Sample records for cold rolling process
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NASA Technical Reports Server (NTRS)
Lahoti, G. D.; Akgerman, N.; Altan, T.
1978-01-01
Mild steel (AISI 1018) was selected as model cold-rolling material and Ti-6Al-4V and INCONEL 718 were selected as typical hot-rolling and cold-rolling alloys, respectively. The flow stress and workability of these alloys were characterized and friction factor at the roll/workpiece interface was determined at their respective working conditions by conducting ring tests. Computer-aided mathematical models for predicting metal flow and stresses, and for simulating the shape-rolling process were developed. These models utilize the upper-bound and the slab methods of analysis, and are capable of predicting the lateral spread, roll-separating force, roll torque and local stresses, strains and strain rates. This computer-aided design (CAD) system is also capable of simulating the actual rolling process and thereby designing roll-pass schedule in rolling of an airfoil or similar shape. The predictions from the CAD system were verified with respect to cold rolling of mild steel plates. The system is being applied to cold and hot isothermal rolling of an airfoil shape, and will be verified with respect to laboratory experiments under controlled conditions.
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NASA Astrophysics Data System (ADS)
Lu, Bohan; Lu, Xiaohui
2018-02-01
This study investigates the correlation between the residual stress and distortion behavior of a cold-rolled ring from the annealing to quenching-tempering (QT) process. Due to the cold-rolled process, the external periphery of the bearing ring experiences a compressive residual stress. To relieve the residual stress, cold-rolled rings are annealed at 700 °C which is higher than the starting temperature of recrystallization. When cold-rolled rings are annealed at 700 °C for 15 min, the compressive residual stress is reduced to zero and the outer diameter of the annealed ring becomes larger than that of a non-annealed sample, which is unrelated to annealing time. Simultaneously, the roundness and taper deviation do not obviously change compared with those of non-annealed sample. The stress relaxation during the annealing process was attributed to the recovery and recrystallization of ferrite. Annealing has a genetic influence on the following QT heat treatment, wherein the lowest residual stress is in the non-annealed cold-rolled ring. From the annealing to QT process, the deviation of the outer diameter, roundness, and taper increased with annealing time, a large extend than that of non-annealed samples.
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Influence of 10 % Cold Rolling Reduction on Ageing Behaviour of Hot Rolled Al-Cu-Si-Mn-Mg Alloy
NASA Astrophysics Data System (ADS)
Ghosh, S. K.
2014-10-01
In the current study, the effect of 10 % cold rolling on the different ageing phenomena of Al-Cu-Si-Mn-Mg alloy was investigated. Both hot rolled and cold rolled alloys were subjected to both natural and artificial ageing processes. Hardness was measured to understand the change in the mechanical property of the alloy before and after rolling and also during ageing processes. From microscopy, it was evident that the cold rolling and subsequent ageing provided the alloy with a structure in which CuAl2 precipitates were uniformly distributed. The alloy exhibited the peak hardness value of 92 VHN after 2 days of natural ageing, whereas the cold deformed (10 %) alloy exhibited the higher peak hardness value of 139 VHN after 3 days of natural ageing. Peak hardness of the alloy reached 94 VHN, when hot rolled alloy was subjected to ageing at 250 °C for 1 h, whereas 10 % cold rolling followed by ageing (100 °C, 15 min) demonstrated accelerated and elevated hardening. The ageing behaviours thus obtained permit the alloy to provide a range of desirable combinations of strength and ductility for high strength weight saving applications.
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NASA Astrophysics Data System (ADS)
Wang, X. F.; Guo, M. X.; Chen, Y.; Zhu, J.; Zhang, J. S.; Zhuang, L. Z.
2017-07-01
The effect of thermomechanical processing on microstructure, texture evolution, and mechanical properties of Al-Mg-Si-Cu alloys with different Zn contents was studied by mechanical properties, microstructure, and texture characterization in the present study. The results show that thermomechanical processing has a significant influence on the evolution of microstructure and texture and on the final mechanical properties, independently of Zn contents. Compared with the T4P-treated (first preaged at 353 K (80 °C) for 12 hours and then naturally aged for 14 days) sheets with high final cold rolling reduction, the T4P-treated sheets with low final cold rolling reduction possess almost identical strength and elongation and higher average r values. Compared with the intermediate annealed sheets with high final cold rolling reduction, the intermediate annealed sheets with low final cold rolling reduction contain a higher number of particles with a smaller size. After solution treatment, in contrast to the sheets with high final cold rolling reduction, the sheets with low final cold rolling reduction possess finer grain structure and tend to form a weaker recrystallization texture. The recrystallization texture may be affected by particle distribution, grain size, and final cold rolling texture. Finally, the visco-plastic self-consistent (VPSC) model was used to predict r values.
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NASA Astrophysics Data System (ADS)
Yonezawa, Toshio; Watanabe, Masashi; Hashimoto, Atsushi
2015-06-01
Primary water stress corrosion cracking growth rates (PWSCCGRs) in highly cold-worked thermally treated (TT) Alloy 690 have been recently reported as exhibiting significant heat-to-heat variability. Authors hypothesized that these significant differences could be due to the metallurgical characteristics of each heat. In order to confirm this hypothesis, the effect of fundamental metallurgical characteristics on PWSCCGR measurements in cold-worked TT Alloy 690 has been investigated. The following new observations were made in this study: (1) Microcracks and voids were observed in or near eutectic crystals of grain boundary (GB) M23C6 carbides (primary carbides) after cold rolling, but were not observed before cold rolling. These primary carbides with microcracks and voids were observed in both lightly forged and as-cast and cold-rolled TT Alloy 690 (heat A) as well as in a cold-rolled TT Alloy 690 (heat Y) that simulated the chemical composition and carbide banded structure of the material previously tested by Paraventi and Moshier. However, this was not observed in precipitated (secondary) M23C6 GB carbides in heavily forged and cold-rolled TT Alloy 690 heat A and a cold-rolled commercial TT Alloy 690. (2) From microstructural analyses carried out on the various TT Alloy 690 test materials before and after cold rolling, the amount of eutectic crystals (primary carbides and nitrides) M23C6 and TiN depended on the chemical composition. In particular, the amount of M23C6 depended on the fabrication process. Microcracks and voids in or near the M23C6 and TiN precipitates were generated by the cold rolling process. (3) The PWSCCGRs observed in TT Alloy 690 were different for each heat and fabrication process. The PWSCCGR decreased with increasing Vickers hardness of each heat. However, for the same heats and fabrication processes, the PWSCCGR increased with increasing Vickers hardness due to cold work. Thus, the PWSCCGR must be affected not only by hardness (or equivalently the cold working ratio) but also by grain size, microcracks, and voids of primary M23C6 carbides, etc., which in turn depend on chemical composition and the fabrication process.
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NASA Technical Reports Server (NTRS)
Lahoti, G. D.; Akgerman, N.; Altan, T.
1978-01-01
Mild steel (AISI 1018) was selected as model cold rolling material and Ti-6A1-4V and Inconel 718 were selected as typical hot rolling and cold rolling alloys, respectively. The flow stress and workability of these alloys were characterized and friction factor at the roll/workpiece interface was determined at their respective working conditions by conducting ring tests. Computer-aided mathematical models for predicting metal flow and stresses, and for simulating the shape rolling process were developed. These models utilized the upper bound and the slab methods of analysis, and were capable of predicting the lateral spread, roll separating force, roll torque, and local stresses, strains and strain rates. This computer-aided design system was also capable of simulating the actual rolling process, and thereby designing the roll pass schedule in rolling of an airfoil or a similar shape.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Li, Rongguang, E-mail: lirongguang1980@126.com; Xin, Renlong; Chapuis, Adrien
Microstructure and mechanical properties of the Mg–4Sm (wt.%) alloy, prepared via combined processes of extrusion, cold rolling and aging, have been investigated. The hot extruded alloy exhibits a weak rare earth magnesium alloy texture with < 11 − 21 >//ED, while the cold-rolled alloy shows a stronger basal texture with < 0001 >//ND. Many tensile twins and double twins are observed in grains after rolling. The cold-rolled alloy shows a weak age-hardening response compared with the extruded alloy, which is the result of more precipitation in the twin boundary during aging. The rolled alloy exhibits almost no precipitate free zonemore » during aging compared with the extruded alloy. The higher proof stress of the rolled alloy in peak-aged condition is attributed to the presence of twin boundaries, stronger basal texture, higher dislocation density, and the suppression of precipitate free zone compared with the extruded alloy. - Highlights: • No precipitate free zone appears in cold-rolled alloy after aging. • Segregation and precipitates are observed in twin boundaries and grain boundaries. • Cold-rolled alloy shows a weak age-hardening response.« less
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Joshi, Vineet V.; Paxton, Dean M.; Lavender, Curt A.
Over the past several years Pacific Northwest National Laboratory (PNNL) has been actively involved in supporting the U.S. Department of Energy National Nuclear Security Administration Office of Material Management and Minimization (formerly Global Threat Reduction Initiative). The U.S. High- Power Research Reactor (USHPRR) project is developing alternatives to existing highly enriched uranium alloy fuel to reduce the proliferation threat. One option for a high-density metal fuel is uranium alloyed with 10 wt% molybdenum (U-10Mo). Forming the U-10Mo fuel plates/foils via rolling is an effective technique and is actively being pursued as part of the baseline manufacturing process. The processing ofmore » these fuel plates requires systematic investigation/understanding of the pre- and post-rolling microstructure, end-state mechanical properties, residual stresses, and defects, their effect on the mill during processing, and eventually, their in-reactor performance. In the work documented herein, studies were conducted to determine the effect of cold and hot rolling the as-cast and homogenized U-10Mo on its microstructure and hardness. The samples were homogenized at 900°C for 48 h, then later annealed for several durations and temperatures to investigate the effect on the material’s microstructure and hardness. The rolling of the as-cast plate, both hot and cold, was observed to form a molybdenum-rich and -lean banded structure. The cold rolling was ineffective, and in some cases exacerbated the as-cast defects. The grains elongated along the rolling direction and formed a pancake shape, while the carbides fractured perpendicularly to the rolling direction and left porosity between fractured particles of UC. The subsequent annealing of these samples at sub-eutectoid temperatures led to rapid precipitation of the ' lamellar phase, mainly in the molybdenum-lean regions. Annealing the samples above the eutectoid temperature did not refine the grain size or the banded microstructure. However, annealing the samples led to quick recovery in hardness as evidenced by a drop in Vickers hardness of 20%. Hot rolling was performed at 650 and 800°C. The hot-rolling mill loads (load separation force) were approximately 40 to 50% less than the cold-rolling for the same reduction and thickness. It was observed that hot rolling the samples with 50% or more reduction in thickness were responsible for dynamic recrystallization in the hot-rolled samples and led to grain refinement. Unlike the cold-rolled samples, the hot-rolled samples did not fracture the carbides and appeared to heal the casting defects. The recovery phenomenon was similar to the cold-rolled samples above the eutectoid temperatures, but owing to the refined grain size, the precipitation of the lamellar phase was far more rapid in these samples and the hardness increased more rapidly than in the cold rolled sample when heated below the eutectoid temperature. The data generated from these rolling efforts has been used to make the process modeling efforts more robust and applicable to all USHPRR partner rolling mills. The flow stress for cold rolling the samples was determined to be between 170-190 ksi, with frictional forces between 0.2 and 0.4 for the PNNL mill. The measured roll separation forces and those simulated using finite element methods for hot and cold rolling for the PNNL rolling mill were in good agreement.« less
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NASA Astrophysics Data System (ADS)
Mandal, Arka; Patra, Sudipta; Chakrabarti, Debalay; Singh, Shiv Brat
2017-12-01
A lean duplex stainless steel (LDSS) has been prepared with low-N content and processed by different thermo-mechanical schedules, similar to the industrial processing that comprised hot-rolling, cold-rolling, and annealing treatments. The microstructure developed in the present study on low-N LDSS has been compared to that of high-N LDSS as reported in the literature. As N is an austenite stabilizer, lower-N content reduced the stability of austenite and the austenite content in low-N LDSS with respect to the conventional LDSS. Due to low stability of austenite in low-N LDSS, cold rolling resulted in strain-induced martensitic transformation and the reversion of martensite to austenite during subsequent annealing contributed to significant grain refinement within the austenite regions. δ-ferrite grains in low-N LDSS, on the other hand, are refined by extended recovery mechanism. Initial solidification texture (mainly cube texture) within the δ-ferrite region finally converted into gamma-fiber texture after cold rolling and annealing. Although MS-brass component dominated the austenite texture in low-N LDSS after hot rolling and cold rolling, that even transformed into alpha-fiber texture after the final annealing. Due to the significant grain refinement and formation of beneficial texture within both austenite and ferrite, good combination of strength and ductility has been achieved in cold-rolled and annealed sample of low-N LDSS steel.
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Microstructure and texture evolution in cold-rolled and annealed alloy MA-956
NASA Astrophysics Data System (ADS)
Hosoda, Takashi
The microstructural and texture development with thermomechanical processing, performed through a combination of cold-rolling and annealing, in MA-956 plate consisting of a layered and inhomogeneous microstructure was systematically assessed. The alloy contained in mass percent, 20 Cr, 4.8 Al, 0.4 Ti, 0.4 Y2O3, and the balance iron. The starting material was as-hot-rolled plate, 9.7 mm thick. The as-hot-rolled plate was subjected to 40%, 60%, and 80% cold-rolling reduction and subsequently annealed at 1000, 1200, or 1380. Assessment of microstructural and texture developments before and after cold-rolling and annealing was performed using light optical microscopy (LOM), Vickers hardness testing, and electron backscatter diffraction (EBSD). Locally introduced misorientations by cold-rolling in each region were evaluated by Kernel Average Misorientation (KAM) maps. The as-hot-rolled condition contained a layered and inhomogeneous microstructure consisting of thin and coarse elongated grains, and aggregated regions which consisted of fine grains and sub-grains with {100} texture parallel to the longitudinal direction. The microstructure of the 40% cold-rolled condition contained deformation bands, and the 60% and 80% cold-rolled conditions also contained highly deformed regions where the deformation bands were intricately tangled. A predominant orientation of (001) parallel to the rolling direction was developed during cold-rolling, becoming more prominent with increasing reduction. The magnitudes of KAM angles varied through the thickness depending on the initial microstructures. Recrystallization occurred in regions where high KAM angles were dense after annealing and nucleation sites were the aggregation regions, deformation bands, and highly deformed regions. The shape and size of the recrystallized grains varied depending on the nucleation sites.
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NASA Astrophysics Data System (ADS)
Ravi Kumar, B.; Mahato, B.; Sharma, Sailaja; Sahu, J. K.
2009-12-01
As-received hot-rolled commercial grade AISI 304L austenitic stainless steel plates were solution treated at 1060 °C to achieve chemical homogeneity. Microstructural characterization of the solution-treated material revealed polygonal grains of about 85- μm size along with annealing twins. The solution-treated plates were heavily cold rolled to about 90 pct of reduction in thickness. Cold-rolled specimens were then subjected to thermal cycles at various temperatures between 750 °C and 925 °C. X-ray diffraction showed about 24.2 pct of strain-induced martensite formation due to cold rolling of austenitic stainless steel. Strain-induced martensite formed during cold rolling reverted to austenite by the cyclic thermal process. The microstructural study by transmission electron microscope of the material after the cyclic thermal process showed formation of nanostructure or ultrafine grain austenite. The tensile testing of the ultrafine-grained austenitic stainless steel showed a yield strength 4 to 6 times higher in comparison to its coarse-grained counterpart. However, it demonstrated very poor ductility due to inadequate strain hardenability. The poor strain hardenability was correlated with the formation of strain-induced martensite in this steel grade.
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NASA Astrophysics Data System (ADS)
Paul, S. K.; Ahmed, U.; Megahed, G. M.
2011-10-01
Low-carbon Al-killed hot rolled strips for direct forming, cold rolling, and galvanizing applications are produced from the similar chemistry at Ezz Flat Steel (EFS) through thin slab casting and rolling (TSCR) technology. The desired mechanical and microstructural properties in hot bands for different applications are achieved through control of hot rolling parameters, which in turn control the precipitation and growth of AlN. Nitrogen in solid solution strongly influences the yield strength (YS), ductility, strain aging index (SAI), and other formability properties of steel. The equilibrium solubility of AlN in austenite at different temperatures and its isothermal precipitation have been studied. To achieve the formability properties for direct forming, soluble nitrogen is fixed as AlN by coiling the strip at higher temperatures. For stringent cold forming, boron was added below the stoichiometric ratio with nitrogen, which improved the formability properties dramatically. The requirements of hot band for processing into cold rolled and annealed deep drawing sheets are high SAI and fine-grain microstructure. Higher finish rolling and low coiling temperatures are used to achieve these. Fully processed cold rolled sheets from these hot strips at customer's end have shown good formability properties. Coil break marks observed in some coils during uncoiling were found to be associated with yielding phenomenon. The spike height (difference between upper and lower yield stresses) and yield point elongation (YPE) were found to be the key material parameters for the break marks. Factors affecting these parameters have been studied and the coiling temperature optimized to overcome the problem.
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Investigation on the cold rolling and structuring of cold sprayed copper-coated steel sheets
NASA Astrophysics Data System (ADS)
Bobzin, K.; Öte, M.; Wiesner, S.; Gerdt, L.; Senge, S.; Hirt, G.
