Operational Experience with the MICE Spectrometer Solenoid System

DOE Office of Scientific and Technical Information (OSTI.GOV)

Feher, Sandor; Bross, Alan; Hanlet, Pierrick

The Muon Ionization Cooling Experiment located at Rutherford Appleton Laboratory in England utilizes a supercon-ducting solenoid system for the muon cooling channel that also holds particle tracking detectors and muon absorbers inside their bores. The solenoid system installation was completed in summer of 2015 and after commissioning the system it has been running successfully. As a result, this paper summarizes the commissioning results and operational experience with the magnets focusing on the per-formance of the two Spectrometer Solenoids built by the US.

Operational Experience with the MICE Spectrometer Solenoid System

DOE PAGES

Feher, Sandor; Bross, Alan; Hanlet, Pierrick

2018-01-11

The Muon Ionization Cooling Experiment located at Rutherford Appleton Laboratory in England utilizes a supercon-ducting solenoid system for the muon cooling channel that also holds particle tracking detectors and muon absorbers inside their bores. The solenoid system installation was completed in summer of 2015 and after commissioning the system it has been running successfully. As a result, this paper summarizes the commissioning results and operational experience with the magnets focusing on the per-formance of the two Spectrometer Solenoids built by the US.

Expert overseer for mass spectrometer system

DOEpatents

Filby, Evan E.; Rankin, Richard A.

1991-01-01

An expert overseer for the operation and real-time management of a mass spectrometer and associated laboratory equipment. The overseer is a computer-based expert diagnostic system implemented on a computer separate from the dedicated computer used to control the mass spectrometer and produce the analysis results. An interface links the overseer to components of the mass spectrometer, components of the laboratory support system, and the dedicated control computer. Periodically, the overseer polls these devices and as well as itself. These data are fed into an expert portion of the system for real-time evaluation. A knowledge base used for the evaluation includes both heuristic rules and precise operation parameters. The overseer also compares current readings to a long-term database to detect any developing trends using a combination of statistical and heuristic rules to evaluate the results. The overseer has the capability to alert lab personnel whenever questionable readings or trends are observed and provide a background review of the problem and suggest root causes and potential solutions, or appropriate additional tests that could be performed. The overseer can change the sequence or frequency of the polling to respond to an observation in the current data.

Electron-Optical System of the Gyrotron Designed for Operation in the DNP-NMR Spectrometer Cryomagnet ("Gyrotrino")

NASA Astrophysics Data System (ADS)

Bratman, V. L.; Fedotov, A. E.; Kalynov, Yu. K.; Manuilov, V. N.

2017-08-01

The formation and utilization of a helical electron beam are studied theoretically for a gyrotron with a very low operating voltage in a range 1.5-1.8 kV. Such a gyrotron ("gyrotrino") was earlier proposed for operation inside a magnetic system of an NMR spectrometer with a dynamic nuclear polarization upgrade. Despite the very low voltage, the optimization of the electrode shape can provide velocity and positional electron spreads not exceeding these values for conventional high-voltage gyrotrons. A very small cathode-anode separation makes the gyrotrino very sensitive to thermal expansion of the gun elements that should be compensated by movement of the cathode. Estimations for long-pulse and CW regimes of the gyrotrino operation show that the ion background significantly decreases the reduction of the beam potential and leads to an acceptable drift of the electron cyclotron frequency at the voltage front. A satisfactory thermal load on the waste-beam collector located in a strong uniform magnetic field can be achieved due to the omnidirectional heat flow regime occurring in the case of thin beam footprint.

A Web-Based Search Service to Support Imaging Spectrometer Instrument Operations

NASA Technical Reports Server (NTRS)

Smith, Alexander; Thompson, David R.; Sayfi, Elias; Xing, Zhangfan; Castano, Rebecca

2013-01-01

Imaging spectrometers yield rich and informative data products, but interpreting them demands time and expertise. There is a continual need for new algorithms and methods for rapid first-draft analyses to assist analysts during instrument opera-tions. Intelligent data analyses can summarize scenes to draft geologic maps, searching images to direct op-erator attention to key features. This validates data quality while facilitating rapid tactical decision making to select followup targets. Ideally these algorithms would operate in seconds, never grow bored, and be free from observation bias about the kinds of mineral-ogy that will be found.

Tropospheric Emission Spectrometer and Airborne Emission Spectrometer

NASA Technical Reports Server (NTRS)

Glavich, T.; Beer, R.

1996-01-01

The Tropospheric Emission Spectrometer (TES) is an instrument being developed for the NASA Earth Observing System Chemistry Platform. TES will measure the distribution of ozone and its precursors in the lower atmosphere. The Airborne Emission Spectrometer (AES) is an aircraft precursor to TES. Applicable descriptions are given of instrument design, technology challenges, implementation and operations for both.

Fast neutron detection with a segmented spectrometer

NASA Astrophysics Data System (ADS)

Langford, T. J.; Bass, C. D.; Beise, E. J.; Breuer, H.; Erwin, D. K.; Heimbach, C. R.; Nico, J. S.

2015-01-01

A fast neutron spectrometer consisting of segmented plastic scintillator and 3He proportional counters was constructed for the measurement of neutrons in the energy range 1-200 MeV. We discuss its design, principles of operation, and the method of analysis. The detector is capable of observing very low neutron fluxes in the presence of ambient gamma background and does not require scintillator pulse-shape discrimination. The spectrometer was characterized for its energy response in fast neutron fields of 2.5 MeV and 14 MeV, and the results are compared with Monte Carlo simulations. Measurements of the fast neutron flux and energy response at 120 m above sea-level (39.130°N, 77.218°W) and at a depth of 560 m in a limestone mine are presented. Finally, the design of a spectrometer with improved sensitivity and energy resolution is discussed.

The University of Colorado OSO-8 spectrometer experiment. IV - Mission operations

NASA Technical Reports Server (NTRS)

Hansen, E. R.; Bruner, E. C., Jr.

1979-01-01

The remote operation of two high-resolution ultraviolet spectrometers on the OSO-8 satellite is discussed. Mission operations enabled scientific observers to plan observations based on current solar data, interact with the observing program using real- or near real-time data and commands, evaluate quick-look instrument data, and analyze the observations for publication. During routine operations, experiments were planned a day prior to their execution, and the data from these experiments received a day later. When a shorter turnaround was required, a real-time mode was available. Here, the real-time data and command links into the remote control center were used to evaluate experiment operation and make satellite pointing or instrument configuration changes with a 1-90 minute turnaround.

Rapid prototyping of solar-powered, battery-operated, atmospheric-pressure, sugar-cube size microplasma on hybrid, 3D chips for elemental analysis of liquid microsamples using a portable optical emission spectrometer

NASA Astrophysics Data System (ADS)

Zhang, X.; Karanassios, V.

2012-06-01

A solar-powered, battery-operated, atmospheric-pressure, self-igniting microplasma the size of a sugar-cube developed on a hybrid, 3d-chip is described. Rapid prototyping of the 3d-chip; some fundamental aspects and a brief characterization of its background spectral emission using a portable, fiber-optic spectrometer are discussed.

SYSTEMATIC EFFECTS IN POLARIZING FOURIER TRANSFORM SPECTROMETERS FOR COSMIC MICROWAVE BACKGROUND OBSERVATIONS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nagler, Peter C.; Tucker, Gregory S.; Fixsen, Dale J.

The detection of the primordial B-mode polarization signal of the cosmic microwave background (CMB) would provide evidence for inflation. Yet as has become increasingly clear, the detection of a such a faint signal requires an instrument with both wide frequency coverage to reject foregrounds and excellent control over instrumental systematic effects. Using a polarizing Fourier transform spectrometer (FTS) for CMB observations meets both of these requirements. In this work, we present an analysis of instrumental systematic effects in polarizing FTSs, using the Primordial Inflation Explorer (PIXIE) as a worked example. We analytically solve for the most important systematic effects inherentmore » to the FTS—emissive optical components, misaligned optical components, sampling and phase errors, and spin synchronous effects—and demonstrate that residual systematic error terms after corrections will all be at the sub-nK level, well below the predicted 100 nK B-mode signal.« less

Proportional-Integral-Derivative (PID) Temperature Control and Data Acquisition System for Faraday Filter based Sodium Spectrometer

NASA Astrophysics Data System (ADS)

Semerjyan, Vardan; Yuan, Tao

2011-04-01

Sodium (Na) Faraday filters based spectrometer is a relatively new instrument to study sodium nightglow as well as sodium and oxygen chemistry in the mesopause region. Successful spectrometer measurement demands highly accurate control of filter temperature. The ideal, long-term operation site for the Na spectrometer is an isolated location with minimum nocturnal sky background. Thus, the remote control of the filter temperature is a requirement for such operation, whereas current temperature controllers can only be operated manually. The proposed approach is aimed to not only enhance the temperature control, but also achieve spectrometer's remote and autonomous operation. In the meantime, the redesign should relief the burden of the cost for multi temperature controllers. The program will give to the operator flexibility in setting the operation temperatures of the Faraday filters, monitoring the temperature variations, and logging the data during the operation. Research will make diligent efforts to attach preliminary data analysis subroutine to the main control program. The real-time observation results will be posted online after the observation is completed. This approach also can be a good substitute for the temperature control system currently used to run the Lidar system at Utah State University (USU).

Background Error Correlation Modeling with Diffusion Operators

DTIC Science & Technology

2013-01-01

RESPONSIBLE PERSON 19b. TELEPHONE NUMBER (Include area code) 07-10-2013 Book Chapter Background Error Correlation Modeling with Diffusion Operators...normalization Unclassified Unclassified Unclassified UU 27 Max Yaremchuk (228) 688-5259 Reset Chapter 8 Background error correlation modeling with diffusion ...field, then a structure like this simulates enhanced diffusive transport of model errors in the regions of strong cur- rents on the background of

Lunar orbital mass spectrometer experiment

NASA Technical Reports Server (NTRS)

Lord, W. P.

1971-01-01

The design, development, manufacture, test and calibration of five lunar orbital mass spectrometers with the four associated ground support equipment test sets are discussed. A mass spectrometer was installed in the Apollo 15 and one in the Apollo 16 Scientific Instrument Module within the Service Module. The Apollo 15 mass spectrometer was operated with collection of 38 hours of mass spectra data during lunar orbit and 50 hours of data were collected during transearth coast. The Apollo 16 mass spectrometer was operated with collection of 76 hours of mass spectra data during lunar orbit. However, the Apollo 16 mass spectrometer was ejected into lunar orbit upon malfunction of spacecraft boom system just prior to transearth insection and no transearth coast data was possible.

Development of a multidimensional gamma-spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Burnett, Jonathan L.; Cantaloub, Michael G.; Mayer, Michael F.

2017-02-28

A high-sensitivity multidimensional gamma-spectrometer is being developed within the shallow underground laboratory at Pacific Northwest National Laboratory (PNNL, USA). The system consists of two Broad Energy Germanium (BEGe) detectors, inside a low-background lead and copper shield, fitted with a cosmic veto background reduction system. The detector has advanced functionality, including operation in single or combined detector mode, with reductions in the cosmic background by 49.6% and Compton suppression of 6.5%. For selected radionuclides this provides an overall MDA improvement of 52.7%. Utilizing both detectors for simultaneous measurements of thermally irradiated highly enriched uranium (HEU) increased peak identification and reduced uncertaintymore » by 27.6%. The design uses commercially off-the-shelf (COTS) components, for which the configuration is described, to provide a practical and powerful solution for low-level nuclear measurements.« less

Cryogen-free operation of the Soft X-ray Spectrometer instrument

NASA Astrophysics Data System (ADS)

Sneiderman, Gary A.; Shirron, Peter J.; Fujimoto, Ryuichi; Bialas, Thomas G.; Boyce, Kevin R.; Chiao, Meng P.; DiPirro, Michael J.; Eckart, Megan E.; Hartz, Leslie; Ishisaki, Yoshitaka; Kelley, Richard L.; Kilbourne, Caroline A.; Masters, Candace; McCammon, Dan; Mitsuda, Kazuhisa; Noda, Hirofumi; Porter, Frederick S.; Szymkowiak, Andrew E.; Takei, Yoh; Tsujimoto, Masahiro; Yoshida, Seiji

2016-07-01

The Soft X-ray Spectrometer (SXS) is the first space-based instrument to implement redundancy in the operation of a sub-Kelvin refrigerator. The SXS cryogenic system consists of a superfluid helium tank and a combination of Stirling and Joule-Thompson (JT) cryocoolers that support the operation of a 3-stage adiabatic demagnetization refrigerator (ADR). When liquid helium is present, the x-ray microcalorimeter detectors are cooled to their 50 mK operating temperature by two ADR stages, which reject their heat directly to the liquid at 1.1 K. When the helium is depleted, all three ADR stages are used to accomplish detector cooling while rejecting heat to the JT cooler operating at 4.5 K. Compared to the simpler helium mode operation, the cryogen-free mode achieves the same instrument performance by controlling the active cooling devices within the cooling system differently. These include the three ADR stages and four active heat switches, provided by NASA, and five cryocoolers, provided by JAXA. Development and verification details of this capability are presented within this paper and offer valuable insights into the challenges, successes, and lessons that can benefit other missions, particularly those employing cryogen-free cooling systems.

Low-background gamma-ray spectrometry for the international monitoring system

DOE PAGES

Greenwood, L. R.; Cantaloub, M. G.; Burnett, J. L.; ...

2016-12-28

PNNL has developed two low-background gamma-ray spectrometers in a new shallow underground laboratory, thereby significantly improving its ability to detect low levels of gamma-ray emitting fission or activation products in airborne particulate in samples from the IMS (International Monitoring System). Furthermore, the combination of cosmic veto panels, dry nitrogen gas to reduce radon and low background shielding results in a reduction of the background count rate by about a factor of 100 compared to detectors operating above ground at our laboratory.

In-Situ Characterization of Cloud Condensation Nuclei, Interstitial, and background Particles using Single Particle Mass Spectrometer, SPLAT II

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zelenyuk, Alla; Imre, D.; Earle, Michael

2010-10-01

Aerosol indirect effect remains the most uncertain aspect of climate change modeling because proper test requires knowledge of individual particles sizes and compositions with high spatial and temporal resolution. We present the first deployment of a single particle mass spectrometer (SPLAT II) that is operated in a dual data acquisition mode to measure all the required individual particle properties with sufficient temporal resolution to definitively resolve the aerosol-cloud interaction in this exemplary case. We measured particle number concentrations, asphericity, and individual particle size, composition, and density with better than 60 seconds resolution. SPLAT II measured particle number concentrations between 70more » particles cm-3and 300 particles cm-3, an average particle density of 1.4 g cm-3. Found that most particles are composed of oxygenated organics, many of which are mixed with sulfates. Biomass burn particles some with sulfates were prevalent, particularly at higher altitudes, and processed sea-salt was observed over the ocean. Analysis of cloud residuals shows that with time cloud droplets acquire sulfate by the reaction of peroxide with SO2. Based on the particle mass spectra and densities we find that the compositions of cloud condensation nuclei are similar to those of background aerosol but, contain on average ~7% more sulfate, and do not include dust and metallic particles. A comparison between the size distributions of background, activated, and interstitial particles shows that while nearly none of the activated particles is smaller than 115 nm, more than 80% of interstitial particles are smaller than 115 nm. We conclude that for this cloud the most important difference between CCN and background aerosol is particle size although having more sulfate also helps.« less

Simulation results of Pulse Shape Discrimination (PSD) for background reduction in INTEGRAL Spectrometer (SPI) germanium detectors

NASA Technical Reports Server (NTRS)

Slassi-Sennou, S. A.; Boggs, S. E.; Feffer, P. T.; Lin, R. P.

1997-01-01

Pulse Shape Discrimination (PSD) for background reduction will be used in the INTErnational Gamma Ray Astrophysics Laboratory (INTEGRAL) imaging spectrometer (SPI) to improve the sensitivity from 200 keV to 2 MeV. The observation of significant astrophysical gamma ray lines in this energy range is expected, where the dominant component of the background is the beta(sup -) decay in the Ge detectors due to the activation of Ge nuclei by cosmic rays. The sensitivity of the SPI will be improved by rejecting beta(sup -) decay events while retaining photon events. The PSD technique will distinguish between single and multiple site events. Simulation results of PSD for INTEGRAL-type Ge detectors using a numerical model for pulse shape generation are presented. The model was shown to agree with the experimental results for a narrow inner bore closed end cylindrical detector. Using PSD, a sensitivity improvement factor of the order of 2.4 at 0.8 MeV is expected.

Spectrometer gun

DOEpatents

Waechter, David A.; Wolf, Michael A.; Umbarger, C. John

1985-01-01

A hand-holdable, battery-operated, microprocessor-based spectrometer gun includes a low-power matrix display and sufficient memory to permit both real-time observation and extended analysis of detected radiation pulses. Universality of the incorporated signal processing circuitry permits operation with various detectors having differing pulse detection and sensitivity parameters.

In-orbit operation of the soft x-ray spectrometer onboard the Hitomi satellite

NASA Astrophysics Data System (ADS)

Tsujimoto, Masahiro; Mitsuda, Kazuhisa; Kelley, Richard L.; den Herder, Jan-Willem; Bialas, Thomas G.; Boyce, Kevin R.; Chiao, Meng P.; de Vries, Cor P.; DiPirro, Michael J.; Eckart, Megan E.; Ezoe, Yuichiro; Fujimoto, Ryuichi; Hoshino, Akio; Ishikawa, Kumi; Ishisaki, Yoshitaka; Kilbourne, Caroline A.; Koyama, Shu; Leutenegger, Maurice A.; Masters, Candace M.; Mitsuishi, Ikuyuki; Noda, Hirofumi; Okajima, Takashi; Okamoto, Atsushi; Porter, Frederic S.; Sato, Kosuke; Sato, Yohichi; Savinell, Joseph C.; Sawada, Makoto; Seta, Hiromi; Shirron, Peter J.; Sneiderman, Gary A.; Takei, Yoh; Tamagawa, Toru; Tashiro, Makoto S.; Watanabe, Tomomi; Yamada, Shinya; Yamasaki, Noriko Y.; Yatsu, Yoichi

2018-01-01

We summarize all of the in-orbit operations of the soft x-ray spectrometer (SXS) onboard the ASTRO-H (Hitomi) satellite. The satellite was launched on February 17, 2016, and the communication with the satellite ceased on March 26, 2016. The SXS was still in the commissioning phase, in which the set-ups were progressively changed. This paper is intended to serve as a concise reference of the events in orbit in order to properly interpret the SXS data taken during its short lifetime and as a test case for planning the in-orbit operation for future microcalorimeter missions.

Spectrometer gun

DOEpatents

Waechter, D.A.; Wolf, M.A.; Umbarger, C.J.

1981-11-03

A hand-holdable, battery-operated, microprocessor-based spectrometer gun is described that includes a low-power matrix display and sufficient memory to permit both real-time observation and extended analysis of detected radiation pulses. Universality of the incorporated signal processing circuitry permits operation with various detectors having differing pulse detection and sensitivity parameters.

Overseas Contingency Operations Funding: Background and Status

DTIC Science & Technology

2016-06-13

Coordinator Analyst in U.S. Defense Budget Policy June 13, 2016 Congressional Research Service 7-5700 www.crs.gov R44519 Overseas Contingency...Operations Funding: Background and Status Congressional Research Service Summary The Department of Defense (DOD) estimates that Congress has

Background radiation in inelastic X-ray scattering and X-ray emission spectroscopy. A study for Johann-type spectrometers

NASA Astrophysics Data System (ADS)

Paredes Mellone, O. A.; Bianco, L. M.; Ceppi, S. A.; Goncalves Honnicke, M.; Stutz, G. E.

2018-06-01

A study of the background radiation in inelastic X-ray scattering (IXS) and X-ray emission spectroscopy (XES) based on an analytical model is presented. The calculation model considers spurious radiation originated from elastic and inelastic scattering processes along the beam paths of a Johann-type spectrometer. The dependence of the background radiation intensity on the medium of the beam paths (air and helium), analysed energy and radius of the Rowland circle was studied. The present study shows that both for IXS and XES experiments the background radiation is dominated by spurious radiation owing to scattering processes along the sample-analyser beam path. For IXS experiments the spectral distribution of the main component of the background radiation shows a weak linear dependence on the energy for the most cases. In the case of XES, a strong non-linear behaviour of the background radiation intensity was predicted for energy analysis very close to the backdiffraction condition, with a rapid increase in intensity as the analyser Bragg angle approaches π / 2. The contribution of the analyser-detector beam path is significantly weaker and resembles the spectral distribution of the measured spectra. Present results show that for usual experimental conditions no appreciable structures are introduced by the background radiation into the measured spectra, both in IXS and XES experiments. The usefulness of properly calculating the background profile is demonstrated in a background subtraction procedure for a real experimental situation. The calculation model was able to simulate with high accuracy the energy dependence of the background radiation intensity measured in a particular XES experiment with air beam paths.

Miniaturized spectrometer for stand-off chemical detection

NASA Astrophysics Data System (ADS)

Henning, Patrick F.; Chadha, Suneet; Damren, Richard; Rowe, Rebecca C.; Stevenson, Chuck; Curtiss, Lawrence E.; DiGiuseppe, Thomas G.

2002-02-01

Advanced autonomous detection of both chemical warfare agents and toxic industrial chemicals has long been of major military concern and is becoming an increasingly realistic need. Foster-Miller has successfully designed and demonstrated a high spectral throughput monolithic wedge spectrometer capable of providing early, stand-off detection of chemical threats. Recent breakthrough innovations in IR source technologies, high D* multispectral array detectors, and IR waveguide materials has allowed for the development of a robust, miniature, monolithic infrared spectrometer. Foster-Miller recently demonstrated a high resolution spectrometer operating in the 8 to 12 micron region for chemical agent detection. Results will be presented demonstrating the feasibility of adapting the wedge spectrometer to operate as an upward looking ground sensor for stand-off chemical detection. Our miniaturized spectrometer forms the basis for deploying low cost, lightweight sensors which may be used for reconnaissance missions or delivered to remote locations for unattended operation. The ability of perform passive stand-off infrared chemical agent and chemical emissions detection with a low cost, compact device that can operate autonomously in remote environments has broad applications in both the military and commercial marketplace.

Measuring Transmission Efficiencies Of Mass Spectrometers

NASA Technical Reports Server (NTRS)

Srivastava, Santosh K.

1989-01-01

Coincidence counts yield absolute efficiencies. System measures mass-dependent transmission efficiencies of mass spectrometers, using coincidence-counting techniques reminiscent of those used for many years in calibration of detectors for subatomic particles. Coincidences between detected ions and electrons producing them counted during operation of mass spectrometer. Under certain assumptions regarding inelastic scattering of electrons, electron/ion-coincidence count is direct measure of transmission efficiency of spectrometer. When fully developed, system compact, portable, and used routinely to calibrate mass spectrometers.

Delivering Microwave Spectroscopy to the Masses: a Design of a Low-Cost Microwave Spectrometer Operating in the 18-26 GHZ Frequency Range

NASA Astrophysics Data System (ADS)

Steber, Amanda; Pate, Brooks

2014-06-01

Advances in chip-level microwave technology in the communications field have led to the possibilities of low cost alternatives for current Fourier transform microwave (FTMW) spectrometers. Many of the large, expensive microwave components in a traditional design can now be replaced by robust, mass market monolithic microwave integrated circuits (MMICs). "Spectrometer on a board" designs are now feasible that offer dramatic cost reduction for microwave spectroscopy. These chip-level components can be paired with miniature computers to produce compact instruments that are operable through USB. A FTMW spectrometer design using the key MMIC components that drive cost reduction will be presented. Two dual channel synthesizers (Valon Technology Model 5008), a digital pattern generator (Byte Paradigm Wav Gen Xpress), and a high-speed digitizer/arbitrary waveform generator combination unit (Tie Pie HS-5 530 XM) form the key components of the spectrometer for operation in the 18-26.5 GHz range. The design performance is illustrated using a spectrometer that is being incorporated into a museum display for astrochemistry. For this instrument a user interface, developed in Python, has been developed and will be shown.

Background field Landau mode operators for the nucleon

NASA Astrophysics Data System (ADS)

Kamleh, Waseem; Bignell, Ryan; Leinweber, Derek B.; Burkardt, Matthias

2018-03-01

The introduction of a uniform background magnetic field breaks threedimensional spatial symmetry for a charged particle and introduces Landau mode effects. Standard quark operators are inefficient at isolating the nucleon correlation function at nontrivial field strengths. We introduce novel quark operators constructed from the twodimensional Laplacian eigenmodes that describe a charged particle on a finite lattice. These eigenmode-projected quark operators provide enhanced precision for calculating nucleon energy shifts in a magnetic field. Preliminary results are obtained for the neutron and proton magnetic polarisabilities using these methods.

Operational Parameters, Considerations, and Design Decisions for Resource-Constrained Ion Trap Mass Spectrometers

NASA Technical Reports Server (NTRS)

Danell, Ryan M.; VanAmerom, Friso H. W.; Pinnick, Veronica; Cotter, Robert J.; Brickerhoff, William; Mahaffy, Paul

2011-01-01

Mass spectrometers are increasingly finding applications in new and unique areas, often in situations where key operational resources (i.e. power, weight and size) are limited. One such example is the Mars Organic Molecule Analyzer (MOMA). This instrument is a joint venture between NASA and the European Space Agency (ESA) to develop an ion trap mass spectrometer for chemical analysis on Mars. The constraints on such an instrument are significant as are the performance requirements. While the ideal operating parameters for an ion trap are generally well characterized, methods to maintain analytical performance with limited power and system weight need to be investigated and tested. Methods Experiments have been performed on two custom ion trap mass spectrometers developed as prototypes for the MOMA instrument. This hardware consists of quadrupole ion trap electrodes that are 70% the size of common commercial instrumentation. The trapping RF voltage is created with a custom tank circuit that can be tuned over a range of RF frequencies and is driven using laboratory supplies and amplifiers. The entire instrument is controlled with custom Lab VIEW software that allows a high degree of flexibility in the definition of the scan function defining the ion trap experiment. Ions are typically generated via an internal electron ionization source, however, a laser desorption source is also in development for analysis of larger intact molecules. Preliminary Data The main goals in this work have been to reduce the power required to generate the radio frequency trapping field used in an ion trap mass spectrometer. Generally minimizing the power will also reduce the volume and mass of the electronics to support the instrument. In order to achieve optimum performance, commercial instruments typically utilize RF frequencies in the 1 MHz range. Without much concern for power usage, they simply generate the voltage required to access the mass range of interest. In order to reduce the

Combined raman spectrometer/laser-induced breakdown spectrometer design concept

NASA Astrophysics Data System (ADS)

Bazalgette Courrèges-Lacoste, Gregory; Ahlers, Berit; Boslooper, Erik; Rull-Perez, Fernando; Maurice, Sylvestre

2017-11-01

Amongst the different instruments that have been preselected to be on-board the Pasteur payload on ExoMars is the Raman/ Laser Induced Breakdown Spectroscopy (LIBS) instrument. Raman spectroscopy and LIBS will be integrated into a single instrument sharing many hardware commonalities. An international team under the lead of TNO has been gathered to produce a design concept for a combined Raman Spectrometer/ LIBS Elegant Bread-Board (EBB). The instrument is based on a specifically designed extremely compact spectrometer with high resolution over a large wavelength range, suitable for both Raman spectroscopy and LIBS measurements. Low mass, size and resources are the main drivers of the instrument's design concept. The proposed design concept, realization and testing programme for the combined Raman/ LIBS EBB is presented as well as background information on Raman and LIBS.

Improved real-time imaging spectrometer

NASA Technical Reports Server (NTRS)

Lambert, James L. (Inventor); Chao, Tien-Hsin (Inventor); Yu, Jeffrey W. (Inventor); Cheng, Li-Jen (Inventor)

1993-01-01

An improved AOTF-based imaging spectrometer that offers several advantages over prior art AOTF imaging spectrometers is presented. The ability to electronically set the bandpass wavelength provides observational flexibility. Various improvements in optical architecture provide simplified magnification variability, improved image resolution and light throughput efficiency and reduced sensitivity to ambient light. Two embodiments of the invention are: (1) operation in the visible/near-infrared domain of wavelength range 0.48 to 0.76 microns; and (2) infrared configuration which operates in the wavelength range of 1.2 to 2.5 microns.

Measurement and reduction of low-level radon background in the KATRIN experiment

DOE Office of Scientific and Technical Information (OSTI.GOV)

Fränkle, F. M.

The KArlsruhe TRItium Neutrino (KATRIN) experiment is a next generation, model independent, large scale experiment to determine the mass of the electron anti-neutrino by investigating the kinematics of tritium beta decay with a sensitivity of 200 meV/c{sup 2}. The measurement setup consists of a high luminosity windowless gaseous molecular tritium source (WGTS), a differential and cryogenic pumped electron transport and tritium retention section, a tandem spectrometer section (pre-spectrometer and main spectrometer) for energy analysis, followed by a detector system for counting transmitted beta decay electrons. Measurements performed at the KATRIN pre-spectrometer test setup showed that the decay of radon (Rn)more » atoms in the volume of the KATRIN spectrometers is a major background source. Rn atoms from low-level radon emanation of materials inside the vacuum region of the KATRIN spectrometers are able to penetrate deep into the magnetic flux tube so that the alpha decay of Rn contributes to the background. Of particular importance are electrons emitted in processes accompanying the Rn alpha decay, such as shake-off, internal conversion of excited levels in the Rn daughter atoms and Auger electrons. Lowenergy electrons (< 100 eV) directly contribute to the background in the signal region. High-energy electrons can be stored magnetically inside the volume of the spectrometer and are able to create thousands of secondary electrons via subsequent ionization processes with residual gas molecules. In order to reduce the Rn induced background different active and passive counter measures were developed and tested. This proceeding will give an overview on Rn sources within the KATRIN spectrometer, describes how Rn decays inside the spectrometer produce background events at the detector and presents different counter measures to reduce the Rn induced background.« less

Measurement and reduction of low-level radon background in the KATRIN experiment

NASA Astrophysics Data System (ADS)

Fränkle, F. M.

2013-08-01

The KArlsruhe TRItium Neutrino (KATRIN) experiment is a next generation, model independent, large scale experiment to determine the mass of the electron anti-neutrino by investigating the kinematics of tritium beta decay with a sensitivity of 200 meV/c2. The measurement setup consists of a high luminosity windowless gaseous molecular tritium source (WGTS), a differential and cryogenic pumped electron transport and tritium retention section, a tandem spectrometer section (pre-spectrometer and main spectrometer) for energy analysis, followed by a detector system for counting transmitted beta decay electrons. Measurements performed at the KATRIN pre-spectrometer test setup showed that the decay of radon (Rn) atoms in the volume of the KATRIN spectrometers is a major background source. Rn atoms from low-level radon emanation of materials inside the vacuum region of the KATRIN spectrometers are able to penetrate deep into the magnetic flux tube so that the alpha decay of Rn contributes to the background. Of particular importance are electrons emitted in processes accompanying the Rn alpha decay, such as shake-off, internal conversion of excited levels in the Rn daughter atoms and Auger electrons. Lowenergy electrons (< 100 eV) directly contribute to the background in the signal region. High-energy electrons can be stored magnetically inside the volume of the spectrometer and are able to create thousands of secondary electrons via subsequent ionization processes with residual gas molecules. In order to reduce the Rn induced background different active and passive counter measures were developed and tested. This proceeding will give an overview on Rn sources within the KATRIN spectrometer, describes how Rn decays inside the spectrometer produce background events at the detector and presents different counter measures to reduce the Rn induced background.

JPL Fourier transform ultraviolet spectrometer

NASA Technical Reports Server (NTRS)

Cageao, R. P.; Friedl, R. R.; Sander, Stanley P.; Yung, Y. L.

1994-01-01

The Fourier Transform Ultraviolet Spectrometer (FTUVS) is a new high resolution interferometric spectrometer for multiple-species detection in the UV, visible and near-IR. As an OH sensor, measurements can be carried out by remote sensing (limb emission and column absorption), or in-situ sensing (long-path absorption or laser-induced fluorescence). As a high resolution detector in a high repetition rate (greater than 10 kHz) LIF system, OH fluorescence can be discriminated against non-resonant background emission and laser scatter, permitting (0, 0) excitation.

Analyses of cosmic ray induced-neutron based on spectrometers operated simultaneously at mid-latitude and Antarctica high-altitude stations during quiet solar activity

NASA Astrophysics Data System (ADS)

Hubert, G.

2016-10-01

In this paper are described a new neutron spectrometer which operate in the Concordia station (Antarctica, Dome C) since December 2015. This instrument complements a network including neutron spectrometers operating in the Pic-du-Midi and the Pico dos Dias. Thus, this work present an analysis of cosmic ray induced-neutron based on spectrometers operated simultaneously in the Pic-du-Midi and the Concordia stations during a quiet solar activity. The both high station platforms allow for investigating the long period dynamics to analyze the spectral variation and effects of local and seasonal changes, but also the short term dynamics during solar flare events. A first part is devoted to analyze the count rates, the spectrum and the neutron fluxes, implying cross-comparisons between data obtained in the both stations. In a second part, measurements analyses were reinforced by modeling based on simulations of atmospheric cascades according to primary spectra which only depend on the solar modulation potential.

Application of imaging spectrometer in gas analysis by Raman scattering

NASA Astrophysics Data System (ADS)

Zuo, Duluo; Yu, Anlan; Li, Zhe; Wang, Xingbing; Xiong, Youhui

2015-09-01

Spontaneous Raman scattering is an effective technique in gas analysis, but the detection of minor constituents is difficult because of the low signal level and the usually existed background. Imaging spectrometer can provide highly spatial resolved spectra, so it should be much easier to pick up Raman signal of minor constituents from the Raman/fluorescence background of the sample cell and transporting optics compared with the widely used fiber-coupled spectrometers. For this reason, an imaging spectrometer was constructed from transmitting volume phase holographic grating, camera lenses and CCD detector. When it was used to analyze the gas sample in metal-lined capillary, which is a sample cell believed with great enhancement of Raman signal, the background was compressed obviously. When it was used to analyze the gas in a sample cell including a parabolic reflector, only weak background signal was observed, as the wide separation between the collecting zone (the focus point of the parabolic surface) and the wall of sample cell benefitted to the analysis by imaging spectrometer. By using the last sample cell, the signal from CO2 in ambient air was able to be found by an exposure time about 20 sec, and limits of detection for H2, CO2 and CO were estimated as 60 ppm, 100 ppm and 300 ppm respectively by the results of a longer exposure time. These results show that an imaging spectrometer paired with a well-arranged sample cell will lower the detecting limit effectively.

Monte-Carlo Simulations of the Suzaku-XRS Residual Background Spectrum

NASA Technical Reports Server (NTRS)

Perinati, E.; Kilbourne, Caroline Anne; Colasanti, L.; Lotti, S.; Macculi, C.; Piro, L.; Mineo, T.; Mitsuda, K.; Bonardi, A.; Santangelo, A.

2012-01-01

Cryogenic micro-calorimeters are suitable to detect small amounts of energy deposited by electromagnetic and nuclear interactions, which makes them attractive in a variety of applications on ground and in space. The only X-ray microcalorimeter that operated in orbit to date is the X-Ray Spectrometer on-board of the Japanese Suzaku satellite. We discuss the analysis of the components of its residual background spectrum with the support of Monte-Carlo simulations.

Digital simulation of hybrid loop operation in RFI backgrounds.

NASA Technical Reports Server (NTRS)

Ziemer, R. E.; Nelson, D. R.

1972-01-01

A digital computer model for Monte-Carlo simulation of an imperfect second-order hybrid phase-locked loop (PLL) operating in radio-frequency interference (RFI) and Gaussian noise backgrounds has been developed. Characterization of hybrid loop performance in terms of cycle slipping statistics and phase error variance, through computer simulation, indicates that the hybrid loop has desirable performance characteristics in RFI backgrounds over the conventional PLL or the costas loop.

Measurement of 0.511-MeV gamma rays with a balloon-borne Ge/Li/ spectrometer

NASA Technical Reports Server (NTRS)

Ling, J. C.; Mahoney, W. A.; Willett, J. B.; Jacobson, A. S.

1977-01-01

A collimated high-resolution gamma ray spectrometer was flown on a balloon over Palestine, Texas, on June 10, 1974, to obtain measurements of the terrestrial and extraterrestrial 0.511-MeV gamma rays. The spectrometer consists of four 40-cu-cm Ge(Li) crystals operating in the energy range 0.06-10 MeV; this cluster of detectors is surrounded by a CsI(Na) anticoincidence shield. This system is used primarily to allow measurements of the two escape peaks associated with high-energy gamma ray lines. It also allows a measurement of the background component of the 0.511-MeV flux produced by beta(+) decays in materials inside the CsI(Na) shield. It is shown that the measurements of the atmospheric fluxes are consistent with earlier results after allowance is made for an additional component of the background due to beta(+) decays produced by neutron- and proton-initiated interactions with materials in and near the detector. Results of the extraterrestrial flux require an extensive detailed analysis of the time-varying background because of activation buildup and balloon spatial drifts.

Superconducting gamma and fast-neutron spectrometers with high energy resolution

DOEpatents

Friedrich, Stephan; , Niedermayr, Thomas R.; Labov, Simon E.

2008-11-04

Superconducting Gamma-ray and fast-neutron spectrometers with very high energy resolution operated at very low temperatures are provided. The sensor consists of a bulk absorber and a superconducting thermometer weakly coupled to a cold reservoir, and determines the energy of the incident particle from the rise in temperature upon absorption. A superconducting film operated at the transition between its superconducting and its normal state is used as the thermometer, and sensor operation at reservoir temperatures around 0.1 K reduces thermal fluctuations and thus enables very high energy resolution. Depending on the choice of absorber material, the spectrometer can be configured either as a Gamma-spectrometer or as a fast-neutron spectrometer.

AUTOMATIC MASS SPECTROMETER

DOEpatents

Hanson, M.L.; Tabor, C.D. Jr.

1961-12-01

A mass spectrometer for analyzing the components of a gas is designed which is capable of continuous automatic operation such as analysis of samples of process gas from a continuous production system where the gas content may be changing. (AEC)

Far-infrared heterodyne spectrometer

NASA Technical Reports Server (NTRS)

Boreiko, Rita T.; Betz, Al L.

1995-01-01

A far-infrared heterodyne spectrometer was designed and built by our group for observations of atomic and molecular lines from interstellar clouds. Linewidths as narrow as 1 km/s can be expected from such regions, and so the spectrometer is designed with sub-km/s resolution so that observed line profiles will be resolved. Since its debut on the Kuiper Airborne Observatory (KAO) in 1985, the instrument has been used in regular annual flight programs from both Moffett Field, CA and Christchurch, NZ. The basic plan of the spectrometer remains unchanged from the original design presented at the previous airborne science symposium. Numerous improvements and updates to the technical capability have of course been included over the many years of operational service.

Final Summary of On-Orbit ADR Operation on Hitomis Soft X-Ray Spectrometer Instrument

NASA Technical Reports Server (NTRS)

Shirron, Peter

2016-01-01

The Soft X-ray Spectrometer (SXS) on the Astro-H observatory contains a 6x6 array of x-ray microcalorimeters that are cooled to 50 mK by an adiabatic demagnetization refrigerator (ADR). The ADR consists of three stages in order to provide stable detector cooling using either a 1.2 K superfluid helium bath or a 4.5 K Joule-Thomson (JT) cryocooler as its heat sink. Astro-H was renamed Hitomi after it was successfully launched in February 2016. The SXS carried approximately 36 liters of helium into orbit, and by day 5 the helium had cooled sufficiently (1.4 K) to allow operation of the ADR. This paper summarizes the ADRs performance during the 38 days that the satellite was operational.

Spacelab energetic ion mass spectrometer

NASA Technical Reports Server (NTRS)

Whalen, B. A.; Mcdiarmid, I. B.; Burrows, J. R.; Sharp, R. D.; Johnson, R. G.; Shelley, E. G.

1980-01-01

Basic design criteria are given for an ion mass spectrometer for use in studying magnetospheric ion populations. The proposed instrument is composed of an electrostatic analyzer followed by a magnetic spectrometer and simultaneously measures the energy per unit and mass per unit charge of the ion species. An electromagnet is used for momentum analysis to extend the operational energy range over a much wider domain than is possible with the permanent magnets used in previous flights. The energetic ion source regions, ion energization mechanisms, field line tracing, coordinated investigations, and orbit considerations are discussed and operations of the momentum analyzer and of the electrostatic energy analyzer are examined.

Ultra-Wideband Optical Modulation Spectrometer (OMS) Development

NASA Technical Reports Server (NTRS)

Gardner, Jonathan (Technical Monitor); Tolls, Volker

2004-01-01

The optical modulation spectrometer (OMS) is a novel, highly efficient, low mass backend for heterodyne receiver systems. Current and future heterodyne receiver systems operating at frequencies up to a few THz require broadband spectrometer backends to achieve spectral resolutions of R approximately 10(exp 5) to 10(exp 6) to carry out many important astronomical investigations. Among these are observations of broad emission and absorption lines from extra-galactic objects at high redshifts, spectral line surveys, and observations of planetary atmospheres. Many of these lines are pressure or velocity broadened with either large half-widths or line wings extending over several GHz. Current backend systems can cover the needed bandwidth only by combining the output of several spectrometers, each with typically up to 1 GHz bandwidth, or by combining several frequency-shifted spectra taken with a single spectrometer. An ultra-wideband optical modulation spectrometer with 10 - 40 GHz bandwidth will enable broadband ob- servations without the limitations and disadvantages of hybrid spectrometers. Spectrometers like the OMS will be important for both ground-based observatories and future space missions like the Single Aperture Far-Infrared Telescope (SAFIR) which might carry IR/submm array heterodyne receiver systems requiring a spectrometer for each array pixel. Small size, low mass and small power consumption are extremely important for space missions. This report summarizes the specifications developed for the OMS and lists already identified commercial parts. The report starts with a review of the principle of operation, then describes the most important components and their specifications which were derived from theory, and finishes with a conclusion and outlook.

The coincidence counting technique for orders of magnitude background reduction in data obtained with the magnetic recoil spectrometer at OMEGA and the NIF.

PubMed

Casey, D T; Frenje, J A; Séguin, F H; Li, C K; Rosenberg, M J; Rinderknecht, H; Manuel, M J-E; Gatu Johnson, M; Schaeffer, J C; Frankel, R; Sinenian, N; Childs, R A; Petrasso, R D; Glebov, V Yu; Sangster, T C; Burke, M; Roberts, S

2011-07-01

A magnetic recoil spectrometer (MRS) has been built and successfully used at OMEGA for measurements of down-scattered neutrons (DS-n), from which an areal density in both warm-capsule and cryogenic-DT implosions have been inferred. Another MRS is currently being commissioned on the National Ignition Facility (NIF) for diagnosing low-yield tritium-hydrogen-deuterium implosions and high-yield DT implosions. As CR-39 detectors are used in the MRS, the principal sources of background are neutron-induced tracks and intrinsic tracks (defects in the CR-39). The coincidence counting technique was developed to reduce these types of background tracks to the required level for the DS-n measurements at OMEGA and the NIF. Using this technique, it has been demonstrated that the number of background tracks is reduced by a couple of orders of magnitude, which exceeds the requirement for the DS-n measurements at both facilities.

Airborne imaging spectrometers developed in China

NASA Astrophysics Data System (ADS)

Wang, Jianyu; Xue, Yongqi

1998-08-01

Airborne imaging spectral technology, principle means in airborne remote sensing, has been developed rapidly both in the world and in China recently. This paper describes Modular Airborne Imaging Spectrometer (MAIS), Operational Modular Airborne Imaging Spectrometer (OMAIS) and Pushbroom Hyperspectral Imagery (PHI) that have been developed or are being developed in Airborne Remote Sensing Lab of Shanghai Institute of Technical Physics, CAS.

Characterization of a turbomolecular-pumped magnetic sector mass spectrometer

NASA Technical Reports Server (NTRS)

Mehta, Narinder K.

1988-01-01

A Perkin Elmer MGA-1200, turbomolecular-pumped, magnetic sector, multiple gas analyzer mass spectrometer with modified inlet for fast response was characterized for the analysis of hydrogen, helium, oxygen and argon in nitrogen and helium background gases. This instrument was specially modified for the Vanderberg AFB SLC-6 Hydrogen Disposal Test Program, as a part of the Hydrogen Sampling System (H2S2). Linearity, precision, drift, detection limits and accuracy among other analytical parameters for each of the background gas were studied to evaluate the performance of the instrument. The result demonstrates that H2S2 mass spectrometer is a stable instrument and can be utilized for the quantitative analytical determination of hydrogen, helium, oxygen and argon in nitrogen and helium background gases.

Electro-optic Imaging Fourier Transform Spectrometer

NASA Technical Reports Server (NTRS)

Chao, Tien-Hsin

2005-01-01

JPL is developing an innovative compact, low mass, Electro-Optic Imaging Fourier Transform Spectrometer (E-O IFTS) for hyperspectral imaging applications. The spectral region of this spectrometer will be 1 - 2.5 micron (1000-4000/cm) to allow high-resolution, high-speed hyperspectral imaging applications. One application will be the remote sensing of the measurement of a large number of different atmospheric gases simultaneously in the same airmass. Due to the use of a combination of birefringent phase retarders and multiple achromatic phase switches to achieve phase delay, this spectrometer is capable of hyperspectral measurements similar to that of the conventional Fourier transform spectrometer but without any moving parts. In this paper, the principle of operations, system architecture and recent experimental progress will be presented.

Electro-optic Imaging Fourier Transform Spectrometer

NASA Technical Reports Server (NTRS)

Chao, Tien-Hsin

2005-01-01

JPL is developing an innovative compact, low mass, Electro-Optic Imaging Fourier Transform Spectrometer (E-0IFTS) for hyperspectral imaging applications. The spectral region of this spectrometer will be 1 - 2.5 pm (1000 -4000 cm-') to allow high-resolution, high-speed hyperspectral imaging applications [l-51. One application will be theremote sensing of the measurement of a large number of different atmospheric gases simultaneously in the sameairmass. Due to the use of a combination of birefiingent phase retarders and multiple achromatic phase switches toachieve phase delay, this spectrometer is capable of hyperspectral measurements similar to that of the conventionalFourier transform spectrometer but without any moving parts. In this paper, the principle of operations, systemarchitecture and recent experimental progress will be presen.

Progress in development of neutron energy spectrometer for deuterium plasma operation in KSTARa)

NASA Astrophysics Data System (ADS)

Tomita, H.; Yamashita, F.; Nakayama, Y.; Morishima, K.; Yamamoto, Y.; Sakai, Y.; Cheon, M. S.; Isobe, M.; Ogawa, K.; Hayashi, S.; Kawarabayashi, J.; Iguchi, T.

2014-11-01

Two types of DD neutron energy spectrometer (NES) are under development for deuterium plasma operation in KSTAR to understand behavior of beam ions in the plasma. One is based on the state-of-the-art nuclear emulsion technique. The other is based on a coincidence detection of a recoiled proton and a scattered neutron caused by an elastic scattering of an incident DD neutron, which is called an associated particle coincidence counting-NES. The prototype NES systems were installed at J-port in KSTAR in 2012. During the 2012 and 2013 experimental campaigns, multiple shots-integrated neutron spectra were preliminarily obtained by the nuclear emulsion-based NES system.

Mass Spectrometer for Airborne Micro-Organisms

NASA Technical Reports Server (NTRS)

Sinha, M. P.; Friedlander, S. K.

1986-01-01

Bacteria and other micro-organisms identified continously with aid of new technique for producing samples for mass spectrometer. Technique generates aerosol of organisms and feeds to spectrometer. Given species of organism produces characteristic set of peaks in mass spectrum and thereby identified. Technique useful for monitoring bacterial makeup in environmental studies and in places where cleanliness is essential, such as hospital operating rooms, breweries, and pharmaceutical plants.

Imaging IR spectrometer, phase 2

NASA Technical Reports Server (NTRS)

Gradie, Jonathan; Lewis, Ralph; Lundeen, Thomas; Wang, Shu-I

1990-01-01

The development is examined of a prototype multi-channel infrared imaging spectrometer. The design, construction and preliminary performance is described. This instrument is intended for use with JPL Table Mountain telescope as well as the 88 inch UH telescope on Mauna Kea. The instrument is capable of sampling simultaneously the spectral region of 0.9 to 2.6 um at an average spectral resolution of 1 percent using a cooled (77 K) optical bench, a concave holographic grating and a special order sorting filter to allow the acquisition of the full spectral range on a 128 x 128 HgCdTe infrared detector array. The field of view of the spectrometer is 0.5 arcsec/pixel in mapping mode and designed to be 5 arcsec/pixel in spot mode. The innovative optical design has resulted in a small, transportable spectrometer, capable of remote operation. Commercial applications of this spectrometer design include remote sensing from both space and aircraft platforms as well as groundbased astronomical observations.

A compact multichannel spectrometer for Thomson scatteringa)

NASA Astrophysics Data System (ADS)

Schoenbeck, N. L.; Schlossberg, D. J.; Dowd, A. S.; Fonck, R. J.; Winz, G. R.

2012-10-01

The availability of high-efficiency volume phase holographic (VPH) gratings and intensified CCD (ICCD) cameras have motivated a simplified, compact spectrometer for Thomson scattering detection. Measurements of Te < 100 eV are achieved by a 2971 l/mm VPH grating and measurements Te > 100 eV by a 2072 l/mm VPH grating. The spectrometer uses a fast-gated (˜2 ns) ICCD camera for detection. A Gen III image intensifier provides ˜45% quantum efficiency in the visible region. The total read noise of the image is reduced by on-chip binning of the CCD to match the 8 spatial channels and the 10 spectral bins on the camera. Three spectrometers provide a minimum of 12 spatial channels and 12 channels for background subtraction.

A compact multichannel spectrometer for Thomson scattering.

PubMed

Schoenbeck, N L; Schlossberg, D J; Dowd, A S; Fonck, R J; Winz, G R

2012-10-01

The availability of high-efficiency volume phase holographic (VPH) gratings and intensified CCD (ICCD) cameras have motivated a simplified, compact spectrometer for Thomson scattering detection. Measurements of T(e) < 100 eV are achieved by a 2971 l∕mm VPH grating and measurements T(e) > 100 eV by a 2072 l∕mm VPH grating. The spectrometer uses a fast-gated (~2 ns) ICCD camera for detection. A Gen III image intensifier provides ~45% quantum efficiency in the visible region. The total read noise of the image is reduced by on-chip binning of the CCD to match the 8 spatial channels and the 10 spectral bins on the camera. Three spectrometers provide a minimum of 12 spatial channels and 12 channels for background subtraction.

Performance of the EBIT calorimeter spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Porter, Frederick Scott; Gygax, John; Kelley, Richard L.

The EBIT calorimeter spectrometer (ECS) is a new high-resolution, broadband x-ray spectrometer that has recently been installed at the Electron Beam Ion Trap Facility (EBIT) at the Lawrence Livermore National Laboratory. The ECS is an entirely new production class spectrometer that replaces the XRS/EBIT spectrometer that has been operating at EBIT since 2000. The ECS utilizes a 32-pixel x-ray calorimeter array from the XRS instrument on the Suzaku x-ray observatory. Eighteen of the pixels are optimized for the 0.1-10 keV band and yield 4.5 eV full width at half maximum energy resolution and 95% quantum efficiency at 6 keV. Inmore » addition, the ECS includes 14 detector pixels that are optimized for the high-energy band with a bandpass from 0.5 to over 100 keV with 34 eV resolution and 32% quantum efficiency at 60 keV. The ECS detector array is operated at 50 mK using a five stage cryogenic system that is entirely automated. The instrument takes data continuously for over 65 h with a 2.5 h recycle time. The ECS is a nondispersive, broadband, highly efficient spectrometer that is one of the prime instruments at the EBIT facility. The instrument is used for studies of absolute cross sections, charge exchange recombination, and x-ray emission from nonequilibrium plasmas, among other measurements in our laboratory astrophysics program.« less

Progress in development of neutron energy spectrometer for deuterium plasma operation in KSTAR

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tomita, H., E-mail: tomita@nagoya-u.jp; Yamashita, F.; Nakayama, Y.

2014-11-15

Two types of DD neutron energy spectrometer (NES) are under development for deuterium plasma operation in KSTAR to understand behavior of beam ions in the plasma. One is based on the state-of-the-art nuclear emulsion technique. The other is based on a coincidence detection of a recoiled proton and a scattered neutron caused by an elastic scattering of an incident DD neutron, which is called an associated particle coincidence counting-NES. The prototype NES systems were installed at J-port in KSTAR in 2012. During the 2012 and 2013 experimental campaigns, multiple shots-integrated neutron spectra were preliminarily obtained by the nuclear emulsion-based NESmore » system.« less

Development and operation of a high-throughput accurate-wavelength lens-based spectrometer a)

DOE PAGES

Bell, Ronald E.

2014-07-11

A high-throughput spectrometer for the 400-820 nm wavelength range has been developed for charge exchange recombination spectroscopy or general spectroscopy. A large 2160 mm -1 grating is matched with fast f /1.8 200 mm lenses, which provide stigmatic imaging. A precision optical encoder measures the grating angle with an accuracy ≤ 0.075 arc seconds. A high quantum efficiency low-etaloning CCD detector allows operation at longer wavelengths. A patch panel allows input fibers to interface with interchangeable fiber holders that attach to a kinematic mount behind the entrance slit. The computer-controlled hardware allows automated control of wavelength, timing, f-number, automated datamore » collection, and wavelength calibration.« less

Infrared fiber coupled acousto-optic tunable filter spectrometer

NASA Technical Reports Server (NTRS)

Levin, K. H.; Kindler, E.; Ko, T.; Lee, F.; Tran, D. C.; Tapphorn, R. M.

1990-01-01

A spectrometer design is introduced which combines an acoustooptic tunable filter (AOTF) and IR-transmitting flouride-glass fibers. The AOTF crystal is fabricated from TeO2 and permits random access to any wavelength in less than 50 microseconds, and the resulting spectrometer is tested for the remote analysis of gases and hydrocarbons. The AOTF spectrometer, when operated with a high-speed frequency synthesizer and optimized algorithms, permits accurate high-speed spectroscopy in the mid-IR spectral region.

Fast Spectrometer Construction and Testing

NASA Astrophysics Data System (ADS)

Menke, John

2012-05-01

This paper describes the construction and operation of a medium resolution spectrometer used in the visual wavelength range. It is homebuilt, but has built in guiding and calibration, is fully remote operable, and operates at a resolution R=3000. It features a fast f3.5 system, which allows it to be used with a fast telescope (18 inch f3.5) with no Barlow or other optical matching devices.

Design of a miniature solid state NIR spectrometer

NASA Astrophysics Data System (ADS)

Zhang, Hanyi; Wang, Xiaolu L.; Soos, Jolanta I.; Crisp, Joy A.

1995-06-01

For aerospace applications a miniature, solid-state near infrared (NIR) spectrometer based on an acousto-optic tunable filter (AOTF) has been developed and built at Brimrose Corp. of America. In this spectrometer a light emitting diode (LED) array as light source, a set of optical fibers as the lightwave transmission route, and a miniature AOTF as a tunable filter were adopted. This approach makes the spectrometer very compact, light-weight, rugged and reliable, with low operating power and long lifetime.

Pseudoslit Spectrometer

NASA Technical Reports Server (NTRS)

Reuter, Dennis C.; McCabe, George H.

2004-01-01

The pseudoslit spectrometer is a conceptual optoelectronic instrument that would offer some of the advantages, without the disadvantages, of prior linear-variable etalon (LVE) spectrometers and prior slit spectrometers. The pseudoslit spectrometer is so named because it would not include a slit, but the combined effects of its optical components would include a spatial filtering effect approximately equivalent to that of a slit. Like a prior LVE spectrometer, the pseudoslit spectrometer would include an LVE (essentially, a wedge-like narrowband- pass filter, the pass wavelength of which varies linearly with position in one dimension) in a focal plane covering an imaging planar array of photodetectors. However, the pseudoslit spectrometer would be more efficient because unlike a prior LVE spectrometer, the pseudoslit spectrometer would not have to be scanned across an entire field of view to obtain the spectrum of an object of interest that may occupy only a small portion of the field of view. Like a prior slit spectrometer, the pseudoslit spectrometer could acquire the entire spectrum of such a small object without need for scanning. However, the pseudoslit spectrometer would be optically and mechanically simpler: it would have fewer components and, hence, would pose less of a problem of alignment of components and would be less vulnerable to misalignment.

A high performance neutron spectrometer for planetary hydrogen measurement

NASA Astrophysics Data System (ADS)

Naito, Masayuki; Hasebe, Nobuyuki; Nagaoka, Hiroshi; Ishii, Junya; Aoki, Daisuke; Shibamura, Eido; Kim, Kyeong J.; Matias-Lopes, José A.; Martínez-Frías, Jesús

2017-08-01

The elemental composition and its distribution on planetary surface provide important constraints on the origin and evolution of the planetary body. The nuclear spectrometer consisting of a neutron spectrometer and a gamma-ray spectrometer obtains elemental compositions by remote sensing. Especially, the neutron spectrometer is able to determine the hydrogen concentration, a piece of information that plays an important role in thermal history of the planets. In this work, numerical and experimental studies on the neutron spectrometer for micro-satellite application were conducted. It is found that background count rate of neutron produced from micro-satellite is very small, which enables to obtain successful results in short time observation. The neutron spectrometer combining a lithium-6 glass scintillator with a boron loaded plastic scintillator was used to be able to detect neutrons in different energy ranges. It was experimentally confirmed that the neutron signals from these scintillators were successfully discriminated by the difference of scintillation decay time between two detectors. The measurement of neutron count rates of two scintillators is found to determine hydrogen concentration on the planetary surfaces in the future missions.

Evaluation of portable Raman spectrometer with 1064 nm excitation for geological and forensic applications

NASA Astrophysics Data System (ADS)

Vítek, Petr; Ali, Esam M. A.; Edwards, Howell G. M.; Jehlička, Jan; Cox, Rick; Page, Kristian

2012-02-01

The development of miniaturized Raman instrumentation is in demand for applications relevant to forensic, pharmaceutical and art analyses, as well as geosciences, and planetary exploration. In this study we report on evaluation of a portable dispersive Raman spectrometer equipped with 1064 nm laser excitation. Selected samples from geological, geobiological and forensic areas of interest have been studied from which the advantages, disadvantages and the analytical potential of the instrument are assessed based on a comparison with bench instrumentation and other portable Raman spectrometers using 785 nm excitation. It is demonstrated that the instrument operating with 1064 nm excitation has potential for expanding the number and types of samples that can be measured by miniaturized Raman spectroscopy without interfering fluorescence background emission. It includes inorganic and organic minerals, biomolecules within living lichen and endolithic cyanobacteria as well as drugs of abuse and explosives.

[Development of X-ray excited fluorescence spectrometer].

PubMed

Ni, Chen; Gu, Mu; Di, Wang; Cao, Dun-Hua; Liu, Xiao-Lin; Huang, Shi-Ming

2009-08-01

An X-ray excited fluorescence spectrometer was developed with an X-ray tube and a spectrometer. The X-ray tube, spectrometer, autocontrol method and data processing selected were roundly evaluated. The wavelength and detecting efficiency of the apparatus were calibrated with the mercury and tungsten bromine standard lamps, and the X-ray excited emission spectra of BaF2, Cs I (Tl) crystals were measured. The results indicate that the apparatus has advantages of good wavelength resolution, high stability, easy to operation and good radioprotection. It is a wery effective tool for exploration of new scintillation materials.

Coupling of the recoil mass spectrometer CAMEL to the γ-ray spectrometer GASP

NASA Astrophysics Data System (ADS)

Spolaore, P.; Ackermann, D.; Bednarczyk, P.; De Angelis, G.; Napoli, D.; Rossi Alvarez, C.; Bazzacco, D.; Burch, R.; Müller, L.; Segato, G. F.; Scarlassara, F.

1995-02-01

A project has been realized to link the CAMEL recoil mass spectrometer to the GASP γ-spectrometer in order to perform high resolution and efficiency γ-recoil coincidence measurements. To preserve high flexibility and autonomy in the operation of the two complex apparatus a rough factor two of reduction in the overall heavy ion transmission was accepted in designing the optics of the particle transport from the GASP center to the CAMEL focal plane. The coupled configuration has been tested with the fusion reaction 58Ni (E = 212 MeV) + 64Ni, obtaining a mass resolution of {1}/{300} and efficiency between ˜ 11% and ˜ 15% for different evaporation products.

Ultra High Mass Range Mass Spectrometer System

DOEpatents

Reilly, Peter T. A. [Knoxville, TN

2005-12-06

Applicant's present invention comprises mass spectrometer systems that operate in a mass range from 1 to 10.sup.16 DA. The mass spectrometer system comprising an inlet system comprising an aerodynamic lens system, a reverse jet being a gas flux generated in an annulus moving in a reverse direction and a multipole ion guide; a digital ion trap; and a thermal vaporization/ionization detector system. Applicant's present invention further comprises a quadrupole mass spectrometer system comprising an inlet system having a quadrupole mass filter and a thermal vaporization/ionization detector system. Applicant's present invention further comprises an inlet system for use with a mass spectrometer system, a method for slowing energetic particles using an inlet system. Applicant's present invention also comprises a detector device and a method for detecting high mass charged particles.

First tritium operation of ITER-prototype VUV spectroscopy on JET

DOE Office of Scientific and Technical Information (OSTI.GOV)

Coffey, I.H.; Barnsley, R.

