Direct measurement of thermal conductivity in solid iron at planetary core conditions.

    PubMed

    Konôpková, Zuzana; McWilliams, R Stewart; Gómez-Pérez, Natalia; Goncharov, Alexander F

    2016-06-02

    The conduction of heat through minerals and melts at extreme pressures and temperatures is of central importance to the evolution and dynamics of planets. In the cooling Earth's core, the thermal conductivity of iron alloys defines the adiabatic heat flux and therefore the thermal and compositional energy available to support the production of Earth's magnetic field via dynamo action. Attempts to describe thermal transport in Earth's core have been problematic, with predictions of high thermal conductivity at odds with traditional geophysical models and direct evidence for a primordial magnetic field in the rock record. Measurements of core heat transport are needed to resolve this difference. Here we present direct measurements of the thermal conductivity of solid iron at pressure and temperature conditions relevant to the cores of Mercury-sized to Earth-sized planets, using a dynamically laser-heated diamond-anvil cell. Our measurements place the thermal conductivity of Earth's core near the low end of previous estimates, at 18-44 watts per metre per kelvin. The result is in agreement with palaeomagnetic measurements indicating that Earth's geodynamo has persisted since the beginning of Earth's history, and allows for a solid inner core as old as the dynamo.

  2. Inductive Measurement of Plasma Jet Electrical Conductivity (MSFC Center Director's discretionary Fund). Part 2

    NASA Technical Reports Server (NTRS)

    Turner, M. W.; Hawk, C. W.; Litchford, R. J.

    2001-01-01

    Measurement of plasma jet electrical conductivity has utility in the development of explosively driven magnetohydrodynamic (MHD) energy converters as well as magnetic flux compression reaction chambers for nuclear/chemical pulse propulsion and power. Within these types of reactors, the physical parameter of critical importance to underlying MHD processes is the magnetic Reynolds number, the value of which depends upon the product of plasma electrical conductivity and velocity. Therefore, a thorough understanding of MHD phenomena at high magnetic Reynolds number is essential, and methods are needed for the accurate and reliable measurement of electrical conductivity in high-speed plasma jets. It is well known that direct measurements using electrodes suffer from large surface resistance, and an electrodeless technique is desired. To address this need, an inductive probing scheme, originally developed for shock tube studies, has been adapted. In this method, the perturbation of an applied magnetic field by a plasma jet induces a voltage in a search coil, which, in turn, can be used to infer electrical conductivity through the inversion of a Fredholm integral equation of the first kind. A 1-in.-diameter probe using a light-gas gun. Exploratory laboratory experiments were carried out using plasma jets expelled from 15-g shaped charges. Measured conductivities were in the range of 4 kS/m for unseeded octol charges and 26 kS/m for seeded octol charges containing 2-percent potassium carbonate by mass.

  3. Real-ear measurements in conductive hearing loss: discrepancies between probe-tube microphone measurements and sound field test results.

    PubMed

    Cleaver, V C

    1998-06-01

    This study was designed to investigate earlier observations that probe-tube microphone measurements of insertion gain overestimates the functional gain received from hearing aids by users with significant conductive hearing losses. This was originally thought to be due to artefacts in the probe-tube measurement caused by middle ear pathology, but is now believed to be the result of the bone conduction stimulation of the ear exposed to high intensities of airborne sound during sound field threshold measurements. Since the functional gain must relate to the true aided benefit in such cases, these findings suggest that probe-tube microphone measurements in ears with significant air-bone gaps should be interpreted with caution.

  4. Initial comparison of energy measures for neural stimulation in a single conductance channel.

    PubMed

    Stahl, John; Miller, Damon A

    2016-08-01

    This paper considers the utility of several alternative energy measures to reduce the energy required by a stimulation current source to charge a neuron membrane capacitance to a prescribed value in the case of a single sodium channel. For a simple case, minimizing the energy of the nonlinear channel conductance provides improved efficiency in terms of stimulator energy as compared to minimizing a squared-integral measure of the stimulation current. This work lays the foundation for expanding this investigation to a full conductance-based Hodgkin-Huxley model.

  5. Note: Electrical resolution during conductive atomic force microscopy measurements under different environmental conditions and contact forces

    SciTech Connect

    Lanza, M.; Porti, M.; Nafria, M.; Aymerich, X.; Whittaker, E.; Hamilton, B.

    2010-10-15

    Conductive atomic force microscopy experiments on gate dielectrics in air, nitrogen, and UHV have been compared to evaluate the impact of the environment on topography and electrical measurements. In current images, an increase of the lateral resolution and a reduction of the conductivity were observed in N{sub 2} and, especially, in UHV (where current depends also on the contact force). Both effects were related to the reduction/elimination of the water layer between the tip and the sample in N{sub 2}/UHV. Therefore, since current measurements are very sensitive to environmental conditions, these factors must be taken into consideration when comparisons between several experiments are performed.

  6. Pulsed photothermal reflectance measurement of the thermal conductivity of sputtered aluminum nitride thin films

    SciTech Connect

    Zhao Yimin; Zhu Chunlin; Wang Sigen; Tian, J.Z.; Yang, D.J.; Chen, C.K.; Cheng Hao; Hing, Peter

    2004-10-15

    We report on measurements of the thermal conductivity of reactively sputtered aluminum nitride (AlN) thin films with different thickness, ranging from 100 nm to 1 {mu}m, on silicon substrates. The measurements were made at room temperature using the pulsed photothermal reflectance technique. The thermal conductivities of the sample are found to be significantly lower than the single-crystal bulk AlN and increase with an increasing thickness. The thermal resistance at the interface between the AlN film and the silicon substrate is found to be about 7-8x10{sup -8} m{sup 2} K/W.

  7. Development of a direct push based in-situ thermal conductivity measurement system

    NASA Astrophysics Data System (ADS)

    Chirla, Marian Andrei; Vienken, Thomas; Dietrich, Peter; Bumberger, Jan

    2016-04-01

    Heat pump systems are commonly utilized in Europe, for the exploitation of the shallow geothermal potential. To guarantee a sustainable use of the geothermal heat pump systems by saving resources and minimizing potential negative impacts induced by temperature changes within soil and groundwater, new geothermal exploration methods and tools are required. The knowledge of the underground thermal properties is a necessity for a correct and optimum design of borehole heat exchangers. The most important parameter that indicates the performance of the systems is thermal conductivity of the ground. Mapping the spatial variability of thermal conductivity, with high resolution in the shallow subsurface for geothermal purposes, requires a high degree of technical effort to procure adequate samples for thermal analysis. A collection of such samples from the soil can disturb sample structure, so great care must be taken during collection to avoid this. Factors such as transportation and sample storage can also influence measurement results. The use of technologies like Thermal Response Test (TRT) require complex mechanical and electrical systems for convective heat transport in the subsurface and longer monitoring times, often three days. Finally, by using thermal response tests, often only one integral value is obtained for the entire coupled subsurface with the borehole heat exchanger. The common thermal conductivity measurement systems (thermal analyzers) can perform vertical thermal conductivity logs only with the aid of sample procurement, or by integration into a drilling system. However, thermal conductivity measurements using direct push with this type of probes are not possible, due to physical and mechanical limitations. Applying vertical forces using direct push technology, in order to penetrate the shallow subsurface, can damage the probe and the sensors systems. The aim of this study is to develop a new, robust thermal conductivity measurement probe, for direct

  8. Method and apparatus for measuring thermal conductivity of small, highly insulating specimens

    NASA Technical Reports Server (NTRS)

    Miller, Robert A. (Inventor); Kuczmarski, Maria A. (Inventor)

    2012-01-01

    A hot plate method and apparatus for the measurement of thermal conductivity combines the following capabilities: 1) measurements of very small specimens; 2) measurements of specimens with thermal conductivity on the same order of that as air; and, 3) the ability to use air as a reference material. Care is taken to ensure that the heat flow through the test specimen is essentially one-dimensional. No attempt is made to use heated guards to minimize the flow of heat from the hot plate to the surroundings. Results indicate that since large correction factors must be applied to account for guard imperfections when specimen dimensions are small, simply measuring and correcting for heat from the heater disc that does not flow into the specimen is preferable. The invention is a hot plate method capable of using air as a standard reference material for the steady-state measurement of the thermal conductivity of very small test samples having thermal conductivity on the order of air.

  9. Measurement uncertainty for the Uniform Engine Testing Program conducted at NASA Lewis Research Center

    NASA Technical Reports Server (NTRS)

    Abdelwahab, Mahmood; Biesiadny, Thomas J.; Silver, Dean

    1987-01-01

    An uncertainty analysis was conducted to determine the bias and precision errors and total uncertainty of measured turbojet engine performance parameters. The engine tests were conducted as part of the Uniform Engine Test Program which was sponsored by the Advisory Group for Aerospace Research and Development (AGARD). With the same engines, support hardware, and instrumentation, performance parameters were measured twice, once during tests conducted in test cell number 3 and again during tests conducted in test cell number 4 of the NASA Lewis Propulsion Systems Laboratory. The analysis covers 15 engine parameters, including engine inlet airflow, engine net thrust, and engine specific fuel consumption measured at high rotor speed of 8875 rpm. Measurements were taken at three flight conditions defined by the following engine inlet pressure, engine inlet total temperature, and engine ram ratio: (1) 82.7 kPa, 288 K, 1.0, (2) 82.7 kPa, 288 K, 1.3, and (3) 20.7 kPa, 288 K, 1.3. In terms of bias, precision, and uncertainty magnitudes, there were no differences between most measurements made in test cells number 3 and 4. The magnitude of the errors increased for both test cells as engine pressure level decreased. Also, the level of the bias error was two to three times larger than that of the precision error.

  10. G-Plus report to Owens Corning-thermal conductivity Measurements of Fiberglass

    SciTech Connect

    Wang, H

    2003-04-15

    . Among the many methods of measuring thermal conductivity, only a few can be used for glass fibers. The traditional heat flow meter is used in testing thermal insulations near room temperature. At higher temperatures this method cannot be used due to material and instrument limitations. Our plan is to use a transient plane source (TPS) method to measure thermal conductivity directly. The advantage of the TPS method is that measurements can be taken at over 700 C, and covers the temperature of the automobile exhausts. The following is a report for the G-Plus project conducted at ORNL to apply the TPS method to characterizing the thermal conductivity of two types of fiberglass and also the effect of packing density.

  11. Performance measurements and operational characteristics of the Storage Tek ACS 4400 tape library with the Cray Y-MP EL

    NASA Technical Reports Server (NTRS)

    Hull, Gary; Ranade, Sanjay

    1993-01-01

    With over 5000 units sold, the Storage Tek Automated Cartridge System (ACS) 4400 tape library is currently the most popular large automated tape library. Based on 3480/90 tape technology, the library is used as the migration device ('nearline' storage) in high-performance mass storage systems. In its maximum configuration, one ACS 4400 tape library houses sixteen 3480/3490 tape drives and is capable of holding approximately 6000 cartridge tapes. The maximum storage capacity of one library using 3480 tapes is 1.2 TB and the advertised aggregate I/O rate is about 24 MB/s. This paper reports on an extensive set of tests designed to accurately assess the performance capabilities and operational characteristics of one STK ACS 4400 tape library holding approximately 5200 cartridge tapes and configured with eight 3480 tape drives. A Cray Y-MP EL2-256 was configured as its host machine. More than 40,000 tape jobs were run in a variety of conditions to gather data in the areas of channel speed characteristics, robotics motion, time taped mounts, and timed tape reads and writes.

  12. Measurement of submilliwatt, picosecond terahertz emission from a femtosecond-laser-pumped solid-state dc to ac radiation converter based on a ZnSe crystal

    SciTech Connect

    Yugami, Noboru; Ohata, Nobuo; Yaegashi, Kenta; Kawanago, Hiroshi

    2006-11-15

    We measured the terahertz pulse emission from a femtosecond-laser-pumped solid-state dc to ac radiation converter using a 150 fs Ti:sapphire laser pulse for dense plasma diagnostics. The laser-produced ionization front was directly modulated from a periodic electrostatic field to pulsed emission. The central frequency of the emission was measured to be 0.13 THz having a bandwidth of 0.1 THz and a peak power of 0.2 mW. This emission source is suitable for use in various novel diagnostic techniques, such as dense plasma diagnostics.

  13. Observations of Spacecraft Bearing Lubricant Redistribution Based on Thermal Conductance Measurements

    NASA Technical Reports Server (NTRS)

    Takeuchi, Yoshimi R.; Frantz, Peter P.; Hilton, Michael R.

    2014-01-01

    The performance and life of precision ball bearings are critically dependent on maintaining a quantity of oil at the ball/race interface that is sufficient to support a robust protective film. In space applications, where parched conditions are intentionally the norm, harsh operating conditions can displace the small reserves of oil, resulting in reduced film thickness and premature wear. In the past, these effects have proven difficult to model or to measure experimentally. This paper describes a study addressing this challenge, where bearing thermal conductance measurements are employed to infer changes in lubricant quantity at the critical rolling interfaces. In the first part of the paper, we explain how the lubricant's presence and its quantity impacts bearing thermal conductance measurements. For a stationary bearing, we show that conductance is directly related to the lubricant quantity in the ball/race contacts. Hence, aspects of bearing performance related to oil quantity can be understood and insights improved with thermal conductance data. For a moving bearing, a different mechanism of heat transfer dominates and is dependent on lubricant film thickness on the ball. In the second part of the report, we discuss lubricant quantity observations based on bearing thermal conductance measurements. Lubricant quantity, and thus bearing thermal conductance, depends on various initial and operating conditions and is impacted further by the run-in process. A significant effect of maximum run-in speed was also observed, with less oil remaining after obtaining higher speeds. Finally, we show that some of the lubricant that is displaced between the ball and race during run-in operation can be recovered during rest, and we measure the rate of recovery for one example.

  14. The difference in the thermal conductivity of nanofluids measured by different methods and its rationalization.

    PubMed

    Zagabathuni, Aparna; Ghosh, Sudipto; Pabi, Shyamal Kumar

    2016-01-01

    A suspension of particles below 100 nm in size, usually termed as nanofluid, often shows a notable enhancement in thermal conductivity, when measured by the transient hot-wire method. In contrast, when the conductivity of the same nanofluid is measured by the laser flash method, the enhancement reported is about one order of magnitude lower. This difference has been quantitatively resolved for the first time on the basis of the collision-mediated heat transfer model for nanofluids proposed earlier by our research group. Based on the continuum simulation coupled with stochastic analysis, the present theoretical prediction agrees well with the experimental observations from different measuring methods reported in the literature, and fully accounts for the different results from the two measuring methods mentioned above. This analysis also gives an indication that the nanofluids are unlikely to be effective for heat transfer in microchannels.

  15. The difference in the thermal conductivity of nanofluids measured by different methods and its rationalization

    PubMed Central

    Ghosh, Sudipto; Pabi, Shyamal Kumar

    2016-01-01

    A suspension of particles below 100 nm in size, usually termed as nanofluid, often shows a notable enhancement in thermal conductivity, when measured by the transient hot-wire method. In contrast, when the conductivity of the same nanofluid is measured by the laser flash method, the enhancement reported is about one order of magnitude lower. This difference has been quantitatively resolved for the first time on the basis of the collision-mediated heat transfer model for nanofluids proposed earlier by our research group. Based on the continuum simulation coupled with stochastic analysis, the present theoretical prediction agrees well with the experimental observations from different measuring methods reported in the literature, and fully accounts for the different results from the two measuring methods mentioned above. This analysis also gives an indication that the nanofluids are unlikely to be effective for heat transfer in microchannels. PMID:28144551

  16. Method and Apparatus for Measuring Thermal Conductivity of Small, Highly Insulating Specimens

    NASA Technical Reports Server (NTRS)

    Miller, Robert A (Inventor); Kuczmarski, Maria A (Inventor)

    2013-01-01

    A method and apparatus for the measurement of thermal conductivity combines the following capabilities: 1) measurements of very small specimens; 2) measurements of specimens with thermal conductivity on the same order of that as air; and, 3) the ability to use air as a reference material. Care is taken to ensure that the heat flow through the test specimen is essentially one-dimensional. No attempt is made to use heated guards to minimize the flow of heat from the hot plate to the surroundings. Results indicate that since large correction factors must be applied to account for guard imperfections when specimen dimensions are small, simply measuring and correcting for heat from the heater disc that does not flow into the specimen is preferable.

  17. Comparison of Measured and Modelled Hydraulic Conductivities of Fractured Sandstone Cores

    NASA Astrophysics Data System (ADS)

    Baraka-Lokmane, S.; Liedl, R.; Teutsch, G.

    - A new method for characterising the detailed fracture geometry in sandstone cores is presented. This method is based on the impregnation of samples with coloured resin, without significant disturbance of the fractures. The fractures are made clearly visible by the resin, thus allowing the fracture geometry to be examined digitally. In order to model the bulk hydraulic conductivity, the samples are sectioned serially perpendicular to the flow direction. The hydraulic conductivity of individual sections is estimated by summing the contribution of the matrix and each fracture from the digital data. Finally, the hydraulic conductivity of the bulk sample is estimated by a harmonic average in series along the flow path. Results of this geometrical method are compared with actual physical conductivity values measured from fluid experiments carried out prior to sectioning. The predicted conductivity from the fracture geometry parameters (e.g., fracture aperture, fracture width, fracture length and fracture relative roughness all measured using an optical method) is in good agreement with the independent physical measurements, thereby validating the approach.

  18. Development and application of diagnostic instrumentation for measurement of electron density and conductivity

    SciTech Connect

    Bauman, L.E.