2017-03-01
A current driving force of research is lightweight design. One of the approaches to reduce the weight of a component without causing an overall stiffness decrease is the use of multi-material components. One of the main challenges of this approach is the low bonding strength between different materials. Focusing on steel-aluminum multi-material components, thermally sprayed copper coatings can come into use as a bonding agent between steel sheets and high pressure die cast aluminum to improve the bonding strength. This paper presents a combination of cold gas spraying of copper coatings and their subsequent structuring by rolling as surface pretreatment method of the steel inserts. Therefore, flat rolling experiments are performed with samples in “as sprayed” and heat treated conditions to determine the influence of the rolling process on the bond strength and the formability of the coating. Furthermore, the influence of the rolling on the roughness and the hardness of the coating was examined. In the next step, the coated surface was structured, to create a surface topology suited for a form closure connection in a subsequent high-pressure die casting process. No cracks were observed after the cold rolling process with a thickness reduction of up to ε = 14 % for heat treated samples. Structuring of heat treated samples could be realized without delamination and cracking.
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NASA Astrophysics Data System (ADS)
Kim, Seung-Gyu; Kim, Najung; Shim, Hyung-Seok; Kwon, Oh Min; Kwon, Dongil
2018-05-01
The superconductor industry considers cold-rolled austenitic stainless 310S steel a less expensive substitute for Hastelloy X as a substrate for coated superconductor. However, the mechanical properties of cold-rolled 310S substrate degrade significantly in the superconductor deposition process. To overcome this, we applied hot rolling at 900 °C (or 1000 °C) to the 310S substrate. To check the property changes, a simulated annealing condition equivalent to that used in manufacturing was determined and applied. The effects of the hot rolling on the substrate were evaluated by analyzing its physical properties and texture.
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Influences of rolling method on deformation force in cold roll-beating forming process
NASA Astrophysics Data System (ADS)
Su, Yongxiang; Cui, Fengkui; Liang, Xiaoming; Li, Yan
2018-03-01
In process, the research object, the gear rack was selected to study the influence law of rolling method on the deformation force. By the mean of the cold roll forming finite element simulation, the variation regularity of radial and tangential deformation was analysed under different rolling methods. The variation of deformation force of the complete forming racks and the single roll during the steady state under different rolling modes was analyzed. The results show: when upbeating and down beating, radial single point average force is similar, the tangential single point average force gap is bigger, the gap of tangential single point average force is relatively large. Add itionally, the tangential force at the time of direct beating is large, and the dire ction is opposite with down beating. With directly beating, deformation force loading fast and uninstall slow. Correspondingly, with down beating, deformat ion force loading slow and uninstall fast.
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Hot rolling of thick uranium molybdenum alloys
DeMint, Amy L.; Gooch, Jack G.
2015-11-17
Disclosed herein are processes for hot rolling billets of uranium that have been alloyed with about ten weight percent molybdenum to produce cold-rollable sheets that are about one hundred mils thick. In certain embodiments, the billets have a thickness of about 7/8 inch or greater. Disclosed processes typically involve a rolling schedule that includes a light rolling pass and at least one medium rolling pass. Processes may also include reheating the rolling stock and using one or more heavy rolling passes, and may include an annealing step.
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NASA Astrophysics Data System (ADS)
Tanhaei, S.; Gheisari, Kh.; Alavi Zaree, S. R.
2018-06-01
This study has evaluated the effect of different levels of cold rolling (from 0 to 50%) on the microstructural, magnetic, and mechanical properties and the corrosion behavior of 316L austenitic stainless steel in NaCl (1 mol/L) + H2SO4 (0.5 mol/L) solution. Microstructural examinations using optical microscopy revealed the development of a morphological texture from coaxial to elongated grains during the cold-rolling process. Phase analysis carried out on the basis of X-ray diffraction confirmed the formation of the ferromagnetic α'-martensite phase under the stresses applied during cold rolling. This finding is in agreement with magnetic measurements using a vibrating sample magnetometer. Mechanical properties determined by tensile and Vickers microhardness tests demonstrated an upward trend in the hardness-to-yield strength ratio with increasing cold-rolling percentage, representing a reduction in the material's work-hardening ability. Uniform and localized corrosion parameters were estimated via potentiodynamic polarization corrosion tests and electrochemical impedance spectroscopy. In contrast to the uniform corrosion, wherein the corrosion current density increased with increasing cold-working degree because of the high density of microstructural defects, the passive potential range and breakdown potential increased by cold working, showing greater resistance to pit nucleation. Although pits were formed, the cold-rolled material repassivation tendency decreased because of the broader hysteresis anodic loop, as confirmed experimentally by observation of the microscopic features after electrochemical cyclic polarization evaluations.
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NASA Astrophysics Data System (ADS)
Pedneault, Sylvain; Huot, Jacques; Roué, Lionel
In the present work, cold rolling has been investigated as a new means of producing Mg-based metal hydrides for nickel-metal hydride (Ni-MH) batteries. Structure and electrochemical evolution of 2Mg-Ni cold-rolled samples were investigated as a function of the number of rolling passes as well as heat treatment. It was found that nanocrystalline Mg 2Ni alloy can be obtained by an appropriate three step process involving rolling, heat treatment and rolling again. It was shown that the number of primary and secondary rolling passes must be carefully optimized in order to favour the complete formation of Mg 2Ni alloy having a nanocrystalline structure (∼10 nm in crystallite size) without excessive sample oxidation. Actually, the best result was obtained by first rolling 90 times, followed by a heat treatment at 400 °C for 4 h and roll again 20 times. The resulting material displayed an initial discharge capacity of 205 mAh g -1, which is quite similar to that obtained with ball-milled Mg 2Ni alloy.
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Method of manufacturing aluminide sheet by thermomechanical processing of aluminide powders
Hajaligol, Mohammad R.; Scorey, Clive; Sikka, Vinod K.; Deevi, Seetharama C.; Fleishhauer, Grier; Lilly, Jr., A. Clifton; German, Randall M.
2003-12-09
A powder metallurgical process of preparing a sheet from a powder having an intermetallic alloy composition such as an iron, nickel or titanium aluminide. The sheet can be manufactured into electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 4 to 32% Al, and optional additions such as .ltoreq.1% Cr, .gtoreq.0.05% Zr .ltoreq.2% Ti, .ltoreq.2% Mo, .ltoreq.1% Ni, .ltoreq.0.75% C, .ltoreq.0.1% B, .ltoreq.1% submicron oxide particles and/or electrically insulating or electrically conductive covalent ceramic particles, .ltoreq.1% rare earth metal, and/or .ltoreq.3% Cu. The process includes forming a non-densified metal sheet by consolidating a powder having an intermetallic alloy composition such as by roll compaction, tape casting or plasma spraying, forming a cold rolled sheet by cold rolling the non-densified metal sheet so as to increase the density and reduce the thickness thereof and annealing the cold rolled sheet. The powder can be a water, polymer or gas atomized powder which is subjecting to sieving and/or blending with a binder prior to the consolidation step. After the consolidation step, the sheet can be partially sintered. The cold rolling and/or annealing steps can be repeated to achieve the desired sheet thickness and properties. The annealing can be carried out in a vacuum furnace with a vacuum or inert atmosphere. During final annealing, the cold rolled sheet recrystallizes to an average grain size of about 10 to 30 .mu.m. Final stress relief annealing can be carried out in the B2 phase temperature range.
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Thermomechanical processing of plasma sprayed intermetallic sheets
Hajaligol, Mohammad R.; Scorey, Clive; Sikka, Vinod K.; Deevi, Seetharama C.; Fleischhauer, Grier; Lilly, Jr., A. Clifton; German, Randall M.
2001-01-01
A powder metallurgical process of preparing a sheet from a powder having an intermetallic alloy composition such as an iron, nickel or titanium aluminide. The sheet can be manufactured into electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 4 to 32% Al, and optional additions such as .ltoreq.1% Cr, .gtoreq.0.05% Zr .ltoreq.2% Ti, .ltoreq.2% Mo, .ltoreq.1% Ni, .ltoreq.0.75% C, .ltoreq.0.1% B, .ltoreq.1% submicron oxide particles and/or electrically insulating or electrically conductive covalent ceramic particles, .ltoreq.1% rare earth metal, and/or .ltoreq.3% Cu. The process includes forming a non-densified metal sheet by consolidating a powder having an intermetallic alloy composition such as by roll compaction, tape casting or plasma spraying, forming a cold rolled sheet by cold rolling the non-densified metal sheet so as to increase the density and reduce the thickness thereof and annealing the cold rolled sheet. The powder can be a water, polymer or gas atomized powder which is subjecting to sieving and/or blending with a binder prior to the consolidation step. After the consolidation step, the sheet can be partially sintered. The cold rolling and/or annealing steps can be repeated to achieve the desired sheet thickness and properties. The annealing can be carried out in a vacuum furnace with a vacuum or inert atmosphere. During final annealing, the cold rolled sheet recrystallizes to an average grain size of about 10 to 30 .mu.m. Final stress relief annealing can be carried out in the B2 phase temperature range.
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Method of manufacturing aluminide sheet by thermomechanical processing of aluminide powders
Hajaligol, Mohammad R.; Scorey, Clive; Sikka, Vinod K.; Deevi, Seetharama C.; Fleischhauer, Grier; Lilly, Jr., A. Clifton; German, Randall M.
2000-01-01
A powder metallurgical process of preparing a sheet from a powder having an intermetallic alloy composition such as an iron, nickel or titanium aluminide. The sheet can be manufactured into electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 4 to 32% Al, and optional additions such as .ltoreq.1% Cr, .gtoreq.0.05% Zr.ltoreq.2% Ti, .ltoreq.2% Mo, .ltoreq.1% Ni, .ltoreq.0.75% C, .ltoreq.0.1% B, .ltoreq.1% submicron oxide particles and/or electrically insulating or electrically conductive covalent ceramic particles, .ltoreq.1% rare earth metal, and/or .ltoreq.3% Cu. The process includes forming a non-densified metal sheet by consolidating a powder having an intermetallic alloy composition such as by roll compaction, tape casting or plasma spraying, forming a cold rolled sheet by cold rolling the non-densified metal sheet so as to increase the density and reduce the thickness thereof and annealing the cold rolled sheet. The powder can be a water, polymer or gas atomized powder which is subjecting to sieving and/or blending with a binder prior to the consolidation step. After the consolidation step, the sheet can be partially sintered. The cold rolling and/or annealing steps can be repeated to achieve the desired sheet thickness and properties. The annealing can be carried out in a vacuum furnace with a vacuum or inert atmosphere. During final annealing, the cold rolled sheet recrystallizes to an average grain size of about 10 to 30 .mu.m. Final stress relief annealing can be carried out in the B2 phase temperature range.
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Control of surface thermal scratch of strip in tandem cold rolling
NASA Astrophysics Data System (ADS)
Chen, Jinshan; Li, Changsheng
2014-07-01
The thermal scratch seriously affects the surface quality of the cold rolled stainless steel strip. Some researchers have carried out qualitative and theoretical studies in this field. However, there is currently a lack of research on effective forecast and control of thermal scratch defects in practical production, especially in tandem cold rolling. In order to establish precise mathematical model of oil film thickness in deformation zone, the lubrication in cold rolling process of SUS410L stainless steel strip is studied, and major factors affecting oil film thickness are also analyzed. According to the principle of statistics, mathematical model of critical oil film thickness in deformation zone for thermal scratch is built, with fitting and regression analytical method, and then based on temperature comparison method, the criterion for deciding thermal scratch defects is put forward. Storing and calling data through SQL Server 2010, a software on thermal scratch defects control is developed through Microsoft Visual Studio 2008 by MFC technique for stainless steel in tandem cold rolling, and then it is put into practical production. Statistics indicate that the hit rate of thermal scratch is as high as 92.38%, and the occurrence rate of thermal scratch is decreased by 89.13%. Owing to the application of the software, the rolling speed is increased by approximately 9.3%. The software developed provides an effective solution to the problem of thermal scratch defects in tandem cold rolling, and helps to promote products surface quality of stainless steel strips in practical production.
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NASA Astrophysics Data System (ADS)
Gaillac, Alexis; Ly, Céline
2018-05-01
Within the forming route of Zirconium alloy cladding tubes, hot extrusion is used to deform the forged billets into tube hollows, which are then cold rolled to produce the final tubes with the suitable properties for in-reactor use. The hot extrusion goals are to give the appropriate geometry for cold pilgering, without creating surface defects and microstructural heterogeneities which are detrimental for subsequent rolling. In order to ensure a good quality of the tube hollows, hot extrusion parameters have to be carefully chosen. For this purpose, finite element models are used in addition to experimental tests. These models can take into account the thermo-mechanical coupling conditions obtained in the tube and the tools during extrusion, and provide a good prediction of the extrusion load and the thermo-mechanical history of the extruded product. This last result can be used to calculate the fragmentation of the microstructure in the die and the meta-dynamic recrystallization after extrusion. To further optimize the manufacturing route, a numerical model of the cold pilgering process is also applied, taking into account the complex geometry of the tools and the pseudo-steady state rolling sequence of this incremental forming process. The strain and stress history of the tube during rolling can then be used to assess the damage risk thanks to the use of ductile damage models. Once validated vs. experimental data, both numerical models were used to optimize the manufacturing route and the quality of zirconium cladding tubes. This goal was achieved by selecting hot extrusion parameters giving better recrystallized microstructure that improves the subsequent formability. Cold pilgering parameters were also optimized in order to reduce the potential ductile damage in the cold rolled tubes.
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NASA Astrophysics Data System (ADS)
Zhou, Xiao; Liu, Qiang; Liu, Ruirui; Zhou, Haitao
2018-06-01
The mechanical properties and microstructure evolution of Mg-8Li-3Al-1Y alloy undergoing different rolling processes were systematically investigated. X-ray diffraction, optical microscope, scanning electron microscopy, transmission electron microscopy as well as electron backscattered diffraction were used for tracking the microstructure evolution. Tensile testing was employed to characterize the mechanical properties. After hot rolling, the MgLi2Al precipitated in β-Li matrix due to the transformation reaction: β-Li → β-Li + MgLi2Al + α-Mg. As for the alloy subjected to annealed hot rolling, β-Li phase was clearly recrystallized while recrystallization rarely occurred in α-Mg phase. With regard to the microstructure undergoing cold rolling, plenty of dislocations and dislocation walls were easily observed. In addition, the microstructure of alloys subjected to annealed cold rolling revealed the formation of new fresh α-Mg grains in β-Li phase due to the precipitation reaction. The mechanical properties and fracture modes of Mg-8Li-3Al-1Y alloys can be effectively tuned by different rolling processes.
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Lin, Hung-Pin; Chen, Delphic; Kuo, Jui-Chao
2015-01-01
In this study, the grain boundary character and texture of 50% and 90% cold-rolled FePd alloy was investigated during recrystallization at 700 °C. Electron backscatter diffraction (EBSD) measurements were performed on the rolling direction to normal direction section. Kernel average misorientation (KAM) calculated from EBSD measurements was employed to determine the recrystallization fraction. The Avrami exponent n of recrystallization is 1.9 and 4.9 for 50% and 90% cold rolling, respectively. The new formation of texture reveals random texture during the recrystallization process. As annealing time increased, the number of high angle boundary (HAGB) and coincidence site lattice (CSL) increased with consumption of low angle boundary (LAGB). In addition, possible transformations between different grain boundaries are observed here.
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Model for texture evolution in cold rolling of 2.4 wt.-% Si non-oriented electrical steel
NASA Astrophysics Data System (ADS)
Wei, X.; Hojda, S.; Dierdorf, J.; Lohmar, J.; Hirt, G.