Results from tritium operation of the VUV survey spectrometer on the JET tokamak are presented. The instrument, located outside the biological shield and offset from a direct plasma 1-o-s for maximum radiation protection, was operational during the trace tritium campaign (TTE) at JET. No discernible increase in detector background noise levels were detected for total neutron rates of up to 1x10{sup 17}/s, demonstrating the shielding effectiveness of the configuration. Some tritium retention in the detector microchannel plate was measurable, but has not hampered subsequent operations. As a reference the unshielded detector of a close-coupled XUV instrument was operated during TTEmore » (the spectrometer itself was valved off from the JET vessel). This was exposed to neutron fluxes of {approx}10{sup 9}/cm{sup 2} s, in excess of those predicted for the corresponding instrument on ITER (10{sup 7}-10{sup 8}/cm{sup 2} s). A corresponding increase in the background level equivalent to {approx}5% of the detector dynamic range was measured. This demonstration of the shielding effectiveness of the SPRED configuration during DT operations, coupled with the tolerable noise levels measured in the SOXMOS detector, give confidence in the planned implementation of such instruments in ITER.« less

Multichannel Spectrometer of Time Distribution

NASA Astrophysics Data System (ADS)

Akindinova, E. V.; Babenko, A. G.; Vakhtel, V. M.; Evseev, N. A.; Rabotkin, V. A.; Kharitonova, D. D.

2015-06-01

For research and control of characteristics of radiation fluxes, radioactive sources in particular, for example, in paper [1], a spectrometer and methods of data measurement and processing based on the multichannel counter of time intervals of accident events appearance (impulses of particle detector) MC-2A (SPC "ASPECT") were created. The spectrometer has four independent channels of registration of time intervals of impulses appearance and correspondent amplitude and spectrometric channels for control along the energy spectra of the operation stationarity of paths of each of the channels from the detector to the amplifier. The registration of alpha-radiation is carried out by the semiconductor detectors with energy resolution of 16-30 keV. Using a spectrometer there have been taken measurements of oscillations of alpha-radiation 239-Pu flux intensity with a subsequent autocorrelative statistical analysis of the time series of readings.

A Low Cost Grism Spectrometer for Small Telescopes

NASA Astrophysics Data System (ADS)

Ludovici, Dominic

2016-06-01

We have designed and built a low cost (appx. $500) low resolution (R ~ 300) grating-prism (grism) spectrometer for the University of Iowa's robotic observatory. Grism spectrometers differ from simple transmission grating systems by partially compensating for the curved focal plane using a wedge prism. The spectrometer has five optical elements, and was designed using a ray tracing program. The collimating and focusing optics are easily modified for other telescope optics. The optics are mounted in an enclosure made with a 3-d printer. The spectrometer was installed in a modified (extended) filter wheel and has been in routine operation since January 2016. I will show sample spectra using this system and discuss spectral calibration, and optical design considerations for other telescopes. I will also discuss how low-resolution spectrometers can be used in undergraduate teaching laboratories.

Method and Apparatus for Accurately Calibrating a Spectrometer

NASA Technical Reports Server (NTRS)

Youngquist, Robert C. (Inventor); Simmons, Stephen M. (Inventor)

2013-01-01

A calibration assembly for a spectrometer is provided. The assembly includes a spectrometer having n detector elements, where each detector element is assigned a predetermined wavelength value. A first source emitting first radiation is used to calibrate the spectrometer. A device is placed in the path of the first radiation to split the first radiation into a first beam and a second beam. The assembly is configured so that one of the first and second beams travels a path-difference distance longer than the other of the first and second beams. An output signal is generated by the spectrometer when the first and second beams enter the spectrometer. The assembly includes a controller operable for processing the output signal and adapted to calculate correction factors for the respective predetermined wavelength values assigned to each detector element.

Artificial intelligence for geologic mapping with imaging spectrometers

NASA Technical Reports Server (NTRS)

Kruse, F. A.

1993-01-01

This project was a three year study at the Center for the Study of Earth from Space (CSES) within the Cooperative Institute for Research in Environmental Science (CIRES) at the University of Colorado, Boulder. The goal of this research was to develop an expert system to allow automated identification of geologic materials based on their spectral characteristics in imaging spectrometer data such as the Airborne Visible/Infrared Imaging Spectrometer (AVIRIS). This requirement was dictated by the volume of data produced by imaging spectrometers, which prohibits manual analysis. The research described is based on the development of automated techniques for analysis of imaging spectrometer data that emulate the analytical processes used by a human observer. The research tested the feasibility of such an approach, implemented an operational system, and tested the validity of the results for selected imaging spectrometer data sets.

Battery-operated, argon-hydrogen microplasma on hybrid, postage stamp-sized plastic-quartz chips for elemental analysis of liquid microsamples using a portable optical emission spectrometer.

PubMed

Weagant, Scott; Chen, Vivian; Karanassios, Vassili

2011-11-01

A battery-operated, atmospheric pressure, self-igniting, planar geometry Ar-H(2) microplasma for elemental analysis of liquid microsamples is described. The inexpensive microplasma device (MPD) fabricated for this work was a hybrid plastic-quartz structure that was formed on chips with an area (roughly) equal to that of a small-sized postage stamp (MPD footprint, 12.5-mm width by 38-mm length). Plastic substrates were chosen due to their low cost, for rapid prototyping purposes, and for a speedy microplasma device evaluation. To enhance portability, the microplasma was operated from an 18-V rechargeable battery. To facilitate portability even further, it was demonstrated that the battery can be recharged by a portable solar panel. The battery-supplied dc voltage was converted to a high-voltage ac. The ~750-μm (diameter) and 12-mm (long) Ar-H(2) (3% H(2)) microplasma was formed by applying the high-voltage ac between two needle electrodes. Spectral interference from the electrode materials or from the plastic substrate was not observed. Operating conditions were found to be key to igniting and sustaining a microplasma that was simply "warm" to the touch (thus alleviating the need for cooling or other thermal management) and that had a stable background emission. A small-sized (900 μL internal volume) electrothermal vaporization system (40-W max power) was used for microsample introduction. Microplasma background emission in the spectral region between 200 and 850 nm obtained using a portable fiber-optic spectrometer is reported and the effect of the operating conditions is described. Analyte emission from microliter volumes of dilute single-element standard solutions of Cd, Cu, K, Li, Mg, Mn, Na, Pb, and Zn is documented. The majority of spectral lines observed for the elements tested were from neutral atoms. The relative lack of emission from ion lines simplified the spectra, thus facilitating the use of a portable spectrometer. Despite the relative spectral

ExoMars Raman laser spectrometer overview

NASA Astrophysics Data System (ADS)

Rull, F.; Sansano, A.; Díaz, E.; Canora, C. P.; Moral, A. G.; Tato, C.; Colombo, M.; Belenguer, T.; Fernández, M.; Manfredi, J. A. R.; Canchal, R.; Dávila, B.; Jiménez, A.; Gallego, P.; Ibarmia, S.; Prieto, J. A. R.; Santiago, A.; Pla, J.; Ramos, G.; González, C.

2010-09-01

The Raman Laser Spectrometer (RLS) is one of the Pasteur Payload instruments, within the ESA's Aurora Exploration Programme, ExoMars mission. The RLS Instrument will perform Raman spectroscopy on crushed powered samples deposited on a small container after crushing the cores obtained by the Rover's drill system. This is the first time that a Raman spectrometer will be launched in an out planetary mission. The Instrument will be accommodated and operate inside the Rover's ALD (Analytical Laboratory Drawer), complying with COSPAR (Committee on Space Research) Planetary Protection requirements. The RLS Instrument is composed by the following units: SPU (Spectrometer Unit); iOH: (Internal Optical Head); ICEU (Instrument Control and Excitation Unit). Other instrument units are EH (Electrical Harness), OH (Optical Harness) and RLS SW On-Board.

Evaluation of portable Raman spectrometer with 1064 nm excitation for geological and forensic applications.

PubMed

Vítek, Petr; Ali, Esam M A; Edwards, Howell G M; Jehlička, Jan; Cox, Rick; Page, Kristian

2012-02-01

The development of miniaturized Raman instrumentation is in demand for applications relevant to forensic, pharmaceutical and art analyses, as well as geosciences, and planetary exploration. In this study we report on evaluation of a portable dispersive Raman spectrometer equipped with 1064 nm laser excitation. Selected samples from geological, geobiological and forensic areas of interest have been studied from which the advantages, disadvantages and the analytical potential of the instrument are assessed based on a comparison with bench instrumentation and other portable Raman spectrometers using 785 nm excitation. It is demonstrated that the instrument operating with 1064 nm excitation has potential for expanding the number and types of samples that can be measured by miniaturized Raman spectroscopy without interfering fluorescence background emission. It includes inorganic and organic minerals, biomolecules within living lichen and endolithic cyanobacteria as well as drugs of abuse and explosives. Copyright © 2011 Elsevier B.V. All rights reserved.

Ruggedized Spectrometers Are Built for Tough Jobs

NASA Technical Reports Server (NTRS)

2015-01-01

The Mars Curiosity Chemistry and Camera instrument, or ChemCam, analyzes the elemental composition of materials on the Red Planet by using a spectrometer to measure the wavelengths of light they emit. Principal investigator Roger Wiens worked with Ocean Optics, out of Dunedin, Florida, to rework the company's spectrometer to operate in cold and rowdy conditions and also during the stresses of liftoff. Those improvements have been incorporated into the firm's commercial product line.

MEMS tunable grating micro-spectrometer

NASA Astrophysics Data System (ADS)

Tormen, Maurizio; Lockhart, R.; Niedermann, P.; Overstolz, T.; Hoogerwerf, A.; Mayor, J.-M.; Pierer, J.; Bosshard, C.; Ischer, R.; Voirin, G.; Stanley, R. P.

2017-11-01

The interest in MEMS based Micro-Spectrometers is increasing due to their potential in terms of flexibility as well as cost, low mass, small volume and power savings. This interest, especially in the Near-Infrared and Mid- Infrared, ranges from planetary exploration missions to astronomy, e.g. the search for extra solar planets, as well as to many other terrestrial fields of application such as, industrial quality and surface control, chemical analysis of soil and water, detection of chemical pollutants, exhausted gas analysis, food quality control, process control in pharmaceuticals, to name a few. A compact MEMS-based Spectrometer for Near- Infrared and Mid-InfraRed operation have been conceived, designed and demonstrated. The design based on tunable MEMS blazed grating, developed in the past at CSEM [1], achieves state of the art results in terms of spectral resolution, operational wavelength range, light throughput, overall dimensions, and power consumption.

Fast Spectrometer Construction and Testing (Abstract)

NASA Astrophysics Data System (ADS)

Menke, J.

2012-12-01

This paper describes the construction and operation of a medium resolution spectrometer used in the visual wavelength range. It is homebuilt, but has built in guiding and calibration, is fully remote-operable, and operates at a resolution R = 3000. It features a fast f/3.5 system, which allows it to be used with a fast telescope (18-inch f/3.5) with no Barlow or other optical matching devices.

Final Report on Jobin Yvon Contained Inductively Coupled Plasma Emission Spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Pennebaker, F.M.

2003-03-17

A new Inductively Coupled Plasma -- Emission Spectrometer (ICP-ES) was recently purchased and installed in Lab B-147/151 at SRTC. The contained JY Model Ultima 170-C ICP-ES has been tested and compared to current ADS ICP-ES instrumentation. The testing has included both performance tests to evaluate instrumental ability, and the measurement of matrix standards commonly analyzed by ICP-ES at Savannah River. In developing operating procedures for this instrument, we have implemented the use of internal standards and off-peak background subtraction. Both of these techniques are recommended by EPA SW-846 ICP-ES methods and are common to current ICP-ES operations. Based on themore » testing and changes, the JY Model Ultima 170-C ICP-ES provides improved performance for elemental analysis of radioactive samples in the Analytical Development Section.« less

Adaptive Tunable Laser Spectrometer for Space Applications

NASA Technical Reports Server (NTRS)

Flesch, Gregory; Keymeulen, Didier

2010-01-01

An architecture and process for the rapid prototyping and subsequent development of an adaptive tunable laser absorption spectrometer (TLS) are described. Our digital hardware/firmware/software platform is both reconfigurable at design time as well as autonomously adaptive in real-time for both post-integration and post-launch situations. The design expands the range of viable target environments and enhances tunable laser spectrometer performance in extreme and even unpredictable environments. Through rapid prototyping with a commercial RTOS/FPGA platform, we have implemented a fully operational tunable laser spectrometer (using a highly sensitive second harmonic technique). With this prototype, we have demonstrated autonomous real-time adaptivity in the lab with simulated extreme environments.

The aCORN backscatter-suppressed beta spectrometer

DOE PAGES

Hassan, M. T.; Bateman, F.; Collett, B.; ...

2017-06-16

Backscatter of electrons from a beta detector, with incomplete energy deposition, can lead to undesirable effects in many types of experiments. We present and discuss the design and operation of a backscatter-suppressed beta spectrometer that was developed as part of a program to measure the electron–antineutrino correlation coefficient in neutron beta decay (aCORN). An array of backscatter veto detectors surrounds a plastic scintillator beta energy detector. The spectrometer contains an axial magnetic field gradient, so electrons are efficiently admitted but have a low probability for escaping back through the entrance after backscattering. Lastly, the design, construction, calibration, and performance ofmore » the spectrometer are discussed.« less

Far Infrared Spectrometry of the Cosmic Background Radiation

DOE R&D Accomplishments Database

Mather, J. C.

1974-01-01

I describe two experiments to measure the cosmic background radiation near 1 mm wavelength. The first was a ground-based search for spectral lines, made with a Fabry-Perot interferometer and an InSb detector. The second is a measurement of the spectrum from 3 to 18 cm{sup -1}, made with a balloon-borne Fourier transform spectrometer. It is a polarizing Michelson interferometer, cooled in liquid helium, and operated with a germanium bolometer. I give the theory of operation, construction details, and experimental results. The first experiment was successfully completed but the second suffered equipment malfunction on its first flight. I describe the theory of Fourier transformations and give a new understanding of convolutional phase correction computations. I discuss for infrared bolometer calibration procedures, and tabulate test results on nine detectors. I describe methods of improving bolometer sensitivity with immersion optics and with conductive film blackening.

The Cosmic Infrared Background Experiment (CIBER): A Sounding Rocket Payload to Study the near Infrared Extragalactic Background Light

NASA Astrophysics Data System (ADS)

Zemcov, M.; Arai, T.; Battle, J.; Bock, J.; Cooray, A.; Hristov, V.; Keating, B.; Kim, M. G.; Lee, D. H.; Levenson, L. R.; Mason, P.; Matsumoto, T.; Matsuura, S.; Nam, U. W.; Renbarger, T.; Sullivan, I.; Suzuki, K.; Tsumura, K.; Wada, T.

2013-08-01

The Cosmic Infrared Background Experiment (CIBER) is a suite of four instruments designed to study the near infrared (IR) background light from above the Earth's atmosphere. The instrument package comprises two imaging telescopes designed to characterize spatial anisotropy in the extragalactic IR background caused by cosmological structure during the epoch of reionization, a low resolution spectrometer to measure the absolute spectrum of the extragalactic IR background, and a narrow band spectrometer optimized to measure the absolute brightness of the zodiacal light foreground. In this paper we describe the design and characterization of the CIBER payload. The detailed mechanical, cryogenic, and electrical design of the system are presented, including all system components common to the four instruments. We present the methods and equipment used to characterize the instruments before and after flight, and give a detailed description of CIBER's flight profile and configurations. CIBER is designed to be recoverable and has flown four times, with modifications to the payload having been informed by analysis of the first flight data. All four instruments performed to specifications during the subsequent flights, and the scientific data from these flights are currently being analyzed.

THE COSMIC INFRARED BACKGROUND EXPERIMENT (CIBER): A SOUNDING ROCKET PAYLOAD TO STUDY THE NEAR INFRARED EXTRAGALACTIC BACKGROUND LIGHT

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zemcov, M.; Bock, J.; Hristov, V.

2013-08-15

The Cosmic Infrared Background Experiment (CIBER) is a suite of four instruments designed to study the near infrared (IR) background light from above the Earth's atmosphere. The instrument package comprises two imaging telescopes designed to characterize spatial anisotropy in the extragalactic IR background caused by cosmological structure during the epoch of reionization, a low resolution spectrometer to measure the absolute spectrum of the extragalactic IR background, and a narrow band spectrometer optimized to measure the absolute brightness of the zodiacal light foreground. In this paper we describe the design and characterization of the CIBER payload. The detailed mechanical, cryogenic, andmore » electrical design of the system are presented, including all system components common to the four instruments. We present the methods and equipment used to characterize the instruments before and after flight, and give a detailed description of CIBER's flight profile and configurations. CIBER is designed to be recoverable and has flown four times, with modifications to the payload having been informed by analysis of the first flight data. All four instruments performed to specifications during the subsequent flights, and the scientific data from these flights are currently being analyzed.« less

Mini ion trap mass spectrometer

DOEpatents

Dietrich, Daniel D.; Keville, Robert F.

1995-01-01

An ion trap which operates in the regime between research ion traps which can detect ions with a mass resolution of better than 1:10.sup.9 and commercial mass spectrometers requiring 10.sup.4 ions with resolutions of a few hundred. The power consumption is kept to a minimum by the use of permanent magnets and a novel electron gun design. By Fourier analyzing the ion cyclotron resonance signals induced in the trap electrodes, a complete mass spectra in a single combined structure can be detected. An attribute of the ion trap mass spectrometer is that overall system size is drastically reduced due to combining a unique electron source and mass analyzer/detector in a single device. This enables portable low power mass spectrometers for the detection of environmental pollutants or illicit substances, as well as sensors for on board diagnostics to monitor engine performance or for active feedback in any process involving exhausting waste products.

Mini ion trap mass spectrometer

DOEpatents

Dietrich, D.D.; Keville, R.F.

1995-09-19

An ion trap is described which operates in the regime between research ion traps which can detect ions with a mass resolution of better than 1:10{sup 9} and commercial mass spectrometers requiring 10{sup 4} ions with resolutions of a few hundred. The power consumption is kept to a minimum by the use of permanent magnets and a novel electron gun design. By Fourier analyzing the ion cyclotron resonance signals induced in the trap electrodes, a complete mass spectra in a single combined structure can be detected. An attribute of the ion trap mass spectrometer is that overall system size is drastically reduced due to combining a unique electron source and mass analyzer/detector in a single device. This enables portable low power mass spectrometers for the detection of environmental pollutants or illicit substances, as well as sensors for on board diagnostics to monitor engine performance or for active feedback in any process involving exhausting waste products. 10 figs.

Resampling algorithm for the Spatial Infrared Imaging Telescope (SPIRIT III) Fourier transform spectrometer

NASA Astrophysics Data System (ADS)

Sargent, Steven D.; Greenman, Mark E.; Hansen, Scott M.

1998-11-01

The Spatial Infrared Imaging Telescope (SPIRIT III) is the primary sensor aboard the Midcourse Space Experiment (MSX), which was launched 24 April 1996. SPIRIT III included a Fourier transform spectrometer that collected terrestrial and celestial background phenomenology data for the Ballistic Missile Defense Organization (BMDO). This spectrometer used a helium-neon reference laser to measure the optical path difference (OPD) in the spectrometer and to command the analog-to-digital conversion of the infrared detector signals, thereby ensuring the data were sampled at precise increments of OPD. Spectrometer data must be sampled at accurate increments of OPD to optimize the spectral resolution and spectral position of the transformed spectra. Unfortunately, a failure in the power supply preregulator at the MSX spacecraft/SPIRIT III interface early in the mission forced the spectrometer to be operated without the reference laser until a failure investigation was completed. During this time data were collected in a backup mode that used an electronic clock to sample the data. These data were sampled evenly in time, and because the scan velocity varied, at nonuniform increments of OPD. The scan velocity profile depended on scan direction and scan length, and varied over time, greatly degrading the spectral resolution and spectral and radiometric accuracy of the measurements. The Convert software used to process the SPIRIT III data was modified to resample the clock-sampled data at even increments of OPD, using scan velocity profiles determined from ground and on-orbit data, greatly improving the quality of the clock-sampled data. This paper presents the resampling algorithm, the characterization of the scan velocity profiles, and the results of applying the resampling algorithm to on-orbit data.

Airborne Visible/Infrared Imaging Spectrometer (AVIRIS) spectrometer design and performance

NASA Technical Reports Server (NTRS)

Macenka, Steven A.; Chrisp, Michael P.

1987-01-01

The development of the Airborne Visible/Infrared Imaging Spectrometer (AVIRIS) has been completed at JPL. This paper outlines the functional requirements of the spectrometer optics subsystem, and describes the spectrometer optical design. The optical subsystem performance is shown in terms of spectral modulation transfer functions, radial energy distributions, and system transmission at selected wavelengths for the four spectrometers. An outline of the spectrometer alignment is included.

The Reflection Grating Spectrometer on Board XMM-Newton

NASA Technical Reports Server (NTRS)

denHerder, J. W.; Brinkman, A. C.; Kahn, S. M.; Branduardi-Raymont, G.; Thomsen, K.; Aarts, H.; Audard, M.; Bixler, J. V.; denBoggende, A. J.

2000-01-01

The ESA X-ray Multi Mirror mission, XMM-Newton, carries two identical Reflection Grating Spectrometers (RGS) behind two of its three nested sets of Wolter I type mirrors. The instrument allows high-resolution (E/(Delta)E = 100 to 500) measurements in the soft X-ray range (6 to 38 A or 2.1 to 0.3 keV) with a maximum effective area of about 140 sq cm at 15 A. Its design is optimized for the detection of the K-shell transitions of carbon, nitrogen, oxygen, neon, magnesium, and silicon. as well as the L shell transitions of iron. The present paper gives a full description of the design of the RGS and its operational modes. We also review details of the calibrations and in-orbit performance including the line spread function, the wavelength calibration, the effective area, and the instrumental background.

Current instrument status of the Airborne Visible/Infrared Imaging Spectrometer (AVIRIS)

NASA Technical Reports Server (NTRS)

Eastwood, Michael L.; Sarture, Charles M.; Chrien, Thomas G.; Green, Robert O.; Porter, Wallace M.

1991-01-01

An upgraded version of AVIRIS, an airborne imaging spectrometer based on a whiskbroom-type scanner coupled via optical fibers to four dispersive spectrometers, that has been in operation since 1987 is described. Emphasis is placed on specific AVIRIS subsystems including foreoptics, fiber optics, and an in-flight reference source; spectrometers and detector dewars; a scan drive mechanism; a signal chain; digital electronics; a tape recorder; calibration systems; and ground support requirements.

Water Mass Map from Neutron Spectrometer

NASA Technical Reports Server (NTRS)

2003-01-01

December 8, 2003

This map shows the estimated lower limit of the water content of the upper meter of Martian soil. The estimates are derived from the hydrogen abundance measured by the neutron spectrometer component of the gamma ray spectrometer suite on NASA's Mars Odyssey spacecraft.

The highest water-mass fractions, exceeding 30 percent to well over 60 percent, are in the polar regions, beyond about 60 degrees latitude north or south. Farther from the poles, significant concentrations are in the area bound in longitude by minus 10 degrees to 50 degrees and in latitude by 30 degrees south to 40 degrees north, and in an area to the south and west of Olympus Mons (30 degrees to 0 degrees south latitude and minus 135 degrees to 110 degrees longitude).

NASA's Jet Propulsion Laboratory, a division of the California Institute of Technology in Pasadena, manages the 2001 Mars Odyssey mission for the NASA Office of Space Science in Washington. Investigators at Arizona State University in Tempe, the University of Arizona in Tucson and NASA's Johnson Space Center, Houston, operate the science instruments. The gamma-ray spectrometer was provided by the University of Arizona in collaboration with the Russian Aviation and Space Agency, which provided the high-energy neutron detector, and the Los Alamos National Laboratories, New Mexico, which provided the neutron spectrometer. Lockheed Martin Space Systems, Denver, is the prime contractor for the project, and developed and built the orbiter. Mission operations are conducted jointly from Lockheed Martin and from JPL.

Handheld spectrometers: the state of the art

NASA Astrophysics Data System (ADS)

Crocombe, Richard A.

2013-05-01

"Small" spectrometers fall into three broad classes: small versions of laboratory instruments, providing data, subsequently processed on a PC; dedicated analyzers, providing actionable information to an individual operator; and process analyzers, providing quantitative or semi-quantitative information to a process controller. The emphasis of this paper is on handheld dedicated analyzers. Many spectrometers have historically been large, possible fragile, expensive and complicated to use. The challenge over the last dozen years, as instruments have moved into the field, has been to make spectrometers smaller, affordable, rugged, easy-to-use, but most of all capable of delivering actionable results. Actionable results can dramatically improve the efficiency of a testing process and transform the way business is done. There are several keys to this handheld spectrometer revolution. Consumer electronics has given us powerful mobile platforms, compact batteries, clearly visible displays, new user interfaces, etc., while telecomm has revolutionized miniature optics, sources and detectors. While these technologies enable miniature spectrometers themselves, actionable information has demanded the development of rugged algorithms for material confirmation, unknown identification, mixture analysis and detection of suspicious materials in unknown matrices. These algorithms are far more sophisticated than the `correlation' or `dot-product' methods commonly used in benchtop instruments. Finally, continuing consumer electronics advances now enable many more technologies to be incorporated into handheld spectrometers, including Bluetooth, wireless, WiFi, GPS, cameras and bar code readers, and the continued size shrinkage of spectrometer `engines' leads to the prospect of dual technology or `hyphenated' handheld instruments.

U.S.-MEXICO BORDER PROGRAM ARIZONA BORDER STUDY--STANDARD OPERATING PROCEDURE FOR OPERATION, CALIBRATION, AND MAINTENANCE OF THE THERMO JARRELL ASH ICAP 61-975 PLASMA ATOMCOMP EMISSION SPECTROMETER (BCO-L-8.0)

EPA Science Inventory

The purpose of this SOP is to detail the procedures for the start-up, operation, calibration, shut-down, and maintenance of the Thermo Jarrell Ash ICAP 61-975 Plasma AtomComp Emission Spectrometer. These procedures were used in determining the trace target metals Al, As, Ba, Cd,...

A method for Removing Surface Contamination on Ultra-pure Copper Spectrometer Components

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hoppe, Eric W.; Seifert, Allen; Aalseth, Craig E.

Spectrometers for the lowest-level radiometric measurements require materials of extreme radiopurity. Measurements of rare nuclear decays, e.g. neutrinoless double-beta decay, can require construction and shielding materials with bulk radiopurity reaching one micro-Becquerel per kilogram or less. When such extreme material purity is achieved, surface contamination, particularly solid daughters in the natural radon decay chains, can become the limiting background. High-purity copper is an important material for ultra-low-background spectrometers and thus is the focus of this work. A method for removing surface contamination at very low levels without attacking the bulk material is described. An assay method using a low-background proportionalmore » counter made of the material under examination is employed, and the resulting preliminary result of achievable surface contamination levels is presented.« less

Performance Calculations for the ITER Core Imaging X-Ray Spectrometer (CIXS)

NASA Astrophysics Data System (ADS)

Hill, K. W.; Delgado-Aparicio, L.; Pablant, N.; Johnson, D.; Feder, R.; Klabacha, J.; Stratton, B.; Bitter, M.; Beiersdorfer, P.; Barnsley, R.; Bertschinger, G.; O'Mullane, M.; Lee, S. G.

2013-10-01

The US is providing a 1D imaging x-ray crystal spectrometer system as a primary diagnostic for measuring profiles of ion temperature (Ti) and toroidal flow velocity (v) in the ITER plasma core (r/a = 0-0.85). The diagnostic must provide high spectral resolution (E/ ΔE > 5,000), spatial resolution of 10 cm, and time resolution of 10-100 ms, and must operate and survive in an environment having high neutron and gamma-ray fluxes. This work presents spectral simulations and tomographic inversions for obtaining local Ti and v, comparisons of the expected count rate profiles to the requirements, the degradation of performance due to the nuclear radiation background, and measurements of the rejection of nuclear background by detector pulse-height discrimination. This work was performed under the auspices of the DOE by PPPL under contract DE-AC02-09CH11466 and by LLNL under contract DE-AC52-07NA27344.

Resonant ultrasound spectrometer

DOEpatents

Migliori, Albert; Visscher, William M.; Fisk, Zachary

1990-01-01

An ultrasound resonant spectrometer determines the resonant frequency spectrum of a rectangular parallelepiped sample of a high dissipation material over an expected resonant response frequency range. A sample holder structure grips corners of the sample between piezoelectric drive and receive transducers. Each transducer is mounted on a membrane for only weakly coupling the transducer to the holder structure and operatively contacts a material effective to remove system resonant responses at the transducer from the expected response range. i.e., either a material such as diamond to move the response frequencies above the range or a damping powder to preclude response within the range. A square-law detector amplifier receives the response signal and retransmits the signal on an isolated shield of connecting cabling to remove cabling capacitive effects. The amplifier also provides a substantially frequency independently voltage divider with the receive transducer. The spectrometer is extremely sensitive to enable low amplitude resonance to be detected for use in calculating the elastic constants of the high dissipation sample.

A Thomson-type mass and energy spectrometer for characterizing ion energy distributions in a coaxial plasma gun operating in a gas-puff mode

PubMed Central

Rieker, G. B.; Poehlmann, F. R.; Cappelli, M. A.

2013-01-01

Measurements of ion energy distribution are performed in the accelerated plasma of a coaxial electromagnetic plasma gun operating in a gas-puff mode at relatively low discharge energy (900 J) and discharge potential (4 kV). The measurements are made using a Thomson-type mass and energy spectrometer with a gated microchannel plate and phosphor screen as the ion sensor. The parabolic ion trajectories are captured from the sensor screen with an intensified charge-coupled detector camera. The spectrometer was designed and calibrated using the Geant4 toolkit, accounting for the effects on the ion trajectories of spatial non-uniformities in the spectrometer magnetic and electric fields. Results for hydrogen gas puffs indicate the existence of a class of accelerated protons with energies well above the coaxial discharge potential (up to 24 keV). The Thomson analyzer confirms the presence of impurities of copper and iron, also of relatively high energies, which are likely erosion or sputter products from plasma-electrode interactions. PMID:23983449

A Thomson-type mass and energy spectrometer for characterizing ion energy distributions in a coaxial plasma gun operating in a gas-puff mode

NASA Astrophysics Data System (ADS)

Rieker, G. B.; Poehlmann, F. R.; Cappelli, M. A.

2013-07-01

Measurements of ion energy distribution are performed in the accelerated plasma of a coaxial electromagnetic plasma gun operating in a gas-puff mode at relatively low discharge energy (900 J) and discharge potential (4 kV). The measurements are made using a Thomson-type mass and energy spectrometer with a gated microchannel plate and phosphor screen as the ion sensor. The parabolic ion trajectories are captured from the sensor screen with an intensified charge-coupled detector camera. The spectrometer was designed and calibrated using the Geant4 toolkit, accounting for the effects on the ion trajectories of spatial non-uniformities in the spectrometer magnetic and electric fields. Results for hydrogen gas puffs indicate the existence of a class of accelerated protons with energies well above the coaxial discharge potential (up to 24 keV). The Thomson analyzer confirms the presence of impurities of copper and iron, also of relatively high energies, which are likely erosion or sputter products from plasma-electrode interactions.

A Thomson-type mass and energy spectrometer for characterizing ion energy distributions in a coaxial plasma gun operating in a gas-puff mode.

PubMed

Rieker, G B; Poehlmann, F R; Cappelli, M A

2013-07-01

Measurements of ion energy distribution are performed in the accelerated plasma of a coaxial electromagnetic plasma gun operating in a gas-puff mode at relatively low discharge energy (900 J) and discharge potential (4 kV). The measurements are made using a Thomson-type mass and energy spectrometer with a gated microchannel plate and phosphor screen as the ion sensor. The parabolic ion trajectories are captured from the sensor screen with an intensified charge-coupled detector camera. The spectrometer was designed and calibrated using the Geant4 toolkit, accounting for the effects on the ion trajectories of spatial non-uniformities in the spectrometer magnetic and electric fields. Results for hydrogen gas puffs indicate the existence of a class of accelerated protons with energies well above the coaxial discharge potential (up to 24 keV). The Thomson analyzer confirms the presence of impurities of copper and iron, also of relatively high energies, which are likely erosion or sputter products from plasma-electrode interactions.

Light output function and assembly of the time-of-flight enhanced diagnostics neutron spectrometer plastic scintillators for background reduction by double kinematic selection at EAST

DOE Office of Scientific and Technical Information (OSTI.GOV)

Peng, X. Y.; Chen, Z. J.; Zhang, X.

The 2.5 MeV neutron spectrometer TOFED (Time-Of-Flight Enhanced Diagnostics) has been constructed to perform advanced neutron emission spectroscopy diagnosis of deuterium plasmas on EAST. The instrument has a double-ring structure which, in combination with pulse shape digitization, allows for a dual kinematic selection in the time-of-flight/recoil proton energy (tof/E{sub p}) space, thus improving the spectrometer capability to resolve fast ion signatures in the neutron spectrum, in principle up to a factor ≈100. The identification and separation of features from the energetic ions in the neutron spectrum depends on the detailed knowledge of the instrument response function, both in terms ofmore » the light output function of the scintillators and the effect of undesired multiple neutron scatterings in the instrument. This work presents the determination of the light output function of the TOFED plastic scintillator detectors and their geometrical assembly. Results from dedicated experiments with γ-ray sources and quasi-monoenergetic neutron beams are presented. Implications on the instrument capability to perform background suppression based on double kinematic selection are discussed.« less

Spherical grating spectrometers

NASA Astrophysics Data System (ADS)

O'Donoghue, Darragh; Clemens, J. Christopher

2014-07-01

We describe designs for spectrometers employing convex dispersers. The Offner spectrometer was the first such instrument; it has almost exclusively been employed on satellite platforms, and has had little impact on ground-based instruments. We have learned how to fabricate curved Volume Phase Holographic (VPH) gratings and, in contrast to the planar gratings of traditional spectrometers, describe how such devices can be used in optical/infrared spectrometers designed specifically for curved diffraction gratings. Volume Phase Holographic gratings are highly efficient compared to conventional surface relief gratings; they have become the disperser of choice in optical / NIR spectrometers. The advantage of spectrometers with curved VPH dispersers is the very small number of optical elements used (the simplest comprising a grating and a spherical mirror), as well as illumination of mirrors off axis, resulting in greater efficiency and reduction in size. We describe a "Half Offner" spectrometer, an even simpler version of the Offner spectrometer. We present an entirely novel design, the Spherical Transmission Grating Spectrometer (STGS), and discuss exemplary applications, including a design for a double-beam spectrometer without any requirement for a dichroic. This paradigm change in spectrometer design offers an alternative to all-refractive astronomical spectrometer designs, using expensive, fragile lens elements fabricated from CaF2 or even more exotic materials. The unobscured mirror layout avoids a major drawback of the previous generation of catadioptric spectrometer designs. We describe laboratory measurements of the efficiency and image quality of a curved VPH grating in a STGS design, demonstrating, simultaneously, efficiency comparable to planar VPH gratings along with good image quality. The stage is now set for construction of a prototype instrument with impressive performance.

NASA Tropospheric Emission Spectrometer TES Instrument Onboard Aura

NASA Image and Video Library

2004-04-01

Technicians install NASA's Tropospheric Emission Spectrometer (TES) instrument on NASA's Aura spacecraft prior to launch. Launched in July 2004 and designed to fly for two years, the TES mission is currently in an extended operations phase. Mission managers at NASA's Jet Propulsion Laboratory, Pasadena, California, are evaluating an alternate way to collect and process science data from the Tropospheric Emission Spectrometer (TES) instrument on NASA's Aura spacecraft following the age-related failure of a critical instrument component. TES is an infrared sensor designed to study Earth's troposphere, the lowermost layer of Earth's atmosphere, which is where we live. The remainder of the TES instrument, and the Aura spacecraft itself, are operating as expected, and TES continues to collect science data. TES is one of four instruments on Aura, three of which are still operating. http://photojournal.jpl.nasa.gov/catalog/PIA15608

A new spectrometer concept for Mars exploration

NASA Astrophysics Data System (ADS)

Rull, F.; Sansano, A.; Díaz, E.; Colombo, M.; Belenguer, T.; Fernández, M.; Guembe, V.; Canchal, R.; Dávila, B.; Sánchez, A.; Laguna, H.; Ramos, G.; González, C.; Fraga, D.; Gallego, P.; Hutchinson, I.; Ingley, R.; Sánchez, J.; Canora, C. P.; Moral, A. G.; Ibarmia, S.; Prieto, J. A. R.; Manfredi, J. A. R.; Cabo, P.; Díaz, C.; Jiménez, A.; Pla, J.; Margoillés, R.

2011-10-01

The Raman Laser Spectrometer instrument is included in ExoMars program Pasteur payload and it is focused on the Mars samples analytical analysis of the geochemistry content and elemental composition of the observed crushed samples obtained by the Rover. One of the most critical Units of the RLS is the Spectrometer unit (SPU) that performs Raman spectroscopy technique and operates in a very demanding environment (operative temperature: from -40 ºC to 6 ºC) with very restrictive design constraints. It is a very small optical instrument capable to cope with 0.09 nm/pixel of resolution. The selected solution is based on a single transmisive holographic grating. At this stage of the project SPU Team is preparing the Conceptual Design Review that will take place at the end of October 2011.

MWIR thermal imaging spectrometer based on the acousto-optic tunable filter.

PubMed

Zhao, Huijie; Ji, Zheng; Jia, Guorui; Zhang, Ying; Li, Yansong; Wang, Daming

2017-09-01

Mid-wavelength IR (MWIR) thermal imaging spectrometers are widely used in remote sensing, industrial detection, and military applications. The acousto-optic tunable filter (AOTF)-based spectrometer has the advantages of fast tuning, light weight, and no moving parts, which make it ideally suited for MWIR applications. However, when designing an AOTF imaging spectrometer, the traditional method uses a refractive grating or parallel glass model in optical design software to simulate the AOTF, lowering the imaging performance of the optical system. In this paper, an accurate simulating model for an actual MWIR AOTF using the user-defined surface function in ZEMAX is presented, and an AOTF-based MWIR thermal imaging spectrometer is designed and tested successfully. It is based on a MWIR tellurium dioxide (TeO 2 ) AOTF with an operational spectral range from 3.0 to 5.0 μm and a spectral resolution of 30.8 nm at 3.392 μm. The optical system employs a three-mirror off-axis afocal telescope with a 2.4°×2.0° field of view. The operation of the MWIR thermal imaging spectrometer and its image acquisition are computer controlled. Furthermore, the imaging spectrometer is tested in the laboratory, and several experiments are also presented. The experimental results indicate that the proposed AOTF model is efficient, and also show that the imaging spectrometer has the ability to distinguish the real hot target from the interfering target effectively.

Gas Measurement Using Static Fourier Transform Infrared Spectrometers.

PubMed

Köhler, Michael H; Schardt, Michael; Rauscher, Markus S; Koch, Alexander W

2017-11-13

Online monitoring of gases in industrial processes is an ambitious task due to adverse conditions such as mechanical vibrations and temperature fluctuations. Whereas conventional Fourier transform infrared (FTIR) spectrometers use rather complex optical and mechanical designs to ensure stable operation, static FTIR spectrometers do not require moving parts and thus offer inherent stability at comparatively low costs. Therefore, we present a novel, compact gas measurement system using a static single-mirror Fourier transform spectrometer (sSMFTS). The system works in the mid-infrared range from 650 cm - 1 to 1250 cm - 1 and can be operated with a customized White cell, yielding optical path lengths of up to 120 cm for highly sensitive quantification of gas concentrations. To validate the system, we measure different concentrations of 1,1,1,2-Tetrafluoroethane (R134a) and perform a PLS regression analysis of the acquired infrared spectra. Thereby, the measured absorption spectra show good agreement with reference data. Since the system additionally permits measurement rates of up to 200 Hz and high signal-to-noise ratios, an application in process analysis appears promising.

Gas Measurement Using Static Fourier Transform Infrared Spectrometers

PubMed Central

Schardt, Michael; Rauscher, Markus S.; Koch, Alexander W.

2017-01-01

Online monitoring of gases in industrial processes is an ambitious task due to adverse conditions such as mechanical vibrations and temperature fluctuations. Whereas conventional Fourier transform infrared (FTIR) spectrometers use rather complex optical and mechanical designs to ensure stable operation, static FTIR spectrometers do not require moving parts and thus offer inherent stability at comparatively low costs. Therefore, we present a novel, compact gas measurement system using a static single-mirror Fourier transform spectrometer (sSMFTS). The system works in the mid-infrared range from 650 cm−1 to 1250 cm−1 and can be operated with a customized White cell, yielding optical path lengths of up to 120 cm for highly sensitive quantification of gas concentrations. To validate the system, we measure different concentrations of 1,1,1,2-Tetrafluoroethane (R134a) and perform a PLS regression analysis of the acquired infrared spectra. Thereby, the measured absorption spectra show good agreement with reference data. Since the system additionally permits measurement rates of up to 200 Hz and high signal-to-noise ratios, an application in process analysis appears promising. PMID:29137193

MGGPOD: a Monte Carlo Suite for Modeling Instrumental Line and Continuum Backgrounds in Gamma-Ray Astronomy

NASA Technical Reports Server (NTRS)

Weidenspointner, G.; Harris, M. J.; Sturner, S.; Teegarden, B. J.; Ferguson, C.

2004-01-01

Intense and complex instrumental backgrounds, against which the much smaller signals from celestial sources have to be discerned, are a notorious problem for low and intermediate energy gamma-ray astronomy (approximately 50 keV - 10 MeV). Therefore a detailed qualitative and quantitative understanding of instrumental line and continuum backgrounds is crucial for most stages of gamma-ray astronomy missions, ranging from the design and development of new instrumentation through performance prediction to data reduction. We have developed MGGPOD, a user-friendly suite of Monte Carlo codes built around the widely used GEANT (Version 3.21) package, to simulate ab initio the physical processes relevant for the production of instrumental backgrounds. These include the build-up and delayed decay of radioactive isotopes as well as the prompt de-excitation of excited nuclei, both of which give rise to a plethora of instrumental gamma-ray background lines in addition t o continuum backgrounds. The MGGPOD package and documentation are publicly available for download. We demonstrate the capabilities of the MGGPOD suite by modeling high resolution gamma-ray spectra recorded by the Transient Gamma-Ray Spectrometer (TGRS) on board Wind during 1995. The TGRS is a Ge spectrometer operating in the 40 keV to 8 MeV range. Due to its fine energy resolution, these spectra reveal the complex instrumental background in formidable detail, particularly the many prompt and delayed gamma-ray lines. We evaluate the successes and failures of the MGGPOD package in reproducing TGRS data, and provide identifications for the numerous instrumental lines.

The VESUVIO Spectrometer Now and When?

NASA Astrophysics Data System (ADS)

Seel, A. G.; Krzystyniak, M.; Fernandez-Alonso, F.

2014-12-01

The current layout and mechanics of the VESUVIO spectrometer are presented in light of spectroscopic measurements using electron-volt neutrons. A brief background to the theoretical framework of deep inelastic neutron scattering is presented, with focus on data collection and instrumental design. The current capabilities and research themes for VESUVIO are discussed, and possible future instrumental developments highlighted which will enhance the instrument's ability to meet scientific inquiry and expectation.

Pencil-like imaging spectrometer for bio-samples sensing.

PubMed

Cai, Fuhong; Wang, Dan; Zhu, Min; He, Sailing

2017-12-01

Spectrally-resolved imaging techniques are becoming central to the investigation of bio-samples. In this paper, we demonstrate the use of a WIFI-camera as a detection module to assemble a pencil-like imaging spectrometer, which weighs only 140 g and has a size of 3.1 cm in diameter and 15.5 cm in length. The spectrometer is standalone, and works wirelessly. A smartphone or network computer can serve as the data receiver and processor. The wavelength resolution of the spectrometer is about 17 nm, providing repeatable measurements of spatial two-dimensional images at various wavelengths for various bio-samples, including bananas, meat, and human hands. The detected spectral range is 400 nm - 675 nm and a white LED array lamp is selected as the light source. Based on the detected spectra, we can monitor the impacts of chlorophyll, myoglobin, and hemoglobin on bananas, pork, and human hands, respectively. For human hand scanning, a 3D spectral image data cube, which exhibits excellent signal to background noise ratio, can be obtained within 16 sec. We envisage that the adaptation of imaging spectrometer devices to the widely-accepted smartphone technology will help to carry out on-site studies in various applications. Besides, our pencil-like imaging spectrometer is cost-effective (<$300) and easy to assemble. This portable imaging spectrometer can facilitate the collection of large amounts of spectral image data. With the help of machine learning, we can realize object recognition based on spectral classification in the future.

Correlation spectrometer

DOEpatents

Sinclair, Michael B [Albuquerque, NM; Pfeifer, Kent B [Los Lunas, NM; Flemming, Jeb H [Albuquerque, NM; Jones, Gary D [Tijeras, NM; Tigges, Chris P [Albuquerque, NM

2010-04-13

A correlation spectrometer can detect a large number of gaseous compounds, or chemical species, with a species-specific mask wheel. In this mode, the spectrometer is optimized for the direct measurement of individual target compounds. Additionally, the spectrometer can measure the transmission spectrum from a given sample of gas. In this mode, infrared light is passed through a gas sample and the infrared transmission signature of the gasses present is recorded and measured using Hadamard encoding techniques. The spectrometer can detect the transmission or emission spectra in any system where multiple species are present in a generally known volume.

Optical design of a CubeSat-compatible imaging spectrometer

NASA Astrophysics Data System (ADS)

Mouroulis, Pantazis; Van Gorp, Byron; Green, Robert O.; Wilson, Daniel W.

2014-09-01

We describe a fast, uniform, low-polarization imaging spectrometer and telescope system that can be integrated in a 6U CubeSat. The spectral range is 350-1700 nm, with 5.7 nm sampling. The telescope and spectrometer operate at F/1.8. At 100 mm focal length, the telescope is the highest resolution form that can fit in the CubeSat frame without deployable mirrors. The field of view is 10° with 600 cross-track pixels. The spectrometer is designed for the new Teledyne CHROMA detector array with 30μm pixel size for maximizing throughput. The primary intended applications are coastal ocean and snow cover monitoring.

[Optical Design of Miniature Infrared Gratings Spectrometer Based on Planar Waveguide].

PubMed

Li, Yang-yu; Fang, Yong-hua; Li, Da-cheng; Liu, Yang

2015-03-01

In order to miniaturize an infrared spectrometer, we analyze the current optical design of miniature spectrometers and propose a method for designing a miniature infrared gratings spectrometer based on planar waveguide. Common miniature spectrometer uses miniature optical elements to reduce the size of system, which also shrinks the effective aperture. So the performance of spectrometer has dropped. Miniaturization principle of planar waveguide spectrometer is different from the principle of common miniature spectrometer. In planar waveguide spectrometer, the propagation of light is limited in a thin planar waveguide, which looks like the whole optical system is squashed flat. In the direction parallel to the planar waveguide, the light through the slit is collimated, dispersed and focused. And a spectral image is formed in the detector plane. This propagation of light is similar to the light in common miniature spectrometer. In the direction perpendicular to the planar waveguide, light is multiple reflected by the upper and lower surfaces of the planar waveguide and propagates in the waveguide. So the size of corresponding optical element could be very small in the vertical direction, which can reduce the size of the optical system. And the performance of the spectrometer is still good. The design method of the planar waveguide spectrometer can be separated into two parts, Czerny-Turner structure design and planar waveguide structure design. First, by using aberration theory an aberration-corrected (spherical aberration, coma, focal curve) Czerny-Turner structure is obtained. The operation wavelength range and spectral resolution are also fixed. Then, by using geometrical optics theory a planar waveguide structure is designed for reducing the system size and correcting the astigmatism. The planar waveguide structure includes a planar waveguide and two cylindrical lenses. Finally, they are modeled together in optical design software and are optimized as a whole. An

Interfacing an aspiration ion mobility spectrometer to a triple quadrupole mass spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Adamov, Alexey; Viidanoja, Jyrki; Kaerpaenoja, Esko

2007-04-15

This article presents the combination of an aspiration-type ion mobility spectrometer with a mass spectrometer. The interface between the aspiration ion mobility spectrometer and the mass spectrometer was designed to allow for quick mounting of the aspiration ion mobility spectrometer onto a Sciex API-300 triple quadrupole mass spectrometer. The developed instrumentation is used for gathering fundamental information on aspiration ion mobility spectrometry. Performance of the instrument is demonstrated using 2,6-di-tert-butyl pyridine and dimethyl methylphosphonate.

Compact terahertz spectrometer based on disordered rough surfaces

NASA Astrophysics Data System (ADS)

Yang, Tao; Jiang, Bing; Ge, Jia-cheng; Zhu, Yong-yuan; Li, Xing-ao; Huang, Wei

2018-01-01

In this paper, a compact spectrometer based on disordered rough surfaces for operation in the terahertz band is presented. The proposed spectrometer consists of three components, which are used for dispersion, modulation and detection respectively. The disordered rough surfaces, which are acted as the dispersion component, are modulated by the modulation component. Different scattering intensities are captured by the detection component with different extent of modulation. With a calibration measurement process, one can reconstruct the spectra of the probe terahertz beam by solving a system of simultaneous linear equations. A Tikhonov regularization approach has been implemented to improve the accuracy of the spectral reconstruction. The reported broadband, compact, high-resolution terahertz spectrometer is well suited for portable terahertz spectroscopy applications.

Characterization and Prediction of the SPI Background

NASA Technical Reports Server (NTRS)

Teegarden, B. J.; Jean, P.; Knodlseder, J.; Skinner, G. K.; Weidenspointer, G.

2003-01-01

The INTEGRAL Spectrometer, like most gamma-ray instruments, is background dominated. Signal-to-background ratios of a few percent are typical. The background is primarily due to interactions of cosmic rays in the instrument and spacecraft. It characteristically varies by +/- 5% on time scales of days. This variation is caused mainly by fluctuations in the interplanetary magnetic field that modulates the cosmic ray intensity. To achieve the maximum performance from SPI it is essential to have a high quality model of this background that can predict its value to a fraction of a percent. In this poster we characterize the background and its variability, explore various models, and evaluate the accuracy of their predictions.

Operation of a 500 MHz high temperature superconducting NMR: towards an NMR spectrometer operating beyond 1 GHz.

PubMed

Yanagisawa, Y; Nakagome, H; Tennmei, K; Hamada, M; Yoshikawa, M; Otsuka, A; Hosono, M; Kiyoshi, T; Takahashi, M; Yamazaki, T; Maeda, H

2010-04-01

We have begun a project to develop an NMR spectrometer that operates at frequencies beyond 1 GHz (magnetic field strength in excess of 23.5 T) using a high temperature superconductor (HTS) innermost coil. As the first step, we developed a 500 MHz NMR with a Bi-2223 HTS innermost coil, which was operated in external current mode. The temporal magnetic field change of the NMR magnet after the coil charge was dominated by (i) the field fluctuation due to a DC power supply and (ii) relaxation in the screening current in the HTS tape conductor; effect (i) was stabilized by the 2H field-frequency lock system, while effect (ii) decreased with time due to relaxation of the screening current induced in the HTS coil and reached 10(-8)(0.01 ppm)/h on the 20th day after the coil charge, which was as small as the persistent current mode of the NMR magnet. The 1D (1)H NMR spectra obtained by the 500 MHz LTS/HTS magnet were nearly equivalent to those obtained by the LTS NMR magnet. The 2D-NOESY, 3D-HNCO and 3D-HNCACB spectra were achieved for ubiquitin by the 500 MHz LTS/HTS magnet; their quality was closely equivalent to that achieved by a conventional LTS NMR. Based on the results of numerical simulation, the effects of screening current-induced magnetic field changes are predicted to be harmless for the 1.03 GHz NMR magnet system. 2010 Elsevier Inc. All rights reserved.

Comparison of two confocal micro-XRF spectrometers with different design aspects

PubMed Central

Smolek, S; Nakazawa, T; Tabe, A; Nakano, K; Tsuji, K; Streli, C; Wobrauschek, P

2014-01-01

Two different confocal micro X-ray fluorescence spectrometers have been developed and installed at Osaka City University and the Vienna University of Technology Atominstitut. The Osaka City University system is a high resolution spectrometer operating in air. The Vienna University of Technology Atominstitut spectrometer has a lower spatial resolution but is optimized for light element detection and operates under vacuum condition. The performance of both spectrometers was compared. In order to characterize the spatial resolution, a set of nine specially prepared single element thin film reference samples (500 nm in thickness, Al, Ti, Cr, Fe Ni, Cu, Zr, Mo, and Au) was used. Lower limits of detection were determined using the National Institute of Standards and Technology standard reference material glass standard 1412. A paint layer sample (cultural heritage application) and paint on automotive steel samples were analyzed with both instruments. The depth profile information was acquired by scanning the sample perpendicular to the surface. © 2013 The Authors. X-Ray Spectrometry published by John Wiley & Sons, Ltd. PMID:26430286

Comparison of two confocal micro-XRF spectrometers with different design aspects.

PubMed

Smolek, S; Nakazawa, T; Tabe, A; Nakano, K; Tsuji, K; Streli, C; Wobrauschek, P

2014-03-01

Two different confocal micro X-ray fluorescence spectrometers have been developed and installed at Osaka City University and the Vienna University of Technology Atominstitut. The Osaka City University system is a high resolution spectrometer operating in air. The Vienna University of Technology Atominstitut spectrometer has a lower spatial resolution but is optimized for light element detection and operates under vacuum condition. The performance of both spectrometers was compared. In order to characterize the spatial resolution, a set of nine specially prepared single element thin film reference samples (500 nm in thickness, Al, Ti, Cr, Fe Ni, Cu, Zr, Mo, and Au) was used. Lower limits of detection were determined using the National Institute of Standards and Technology standard reference material glass standard 1412. A paint layer sample (cultural heritage application) and paint on automotive steel samples were analyzed with both instruments. The depth profile information was acquired by scanning the sample perpendicular to the surface. © 2013 The Authors. X-Ray Spectrometry published by John Wiley & Sons, Ltd.

Portable gas chromatograph-mass spectrometer

DOEpatents

Andresen, B.D.; Eckels, J.D.; Kimmons, J.F.; Myers, D.W.

1996-06-11

A gas chromatograph-mass spectrometer (GC-MS) is described for use as a field portable organic chemical analysis instrument. The GC-MS is designed to be contained in a standard size suitcase, weighs less than 70 pounds, and requires less than 600 watts of electrical power at peak power (all systems on). The GC-MS includes: a conduction heated, forced air cooled small bore capillary gas chromatograph, a small injector assembly, a self-contained ion/sorption pump vacuum system, a hydrogen supply, a dual computer system used to control the hardware and acquire spectrum data, and operational software used to control the pumping system and the gas chromatograph. This instrument incorporates a modified commercial quadrupole mass spectrometer to achieve the instrument sensitivity and mass resolution characteristic of laboratory bench top units. 4 figs.

Portable gas chromatograph-mass spectrometer

DOEpatents

Andresen, Brian D.; Eckels, Joel D.; Kimmons, James F.; Myers, David W.

1996-01-01

A gas chromatograph-mass spectrometer (GC-MS) for use as a field portable organic chemical analysis instrument. The GC-MS is designed to be contained in a standard size suitcase, weighs less than 70 pounds, and requires less than 600 watts of electrical power at peak power (all systems on). The GC-MS includes: a conduction heated, forced air cooled small bore capillary gas chromatograph, a small injector assembly, a self-contained ion/sorption pump vacuum system, a hydrogen supply, a dual computer system used to control the hardware and acquire spectrum data, and operational software used to control the pumping system and the gas chromatograph. This instrument incorporates a modified commercial quadrupole mass spectrometer to achieve the instrument sensitivity and mass resolution characteristic of laboratory bench top units.

Mobile environment for an emission spectrometer

NASA Astrophysics Data System (ADS)

Radziak, Kamil; Litwin, Dariusz; Galas, Jacek; Tyburska-Staniewska, Anna; Ramsza, Andrzej

2017-08-01

The paper describes a mobile application to be used in a chemical analytical laboratory. The program running under the control of Android operating system allows for preview of measurements recorded by the emission spectrometer. Another part of the application monitors operational and configuration parameters of the device in real time. The first part of this paper includes an overview of the atomic spectrometry. The second part contains a description of the application and its further potential development direction.

A field portable mass spectrometer for monitoring organic vapors.

PubMed

Meier, R W

1978-03-01

A portable mass spectrometer has been designed and built under the sponsorship of the US Army for the purpose of monitoring low concentrations of specified organics in the ambient atmosphere. The goals of the development were discrimination, sensitivity, portability, simplicity of operation, economy and convenience. These objectives were met in a system consisting of a computer operated mass spectrometer with a Llewellyn membrane separator inlet system housed in two 26 x 18 x 9 inch aluminum cases with a total weight less than 150 pounds. This system has shown the capability for field detection of hundreds of specific organic vapors at the parts per billion level in the ambient and workplace environments.

SW-MW infrared spectrometer for lunar mission

NASA Astrophysics Data System (ADS)

Banerjee, Arup; Biswas, Amiya; Joshi, Shaunak; Kumar, Ankush; Rehman, Sami; Sharma, Satish; Somani, Sandip; Bhati, Sunil; Karelia, Jitendra; Saxena, Anish; Chowdhury, Arup R.

2016-04-01

SW-MW Imaging Infrared Spectrometer, the Hyperspectral optical imaging instrument is envisaged to map geomorphology and mineralogy of lunar surface. The instrument is designed to image the electro-magnetic energy emanating from moon's surface with high spectral and spatial resolution for the mission duration from an altitude of 100 km. It is designed to cover 0.8 to 5 μm in 250 spectral bands with GSD 80m and swath 20km. Primarily, there are three basic optical segments in the spectrometer. They are fore optics, dispersing element and focusing elements. The payload is designed around a custom developed multi-blaze convex grating optimized for system throughput. The considerations for optimization are lunar radiation, instrument background, optical throughput, and detector sensitivity. HgCdTe (cooled using a rotary stirling cooler) based detector array (500x256 elements, 30μm) is being custom developed for the spectrometer. Stray light background flux is minimized using a multi-band filter cooled to cryogenic temperature. Mechanical system realization is being performed considering requirements such as structural, opto-mechanical, thermal, and alignment. The entire EOM is planned to be maintained at 240K to reduce and control instrument background. Al based mirror, grating, and EOM housing is being developed to maintain structural requirements along with opto- mechanical and thermal. Multi-tier radiative isolation and multi-stage radiative cooling approach is selected for maintaining the EOM temperature. EOM along with precision electronics packages are planned to be placed on the outer and inner side of Anti-sun side (ASS) deck. Power and Cooler drive electronics packages are planned to be placed on bottom side of ASS panel. Cooler drive electronics is being custom developed to maintain the detector temperature within 100mK during the imaging phase. Low noise detector electronics development is critical for maintaining the NETD requirements at different target

Differential optical absorption spectrometer for measurement of tropospheric pollutants

NASA Astrophysics Data System (ADS)

Evangelisti, F.; Baroncelli, A.; Bonasoni, P.; Giovanelli, G.; Ravegnani, F.

1995-05-01

Our institute has recently developed a differential optical absorption spectrometry system called the gas analyzer spectrometer correlating optical absorption differences (GASCOAD), which features as a detector a linear image sensor that uses an artificial light source for long-path tropospheric-pollution monitoring. The GASCOAD, its method of eliminating interference from background sky light, and subsequent spectral analysis are reported and discussed. The spectrometer was used from 7 to 22 February 1993 in Milan, a heavily polluted metropolitan area, to measure the concentrations of SO2, NO2, O3, and HNO2 averaged over a 1.7-km horizontal light path. The findings are reported and briefly discussed.

Research on imaging spectrometer using LC-based tunable filter

NASA Astrophysics Data System (ADS)

Shen, Zhixue; Li, Jianfeng; Huang, Lixian; Luo, Fei; Luo, Yongquan; Zhang, Dayong; Long, Yan

2012-09-01

A liquid crystal tunable filter (LCTF) with large aperture is developed using PDLC liquid crystal. A small scale imaging spectrometer is established based on this tunable filter. This spectrometer can continuously tuning, or random-access selection of any wavelength in the visible and near infrared (VNIR) band synchronized with the imaging processes. Notable characteristics of this spectrometer include the high flexibility control of its operating channels, the image cubes with high spatial resolution and spectral resolution and the strong ability of acclimation to environmental temperature. The image spatial resolution of each tuning channel is almost near the one of the same camera without the LCTF. The spectral resolution is about 20 nm at 550 nm. This spectrometer works normally under 0-50°C with a maximum power consumption of 10 Watts (with exclusion of the storage module). Due to the optimization of the electrode structure and the driving mode of the Liquid Crystal cell, the switch time between adjacent selected channels can be reduced to 20 ms or even shorter. Spectral imaging experiments in laboratory are accomplished to verify the performance of this spectrometer, which indicate that this compact imaging spectrometer works reliably, and functionally. Possible applications of this imaging spectrometer include medical science, protection of historical relics, criminal investigation, disaster monitoring and mineral detection by remote sensing.

Micro-spec: an Integrated Direct-detection Spectrometer for Far-infrared Space Telescopes

NASA Technical Reports Server (NTRS)

Cataldo, Giuseppe; Hsieh, Wen-Ting; Huang, Wei-Chung; Moseley, S. Harvey; Stevenson, Thomas R.; Wollack, Edward J.