    1990-05-01

    The purpose of this contract was to assemble and demonstrate in the laboratory a Faraday rotation system for measurement of electron density and conductivity, with the intent to produce a system suitable for diagnostic support of the development of pulsed, space-based magnetohydrodynamic (MHD) power systems. Two system configurations were tested: (1) a rotating polarizer and (2) a beam splitting polarizer. Due to the short path length plasma produced in the laboratory flame, the long wavelength 496 {mu}m methyl fluoride laser line was used and only the more sensitive rotating polarizer configuration was used for the demonstration experiments. Electron number densities from 2 {times} 10{sup 19} to 9 {times} 10{sup 19} were measured with good agreement to statistical equilibrium (Saha) calculations using emission absorption-measured flame temperatures and neutral seed atom number seed atom nuclear densities. The electron collision frequencies were measured by transmission measurements. Combining these two measurements gave measured electron conductivities of between 4 and 12 mohs/m. These results compared reasonably well with those found with an electron collision frequency model combined with chemical equilibrium calculations and the emission absorption measurements. Ellipticity measurements of electron collision frequency were not possible due to the short path length of the laboratory plasma. 46 refs., 25 figs., 9 tabs.

  19. Contact-independent measurement of electrical conductance of a thin film with a nanoscale sensor.

    PubMed

    Mentzel, Tamar S; Maclean, Kenneth; Kastner, Marc A

    2011-10-12

    Contact effects are a common impediment to electrical measurements throughout the fields of nanoelectronics, organic electronics, and the emerging field of graphene electronics. We demonstrate a novel method of measuring electrical conductance in a thin film of amorphous germanium that is insensitive to contact effects. The measurement is based on the capacitive coupling of a nanoscale metal-oxide-semiconductor field-effect transistor (MOSFET) to the thin film so that the MOSFET senses charge diffusion in the film. We tune the contact resistance between the film and contact electrodes and show that our measurement is unaffected. With the MOSFET, we measure the temperature and field dependence of the conductance of the amorphous germanium, which are fit to a model of variable-range hopping. The device structure enables both a contact-independent and a conventional, contact-dependent measurement, which makes it possible to discern the effect of the contacts in the latter measurement. This measurement method can be used for reliable electrical characterization of new materials and to determine the effect of contacts on conventional electron transport measurements, thus guiding the choice of optimal contact materials.

  20. Can standards be set for reliable measurements of thermal contact conductance

    NASA Astrophysics Data System (ADS)

    Snaith, B.; Ocallaghan, P. W.; Probert, S. D.

    1983-01-01

    Problems encountered in the search for accurate experimental contact conductance measurements are reviewed. The factors examined include specimen geometry and physical details, apparatus design, temperature measurement procedures, test schedules, experimental errors, and the comprehensiveness of reporting. It is pointed out that a lack of set standards has led to an unsatisfactory state of the art despite the large amount of experimental research accomplished. Recommendations on how to overcome the problems discussed are presented together with an outline of a standard test procedure.

  1. Tevatron AC dipole system

    SciTech Connect

    Miyamoto, R.; Kopp, S.E.; Jansson, A.; Syphers, M.J.; /Fermilab

    2007-06-01

    The AC dipole is an oscillating dipole magnet which can induce large amplitude oscillations without the emittance growth and decoherence. These properties make it a good tool to measure optics of a hadron synchrotron. The vertical AC dipole for the Tevatron is powered by an inexpensive high power audio amplifier since its operating frequency is approximately 20 kHz. The magnet is incorporated into a parallel resonant system to maximize the current. The use of a vertical pinger magnet which has been installed in the Tevatron made the cost relatively inexpensive. Recently, the initial system was upgraded with a more powerful amplifier and oscillation amplitudes up to 2-3{sigma} were achieved with the 980 GeV proton beam. This paper discusses details of the Tevatron AC dipole system and also shows its test results.

  2. Electrical conductivity of polyazomethine/fullerene C60 nanocomposites

    NASA Astrophysics Data System (ADS)

    Bronnikov, Sergei; Podshivalov, Aleksandr; Kostromin, Sergei; Asandulesa, Mihai; Cozan, Vasile

    2017-02-01

    We prepared the polyazomethine/fullerene C60 nanocomposites varying in C60 loading. With a broadband dielectric relaxation spectrometer, we measured their electrical conductivity σm being a sum of dc conductivity σdc and ac conductivity σac. A small C60 content (0.25 and 0.5 wt.%) was shown to decrease σdc, whereas a larger amount of C60 (2.5 wt.%) was found to increase σdc of the nanocomposite. The temperature dependences of σac were described with the Arrhenius equation, while the frequency dependences of σac were characterized with a power function. The correlated barrier hopping was accepted as the most suitable mechanism to explain the σac behavior of the nanocomposites.

  3. Conductance measurement of pyridyl-based single molecule junctions with Cu and Au contacts.

    PubMed

    Zhou, Xiao-Yi; Peng, Zheng-Lian; Sun, Yan-Yan; Wang, Li-Na; Niu, Zhen-Jiang; Zhou, Xiao-Shun

    2013-11-22

    We studied the conductance of pyridyl-based single molecule junctions with Cu contacts by using an electrochemical jump-to-contact scanning tunneling microscopy break junction (ECSTM-BJ) approach. The single molecule junctions of 4,4'-bipyridine (BPY), 1,2-di(pyridin-4-yl)ethene (BPY-EE) and 1,2-di(pyridin-4-yl)ethane (BPY-EA) bridged with Cu clusters show three sets of conductance values. These values are smaller than the conductance values of single molecule junctions with Au electrodes measured by the traditional scanning tunneling microscopy break junction in acidic or neutral solutions, which can be attributed to the different electronic coupling efficiencies between molecules and electrodes. The consistent conductance of pyridyl-based molecules in acidic and neutral solutions may show that the protonated pyridyl group contacts to the electrode through the deprotonated form.

  4. Measurement of Apparent Thermal Conductivity of JSC-1A Under Ambient Pressure

    NASA Technical Reports Server (NTRS)

    Yuan, Zeng-Guang; Kleinhenz, Julie E.

    2011-01-01

    The apparent thermal conductivity of JSC-1A lunar regolith simulant was measured experimentally using a cylindrical apparatus. Eleven thermocouples were embedded in the simulant bed to obtain the steady state temperature distribution at various radial, axial, and azimuthal locations. The high aspect ratio of a cylindrical geometry was proven to provide a one-dimensional, axisymmetric temperature field. A test series was performed at atmospheric pressure with varying heat fluxes. The radial temperature distribution in each test fit a logarithmic function, indicating a constant thermal conductivity throughout the soil bed. However, thermal conductivity was not constant between tests at different heat fluxes. This variation is attributed to stresses created by thermal expansion of the simulant particles against the rigid chamber wall. Under stress-free conditions (20 deg C), the data suggest a temperature independent apparent conductivity of 0.1961 +/- 0.0070 W/m/ deg C

  5. High-resolution saturated hydraulic conductivity logging of borehole cores using air permeability measurements

    NASA Astrophysics Data System (ADS)

    Rogiers, B.; Winters, P.; Huysmans, M.; Beerten, K.; Mallants, D.; Gedeon, M.; Batelaan, O.; Dassargues, A.

    2014-09-01

    Saturated hydraulic conductivity ( K s) is one of the most important parameters determining groundwater flow and contaminant transport in both unsaturated and saturated porous media. The hand-held air permeameter technique was investigated for high-resolution hydraulic conductivity determination on borehole cores using a spatial resolution of ˜0.05 m. The suitability of such air permeameter measurements on friable to poorly indurated sediments was tested to improve the spatial prediction of classical laboratory-based K s measurements obtained at a much lower spatial resolution (˜2 m). In total, 368 K s measurements were made on ˜350 m of borehole cores originating from the Campine basin, northern Belgium, while ˜5,230 air permeability measurements were performed on the same cores, resulting in a K s range of seven orders of magnitude. Cross-validation demonstrated that, using air permeameter data as the secondary variable for laboratory based K s measurements, the performance increased from R 2 = 0.35 for ordinary kriging (laboratory K s only) to R 2 = 0.61 for co-kriging. The separate treatment of horizontal and vertical hydraulic conductivity revealed considerable anisotropy in certain lithostratigraphical units, while others were clearly isotropic at the sample scale. Air permeameter measurements on borehole cores provide a cost-effective way to improve spatial predictions of traditional laboratory based K s.

  6. Measurements of middle-atmosphere electric fields and associated electrical conductivities

    NASA Technical Reports Server (NTRS)

    Hale, L. C.; Croskey, C. L.; Mitchell, J. D.

    1981-01-01

    A simple antenna for measuring the vertical electric field in the 'middle atmosphere' has been flown on a number of rocket-launched parachute-borne payloads. The data from the first nine such flights, launched under a variety of geophysical conditions, are presented, along with electrical conductivities measured simultaneously. The data include indications of layered peaks of several volts per meter in the mesospheric field at high and low latitudes in situations of relatively low conductivity. During an auroral 'REP' event the electric field reversed direction in the lower stratosphere, accompanied by a substantial enhancement in conductivity. The data generally do not confirm speculations based only on the extension of the thunderstorm circuit from below or the mapping of ionospheric and magnetospheric fields from above, but seem to require, in addition, internal generation processes in the middle atmosphere.

  7. Conductance catheter measurements of lumen area of stenotic coronary arteries: theory and experiment.

    PubMed

    Choi, Hyo Won; Farren, Neil D; Zhang, Zhen-Du; Huo, Yunlong; Kassab, Ghassan S

    2011-09-01

    An injection of saline solution is required for the measurement of vessel lumen area using a conductance catheter. The injection of room temperature saline to displace blood in a vessel inevitably involves mass and heat transport and electric field conductance. The objective of the present study is to understand the accuracy of conductance method based on the phenomena associated with the saline injection into a stenotic blood vessel. Computational fluid dynamics were performed to simulate flow and its relation to transport and electric field in a stenotic artery for two different sized conductance catheters (0.9 and 0.35 mm diameter) over a range of occlusions [56-84% cross-sectional area (CSA) stenosis]. The results suggest that the performance of conductance catheter is dependent on catheter size and severity of stenosis more significantly for 0.9 mm than for 0.35 mm catheter. Specifically, the time of detection of 95% of injected saline solution at the detection electrodes was shown to range from 0.67 to 3.7 s and 0.82 to 0.94 s for 0.9 mm and 0.35 mm catheter, respectively. The results also suggest that the detection electrodes of conductance catheter should be placed outside of flow recirculation region distal to the stenosis to minimize the detection time. Finally, the simulations show that the accuracy in distal CSA measurements, however, is not significantly altered by whether the position of detection electrodes is inside or outside of recirculation zone (error was within 12% regardless of detection electrodes position). The results were experimentally validated for one lesion geometry and the simulation results are within 8% of actual measurements. The simulation of conductance catheter injection method may lead to further optimization of device and method for accurate sizing of diseased coronary arteries, which has clinical relevance to percutaneous intervention.

  8. Temperature and electrical conductivity of the lunar interior from magnetic transient measurements in the geomagnetic tail

    NASA Technical Reports Server (NTRS)

    Dyal, P.; Parkin, C. W.; Daily, W. D.

    1974-01-01

    Magnetometers were deployed at four Apollo sites on the moon to measure remanent and induced lunar magnetic fields. Measurements from this network of instruments were used to calculate the electrical conductivity, temperature, magnetic permeability, and iron abundance of the lunar interior. Global lunar fields due to eddy currents, induced in the lunar interior by magnetic transients in the geomagnetic tail field, were analyzed to calculate an electrical conductivity profile for the moon: the conductivity increases rapidly with depth from 10 to the minus 9 power mhos/meter at the lunar surface to .0001 mhos/meter at 200 km depth, then less rapidly to .02 mhos/meter at 1000 km depth. A temperature profile is calculated from conductivity: temperature rises rapidly with depth to 1100 K at 200 km depth, then less rapidly to 1800 K at 1000 km depth. Velocities and thicknesses of the earth's magnetopause and bow shock are estimated from simultaneous magnetometer measurements. Average speeds are determined to be about 50 km/sec for the magnetopause and 70 km/sec for the bow shock, although there are large variations in the measurements for any particular boundary crossing.

  9. A Hot-Wire Method Based Thermal Conductivity Measurement Apparatus for Teaching Purposes

    ERIC Educational Resources Information Center

    Alvarado, S.; Marin, E.; Juarez, A. G.; Calderon, A.; Ivanov, R.

    2012-01-01

    The implementation of an automated system based on the hot-wire technique is described for the measurement of the thermal conductivity of liquids using equipment easily available in modern physics laboratories at high schools and universities (basically a precision current source and a voltage meter, a data acquisition card, a personal computer…

  10. Analysis and measurement of thermal conductivity of polypropylene laminated paper impregnated with subcooled liquid nitrogen

    NASA Astrophysics Data System (ADS)

    Furuse, Mitsuho; Fuchino, Shuichiro

    2014-09-01

    We measured the thermal conductivity of polypropylene laminated paper (PPLP) impregnated with subcooled liquid nitrogen. PPLP is widely used for the electrical insulation of high-Tc superconducting (HTS) power transmission cables. Although the thermal conductivity of PPLP is an important factor in the design of HTS cables, there has been very limited work on its measurement in subcooled liquid nitrogen. We prepared PPLP samples and symmetrically stacked them on both sides of a heater. The stacked samples were immersed in liquid nitrogen in an open cryostat. A cryocooler mounted on the cryostat was used to maintain the subcooled temperature of the liquid nitrogen. The thermal conductivity of the stacked PPLPs was measured by the steady state method at a bath temperature of 65-75 K and was found to be 0.23-0.26 W/m K, which is about five times that measured in a vacuum as presented in available literature. We also discuss possible mechanisms for boosting the thermal conductivity of PPLP by liquid nitrogen impregnation.

  11. Analysis of Thermal-Conductivity Measurement Data from International Comparison of National Laboratories

    NASA Astrophysics Data System (ADS)

    Hay, B.; Zarr, R.; Stacey, C.; Lira-Cortes, L.; Hammerschmidt, U.; Sokolov, N.; Zhang, J.; Filtz, J.-R.; Fleurence, N.

    2013-05-01

    For the first time under the auspices of the Bureau International des Poids et Mesures (BIPM), seven national metrology institutes (NMIs) participated in an international interlaboratory comparison on thermal-conductivity measurements by the guarded hot-plate method. Measurements were conducted successively by all participants on the same set of specimens of insulating materials (mineral wool and expanded polystyrene) at temperatures ranging from 10 °C to 40 °C, according to the International Standard ISO 8302. This protocol aims to minimize issues of material variability by circulating the same pairs of specimens among the laboratories following the strict format of a round-robin test program. This comparison is a pilot study which is intended as a first stage for future key comparisons between NMIs. The descriptive analysis of obtained results shows good agreement between laboratories for the mineral wool (MW) specimens and the thicker specimens of expanded polystyrene (EPS), with relative deviations within the uncertainties of measurement. A positive drift of thermal-conductivity values, which has appeared progressively during the comparison process, seems to be correlated with the size of the metering area of the guarded hot plates used. A statistical analysis was applied to repeated thermal-conductivity measurements at 23 °C, to identify anomalous and outlying data, to assess the within- and between-laboratory variability, and to evaluate the participant laboratories' performance.

  12. Design and Construction of a Thermal Contact Resistance and Thermal Conductivity Measurement System

    DTIC Science & Technology

    2015-09-01

    systems to improve fuel efficiency and performance. Comprehensive details of the design, construction, and operation of the experimental device are... heat transfer issues facing the Department of Defense. 14. SUBJECT TERMS Thermal contact resistance, thermal conductivity, measurement system 15...analyze component interfaces and advanced material applications within Department of Defense’s energy systems to improve fuel efficiency and

  13. Using Conductivity Measurements to Determine the Identities and Concentrations of Unknown Acids: An Inquiry Laboratory Experiment

    ERIC Educational Resources Information Center

    Smith, K. Christopher; Garza, Ariana

    2015-01-01

    This paper describes a student designed experiment using titrations involving conductivity measurements to identify unknown acids as being either HCl or H[subscript 2]SO[subscript 4], and to determine the concentrations of the acids, thereby improving the utility of standard acid-base titrations. Using an inquiry context, students gain experience…

  14. Enhanced Temporal Resolution with Ion Channel-Functionalized Sensors Using a Conductance-Based Measurement Protocol.

    PubMed

    Agasid, Mark T; Comi, Troy J; Saavedra, S Scott; Aspinwall, Craig A

    2017-01-17

    The binding of a target analyte to an ion channel (IC), which is readily detected electrochemically in a label-free manner with single-molecule selectivity and specificity, has generated widespread interest in using natural and engineered ICs as transducers in biosensing platforms. To date, the majority of developments in IC-functionalized sensing have focused on IC selectivity or sensitivity or development of suitable membrane environments and aperture geometries. Comparatively little work has addressed analytical performance criteria, particularly criteria required for temporal measurements of dynamic processes. We report a measurement protocol suitable for rapid, time-resolved monitoring (≤30 ms) of IC-modulated membrane conductance. Key features of this protocol include the reduction of membrane area and the use of small voltage steps (10 mV) and short duration voltage pulses (10 ms), which have the net effect of reducing the capacitive charging and decreasing the time required to achieve steady state currents. Application of a conductance protocol employing three sequential, 10 ms voltage steps (-10 mV, -20 mV, -30 mV) in an alternating, pyramid-like arrangement enabled sampling of membrane conductance every 30 ms. Using this protocol, dynamic IC measurements on black lipid membranes (BLMs) functionalized with gramicidin A were conducted using a fast perfusion system. BLM conductance decreased by 76 ± 7.5% within 30 ms of switching from solutions containing 0 to 1 M Ca(2+), which demonstrates the feasibility of using this approach to monitor rapid, dynamic chemical processes. Rapid conductance measurements will be broadly applicable to IC-based sensors that undergo analyte-specific gating.