2017-10-01
Iron loss and limited magnetic flux density are constraints for NGO electrical steel used in highly efficient electrical machinery cores. The most important factors that affect these properties are the final microstructure and the texture of the NGO steel. Reviewing the whole process chain, cold rolling plays an important role because the recrystallization and grain growth during the final heat treatment can be strongly affected by the stored energy and microstructure of cold rolling, and some texture characteristics can be inherited as well. Therefore, texture evolution during cold rolling of NGO steel is worth a detailed investigation. In this paper, texture evolution in cold rolling of non-oriented (NGO) electrical steel is simulated with a crystal plasticity finite element method (CPFEM) model. In previous work, a CPFEM model has been implemented for simulating the texture evolution with periodic boundary conditions and a phenomenological constitutive law. In a first step the microstructure in the core of the workpiece was investigated and mapped to a representative volume element to predict the texture evolution. In this work an improved version of the CPFEM model is described that better reflects the texture evolution in cold rolling of NGO electrical steel containing 2.4 wt.-% Si. This is achieved by applying the deformation gradient and calibrating the flow curve within the CPFEM model. Moreover, the evolution of dislocation density is calculated and visualized in this model. An in depth comparison of the numerical and experimental results reveals, that the improved CPFEM model is able to represent the important characteristics of texture evolution in the core of the workpiece during cold rolling with high precision.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Wang Wei; Helbert, Anne-Laure, E-mail: anne-laure.helbert@u-psud.fr; Baudin, Thierry
In high purity Aluminum, very strong {l_brace}100{r_brace}<001> recrystallization texture is developed after 98% cold rolling and annealing at 500 Degree-Sign C. On the contrary, in Aluminum alloys of commercial purity, the Cube component hardly exceeds 30% after complete recrystallization. Parameters controlling Cube orientation development are mainly the solute dragging due to impurities in solid solution and the stored deformation energy. In the present study, besides the 85% cold rolling, two extra annealings and a slight cold rolling are introduced in the processing route to increase the Cube volume fraction. The Cube development was analyzed by X-ray diffraction and Electron BackScatteredmore » Diffraction (EBSD). The nucleation and growth mechanisms responsible for the large Cube growth were investigated using FEG/EBSD in-situ heating experiments. Continuous recrystallization was observed in Cube oriented grains and competed with SIBM (Strain Induced Boundary Migration) mechanism. This latter was favored by the stored energy gap introduced during the additional cold-rolling between the Cube grains and their neighbors. Finally, a Cube volume fraction of 65% was reached after final recrystallization. - Highlights: Black-Right-Pointing-Pointer EBSD in-situ heating experiments of aluminum alloy of commercial purity. Black-Right-Pointing-Pointer A 10% cold-rolling after a partial recrystallization improved Cube nucleation and growth. Black-Right-Pointing-Pointer Annealing before cold-rolling limited the solute drag effect and permitted a large Cube growth. Black-Right-Pointing-Pointer Cube development is enhanced by continuous recrystallization of Cube sub-grains. Black-Right-Pointing-Pointer The preferential Cube growth occurs by SIBM of small Cube grains.« less
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NASA Astrophysics Data System (ADS)
He, Youliang; Mehdi, Mehdi; Hilinski, Erik J.; Edrisy, Afsaneh
2018-05-01
Magnetic Barkhausen noise (MBN) signals were measured on a non-oriented electrical steel through all the thermomechanical processing stages, i.e. hot rolling, hot band annealing, cold rolling and final annealing. The temperature of the final annealing was varied from 600 °C to 750 °C so that the steel consisted of partially or completely recrystallized microstructures and different levels of residual stresses. The angular MBNrms (root mean square) values were compared to the texture factors in the same directions, the latter being calculated from the crystallographic texture measured by electron backscatter diffraction (EBSD). It was found that, in the cold-rolled, hot-rolled and completely recrystallized steels, the angular MBNrms followed a cosine function with respect to the angle of magnetization, while in partially recrystallized state such a relation does not exist. After cold rolling, the maximum MBNrms was observed in the rolling direction (RD) and the minimum MBNrms was in the transverse direction (TD), which was inconsistent with the magnetocrystalline anisotropy as indicated by the texture factor. After hot rolling, the maximum and minimum MBNrms values were observed in the TD and RD, respectively, exactly opposite to the cold-rolled state. If the steel was completely recrystallized, the maximum MBNrms was normally observed at a direction that was 15-30° from the minimum texture factor. If the steel was partially recrystallized, both the magnetocrystalline anisotropy of the material and the residual stress contributed to the angular MBNrms, which resulted in the deviation of the relationship from a cosine function. The relative strength of the two factors determined which factor would dominate the overall magnetic anisotropy.
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The Evolution of Second-Phase Particles in 6111 Aluminum Alloy Processed by Hot and Cold Rolling
NASA Astrophysics Data System (ADS)
Zhang, Lixin; Wang, Yihan; Ni, Song; Chen, Gang; Li, Kai; Du, Yong; Song, Min
2018-03-01
The evolution of coarse Al9.9Fe2.65Ni1.45 phase, spherical Al12(Mn,Fe)3Si phase and rod-like Q phase in a 6111 aluminum alloy during hot and cold rolling deformation processes was systematically investigated in this work. The results showed that the coarse Al9.9Fe2.65Ni1.45 particles are mainly distributed at the grain boundaries, accompanied by the co-formation of Al12(Fe,Mn)3Si phase and Mg2Si phase, while the spherical Al12(Mn,Fe)3Si particles are mainly distributed in the grain interiors. Hot rolling has little effects on the size and distribution of both phases, but cold deformation can severely decrease the size of the particles by breaking the particles into small pieces. In addition, the temperature of 450 °C is not high enough for the dissolution of Q phase in the Al matrix, but the Q particles can be broken into small pieces due to the stress concentration during both hot and cold rolling deformation. In addition, the influences of phase evolution, dislocations and recrystallization on the mechanical properties evolution were also discussed.
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NASA Astrophysics Data System (ADS)
Sych, O. V.; Khlusova, E. I.; Yashin, E. A.
2017-12-01
The paper presents the results of quantitative analysis of C, Mn, Ni and Cu content on strength and cold-resistance of rolled plates. Relations between the ferritic-bainitic structure morphology and anisotropy and steel performance characteristics have been established. Influence of thermal and deformation rolling patterns on steel structure has been studied. The steel chemical composition has been improved and precision thermomechanical processing conditions for production of cold-resistant Arc-steel plates have been developed.
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Polymer quenched prealloyed metal powder
Hajaligol, Mohammad R.; Fleischhauer, Grier; German, Randall M.
2001-01-01
A powder metallurgical process of preparing a sheet from a powder having an intermetallic alloy composition such as an iron, nickel or titanium aluminide. The sheet can be manufactured into electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 4 to 32% Al, and optional additions such as .ltoreq.1% Cr, .gtoreq.0.05% Zr .ltoreq.2% Ti, .ltoreq.2% Mo, .ltoreq.1% Ni, .ltoreq.0.75% C, .ltoreq.0.1% B, .ltoreq.1% submicron oxide particles and/or electrically insulating or electrically conductive covalent ceramic particles, .ltoreq.1% rare earth metal, and/or .ltoreq.3 % Cu. The process includes forming a non-densified metal sheet by consolidating a powder having an intermetallic alloy composition such as by roll compaction, tape casting or plasma spraying, forming a cold rolled sheet by cold rolling the non-densified metal sheet so as to increase the density and reduce the thickness thereof and annealing the cold rolled sheet. The powder can be a water, polymer or gas atomized powder which is subjecting to sieving and/or blending with a binder prior to the consolidation step. After the consolidation step, the sheet can be partially sintered. The cold rolling and/or annealing steps can be repeated to achieve the desired sheet thickness and properties. The annealing can be carried out in a vacuum furnace with a vacuum or inert atmosphere. During final annealing, the cold rolled sheet recrystallizes to an average grain size of about 10 to 30 .mu.m. Final stress relief annealing can be carried out in the B2 phase temperature range.
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Analysis of Fatigue Crack Paths in Cold Drawn Pearlitic Steel
Toribio, Jesús; González, Beatriz; Matos, Juan-Carlos
2015-01-01
In this paper, a fracto-metallographic analysis was performed on the cracked specimens of cold drawn pearlitic steel subjected to fatigue tests. Fatigue cracks are transcollonial and exhibit a preference for fracturing pearlitic lamellae, with non-uniform crack opening displacement values, micro-discontinuities, branchings, bifurcations and frequent local deflections that create microstructural roughness. At the micro-level, the cold drawn pearlitic steel exhibits higher micro-roughness than the hot rolled bar (this is a consequence of the manufacturing process by cold drawing), so that the actual fractured surface in the cold drawn wire is greater than that in the hot rolled bar, due to the fact that the crack deflection events are more frequent and with higher angle in the former (the heavily drawn prestressing steel wire). These findings show the relevant role on the manufacturing process by cold drawing in the fatigue crack propagation in pearlitic steel. PMID:28793647
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Analysis of Fatigue Crack Paths in Cold Drawn Pearlitic Steel.
Toribio, Jesús; González, Beatriz; Matos, Juan-Carlos
2015-11-04
In this paper, a fracto-metallographic analysis was performed on the cracked specimens of cold drawn pearlitic steel subjected to fatigue tests. Fatigue cracks are transcollonial and exhibit a preference for fracturing pearlitic lamellae, with non-uniform crack opening displacement values, micro-discontinuities, branchings, bifurcations and frequent local deflections that create microstructural roughness. At the micro-level, the cold drawn pearlitic steel exhibits higher micro-roughness than the hot rolled bar (this is a consequence of the manufacturing process by cold drawing), so that the actual fractured surface in the cold drawn wire is greater than that in the hot rolled bar, due to the fact that the crack deflection events are more frequent and with higher angle in the former (the heavily drawn prestressing steel wire). These findings show the relevant role on the manufacturing process by cold drawing in the fatigue crack propagation in pearlitic steel.
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Tang, Yan; Le, Qichi; Wang, Tong; Chen, Xingrui
2017-10-12
The microstructural evolution, mechanical properties, and mathematical relationship of an α, α + β, and β phase Mg-Li alloy during the cold rolling and annealing process were investigated. The results showed that the increased Li element gradually transformed the Mg matrix structure from hcp to bcc. Simultaneously, the alloy plasticity was improved remarkably during cold rolling. In the annealing process, a sort of abnormal grain growth was found in Mg-11Li-3Al-2Zn-0.2Y, but was not detected in Mg-5Li-3Al-2Zn-0.2Y and Mg-8Li-3Al-2Zn-0.2Y. Moreover, the mechanical properties of alloy were evidently improved through a kind of solid solution in the β matrix. To accurately quantify this strengthening effect, the method of mathematical modeling was used to determine the relationship between strength and multiple factors.
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A novel ultra-low carbon grain oriented silicon steel produced by twin-roll strip casting
NASA Astrophysics Data System (ADS)
Wang, Yang; Zhang, Yuan-Xiang; Lu, Xiang; Fang, Feng; Xu, Yun-Bo; Cao, Guang-Ming; Li, Cheng-Gang; Misra, R. D. K.; Wang, Guo-Dong
2016-12-01
A novel ultra-low carbon grain oriented silicon steel was successfully produced by strip casting and two-stage cold rolling method. The microstructure, texture and precipitate evolution under different first cold rolling reduction were investigated. It was shown that the as-cast strip was mainly composed of equiaxed grains and characterized by very weak Goss texture ({110}<001>) and λ-fiber (<001>//ND). The coarse sulfides of size 100 nm were precipitated at grain boundaries during strip casting, while nitrides remained in solution in the as-cast strip and the fine AlN particles of size 20-50 nm, which were used as grain growth inhibitors, were formed in intermediate annealed sheet after first cold rolling. In addition, the suitable Goss nuclei for secondary recrystallization were also formed during intermediate annealing, which is totally different from the conventional process that the Goss nuclei originated in the subsurface layer of the hot rolled sheet. Furthermore, the number of AlN inhibitors and the intensity of desirable Goss texture increased with increasing first cold rolling reduction. After secondary recrystallization annealing, very large grains of size 10-40 mm were formed and the final magnetic induction, B8, was as high as 1.9 T.
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NASA Astrophysics Data System (ADS)
He, Tong; Bai, Yang; Liu, Xiuting; Guo, Dan; Liu, Yandong
2018-04-01
We investigated the effect of Sn micro-alloying on recrystallization nucleation and growth processes of ferritic stainless steels. The as-received hot rolled sheets were cold rolled up to 80% reduction and then annealed at 740-880 °C for 5 min. The cold rolling and recrystallization microstructures and micro-textures of Sn-containing and Sn-free ferritic stainless steels were all determined by electron backscatter diffraction. Our Results show that Sn micro-alloying has important effects on recrystallization nucleation and growth processes of ferritic stainless steels. Sn micro-alloying conduces to grain fragmentation in the deformation band, more fragmented grains are existed in Sn-containing cold rolled sheets, which provides more sites for recrystallization nucleation. Sn micro-alloying also promotes recrystallization process and inhibits the growth of recrystallized grains. The recrystallization nucleation and growth mechanism of Sn-containing and Sn-free ferritic stainless steels are both characterized by orientation nucleation and selective growth, but Sn micro-alloying promotes the formation of γ-oriented grains. Furthermore, Sn micro-alloying contributes to the formation of Σ13b CSL boundaries and homogeneous γ-fiber texture. Combining the results of microstructure and micro-texture, the formability of Sn-containing ferritic stainless steels will be improved to some extent.
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Effect of Cold-rolling on Mechanical Properties and Microstructure of an Al-12%Si-0.2%Mg Alloy
NASA Astrophysics Data System (ADS)
Liao, Hengcheng; Cai, Mingdong; Jing, Qiumin; Ding, Ke
2011-11-01
Effect of multi-pass cold-rolling on the mechanical properties and microstructure of a near-eutectic Al-12%Si-0.2%Mg casting alloy was investigated. Optical microscopy, SEM, and TEM were employed to resolve the as-rolled microstructure, and the microstructure of samples after aging treatment. It has been found that Brinell hardness increases considerably with rolling reduction ratio; and further annealing leads to a remarkable drop in hardness. Two mechanisms, namely precipitation hardening and recovery softening, were found to develop simultaneously in the subsequent aging treatment following cold rolling. In contrast, recovery softening dominated the aging of cold-rolled specimen with prior intermediate annealing. Tensile properties were also performed to measure the effect of cold rolling and subsequent aging treatment.
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Manufacturing Methods and Technology Project Summary Reports.
1980-12-01
deposition of chrome-copper (Cr- Cu ), dry-film photoresist application, photolithographic masking, spray etching, die bonding, ultrasonic...4) cold roll forging. Of these, the cold roll forging process is the most widely used for the pro- duction of steel and low alloy blades. It provides... sprayed Mo- Al -Ni both provide relatively good wear resistance, see Figure 1. The powder -flame sprayed aluminum bronze did not perform as well. 147 -S t. I
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Lin, Hung-Pin; Chen, Yen-Chun; Chen, Delphic
2014-08-15
In this study, the evolution of the recrystallization texture and microstructure was investigated after annealing of 50% and 90% cold-rolled FePd alloy at 530 °C. The FePd alloy was produced by vacuum arc melting in an atmosphere of 97% Ar and 3% H{sub 2}. The specimens were cold rolled to achieve 50% and 90% reduction in thickness. Electron backscatter diffraction measurements were performed on the rolling direction–normal direction section. With increased deformation from 50% to 90%, recrystallized texture transition occurs. For the 50% cold-rolled alloy, the preferred orientation is (0 1 0) [11 0 1], which is close to themore » cubic orientation after 400 h of annealing. For the 90% cold-rolled alloy, the orientation changes to (0 5 4) [22–4 5] after 16 h of annealing. - Highlights: • Texture and microstructure in cold-rolled FePd alloy was investigated during annealing using EBSD. • The recrystallized texture of 50% cold-rolled FePd is (0 1 0) [11 0 1] at 530 °C for 400 hours. • The recrystallized texture of 90% cold-rolled FePd is changed to (0 5 4) [22–4 5] at 530 °C after 16 hours.« less
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NASA Astrophysics Data System (ADS)
Kim, Young Suk; Kim, Sung Soo
2016-09-01
We show that enhanced stress corrosion cracking (SCC) initiation in cold-rolled Alloy 690 with decreasing strain rate is related to the rate of short-range ordering (SRO) but not to the time-dependent corrosion process. Evidence for SRO is provided by aging tests on cold-rolled Alloy 690 at 623 K and 693 K (350 °C and 420 °C), respectively, which demonstrate its enhanced lattice contraction and hardness increase with aging temperature and time, respectively. Secondary intergranular cracks formed only in thermally treated and cold-rolled Alloy 690 during SCC tests, which are not SCC cracks, are caused by its lattice contraction by SRO before SCC tests but not by the orientation effect.
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NASA Astrophysics Data System (ADS)
Schmidt, Hans Christian; Homberg, Werner; Orive, Alejandro Gonzalez; Grundmeier, Guido; Hordych, Illia; Maier, Hans Jürgen
2018-05-01
In this study the manufacture of aluminium-steel blanks by cold pressure welding and their preparation for a welding process through electrochemical surface treatment are investigated and discussed. The cold pressure welding process was done with an incremental rolling tool that allows for the partial pressure welding of two blanks along a prepared path. The influence of the surface preparation by electrochemical deposition of bond promoting organosilane-based agents and roughening on a nano-scale is investigated and compared to conventional surface treatments. Coating the surfaces with a thin organosilane-based film incorporating specific functional groups should promote additional bonding between the mating oxide layers; its influence on the total weld strength is studied. Pressure welding requires suitable process strategies, and the current advances in the proposed incremental rolling process for the combination of mild steel and aluminium are presented.
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Defining rolled metal performance for cold bolt upsetting (bolt head)
NASA Astrophysics Data System (ADS)
Pachurin, G. V.; Shevchenko, S. M.; Filippov, A. A.; Mukhina, M. V.; Kuzmin, N. A.
2018-03-01
Hardware items are one of the products for mass consumption. Rolled metal for cold forging shall have the required ductility, uniform mechanical characteristics along the mill length, corresponding chemical composition and shall be free from internal or superficial defects. Standard mechanical characteristics have been reviewed in this document and fracture criteria of calibrated rolled steel 40X have been calculated after its isothermal treatment at different temperatures in nitre bath and subsequent drawing with different deformation degrees. Comparison of synergy fracture criteria showed that rolled stock, treated as per the proposed conditions: bath patenting at the temperature of 400°C and drawing with reduction rate of 5% and 10%, are more preferable, comparing to processing conditions, existing in the industry.
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NASA Astrophysics Data System (ADS)
Trivedi, Shefali; Ravi Kumar, D.; Aravindan, S.
2016-10-01
Phosphorus in steel is known to increase strength and hardness and decrease ductility. Higher phosphorus content (more than 0.05%), however, promotes brittle behavior due to segregation of Fe3P along the grain boundaries which makes further mechanical working of these alloys difficult. In this work, thin sheets of Fe-P alloys (with phosphorus in range of 0.1-0.35%) have been developed through processing by powder metallurgy followed by hot rolling and cold rolling. The effect of phosphorus content and annealing parameters (temperature and time) on microstructure, mechanical properties, formability in biaxial stretching and fracture behavior of the cold rolled and annealed sheets has been studied. A comparison has also been made between the properties of the sheets made through P/M route and the conventional cast route with similar phosphorus content. It has been shown that thin sheets of Fe-P alloys with phosphorous up to 0.35% possessing a good combination of strength and formability can be produced through rolling of billets of these alloys made through powder metallurgy technique without the problem of segregation.
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NASA Astrophysics Data System (ADS)
Park, S. A.; Kim, J. G.; He, Y. S.; Shin, K. S.; Yoon, J. B.