2014-01-01

The far-infrared and submillimeter portions of the electromagnetic spectrum provide a unique view of the astrophysical processes present in the early universe. Our ability to fully explore this rich spectral region has been limited, however, by the size and cost of the cryogenic spectrometers required to carry out such measurements.Micro-Spec (µ-Spec) is a high-sensitivity, direct-detection spectrometer concept working in the 450-1000 (micrometers) wavelength range which will enable a wide range of flight missions that would otherwise be challenging due tothe large size of current instruments with the required spectral resolution and sensitivity. The spectrometer design utilizes two internal antenna arrays, one for transmitting and one for receiving, superconducting microstrip transmission lines for power division and phase delay, and an array of microwave kinetic inductance detectors (MKIDs) to achieve these goals. The instrument will be integrated on a approximately 10 sq cm silicon chip and can therefore become an important capability under the low background conditions accessible via space and high-altitude borne platforms. In this paper, an optical design methodology for micro-Spec is presented, with particular attention given to its two-dimensional diffractive region, where the light of different wavelengths is focused on the different detectors. The method is based on the maximization of the instrument resolving power and minimization of the RMS phase error on the instrument focal plane. This two-step optimization can generate geometrical configurations given specific requirements on spectrometer size, operating spectral range and performance.Two point designs with resolving power of 260 and 520 and an RMS phase error less than approximately 0.004 radians were developed for initial demonstration and will be the basis of future instruments with resolving power up to about 1200.

Micro-Spec: an integrated direct-detection spectrometer for far-infrared space telescopes

NASA Astrophysics Data System (ADS)

Cataldo, Giuseppe; Hseih, Wen-Ting; Huang, Wei-Chung; Moseley, S. H.; Stevenson, Thomas R.; Wollack, Edward J.

2014-08-01

The far-infrared and submillimeter portions of the electromagnetic spectrum provide a unique view of the astrophysical processes present in the early universe. Our ability to fully explore this rich spectral region has been limited, however, by the size and cost of the cryogenic spectrometers required to carry out such measurements. Micro-Spec (μ-Spec) is a high-sensitivity, direct-detection spectrometer concept working in the 450-1000 μm wavelength range which will enable a wide range of flight missions that would otherwise be challenging due to the large size of current instruments with the required spectral resolution and sensitivity. The spectrometer design utilizes two internal antenna arrays, one for transmitting and one for receiving, superconducting microstrip transmission lines for power division and phase delay, and an array of microwave kinetic inductance detectors (MKIDs) to achieve these goals. The instrument will be integrated on a ~10 cm2 silicon chip and can therefore become an important capability under the low background conditions accessible via space and high-altitude borne platforms. In this paper, an optical design methodology for μ-Spec is presented, with particular attention given to its two-dimensional diffractive region, where the light of different wavelengths is focused on the different detectors. The method is based on the maximization of the instrument resolving power and minimization of the RMS phase error on the instrument focal plane. This two-step optimization can generate geometrical configurations given specific requirements on spectrometer size, operating spectral range and performance. Two point designs with resolving power of 260 and 520 and an RMS phase error less than ~0:004 radians were developed for initial demonstration and will be the basis of future instruments with resolving power up to about 1200.

Safari: instrument design of the far-infrared imaging spectrometer for spica

NASA Astrophysics Data System (ADS)

Jellema, W.; Pastor, C.; Naylor, D.; Jackson, B.; Sibthorpe, B.; Roelfsema, P.

2017-11-01

The next great leap forward in space-based far-infrared astronomy will be made by the Japanese-led SPICA mission, which is anticipated to be launched late 2020's as the next large astrophysics mission of JAXA, in partnership with ESA and with key European contributions. Filling in the gap between JWST and ALMA, the SPICA mission will study the evolution of galaxies, stars and planetary systems. SPICA will utilize a deeply cooled 3m-class telescope, provided by European industry, to realize zodiacal background limited performance, high spatial resolution and large collecting area. Making full advantage of the deeply cooled telescope (<6K), the SAFARI instrument on SPICA is a highly sensitive wide-field imaging photometer and spectrometer operating in the 34-210 μm wavelength range. Utilizing Nyquist-sampled focal-plane arrays of very sensitive Transition Edge Sensors (TES), SAFARI will offer a photometric imaging (R ≍ 2), and a low (R = 100) and medium resolution (R = 2000 at 100 μm) imaging spectroscopy mode in three photometric bands within a 2'x2' instantaneous FoV by means of a cryogenic Mach-Zehnder Fourier Transform Spectrometer. In this paper we will provide an overview of the SAFARI instrument design and system architecture. We will describe the reference design of the SAFARI focal- plane unit, the implementation of the various optical instrument functions designed around the central large-stroke FTS system, the photometric band definition and out-of-band filtering by quasioptical elements, the control of straylight, diffraction and thermal emission in the long-wavelength limit, and how we interface to the large-format FPA arrays at one end and the SPICA telescope assembly at the other end. We will briefly discuss the key performance drivers with special emphasis on the optical techniques adopted to overcome issues related to very low background operation of SAFARI. A summary and discussion of the expected instrument performance and an overview of the

MASS SPECTROMETER LEAK

DOEpatents

Shields, W.R.

1960-10-18

An improved valve is described for precisely regulating the flow of a sample fluid to be analyzed, such as in a mass spectrometer, where a gas sample is allowed to "leak" into an evacuated region at a very low, controlled rate. The flow regulating valve controls minute flow of gases by allowing the gas to diffuse between two mating surfaces. The structure of the valve is such as to prevent the corrosive feed gas from contacting the bellows which is employed in the operation of the valve, thus preventing deterioration of the bellows.

Monolithic spectrometer

DOEpatents

Rajic, Slobodan; Egert, Charles M.; Kahl, William K.; Snyder, Jr., William B.; Evans, III, Boyd M.; Marlar, Troy A.; Cunningham, Joseph P.

1998-01-01

A monolithic spectrometer is disclosed for use in spectroscopy. The spectrometer is a single body of translucent material with positioned surfaces for the transmission, reflection and spectral analysis of light rays.

High resolution Fouier transform spectrometer Serial No. 091002: Instruction manual

NASA Technical Reports Server (NTRS)

1971-01-01

A description of the spectrometer and procedures for its operation, maintenance, alignments, adjustments, and control functions are presented. The interferometer spectrometer is a modified Model 296 capable of 0.5/cm resolution over the spectral region of 5 to 15 microns configured for operation with the optical head at a temperature of approximately 80 K. Details are given on the optical system and the electronic circuits. The detector used with the optical head is mercury doped germanium kept at a temperature of about 4 K by means of liquid helium. Electronic schematics, and instruction manuals for handling the liquid helium dewars, tape recorder for analog outputs, and playback console are included.

Composite Infrared Spectrometer (CIRS) on Cassini

NASA Technical Reports Server (NTRS)

Jennings, Donald E.; Flasar, F. M.; Kunde, V. G.; Nixon, C. A.; Segura, M. E.; Romani, P. N.; Gorius, N.; Albright, S.; Brasunas, J. C.; Carlson, R. C.;

Miniaturized Ion Mobility Spectrometer

NASA Technical Reports Server (NTRS)

Stimac, Robert M. (Inventor); Kaye, William J (Inventor)

2017-01-01

By utilizing the combination of a unique electronic ion injection control circuit in conjunction with a particularly designed drift cell construction, the instantly disclosed ion mobility spectrometer (IMS) achieves increased levels of sensitivity, while achieving significant reductions in size and weight. The instant IMS is of a much simpler and easy to manufacture design, rugged and hermetically sealed, capable of operation at high temperatures to at least 250 degrees Centigrade, and is uniquely sensitive, particularly to explosive chemicals.

Miniaturized Ion Mobility Spectrometer

NASA Technical Reports Server (NTRS)

Kaye, William J. (Inventor); Stimac, Robert M. (Inventor)

2015-01-01

By utilizing the combination of a unique electronic ion injection control circuit in conjunction with a particularly designed drift cell construction, the instantly disclosed ion mobility spectrometer achieves increased levels of sensitivity, while achieving significant reductions in size and weight. The instant IMS is of a much simpler and easy to manufacture design, rugged and hermetically sealed, capable of operation at high temperatures to at least 250.degree. C., and is uniquely sensitive, particularly to explosive chemicals.

Monolithic spectrometer

DOEpatents

Rajic, S.; Egert, C.M.; Kahl, W.K.; Snyder, W.B. Jr.; Evans, B.M. III; Marlar, T.A.; Cunningham, J.P.

1998-05-19

A monolithic spectrometer is disclosed for use in spectroscopy. The spectrometer is a single body of translucent material with positioned surfaces for the transmission, reflection and spectral analysis of light rays. 6 figs.

Development of mercuric iodide uncooled x ray detectors and spectrometers

NASA Technical Reports Server (NTRS)

Iwanczyk, Jan S.

1990-01-01

The results obtained in the development of miniature, lowpower, light weight mercuric iodide, HgI2, x ray spectrometers for future space missions are summarized. It was demonstrated that HgI2 detectors can be employed in a high resolution x ray spectrometer, operating in a scanning electron microscope. Also, the development of HgI2 x ray detectors to augment alpha backscattering spectrometers is discussed. These combination instruments allow for the identification of all chemical elements, with the possible exception of hydrogen, and their respective concentrations. Additionally, further investigations of questions regarding radiation damage effects in the HgI2 x ray detectors are reported.

HyTES: Thermal Imaging Spectrometer Development

NASA Technical Reports Server (NTRS)

Johnson, William R.; Hook, Simon J.; Mouroulis, Pantazis; Wilson, Daniel W.; Gunapala, Sarath D.; Realmuto, Vincent; Lamborn, Andy; Paine, Chris; Mumolo, Jason M.; Eng, Bjorn T.

2011-01-01

The Jet Propulsion Laboratory has developed the Hyperspectral Thermal Emission Spectrometer (HyTES). It is an airborne pushbroom imaging spectrometer based on the Dyson optical configuration. First low altitude test flights are scheduled for later this year. HyTES uses a compact 7.5-12 micrometer m hyperspectral grating spectrometer in combination with a Quantum Well Infrared Photodetector (QWIP) and grating based spectrometer. The Dyson design allows for a very compact and optically fast system (F/1.6). Cooling requirements are minimized due to the single monolithic prism-like grating design. The configuration has the potential to be the optimal science-grade imaging spectroscopy solution for high altitude, lighter-than-air (HAA, LTA) vehicles and unmanned aerial vehicles (UAV) due to its small form factor and relatively low power requirements. The QWIP sensor allows for optimum spatial and spectral uniformity and provides adequate responsivity which allows for near 100mK noise equivalent temperature difference (NEDT) operation across the LWIR passband. The QWIP's repeatability and uniformity will be helpful for data integrity since currently an onboard calibrator is not planned. A calibration will be done before and after eight hour flights to gage any inconsistencies. This has been demonstrated with lab testing. Further test results show adequate NEDT, linearity as well as applicable earth science emissivity target results (Silicates, water) measured in direct sunlight.

Analysis of aircraft spectrometer data with logarithmic residuals

NASA Technical Reports Server (NTRS)

Green, A. A.; Craig, M. D.

1985-01-01

Spectra from airborne systems must be analyzed in terms of their mineral-related absorption features. Methods for removing backgrounds and extracting these features one at a time from reflectance spectra are discussed. Methods for converting radiance spectra into a form similar to reflectance spectra so that the feature extraction procedures can be implemented on aircraft spectrometer data are also discussed.

A Ka-band chirped-pulse Fourier transform microwave spectrometer

NASA Astrophysics Data System (ADS)

Zaleski, Daniel P.; Neill, Justin L.; Muckle, Matt T.; Seifert, Nathan A.; Brandon Carroll, P.; Widicus Weaver, Susanna L.; Pate, Brooks H.

2012-10-01

The design and performance of a new chirped-pulse Fourier transform microwave (CP-FTMW) spectrometer operating from 25 to 40 GHz (Ka-band) is presented. This spectrometer is well-suited for the study of complex organic molecules of astronomical interest in the size range of 6-10 atoms that have strong rotational transitions in Ka-band under pulsed jet sample conditions (Trot = 1-10 K). The spectrometer permits acquisition of the full spectral band in a single data acquisition event. Sensitivity is enhanced by using two pulsed jet sources and acquiring 10 broadband measurements for each sample injection cycle. The spectrometer performance is benchmarked by measuring the pure rotational spectrum of several isotopologues of acetaldehyde in natural abundance. The rotational spectra of the singly substituted 13C and 18O isotopologues of the two lowest energy conformers of ethyl formate have been analyzed and the resulting substitution structures for these conformers are compared to electronic structure theory calculations.

Diode-Laser-Based Spectrometer for Sensing Gases

NASA Technical Reports Server (NTRS)

Silver, Joel A.

2005-01-01

A diode-laser-based spectrometer has been developed for measuring concentrations of gases and is intended particularly for use in analyzing and monitoring combustion processes under microgravitational conditions in a drop tower or a spacecraft. This instrument is also well suited for use on Earth in combustion experiments and for such related purposes as fire-safety monitoring and monitoring toxic and flammable gases in industrial settings. Of the gas-sensing spectrometers available prior to the development of this instrument, those that were sensitive enough for measuring the combustion gases of interest were too large, required critical optical alignments, used far too much electrical power, and were insufficiently rugged for use under the severe conditions of spacecraft launch and space flight. In contrast, the present instrument is compact, consumes relatively little power, and is rugged enough to withstand launch vibrations and space flight. In addition, this instrument is characterized by long-term stability, accuracy, and reliability. The diode laser in this spectrometer is operated in a wavelength-modulation mode. Different gases to be measured can be selected by changing modular laser units. The operation of the laser is controlled by customized, low-power electronic circuitry built around a digital signal-processor board. This customized circuitry also performs acquisition and analysis of data, controls communications, and manages errors.

Enhanced Analysis Techniques for an Imaging Neutron and Gamma Ray Spectrometer

NASA Astrophysics Data System (ADS)

Madden, Amanda C.

The presence of gamma rays and neutrons is a strong indicator of the presence of Special Nuclear Material (SNM). The imaging Neutron and gamma ray SPECTrometer (NSPECT) developed by the University of New Hampshire and Michigan Aerospace corporation detects the fast neutrons and prompt gamma rays from fissile material, and the gamma rays from radioactive material. The instrument operates as a double scatter device, requiring a neutron or a gamma ray to interact twice in the instrument. While this detection requirement decreases the efficiency of the instrument, it offers superior background rejection and the ability to measure the energy and momentum of the incident particle. These measurements create energy spectra and images of the emitting source for source identification and localization. The dual species instrument provides superior detection than a single species alone. In realistic detection scenarios, few particles are detected from a potential threat due to source shielding, detection at a distance, high background, and weak sources. This contributes to a small signal to noise ratio, and threat detection becomes difficult. To address these difficulties, several enhanced data analysis tools were developed. A Receiver Operating Characteristic Curve (ROC) helps set instrumental alarm thresholds as well as to identify the presence of a source. Analysis of a dual-species ROC curve provides superior detection capabilities. Bayesian analysis helps to detect and identify the presence of a source through model comparisons, and helps create a background corrected count spectra for enhanced spectroscopy. Development of an instrument response using simulations and numerical analyses will help perform spectra and image deconvolution. This thesis will outline the principles of operation of the NSPECT instrument using the double scatter technology, traditional analysis techniques, and enhanced analysis techniques as applied to data from the NSPECT instrument, and an

Study on ultra-fast single photon counting spectrometer based on PCI

NASA Astrophysics Data System (ADS)

Zhang, Xi-feng

2010-10-01

The time-correlated single photon counting spectrometer developed uses PCI bus technology. We developed the ultrafast data acquisition card based on PCI, replace multi-channel analyzer primary. The system theory and design of the spectrometer are presented in detail, and the process of operation is introduced with the integration of the system. Many standard samples have been measured and the data have been analyzed and contrasted. Experimental results show that the spectrometer, s sensitive is single photon counting, and fluorescence life-span and time resolution is picosecond level. And the instrument could measure time-resolved spectroscopy.

The Spectral Image Processing System (SIPS) - Interactive visualization and analysis of imaging spectrometer data

NASA Technical Reports Server (NTRS)

Kruse, F. A.; Lefkoff, A. B.; Boardman, J. W.; Heidebrecht, K. B.; Shapiro, A. T.; Barloon, P. J.; Goetz, A. F. H.

1993-01-01

The Center for the Study of Earth from Space (CSES) at the University of Colorado, Boulder, has developed a prototype interactive software system called the Spectral Image Processing System (SIPS) using IDL (the Interactive Data Language) on UNIX-based workstations. SIPS is designed to take advantage of the combination of high spectral resolution and spatial data presentation unique to imaging spectrometers. It streamlines analysis of these data by allowing scientists to rapidly interact with entire datasets. SIPS provides visualization tools for rapid exploratory analysis and numerical tools for quantitative modeling. The user interface is X-Windows-based, user friendly, and provides 'point and click' operation. SIPS is being used for multidisciplinary research concentrating on use of physically based analysis methods to enhance scientific results from imaging spectrometer data. The objective of this continuing effort is to develop operational techniques for quantitative analysis of imaging spectrometer data and to make them available to the scientific community prior to the launch of imaging spectrometer satellite systems such as the Earth Observing System (EOS) High Resolution Imaging Spectrometer (HIRIS).

A miniaturized NQR spectrometer for a multi-channel NQR-based detection device

NASA Astrophysics Data System (ADS)

Beguš, Samo; Jazbinšek, Vojko; Pirnat, Janez; Trontelj, Zvonko

2014-10-01

A low frequency (0.5-5 MHz) battery operated sensitive pulsed NQR spectrometer with a transmitter power up to 5 W and a total mass of about 3 kg aimed at detecting 14 N NQR signals, predominantly of illicit materials, was designed and assembled. This spectrometer uses a standard software defined radio (SDR) platform for the data acquisition unit. Signal processing is done with the LabView Virtual instrument on a personal computer. We successfully tested the spectrometer by measuring 14 N NQR signals from aminotetrazole monohydrate (ATMH), potassium nitrate (PN), paracetamol (PCM) and trinitrotoluene (TNT). Such a spectrometer is a feasible component of a portable single or multichannel 14 N NQR based detection device.

Micro-Spec: an Integrated, Direct-Detection Spectrometer for Far-Infrared and Submillimeter Astronomy

NASA Technical Reports Server (NTRS)

Cataldo, Giuseppe

2014-01-01

The far-infrared and submillimeter portions of the electromagnetic spectrum provide a unique view of the astrophysical processes present in the early universe. Our ability to fully explore this rich spectral region has been limited, however, by the size and cost of the cryogenic spectrometers required to carry out such measurements. Micro-Spec (u-Spec) is a high-sensitivity, direct-detection spectrometer concept working in the 450-1000 micromillimeter wavelength range which will enable a wide range of flight missions that would otherwise be challenging due to the large size of current instruments with the required spectral resolution and sensitivity. The spectrometer design utilizes two internal antenna arrays, one for transmitting and one for receiving, superconducting microstrip transmission lines for power division and phase delay, and an array of microwave kinetic inductance detectors (MKIDs) to achieve these goals. The instrument will be integrated on a approximately 10 square cm silicon chip and can therefore become an important capability under the low background conditions accessible via space and high-altitude borne platforms. In this paper, an optical design methodology for Micro-Spec is presented, with particular attention given to its twodimensional diffractive region, where the light of different wavelengths is focused on the different detectors. The method is based on the maximization of the instrument resolving power and minimization of the RMS phase error on the instrument focal plane. This two-step optimization can generate geometrical configurations given specific requirements on spectrometer size, operating spectral range and performance. A point design with resolving power of 257, an RMS phase error less than 0.1 radians and four stigmatic points was developed for initial demonstration and will be the basis of future instruments with resolving power up to about 1200.

A Dual Source Ion Trap Mass Spectrometer for the Mars Organic Molecule Analyzer of ExoMars 2018

NASA Technical Reports Server (NTRS)

Brickerhoff, William B.; vanAmerom, F. H. W.; Danell, R. M.; Arevalo, R.; Atanassova, M.; Hovmand, L.; Mahaffy, P. R.; Cotter, R. J.

2011-01-01

We present details on the objectives, requirements, design and operational approach of the core mass spectrometer of the Mars Organic Molecule Analyzer (MOMA) investigation on the 2018 ExoMars mission. The MOMA mass spectrometer enables the investigation to fulfill its objective of analyzing the chemical composition of organic compounds in solid samples obtained from the near surface of Mars. Two methods of ionization are realized, associated with different modes of MOMA operation, in a single compact ion trap mass spectrometer. The stringent mass and power constraints of the mission have led to features such as low voltage and low frequency RF operation [1] and pulse counting detection.

Rugged optical mirrors for the operation of Fourier-Transform Spectrometers in rough environments

NASA Astrophysics Data System (ADS)

Feist, Dietrich G.

2014-05-01

The Total Carbon Column Observing Network (TCCON) and the Network for the Detection of Atmospheric Composition Change (NDACC) operate a growing number of Fourier-Transform Spectrometers (FTS) that measure the total column of several atmospheric trace gases. For these measurements, the sun is used as a light source. This is typically achieved by a solar tracker that uses a pair of optical mirrors to guide the sunlight into the instrument. There is a growing demand to operate these instruments in remote locations that fill the gaps in the global observation network. Besides the logistical challenges of running a remote site, the environment at these locations can be very harsh compared to the sheltered environment of the instruments' home institutions. While the FTS itself is usually well protected inside a building or container, the solar tracker and especially its mirrors are exposed to the environment. There they may suffer from - temperature fluctuations - high humidity - sea salt corrosion at coastal sites - dirt and dust - air pollution from anthropogenic sources - deposition from plants or animals The Max Planck Institute for Biogeochemistry (MPI-BGC) operates a TCCON station on Ascension Island, about 200 m from the sea. Under the rough conditions at this site, typical optical mirrors that are made for laboratory conditions are destroyed by sea salt spray within a few weeks. Besides, typical gold-coated mirrors cannot be cleaned as their soft surface is easily scratched or damaged. To overcome these problems, the MPI-BGC has developed optical mirrors that - offer good reflectivity in the near and mid infrared - are highly resistant to salt and chlorine - have a hard surface so that they can be cleaned often and easily - are not affected by organic solvents - last for months in very harsh environments - can be reused after polishing These mirrors could be applied to most TCCON and NDACC sites. This way, the network could be expanded to regions where operation

Study and evaluation of impulse mass spectrometers for ion analysis in the D and E regions of the ionosphere

NASA Technical Reports Server (NTRS)

Kendall, B. R.

1979-01-01

Theoretical and numerical analyses were made of planar, cylindrical and spherical electrode time-of-flight mass spectrometers in order to optimize their operating conditions. A numerical analysis of potential barrier gating in time-of-flight spectrometers was also made. The results were used in the design of several small mass spectrometers. These were constructed and tested in a laboratory space simulator. Detailed experimental studies of a miniature cylindrical electrode time of flight mass spectrometer and of a miniature hemispherical electrode time of flight mass spectrometer were made. The extremely high sensitivity of these instruments and their ability to operate at D region pressures with an open source make them ideal instruments for D region ion composition measurements.

Hong-Ou-Mandel Gravitational Wave Space spectrometER - HOMER mission

NASA Astrophysics Data System (ADS)

Jacinto de Matos, Clovis; Tajmar, Martin

2018-06-01

Michelson type gravitational wave detectors measure the strain caused by gravitational waves on the interferometer's arms. Gravitational waves can also cause the rotation of photon's linear polarization vector, thus disturbing the interference of entangled photons in Hong-Ou-Mandel (HOM) interferometers. Here one uses that physical phenomenon to devise a spectrometer for gravitational waves through the implementation of a Hong-Ou-Mandel interferometer in Earth geostationary orbit with a constellation of three different spacecraft in accurate formation flight. We call this mission, the Hong-Ou-Mandel Gravitational Waves Space SpectrometER (HOMER). HOMER will cover the part of the gravitational wave spectrum with wavelengths around λ =105 km, which falls between the long wavelength detection range of LISA, around λ =106 km, and of ground based detectors like LIGO, around λ =103 km. With respect to Michelson type detectors, the proposed concept for the detection and spectral analysis of gravitational waves has the advantage of operating without the need of drag free satellites, however it requires a relative precision of the attitude between satellites of the order of the gravitational waves amplitude δθ / θ ∼ h ∼10-20 , which makes the architecture of the HOMER mission as challenging as the Michelson type space detectors. The difficulty being however transferred from the monitoring of the relative distance between spacecraft (for Michelson antennas) to their relative attitude. By focusing on photons polarization instead of photons phase one can measure the spectrum of the detected gravitational signal. As a bonus, the proposed instrument could also investigate the influence of spacetime curvature on photons quantum entanglement, thus experimentally peering into the relation between general relativity and quantum mechanics, which is currently a subject of high interest in theoretical physics. This paper will describe the HOMER mission concept in general and

Multidimensional spectrometer

DOEpatents

Zanni, Martin Thomas; Damrauer, Niels H.

2010-07-20

A multidimensional spectrometer for the infrared, visible, and ultraviolet regions of the electromagnetic spectrum, and a method for making multidimensional spectroscopic measurements in the infrared, visible, and ultraviolet regions of the electromagnetic spectrum. The multidimensional spectrometer facilitates measurements of inter- and intra-molecular interactions.

A feasibility study of ion implantation techniques for mass spectrometer calibration

NASA Technical Reports Server (NTRS)

Koslin, M. E.; Krycuk, G. A.; Schatz, J. G., Jr.; White, F. A.; Wood, G. M.

1978-01-01

An experimental study was undertaken to examine the feasibility of using ion-implanted filaments doped with either an alkali metal or noble gas for in situ recalibration of onboard mass spectrometers during extended space missions. Implants of rubidium and krypton in rhenium ribbon filaments were subsequently tested in a bakeable 60 deg sector mass spectrometer operating in the static mode. Surface ionization and electron impact ion sources were both used, each yielding satisfactory results. The metallic implant with subsequent ionization provided a means of mass scale calibration and determination of system operating parameters, whereas the noble gas thermally desorbed into the system was more suited for partial pressure and sensitivity determinations.

Design and Performance of a Spectrometer for Deployment on MISSE 7

NASA Technical Reports Server (NTRS)

Pippin, Gary; Beymer, Jim; Robb, Andrew; Longino, James; Perry, George; Stewart, Alan; Finkenor, Miria

2009-01-01

A spectrometer for reflectance and transmission measurements of samples exposed to the space environment has been developed for deployment on the Materials on the International Space Station Experiment (MISSE) 7. The instrument incorporates a miniature commercial fiber optic coupled spectrometer with a computer control system for detector operation, sample motion and illumination. A set of three spectrometers were recently integrated on the MISSE7 platform with launch and deployment on the International Space Station scheduled for summer of this year. The instrument is one of many active experiments on the platform. The performance of the instrument prior to launch will be discussed. Data from samples measured in the laboratory will be compared to those from the instrument prior to launch. These comparisons will illustrate the capabilities of the current design. The space environment challenges many materials. When in operation on the MISSE 7 platform, the new spectrometer will provide real time data on the how the space environment affects the optical properties of thermal control paints and optical coatings. Data obtained from comparison of pre and post flight measurements on hundreds of samples exposed on previous MISSE platforms have been reported at these meetings. With the new spectrometer and the ability to correlate measured changes with time on orbit and the occurrence of both natural events and human activities, a better understanding of the processes responsible for degradation of materials in space will be possible.

A low-volume cavity ring-down spectrometer for sample-limited applications

NASA Astrophysics Data System (ADS)

Stowasser, C.; Farinas, A. D.; Ware, J.; Wistisen, D. W.; Rella, C.; Wahl, E.; Crosson, E.; Blunier, T.

2014-08-01

In atmospheric and environmental sciences, optical spectrometers are used for the measurements of greenhouse gas mole fractions and the isotopic composition of water vapor or greenhouse gases. The large sample cell volumes (tens of milliliters to several liters) in commercially available spectrometers constrain the usefulness of such instruments for applications that are limited in sample size and/or need to track fast variations in the sample stream. In an effort to make spectrometers more suitable for sample-limited applications, we developed a low-volume analyzer capable of measuring mole fractions of methane and carbon monoxide based on a commercial cavity ring-down spectrometer. The instrument has a small sample cell (9.6 ml) and can selectively be operated at a sample cell pressure of 140, 45, or 20 Torr (effective internal volume of 1.8, 0.57, and 0.25 ml). We present the new sample cell design and the flow path configuration, which are optimized for small sample sizes. To quantify the spectrometer's usefulness for sample-limited applications, we determine the renewal rate of sample molecules within the low-volume spectrometer. Furthermore, we show that the performance of the low-volume spectrometer matches the performance of the standard commercial analyzers by investigating linearity, precision, and instrumental drift.

A miniaturized NQR spectrometer for a multi-channel NQR-based detection device.

PubMed

Beguš, Samo; Jazbinšek, Vojko; Pirnat, Janez; Trontelj, Zvonko

2014-10-01

A low frequency (0.5-5 MHz) battery operated sensitive pulsed NQR spectrometer with a transmitter power up to 5 W and a total mass of about 3 kg aimed at detecting (14)N NQR signals, predominantly of illicit materials, was designed and assembled. This spectrometer uses a standard software defined radio (SDR) platform for the data acquisition unit. Signal processing is done with the LabView Virtual instrument on a personal computer. We successfully tested the spectrometer by measuring (14)N NQR signals from aminotetrazole monohydrate (ATMH), potassium nitrate (PN), paracetamol (PCM) and trinitrotoluene (TNT). Such a spectrometer is a feasible component of a portable single or multichannel (14)N NQR based detection device. Copyright © 2014 Elsevier Inc. All rights reserved.

Photoelectron spectrometer for liquid and gas-phase attosecond spectroscopy with field-free and magnetic bottle operation modes

NASA Astrophysics Data System (ADS)

Jordan, Inga; Jain, Arohi; Gaumnitz, Thomas; Ma, Jun; Wörner, Hans Jakob

2018-05-01

A compact time-of-flight spectrometer for applications in attosecond spectroscopy in the liquid and gas phases is presented. It allows for altering the collection efficiency by transitioning between field-free and magnetic-bottle operation modes. High energy resolution (ΔE/E = 0.03 for kinetic energies >20 eV) is achieved despite the short flight-tube length through a homogeneous deceleration potential at the beginning of the flight tube. A closing mechanism allows isolating the vacuum system of the flight tube from the interaction region in order to efficiently perform liquid-microjet experiments. The capabilities of the instrument are demonstrated through photoelectron spectra from multiphoton ionization of argon and xenon, as well as photoelectron spectra of liquid and gaseous water generated by an attosecond pulse train.

Airborne Visible/Infrared Imaging Spectrometer (AVIRIS): Sensor improvements for 1994 and 1995

NASA Technical Reports Server (NTRS)

Sarture, C. M.; Chrien, T. G.; Green, R. O.; Eastwood, M. L.; Raney, J. J.; Hernandez, M. A.

1995-01-01

AVIRIS is a NASA-sponsored Earth-remote-sensing imaging spectrometer designed, built and operated by the Jet Propulsion Laboratory (JPL). While AVIRIS has been operational since 1989, major improvements have been completed in most of the sensor subsystems during the winter maintenance cycles. As a consequence of these efforts, the capabilities of AVIRIS to reliably acquire and deliver consistently high quality, calibrated imaging spectrometer data continue to improve annually, significantly over those in 1989. Improvements to AVIRIS prior to 1994 have been described previously. This paper details recent and planned improvements to AVIRIS in the sensor task.

A novel dual-detector micro-spectrometer

NASA Astrophysics Data System (ADS)

Otto, Thomas; Saupe, Ray; Stock, Volker; Bruch, Reinhard; Gruska, Bernd; Gessner, Thomas

2005-01-01

Infrared analysis is a well-established tool for measuring composition and purity of various materials in industrial-, medical- and environmental applications. Traditional spectrometers, for example Fourier Transform Infrared (FTIR) Instruments are mainly designed for laboratory use and are generally, too large, heavy, costly and delicate to handle for remote applications. With important advances in the miniaturization, ruggedness and cost efficiency we have designed and created a new type of a micromirror spectrometer that can operate in harsh temperature and vibrating environments This device is ideally suited for environmental monitoring, chemical and biological applications as well as detection of biological warfare agents and sensing in important security locations In order to realize such compact, portable and field-deployable spectrometers we have applied MOEMS technology. Thus our novel dual detector micro mirror system is composed of a scanning micro mirror combined with a diffraction grating and other essential optical components in order to miniaturize the basic modular set-up. Especially it periodically disperses polychromatic radiation into its spectral components, which are measured by a combination of a visible (VIS) and near infrared (NIR) single element detector. By means of integrated preamplifiers high-precise measurements over a wide dynamic wavelength range are possible. In addition the spectrometer, including the radiation source, detectors and electronics can be coupled to a minimum-volume liquid or gas-flow cell. Furthermore a SMA connector as a fiber optical input allows easy attachment of fiber based probes. By utilizing rapid prototyping techniques, where all components are directly integrated, the micro mirror spectrometer is manufactured for the 700-1700 nm spectral range. In this work the advanced optical design and integration of the electronic interface will be reviewed. Furthermore we will demonstrate the performance of the system

Acousto-optic tunable filter spectrometers in space missions [Invited].

PubMed

Korablev, Oleg I; Belyaev, Denis A; Dobrolenskiy, Yuri S; Trokhimovskiy, Alexander Y; Kalinnikov, Yuri K

2018-04-01

Spectrometers employing acousto-optic tunable filters (AOTFs) rapidly gain popularity in space, and in particular on interplanetary missions. They allow for reducing volume, mass, and complexity of the instrumentation. To date, space operations of 11 AOTF spectrometers are reported in the literature. They were used for analyzing ocean color, greenhouse gases, atmospheres of Mars and Venus, and for lunar mineralogy. More instruments for the Moon, Mars, and asteroid mineralogy are in flight, awaiting launch, or in the state of advanced development. The AOTFs are used in point (pencil-beam) spectrometers for selecting echelle diffraction orders, or in hyper-spectral imagers and microscopes. We review the AOTF-employing devices flown in space or ready to set off. The paper considers basic principles of the AOTF and science applications of the AOTF spectrometers, and describes developed instruments in some detail. We also address some advanced developments for future missions and plans. In addition, we discuss lessons learned during instrument design, build, calibration, and exploitation, and advantages and limitations in implementing the AOTF-based systems in space instrumentation.

The SPEDE spectrometer

NASA Astrophysics Data System (ADS)

Papadakis, P.; Cox, D. M.; O'Neill, G. G.; Borge, M. J. G.; Butler, P. A.; Gaffney, L. P.; Greenlees, P. T.; Herzberg, R.-D.; Illana, A.; Joss, D. T.; Konki, J.; Kröll, T.; Ojala, J.; Page, R. D.; Rahkila, P.; Ranttila, K.; Thornhill, J.; Tuunanen, J.; Van Duppen, P.; Warr, N.; Pakarinen, J.

2018-03-01

The electron spectrometer, SPEDE, has been developed and will be employed in conjunction with the Miniball spectrometer at the HIE-ISOLDE facility, CERN. SPEDE allows for direct measurement of internal conversion electrons emitted in-flight, without employing magnetic fields to transport or momentum filter the electrons. Together with the Miniball spectrometer, it enables simultaneous observation of γ rays and conversion electrons in Coulomb excitation experiments using radioactive ion beams.

A Macintosh based data system for array spectrometers (Poster)

NASA Astrophysics Data System (ADS)

Bregman, J.; Moss, N.

An interactive data aquisition and reduction system has been assembled by combining a Macintosh computer with an instrument controller (an Apple II computer) via an RS-232 interface. The data system provides flexibility for operating different linear array spectrometers. The standard Macintosh interface is used to provide ease of operation and to allow transferring the reduced data to commercial graphics software.

BiFCROS: A Low-Background Fluorescence Repressor Operator System for Labeling of Genomic Loci.

PubMed

Milbredt, Sarah; Waldminghaus, Torsten

2017-06-07

Fluorescence-based methods are widely used to analyze elementary cell processes such as DNA replication or chromosomal folding and segregation. Labeling DNA with a fluorescent protein allows the visualization of its temporal and spatial organization. One popular approach is FROS (fluorescence repressor operator system). This method specifically labels DNA in vivo through binding of a fusion of a fluorescent protein and a repressor protein to an operator array, which contains numerous copies of the repressor binding site integrated into the genomic site of interest. Bound fluorescent proteins are then visible as foci in microscopic analyses and can be distinguished from the background fluorescence caused by unbound fusion proteins. Even though this method is widely used, no attempt has been made so far to decrease the background fluorescence to facilitate analysis of the actual signal of interest. Here, we present a new method that greatly reduces the background signal of FROS. BiFCROS (Bimolecular Fluorescence Complementation and Repressor Operator System) is based on fusions of repressor proteins to halves of a split fluorescent protein. Binding to a hybrid FROS array results in fluorescence signals due to bimolecular fluorescence complementation. Only proteins bound to the hybrid FROS array fluoresce, greatly improving the signal to noise ratio compared to conventional FROS. We present the development of BiFCROS and discuss its potential to be used as a fast and single-cell readout for copy numbers of genetic loci. Copyright © 2017 Milbredt and Waldminghaus.

BiFCROS: A Low-Background Fluorescence Repressor Operator System for Labeling of Genomic Loci

PubMed Central

Milbredt, Sarah; Waldminghaus, Torsten

2017-01-01

Fluorescence-based methods are widely used to analyze elementary cell processes such as DNA replication or chromosomal folding and segregation. Labeling DNA with a fluorescent protein allows the visualization of its temporal and spatial organization. One popular approach is FROS (fluorescence repressor operator system). This method specifically labels DNA in vivo through binding of a fusion of a fluorescent protein and a repressor protein to an operator array, which contains numerous copies of the repressor binding site integrated into the genomic site of interest. Bound fluorescent proteins are then visible as foci in microscopic analyses and can be distinguished from the background fluorescence caused by unbound fusion proteins. Even though this method is widely used, no attempt has been made so far to decrease the background fluorescence to facilitate analysis of the actual signal of interest. Here, we present a new method that greatly reduces the background signal of FROS. BiFCROS (Bimolecular Fluorescence Complementation and Repressor Operator System) is based on fusions of repressor proteins to halves of a split fluorescent protein. Binding to a hybrid FROS array results in fluorescence signals due to bimolecular fluorescence complementation. Only proteins bound to the hybrid FROS array fluoresce, greatly improving the signal to noise ratio compared to conventional FROS. We present the development of BiFCROS and discuss its potential to be used as a fast and single-cell readout for copy numbers of genetic loci. PMID:28450375

Airborne Remote Earth Sensing (ARES) Program: an operational airborne MWIR imaging spectrometer and applications

NASA Astrophysics Data System (ADS)

Bishop, Kevin D.; Diestel, Michael J.

1996-11-01

Since 1993, the Airborne Remote Earth Sensing (ARES) Program has collected a wide variety of mid-wave infrared hyperspectral data on an interesting assortment of atmospheric, geologic, urban and chemical emission/absorption features. Flown in NASA's high altitude WB-57F aircraft, the ARES sensor is a 75 channel cryo-cooled prism spectrometer covering the 2 - 6 micrometers spectral region, and is capable of up or down-looking measurements over a wide range of collection geometries. Sensor characteristics, pointing capabilities, and overall performance are discussed. Highlights from some of the recent data collections, such as the 1993 and 95 thermal mapping of the active lava flow areas from the Kilauea volcano; the 1993 collection of the direct solar specular reflection off high altitude (ice) cloud layers over West Texas; upper atmospheric H2O vapor sounding using the 6 micrometers solar absorption spectra; Sulfur Dioxide detection from a coal burning power plant in Page, AZ (SO2 in emission) and from the Pu'u O'o vent of the Kilauea volcano (SO2 in absorption); and MWIR imagery from various terrestrial and urban background scenes, including West Los Angeles, and the Capitol area of Washington, D.C. Supporting spectral analysis and radiometric modeling are presented.

The cosmic infrared background experiment (CIBER): instrumentation and first results

NASA Astrophysics Data System (ADS)

Zemcov, M.; Battle, J.; Bock, J.; Cooray, A.; Hristov, V.; Keating, B.; Lee, D. H.; Levenson, L.; Mason, P.; Matsumoto, T.; Matsuura, S.; Nam, U. W.; Renbarger, T.; Sullivan, I.; Tsumura, K.; Wada, T.

2010-07-01

Ultraviolet emission from the first generation of stars in the Universe ionized the intergalactic medium in a process which was completed by z ~ 6; the wavelength of these photons has been redshifted by (1 + z) into the near infrared today and can be measured using instruments situated above the Earth's atmosphere. First flying in February 2009, the Cosmic Infrared Background ExpeRiment (CIBER) comprises four instruments housed in a single reusable sounding rocket borne payload. CIBER will measure spatial anisotropies in the extragalactic IR background caused by cosmological structure from the epoch of reionization using two broadband imaging instruments, make a detailed characterization of the spectral shape of the IR background using a low resolution spectrometer, and measure the absolute brightness of the Zodiacal light foreground with a high resolution spectrometer in each of our six science fields. The scientific motivation for CIBER and details of its first and second flight instrumentation will be discussed. First flight results on the color of the zodiacal light around 1 μm and plans for the future will also be presented.

An Optics Free Spectrometer for the Extreme Ultraviolet

NASA Technical Reports Server (NTRS)

Judge, D. L.; Daybell, M. D.; Hoffman, J. R.; Gruntman, M. A.; Ogawa, H. S.; Samson, J. A. R.

1994-01-01

The optics-free spectrometer is a photon spectrometer. It provides the photon spectrum of a broadband source by converting photons of energy E into electrons of energy E', according to the Einstein relation, E' = E - Ei. E, is the ionization threshold of the gas target of interest (any of the rare gases are suitable) and E is the incoming photon energy. As is evident from the above equation, only a single order spectrum is produced throughout the energy range between the first and second ionization potentials of the rare gas used. Photons with energy above the second ionization potential produce two groups of electrons, but they are readily distinguished from each other. This feature makes this device extremely useful for determining the true spectrum of a continuum source or a many line source. The principle of operation and the laboratory results obtained with a representative configuration of the optics-free spectrometer are presented.

The MARTE VNIR imaging spectrometer experiment: design and analysis.

PubMed

Brown, Adrian J; Sutter, Brad; Dunagan, Stephen

2008-10-01

We report on the design, operation, and data analysis methods employed on the VNIR imaging spectrometer instrument that was part of the Mars Astrobiology Research and Technology Experiment (MARTE). The imaging spectrometer is a hyperspectral scanning pushbroom device sensitive to VNIR wavelengths from 400-1000 nm. During the MARTE project, the spectrometer was deployed to the Río Tinto region of Spain. We analyzed subsets of three cores from Río Tinto using a new band modeling technique. We found most of the MARTE drill cores to contain predominantly goethite, though spatially coherent areas of hematite were identified in Core 23. We also distinguished non Fe-bearing minerals that were subsequently analyzed by X-ray diffraction (XRD) and found to be primarily muscovite. We present drill core maps that include spectra of goethite, hematite, and non Fe-bearing minerals.

The MARTE VNIR Imaging Spectrometer Experiment: Design and Analysis

NASA Astrophysics Data System (ADS)

Brown, Adrian J.; Sutter, Brad; Dunagan, Stephen

2008-10-01

We report on the design, operation, and data analysis methods employed on the VNIR imaging spectrometer instrument that was part of the Mars Astrobiology Research and Technology Experiment (MARTE). The imaging spectrometer is a hyperspectral scanning pushbroom device sensitive to VNIR wavelengths from 400-1000 nm. During the MARTE project, the spectrometer was deployed to the Río Tinto region of Spain. We analyzed subsets of three cores from Río Tinto using a new band modeling technique. We found most of the MARTE drill cores to contain predominantly goethite, though spatially coherent areas of hematite were identified in Core 23. We also distinguished non Fe-bearing minerals that were subsequently analyzed by X-ray diffraction (XRD) and found to be primarily muscovite. We present drill core maps that include spectra of goethite, hematite, and non Fe-bearing minerals.

Time Projection Compton Spectrometer (TPCS). User`s guide

DOE Office of Scientific and Technical Information (OSTI.GOV)

Landron, C.O.; Baldwin, G.T.

1994-04-01

The Time Projection Compton Spectrometer (TPCS) is a radiation diagnostic designed to determine the time-integrated energy spectrum between 100 keV -- 2 MeV of flash x-ray sources. This guide is intended as a reference for the routine operator of the TPCS. Contents include a brief overview of the principle of operation, detailed component descriptions, detailed assembly and disassembly procedures, guide to routine operations, and troubleshooting flowcharts. Detailed principle of operation, signal analysis and spectrum unfold algorithms are beyond the scope of this guide; however, the guide makes reference to sources containing this information.

High-resolution x-ray spectroscopy with the EBIT Calorimeter Spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Porter, F. Scott; Adams, Joseph S.; Kelley, Richard L.

The EBIT Calorimeter Spectrometer (ECS) is a production-class 36 pixel x-ray calorimeter spectrometer that has been continuously operating at the Electron Beam Ion Trap (EBIT) facility at Lawrence Livermore National Laboratory for almost 2 years. The ECS was designed to be a long-lifetime, turn-key spectrometer that couples high performance with ease of operation and minimal operator intervention. To this end, a variant of the Suzaku/XRS spaceflight detector system has been coupled to a low-maintenance cryogenic system consisting of a long-lifetime liquid He cryostat, and a closed cycle, {sup 3}He pre-cooled adiabatic demagnetization refrigerator. The ECS operates for almost 3 weeksmore » between cryogenic servicing and the ADR operates at 0.05 K for more than 60 hours between automatic recycles under software control. Half of the ECS semiconductor detector array is populated with mid-band pixels that have a resolution of 4.5 eV FWHM, a bandpass from 0.05-12 keV, and a quantum efficiency of 95% at 6 keV. The other half of the array has thick HgTe absorbers that have a bandpass from 0.3 to over 100 keV, an energy resolution of 33 eV FWHM, and a quantum efficiency of 32% at 60 keV. In addition, the ECS uses a real-time, autonomous, data collection and analysis system developed for the Suzaku/XRS instrument and implemented in off-the-shelf hardware for the ECS. Here we will discuss the performance of the ECS instrument and its implementation as a turnkey cryogenic detector system.« less

Apollo 17 ultraviolet spectrometer experiment (S-169)

NASA Technical Reports Server (NTRS)

Fastie, W. G.

1974-01-01

The scientific objectives of the ultraviolet spectrometer experiment are discussed, along with design and operational details, instrument preparation and performance, and scientific results. Information gained from the experiment is given concerning the lunar atmosphere and albedo, zodiacal light, astronomical observations, spacecraft environment, and the distribution of atomic hydrogen in the solar system and in the earth's atmosphere.

A compact high-resolution X-ray ion mobility spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Reinecke, T.; Kirk, A. T.; Heptner, A.

For the ionization of gaseous samples, most ion mobility spectrometers employ radioactive ionization sources, e.g., containing {sup 63}Ni or {sup 3}H. Besides legal restrictions, radioactive materials have the disadvantage of a constant radiation with predetermined intensity. In this work, we replaced the {sup 3}H source of our previously described high-resolution ion mobility spectrometer with 75 mm drift tube length with a commercially available X-ray source. It is shown that the current configuration maintains the resolving power of R = 100 which was reported for the original setup containing a {sup 3}H source. The main advantage of an X-ray source ismore » that the intensity of the radiation can be adjusted by varying its operating parameters, i.e., filament current and acceleration voltage. At the expense of reduced resolving power, the sensitivity of the setup can be increased by increasing the activity of the source. Therefore, the performance of the setup can be adjusted to the specific requirements of any application. To investigate the relation between operating parameters of the X-Ray source and the performance of the ion mobility spectrometer, parametric studies of filament current and acceleration voltage are performed and the influence on resolving power, peak height, and noise is analyzed.« less

Performance of a miniature mechanically cooled HPGe gamma-spectrometer for space applications

NASA Astrophysics Data System (ADS)

Kondratjev, V.; Pchelintsev, A.; Jakovlevs, O.; Sokolov, A.; Gostilo, V.; Owens, A.

2018-01-01

We report on the development of a miniaturized HPGe gamma-spectrometer for space applications. The instrument is designed around a 158 cm3 intrinsically pure Ge crystal in the closed-end coaxial configuration, cooled by a Thales RM3 miniature Stirling cycle electric cooler. To compensate the noise induced by the mechanical cooler the digital procession of the spectrometric signals with low frequency reject filter (LFR) is applied. The complete spectrometer assembly has a mass of 3.1 kg and consumes less than 10 W under working operation. The spectrometer was tested under a number of operating conditions in a specially designed chamber, which simulates the space environment. With the mechanical cooler switched off, FWHM energy resolutions of 1.5 keV and 2.2 keV were obtained at 122 keV and 1333 keV, respectively, at the nominal operating temperature of 90 K. When the cooler was switched on the energy resolutions degraded to 2.5 keV and 4 keV respectively. However, with the LFR filter switched in, the resolutions improved significantly to 1.8 keV and 2.4 keV.

Ultra-Sensitive Elemental Analysis Using Plasmas 3.For Understanding an Inductively Coupled Plasma Mass Spectrometer

NASA Astrophysics Data System (ADS)

Sakata, Kenichi

Aplasma-interface is considered the most mysterious part of an inductively coupled plasma mass spectrometer system in terms of understanding its operational mechanism. After a brief explanation of the basic structure of the inductively coupled plasma mass spectrometer and how it works, the plasma-interface is discussed in regard to its complex operation and approaches to investigating its behavior. In particular, the position and shape of the plasma boundary seem to be important to understand the instrument's sensitivity.

Design of a miniaturized integrated spectrometer for spectral tissue sensing

NASA Astrophysics Data System (ADS)

Belay, Gebirie Yizengaw; Hoving, Willem; Ottevaere, Heidi; van der Put, Arthur; Weltjens, Wim; Thienpont, Hugo

2016-04-01

Minimally-invasive image-guided procedures become increasingly used by physicians to obtain real-time characterization feedback from the tissue at the tip of their interventional device (needle, catheter, endoscopic or laparoscopic probes, etc…) which can significantly improve the outcome of diagnosis and treatment, and ultimately reduce cost of the medical treatment. Spectral tissue sensing using compact photonic probes has the potential to be a valuable tool for screening and diagnostic purposes, e.g. for discriminating between healthy and tumorous tissue. However, this technique requires a low-cost broadband miniature spectrometer so that it is commercially viable for screening at point-of-care locations such as physicians' offices and outpatient centers. Our goal is therefore to develop a miniaturized spectrometer based on diffractive optics that combines the functionalities of a visible/near-infrared (VIS/NIR) and shortwave-infrared (SWIR) spectrometer in one very compact housing. A second goal is that the hardware can be produced in high volume at low cost without expensive time consuming alignment and calibration steps. We have designed a miniaturized spectrometer which operates both in the visible/near-infrared and shortwave-infrared wavelength regions ranging from 400 nm to 1700 nm. The visible/near-infrared part of the spectrometer is designed for wavelengths from 400 nm to 800 nm whereas the shortwave-infrared segment ranges from 850 nm to 1700 nm. The spectrometer has a resolution of 6 nm in the visible/near-infrared wavelength region and 10 nm in the shortwave-infrared. The minimum SNR of the spectrometer for the intended application is about 151 in the VIS/NIR range and 6000 for SWIR. In this paper, the modelling and design, and power budget analysis of the miniaturized spectrometer are presented. Our work opens a door for future affordable micro- spectrometers which can be integrated with smartphones and tablets, and used for point

Use of a Fourier transform spectrometer on a balloon-borne telescope and at the multiple mirror telescope (MMT)

NASA Technical Reports Server (NTRS)

Traub, W. A.; Chance, K. V.; Brasunas, J. C.; Vrtilek, J. M.; Carleton, N. P.

1982-01-01

The design and use of an infrared Fourier transform spectrometer which has been used for observations of laboratory, stratospheric, and astronomical spectra are described. The spectrometer has a spectral resolution of 0.032/cm and has operated in the mid-infrared (12 to 13 microns) as well as the far-infrared (40 to 140 microns), using both bolometer and photoconductor cryogenic detectors. The spectrometer is optically sized to accept an f/9 beam from the multi-mirror telescope (MMT). The optical and electronic design are discussed, including remote operation of the spectrometer on a balloon-borne 102-cm telescope. The performance of the laser-controlled, screw-driven moving cat's-eye mirror is discussed. Segments of typical far-infrared balloon flight spectra, lab spectra, and mid-infrared MMT spectra are presented. Data reduction, interferogram processing, artifact removal, wavelength calibration, and intensity calibration methods are discussed. Future use of the spectrometer is outlined.

A retarding ion mass spectrometer for the Dynamics Explorer-1

NASA Technical Reports Server (NTRS)

Wright, W.

1985-01-01

The Retarding Ion Mass Spectrometer (RIMS) for Dynamics Explorer-1 is an instrument designed to measure the details of the thermal plasma distribution. It combines the ion temperature determining capability of the retarding potential analyzer with the compositional capabilities of the mass spectrometer and adds multiple sensor heads to sample all directions relative to the spacecraft ram direction. This manual provides a functional description of the RIMS, the instrument calibration, and a description of the commands which can be stored in the instrument logic to control its operation.

Miniature high-resolution guided-wave spectrometer for atmospheric remote sensing

NASA Astrophysics Data System (ADS)

Sloan, James; Kruzelecky, Roman; Wong, Brian; Zou, Jing; Jamroz, Wes; Haddad, Emile; Poirier, Michel

This paper describes the design and application of an innovative spectrometer in which a guided-wave integrated optical spectrometer (IOSPEC) has been coupled with a Fabry-Perot (FP) interferometer. This miniature spectrometer has a net mass under 3 kg, but is capable of broadband operation at spectral resolutions below 0.03 nm full width half maximum (FWHM). The tuneable FP filter provides very high spectral resolution combined with a large input aper-ture. The solid state guided-wave spectrometer is currently configured for a 512-channel array detector, which provides sub-nm coarse resolution. The ultimate resolution is determined by the FP filter, which is tuned across the desired spectral bands, thereby providing a signal-to-noise ratio (SNR) advantage over scanned spectrometer systems of the square root of the number of detector channels. The guided-wave optics provides robust, long-term optical alignment, while minimising the mechanical complexity. The miniaturisation of the FP-IOSPEC spectrometer allows multiple spectrometers to be accommodated on a single MicroSat. Each of these can be optimised for selected measurement tasks and views, thereby enabling more flexible data acquisition strategies with enhanced information content, while minimizing the mission cost. The application of this innovative technology in the proposed Miniature Earth Observation Satellite (MEOS) mission will also be discussed. The MEOS mission, which is designed for the investigation of the carbon and water cycles, relies on multiple IO-SPEC instruments for the simultaneous measurement of a range of atmospheric and surface properties important to climate change.

Tropospheric Emission Spectrometer for the Earth Observing System

NASA Technical Reports Server (NTRS)

Glavich, Thomas A.; Beer, Reinhard

1991-01-01

A Tropospheric Emission Spectrometer (TES) for the Earth Observing System (EOS) series of polar-orbiting platforms is described. TES is aimed at studying tropospheric chemistry, in particular, the exchange of gases between the surface and the atmosphere, urban and regional pollution, acid rain precursors, sources and sinks of greenhouse gases, and the interchange of gases between the troposphere and the stratosphere. TES is a high-resolution (0.025/cm) infrared Fourier transform spectrometer operating in the passive thermal-emission mode in a very wide spectral range (600 to 4350/cm; 2.3 to 16.7 microns). TES has 32 spatial pixels in each of four optically conjugated linear detector arrays, each optimized for a different spectral region.

Bulk and integrated acousto-optic spectrometers for molecular astronomy with heterodyne spectrometers

NASA Technical Reports Server (NTRS)

Chin, G.; Buhl, D.; Florez, J. M.

1981-01-01

A survey of acousto-optic spectrometers for molecular astronomy is presented, noting a technique of combining the acoustic bending of a collimated coherent light beam with a Bragg cell followed by an array of sensitive photodetectors. This acousto-optic spectrometer has a large bandwidth, a large number of channels, high resolution, and is energy efficient. Receiver development has concentrated on high-frequency heterodyne systems for the study of the chemical composition of the interstellar medium. RF spectrometers employing acousto-optic diffraction cells are described. Acousto-optic techniques have been suggested for applications to electronic warfare, electronic countermeasures and electronic support systems. Plans to use integrated optics for the further miniaturization of acousto-optic spectrometers are described. Bulk acousto-optic spectrometers with 300 MHz and 1 GHz bandwidths are being developed for use in the back-end of high-frequency heterodyne receivers for astronomical research.

Thermal analyses for initial operations of the soft x-ray spectrometer onboard the Hitomi satellite

NASA Astrophysics Data System (ADS)

Noda, Hirofumi; Mitsuda, Kazuhisa; Okamoto, Atsushi; Ezoe, Yuichiro; Ishikawa, Kumi; Fujimoto, Ryuichi; Yamasaki, Noriko; Takei, Yoh; Ohashi, Takaya; Ishisaki, Yoshitaka; Mitsuishi, Ikuyuki; Yoshida, Seiji; DiPirro, Michel; Shirron, Peter

2018-01-01

The soft x-ray spectrometer (SXS) onboard the Hitomi satellite achieved a high-energy resolution of ˜4.9 eV at 6 keV with an x-ray microcalorimeter array cooled to 50 mK. The cooling system utilizes liquid helium, confined in zero gravity by means of a porous plug (PP) phase separator. For the PP to function, the helium temperature must be kept lower than the λ point of 2.17 K in orbit. To determine the maximum allowable helium temperature at launch, taking into account the uncertainties in both the final ground operations and initial operation in orbit, we constructed a thermal mathematical model of the SXS dewar and PP vent and carried out time-series thermal simulations. Based on the results, the maximum allowable helium temperature at launch was set at 1.7 K. We also conducted a transient thermal calculation using the actual temperatures at launch as initial conditions to determine flow and cooling rates in orbit. From this, the equilibrium helium mass flow rate was estimated to be ˜34 to 42 μg/s, and the lifetime of the helium mode was predicted to be ˜3.9 to 4.7 years. This paper describes the thermal model and presents simulation results and comparisons with temperatures measured in the orbit.

A photoacoustic spectrometer for trace gas detection

NASA Astrophysics Data System (ADS)

Telles, E. M.; Bezerra, E.; Scalabrin, A.

2005-06-01

A high-resolution external laser photoacoustic spectrometer has been developed for trace gas detection with absorption transitions in coincidence with CO2 laser emission lines (9,2-10,9 μm: 920-1086 cm-1). The CO2 laser operates in 90 CW lines with power of up to 15 W. A PC-controlled step motor can tune the laser lines. The resonance frequency of first longitudinal mode of the photoacoustic cell is at 1600 Hz. The cell Q-factor and cell constant are measured close to 50 and 28 mVcmW-1, respectively. The spectrometer has been tested in preliminary studies to analyze the absorption transitions of ozone (O_3). The ethylene (C_2H_4) from papaya fruit is also investigated using N2 as carrier gas at a constant flow rate.

Berkeley extreme-ultraviolet airglow rocket spectrometer - BEARS

NASA Technical Reports Server (NTRS)

Cotton, D. M.; Chakrabarti, S.

1992-01-01

The Berkeley EUV airglow rocket spectrometer (BEARS) instrument is described. The instrument was designed in particular to measure the dominant lines of atomic oxygen in the FUV and EUV dayglow at 1356, 1304, 1027, and 989 A, which is the ultimate source of airglow emissions. The optical and mechanical design of the instrument, the detector, electronics, calibration, flight operations, and results are examined.

Gas Chromatic Mass Spectrometer

NASA Technical Reports Server (NTRS)

Wey, Chowen

1995-01-01

Gas chromatograph/mass spectrometer (GC/MS) used to measure and identify combustion species present in trace concentration. Advanced extractive diagnostic method measures to parts per billion (PPB), as well as differentiates between different types of hydrocarbons. Applicable for petrochemical, waste incinerator, diesel transporation, and electric utility companies in accurately monitoring types of hydrocarbon emissions generated by fuel combustion, in order to meet stricter environmental requirements. Other potential applications include manufacturing processes requiring precise detection of toxic gaseous chemicals, biomedical applications requiring precise identification of accumulative gaseous species, and gas utility operations requiring high-sensitivity leak detection.

Compact Infrared Spectrometers

NASA Technical Reports Server (NTRS)

Mouroulis, Pantazis

2009-01-01

Concentric spectrometer forms are advantageous for constructing a variety of systems spanning the entire visible to infrared range. Spectrometer examples are given, including broadband or high resolution forms. Some issues associated with the Dyson catadioptric type are also discussed.

Detection of fatty product falsifications using a portable near infrared spectrometer

NASA Astrophysics Data System (ADS)

Kalinin, A. V.; Krasheninnikov, V. N.

2017-01-01

Spreading sales of counterfeited fatty-oil foods leads to a development of portable and operational analyzer of typical fatty acids (FA) which may be a near infrared (NIR) spectrometer. In this work the calibration models for prediction of named FA were built with the spectra of FT-NIR spectrometer for different absorption bands of the FA. The best parameters were obtained for the wavelength sub-band 1.0-1.8 μ, which includes the 2nd and 3rd overtones of C-H stretching vibrations (near 1.7 and 1.2 μ) and the combination band (1.42 μ). Applicability of the portable spectrometer based on linear NIR array photosensor for the quality analysis of spread, butter and fish oil by the typical FA has been tested.