  15. DEVELOPMENT OF AN IN-PILE TECHNIQUE FOR THERMAL CONDUCTIVITY MEASUREMENT

    SciTech Connect

    Brandon Fox; Heng Ban; Joy L. Rempe; Joshua E. Daw; Keith G. Condie; Darrell L. Knudson

    2009-04-01

    Thermophysical properties of advanced fuels and materials during irradiation must be known prior to their use in existing, advanced, or next generation reactors. Fuel thermal conductivity is one of the most important properties for predicting fuel performance and reactor safety. This paper discusses a joint Utah State University (USU)/Idaho National Laboratory (INL) project to investigate an in-pile fuel thermal conductivity measurement technique using a surrogate fuel rod. The method used a surrogate fuel rod with Joule heating to simulate volumetric heat generation as a proof-of-concept test in-pile application. Carbon structural foam, CFOAM®, a product of Touchtone Research Laboratory was chosen as the surrogate material because of the variable electrical and thermal properties upon fabrication. To stay within the surrogate fuel rod requirements, electrical and thermal properties were tailored by Touchtone Research Laboratory to match required values. This paper describes are the techniques used for quantifying thermal conductivity. A description of the test setup and preliminary results are presented. Two thermocouples are inserted into a 1-inch diameter, 6-inch long rod of CFOAM® at known locations. Knowing the applied volumetric heat to the rod by electrical resistance heating, the thermal conductivity can be calculated. Sensitivities of this measurement can also found by analysis and testing of different configurations of the sample setup. Verification of thermal conductivity is found by measuring the thermal properties of the CFOAM® using different methods. Thermal properties including thermal conductivity, specific heat capacity, and expansion coefficient of two types of CFOAM®, CFOAM20 and CFOAM25, were characterized using standard measurement techniques, such as laser flash, differential scanning calorimetry, and pushrod dilatometry.

  16. A study of rock matrix diffusion properties by electrical conductivity measurements

    SciTech Connect

    Ohlsson, Y.; Neretnieks, I.

    1999-07-01

    Traditional rock matrix diffusion experiments on crystalline rock are very time consuming due to the low porosity and extensive analysis requirements. Electrical conductivity measurements are, on the other hand, very fast and larger samples can be used than are practical in ordinary diffusion experiments. The effective diffusivity of a non-charged molecule is readily evaluated from the measurements, and influences from surface conductivity on diffusion of cations can be studied. A large number of samples of varying thickness can be measured within a short period, and the changes in transport properties with position in a rock core can be examined. In this study the formation factor of a large number of Aespoe diorite samples is determined by electrical conductivity measurements. The formation factor is a geometric factor defined as the ratio between the effective diffusivity of a non-charged molecule, to that of the same molecule in free liquid. The variation of this factor with position among a borecore and with sample length, and its coupling to the porosity of the sample is studied. Also the surface conductivity is studied. This was determined as the residual conductivity after leaching of the pore solution ions. The formation factor of most of the samples is in the range 1E-5 to 1E-4, with a mean value of about 5E-5. Even large samples (4--13 cm) give such values. The formation factor increases with increasing porosity and the change in both formation factor and porosity with position in the borecore can be large, even for samples close to each other. The surface conductivity increases with increasing formation factor for the various samples but the influence on the pore diffusion seems to be higher for samples of lower formation factor. This suggests that the relation between the pore surface area and the pore volume is larger for samples of low formation factor.

  17. Reliability of AcuGraph system for measuring skin conductance at acupoints

    PubMed Central

    Mist, Scott D; Aickin, Mikel; Kalnins, Paul; Cleaver, Jim; Batchelor, Roger; Thorne, Tracy; Chamberlin, Steve; Tippens, Kim; Colbert, Agatha P

    2012-01-01

    Objective There are many commercially available instruments for measuring electrical conductance, but there is little information about their reliability. The aim of this study was to quantify measurement variability and assess reliability of the AcuGraph system—a commonly used electrodermal screening device. Methods Four experiments were conducted to measure variability in electrical conductance readings obtained by the AcuGraph system. The fi rst involved measuring known resistors. The second measured non-human organic matter. The third was a test–retest assessment of the Yuan-Source and Jing-Well points in 30 healthy volunteers who were measured by a single operator. The fourth was an interoperator reliability evaluation of seven acupuncturists at the Yuan-Source and Jing-Well acupoints on four individuals at two time points. Results Against known resistors, the AcuGraph had an average coeffi cient of variability (CV) of 1.8% between operators and test–retests. On non-human organic material the AcuGraph had an average CV of 0.9% and 2.8%. When a single operator tested 30 participants, the average reliability for the Yuan-Source points was 0.86 and 0.76 for Jing-Well points with a CV of 23.2% and 25.9% respectively. The average CV for the seven acupuncturists was 24.5% on Yuan-Source points and 23.7% on Jing-Well points. Conclusions The AcuGraph measures known resistors and organic matter accurately and reliably. Skin conductance at acupoints recorded by one operator was also reliable. There was less consistency in electrodermal recordings obtained by seven different operators. Operator training and technical improvements to the AcuGraph may improve consistency among operators. PMID:21602233

  18. Flexibility and non-destructive conductivity measurements of Ag nanowire based transparent conductive films via terahertz time domain spectroscopy.

    PubMed

    Hwang, Gyujeong; Balci, Soner; Güngördü, M Zeki; Maleski, Alex; Waters, Joseph; Lee, Sunjong; Choi, Sangjun; Kim, Kyoungkook; Cho, Soohaeng; Kim, Seongsin M

    2017-02-20

    Highly stable and flexible transparent electrodes are fabricated based on silver nanowires (AgNWs) on both polyethylene-terephthalate (PET) and polyimide (PI) substrates. Terahertz time domain spectroscopy (THz-TDS) was utilized to probe AgNW films while bended with a radius 5 mm to discover conductivity of bended films which was further analyzed through Drude-Smith model. AgNW films experience little degradation in conductivity (<3%) before, after, and during 1000 bending cycles. Highly stable AgNW flexible electrodes have broad applications in flexible optoelectronic and electronic devices. THz-TDS is an effective technique to investigate the electrical properties of the bended and flattened conducting films in a nondestructive manner.

  19. Thermal boundary conductance accumulation and interfacial phonon transmission: Measurements and theory

    NASA Astrophysics Data System (ADS)

    Cheaito, Ramez; Gaskins, John T.; Caplan, Matthew E.; Donovan, Brian F.; Foley, Brian M.; Giri, Ashutosh; Duda, John C.; Szwejkowski, Chester J.; Constantin, Costel; Brown-Shaklee, Harlan J.; Ihlefeld, Jon F.; Hopkins, Patrick E.

    2015-01-01

    The advances in phonon spectroscopy in homogeneous solids have unveiled extremely useful physics regarding the contribution of phonon energies and mean-free paths to the thermal transport in solids. However, as material systems decrease to length scales less than the phonon mean-free paths, thermal transport can become much more impacted by scattering and transmission across interfaces between two materials than the intrinsic relaxation in the homogeneous solid. To elucidate the fundamental interactions driving this thermally limiting interfacial phonon scattering process, we analytically derive and experimentally measure a thermal boundary conductance accumulation function. We develop a semiclassical theory to calculate the thermal boundary conductance accumulation function across interfaces using the diffuse mismatch model, and validate this derivation by measuring the interface conductance between eight different metals on native oxide/silicon substrates and four different metals on sapphire substrates. Measurements were performed at room temperature using time-domain thermoreflectance and represent the first-reported values for interface conductance across several metal/native oxide/silicon and metal/sapphire interfaces. The various metal films provide a variable bandwidth of phonons incident on the metal/substrate interface. This method of varying phonons' cutoff frequency in the film while keeping the same substrate allows us to mimic the accumulation of thermal boundary conductance and thus provides a direct method to experimentally validate our theory. We show that the accumulation function can be written as the product of a weighted average of the interfacial phonon transmission function and the accumulation of the temperature derivative of the phonon flux incident on the interface; this provides the framework to extract an average, spectrally dependent phonon transmissivity from a series of thermal boundary conductance measurements. Our approach provides

  20. Invited Review Article: Error and uncertainty in Raman thermal conductivity measurements

    NASA Astrophysics Data System (ADS)

    Beechem, Thomas; Yates, Luke; Graham, Samuel

    2015-04-01

    Error and uncertainty in Raman thermal conductivity measurements are investigated via finite element based numerical simulation of two geometries often employed—Joule-heating of a wire and laser-heating of a suspended wafer. Using this methodology, the accuracy and precision of the Raman-derived thermal conductivity are shown to depend on (1) assumptions within the analytical model used in the deduction of thermal conductivity, (2) uncertainty in the quantification of heat flux and temperature, and (3) the evolution of thermomechanical stress during testing. Apart from the influence of stress, errors of 5% coupled with uncertainties of ±15% are achievable for most materials under conditions typical of Raman thermometry experiments. Error can increase to >20%, however, for materials having highly temperature dependent thermal conductivities or, in some materials, when thermomechanical stress develops concurrent with the heating. A dimensionless parameter—termed the Raman stress factor—is derived to identify when stress effects will induce large levels of error. Taken together, the results compare the utility of Raman based conductivity measurements relative to more established techniques while at the same time identifying situations where its use is most efficacious.

  1. Study of AC/RF properties of SRF ingot niobium

    SciTech Connect

    Dhakal, Pashupati; Tsindlekht, Menachem I; Genkin, Valery M; Ciovati, Gianluigi; Myneni, Ganapati Rao

    2013-09-01

    In an attempt to correlate the performance of superconducting radiofrequency cavities made of niobium with the superconducting properties, we present the results of the magnetization and ac susceptibility of the niobium used in the superconducting radiofrequency cavity fabrication. The samples were subjected to buffer chemical polishing (BCP) surface and high temperature heat treatments, typically applied to the cavities fabrications. The analysis of the results show the different surface and bulk ac conductivity for the samples subjected to BCP and heat treatment. Furthermore, the RF surface impedance is measured on the sample using a TE011 microwave cavity for a comparison to the low frequency measurements.

  2. Thermal Conductivity Measurement of Thermoelectric Thin Films by a Versatility-Enhanced 2ω Method

    NASA Astrophysics Data System (ADS)

    Okuhata, Ryo; Watanabe, Kentaro; Ikeuchi, Satoaki; Ishida, Akihiro; Nakamura, Yoshiaki

    2016-12-01

    The 2ω method is a technique to measure the cross-plane thermal conductivity, κ, of a film sample based on sinusoidal Joule-heating of a metal film deposited on the sample surface and its thermoreflectance (TR) measurement of surface temperature cooling due to the heat dissipation. The 2ω method is being paid attention because it is more cost-effective and easier to use than the conventional time domain thermoreflectance (TDTR) method or the 3ω method. In some cases, however, it is difficult to apply the conventional 2ω method to the κ measurement of high thermal resistance films such as general thermoelectric films due to its non-linear TR signal response to (2ω)-0.5. Here, we present a 2ω method based on a versatile TR signal analysis which enables the κ measurement of high thermal resistance film more explicitly than the conventional analysis based on a linear TR signal response. This method determines explicitly the thermal conductivities of PbTe films and PbTe/GeS superlattices grown on BaF2(111) substrates by hot wall epitaxy: κ = 2.1 ± 0.13 Wm-1 K-1 and κ = 0.71 ± 0.05 Wm-1 K-1, respectively. Furthermore, a significant impact of PbTe film crystallinity on thermal conductivity is demonstrated by comparative measurements between polycrystalline PbTe film and epitaxial PbTe film grown on the BaF2(111) substrates. These results demonstrate that our method can be a powerful tool to measure the thermal conductivity of thermoelectric films.

  3. A transient divided-bar method for simultaneous measurements of thermal conductivity and thermal diffusivity

    NASA Astrophysics Data System (ADS)

    Bording, Thue S.; Nielsen, Søren B.; Balling, Niels

    2016-04-01

    Accurate information on thermal conductivity and thermal diffusivity of materials is of central importance in relation to geoscience and engineering problems involving the transfer of heat. Within the geosciences, this applies to all aspects regarding the determination of terrestrial heat flow and subsurface temperature modelling. Several methods, including the classical divided-bar technique, are available for laboratory measurements of thermal conductivity, and much fewer for thermal diffusivity. We have generalized the divided-bar technique to the transient case, in which thermal conductivity and volumetric heat capacity, and thereby also thermal diffusivity, are measured simultaneously. As the density of samples is easily determined independently, specific heat capacity may also be determined. Finite element formulation provides a flexible forward solution for heat transfer across the bar and thermal properties are estimated by inverse Monte Carlo modelling. This methodology enables a proper quantification of experimental uncertainties on measured thermal properties. The developed methodology was applied to laboratory measurements of various materials, including a standard ceramic material and different rock samples, and measuring results were compared with results applying traditional steady-state divided-bar and an independent line-source method. All measurements show highly consistent results and with excellent reproducibility and high accuracy. For conductivity, uncertainty is typically 1-3 %, and for diffusivity uncertainty may be reduced to about 3-5 %. The main uncertainty originates from the presence of thermal contact resistance associated with the internal interfaces of the bar. They are not resolved during inversion, and it is highly important that they are minimized by careful sample preparation.

  4. Microwave conductance of aligned multiwall carbon nanotube textile sheets

    NASA Astrophysics Data System (ADS)

    Brown, Brian L.; Bykova, Julia S.; Howard, Austin R.; Zakhidov, Anvar A.; Shaner, Eric A.; Lee, Mark

    2014-12-01

    Multiwall carbon nanotube (MWNT) sheets are a class of nanomaterial-based multifunctional textile with potentially useful microwave properties. To understand better the microwave electrodynamics, complex AC conductance measurements from 0.01 to 50 GHz were made on sheets of highly aligned MWNTs with the alignment texture both parallel and perpendicular to the microwave electric field polarization. In both orientations, the AC conductance is modeled to first order by a parallel frequency-independent conductance and capacitance with no inductive contribution. This is consistent with low-frequency diffusive Drude AC conduction up to 50 GHz, in contrast to the "universal disorder" AC conduction reported in many types of single-wall nanotube materials.

  5. Room temperature screening of thermal conductivity by means of thermal transient measurements

    NASA Astrophysics Data System (ADS)

    García-Cañadas, Jorge; Cheng, Shudan; Márquez-García, Lourdes; Prest, Martin J.; Akbari-Rahimabadi, Ahmad; Min, Gao

    2016-10-01

    A proof of concept of the possibility to estimate thermal conductivity of bulk disc samples at room temperature by means of thermal decays is demonstrated. An experimental set-up was designed and fabricated, which is able to perform thermal transient measurements by using a specially designed multifunctional probe that has the ability to measure temperature at its tip. Initially, the probe is heated by a heater coil located in its interior until the tip temperature reaches a steady state. Then, the probe is contacted with a disc sample which produces a temperature decay until a new state is reached. The difference between the initial and final states temperatures shows a correlation with the thermal conductivity of the sample. Employing a calibration equation, obtained using reference materials, the thermal conductivity can be calculated. Reasonably good random and systematic errors (<13% and ~9% respectively) are obtained. Theoretical simulations performed using COMSOL show a good qualitative agreement with experimental results. This new method involves an inexpensive and simple set-up which can be especially useful for thermal conductivity screening and high-throughput measurements.

  6. Time- and Space-Domain Measurements of the Thermal Conductivity in Diamond Anvil Cells

    NASA Astrophysics Data System (ADS)

    Goncharov, A. F.

    2011-12-01

    I will give an overview of recent developments of experimental techniques to measure the thermal conductivity in diamond anvil cell (DAC) under conditions of high pressure and high temperature (P-T) which are relevant for the planetary interiors. To measure the lattice contributions to the thermal conductivity, we developed a transient heating technique (THT) in the diamond anvil cell (DAC) [1]. This technique utilizes a periodic front surface temperature variation (measured by the spectroradiometry) of a metallic absorber surrounded by the material of interest and exposed to a pulsed laser radiation (10 nanoseconds pulses). We extract the thermal diffusivity of minerals by fitting the experimental results to the model finite element (FE) calculations. We have recently modified this technique for microseconds laser pulses as this allows avoiding nonequilibrium heat transfer processes. We have measured the thermal conductivity of Ar up to 50 GPa and 2500 K; the results are in agreement with the theoretical calculations [2] in the limit of high temperatures. In collaboration with a group from the University of Illinois we have utilized a time-domain thermoreflectance (TDTR)- ultrafast (femtosecond) laser pump-probe technique for measurement of the lattice thermal conductivity at high P-T conditions. We have measured the thermal conductivity of MgO up to 60 GPa and 300 K and up to 45 GPa at 600 K. The detailed results of this study will be presented in a separate paper at this Meeting. Finally, we have combined static and pulsed laser techniques to determine the thermal conductivity of Fe and its temperature dependence at high pressures up to 70 GPa and 2000 K [3]. A thin plate of Fe was positioned in an Ar medium, laser heated from one side and the temperature is being measured from both sides of the sample radiometrically. The thermal conductivity has been determined by fitting the results of FE calculations to the experimental results. These examples demonstrate

  7. Spatial relationship between the productivity of cane sugar and soil electrical conductivity measured by electromagnetic induction

    NASA Astrophysics Data System (ADS)

    Siqueira, Glecio; Silva, Jucicléia; Bezerra, Joel; Silva, Enio; Montenegro, Abelardo

    2013-04-01

    The cultivation of sugar cane in Brazil occupies a prominent place in national production chain, because the country is the main world producer of sugar and ethanol. Accordingly, studies are needed that allow an integrated production and technified, and especially that estimates of crops are consistent with the actual production of each region. The objective of this study was to determine the spatial relationship between the productivity of cane sugar and soil electrical conductivity measured by electromagnetic induction. The field experiment was conducted at an agricultural research site located in Goiana municipality, Pernambuco State, north-east of Brazil (Latitude 07 ° 34 '25 "S, Longitude 34 ° 55' 39" W). The surface of the studied field is 6.5 ha, and its mean height 8.5 m a.s.l. This site has been under sugarcane (Saccharum officinarum sp.) monoculture during the last 24 years and it was managed burning the straw each year after harvesting, renewal of plantation was performed every 7 years. Studied the field is located 10 km east from Atlantic Ocean and it is representative of the regional landscape lowlands, whose soils are affected by salinity seawater, sugarcane plantations with the main economical activity. Soil was classified an orthic the Podsol. The productivity of cane sugar and electrical conductivity were measured in 90 sampling points. The productivity of cane sugar was determined in each of the sampling points in plots of 9 m2. The Apparent soil electrical conductivity (ECa, mS m-1) was measured with an electromagnetic induction device EM38-DD (Geonics Limited). The equipment consists of two units of measurement, one in a horizontal dipole (ECa-H) to provide effective measurement distance of 1.5 m approximately and other one in vertical dipole (ECa-V) with an effective measurement depth of approximately 0.75 m. Data were analyzed using descriptive statistics and geostatistical tools. The results showed that productivity in the study area

  8. Scanning electrochemical cell microscopy: theory and experiment for quantitative high resolution spatially-resolved voltammetry and simultaneous ion-conductance measurements.