2014-12-01
The correlation between the corrosion and microstructual characteristics of cold rolled and hot rolled low-alloy steels containing copper and antimony was established. The corrosion behavior of the specimens used in flue gas desulfurization systems was examined by electrochemical and weight loss measurements in an aggressive solution of 16.9 vol % H2SO4 + 0.35 vol % HCl at 60°C, pH 0.3. It has been shown that the corrosion rate of hot rolled steel is lower than that of cold rolled steel. The corrosion rate of cold rolled steel was increased by grain refinement, inclusion formation, and preferred grain orientation.
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Combustion Synthesis Reaction Behavior of Cold-Rolled Ni/Al and Ti/Al Multilayers
2011-04-01
6 Figure 4 . Combustion synthesis process of the cold-rolled Ni/Al multilayer foils: (a) reaction front of the displacement of the reaction...Reactive Nanostructured Foil Used as a Heat Source for Joining Titanium . J. Appl. Phys. 2004, 96 ( 4 ), 2336–2342. 16. Wang, J.; Besnoin, E...2011 2. REPORT TYPE Final 3. DATES COVERED (From - To) January 2006–January 2008 4 . TITLE AND SUBTITLE Combustion Synthesis Reaction Behavior of
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Effect of Thermomechanical Processing on Texture and Superelasticity in Fe-Ni-Co-Al-Ti-B Alloy
NASA Astrophysics Data System (ADS)
Lee, Doyup; Omori, Toshihiro; Han, Kwangsik; Hayakawa, Yasuyuki; Kainuma, Ryosuke
2018-03-01
The texture and superelasticity were investigated in austenitic Fe-Ni-Co-Al-Ti-B alloy with various reduction ratios of cold rolling and heating ratios in annealing. The rolled sheets show the {110} <112> deformation texture at a reduction ratio higher than 80%, while the texture hardly changes in the primary recrystallization at 1000 °C. The β (B2) precipitates inhibit the grain growth at this temperature, but they dissolve during heating, and secondary recrystallization occurs due to decreased pinning force at temperatures higher than 1100 °C, resulting in texture change to {210} <001> . The recrystallization texture is more strongly developed when the reduction ratio and heating rate are high and slow, respectively. The 90% cold-rolled and slowly heated sheet shows the recrystallization texture and high fraction of low-angle boundaries. As a result, ductility and superelasticity can be drastically improved in the 90% cold-rolled sheet, although superelasticity was previously obtained only in thin sheets with 98.5% reduction.
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NASA Astrophysics Data System (ADS)
Chu, J. P.; Rigsbee, J. M.; Banaś, G.; Lawrence, F. V.; Elsayed-Ali, H. E.
1995-06-01
The effects of laser-shock processing (LSP) on the microstructure, hardness, and residual stress of Hadfield manganese (1 pct C and 14 pct Mn) steels were studied. Laser-shock processing was performed using a Nd: glass phosphate laser with 600 ps pulse width and up to 120 J/pulse energy at power density above 1012 W/cm2. The effects of cold rolling and shot peening were also studied for comparison. Laser-shock processing caused extensive formation of ɛ hexagonal close-packed (hep) martensite (35 vol pct), producing up to a 130 pct increase of surface hardness. The surface hardness increase was 40 to 60 pct for the shot-peened specimen and about 60 pct for the cold-rolled specimen. The LSP strengthening effect on Hadfield steel was attributed to the combined effects of the partial dislocation/stacking fault arrays and the grain refinement due to the presence of the ɛ-hcp martensite. For the cold-rolled and shot-peened specimens, the strengthening was a result of ɛ-hcp martensite and twins with dislocation effects, respectively. Shot peening resulted in a relatively higher compressive residual stress throughout the specimen than LSP.
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Liu, Qiang; Chai, Tianyou; Wang, Hong; Qin, Si-Zhao Joe
2011-12-01
The continuous annealing process line (CAPL) of cold rolling is an important unit to improve the mechanical properties of steel strips in steel making. In continuous annealing processes, strip tension is an important factor, which indicates whether the line operates steadily. Abnormal tension profile distribution along the production line can lead to strip break and roll slippage. Therefore, it is essential to estimate the whole tension profile in order to prevent the occurrence of faults. However, in real annealing processes, only a limited number of strip tension sensors are installed along the machine direction. Since the effects of strip temperature, gas flow, bearing friction, strip inertia, and roll eccentricity can lead to nonlinear tension dynamics, it is difficult to apply the first-principles induced model to estimate the tension profile distribution. In this paper, a novel data-based hybrid tension estimation and fault diagnosis method is proposed to estimate the unmeasured tension between two neighboring rolls. The main model is established by an observer-based method using a limited number of measured tensions, speeds, and currents of each roll, where the tension error compensation model is designed by applying neural networks principal component regression. The corresponding tension fault diagnosis method is designed using the estimated tensions. Finally, the proposed tension estimation and fault diagnosis method was applied to a real CAPL in a steel-making company, demonstrating the effectiveness of the proposed method.
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Research of thread rolling on difficult-to-cut material workpieces
NASA Astrophysics Data System (ADS)
Popov, A. Yu; Bugay, I. A.; Nazarov, P. V.; Evdokimova, O. P.; Popov, P. E.; Vasilyev, E. V.
2018-01-01
In medicine production Ti-6Al-4V Grade 5 alloys are used. One of the most important tasks is to increase the strength of the products and decrease in value. The possibility to roll special thread on Ti-6Al-4V Grade 5 alloy workpiece on 2-roller thread rolling machine has been studied. This is wrought alloy, treatment of which in cold condition causes difficulties due to low plasticity. To obtain Ti-6Al-4V Grade 5 alloy product with thread by rolling is rather difficult. This is due to large axial workpiece displacements resulting from large alloy resistance to cold plastic deformation. The provision of adequate kinematics requires experimental researches and the selection of modes - speed of rolling and pressure on the movable roller. The purpose of the work is to determine the optimal modes for rolling thread on titanium alloy workpiece. It has been stated that, after rolling, the product strength has increased up to 30%. As a result of the work, the unit has been made and recommendations to choose the optimal rolling process modes have been offered.
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Experimental research on micro-pit defects of SUS 430 stainless steel strip in cold rolling process
NASA Astrophysics Data System (ADS)
Li, Changsheng; Li, Miao; Zhu, Tao; Huo, Gang
2013-05-01
In order to improve surface glossiness of stainless steel strip in tandem cold rolling, experimental research on micro-pit defects of SUS 430 ferrite stainless steel was investigated in laboratory. The surface morphology of micro-pit defects was observed by SEM. The effects of micro-pit defects on rolling reduction, roll surface roughness and emulsion parameters were analyzed. With the pass number increasing, the quantity and surface of micro-pit defects were reduced, uneven peak was decreased and gently along rolling direction, micro-pit defects had equally distributed tendency along tranverse direction. The micro-pit defects were increased with the roll surface roughness increase. The defects ratio was declined with larger gradient at pass number 1 to 3, but gentle slope at pass number 4 to 5. The effects of temperature 55° and 63°, concentration 3% and 6% of emulsion on micro-pit effects had not obvious difference. Maintain of micro-pit was effected by rolling oil or air in the micro-pit, the quality of oil was much more than the air in the micro-pit in lubrication rolling.
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NASA Astrophysics Data System (ADS)
Bruemmer, S. M.; Olszta, M. J.; Toloczko, M. B.; Thomas, L. E.
Unidirectional cold rolling has been shown to promote intergranular stress corrosion cracking (IGSCC) in alloy 690 tested in PWR primary water. High-resolution scanning (SEM) and transmission electron microscopy (TEM) have been employed to investigate the microstructural reasons for this enhanced susceptibility in two stages, first examining grain boundary damage produced by cold rolling and second by characterization of stress corrosion crack tips. The degree of permanent grain boundary damage from cold rolling was found to depend directly on the initial IG precipitate distribution. Cold rolling to high levels of reduction was discovered to produce small IG voids and cracked carbides in alloys with a high density of grain boundary carbides. For the same degree of cold rolling, alloys with few IG carbides exhibited much less permanent damage. Although this difference in grain boundary damage appears to correlate with measured SCC growth rates, crack tip examinations reveal no interaction between the preexisting voids and cracked carbides with the propagation. In many cases, these features appeared to blunt propagation of IGSCC cracks. High-resolution characterizations are described for cold-rolled alloy 690 CRDM tubing and plate materials to gain insights into IGSCC mechanisms.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Jana, Saumyadeep; Overman, Nicole; Varga, Tamas
The effect of sub-eutectoid heat treatment on the phase transformation behavior in rolled U-10 wt.percent Mo (U10Mo) foils was systematically investigated. The as-cast 5 mm thick foils were initially homogenized at 900 degrees C for 48 hours and were hot rolled to 2 mm and later cold rolled down to 0.2 mm. Three starting microstructures were evaluated: (i) hot- + cold-rolled to 0.2 mm (as-rolled condition), (ii) hot- + cold-rolled to 0.2 mm + annealed at 700 deg. C for 1 hour, and (iii) hot- + cold-rolled to 0.2 mm + annealed at 1000 deg. C for 60 hours. U10Momore » rolled foils went through various degrees of decomposition when subjected to the sub-eutectoid heat-treatment step and formed a lamellar microstructure through a cellular reaction mostly along the previous γ-UMo grain boundaries.« less
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40 CFR 420.101 - Specialized definitions.
Code of Federal Regulations, 2011 CFR
2011-07-01
... AND STANDARDS IRON AND STEEL MANUFACTURING POINT SOURCE CATEGORY Cold Forming Subcategory § 420.101 Specialized definitions. (a) The term recirculation means those cold rolling operations which include recirculation of rolling solutions at all mill stands. (b) The term combination means those cold rolling...
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40 CFR 420.101 - Specialized definitions.
Code of Federal Regulations, 2014 CFR
2014-07-01
... AND STANDARDS IRON AND STEEL MANUFACTURING POINT SOURCE CATEGORY Cold Forming Subcategory § 420.101 Specialized definitions. (a) The term recirculation means those cold rolling operations which include recirculation of rolling solutions at all mill stands. (b) The term combination means those cold rolling...
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40 CFR 420.101 - Specialized definitions.
Code of Federal Regulations, 2012 CFR
2012-07-01
... AND STANDARDS IRON AND STEEL MANUFACTURING POINT SOURCE CATEGORY Cold Forming Subcategory § 420.101 Specialized definitions. (a) The term recirculation means those cold rolling operations which include recirculation of rolling solutions at all mill stands. (b) The term combination means those cold rolling...
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40 CFR 420.101 - Specialized definitions.
Code of Federal Regulations, 2013 CFR
2013-07-01
... AND STANDARDS IRON AND STEEL MANUFACTURING POINT SOURCE CATEGORY Cold Forming Subcategory § 420.101 Specialized definitions. (a) The term recirculation means those cold rolling operations which include recirculation of rolling solutions at all mill stands. (b) The term combination means those cold rolling...
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Thomas, G.; Ahn, J.H.; Kim, N.J.
1986-10-28
An improved, energy efficient, hot rolling method for direct production of cold formable dual-phase steel is provided. The steel is heated to completely austenitize it and then continuously hot rolled and cooled down into the ferrite-austenite two phase region to a temperature which is just below the effective Ar[sub 3] temperature. The hot rolled steel is then rapidly quenched to provide an alloy containing strong, tough lath martensite (fibers) in a ductile soft ferrite matrix. The method is particularly useful for providing rods in which form the alloy is capable of being drawn into high strength wire or the like in a cold drawing operation without any intermediate annealing or patenting, and has excellent strength, ductility and fatigue characteristics. 3 figs.
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Thomas, Gareth; Ahn, Jae-Hwan; Kim, Nack-Joon
1986-01-01
An improved, energy efficient, hot rolling method for direct production of cold formable dual-phase steel is provided. The steel is heated to completely austenitize it and then continuously hot rolled and cooled down into the ferrite-austenite two phase region to a temperature which is just below the effective Ar.sub.3 temperature. The hot rolled steel is then rapidly quenched to provide an alloy containing strong, tough lath martensite (fibers) in a ductile soft ferrite matrix. The method is particularly useful for providing rods in which form the alloy is capable of being drawn into high strength wire or the like in a cold drawing operation without any intermediate annealing or patenting, and has excellent strength, ductility and fatigue characteristics.
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The rolling performance of Fe-6.5 wt.% Si sheets edged with stainless steel
NASA Astrophysics Data System (ADS)
Zhang, B.; Ye, F.; Liang, Y. F.; Shi, X. J.; Lin, J. P.
2017-10-01
Compared with common electrical steel, high silicon electrical steel (Fe-6.5 wt.% Si alloy) exhibits excellent soft magnetic properties and a wide application prospect in high frequency electromagnetic fields. In the process of cold rolling Fe-6.5 wt.% Si alloy, edge-crack often occurs on the sheets due to the inadequate ductility and limited formability. It was found that the Fe-6.5 wt.% Si alloy sheet edged with 304 stainless steel by laser welding show an improved rolling performance. The composite sheet could be cold rolled to a thickness of 0.07 mm without observed edge cracks. The mechanical property of the edging material should be in an appropriate window in reference to that of the Fe-6.5 wt.% Si alloy.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Choi, Gwnaghyo; Lee, Kwangmin, E-mail: kmlee@jnu.a
A Ti–6Mo–6V–5Cr–3Sn–2.5Zr (wt.%) alloy was designed as a new metastable β-Ti alloy. The effect that cold rolling had on the microstructural evolution of the material was investigated via optical microscopy (OM), X-ray diffraction (XRD), electron back-scattered diffraction (EBSD) and transmission electron microscopy (TEM) measurements. A single β phase formed in the alloy after solution treatment at 780 °C for 30 min followed by water quenching. The solution-treated alloy was cold rolled with thickness reductions of 10%, 30%, 50% and 70%, and the hardness values increased as the thickness of the specimen decreased. The textures of the cold rolled specimen weremore » characterized according to the 〈110〉 partial parallel to the rolling direction as the rolling reduction increased. The crystallographic orientation showed principal α-fiber textures for (111)〈110〉 and (112)〈110〉. The cold deformation led to the appearance of martensite α″ phases, particularly stress-induced martensite (SIM) α″ phases. - Highlights: • Effect of cold rolling on new β-typed Ti-6Mo-6V-5Cr-3Sn-2.5Zr alloy was studied. • A single β phase was obtained after solution treatment at 780 °C for 30 min. • α-Fiber textures became dominated with the increase in cold rolling reduction. • A stress-induced α″ martensite was caused by cold rolling.« less
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78 FR 32471 - Amended Revised Determination on Reconsideration
Federal Register 2010, 2011, 2012, 2013, 2014
2013-05-30
..., including workers whose unemployment insurance (UI) wages are reported through Ohio cold rolling company... reported through Ohio cold rolling company Yorkville, Ohio [TA-W-71,572B] Severstal Wheeling, Inc., A... whose unemployment insurance (UI) wages are reported through Ohio cold rolling company Mingo Junction...
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Annealing of (DU-10Mo)-Zr Co-Rolled Foils
DOE Office of Scientific and Technical Information (OSTI.GOV)
Pacheco, Robin Montoya; Alexander, David John; Mccabe, Rodney James
2017-01-20
Producing uranium-10wt% molybdenum (DU-10Mo) foils to clad with Al first requires initial bonding of the DU-10Mo foil to zirconium (Zr) by hot rolling, followed by cold rolling to final thickness. Rolling often produces wavy (DU-10Mo)-Zr foils that should be flattened before further processing, as any distortions could affect the final alignment and bonding of the Al cladding to the Zr co-rolled surface layer; this bonding is achieved by a hot isostatic pressing (HIP) process. Distortions in the (DU-10Mo)-Zr foil may cause the fuel foil to press against the Al cladding and thus create thinner or thicker areas in the Almore » cladding layer during the HIP cycle. Post machining is difficult and risky at this stage in the process since there is a chance of hitting the DU-10Mo. Therefore, it is very important to establish a process to flatten and remove any waviness. This study was conducted to determine if a simple annealing treatment could flatten wavy foils. Using the same starting material (i.e. DU-10Mo coupons of the same thickness), five different levels of hot rolling and cold rolling, combined with five different annealing treatments, were performed to determine the effect of these processing variables on flatness, bonding of layers, annealing response, microstructure, and hardness. The same final thickness was reached in all cases. Micrographs, textures, and hardness measurements were obtained for the various processing combinations. Based on these results, it was concluded that annealing at 650°C or higher is an effective treatment to appreciably reduce foil waviness.« less
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NASA Astrophysics Data System (ADS)
Ghasemi-Nanesa, H.; Nili-Ahmadabadi, M.; Shirazi, H.
2010-07-01
Fe-Ni-Mn martensitic steels are one of the major groups of ultra-high strength steels that have good mechanical properties and ductility in as annealed condition but they suffer from severe inter-granular embitterment after aging. In this paper, the effect of heavy shaped cold rolling and wire drawing on the mechanical properties of Fe-Ni-Mn steel was investigated. This process could provide a large strain deformation in this alloy. The total strain was epsilon ~7. Aging behavior and tensile properties of Fe-10Ni-7Mn were studied after aging at 753 K. The results showed that the ultimate tensile strength and ductility after cold rolling, wire drawing and aging increased up to 2540 MPa and 7.1 %, respectively, while the conventional steels show a premature fracture stress of 830 MPa with about zero ductility after aging.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Bruemmer, Stephen M.; Olszta, Matthew J.; Toloczko, Mychailo B.