Biogeological Analysis of Desert Varnish Using Portable Raman Spectrometers.

PubMed

Malherbe, Cedric; Ingley, Richard; Hutchinson, Ian; Edwards, Howell; Carr, Andrew S; Harris, Liam; Boom, Arnoud

2015-06-01

Desert varnishes are thin, dark mineral coatings found on some rocks in arid or semi-arid environments on Earth. Microorganisms may play an active role in their formation, which takes many hundreds of years. Their mineral matrix may facilitate the preservation of organic matter and is therefore of great relevance to martian exploration. Miniaturized Raman spectrometers (which allow nondestructive analysis of the molecular composition of a specimen) will equip rovers in forthcoming planetary exploration missions. In that context, and for the first time, portable Raman spectrometers operating in the green visible (532 nm as currently baselined for flight) and in the near-infrared (785 nm) were used in this study to investigate the composition (and substrate) of several samples of desert varnish. Rock samples that were suspected (and later confirmed) to be coated with desert varnish were recovered from two sites in the Mojave Desert, USA. The portable spectrometers were operated in flight-representative acquisition modes to identify the key molecular components of the varnish. The results demonstrate that the coatings typically comprise silicate minerals such as quartz, plagioclase feldspars, clays, ferric oxides, and hydroxides and that successful characterization of the samples can be achieved by using flightlike portable spectrometers for both the 532 and 785 nm excitation sources. In the context of searching for spectral signatures and identifying molecules that indicate the presence of extant and/or extinct life, we also report the detection of β-carotene in some of the samples. Analysis complications caused by the presence of rare earth element photoluminescence (which overlaps with and overwhelms the organic Raman signal when a 785 nm laser is employed) are also discussed.

On-Orbit Operation of the Adiabatic Demagnetization Refrigerator on the Astro-H/Hitomi Soft X-ray Spectrometer Instrument

NASA Technical Reports Server (NTRS)

Shirron, Peter; Kimball, Mark; James, Bryan; Muench, Theodore; Canavan, Edgar; DiPirro, Michael; Bialas, Thomas; Sneiderman, Gary; Boyce, Kevin; Kilbourne, Caroline;

Design and on-orbit operation of the adiabatic demagnetization refrigerator on the Hitomi Soft X-ray Spectrometer instrument

NASA Astrophysics Data System (ADS)

Shirron, Peter J.; Kimball, Mark O.; James, Bryan L.; Muench, Theodore; Canavan, Edgar R.; DiPirro, Michael J.; Bialas, Thomas G.; Sneiderman, Gary A.; Boyce, Kevin R.; Kilbourne, Caroline A.; Porter, Frederick S.; Kelley, Richard L.; Fujimoto, Ryuichi; Takei, Yoh; Yoshida, Seiji; Mitsuda, Kazuhisa

2016-07-01

The Soft X-ray Spectrometer instrument on the Astro-H observatory contains a 6x6 array of x-ray microcalorimeters, which is cooled to 50 mK by an adiabatic demagnetization refrigerator (ADR). The ADR consists of three stages in order to provide stable detector cooling using either a 1.2 K superfluid helium bath or a 4.5 K Joule-Thomson (JT) cryocooler as its heat sink. When liquid helium is present, two of the ADR's stages are used to single-shot cool the detectors while rejecting heat to the helium. After the helium is depleted, all three stages are used to cool both the helium tank (to about 1.5 K) and the detectors (to 50 mK) using the JT cryocooler as its heat sink. The Astro-H observatory, renamed Hitomi after its successful launch in February 2016, carried approximately 36 liters of helium into orbit. On day 5, the helium had cooled sufficiently (<1.4 K) to allow operation of the ADR. This paper describes the design, operation and on-orbit performance of the ADR.

A Virtual Research Environment for a Secondary Ion Mass Spectrometer (SIMS)

NASA Astrophysics Data System (ADS)

Wiedenbeck, M.; Schäfer, L.; Klump, J.; Galkin, A.

2013-12-01

Overview: This poster describes the development of a Virtual Research Environment for the Secondary Ion Mass Spectrometer (SIMS) at GFZ Potsdam. Background: Secondary Ion Mass Spectrometers (SIMS) are extremely sensitive instruments for analyzing the surfaces of solid and thin film samples. These instruments are rare, expensive and experienced operators are very highly sought after. As such, measurement time is a precious commodity, until now only accessible to small numbers of researchers. The challenge: The Virtual SIMS Project aims to set up a Virtual Research Environment for the operation of the CAMECA IMS 1280-HR instrument at the GFZ Potsdam. The objective of the VRE is to provide SIMS access not only to researchers locally present in Potsdam but also to scientists working with SIMS cooperation partners in e.g., South Africa, Brazil or India. The requirements: The system should address the complete spectrum of laboratory procedures - from online application for measurement time, to remote access for data acquisition to data archiving for the subsequent publication and for future reuse. The approach: The targeted Virtual SIMS Environment will consist of a: 1. Web Server running the Virtual SIMS website providing general information about the project, lab access proposal forms and calendar for the timing of project related tasks. 2. LIMS Server, responsible for scheduling procedures, data management and, if applicable, accounting and billing. 3. Remote SIMS Tool, devoted to the operation of the experiment within a remote control environment. 4. Publishing System, which supports the publication of results in cooperation with the GFZ Library services. 5. Training Simulator, which offers the opportunity to rehearse experiments and to prepare for possible events such as a power outages or interruptions to broadband services. First results: The SIMS Virtual Research Environment will be mainly based on open source software, the only exception being the CAMECA IMS

Multi-Grid detector for neutron spectroscopy: results obtained on time-of-flight spectrometer CNCS

NASA Astrophysics Data System (ADS)

Anastasopoulos, M.; Bebb, R.; Berry, K.; Birch, J.; Bryś, T.; Buffet, J.-C.; Clergeau, J.-F.; Deen, P. P.; Ehlers, G.; van Esch, P.; Everett, S. M.; Guerard, B.; Hall-Wilton, R.; Herwig, K.; Hultman, L.; Höglund, C.; Iruretagoiena, I.; Issa, F.; Jensen, J.; Khaplanov, A.; Kirstein, O.; Lopez Higuera, I.; Piscitelli, F.; Robinson, L.; Schmidt, S.; Stefanescu, I.

2017-04-01

The Multi-Grid detector technology has evolved from the proof-of-principle and characterisation stages. Here we report on the performance of the Multi-Grid detector, the MG.CNCS prototype, which has been installed and tested at the Cold Neutron Chopper Spectrometer, CNCS at SNS. This has allowed a side-by-side comparison to the performance of 3He detectors on an operational instrument. The demonstrator has an active area of 0.2 m2. It is specifically tailored to the specifications of CNCS. The detector was installed in June 2016 and has operated since then, collecting neutron scattering data in parallel to the He-3 detectors of CNCS. In this paper, we present a comprehensive analysis of this data, in particular on instrument energy resolution, rate capability, background and relative efficiency. Stability, gamma-ray and fast neutron sensitivity have also been investigated. The effect of scattering in the detector components has been measured and provides input to comparison for Monte Carlo simulations. All data is presented in comparison to that measured by the 3He detectors simultaneously, showing that all features recorded by one detector are also recorded by the other. The energy resolution matches closely. We find that the Multi-Grid is able to match the data collected by 3He, and see an indication of a considerable advantage in the count rate capability. Based on these results, we are confident that the Multi-Grid detector will be capable of producing high quality scientific data on chopper spectrometers utilising the unprecedented neutron flux of the ESS.

Electron source for a mini ion trap mass spectrometer

DOEpatents

Dietrich, D.D.; Keville, R.F.

1995-12-19

An ion trap is described which operates in the regime between research ion traps which can detect ions with a mass resolution of better than 1:10{sup 9} and commercial mass spectrometers requiring 10{sup 4} ions with resolutions of a few hundred. The power consumption is kept to a minimum by the use of permanent magnets and a novel electron gun design. By Fourier analyzing the ion cyclotron resonance signals induced in the trap electrodes, a complete mass spectra in a single combined structure can be detected. An attribute of the ion trap mass spectrometer is that overall system size is drastically reduced due to combining a unique electron source and mass analyzer/detector in a single device. This enables portable low power mass spectrometers for the detection of environmental pollutants or illicit substances, as well as sensors for on board diagnostics to monitor engine performance or for active feedback in any process involving exhausting waste products. 10 figs.

Electron source for a mini ion trap mass spectrometer

DOEpatents

Dietrich, Daniel D.; Keville, Robert F.

1995-01-01

An ion trap which operates in the regime between research ion traps which can detect ions with a mass resolution of better than 1:10.sup.9 and commercial mass spectrometers requiring 10.sup.4 ions with resolutions of a few hundred. The power consumption is kept to a minimum by the use of permanent magnets and a novel electron gun design. By Fourier analyzing the ion cyclotron resonance signals induced in the trap electrodes, a complete mass spectra in a single combined structure can be detected. An attribute of the ion trap mass spectrometer is that overall system size is drastically reduced due to combining a unique electron source and mass analyzer/detector in a single device. This enables portable low power mass spectrometers for the detection of environmental pollutants or illicit substances, as well as sensors for on board diagnostics to monitor engine performance or for active feedback in any process involving exhausting waste products.

System design and simulation of a long-wave infrared hyperspectral imaging spectrometer

NASA Astrophysics Data System (ADS)

Yuan, Li-yin; Xu, Wei-ming; He, Zhi-ping; Lin, Ying; Shu, Rong; Wang, Jian-yu

2009-07-01

A ground-based long-wave hyperspectral imaging spectrometer (LWHIS) is designed and simulated. The spectrometer is based on a focal plane array detector with a spectral response that covers the range 7700 to 9300 nm. Optical system of this instrument is all-reflective and provides up to 30 continuous spectral channels with 54 nm of dispersion per pixel. The entrance aperture is 20 mm and feeds an F/2 telescope front end. The telescope has a 11-deg field of view with 256 spatially resolved elements (detector pixel size is 30 μm). To get high enough signal noise rate (SNR), no concern about the electronic part, first, the cool stop of the detector is used as soon as possible, and second, background thermal radiance of the opto-mechanical system seen by the focal plane must be suppressed. Thus, the entire instrument is set in a vacuum chamber and the opto-mechanical subsystem is cooled by liquid nitrogen. The background thermal radiance verse different cases is discussed. Based on the radiation simulation and analysis, if the opto-mechanical subsystem of the spectrometer within the vacuum chamber is cooled blew 100 Kelvin, significant performance gains can be realized. The design and simulation provides an example for illustrating the design principles specific and radiation simulation to this type of system.

Operation of the “Small” BioAMS spectrometers at CAMS: Past and future prospects

DOE PAGES

Ognibene, T. J.; Haack, K. W.; Bench, G.; ...

2015-05-26

A summary of results from the solid samples run on our compact 1 MV AMS system over its 13.5 years of operation is presented. On average 7065 samples per year were measured with that average dropping to 3278 samples per year following the deployment of our liquid sample capability. Although the dynamic range of our spectrometer is 4.5 orders in magnitude, most of the measured graphitic samples had 14C/C concentrations between 0.1 and 1 modern. Furthermore, the measurements of our ANU sucrose standard followed a Gaussian distribution with an average of 1.5082 ± 0.0134 modern. The LLNL biomedical AMS programmore » supported many different types of experiments, however, the large majority of samples measured were derived from animal model systems. We have transitioned all of our biomedical AMS measurements to the recently installed 250 kV SSAMS instrument with good agreement compared in measured 14C/C isotopic ratios between sample splits. We then present results from replacement of argon stripping gas with helium in the SSAMS with a 22% improvement in ion transmission through the accelerator and high-energy analyzing magnet.« less

Operation of the “Small” BioAMS Spectrometers at CAMS: Past and Future Prospects

PubMed Central

Ognibene, T.J.; Haack, K.W.; Bench, G.; Brown, T.A.; Turteltaub, K.W.

2015-01-01

A summary of results from the solid samples run on our compact 1 MV AMS system over its 13.5 years of operation is presented. On average 7065 samples per year were measured with that average dropping to 3278 samples per year following the deployment of our liquid sample capability. Although the dynamic range of our spectrometer is 4.5 orders in magnitude, most of the measured graphitic samples had 14C/C concentrations between 0.1 and 1 modern. The measurements of our ANU sucrose standard followed a Gaussian distribution with an average of 1.5082 ± 0.0134 modern. The LLNL biomedical AMS program supported many different types of experiments, however, the large majority of samples measured were derived from animal model systems. We have transitioned all of our biomedical AMS measurements to the recently installed 250 kV SSAMS instrument with good agreement compared in measured 14C/C isotopic ratios between sample splits. Finally, we present results from replacement of argon stripping gas with helium in the SSAMS with a 22% improvement in ion transmission through the accelerator and high-energy analyzing magnet. PMID:26456990

Miniaturized time-resolved Raman spectrometer for planetary science based on a fast single photon avalanche diode detector array.

PubMed

Blacksberg, Jordana; Alerstam, Erik; Maruyama, Yuki; Cochrane, Corey J; Rossman, George R

2016-02-01

We present recent developments in time-resolved Raman spectroscopy instrumentation and measurement techniques for in situ planetary surface exploration, leading to improved performance and identification of minerals and organics. The time-resolved Raman spectrometer uses a 532 nm pulsed microchip laser source synchronized with a single photon avalanche diode array to achieve sub-nanosecond time resolution. This instrument can detect Raman spectral signatures from a wide variety of minerals and organics relevant to planetary science while eliminating pervasive background interference caused by fluorescence. We present an overview of the instrument design and operation and demonstrate high signal-to-noise ratio Raman spectra for several relevant samples of sulfates, clays, and polycyclic aromatic hydrocarbons. Finally, we present an instrument design suitable for operation on a rover or lander and discuss future directions that promise great advancement in capability.

Low-Pressure, Field-Ionizing Mass Spectrometer

NASA Technical Reports Server (NTRS)

Hartley, Frank; Smith, Steven

2009-01-01

A small mass spectrometer utilizing a miniature field ionization source is now undergoing development. It is designed for use in a variety of applications in which there are requirements for a lightweight, low-power-consumption instrument that can analyze the masses of a wide variety of molecules and ions. The device can operate without need for a high-vacuum, carrier-gas feed radioactive ionizing source, or thermal ionizer. This mass spectrometer can operate either in the natural vacuum of outer space or on Earth at any ambient pressure below 50 torr (below about 6.7 kPa) - a partial vacuum that can easily be reached by use of a small sampling pump. This mass spectrometer also has a large dynamic range - from singly charged small gas ions to deoxyribonucleic acid (DNA) fragments larger than 104 atomic mass units - with sensitivity adequate for detecting some molecules and ions at relative abundances of less than one part per billion. This instrument (see figure) includes a field ionizer integrated with a rotating-field mass spectrometer (RFMS). The field ionizer effects ionization of a type characterized as "soft" in the art because it does not fragment molecules or initiate avalanche arcing. What makes the "soft" ionization mode possible is that the distance between the ionizing electrodes is less than mean free path for ions at the maximum anticipated operating pressure, so that the ionizer always operates on the non-breakdown side of the applicable Paschen curve (a standard plot of breakdown potential on the ordinate and pressure electrode separation on the abscissa). The field ionizer in this instrument is fabricated by micromachining a submicron-thick membrane out of an electrically nonconductive substrate, coating the membrane on both sides to form electrodes, then micromachining small holes through the electrodes and membrane. Because of the submicron electrode separation, even a potential of only 1 V applied between the electrodes gives rise to an electric

Ion Mobility Spectrometer Field Test

DOE Office of Scientific and Technical Information (OSTI.GOV)

Smith, Nicholas; McLain, Derek; Steeb, Jennifer

The Morpho Saffran Itemizer 4DX Ion Mobility Spectrometer previously used to detect uranium signatures in FY16 was used at the former New Brunswick Facility, a past uranium facility located on site at Argonne National Laboratory. This facility was chosen in an attempt to detect safeguards relevant signatures and has a history of processing uranium at various enrichments, chemical forms, and purities; various chemicals such as nitric acid, uranium fluorides, phosphates and metals are present at various levels. Several laboratories were sampled for signatures of nuclear activities around the laboratory. All of the surfaces that were surveyed were below background levelsmore » of the radioanalytical instrumentation and determined to be radiologically clean.« less

The retarding ion mass spectrometer on dynamics Explorer-A. [measuring thermal plasma distribution

NASA Technical Reports Server (NTRS)

Chappell, C. R.; Fields, S. A.; Baugher, C. R.; Hoffman, J. H.; Hanson, W. B.; Wright, W. W.; Hammack, H. D.; Carignan, G. R.; Nagy, A. F.

1981-01-01

An instrument designed to measure the details of the thermal plasma distribution combines the ion temperature-determining capability of the retarding potential analyzer with the compositional capabilities of the mass spectrometer and adds multiple sensor heads to sample all directions relative to the spacecraft ram directions. The retarding ion mass spectrometer, its operational modes and calibration are described as well as the data reduction plan, and the anticipated results.

First high-statistics and high-resolution recoil-ion data from the WITCH retardation spectrometer

NASA Astrophysics Data System (ADS)

Finlay, P.; Breitenfeldt, M.; Porobić, T.; Wursten, E.; Ban, G.; Beck, M.; Couratin, C.; Fabian, X.; Fléchard, X.; Friedag, P.; Glück, F.; Herlert, A.; Knecht, A.; Kozlov, V. Y.; Liénard, E.; Soti, G.; Tandecki, M.; Traykov, E.; Van Gorp, S.; Weinheimer, Ch.; Zákoucký, D.; Severijns, N.

2016-07-01

The first high-statistics and high-resolution data set for the integrated recoil-ion energy spectrum following the β^+ decay of 35Ar has been collected with the WITCH retardation spectrometer located at CERN-ISOLDE. Over 25 million recoil-ion events were recorded on a large-area multichannel plate (MCP) detector with a time-stamp precision of 2ns and position resolution of 0.1mm due to the newly upgraded data acquisition based on the LPC Caen FASTER protocol. The number of recoil ions was measured for more than 15 different settings of the retardation potential, complemented by dedicated background and half-life measurements. Previously unidentified systematic effects, including an energy-dependent efficiency of the main MCP and a radiation-induced time-dependent background, have been identified and incorporated into the analysis. However, further understanding and treatment of the radiation-induced background requires additional dedicated measurements and remains the current limiting factor in extracting a beta-neutrino angular correlation coefficient for 35Ar decay using the WITCH spectrometer.

In-Flight Performance of the Soft X-Ray Spectrometer Detector System on ASTRO-H

NASA Technical Reports Server (NTRS)

Porter, Frederick S.; Boyce, Kevin R.; Chiao, Meng P.; Eckart, Megan E.; Fujimoto, Ryuichi; Ishisaki, Yoshitaka; Kelley, Richard L.; Kilbourne, Carolina A.; Leutenegger, Maurice A.; McCammon, Dan;

In-flight performance of the soft x-ray spectrometer detector system on Astro-H

NASA Astrophysics Data System (ADS)

Porter, Frederick S.; Boyce, Kevin R.; Chiao, Meng P.; Eckart, Megan E.; Fujimoto, Ryuichi; Ishisaki, Yoshitaka; Kilbourne, Caroline Anne; Leutenegger, Maurice A.; McCammon, Daniel; Mitsuda, Kazuhisa; Sato, Kosuke; Seta, Hiromi; Sawada, Makoto; Sneiderman, Gary A.; Szymkowiak, Andrew E.; Takei, Yoh; Tashiro, Makoto S.; Tsujimoto, Masahiro; Watanabe, Tomomi; Yamada, Shinya

2018-01-01

The soft x-ray spectrometer (SXS) instrument was launched aboard the Astro-H (Hitomi) observatory on February 17, 2016. The SXS is based on a high-sensitivity x-ray calorimeter detector system that has been successfully deployed in many ground and suborbital spectrometers. The instrument was to provide essential diagnostics for nearly every class of x-ray emitting objects from the atmosphere of Jupiter to the outskirts of galaxy clusters, without degradation for spatially extended objects. The SXS detector system consisted of a 36-pixel cryogenic microcalorimeter array operated at a heat sink temperature of 50 mK. In preflight testing, the detector system demonstrated a resolving power of better than 1300 at 6 keV with a simultaneous bandpass from below 0.3 keV to above 12 keV with a timing precision better than 100 μs. In addition, a solid-state anticoincidence detector was placed directly behind the detector array for background suppression. The detector error budget included the measured interference from the SXS cooling system and the spacecraft. Additional margin for on-orbit gain stability and on-orbit spacecraft interference were also included predicting an on-orbit performance that meets or exceeds the 7-eV FWHM at 6-keV requirement. The actual on-orbit spectral resolution was better than 5 eV FWHM at 6 keV, easily satisfying the instrument requirement. Here, we discuss the actual on-orbit performance of the SXS detector system and compare this to performance in preflight testing and the on-orbit predictions. We will also discuss the on-orbit gain stability, additional on-orbit interference, and measurements of the on-orbit background.

Field observations using an AOTF polarimetric imaging spectrometer

NASA Technical Reports Server (NTRS)

Cheng, Li-Jen; Hamilton, Mike; Mahoney, Colin; Reyes, George

1993-01-01

This paper reports preliminary results of recent field observations using a prototype acousto-optic tunable filter (AOTF) polarimetric imaging spectrometer. The data illustrate application potentials for geoscience. The operation principle of this instrument is different from that of current airborne multispectral imaging instruments, such as AVIRIS. The AOTF instrument takes two orthogonally polarized images at a desired wavelength at one time, whereas AVIRIS takes a spectrum over a predetermined wavelength range at one pixel at a time and the image is constructed later. AVIRIS does not have any polarization measuring capability. The AOTF instrument could be a complement tool to AVIRIS. Polarization measurement is a desired capability for many applications in remote sensing. It is well know that natural light is often polarized due to various scattering phenomena in the atmosphere. Also, scattered light from canopies is reported to have a polarized component. To characterize objects of interest correctly requires a remote sensing imaging spectrometer capable of measuring object signal and background radiation in both intensity and polarization so that the characteristics of the object can be determined. The AORF instrument has the capability to do so. The AOTF instrument has other unique properties. For example, it can provide spectral images immediately after the observation. The instrument can also allow observations to be tailored in real time to perform the desired experiments and to collect only required data. Consequently, the performance in each mission can be increased with minimal resources. The prototype instrument was completed in the beginning of this year. A number of outdoor field experiments were performed with the objective to evaluate the capability of this new technology for remote sensing applications and to determine issues for further improvements.

Note: A flexible light emitting diode-based broadband transient-absorption spectrometer

NASA Astrophysics Data System (ADS)

Gottlieb, Sean M.; Corley, Scott C.; Madsen, Dorte; Larsen, Delmar S.

2012-05-01

This Note presents a simple and flexible ns-to-ms transient absorption spectrometer based on pulsed light emitting diode (LED) technology that can be incorporated into existing ultrafast transient absorption spectrometers or operate as a stand-alone instrument with fixed-wavelength laser sources. The LED probe pulses from this instrument exhibit excellent stability (˜0.5%) and are capable of producing high signal-to-noise long-time (>100 ns) transient absorption signals either in a broadband multiplexed (spanning 250 nm) or in tunable narrowband (20 ns) operation. The utility of the instrument is demonstrated by measuring the photoinduced ns-to-ms photodynamics of the red/green absorbing fourth GMP phosphodiesterase/adenylyl cyclase/FhlA domain of the NpR6012 locus of the nitrogen-fixing cyanobacterium Nostoc punctiforme.

Portable neutron spectrometer and dosimeter

DOEpatents

Waechter, D.A.; Erkkila, B.H.; Vasilik, D.G.

The disclosure relates to a battery operated neutron spectrometer/dosimeter utilizing a microprocessor, a built-in tissue equivalent LET neutron detector, and a 128-channel pulse height analyzer with integral liquid crystal display. The apparatus calculates doses and dose rates from neutrons incident on the detector and displays a spectrum of rad or rem as a function of keV per micron of equivalent tissue and also calculates and displays accumulated dose in millirads and millirem as well as neutron dose rates in millirads per hour and millirem per hour.

Portable neutron spectrometer and dosimeter

DOEpatents

Waechter, David A.; Erkkila, Bruce H.; Vasilik, Dennis G.

1985-01-01

The disclosure relates to a battery operated neutron spectrometer/dosimeter utilizing a microprocessor, a built-in tissue equivalent LET neutron detector, and a 128-channel pulse height analyzer with integral liquid crystal display. The apparatus calculates doses and dose rates from neutrons incident on the detector and displays a spectrum of rad or rem as a function of keV per micron of equivalent tissue and also calculates and displays accumulated dose in millirads and millirem as well as neutron dose rates in millirads per hour and millirem per hour.

Micro-optical-mechanical system photoacoustic spectrometer

DOEpatents

Kotovsky, Jack; Benett, William J.; Tooker, Angela C.; Alameda, Jennifer B.

2013-01-01

All-optical photoacoustic spectrometer sensing systems (PASS system) and methods include all the hardware needed to analyze the presence of a large variety of materials (solid, liquid and gas). Some of the all-optical PASS systems require only two optical-fibers to communicate with the opto-electronic power and readout systems that exist outside of the material environment. Methods for improving the signal-to-noise are provided and enable mirco-scale systems and methods for operating such systems.

Balloon Borne Ultraviolet Spectrometer.

DTIC Science & Technology

1978-12-28

n.c.aaary ond lden lfy by block numb.r) ultraviolet ground support equipment (GSE) spectrometers flight electronics instrumentation balloons \\ solar ...Assembly 4 Fig. 3 Solar Balloon Experiment Ass ’y 7 Fig. 4 Mechanical Interface , UV Spectrometer 8 Fig . 5 Spectrometer Body Assemb ly 10 Fig. 6...Diagram, GSE )bnitor 48 Selector and Battery Charger Fig. 25 Schematic Diagram, GSE Serial to 49 Parallel Data Converter Fig. 26 Schematic Diagram

Application of an atmospheric pressure sampling mass spectrometer to chlorination reactions

NASA Technical Reports Server (NTRS)

Jacobson, N. S.

1986-01-01

An atmospheric pressure mass spectrometric sampling system, based on a free jet expansion was used to study certain M-Cl-O reactions at high temperatures. The apparatus enables the volatile species from a 1-atm chemical process to be directly identified with a mass spectrometer which operates at approx. 10 to the minus 8th power torr. Studies for both pure metals and alloys are discussed. It is shown that this mass spectrometer system aids in identifying the volatile species, and provides fundamental information on the reaction mechanism.

Deep Atmosphere Ammonia Mixing Ratio at Jupiter from the Galileo Probe Mass Spectrometer

NASA Technical Reports Server (NTRS)

Mahaffy, P. R.; Niemann, H. B.; Demick, J. E.

1999-01-01

New laboratory studies employing the Engineering Unit (EU) of the Galileo Probe Mass Spectrometer (GPMS) have resulted in a substantial reduction in the previously reported upper limit on the ammonia mixing ratio derived from the GPMS experiment at Jupiter. This measurement is complicated by background ammonia contributions in the GPMS during direct atmospheric sampling produced from the preceding gas enrichment experiments. These backgrounds can be quantified with the data from the EU studies when they are carried out in a manner that duplicates the descent profile of pressure and enrichment cell loading. This background is due to the tendency of ammonia to interact strongly with the walls of the mass spectrometer and on release to contribute to the gas being directly directed into the ion source from the atmosphere through a capillary pressure reduction leak. It is evident from the GPMS and other observations that the mixing ratio of ammonia at Jupiter reaches the deep atmosphere value at substantially higher pressures than previously assumed. This is a likely explanation for the previously perceived discrepancy between ammonia values derived from ground based microwave observations and those obtained from attenuation of the Galileo Probe radio signal.

Environmental radionuclides as contaminants of HPGe gamma-ray spectrometers: Monte Carlo simulations for Modane underground laboratory.

PubMed

Breier, R; Brudanin, V B; Loaiza, P; Piquemal, F; Povinec, P P; Rukhadze, E; Rukhadze, N; Štekl, I

2018-05-21

The main limitation in the high-sensitive HPGe gamma-ray spectrometry has been the detector background, even for detectors placed deep underground. Environmental radionuclides such as 40 K and decay products in the 238 U and 232 Th chains have been identified as the most important radioactive contaminants of construction parts of HPGe gamma-ray spectrometers. Monte Carlo simulations have shown that the massive inner and outer lead shields have been the main contributors to the HPGe-detector background, followed by aluminum cryostat, copper cold finger, detector holder and the lead ring with FET. The Monte Carlo simulated cosmic-ray background gamma-ray spectrum has been by about three orders of magnitude lower than the experimental spectrum measured in the Modane underground laboratory (4800 m w.e.), underlying the importance of using radiopure materials for the construction of ultra-low-level HPGe gamma-ray spectrometers. Copyright © 2018 Elsevier Ltd. All rights reserved.

Effects of variation in background mixing ratios of N2, O2, and Ar on the measurement of δ18O-H2O and δ2H-H2O values by cavity ring-down spectroscopy

NASA Astrophysics Data System (ADS)

Johnson, Jennifer E.; Rella, Chris W.

2017-08-01

Cavity ring-down spectrometers have generally been designed to operate under conditions in which the background gas has a constant composition. However, there are a number of observational and experimental situations of interest in which the background gas has a variable composition. In this study, we examine the effect of background gas composition on a cavity ring-down spectrometer that measures δ18O-H2O and δ2H-H2O values based on the amplitude of water isotopologue absorption features around 7184 cm-1 (L2120-i, Picarro, Inc.). For background mixtures balanced with N2, the apparent δ18O values deviate from true values by -0.50 ± 0.001 ‰ O2 %-1 and -0.57 ± 0.001 ‰ Ar %-1, and apparent δ2H values deviate from true values by 0.26 ± 0.004 ‰ O2 %-1 and 0.42 ± 0.004 ‰ Ar %-1. The artifacts are the result of broadening, narrowing, and shifting of both the target absorption lines and strong neighboring lines. While the background-induced isotopic artifacts can largely be corrected with simple empirical or semi-mechanistic models, neither type of model is capable of completely correcting the isotopic artifacts to within the inherent instrument precision. The development of strategies for dynamically detecting and accommodating background variation in N2, O2, and/or Ar would facilitate the application of cavity ring-down spectrometers to a new class of observations and experiments.

High-speed Continuous-wave Stimulated Brillouin Scattering Spectrometer for Material Analysis.

PubMed

Remer, Itay; Cohen, Lear; Bilenca, Alberto

2017-09-22

Recent years have witnessed a significant increase in the use of spontaneous Brillouin spectrometers for non-contact analysis of soft matter, such as aqueous solutions and biomaterials, with fast acquisition times. Here, we discuss the assembly and operation of a Brillouin spectrometer that uses stimulated Brillouin scattering (SBS) to measure stimulated Brillouin gain (SBG) spectra of water and lipid emulsion-based tissue-like samples in transmission mode with <10 MHz spectral-resolution and <35 MHz Brillouin-shift measurement precision at <100 ms. The spectrometer consists of two nearly counter-propagating continuous-wave (CW) narrow-linewidth lasers at 780 nm whose frequency detuning is scanned through the material Brillouin shift. By using an ultra-narrowband hot rubidium-85 vapor notch filter and a phase-sensitive detector, the signal-to-noise-ratio of the SBG signal is significantly enhanced compared to that obtained with existing CW-SBS spectrometers. This improvement enables measurement of SBG spectra with up to 100-fold faster acquisition times, thereby facilitating high spectral-resolution and high-precision Brillouin analysis of soft materials at high speed.

The new double energy-velocity spectrometer VERDI

NASA Astrophysics Data System (ADS)

Jansson, Kaj; Frégeau, Marc Olivier; Al-Adili, Ali; Göök, Alf; Gustavsson, Cecilia; Hambsch, Franz-Josef; Oberstedt, Stephan; Pomp, Stephan

2017-09-01

VERDI (VElocity foR Direct particle Identification) is a fission-fragment spectrometer recently put into operation at JRC-Geel. It allows measuring the kinetic energy and velocity of both fission fragments simultaneously. The velocity provides information about the pre-neutron mass of each fission fragment when isotropic prompt-neutron emission from the fragments is assumed. The kinetic energy, in combination with the velocity, provides the post-neutron mass. From the difference between pre- and post-neutron masses, the number of neutrons emitted by each fragment can be determined. Multiplicity as a function of fragment mass and total kinetic energy is one important ingredient, essential for understanding the sharing of excitation energy between fission fragments at scission, and may be used to benchmark nuclear de-excitation models. The VERDI spectrometer design is a compromise between geometrical efficiency and mass resolution. The spectrometer consists of an electron detector located close to the target and two arrays of silicon detectors, each located 50 cm away from the target. In the present configuration pre-neutron and post-neutron mass distributions are in good agreement with reference data were obtained. Our latest measurements performed with spontaneously fissioning 252Cf is presented along with the developed calibration procedure to obtain pulse height defect and plasma delay time corrections.

The compact neutron spectrometer at ASDEX Upgrade.

PubMed

Giacomelli, L; Zimbal, A; Tittelmeier, K; Schuhmacher, H; Tardini, G; Neu, R

2011-12-01

The first neutron spectrometer of ASDEX Upgrade (AUG) was installed in November 2008. It is a compact neutron spectrometer (CNS) based on a BC501A liquid scintillating detector, which can simultaneously measure 2.45-MeV and 14-MeV neutrons emitted from deuterium (D) plasmas and γ radiation. The scintillating detector is coupled to a digital pulse shape discrimination data acquisition (DPSD) system capable of count rates up to 10(6) s(-1). The DPSD system can operate in acquisition and processing mode. With the latter n-γ discrimination is performed off-line based on the two-gate method. The paper describes the tests of the CNS and its installation at AUG. The neutron emission from the D plasma measured during a discharge with high auxiliary heating power was used to validate the CNS performance. The study of the optimal settings for the DPSD data processing to maximize the n-γ discrimination capability of the CNS is reported. The CNS measured both 2.45-MeV and 14-MeV neutrons emitted in AUG D plasmas with a maximum count rate of 5.4 × 10(5) s(-1) (>10 times higher than similar spectrometers previously achieved) with an efficiency of 9.3 × 10(-10) events per AUG neutron.

UV Spectrometer System AFGL 801 A HUP

DTIC Science & Technology

1989-05-01

These criteria can be established when more is known about the launch vehicles . The spectrometer will be operated before, during and after each test to...between flights would also be cut dramatically. The Forth code would be written on an IBM PC and transferred to EEPROMs ( Electrically Erasab!- Programmable...Read Only Memory) in the flight instruments. The use of EEPROMs, which are electrically programmable and erasable, allows the whole process of

SEQUOIA: A Newly Operating Chopper Spectrometer at the SNS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kolesnikov, Alexander I; Sherline, Todd E; Clancy, James P

2010-01-01

A fine resolution chopper spectrometer (SEQUOIA) recently received first neutrons at the SNS. The commissioning phase of the instrument is underway. SEQUOIA is designed to utilize neutrons of an incident energy (Ei) between 10-2000 meV. A monochromatic beam is provided on a sample, 20 m from the decoupled ambient temperature H2O moderator, by filtering the white beam with a Fermi chopper located 18 m from the source. After interacting with the sample, neutrons are detected by an array of 3He linear position sensitive tubes located on a vertical cylinder with a radius of 5.5 m. This contribution presents current resultsmore » from the commissioning experiments and compares SEQUOIA s actual and predicted performance. These commissioning experiments include characterization of the beam by monitors, determination of the chopper phase offsets, and runs with V and C4H2I2S. The predicted performance is provided by analytical calculations and Monte Carlo simulations.« less

Neutral Kaon Spectrometer 2

NASA Astrophysics Data System (ADS)

Kaneta, M.; Beckford, B.; Fujii, T.; Fujii, Y.; Futatsukawa, K.; Han, Y. C.; Hashimoto, O.; Hirose, K.; Ishikawa, T.; Kanda, H.; Kimura, C.; Maeda, K.; Nakamura, S. N.; Suzuki, K.; Tsukada, K.; Yamamoto, F.; Yamazaki, H.

2018-04-01

A large-acceptance spectrometer, Neutral Kaon Spectrometer 2 (NKS2), was newly constructed to explore various photoproduction reactions in the gigaelectronvolt region at the Laboratory of Nuclear Science (LNS, currently ELPH), Tohoku University. The spectrometer consisted of a dipole magnet, drift chambers, and plastic scintillation counters. NKS2 was designed to separate pions and protons in a momentum range of less than 1 GeV/ c, and was placed in a tagged photon beamline. A cryogenic H2/D2 target fitted to the spectrometer were designed. The design and performance of the detectors are described. The results of the NKS2 experiment on analyzing strangeness photoproduction data using a 0.8-1.1 GeV tagged photon beam are also presented.

Fourier Transform Spectrometer System

NASA Technical Reports Server (NTRS)

Campbell, Joel F. (Inventor)

2014-01-01

A Fourier transform spectrometer (FTS) data acquisition system includes an FTS spectrometer that receives a spectral signal and a laser signal. The system further includes a wideband detector, which is in communication with the FTS spectrometer and receives the spectral signal and laser signal from the FTS spectrometer. The wideband detector produces a composite signal comprising the laser signal and the spectral signal. The system further comprises a converter in communication with the wideband detector to receive and digitize the composite signal. The system further includes a signal processing unit that receives the composite signal from the converter. The signal processing unit further filters the laser signal and the spectral signal from the composite signal and demodulates the laser signal, to produce velocity corrected spectral data.

A neutron spectrometer for studying giant resonances with (p,n) reactions in inverse kinematics

NASA Astrophysics Data System (ADS)

Stuhl, L.; Krasznahorkay, A.; Csatlós, M.; Algora, A.; Gulyás, J.; Kalinka, G.; Timár, J.; Kalantar-Nayestanaki, N.; Rigollet, C.; Bagchi, S.; Najafi, M. A.

2014-02-01

A neutron spectrometer, the European Low-Energy Neutron Spectrometer (ELENS), has been constructed to study exotic nuclei in inverse-kinematics experiments. The spectrometer, which consists of plastic scintillator bars, can be operated in the neutron energy range of 100 keV-10 MeV. The neutron energy is determined using the time-of-flight technique, while the position of the neutron detection is deduced from the time-difference information from photomultipliers attached to both ends of each bar. A novel wrapping method has been developed for the plastic scintillators. The array has a larger than 25% detection efficiency for neutrons of approximately 500 keV in kinetic energy and an angular resolution of less than 1°. Details of the design, construction and experimental tests of the spectrometer will be presented.

Fluorescence Behavior and Dural Infiltration of Meningioma Analyzed by 5-Aminolevulinic Acid-Based Fluorescence: Operating Microscope Versus Mini-Spectrometer.

PubMed

Knipps, Johannes; Beseoglu, Kerim; Kamp, Marcel; Fischer, Igor; Felsberg, Joerg; Neumann, Lisa M; Steiger, Hans-Jakob; Cornelius, Jan F

2017-12-01

To compare fluorescence intensity of tumor specimens, as measured by a fluorescence-guided surgery microscope and a spectrometer, to evaluate tumor infiltration of dura mater around meningiomas with help of these 2 different 5-aminolevulinic acid (5-ALA)-based fluorescence tools, and to correlate fluorescence intensity with histopathologic data. In a clinical series, meningiomas were resected by 5-ALA fluorescence-guided surgery. Fluorescence intensity was semiquantitatively rated by the surgeon at predefined points. Biopsies were harvested and fluorescence intensity measured by a spectrometer and histopathologically analyzed. Sampling was realized at the level of the dura in a centrifugal direction. A total of 104 biopsies (n = 13 tumors) were analyzed. Specificity and sensitivity of the microscope were 0.96 and 0.53 and of the spectrometer 0.95 and 0.93, respectively. Fluorescence intensity as measured by the spectrometer was correlated to histologically confirmed tumor burden. In a centrifugal direction, tumor burden and fluorescence intensity continuously decreased (along the dural tail). Below a threshold value of 639 arbitrary units no tumor was histologically detectable. At the level of the dura the spectrometer was highly sensitive for detection of meningioma cells. The surgical microscope showed false negative results and missed residual tumor cells in more than one half of the cases. The complementary use of both fluorescence tools may improve resection quality. Copyright © 2017 Elsevier Inc. All rights reserved.

Development of a Gamma-Ray Spectrometer for Korean Pathfinder Lunar Orbiter

NASA Astrophysics Data System (ADS)

Kim, Kyeong Ja; Park, Junghun; Choi, Yire; Lee, Sungsoon; Yeon, Youngkwang; Yi, Eung Seok; Jeong, Meeyoung; Sun, Changwan; van Gasselt, Stephan; Lee, K. B.; Kim, Yongkwon; Min, Kyungwook; Kang, Kyungin; Cho, Jinyeon; Park, Kookjin; Hasebe, Nobuyuki; Elphic, Richard; Englert, Peter; Gasnault, Olivier; Lim, Lucy; Shibamura, Eido; GRS Team

2016-10-01

Korea is preparing for a lunar orbiter mission (KPLO) to be developed in no later than 2018. Onboard the spacecraft is a gamma ray spectrometer (KLGRS) allowing to collect low energy gamma-ray signals in order to detect elements by either X-ray fluorescence or by natural radioactive decay in the low as well as higher energy regions of up to 10 MeV. Scientific objectives include lunar resources (water and volatile measurements, rare earth elements and precious metals, energy resources, major elemental distributions for prospective in-situ utilizations), investigation of the lunar geology and studies of the lunar environment (mapping of the global radiation environment from keV to 10 MeV, high energy cosmic ray flux using the plastic scintillator).The Gamma-Ray Spectrometer (GRS) system is a compact low-weight instrument for the chemical analysis of lunar surface materials within a gamma-ray energy range from 10s keV to 10 MeV. The main LaBr3 detector is surrounded by an anti-coincidence counting module of BGO/PS scintillators to reduce both low gamma-ray background from the spacecraft and housing materials and high energy gamma-ray background from cosmic rays. The GRS system will determine the elemental compositions of the near surface of the Moon.The GRS system is a recently developed gamma-ray scintillation based detector which can be used as a replacement for the HPGe GRS sensor with the advantage of being able to operate at a wide range of temperatures with remarkable energy resolution. LaBr3 also has a high photoelectron yield, fast scintillation response, good linearity and thermal stability. With these major advantages, the LaBr3 GRS system will allow us to investigate scientific objectives and assess important research questions on lunar geology and resource exploration.The GRS investigation will help to assess open questions related to the spatial distribution and origin of the elements on the lunar surface and will contribute to unravel geological surface

Optimization of an underwater in-situ LaBr3:Ce spectrometer with energy self-calibration and efficiency calibration.

PubMed

Zeng, Zhi; Pan, Xingyu; Ma, Hao; He, Jianhua; Cang, Jirong; Zeng, Ming; Mi, Yuhao; Cheng, Jianping

2017-03-01

An underwater in-situ gamma-ray spectrometer based on LaBr 3 :Ce was developed and optimized to monitor marine radioactivity. The intrinsic background mainly from 138 La and 227 Ac of LaBr 3 :Ce was well determined by low background measurement and pulse shape discrimination method. A method of self-calibration using three internal contaminant peaks was proposed to eliminate the peak shift during long-term monitoring. With experiments under different temperatures, the method was proved to be helpful for maintaining long-term stability. To monitor the marine radioactivity, the spectrometer's efficiency was calculated via water tank experiment as well as Monte Carlo simulation. Copyright © 2016 Elsevier Ltd. All rights reserved.

The Wavelength-Dispersive Spectrometer and Its Proposed Use in the Analytical Electron Microscope

NASA Technical Reports Server (NTRS)

Goldstein, Joseph I.; Lyman, Charles E.; Williams, David B.

1989-01-01

The Analytical Electron Microscope (AEM) equipped with a wavelength-dispersive spectrometer (WDS) should have the ability to resolve peaks which normally overlap in the spectra from an energy-dispersive spectrometer (EDS). With a WDS it should also be possible to measure lower concentrations of elements in thin foils due to the increased peak-to-background ratio compared with EDS. The WDS will measure X-ray from the light elements (4 less than Z less than 1O) more effectively. This paper addresses the possibility of interfacing a compact WDS with a focussing circle of approximately 4 cm to a modem AEM with a high-brightness (field emission) source of electrons.

Tropospheric and Airborne Emission Spectrometers

NASA Technical Reports Server (NTRS)

Glavich, Thomas; Beer, Reinhard

1996-01-01

X This paper describes the development of two related instruments, the Tropospheric Emission Spectrometer (TES) and the Airborne Emission Spectrometer (AES). Both instruments are infrared imaging Fourier Transform Spectrometers, used for measuring the state of the lower atmosphere, and in particular the measurement of ozone and ozone sources and sinks.

The EBIT Calorimeter Spectrometer: a new, permanent user facility at the LLNL EBIT

DOE Office of Scientific and Technical Information (OSTI.GOV)

Porter, F S; Beiersdorfer, P; Brown, G V

The EBIT Calorimeter Spectrometer (ECS) is currently being completed and will be installed at the EBIT facility at the Lawrence Livermore National Laboratory in October 2007. The ECS will replace the smaller XRS/EBIT microcalorimeter spectrometer that has been in almost continuous operation since 2000. The XRS/EBIT was based on a spare laboratory cryostat and an engineering model detector system from the Suzaku/XRS observatory program. The new ECS spectrometer was built to be a low maintenance, high performance implanted silicon microcalorimeter spectrometer with 4 eV resolution at 6 keV, 32 detector channels, 10 {micro}s event timing, and capable of uninterrupted acquisitionmore » sessions of over 60 hours at 50 mK. The XRS/EBIT program has been very successful, producing many results on topics such as laboratory astrophysics, atomic physics, nuclear physics, and calibration of the spectrometers for the National Ignition Facility. The ECS spectrometer will continue this work into the future with improved spectral resolution, integration times, and ease-of-use. We designed the ECS instrument with TES detectors in mind by using the same highly successful magnetic shielding as our laboratory TES cryostats. This design will lead to a future TES instrument at the LLNL EBIT. Here we discuss the legacy of the XRS/EBIT program, the performance of the new ECS spectrometer, and plans for a future TES instrument.« less

VUV spectroscopy in impurity injection experiments at KSTAR using prototype ITER VUV spectrometer.

PubMed

Seon, C R; Hong, J H; Song, I; Jang, J; Lee, H Y; An, Y H; Kim, B S; Jeon, T M; Park, J S; Choe, W; Lee, H G; Pak, S; Cheon, M S; Choi, J H; Kim, H S; Biel, W; Bernascolle, P; Barnsley, R

2017-08-01

The ITER vacuum ultra-violet (VUV) core survey spectrometer has been designed as a 5-channel spectral system so that the high spectral resolving power of 200-500 could be achieved in the wavelength range of 2.4-160 nm. To verify the design of the ITER VUV core survey spectrometer, a two-channel prototype spectrometer was developed. As a subsequent step of the prototype test, the prototype VUV spectrometer has been operated at KSTAR since the 2012 experimental campaign. From impurity injection experiments in the years 2015 and 2016, strong emission lines, such as Kr xxv 15.8 nm, Kr xxvi 17.9 nm, Ne vii 46.5 nm, Ne vi 40.2 nm, and an array of largely unresolved tungsten lines (14-32 nm) could be measured successfully, showing the typical photon number of 10 13 -10 15 photons/cm 2 s.

Electronics for a Spectrometer

NASA Image and Video Library

2014-01-24

NASA has provided part of the electronics package for an instrument called the Double Focusing Mass Spectrometer, which is part of the Swiss-built Rosetta Orbiter Spectrometer for Ion and Neutral Analysis ROSINA instrument.

A hybrid thermal video and FTIR spectrometer system for rapidly locating and characterizing gas leaks

NASA Astrophysics Data System (ADS)

Williams, David J.; Wadsworth, Winthrop; Salvaggio, Carl; Messinger, David W.

2006-08-01

Undiscovered gas leaks, known as fugitive emissions, in chemical plants and refinery operations can impact regional air quality and present a loss of product for industry. Surveying a facility for potential gas leaks can be a daunting task. Industrial leak detection and repair programs can be expensive to administer. An efficient, accurate and cost effective method for detecting and quantifying gas leaks would both save industries money by identifying production losses and improve regional air quality. Specialized thermal video systems have proven effective in rapidly locating gas leaks. These systems, however, do not have the spectral resolution for compound identification. Passive FTIR spectrometers can be used for gas compound identification, but using these systems for facility surveys is problematic due to their small field of view. A hybrid approach has been developed that utilizes the thermal video system to locate gas plumes using real time visualization of the leaks, coupled with the high spectral resolution FTIR spectrometer for compound identification and quantification. The prototype hybrid video/spectrometer system uses a sterling cooled thermal camera, operating in the MWIR (3-5 μm) with an additional notch filter set at around 3.4 μm, which allows for the visualization of gas compounds that absorb in this narrow spectral range, such as alkane hydrocarbons. This camera is positioned alongside of a portable, high speed passive FTIR spectrometer, which has a spectral range of 2 - 25 μm and operates at 4 cm -1 resolution. This system uses a 10 cm telescope foreoptic with an onboard blackbody for calibration. The two units are optically aligned using a turning mirror on the spectrometer's telescope with the video camera's output.

Thermal design and performance of the REgolith x-ray imaging spectrometer (REXIS) instrument

NASA Astrophysics Data System (ADS)

Stout, Kevin D.; Masterson, Rebecca A.

2014-08-01

The REgolith X-ray Imaging Spectrometer (REXIS) instrument is a student collaboration instrument on the OSIRIS-REx asteroid sample return mission scheduled for launch in September 2016. The REXIS science mission is to characterize the elemental abundances of the asteroid Bennu on a global scale and to search for regions of enhanced elemental abundance. The thermal design of the REXIS instrument is challenging due to both the science requirements and the thermal environment in which it will operate. The REXIS instrument consists of two assemblies: the spectrometer and the solar X-ray monitor (SXM). The spectrometer houses a 2x2 array of back illuminated CCDs that are protected from the radiation environment by a one-time deployable cover and a collimator assembly with coded aperture mask. Cooling the CCDs during operation is the driving thermal design challenge on the spectrometer. The CCDs operate in the vicinity of the electronics box, but a 130 °C thermal gradient is required between the two components to cool the CCDs to -60 °C in order to reduce noise and obtain science data. This large thermal gradient is achieved passively through the use of a copper thermal strap, a large radiator facing deep space, and a two-stage thermal isolation layer between the electronics box and the DAM. The SXM is mechanically mounted to the sun-facing side of the spacecraft separately from the spectrometer and characterizes the highly variable solar X-ray spectrum to properly interpret the data from the asteroid. The driving thermal design challenge on the SXM is cooling the silicon drift detector (SDD) to below -30 °C when operating. A two-stage thermoelectric cooler (TEC) is located directly beneath the detector to provide active cooling, and spacecraft MLI blankets cover all of the SXM except the detector aperture to radiatively decouple the SXM from the flight thermal environment. This paper describes the REXIS thermal system requirements, thermal design, and analyses, with

An off Axis Cavity Enhanced Absorption Spectrometer and a Rapid Scan Spectrometer with a Room-Temperature External Cavity Quantum Cascade Laser

NASA Astrophysics Data System (ADS)

Liu, Xunchen; Kang, Cheolhwa; Xu, Yunjie

2009-06-01

Quantum cascade laser (QCL) is a new type of mid-infrared tunable diode lasers with superior output power and mode quality. Recent developments, such as room temperature operation, wide frequency tunability, and narrow line width, make QCLs an ideal light source for high resolution spectroscopy. Two slit jet infrared spectrometers, namely an off-axis cavity enhanced absorption (CEA) spectrometer and a rapid scan spectrometer with an astigmatic multi-pass cell assembly, have been coupled with a newly purchased room temperature tunable mod-hop-free QCL with a frequency coverage from 1592 cm^{-1} to 1698 cm^{-1} and a scan rate of 0.1 cm^{-1}/ms. Our aim is to utilize these two sensitive spectrometers, that are equipped with a molecular jet expansion, to investigate the chiral molecules-(water)_n clusters. To demonstrate the resolution and sensitivity achieved, the rovibrational transitions of the static N_2O gas and the bending rovibrational transitions of the Ar-water complex, a test system, at 1634 cm^{-1} have been measured. D. Hofstetter and J. Faist in High performance quantum cascade lasers and their applications, Vol.89 Springer-Verlag Berlin & Heidelberg, 2003, pp. 61-98. Y. Xu, X. Liu, Z. Su, R. M. Kulkarni, W. S. Tam, C. Kang, I. Leonov and L. D'Agostino, Proc. Spie, 2009, 722208 (1-11). M. J. Weida and D. J. Nesbitt, J. Chem. Phys. 1997, 106, 3078-3089.

Development of Compton X-ray spectrometer for high energy resolution single-shot high-flux hard X-ray spectroscopy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kojima, Sadaoki, E-mail: kojima-s@ile.osaka-u.ac.jp, E-mail: sfujioka@ile.osaka-u.ac.jp; Ikenouchi, Takahito; Arikawa, Yasunobu

Hard X-ray spectroscopy is an essential diagnostics used to understand physical processes that take place in high energy density plasmas produced by intense laser-plasma interactions. A bundle of hard X-ray detectors, of which the responses have different energy thresholds, is used as a conventional single-shot spectrometer for high-flux (>10{sup 13} photons/shot) hard X-rays. However, high energy resolution (Δhv/hv < 0.1) is not achievable with a differential energy threshold (DET) X-ray spectrometer because its energy resolution is limited by energy differences between the response thresholds. Experimental demonstration of a Compton X-ray spectrometer has already been performed for obtaining higher energy resolutionmore » than that of DET spectrometers. In this paper, we describe design details of the Compton X-ray spectrometer, especially dependence of energy resolution and absolute response on photon-electron converter design and its background reduction scheme, and also its application to the laser-plasma interaction experiment. The developed spectrometer was used for spectroscopy of bremsstrahlung X-rays generated by intense laser-plasma interactions using a 200 μm thickness SiO{sub 2} converter. The X-ray spectrum obtained with the Compton X-ray spectrometer is consistent with that obtained with a DET X-ray spectrometer, furthermore higher certainly of a spectral intensity is obtained with the Compton X-ray spectrometer than that with the DET X-ray spectrometer in the photon energy range above 5 MeV.« less

Radiation Design of Ion Mass Spectrometers

NASA Technical Reports Server (NTRS)

Sittler, Ed; Cooper, John; Christian, Eric; Moore, Tom; Sturner, Steve; Paschalidis, Nick

2011-01-01

In the harsh radiation environment of Jupiter and with the JUpiter ICy moon Explorer (JUICE) mission including two Europa flybys where local intensities are approx. 150 krad/month behind 100 mils of Al shielding, so background from penetrating radiation can be a serious issue for detectors inside an Ion Mass Spectrometer (IMS). This can especially be important for minor ion detection designs. Detectors of choice for time-of-flight (TOF) designs are microchannel plates (MCP) and some designs may include solid state detectors (SSD). The standard approach is to use shielding designs so background event rates are low enough that the detector max rates and lifetimes are first not exceeded and then the more stringent requirement that the desired measurement can successfully be made (i.e., desired signal is sufficiently greater than background noise after background subtraction is made). GEANT codes are typically used along with various electronic techniques, but such designs need to know how the detectors will respond to the simulated primary and secondary radiations produced within the instrument. We will be presenting some preliminary measurements made on the response of MCPs to energetic electrons (20 ke V to 1400 ke V) using a Miniature TOF (MTOF) device and the High Energy Facility at Goddard Space Flight Center which has a Van de Graaff accelerator.

The design of the Spectrometer Ring at the HIAF

NASA Astrophysics Data System (ADS)

Wu, B.; Yang, J. C.; Xia, J. W.; Yan, X. L.; Hu, X. J.; Mao, L. J.; Sheng, L. N.; Wu, J. X.; Yin, D. Y.; Chai, W. P.; Shen, G. D.; Ge, W. W.; Wang, G.; Zhao, H.; Ruan, S.; Ma, X. W.; Wang, M.; Litvinov, S.; Wen, W. Q.; Chen, X. C.; Chen, R. J.; Tang, M. T.; Wu, W.; Luo, C.; Zhao, T. C.; Shi, C. F.; Fu, X.; Liu, J.; Liang, L.

2018-02-01

The Spectrometer Ring (SRing) is an essential part of the High Intensity heavy-ion Accelerator Facility project (HIAF) in China. It is designed as a multi-functional experimental storage ring, which will be able to operate in three ion optical operation modes. The SRing will be used as a time-of-flight mass spectrometer for short-lived, especially neutron-rich nuclei. It will also be used to collect and cool Rare Isotope Beams (RIBs) or highly-charged stable ion beams for nuclear and atomic physics experiments. The design magnetic rigidity is in the range 1.5 to 15 Tm. The beam cooling system consists of stochastic cooling and electron cooling devices. With a help of an electron cooler, stored ions will be decelerated to a minimum energy of 30 MeV/u by RF cavities. The extraction system of the SRing will allow cooled ion beams to be extracted to an external target for further ion manipulations or reaction experiments. The general ion optics design and technical requirements of SRing subsystems are presented and discussed in this paper.

a KA-BAND Chirped-Pulse Fourier Transform Microwave Spectrometer.

NASA Astrophysics Data System (ADS)

Zaleski, Daniel P.; Neill, Justin L.; Muckle, Matthew T.; Pate, Brooks H.; Carroll, P. Brandon; Weaver, Susanna L. Widicus

2010-06-01

The design and performance of a new chirped-pulse Fourier transform microwave (CP-FTMW) spectrometer operating from 25-40 GHz will be discussed. A 10.5-3 GHz linear frequency sweep, generated by a 24 GS/s arbitrary waveform generator, is upconverted by a 23.00 GHz phase-locked oscillator, then fed into an active doubler to create a 25-40 GHz chirped pulse. After amplification with a 60-80 W pulsed traveling wave tube amplifier, the pulse is broadcast across a molecular beam chamber where it interacts with a molecular sample. The molecular FID signal is downconverted with the 23 GHz oscillator so that it can be digitized on a 50 GS/s oscilloscope with 16 GHz hardware bandwidth. The sensitivity and phase stability of this spectrometer is comparable to that of the previously reported 6.5-18.5 CP-FTMW spectrometer. On propyne (μ=0.78 D), a single-shot signal to noise ratio of approximately 200:1 is observed on the J=2-1 rotational transition at 34183 MHz when the full bandwidth is swept; optimal excitation is observed for this transition with a 250 MHz bandwidth sweep. The emission has a T_2 lifetime of 4 μs. Early results from this spectrometer, particularly in the study of species of astrochemical interest, will be presented. G.G. Brown et al., Rev. Sci. Instrum. 79 (2008) 053103.

Application of the BINS superheated drop detector spectrometer to the 9Be(p,xn) neutron energy spectrum determination

NASA Astrophysics Data System (ADS)

Di Fulvio, A.; Ciolini, R.; Mirzajani, N.; Romei, C.; d'Errico, F.; Bedogni, R.; Esposito, J.; Zafiropoulos, D.; Colautti, P.

2013-07-01

In the framework of TRASCO-BNCT project, a Bubble Interactive Neutron Spectrometer (BINS) device was applied to the characterization of the angle-and energy-differential neutron spectra generated by the 9Be(p,xn)reaction. The BINS spectrometer uses two superheated emulsion detectors, sequentially operated at different temperatures and thus provides a series of six sharp threshold responses, covering the 0.1-10 MeV neutron energy range. Spectrum unfolding of the data was performed by means of MAXED code. The obtained angle, energy-differential spectra were compared with those measured with a Bonner sphere spectrometer, a silicon telescope spectrometer and literature data.

The OPERA muon spectrometer tracking electronics

NASA Astrophysics Data System (ADS)

Ambrosio, M.; Barichello, G.; Brugnera, R.; Carrara, E.; Consiglio, L.; Corradi, A.; Dal Corso, F.; Dusini, S.; Felici, G.; Garfagnini, A.; Manea, C.; Masone, V.; Paoloni, A.; Paoluzzi, G.; Papalino, G.; Parascandolo, P.; Sorrentino, G.; Spinetti, M.; Stanco, L.; Terranova, F.; Votano, L.

2004-11-01

The document describes the front-end electronics that instrument the spectrometer of the OPERA experiment. The spectrometer is made of two separate modules. Each module consists of 22 RPC planes equipped with horizontal and vertical strips readout for a total amount of about 25,000 digital channels. The front end electronics is self-triggered and has single plane readout capability. It is made of three different stages: the Front End Boards (FEBs) system, the Controller Boards (CBs) system and the Timing Boards (TBs) system. The FEB system provides discrimination of the strip incoming signals; a FAST OR output of the input signals is also available for trigger plane signal generation. FEBs discriminated signals are acquired by the CBs system that manages also the communication to the experiment DAQ and Slow Control interface. A Trigger Board allows to operate in both self-trigger (the FEB FAST OR signal starts the plane acquisition) or external-trigger (different conditions can be set on the OR signals generated from different planes) modes.

Spectra of clinical CT scanners using a portable Compton spectrometer.