    PubMed

    Snowden, Michael E; Güell, Aleix G; Lai, Stanley C S; McKelvey, Kim; Ebejer, Neil; O'Connell, Michael A; Colburn, Alexander W; Unwin, Patrick R

    2012-03-06

    Scanning electrochemical cell microscopy (SECCM) is a high resolution electrochemical scanning probe technique that employs a dual-barrel theta pipet probe containing electrolyte solution and quasi-reference counter electrodes (QRCE) in each barrel. A thin layer of electrolyte protruding from the tip of the pipet ensures that a gentle meniscus contact is made with a substrate surface, which defines the active surface area of an electrochemical cell. The substrate can be an electrical conductor, semiconductor, or insulator. The main focus here is on the general case where the substrate is a working electrode, and both ion-conductance measurements between the QRCEs in the two barrels and voltammetric/amperometric measurements at the substrate can be made simultaneously. In usual practice, a small perpendicular oscillation of the probe with respect to the substrate is employed, so that an alternating conductance current (ac) develops, due to the change in the dimensions of the electrolyte contact (and hence resistance), as well as the direct conductance current (dc). It is shown that the dc current can be predicted for a fixed probe by solving the Nernst-Planck equation and that the ac response can also be derived from this response. Both responses are shown to agree well with experiment. It is found that the pipet geometry plays an important role in controlling the dc conductance current and that this is easily measured by microscopy. A key feature of SECCM is that mass transport to the substrate surface is by diffusion and, for charged analytes, ion migration which can be controlled and varied quantifiably via the bias between the two QRCEs. For a working electrode substrate this means that charged redox-active analytes can be transported to the electrode/solution interface in a well-defined and controllable manner and that relatively fast heterogeneous electron transfer kinetics can be studied. The factors controlling the voltammetric response are determined by

  9. Estimation of in-situ thermal conductivities from temperature gradient measurements

    SciTech Connect

    Hoang, V.T.

    1980-12-01

    A mathematical model has been developed to study the effect of variable thermal conductivity of the formations, and the wellbore characteristics, on the fluid temperature behavior inside the wellbore during injection or production and after shut-in. During the injection or production period the wellbore fluid temperature is controlled mainly by the fluid flow rate and the heat lost from the fluid to the formation. During the shut-in period, the fluid temperature is strongly affected by differences in the formation thermal conductivities. Based on the results of the present analysis, two methods for estimating in-situ thermal conductivity were derived. First, the line source concept is extended to estimate values of the formation thermal conductivities utilizing the fluid temperature record during the transient period of injection or production and shut-in. The second method is applied when a well is under thermal equilibrium conditions. Values of the formation thermal conductivities can also be estimated by using a continuous temperature gradient log and by measuring the thermal conductivity of the formation at a few selected wellbore locations.

  10. Dielectric Relaxation Behavior and AC Electrical Conductivity Study of 2-(1,2-Dihydro-7-Methyl-2-Oxoquinoline-5-yl) Malononitrile (DMOQMN)

    NASA Astrophysics Data System (ADS)

    El-Nahass, M. M.; El-Zaidia, E. F. M.; Darwish, A. A. A.; Salem, G. F.

    2017-02-01

    Dielectric relaxation and alternative current conductivity of a new organic compound 2-(1,2-dihydro-7-methyl-2-oxoquinoline-5-yl) malononitrile (DMOQMN) have been investigated. X-ray diffraction (XRD) at room temperature reveals that DMOQMN samples have a polycrystalline structure of the triclinic system. The analysis of the dielectric constant and dielectric loss index suggested the dominant polarization is performed and the Maxwell-Wagner-Sillar type polarization is dominating at low frequency and high temperature. These results have been confirmed by the XRD and dielectric modulus. The estimated relaxation time and the activation energy are 9 × 10-13 s and 0.43 eV, respectively. Our results indicated that the conduction mechanism of DMOQMN is controlled by the correlation barrier hopping (CBH) model.

  11. Predicting thermal conductivity of rocks from the Los Azufres geothermal field, Mexico, from easily measurable properties

    SciTech Connect

    Garcia, Alfonso; Contreras, Enrique; Dominquez, Bernardo A.

    1988-01-01

    A correlation is developed to predict thermal conductivity of drill cores from the Los Azufres geothermal field. Only andesites are included as they are predominant. Thermal conductivity of geothermal rocks is in general scarce and its determination is not simple. Almost all published correlations were developed for sedimentary rocks. Typically, for igneous rocks, chemical or mineral analyses are used for estimating conductivity by using some type of additive rule. This requires specialized analytical techniques and the procedure may not be sufficiently accurate if, for instance, a chemical analysis is to be changed into a mineral analysis. Thus a simple and accurate estimation method would be useful for engineering purposes. The present correlation predicts thermal conductivity from a knowledge of bulk density and total porosity, properties which provide basic rock characterization and are easy to measure. They may be determined from drill cores or cuttings, and the procedures represent a real advantage given the cost and low availability of cores. The multivariate correlation proposed is a quadratic polynomial and represents a useful tool to estimate thermal conductivity of igneous rocks since data on this property is very limited. For porosities between 0% and 25%, thermal conductivity is estimated with a maximum deviation of 22% and a residual mean square deviation of 4.62E-3 n terms of the log{sub 10}(k{rho}{sub b}) variable. The data were determined as part of a project which includes physical, thermal and mechanical properties of drill cores from Los Azufres. For the correlation, sixteen determinations of thermal conductivity, bulk density and total porosity are included. The conductivity data represent the first determinations ever made on these rocks.

  12. AC Electrokinetics of Physiological Fluids for Biomedical Applications.

    PubMed

    Lu, Yi; Liu, Tingting; Lamanda, Ariana C; Sin, Mandy L Y; Gau, Vincent; Liao, Joseph C; Wong, Pak Kin

    2015-12-01

    Alternating current (AC) electrokinetics is a collection of processes for manipulating bulk fluid mass and embedded objects with AC electric fields. The ability of AC electrokinetics to implement the major microfluidic operations, such as pumping, mixing, concentration, and separation, makes it possible to develop integrated systems for clinical diagnostics in nontraditional health care settings. The high conductivity of physiological fluids presents new challenges and opportunities for AC electrokinetics-based diagnostic systems. In this review, AC electrokinetic phenomena in conductive physiological fluids are described followed by a review of the basic microfluidic operations and the recent biomedical applications of AC electrokinetics. The future prospects of AC electrokinetics for clinical diagnostics are presented.

  13. AC Electrokinetics of Physiological Fluids for Biomedical Applications

    PubMed Central

    Lu, Yi; Liu, Tingting; Lamanda, Ariana C.; Sin, Mandy L Y; Gau, Vincent; Liao, Joseph C.; Wong, Pak Kin

    2016-01-01

    AC electrokinetics is a collection of processes for manipulating bulk fluid mass and embedded objects with AC electric fields. The ability of AC electrokinetics to implement the major microfluidic operations, such as pumping, mixing, concentration and separation, makes it possible to develop integrated systems for clinical diagnostics in non-traditional healthcare settings. The high conductivity of physiological fluids presents new challenges and opportunities for AC electrokinetics based diagnostic systems. In this review, AC electrokinetic phenomena in conductive physiological fluids are described followed by a review of the basic microfluidic operations and the recent biomedical applications of AC electrokinetics. The future prospects of AC electrokinetics for clinical diagnostics are presented. PMID:25487557

  14. A simulation of the measurement of electrical conductivity in randomly generated two-phase rocks.

    NASA Astrophysics Data System (ADS)

    Mandolesi, Eric; Moorkamp, Max; Jones, Alan G.

    2014-05-01

    Geological models of the subsurface require detailed data, often unavailable from direct observation or well logs. Hence imaging the subsurface relies on models obtained by interpretation of geophysical data. Several electromagnetic (EM) geophysical methods focus on the EM properties of rocks and sediments to determine a reliable image of the subsurface, while the same electromagnetic properties are directly measured in laboratories. Often these laboratory measurements return equivocal results that are difficult to reconcile with field observations. Recently different numerical approaches have been investigated in order to understand the effects of the geometry and continuity of interconnected pathways of conductors on EM field measurements, often restricting the studies to direct current (DC) sources. Bearing in mind the time-varying nature of the natural electromagnetic sources that play a role in field measurements, we numerically simulate the effects of such EM sources on the conductivity measured on the surface of a randomly generated three-dimensional body embedded in a uniform host by using electromagnetic induction equations, thus simulating a magnetotelluric (MT) survey. A key point in such a simulation is the scalability of the problem: the deeper the target, the longer the period of the EM source is needed. On the other hand, a long period signal ignores small heterogeneous conductors in the target bulk of the material, averaging the different conductivities in a median value. Since most real rocks are poor conductors, we have modeled a two-phase mixture of rock and interconnected conductive elements (representing melts, saline fluids, sulphidic, carbonitic, or metallic sediments, etc.), randomly generated within the background host. We have compared the results from the simulated measurements with the target rock embedded at different depths with electrical conductivity predicted by both Hashin-Shtrikman (HS) bounds and an updated multi-phase Archie

  15. Copper and silver selenide crystal growth rate measurements as a method for determination of ionic conductivity

    NASA Astrophysics Data System (ADS)

    Vučić, Zlatko; Lovrić, Davorin; Gladić, Jadranko; Etlinger, Božidar

    2004-03-01

    The motivation behind this work is the discrepancy between the measured and calculated growth rates of copper selenide spherical single crystals between 740 and 800 K. The growth of cylindrical polycrystalline samples of copper selenide at high temperatures was monitored in experiments that enabled full control of the geometry of growth. Together with the calculations based on Yokota's transport equation, these measurements eliminated ionic conductivity data as a possible reason behind too high values of the calculated growth rates. The equivalent growth experiments on polycrystalline silver selenide samples were performed as a test of the method, yielding excellent agreement with the results obtained by extrapolation of existing data. On the basis of these measurements and associated analysis, this method is proposed as a method for determination of ionic conductivity of mixed superionic conductors on temperatures up to the temperatures of melting, i.e. in the range in which other methods of ionic conductivity measurements either do not work or are not accurate enough.

  16. Hydrostatic Pressure Study on 3-K Phase Superconductivity in Sr2RuO4-Ru Eutectic Crystals by AC Magnetic Susceptibility Measurements

    NASA Astrophysics Data System (ADS)

    Yaguchi, Hiroshi; Watanabe, Hiromichi; Sakaue, Akira

    2012-12-01

    We have investigated the effect of hydrostatic pressure on 3-K phase superconductivity in Sr2RuO4-Ru eutectic crystals by means of AC magnetic susceptibility measurements. We have found that the application of hydrostatic pressure suppresses the superconducting transition temperature Tc of the 3-K phase with a pressure coefficient of dTc/dP ≈ -0.2 K/GPa, similar to the case of the 1.5-K phase. We have also observed that the effect of hydrostatic pressure on the 3-K phase seems to be elastic whilst that of uniaxial pressure is plastic.

  17. Photoacoustic infrared spectroscopy for conducting gas tracer tests and measuring water saturations in landfills

    SciTech Connect

    Jung, Yoojin; Han, Byunghyun; Mostafid, M. Erfan; Chiu, Pei; Yazdani, Ramin; Imhoff, Paul T.

    2012-02-15

    Highlights: Black-Right-Pointing-Pointer Photoacoustic infrared spectroscopy tested for measuring tracer gas in landfills. Black-Right-Pointing-Pointer Measurement errors for tracer gases were 1-3% in landfill gas. Black-Right-Pointing-Pointer Background signals from landfill gas result in elevated limits of detection. Black-Right-Pointing-Pointer Technique is much less expensive and easier to use than GC. - Abstract: Gas tracer tests can be used to determine gas flow patterns within landfills, quantify volatile contaminant residence time, and measure water within refuse. While gas chromatography (GC) has been traditionally used to analyze gas tracers in refuse, photoacoustic spectroscopy (PAS) might allow real-time measurements with reduced personnel costs and greater mobility and ease of use. Laboratory and field experiments were conducted to evaluate the efficacy of PAS for conducting gas tracer tests in landfills. Two tracer gases, difluoromethane (DFM) and sulfur hexafluoride (SF{sub 6}), were measured with a commercial PAS instrument. Relative measurement errors were invariant with tracer concentration but influenced by background gas: errors were 1-3% in landfill gas but 4-5% in air. Two partitioning gas tracer tests were conducted in an aerobic landfill, and limits of detection (LODs) were 3-4 times larger for DFM with PAS versus GC due to temporal changes in background signals. While higher LODs can be compensated by injecting larger tracer mass, changes in background signals increased the uncertainty in measured water saturations by up to 25% over comparable GC methods. PAS has distinct advantages over GC with respect to personnel costs and ease of use, although for field applications GC analyses of select samples are recommended to quantify instrument interferences.

  18. Planar system for magnetic induction conductivity measurement using a sensor matrix.

    PubMed

    Riedel, C H; Keppelen, M; Nani, S; Merges, R D; Dössel, O

    2004-02-01

    In this study the performance of an axial gradiometer sensor for magnetic induction tomography was investigated and the results of measurements to determine the precision and sensitivity of the sensor were undertaken. In the first part of the study a single gradiometer sensor was used and the noise and drift were measured for two excitation current values at a single frequency of 600 kHz. The variations of the real and imaginary received signal components with conductivity were then obtained for samples with 0-5 S m(-1). Both sets of measurements were repeated using two different forms of capacitive shielding. In the second part of the study the results of preliminary measurements obtained with a 2 x 2 planar matrix of axial gradiometers are given. The results of a simulation of a similar matrix using a commercial electromagnetic field calculation programme are also presented for comparison. For the sample utilized, the sensor output showed a linear variation with conductivity for the imaginary component of 0.033 mV S(-1) m using an excitation current of 316 mA at 600 kHz. No apparent correlation with conductivity for the real component was observed. The noise and drift of the imaginary component of the sensor output were 0.001 mV and 0.006 mV respectively, for the same excitation current. The results of the planar matrix measurements and simulations suggest that significant sensitivity is provided by using the measurement coils of the adjacent sensors. The measurement results however suggest that large improvements in the sensor noise and drift performance are required for these data to be of use.

  19. Conductive heat flux in measurements of the Nusselt number in turbulent Rayleigh-Bénard convection

    NASA Astrophysics Data System (ADS)

    Shishkina, Olga; Weiss, Stephan; Bodenschatz, Eberhard

    2016-10-01

    We propose a recipe to calculate accurately the Nusselt number Nu in turbulent Rayleigh-Bénard convection, using the measured total heat flux q and known parameters of the fluid and convection cell. More precisely, we present a method to compute the conductive heat flux q ̂, which is a normalization of q in the definition of Nu, for conditions where the fluid parameters may vary strongly across the fluid layer. We show that in the Oberbeck-Boussinesq approximation and also when the thermal conductivity depends exclusively on the temperature, the value of q ̂ is determined by simple explicit formulas. For a general non-Oberbeck-Boussinesq (NOB) case we propose an iterative procedure to compute q ̂. Using our procedure, we critically analyze some already conducted and some hypothetical experiments and show how q ̂ is influenced by the NOB effects.

  20. Insulator-protected mechanically controlled break junctions for measuring single-molecule conductance in aqueous environments

    NASA Astrophysics Data System (ADS)

    Muthusubramanian, N.; Galan, E.; Maity, C.; Eelkema, R.; Grozema, F. C.; van der Zant, H. S. J.

    2016-07-01

    We present a method to fabricate insulated gold mechanically controlled break junctions (MCBJ) by coating the metal with a thin layer of aluminum oxide using plasma enhanced atomic layer deposition. The Al2O3 thickness deposited on the MCBJ devices was varied from 2 to 15 nm to test the suppression of leakage currents in deionized water and phosphate buffered saline. Junctions coated with a 15 nm thick oxide layer yielded atomically sharp electrodes and negligible conductance counts in the range of 1 to 10-4 G0 (1 G0 = 77 μS), where single-molecule conductances are commonly observed. The insulated devices were used to measure the conductance of an amphiphilic oligophenylene ethynylene derivative in deionized water.

  1. Measurement of conductivity and permittivity on samples sealed in nuclear magnetic resonance tubes

    SciTech Connect

    Huang, W.; Angell, C. A.; Yarger, J. L.; Richert, R.