2012-10-01
Grain boundary microstructures and microchemistries are examined in cold-rolled alloy 690 tubing and plate materials and comparisons are made to intergranular stress corrosion cracking (IGSCC) behavior in PWR primary water. Chromium carbide precipitation is found to be a key aspect for materials in both the mill annealed and thermally treated conditions. Cold rolling to high levels of reduction was discovered to produce small IG voids and cracked carbides in alloys with a high density of grain boundary carbides. The degree of permanent grain boundary damage from cold rolling was found to depend directly on the initial IG carbide distribution. Formore » the same degree of cold rolling, alloys with few IG precipitates exhibited much less permanent damage. Although this difference in grain boundary damage appears to correlate with measured SCC growth rates, crack tip examinations reveal that cracked carbides appeared to blunt propagation of IGSCC cracks in many cases. Preliminary results suggest that the localized grain boundary strains and stresses produced during cold rolling promote IGSCC susceptibility and not the cracked carbides and voids.« less
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NASA Astrophysics Data System (ADS)
Elramady, Alyaa Gamal
The aim of this research project is to correlate the plastic deformation and mechanical instability of casing steel materials with corrosion behavior and surface change, in order to identify a tolerable degree of deformation for casing steel materials. While the corrosion of pipeline and casing steels has been investigated extensively, corrosion of these steels in sweet environments with respect to plastic deformation due to bending, rolling, autofrettage, or handling needs more investigation. Downhole tubular expansion of pipes (casings) is becoming standard practice in the petroleum industry to repair damaged casings, shutdown perforations, and ultimately achieve mono-diameter wells. Tubular expansion is a cold-drawing metal forming process, which consists of running conical mandrels through casings either mechanically using a piston or hydraulically by applying a back pressure. This mechanism subjects the pipes to large radial plastic deformations of up to 30 pct. of the inner diameter. It is known that cold-working is a way of strengthening materials such as low carbon steel, but given that this material will be subjected to corrosive environments, susceptibility to stress corrosion cracking (SCC) should be investigated. This research studies the effect of cold-work, in the form of cold-rolling and cold-expansion, on the surface behavior of API 5CT steels when it is exposed to a CO2-containing environment. Cold-work has a pronounced influence on the corrosion behavior of both API 5CT K55 and P110 grade steels. The lowest strength grade steel, API 5CT K55, performed poorly in a corrosive environment in the slow strain rate test. The ductile material exhibited the highest loss in strength and highest susceptibility to stress corrosion cracking in a CO 2-containing environment. The loss in strength declined with cold-rolling, which can be ascribed to the surface compressive stresses induced by cold-work. On the other hand, API 5CT P110 grade steels showed higher susceptibility to SCC when they were cold-rolled and cold-expanded. The research found that surface compressive stresses have an effect on the SCC behavior of casing and tubing steels. The CO2 corrosion behavior and atomic processes at the corroding interface were investigated at laboratory temperature using electrochemical techniques. Cold-work was found to have an influence on the corrosion behavior of both API 5CT K55 and P110 grade steels. These behaviors were found to be material and process dependent. Surface evaluation techniques such as field emission scanning electron microscope (FE-SEM) and X-ray diffraction (XRD) analysis did not detect formation of a protective scale. X-ray diffraction and X-ray photoelectron spectroscopy (XPS) analysis both detected the appearance of a scale that was traced back to magnetite.
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In Situ XRD Studies of the Process Dynamics During Annealing in Cold-Rolled Copper
NASA Astrophysics Data System (ADS)
Dey, Santu; Gayathri, N.; Bhattacharya, M.; Mukherjee, P.
2016-12-01
The dynamics of the release of stored energy during annealing along two different crystallographic planes, i.e., {111} and {220}, in deformed copper have been investigated using in situ X-ray diffraction measurements at 458 K and 473 K (185 °C and 200 °C). The study has been carried out on 50 and 80 pct cold-rolled Cu sheets. The microstructures of the rolled samples have been characterized using optical microscopy and electron backscattered diffraction measurements. The microstructural parameters were evaluated from the X-ray diffractogram using the Scherrer equation and the modified Rietveld method. The stored energy along different planes was determined using the modified Stibitz formula from the X-ray peak broadening, and the bulk stored energy was evaluated using differential scanning calorimetry. The process dynamics of recovery and recrystallization as observed through the release of stored energy have been modeled as the second-order and first-order processes, respectively.
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Comparative Mechanical Improvement of Stainless Steel 304 Through Three Methods
NASA Astrophysics Data System (ADS)
Mubarok, N.; Notonegoro, H. A.; Thosin, K. A. Z.
2018-05-01
Stainless Steel 304 (SS304) is one of stainless steel group widely used in industries for various purposes. In this paper, we compared the experimental process to enhance the mechanical properties of the surface SS304 through three different methods, cold rolled, annealed salt baht bronzing (ASB), and annealed salt baht boronizing-quench (ASB-Q). The phase change in SS304 due to the cold rolled process makes this method is to abandon. The increasing of the annealing time in the ASB method has a nonlinear relationship with the increases in hardness value. Comparing to the increases in hardness value of the ASB method, the hardness value of ASB-Q methods is still lower than that method.
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Ultrafine-grained titanium for medical implants
Zhu, Yuntian T.; Lowe, Terry C.; Valiev, Ruslan Z.; Stolyarov, Vladimir V.; Latysh, Vladimir V.; Raab, Georgy J.
2002-01-01
We disclose ultrafine-grained titanium. A coarse-grained titanium billet is subjected to multiple extrusions through a preheated equal channel angular extrusion (ECAE) die, with billet rotation between subsequent extrusions. The resulting billet is cold processed by cold rolling and/or cold extrusion, with optional annealing. The resulting ultrafine-grained titanium has greatly improved mechanical properties and is used to make medical implants.
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NASA Astrophysics Data System (ADS)
Babacan, N.; Ma, J.; Turkbas, O. S.; Karaman, I.; Kockar, B.
2018-01-01
In the present study, the effect of thermo-mechanical treatments on the shape memory and the superelastic characteristics of Cu73Al16Mn11 (at%) shape memory alloy were investigated. 10%, 50% and 70% cold rolling and subsequent heat treatment processes were conducted to achieve strengthening via grain size refinement. 70% grain size reduction compared to the homogenized condition was obtained using 70% cold rolling and subsequent recrystallization heat treatment technique. Moreover, 10% cold rolling was applied to homogenized specimen to reveal the influence of the low percentage cold rolling reduction with no heat treatment on shape memory properties of Cu73Al16Mn11 (at%) alloy. Stress free transformation temperatures, monotonic tension and superelasticity behaviors of these samples were compared with those of the as-aged sample. Isobaric heating-cooling experiments were also conducted to see the dimensional stability of the samples as a function of applied stress. The 70% grain-refined sample exhibited better dimensional stability showing reduced residual strain levels upon thermal cycling under constant stress compared with the as-aged material. However, no improvement was achieved with grain size reduction in the superelasticity experiments. This distinctive observation was attributed to the difference in the magnitude of the stress levels achieved during two different types of experiments which were the isobaric heating-cooling and superelasticity tests. Intergranular fracture due to the stress concentration overcame the strengthening effect via grain refinement in the superelasticity tests at higher stress values. On the other hand, the strength of the material and resistance of material against plastic deformation upon phase transformation were increased as a result of the grain refinement at lower stress values in the isobaric heating-cooling experiments.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Liu, Hai-Tao, E-mail: liuht@ral.neu.edu.cn; Institute of Research of Iron and Steel, Shasteel, Zhangjiagang 215625, Jiangsu; Yao, Sheng-Jie
2015-08-15
In the present work, a regular grade GO sheet was produced successively by strip casting, hot rolling, normalizing annealing, two-stage cold rolling with intermediate annealing, primary recrystallization annealing, secondary recrystallization annealing and purification. The aim of this paper was to characterize the evolution of microstructure, texture and inhibitor along the new processing route by comprehensive utilization of optical microscopy, X-ray diffraction and transmission electron microscopy. It was found that a fine microstructure with the ferrite grain size range of 7–12 μm could be obtained in the primary recrystallization annealed sheet though a very coarse microstructure was produced in the initialmore » as-cast strip. The main finding was that the “texture memory” effect on Goss texture started on the through-thickness intermediate annealed strip after first cold rolling, which was not similar to the “texture memory” effect on Goss texture starting on the surface layers of the hot rolled strip in the conventional production route. As a result, the origin of Goss nuclei capable of secondary recrystallization lied in the grains already presented in Goss orientation in the intermediate annealed strip after first cold rolling. Another finding was that fine and dispersive inhibitors (mainly AlN) were easy to be produced in the primary recrystallization microstructure due to the initial rapid solidification during strip casting and the subsequent rapid cooling, and the very high temperature reheating usually used before hot rolling in the conventional production route could be avoided. - Highlights: • A regular grade grain-oriented electrical steel was produced. • Evolution of microstructure, texture and inhibitor was characterized. • Origin of Goss nuclei lied in the intermediate annealed strip. • A fine primary recrystallization microstructure could be produced. • Effective inhibitors were easy to be obtained in the new processing route.« less
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NASA Astrophysics Data System (ADS)
Seyfpour, M.; Ghanei, S.; Mazinani, M.; Kashefi, M.; Davis, C.
2018-04-01
The recovery process in steel is usually investigated by conventional destructive tests that are expensive, time-consuming and also cumbersome. In this study, an alternative non-destructive test technique (based on eddy current testing) is used to characterise the recovery process during annealing of cold-rolled low-carbon steels. For assessing the reliability of eddy current results corresponding to different levels of recovery, X-ray line broadening analysis is also employed. It is shown that there is a strong relationship between eddy current outputs and the extent to which recovery occurs at different annealing temperatures. Accordingly, the non-destructive eddy current test technique represents the potential to be used as a reliable process for detection of the occurrence of recovery in the steel microstructure.
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NASA Astrophysics Data System (ADS)
Lu, Cheng-zhuang; Li, Jing-yuan; Fang, Zhi
2018-02-01
In ferritic stainless steels, a significant non-uniform recrystallization orientation and a substantial texture gradient usually occur, which can degrade the ridging resistance of the final sheets. To improve the homogeneity of the recrystallization orientation and reduce the texture gradient in ultra-purified 17%Cr ferritic stainless steel, in this work, we performed conventional and asymmetric rolling processes and conducted macro and micro-texture analyses to investigate texture evolution under different cold-rolling conditions. In the conventional rolling specimens, we observed that the deformation was not uniform in the thickness direction, whereas there was homogeneous shear deformation in the asymmetric rolling specimens as well as the formation of uniform recrystallized grains and random orientation grains in the final annealing sheets. As such, the ridging resistance of the final sheets was significantly improved by employing the asymmetric rolling process. This result indicates with certainty that the texture gradient and orientation inhomogeneity can be attributed to non-uniform deformation, whereas the uniform orientation gradient in the thickness direction is explained by the increased number of shear bands obtained in the asymmetric rolling process.
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NASA Astrophysics Data System (ADS)
Naghizadeh, Meysam; Mirzadeh, Hamed
2018-05-01
An advanced thermomechanical process based on the formation and reversion of deformation-induced martensite was used to refine the grain size and enhance the hardness of an AISI 304L austenitic stainless steel. Both low and high reversion annealing temperatures and also the repetition of the whole thermomechanical cycle were considered. While a microstructure with average austenite grain size of a few micrometers was achieved based on cold rolling and high-temperature short-term annealing, an extreme grain refinement up to submicrometer regime was obtained by cold rolling followed by low-temperature long-term annealing. However, the required annealing time was found to be much longer, which negates its appropriateness for industrial production. While a magnificent grain refinement was achieved by one pass of the high-temperature thermomechanical process, the reduction in grain size was negligible by the repetition of the whole cycle. It was found that the hardness of the thermomechanically processed material is much higher than that of the as-received material. The results of the present work were shown to be compatible with the general trend of grain size dependence of hardness for AISI 304L stainless steel based on the Hall-Petch relationship. The results were also discussed based on the X-ray evaluation of dislocation density by modified Williamson-Hall plots.
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Cold rolled Fe-6.5 wt. % Si alloy foils with high magnetic induction
NASA Astrophysics Data System (ADS)
Fang, X. S.; Liang, Y. F.; Ye, F.; Lin, J. P.
2012-05-01
Fe-6.5 wt. % Si alloy foils with 95 mm in width and 0.30 mm in thickness were successfully fabricated by cold rolling process. Excellent magnetic properties (Hc = 20.4 A/m, µm = 22 200, and Bs = 1.69 T) were obtained after annealing at the temperature of 1273 K for 1.5 h. This high magnetic induction is considered to be due to the formation of {hk0}<001> textures. Cut cores from this material have a very low iron loss at frequencies from 400 Hz to 10 kHz.
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NASA Astrophysics Data System (ADS)
Miura, H.; Kobayashi, T.; Kobayashi, M.
2014-08-01
Cu-18.2Zn-1.5Si-0.25Fe (mass%) alloy was heavily cold rolled. Ultrafine grained (UFGed) structure, containing a mixture of lamellar and mechanical twins, was easily and homogeneously formed. The average grain size was approximately 100 nm. The as-rolled sample showed quite high ultimate tensile strength (UTS) over 1 GPa. The UTS was higher than those obtained by multi directional forging. When the samples were annealed at relatively low temperatures between 553 K and 653 K, they showed slight hardening followed by large softening due to occurrence of static recrystallization (SRX). Annealing of UFGed structure at relatively low temperature of around 0.4 Tm caused extensive SRX that, in turn, induces ultrafine RXed grained structure. The grain size of the RXed sample was as fine as 200 nm. Although the annealing induced recovery of ductility while UTS gradually reduces, UTS over 1 GPa with ductility of 15 % were attained. The RXed grains mainly contained ultrafine annealing twins. Therefore, UFGed structure and superior mechanical properties could be achieved by a simple process of cold rolling, i.e., without severe plastic deformation.
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NASA Astrophysics Data System (ADS)
Chen, S.; Butler, J.; Melzer, S.
2014-11-01
In this study, both asymmetric hot rolling (AHR) and conventional hot rolling (CHR) were carried out to study the effect of the hot rolling conditions on the evolution of the texture and microstructure in a non-grain oriented (NGO) steel. The microstructure and texture in the subsequent processing stages were characterised and related to the final magnetic properties. The results show that AHR, compared with CHR, tends to homogenise texture through thickness of the hot band strips. AHR results in a higher fraction of the θ-fibre ({0 0 1}) and a lower fraction of the γ-fibre ({1 1 1}) in the hot band strips, which are favourable features in relation to the magnetic properties of the strip. However, the favourable features observed in hot rolled AHR strips are eliminated after cold rolling and annealing. Contrarily, the required θ-fibre is decreased and the unwanted γ-fibre is intensified in the AHR sheet after cold rolling and their strength is maintained in the subsequent process steps. On the other hand, AHR does not produce a discernible change in the grain size in the hot band annealed strip and in the final annealed sheet, except that the magnetic anisotropy in the AHR is improved after skin pass and extra annealing as the result of the redistribution of the texture components within the θ-fibre, no significant improvement of the magnetic properties as a direct consequence of the application of asymmetric hot rolling has been observed under the current AHR experimental conditions.
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Method of manufacturing metallic products such as sheet by cold working and flash anealing
Hajaligol, Mohammad R.; Sikka, Vinod K.
2001-01-01
A metallic alloy composition is manufactured into products such as press formed or stamped products or rolled products such as sheet, strip, rod, wire or band by one or more cold working steps with intermediate or final flash annealing. The method can include cold rolling an iron, nickel or titanium aluminide alloy and annealing the cold worked product in a furnace by infrared heating. The flash annealing is preferably carried out by rapidly heating the cold worked product to an elevated temperature for less than one minute. The flash annealing is effective to reduce surface hardness of the cold worked product sufficiently to allow further cold working. The product to be cold worked can be prepared by casting the alloy or by a powder metallurgical technique such as tape casting a mixture of metal powder and a binder, roll compacting a mixture of the powder and a binder or plasma spraying the powder onto a substrate. In the case of tape casting or roll compaction, the initial powder product can be heated to a temperature sufficient to remove volatile components. The method can be used to form a cold rolled sheet which is formed into an electrical resistance heating element capable of heating to 900.degree. C. in less than 1 second when a voltage up to 10 volts and up to 6 amps is passed through the heating element.
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Method of manufacturing metallic products such as sheet by cold working and flash annealing
Hajaligol, Mohammad R.; Sikka, Vinod K.
2000-01-01
A metallic alloy composition is manufactured into products such as press formed or stamped products or rolled products such as sheet, strip, rod, wire or band by one or more cold working steps with intermediate or final flash annealing. The method can include cold rolling an iron, nickel or titanium aluminide alloy and annealing the cold worked product in a furnace by infrared heating. The flash annealing is preferably carried out by rapidly heating the cold worked product to an elevated temperature for less than one minute. The flash annealing is effective to reduce surface hardness of the cold worked product sufficiently to allow further cold working. The product to be cold worked can be prepared by casting the alloy or by a powder metallurgical technique such as tape casting a mixture of metal powder and a binder, roll compacting a mixture of the powder and a binder or plasma spraying the powder onto a substrate. In the case of tape casting or roll compaction, the initial powder product can be heated to a temperature sufficient to remove volatile components. The method can be used to form a cold rolled sheet which is formed into an electrical resistance heating element capable of heating to 900.degree. C. in less than 1 second when a voltage up to 10 volts and up to 6 amps is passed through the heating element.
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Code of Federal Regulations, 2014 CFR
2014-07-01
... cold rolling wastewaters. 2 Within the range of 6.0 to 9.0. (2) Bar, billet and bloom. Subpart I... treated with cold rolling wastewaters. 2 Within the range of 6.0 to 9.0. (3) Strip, sheet and plate... are treated with cold rolling wastewaters. 2 Within the range of 6.0 to 9.0. (4) Pipe, tube and other...