PubMed

Duisterwinkel, H A; van Abbema, J K; van Goethem, M J; Kawachimaru, R; Paganini, L; van der Graaf, E R; Brandenburg, S

2015-04-01

Spectral information of the output of x-ray tubes in (dual source) computer tomography (CT) scanners can be used to improve the conversion of CT numbers to proton stopping power and can be used to advantage in CT scanner quality assurance. The purpose of this study is to design, validate, and apply a compact portable Compton spectrometer that was constructed to accurately measure x-ray spectra of CT scanners. In the design of the Compton spectrometer, the shielding materials were carefully chosen and positioned to reduce background by x-ray fluorescence from the materials used. The spectrum of Compton scattered x-rays alters from the original source spectrum due to various physical processes. Reconstruction of the original x-ray spectrum from the Compton scattered spectrum is based on Monte Carlo simulations of the processes involved. This reconstruction is validated by comparing directly and indirectly measured spectra of a mobile x-ray tube. The Compton spectrometer is assessed in a clinical setting by measuring x-ray spectra at various tube voltages of three different medical CT scanner x-ray tubes. The directly and indirectly measured spectra are in good agreement (their ratio being 0.99) thereby validating the reconstruction method. The measured spectra of the medical CT scanners are consistent with theoretical spectra and spectra obtained from the x-ray tube manufacturer. A Compton spectrometer has been successfully designed, constructed, validated, and applied in the measurement of x-ray spectra of CT scanners. These measurements show that our compact Compton spectrometer can be rapidly set-up using the alignment lasers of the CT scanner, thereby enabling its use in commissioning, troubleshooting, and, e.g., annual performance check-ups of CT scanners.

Advanced technologies demonstrated by the miniature integrated camera and spectrometer (MICAS) aboard deep space 1

USGS Publications Warehouse

Rodgers, D.H.; Beauchamp, P.M.; Soderblom, L.A.; Brown, R.H.; Chen, G.-S.; Lee, M.; Sandel, B.R.; Thomas, D.A.; Benoit, R.T.; Yelle, R.V.

2007-01-01

MICAS is an integrated multi-channel instrument that includes an ultraviolet imaging spectrometer (80-185 nm), two high-resolution visible imagers (10-20 ??rad/pixel, 400-900 nm), and a short-wavelength infrared imaging spectrometer (1250-2600 nm). The wavelength ranges were chosen to maximize the science data that could be collected using existing semiconductor technologies and avoiding the need for multi-octave spectrometers. It was flown on DS1 to validate technologies derived from the development of PICS (Planetary Imaging Camera Spectrometer). These technologies provided a novel systems approach enabling the miniaturization and integration of four instruments into one entity, spanning a wavelength range from the UV to IR, and from ambient to cryogenic temperatures with optical performance at a fraction of a wavelength. The specific technologies incorporated were: a built-in fly-by sequence; lightweight and ultra-stable, monolithic silicon-carbide construction, which enabled room-temperature alignment for cryogenic (85-140 K) performance, and provided superb optical performance and immunity to thermal distortion; diffraction-limited, shared optics operating from 80 to 2600 nm; advanced detector technologies for the UV, visible and short-wavelength IR; high-performance thermal radiators coupled directly to the short-wave infrared (SWIR) detector optical bench, providing an instrument with a mass less than 10 kg, instrument power less than 10 W, and total instrument cost of less than ten million dollars. The design allows the wavelength range to be extended by at least an octave at the short wavelength end and to 50 microns at the long wavelength end. Testing of the completed instrument demonstrated excellent optical performance down to 77 K, which would enable a greatly reduced background for longer wavelength detectors. During the Deep Space 1 Mission, MICAS successfully collected images and spectra for asteroid 9969 Braille, Mars, and comet 19/P Borrelly. The

AI mass spectrometers for space shuttle health monitoring

NASA Technical Reports Server (NTRS)

Adams, F. W.

1991-01-01

The facility Hazardous Gas Detection System (HGDS) at Kennedy Space Center (KSC) is a mass spectrometer based gas analyzer. Two instruments make up the HGDS, which is installed in a prime/backup arrangement, with the option of using both analyzers on the same sample line, or on two different lines simultaneously. It is used for monitoring the Shuttle during fuel loading, countdown, and drainback, if necessary. The use of complex instruments, operated over many shifts, has caused problems in tracking the status of the ground support equipment (GSE) and the vehicle. A requirement for overall system reliability has been a major force in the development of Shuttle GSE, and is the ultimate driver in the choice to pursue artificial intelligence (AI) techniques for Shuttle and Advanced Launch System (ALS) mass spectrometer systems. Shuttle applications of AI are detailed.

The neutral mass spectrometer on Dynamics Explorer B

NASA Technical Reports Server (NTRS)

Carignan, G. R.; Block, B. P.; Maurer, J. C.; Hedin, A. E.; Reber, C. A.; Spencer, N. W.

1981-01-01

A neutral gas mass spectrometer has been developed to satisfy the measurement requirements of the Dynamics Explorer mission. The mass spectrometer, a quadrupole, will measure the abundances of neutral species in the region 300-500 km in the earth's atmosphere. These measurements will be used in concert with other simultaneous observations on Dynamics Explorer to study the physical processes involved in the interactions of the magnetosphere-ionosphere-atmosphere system. The instrument, which is similar to that flown on Atmosphere Explorer, employs an electron beam ion source operating in the closed mode and a discrete dynode multiplier as a detector. The mass range is 22 to 50 amu. The abundances of atomic oxygen, molecular nitrogen, helium, argon, and possibly atomic nitrogen will be measured to an accuracy of about + or - 15% over the specified altitude range, with a temporal resolution of one second.

Emirates Mars Infrared Spectrometer (EMIRS) Overview from the Emirates Mars Mission

NASA Astrophysics Data System (ADS)

Altunaiji, Eman; Edwards, Christopher; Smith, Michael; Christensen, Philip; AlMheiri, Suhail; Reed, Heather

2017-04-01

Emirates Mars Infrared Spectrometer (EMIRS) instrument is one of three scientific instruments aboard the Emirate Mars Mission (EMM), with the name of "Hope". EMM is United Arab Emirates' (UAE) mission to be launched in 2020, with the aim of exploring the dynamics of the atmosphere of Mars on a global scale with sampling on a diurnal and sub-seasonal time-scales. EMM has three scientific instruments selected to provide an improved understanding of circulation and weather in the Martian lower atmosphere as well as the thermosphere and exosphere. The EMIRS instrument is an interferometric thermal infrared spectrometer that is jointly developed by Arizona State University (ASU) and Mohammed Bin Rashid Space Centre (MBRSC), Dubai, UAE. It builds on a long heritage of thermal infrared spectrometers designed, built, and managed, by ASU's Mars Space Flight Facility, including the Thermal Emission Spectrometer (TES), Miniature Thermal Emission Spectrometer (Mini-TES), and the OSIRIS-REx Thermal Emission Spectrometer (OTES). EMIRS operates in the 6-40+ μm range with 5 cm-1 spectral sampling, enabled by a Chemical Vapor-Deposited (CVD) diamond beam splitter and state of the art electronics. This instrument utilizes a 3×3 line array detector and a scan mirror to make high-precision infrared radiance measurements over most of the Martian hemisphere. The EMIRS instrument is optimized to capture the integrated, lower-middle atmosphere dynamics over a Martian hemisphere, using a scan-mirror to make 60 global images per week ( 20 images per orbit) at a resolution of 100-300 km/pixel while requiring no special spacecraft maneuvers.

Operating Modes and Cooling Capabilities of the 3-Stage ADR Developed for the Soft-X-ray Spectrometer Instrument on Astro-H

PubMed Central

Shirron, Peter J; Kimball, Mark O; James, Bryan L; Muench, Theo; DiPirro, Michael J; Letmate, Richard V; Sampson, Michael A; Bialas, Tom G; Sneiderman, Gary A; Porter, Frederick S; Kelley, Richard L

2017-01-01

A 3-stage adiabatic demagnetization refrigerator (ADR)[1] is used on the Soft X-ray Spectrometer instrument[2] on Astro-H[3] to cool a 6×6 array of x-ray microcalorimeters to 50 mK. The ADR is supported by a cryogenic system[4] consisting of a superfluid helium tank, a 4.5 K Joule-Thomson (JT) cryocooler, and additional 2-stage Stirling cryocoolers that pre-cool the JT cooler and cool radiation shields within the cryostat. The ADR is configured so that it can use either the liquid helium or the JT cryocooler as its heat sink, giving the instrument an unusual degree of tolerance for component failures or degradation in the cryogenic system. The flight detector assembly, ADR and dewar were integrated into the flight dewar in early 2014, and have since been extensively characterized and calibrated. This paper summarizes the operation and performance of the ADR in all of its operating modes. PMID:28111478

Operating Modes and Cooling Capabilities of the 3-Stage ADR Developed for the Soft-X-ray Spectrometer Instrument on Astro-H.

PubMed

Shirron, Peter J; Kimball, Mark O; James, Bryan L; Muench, Theo; DiPirro, Michael J; Letmate, Richard V; Sampson, Michael A; Bialas, Tom G; Sneiderman, Gary A; Porter, Frederick S; Kelley, Richard L

2016-03-01

A 3-stage adiabatic demagnetization refrigerator (ADR)[1] is used on the Soft X-ray Spectrometer instrument[2] on Astro-H[3] to cool a 6×6 array of x-ray microcalorimeters to 50 mK. The ADR is supported by a cryogenic system[4] consisting of a superfluid helium tank, a 4.5 K Joule-Thomson (JT) cryocooler, and additional 2-stage Stirling cryocoolers that pre-cool the JT cooler and cool radiation shields within the cryostat. The ADR is configured so that it can use either the liquid helium or the JT cryocooler as its heat sink, giving the instrument an unusual degree of tolerance for component failures or degradation in the cryogenic system. The flight detector assembly, ADR and dewar were integrated into the flight dewar in early 2014, and have since been extensively characterized and calibrated. This paper summarizes the operation and performance of the ADR in all of its operating modes.

Operating Modes and Cooling Capabilities of the 3-Stage ADR Developed for the Soft-X-Ray Spectrometer Instrument on Astro-H

NASA Technical Reports Server (NTRS)

Shirron, Peter J.; Kimball, Mark O.; James, Bryan L.; Muench, Theo; DiPirro, Michael J.; Letmate, Richard V.; Sampson, Michael A.; Bialas, Tom G.; Sneiderman, Gary A.; Porter, Frederick S.;

Portable gas chromatograph mass spectrometer for on-site chemical analyses

DOEpatents

Haas, Jeffrey S.; Bushman, John F.; Howard, Douglas E.; Wong, James L.; Eckels, Joel D.

2002-01-01

A portable, lightweight (approximately 25 kg) gas chromatograph mass spectrometer, including the entire vacuum system, can perform qualitative and quantitative analyses of all sample types in the field. The GC/MS has a conveniently configured layout of components for ease of serviceability and maintenance. The GC/MS system can be transported under operating or near-operating conditions (i.e., under vacuum and at elevated temperature) to reduce the downtime before samples can be analyzed on-site.

VEGAS: VErsatile GBT Astronomical Spectrometer

NASA Astrophysics Data System (ADS)

Bussa, Srikanth; VEGAS Development Team

2012-01-01

The National Science Foundation Advanced Technologies and Instrumentation (NSF-ATI) program is funding a new spectrometer backend for the Green Bank Telescope (GBT). This spectrometer is being built by the CICADA collaboration - collaboration between the National Radio Astronomy Observatory (NRAO) and the Center for Astronomy Signal Processing and Electronics Research (CASPER) at the University of California Berkeley.The backend is named as VErsatile GBT Astronomical Spectrometer (VEGAS) and will replace the capabilities of the existing spectrometers. This backend supports data processing from focal plane array systems. The spectrometer will be capable of processing up to 1.25 GHz bandwidth from 8 dual polarized beams or a bandwidth up to 10 GHz from a dual polarized beam.The spectrometer will be using 8-bit analog to digital converters (ADC), which gives a better dynamic range than existing GBT spectrometers. There will be 8 tunable digital sub-bands within the 1.25 GHz bandwidth, which will enhance the capability of simultaneous observation of multiple spectral transitions. The maximum spectral dump rate to disk will be about 0.5 msec. The vastly enhanced backend capabilities will support several science projects with the GBT. The projects include mapping temperature and density structure of molecular clouds; searches for organic molecules in the interstellar medium; determination of the fundamental constants of our evolving Universe; red-shifted spectral features from galaxies across cosmic time and survey for pulsars in the extreme gravitational environment of the Galactic Center.

Fluorescence-spectrometer helps Mobil increase analytical output by 50%

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hamm, J.C.; Peckham, M.R.; Powers, J.

1987-09-01

A wide range of gear-oil packages and synthetic oil bases for motor vehicle use are produced at Mobil Chemical Company's Beaumont, TX, Chemical Specialties Plant (BCSP). Also manufactured are industrial lubricants, hydraulic fluids, and a selection of specialty oils. For a number of years, Mobil used what at that time represented up-to-date X-ray fluorescence technology for analyzing its oil products. Mobil decided to search for a more efficient X-ray fluorescence spectrometer for oil analyses that would provide a number of major features such a high speed, accuracy and reproducibility, appropriate software for matrix correction, a helium atmosphere for determining lightmore » elements in liquids, and the ability to determine both high and low (ppm level) concentrations quantitatively. In the spring of 1985, Mobil installed new X-ray fluorescence equipment that gives much faster analysis of liquid samples, greater analytical sensitivity, and a much more stable system. In addition, the unit produces calibration curves, retains reference-standards data in memory, and gives numerical or graphical readouts which directly show deviations from the specified levels of Cl, S, and P components for each sample, analyzed sequentially or simultaneously. The spectrometer combines the speed and high throughput of multichannel spectrometers along with the high flexibility of sequential goniometers. The hybrid configuration incorporates a versatile goniometer with as many as 10 monochromators and operates under computer control. All benefits of the modern equipment have given Mobil better product quality, faster production approvals, and greater overall operational economics.« less

Resolution-enhanced Mapping Spectrometer

NASA Technical Reports Server (NTRS)

Kumer, J. B.; Aubrun, J. N.; Rosenberg, W. J.; Roche, A. E.

1993-01-01

A familiar mapping spectrometer implementation utilizes two dimensional detector arrays with spectral dispersion along one direction and spatial along the other. Spectral images are formed by spatially scanning across the scene (i.e., push-broom scanning). For imaging grating and prism spectrometers, the slit is perpendicular to the spatial scan direction. For spectrometers utilizing linearly variable focal-plane-mounted filters the spatial scan direction is perpendicular to the direction of spectral variation. These spectrometers share the common limitation that the number of spectral resolution elements is given by the number of pixels along the spectral (or dispersive) direction. Resolution enhancement by first passing the light input to the spectrometer through a scanned etalon or Michelson is discussed. Thus, while a detector element is scanned through a spatial resolution element of the scene, it is also temporally sampled. The analysis for all the pixels in the dispersive direction is addressed. Several specific examples are discussed. The alternate use of a Michelson for the same enhancement purpose is also discussed. Suitable for weight constrained deep space missions, hardware systems were developed including actuators, sensor, and electronics such that low-resolution etalons with performance required for implementation would weigh less than one pound.

An Evaluation of a Passively Cooled Cylindrical Spectrometer Array in Lunar Orbit

NASA Technical Reports Server (NTRS)

Waggoner, Jason

2014-01-01

This thesis will evaluate a passively cooled cylindrical spectrometer array in lunar orbit characterizing the thermal response in order to provide context for decision-making to scientists and engineers. To provide perspective on thermal issues and controls of space science instruments, a background search of historical lunar missions is provided. Next, a trial science mission is designed and analyzed which brings together the elements of the background search, lunar orbit environment and passive cooling. Finally, the trial science mission analysis results are provided along with the conclusions drawn. Scintillators are materials that when struck by particle radiation, absorb the particle energy which is then reemitted as light in or near the visible range. Nuclear astrophysics utilizes scintillating materials for observation of high-energy photons which are generated by sources such as solar flares, supernovae and neutron stars. SPMs are paired with inorganic scintillators to detect the light emitted which is converted into electronic signals. The signals are captured and analyzed in order to map the number and location of the high-energy sources. The SPM is utilized as it has single photon sensitivity, low voltage requirements and a fast response. SPMs are also compact, relatively inexpensive and allow the usage of lower-cost scintillating materials within the spectrometer. These characteristics permit large-area arrays while lowering cost and power requirements. The ability of a spectrometer to record and identify the interaction of high-energy photons for scientific return is not a trivial matter. Background noise is generated when particles that have not originated from the desired distant source impact the spectrometer. Additionally, thermally induced electrical signals are randomly generated within the SPM even in the absence of light which is referred to as dark current. Overcoming these obstacles requires greater light emittance and energy resolution with

Operating principles and detection characteristics of the Visible and Near-Infrared Imaging Spectrometer in the Chang'e-3

NASA Astrophysics Data System (ADS)

He, Zhi-Ping; Wang, Bin-Yong; Lü, Gang; Li, Chun-Lai; Yuan, Li-Yin; Xu, Rui; Liu, Bin; Chen, Kai; Wang, Jian-Yu

2014-12-01

The Visible and Near-Infrared Imaging Spectrometer (VNIS), using two acousto-optic tunable filters as dispersive components, consists of a VIS/NIR imaging spectrometer (0.45-0.95 μm), a shortwave IR spectrometer (0.9-2.4 μm) and a calibration unit with dust-proofing functionality. The VNIS was utilized to detect the spectrum of the lunar surface and achieve in-orbit calibration, which satisfied the requirements for scientific detection. Mounted at the front of the Yutu rover, lunar objects that are detected with the VNIS with a 45° visual angle to obtain spectra and geometrical data in order to analyze the mineral composition of the lunar surface. After landing successfully on the Moon, the VNIS performed several explorations and calibrations, and obtained several spectral images and spectral reflectance curves of the lunar soil in the region of Mare Imbrium. This paper describes the working principle and detection characteristics of the VNIS and provides a reference for data processing and scientific applications.

Accurate Transmittance Measurements of Thick, High-Index, High- Dispersion, IR Windows, Using a Fourier Transform IR Spectrometer

NASA Astrophysics Data System (ADS)

Kupferberg, Lenn C.

1996-03-01

Fourier transform IR [FT-IR] spectrometers have virtually replaced scanned grating IR spectrometers in the commercial market. While FTIR spectrometers have been a boon for the chemist, they present problems for the measurement of transmittance of thick, high-index, high-dispersion, IR windows. Reflection and refraction of light by the windows introduce measurement errors. The principles of the FT-IR spectrometer will be briefly reviewed. The origins of the measurement errors will be discussed. Simple modifications to the operation of commercially available instruments will be presented. These include using strategically placed apertures and the use of collimated vs. focused beams at the sample position. They are essential for removing the effects of reflected light entering the interferometer and limiting the divergence angle of light in the interferometer. The latter minimizes refractive effects and insures consistent underfilling of the detector. Data will be shown from FT-IR spectrometers made by four manufactures and compared to measurements from a dispersive spectrometer.

Ultra-Low Background Measurements Of Decayed Aerosol Filters

NASA Astrophysics Data System (ADS)

Miley, H.

2009-04-01

To experimentally evaluate the opportunity to apply ultra-low background measurement methods to samples collected, for instance, by the Comprehensive Test Ban Treaty International Monitoring System (IMS), aerosol samples collected on filter media were measured using HPGe spectrometers of varying low-background technology approaches. In this way, realistic estimates of the impact of low-background methodology can be assessed on the Minimum Detectable Activities obtained in systems such as the IMS. The current measurement requirement of stations in the IMS is 30 microBq per cubic meter of air for 140Ba, or about 106 fissions per daily sample. Importantly, this is for a fresh aerosol filter. Decay varying form 3 days to one week reduce the intrinsic background from radon daughters in the sample. Computational estimates of the improvement factor for these decayed filters for underground-based HPGe in clean shielding materials are orders of magnitude less, even when the decay of the isotopes of interest is included.

The JET neutron time-of-flight spectrometer

NASA Astrophysics Data System (ADS)

Elevant, T.; Aronsson, D.; van Belle, P.; Grosshoeg, G.; Hoek, M.; Olsson, M.; Sadler, G.

1991-08-01

An instrument for measuring neutron energy spectra over the interval 1 to 20 MeV has been developed and tested. It is based on time-of-flight measurements in between correlated events in two spatially separated sets of plastic scintillators. This instrument has been installed at the Joint European Tours (JET). We describe here the required operating conditions, performance tests and results of three years of operation during which neutron energy spectra in the 2-3 MeV range from D(d, n) 3He reactions in JET were studied. Some technical details are given and the results from Monte Carlo and analytical model calculations of the spectrometer energy resolution and response function are presented. The efficiency of the system is ≈ 1 × 10 -2 cm 2 counted at the position of the first detector. Together with the geometry conditions at JET this yields 6 × 10 2 counts per 10 15 neutrons emitted. The energy resolution is in the interval from 125 to 133 keV (FWHM) depending on conditions and is known to an accuracy of ±5 keV. Correction for the inevitable random background is dealt with in detail and a reduction procedure valid for fast variations in neutron count-rates is provided. Plasma ion temperatures deduced from the neutron spectra agree within statistical limits with the results from other diagnostic techniques in use at JET. Stable behaviour up to useful count-rates of 3 × 10 3 counts/s have been obtained, making possible the study of neutron spectra on the short time-scales typical of fusion plasmas.

Neutron spectrometry and dosimetry study at two research nuclear reactors using Bonner sphere spectrometer (BSS), rotational spectrometer (ROSPEC) and cylindrical nested neutron spectrometer (NNS).

PubMed

Atanackovic, J; Matysiak, W; Hakmana Witharana, S S; Aslam, I; Dubeau, J; Waker, A J

2013-01-01

Neutron spectrometry and subsequent dosimetry measurements were undertaken at the McMaster Nuclear Reactor (MNR) and AECL Chalk River National Research Universal (NRU) Reactor. The instruments used were a Bonner sphere spectrometer (BSS), a cylindrical nested neutron spectrometer (NNS) and a commercially available rotational proton recoil spectrometer. The purposes of these measurements were to: (1) compare the results obtained by three different neutron measuring instruments and (2) quantify neutron fields of interest. The results showed vastly different neutron spectral shapes for the two different reactors. This is not surprising, considering the type of the reactors and the locations where the measurements were performed. MNR is a heavily shielded light water moderated reactor, while NRU is a heavy water moderated reactor. The measurements at MNR were taken at the base of the reactor pool, where a large amount of water and concrete shielding is present, while measurements at NRU were taken at the top of the reactor (TOR) plate, where there is only heavy water and steel between the reactor core and the measuring instrument. As a result, a large component of the thermal neutron fluence was measured at MNR, while a negligible amount of thermal neutrons was measured at NRU. The neutron ambient dose rates at NRU TOR were measured to be between 0.03 and 0.06 mSv h⁻¹, while at MNR, these values were between 0.07 and 2.8 mSv h⁻¹ inside the beam port and <0.2 mSv h⁻¹ between two operating beam ports. The conservative uncertainty of these values is 15 %. The conservative uncertainty of the measured integral neutron fluence is 5 %. It was also found that BSS over-responded slightly due to a non-calibrated response matrix.

Solar Imaging UV/EUV Spectrometers Using TVLS Gratings

NASA Astrophysics Data System (ADS)

Thomas, R. J.

2003-05-01

It is a particular challenge to develop a stigmatic spectrograph for UV/EUV wavelengths since the very low normal-incidence reflectance of standard materials most often requires that the design be restricted to a single optical element which must simultaneously provide both re-imaging and spectral dispersion. This problem has been solved in the past by the use of toroidal gratings with uniform line-spaced rulings (TULS). A number of solar EUV spectrometers have been based on such designs, including SOHO/CDS, Solar-B/EIS, and the sounding rockets SERTS and EUNIS. More recently, Kita, Harada, and collaborators have developed the theory of spherical gratings with varied line-space rulings (SVLS) operated at unity magnification, which have been flown on several astronomical satellite missions. We now combine these ideas into a spectrometer concept that puts varied-line space rulings onto toroidal gratings. Such TVLS designs are found to provide excellent imaging even at very large spectrograph magnifications and beam-speeds, permitting extremely high-quality performance in remarkably compact instrument packages. Optical characteristics of three new solar spectrometers based on this concept are described: SUMI and RAISE, two sounding rocket payloads, and NEXUS, currently being proposed as a Small-Explorer (SMEX) mission.

Solar Imaging UV/EUV Spectrometers Using TVLS Gratings

NASA Technical Reports Server (NTRS)

Thomas, Roger J.

2003-01-01

It is a particular challenge to develop a stigmatic spectrograph for UV, EUV wavelengths since the very low normal-incidence reflectance of standard materials most often requires that the design be restricted to a single optical element which must simultaneously provide both reimaging and spectral dispersion. This problem has been solved in the past by the use of toroidal gratings with uniform line-spaced rulings (TULS). A number of solar extreme ultraviolet (EUV) spectrometers have been based on such designs, including SOHO/CDS, Solar-B/EIS, and the sounding rockets Solar Extreme ultraviolet Research Telescope and Spectrograph (SERTS) and Extreme Ultraviolet Normal Incidence Spectrograph (EUNIS). More recently, Kita, Harada, and collaborators have developed the theory of spherical gratings with varied line-space rulings (SVLS) operated at unity magnification, which have been flown on several astronomical satellite missions. We now combine these ideas into a spectrometer concept that puts varied-line space rulings onto toroidal gratings. Such TVLS designs are found to provide excellent imaging even at very large spectrograph magnifications and beam-speeds, permitting extremely high-quality performance in remarkably compact instrument packages. Optical characteristics of three new solar spectrometers based on this concept are described: SUMI and RAISE, two sounding rocket payloads, and NEXUS, currently being proposed as a Small-Explorer (SMEX) mission.

Electron/proton spectrometer certification documentation analyses

NASA Technical Reports Server (NTRS)

Gleeson, P.

1972-01-01

A compilation of analyses generated during the development of the electron-proton spectrometer for the Skylab program is presented. The data documents the analyses required by the electron-proton spectrometer verification plan. The verification plan was generated to satisfy the ancillary hardware requirements of the Apollo Applications program. The certification of the spectrometer requires that various tests, inspections, and analyses be documented, approved, and accepted by reliability and quality control personnel of the spectrometer development program.

Photo ion spectrometer

DOEpatents

Gruen, D.M.; Young, C.E.; Pellin, M.J.

1989-12-26

A charged particle spectrometer is described for performing ultrasensitive quantitative analysis of selected atomic components removed from a sample. Significant improvements in performing energy and angular refocusing spectroscopy are accomplished by means of a two dimensional structure for generating predetermined electromagnetic field boundary conditions. Both resonance and non-resonance ionization of selected neutral atomic components allow accumulation of increased chemical information. A multiplexed operation between a SIMS mode and a neutral atomic component ionization mode with EARTOF analysis enables comparison of chemical information from secondary ions and neutral atomic components removed from the sample. An electronic system is described for switching high level signals, such as SIMS signals, directly to a transient recorder and through a charge amplifier to the transient recorder for a low level signal pulse counting mode, such as for a neutral atomic component ionization mode. 12 figs.

Photo ion spectrometer

DOEpatents

Gruen, Dieter M.; Young, Charles E.; Pellin, Michael J.

1989-01-01

A charged particle spectrometer for performing ultrasensitive quantitative analysis of selected atomic components removed from a sample. Significant improvements in performing energy and angular refocusing spectroscopy are accomplished by means of a two dimensional structure for generating predetermined electromagnetic field boundary conditions. Both resonance and non-resonance ionization of selected neutral atomic components allow accumulation of increased chemical information. A multiplexed operation between a SIMS mode and a neutral atomic component ionization mode with EARTOF analysis enables comparison of chemical information from secondary ions and neutral atomic components removed from the sample. An electronic system is described for switching high level signals, such as SIMS signals, directly to a transient recorder and through a charge amplifier to the transient recorder for a low level signal pulse counting mode, such as for a neutral atomic component ionization mode.

High-resolution crystal spectrometer for the 10-60 (angstrom) EUV region

DOE Office of Scientific and Technical Information (OSTI.GOV)

Beiersdorfer, P; Brown, G V; Goddard, R

2004-02-20

A vacuum crystal spectrometer with nominal resolving power approaching 1000 is described for measuring emission lines with wavelength in the extreme ultraviolet region up to 60 Angstroms. The instrument utilizes a flat octadecyl hydrogen maleate (OHM) crystal and a thin-window 1-D position-sensitive gas proportional detector. This detector employs a 1 {micro}m-thick 100 x8 mm{sup 2} aluminized polyimide window and operates at one atmosphere pressure. The spectrometer has been implemented on the Livermore electron beam ion traps. The performance of the instrument is illustrated in measurements of the newly discovered magnetic field-sensitive line in Ar{sup 8+}.

Spectrometer system for diffuse extreme ultraviolet radiation

NASA Technical Reports Server (NTRS)

Labov, Simon E.

1989-01-01

A unique grazing incidence spectrometer system has been designed to study diffuse line emission between 80 and 650 A with 10-30 A resolution. The minimum detectable emission line strength during a 5-min observation ranges from 100-2000 ph/sq cm sec str. The instrument uses mechanically ruled reflection gratings placed in front of a linear array of mirrors. These mirrors focus the spectral image on microchannel plate detectors located behind thin filters. The field of view is 40 min of arc by 15 deg, and there is no spatial imaging. This instrument has been fabricated, calibrated, and successfully flown on a sounding rocket to observe the astronomical background radiation.

DC superconducting quantum interference device usable in nuclear quadrupole resonance and zero field nuclear magnetic spectrometers

DOEpatents

Fan, N.Q.; Clarke, J.

1993-10-19

A spectrometer for measuring the nuclear quadrupole resonance spectra or the zero-field nuclear magnetic resonance spectra generated by a sample is disclosed. The spectrometer uses an amplifier having a dc SQUID operating in a flux-locked loop for generating an amplified output as a function of the intensity of the signal generated by the sample. The flux-locked loop circuit includes an integrator. The amplifier also includes means for preventing the integrator from being driven into saturation. As a result, the time for the flux-locked loop to recover from the excitation pulses generated by the spectrometer is reduced. 7 figures.

DC superconducting quantum interference device usable in nuclear quadrupole resonance and zero field nuclear magnetic spectrometers

DOEpatents

Fan, Non Q.; Clarke, John

1993-01-01

A spectrometer for measuring the nuclear quadrupole resonance spectra or the zero-field nuclear magnetic resonance spectra generated by a sample is disclosed. The spectrometer uses an amplifier having a dc SQUID operating in a flux-locked loop for generating an amplified output as a function of the intensity of the signal generated by the sample. The flux-locked loop circuit includes an integrator. The amplifier also includes means for preventing the integrator from being driven into saturation. As a result, the time for the flux-locked loop to recover from the excitation pulses generated by the spectrometer is reduced.

Inverse time-of-flight spectrometer for beam plasma research

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yushkov, Yu. G., E-mail: yuyushkov@gmail.com; Zolotukhin, D. B.; Tyunkov, A. V.

2014-08-15

The paper describes the design and principle of operation of an inverse time-of-flight spectrometer for research in the plasma produced by an electron beam in the forevacuum pressure range (5–20 Pa). In the spectrometer, the deflecting plates as well as the drift tube and the primary ion beam measuring system are at high potential with respect to ground. This provides the possibility to measure the mass-charge constitution of the plasma created by a continuous electron beam with a current of up to 300 mA and electron energy of up to 20 keV at forevacuum pressures in the chamber placed atmore » ground potential. Research results on the mass-charge state of the beam plasma are presented and analyzed.« less

15 pixels digital autocorrelation spectrometer system

NASA Astrophysics Data System (ADS)

Lee, Changhoon; Kim, Hyo-Ryung; Kim, Kwang-Dong; Chung, Mun-Hee; Timoc, C.

2006-06-01

In this paper describes the system configuration and the some performance test results of the 15 pixels digital autocorrelation spectrometer to be used at the Taeduk Radio Astronomy Observatory (TRAO) of Korea. This autocorrelation spectrometer instrument enclosed in a 3-slot VXI module and controlled via a USB port by a backend PC. This spectrometer system consists of the 4 band-pass filters unit, the digitizer, the 512 lags correlator, the clock distribution unit, and USB controller. And here we describe the frequency accuracy and the root-mean-square noise characteristic of this spectrometer. After some calibration procedure, this spectrometer can be use as the back-end system at TRAO for the 3x5 focal plane array receivers.

Hydrazine Detection with a Tunable Diode Laser Spectrometer

NASA Technical Reports Server (NTRS)

Houseman, John; Webster, C. R.; May, R. D.; Anderson, M. S.; Margolis, J. S.; Jackson, Julie R.; Brown, Pamela R.

1999-01-01

Several instruments have been developed to measure low concentrations of hydrazine but none completely meet the sensitivity requirements while satisfying additional criteria such as quick response, stable calibration, interference free operation, online operation, reasonable cost, etc. A brief review is presented of the current technology including the electrochemical cell, the ion mobility spectrometer, the mass spectrometer, and the gas chromatograph. A review of the advantages and disadvantages of these instruments are presented here. The review also includes commercially unavailable technology such as the electronic nose and the Tunable Diode Laser (TDL) IR Spectrometer. It was found that the TDL could meet the majority of these criteria including fast response, minimum maintenance, portability, and reasonable cost. An experiment was conducted to demonstrate the feasibility of such a system using an existing (non-portable) instrument. A lead-salt tunable diode laser, cooled to 85 degrees Kelvin was used to record direct absorption and second-derivative spectra of Hydrazine at several pressures to study the sensitivity to low levels of Hydrazine. Spectra of NH3 and CO2 were used for wavelength identification of the scanned region. With a pathlength of 80 m, detection sensitivities of about 1 ppb were achieved for hydrazine in dry nitrogen at a cell pressure of 100 mbar. For spectroscopic detection of Hydrazine, spectral regions including strong Ammonia or Carbon Dioxide lines must be avoided. Strong Hydrazine absorption features were identified at 940/cm showing minimal contribution from Ammonia interferences as suitable candidates for Hydrazine gas detection. For the studies reported here, the particular laser diode could only cover the narrow regions near 962/cm and 965/cm where strong Ammonia interferences were expected. However, the high resolution (0.001/cm) of the TDL spectrometer allowed individual lines of Hydrazine to be identified away from

A seven-crystal Johann-type hard x-ray spectrometer at the Stanford Synchrotron Radiation Lightsource

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sokaras, D.; Weng, T.-C.; Nordlund, D.

2013-05-15

We present a multicrystal Johann-type hard x-ray spectrometer ({approx}5-18 keV) recently developed, installed, and operated at the Stanford Synchrotron Radiation Lightsource. The instrument is set at the wiggler beamline 6-2 equipped with two liquid nitrogen cooled monochromators - Si(111) and Si(311) - as well as collimating and focusing optics. The spectrometer consists of seven spherically bent crystal analyzers placed on intersecting vertical Rowland circles of 1 m of diameter. The spectrometer is scanned vertically capturing an extended backscattering Bragg angular range (88 Degree-Sign -74 Degree-Sign ) while maintaining all crystals on the Rowland circle trace. The instrument operates in atmosphericmore » pressure by means of a helium bag and when all the seven crystals are used (100 mm of projected diameter each), has a solid angle of about 0.45% of 4{pi} sr. The typical resolving power is in the order of (E/{Delta}E){approx}10 000. The spectrometer's high detection efficiency combined with the beamline 6-2 characteristics permits routine studies of x-ray emission, high energy resolution fluorescence detected x-ray absorption and resonant inelastic x-ray scattering of very diluted samples as well as implementation of demanding in situ environments.« less

Second-Generation Design of Micro-Spec: A Medium-Resolution, Submillimeter-Wavelength Spectrometer-on-a-Chip

NASA Astrophysics Data System (ADS)

Cataldo, G.; Barrentine, E. M.; Bulcha, B. T.; Ehsan, N.; Hess, L. A.; Noroozian, O.; Stevenson, T. R.; U-Yen, K.; Wollack, E. J.; Moseley, S. H.

2018-04-01

Micro-Spec (µ-Spec) is a direct-detection spectrometer which integrates all the components of a diffraction-grating spectrometer onto a ˜ 10-cm^2 chip through the use of superconducting microstrip transmission lines on a single-crystal silicon substrate. A second-generation µ-Spec is being designed to operate with a spectral resolution of 512 in the submillimeter (500-1000 µm, 300-600 GHz) wavelength range, a band of interest for several spectroscopic applications in astrophysics. High-altitude balloon missions would provide the first test bed to demonstrate the µ-Spec technology in a space-like environment and would be an economically viable venue for multiple observation campaigns. This work reports on the current status of the instrument design and will provide a brief overview of each instrument subsystem. Particular emphasis will be given to the design of the spectrometer's two-dimensional diffractive region, through which the light of different wavelengths is focused on the detectors along the focal plane. An optimization process is employed to generate geometrical configurations of the diffractive region that satisfy specific requirements on spectrometer size, operating spectral range, and performance. An optical design optimized for balloon missions will be presented in terms of geometric layout, spectral purity, and efficiency.

Thermostatic system of sensor in NIR spectrometer based on PID control

NASA Astrophysics Data System (ADS)

Wang, Zhihong; Qiao, Liwei; Ji, Xufei

2016-11-01

Aiming at the shortcomings of the primary sensor thermostatic control system in the near infrared (NIR) spectrometer, a novel thermostatic control system based on proportional-integral-derivative (PID) control technology was developed to improve the detection precision of the NIR spectrometer. There were five parts including bridge amplifier circuit, analog-digital conversion (ADC) circuit, microcontroller, digital-analog conversion (DAC) circuit and drive circuit in the system. The five parts formed a closed-loop control system based on PID algorithm that was used to control the error between the temperature calculated by the sampling data of ADC and the designed temperature to ensure the stability of the spectrometer's sensor. The experimental results show that, when the operating temperature of sensor is -11°, compared with the original system, the temperature control precision of the new control system is improved from ±0.64° to ±0.04° and the spectrum signal to noise ratio (SNR) is improved from 4891 to 5967.

Outdoor chamber measurements of biological aerosols with a passive FTIR spectrometer

NASA Astrophysics Data System (ADS)

D'Amico, Francis M.; Emge, Darren K.; Roelant, Geoffrey J.

2004-02-01

Outdoor measurements of dry bacillus subtilis (BG) spores were conducted with a passive Fourier transform infrared (FTIR) spectrometer using two types of chambers. One was a large open-ended cell, and the other was a canyon of similar dimensions. The canyon exposes the aerosol plume to downwelling sky radiance, while the open-ended cell does not. The goal of the experiments was to develop a suitable test methodology for evaluation of passive standoff detectors for open-air aerosol measurements. Dry BG aerosol particles were dispersed with a blower through an opening in the side of the chamber to create a pseudo-stationary plume, wind conditions permitting. Numerous trials were performed with the FTIR spectrometer positioned to view mountain, sky and mixed mountain-sky backgrounds. This paper will discuss the results of the FTIR measurements for BG and Kaolin dust releases.

Ultra-compact MEMS FTIR spectrometer

NASA Astrophysics Data System (ADS)

Sabry, Yasser M.; Hassan, Khaled; Anwar, Momen; Alharon, Mohamed H.; Medhat, Mostafa; Adib, George A.; Dumont, Rich; Saadany, Bassam; Khalil, Diaa

2017-05-01

Portable and handheld spectrometers are being developed and commercialized in the late few years leveraging the rapidly-progressing technology and triggering new markets in the field of on-site spectroscopic analysis. Although handheld devices were commercialized for the near-infrared spectroscopy (NIRS), their size and cost stand as an obstacle against the deployment of the spectrometer as spectral sensing components needed for the smart phone industry and the IoT applications. In this work we report a chip-sized microelectromechanical system (MEMS)-based FTIR spectrometer. The core optical engine of the solution is built using a passive-alignment integration technique for a selfaligned MEMS chip; self-aligned microoptics and a single detector in a tiny package sized about 1 cm3. The MEMS chip is a monolithic, high-throughput scanning Michelson interferometer fabricated using deep reactive ion etching technology of silicon-on-insulator substrate. The micro-optical part is used for conditioning the input/output light to/from the MEMS and for further light direction to the detector. Thanks to the all-reflective design of the conditioning microoptics, the performance is free of chromatic aberration. Complemented by the excellent transmission properties of the silicon in the infrared region, the integrated solution allows very wide spectral range of operation. The reported sensor's spectral resolution is about 33 cm-1 and working in the range of 1270 nm to 2700 nm; upper limited by the extended InGaAs detector. The presented solution provides a low cost, low power, tiny size, wide wavelength range NIR spectral sensor that can be manufactured with extremely high volumes. All these features promise the compatibility of this technology with the forthcoming demand of smart portable and IoT devices.

A COMPARISON OF PARTICLE MASS SPECTROMETERS DURING THE 1999 ATLANTA SUPERSITES EXPERIMENT

EPA Science Inventory

During the Atlanta SuperSite Experiment, four particle mass spectrometers were operated together for the first time: NOAA's PALMS (Particle Analysis by Laser Mass Spectrometry), U. C. Riverside's ATOFMS (Aerosol Time-of-Flight Mass Spectrometry), U. Delaware's RSMS-II (Rapid Si...

Automated mass spectrometer analysis system

NASA Technical Reports Server (NTRS)

Giffin, Charles E. (Inventor); Kuppermann, Aron (Inventor); Dreyer, William J. (Inventor); Boettger, Heinz G. (Inventor)

1982-01-01

An automated mass spectrometer analysis system is disclosed, in which samples are automatically processed in a sample processor and converted into volatilizable samples, or their characteristic volatilizable derivatives. Each volatilizable sample is sequentially volatilized and analyzed in a double focusing mass spectrometer, whose output is in the form of separate ion beams all of which are simultaneously focused in a focal plane. Each ion beam is indicative of a different sample component or different fragments of one or more sample components and the beam intensity is related to the relative abundance of the sample component. The system includes an electro-optical ion detector which automatically and simultaneously converts the ion beams, first into electron beams which in turn produce a related image which is transferred to the target of a vilicon unit. The latter converts the images into electrical signals which are supplied to a data processor, whose output is a list of the components of the analyzed sample and their abundances. The system is under the control of a master control unit, which in addition to monitoring and controlling various power sources, controls the automatic operation of the system under expected and some unexpected conditions and further protects various critical parts of the system from damage due to particularly abnormal conditions.

Automated mass spectrometer analysis system

NASA Technical Reports Server (NTRS)

Boettger, Heinz G. (Inventor); Giffin, Charles E. (Inventor); Dreyer, William J. (Inventor); Kuppermann, Aron (Inventor)

1978-01-01

An automated mass spectrometer analysis system is disclosed, in which samples are automatically processed in a sample processor and converted into volatilizable samples, or their characteristic volatilizable derivatives. Each volatizable sample is sequentially volatilized and analyzed in a double focusing mass spectrometer, whose output is in the form of separate ion beams all of which are simultaneously focused in a focal plane. Each ion beam is indicative of a different sample component or different fragments of one or more sample components and the beam intensity is related to the relative abundance of the sample component. The system includes an electro-optical ion detector which automatically and simultaneously converts the ion beams, first into electron beams which in turn produce a related image which is transferred to the target of a vidicon unit. The latter converts the images into electrical signals which are supplied to a data processor, whose output is a list of the components of the analyzed sample and their abundances. The system is under the control of a master control unit, which in addition to monitoring and controlling various power sources, controls the automatic operation of the system under expected and some unexpected conditions and further protects various critical parts of the system from damage due to particularly abnormal conditions.

High-resolution crystal spectrometer for the 10-60 A extreme ultraviolet region

DOE Office of Scientific and Technical Information (OSTI.GOV)

Beiersdorfer, P.; Brown, G.V.; Goddard, R.

2004-10-01

A vacuum crystal spectrometer with nominal resolving power approaching 1000 is described for measuring emission lines with wavelength in the extreme ultraviolet region up to 60 A. The instrument utilizes a flat octadecyl hydrogen maleate crystal and a thin-window 1D position-sensitive gas proportional detector. This detector employs a 1-{mu}m-thick 100x8 mm{sup 2} aluminized polyimide window and operates at one atmosphere pressure. The spectrometer has been implemented on the Livermore electron beam ion traps. The performance of the instrument is illustrated in measurements of the newly discovered magnetic field-sensitive line in Ar{sup 8+}.

Imaging spectrometer/camera having convex grating

NASA Technical Reports Server (NTRS)

Reininger, Francis M. (Inventor)

2000-01-01

An imaging spectrometer has fore-optics coupled to a spectral resolving system with an entrance slit extending in a first direction at an imaging location of the fore-optics for receiving the image, a convex diffraction grating for separating the image into a plurality of spectra of predetermined wavelength ranges; a spectrometer array for detecting the spectra; and at least one concave sperical mirror concentric with the diffraction grating for relaying the image from the entrance slit to the diffraction grating and from the diffraction grating to the spectrometer array. In one embodiment, the spectrometer is configured in a lateral mode in which the entrance slit and the spectrometer array are displaced laterally on opposite sides of the diffraction grating in a second direction substantially perpendicular to the first direction. In another embodiment, the spectrometer is combined with a polychromatic imaging camera array disposed adjacent said entrance slit for recording said image.

Gas Ring-Imagining Cherenkov (GRINCH) Detector for the Super BigBite Spectrometer at Jefferson Lab

NASA Astrophysics Data System (ADS)

Averett, Todd; Wojtsekhowski, Bogdan; Amidouch, Abdellah; Danagoulian, Samuel; Niculescu, Gabriel; Niculescu, Ioana; Jefferson Lab SBS Collaboration Collaboration

2017-01-01

A new gas Cherenkov detector is under construction for the upcoming SuperBigBite spectrometer research program in Hall A at Jefferson Lab. The existing BigBite spectrometer is being upgraded to handle expected increases in event rate and background rate due to the increased luminosity required for the experimental program. The detector will primarily be used to separate good electron events from significant pion and electromagnetic contamination. In contrast to typical gas Cherenkov detectors that use large-diameter photomultiplier tubes and charge integrating ADCs, this detector uses an array of 510 small-diameter tubes that are more than 25x less sensitive to background. Cherenkov radiation clusters will be identified in this array using fast TDCs and a narrow timing window relative to typical ADC gates. In addition, a new FPGA-based DAQ system is being tested to provide a PID trigger using real-time cluster finding. Details of the detector and current status of the project will be presented.

Development of a ten inch manipulators-based, flexible, broadband two-crystal spectrometer

NASA Astrophysics Data System (ADS)

Steel, A. B.; Dunn, J.; Emig, J.; Beiersdorfer, P.; Brown, G. V.; Shepherd, R.; Marley, E. V.; Hoarty, D. J.

2014-11-01

We have developed and implemented a broadband X-ray spectrometer with a variable energy range for use at the Atomic Weapons Establishment's Orion Laser. The spectrometer covers an energy bandwidth of ˜1-2 keV using two independently mounted, movable Bragg diffraction crystals. Using combinations of cesium hydrogen pthlate, ammonium dihydrogen phosphate, and pentaerythritol crystals, spectra covering the 1.4-2.5, 1.85-3.15, or 3.55-5.1 keV energy bands have been measured. Image plate is used for detection owing to its high dynamic range. Background signals caused by high energy X-rays and particles commonly produced in high energy laser experiments are reduced by a series of tantalum baffles and filters installed between the source and crystal and also between the crystals and detector.

Development of a ten inch manipulators-based, flexible, broadband two-crystal spectrometer.

PubMed

Steel, A B; Dunn, J; Emig, J; Beiersdorfer, P; Brown, G V; Shepherd, R; Marley, E V; Hoarty, D J

2014-11-01

We have developed and implemented a broadband X-ray spectrometer with a variable energy range for use at the Atomic Weapons Establishment's Orion Laser. The spectrometer covers an energy bandwidth of ∼1-2 keV using two independently mounted, movable Bragg diffraction crystals. Using combinations of cesium hydrogen pthlate, ammonium dihydrogen phosphate, and pentaerythritol crystals, spectra covering the 1.4-2.5, 1.85-3.15, or 3.55-5.1 keV energy bands have been measured. Image plate is used for detection owing to its high dynamic range. Background signals caused by high energy X-rays and particles commonly produced in high energy laser experiments are reduced by a series of tantalum baffles and filters installed between the source and crystal and also between the crystals and detector.

Design of a transportable high efficiency fast neutron spectrometer

DOE PAGES

Roecker, C.; Bernstein, A.; Bowden, N. S.; ...

2016-04-12

A transportable fast neutron detection system has been designed and constructed for measuring neutron energy spectra and flux ranging from tens to hundreds of MeV. The transportability of the spectrometer reduces the detector-related systematic bias between different neutron spectra and flux measurements, which allows for the comparison of measurements above or below ground. The spectrometer will measure neutron fluxes that are of prohibitively low intensity compared to the site-specific background rates targeted by other transportable fast neutron detection systems. To measure low intensity high-energy neutron fluxes, a conventional capture-gating technique is used for measuring neutron energies above 20 MeV andmore » a novel multiplicity technique is used for measuring neutron energies above 100 MeV. The spectrometer is composed of two Gd containing plastic scintillator detectors arranged around a lead spallation target. To calibrate and characterize the position dependent response of the spectrometer, a Monte Carlo model was developed and used in conjunction with experimental data from gamma ray sources. Multiplicity event identification algorithms were developed and used with a Cf-252 neutron multiplicity source to validate the Monte Carlo model Gd concentration and secondary neutron capture efficiency. The validated Monte Carlo model was used to predict an effective area for the multiplicity and capture gating analyses. For incident neutron energies between 100 MeV and 1000 MeV with an isotropic angular distribution, the multiplicity analysis predicted an effective area of 500 cm 2 rising to 5000 cm 2. For neutron energies above 20 MeV, the capture-gating analysis predicted an effective area between 1800 cm 2 and 2500 cm 2. As a result, the multiplicity mode was found to be sensitive to the incident neutron angular distribution.« less

The CMS-TOTEM Precision Proton Spectrometer: CT-PPS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Albrow, Michael G.

The CMS-TOTEM Precison Proton Spectrometer, CT-PPS, is an approved project to add 3D silicon tracking and quartz Cherenkov timing detectors in Roman pots at z = ±204-215 m from the CMS collision point to study final states p+X + p. The central state X can be aW-pair from a photon-photon interaction, high ET jets from gluon collisions, etc., with M(X) obtained directly as well as from the two outgoing protons. The project is designed to operate at high luminosity, with up to about 50 interactions per 25 ns bunch crossing, and to be fully operational for physics in 2016.

Miniature and micro spectrometers market: who is going to catch the value?

NASA Astrophysics Data System (ADS)

Bouyé, Clémentine; d'Humières, Benoît

2017-02-01

The market of miniature and micro spectrometers is evolving fast. The technology is getting ever smaller and cheaper while keeping high performances. The market is attracting new players: spin-offs from major research institutes, large companies outside the classic spectroscopy market, software providers with innovative analytical solutions, … The goal of this involvement is to bring spectroscopy closer to the end-users and provide spectrometers able to operate on-field or in-line. The high potential of compact spectrometers is recognized for a wide variety of applications: chemistry, pharmaceutics, agro-food, agriculture, forensics, healthcare, consumer applications, … But its emergence as a large volume market faces a major bottleneck. Each application implies specific processes and analyses and specific parameters to control, i.e. a specific interpretation of the raw spectra in order to provide information usable by nonphotonic experts. Who is going to pay for that adaptation effort? Are there ways for reducing the adaptation costs, by means of selflearning algorithms and/or flexible and easily adaptable sensors? In other words, who is going to catch the value? In this article, we will investigate the potential of each major industrial application market and provide market data. We will also wonder, what are the strengths and weaknesses of the different players - spectrometer manufacturers, algorithms developers, full-systems providers, … - to catch the value of the compact spectrometer market.

Resolving the Origin of the Diffuse Soft X-ray Background

NASA Technical Reports Server (NTRS)

Smith, Randall K.; Foster, Adam R.; Edgar, Ricard J.; Brickhouse, Nancy S.; Sanders, Wilton T.

2012-01-01

In January 1993, the Diffuse X-ray Spectrometer (DXS) measured the first high-resolution spectrum of the diffuse soft X-ray background between 44-80A. A line-dominated spectrum characteristic of a 10(exp 6)K collisionally ionized plasma' was expected but while the observed spectrum was clearly line-dominated, no model would fit. Then in 2003 the Cosmic Hot Interstellar Plasma Spectrometer (CHIPS) launched and observed the diffuse extreme-ultraviolet (EUV) spectrum between 90- 265A. Although many emission lines were again expected; only Fe IX at 171.1A was detected. The discovery of X-rays from comets led to the realization that heavy ions (Z=6-28) in the solar wind will emit soft X-rays as the ions interact via charge exchange with neutral atoms in the heliosphere and geocorona. Using a new model for solar wind charge exchange (SWCX) emission, we show that the diffuse soft X-ray background can be understood as a combination of emission from charge exchange onto the slow and fast solar wind together with a more distant and diffuse hot (10(exp 6)K) plasma.

A practical superconducting-microcalorimeter X-ray spectrometer for beamline and laboratory science

DOE PAGES

Doriese, W. B.; Abbamonte, P.; Alpert, B. K.; ...

2017-05-01

-resolved scattering; accelerator-based spectroscopy of hadronic atoms and particle-induced-emission spectroscopy; laboratory-based time-resolved absorption and emission spectroscopy with a tabletop, broadband source; and laboratory-based metrology of X-ray-emission lines. Here, we discuss the design, construction, and operation of our TES spectrometers and show first-light measurements from the various systems. Finally, because X-ray-TES technology continues to mature, we discuss improvements to array size, energy resolution, and counting speed that we anticipate in our next generation of TES-X-ray spectrometers and beyond.« less

A practical superconducting-microcalorimeter X-ray spectrometer for beamline and laboratory science

DOE Office of Scientific and Technical Information (OSTI.GOV)

Doriese, W. B.; Abbamonte, P.; Alpert, B. K.

-resolved scattering; accelerator-based spectroscopy of hadronic atoms and particle-induced-emission spectroscopy; laboratory-based time-resolved absorption and emission spectroscopy with a tabletop, broadband source; and laboratory-based metrology of X-ray-emission lines. Here, we discuss the design, construction, and operation of our TES spectrometers and show first-light measurements from the various systems. Finally, because X-ray-TES technology continues to mature, we discuss improvements to array size, energy resolution, and counting speed that we anticipate in our next generation of TES-X-ray spectrometers and beyond.« less

A practical superconducting-microcalorimeter X-ray spectrometer for beamline and laboratory science

NASA Astrophysics Data System (ADS)

Doriese, W. B.; Abbamonte, P.; Alpert, B. K.; Bennett, D. A.; Denison, E. V.; Fang, Y.; Fischer, D. A.; Fitzgerald, C. P.; Fowler, J. W.; Gard, J. D.; Hays-Wehle, J. P.; Hilton, G. C.; Jaye, C.; McChesney, J. L.; Miaja-Avila, L.; Morgan, K. M.; Joe, Y. I.; O'Neil, G. C.; Reintsema, C. D.; Rodolakis, F.; Schmidt, D. R.; Tatsuno, H.; Uhlig, J.; Vale, L. R.; Ullom, J. N.; Swetz, D. S.

2017-05-01

; accelerator-based spectroscopy of hadronic atoms and particle-induced-emission spectroscopy; laboratory-based time-resolved absorption and emission spectroscopy with a tabletop, broadband source; and laboratory-based metrology of X-ray-emission lines. Here, we discuss the design, construction, and operation of our TES spectrometers and show first-light measurements from the various systems. Finally, because X-ray-TES technology continues to mature, we discuss improvements to array size, energy resolution, and counting speed that we anticipate in our next generation of TES-X-ray spectrometers and beyond.

A practical superconducting-microcalorimeter X-ray spectrometer for beamline and laboratory science.

PubMed

Doriese, W B; Abbamonte, P; Alpert, B K; Bennett, D A; Denison, E V; Fang, Y; Fischer, D A; Fitzgerald, C P; Fowler, J W; Gard, J D; Hays-Wehle, J P; Hilton, G C; Jaye, C; McChesney, J L; Miaja-Avila, L; Morgan, K M; Joe, Y I; O'Neil, G C; Reintsema, C D; Rodolakis, F; Schmidt, D R; Tatsuno, H; Uhlig, J; Vale, L R; Ullom, J N; Swetz, D S

2017-05-01

; accelerator-based spectroscopy of hadronic atoms and particle-induced-emission spectroscopy; laboratory-based time-resolved absorption and emission spectroscopy with a tabletop, broadband source; and laboratory-based metrology of X-ray-emission lines. Here, we discuss the design, construction, and operation of our TES spectrometers and show first-light measurements from the various systems. Finally, because X-ray-TES technology continues to mature, we discuss improvements to array size, energy resolution, and counting speed that we anticipate in our next generation of TES-X-ray spectrometers and beyond.

Time-resolved hard x-ray spectrometer

NASA Astrophysics Data System (ADS)

Moy, Kenneth; Cuneo, Michael; McKenna, Ian; Keenan, Thomas; Sanford, Thomas; Mock, Ray

2006-08-01

Wired array studies are being conducted at the SNL Z accelerator to maximize the x-ray generation for inertial confinement fusion targets and high energy density physics experiments. An integral component of these studies is the characterization of the time-resolved spectral content of the x-rays. Due to potential spatial anisotropy in the emitted radiation, it is also critical to diagnose the time-evolved spectral content in a space-resolved manner. To accomplish these two measurement goals, we developed an x-ray spectrometer using a set of high-speed detectors (silicon PIN diodes) with a collimated field-of-view that converged on a 1-cm-diameter spot at the pinch axis. Spectral discrimination is achieved by placing high Z absorbers in front of these detectors. We built two spectrometers to permit simultaneous different angular views of the emitted radiation. Spectral data have been acquired from recent Z shots for the radial and axial (polar) views. UNSPEC 1 has been adapted to analyze and unfold the measured data to reconstruct the x-ray spectrum. The unfold operator code, UFO2, is being adapted for a more comprehensive spectral unfolding treatment.

Results of a search for deuterium at 25-50 GC/c using a magnetic spectrometer

NASA Technical Reports Server (NTRS)

Golden, R. L.; Stephens, S. A.; Webber, W. R.

1985-01-01

A method is presented for separately identifying isotopes using a Cerenkov detector and a magnet spectrometer. Simulations of the method are given for separating deuterium from protons. The simulations are compared with data gathered from the 1979 flight of the New Mexico State University balloonborne magnet spectrometer. The simulation and the data show the same general characteristics lending credence to the technique. The data show an apparent deuteron signal which is (11 + or - 3)% of the total sample in the rigidity region 38.5 to 50 GV/c. Until further background analysis and subtraction is performed this should be regarded as an upper limit to the deuteron/(deuteron+proton) ratio.

The EBIT Calorimeter Spectrometer: A New, Permanent User Facility at the LLNL EBIT

NASA Technical Reports Server (NTRS)

Porter, S.

2007-01-01

The EBIT Calorimeter Spectrometer (ECS) has recently been completed and is currently being installed at the EBIT facility at the Lawrence Livermore National Laboratory. The ECS will replace the smaller XRS/EBIT spectrometer that has been in almost continuous operation since 2000. The XRS/EBIT was based on a spare laboratory cryostat and an engineering model detector system from the Suzaku/XRS observatory. The new ECS spectrometer was built from the ground up to be a low maintenance, high performance microcalorimeter spectrometer with 4 eV resolution at 6 keV, 32 detector channels, 10 us event timing, and capable of uninterrupted acquisition sessions of over 70 hours at 50 mK. The XRSIEBIT program has been extremely successful, producing over two-dozen refereed publications on topics such as laboratory astrophysics, atomic physics, nuclear physics, and calibration of the spectrometers for the National Ignition Facility, with many more publications in preparation. The ECS spectrometer will continue this work into the future with improved spectral resolution, integration times, and ease-of-use. We designed the ECS instrument with TES detectors in mind by using the same highly successful magnetic shielding as our laboratory TES cryostats. This design will lead to a future TES instrument at the LLNL EBIT. This proposed future instrument would include a hybrid detector system with 0.8 eV resolution in the band from 0.1-1.0 keV, 2 eV from 0.1-10 keV, and 30 eV from 0.5-100 keV, with high quantum efficiency in each band. Here we discuss the legacy of the XRS/EBIT program, the performance of the new ECS spectrometer, and plans for a future TES spectrometer.

Modular soft x-ray spectrometer for applications in energy sciences and quantum materials

DOE PAGES

Chuang, Yi -De; Shao, Yu -Cheng; Cruz, Alejandro; ...