    2013-07-15

    We present a broadband impedance spectroscopy instrument designed to measure conductivity and/or permittivity for samples that are sealed in glass tubes, such as the standard 5 mm tubes used for nuclear magnetic resonance experiments. The calibrations and corrections required to extract the dielectric properties of the sample itself are outlined. It is demonstrated that good estimates of the value of dc-conductivity can be obtained even without correcting for the effects of glass or air on the overall impedance. The approach is validated by comparing data obtained from samples sealed in nuclear magnetic resonance tubes with those from standard dielectric cells, using glycerol and butylmethylimidazolium-hexafluorophosphate as respective examples of a molecular and an ionic liquid. This instrument and approach may prove useful for other studies of permittivity and conductivity where contact to the metal electrodes or to the ambient atmosphere needs to be avoided.

  2. Experimental Investigation of Electrical Conductivity and Permittivity of SC-TiO 2 -EG Nanofluids.

    PubMed

    Fal, Jacek; Barylyak, Adriana; Besaha, Khrystyna; Bobitski, Yaroslav V; Cholewa, Marian; Zawlik, Izabela; Szmuc, Kamil; Cebulski, Józef; Żyła, Gaweł

    2016-12-01

    The paper presents experimental studies of dielectric properties of nanofluids based on ethylene glycol and SC-TiO2 nanoparticles with average size of 15-40 nm with various mass concentrations. The dielectric permittivity both real part and imaginary part as a function of temperature and frequency were measured. Also, dependence ac conductivity on frequency, temperature, and mass concentration were investigated. Based on the curves of ac conductivity, dc conductivity was calculated, and 400 % enhancement in dc conductivity was exposed.

  3. Experimental Investigation of Electrical Conductivity and Permittivity of SC-TiO 2 -EG Nanofluids

    NASA Astrophysics Data System (ADS)

    Fal, Jacek; Barylyak, Adriana; Besaha, Khrystyna; Bobitski, Yaroslav V.; Cholewa, Marian; Zawlik, Izabela; Szmuc, Kamil; Cebulski, Józef; żyła, Gaweł

    2016-08-01

    The paper presents experimental studies of dielectric properties of nanofluids based on ethylene glycol and SC-TiO2 nanoparticles with average size of 15-40 nm with various mass concentrations. The dielectric permittivity both real part and imaginary part as a function of temperature and frequency were measured. Also, dependence ac conductivity on frequency, temperature, and mass concentration were investigated. Based on the curves of ac conductivity, dc conductivity was calculated, and 400 % enhancement in dc conductivity was exposed.

  4. A novel method for measuring hydraulic conductivity at the human blood-nerve barrier in vitro.

    PubMed

    Helton, E Scott; Palladino, Steven; Ubogu, Eroboghene E

    2017-01-01

    Microvascular barrier permeability to water is an essential biophysical property required for the homeostatic maintenance of unique tissue microenvironments. This is of particular importance in peripheral nerves where strict control of ionic concentrations is needed for axonal signal transduction. Previous studies have associated inflammation, trauma, toxin exposure and metabolic disease with increases in water influx and hydrostatic pressure in peripheral nerves with resultant endoneurial edema that may impair axonal function. The regulation of water permeability across endoneurial microvessels that form the blood-nerve barrier (BNB) is poorly understood. Variations exist in apparatus and methods used to measure hydraulic conductivity. The objective of the study was to develop a simplified hydraulic conductivity system using commercially available components to evaluate the BNB. We determined the mean hydraulic conductivity of cultured confluent primary and immortalized human endoneurial endothelial cell layers as 2.00×10(-7) and 2.17×10(-7)cm/s/cm H₂O respectively, consistent with restrictive microvascular endothelial cells in vitro. We also determined the mean hydraulic conductivity of immortalized human brain microvascular endothelial cell layers, a commonly used blood-brain barrier (BBB) cell line, as 0.20×10(-7)cm/s/cm H₂O, implying a mean 10-fold higher resistance to transendothelial water flux in the brain compared to peripheral nerves. To our knowledge, this is the first reported measurement of human BNB and BBB hydraulic conductivities. This model represents an important tool to further characterize the human BNB and deduce the molecular determinants and signaling mechanisms responsible for BNB hydraulic conductivity in normal and disease states in vitro.

  5. Electronmagnetic induction probe calibration for electrical conductivity measurements and moisture content determination of Hanford high level waste

    SciTech Connect

    Wittekind, W.D., Westinghouse Hanford

    1996-05-23

    Logic of converting EMI measured electrical conductivity to moisture with expected uncertainty. Estimates from present knowledge, assumptions, and measured data. Archie`s Law has been used since the 1940`s to relate electrical conductivity in porous media to liquid volume fraction. Measured electrical conductivity to moisture content uses: Porosity, Interstitial liquid electrical conductivity, Solid particle density,Interstitial liquid density, and interstitial liquid water content. The uncertainty of assumed values is calculated to determine the final moisture wt.% result uncertainty.

  6. Thermal conductivity measurement and interface thermal resistance estimation using SiO2 thin film.

    PubMed

    Chien, Heng-Chieh; Yao, Da-Jeng; Huang, Mei-Jiau; Chang, Tien-Yao

    2008-05-01

    In this paper, we describe an easy-to-use method to measure the thermal conductivity of thin films based on an electrical heating/sensing mechanism and a steady-state technique. The method used relative commonly used instruments, and without any signal processing circuit, is easy to be used in such thin-film thermal conductivity measurement. The SiO2 thin-film samples, prepared by thermal oxidation, plasma enhanced chemical vapor deposition (PECVD), and E-beam evaporator, were deposited on a silicon substrate. The apparent thermal conductivity, the intrinsic thermal conductivity of SiO2 films, and the total interface thermal resistance of the heater/SiO2/silicon system were evaluated. Our data showed agreement with those data obtained from previous literatures and from the 3 omega method. Furthermore, by using a sandwiched structure, the interface thermal resistance of Cr/PECVD SiO2 and PECVD SiO2/silicon were also separately evaluated in this work. The data showed that the interface thermal resistance of Cr/PECVD SiO2 (metal/dielectric) is about one order of magnitude larger than that of PECVD SiO2/silicon (dielectric/dielectric).

  7. A novel apparatus for in situ measurement of thermal conductivity of hydrate-bearing sediments

    NASA Astrophysics Data System (ADS)

    Zhao, Jiafei; Wang, Bin; Yang, Lei; Cheng, Chuanxiao; Song, Yongchen

    2015-08-01

    An experimental apparatus was developed to synthesize natural gas hydrates and measure the thermal conductivity of hydrate-bearing sediments in situ. The apparatus works over a temperature range varying from -20 °C to 50 °C and up to a maximum pressure of 20 MPa. This apparatus is mainly composed of a thermal conductivity test system and a reaction cell, into which a lab-fabricated thermistor probe is inserted. This thermistor has excellent temperature sensitivity and can work at high pressures. The basic principles of this apparatus are discussed, and a series of experiments were performed to verify that the apparatus can be practically applied in chemical engineering. The thermistor-based measuring method was applied successfully in a high-pressure environment both with and without porous media.

  8. A novel apparatus for in situ measurement of thermal conductivity of hydrate-bearing sediments.

    PubMed

    Zhao, Jiafei; Wang, Bin; Yang, Lei; Cheng, Chuanxiao; Song, Yongchen

    2015-08-01

    An experimental apparatus was developed to synthesize natural gas hydrates and measure the thermal conductivity of hydrate-bearing sediments in situ. The apparatus works over a temperature range varying from -20 °C to 50 °C and up to a maximum pressure of 20 MPa. This apparatus is mainly composed of a thermal conductivity test system and a reaction cell, into which a lab-fabricated thermistor probe is inserted. This thermistor has excellent temperature sensitivity and can work at high pressures. The basic principles of this apparatus are discussed, and a series of experiments were performed to verify that the apparatus can be practically applied in chemical engineering. The thermistor-based measuring method was applied successfully in a high-pressure environment both with and without porous media.

  9. Electrical conductivity measurements of aqueous electrolyte solutions at high temperatures and high pressures

    SciTech Connect

    Ho, P.C.; Palmer, D.A.

    1995-02-01

    In aqueous solutions all electrolytes tend to associate at high temperatures (low dielectric constants). Ion association results in the formation of uncharged substrates, which are substantially more volatile than their precursor ions. Thus knowledge of the association constants is important in interpreting the thermodynamics of the partitioning of electrolytes to the vapor phase in a fully speciated approach. Electrical conductance measurements provide a unique window into ionic interactions of solutions at high temperatures and pressures. In this study, the electrical conductivities of dilute (<0.1 molal) aqueous solutions of NaCl (100-600{degrees}C to 300 MPa) and sodium and potassium hydroxides (0-600 and 100-600{degrees}C, respectively, and to 300 MPa) were measured. The results show that the extent of association of Na{sup +} and Cl{sup -} is similar to those for Na{sup +} and K{sup +} with OH{sup -} in solution from subcritical to supercritical conditions.

  10. Measurement of temperature-dependent viscosity and thermal conductivity of alumina and titania thermal oil nanofluids

    NASA Astrophysics Data System (ADS)

    Cieśliński, Janusz T.; Ronewicz, Katarzyna; Smoleń, Sławomir

    2015-12-01

    In this study the results of simultaneous measurements of dynamic viscosity, thermal conductivity, electrical conductivity and pH of two nanofluids, i.e., thermal oil/Al2O3 and thermal oil/TiO2 are presented. Thermal oil is selected as a base liquid because of possible application in ORC systems as an intermediate heating agent. Nanoparticles were tested at the concentration of 0.1%, 1%, and 5% by weight within temperature range from 20 °C to 60 °C. Measurement devices were carefully calibrated by comparison obtained results for pure base liquid (thermal oil) with manufacturer's data. The results obtained for tested nanofluids were compared with predictions made by use of existing models for liquid/solid particles mixtures.

  11. Thermal separation of soil particles from thermal conductivity measurement under various air pressures

    NASA Astrophysics Data System (ADS)

    Lu, Sen; Ren, Tusheng; Lu, Yili; Meng, Ping; Zhang, Jinsong

    2017-01-01

    The thermal conductivity of dry soils is related closely to air pressure and the contact areas between solid particles. In this study, the thermal conductivity of two-phase soil systems was determined under reduced and increased air pressures. The thermal separation of soil particles, i.e., the characteristic dimension of the pore space (d), was then estimated based on the relationship between soil thermal conductivity and air pressure. Results showed that under both reduced and increased air pressures, d estimations were significantly larger than the geometrical mean separation of solid particles (D), which suggested that conductive heat transfer through solid particles dominated heat transfer in dry soils. The increased air pressure approach gave d values lower than that of the reduced air pressure method. With increasing air pressure, more collisions between gas molecules and solid surface occurred in micro-pores and intra-aggregate pores due to the reduction of mean free path of air molecules. Compared to the reduced air pressure approach, the increased air pressure approach expressed more micro-pore structure attributes in heat transfer. We concluded that measuring thermal conductivity under increased air pressure procedures gave better-quality d values, and improved soil micro-pore structure estimation.

  12. Thermal conductivity of a film of single walled carbon nanotubes measured with infrared thermal imager

    NASA Astrophysics Data System (ADS)

    Feng, Ya; Inoue, Taiki; Xiang, Rong; Chiashi, Shohei; Maruyama, Shigeo

    Heat dissipation has restricted the modern miniaturization trend with the development of electronic devices. Theoretically proven to be with high axial thermal conductivity, single walled carbon nanotubes (SWNT) have long been expected to cool down the nanoscale world. Even though the tube-tube contact resistance limits the capability of heat transfer of the bulk film, the high intrinsic thermal conductivity of SWNT still glorify the application of films of SWNT network as a thermal interface material. In this work, we proposed a new method to straightly measure the thermal conductivity of SWNT film. We bridged two cantilevered Si thin plate with SWNT film, and kept a steady state heat flow in between. With the infrared camera to record the temperature distribution, the Si plates with known thermal conductivity can work as a reference to calculate the heat flux going through the SWNT film. Further, the thermal conductivity of the SWNT film can be obtained through Fourier's law after deducting the effect of thermal radiation. The sizes of the structure, the heating temperature, the vacuum degree and other crucial impact factors are carefully considered and analyzed. The author Y. F. was supported through the Advanced Integration Science Innovation Education and Research Consortium Program by the Ministry of Education, Culture, Sport, Science and Technology.

  13. Auto-Tuned Induction Coil Conductivity Sensor for In-Vivo Human Tissue Measurements

    NASA Astrophysics Data System (ADS)

    Heller, J.; Feldkamp, J. R.

    2009-01-01

    Auto-tuned induction coil technology, based upon phase-locked loop circuitry (PLL), was developed and shown to be an effective tool for in-vivo measurement of electrical conductivity of human tissues. Because electrical contact is not required, several disadvantages of the electrode method for conductivity determination are avoided, such as electrode polarization and variable conductivity associated with the stratum corneum of the epidermis. Fixed frequency excitation is supplied to a parallel tuned RLC circuit, or "sensor", while bias applied to a varactor diode is automatically adjusted via PLL circuitry to maintain the RLC sensor at resonance. Since resonant impedance of a coil positioned near a conductive object is known to be frequency dependent, such an arrangement permits precise calibration of the sensor against a set of standard Potassium Chloride solutions. In our experiments, a two-layer spiral coil is used with upper and lower spiral arms staggered so as to reduce inter-winding coil capacitance. Preliminary in-vivo testing was done on the forearms of a single male subject as a prelude to more extensive use in a clinical setting. In that instance, electrical conductivity at the proximal volar forearm location was shown to depend on forearm elevation. Clinical studies using our prototype, as well as further consideration of the "elevation effect", are discussed in a companion paper.

  14. Thermal conductivity and viscosity measurements of ethylene glycol-based Al2O3 nanofluids

    PubMed Central

    2011-01-01

    The dispersion and stability of nanofluids obtained by dispersing Al2O3 nanoparticles in ethylene glycol have been analyzed at several concentrations up to 25% in mass fraction. The thermal conductivity and viscosity were experimentally determined at temperatures ranging from 283.15 K to 323.15 K using an apparatus based on the hot-wire method and a rotational viscometer, respectively. It has been found that both thermal conductivity and viscosity increase with the concentration of nanoparticles, whereas when the temperature increases the viscosity diminishes and the thermal conductivity rises. Measured enhancements on thermal conductivity (up to 19%) compare well with literature values when available. New viscosity experimental data yield values more than twice larger than the base fluid. The influence of particle size on viscosity has been also studied, finding large differences that must be taken into account for any practical application. These experimental results were compared with some theoretical models, as those of Maxwell-Hamilton and Crosser for thermal conductivity and Krieger and Dougherty for viscosity. PMID:21711737

  15. Thermal separation of soil particles from thermal conductivity measurement under various air pressures.

    PubMed

    Lu, Sen; Ren, Tusheng; Lu, Yili; Meng, Ping; Zhang, Jinsong

    2017-01-05

    The thermal conductivity of dry soils is related closely to air pressure and the contact areas between solid particles. In this study, the thermal conductivity of two-phase soil systems was determined under reduced and increased air pressures. The thermal separation of soil particles, i.e., the characteristic dimension of the pore space (d), was then estimated based on the relationship between soil thermal conductivity and air pressure. Results showed that under both reduced and increased air pressures, d estimations were significantly larger than the geometrical mean separation of solid particles (D), which suggested that conductive heat transfer through solid particles dominated heat transfer in dry soils. The increased air pressure approach gave d values lower than that of the reduced air pressure method. With increasing air pressure, more collisions between gas molecules and solid surface occurred in micro-pores and intra-aggregate pores due to the reduction of mean free path of air molecules. Compared to the reduced air pressure approach, the increased air pressure approach expressed more micro-pore structure attributes in heat transfer. We concluded that measuring thermal conductivity under increased air pressure procedures gave better-quality d values, and improved soil micro-pore structure estimation.

  16. Thermal separation of soil particles from thermal conductivity measurement under various air pressures

    PubMed Central

    Lu, Sen; Ren, Tusheng; Lu, Yili; Meng, Ping; Zhang, Jinsong

    2017-01-01

    The thermal conductivity of dry soils is related closely to air pressure and the contact areas between solid particles. In this study, the thermal conductivity of two-phase soil systems was determined under reduced and increased air pressures. The thermal separation of soil particles, i.e., the characteristic dimension of the pore space (d), was then estimated based on the relationship between soil thermal conductivity and air pressure. Results showed that under both reduced and increased air pressures, d estimations were significantly larger than the geometrical mean separation of solid particles (D), which suggested that conductive heat transfer through solid particles dominated heat transfer in dry soils. The increased air pressure approach gave d values lower than that of the reduced air pressure method. With increasing air pressure, more collisions between gas molecules and solid surface occurred in micro-pores and intra-aggregate pores due to the reduction of mean free path of air molecules. Compared to the reduced air pressure approach, the increased air pressure approach expressed more micro-pore structure attributes in heat transfer. We concluded that measuring thermal conductivity under increased air pressure procedures gave better-quality d values, and improved soil micro-pore structure estimation. PMID:28054663

  17. Estimating Concentrations of Road-Salt Constituents in Highway-Runoff from Measurements of Specific Conductance

    USGS Publications Warehouse

    Granato, Gregory E.; Smith, Kirk P.