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NASA Astrophysics Data System (ADS)
Garber, E. A.; Diligenskii, E. V.; Antonov, P. V.; Shalaevskii, D. L.; Dyatlov, I. A.
2017-09-01
The factors of the process of production of cold-rolled steel strips that promote and hinder the appearance of a coil lap welding defect upon annealing in bell-type furnaces are analyzed using statistical methods. The works dealing with this problem are analytically reviewed to reveal the problems to be studied and refined. The ranking of the technological factors according to the significance of their influence on the probability of appearance of this defect is determined and supported by industrial data, and a regression equation is derived to calculate this probability. The process of production is improved to minimize the rejection of strips caused by the welding of coil laps.
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CRACK GROWTH RESPONSE OF ALLOY 690 IN SIMULATED PWR PRIMARY WATER
DOE Office of Scientific and Technical Information (OSTI.GOV)
Toloczko, Mychailo B.; Bruemmer, Stephen M.
2009-12-01
The stress corrosion crack growth response of three extruded alloy 690 CRDM tube heats was investigated in several thermomechanical conditions. Extremely low propagation rates (< 1 x 10{sup -9} mm/s) were observed under constant stress intensity factor (K) loading at 325-350 C in the as-received, thermally treated (TT) materials despite using a variety of transitioning techniques. Post-test observation of the crack-growth surfaces revealed only isolated intergranular (IG) cracking. One-dimensional cold rolling to 17% reduction and testing in the S-L orientation did not promote enhanced stress corrosion rates. However, somewhat higher propagation rates were observed in a 30% cold-rolled alloy 690TTmore » specimen tested in the T-L orientation. Cracking of the cold-rolled material was promoted on grain boundaries oriented parallel to the rolling plane with the % IG increasing with the amount of cold rolling.« less
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Nezakat, Majid, E-mail: majid.nezakat@usask.ca
We studied the texture evolution of thermo-mechanically processed austenitic stainless steel 310S. This alloy was cold rolled up to 90% reduction in thickness and subsequently annealed at 1050 °C. At the early stages of deformation, strain-induced martensite was formed from deformed austenite. By increasing the deformation level, slip mechanism was found to be insufficient to accommodate higher deformation strains. Our results demonstrated that twinning is the dominant deformation mechanism at higher deformation levels. Results also showed that cold rolling in unidirectional and cross rolling modes results in Goss/Brass and Brass dominant textures in deformed samples, respectively. Similar texture components aremore » observed after annealing. Thus, the annealing texture was greatly affected by texture of the deformed parent phase and martensite did not contribute as it showed an athermal reversion during annealing. Results also showed that when the fraction of martensite exceeds a critical point, its grain boundaries impeded the movement of austenite grain boundaries during annealing. As a result, recrystallization incubation time would increase. This caused an incomplete recrystallization of highly deformed samples, which led to a rational drop in the intensity of the texture components. - Highlights: •Thermo-mechanical processing through different cold rolling modes can induce different textures. •Martensite reversion is athermal during annealing. •Higher fraction of deformation-induced martensite can increase the annealing time required for complete recrystallization. •Annealing texture is mainly influenced by the deformation texture of austenite.« less
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NASA Astrophysics Data System (ADS)
Zheng, Yanwen; Zhang, Zhihao; Jiang, Yanbin
2018-04-01
The Ga liquid and Al powder were mechanically mixed and poured into a hollow iron plate, after alloying, the composite plate was rolled at room temperature for preparing an Fe/Ga-Al composite strip. The effect of annealing conditions on the diffusion, microstructures and magnetostrictive properties of the strip were studied. The composite plate had good cold rolling formability. After annealing at 750-850 °C for 5 h of the cold-rolled sample with a reduction of 97%, the diffusion distance of Ga and Al in the Fe matrix increased with an increase of the annealing temperature. However, some holes appeared in the center of the sample annealed at a temperature of more than 830 °C, which was detrimental to the subsequent rolling. The combination of the secondary cold rolling and annealing was beneficial to improve the composition homogeneity and magnetic properties of the sample. The magnetostriction coefficient (λ//) of the primary rolled sample was low, ∼4 × 10-6. After annealing and secondary cold rolling, the λ// of the sample increased to 9 × 10-6 and the λ// of the sample conducted by further annealing at 820 °C for 20 h reached 27.5 × 10-6.
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NASA Astrophysics Data System (ADS)
Ashiq, Mohammad; Dhekne, Pushkar; Hamada, Atef Saad; Sahu, Puspendu; Mahato, B.; Minz, R. K.; Ghosh Chowdhury, Sandip; Pentti Karjalainen, L.
2017-10-01
The evolution of microstructure and texture of a two-phase austenite-ferrite twinning-induced plasticity steel during cold rolling was investigated and different deformation mechanisms were found to become active with increasing thickness reductions. Optical microscopy showed the formation of brass-type shear bands across several austenite grains at reductions greater than 50 pct. TEM observations reveal the presence of deformation twinning in austenite. The austenite phase initially shows the Cu-type texture, i.e., Cu {1 1 2}〈1 1 1〉, Goss {0 1 1}〈1 0 0〉 with a spread toward Brass {1 1 0}〈1 1 2〉. With continued cold rolling, the Cu {1 1 2}〈1 1 1〉 component moves toward CuT component {552}〈115〉 and the other two components increase in intensity. There is also emergence of {111} fiber after 90 pct cold rolling. The ferrite phase exhibits the evolution of ND-rotated Cube component {001}〈110〉 along with 〈110〉 fiber at lower as well as at higher rolling reductions. An exception is at 75 pct reduction, when the ferrite texture contains {111} fiber in place of 〈110〉 fiber with a weak rotated-Cube component. Phase fraction analysis by X-ray diffraction indicates a decrease in the austenite fraction up to 75 pct reduction followed by an increase at 90 pct reduction. After 90 pct cold rolling, the phase fraction is similar to that of the "as-received" state. Elongated grains of ferrite phase in finer dimensions after 90 pct cold rolling indicate softening within that phase; at similar stage, there are finer scale austenite grains mostly at the grain boundaries. The above has been suggested to be related with the adiabatic heating during cold rolling due to the high strain hardening of the austenite phase.
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Method of fabricating a uranium-bearing foil
Gooch, Jackie G [Seymour, TN; DeMint, Amy L [Kingston, TN
2012-04-24
Methods of fabricating a uranium-bearing foil are described. The foil may be substantially pure uranium, or may be a uranium alloy such as a uranium-molybdenum alloy. The method typically includes a series of hot rolling operations on a cast plate material to form a thin sheet. These hot rolling operations are typically performed using a process where each pass reduces the thickness of the plate by a substantially constant percentage. The sheet is typically then annealed and then cooled. The process typically concludes with a series of cold rolling passes where each pass reduces the thickness of the plate by a substantially constant thickness amount to form the foil.
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NASA Astrophysics Data System (ADS)
Wang, Yin-Ping; Liu, Hai-Tao; Song, Hong-Yu; Liu, Jia-Xin; Shen, Hui-Ying; Jin, Yang; Wang, Guo-Dong
2018-04-01
0.05-0.15 mm-thick ultra-thin grain-oriented silicon steel sheets were successfully produced by a novel processing route including strip casting, hot rolling, normalizing, two-stage cold rolling with intermediate annealing, primary recrystallization annealing and secondary recrystallization annealing. The evolutions of microstructure, texture and inhibitor along the processing were briefly investigated. The results showed that the initial Goss orientation originated due to the heterogenous nucleation of δ-ferrite grains during solidification. Because of the lack of shear deformation, only a few Goss grains were observed in the hot rolled sheet. After the first cold rolling and intermediate annealing, Goss texture was enhanced and distributed in the whole thickness. A small number of Goss grains having a high fraction of high energy boundaries exhibited in the primary recrystallization annealed sheet. A large number of fine and dispersed MnS and AlN and a few co-precipitates MnS and AlN with the size range of 10-70 nm were also observed. Interestingly, a well-developed secondary recrystallization microstructure characterized by 10-60 mm grains and a sharp Goss texture were finally produced in the 0.05-0.15 mm-thick ultra-thin sheets. A magnetic induction B8 of 1.72-1.84 T was obtained. Another new finding was that a few {2 3 0}〈0 0 1〉 and {2 1 0}〈1 2 7〉 grains also can grow up abnormally because of the high fraction of high energy boundaries and the size and number advantage, respectively. These non-Goss grains finally deteriorated the magnetic properties of the ultra-thin sheets. In addition, low surface energies of {hk0} planes may also contribute to the abnormal growth of Goss, {2 3 0}〈0 0 1〉 and {2 1 0}〈1 2 7〉 grains.
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NASA Astrophysics Data System (ADS)
Mazaheri, Y.; Kermanpur, A.; Najafizadeh, A.
2015-07-01
A dual phase (DP) steel was produced by a new process utilizing an uncommon cold-rolling and subsequent intercritical annealing of a martensite-ferrite duplex starting structure. Ultrafine grained DP steels with an average grain size of about 2 μm and chain-networked martensite islands were achieved by short intercritical annealing of the 80 pct cold-rolled duplex microstructure. The strength of the low carbon steel with the new DP microstructure was reached about 1300 MPa (140 pct higher than that of the as-received state, e.g., 540 MPa), without loss of ductility. Tensile testing revealed good strength-elongation balance for the new DP steels (UTS × UE ≈ 11,000 to 15,000 MPa pct) in comparison with the previous works and commercially used high strength DP steels. Two strain hardening stages with comparable exponents were observed in the Holloman analysis of all DP steels. The variations of hardness, strength, elongation, and strain hardening behavior of the specimens with thermomechanical parameters were correlated to microstructural features.
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NASA Astrophysics Data System (ADS)
Overhagen, Christian; Mauk, Paul Josef
2018-05-01
For flat rolled products, the thickness profile in the transversal direction is one of the most important product properties. For further processing, a defined crown of the product is necessary. In the rolling process, several mechanical and thermal influences interact with each other to form the strip shape at the roll gap exit. In the present analysis, a process model for rolling of strip and sheet is presented. The core feature of the process model is a two-dimensional stress distribution model based on von Karman's differential equation. Sub models for the mechanical influences of work roll flattening as well as work and backup roll deflection and the thermal influence of work roll expansion have been developed or extended. The two-dimensional stress distribution serves as an input parameter for the roll deformation models. For work roll flattening, a three-dimensional model based on the Boussinesq problem is adopted, while the work and backup roll deflection, including contact flattening is calculated by means of finite beam elements. The thermal work roll crown is calculated with help of an axisymmetric numerical solution of the heat equation for the work roll, considering azimuthal averaging for the boundary conditions at the work roll surface. Results are presented for hot rolling of a strip in a seven-stand finishing train of a hot strip mill, showing the calculated evolution of the strip profile. A variation of the strip profile from the first to the 20th rolled strip is shown. This variation is addressed to the progressive increase of work roll temperature during the first 20 strips. It is shown that a CVC® system can lead to improvements in strip profile and therefore flatness.
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Analysis of factors influencing the bond strength in roll bonding processes
NASA Astrophysics Data System (ADS)
Khaledi, Kavan; Wulfinghoff, Stephan; Reese, Stefanie
2018-05-01
Cold Roll Bonding (CRB) is recognized as an industrial technique in which the metal sheets are joined together in order to produce laminate metal composites. In this technique, a metallurgical bond resulting from severe plastic deformation is formed between the rolled metallic layers. The main objective of this paper is to analyse different factors which may affect the bond formation in rolling processes. To achieve this goal, first, an interface model is employed which describes both the bonding and debonding. In this model, the bond strength evolution between the metallic layers is calculated based on the film theory of bonding. On the other hand, the debonding process is modelled by means of a bilinear cohesive zone model. In the numerical section, different scenarios are taken into account to model the roll bonding process of metal sheets. The numerical simulation includes the modelling of joining during the roll bonding process followed by debonding in a Double Cantilever Beam (DCB) peeling test. In all simulations, the metallic layers are regarded as elastoplastic materials subjected to large plastic deformations. Finally, the effects of some important factors on the bond formation are numerically investigated.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Soulami, Ayoub; Lavender, Curt A.; Paxton, Dean M.
2015-06-15
Pacific Northwest National Laboratory (PNNL) has been investigating manufacturing processes for the uranium-10% molybdenum alloy plate-type fuel for high-performance research reactors in the United States. This work supports the U.S. Department of Energy National Nuclear Security Administration’s Office of Material Management and Minimization Reactor Conversion Program. This report documents modeling results of PNNL’s efforts to perform finite-element simulations to predict roll-separating forces for various rolling mill geometries for PNNL, Babcock & Wilcox Co., Y-12 National Security Complex, Los Alamos National Laboratory, and Idaho National Laboratory. The model developed and presented in a previous report has been subjected to further validationmore » study using new sets of experimental data generated from a rolling mill at PNNL. Simulation results of both hot rolling and cold rolling of uranium-10% molybdenum coupons have been compared with experimental results. The model was used to predict roll-separating forces at different temperatures and reductions for five rolling mills within the National Nuclear Security Administration Fuel Fabrication Capability project. This report also presents initial results of a finite-element model microstructure-based approach to study the surface roughness at the interface between zirconium and uranium-10% molybdenum.« less
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Vision-based surface defect inspection for thick steel plates
NASA Astrophysics Data System (ADS)
Yun, Jong Pil; Kim, Dongseob; Kim, KyuHwan; Lee, Sang Jun; Park, Chang Hyun; Kim, Sang Woo
2017-05-01
There are several types of steel products, such as wire rods, cold-rolled coils, hot-rolled coils, thick plates, and electrical sheets. Surface stains on cold-rolled coils are considered defects. However, surface stains on thick plates are not considered defects. A conventional optical structure is composed of a camera and lighting module. A defect inspection system that uses a dual lighting structure to distinguish uneven defects and color changes by surface noise is proposed. In addition, an image processing algorithm that can be used to detect defects is presented in this paper. The algorithm consists of a Gabor filter that detects the switching pattern and employs the binarization method to extract the shape of the defect. The optics module and detection algorithm optimized using a simulator were installed at a real plant, and the experimental results conducted on thick steel plate images obtained from the steel production line show the effectiveness of the proposed method.
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NASA Astrophysics Data System (ADS)
Philippot, C.; Bellavoine, M.; Dumont, M.; Hoummada, K.; Drillet, J.; Hebert, V.; Maugis, P.
2018-01-01
Compared with other dual-phase (DP) steels, initial microstructures of cold-rolled martensite-ferrite have scarcely been investigated, even though they represent a promising industrial alternative to conventional ferrite-pearlite cold-rolled microstructures. In this study, the influence of the heating rate (over the range of 1 to 10 K/s) on the development of microstructures in a microalloyed DP steel is investigated; this includes the tempering of martensite, precipitation of microalloying elements, recrystallization, and austenite formation. This study points out the influence of the degree of ferrite recrystallization prior to the austenite formation, as well as the importance of the cementite distribution. A low heating rate giving a high degree of recrystallization, leads to the formation of coarse austenite grains that are homogenously distributed in the ferrite matrix. However, a high heating rate leading to a low recrystallization degree, results in a banded-like structure with small austenite grains surrounded by large ferrite grains. A combined approach, involving relevant multiscale microstructural characterization and modeling to rationalize the effect of the coupled processes, highlights the role of the cold-worked initial microstructure, here a martensite-ferrite mixture: recrystallization and austenite formation commence in the former martensite islands before extending in the rest of the material.
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NASA Astrophysics Data System (ADS)
Zhao, Yan; Zhang, Weina; Liu, Xin; Liu, Zhenyu; Wang, Guodong
2016-12-01
In the present work, twin-roll strip casting was carried out to fabricate thin strip of a Mn-N alloyed lean duplex stainless steel with the composition of Fe-19Cr-6Mn-0.4N, in which internal pore defects had been effectively avoided as compared to conventional cast ingots. The solidification structure observed by optical microscope indicated that fine Widmannstatten structure and coarse-equiaxed crystals had been formed in the surface and center, respectively, with no columnar crystal structures through the surface to center of the cast strip. By applying hot rolling and cold rolling, thin sheets with the thickness of 0.5 mm were fabricated from the cast strips, and no edge cracks were formed during the rolling processes. With an annealing treatment at 1323 K (1050 °C) for 5 minutes after cold rolling, the volume fractions of ferrite and austenite were measured to be approximately equal, and the distribution of alloying elements in the strip was further homogenized. The cold-rolled and annealed sheet exhibited an excellent combination of strength and ductility, with the ultimate tensile strength and elongation having been measured to be 1000 MPa and 65 pct, respectively. The microstructural evolution during deformation was investigated by XRD, EBSD, and TEM, indicating that ferrite and austenite had different deformation mechanisms. The deformation of ferrite phase was dominated by dislocation slipping, and the deformation of austenite phase was mainly controlled by martensitic transformation in the sequence of γ→ ɛ-martensite→ α'-martensite, leading to the improvement of strength and plasticity by the so-called transformation-induced plasticity (TRIP) effect. By contrast, lean duplex stainless steels of Fe-21Cr-6Mn-0.5N and Fe-23Cr-7Mn-0.6N fabricated by twin-roll strip casting did not show TRIP effects and exhibited lower strength and elongation as compared to Fe-19Cr-6Mn-0.4N.