2017-01-27

Over the past decade, the advances in grating-based soft X-ray spectrometers have revolutionized the soft X-ray spectroscopies in materials research. However, these novel spectrometers are mostly dedicated designs, which cannot be easily adopted for applications with diverging demands. Here we present a versatile spectrometer design concept based on the Hettrick-Underwood optical scheme that uses modular mechanical components. The spectrometer’s optics chamber can be used with gratings operated in either inside or outside orders, and the detector assembly can be reconfigured accordingly. The spectrometer can be designed to have high spectral resolution, exceeding 10 000 resolving power when using small sourcemore » (~1μm) and detector pixels (~5μm) with high line density gratings (~3000 lines/mm), or high throughput at moderate resolution. We report two such spectrometers with slightly different design goals and optical parameters in this paper. We show that the spectrometer with high throughput and large energy window is particularly useful for studying the sustainable energy materials. We demonstrate that the extensive resonant inelastic X-ray scattering (RIXS) map of battery cathode material LiNi 1/3Co 1/3Mn 1/3O 2 can be produced in few hours using such a spectrometer. Unlike analyzing only a handful of RIXS spectra taken at selected excitation photon energies across the elemental absorption edges to determine various spectral features like the localized dd excitations and non-resonant fluorescence emissions, these features can be easily identified in the RIXS maps. Studying such RIXS maps could reveal novel transition metal redox in battery compounds that are sometimes hard to be unambiguously identified in X-ray absorption and emission spectra. As a result, we propose that this modular spectrometer design can serve as the platform for further customization to meet specific scientific demands.« less

Modular soft x-ray spectrometer for applications in energy sciences and quantum materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chuang, Yi -De; Shao, Yu -Cheng; Cruz, Alejandro

Over the past decade, the advances in grating-based soft X-ray spectrometers have revolutionized the soft X-ray spectroscopies in materials research. However, these novel spectrometers are mostly dedicated designs, which cannot be easily adopted for applications with diverging demands. Here we present a versatile spectrometer design concept based on the Hettrick-Underwood optical scheme that uses modular mechanical components. The spectrometer’s optics chamber can be used with gratings operated in either inside or outside orders, and the detector assembly can be reconfigured accordingly. The spectrometer can be designed to have high spectral resolution, exceeding 10 000 resolving power when using small sourcemore » (~1μm) and detector pixels (~5μm) with high line density gratings (~3000 lines/mm), or high throughput at moderate resolution. We report two such spectrometers with slightly different design goals and optical parameters in this paper. We show that the spectrometer with high throughput and large energy window is particularly useful for studying the sustainable energy materials. We demonstrate that the extensive resonant inelastic X-ray scattering (RIXS) map of battery cathode material LiNi 1/3Co 1/3Mn 1/3O 2 can be produced in few hours using such a spectrometer. Unlike analyzing only a handful of RIXS spectra taken at selected excitation photon energies across the elemental absorption edges to determine various spectral features like the localized dd excitations and non-resonant fluorescence emissions, these features can be easily identified in the RIXS maps. Studying such RIXS maps could reveal novel transition metal redox in battery compounds that are sometimes hard to be unambiguously identified in X-ray absorption and emission spectra. As a result, we propose that this modular spectrometer design can serve as the platform for further customization to meet specific scientific demands.« less

A new Ion Mobility Spectrometer

NASA Astrophysics Data System (ADS)

Butler, M. A.

1998-03-01

A new ion mobility spectrometer (IMS) concept has been demonstrated that traps ions in a potential well and then moves the well down a tube to a detector. The charge remaining in the well is measured as a function of well velocity or electric field that the ion experiences; thus separating the ions by mobility. The potential wave is generated and propagated down the tube by a series of ring electrodes along the tube under real-time computer control via an array of DACs. The operating characteristics of this device have been explored including the effects of ion "lifetime," well shape, and well velocity. The ion "lifetime" results from a radial field at the bottom of the potential well that pushes the ions toward the tube wall. This work was supported by the United States Department of Energy under Contract DE-AC04-94AL85000. Sandia is a multiprogram laboratory operated by Sandia Corporation, a Lockheed Martin Company, for the United States Department of Energy.

Recent developments and applications with gas cell correlation spectrometer. [IR sensing of air pollution

NASA Technical Reports Server (NTRS)

Barringer, A. R.; Davies, J. H.; Floyd, G.

1978-01-01

Gaspec, a gas filter correlation spectrometer, is described. Gaspec is a dual-gas three-channel instrument using two detectors which receive amplitude-shared source signals modulated at the frequency of the chopper. Several units for operation around the 3-5 micron and the 8-15 micron region have been constructed, and gases such as CO2, CO, CH4, HCl, NO, and hydrazines can be detected. Advantages of Gaspec are considered with reference to improvements developed for the basic Cospec (gas cell correlation spectrometer) instrument.

Airborne volcanic plume measurements using a FTIR spectrometer, Kilauea volcano, Hawaii

USGS Publications Warehouse

McGee, K.A.; Gerlach, T.M.

1998-01-01

A prototype closed-path Fourier transform infrared spectrometer system (FTIK), operating from battery power and with a Stirling engine microcooler for detector cooling, was successfully used for airborne measurements of sulfur dioxide at Kilauea volcano. Airborne profiles of the volcanic plume emanating from the erupting Pu'u 'O'o vent on the East Rift of Kilauea revealed levels of nearly 3 ppm SO2 in the core of the plume. An emission rate of 2,160 metric tons per day of sulfur dioxide was calculated from the FTIR data, which agrees closely with simultaneous measurements by a correlation spectrometer (COSPEC). The rapid spatial sampling possible from an airborne platform distinguishes the methodology described here from previous FTIR measurements.

[Optimum design of imaging spectrometer based on toroidal uniform-line-spaced (TULS) spectrometer].

PubMed

Xue, Qing-Sheng; Wang, Shu-Rong

2013-05-01

Based on the geometrical aberration theory, a optimum-design method for designing an imaging spectrometer based on toroidal uniform grating spectrometer is proposed. To obtain the best optical parameters, twice optimization is carried out using genetic algorithm(GA) and optical design software ZEMAX A far-ultraviolet(FUV) imaging spectrometer is designed using this method. The working waveband is 110-180 nm, the slit size is 50 microm x 5 mm, and the numerical aperture is 0.1. Using ZEMAX software, the design result is analyzed and evaluated. The results indicate that the MTF for different wavelengths is higher than 0.7 at Nyquist frequency 10 lp x mm(-1), and the RMS spot radius is less than 14 microm. The good imaging quality is achieved over the whole working waveband, the design requirements of spatial resolution 0.5 mrad and spectral resolution 0.6 nm are satisfied. It is certificated that the optimum-design method proposed in this paper is feasible. This method can be applied in other waveband, and is an instruction method for designing grating-dispersion imaging spectrometers.

Overseas Contingency Operations Funding: Background and Status

DTIC Science & Technology

2017-02-07

emergency” or “Overseas Contingency Operation/ Global War on Terror” (OCO/GWOT) requirement in annual agency budget requests—or both. Funds designated as...to be excluded from budget control limits. The BCA added the designation “Overseas Contingency Operation/ Global War on Terror” to the BBEDCA...been largely provided through supplemental appropriation acts or has been designated as an “emergency” or “overseas contingency operation/ global war on

Solar minimum Lyman alpha sky background observations from Pioneer Venus orbiter ultraviolet spectrometer - Solar wind latitude variation

NASA Technical Reports Server (NTRS)

Ajello, J. M.

1990-01-01

Measurements of interplanetary H I Lyman alpha over a large portion of the celestial sphere were made at the recent solar minimum by the Pioneer Venus orbiter ultraviolet spectrometer. These measurements were performed during a series of spacecraft maneuvers conducted to observe Halley's comet in early 1986. Analysis of these data using a model of the passage of interstellar wind hydrogen through the solar system shows that the rate of charge exchange with solar wind protons is 30 percent less over the solar poles than in the ecliptic. This result is in agreement with a similar experiment performed with Mariner 10 at the previous solar minimum.

A Fully Redundant On-Line Mass Spectrometer System Used to Monitor Cryogenic Fuel Leaks on the Space Shuttle

NASA Technical Reports Server (NTRS)

Griffin, T. P.; Naylor, G. R.; Haskell, W. D.; Breznik, G. S.; Mizell, C. A.; Steinrock, Todd (Technical Monitor)

2001-01-01

This paper presents an on-line mass spectrometer designed to monitor for cryogenic leaks on the Space Shuttle. The topics include: 1) Hazardous Gas Detection Lab; 2) LASRE Test Support; 3) Background; 4) Location of Systems; 5) Sample Lines for Gas Detection; 6) Problems with Current Systems; 7) Requirements for New System (Nitrogen and Helium Background); and 8) HGDS 2000. This paper is in viewgraph form.

A Compton scatter attenuation gamma ray spectrometer

NASA Technical Reports Server (NTRS)

Austin, W. E.

1972-01-01

A Compton scatter attenuation gamma ray spectrometer conceptual design is discussed for performing gamma spectral measurements in monodirectional gamma fields from 100 R per hour to 1,000,000 R per hour. Selectable Compton targets are used to scatter gamma photons onto an otherwise heavily shielded detector with changeable scattering efficiencies such that the count rate is maintained between 500 and 10,000 per second. Use of two sum-Compton coincident detectors, one for energies up to 1.5 MeV and the other for 600 keV to 10 MeV, will allow good peak to tail pulse height ratios to be obtained over the entire spectrum and reduces the neutron recoil background rate.

Spectrometers for compact neutron sources

NASA Astrophysics Data System (ADS)

Voigt, J.; Böhm, S.; Dabruck, J. P.; Rücker, U.; Gutberlet, T.; Brückel, T.

2018-03-01

We discuss the potential for neutron spectrometers at novel accelerator driven compact neutron sources. Such a High Brilliance Source (HBS) relies on low energy nuclear reactions, which enable cryogenic moderators in very close proximity to the target and neutron optics at comparably short distances from the moderator compared to existing sources. While the first effect aims at increasing the phase space density of a moderator, the second allows the extraction of a large phase space volume, which is typically requested for spectrometer applications. We find that competitive spectrometers can be realized if (a) the neutron production rate can be synchronized with the experiment repetition rate and (b) the emission characteristics of the moderator can be matched to the phase space requirements of the experiment. MCNP simulations for protons or deuterons on a Beryllium target with a suitable target/moderator design yield a source brightness, from which we calculate the sample fluxes by phase space considerations for different types of spectrometers. These match closely the figures of todays spectrometers at medium flux sources. Hence we conclude that compact neutron sources might be a viable option for next generation neutron sources.

The cold neutron chopper spectrometer at the Spallation Neutron Source—A review of the first 8 years of operation

DOE PAGES

Ehlers, G.; Podlesnyak, A. A.; Kolesnikov, A. I.

2016-09-13

The first eight years of operation of the Cold Neutron Chopper Spectrometer (CNCS) at the Spallation Neutron Source in Oak Ridge is being reviewed. The instrument has been part of the facility user program since 2009, and more than 250 individual user experiments have been performed to date. CNCS is an extremely powerful and versatile instrument and offers leading edge performance in terms of beam intensity, energy resolution, and flexibility to trade one for another. In addition, experiments are being routinely performed with the sample at extreme conditions: T ≲ 0.05 K, p ≳ 2 GPa, and B = 8more » T can be achieved individually or in combination. In particular, CNCS is in a position to advance the state of the art with inelastic neutron scattering under pressure, and some of the recent accomplishments in this area will be presented in more detail.« less

Operating modes and cooling capabilities of the 3-stage ADR developed for the Soft-X-ray Spectrometer instrument on Astro-H

NASA Astrophysics Data System (ADS)

Shirron, Peter J.; Kimball, Mark O.; James, Bryan L.; Muench, Theodore; DiPirro, Michael J.; Letmate, Richard V.; Sampson, Michael A.; Bialas, Tom G.; Sneiderman, Gary A.; Porter, Frederick S.; Kelley, Richard L.

2016-03-01

A 3-stage adiabatic demagnetization refrigerator (ADR) (Shirron et al., 2012) is used on the Soft X-ray Spectrometer instrument (Mitsuda et al., 2010) on Astro-H (Takahashi et al., 2010) [3] to cool a 6 × 6 array of X-ray microcalorimeters to 50 mK. The ADR is supported by a cryogenic system (Fujimoto et al., 2010) consisting of a superfluid helium tank, a 4.5 K Joule-Thomson (JT) cryocooler, and additional 2-stage Stirling cryocoolers that pre-cool the JT cooler and cool radiation shields within the cryostat. The ADR is configured so that it can use either the liquid helium or the JT cryocooler as its heat sink, giving the instrument an unusual degree of tolerance for component failures or degradation in the cryogenic system. The flight detector assembly, ADR and dewar were integrated into the flight dewar in early 2014, and have since been extensively characterized and calibrated. This paper summarizes the operation and performance of the ADR in all of its operating modes.

Dual mode ion mobility spectrometer and method for ion mobility spectrometry

DOEpatents

Scott, Jill R [Idaho Falls, ID; Dahl, David A [Idaho Falls, ID; Miller, Carla J [Idaho Falls, ID; Tremblay, Paul L [Idaho Falls, ID; McJunkin, Timothy R [Idaho Falls, ID

2007-08-21

Ion mobility spectrometer apparatus may include an ion interface that is operable to hold positive and negative ions and to simultaneously release positive and negative ions through respective positive and negative ion ports. A first drift chamber is operatively associated with the positive ion port of the ion interface and encloses an electric field therein. A first ion detector operatively associated with the first drift chamber detects positive ions from the first drift chamber. A second drift chamber is operatively associated with the negative ion port of the ion interface and encloses an electric field therein. A second ion detector operatively associated with the second drift chamber detects negative ions from said second drift chamber.

Non-destructive ion trap mass spectrometer and method

DOEpatents

Frankevich, Vladimir E.; Soni, Manish H.; Nappi, Mario; Santini, Robert E.; Amy, Jonathan W.; Cooks, Robert G.

1997-01-01

The invention relates to an ion trap mass spectrometer of the type having an ion trapping volume defined by spaced end caps and a ring electrode. The ion trap includes a small sensing electrode which senses characteristic motion of ions trapped in said trapping volume and provides an image current. Ions are excited into characteristic motion by application of an excitation pulse to the trapped ions. The invention also relates to a method of operating such an ion trap.

Combined VIS-IR spectrometer with vertical probe beam

NASA Astrophysics Data System (ADS)

Protopopov, V.

2017-12-01

A prototype of a combined visible-infrared spectrometer with a vertical probe beam is designed and tested. The combined spectral range is 0.4-20 μ with spatial resolution 1 mm. Basic features include the ability to measure both visibly transparent and opaque substances, as well as buried structures, such as in semiconductor industry; horizontal orientation of a sample, including semiconductor wafers; and reflection mode of operation, delivering twice the sensitivity compared to the transmission mode.

Method for calibrating mass spectrometers

DOEpatents

Anderson, Gordon A [Benton City, WA; Brands, Michael D [Richland, WA; Bruce, James E [Schwenksville, PA; Pasa-Tolic, Ljiljana [Richland, WA; Smith, Richard D [Richland, WA

2002-12-24

A method whereby a mass spectra generated by a mass spectrometer is calibrated by shifting the parameters used by the spectrometer to assign masses to the spectra in a manner which reconciles the signal of ions within the spectra having equal mass but differing charge states, or by reconciling ions having known differences in mass to relative values consistent with those known differences. In this manner, the mass spectrometer is calibrated without the need for standards while allowing the generation of a highly accurate mass spectra by the instrument.

PDS4 vs PDS3 - A Comparison of PDS Data for Two Mars Rovers - Existing Mars Curiosity Mission Mass Spectrometer (SAM) PDS3 Data vs Future ExoMars Rover Mass Spectrometer (MOMA) PDS4 Data

NASA Astrophysics Data System (ADS)

Lyness, E.; Franz, H. B.; Prats, B.

2017-12-01

The Sample Analysis at Mars (SAM) instrument is a suite of instruments on Mars aboard the Mars Science Laboratory rover. Centered on a mass spectrometer, SAM delivers its data to the PDS Atmosphere's node in PDS3 format. Over five years on Mars the process of operating SAM has evolved and extended significantly from the plan in place at the time the PDS3 delivery specification was written. For instance, SAM commonly receives double or even triple sample aliquots from the rover's drill. SAM also stores samples in spare cups for long periods of time for future analysis. These unanticipated operational changes mean that the PDS data deliveries are absent some valuable metadata without which the data can be confusing. The Mars Organic Molecule Analyzer (MOMA) instrument is another suite of instruments centered on a mass spectrometer bound for Mars. MOMA is part of the European ExoMars rover mission schedule to arrive on Mars in 2021. While SAM and MOMA differ in some important scientific ways - MOMA uses an linear ion trap compared to the SAM quadropole mass spectrometer and MOMA has a laser desorption experiment that SAM lacks - the data content from the PDS point of view is comparable. Both instruments produce data containing mass spectra acquired from solid samples collected on the surface of Mars. The MOMA PDS delivery will make use of PDS4 improvements to provide a metadata context to the data. The MOMA PDS4 specification makes few assumptions of the operational processes. Instead it provides a means for the MOMA operators to provide the important contextual metadata that was unanticipated during specification development. Further, the software tools being developed for instrument operators will provide a means for the operators to add this crucial metadata at the time it is best know - during operations.

A firmware-defined digital direct-sampling NMR spectrometer for condensed matter physics

DOE Office of Scientific and Technical Information (OSTI.GOV)

Pikulski, M., E-mail: marekp@ethz.ch; Shiroka, T.; Ott, H.-R.

2014-09-15

We report on the design and implementation of a new digital, broad-band nuclear magnetic resonance (NMR) spectrometer suitable for probing condensed matter. The spectrometer uses direct sampling in both transmission and reception. It relies on a single, commercially-available signal processing device with a user-accessible field-programmable gate array (FPGA). Its functions are defined exclusively by the FPGA firmware and the application software. Besides allowing for fast replication, flexibility, and extensibility, our software-based solution preserves the option to reuse the components for other projects. The device operates up to 400 MHz without, and up to 800 MHz with undersampling, respectively. Digital down-conversion with ±10 MHzmore » passband is provided on the receiver side. The system supports high repetition rates and has virtually no intrinsic dead time. We describe briefly how the spectrometer integrates into the experimental setup and present test data which demonstrates that its performance is competitive with that of conventional designs.« less

Miniature spectrometer and multispectral imager as a potential diagnostic aid in dermatology

NASA Astrophysics Data System (ADS)

Zeng, Haishan; MacAulay, Calum E.; McLean, David I.; Lui, Harvey; Palcic, Branko

1995-04-01

A miniature spectrometer system has been constructed for both reflectance and autofluorescence spectral measurements of skin. The system is based on PC plug-in spectrometer, therefore, it is miniature and easy to operate. The spectrometer has been used clinically to collect spectral data from various skin lesions including skin cancer. To date, 48 patients with a total of 71 diseased skin sites have been measured. Analysis of these preliminary data suggests that unique spectral characteristics exist for certain types of skin lesions, i.e. seborrheic keratosis, psoriasis, etc.. These spectral characteristics will help the differential diagnosis in Dermatology practice. In conjunction with the spectral point measurements, we are building and testing a multispectral imaging system to measure the spatial distribution of skin reflectance and autofluorescence. Preliminary results indicate that a cutaneous squamous cell carcinoma has a weak autofluorescence signal at the edge of the lesion, but a higher autofluorescence signal in the central area.

A firmware-defined digital direct-sampling NMR spectrometer for condensed matter physics.

PubMed

Pikulski, M; Shiroka, T; Ott, H-R; Mesot, J

2014-09-01

We report on the design and implementation of a new digital, broad-band nuclear magnetic resonance (NMR) spectrometer suitable for probing condensed matter. The spectrometer uses direct sampling in both transmission and reception. It relies on a single, commercially-available signal processing device with a user-accessible field-programmable gate array (FPGA). Its functions are defined exclusively by the FPGA firmware and the application software. Besides allowing for fast replication, flexibility, and extensibility, our software-based solution preserves the option to reuse the components for other projects. The device operates up to 400 MHz without, and up to 800 MHz with undersampling, respectively. Digital down-conversion with ±10 MHz passband is provided on the receiver side. The system supports high repetition rates and has virtually no intrinsic dead time. We describe briefly how the spectrometer integrates into the experimental setup and present test data which demonstrates that its performance is competitive with that of conventional designs.

Engine spectrometer probe and method of use

NASA Technical Reports Server (NTRS)

Barkhoudarian, Sarkis (Inventor); Kittinger, Scott A. (Inventor)

2006-01-01

The engine spectrometer probe and method of using the same of the present invention provides a simple engine spectrometer probe which is both lightweight and rugged, allowing an exhaust plume monitoring system to be attached to a vehicle, such as the space shuttle. The engine spectrometer probe can be mounted to limit exposure to the heat and debris of the exhaust plume. The spectrometer probe 50 comprises a housing 52 having an aperture 55 and a fiber optic cable 60 having a fiber optic tip 65. The fiber optic tip 65 has an acceptance angle 87 and is coupled to the aperture 55 so that the acceptance angle 87 intersects the exhaust plume 30. The spectrometer probe can generate a spectrum signal from light in the acceptance angle 506 and the spectrum signal can be provided to a spectrometer 508.

Development of an ion time-of-flight spectrometer for neutron depth profiling

NASA Astrophysics Data System (ADS)

Cetiner, Mustafa Sacit

electric field accelerates and then decelerates the emitted secondary electron beam, the magnetic field steers the beam away from the source and focuses it onto the electron microchannel plate detector. The initial momentum distribution of the electron beam is observed to have profound effect on the electron transport time. Hence, the CEM field spectrometer measurements suffer more from spectral broadening at similar operating parameters. The CEM field spectrometer measurements were obtained with a 210Po alpha source at the Penn State Radiation Science and Engineering Center, University Park, PA. Although the PEM field spectrometer suffers less from electron transport time dispersion, the CEM field spectrometer is more suited for application to neutron depth profiling. The multiple small-diameter apertures used in the PEM field configuration considerably reduces the geometric efficiency of the spectrometer. Most of the neutron depth profiling measurements, where isotropic emission of charged particles is observed, have relatively low count rates; hence, high detection efficiency is essential.

[Raman spectroscopy fluorescence background correction and its application in clustering analysis of medicines].

PubMed

Chen, Shan; Li, Xiao-ning; Liang, Yi-zeng; Zhang, Zhi-min; Liu, Zhao-xia; Zhang, Qi-ming; Ding, Li-xia; Ye, Fei

2010-08-01

During Raman spectroscopy analysis, the organic molecules and contaminations will obscure or swamp Raman signals. The present study starts from Raman spectra of prednisone acetate tablets and glibenclamide tables, which are acquired from the BWTek i-Raman spectrometer. The background is corrected by R package baselineWavelet. Then principle component analysis and random forests are used to perform clustering analysis. Through analyzing the Raman spectra of two medicines, the accurate and validity of this background-correction algorithm is checked and the influences of fluorescence background on Raman spectra clustering analysis is discussed. Thus, it is concluded that it is important to correct fluorescence background for further analysis, and an effective background correction solution is provided for clustering or other analysis.

a Low-Cost Chirped-Pulse Fourier Transform Microwave Spectrometer for Undergraduate Physical Chemistry Lab

NASA Astrophysics Data System (ADS)

Carroll, Brandon; Finneran, Ian; Blake, Geoffrey

2014-06-01

We present the design and construction of a simple and low-cost waveguide chirped pulse Fourier transform microwave (CP-FTMW) spectrometer suitable for gas-phase rotational spectroscopy experiments in undergraduate physical chemistry labs as well as graduate level research. The spectrometer operates with modest bandwidth, using phased locked loop (PLL) microwave sources and a direct digital synthesis (DDS) chirp source, making it an affordable for undergraduate labs. The performance of the instrument is benchmarked by acquiring the pure rotational spectrum of the J = 1 - 0 transition OCS and its isotopologues from 11-12.5 GHz.

Particulate contamination spectrometer. Volume 1: Technical report

NASA Technical Reports Server (NTRS)

Schmitt, R. J.; Boyd, B. A.; Linford, R. M. F.

1975-01-01

A laser particulate spectrometer (LPS) system was developed to measure the size and speed distributions of particulate (dusts, aerosols, ice particles, etc.) contaminants. Detection of the particulates was achieved by means of light scattering and extinction effects using a single laser beam to cover a size range of 0.8 to 275 microns diameter and a speed range of 0.2 to 20 meter/second. The LPS system was designed to operate in the high vacuum environment of a space simulation chamber with cold shroud temperatures ranging from 77 to 300 K.

Experiment S-191 visible and infrared spectrometer

NASA Technical Reports Server (NTRS)

Linnell, E. R.

1974-01-01

The design, development, fabrication test, and utilization of the visible and infrared spectrometer portion of the S-191 experiment, part of the Earth Resources Experiment Package, on board Skylab is discussed. The S-191 program is described, as well as conclusions and recommendations for improvement of this type of instrument for future applications. Design requirements, instrument design approaches, and the test verification program are presented along with test results, including flight hardware calibration data. A brief discussion of operation during the Skylab mission is included. Documentation associated with the program is listed.

Development of a new linearly variable edge filter (LVEF)-based compact slit-less mini-spectrometer

NASA Astrophysics Data System (ADS)

Mahmoud, Khaled; Park, Seongchong; Lee, Dong-Hoon

2018-02-01

This paper presents the development of a compact charge-coupled detector (CCD) spectrometer. We describe the design, concept and characterization of VNIR linear variable edge filter (LVEF)- based mini-spectrometer. The new instrument has been realized for operation in the 300 nm to 850 nm wavelength range. The instrument consists of a linear variable edge filter in front of CCD array. Low-size, light-weight and low-cost could be achieved using the linearly variable filters with no need to use any moving parts for wavelength selection as in the case of commercial spectrometers available in the market. This overview discusses the main components characteristics, the main concept with the main advantages and limitations reported. Experimental characteristics of the LVEFs are described. The mathematical approach to get the position-dependent slit function of the presented prototype spectrometer and its numerical de-convolution solution for a spectrum reconstruction is described. The performance of our prototype instrument is demonstrated by measuring the spectrum of a reference light source.

MEMS based digital transform spectrometers

NASA Astrophysics Data System (ADS)

Geller, Yariv; Ramani, Mouli

2005-09-01

Earlier this year, a new breed of Spectrometers based on Micro-Electro-Mechanical-System (MEMS) engines has been introduced to the commercial market. The use of these engines combined with transform mathematics, produces powerful spectrometers at unprecedented low cost in various spectral regions.

Feasibility study of SiGHT: a novel ultra low background photosensor for low temperature operation

DOE PAGES

Wang, Y.; Fan, A.; Fiorillo, G.; ...

2017-02-27

Rare event search experiments, such as those searching for dark matter and observations of neutrinoless double beta decay, require ultra low levels of radioactive background for unmistakable identification. In order to reduce the radioactive background of detectors used in these types of event searches, low background photosensors are required, as the physical size of these detectors become increasing larger, and hence the number of such photosensors used also increases rapidly. Considering that most dark matter and neutrinoless double beta decay experiments are turning towards using noble liquids as the target choice, liquid xenon and liquid argon for instance, photosensors thatmore » can work well at cryogenic temperatures are required, 165 K and 87 K for liquid xenon and liquid argon, respectively. The Silicon Geiger Hybrid Tube (SiGHT) is a novel photosensor designed specifically for use in ultra low background experiments operating at cryogenic temperatures. It is based on the proven photocathode plus silicon photomultiplier (SiPM) hybrid technology and consists of very few other, but also ultra radio-pure, materials like fused silica and silicon for the SiPM. Lastly, the introduction of the SiGHT concept, as well as a feasibility study for its production, is reported in this article.« less

Effect of cessation of beef cattle pasture-feedlot type backgrounding operation on the persistence of antibiotic resistance genes in the environment

USDA-ARS?s Scientific Manuscript database

Introduction It is not known how removal of cattle from a backgrounding operation will affect the persistence of antibiotic resistance genes (ARGs) in the environment. Our objective was to investigate the effect of destocking on the persistence and distribution of ARGs in the backgrounding environm...

Sample rotating turntable kit for infrared spectrometers

DOEpatents

Eckels, Joel Del [Livermore, CA; Klunder, Gregory L [Oakland, CA

2008-03-04

An infrared spectrometer sample rotating turntable kit has a rotatable sample cup containing the sample. The infrared spectrometer has an infrared spectrometer probe for analyzing the sample and the rotatable sample cup is adapted to receive the infrared spectrometer probe. A reflectance standard is located in the rotatable sample cup. A sleeve is positioned proximate the sample cup and adapted to receive the probe. A rotator rotates the rotatable sample cup. A battery is connected to the rotator.

First operations of the SOIR occultation infrared spectrometer in Venus orbit.

NASA Astrophysics Data System (ADS)

Nevejans, D.; Neefs, E.; Vandaele, A. C.; Muller, C.; Fussen, D.; Berkenbosch, S.; Clairquin, R.; Korablev, O.; Federova, A.; Bertaux, J. L.

Since May 2006, the Venus-Express spacecraft is in its nominal orbit around VENUS and the SPICAV optical package has begun to acquire spectra. The SOIR extension to SPICAV is an echelle spectrometer associated to an AOTF (Acousto-Optical Tunable Filter) for the order selection, which performs solar occultation measurements in the IR region (2.2-4.3 µm) at a resolution of 0.1 cm-1 . The detailed optical study and design as well as the manufacturing were performed at the BIRA/IASB in collaboration with its industrial partners OIP and PEDEO. It was funded by the Belgian Federal Science Policy Office under the ESA PRODEX programme. The wavelength range allows a detailed chemical inventory of the Venus atmosphere above the cloud layer with an emphasis on vertical distribution of gases. The first results look promising and will be qualitatively presented.

Electro-Optical Imaging Fourier-Transform Spectrometer

NASA Technical Reports Server (NTRS)

Chao, Tien-Hsin; Zhou, Hanying

2006-01-01

An electro-optical (E-O) imaging Fourier-transform spectrometer (IFTS), now under development, is a prototype of improved imaging spectrometers to be used for hyperspectral imaging, especially in the infrared spectral region. Unlike both imaging and non-imaging traditional Fourier-transform spectrometers, the E-O IFTS does not contain any moving parts. Elimination of the moving parts and the associated actuator mechanisms and supporting structures would increase reliability while enabling reductions in size and mass, relative to traditional Fourier-transform spectrometers that offer equivalent capabilities. Elimination of moving parts would also eliminate the vibrations caused by the motions of those parts. Figure 1 schematically depicts a traditional Fourier-transform spectrometer, wherein a critical time delay is varied by translating one the mirrors of a Michelson interferometer. The time-dependent optical output is a periodic representation of the input spectrum. Data characterizing the input spectrum are generated through fast-Fourier-transform (FFT) post-processing of the output in conjunction with the varying time delay.

21 Tesla Fourier Transform Ion Cyclotron Resonance Mass Spectrometer Greatly Expands Mass Spectrometry Toolbox

NASA Astrophysics Data System (ADS)

Shaw, Jared B.; Lin, Tzu-Yung; Leach, Franklin E.; Tolmachev, Aleksey V.; Tolić, Nikola; Robinson, Errol W.; Koppenaal, David W.; Paša-Tolić, Ljiljana

2016-12-01

We provide the initial performance evaluation of a 21 Tesla Fourier transform ion cyclotron resonance mass spectrometer operating at the Environmental Molecular Sciences Laboratory at the Pacific Northwest National Laboratory. The spectrometer constructed for the 21T system employs a commercial dual linear ion trap mass spectrometer coupled to a FTICR spectrometer designed and built in-house. Performance gains from moving to higher magnetic field strength are exemplified by the measurement of peptide isotopic fine structure, complex natural organic matter mixtures, and large proteins. Accurate determination of isotopic fine structure was demonstrated for doubly charged Substance P with minimal spectral averaging, and 8158 molecular formulas assigned to Suwannee River Fulvic Acid standard with root-mean-square (RMS) error of 10 ppb. We also demonstrated superior performance for intact proteins; namely, broadband isotopic resolution of the entire charge state distribution of apo-transferrin (78 kDa) and facile isotopic resolution of monoclonal antibody under a variety of acquisition parameters (e.g., 6 s time-domains with absorption mode processing yielded resolution of approximately 1 M at m/z = 2700).

21 Tesla Fourier Transform Ion Cyclotron Resonance Mass Spectrometer Greatly Expands Mass Spectrometry Toolbox

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shaw, Jared B.; Lin, Tzu-Yung; Leach, Franklin E.

We provide the initial performance evaluation of a 21 Tesla Fourier transform ion cyclotron resonance mass spectrometer operating at the Environmental Molecular Sciences Laboratory at Pacific Northwest National Laboratory. The spectrometer constructed for the 21T system employs a commercial dual linear ion trap mass spectrometer coupled to a FTICR spectrometer designed and built in-house. Performance gains from moving to higher magnetic field strength are exemplified by the measurement of peptide isotopic fine structure, complex natural organic matter mixtures, and large proteins. Accurate determination of isotopic fine structure was demonstrated for doubly charged substance P with minimal spectral averaging, and 8,158more » molecular formulas assigned to Suwannee River Fulvic Acid standard with RMS error of 10 ppb. We also demonstrated superior performance for intact proteins; namely, broadband isotopic resolution of the entire charge state distribution of apotransferrin (78 kDa) and facile isotopic resolution of monoclonal antibody under a variety of acquisition parameters (e.g. 6 s time-domains with absorption mode processing yielded resolution of approximately 1M at m/z =2,700).« less

Portable laser-induced breakdown spectroscopy/diffuse reflectance hybrid spectrometer for analysis of inorganic pigments

NASA Astrophysics Data System (ADS)

Siozos, Panagiotis; Philippidis, Aggelos; Anglos, Demetrios

2017-11-01

A novel, portable spectrometer, combining two analytical techniques, laser-induced breakdown spectroscopy (LIBS) and diffuse reflectance spectroscopy, was developed with the aim to provide an enhanced instrumental and methodological approach with regard to the analysis of pigments in objects of cultural heritage. Technical details about the hybrid spectrometer and its operation are presented and examples are given relevant to the analysis of paint materials. Both LIBS and diffuse reflectance spectra in the visible and part of the near infrared, corresponding to several neat mineral pigment samples, were recorded and the complementary information was used to effectively distinguish different types of pigments even if they had similar colour or elemental composition. The spectrometer was also employed in the analysis of different paints on the surface of an ancient pottery sherd demonstrating the capabilities of the proposed hybrid diagnostic approach. Despite its instrumental simplicity and compact size, the spectrometer is capable of supporting analytical campaigns relevant to archaeological, historical or art historical investigations, particularly when quick data acquisition is required in the context of surveys of large numbers of objects and samples.

FY16 Safeguards Technology Cart-Portable Mass Spectrometer Project Final Report

DOE Office of Scientific and Technical Information (OSTI.GOV)

Thompson, Cyril V.; Whitten, William B.

The Oak Ridge National Laboratory project for the Next Generation Safeguards Initiative Safeguards Technology Development Subprogram has been involved in the development of a cart portable mass spectrometer based on a Thermo ITQ ion trap mass spectrometer (referred to simply as the ITQ) for the field analysis of 235U/238U ratios in UF6. A recent discovery of the project was that combining CO2 with UF6 and introducing the mixture to the mass spectrometer (MS) appeared to increase the ionization efficiency and, thus, reduce the amount of UF6 needed for an analysis while also reducing the corrosive effects of the sample. However,more » initial experimentation indicated that mixing parameters should be closely controlled to ensure reproducible results. To this end, a sample manifold (SM) that would ensure the precise mixing of UF6 and CO2 was designed and constructed. A number of experiments were outlined and conducted to determine optimum MS and SM conditions which would provide the most stable isotope ratio analysis. The principal objective of the project was to provide a retrofit ITQ mass spectrometer operating with a SM capable of achieving a variation in precision of less than 1% over 1 hour of sampling. This goal was achieved by project end with a variation in precision of 0.5 to 0.8% over 1 hour of sampling.« less

Wide-Field Ultraviolet Spectrometer for Planetary Exospheres and Thermospheres

NASA Astrophysics Data System (ADS)

Fillingim, M. O.; Wishnow, E. H.; Miller, T.; Edelstein, J.; Lillis, R. J.; Korpela, E.; England, S.; Shourt, W. V.; Siegmund, O.; McPhate, J.; Courtade, S.; Curtis, D. W.; Deighan, J.; Chaffin, M.; Harmoul, A.; Almatroushi, H. R.

2016-12-01

Understanding the composition, structure, and variability of a planet's upper atmosphere - the exosphere and thermosphere - is essential for understanding how the upper atmosphere is coupled to the lower atmosphere, magnetosphere and near-space environment, and the Sun. Ultraviolet spectroscopy can directly observe emissions from constituents in the exosphere and thermosphere. From such observations, the structure, composition, and variability can be determined.We will present the preliminary design for a wide field ultraviolet imaging spectrometer for remote sensing of planetary atmospheres. The imaging spectrometer achieves an extremely large instantaneous 110 degree field of view with no moving scanning mirror. The imaging resolution is very appropriate for extended atmospheric emission studies, with a resolution of better than 0.3 degrees at the center to 0.4 degrees at the edges of the field. The spectral range covers 120 - 170 nm, encompassing emissions from H, O, C, N, CO, and N2, with an average spectral resolution of 1.5 nm. The instrument is composed of a 2-element wide-field telescope, a 3-element Offner spectrometer, and a sealed MCP detector system contained within a compact volume of about 40 x 25 x 20 cm. We will present the optical and mechanical design as well as the predicted optical performance.The wide instantaneous FOV simplifies instrument and spacecraft operations by removing the need for multiple scans (either from a scan mirror or spacecraft slews) to cover the regions of interest. This instrumentation can allow for two-dimensional spectral information to be built up with simple spacecraft operation or just using spacecraft motion. Applications to the terrestrial geocorona and thermosphere will be addressed as well as applications to the upper atmospheres of other planetary objects.

System Design and Implementation of the Detector Assembly of the Astro-H Soft X-Ray Spectrometer

NASA Technical Reports Server (NTRS)

Chiao, M. P.; Adams, J.; Goodwin, P.; Hobson, C.W.; Kelley, R. L.; Kilbourne, C. A.; McCammom, D.; McGuinness, D. S.; Moseley, S. J.; Porter, F. S.;

NIST Calibration of a Neutron Spectrometer ROSPEC.

PubMed

Heimbach, Craig

2006-01-01

A neutron spectrometer was acquired for use in the measurement of National Institute of Standards and Technology neutron fields. The spectrometer included options for the measurement of low and high energy neutrons, for a total measurement range from 0.01 eV up to 17 MeV. The spectrometer was evaluated in calibration fields and was used to determine the neutron spectrum of an Americium-Beryllium neutron source. The calibration fields used included bare and moderated (252)Cf, monoenergetic neutron fields of 2.5 MeV and 14 MeV, and a thermal-neutron beam. Using the calibration values determined in this exercise, the spectrometer gives a good approximation of the neutron spectrum, and excellent values for neutron fluence, for all NIST calibration fields. The spectrometer also measured an Americium-Beryllium neutron field in a NIST exposure facility and determined the field quite well. The spectrometer measured scattering effects in neutron spectra which previously could be determined only by calculation or integral measurements.

Scientific Payload Of The Emirates Mars Mission: Emirates Mars Infrared Spectrometer (Emirs) Overview.

NASA Astrophysics Data System (ADS)

Altunaiji, E. S.; Edwards, C. S.; Christensen, P. R.; Smith, M. D.; Badri, K. M., Sr.

2017-12-01

The Emirates Mars Mission (EMM) will launch in 2020 to explore the dynamics in the atmosphere of Mars on a global scale. EMM has three scientific instruments to an improved understanding of circulation and weather in the Martian lower and middle atmosphere. Two of the EMM's instruments, which are the Emirates eXploration Imager (EXI) and Emirates Mars Infrared Spectrometer (EMIRS) will focus on the lower atmosphere observing dust, ice clouds, water vapor and ozone. On the other hand, the third instrument Emirates Mars Ultraviolet Spectrometer (EMUS) will focus on both the thermosphere of the planet and its exosphere. The EMIRS instrument, shown in Figure 1, is an interferometric thermal infrared spectrometer that is jointly developed by Arizona State University (ASU) and Mohammed Bin Rashid Space Centre (MBRSC). It builds on a long heritage of thermal infrared spectrometers designed, built, and managed, by ASU's Mars Space Flight Facility, including the Thermal Emission Spectrometer (TES), Miniature Thermal Emission Spectrometer (Mini-TES), and the OSIRIS-REx Thermal Emission Spectrometer (OTES). EMIRS operates in the 6-40+ µm range with 5 cm-1 spectral sampling, enabled by a Chemical Vapor-Deposited (CVD) diamond beamsplitter and state of the art electronics. This instrument utilizes a 3×3 detector array and a scan mirror to make high-precision infrared radiance measurements over most of a Martian hemisphere. The EMIRS instrument is optimized to capture the integrated, lower-middle atmosphere dynamics over a Martian hemisphere and will capture 60 global images per week ( 20 images per orbit) at a resolution of 100-300 km/pixel. After processing through an atmospheric retrieval algorithm, EMIRS will determine the vertical temperature profiles to 50km altitude and measure the column integrated global distribution and abundances of key atmospheric parameters (e.g. dust, water ice (clouds) and water vapor) over the Martian day, seasons and year.

Skylab S191 visible-infrared spectrometer. [in Earth Resources Experiment Package

NASA Technical Reports Server (NTRS)

Barnett, T. L.; Juday, R. D.

1977-01-01

The paper describes the S191 visible-infrared spectrometer of the Skylab Earth Resources Experiment Package - a manually pointed two-channel instrument operating in the reflective (0.4-2.5 micron) and thermal emissive (6-15 micron) regions. A sensor description is provided and attention is given to data quality in the short wavelength and thermal infrared regions.

Study for the dispersion of double-diffraction spectrometers

NASA Astrophysics Data System (ADS)

Pang, Yajun; Zhang, Yinxin; Yang, Huaidong; Huang, Zhanhua; Xu, Mingming; Jin, Guofan

2018-01-01

Double-cascade spectrometers and double-pass spectrometers can be uniformly called double-diffraction spectrometers. In current double-diffraction spectrometers design theory, the differences of the incident angles in the second diffraction are ignored. There is a significant difference between the design in theory and the actual result. In this study, based on the geometries of the double-diffraction spectrometers, we strictly derived the theoretical formulas of their dispersion. By employing the ZEMAX simulation software, verification of our theoretical model is implemented, and the simulation results show big agreement with our theoretical formulas. Based on the conclusions, a double-pass spectrometer was set up and tested, and the experiment results agree with the theoretical model and the simulation.

INTEGRAL/SPI γ-ray line spectroscopy. Response and background characteristics

NASA Astrophysics Data System (ADS)

Diehl, Roland; Siegert, Thomas; Greiner, Jochen; Krause, Martin; Kretschmer, Karsten; Lang, Michael; Pleintinger, Moritz; Strong, Andrew W.; Weinberger, Christoph; Zhang, Xiaoling

2018-03-01

Context. The space based γ-ray observatory INTEGRAL of the European Space Agency (ESA) includes the spectrometer instrument "SPI". This is a coded mask telescope featuring a 19-element Germanium detector array for high-resolution γ-ray spectroscopy, encapsulated in a scintillation detector assembly that provides a veto for background from charged particles. In space, cosmic rays irradiate spacecraft and instruments, which, in spite of the vetoing detectors, results in a large instrumental background from activation of those materials, and leads to deterioration of the charge collection properties of the Ge detectors. Aim. We aim to determine the measurement characteristics of our detectors and their evolution with time, that is, their spectral response and instrumental background. These incur systematic variations in the SPI signal from celestial photons, hence their determination from a broad empirical database enables a reduction of underlying systematics in data analysis. For this, we explore compromises balancing temporal and spectral resolution within statistical limitations. Our goal is to enable modelling of background applicable to spectroscopic studies of the sky, accounting separately for changes of the spectral response and of instrumental background. Methods: We use 13.5 years of INTEGRAL/SPI data, which consist of spectra for each detector and for each pointing of the satellite. Spectral fits to each such spectrum, with independent but coherent treatment of continuum and line backgrounds, provides us with details about separated background components. From the strongest background lines, we first determine how the spectral response changes with time. Applying symmetry and long-term stability tests, we eliminate degeneracies and reduce statistical fluctuations of background parameters, with the aim of providing a self-consistent description of the spectral response for each individual detector. Accounting for this, we then determine how the

Development and applications of ruggedized VIS/NIR spectrometer system for oilfield wellbores

NASA Astrophysics Data System (ADS)

Fujisawa, Go; Yamate, Tsutomu

2013-12-01

The development and applications of a ruggedized visible to near-infrared (VIS/NIR) spectrometer system capable of measuring fluid spectra in oilfield wellbores are presented. Real-time assessment of formation fluid properties penetrated by an oilfield wellbore is critically important for oilfield operating companies to make informed decisions to optimize the development plan of the well and hydrocarbon reservoir. A ruggedized VIS/NIR spectrometer was designed and built to measure and analyze hydrocarbon spectra reliably under the harsh conditions of the oilfield wellbore environment, including temperature up to 175 °C, pressure up to 170 MPa, and severe mechanical shocks and vibrations. The accuracy of hydrocarbon group composition analysis was compared well with gas chromatography results in the laboratory.

Study on a liquid-moderator-based neutron spectrometer for BNCT-Development and experimental test of the prototype spectrometer

NASA Astrophysics Data System (ADS)

Tamaki, S.; Sato, F.; Murata, I.

2017-10-01

Boron neutron capture therapy (BNCT) is known to be an effective radiation cancer therapy that requires neutron irradiation. A neutron field generated by an accelerator-based neutron source has various energy spectra, and it is necessary to evaluate the neutron spectrum in the treatment field. However, the method used to measure the neutron spectrum in the treatment field is not well established, and many researchers are making efforts to improve the spectrometers used. In the present study, we developed a prototype of a new neutron spectrometer that can measure the neutron spectra more accurately and precisely. The spectrometer is based on the same theory as that of the Bonner sphere spectrometer, and it uses a liquid moderator and an absorber. By carrying out an experimental test of the developed spectrometer, we finally revealed the problems and necessary conditions of the prototype detector.

Mathematical Simulation for Integrated Linear Fresnel Spectrometer Chip

NASA Technical Reports Server (NTRS)

Park, Yeonjoon; Yoon, Hargoon; Lee, Uhn; King, Glen C.; Choi, Sang H.

2012-01-01

A miniaturized solid-state optical spectrometer chip was designed with a linear gradient-gap Fresnel grating which was mounted perpendicularly to a sensor array surface and simulated for its performance and functionality. Unlike common spectrometers which are based on Fraunhoffer diffraction with a regular periodic line grating, the new linear gradient grating Fresnel spectrometer chip can be miniaturized to a much smaller form-factor into the Fresnel regime exceeding the limit of conventional spectrometers. This mathematical calculation shows that building a tiny motionless multi-pixel microspectrometer chip which is smaller than 1 cubic millimter of optical path volume is possible. The new Fresnel spectrometer chip is proportional to the energy scale (hc/lambda), while the conventional spectrometers are proportional to the wavelength scale (lambda). We report the theoretical optical working principle and new data collection algorithm of the new Fresnel spectrometer to build a compact integrated optical chip.

Exploration of Mars in SPICAM-IR experiment onboard the Mars-Express spacecraft: 1. Acousto-optic spectrometer SPICAM-IR

NASA Astrophysics Data System (ADS)

Korablev, O. I.; Bertaux, J. L.; Kalinnikov, Yu. K.; Fedorova, A. A.; Moroz, V. I.; Kiselev, A. V.; Stepanov, A. V.; Grigoriev, A. V.; Zhegulev, V. S.; Rodin, A. V.; Dimarellis, E.; Dubois, J. P.; Reberac, A.; van Ransbeeck, E.; Gondet, B.

2006-07-01

The acousto-optic spectrometer of the near infrared range, which is a part of the spectrometer SPICAM onboard the Mars-Express spacecraft, began to operate in the orbit of Mars in January 2004. In the SPICAM experiment, a spectrometer on the basis of an acousto-optic filter was used for the first time to investigate other planets. During one and a half years of operation, the IR channel of SPICAM obtained more than half a million spectra in the 1-1.7 μm range with a resolving power of more than 1500 in different modes of observation: limb, nadir, and solar eclipses. The main goal of the experiment is to study the content of water vapor in the Martian atmosphere by measuring the absorption spectrum in the 1.38 μm band. Characteristics of the instrument (high spectral resolution and signal-to-noise ratio) allow one to solve a number of additional scientific problems including the study of ozone distribution by emission of singlet oxygen (O2 1Δg), detection of the water and carbonic dioxide ices, and also the study of the vertical distribution and optical characteristics of aerosol in the Martian atmosphere. We present a description of the instrument, the results of its ground and in-flight calibrations, and a brief survey of the basic scientific results obtained by the SPICAM spectrometer during a year-and-half of operation.

Two-years of In-flight Spectrometer Calibration Results for the Fast Plasma Investigation (FPI) on the Magmetospheric Multiscale (MMS) Mission

NASA Astrophysics Data System (ADS)

Schiff, C.; Gershman, D. J.; Avanov, L. A.; Giles, B. L.; Paterson, W. R.; Kriesler, S.; Barrie, A. C.; Rand, D. K.; Gliese, U.; Burch, J.

2017-12-01

Scientifically accurate measurements depend on careful calibration of in-flight instrumentation. We review two years of calibration results for the Fast Plasma Investigation (FPI) electron and ion spectrometers over the MMS fleet. We focus on the operating point calibration by which the operating voltage on each of the 64 spectrometers is set to best balance between gain, signal loss, and anode-to-anode cross talk. In addition, we map the calibration and housekeeping telemetry to infer charge extracted evolution from the microchannel plates and, subsequently, the project lifetime of the instrumentation.

A beta-ray spectrometer based on a two-or three silicon detector coincidence telescope

NASA Astrophysics Data System (ADS)

Horowitz, Y. S.; Weizman, Y.; Hirning, C. R.

1996-02-01

This report describes the operation of a beta-ray energy spectrometer based on a silicon detector telescope using two or three elements. The front detector is a planar, totally-depleted, silicon surface barrier detector that is 97 μm thick, the back detector is a room-temperature, lithium compensated, silicon detector that is 5000 μm thick, and the intermediate detector is similar to the front detector but 72 μm thick and intended to be used only in intense photon fields. The three detectors are mounted in a light-tight aluminum housing. The capability of the spectrometer to reject photons is based upon the fact that the incident photon will have a small probability of simultaneously losing detectable energy in two detectors, and an even smaller probability of losing detectable energy in all three detectors. Electrons will, however, almost always record measurable events in either the front two or all three detectors. A coincidence requirement between the detectors thus rejects photon induced events. With a 97 μm thick detector the lower energy coincidence threshold is approximately 110 keV. With an ultra-thin 40 μm thick front detector, and operated at 15°C, the spectrometer is capable of detecting even 60-70 keV electrons with a coincidence efficiency of 60%. The spectrometer has been used to measure beta radiation fields in CANDU reactor working environments, and the spectral information is intended to support dose algorithms for the LiF TLD chips used in the Ontario Hydro dosimetry program.

Optimization of Micro-Spec, an Ultra-Compact High-Performance Spectrometer for Far-Infrared Astronomy

NASA Astrophysics Data System (ADS)

Cataldo, Giuseppe; Moseley, S. H.; Wollack, E.; Hsieh, W.; Huang, W.; Stevenson, T.

2013-06-01

Micro-Spec (µ-Spec) is a high-sensitivity direct-detection spectrometer operating in the far-infrared and submillimeter regime. When combined with a cryogenic telescope, it provides an enabling technology for studying the epoch of reionization and initial galaxy formation. As a direct-detection spectrometer, µ-Spec can provide high sensitivity under the low background conditions provided by cryogenic telescopes such as the space infrared telescope for cosmology and astrophysics SPICA. The µ-Spec modules use low-loss superconducting microstrip transmission lines implemented on a single 4-inch-diameter wafer. Such a dramatic size reduction is enabled by the use of silicon, a material with an index of refraction about three times that of vacuum, which thus allows the microstrip lines to be one third their vacuum length. Using a large number of modules as well as reducing the negative effects of stray light also contributes positively to the enhanced sensitivity of such an instrument. µ-Spec can be compared to a grating spectrometer, in which the phase retardation generated by the reflection from the grating grooves is instead produced by propagation through transmission lines of different length. The µ-Spec optical design is based on the stigmatization and minimization of the light path function in a two-dimensional diffractive region. The power collected through a broadband antenna is progressively divided by binary microstrip power dividers. The position of the radiators is selected to provide zero phase errors at two stigmatic points, and a third stigmatic point is generated by introducing a differential phase shift in each radiator. To optimize the overall efficiency of the instrument, the emitters are directed to the center of the focal surface. A point design was developed for initial demonstration. Because of losses to other diffraction orders, the efficiency of the design presented is about 30%. Design variations on this implementation are illustrated

Ultraviolet spectrometer and polarimeter (UVSP) software development and hardware tests for the solar maximum mission

NASA Technical Reports Server (NTRS)

Bruner, M. E.; Haisch, B. M.

1986-01-01

The Ultraviolet Spectrometer/Polarimeter Instrument (UVSP) for the Solar Maximum Mission (SMM) was based on the re-use of the engineering model of the high resolution ultraviolet spectrometer developed for the OSO-8 mission. Lockheed assumed four distinct responsibilities in the UVSP program: technical evaluation of the OSO-8 engineering model; technical consulting on the electronic, optical, and mechanical modifications to the OSO-8 engineering model hardware; design and development of the UVSP software system; and scientific participation in the operations and analysis phase of the mission. Lockheed also provided technical consulting and assistance with instrument hardware performance anomalies encountered during the post launch operation of the SMM observatory. An index to the quarterly reports delivered under the contract are contained, and serves as a useful capsule history of the program activity.

Remote sensing of Earth's atmosphere and surface using a digital array scanned interferometer: A new type of imaging spectrometer

NASA Technical Reports Server (NTRS)

Hammer, Philip D.; Valero, Francisco P. J.; Peterson, David L.; Smith, William Hayden

1991-01-01

The capabilities of the digital array scanned interferometer (DASI) class of instruments for measuring terrestrial radiation fields over the visible to mid-infrared are evaluated. DASI's are capable of high throughput, sensitivity and spectral resolution and have the potential for field-of-view spatial discrimination (an imaging spectrometer). The simplicity of design and operation of DASI's make them particularly suitable for field and airborne platform based remote sensing. The long term objective is to produce a versatile field instrument which may be applied toward a variety of atmospheric and surface studies. The operation of DASI and its advantages over other spectrometers are discussed.

A gamma-gamma coincidence/anticoincidence spectrometer for low-level cosmogenic (22)Na/(7)Be activity ratio measurement.

PubMed

Zhang, Weihua; Ungar, Kurt; Stukel, Matthew; Mekarski, Pawel

2014-04-01

In this study, a digital gamma-gamma coincidence/anticoincidence spectrometer was developed and examined for low-level cosmogenic (22)Na and (7)Be in air-filter sample monitoring. The spectrometer consists of two bismuth germanate scintillators (BGO) and an XIA LLC Digital Gamma Finder (DGF)/Pixie-4 software and card package. The spectrometer design allows a more selective measurement of (22)Na with a significant background reduction by gamma-gamma coincidence events processing. Hence, the system provides a more sensitive way to quantify trace amounts of (22)Na than normal high resolution gamma spectrometry providing a critical limit of 3 mBq within a 20 h count. The use of a list-mode data acquisition technique enabled simultaneous determination of (22)Na and (7)Be activity concentrations using a single measurement by coincidence and anticoincidence mode respectively. Copyright © 2014 Elsevier Ltd. All rights reserved.

SUB 1-Millimeter Size Fresnel Micro Spectrometer

NASA Technical Reports Server (NTRS)

Park, Yeonjoon; Koch, Laura; Song, Kyo D.; Park, Sangloon; King, Glen; Choi, Sang

2010-01-01

An ultra-small micro spectrometer with less than 1mm diameter was constructed using Fresnel diffraction. The fabricated spectrometer has a diameter of 750 nmicrometers and a focal length of 2.4 mm at 533nm wavelength. The micro spectrometer was built with a simple negative zone plate that has an opaque center with an ecliptic shadow to remove the zero-order direct beam to the aperture slit. Unlike conventional approaches, the detailed optical calculation indicates that the ideal spectral resolution and resolving power do not depend on the miniaturized size but only on the total number of rings. We calculated 2D and 3D photon distribution around the aperture slit and confirmed that improved micro-spectrometers below 1mm size can be built with Fresnel diffraction. The comparison between mathematical simulation and measured data demonstrates the theoretical resolution, measured performance, misalignment effect, and improvement for the sub-1mm Fresnel micro-spectrometer. We suggest the utilization of an array of micro spectrometers for tunable multi-spectral imaging in the ultra violet range.

AIRES: An Airborne Infra-Red Echelle Spectrometer for SOFIA

NASA Technical Reports Server (NTRS)

Dotson, Jessie J.; Erickson, Edwin F.; Haas, Michael R.; Colgan, Sean W. J.; Simpson, Janet P.; Telesco, Charles M.; Pina, Robert K.; Wolf, Juergen; Young, Erick T.

1999-01-01

SOFIA will enable astronomical observations with unprecedented angular resolution at infrared wavelengths obscured from the ground. To help open this new chapter in the exploration of the infrared universe, we are building AIRES, an Airborne Infra-Red Echelle Spectrometer. AIRES will be operated as a first generation, general purpose facility instrument by USRA, NASA's prime contractor for SOFIA. AIRES is a long slit spectrograph operating from 17 - 210 microns. In high resolution mode the spectral resolving power is approx. 10(exp 6) microns/A or approx. 10(exp 4) at 100 microns. Unfortunately, since the conference, a low resolution mode with resolving power about 100 times lower has been deleted due to budgetary constraints. AIRES includes a slit viewing camera which operates in broad bands at 18 and 25 microns.

Infrared Spectrometer for ExoMars: A Mast-Mounted Instrument for the Rover

NASA Astrophysics Data System (ADS)

Korablev, Oleg I.; Dobrolensky, Yurii; Evdokimova, Nadezhda; Fedorova, Anna A.; Kuzmin, Ruslan O.; Mantsevich, Sergei N.; Cloutis, Edward A.; Carter, John; Poulet, Francois; Flahaut, Jessica; Griffiths, Andrew; Gunn, Matthew; Schmitz, Nicole; Martín-Torres, Javier; Zorzano, Maria-Paz; Rodionov, Daniil S.; Vago, Jorge L.; Stepanov, Alexander V.; Titov, Andrei Yu.; Vyazovetsky, Nikita A.; Trokhimovskiy, Alexander Yu.; Sapgir, Alexander G.; Kalinnikov, Yurii K.; Ivanov, Yurii S.; Shapkin, Alexei A.; Ivanov, Andrei Yu.

2017-07-01

ISEM (Infrared Spectrometer for ExoMars) is a pencil-beam infrared spectrometer that will measure reflected solar radiation in the near infrared range for context assessment of the surface mineralogy in the vicinity of the ExoMars rover. The instrument will be accommodated on the mast of the rover and will be operated together with the panoramic camera (PanCam), high-resolution camera (HRC). ISEM will study the mineralogical and petrographic composition of the martian surface in the vicinity of the rover, and in combination with the other remote sensing instruments, it will aid in the selection of potential targets for close-up investigations and drilling sites. Of particular scientific interest are water-bearing minerals, such as phyllosilicates, sulfates, carbonates, and minerals indicative of astrobiological potential, such as borates, nitrates, and ammonium-bearing minerals. The instrument has an ˜1° field of view and covers the spectral range between 1.15 and 3.30 μm with a spectral resolution varying from 3.3 nm at 1.15 μm to 28 nm at 3.30 μm. The ISEM optical head is mounted on the mast, and its electronics box is located inside the rover's body. The spectrometer uses an acousto-optic tunable filter and a Peltier-cooled InAs detector. The mass of ISEM is 1.74 kg, including the electronics and harness. The science objectives of the experiment, the instrument design, and operational scenarios are described.

Development of Portable Aerosol Mobility Spectrometer for Personal and Mobile Aerosol Measurement

PubMed Central

Kulkarni, Pramod; Qi, Chaolong; Fukushima, Nobuhiko

2017-01-01

We describe development of a Portable Aerosol Mobility Spectrometer (PAMS) for size distribution measurement of submicrometer aerosol. The spectrometer is designed for use in personal or mobile aerosol characterization studies and measures approximately 22.5 × 22.5 × 15 cm and weighs about 4.5 kg including the battery. PAMS uses electrical mobility technique to measure number-weighted particle size distribution of aerosol in the 10–855 nm range. Aerosol particles are electrically charged using a dual-corona bipolar corona charger, followed by classification in a cylindrical miniature differential mobility analyzer. A condensation particle counter is used to detect and count particles. The mobility classifier was operated at an aerosol flow rate of 0.05 L/min, and at two different user-selectable sheath flows of 0.2 L/min (for wider size range 15–855 nm) and 0.4 L/min (for higher size resolution over the size range of 10.6–436 nm). The instrument was operated in voltage stepping mode to retrieve the size distribution, which took approximately 1–2 minutes, depending on the configuration. Sizing accuracy and resolution were probed and found to be within the 25% limit of NIOSH criterion for direct-reading instruments (NIOSH 2012). Comparison of size distribution measurements from PAMS and other commercial mobility spectrometers showed good agreement. The instrument offers unique measurement capability for on-person or mobile size distribution measurements of ultrafine and nanoparticle aerosol. PMID:28413241

Method of multiplexed analysis using ion mobility spectrometer

DOEpatents

Belov, Mikhail E [Richland, WA; Smith, Richard D [Richland, WA

2009-06-02

A method for analyzing analytes from a sample introduced into a Spectrometer by generating a pseudo random sequence of a modulation bins, organizing each modulation bin as a series of submodulation bins, thereby forming an extended pseudo random sequence of submodulation bins, releasing the analytes in a series of analyte packets into a Spectrometer, thereby generating an unknown original ion signal vector, detecting the analytes at a detector, and characterizing the sample using the plurality of analyte signal subvectors. The method is advantageously applied to an Ion Mobility Spectrometer, and an Ion Mobility Spectrometer interfaced with a Time of Flight Mass Spectrometer.