    1999-01-01

    Discrete or composite samples of highway runoff may not adequately represent in-storm water-quality fluctuations because continuous records of water stage, specific conductance, pH, and temperature of the runoff indicate that these properties fluctuate substantially during a storm. Continuous records of water-quality properties can be used to maximize the information obtained about the stormwater runoff system being studied and can provide the context needed to interpret analyses of water samples. Concentrations of the road-salt constituents calcium, sodium, and chloride in highway runoff were estimated from theoretical and empirical relations between specific conductance and the concentrations of these ions. These relations were examined using the analysis of 233 highwayrunoff samples collected from August 1988 through March 1995 at four highway-drainage monitoring stations along State Route 25 in southeastern Massachusetts. Theoretically, the specific conductance of a water sample is the sum of the individual conductances attributed to each ionic species in solution-the product of the concentrations of each ion in milliequivalents per liter (meq/L) multiplied by the equivalent ionic conductance at infinite dilution-thereby establishing the principle of superposition. Superposition provides an estimate of actual specific conductance that is within measurement error throughout the conductance range of many natural waters, with errors of less than ?5 percent below 1,000 microsiemens per centimeter (?S/cm) and ?10 percent between 1,000 and 4,000 ?S/cm if all major ionic constituents are accounted for. A semi-empirical method (adjusted superposition) was used to adjust for concentration effects-superposition-method prediction errors at high and low concentrations-and to relate measured specific conductance to that calculated using superposition. The adjusted superposition method, which was developed to interpret the State Route 25 highway-runoff records, accounts for

  18. Summary of round robin measurements of radiation induced conductivity in Wesgo AL995 alumina

    SciTech Connect

    Zinkle, S.J.

    1996-10-01

    This existing data on radiation induced conductivity (RIC) measurements performed on the same heat of the IEA reference ceramic insulator are summarized. Six different sets of RIC measurements have been performed on Wesgo AL995 at dose rates between 10 Gy/s and 1 MGy/s. In general, good agreement was obtained between the different groups of researchers. The data indicate that the RIC at a test temperature of 400-500{degrees}C is approximately linear with ionizing dose rate up to {approximately}1000 Gy/s, and exhibits an approximately square root dependence on dose rate between 1 kGy/s and 1 MGy/s.

  19. Technique for direct measurement of thermal conductivity of elastomers and a detailed uncertainty analysis

    NASA Astrophysics Data System (ADS)

    Ralphs, Matthew I.; Smith, Barton L.; Roberts, Nicholas A.

    2016-11-01

    High thermal conductivity thermal interface materials (TIMs) are needed to extend the life and performance of electronic circuits. A stepped bar apparatus system has been shown to work well for thermal resistance measurements with rigid materials, but most TIMs are elastic. This work studies the uncertainty of using a stepped bar apparatus to measure the thermal resistance and a tensile/compression testing machine to estimate the compressed thickness of polydimethylsiloxane for a measurement on the thermal conductivity, k eff. An a priori, zeroth order analysis is used to estimate the random uncertainty from the instrumentation; a first order analysis is used to estimate the statistical variation in samples; and an a posteriori, Nth order analysis is used to provide an overall uncertainty on k eff for this measurement method. Bias uncertainty in the thermocouples is found to be the largest single source of uncertainty. The a posteriori uncertainty of the proposed method is 6.5% relative uncertainty (68% confidence), but could be reduced through calibration and correlated biases in the temperature measurements.

  20. On-chip electrochemical microsystems for measurements of copper and conductivity in artificial seawater.

    PubMed

    Herzog, Grégoire; Moujahid, Waleed; Twomey, Karen; Lyons, Conor; Ogurtsov, Vladimir I

    2013-11-15

    The fabrication and characterisation of microelectrochemical sensors for Cu(2+) and conductivity suitable for operation in the marine environment are presented. The impact of the designs on sensor performance and their adequacy to operate in real conditions are discussed. The sensors, tailored to voltammetric and impedimetric measurements, are fabricated on silicon using photolithographic and thin film deposition techniques. The impedimetric sensor is made of Pt interdigitated electrodes which are used for the measurement of conductivity. The voltammetric sensors are based on a three electrode electrochemical cell with on-chip Ag|AgCl reference and Pt counter and working electrodes, used for detection of copper by underpotential deposition-stripping voltammetry at microelectrode array. The sensors operated in the Cu(2+) concentrations ranging from 0.48 to 3.97 µM with a limit of detection of 0.115 μM. The impact of the temperature, the pH and the salinity of the artificial seawater on the sensitivity for Cu(2+) detection are also considered. Measurements of copper concentration and conductivity are validated using certified reference materials and standard solutions.

  1. Measurement of thermal conductivity and thermal diffusivity using a thermoelectric module

    NASA Astrophysics Data System (ADS)

    Beltrán-Pitarch, Braulio; Márquez-García, Lourdes; Min, Gao; García-Cañadas, Jorge

    2017-04-01

    A proof of concept of using a thermoelectric module to measure both thermal conductivity and thermal diffusivity of bulk disc samples at room temperature is demonstrated. The method involves the calculation of the integral area from an impedance spectrum, which empirically correlates with the thermal properties of the sample through an exponential relationship. This relationship was obtained employing different reference materials. The impedance spectroscopy measurements are performed in a very simple setup, comprising a thermoelectric module, which is soldered at its bottom side to a Cu block (heat sink) and thermally connected with the sample at its top side employing thermal grease. Random and systematic errors of the method were calculated for the thermal conductivity (18.6% and 10.9%, respectively) and thermal diffusivity (14.2% and 14.7%, respectively) employing a BCR724 standard reference material. Although errors are somewhat high, the technique could be useful for screening purposes or high-throughput measurements at its current state. This new method establishes a new application for thermoelectric modules as thermal properties sensors. It involves the use of a very simple setup in conjunction with a frequency response analyzer, which provides a low cost alternative to most of currently available apparatus in the market. In addition, impedance analyzers are reliable and widely spread equipment, which facilities the sometimes difficult access to thermal conductivity facilities.

  2. Study of single-nucleotide polymorphisms by means of electrical conductance measurements

    NASA Astrophysics Data System (ADS)

    Hihath, Joshua; Xu, Bingqian; Zhang, Peiming; Tao, Nongjian

    2005-11-01

    Understanding the complexities of DNA has been a hallmark of science for over a half century, and one of the important topics in DNA research is recognizing the occurrence of mutations in the base-stack. In this article, we present a study of SNPs by direct-contact electrical measurements to a single DNA duplex. We have used short, 11- and 12-bp dsDNA to investigate the change in conductance that occurs if a single base pair, a single base, or two separate bases in the stack are modified. All measurements are carried out in aqueous solution with the DNA chemically bound to the electrodes. These measurements demonstrate that the presence of a single base pair mismatch can be identified by the conductance of the molecule and can cause a change in the conductance of dsDNA by as much as an order of magnitude, depending on the specific details of the double helix and the single nucleotide polymorphism. molecular electronics | scanning tunneling microscope break junction

  3. Thermal conductivity measurements via time-domain thermoreflectance for the characterization of radiation induced damage

    SciTech Connect

    Cheaito, Ramez; Gorham, Caroline S.; Misra, Amit; Hattar, Khalid; Hopkins, Patrick E.

    2015-05-01

    The progressive build up of displacement damage and fission products inside different systems and components of a nuclear reactor can lead to significant defect formation, degradation, and damage of the constituent materials. This structural modification can highly influence the thermal transport mechanisms and various mechanical properties of solids. In this paper we demonstrate the use of time-domain thermoreflectance (TDTR), a non-destructive method capable of measuring the thermal transport in material systems from nano to bulk scales, to study the effect of radiation damage and the subsequent changes in the thermal properties of materials. We use TDTR to show that displacement damage from ion irradiation can significantly reduce the thermal conductivity of Optimized ZIRLO, a material used as fuel cladding in several current nuclear reactors. We find that the thermal conductivity of copper-niobium nanostructured multilayers does not change with helium ion irradiation doses of up to 1015 cm-2 and ion energy of 200 keV suggesting that these structures can be used and radiation tolerant materials in nuclear reactors. We compare the effect of ion doses and ion beam energies on the measured thermal conductivity of bulk silicon. Results demonstrate that TDTR thermal measurements can be used to quantify depth dependent damage.

  4. Thermal conductivity measurements via time-domain thermoreflectance for the characterization of radiation induced damage

    DOE PAGES

    Cheaito, Ramez; Gorham, Caroline S.; Carnegie Mellon Univ., Pittsburgh, PA; ...

    2015-05-01

    The progressive build up of displacement damage and fission products inside different systems and components of a nuclear reactor can lead to significant defect formation, degradation, and damage of the constituent materials. This structural modification can highly influence the thermal transport mechanisms and various mechanical properties of solids. In this paper we demonstrate the use of time-domain thermoreflectance (TDTR), a non-destructive method capable of measuring the thermal transport in material systems from nano to bulk scales, to study the effect of radiation damage and the subsequent changes in the thermal properties of materials. We use TDTR to show that displacementmore » damage from ion irradiation can significantly reduce the thermal conductivity of Optimized ZIRLO, a material used as fuel cladding in several current nuclear reactors. We find that the thermal conductivity of copper-niobium nanostructured multilayers does not change with helium ion irradiation doses of up to 1015 cm-2 and ion energy of 200 keV suggesting that these structures can be used and radiation tolerant materials in nuclear reactors. We compare the effect of ion doses and ion beam energies on the measured thermal conductivity of bulk silicon. Results demonstrate that TDTR thermal measurements can be used to quantify depth dependent damage.« less

  5. Apparatus Measures Thermal Conductance Through a Thin Sample from Cryogenic to Room Temperature

    NASA Technical Reports Server (NTRS)

    Tuttle, James G.

    2009-01-01

    An apparatus allows the measurement of the thermal conductance across a thin sample clamped between metal plates, including thermal boundary resistances. It allows in-situ variation of the clamping force from zero to 30 lb (133.4 N), and variation of the sample temperature between 40 and 300 K. It has a special design feature that minimizes the effect of thermal radiation on this measurement. The apparatus includes a heater plate sandwiched between two identical thin samples. On the side of each sample opposite the heater plate is a cold plate. In order to take data, the heater plate is controlled at a slightly higher temperature than the two cold plates, which are controlled at a single lower temperature. The steady-state controlling power supplied to the hot plate, the area and thickness of samples, and the temperature drop across the samples are then used in a simple calculation of the thermal conductance. The conductance measurements can be taken at arbitrary temperatures down to about 40 K, as the entire setup is cooled by a mechanical cryocooler. The specific geometry combined with the pneumatic clamping force control system and the steady-state temperature control approach make this a unique apparatus.

  6. Conductive shield for ultra-low-field magnetic resonance imaging: Theory and measurements of eddy currents

    PubMed Central

    Zevenhoven, Koos C. J.; Busch, Sarah; Hatridge, Michael; Öisjöen, Fredrik; Ilmoniemi, Risto J.; Clarke, John

    2014-01-01

    Eddy currents induced by applied magnetic-field pulses have been a common issue in ultra-low-field magnetic resonance imaging. In particular, a relatively large prepolarizing field—applied before each signal acquisition sequence to increase the signal—induces currents in the walls of the surrounding conductive shielded room. The magnetic-field transient generated by the eddy currents may cause severe image distortions and signal loss, especially with the large prepolarizing coils designed for in vivo imaging. We derive a theory of eddy currents in thin conducting structures and enclosures to provide intuitive understanding and efficient computations. We present detailed measurements of the eddy-current patterns and their time evolution in a previous-generation shielded room. The analysis led to the design and construction of a new shielded room with symmetrically placed 1.6-mm-thick aluminum sheets that were weakly coupled electrically. The currents flowing around the entire room were heavily damped, resulting in a decay time constant of about 6 ms for both the measured and computed field transients. The measured eddy-current vector maps were in excellent agreement with predictions based on the theory, suggesting that both the experimental methods and the theory were successful and could be applied to a wide variety of thin conducting structures. PMID:24753629

  7. Flow Velocimetry for Weakly Conducting Electrolytes Based on High Resolution Lorentzforce Measurement

    NASA Astrophysics Data System (ADS)

    Ebert, R.; Vasilyan, S.; Wiederhold, A.

    We demonstrate that a flow velocity measurement can be transformed into a non-invasive force measurement by metering the dragforce acting on a system of magnets that is arranged around a flow channel. This method is called Lorentzforce velocimetry and has been developed in the last years in our institute. It is a highly feasible principle for materials with large conductivity like liquid metals. To evolve this method for weakly conducting fluids like salt water or molten glass the dragforce measurement is the challenging bottleneck. Here forces of 10-8 and less of the weightforce of the magnet system have to be resolved in the rather noisy environment of the flow channel. In this paper different force measurement techniques get tested and compared. In the first setup the drag-force is acting on the magnets that are hanging as a pendulum with 0.5 m long wires on a mounting. Here the displacement in the range of a few μm can be detected with a laser interferometer and another optical positioning sensor. For the second setup the magnet system is attached to a state of the art electromagnetic force compensation balance. The balance is used in an unusual orientation: It is turned by 90 degrees to measure the horizontally acting Lorentzforce. Different ways of getting the correct force signal out of the two measurement setups will be presented and discussed. For generalization of the measurement principle the Lorentzforce is determined for different fluid profiles. In addition to that we have developed new systematic noise reduction methods to increase the resolution of both force measurement techniques by a factor of ten or larger which we will present here.

  8. Automated multi-point mini-disk infiltrometer measurements of unsaturated hydraulic conductivity

    NASA Astrophysics Data System (ADS)

    Klipa, Vladimir; Sacha, Jan; Snehota, Michal; Dohnal, Michal; Zumr, David; Tacheci, Pavel

    2014-05-01

    Unsaturated hydraulic conductivity function K(h) is one of hydraulic characteristics needed for numerical modeling of water flow and solute transport in the vadose zone. Tension infiltrometer is advantageous tool to conduct the measurement of unsaturated hydraulic conductivity in field under near saturated conditions. Manually operated minidisk infiltrometers are often used for performing infiltration experiments, but their disadvantage is that permanent attendance is needed during experiments. Therefore automatization of the tension infiltrometer is desirable. A new automated multi-disk tension infiltrometer has been designed at the Faculty of Civil Engineering, Czech Technical University in Prague to facilitate the measurements of near-saturated hydraulic conductivity. Infiltration experiment performed by device is simultaneously carried out by six tension mini-disk infiltrometer modules forming a fixed matrix as they are held by a lightweight aluminum frame. This setup is divided into the two groups of three infiltrometers. Each triplet of modules is controlled by Mariotte`s bottle. Therefore it is possible to conduct six simultaneous infiltration experiments at two different pressure heads. Amount of infiltrated water is registered via changes of buoyant force of vertical bar attached to the weighing sensor in each infiltrometer module and recorded automatically using datalogger. Cumulative infiltration and volumetric flux are calculated and displayed in real time. Near saturated hydraulic conductivity is determined from cumulative infiltration data using nonlinear optimization and improved procedure of Zhang. Device developed was to date tested on four experimental locations. Two sites were arable land (Nucice and Kopaninsky stream) and two located in headwater catchments (Sumava and Jizera Mountains). Soils at experimental sites were classified as Cambisols (empirical van Genuchten parameters α and n ranged from 0.007 to 0.043 cm-1 and from 1.13 to 1

  9. Electrical characterization of Cu(In,Ga)Se2 thin films peeled off from Mo-coated soda-lime glass substrate by AC Hall measurement

    NASA Astrophysics Data System (ADS)

    Umehara, Takeshi; Iinuma, Shohei; Sadono, Adiyudha; Kurokawa, Yasuyoshi; Yamada, Akira

    2015-01-01

    We have developed a new evaluation method for electrical properties of Cu(In,Ga)Se2 (CIGS) grown on a Mo-coated soda-lime glass (SLG). The method consists of the peel-off process and the AC Hall measurement, which enables us to evaluate CIGS films grown on the Mo electrode. It was found, from the measurement, that the hole concentration of CIGS grown on a Mo-coated SLG was approximately two orders of magnitude higher than that on a SLG, suggesting the Na-doping effect. Furthermore, the hole mobility of 0.47 cm2/(V·s) was simultaneously measured, even though the film was deposited on the Mo electrode.

  10. Mechanical muscle fibre conduction velocity of the biceps as measured by a new seismic technique.

    PubMed

    Journée, H L; de Jonge, A B; van Calker, R; Gräler, G

    1995-01-01

    A recently-developed technique, called seismic myography (SMG) has the characteristic of recording fast micro-mechanical response times. These times can be determined with sub-millisecond accuracy. The response times can be compared to response times of EMG recordings. The "muscular electro-seismic response" (MESR) latencies, due to direct electrical stimulation of the biceps muscle, are used for explorative measurements of the mechanical conduction velocity of the muscle fibres. The measurements are performed by means of a general-purpose physiological multimeter which is equiped with the micro-seismic function. Measurements are performed on two healthy subjects, aged 22 years. The MESR-latencies are measured along a medial and a lateral trajectory on their biceps muscles. The MESR-latencies at stimulus-cathodal to seismic transducer distances of 2,0-3,5 cm, are in the range of 2.0-3.8 ms, while at distances in the range of 7.5-8.9 cm the MESR-latencies varied between 3.4 and 4.7 ms. The calculated mechanical muscle fibre conduction velocities (MMFCV) are in the range between 36 and 89 m/s. There is a reproducability error of maximum 20%. The MMFCV's of the lateral and medial trajectory do not differ within the accuracy of the present method. However, the MMFCV's are considerably higher than the electrical muscle fibre conduction velocities of MUAPS ((E)MFCV). Some aspects of the MMFCV and possible consequences to surface EMG recordings are discussed. It is concluded that this seismic method for measuring MMFCV is a new accessible and simple to handle tool for the description of muscle function, and offers an interesting new contribution in experimental muscular research.

  11. Lateral electrical conductivity of mica-supported lipid bilayer membranes measured by scanning tunneling microscopy.

    PubMed Central

    Heim, M.; Cevc, G.; Guckenberger, R.; Knapp, H. F.; Wiegräbe, W.