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Hydrogen Permeation in Cold-Rolled High-Mn Twinning-Induced Plasticity Steels
NASA Astrophysics Data System (ADS)
Han, Do Kyeong; Hwang, A. In; Byeon, Woo Jun; Noh, Seung Jeong; Suh, Dong-Woo
2017-11-01
Hydrogen permeation is investigated in cold-rolled Fe-0.6C-18Mn-(1.5Al) alloys. The hydrogen mobility is lower in cold-rolled alloys compared with annealed alloys. Al-containing alloy shows less deceleration of hydrogen mobility compared with the Al-free alloy. This is attributed to the reduced formation of mechanical twins and dislocations. Mechanical twins trap hydrogen strongly but are vulnerable to crack initiation; suppression of these is thought to be a major favorable influence of Al on hydrogen-induced mechanical degradation.
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Super-formable pure magnesium at room temperature.
Zeng, Zhuoran; Nie, Jian-Feng; Xu, Shi-Wei; H J Davies, Chris; Birbilis, Nick
2017-10-17
Magnesium, the lightest structural metal, is difficult to form at room temperature due to an insufficient number of deformation modes imposed by its hexagonal structure and a strong texture developed during thermomechanical processes. Although appropriate alloying additions can weaken the texture, formability improvement is limited because alloying additions do not fundamentally alter deformation modes. Here we show that magnesium can become super-formable at room temperature without alloying. Despite possessing a strong texture, magnesium can be cold rolled to a strain at least eight times that possible in conventional processing. The resultant cold-rolled sheet can be further formed without cracking due to grain size reduction to the order of one micron and inter-granular mechanisms becoming dominant, rather than the usual slip and twinning. These findings provide a pathway for developing highly formable products from magnesium and other hexagonal metals that are traditionally difficult to form at room temperature.Replacing steel or aluminium vehicle parts with magnesium would result in reduced emissions, but shaping magnesium without cracking remains challenging. Here, the authors successfully extrude and roll textured magnesium into ductile foil at low temperatures by activating intra-granular mechanisms.
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Manufacture of thin-walled clad tubes by pressure welding of roll bonded sheets
NASA Astrophysics Data System (ADS)
Schmidt, Hans Christian; Grydin, Olexandr; Stolbchenko, Mykhailo; Homberg, Werner; Schaper, Mirko
2017-10-01
Clad tubes are commonly manufactured by fusion welding of roll bonded metal sheets or, mechanically, by hydroforming. In this work, a new approach towards the manufacture of thin-walled tubes with an outer diameter to wall thickness ratio of about 12 is investigated, involving the pressure welding of hot roll bonded aluminium-steel strips. By preparing non-welded edges during the roll bonding process, the strips can be zip-folded and (cold) pressure welded together. This process routine could be used to manufacture clad tubes in a continuous process. In order to investigate the process, sample tube sections with a wall thickness of 2.1 mm were manufactured by U-and O-bending from hot roll bonded aluminium-stainless steel strips. The forming and welding were carried out in a temperature range between RT and 400°C. It was found that, with the given geometry, a pressure weld is established at temperatures starting above 100°C. The tensile tests yield a maximum bond strength at 340°C. Micrograph images show a consistent weld of the aluminium layer over the whole tube section.
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Mhaede, Mansour; Ahmed, Aymen; Wollmann, Manfred; Wagner, Lothar
2015-05-01
The present work investigates the effects of severe plastic deformation by cold rolling on the microstructure, the mechanical properties and the corrosion behavior of austenitic stainless steel (SS) 316Ti. Hydroxyapatite coating (HA) was applied on the deformed material to improve their corrosion resistance. The martensitic transformation due to cold rolling was recorded by X-ray diffraction spectra. The effects of cold rolling on the corrosion behavior were studied using potentiodynamic polarization. The electrochemical tests were carried out in Ringer's solution at 37±1 °C. Cold rolling markedly enhanced the mechanical properties while the electrochemical tests referred to a lower corrosion resistance of the deformed material. The best combination of both high strength and good corrosion resistance was achieved after applying hydroxyapatite coating. Copyright © 2015 Elsevier B.V. All rights reserved.
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Producing Foils From Direct Cast Titanium Alloy Strip
NASA Technical Reports Server (NTRS)
Stuart, T. A.; Gaspar, T. A.; Sukonnik, I. M.; Semiatan, S. L.; Batawi, E.; Peters, J. A.; Fraser, H. L.
1996-01-01
This research was undertaken to demonstrate the feasibility of producing high-quality, thin-gage, titanium foil from direct cast titanium strip. Melt Overflow Rapid Solidification Technology (MORST) was used to cast several different titanium alloys into 500 microns thick strip, 10 cm wide and up to 3 m long. The strip was then either ground, hot pack rolled or cold rolled, as appropriate, into foil. Gamma titanium aluminide (TiAl) was cast and ground to approximately 100 microns thick foil and alpha-2 titanium aluminide (Ti3AI) was cast and hot pack rolled to approximately 70 microns thick foil. CP Ti, Ti6Al2Sn4Zr2Mo, and Ti22AI23Nb (Orthorhombic), were successfully cast and cold-rolled into good quality foil (less than 125 microns thick). The foils were generally fully dense with smooth surfaces, had fine, uniform microstructures, and demonstrated mechanical properties equivalent to conventionally produced titanium. By eliminating many manufacturing steps, this technology has the potential to produce thin gage, titanium foil with good engineering properties at significantly reduced cost relative to conventional ingot metallurgy processing.
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Jana, Saumyadeep; Overman, Nicole; Varga, Tamas; ...
2017-09-25
Here, the effect of sub-eutectoid heat treatment on the phase transformation behavior in rolled U-10 wt.% Mo (U10Mo) foils was systematically investigated. The as-cast 5 mm thick foils were initially homogenized at 900 °C for 48 h and were hot rolled to 2 mm and later cold rolled down to 0.2 mm. Three starting microstructures were evaluated: (i) hot + cold-rolled to 0.2 mm (as-rolled condition), (ii) hot + cold-rolled to 0.2 mm + annealed at 700 °C for 1 h, and (iii) hot + cold-rolled to 0.2 mm + annealed at 1000 °C for 60 h. Annealing of as-rolledmore » materials at 700 °C resulted in small grain size (15 ± 9 μm average grain size), while annealing at 1000 °C led to very large grains (156 ± 118 μm average grain size) in rolled U10Mo foils. Later the samples were subjected to sub-eutectoid heat-treatment temperatures of 550 °C, 500 °C, and 400 °C for different durations of time starting from 1 h up to 100 h. U10Mo rolled foils went through various degrees of decomposition when subjected to the sub-eutectoid heat-treatment step and formed a lamellar microstructure through a cellular reaction mostly along the previous γ-UMo grain boundaries. The least amount of cellular reaction was observed in the large-grain microstructure at all temperatures. Conversely, a substantial amount of cellular reaction was observed in both the as-rolled and the small-grain microstructure. After 100 h of heat treatment at 500 °C, the volume fraction of the lamellar phase was found to be 4%, 22%, and 82% in large-grain, as-rolled, and small-grain samples, respectively.« less
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Jana, Saumyadeep; Overman, Nicole; Varga, Tamas
Here, the effect of sub-eutectoid heat treatment on the phase transformation behavior in rolled U-10 wt.% Mo (U10Mo) foils was systematically investigated. The as-cast 5 mm thick foils were initially homogenized at 900 °C for 48 h and were hot rolled to 2 mm and later cold rolled down to 0.2 mm. Three starting microstructures were evaluated: (i) hot + cold-rolled to 0.2 mm (as-rolled condition), (ii) hot + cold-rolled to 0.2 mm + annealed at 700 °C for 1 h, and (iii) hot + cold-rolled to 0.2 mm + annealed at 1000 °C for 60 h. Annealing of as-rolledmore » materials at 700 °C resulted in small grain size (15 ± 9 μm average grain size), while annealing at 1000 °C led to very large grains (156 ± 118 μm average grain size) in rolled U10Mo foils. Later the samples were subjected to sub-eutectoid heat-treatment temperatures of 550 °C, 500 °C, and 400 °C for different durations of time starting from 1 h up to 100 h. U10Mo rolled foils went through various degrees of decomposition when subjected to the sub-eutectoid heat-treatment step and formed a lamellar microstructure through a cellular reaction mostly along the previous γ-UMo grain boundaries. The least amount of cellular reaction was observed in the large-grain microstructure at all temperatures. Conversely, a substantial amount of cellular reaction was observed in both the as-rolled and the small-grain microstructure. After 100 h of heat treatment at 500 °C, the volume fraction of the lamellar phase was found to be 4%, 22%, and 82% in large-grain, as-rolled, and small-grain samples, respectively.« less
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Numerical Modeling of Tube Forming by HPTR Cold Pilgering Process
NASA Astrophysics Data System (ADS)
Sornin, D.; Pachón-Rodríguez, E. A.; Vanegas-Márquez, E.; Mocellin, K.; Logé, R.
2016-09-01
For new fast-neutron sodium-cooled Generation IV nuclear reactors, the candidate cladding materials for the very strong burn-up are ferritic and martensitic oxide dispersion strengthened grades. Classically, the cladding tube is cold formed by a sequence of cold pilger milling passes with intermediate heat treatments. This process acts upon the geometry and the microstructure of the tubes. Consequently, crystallographic texture, grain sizes and morphologies, and tube integrity are highly dependent on the pilgering parameters. In order to optimize the resulting mechanical properties of cold-rolled cladding tubes, it is essential to have a thorough understanding of the pilgering process. Finite Element Method (FEM) models are used for the numerical predictions of this task; however, the accuracy of the numerical predictions depends not only on the type of constitutive laws but also on the quality of the material parameters identification. Therefore, a Chaboche-type law which parameters have been identified on experimental observation of the mechanical behavior of the material is used here. As a complete three-dimensional FEM mechanical analysis of the high-precision tube rolling (HPTR) cold pilgering of tubes could be very expensive, only the evolution of geometry and deformation is addressed in this work. The computed geometry is compared to the experimental one. It is shown that the evolution of the geometry and deformation is not homogeneous over the circumference. Moreover, it is exposed that the strain is nonhomogeneous in the radial, tangential, and axial directions. Finally, it is seen that the dominant deformation mode of a material point evolves during HPTR cold pilgering forming.
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On the impact of forced roll convection on vertical turbulent transport in cold air outbreaks
NASA Astrophysics Data System (ADS)
Gryschka, Micha; Fricke, Jens; Raasch, Siegfried
2014-11-01
We investigated the impact of roll convection on the convective boundary layer and vertical transports in different cold air outbreak (CAO) scenarios using large eddy simulations (LES). The organization of convection into rolls was triggered by upstream heterogeneities in the surface temperature, representing ice and water. By changing the sea ice distribution in our LES, we were able to simulate a roll and a nonroll case for each scenario. Furthermore, the roll wavelength was varied by changing the scale of the heterogeneity. The characteristics of the simulated rolls and cloud streets, such as aspect ratios, orientation of the roll axes, and downstream extensions of single rolls agreed closely with observations in CAO situations. The vertical turbulent fluxes, calculated for each simulation, were decomposed into contributions from rolls and from unorganized turbulence. Even though our results confirmed that rolls triggered by upstream heterogeneities can substantially contribute to vertical turbulent fluxes, the total fluxes were not affected by the rolls.
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NASA Astrophysics Data System (ADS)
Mehta, K. K.; Mandal, R. K.; Singh, A. K.
2018-07-01
The high ratio of relative resolved shear stress on a twin to planar slip system results in microstructural latent hardening (some kind of overshooting) by the twin system on the primary slip planes, which leads to development of the {111}-fiber in Ni-16Cr alloy. The development of {111}-fiber starts as early as around 16 pct cold reduction in Ni-16Cr alloy and persists with maximum average intensity ranging from 35 to 40 pct additional deformation, i.e., around 50 pct cold reduction in unidirectional (U) and two-step cross (T)-rolling modes. In between 50 and 68 pct reductions in U and T modes, the fiber becomes unstable and starts disappearing. However, in multistep cross (M) rolling, the {111}-fiber formation starts late, i.e., at around 50 pct reduction, and maintains its stability up to additional deformation ranging from 35 to 40 pct, i.e., around 90 pct cold reduction. Thus, the life of {111}-fiber remains stable only within the range from 35 to 40 pct intermediate deformation during cold rolling of Ni-16Cr alloy irrespective of modes of rolling. However, the start and end of fiber stabilities depend on the modes of deformation by rolling. The maximum average intensity of {111}-fiber that can be attained in Ni-16Cr alloy is around 3.6× random in any of the deformation modes.
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NASA Astrophysics Data System (ADS)
Mehta, K. K.; Mandal, R. K.; Singh, A. K.
2018-04-01
The high ratio of relative resolved shear stress on a twin to planar slip system results in microstructural latent hardening (some kind of overshooting) by the twin system on the primary slip planes, which leads to development of the {111}-fiber in Ni-16Cr alloy. The development of {111}-fiber starts as early as around 16 pct cold reduction in Ni-16Cr alloy and persists with maximum average intensity ranging from 35 to 40 pct additional deformation, i.e., around 50 pct cold reduction in unidirectional (U) and two-step cross (T)-rolling modes. In between 50 and 68 pct reductions in U and T modes, the fiber becomes unstable and starts disappearing. However, in multistep cross (M) rolling, the {111}-fiber formation starts late, i.e., at around 50 pct reduction, and maintains its stability up to additional deformation ranging from 35 to 40 pct, i.e., around 90 pct cold reduction. Thus, the life of {111}-fiber remains stable only within the range from 35 to 40 pct intermediate deformation during cold rolling of Ni-16Cr alloy irrespective of modes of rolling. However, the start and end of fiber stabilities depend on the modes of deformation by rolling. The maximum average intensity of {111}-fiber that can be attained in Ni-16Cr alloy is around 3.6× random in any of the deformation modes.
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NASA Astrophysics Data System (ADS)
Fattah-alhosseini, Arash; Naseri, Majid; Gashti, Seyed Omid; Vafaeian, Saeed; Keshavarz, Mohsen K.
2018-06-01
In the present work, influences of the cold deformation on electrochemical and passive response of pure nickel in three solutions with adjusted pH values of 8.5, 9.0, and 9.5 at 298 ± 1 K (25 ± 1 °C) were investigated. A cold deformation process was applied by means of cold rolling. Implementation of the cold deformation process resulted in samples having a finer microstructure. Also, the cold work and grain refinement led to increased hardness. In addition, open-circuit potential and potentiodynamic polarization tests were performed and results showed that corrosion current density was reduced by applying the cold deformation. Moreover, the results of the electrochemical impedance spectroscopy and Mott-Schottky analyses indicated higher corrosion resistance of pure nickel after cold deformation. This behavior is attributed to the growth of much thicker, with less point defects, passive layer on the surface of cold-deformed samples.
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Processing and microstructure of Nb-1 percent Zr-0.1 percent C alloy sheet
NASA Technical Reports Server (NTRS)
Uz, Mehmet; Titran, Robert H.
1992-01-01
A systematic study was carried out to evaluate the effects of processing on the microstructure of Nb-1 wt. pct. Zr-0.1 wt. pct. C alloy sheet. The samples were fabricated by cold rolling different sheet bars that were single-, double- or triple-extruded at 1900 K. Heat treatment consisted on one- or two-step annealing of different samples at temperatures ranging from 1350 to 1850 K. The assessment of the effects of processing on microstructure involved characterization of the precipitates including the type, crystal structure, chemistry and distribution within the material as well as an examination of the grain structure. A combination of various analytical and metallographic techniques were used on both the sheet samples and the residue extracted from them. The results show that the relatively coarse orthorhombic Nb2C carbides in the as-rolled samples transformed to rather fine cubic monocarbides of Nb and Zr with varying Zr/Nb ratios upon subsequent heat treatment. The relative amount of the cubic carbides and the Zr/Nb ratio increased with increasing number of extrusions prior to cold rolling. Furthermore, the size and the aspect ratio of the grains appear to be strong functions of the processing history of the material. These and other results obtained will be presented with the emphasis on a possible relationship between processing and microstructure.
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A Study of the Batch Annealing of Cold-Rolled HSLA Steels Containing Niobium or Titanium
NASA Astrophysics Data System (ADS)
Fang, Chao; Garcia, C. Isaac; Choi, Shi-Hoon; DeArdo, Anthony J.
2015-08-01
The batch annealing behavior of two cold-rolled, microalloyed HSLA steels has been studied in this program. One steel was microalloyed with niobium while the other with titanium. A successfully batch annealed steel will exhibit minimum variation in properties along the length of the coil, even though the inner and outer wraps experience faster heating and cooling rates and lower soaking temperatures, i.e., the so-called "cold spot" areas, than the mid-length portion of the coil, i.e., the so-called "hot spot" areas. The variation in strength and ductility is caused by differences in the extent of annealing in the different areas. It has been known for 30 years that titanium-bearing HSLA steels show more variability after batch annealing than do the niobium-bearing steels. One of the goals of this study was to try to explain this observation. In this study, the annealing kinetics of the surface and center layers of the cold-rolled sheet were compared. The surface and center layers of the niobium steel and the surface layer of the titanium steel all showed similar annealing kinetics, while the center layer of the titanium steel exhibited much slower kinetics. Metallographic results indicate that the stored energy of the cold-rolled condition, as revealed by grain center sub-grain boundary density, appeared to strongly influence the annealing kinetics. The kinetics were followed by the Kernel Average Misorientation reconstruction of the microstructure at different stages on annealing. Possible pinning effects caused by microalloy precipitates were also considered. Methods of improving uniformity and increasing kinetics, involving optimizing both hot-rolled and cold-rolled microstructure, are suggested.
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NASA Astrophysics Data System (ADS)
Gaur, Rishi; Gupta, R. K.; AnilKumar, V.; Banwait, S. S.