Mid infrared MEMS FTIR spectrometer

NASA Astrophysics Data System (ADS)

Erfan, Mazen; Sabry, Yasser M.; Mortada, Bassem; Sharaf, Khaled; Khalil, Diaa

2016-03-01

In this work we report, for the first time to the best of our knowledge, a bulk-micromachined wideband MEMS-based spectrometer covering both the NIR and the MIR ranges and working from 1200 nm to 4800 nm. The core engine of the spectrometer is a scanning Michelson interferometer micro-fabricated using deep reactive ion etching (DRIE) technology. The spectrum is obtained using the Fourier Transform techniques that allows covering a very wide spectral range limited by the detector responsivity. The moving mirror of the interferometer is driven by a relatively large stroke electrostatic comb-drive actuator. Zirconium fluoride (ZrF4) multimode optical fibers are used to connect light between the white light source and the interferometer input, as well as the interferometer output to a PbSe photoconductive detector. The recorded signal-to-noise ratio is 25 dB at the wavelength of 3350 nm. The spectrometer is successfully used in measuring the absorption spectra of methylene chloride, quartz glass and polystyrene film. The presented solution provides a low cost method for producing miniaturized spectrometers in the near-/mid-infrared.

Realizing the full potential of a RITA spectrometer

NASA Astrophysics Data System (ADS)

Lefmann, K.; Niedermayer, Ch.; Abrahamsen, A. B.; Bahl, C. R. H.; Christensen, N. B.; Jacobsen, H. S.; Larsen, T. L.; Häfliger, P.; Filges, U.; Rønnow, H. M.

2006-11-01

The “re-invented triple-axis spectrometer (RITA) concept has existed for a decade. Recent developments at RITA-2 at PSI, have revealed more of the potential of this instrument class. We demonstrate the performance of the multi-blade imaging mode, which has been applied e.g. to studies of dispersion relations and emphasize the power of this mode in combination with the low background of RITA-2. In addition, we present other ways of utilizing the position sensitive detector in a RITA instrument. Simulations of a planned upgrade of the guide-monochromator system at RITA-2 have shown a potential to increase the flux at the sample position by a factor 5.

Development of Fast, Background-Limited Transition-Edge Sensors for the Background-Limited Infrared/Sub-Millimetre Spectrograph (BLISS) for SPICA

NASA Technical Reports Server (NTRS)

Beyer, Andrew D.; Runyan, M. C.; Kenyon, M.; Echternach, P. M.; Chui, T.; Bumble, B.; Bradford, C. M.; Holmes, W. A.; Bock, J. J.

2012-01-01

We report experimental progress toward demonstrating background-limited arrays of membrane-isolated transition-edge sensors (TESs) for the Background Limited Infrared/Sub-mm Spectrograph (BLISS). BLISS is a space-borne instrument with grating spectrometers for wavelengths lambda = 35-435 microns and with R = lambda/(delta)lambda approx. 500. The goals for BLISS TESs are: noise equivalent power (NEP) = 5x10(exp -20) W/Hz(1/2) and response time t<30ms. We expect background-limited performance from bilayers TESs with T(sub c)=65mK and G=15fW/K. However, such TESs cannot be operated at 50mK unless stray power on the devices, or dark power PD, is less than 200aW. We describe criteria for measuring P? that requires accurate knowledge of TC. Ultimately, we fabricated superconducting thermistors from Ir (T(sub c) > or = 135mK) and Mo/Cu proximitized bilayers, where T(sub c) is the thermistor transition temperature. We measured the Ir TES arrays in our 50mK adiabatic demagnetization refrigerator test system, which can measure up to eight 1x32 arrays simultaneously using a time-division multiplexer, as well as our single-pixel test system which can measure down to 15mK. In our previous Ir array measurements our best reported performance was NEP=2.5x10(exp -19) W/Hz(1/2) and tapprox.5ms for straight-beam TESs. In fact, we expected NEPapprox.1.5x10(exp -19)W/Hz(1/2) for meander beam TESs, but did not achieve this previously due to 1/f noise. Here, we detail improvements toward measuring the expected NEP and demonstrate NEP=(1.3+0.2)x10(exp -19)W/Hz(1/2) in our single-pixel test system and NEP=(1.6+0.3)x10(exp -19)W/Hz(1/2) in our array test system.

Development of Fast, Background-Limited Transition-Edge Sensors for the Background-Limited Infrared/Sub-mm Spectrograph (BLISS) for SPICA

NASA Technical Reports Server (NTRS)

Beyer, Andrew D.; Runyan, M. C.; Kenyon, M.; Echternach, P. M .; Chui, T.; Bumble, B.; Bradford, C. M.; Holmes, W. A.; Bock, J. J.

2012-01-01

We report experimental progress toward demonstrating background-limited arrays of membrane-isolated transition-edge sensors (TESs) for the Background Limited Infrared/Sub-mm Spectrograph (BLISS). BLISS is a space-borne instrument with grating spectrometers for wavelengths lambda=35-435 micron and with R=lambda/delta lambda approximately equals 500. The goals for BLISS TESs are: noise equivalent power (NEP) = 5x10 (sup -20) W/Hz(exp 1/2) and response time tau <30ms. We expect background-limited performance from bilayers TESs with T(sub c) = 65mK and G=15fW/K. However, such TESs cannot be operated at 50mK unless stray power on the devices, or dark power P(sub D), is less than 200aW. We describe criteria for measuring P(sub D) that requires accurate knowledge of TC. Ultimately, we fabricated superconducting thermistors from Ir (T(sub c) >= 135mK) and Mo/Cu proximitized bilayers, where T(sub c) is the thermistor transition temperature. We measured the Ir TES arrays in our 50mK adiabatic demagnetization refrigerator test system, which can measure up to eight 1x32 arrays simultaneously using a time-division multiplexer, as well as our single-pixel test system which can measure down to 15mK. In our previous Ir array measurements our best reported performance was NEP=2.5x10(exp -19) W/Hz(sub 1/2) and Tau approximately equals 5ms for straight-beam TESs. In fact, we expected NEP approximately equals 1.5x10(exp -19)?W/Hz(sup 1/2) for meander beam TESs, but did not achieve this previously due to 1/f noise. Here, we detail improvements toward measuring the expected NEP and demonstrate NEP=(1.3+0.2)x10 (sup -19)W/Hz(exp 1/2) in our single-pixel test system and NEP=(1.6+/-0.3)x10(sup -19)W/Hz(sup 1/2) in our array test system.

A simple, low-cost, versatile CCD spectrometer for plasma spectroscopy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Den Hartog, D. J.; Holly, D. J.

1996-06-01

The authors have constructed a simple, low-cost CCD spectrometer capable of both high resolution ({Delta}{lambda} {le} 0.015 nm) and large bandpass (110 nm with {Delta}{lambda} {approximately}0.3 nm). These two modes of operation provide two broad areas of capability for plasma spectroscopy. The first major application is measurement of emission line broadening; the second is emission line surveys from the ultraviolet to the near infrared. Measurements have been made on a low-temperature plasma produced by a miniature electrostatic plasma source and the high-temperature plasma in the MST Reversed-Field Pinch. The spectrometer is a modified Jarrell-Ash 0.5 m Ebert-Fastie monochromator. Light ismore » coupled into the entrance slit with a fused silica fiber optic bundle. The exposure time (2 ms minimum) is controlled by a fast electromechanical shutter. The exit plane detector is a compact and robust CCD detector developed for amateur astronomy by Santa Barbara Instrument Group. The CCD detector is controlled and read out by a Macintosh{reg_sign} computer. This spectrometer is sophisticated enough to serve well in a research laboratory, yet is simple and inexpensive enough to be affordable for instructional use.« less

A cryogenically cooled, multidetector spectrometer for infrared astronomy

NASA Technical Reports Server (NTRS)

Witteborn, F. C.; Bregman, J. D.

1984-01-01

A liquid helium-cooled, 24 detector grating spectrometer was developed and used for low resolution astronomical observations in the 5 to 14 micron spectral range. The instrument operated on the 91 cm Kuiper Airborne Observatory, the 3 m IRTF (Mauna Kea), the 3 m Shane telescope Observatory, the 3 m Shane telescope (Lick Observatory), and the 152 cm NASA and University of Arizona telescope. The detectors are discrete Si:Bi photoconductors with individual metal oxide semiconductor field effect transistor preamplifiers operating at 4 K. The system uses a liquid helium-cooled slit, order-sorter filter, collimator mirror, grating, and camera mirror arranged in a Czerny-Turner configuration with a cold stop added between the collimator mirror and the grating. The distances between components are chosen so that the collimator mirror images the secondary mirror of the telescope onto the cold stop, thus providing a very effective baffle. Scattered radiation is effectively reduced by using liquid helium-cooled, black baffles to divide the spectrometer into three separate compartments. The system noise-equivalent flux density, when used on the 152 cm telescope from 8 to 13 microns with a resolving power of 50, is 4.4 x 10 to the minus 17th power W/sq cm micron square root of Hz. The main applications are for measuring continuum radiation levels and solid state emission and absorption features in regions of star and planet formation.

Electronics design of the RPC system for the OPERA muon spectrometer

NASA Astrophysics Data System (ADS)

Acquafredda, R.; Ambrosio, M.; Balsamo, E.; Barichello, G.; Bergnoli, A.; Consiglio, L.; Corradi, G.; dal Corso, F.; Felici, G.; Manea, C.; Masone, V.; Parascandolo, P.; Sorrentino, G.

2004-09-01

The present document describes the front-end electronics of the RPC system that instruments the magnet muon spectrometer of the OPERA experiment. The main task of the OPERA spectrometer is to provide particle tracking information for muon identification and simplify the matching between the Precision Trackers. As no trigger has been foreseen for the experiment, the spectrometer electronics must be self-triggered with single-plane readout capability. Moreover, precision time information must be added within each event frame for off-line reconstruction. The read-out electronics is made of three different stages: the Front-End Boards (FEBs) system, the Controller Boards (CBs) system and the Trigger Boards (TBs) system. The FEB system provides discrimination of the strip incoming signals; a FAST-OR output of the input signals is also available for trigger plane signal generation. FEB signals are acquired by the CB system that provides the zero suppression and manages the communication to the DAQ and Slow Control. A Trigger Board allows to operate in both self-trigger mode (the FEB's FAST-OR signal starts the plane acquisition) or in external-trigger mode (different conditions can be set on the FAST-OR signals generated from different planes).

Pulsed Multiple Reaction Monitoring Approach to Enhancing Sensitivity of a Tandem Quadrupole Mass Spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Belov, Mikhail E.; Prasad, Satendra; Prior, David C.

2011-02-23

Liquid chromatography (LC)-triple quadrupole mass spectrometers operating in a Multiple Reaction Monitoring (MRM) mode are increasingly used for quantitative analysis of low abundance analytes in highly complex biochemical matrices. After development and selection of optimum MRM transition, sensitivity and data quality limitations are largely related to mass spectral peak interferences from sample or matrix constituents and statistical limitations at low number of ions reaching the detector. Herein, we report a new approach to enhancing MRM sensitivity by converting the continuous stream of ions from the ion source into a pulsed ion beam through the use of an Ion Funnel Trapmore » (IFT). Evaluation of the pulsed MRM approach was performed with a tryptic digest of Shewanella oneidensis strain MR-1 spiked with several reference peptides. The sensitivity improvement observed with the IFT coupled to the triple quadrupole instrument is based on several unique features. First, ion accumulation in the radio frequency (RF) ion trap facilitates improved droplet desolvation, which is manifested in the reduced background ion noise at the detector. Second, signal amplitude for a given transition is enhanced because of an order-of-magnitude increase in the ion charge density per unit time compared to a continuous mode of operation. Third, signal detection at the full duty cycle is obtained, as the trap use eliminates dead times between transitions, which are inevitable with continuous ion streams. In comparison with the conventional approach, the pulsed MRM signals showed up to 5-fold enhanced peak amplitude and 2-3 fold reduced chemical background, resulting in an improvement in the limit of detection (LOD) by a factor of ~ 4 to ~ 8.« less

Coherent-Radiation Spectroscopy of Few-Femtosecond Electron Bunches Using a Middle-Infrared Prism Spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Maxwell, T. J.; Behrens, C.; Ding, Y.

2013-10-28

Modern, high-brightness electron beams such as those from plasma wakefield accelerators and free-electron laser linacs continue the drive to ever-shorter bunch durations. In low-charge operation ( ~ 20 pC ), bunches shorter than 10 fs are reported at the Linac Coherent Light Source (LCLS). Though suffering from a loss of phase information, spectral diagnostics remain appealing as compact, low-cost bunch duration monitors suitable for deployment in beam dynamics studies and operations instrumentation. Progress in middle-infrared (MIR) imaging has led to the development of a single-shot, MIR prism spectrometer to characterize the corresponding LCLS coherent beam radiation power spectrum for few-femtosecondmore » scale bunch length monitoring. In this Letter, we report on the spectrometer installation as well as the temporal reconstruction of 3 to 60 fs-long LCLS electron bunch profiles using single-shot coherent transition radiation spectra.« less

[Current status and prospects of portable NIR spectrometer].

PubMed

Yu, Xin-Yang; Lu, Qi-Peng; Gao, Hong-Zhi; Peng, Zhong-Qi

2013-11-01

Near-infrared spectroscopy (NIRS) is a reliable, rapid, and non-destructive analytical method widely applied in as a number of fields such as agriculture, food, chemical and oil industry. In order to suit different applications, near-infrared spectrometers are now varied. Portable near-infrared spectrometers are needed for rapid on-site identification and analysis. Instruments of this kind are rugged, compact and easy to be transported. In this paper, the current states of portable near-infrared spectrometers are reviewed. Portable near-infrared spectrometers are built of different monochromator systems: filter, grating, Fourier-transform methods, acousto-optic tunable filter (AOTF) and a large number of new methods based on micro-electro-mechanical systems (MEMS). The first part focuses on working principles of different monochromator systems. Advantages and disadvantages of different systems are also briefly mentioned. Descriptions of each method are given in turn. Typical spectrometers of each kind are introduced, and some parameters of these instruments are listed. In the next part we discuss sampling adapters, display, power supply and some other parts, which are designed to make the spectrometer more portable and easier to use. In the end, the current states of portable near-infrared spectrometers are summarized. Future trends of development of portable near-infrared spectrometers in China and abroad are discussed.

Compact NE213 neutron spectrometer with high energy resolution for fusion applications

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zimbal, A.; Reginatto, M.; Schuhmacher, H.

Neutron spectrometry is a tool for obtaining important information on the fuel ion composition, velocity distribution and temperature of fusion plasmas. A compact NE213 liquid scintillator, fully characterized at Physikalisch-Technische Bundesanstalt, was installed and operated at the Joint European Torus (JET) during two experimental campaigns (C8-2002 and trace tritium experiment-TTE 2003). The results show that this system can operate in a real fusion experiment as a neutron (1.5 MeVspectrometer with good energy resolution ({delta}E/E<4% at E{sub n}=2.5 MeV and {delta}E/E<2% at E{sub n}=14 MeV). First measurements performed under different plasma scenarios, including trace tritium experiments, are presented.more » The analysis of the pulse height data was carried out using a newly developed method based on maximum entropy unfolding. The results indicate that this efficient, inexpensive, and compact scintillator is suitable for use as a broadband spectrometer in large fusion devices (JET and the International Thermonuclear Experimental Reactor)« less

General study of asymmetrical crossed Czerny-Turner spectrometer.

PubMed

Tang, Ming; Fan, Xianguang; Wang, Xin; Xu, Yingjie; Que, Jing; He, Jian

2015-11-20

A study of the spectrum resolution, wavelength range, and primary aberration of the asymmetrical crossed Czerny-Turner spectrometer is presented by deducing the relationship between them and structural parameters of the spectrometer in a new way of thinking based on simple but effective geometric models. The analysis was verified in an experiment and simulation performed on the optical design program ZEMAX, and the obtained results agree with the analysis. Owing to the analysis, initial designed parameters of the spectrometer were given and then optimized by ZEMAX; with the instruction of the study, a small adjustment was made in the actual alignment to obtain the desired final spectrometer. The spectrometer successfully measured the last four characteristic peaks of the Raman spectrum of CCL4, which demonstrates that the research provides important guidance to the design and alignment of an asymmetrical crossed Czerny-Turner spectrometer.

A New Control System Software for SANS BATAN Spectrometer in Serpong, Indonesia

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bharoto; Putra, Edy Giri Rachman

2010-06-22

The original main control system of the 36 meter small-angle neutron scattering (SANS) BATAN Spectrometer (SMARTer) has been replaced with the new ones due to the malfunction of the main computer. For that reason, a new control system software for handling all the control systems was also developed in order to put the spectrometer back in operation. The developed software is able to control the system such as rotation movement of six pinholes system, vertical movement of four neutron guide system with the total length of 16.5 m, two-directional movement of a neutron beam stopper, forward-backward movement of a 2Dmore » position sensitive detector (2D-PSD) along 16.7 m, etc. A Visual Basic language program running on Windows operating system was employed to develop the software and it can be operated by other remote computers in the local area network. All device positions and command menu are displayed graphically in the main monitor or window and each device control can be executed by clicking the control button. Those advantages are necessary required for developing a new user-friendly control system software. Finally, the new software has been tested for handling a complete SANS experiment and it works properly.« less

A New Control System Software for SANS BATAN Spectrometer in Serpong, Indonesia

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bharoto,; Putra, Edy Giri Rachman

2010-06-22

The original main control system of the 36 meter small‐angle neutron scattering (SANS) BATAN Spectrometer (SMARTer) has been replaced with the new ones due to the malfunction of the main computer. For that reason, a new control system software for handling all the control systems was also developed in order to put the spectrometer back in operation. The developed software is able to control the system such as rotation movement of six pinholes system, vertical movement of four neutron guide system with the total length of 16.5 m, two‐directional movement of a neutron beam stopper, forward‐backward movement of a 2Dmore » position sensitive detector (2D‐PSD) along 16.7 m, etc. A Visual Basic language program running on Windows operating system was employed to develop the software and it can be operated by other remote computers in the local area network. All device positions and command menu are displayed graphically in the main monitor or window and each device control can be executed by clicking the control button. Those advantages are necessary required for developing a new user‐friendly control system software. Finally, the new software has been tested for handling a complete SANS experiment and it works properly.« less

A novel approach for predicting the response of the spectrometer for INTEGRAL satellite.

PubMed

Kshetri, R

2013-05-01

A basic phenomenological approach has been presented in three recent papers (Kshetri R., 2012. JINST 7, P04008; Kshetri R., 2012. JINST 7, P07006; Kshetri R., 2012. JINST 7, P12007) for understanding the operation of encapsulated type composite detectors including the SPI spectrometer. In the present paper, we have considered the fact that the experimental two-fold events between two detectors include the three and higher fold events between the same two detectors. The formalism has been further developed and the peak-to-total ratio of a general composite detector are predicted for energy region with no direct experimental information about them. At 8MeV, the peak-to-total ratio for the SPI spectrometer and a very large detector (comprising of infinite number of single HPGe modules) are found to be 9% and 12%, respectively. The predictions for fold distribution of the SPI spectrometer are found to be in agreement with experimental data. Our formulation does not include ad-hoc fits, but expressions that are justifiable by probability flow arguments. Instead of using an empirical method or simulation, we present a novel approach for calculating the peak-to-total ratio of the SPI spectrometer for high gamma energies. Copyright © 2013 Elsevier Ltd. All rights reserved.

Dynamics Explorer 1: Energetic Ion Composition Spectrometer (EICS)

NASA Technical Reports Server (NTRS)

Shelley, E. G.; Peterson, W. K.; Collin, H. L.

1994-01-01

The Energetic Ion Composition Spectrometer (EICS) experiment was selected as part of the Dynamics Explorer (DE) Program. One of the primary goals of the DE program was to investigate in detail the plasma physics processes responsible for energizing thermal (approximately 1 eV) ionospheric ions and transporting them to the earth's plasma sheet and distant polar cap. The results of the EICS data analysis (including support of other investigators) and of the archiving efforts supported by this contract are summarized in this document. Also reported are some aspects of our operational support activities.

Multi-spectrometer calibration transfer based on independent component analysis.

PubMed

Liu, Yan; Xu, Hao; Xia, Zhenzhen; Gong, Zhiyong

2018-02-26

Calibration transfer is indispensable for practical applications of near infrared (NIR) spectroscopy due to the need for precise and consistent measurements across different spectrometers. In this work, a method for multi-spectrometer calibration transfer is described based on independent component analysis (ICA). A spectral matrix is first obtained by aligning the spectra measured on different spectrometers. Then, by using independent component analysis, the aligned spectral matrix is decomposed into the mixing matrix and the independent components of different spectrometers. These differing measurements between spectrometers can then be standardized by correcting the coefficients within the independent components. Two NIR datasets of corn and edible oil samples measured with three and four spectrometers, respectively, were used to test the reliability of this method. The results of both datasets reveal that spectra measurements across different spectrometers can be transferred simultaneously and that the partial least squares (PLS) models built with the measurements on one spectrometer can predict that the spectra can be transferred correctly on another.

An imaging spectrometer for microgravity application

NASA Technical Reports Server (NTRS)

Wong, Wallace K.

1995-01-01

Flame structure is the result of complex interaction of mechanisms operating in both unwanted fires and controlled combustion systems. The scientific study of gas-jet diffusion flames in reduced-gravity environment is of interest because the effects of buoyancy on flow entrainment and acceleration are lessened. Measurements of flames have been restricted to cinematography, thermocouples, and radiometers. SSG, Inc. is developing an MWIR imaging spectrometer (MIS) for microgravity flame measurements. The device will be delivered to NASA Lewis at the end of this project to demonstrate flame measurements in the laboratory. With proper modifications, the MIS can be used to monitor a gas-jet flame under microgravity on a NASA Learjet or DC-9.

[Design of Dual-Beam Spectrometer in Spectrophotometer for Colorimetry].

PubMed

Liu, Yi-xuan; Yan, Chang-xiang

2015-07-01

Spectrophotometers for colorimetry are usually composed of two independent and identical spectrometers. In order to reduce the volume of spectrophotometer for colorimetry, a design method of double-beam spectrometer is put forward. A traditional spectrometer is modified so that a new spectrometer can realize the function of double spectrometers, which is especially suitable for portable instruments. One slit is replaced by the double-slit, than two beams of spectrum can be detected. The working principle and design requirement of double-beam spectrometer are described. A spectrometer of portable spectrophotometer is designed by this method. A toroidal imaging mirror is used for the Czerny-Turner double-beam spectrometer in this paper, which can better correct astigmatism, and prevent the dual-beam spectral crosstalk. The results demonstrate that the double-beam spectrometer designed by this method meets the design specifications, with the spectral resolution less than 10 nm, the spectral length of 9.12 mm, and the volume of 57 mm x 54 mm x 23 mm, and without the dual-beam spectral overlap in the detector either. Comparing with a traditional spectrophotometer, the modified spectrophotometer uses a set of double-beam spectrometer instead of two sets of spectrometers, which can greatly reduce the volume. This design method can be specially applied in portable spectrophotometers, also can be widely applied in other double-beam spectrophotometers, which offers a new idea for the design of dual-beam spectrophotometers.

DAC-board based X-band EPR spectrometer with arbitrary waveform control

NASA Astrophysics Data System (ADS)

Kaufmann, Thomas; Keller, Timothy J.; Franck, John M.; Barnes, Ryan P.; Glaser, Steffen J.; Martinis, John M.; Han, Songi

2013-10-01

We present arbitrary control over a homogenous spin system, demonstrated on a simple, home-built, electron paramagnetic resonance (EPR) spectrometer operating at 8-10 GHz (X-band) and controlled by a 1 GHz arbitrary waveform generator (AWG) with 42 dB (i.e. 14-bit) of dynamic range. Such a spectrometer can be relatively easily built from a single DAC (digital to analog converter) board with a modest number of stock components and offers powerful capabilities for automated digital calibration and correction routines that allow it to generate shaped X-band pulses with precise amplitude and phase control. It can precisely tailor the excitation profiles "seen" by the spins in the microwave resonator, based on feedback calibration with experimental input. We demonstrate the capability to generate a variety of pulse shapes, including rectangular, triangular, Gaussian, sinc, and adiabatic rapid passage waveforms. We then show how one can precisely compensate for the distortion and broadening caused by transmission into the microwave cavity in order to optimize corrected waveforms that are distinctly different from the initial, uncorrected waveforms. Specifically, we exploit a narrow EPR signal whose width is finer than the features of any distortions in order to map out the response to a short pulse, which, in turn, yields the precise transfer function of the spectrometer system. This transfer function is found to be consistent for all pulse shapes in the linear response regime. In addition to allowing precise waveform shaping capabilities, the spectrometer presented here offers complete digital control and calibration of the spectrometer that allows one to phase cycle the pulse phase with 0.007° resolution and to specify the inter-pulse delays and pulse durations to ⩽250 ps resolution. The implications and potential applications of these capabilities will be discussed.

Compact reflective imaging spectrometer utilizing immersed gratings

DOEpatents

Chrisp, Michael P [Danville, CA

2006-05-09

A compact imaging spectrometer comprising an entrance slit for directing light, a first mirror that receives said light and reflects said light, an immersive diffraction grating that diffracts said light, a second mirror that focuses said light, and a detector array that receives said focused light. The compact imaging spectrometer can be utilized for remote sensing imaging spectrometers where size and weight are of primary importance.

How to Design a Spectrometer.

PubMed

Scheeline, Alexander

2017-10-01

Designing a spectrometer requires knowledge of the problem to be solved, the molecules whose properties will contribute to a solution of that problem and skill in many subfields of science and engineering. A seemingly simple problem, design of an ultraviolet, visible, and near-infrared spectrometer, is used to show the reasoning behind the trade-offs in instrument design. Rather than reporting a fully optimized instrument, the Yin and Yang of design choices, leading to decisions about financial cost, materials choice, resolution, throughput, aperture, and layout are described. To limit scope, aspects such as grating blaze, electronics design, and light sources are not presented. The review illustrates the mixture of mathematical rigor, rule of thumb, esthetics, and availability of components that contribute to the art of spectrometer design.

The Apollo Alpha Spectrometer.

NASA Technical Reports Server (NTRS)

Jagoda, N.; Kubierschky, K.; Frank, R.; Carroll, J.

1973-01-01

Located in the Science Instrument Module of Apollo 15 and 16, the Alpha Particle Spectrometer was designed to detect and measure the energy of alpha particles emitted by the radon isotopes and their daughter products. The spectrometer sensor consisted of an array of totally depleted silicon surface barrier detectors. Biased amplifier and linear gate techniques were utilized to reduce resolution degradation, thereby permitting the use of a single 512 channel PHA. Sensor identification and in-flight radioactive calibration were incorporated to enhance data reduction.

The laser absorption spectrometer - A new remote sensing instrument for atmospheric pollution monitoring

NASA Technical Reports Server (NTRS)

Shumate, M. S.

1974-01-01

An instrument capable of remotely monitoring trace atmospheric constituents is described. The instrument, called a laser absorption spectrometer, can be operated from an aircraft or spacecraft to measure the concentration of selected gases in three dimensions. This device will be particularly useful for rapid determination of pollutant levels in urban areas.

The Nagoya cosmic-ray muon spectrometer 3, part 3: Automatic film scanning equipment

NASA Technical Reports Server (NTRS)

Shibata, S.; Kamiya, Y.; Iijima, K.; Iida, S.

1985-01-01

In the regular operation of the Nagoya cosmic-ray muon spectrometer, about 2000 events per day will be recorded on the photographic film. To derive the track locations from such a huge number of photographs with high accuracy in a short time, an automatic film scanning device has been developed.

Soft x-ray spectrometer (SXS): the high-resolution cryogenic spectrometer onboard ASTRO-H

NASA Astrophysics Data System (ADS)

Mitsuda, Kazuhisa; Kelley, Richard L.; Akamatsu, Hiroki; Bialas, Thomas; Boyce, Kevin R.; Brown, Gregory V.; Canavan, Edgar; Chiao, Meng; Costantini, Elisa; den Herder, Jan-Willem; de Vries, Cor; DiPirro, Michael J.; Eckart, Megan E.; Ezoe, Yuichiro; Fujimoto, Ryuichi; Haas, Daniel; Hoshino, Akio; Ishikawa, Kumi; Ishisaki, Yoshitaka; Iyomoto, Naoko; Kilbourne, Caroline A.; Kimball, Mark; Kitamoto, Shunji; Konami, Saori; Leutenegger, Maurice A.; McCammon, Dan; Miko, Joseph; Mitsuishi, Ikuyuki; Murakami, Hiroshi; Murakami, Masahide; Noda, Hirofumi; Ogawa, Mina; Ohashi, Takaya; Okamoto, Atsushi; Ota, Naomi; Paltani, Stéphane; Porter, F. Scott; Sato, Kosuke; Sato, Yoichi; Sawada, Makoto; Seta, Hiromi; Shinozaki, Keisuke; Shirron, Peter J.; Sneiderman, Gary A.; Sugita, Hiroyuki; Szymkowiak, Andrew; Takei, Yoh; Tamagawa, Toru; Tashiro, Makoto S.; Terada, Yukikatsu; Tsujimoto, Masahiro; Yamada, Shinya; Yamasaki, Noriko Y.

2014-07-01

We present the development status of the Soft X-ray Spectrometer (SXS) onboard the ASTRO-H mission. The SXS provides the capability of high energy-resolution X-ray spectroscopy of a FWHM energy resolution of < 7eV in the energy range of 0.3 - 10 keV. It utilizes an X-ray micorcalorimeter array operated at 50 mK. The SXS microcalorimeter subsystem is being developed in an EM-FM approach. The EM SXS cryostat was developed and fully tested and, although the design was generally confirmed, several anomalies and problems were found. Among them is the interference of the detector with the micro-vibrations from the mechanical coolers, which is the most difficult one to solve. We have pursued three different countermeasures and two of them seem to be effective. So far we have obtained energy resolutions satisfying the requirement with the FM cryostat.

Signal and background considerations for the MRSt on the National Ignition Facility (NIF).

PubMed

Wink, C W; Frenje, J A; Hilsabeck, T J; Bionta, R; Khater, H Y; Gatu Johnson, M; Kilkenny, J D; Li, C K; Séguin, F H; Petrasso, R D

2016-11-01

A Magnetic Recoil Spectrometer (MRSt) has been conceptually designed for time-resolved measurements of the neutron spectrum at the National Ignition Facility. Using the MRSt, the goals are to measure the time-evolution of the spectrum with a time resolution of ∼20-ps and absolute accuracy better than 5%. To meet these goals, a detailed understanding and optimization of the signal and background characteristics are required. Through ion-optics, MCNP simulations, and detector-response calculations, it is demonstrated that the goals and a signal-to background >5-10 for the down-scattered neutron measurement are met if the background, consisting of ambient neutrons and gammas, at the MRSt is reduced 50-100 times.

Signal and background considerations for the MRSt on the National Ignition Facility (NIF)

DOE PAGES

Wink, C. W.; Frenje, J. A.; Hilsabeck, T. J.; ...

2016-08-03

A Magnetic Recoil Spectrometer (MRSt) has been conceptually designed for time-resolved measurements of the neutron spectrum at the National Ignition Facility. Using the MRSt, the goals are to measure the time-evolution of the spectrum with a time resolution of ~20-ps and absolute accuracy better than 5%. To meet these goals, a detailed understanding and optimization of the signal and background characteristics are required. Through ion-optics, MCNP simulations, and detector-response calculations, we demonstrate that the goals and a signal-to background >5-10 for the down-scattered neutron measurement are met if the background, consisting of ambient neutrons and gammas, at the MRSt ismore » reduced 50-100 times.« less

Permanent-magnet energy spectrometer for electron beams from radiotherapy accelerators

DOE Office of Scientific and Technical Information (OSTI.GOV)

McLaughlin, David J.; Shikhaliev, Polad M.; Matthews, Kenneth L.

2015-09-15

Purpose: The purpose of this work was to adapt a lightweight, permanent magnet electron energy spectrometer for the measurement of energy spectra of therapeutic electron beams. Methods: An irradiation geometry and measurement technique were developed for an approximately 0.54-T, permanent dipole magnet spectrometer to produce suitable latent images on computed radiography (CR) phosphor strips. Dual-pinhole electron collimators created a 0.318-cm diameter, approximately parallel beam incident on the spectrometer and an appropriate dose rate at the image plane (CR strip location). X-ray background in the latent image, reduced by a 7.62-cm thick lead block between the pinhole collimators, was removed usingmore » a fitting technique. Theoretical energy-dependent detector response functions (DRFs) were used in an iterative technique to transform CR strip net mean dose profiles into energy spectra on central axis at the entrance to the spectrometer. These spectra were transformed to spectra at 95-cm source to collimator distance (SCD) by correcting for the energy dependence of electron scatter. The spectrometer was calibrated by comparing peak mean positions in the net mean dose profiles, initially to peak mean energies determined from the practical range of central-axis percent depth-dose (%DD) curves, and then to peak mean energies that accounted for how the collimation modified the energy spectra (recalibration). The utility of the spectrometer was demonstrated by measuring the energy spectra for the seven electron beams (7–20 MeV) of an Elekta Infinity radiotherapy accelerator. Results: Plots of DRF illustrated their dependence on energy and position in the imaging plane. Approximately 15 iterations solved for the energy spectra at the spectrometer entrance from the measured net mean dose profiles. Transforming those spectra into ones at 95-cm SCD increased the low energy tail of the spectra, while correspondingly decreasing the peaks and shifting them to

Permanent-magnet energy spectrometer for electron beams from radiotherapy accelerators.

PubMed

McLaughlin, David J; Hogstrom, Kenneth R; Carver, Robert L; Gibbons, John P; Shikhaliev, Polad M; Matthews, Kenneth L; Clarke, Taylor; Henderson, Alexander; Liang, Edison P

2015-09-01

The purpose of this work was to adapt a lightweight, permanent magnet electron energy spectrometer for the measurement of energy spectra of therapeutic electron beams. An irradiation geometry and measurement technique were developed for an approximately 0.54-T, permanent dipole magnet spectrometer to produce suitable latent images on computed radiography (CR) phosphor strips. Dual-pinhole electron collimators created a 0.318-cm diameter, approximately parallel beam incident on the spectrometer and an appropriate dose rate at the image plane (CR strip location). X-ray background in the latent image, reduced by a 7.62-cm thick lead block between the pinhole collimators, was removed using a fitting technique. Theoretical energy-dependent detector response functions (DRFs) were used in an iterative technique to transform CR strip net mean dose profiles into energy spectra on central axis at the entrance to the spectrometer. These spectra were transformed to spectra at 95-cm source to collimator distance (SCD) by correcting for the energy dependence of electron scatter. The spectrometer was calibrated by comparing peak mean positions in the net mean dose profiles, initially to peak mean energies determined from the practical range of central-axis percent depth-dose (%DD) curves, and then to peak mean energies that accounted for how the collimation modified the energy spectra (recalibration). The utility of the spectrometer was demonstrated by measuring the energy spectra for the seven electron beams (7-20 MeV) of an Elekta Infinity radiotherapy accelerator. Plots of DRF illustrated their dependence on energy and position in the imaging plane. Approximately 15 iterations solved for the energy spectra at the spectrometer entrance from the measured net mean dose profiles. Transforming those spectra into ones at 95-cm SCD increased the low energy tail of the spectra, while correspondingly decreasing the peaks and shifting them to slightly lower energies. Energy calibration

Small Explorer (SMEX) POsitron Electron Magnet Spectrometer (POEMS)

NASA Technical Reports Server (NTRS)

LHeureux, Jacques; Evenson, Paul A.; Aleman, R. (Technical Monitor)

1995-01-01

This report covers the activities of Louisiana State University (LSU) under subcontract 26053-EX between LSU and the Bartol Research Institute (Bartol), which began January 1, 1994. The purpose of this subcontract was for LSU to participate in and support Bartol in the work to define the SMEX (Small Explorer)/POEMS (Positron Electron Magnet Spectrometer) spaceflight mission under NASA Contract NAS5-38098 between NASA and Bartol. The conclusions of this study were that for a 1998 launch into a 600km altitude, 98 degrees, approximately sun synchronous orbit, (a) the total radiation dose would be typically a few k-rad per year, certainly less than 20 k-rad per year for the anticipated shielding and potential solar flare environment, (b) detector counting rates would be dominated by the South Atlantic Anomaly (SAA) and the horns of the Van Allen belts, (c) the galactic electron and positron 'signal' can be extracted from the albedo background and the trapped populations by detailed evaluation of the geomagnetic transmission function (cut-off) for each event, (d) POEMS could make significant contributions to magnetospheric science if sufficient downlink capacity were provided and, (e) a fully functioning, cost efficient, data processing and analysis facility design was developed for the mission. Overall, POEMS was found to be a relatively simple experiment to manifest, operate and analyze and had potential for fundamental new discoveries in cosmic, heliospheric, solar and magnetospheric science.

Construction and test of new precision drift-tube chambers for the ATLAS muon spectrometer

NASA Astrophysics Data System (ADS)

Kroha, H.; Kortner, O.; Schmidt-Sommerfeld, K.; Takasugi, E.

2017-02-01

ATLAS muon detector upgrades aim for increased acceptance for muon triggering and precision tracking and for improved rate capability of the muon chambers in the high-background regions of the detector with increasing LHC luminosity. The small-diameter Muon Drift Tube (sMDT) chambers have been developed for these purposes. With half of the drift-tube diameter of the MDT chambers and otherwise unchanged operating parameters, sMDT chambers share the advantages of the MDTs, but have an order of magnitude higher rate capability and can be installed in detector regions where MDT chambers do not fit in. The chamber assembly methods have been optimized for mass production, minimizing construction time and personnel. Sense wire positioning accuracies of 5 μm have been achieved in serial production for large-size chambers comprising several hundred drift tubes. The construction of new sMDT chambers for installation in the 2016/17 winter shutdown of the LHC and the design of sMDT chambers in combination with new RPC trigger chambers for replacement of the inner layer of the barrel muon spectrometer are in progress.

Handheld dual thermal neutron detector and gamma-ray spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Stowe, Ashley C.; Burger, Arnold; Bhattacharya, Pijush

2017-05-02

A combined thermal neutron detector and gamma-ray spectrometer system, including: a first detection medium including a lithium chalcopyrite crystal operable for detecting neutrons; a gamma ray shielding material disposed adjacent to the first detection medium; a second detection medium including one of a doped metal halide, an elpasolite, and a high Z semiconductor scintillator crystal operable for detecting gamma rays; a neutron shielding material disposed adjacent to the second detection medium; and a photodetector coupled to the second detection medium also operable for detecting the gamma rays; wherein the first detection medium and the second detection medium do not overlapmore » in an orthogonal plane to a radiation flux. Optionally, the first detection medium includes a .sup.6LiInSe.sub.2 crystal. Optionally, the second detection medium includes a SrI.sub.2(Eu) scintillation crystal.« less

The GRB All-sky Spectrometer Experiment II: Data Collection and Analysis

NASA Astrophysics Data System (ADS)

Voigt, Elana; Martinot, Zachary; Banks, Zachary; Pober, Jonathan; Morales, Miguel F.

2015-01-01

The GRB All-sky Spectrometer Experiment (GASE) is a widefield interferometer radio telescope designed to look for Gamma Ray Bursts in the 30 to 50 MHz range. It is based and operated as a wholly undergraduate experiment at the University of Washington. This poster will focus on data analysis and the relation of data analysis to the commissioning process of our 8 element GASE array.

Miniature Raman spectrometer development

NASA Astrophysics Data System (ADS)

Bonvallet, Joseph; Auz, Bryan; Rodriguez, John; Olmstead, Ty

2018-02-01

The development of techniques to rapidly identify samples ranging from, molecule and particle imaging to detection of high explosive materials, has surged in recent years. Due to this growing want, Raman spectroscopy gives a molecular fingerprint, with no sample preparation, and can be done remotely. These systems can be small, compact, lightweight, and with a user interface that allows for easy use and sample identification. Ocean Optics Inc. has developed several systems that would meet all these end user requirements. This talk will describe the development of different Ocean Optics Inc miniature Raman spectrometers. The spectrometer on a phone (SOAP) system was designed using commercial off the shelf (COTS) components, in a rapid product development cycle. The footprint of the system measures 40x40x14 mm (LxWxH) and was coupled directly to the cell phone detector camera optics. However, it gets roughly only 40 cm-1 resolution. The Accuman system is the largest (290x220X100 mm) of the three, but uses our QEPro spectrometer and get 7-11 cm-1 resolution. Finally, the HRS-30 measuring 165x85x40 mm is a combination of the other two systems. This system uses a modified EMBED spectrometer and gets 7-12 cm-1 resolution. Each of these units uses a peak matching algorithm that then correlates the results to the pre-loaded and customizable spectral libraries.

Ultraviolet spectrometer experiment for the Voyager mission

NASA Technical Reports Server (NTRS)

Broadfoot, A. L.; Sandel, B. R.; Shemansky, D. E.; Atreya, S. K.; Donahue, T. M.; Moos, H. W.; Bertaux, J. L.; Blamont, J. E.; Ajello, J. M.; Strobel, D. F.

1977-01-01

An objective grating spectrometer covering the wavelength range of 500 to 1700 A with a 10-A resolution is employed for the Voyager ultraviolet spectrometer experiment. In determining the composition and structure of the atmospheres of Saturn, Jupiter and several satellites, the ultraviolet spectrometer will rely on airglow mode observations to measure radiation from the atmospheres due to resonant scattering of solar flux, and the occultation mode for assessments of the atmospheric extinction of solar or stellar radiation as the spacecraft enters shadow zones. Since it is capable of prolonged stellar observations in the 500 to 1000 A wavelength range, the spectrometer is expected to make important contributions to exploratory studies of UV sources.

Ultralow field NMR spectrometer with an atomic magnetometer near room temperature

NASA Astrophysics Data System (ADS)

Liu, Guobin; Li, Xiaofeng; Sun, Xianping; Feng, Jiwen; Ye, Chaohui; Zhou, Xin

2013-12-01

We present a Cs atomic magnetometer with a sensitivity of 150 fT/Hz1/2 operating near room temperature. The nuclear magnetic resonance (NMR) signal of 125 μL tap water was detected at an ultralow magnetic field down to 47 nT, with the signal-to-noise ratio (SNR) of the NMR signal approaching 50 after eight averages. Relaxivity experiments with a Gd(DTPA) contrast agent in zero field were performed, in order to show the magnetometer's ability to measure spin-lattice relaxation time with high accuracy. This demonstrates the feasibility of an ultralow field NMR spectrometer based on a Cs atomic magnetometer, which has a low working temperature, short data acquisition time and high sensitivity. This kind of NMR spectrometer has great potential in applications such as chemical analysis and magnetic relaxometry detection in ultralow or zero fields.

The SOFIA/SAFIRE Far-Infrared Spectrometer: Highlighting Submillimeter Astrophysics and Technology

NASA Technical Reports Server (NTRS)

Benford, Dominic J.

2009-01-01

The Submillimeter and Far-InfraRed Experiment (SAFIRE) on the SOFIA airborne observatory is an imaging spectrometer for wavelengths between 28 microns and 440 microns. Our design is a dual-band long-slit grating spectrometer, which provides broadband (approx. 4000 km/s) observations in two lines simultaneously over a field of view roughly 10" wide by 320" long. The low backgrounds in spectroscopy require very sensitive detectors with noise equivalent powers of order 10(exp -18) W/square root of Hz. We are developing a kilopixel, filled detector array for SAFIRE in a 32 x 40 format. The detector consists of a transition edge sensor (TES) bolometer array, a per-pixel broadband absorbing backshort array, and a NIST SQUID multiplexer readout array. This general type of array has been used successfully in the GISMO instrument, so we extrapolate to the sensitivity needed for airborne spectroscopy. Much of the cryogenic, electronics, and software infrastructure for SAFIRE have been developed. I provide here an overview of the progress on SAFIRE.

The RITA spectrometer at Risø - design considerations and recent results

NASA Astrophysics Data System (ADS)

Clausen, K. N.; McMorrow, D. F.; Lefmann, K.; Aeppli, G.; Mason, T. E.; Schröder, A.; Issikii, M.; Nohara, M.; Takagi, H.

In the new cold triple axis spectrometer RITA at Risø we have improved the front end by extensive use of state of the art optical elements and better shielding material. The analyser system is situated in one large open tank and consists of seven individually orientable PG(002) crystal analyser blades, and a 170 mm by 120 mm 2 areas sensitive micro-strip detector. In comparison to the old TAS6 spectrometer we have obtained a factor 2-5 gain in intensity on the sample, a substantially lower background, much more flexibility for optimising the instrument and the possibility to go beyond simple point-by-point inspection. The excellent performance of RITA in the standard TAS mode is exemplified by a study of the dynamics of ≈ 15 nm hematite (α-Fe 2O 3) nano-particles, and utilisation of horizontal and vertical focusing modes to study two dimensional systems is illustrated by a study of the spin fluctuations in the high Tc superconductor La 1.83Sr 0.17CuO 4.

Performance of the helium dewar and the cryocoolers of the Hitomi soft x-ray spectrometer

NASA Astrophysics Data System (ADS)

Fujimoto, Ryuichi; Takei, Yoh; Mitsuda, Kazuhisa; Yamasaki, Noriko Y.; Tsujimoto, Masahiro; Koyama, Shu; Ishikawa, Kumi; Sugita, Hiroyuki; Sato, Yoichi; Shinozaki, Keisuke; Okamoto, Atsushi; Kitamoto, Shunji; Hoshino, Akio; Sato, Kosuke; Ezoe, Yuichiro; Ishisaki, Yoshitaka; Yamada, Shinya; Seta, Hiromi; Ohashi, Takaya; Tamagawa, Toru; Noda, Hirofumi; Sawada, Makoto; Tashiro, Makoto; Yatsu, Yoichi; Mitsuishi, Ikuyuki; Kanao, Kenichi; Yoshida, Seiji; Miyaoka, Mikio; Tsunematsu, Shoji; Otsuka, Kiyomi; Narasaki, Katsuhiro; DiPirro, Michael J.; Shirron, Peter J.; Sneiderman, Gary A.; Kilbourne, Caroline A.; Porter, Frederick Scott; Chiao, Meng P.; Eckart, Megan E.

2018-01-01

The soft x-ray spectrometer (SXS) was a cryogenic high-resolution x-ray spectrometer onboard the Hitomi (ASTRO-H) satellite that achieved energy resolution of 5 eV at 6 keV, by operating the detector array at 50 mK using an adiabatic demagnetization refrigerator (ADR). The cooling chain from room temperature to the ADR heat sink was composed of two-stage Stirling cryocoolers, a He4 Joule-Thomson cryocooler, and superfluid liquid helium and was installed in a dewar. It was designed to achieve a helium lifetime of more than 3 years with a minimum of 30 L. The satellite was launched on February 17, 2016, and the SXS worked perfectly in orbit, until March 26 when the satellite lost its function. It was demonstrated that the heat load on the helium tank was about 0.7 mW, which would have satisfied the lifetime requirement. This paper describes the design, results of ground performance tests, prelaunch operations, and initial operation and performance in orbit of the flight dewar and the cryocoolers.

From a single encapsulated detector to the spectrometer for INTEGRAL satellite: predicting the peak-to-total ratio at high γ-energies

NASA Astrophysics Data System (ADS)

Kshetri, R.

2012-12-01

In two recent papers (R. Kshetri, JINST 2012 7 P04008; ibid., P07006), a probabilistic formalism was introduced to predict the response of encapsulated type composite germanium detectors like the SPI (spectrometer for INTEGRAL satellite). Predictions for the peak-to-total and peak-to-background ratios are given at 1.3 MeV for the addback mode of operation. The application of the formalism to clover germanium detector is discussed in two separate papers (R. Kshetri, JINST 2012 7 P07008; ibid., P08015). Using the basic approach developed in those papers, for the first time we present a procedure for calculating the peak-to-total ratio of the cluster detector for γ-energies up to 8 MeV. Results are shown for both bare and suppressed detectors as well as for the single crystal and addback modes of operation. We have considered the experimental data of (i) peak-to-total ratio at 1.3 MeV, and (ii) single detector efficiency and addback factor for other energies up to 8 MeV. Using this data, an approximate method of calculating the peak-to-total ratio of other composite detectors, is shown. Experimental validation of our approach (for energies up to 8 MeV) has been confirmed considering the data of the SPI spectrometer. We have discussed about comparisons between various modes of operation and suppression cases. The present paper is the fifth in the series of papers on composite germanium detectors and for the first time discusses about the change in fold distribution and peak-to-total ratio for sophisticated detectors consisting of several modules of miniball, cluster and SPI detectors. Our work could provide a guidance in designing new composite detectors and in performing experimental studies with the existing detectors for high energy gamma-rays.

SuperSpec, The On-Chip Spectrometer: Improved NEP and Antenna Performance

NASA Astrophysics Data System (ADS)

Wheeler, Jordan; Hailey-Dunsheath, S.; Shirokoff, E.; Barry, P. S.; Bradford, C. M.; Chapman, S.; Che, G.; Doyle, S.; Glenn, J.; Gordon, S.; Hollister, M.; Kovács, A.; LeDuc, H. G.; Mauskopf, P.; McGeehan, R.; McKenney, C.; Reck, T.; Redford, J.; Ross, C.; Shiu, C.; Tucker, C.; Turner, J.; Walker, S.; Zmuidzinas, J.

2018-05-01

SuperSpec is a new technology for mm and sub-mm spectroscopy. It is an on-chip spectrometer being developed for multi-object, moderate-resolution (R˜ 300 ), large bandwidth survey spectroscopy of high-redshift galaxies for the 1 mm atmospheric window. This band accesses the CO ladder in the redshift range of z = 0-4 and the [CII] 158 μm line from redshift z = 5-9. SuperSpec employs a novel architecture in which detectors are coupled to a series of resonant filters along a single microwave feedline instead of using dispersive optics. This construction allows for the creation of a full spectrometer occupying only ˜ 10 cm^2 of silicon, a reduction in size of several orders of magnitude when compared to standard grating spectrometers. This small profile enables the production of future multi-beam spectroscopic instruments envisioned for the millimeter band to measure the redshifts of dusty galaxies efficiently. The SuperSpec collaboration is currently pushing toward the deployment of a SuperSpec demonstration instrument in fall of 2018. The progress with the latest SuperSpec prototype devices is presented; reporting increased responsivity via a reduced inductor volume (2.6 μm^3 ) and the incorporation of a new broadband antenna. A detector NEP of 3-4 × 10^{-18} W/Hz^{0.5} is obtained, sufficient for background-limited observation on mountaintop sites. In addition, beam maps and efficiency measurements of a new wide-band dual bow-tie slot antenna are shown.

Infrared Spectrometer for ExoMars: A Mast-Mounted Instrument for the Rover.

PubMed

Korablev, Oleg I; Dobrolensky, Yurii; Evdokimova, Nadezhda; Fedorova, Anna A; Kuzmin, Ruslan O; Mantsevich, Sergei N; Cloutis, Edward A; Carter, John; Poulet, Francois; Flahaut, Jessica; Griffiths, Andrew; Gunn, Matthew; Schmitz, Nicole; Martín-Torres, Javier; Zorzano, Maria-Paz; Rodionov, Daniil S; Vago, Jorge L; Stepanov, Alexander V; Titov, Andrei Yu; Vyazovetsky, Nikita A; Trokhimovskiy, Alexander Yu; Sapgir, Alexander G; Kalinnikov, Yurii K; Ivanov, Yurii S; Shapkin, Alexei A; Ivanov, Andrei Yu

ISEM (Infrared Spectrometer for ExoMars) is a pencil-beam infrared spectrometer that will measure reflected solar radiation in the near infrared range for context assessment of the surface mineralogy in the vicinity of the ExoMars rover. The instrument will be accommodated on the mast of the rover and will be operated together with the panoramic camera (PanCam), high-resolution camera (HRC). ISEM will study the mineralogical and petrographic composition of the martian surface in the vicinity of the rover, and in combination with the other remote sensing instruments, it will aid in the selection of potential targets for close-up investigations and drilling sites. Of particular scientific interest are water-bearing minerals, such as phyllosilicates, sulfates, carbonates, and minerals indicative of astrobiological potential, such as borates, nitrates, and ammonium-bearing minerals. The instrument has an ∼1° field of view and covers the spectral range between 1.15 and 3.30 μm with a spectral resolution varying from 3.3 nm at 1.15 μm to 28 nm at 3.30 μm. The ISEM optical head is mounted on the mast, and its electronics box is located inside the rover's body. The spectrometer uses an acousto-optic tunable filter and a Peltier-cooled InAs detector. The mass of ISEM is 1.74 kg, including the electronics and harness. The science objectives of the experiment, the instrument design, and operational scenarios are described. Key Words: ExoMars-ISEM-Mars-Surface-Mineralogy-Spectroscopy-AOTF-Infrared. Astrobiology 17, 542-564.

Landsat-Swath Imaging Spectrometer Design

NASA Technical Reports Server (NTRS)

Mouroulis, Pantazis; Green, Robert O.; Van Gorp, Byron; Moore, Lori; Wilson, Daniel W.; Bender, Holly A.

2015-01-01

We describe the design of a high-throughput pushbroom imaging spectrometer and telescope system that is capable of Landsat swath and resolution while providing better than 10 nm per pixel spectral resolution. The design is based on a 3200 x 480 element x 18 µm pixel size focal plane array, two of which are utilized to cover the full swath. At an optical speed of F/1.8, the system is the fastest proposed to date to our knowledge. The utilization of only two spectrometer modules fed from the same telescope reduces system complexity while providing a solution within achievable detector technology. Predictions of complete system response are shown. Also, it is shown that detailed ghost analysis is a requirement for this type of spectrometer and forms an essential part of a complete design.

Imaging spectrometer using a liquid crystal tunable filter

NASA Astrophysics Data System (ADS)

Chrien, Thomas G.; Chovit, Christopher; Miller, Peter J.

1993-09-01

A demonstration imaging spectrometer using a liquid crystal tunable filter (LCTF) was built and tested on a hot air balloon platform. The LCTF is a tunable polarization interference or Lyot filter. The LCTF enables a small, light weight, low power, band sequential imaging spectrometer design. An overview of the prototype system is given along with a description of balloon experiment results. System model performance predictions are given for a future LCTF based imaging spectrometer design. System design considerations of LCTF imaging spectrometers are discussed.

Design and manufacture of the integrated field unit for the NIRSpec spectrometer on JWST

NASA Astrophysics Data System (ADS)

Lobb, Daniel; Robertson, David; Closs, Martin; Barnes, Andy

2008-09-01

The NIRSpec imaging spectrometer, which forms part of the James Webb Space Telescope instrumentation, will include an integrated field unit (IFU). The IFU will be tasked specifically with efficient analysis of extended objects, including galaxies; it will accept a square image area at the spectrometer entrance field, dissect this area into 30 parallel sub-slits, and image the sub-slits end-to-end, forming a single virtual entrance slit. The IFU, uses all-mirror optics to operate over the spectral range 700nm to 5000nm. 95 mirrors and the main support structure are made in a common aluminium alloy, to achieve athermal performance down to an operating temperature of around 30K. Relatively complex mirror surface shapes are produced by diamond machining. The IFU has been designed and constructed by SSTL, with optics produced by CfAI; the unit is currently undergoing performance tests. This paper describes the IFU optical design and performance, and outlines the mirror manufacturing methods and alignment procedures.

JWST-MIRI spectrometer main optics design and main results

NASA Astrophysics Data System (ADS)

Navarro, Ramón; Schoenmaker, Ton; Kroes, Gabby; Oudenhuysen, Ad; Jager, Rieks; Venema, Lars

2017-11-01

MIRI ('Mid InfraRed Instrument') is the combined imager and integral field spectrometer for the 5-29 micron wavelength range under development for the James Webb Space Telescope JWST. The flight acceptance tests of the Spectrometer Main Optics flight models (SMO), part of the MIRI spectrometer, are completed in the summer of 2008 and the system is delivered to the MIRI-JWST consortium. The two SMO arms contain 14 mirrors and form the MIRI optical system together with 12 selectable gratings on grating wheels. The entire system operates at a temperature of 7 Kelvin and is designed on the basis of a 'no adjustments' philosophy. This means that the optical alignment precision depends strongly on the design, tolerance analysis and detailed knowledge of the manufacturing process. Because in principle no corrections are needed after assembly, continuous tracking of the alignment performance during the design and manufacturing phases is important. The flight hardware is inspected with respect to performance parameters like alignment and image quality. The stability of these parameters is investigated after exposure to various vibration levels and successive cryogenic cool downs. This paper describes the philosophy behind the acceptance tests, the chosen test strategy and reports the results of these tests. In addition the paper covers the design of the optical test setup, focusing on the simulation of the optical interfaces of the SMO. Also the relation to the SMO qualification and verification program is addressed.

New search for double electron capture in {sup 106}Cd decay with the TGV-2 spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Briançon, Ch.; Brudanin, V. B.; Egorov, V. G.

2015-09-15

A new experiment devoted to searches for double electron capture in {sup 106}Cd decay is being performed at the Modane underground laboratory (4800 mwe) with the 32-detector TGV-2 spectrometer. The limit T{sub 1/2}(2νEC/EC) > 2.0×10{sup 20} yr at a 90%confidence level (C.L.) was obtained from a preliminary analysis of data obtained over 2250 h of measurements with about 23.2 g sample enriched in the isotope {sup 106}Cd to 99.57%. The limits T{sub 1/2}(KL, 2741 keV) > 0.9 × 10{sup 20} yr and T{sub 1/2}(KK, 2718 keV) ≫ 1.4 × 10{sup 20} yr at a 90% C.L. on the neutrinoless decaymore » of {sup 106}Cd were obtained from measurements performed with the Obelix low-background spectrometer from high-purity germanium (HPGe spectrometer) for a sample of mass about 23.2 g enriched in the isotope {sup 106}Cd.« less

Conversion electrons from high-statistics β-decay measurements with the 8π spectrometer at TRIUMF-ISAC

NASA Astrophysics Data System (ADS)

Garrett, P. E.; Jigmeddorj, B.; Radich, A. J.; Andreoiu, C.; Ball, G. C.; Bangay, J. C.; Bianco, L.; Bildstein, V.; Chagnon-Lessard, S.; Cross, D. S.; Demand, G. A.; Diaz Varela, A.; Dunlop, R.; Finlay, P.; Garnsworthy, A. B.; Green, K. L.; Hackman, G.; Hadinia, B.; Leach, K. G.; Michetti-Wilson, J.; Orce, J. N.; Rajabali, M. M.; Rand, E. T.; Starosta, K.; Sumithrarachchi, C.; Svensson, C. E.; Triambak, S.; Wang, Z. M.; Williams, S. J.; Wood, J. L.; Wong, J.; Yates, S. W.; Zganjar, E. F.

2016-09-01

The 8π spectrometer, located at TRIUMF-ISAC, was the world's most powerful spectrometer dedicated to β-decay studies until its decommissioning in early 2014 for replacement with the GRIFFIN array. An integral part of the 8π spectrometer was the Pentagonal Array for Conversion Electron Spectroscopy (PACES) consisting of 5 Si(Li) detectors used for charged-particle detection. PACES enabled both γ - e- and e- - e- coincidence measurements, which were crucial for increasing the sensitivity for discrete e- lines in the presence of large backgrounds. Examples from a 124Cs decay experiment, where the data were vital for the expansion of the 124Cs decay scheme, are shown. With suffcient statistics, measurements of conversion coeffcients can be used to extract the E0 components of Jπ → Jπ transitions for J ≠ 0, which is demonstrated for data obtained in 110In→110Cd decay. With knowledge of the shapes of the states involved, as obtained, for example, from the use of Kumar-Cline shape invariants, the mixing of the states can be extracted.

Ion mass spectrometer

NASA Technical Reports Server (NTRS)

Neugebauer, M. (Inventor); Clay, D. R.; Goldstein, B. E.; Goldstein, R.

1984-01-01

An ion mass spectrometer is described which detects and indicates the characteristics of ions received over a wide angle, and which indicates the mass to charge ratio, the energy, and the direction of each detected ion. The spectrometer includes a magnetic analyzer having a sector magnet that passes ions received over a wide angle, and an electrostatic analyzer positioned to receive ions passing through the magnetic analyzer. The electrostatic analyzer includes a two dimensional ion sensor at one wall of the analyzer chamber, that senses not only the lengthwise position of the detected ion to indicate its mass to charge ratio, but also detects the ion position along the width of the chamber to indicate the direction in which the ion was traveling.

FAST NEUTRON SPECTROMETER

DOEpatents

Davis, F.J.; Hurst, G.S.; Reinhardt, P.W.

1959-08-18

An improved proton recoil spectrometer for determining the energy spectrum of a fast neutron beam is described. Instead of discriminating against and thereby"throwing away" the many recoil protons other than those traveling parallel to the neutron beam axis as do conventional spectrometers, this device utilizes protons scattered over a very wide solid angle. An ovoidal gas-filled recoil chamber is coated on the inside with a scintillator. The ovoidal shape of the sensitive portion of the wall defining the chamber conforms to the envelope of the range of the proton recoils from the radiator disposed within the chamber. A photomultiplier monitors the output of the scintillator, and a counter counts the pulses caused by protons of energy just sufficient to reach the scintillator.

Achromatic half-wave plate for submillimeter instruments in cosmic microwave background astronomy: experimental characterization.

PubMed

Pisano, Giampaolo; Savini, Giorgio; Ade, Peter A R; Haynes, Vic; Gear, Walter K

2006-09-20

An achromatic half-wave plate (HWP) to be used in millimeter cosmic microwave background (CMB) polarization experiments has been designed, manufactured, and tested. The design is based on the 5-plates Pancharatnam recipe and it works in the frequency range 85-185 GHz. A model has been used to predict the transmission, reflection, absorption, and phase shift as a function of frequency. The HWP has been tested by using coherent radiation from a back-wave oscillator to investigate its modulation efficiency and with incoherent radiation from a polarizing Fourier transform spectrometer (FTS) to explore its frequency behavior. The FTS measurements have been fitted with an optical performance model which is in excellent agreement with the data. A detailed analysis of the data also allows a precise determination of the HWP fast and slow axes in the frequency band of operation. A list of the HWP performance characteristics is reported including estimates of its cross polarization.