    1995-01-01

    Lateral electric conductivity of mica-supported lipid monolayers and of the corresponding lipid bilayers has been studied by means of scanning tunneling microscopy (STM). The surface of freshly cleaved mica itself was found to be conductive when exposed to humid air. Lipid monolayers were transferred onto such a surface by means of the Langmuir-Blodgett technique, which makes the mica surface hydrophobic and suppresses the electric current along the surface in the experimentally accessible humidity (5-80%) and applied voltage (0-10 V) range. This is true for dipalmitoylphosphatidylethanolamine (DPPE) as well as dipalmitoylphosphatidylcholine (DPPC) monolayers. Repeated deposition of DPPC layers by means of the Langmuir-Blodgett LB technique does not lead to the formation of a stable surface-supported bilayer because of the high hydrophilicity of the phosphatidylcholine headgroups that causes DPPC/DPPC bilayers to peel off the supporting surface during the sample preparation. In contrast to this, a DPPE or a DPPC monolayer on top of a DPPE monolayer gives rise to a rather stable mica-supported bilayer that can be studied by STM. Electric currents between 10 and 100 fA, depending on the ambient humidity, flow along the DPPE bilayer surface, in the humidity range between 35 and 60%. The DPPC surface, which is more hydrophilic, is up to 100 times more conductive under comparable conditions. Anomalous high lateral conductivity thus depends on, and probably proceeds via, the surface-adsorbed water layers. The prominence of ambient humidity and surface hydrophilicity on the measured lateral currents suggests this. The combination of our STM data and previously published water adsorption isotherms as a function of the relative humidity indicate that one layer or less of adsorbed water suffices for mediating the measurable lateral currents. The fact that similar observations are also made for other hydrophilic substrates supports the conclusion that lateral conductivity via

  12. Getting saturated hydraulic conductivity from surface Ground-Penetrating Radar measurements inside a ring infiltrometer

    NASA Astrophysics Data System (ADS)

    Leger, E.; Saintenoy, A.; Coquet, Y.

    2013-12-01

    fixed time steps, during an infiltration of 5 cm of water, inside a ring infiltrometer. We used the ring to demarcate the infiltration area, and to create reflexions at known depths. GPR reflexions coming from the wetting front as well as the buried edges of the cylinder were recorded. Modeling of the infiltration were made using SWMS-2D, GPR data of the infiltration were computed using GprMax suite programs. We generated 2D water content profiles associated with a saturated hydraulic conductivity value, at each experimental time step with SWMS-2D. Then we convert those profiles to 2D permittivity profiles using the Complex Refractive Index Method relation, to compute the reflexion time of the wetting front. We found the saturated hydraulic conductivity of soil by minimizing the differences between experimental and simulated data. Our retrieved saturated hydraulic conductivity from GPR data was compared to disk infiltrometer measurements.

  13. AC-Susceptibility and Ultrasonic Attenuation Measurements of Vortex Dynamics in the Vicinity of the Peak Effect in V-Ti Alloys - Multicriticality Revisited

    NASA Astrophysics Data System (ADS)

    Dimitrov, I. K.

    2005-03-01

    In-situ SANS and ac-susceptibility measurements have provided evidence for a first-order Bragg glass transition into a disordered vortex state in a Nb single crystal. This transition manifests itself in the peak effect (PE) in the critical current density, widely believed to be associated with the sudden softening of the vortex lattice. Subsequent studies mapping the full phase diagram in the same sample have suggested the existence of four distinct phase boundaries meeting at a single multicritical point (MCP). The natures of the transition lines combined with simple thermodynamic requirements suggest that the MCP is a bicritical point. This would rule out either the bulk transition line Tc2(T) or the surface superconducting transition Hc3(T) as being related to the MCP. Mutual inductance magnetic ac-susceptibility and ultrasonic attenuation measurements in V-21at.%Ti have unequivocally established the presence of a PE in this alloy. The H-T phase diagram for this sample will be presented and vortex dynamics in the vicinity of the PE will be discussed. We are indebted to Prof. Shapira of Tufts University for providing us with the sample. This work was supported by the NSF under Grant No. DMR-0406626.

  14. A passive guard for low thermal conductivity measurement of small samples by the hot plate method

    NASA Astrophysics Data System (ADS)

    Jannot, Yves; Degiovanni, Alain; Grigorova-Moutiers, Veneta; Godefroy, Justine

    2017-01-01

    Hot plate methods under steady state conditions are based on a 1D model to estimate the thermal conductivity, using measurements of the temperatures T 0 and T 1 of the two sides of the sample and of the heat flux crossing it. To be consistent with the hypothesis of the 1D heat flux, either a hot plate guarded apparatus is used, or the temperature is measured at the centre of the sample. On one hand the latter method can be used only if the ratio thickness/width of the sample is sufficiently low and on the other hand the guarded hot plate method requires large width samples (typical cross section of 0.6  ×  0.6 m2). That is why both methods cannot be used for low width samples. The method presented in this paper is based on an optimal choice of the temperatures T 0 and T 1 compared to the ambient temperature T a, enabling the estimation of the thermal conductivity with a centered hot plate method, by applying the 1D heat flux model. It will be shown that these optimal values do not depend on the size or on the thermal conductivity of samples (in the range 0.015-0.2 W m-1 K-1), but only on T a. The experimental results obtained validate the method for several reference samples for values of the ratio thickness/width up to 0.3, thus enabling the measurement of the thermal conductivity of samples having a small cross-section, down to 0.045  ×  0.045 m2.

  15. A transient hot-wire method for measuring the thermal conductivity of gases and liquids

    NASA Astrophysics Data System (ADS)

    Richard, R. G.; Shankland, I. R.

    1989-05-01

    In this paper we describe a version of a transient hot-wire apparatus which employs an integrating digital voltmeter to measure the bridge out-of-balance signal. The integrating period of the voltmeter is variable and is routinely set equal to one 60-Hz power-line cycle, 16.67 ms. Use of measurement or integration periods less than an integral multiple of the power-line period results in substantially more electronic noise and a significant degradation in experimental precision. A correction to the working equation which accounts for the integration of the out-of-balance signal is also presented. The precision of the digital voltmeter used with the apparatus is ±0.1 μV, which translates into an ultimate precision of ±0.03 mK in the measured temperature rise. In practice the precision in the temperature rise is typically ±0.3 mK, which represents a moderate improvement over the precision generally obtained with transient techniques employing automatic bridge balancing schemes. Although the current apparatus is designed principally for measurements of the thermal conductivity of liquids, it can been used for gas-phase measurements, with some decrease in accuracy due to the somewhat larger heat capacity correction which must be applied to the temperature rise measurements. The operation of the instrument was verified by measuring the thermal conductivities of toluene and nitrogen. Preliminary data are presented for the new environmentally acceptable fluorocarbons such as R-134a (CF3CH2F), R-123 (CHCl2CF3), and R-141b (CCl2FCH3).

  16. Analysis of conductive target influence in plasma jet experiments through helium metastable and electric field measurements

    NASA Astrophysics Data System (ADS)

    Darny, T.; Pouvesle, J.-M.; Puech, V.; Douat, C.; Dozias, S.; Robert, Eric

    2017-04-01

    The use of cold atmospheric pressure plasma jets for in vivo treatments implies most of the time plasma interaction with conductive targets. The effect of conductive target contact on the discharge behavior is studied here for a grounded metallic target and compared to the free jet configuration. In this work, realized with a plasma gun, we measured helium metastable HeM (23S1) concentration (by laser absorption spectroscopy) and electric field (EF) longitudinal and radial components (by electro-optic probe). Both diagnostics were temporally and spatially resolved. Mechanisms after ionization front impact on the target surface have been identified. The remnant conductive ionized channel behind the ionization front electrically transiently connects the inner high voltage electrode to the target. Due to impedance mismatching between the ionized channel and the target, a secondary ionization front is initiated and rapidly propagates from the target surface to the inner electrode through this ionized channel. This leads to a greatly enhanced HeM production inside the plasma plume and the capillary. Forward and reverse dynamics occur with further multi reflections of more or less damped ionization fronts between the inner electrode and the target as long as the ionized channel is persisting. This phenomenon is very sensitive to parameters such as target distance and ionized channel conductivity affecting electrical coupling between these two and evidenced using positive or negative voltage polarity and nitrogen admixture. In typical operating conditions for the plasma gun used in this work, it has been found that after the secondary ionization front propagation, when the ionized channel is conductive enough, a glow like discharge occurs with strong conduction current. HeM production and all species excitation, especially reactive ones, are then driven by high voltage pulse evolution. The control of forward and reverse dynamics, impacting on the production of the glow

  17. Interrelationship between Number of Mobile Protons, Diffusion Coefficient, and AC Conductivity in Superprotonic Conductors, CsHSO4 and Rb3H(SeO4)2

    NASA Astrophysics Data System (ADS)

    Kamazawa, Kazuya; Harada, Masashi; Araki, Toru; Matsuo, Yasumitsu; Tyagi, Madhusudan; Sugiyama, Jun

    2014-07-01

    Using quasielastic neutron scattering (QENS), we investigated the proton dynamics for two superprotonic conductors, CsHSO4 and Rb3H(SeO4)2. To evaluate the self-diffusion coefficients and the number of mobile protons on both superprotonic and normal phases, we focused on proton dynamics not only in the phase above Tc, but also in the phase below Tc. In Rb3H(SeO4)2, the self-diffusion of protons was observed even below the Tc phase. In contrast to popular belief, no large changes in the self-diffusion coefficients were observed across Tc. Nevertheless, the increase in the number of mobile protons across Tc was about 14.5 times, which was estimated from the integrated intensity of QENS spectra, and this change could not account for the increased magnitude of proton conductivity, which is about 500 times. As a large translational self-diffusion coefficient has not been reported in previous works by QENS experiments, there are still unknown factors that contribute to the Nernst-Einstein relation that need to be discovered.

  18. Commensurability Oscillations in the Radio-Frequency Conductivity of Unidirectional Lateral Superlattices: Measurement of Anisotropic Conductivity by Coplanar Waveguide

    NASA Astrophysics Data System (ADS)

    Endo, Akira; Kajioka, Toshiyuki; Iye, Yasuhiro

    2013-05-01

    We have measured the rf magnetoconductivity of unidirectional lateral superlattices (ULSLs) by detecting the attenuation of microwave through a coplanar waveguide placed on the surface. ULSL samples with the principal axis of the modulation perpendicular (S\\bot) and parallel (S\\|) to the microwave electric field are examined. For low microwave power, we observe expected anisotropic behavior of the commensurability oscillations (CO), with CO in samples S\\bot and S\\| dominated by the diffusion and the collisional contributions, respectively. Amplitude modulation of the Shubnikov--de Haas oscillations is observed to be more prominent in sample S\\|. The difference between the two samples is washed out with the increase of the microwave power, letting the diffusion contribution govern the CO in both samples. The dominance of the diffusion contribution even in sample S\\| in the CO measured with high microwave power is interpreted in terms of large-angle electron--phonon scattering.

  19. Thermal conductivity measurements of high and low thermal conductivity films using a scanning hot probe method in the 3ω mode and novel calibration strategies.

    PubMed

    Wilson, Adam A; Muñoz Rojo, Miguel; Abad, Begoña; Perez, Jaime Andrés; Maiz, Jon; Schomacker, Jason; Martín-Gonzalez, Marisol; Borca-Tasciuc, Diana-Andra; Borca-Tasciuc, Theodorian

    2015-10-07

    This work discusses measurement of thermal conductivity (k) of films using a scanning hot probe method in the 3ω mode and investigates the calibration of thermal contact parameters, specifically the thermal contact resistance (R(th)C) and thermal exchange radius (b) using reference samples with different thermal conductivities. R(th)C and b were found to have constant values (with b = 2.8 ± 0.3 μm and R(th)C = 44,927 ± 7820 K W(-1)) for samples with thermal conductivity values ranging from 0.36 W K(-1) m(-1) to 1.1 W K(-1) m(-1). An independent strategy for the calibration of contact parameters was developed and validated for samples in this range of thermal conductivity, using a reference sample with a previously measured Seebeck coefficient and thermal conductivity. The results were found to agree with the calibration performed using multiple samples of known thermal conductivity between 0.36 and 1.1 W K(-1) m(-1). However, for samples in the range between 16.2 W K(-1) m(-1) and 53.7 W K(-1) m(-1), calibration experiments showed the contact parameters to have considerably different values: R(th)C = 40,191 ± 1532 K W(-1) and b = 428 ± 24 nm. Finally, this work demonstrates that using these calibration procedures, measurements of both highly conductive and thermally insulating films on substrates can be performed, as the measured values obtained were within 1-20% (for low k) and 5-31% (for high k) of independent measurements and/or literature reports. Thermal conductivity results are presented for a SiGe film on a glass substrate, Te film on a glass substrate, polymer films (doped with Fe nano-particles and undoped) on a glass substrate, and Au film on a Si substrate.

  20. ac Stark shift measurements of the clock transition in cold Cs atoms: Scalar and tensor light shifts of the D2 transition

    NASA Astrophysics Data System (ADS)

    Costanzo, G. A.; Micalizio, S.; Godone, A.; Camparo, J. C.; Levi, F.

    2016-06-01

    The ac Stark shift, or light shift, is a physical phenomenon that plays a fundamental role in many applications ranging from basic atomic physics to applied quantum electronics. Here, we discuss experiments testing light-shift theory in a cold-atom cesium fountain clock for the Cs D2 transition (i.e., 6 2S1 /2→6 2P3 /2 at 852 nm). Cold-atom fountains represent a nearly ideal system for the study of light shifts: (1) The atoms can be perturbed by a field of arbitrary character (e.g., coherent field or nonclassical field); (2) there are no trapping fields to complicate data interpretation; (3) the probed atoms are essentially motionless in their center-of-mass reference frame, T ˜ 1 μK; and (4) the atoms are in an essentially collisionless environment. Moreover, in the present work the resolution of the Cs excited-state hyperfine splittings implies that the D2 ac Stark shift contains a nonzero tensor polarizability contribution, which does not appear in vapor phase experiments due to Doppler broadening. Here, we test the linearity of the ac Stark shift with field intensity, and measure the light shift as a function of field frequency, generating a "light-shift curve." We have improved on the previous best test of theory by a factor of 2, and after subtracting the theoretical scalar light shift from the experimental light-shift curves, we have isolated and tested the tensor light shift for an alkali D2 transition.

  1. Lunar magnetic field measurements, electrical conductivity calculations and thermal profile inferences

    NASA Technical Reports Server (NTRS)

    Colburn, D. S.

    1971-01-01

    Steady magnetic field measurements of magnitude 30 to 100 gamma on the lunar surface impose problems of interpretation when coupled with the nondetectability of a lunar field at 0.4 lunar radius altitude and the limb induced perturbations of the solar wind at the Explorer orbit. The lunar time-varying magnetic field clearly indicates the presence of eddy currents in the lunar interior and permits calculation of an electrical conductivity profile. The problem is complicated by the day-night asymmetry of the moon's electromagnetic environment, the possible presence of the transverse magnetic mode, and the variable wave directions of the driving function. The electrical conductivity is calculated to be low near the surface, rising to a peak of .006/ohm meter at 250 km, dropping steeply inwards to a value of about .00005/ohm meter, and then rising toward the interior. A transition at 250 km depth from a high conductivity to a low conductivity material is inferred, suggesting an olivine-like core at approximately 800 C, although other models are possible.

  2. A practical technique for measuring human biofluid conductivity using high gain-frequency characteristics.

    PubMed

    Al-Nabulsi, Jamal I; Aloquili, Osama; Ausheva, Vektoria; Yuldashev, Zafar M

    2011-11-01

    Currently, the study of ion composition and performance in human biofluids plays an important role in biomedical engineering research and technology. This field may become universal for human diagnostics; it allows early detection of different diseases in humans by measuring changes in ion behaviour in human biofluids. Practical experiments were conducted to analyse the liquid composite electrolyte conductivity in an alternating electric current field. These experiments allow the contribution of separate types of ions to the overall conductivity to be estimated. The method of estimating the concentration of active ions contained in biofluids is also introduced; it illustrates the possibility of performing qualitative and quantitative analysis over a wide range of concentrations and compositions. The authors present a procedure to determine the concentration of active liquid ions based on conductivity gain-frequency characteristic curve tracing. The experimental results validate the practical use of the proposed method. The results of this research are promising, and further investigation is required to further improve the method.

  3. Measurement of local two-phase flow parameters of nanofluids using conductivity double-sensor probe

    PubMed Central

    2011-01-01

    A two-phase flow experiment using air and water-based γ-Al2O3 nanofluid was conducted to observe the basic hydraulic phenomenon of nanofluids. The local two-phase flow parameters were measured with a conductivity double-sensor two-phase void meter. The void fraction, interfacial velocity, interfacial area concentration, and mean bubble diameter were evaluated, and all of those results using the nanofluid were compared with the corresponding results for pure water. The void fraction distribution was flattened in the nanofluid case more than it was in the pure water case. The higher interfacial area concentration resulted in a smaller mean bubble diameter in the case of the nanofluid. This was the first attempt to measure the local two-phase flow parameters of nanofluids using a conductivity double-sensor two-phase void meter. Throughout this experimental study, the differences in the internal two-phase flow structure of the nanofluid were identified. In addition, the heat transfer enhancement of the nanofluid can be resulted from the increase of the interfacial area concentration which means the available area of the heat and mass transfer. PMID:21711823

  4. Graphene Nanopore Support System for Simultaneous High-Resolution AFM Imaging and Conductance Measurements

    PubMed Central

    2015-01-01

    Accurately defining the nanoporous structure and sensing the ionic flow across nanoscale pores in thin films and membranes has a wide range of applications, including characterization of biological ion channels and receptors, DNA sequencing, molecule separation by nanoparticle films, sensing by block co-polymers films, and catalysis through metal–organic frameworks. Ionic conductance through nanopores is often regulated by their 3D structures, a relationship that can be accurately determined only by their simultaneous measurements. However, defining their structure–function relationships directly by any existing techniques is still not possible. Atomic force microscopy (AFM) can image the structures of these pores at high resolution in an aqueous environment, and electrophysiological techniques can measure ion flow through individual nanoscale pores. Combining these techniques is limited by the lack of nanoscale interfaces. We have designed a graphene-based single-nanopore support (∼5 nm thick with ∼20 nm pore diameter) and have integrated AFM imaging and ionic conductance recording using our newly designed double-chamber recording system to study an overlaid thin film. The functionality of this integrated system is demonstrated by electrical recording (<10 pS conductance) of suspended lipid bilayers spanning a nanopore and simultaneous AFM imaging of the bilayer. PMID:24581087

  5. A new method to measure caudal motor conduction time using magnetic stimulation.

    PubMed

    Han, Tai Ryoon; Paik, Nam Jong; Lee, Seong Jae; Kwon, Bum Sun

    2004-12-01

    Although central motor conduction time (CMCT) has been used for the diagnosis of lumbosacral spinal stenosis (LSSS), its diagnostic value is limited due to the short length of the involved segment compared to the long length of the total conduction distance. To overcome this, we introduce a new method to measure the caudal motor conduction time (caudal MCT) using magnetic stimulation. Magnetic stimulation was applied to the vertex and the T12 and S1 spinous processes for transcortical, thoracic, and sacral stimulation, respectively, and compound muscle action potentials were recorded simultaneously from the rectus abdominis (RA) and the right and left abductor hallucis (AH) muscles using three channels. CMCT was calculated by the latency difference in the AH response between transcortical and sacral stimulation, and between transcortical and thoracic stimulation for RA. Caudal MCT was calculated by subtracting CMCT for RA from that for AH. Caudal MCT was delayed in patients with LSSS compared to normal persons. We suggest that measuring caudal MCT may be useful for the diagnosis of LSSS, but its diagnostic sensitivity and specificity requires prospective study.

  6. Measurement of local two-phase flow parameters of nanofluids using conductivity double-sensor probe.

    PubMed

    Park, Yu Sun; Chang, Soon Heung

    2011-04-04

    A two-phase flow experiment using air and water-based γ-Al2O3 nanofluid was conducted to observe the basic hydraulic phenomenon of nanofluids. The local two-phase flow parameters were measured with a conductivity double-sensor two-phase void meter. The void fraction, interfacial velocity, interfacial area concentration, and mean bubble diameter were evaluated, and all of those results using the nanofluid were compared with the corresponding results for pure water. The void fraction distribution was flattened in the nanofluid case more than it was in the pure water case. The higher interfacial area concentration resulted in a smaller mean bubble diameter in the case of the nanofluid. This was the first attempt to measure the local two-phase flow parameters of nanofluids using a conductivity double-sensor two-phase void meter. Throughout this experimental study, the differences in the internal two-phase flow structure of the nanofluid were identified. In addition, the heat transfer enhancement of the nanofluid can be resulted from the increase of the interfacial area concentration which means the available area of the heat and mass transfer.

  7. A high sensitivity ultralow temperature RF conductance and noise measurement setup.

    PubMed

    Parmentier, F D; Mahé, A; Denis, A; Berroir, J-M; Glattli, D C; Plaçais, B; Fève, G

    2011-01-01

    We report on the realization of a high sensitivity RF noise measurement scheme to study small current fluctuations of mesoscopic systems at milli-Kelvin temperatures. The setup relies on the combination of an interferometric amplification scheme and a quarter-wave impedance transformer, allowing the measurement of noise power spectral densities with gigahertz bandwidth up to five orders of magnitude below the amplifier noise floor. We simultaneously measure the high frequency conductance of the sample by derivating a portion of the signal to a microwave homodyne detection. We describe the principle of the setup, as well as its implementation and calibration. Finally, we show that our setup allows to fully characterize a subnanosecond on-demand single electron source. More generally, its sensitivity and bandwidth make it suitable for applications manipulating single charges at GHz frequencies.

  8. Unsaturated flow in a centrifugal fields--Measurement of hydraulic conductivity and testing of Darcy's Law

    USGS Publications Warehouse

    Nimmo, J.R.; Rubin, J.; Hammermeister, D.P.

    1987-01-01

    A method has been developed to establish steady flow of water in unsaturated soil sample spinning in a centrifuge. Theoretical analysis predicts moisture conditions in the sample that depend strongly on soil type and certain operating parameter. For Oakley sand, measurements of flux, water content, and matric potential during and after centrifugation verify that steady state flow can be achieved. Experiments have confirmed the theoretical prediction of a nearly uniform moisture distribution for this medium and have demonstrated that the flow can be effectively one-dimensional. The method was used for steady state measurements of hydraulic conductivity K for relatively dry soil, giving values at low as 7. 6 multiplied by 10** minus **1**1 m/s with data obtained in a few hours. Darcy's law was tested by measuring K for different centrifugal driving forces but with the same water content.

  9. G-300: The first French Getaway Special microgravity measurements of fluid thermal conductivity

    NASA Technical Reports Server (NTRS)

    Perron, J. C.; Chretien, P.; Garnier, C.; Lecaude, N.

    1987-01-01

    Thermal conductivity measurements on liquids are difficult to perform on Earth because of thermal motions due to convection. In microgravity, the convection due to buoyancy is evanescent, and a strong reduction of Rayleigh and Nusselt numbers can be expected. Three low viscosity liquids are selected to carry out the measurements; distilled water (standard) and two silicone oils. A modified hot plate method with a simplified guard ring is used; the reduction of convective motions permitted the use in the experimental cells of larger interplate distances and/or temperature differences than in Earth measurements, improving the accuracy. Comparisons between Earth and orbit results may help to understand the convection occurrence in the cells. Thermal, vibrational, and EMI tests have proved that the design satisfies the NASA requirements.

  10. Rock matrix diffusivity determinations by in-situ electrical conductivity measurements.

    PubMed

    Ohlsson, Y; Löfgren, M; Neretnieks, I

    2001-02-01

    A fast method to determine rock matrix diffusion properties directly in the bedrock would be valuable in the investigation of a possible site for disposal of nuclear waste. An "effective diffusivity borehole log" would provide important information on the variability of this entity over the area studied. As opposed to traditional matrix diffusion laboratory experiments, electrical conductivity measurements are fast, inexpensive and also easy to carry out in-situ. In this study, electrical resistivity data from borehole logging, as well as from measurements on the actual core, is evaluated with the purpose of extracting matrix diffusivity data. The influence of migration of ions in the electrical double layer, which can be of great importance in low ionic strength pore water, is also considered in evaluating the in-situ data to accurately determine the effective pore diffusivity. The in-situ data compare fairly well to those measured in the rock core.

  11. Intervalley energy of GaN conduction band measured by femtosecond pump-probe spectroscopy

    NASA Astrophysics Data System (ADS)

    Marcinkevičius, Saulius; Uždavinys, Tomas K.; Foronda, Humberto M.; Cohen, Daniel A.; Weisbuch, Claude; Speck, James S.

    2016-12-01

    Time-resolved transmission and reflection measurements were performed for bulk GaN at room temperature to evaluate the energy of the first conduction band satellite valley. The measurements showed clear threshold-like spectra for transmission decay and reflection rise times. The thresholds were associated with the onset of the intervalley electron scattering. Transmission measurements with pump and probe pulses in the near infrared produced an intervalley energy of 0.97 ±0.02 eV. Ultraviolet pump and infrared probe reflection provided a similar value. Comparison of the threshold energies obtained in these experiments allowed estimating the hole effective mass in the upper valence band to be 1.4 m0 . Modeling of the reflection transients with rate equations has allowed estimating electron-LO (longitudinal optical) phonon scattering rates and the satellite valley effective mass.

  12. Critical Review of Industrial Techniques for Thermal-Conductivity Measurements of Thermal Insulation Materials

    NASA Astrophysics Data System (ADS)

    Hammerschmidt, Ulf; Hameury, Jacques; Strnad, Radek; Turzó-Andras, Emese; Wu, Jiyu

    2015-07-01

    This paper presents a critical review of current industrial techniques and instruments to measure the thermal conductivity of thermal insulation materials, especially those insulations that can operate at temperatures above and up to . These materials generally are of a porous nature. The measuring instruments dealt with here are selected based on their maximum working temperature that should be higher than at least . These instruments are special types of the guarded hot-plate apparatus, the guarded heat-flow meter, the transient hot-wire and hot-plane instruments as well as the laser/xenon flash devices. All technical characteristics listed are quoted from the generally accessible information of the relevant manufacturers. The paper includes rankings of the instruments according to their standard retail price, the maximum sample size, and maximum working temperature, as well as the minimum in their measurement range.

  13. Measuring the Complex Optical Conductivity of Graphene by Fabry-Pérot Reflectance Spectroscopy

    PubMed Central

    Ghamsari, Behnood G.; Tosado, Jacob; Yamamoto, Mahito; Fuhrer, Michael S.; Anlage, Steven M.

    2016-01-01

    We have experimentally studied the dispersion of optical conductivity in few-layer graphene through reflection spectroscopy at visible wavelengths. A laser scanning microscope (LSM) with a supercontinuum laser source measured the frequency dependence of the reflectance of exfoliated graphene flakes, including monolayer, bilayer and trilayer graphene, loaded on a Si/SiO2 Fabry-Pérot resonator in the 545–700 nm range. The complex refractive index of few-layer graphene, n − ik, was extracted from the reflectance contrast to the bare substrate. It was found that each few-layer graphene possesses a unique dispersionless optical index. This feature indicates that the optical conductivity does not simply scale with the number of layers, and that inter-layer electrodynamics are significant at visible energies. PMID:27682974

  14. Separation of conductivity and distance measurements for eddy current nondestructive inspection of graphite composite materials

    NASA Astrophysics Data System (ADS)

    Dufour, Isabelle; Placko, Dominique

    1993-06-01

    This article deals with the study of a process based on the principle of eddy current sensors for the nondestructive evaluation of graphite composite plates. This research has been carried out in the Laboratoire d'Electricitd Signaux et Robotique by the team working on datacollecting sensors for robotics in collaboration with Aerospatiale. Eddy current sensors are characterized by their impedance, which varies when a conducting material is approached in their sensitive area. For a given sensor, the output signal depends directly on the electrical and geometrical properties of the object. In the case discussed here, the interesting data are the distance between the sensor and the object, and its local conductivity. In order to invert the relationships between the sensor signal and the properties of the material, an external parametrical model has been developed. A scanning of the surface with a sensor designed for good spatial resolution measurements gives two accurate maps of the useful data.

  15. New contactless eddy current non-destructive methodology for electric conductivity measurement

    NASA Astrophysics Data System (ADS)

    Bouchala, T.; Abdelhadi, B.; Benoudjit, A.

    2015-01-01

    In this paper, a new method of contactless electric conductivity measurement is developed. This method is essentially based on the association of the coupled electric field forward model, which we have recently developed, with a simple and efficient research algorithm. The proposed method is very fast because 1.3 s are sufficient to calculate electric conductivity, in a CPU of 2 GHz and RAM of 3 GB, for a starting research interval of 1.72-17.2 %IACS and tolerance of 1.72 × 10- 5 %IACS. The study of the calculation time according to mesh density and starting interval width has showed that an optimal choice has to be made in order to improve the rapidity while preserving its precision. Considering its rapidity and its simplicity of implementation, this method is more adapted, in comparison to direct current techniques using Van der Pauw geometry, for automated applications.

  16. Microchip electrophoresis in low-temperature co-fired ceramics technology with contactless conductivity measurement.

    PubMed

    Fercher, Georg; Smetana, Walter; Vellekoop, Michiel J

    2009-07-01

    In this paper a novel micromachined contactless conductivity CE device produced in low temperature co-fired ceramics (LTCC) is introduced. The application of LTCC multilayer technology provides a promising method for the contactless detection of conductive compounds because of its increased dielectric constant compared with glass or plastics. The capacitive coupling of the excitation signal into the microchannel across the LTCC substrate is improved, resulting in better detection sensitivity. Two silver electrodes located externally at opposite sides at the end of the separation channel act as detector. Impedance variations in the channel are measured without galvanic contact between electrodes and fluid. Inorganic ions are separated in less than 1 min with this novel ceramic device. The limit of detection is 10 microM for potassium.

  17. Monitoring sodium chloride concentrations and density profiles in solar ponds by electrical conductivity and temperature measurement

    SciTech Connect

    Fynn, R.P.; Short, T.H.; Badger, P.C.; Sciarini, M.J.

    1980-01-01

    A simple accurate and semi-automatic system was developed for monitoring sodium chloride concentrations and density profiles in a solar pond. The profile meter, which measures pond solution conductivity and temperature, and the equations which convert this data into salt concentration and/or brine density, are covered in detail so that any potential users may construct their own equipment. The use of the profile meter, its advantages and disadvantages, are discussed. Emphasis is placed on the day-to-day profile monitoring that the conductivity-temperature method enables, and the use of the meter during modification of the pond profiles. A program is also available to calculate the pond profile using a Hewlett-Packard HP-97 programmable calculator.

  18. Repeatability and Reproducibility of Compression Strength Measurements Conducted According to ASTM E9

    NASA Technical Reports Server (NTRS)

    Luecke, William E.; Ma, Li; Graham, Stephen M.; Adler, Matthew A.

    2010-01-01

    Ten commercial laboratories participated in an interlaboratory study to establish the repeatability and reproducibility of compression strength tests conducted according to ASTM International Standard Test Method E9. The test employed a cylindrical aluminum AA2024-T351 test specimen. Participants measured elastic modulus and 0.2 % offset yield strength, YS(0.2 % offset), using an extensometer attached to the specimen. The repeatability and reproducibility of the yield strength measurement, expressed as coefficient of variations were cv(sub r)= 0.011 and cv(sub R)= 0.020 The reproducibility of the test across the laboratories was among the best that has been reported for uniaxial tests. The reported data indicated that using diametrically opposed extensometers, instead of a single extensometer doubled the precision of the test method. Laboratories that did not lubricate the ends of the specimen measured yield stresses and elastic moduli that were smaller than those measured in laboratories that lubricated the specimen ends. A finite element analysis of the test specimen deformation for frictionless and perfect friction could not explain the discrepancy, however. The modulus measured from stress-strain data were reanalyzed using a technique that finds the optimal fit range, and applies several quality checks to the data. The error in modulus measurements from stress-strain curves generally increased as the fit range decreased to less than 40 % of the stress range.

  19. Design of a dual chamber heat conduction calorimeter for ultrasonic beam measurement

    NASA Astrophysics Data System (ADS)

    Ong, Hang See

    1997-12-01

    The recent emergence of medical ultrasound dosimetry in terms of Thermal and Mechanical Indices gives rise to the need for a device that is capable of measuring ultrasonic output power quickly and accurately. In the research project described in this dissertation, a dual chamber heat conduction calorimeter (HCC) is designed, built, and tested for the purpose of measuring ultrasonic output power of clinical diagnostic ultrasound devices. The HCC is composed of two identical water filled Aluminum wells housed in two separated compartments of an insulated box. The two compartments form the measuring and reference chambers of the calorimeter. The wells are sealed with plastic membranes that constitute the entrance window for the ultrasound. The bottom of each well is stuffed with a 4cm layer of 0.5cm thick rubber pads. These pads serve as a sonic-to-heat energy exchanger. A small resistive heater is embedded in both rubber pads for calibration purposes. Heat is measured with a series of Seebeck effect thermoelectric devices (thermopiles) sandwiched between the well and the heat sink surrounding the wells. The output voltage signal from the thermopiles is amplified, digitized, then analyzed and displayed in term of Thermal Index with a PC-based system. An optimum measurement technique is derived from an electric circuit model that is representative of the HCC. The performance and sensitivity of the HCC is tested and measured, initially with the embedded resistive heaters, then with an experimental transducer, and lastly with transducers from clinical ultrasound scanners.

  20. Study on the response of the full-bore conductance sensor for water cut measurement

    NASA Astrophysics Data System (ADS)

    Xie, Ronghua; Liu, Xingbin; Hu, Jinhai; Dai, Xuefei; Shan, Fujun; Xu, Wenfeng

    2009-02-01

    This paper has proposed a new structure of full-bore conductance sensor, which is designed for measuring water cut of the oil-water two-phase flow. The structure of the full-bore conductance sensor and the measurement principle are introduced in the paper. The mental ring-shaped electrode is mounted on the outside wall of the cylindrical insulation body. When the electrode is provided with constant current, according to the electrical theory, the electrode generates a voltage, the value of which is inversely proportional to the conductivity of fluid flowing between the sensor and the casing. The electrostatic field simulations of the sensor are accomplished by using ANSYS software. The results of the potential distribution simulation show that the potential decays quickly from the electrode along r direction (radial) and z direction (axial)to both sides, and the potential only distributes in a very narrow area near the electrode. A series of static experiments on the sensor are carried out in laboratory. The experiment results agree with the simulation results. In radial direction, the closer the rod is to the sensor, the more sensitive the sensor becomes and the greater the relative response becomes. In axial direction, the electrode only responds in a certain region on both sides of the electrode and decays rapidly from the electrode to both sides. And the salinity experiment is conducted in salt solution (3000 ppm), which shows that within the allowable range of experiment error, there is no effect of salinity on the sensor response. response.