Applications of the low-background gamma spectroscopy to the geographical origin of marine salts and prunes

DOE Office of Scientific and Technical Information (OSTI.GOV)

Perrot, F.

The low background gamma spectroscopy has been applied to try to sign the geographical origin of the French atlantic marine salts and of the prunes from Agen. Most of the activity measurements have been done using low background Ge spectrometers located in Bordeaux. Results have shown that a clear signature exists in the case of the French atlantic salts using the 40K, 137Cs and 226Ra isotopes but not in the case of the prunes.

Quantum states of neutrons in the gravitational and centrifugal potentials in a new GRANIT spectrometer

ScienceCinema

Nesvizhevsky, Valery

2018-05-14

We will discuss the scientific program to be studied in a new gravitational spectrometer GRANIT in a broad context of quantum states (quantum behaviour) of ultracold neutrons (UCN) in gravitational [1] and centrifugal [2] potentials, as well as applications of these phenomena/spectrometer to various domains of physics, ranging from studies of fundamental short-range interactions and symmetries to neutron quantum optics and reflectometry using UCN. All these topics, as well as related instrumental and methodical developments have been discussed during dedicated GRANIT-2010 Workshop [3]. The GRANIT spectrometer has been recently installed at the Institut Laue-Langevin, Grenoble, France [4] and could become operational in near future. 1. V.V. Nesvizhevsky et al (2002), Nature 415, 297. 2. V.V. Nesvizhevsky et al (2010), Nature Physics 6, 114. 3. GRANIT-2010, Les Houches, 14-19 february 2010. 4. M. Kreuz et al (2009), NIM 611, 326.

Visible and near-infrared imaging spectrometer (VNIS) for in-situ lunar surface measurements

NASA Astrophysics Data System (ADS)

He, Zhiping; Xu, Rui; Li, Chunlai; Lv, Gang; Yuan, Liyin; Wang, Binyong; Shu, Rong; Wang, Jianyu

2015-10-01

The Visible and Near-Infrared Imaging Spectrometer (VNIS) onboard China's Chang'E 3 lunar rover is capable of simultaneously in situ acquiring full reflectance spectra for objects on the lunar surface and performing calibrations. VNIS uses non-collinear acousto-optic tunable filters and consists of a VIS/NIR imaging spectrometer (0.45-0.95 μm), a shortwave IR spectrometer (0.9-2.4 μm), and a calibration unit with dust-proofing functionality. To been underwent a full program of pre-flight ground tests, calibrations, and environmental simulation tests, VNIS entered into orbit around the Moon on 6 December 2013 and landed on 14 December 2013 following Change'E 3. The first operations of VNIS were conducted on 23 December 2013, and include several explorations and calibrations to obtain several spectral images and spectral reflectance curves of the lunar soil in the Imbrium region. These measurements include the first in situ spectral imaging detections on the lunar surface. This paper describes the VNIS characteristics, lab calibration, in situ measurements and calibration on lunar surface.

Design of a novel noninvasive spectrometer for pesticide residues monitor

NASA Astrophysics Data System (ADS)

Ren, Zhong; Liu, Guodong; Huang, Zhen

2014-11-01

Although the gas or liquid chromatography had been widely used into pesticide residues monitoring, some drawbacks such as time-consuming, complicated operation and especially the destructivity for samples were existed. To overcome the limits of destructive detection methods, the noninvasive detection method based on spectroscopy was used to detect the pesticide residues in this paper. To overcome low resolution and light-efficiency due to the drawbacks of the classical plane and holography concave gratings, a novel noninvasive spectrometer for pesticide residues monitor (PRM) based on volume holography transmission (VHT) grating was designed. Meanwhile, a custom-built splitting light system for PRM based on the VHT grating was developed. In addition, the linear charge coupled device (CCD) with combined data acquisition (DAQ) card and the virtual-PRM based on LabVIEW were respectively used as the spectral acquisition hardware and software-platform. Experimental results showed that the spectral resolution of this spectrometer reached 2nm, and the VHT grating's diffraction efficiency was gotten via the simulation experiment.

Balloon-borne photoionization mass spectrometer for measurement of stratospheric gases

NASA Technical Reports Server (NTRS)

Aikin, A. C.; Maier, E. J. R.

1978-01-01

A balloon-borne photoionization mass spectrometer used to measure stratospheric trace gases is described. Ions are created with photons from high-intensity krypton discharge lamps and a quadrupole mass analyzer is employed for ion identification. Differential pumping is achieved with liquid helium cryopumping. To insure measurement of unperturbed stratospheric air, the entire system is contained in a sealed gondola and the atmospheric sample is taken some distance away during descent. The photoionization technique allows the detection of a low ionization potential constituent, such as nitric oxide, at less than a part in one billion in the presence of the major atmospheric gases and their isotopes. Operation of the mass spectrometer system was demonstrated during a daytime flight from Palestine, Texas on 26 April 1977. The sensitivity achieved and the unique selectivity afforded by this technique offer a capability for trace constituent measurement not possible with the more conventional electron impact ionization approach.

Dynamic interferometer alignment and its utility in UV Fourier transform spectrometer systems

NASA Technical Reports Server (NTRS)

Dorval, Rick K.; Engel, James R.; Wyntjes, Geert J.

1993-01-01

Dynamic alignment has been demonstrated as a practical approach to alignment maintenance for systems in the infrared region of the spectrum. On the basis of work done by OPTRA, this technique was introduced in commercial Fourier transform spectrometer systems in 1982 and in various forms is now available from a number of manufacturers. This paper reports on work by OPTRA to extend the basic technique to systems operating in the ultraviolet. In addition, this paper reports the preliminary results of the development of an alignment system using a laser diode in place of a gas laser normally found in dynamic alignment systems. A unique optical system and spatial heterodyne technique allows for achievement of a metrology system with characteristics that fully satisfy the requirements of an ultraviolet spectrometer system.

Composite Spectrometer Prisms

NASA Technical Reports Server (NTRS)

Breckinridge, J. B.; Page, N. A.; Rodgers, J. M.

1985-01-01

Efficient linear dispersive element for spectrometer instruments achieved using several different glasses in multiple-element prism. Good results obtained in both two-and three-element prisms using variety of different glass materials.

Automatic detection of recoil-proton tracks and background rejection criteria in liquid scintillator-micro-capillary-array fast neutron spectrometer

NASA Astrophysics Data System (ADS)

Mor, Ilan; Vartsky, David; Dangendorf, Volker; Tittelmeier, Kai.; Weierganz, Mathias; Goldberg, Mark Benjamin; Bar, Doron; Brandis, Michal

2018-06-01

We describe an analysis procedure for automatic unambiguous detection of fast-neutron-induced recoil proton tracks in a micro-capillary array filled with organic liquid scintillator. The detector is viewed by an intensified CCD camera. This imaging neutron detector possesses the capability to perform high position-resolution (few tens of μm), energy-dispersive transmission-imaging using ns-pulsed beams. However, when operated with CW or DC beams, it also features medium-quality spectroscopic capabilities for incident neutrons in the energy range 2-20 MeV. In addition to the recoil proton events which display a continuous extended track structure, the raw images exhibit complex ion-tracks from nuclear interactions of fast-neutrons in the scintillator, capillaries quartz-matrix and CCD. Moreover, as expected, one also observes a multitude of isolated scintillation spots of varying intensity (henceforth denoted "blobs") that originate from several different sources, such as: fragmented proton tracks, gamma-rays, heavy-ion reactions as well as events and noise that occur in the image-intensifier and CCD. In order to identify the continuous-track recoil proton events and distinguish them from all these background events, a rapid, computerized and automatic track-recognition-procedure was developed. Based on an appropriately weighted analysis of track parameters such as: length, width, area and overall light intensity, the method is capable of distinguishing a single continuous-track recoil proton from typically surrounding several thousands of background events that are found in each CCD frame.

An extreme ultraviolet spectrometer experiment for the Shuttle Get Away Special Program

NASA Technical Reports Server (NTRS)

Conway, R. R.; Mccoy, R. P.; Meier, R. R.; Mount, G. H.; Prinz, D. K.; Young, J. M.; Carruthers, G. R.

1984-01-01

An extreme ultraviolet (EUV) spectrometer experiment operated successfully during the STS-7 mission in an experiment to measure the global and diurnal variation of the EUV airglow. The spectrometer is an F 3.5 Wadsworth mount with mechanical collimator, a 75 x 75 mm grating, and a bare microchannel plate detector providing a spectral resolution of 7 X FWHM. Read-out of the signal is through discrete channels or resistive anode techniques. The experiment includes a microcomputer, 20 Mbit tape recorder, and a 28V, 40 Ahr silver-zinc battery. It is the first GAS payload to use an opening door. The spectrometer's 0.1 x 4.2 deg field of view is pointed vertically out of the shuttle bay. During the STS-7 flight data were acquired continuously for a period of 5 hours and 37 minutes, providing spectra of the 570 A to 850 A wavelength region of the airglow. Five diurnal cycles of the 584 A emission of neutral helium and the 834 A emission of ionized atomic oxygen were recorded. The experiment also recorded ion events and pressure pulses associated with thruster firings. The experiment is to fly again on Mission 41-F.

Thermal stabilization of static single-mirror Fourier transform spectrometers

NASA Astrophysics Data System (ADS)

Schardt, Michael; Schwaller, Christian; Tremmel, Anton J.; Koch, Alexander W.

2017-05-01

Fourier transform spectroscopy has become a standard method for spectral analysis of infrared light. With this method, an interferogram is created by two beam interference which is subsequently Fourier-transformed. Most Fourier transform spectrometers used today provide the interferogram in the temporal domain. In contrast, static Fourier transform spectrometers generate interferograms in the spatial domain. One example of this type of spectrometer is the static single-mirror Fourier transform spectrometer which offers a high etendue in combination with a simple, miniaturized optics design. As no moving parts are required, it also features a high vibration resistance and high measurement rates. However, it is susceptible to temperature variations. In this paper, we therefore discuss the main sources for temperature-induced errors in static single-mirror Fourier transform spectrometers: changes in the refractive index of the optical components used, variations of the detector sensitivity, and thermal expansion of the housing. As these errors manifest themselves in temperature-dependent wavenumber shifts and intensity shifts, they prevent static single-mirror Fourier transform spectrometers from delivering long-term stable spectra. To eliminate these shifts, we additionally present a work concept for the thermal stabilization of the spectrometer. With this stabilization, static single-mirror Fourier transform spectrometers are made suitable for infrared process spectroscopy under harsh thermal environmental conditions. As the static single-mirror Fourier transform spectrometer uses the so-called source-doubling principle, many of the mentioned findings are transferable to other designs of static Fourier transform spectrometers based on the same principle.

Galileo Ultraviolet Spectrometer experiment

NASA Technical Reports Server (NTRS)

Hord, C. W.; Mcclintock, W. E.; Stewart, A. I. F.; Barth, C. A.; Esposito, L. W.; Thomas, G. E.; Sandel, B. R.; Hunten, D. M.; Broadfoot, A. L.; Shemansky, D. E.

1992-01-01

The Galileo ultraviolet spectrometer experiment uses data obtained by the Ultraviolet Spectrometer (UVS) mounted on the pointed orbiter scan platform and from the Extreme Ultraviolet Spectrometer (EUVS) mounted on the spinning part of the orbiter with the field of view perpendicular to the spin axis. The UVS is a Ebert-Fastie design that covers the range 113-432 nm with a wavelength resolution of 0.7 nm below 190 and 1.3 nm at longer wavelengths. The UVS spatial resolution is 0.4 deg x 0.1 deg for illuminated disk observations and 1 deg x 0.1 deg for limb geometries. The EUVS is a Voyager design objective grating spectrometer, modified to cover the wavelength range from 54 to 128 nm with wavelength resolution 3.5 nm for extended sources and 1.5 nm for point sources and spatial resolution of 0.87 deg x 0.17 deg. The EUVS instrument will follow up on the many Voyager UVS discoveries, particularly the sulfur and oxygen ion emissions in the Io torus and molecular and atomic hydrogen auroral and airglow emissions from Jupiter. The UVS will obtain spectra of emission, absorption, and scattering features in the unexplored, by spacecraft, 170-432 nm wavelength region. The UVS and EUVS instruments will provide a powerful instrument complement to investigate volatile escape and surface composition of the Galilean satellites, the Io plasma torus, micro- and macro-properties of the Jupiter clouds, and the composition structure and evolution of the Jupiter upper atmosphere.

Mass Spectrometers in Space!

NASA Technical Reports Server (NTRS)

Brinckerhoff, William B.

2012-01-01

Exploration of our solar system over several decades has benefitted greatly from the sensitive chemical analyses offered by spaceflight mass spectrometers. When dealing with an unknown environment, the broadband detection capabilities of mass analyzers have proven extremely valuable in determining the composition and thereby the basic nature of space environments, including the outer reaches of Earth s atmosphere, interplanetary space, the Moon, and the planets and their satellites. Numerous mass analyzer types, including quadrupole, monopole, sector, ion trap, and time-of-flight have been incorporated in flight instruments and delivered robotically to a variety of planetary environments. All such instruments went through a rigorous process of application-specific development, often including significant miniaturization, testing, and qualification for the space environment. Upcoming missions to Mars and opportunities for missions to Venus, Europa, Saturn, Titan, asteroids, and comets provide new challenges for flight mass spectrometers that push to state of the art in fundamental analytical technique. The Sample Analysis at Mars (SAM) investigation on the recently-launch Mars Science Laboratory (MSL) rover mission incorporates a quadrupole analyzer to support direct evolved gas as well as gas chromatograph-based analysis of martian rocks and atmosphere, seeking signs of a past or present habitable environment. A next-generation linear ion trap mass spectrometer, using both electron impact and laser ionization, is being incorporated into the Mars Organic Molecule Analyzer (MOMA) instrument, which will be flown to Mars in 2018. These and other mass spectrometers and mission concepts at various stages of development will be described.

Double difference method in deep inelastic neutron scattering on the VESUVIO spectrometer

NASA Astrophysics Data System (ADS)

Andreani, C.; Colognesi, D.; Degiorgi, E.; Filabozzi, A.; Nardone, M.; Pace, E.; Pietropaolo, A.; Senesi, R.

2003-02-01

The principles of the Double Difference (DD) method, applied to the neutron spectrometer VESUVIO, are discussed. VESUVIO, an inverse geometry spectrometer operating at the ISIS pulsed neutron source in the eV energy region, has been specifically designed to measure the single particle dynamical properties in condensed matter. The width of the nuclear resonance of the absorbing filter, used for the neutron energy analysis, provides the most important contribution to the energy resolution of the inverse geometry instruments. In this paper, the DD method, which is based on a linear combination of two measurements recorded with filter foils of the same resonance material but of different thickness, is shown to improve significantly the instrumental energy resolution, as compared with the Single Difference (SD) method. The asymptotic response functions, derived through Monte-Carlo simulations for polycrystalline Pb and ZrH 2 samples, are analysed in both DD and SD methods, and compared with the experimental ones for Pb sample. The response functions have been modelled for two distinct experimental configurations of the VESUVIO spectrometer, employing 6Li-glass neutron detectors and NaI γ detectors revealing the γ-ray cascade from the ( n,γ) reaction, respectively. The DD method appears to be an effective experimental procedure for Deep Inelastic Neutron Scattering measurements on VESUVIO spectrometer, since it reduces the experimental resolution of the instrument in both 6Li-glass neutron detector and γ detector configurations.

Spectrometer Development in Support of Thomson Scattering Investigations for the Helicon Plasma Experiment (HPX)

NASA Astrophysics Data System (ADS)

Sandri, Eva; Davies, Richard; Azzari, Phil; Frank, John; Frank, Jackson; James, Royce; Hopson, Jordon; Duke-Tinson, Omar; Paolino, Richard; Sherman, Justin; Wright, Erin; Turk, Jeremy

2016-10-01

Now that reproducible plasmas have been created on the Helicon Plasma Experiment (HPX) at the Coast Guard Academy Plasma Laboratory (CGAPL), a high-performance spectrometer utilizing volume-phase-holographic (VPH) grating and a charge coupled device (CCD) camera with a range of 380-1090 nm and resolution of 1024x1024 is being assembled. This spectrometer will collect doppler shifted photons created by exciting the plasma with the first harmonic of a 2.5 J Nd:YAG laser at a wavelength of 1064 nm. Direct measurements of the plasma's temperature and density will be determined using HPX's Thomson Scattering (TS) system as a single spatial point diagnostic. TS has the capability of determining plasma properties on short time scales and will be used to create a robust picture of the internal plasma parameters. A prototype spectrometer has been constructed to explore the Andor CCD camera's resolution and sensitivity. Concurrently, through intensive study of the high energy TS system, safety protocols and standard operation procedures (SOP) for the Coast Guard's largest and most powerful Laser have been developed. The current status of the TS SOP, diagnostic development, and the collection optic's spectrometer will be reported. Supported by U.S. DEPS Grant [HEL-JTO] PRWJFY15-16.

Spacecraft Applications of Compact Optical and Mass Spectrometers

NASA Technical Reports Server (NTRS)

Davinic, N. M.; Nagel, D. J.

1995-01-01

Optical spectrometers, and mass spectrometers to a lesser extent, have a long and rich history of use aboard spacecraft. Space mission applications include deep space science spacecraft, earth orbiting satellites, atmospheric probes, and surface landers, rovers, and penetrators. The large size of capable instruments limited their use to large, expensive spacecraft. Because of the novel application of micro-fabrication technologies, compact optical and mass spectrometers are now available. The new compact devices are especially attractive for spacecraft because of their small mass and volume, as well as their low power consumption. Dispersive optical multi-channel analyzers which cover the 0.4-1.1 micrometer wavelength are now commercially available in packages as small as 3 x 6 x 18 mm exclusive of drive and recording electronics. Mass spectrometers as small as 3 x 3 mm, again without electronics, are under development. A variety of compact optical and mass spectrometers are reviewed in this paper. A number of past space applications are described, along with some upcoming opportunities that are likely candidate missions to fly this new class of compact spectrometers.

An improved nuclear magnetic resonance spectrometer

NASA Technical Reports Server (NTRS)

Elleman, D. D.; Manatt, S. L.

1967-01-01

Cylindrical sample container provides a high degree of nuclear stabilization to a nuclear magnetic resonance /nmr/ spectrometer. It is placed coaxially about the nmr insert and contains reference sample that gives a signal suitable for locking the field and frequency of an nmr spectrometer with a simple audio modulation system.

Geometric correction of synchronous scanned Operational Modular Imaging Spectrometer II hyperspectral remote sensing images using spatial positioning data of an inertial navigation system

NASA Astrophysics Data System (ADS)

Zhou, Xiaohu; Neubauer, Franz; Zhao, Dong; Xu, Shichao

2015-01-01

The high-precision geometric correction of airborne hyperspectral remote sensing image processing was a hard nut to crack, and conventional methods of remote sensing image processing by selecting ground control points to correct the images are not suitable in the correction process of airborne hyperspectral image. The optical scanning system of an inertial measurement unit combined with differential global positioning system (IMU/DGPS) is introduced to correct the synchronous scanned Operational Modular Imaging Spectrometer II (OMIS II) hyperspectral remote sensing images. Posture parameters, which were synchronized with the OMIS II, were first obtained from the IMU/DGPS. Second, coordinate conversion and flight attitude parameters' calculations were conducted. Third, according to the imaging principle of OMIS II, mathematical correction was applied and the corrected image pixels were resampled. Then, better image processing results were achieved.

Tunable hard X-ray spectrometer utilizing asymmetric planes of a quartz transmission crystal

DOE Office of Scientific and Technical Information (OSTI.GOV)

Seely, John F., E-mail: seelyjf@gmail.com; Feldman, Uri; Henins, Albert

2016-05-15

A Cauchois type hard x-ray spectrometer was developed that utilizes the (301) diffraction planes at an asymmetric angle of 23.51° to the normal to the surface of a cylindrically curved quartz transmission crystal. The energy coverage is tunable by rotating the crystal and the detector arm, and spectra were recorded in the 8 keV to 20 keV range with greater than 2000 resolving power. The high resolution results from low aberrations enabled by the nearly perpendicular angle of the diffracted rays with the back surface of the crystal. By using other asymmetric planes of the same crystal and rotating tomore » selected angles, the spectrometer can operate with high resolution up to 50 keV.« less

Isotopic response with small scintillator based gamma-ray spectrometers

DOEpatents

Madden, Norman W [Sparks, NV; Goulding, Frederick S [Lafayette, CA; Asztalos, Stephen J [Oakland, CA

2012-01-24

The intrinsic background of a gamma ray spectrometer is significantly reduced by surrounding the scintillator with a second scintillator. This second (external) scintillator surrounds the first scintillator and has an opening of approximately the same diameter as the smaller central scintillator in the forward direction. The second scintillator is selected to have a higher atomic number, and thus has a larger probability for a Compton scattering interaction than within the inner region. Scattering events that are essentially simultaneous in coincidence to the first and second scintillators, from an electronics perspective, are precluded electronically from the data stream. Thus, only gamma-rays that are wholly contained in the smaller central scintillator are used for analytic purposes.

Evaluation of Aerosol Optical Thickness algorithm for Geostationary Environmental Monitoring Spectrometer (GEMS) Using the OMI Instrument over East Asia

NASA Astrophysics Data System (ADS)

Go, S.; Kim, J.; KIM, M.; Choi, M.; Lim, H.; Torres, O.; Chang, L.; Hong, J.

2016-12-01

Nitrous oxide (N2O) is a powerful greenhouse gas and ozone depleting substance. With high atmospheric backgrounds and small relative signals, N2O emissions have been challenging to observe and understand on regional scales with traditional instrumentation. Fast-response airborne measurements with high precision and accuracy can potentially bridge this observational gap. Here we present flight assessments of a new flight system based on an Aerodyne mini-spectrometer as well as a Los Gatos N2O/CO analyzer during the Fertilizer Emissions Airborne Study (FEAST). With the Scientific Aviation Mooney aircraft, we conducted test flights for both analyzers where a known calibration gas was sampled throughout the flight (`null' tests). Clear altitude/cabin-pressure dependencies were observed for both analyzers if operated in an "off-the-shelf' manner. For the remainder of test flights and the FEAST campaign we used a new flight system based on an Aerodyne mini-spectrometer with the addition of a custom pressure control/calibration system. Instead of using traditional approaches with spectral-zeros and infrequent in-flight calibrations, we employ a high-flow system with stable flow control to enable high frequency (2 minutes), short duration (15 seconds) sampling of a known calibration gas. This approach, supported by the null test, enables correction for spectral drift caused by a variety of factors while maintaining a 90% duty cycle for 1Hz sampling from an aircraft. Preliminary in-flight precisions are estimated at 0.05 ppb, 0.1 ppm, 1 ppb, and 10 ppm for N2O, CO2, CO, and H2O respectively. We also present a further 40 hours of inter-comparison in flight with a Picarro 2301-f ring-down spectrometer demonstrating consistency between CO2 and H2O measurements and no altitude dependent error.

ESR spectrometer with a loop-gap resonator for cw and time resolved studies in a superconducting magnet.

PubMed

Simon, Ferenc; Murányi, Ferenc

2005-04-01

The design and performance of an electron spin resonance spectrometer operating at 3 and 9 GHz microwave frequencies combined with a 9-T superconducting magnet are described. The probehead contains a compact two-loop, one gap resonator, and is inside the variable temperature insert of the magnet enabling measurements in the 0-9T magnetic field and 1.5-400 K temperature range. The spectrometer allows studies on systems where resonance occurs at fields far above the g approximately 2 paramagnetic condition such as in antiferromagnets. The low quality factor of the resonator allows time resolved experiments such as, e.g., longitudinally detected ESR. We demonstrate the performance of the spectrometer on the NaNiO2 antiferromagnet, the MgB2 superconductor, and the RbC60 conducting alkaline fulleride polymer.

Uranium beam characterization at CIRCE for background and contamination determinations.

PubMed

De Cesare, M; De Cesare, N; D'Onofrio, A; Fifield, L K; Gialanella, L; Terrasi, F

2015-09-01

The Accelerator Mass Spectrometry (AMS) is the most sensitive technique, compared either to the Inductively Coupled Plasma (ICP-MS) or Thermal Ionization (TI-MS) mass spectrometer, for the actinide (e.g. (236)U, (x)Pu isotopes) measurements. They are present in environmental samples at the ultra trace level since atmospheric tests of Nuclear Weapons (NWs) performed in the past, deliberate dumping of nuclear waste, nuclear fuel reprocessing, on a large scale, and operation of Nuclear Power Plants (NPPs), on a small scale, have led to the release of a wide range of radioactive nuclides in the environment. At the Center for Isotopic Research on Cultural and Environmental heritage (CIRCE) in Caserta, Italy, an upgraded actinide AMS system, based on a 3-MV pelletron tandem accelerator, has been developed and routinely operated. At CIRCE a charge state distribution as a function of terminal voltage, the beam emittance, measured in the 20° actinides dedicated beam line, as well as the energy and position validation of the U ions were performed in order to determine the best measurement conditions. A (236)U/(238)U isotopic ratio background level of about 5×10(-12) or 3×10(-13), depending on the Time of Flight-Energy (TOF-E) configurations, as well as the spatial distribution of the (235)U, (238)U interferences ions and a (236)U contamination mass of about 0.5 fg have been determined. Copyright © 2015 Elsevier Ltd. All rights reserved.

Signal and background considerations for the MRSt on the National Ignition Facility (NIF)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wink, C. W., E-mail: cwink@mit.edu; Frenje, J. A.; Gatu Johnson, M.

2016-11-15

A Magnetic Recoil Spectrometer (MRSt) has been conceptually designed for time-resolved measurements of the neutron spectrum at the National Ignition Facility. Using the MRSt, the goals are to measure the time-evolution of the spectrum with a time resolution of ∼20-ps and absolute accuracy better than 5%. To meet these goals, a detailed understanding and optimization of the signal and background characteristics are required. Through ion-optics, MCNP simulations, and detector-response calculations, it is demonstrated that the goals and a signal-to background >5–10 for the down-scattered neutron measurement are met if the background, consisting of ambient neutrons and gammas, at the MRStmore » is reduced 50–100 times.« less

The superconducting high-resolution soft X-ray spectrometer at the advanced biological and environmental X-ray facility

NASA Astrophysics Data System (ADS)

Friedrich, S.; Drury, O. B.; George, S. J.; Cramer, S. P.

2007-11-01

We have built a 36-pixel superconducting tunnel junction X-ray spectrometer for chemical analysis of dilute samples in the soft X-ray band. It offers an energy resolution of ˜10-20 eV FWHM below 1 keV, a solid angle coverage of ˜10 -3, and can be operated at total rates of up to ˜10 6 counts/s. Here, we describe the spectrometer performance in speciation measurements by fluorescence-detected X-ray absorption spectroscopy at the Advanced Biological and Environmental X-ray facility at the ALS synchrotron.

The transient gamma-ray spectrometer

NASA Technical Reports Server (NTRS)

Owens, A.; Baker, R.; Cline, T. L.; Gehrels, N.; Jermakian, J.; Nolan, T.; Ramaty, R.; Smith, G.; Stilwell, D. E.; Teegarden, B. J.

1991-01-01

The authors describe the Transient Gamma-Ray Spectrometer (TGRS) to be flown onboard the WIND spacecraft. This instrument is designed to detect cosmic gamma-ray bursts over the energy range of 20 keV to 10 MeV with an expected spectroscopic resolution of 2 keV at 1 MeV (E/Delta-E = 500). The active detection element is a 215-cu cm high-purity n-type Ge crystal cooled to cryogenic temperatures by a passive radiative cooler. The geometric field of view (FOV) defined by the cooler is 170 deg FWFM. Burst data are stored directly in an onboard 2.75-Mb burst memory with an absolute timing accuracy of +/-1.5 ms. This capacity is sufficient to store the entire spectral data set of all but the largest bursts. In addition to burst measurements, the instrument will also study solar flares, search for possible diffuse background lines, and monitor the 511-keV positron annihilation radiation from the galactic center. The experiment is scheduled to be launched on a Delta II launch vehicle from Cape Canaveral on December 31, 1992.

STS-46 plasma composition measurements using the EOIM-3 mass spectrometer

NASA Technical Reports Server (NTRS)

Hunton, Donald E.; Trzcinski, Edmund; Gosselin, Roger; Koontz, Steven; Leger, Lubert; Visentine, James T.

1995-01-01

One of the active instruments incorporated into the Evaluation of Oxygen Interactions with Materials - 3 experiment was a quadrupole mass spectrometer. The primary objectives for this instrument, which was built by the Air Force Phillips Laboratory and was a veteran of the STS-4 flight in 1982, were to quantify the flux of atomic oxygen striking the test surfaces in the EOIM-3 payload and to detect surface reaction products from the materials in the carousel. Other speakers in this session have covered the results of these experiments. Prior to the 40-hour-long dedicated EOIM-3 mission segment at the end of the STS-46 flight, the authors used the mass spectrometer to make measurements of ion and neutral gas composition in the shuttle environment. About 25 hours of data were collected during a variety of mission events, including Eureca deployment at high altitude and many tethered satellite system operations.

Solar Radio Observation using Callisto Spectrometer at Sumedang West Java Indonesia: Current Status and Future Development Plan in Indonesia

NASA Astrophysics Data System (ADS)

Manik, T.; Sitompul, P.; Batubara, M.; Harjana, T.; Yatini, C. Y.; Monstein, C.

2016-04-01

Sumedang Observatory (6.91°S, 107,84°E) was established in 1975 and is one of the solar observation facilities of the Space Science Center of Indonesian National Institute of Aeronautics and Space (LAPAN), located around 40 km, east part of Bandung City, West Java, Indonesia. Several instrumentations for solar and space observation such as optical telescopes, radio solar spectrograph, flux gate magnetometer, etc. are operated there, together with an ionosphere sounding system (ionosonde) that was set up later. In July 2014, a standard Callisto (Compound Astronomical Low-cost Low-frequency Instrument for Spectroscopy and Transportable Observatory) spectrometer was installed at Sumedang Observatory for solar radio activity monitoring. Callisto has been developed in the framework of IHY2007 and ISWI, supported by UN and NASA. Callisto spectrometer has observation capability in the frequency range of 45-870 MHz. The Callisto spectrometer receives signal by using a set of 21 elements log-periodic antenna, model CLP5130-1N, pointed to the Sun and equipped with a low noise pre-amplifier. With respect to the Radio Frequency Interferences (RFI) measurements, the Callisto spectrometer is operated individually in frequency ranges of 45-80 MHz and 180-450 MHz. Observation status and data flow are monitored in on-line from center office located in Bandung. The data was transferred to central database at FHNW (Fachhochschule Nordwestschweiz) server every 15 minutes to appear on e-Callisto network subsequently. A real time data transfer and data processing based on Python software also has been developed successfully to be used as an input for Space Weather Information and Forecasting Services (SWIFtS) provided by LAPAN. On 5th November 2014, Callisto spectrometer at Sumedang observed the first clear solar radio event, a solar radio burst type II corresponding to a coronal mass ejection (CME), indicated by a strong X-ray event of M7.9 that was informed on by Space Weather

A Dynamic Nuclear Polarization spectrometer at 95 GHz/144 MHz with EPR and NMR excitation and detection capabilities.

PubMed

Feintuch, Akiva; Shimon, Daphna; Hovav, Yonatan; Banerjee, Debamalya; Kaminker, Ilia; Lipkin, Yaacov; Zibzener, Koby; Epel, Boris; Vega, Shimon; Goldfarb, Daniella

2011-04-01

A spectrometer specifically designed for systematic studies of the spin dynamics underlying Dynamic Nuclear Polarization (DNP) in solids at low temperatures is described. The spectrometer functions as a fully operational NMR spectrometer (144 MHz) and pulse EPR spectrometer (95 GHz) with a microwave (MW) power of up to 300 mW at the sample position, generating a MW B(1) field as high as 800 KHz. The combined NMR/EPR probe comprises of an open-structure horn-reflector configuration that functions as a low Q EPR cavity and an RF coil that can accommodate a 30-50 μl sample tube. The performance of the spectrometer is demonstrated through some basic pulsed EPR experiments, such as echo-detected EPR, saturation recovery and nutation measurements, that enable quantification of the actual intensity of MW irradiation at the position of the sample. In addition, DNP enhanced NMR signals of samples containing TEMPO and trityl are followed as a function of the MW frequency. Buildup curves of the nuclear polarization are recorded as a function of the microwave irradiation time period at different temperatures and for different MW powers. Copyright © 2011 Elsevier Inc. All rights reserved.

Fast Infrared Exoplanet Spectroscopy Survey Explorer (FINESSE) prism spectrometer

NASA Astrophysics Data System (ADS)

McGuire, James P.

2017-11-01

The FINESSE spectrometer design (0.45 to 5 μm at a resolution of greater than 80 at f/12) is placed in context by reviewing history of unit magnification relays and spectrometers. Related imaging spectrometers are also described.

28 CFR 23.2 - Background.

Code of Federal Regulations, 2011 CFR

2011-07-01

... 28 Judicial Administration 1 2011-07-01 2011-07-01 false Background. 23.2 Section 23.2 Judicial Administration DEPARTMENT OF JUSTICE CRIMINAL INTELLIGENCE SYSTEMS OPERATING POLICIES § 23.2 Background. It is... of intelligence data necessary to support control of serious criminal activity may represent...

28 CFR 23.2 - Background.

Code of Federal Regulations, 2014 CFR

2014-07-01

... 28 Judicial Administration 1 2014-07-01 2014-07-01 false Background. 23.2 Section 23.2 Judicial Administration DEPARTMENT OF JUSTICE CRIMINAL INTELLIGENCE SYSTEMS OPERATING POLICIES § 23.2 Background. It is... of intelligence data necessary to support control of serious criminal activity may represent...

28 CFR 23.2 - Background.

Code of Federal Regulations, 2013 CFR

2013-07-01

... 28 Judicial Administration 1 2013-07-01 2013-07-01 false Background. 23.2 Section 23.2 Judicial Administration DEPARTMENT OF JUSTICE CRIMINAL INTELLIGENCE SYSTEMS OPERATING POLICIES § 23.2 Background. It is... of intelligence data necessary to support control of serious criminal activity may represent...

28 CFR 23.2 - Background.

Code of Federal Regulations, 2010 CFR

2010-07-01

... 28 Judicial Administration 1 2010-07-01 2010-07-01 false Background. 23.2 Section 23.2 Judicial Administration DEPARTMENT OF JUSTICE CRIMINAL INTELLIGENCE SYSTEMS OPERATING POLICIES § 23.2 Background. It is... of intelligence data necessary to support control of serious criminal activity may represent...

28 CFR 23.2 - Background.

Code of Federal Regulations, 2012 CFR

2012-07-01

... 28 Judicial Administration 1 2012-07-01 2012-07-01 false Background. 23.2 Section 23.2 Judicial Administration DEPARTMENT OF JUSTICE CRIMINAL INTELLIGENCE SYSTEMS OPERATING POLICIES § 23.2 Background. It is... of intelligence data necessary to support control of serious criminal activity may represent...

Tunable far infrared laser spectrometers

DOE Office of Scientific and Technical Information (OSTI.GOV)

Blake, G.A.; Laughlin, K.B.; Cohen, R.C.

The state of the art in far infrared (FIR) spectroscopy is reviewed. The development of tunable, coherent FIR radiation sources is discussed. Applications of tunable FIR laser spectrometers for measurement of rotational spectra and dipole moments of molecular ions and free radicals, vibration-rotation-tunneling (VRT) spectra of weakly bound complexes, and vibration-rotation spectra of linear carbon clusters are presented. A detailed description of the Berkeley tunable FIR laser spectrometers is presented in the following article.

Compact hydrogen/helium isotope mass spectrometer

DOEpatents

Funsten, Herbert O.; McComas, David J.; Scime, Earl E.

1996-01-01

The compact hydrogen and helium isotope mass spectrometer of the present invention combines low mass-resolution ion mass spectrometry and beam-foil interaction technology to unambiguously detect and quantify deuterium (D), tritium (T), hydrogen molecule (H.sub.2, HD, D.sub.2, HT, DT, and T.sub.2), .sup.3 He, and .sup.4 He concentrations and concentration variations. The spectrometer provides real-time, high sensitivity, and high accuracy measurements. Currently, no fieldable D or molecular speciation detectors exist. Furthermore, the present spectrometer has a significant advantage over traditional T detectors: no confusion of the measurements by other beta-emitters, and complete separation of atomic and molecular species of equivalent atomic mass (e.g., HD and .sup.3 He).

Improved detection limits for electrospray ionization on a magnetic sector mass spectrometer by using an array detector.

PubMed

Cody, R B; Tamura, J; Finch, J W; Musselman, B D

1994-03-01

Array detection was compared with point detection for solutions of hen egg-white lysozyme, equine myoglobin, and ubiquitin analyzed by electrospray ionization with a magnetic sector mass spectrometer. The detection limits for samples analyzed by using the array detector system were at least 10 times lower than could be achieved by using a point detector on the same mass spectrometer. The minimum detectable quantity of protein corresponded to a signal-to-background ratio of approximately 2∶1 for a 500 amol/μL solution of hen egg-white lysozyme. However, the ultimate practical sample concentrations appeared to be in the 10-100 fmol/μL range for the analysis of dilute solutions of relatively pure proteins or simple mixtures.

Bi-dimensional empirical mode decomposition based fringe-like pattern suppression in polarization interference imaging spectrometer

NASA Astrophysics Data System (ADS)

Ren, Wenyi; Cao, Qizhi; Wu, Dan; Jiang, Jiangang; Yang, Guoan; Xie, Yingge; Wang, Guodong; Zhang, Sheqi

2018-01-01

Many observers using interference imaging spectrometer were plagued by the fringe-like pattern(FP) that occurs for optical wavelengths in red and near-infrared region. It brings us more difficulties in the data processing such as the spectrum calibration, information retrieval, and so on. An adaptive method based on the bi-dimensional empirical mode decomposition was developed to suppress the nonlinear FP in polarization interference imaging spectrometer. The FP and corrected interferogram were separated effectively. Meanwhile, the stripes introduced by CCD mosaic was suppressed. The nonlinear interferogram background removal and the spectrum distortion correction were implemented as well. It provides us an alternative method to adaptively suppress the nonlinear FP without prior experimental data and knowledge. This approach potentially is a powerful tool in the fields of Fourier transform spectroscopy, holographic imaging, optical measurement based on moire fringe, etc.

Crossed, Small-Deflection Energy Analyzer for Wind/Temperature Spectrometer

NASA Technical Reports Server (NTRS)

Herrero, Federico A.; Finne, Theodore T.

2010-01-01

Determination of neutral winds and ion drifts in low-Earth-orbit missions requires measurements of the angular and energy distributions of the flux of neutrals and ions entering the satellite from the ram direction. The magnitude and direction of the neutral-wind (or ion-drift) determine the location of the maximum in the angular distribution of the flux. Knowledge of the angle of maximum flux with respect to satellite coordinates (pointing) is essential to determine the wind (or ion-drift) vector. The crossed Small-Deflection Energy Analyzer (SDEA) spectrometer (see Figure 1) occupies minimal volume and consumes minimal power. Designed for upper atmosphere/ionosphere investigations at Earth altitudes above 100 km, the spectrometer operates by detecting the angular and energy distributions of neutral atoms/molecules and ions in two mutually perpendicular planes. In this configuration, the two detection planes actually cross at the spectrometer center. It is possible to merge two SDEAs so they share a common optical axis and alternate measurements between two perpendicular planes, and reduce the number of ion sources from two to one. This minimizes the volume and footprint significantly and reduces the ion source power by a factor of two. The area of the entrance aperture affects the number of ions detected/second and also determines the energy resolution. Thermionic emitters require heater power of about 100 mW to produce 1 mA of electron beam current. Typically, electron energy is about 100 eV and requires a 100-V supply for electron acceleration to supply an additional 100 mW of power. Thus, ion source power is at most 200 mW. If two ion sources were to be used, the ion source power would be, at most, 400 mW. Detector power, deflection voltage power, and microcontroller and other functions require less than 150 mW. A WTS (wind/ temperature spectrometer) with two separate optical axes would consume about 650 mW, while the crossed SDEA described here consumes about

The moderate resolution imaging spectrometer (MODIS) science and data system requirements

NASA Technical Reports Server (NTRS)

Ardanuy, Philip E.; Han, Daesoo; Salomonson, Vincent V.

1991-01-01

The Moderate Resolution Imaging Spectrometer (MODIS) has been designated as a facility instrument on the first NASA polar orbiting platform as part of the Earth Observing System (EOS) and is scheduled for launch in the late 1990s. The near-global daily coverage of MODIS, combined with its continuous operation, broad spectral coverage, and relatively high spatial resolution, makes it central to the objectives of EOS. The development, implementation, production, and validation of the core MODIS data products define a set of functional, performance, and operational requirements on the data system that operate between the sensor measurements and the data products supplied to the user community. The science requirements guiding the processing of MODIS data are reviewed, and the aspects of an operations concept for the production of data products from MODIS for use by the scientific community are discussed.

Near infrared measurements of SPICAM AOTF spectrometer on Mars Express

NASA Astrophysics Data System (ADS)

Korablev, O.; Bertaux, J. L.; Fedorova, A.; Perrier, S.; Moroz, V. I.; Rodin, A.; Stepanov, A.; Grigoriev, A.; Dimarellis, E.; Kalinnikov, Yu. K.

The Near-Infrared channel of SPICAM, a lightweight (800 g) acousto-optical tuneable filter (AOTF) spectrometer observes the atmosphere and the surface of Mars from Mars Express orbiter. The spectrometer covers the spectral range between 1000 and 1700 nm with the resolving power λ /Δ λ superior to 1300. Signal-to noise ratio in individual Mars spectra varies from 30 to 100 and more depending on observation conditions. The total column abundance of water vapour is measured in nadir at 1380 nm simultaneously with ozone measured in the UV channel of SPICAM. Moreover, the O21Δ g emission at 1270 nm produced by photodissociation of ozone above 15-20km is systematically observed in nadir at the background of bright disk constraining (with the UV measurements of total ozone) its vertical distribution. Airmass reference is provided self-consistently from carbon dioxide measurements at 1430 and 1580 nm. At LS≈ 280 clear spectral signatures of CO2 and H2O ices has been detected at the permanent South Polar Cap (simultaneously with OMEGA and PFS findings) and above 55N. Limb measurements show that at the time when TES/MGS measurements indicate very clear atmosphere, the dust at the limb is observed up to 50-60km. We will present description of the spectrometer and its characterization, and describe the collected data, including nadir, limb and solar occultation measurements. Spectro-polarimetry capabilities of the AOTF will be discussed. This is the first experience of AOTF use in deep space, and we believe that a 800-g instrument capable to measure water vapour and much more on Mars should become a routine climate/environment tool on future missions.

Broad-Bandwidth FPGA-Based Digital Polyphase Spectrometer

NASA Technical Reports Server (NTRS)

Jamot, Robert F.; Monroe, Ryan M.

2012-01-01

With present concern for ecological sustainability ever increasing, it is desirable to model the composition of Earth s upper atmosphere accurately with regards to certain helpful and harmful chemicals, such as greenhouse gases and ozone. The microwave limb sounder (MLS) is an instrument designed to map the global day-to-day concentrations of key atmospheric constituents continuously. One important component in MLS is the spectrometer, which processes the raw data provided by the receivers into frequency-domain information that cannot only be transmitted more efficiently, but also processed directly once received. The present-generation spectrometer is fully analog. The goal is to include a fully digital spectrometer in the next-generation sensor. In a digital spectrometer, incoming analog data must be converted into a digital format, processed through a Fourier transform, and finally accumulated to reduce the impact of input noise. While the final design will be placed on an application specific integrated circuit (ASIC), the building of these chips is prohibitively expensive. To that end, this design was constructed on a field-programmable gate array (FPGA). A family of state-of-the-art digital Fourier transform spectrometers has been developed, with a combination of high bandwidth and fine resolution. Analog signals consisting of radiation emitted by constituents in planetary atmospheres or galactic sources are downconverted and subsequently digitized by a pair of interleaved analog-to-digital converters (ADCs). This 6-Gsps (gigasample per second) digital representation of the analog signal is then processed through an FPGA-based streaming fast Fourier transform (FFT). Digital spectrometers have many advantages over previously used analog spectrometers, especially in terms of accuracy and resolution, both of which are particularly important for the type of scientific questions to be addressed with next-generation radiometers.

HDice, Highly-Polarized Low-Background Frozen-Spin HD Targets for CLAS experiments at Jefferson Lab

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wei, Xiangdong; Bass, Christopher; D'Angelo, Annalisa

2012-12-01

Large, portable frozen-spin HD (Deuterium-Hydride) targets have been developed for studying nucleon spin properties with low backgrounds. Protons and Deuterons in HD are polarized at low temperatures (~10mK) inside a vertical dilution refrigerator (Oxford Kelvinox-1000) containing a high magnetic field (up to 17T). The targets reach a frozen-spin state within a few months, after which they can be cold transferred to an In-Beam Cryostat (IBC). The IBC, a thin-walled dilution refrigerator operating either horizontally or vertically, is use with quasi-4{pi} detector systems in open geometries with minimal energy loss for exiting reaction products in nucleon structure experiments. The first applicationmore » of this advanced target system has been used for Spin Sum Rule experiments at the LEGS facility in Brookhaven National Laboratory. An improved target production and handling system has been developed at Jefferson Lab for experiments with the CEBAF Large Acceptance Spectrometer, CLAS.« less

The Airborne Visible / Infrared Imaging Spectrometer AVIS: Design, Characterization and Calibration.

PubMed

Oppelt, Natascha; Mauser, Wolfram

2007-09-14

The Airborne Visible / Infrared imaging Spectrometer AVIS is a hyperspectralimager designed for environmental monitoring purposes. The sensor, which wasconstructed entirely from commercially available components, has been successfullydeployed during several experiments between 1999 and 2007. We describe the instrumentdesign and present the results of laboratory characterization and calibration of the system'ssecond generation, AVIS-2, which is currently being operated. The processing of the datais described and examples of remote sensing reflectance data are presented.

Broad band waveguide spectrometer

DOEpatents

Goldman, Don S.

1995-01-01

A spectrometer for analyzing a sample of material utilizing a broad band source of electromagnetic radiation and a detector. The spectrometer employs a waveguide possessing an entry and an exit for the electromagnetic radiation emanating from the source. The waveguide further includes a surface between the entry and exit portions which permits interaction between the electromagnetic radiation passing through the wave guide and a sample material. A tapered portion forms a part of the entry of the wave guide and couples the electromagnetic radiation emanating from the source to the waveguide. The electromagnetic radiation passing from the exit of the waveguide is captured and directed to a detector for analysis.

Radiation calibration for LWIR Hyperspectral Imager Spectrometer

NASA Astrophysics Data System (ADS)

Yang, Zhixiong; Yu, Chunchao; Zheng, Wei-jian; Lei, Zhenggang; Yan, Min; Yuan, Xiaochun; Zhang, Peizhong

2014-11-01

The radiometric calibration of LWIR Hyperspectral imager Spectrometer is presented. The lab has been developed to LWIR Interferometric Hyperspectral imager Spectrometer Prototype(CHIPED-I) to study Lab Radiation Calibration, Two-point linear calibration is carried out for the spectrometer by using blackbody respectively. Firstly, calibration measured relative intensity is converted to the absolute radiation lightness of the object. Then, radiation lightness of the object is is converted the brightness temperature spectrum by the method of brightness temperature. The result indicated †that this method of Radiation Calibration calibration was very good.

A mini-photofragment translational spectrometer with ion velocity map imaging using low voltage acceleration

NASA Astrophysics Data System (ADS)

Qi, Wenke; Jiang, Pan; Lin, Dan; Chi, Xiaoping; Cheng, Min; Du, Yikui; Zhu, Qihe

2018-01-01

A mini time-sliced ion velocity map imaging photofragment translational spectrometer using low voltage acceleration has been constructed. The innovation of this apparatus adopts a relative low voltage (30-150 V) to substitute the traditional high voltage (650-4000 V) to accelerate and focus the fragment ions. The overall length of the flight path is merely 12 cm. There are many advantages for this instrument, such as compact structure, less interference, and easy to operate and control. Low voltage acceleration gives a longer turn-around time to the photofragment ions forming a thicker Newton sphere, which provides sufficient time for slicing. Ion trajectory simulation has been performed for determining the structure dimensions and the operating voltages. The photodissociation and multiphoton ionization of O2 at 224.999 nm is used to calibrate the ion images and examine the overall performance of the new spectrometer. The velocity resolution (Δν/ν) of this spectrometer from O2 photodissociation is about 0.8%, which is better than most previous results using high acceleration voltage. For the case of CF3I dissociation at 277.38 nm, many CF3 vibrational states have been resolved, and the anisotropy parameter has been measured. The application of low voltage acceleration has shown its advantages on the ion velocity map imaging (VMI) apparatus. The miniaturization of the VMI instruments can be realized on the premise of high resolution.

Superconducting High Resolution Fast-Neutron Spectrometers

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hau, Ionel Dragos

2006-01-01

Superconducting high resolution fast-neutron calorimetric spectrometers based on 6LiF and TiB{sub 2} absorbers have been developed. These novel cryogenic spectrometers measure the temperature rise produced in exothermal (n, α) reactions with fast neutrons in 6Li and 10B-loaded materials with heat capacity C operating at temperatures T close to 0.1 K. Temperature variations on the order of 0.5 mK are measured with a Mo/Cu thin film multilayer operated in the transition region between its superconducting and its normal state. The advantage of calorimetry for high resolution spectroscopy is due to the small phonon excitation energies k BT on the order ofmore » μeV that serve as signal carriers, resulting in an energy resolution ΔE ~ (k BT 2C) 1/2, which can be well below 10 keV. An energy resolution of 5.5 keV has been obtained with a Mo/Cu superconducting sensor and a TiB 2 absorber using thermal neutrons from a 252Cf neutron source. This resolution is sufficient to observe the effect of recoil nuclei broadening in neutron spectra, which has been related to the lifetime of the first excited state in 7Li. Fast-neutron spectra obtained with a 6Li-enriched LiF absorber show an energy resolution of 16 keV FWHM, and a response in agreement with the 6Li(n, α) 3H reaction cross section and Monte Carlo simulations for energies up to several MeV. The energy resolution of order of a few keV makes this novel instrument applicable to fast-neutron transmission spectroscopy based on the unique elemental signature provided by the neutron absorption and scattering resonances. The optimization of the energy resolution based on analytical and numerical models of the detector response is discussed in the context of these applications.« less

UV spectroscopy with the CETUS multi-object spectrometer

NASA Astrophysics Data System (ADS)

Kendrick, Stephen E.; Woodruff, Robert; Hull, Anthony; Heap, Sara; Kutyrev, Alexander; Purves, Lloyd; Danchi, William

2018-01-01

The ultraviolet multi-object spectrograph (MOS) for the Cosmic Evolution Through UV Spectroscopy (CETUS) concept is a slit-based instrument allowing multiple simultaneous observations over a wide field of view. The UV MOS will be able to target up to 100 objects at a time without the issues of confusion with nearby sources or unwanted background like zodiacal stray light. The multiplexing will allow over 100,000 galaxies to be observed over a typical mission lifetime which greatly enhances the scientific yield. The MOS utilizes a next-generation micro-shutter array, an efficient aspheric Offner-like spectrometer design with a convex grating, and nanotube light traps for suppressing unwanted wavelengths. The optical coatings are also designed for optimizing the UV throughput while minimizing out-of-band signal at the detector.

Direct bonded HOPG - Analyzer support without background source

NASA Astrophysics Data System (ADS)

Groitl, Felix; Kitaura, Hidetoshi; Nishiki, Naomi; Rønnow, Henrik M.

2018-04-01

A new production process allows a direct bonding of HOPG crystals on Si wafers. This new method facilitates the production of analyzer crystals with support structure without the use of additional, background inducing fixation material, e.g. glue, wax and screws. This new method is especially interesting for the upcoming generation of CAMEA-type multiplexing spectrometers. These instruments allow for a drastic performance increase due to the increased angular coverage and multiple energy analysis. Exploiting the transparency of multiple HOPG for cold neutrons, a consecutive arrangement of HOPG analyzer crystals per Q-channel can be achieved. This implies that neutrons travel through up to 10 arrays of analyzer crystals before reaching the analyzer corresponding to their energy. Hence, a careful choice of the fixation method for the analyzer crystals in regards to transparency and background is necessary. Here, we present first results on the diffraction and mechanical performance of direct bonded analyzer crystals.

Low Noise Titanium Nitride KIDs for SuperSpec: A Millimeter-Wave On-Chip Spectrometer

NASA Astrophysics Data System (ADS)

Hailey-Dunsheath, S.; Shirokoff, E.; Barry, P. S.; Bradford, C. M.; Chapman, S.; Che, G.; Glenn, J.; Hollister, M.; Kovács, A.; LeDuc, H. G.; Mauskopf, P.; McKenney, C.; O'Brient, R.; Padin, S.; Reck, T.; Shiu, C.; Tucker, C. E.; Wheeler, J.; Williamson, R.; Zmuidzinas, J.

2016-07-01

SuperSpec is a novel on-chip spectrometer we are developing for multi-object, moderate resolution (R = 100-500), large bandwidth ({˜ }1.65:1), submillimeter and millimeter survey spectroscopy of high-redshift galaxies. The spectrometer employs a filter bank architecture, and consists of a series of half-wave resonators formed by lithographically-patterned superconducting transmission lines. The signal power admitted by each resonator is detected by a lumped element titanium nitride (TiN) kinetic inductance detector operating at 100-200 MHz. We have tested a new prototype device that achieves the targeted R=100 resolving power, and has better detector sensitivity and optical efficiency than previous devices. We employ a new method for measuring photon noise using both coherent and thermal sources of radiation to cleanly separate the contributions of shot and wave noise. We report an upper limit to the detector NEP of 1.4× 10^{-17} W Hz^{-1/2}, within 10 % of the photon noise-limited NEP for a ground-based R=100 spectrometer.

Acquisition of Raman Spectrometer and High Temperature and Pressure Reactor for Synthesis and Characterization of Carbon Based Hybrid Nanoparticles from Waste Wood

DTIC Science & Technology

2015-04-27

from waste biomass using these two high temperature reactors. We have extensively used a Raman spectrometer to analyse as synthesized carbon materials...corporation). These tools were fully installed and operational. We have also synthesized carbon materials from waste biomass using these two high...materials from waste biomass using these two high temperature reactors. We have extensively used a Raman spectrometer to analyse as synthesized carbon

SU-D-BRCD-06: Measurement of Elekta Electron Energy Spectra Using a Small Magnetic Spectrometer.

PubMed

Hogstrom, K; McLaughlin, D; Gibbons, J; Shikhaliev, P; Clarke, T; Henderson, A; Taylor, D; Shagin, P; Liang, E

2012-06-01

To demonstrate how a small magnetic spectrometer can measure the energy spectra of seven electron beams on an Elekta Infinity tuned to match beams on a previously commissioned machine. Energyspectra were determined from measurements of intensity profiles on 6″-long computed radiographic (CR) strips after deflecting a narrow incident beam using a small (28 lbs.), permanent magnetic spectrometer. CR plateexposures (<1cGy) required special beam reduction techniques and bremsstrahlung shielding. Curves of CR intensity (corrected for non- linearity and background) versus position were transformed into energy spectra using the transformation from position (x) on the CR plate to energy (E) based on the Lorentz force law. The effective magnetic field and its effective edge, parameters in the transformation, were obtained by fitting a plot of most probable incident energy (determined from practical range) to the peak position. The calibration curve (E vs. x) fit gave 0.423 Tesla for the effective magnetic field. Most resulting energy spectra were characterized by a single, asymmetric peak with peak position and FWHM increasing monotonically with beam energy. Only the 9-MeV spectrum was atypical, possibly indicating suboptimal beam tuning. These results compared well with energy spectra independently determined by adjusting each spectrum until the EGSnrc Monte Carlo calculated percent depth-dose curve agreed well with the corresponding measured curve. Results indicate that this spectrometer and methodology could be useful for measuring energy spectra of clinical electron beams at isocenter. Future work will (1) remove the small effect of the detector response function (due to pinhole size and incident angular spread) from the energy spectra, (2) extract the energy spectra exiting the accelerator from current results, (3) use the spectrometer to compare energy spectra of matched beams among our clinical sites, and (4) modify the spectrometer to utilize radiochromic film. �

Microbolometer spectrometer opens hoist of new applications

NASA Astrophysics Data System (ADS)

Leijtens, J.; Smorenburg, C.; Escudero, I.; Boslooper, E.; Visser, H.; Helden, W. v.; Breussin, F.

2017-11-01

Current Thermal infra red ( 7..14μm) multispectral imager instruments use cryogenically cooled Mercury Cadmium Telluride (MCT or HgCdTe) detectors. This causes the instruments to be bulky, power hungry and expensive. For systems that have medium NETD (Noise Equivalent Temperature Difference) requirements and can operate with high speed optics (<1.5), room temperature microbolometer performance has increased enough to enable people to design multispectral instruments based on this new detector technology. Because microbolometer technology has been driven by the military need for inexpensive, reliable and small thermal imagers, microbolometer based detectors are almost exclusively available in 2D format, and performance is still increasing. Building a spectrometer for the 7 to 12 μm wavelength region using microbolometers has been discarded until now, based on the expected NETD performance. By optimising the throughput of the optical system, and using the latest improvements in detector performance, TNO TPD has been able to design a spectrometer that is able to provide co-registered measurements in the 7 to 12 μm wavelength region yielding acceptable NETD performance. Apart from the usual multispectral imaging, the concept can be used for several other applications, among which imaging in both the 3 to 5 and 7 to 12 μm atmospheric windows at the same time (forest fire detection and military recognisance) or wideband flame analysis (Nox detection in industrial ovens).

Frequency-scanning MALDI linear ion trap mass spectrometer for large biomolecular ion detection.

PubMed

Lu, I-Chung; Lin, Jung Lee; Lai, Szu-Hsueh; Chen, Chung-Hsuan

2011-11-01

This study presents the first report on the development of a matrix-assisted laser desorption ionization (MALDI) linear ion trap mass spectrometer for large biomolecular ion detection by frequency scan. We designed, installed, and tested this radio frequency (RF) scan linear ion trap mass spectrometer and its associated electronics to dramatically extend the mass region to be detected. The RF circuit can be adjusted from 300 to 10 kHz with a set of operation amplifiers. To trap the ions produced by MALDI, a high pressure of helium buffer gas was employed to quench extra kinetic energy of the heavy ions produced by MALDI. The successful detection of the singly charged secretory immunoglobulin A ions indicates that the detectable mass-to-charge ratio (m/z) of this system can reach ~385 000 or beyond.

Development of high resolution x-ray spectrometers for the investigation of bioinorganic chemistry in metalloproteins

NASA Astrophysics Data System (ADS)

Drury, Owen Byron

We have built an X-ray spectrometer for synchrotron-based high-resolution soft X-ray spectroscopy. The spectrometer uses four 9-pixel arrays of superconducting tunnel junctions (STJs) as sensors. They infer the energy of an absorbed X-ray from a temporary increase in tunneling current. The STJs are operated in a two-stage adiabatic demagnetization refrigerator (ADR) that uses liquid nitrogen and helium for precooling to 77 K and 4.2 K, and gallium gadolinium garnet and iron ammonium sulfate to attain a base temperature below 0.1 K. The sensors are held at the end of a 40-cm-long cold finger within ˜1 cm of a sample located inside the vacuum chamber of a synchrotron beam line end station. The spectrometer has an energy resolution between 10 eV and 20 eV FWHM below 1 keV, can be operated at rates up to ˜106 counts/s. STJ spectrometers are suited for chemical analysis of dilute samples by fluorescence-detected X-ray absorption spectroscopy (XAS) in cases where conventional germanium detectors do not have enough energy resolution. We have used this STJ spectrometer at the Advanced Light Source synchrotron for spectroscopy on the lower energy X-ray absorption edges of the elements Mo, S, Fe and N. These elements play an important role in biological nitrogen fixation at the metalloprotein nitrogenase, and we have examined if STJ spectrometers can be used to provide new insights into some of the open questions regarding the reaction mechanism of this protein. We have taken X-ray absorption near-edge spectra (XANES) and extended fine structure spectra (EXAFS) of an Fe 6N(CO)15-compound containing a single N atom inside a cluster of six Fe atoms, as postulated to exist inside the Fe-S cluster of the FeMo-cofactor (FeMo-co) in nitrogenase. The STJ detector has enabled the first-ever extended range EXAFS scans on nitrogen through the oxygen K-edge, enabling a comparison with N EXAFS on FeMo-co. We have taken iron L23-edge spectra of the Fe-S cluster in FeMo-co, which can be

Differentially pumped dual linear quadrupole ion trap mass spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Owen, Benjamin C.; Kenttamaa, Hilkka I.

The present disclosure provides a new tandem mass spectrometer and methods of using the same for analyzing charged particles. The differentially pumped dual linear quadrupole ion trap mass spectrometer of the present disclose includes a combination of two linear quadrupole (LQIT) mass spectrometers with differentially pumped vacuum chambers.

Pandora Operation and Analysis Software