2018-05-01
Mechanical behavior of Ti-4Al-1Mn titanium alloy has been studied in annealed, cold-rolled and heat-treated conditions. Room temperature tensile strength as well as % elongation has been found to be low with increasing amount of cold rolling. Lowering of strength in cold worked condition is attributed to premature failure. However, the same has been mitigated after heat treatment. Significant effect of cooling media (air and water) from heat treatment temperature on microstructure was not found except for the degree of fineness of α plates. Optimum properties (strength as well as ductility) were exhibited by samples subjected to 15% cold rolling and heat treatment below β transus temperature, which can be attributed to presence of recrystallized microstructure. In cold worked condition, the microstructure shows fine fragmented α plates/Widmanstätten morphology with high dislocation density along with a large amount of strain fields and twinning, which gets transformed to recrystallized equiaxed microstructure and with plate-like morphology after near β heat treatment. Prior cold work is found to have a significant effect on mechanical properties supported by evolution of microstructure. Twinning is found to be assisting in deformation as well as in recrystallization through the formation of deformation and annealing twins during cold working and heat treatment. Fracture analysis of the tested sample with prior cold work and heat-treated condition revealed quasi-ductile failure as compared to only ductile failure features seen for samples heat treated without prior cold work.
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Effects of Casting Conditions on End Product Defects in Direct Chill Casted Hot Rolling Ingots
NASA Astrophysics Data System (ADS)
Yorulmaz, Arda; Yüksel, Çağlar; Erzi, Eraz; Dispinar, Derya
Direct chill casting is a reliable casting process for almost any wrought aluminum alloy for subsequent deformation via hot rolling to supply vital industries such as aerospace, automotive, construction, packaging and maritime. While some defects occur during casting, like hot tearing, some others like surface defect causing blisters, appear after hot rolling process or annealing after final cold rolling steps. It was found that some of these defects are caused by melt impurities formed from entrained folded aluminum oxides or bifilms. A study in a hot rolling casting facility was carried out with different melt cleaning practices, launder and molten metal transferring designs. Bifilm index and reduced pressure test were used for determining melt cleanliness measurement. It was found that porous plug gas diffusons for degassing are more effective than lance type degassers and a design towards less turbulent molten metal flow from furnace to mould cavity are necessary for reducing defects caused by bifilms.
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Improvement of mechanical properties on metastable stainless steels by reversion heat treatments
NASA Astrophysics Data System (ADS)
Mateo, A.; Zapata, A.; Fargas, G.
2013-12-01
AISI 301LN is a metastable austenitic stainless steel that offers an excellent combination of high strength and ductility. This stainless grade is currently used in applications where severe forming operations are required, such as automotive bodies. When these metastable steels are plastically deformed at room temperature, for example by cold rolling, austenite transforms to martensite and, as a result, yield strength increases but ductility is reduced. Grain refinement is the only method that allows improving strength and ductility simultaneously. Several researchers have demonstrated that fine grain AISI 301LN can be obtained by heat treatment after cold rolling. This heat treatment is called reversion because it provokes the reversion of strain induced martensite to austenite. In the present work, sheets of AISI 301LN previously subjected to 20% of cold rolling reduction were treated and a refined grain austenitic microstructure was obtained. Mechanical properties, including fatigue limit, were determined and compared with those corresponding to the steel both before and after the cold rolling.
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On the Influence of Surface Heterogeneities onto Roll Convection
NASA Astrophysics Data System (ADS)
Gryschka, M.; Drüe, C.; Raasch, S.; Etling, D.
2009-04-01
Roll convection is a common phenomenon in atmospheric convective boundary layers (CBL) with background wind. Roll convection is observed both over land and over sea for different synoptic situations. There is still some debate about the different types of roll convection and their causes or rather the necessary conditions for their appearance. The stability parameter ζ = -ziL (zi: boundary layer height, L: Monin-Obukhov stability length) is widely used as a predictor for roll convection, since numerous studies suggest that convective rolls only appear when 0 < ζ < 20. In other words, roll development becomes unlikely for strong surface heating and weak vertical wind shear. In contrast to those studies the presence of roll convection in almost any polar cold air outbreak (as can be seen in numerous satellite images as cloud streets) reveals that even for large ζ roll convection can develop. Some studies report roll convection in cold air outbreaks for ζ = 250. Our large eddy simulations (LES) on roll convection suggests that the contrasting results concerning the dependency of roll convection on ζ are due to two different types of roll convection: One type which develops purely by self organization if ζ < 20 ("free rolls") and another type which is triggered by heterogeneities in surface temperature and develops also for large ζ ("forced rolls"). We think that most of the cloud streets observed in polar cold air outbreaks over open water are due to rolls of forced type which are tied to upstream located heterogeneities in the sea-ice distribution. The results of this study suggests that the omission of surface inhomogeneities in previous LES is the reason for the absence of rolls in all LES with strong surface heating and weak vertical wind shear so far. In this contribution we will present a large eddy simulation which successfully represents forced rolls under such conditions.
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NASA Astrophysics Data System (ADS)
T, Morimoto; F, Yoshida; A, Yanagida; J, Yanagimoto
2015-04-01
First, hardening model in f.c.c. metals was formulated with collinear interactions slips, Hirth slips and Lomer-Cottrell slips. Using the Taylor and the Sachs rolling texture prediction model, the residual dislocation densities of cold-rolled commercial pure aluminum were estimated. Then, coincidence site lattice grains were investigated from observed cold rolling texture. Finally, on the basis of oriented nucleation theory and coincidence site lattice theory, the recrystallization texture of commercial pure aluminum after low-temperature annealing was predicted.
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Research and Development Trend of Shape Control for Cold Rolling Strip
NASA Astrophysics Data System (ADS)
Wang, Dong-Cheng; Liu, Hong-Min; Liu, Jun
2017-09-01
Shape is an important quality index of cold rolling strip. Up to now, many problems in the shape control domain have not been solved satisfactorily, and a review on the research progress in the shape control domain can help to seek new breakthrough directions. In the past 10 years, researches and applications of shape control models, shape control means, shape detection technology, and shape control system have achieved significant progress. In the aspect of shape control models, the researches in the past improve the accuracy, speed and robustness of the models. The intelligentization of shape control models should be strengthened in the future. In the aspect of the shape control means, the researches in the past focus on the roll optimization, mill type selection, process optimization, local strip shape control, edge drop control, and so on. In the future, more attention should be paid to the coordination control of both strip shape and other quality indexes, and the refinement of control objective should be strengthened. In the aspects of shape detection technology and shape control system, some new types of shape detection meters and shape control systems are developed and have successfully industrial applications. In the future, the standardization of shape detection technology and shape control system should be promoted to solve the problem of compatibility. In general, the four expected development trends of shape control for cold rolling strip in the future are intelligentization, coordination, refinement, and standardization. The proposed research provides new breakthrough directions for improving shape quality.
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Through-process modelling of texture and anisotropy in AA5182
NASA Astrophysics Data System (ADS)
Crumbach, M.; Neumann, L.; Goerdeler, M.; Aretz, H.; Gottstein, G.; Kopp, R.
2006-07-01
A through-process texture and anisotropy prediction for AA5182 sheet production from hot rolling through cold rolling and annealing is reported. Thermo-mechanical process data predicted by the finite element method (FEM) package T-Pack based on the software LARSTRAN were fed into a combination of physics based microstructure models for deformation texture (GIA), work hardening (3IVM), nucleation texture (ReNuc), and recrystallization texture (StaRT). The final simulated sheet texture was fed into a FEM simulation of cup drawing employing a new concept of interactively updated texture based yield locus predictions. The modelling results of texture development and anisotropy were compared to experimental data. The applicability to other alloys and processes is discussed.
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Hsu, Chia-Hao; Chen, Tai-Cheng; Huang, Rong-Tan; Tsay, Leu-Wen
2017-01-01
304 stainless steels (SS) were considered as the materials for a dry storage canister. In this study, ER (Electrode Rod) 308L was utilized as the filler metal for the groove and overlay welds of a 304L stainless steel substrate, which was prepared via a gas tungsten arc-welding process in multiple passes. The electron backscatter diffraction (EBSD) map was used to identify the inherent microstructures in distinct specimens. U-bend and weight-loss tests were conducted by testing the 304L substrates and welds in a salt spray containing 5 wt % NaCl at 80 °C to evaluate their susceptibility to stress corrosion cracking (SCC). Generally, the weight loss of the ER 308L deposit was higher than that of the 304L substrate in a salt spray in the same sample-prepared condition. The dissolution of the skeletal structure in the fusion zone (FZ) was responsible for a greater weight loss of the 308L deposit, especially for the cold-rolled and sensitized specimen. Cold rolling was detrimental and sensitization after cold rolling was very harmful to the SCC resistance of the 304L substrate and 308L deposit. Overall, the SCC susceptibility of each specimen was correlated with its weight loss in each group. PMID:28772547
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Quantitative Residual Strain Analyses on Strain Hardened Nickel Based Alloy
NASA Astrophysics Data System (ADS)
Yonezawa, Toshio; Maeguchi, Takaharu; Goto, Toru; Juan, Hou
Many papers have reported about the effects of strain hardening by cold rolling, grinding, welding, etc. on stress corrosion cracking susceptibility of nickel based alloys and austenitic stainless steels for LWR pipings and components. But, the residual strain value due to cold rolling, grinding, welding, etc. is not so quantitatively evaluated.
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Large grain cavities from pure niobium ingot
Myneni, Ganapati Rao [Yorktown, VA; Kneisel, Peter [Williamsburg, VA; Cameiro, Tadeu [McMurray, PA
2012-03-06
Niobium cavities are fabricated by the drawing and ironing of as cast niobium ingot slices rather than from cold rolled niobium sheet. This method results in the production of niobium cavities having a minimum of grain boundaries at a significantly reduced cost as compared to the production of such structures from cold rolled sheet.
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NASA Astrophysics Data System (ADS)
Toloczko, Mychailo B.; Olszta, Matthew J.; Bruemmer, Stephen M.
Stress corrosion crack-growth experiments have been performed on cold-rolled alloy 690 materials in simulated PWR primary water at 360°C. Extruded alloy 690 CRDM tubing in two conditions, thermally treated (TT) and solution annealed (SA), was cold rolled (CR) in one direction to several reductions reaching a maximum of 31% and tested in the S-L orientation. High stress corrosion cracking (SCC) propagation rates ( 8x10-8 mm/s) were observed for the 31%CR alloy 690TT material, while the 31%CR alloy 690SA exhibited 10X lower rates. The difference in intergranular SCC susceptibility appears to be related to grain boundary carbide distribution before cold rolling. SCC growth rates were found to depend on test temperature and hydrogen concentration. Tests were also performed on two alloy 690 plate heats, one CR to a reduction of 26% and the other to 20%. SCC growth rates at 360°C were similar to that measured for the 31%CR alloy 690TT CRDM tubing. Comparisons will be made to other results on CR alloy 690 materials.
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Wang, Z.; Gao, M. C.; Ma, S. G.; ...
2015-08-05
Cold rolling can break down the as-cast dendrite microstructure and thus may have pronounced impact on the mechanical behavior of the alloy. In the present study, the effect of cold rolling on the microstructure and mechanical properties of Al 0.25CoCrFe 1.25Ni 1.25 high-entropy alloy in the face-centered cubic structure was investigated. With increasing the thickness reduction from cold rolling, the hardness, the yield strength, and the fracture strength increased at the cost of reducing ductility. At the thickness reduction of 80%, the tensile strength (hardness) was 702 MPa (406 MPa), 1.62 (2.43) times that in the as-cast condition. Compared tomore » traditional alloys, Al 0.25CoCrFe 1.25Ni 1.25 has the highest hardening rate with respect to CR thickness reduction. Lastly, the phase relation and the mixing properties of Gibbs free energy, enthalpy and entropy of Al xCoCrFe 1.25Ni 1.25 were predicted using the CALPHAD method.« less
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NASA Astrophysics Data System (ADS)
Jeong, S. W.; Kang, U. G.; Choi, J. Y.; Nam, W. J.
2012-09-01
Strain aging and hardening behaviors of a 304 stainless steel containing deformation-induced martensite were investigated by examining mechanical properties and microstructural evolution for different aging temperature and time. Introduced age hardening mechanisms of a cold rolled 304 stainless steel were the additional formation of α'-martensite, hardening of α'-martensite, and hardening of deformed austenite. The increased amount of α'-martensite at an aging temperature of 450 °C confirmed the additional formation of α'-martensite as a hardening mechanism in a cold rolled 304 stainless steel. Additionally, the increased hardness in both α'-martensite and austenite phases with aging temperature proved that hardening of both α'-martensite and austenite phases would be effective as hardening mechanisms in cold rolled and aged 304 stainless steels. The results suggested that among hardening mechanisms, hardening of an α'-martensite phase, including the diffusion of interstitial solute carbon atoms to dislocations and the precipitation of fine carbide particles would become a major hardening mechanism during aging of cold rolled 304 stainless steels.
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Synthesis, Characterization and Cold Workability of Cast Copper-Magnesium-Tin Alloys
NASA Astrophysics Data System (ADS)
Bravo Bénard, Agustín Eduardo; Martínez Hernández, David; González Reyes, José Gonzalo; Ortiz Prado, Armando; Schouwenaars Franssens, Rafael
2014-02-01
The use of Mg as an alloying element in copper alloys has largely been overlooked in scientific literature and technological applications. Its supposed tribological compatibility with iron makes it an interesting option to replace Pb in tribological alloys. This work describes the casting process of high-quality thin slabs of Cu-Mg-Sn alloys with different compositions by means of conventional methods. The resulting phases were analyzed using X-ray diffraction, scanning electron microscopy, optical microscopy, and energy dispersive X-ray spectroscopy techniques. Typical dendritic α-Cu, eutectic Cu2Mg(Sn) and eutectoid non-equilibrium microstructures were found. Tensile tests and Vickers microhardness show the excellent hardening capability of Mg as compared to other copper alloys in the as-cast condition. For some of the slabs and compositions, cold rolling reductions of over 95 pct have been easily achieved. Other compositions and slabs have failed during the deformation process. Failure analysis after cold rolling reveals that one cause for brittleness is the presence of casting defects such as microshrinkage and inclusions, which can be eliminated. However, for high Mg contents, a high volume fraction of the intermetallic phase provides a contiguous path for crack propagation through the connected interdendritic regions.
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Chen, Ming-biao; Ma, Min; Yang, Qing-xiang; Wang, Shan; Liu, Wen-chang; Zhao, Ying-mei
2013-09-01
To provide gist of DC AA 5052 and CC AA 5052 aluminum alloy to industry production and application, the texture variation of cold rolled sheets through thickness direction was studied by X-ray diffraction method, and the difference in texture at surface, quarter and center layer was analyzed. The hot plates of direct chill cast (DC) AA 5052 and continuous cast (CC) AA 5052 aluminum alloy were annealed at 454 degrees C for 4 hours and then cold rolled to different reductions. The strength and volume fraction of the fiber in CC AA 5052 aluminum alloy is larger than in DC AA 5052 aluminum alloy after same rolling reduction The volume fraction of the recrystallization texture cube in the CC AA 5052 aluminum alloy is less than in the DC AA 5052 aluminum alloy, which result in that CC AA 5052 aluminum alloy needs less cold rolling reduction than DC AA 5052 aluminum alloy for generating the texture with same intensity and volume fraction at surface layer, quarter layer and center layer. The manufacturability and performance of CC AA 5052 aluminum alloy is superior to DC AA 5052 aluminum alloy for use in stamping.
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NASA Astrophysics Data System (ADS)
Kumar, Amit; Khatirkar, Rajesh Kisni; Chalapathi, Darshan; Kumar, Gulshan; Suwas, Satyam
2017-05-01
In the present study, microstructure and texture evolution during cold rolling in UNS S32205 and UNS S32760 duplex stainless steel was investigated. Both steels were unidirectionally cold rolled up to 80 pct thickness reduction. Scanning electron microscopy and electron backscattered diffraction (EBSD) were used for microstructural characterization, while X-ray diffraction (XRD) was used for the measurement of bulk texture. Strain-induced martensite (SIM) was identified and quantified with the help of magnetic measurements (B-H curve and magnetization saturation). With the increase in plastic strain, the grains became morphologically elongated along the rolling direction with the reduction in average band thickness and band spacing. SIM increased with the increase in deformation and was found to be a function of strain and the SFE of austenite. The increase in SIM was much more pronounced in UNS S32205 steel as compared to UNS S32760 steel. After cold rolling, strong α-fiber (RD//<110>) texture was developed in ferrite, while brass texture was dominant in austenite for both steels. The strength of texture components and fibers was stronger in UNS S32760 steel. Another significant feature was the development of weak γ-fiber (ND//<111>) in UNS S32760 steel at intermediate deformation.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Guo, Zhanying; Department of Applied Science, University of Québec at Chicoutimi, Saguenay, QC G7H 2B1; Zhao, Gang
2016-04-15
The effects of two homogenization treatments applied to the direct chill (DC) cast billet on the recrystallization behavior in 7150 aluminum alloy during post-rolling annealing have been investigated using the electron backscatter diffraction (EBSD) technique. Following hot and cold rolling to the sheet, measured orientation maps, the recrystallization fraction and grain size, the misorientation angle and the subgrain size were used to characterize the recovery and recrystallization processes at different annealing temperatures. The results were compared between the conventional one-step homogenization and the new two-step homogenization, with the first step being pretreated at 250 °C. Al{sub 3}Zr dispersoids with highermore » densities and smaller sizes were obtained after the two-step homogenization, which strongly retarded subgrain/grain boundary mobility and inhibited recrystallization. Compared with the conventional one-step homogenized samples, a significantly lower recrystallized fraction and a smaller recrystallized grain size were obtained under all annealing conditions after cold rolling in the two-step homogenized samples. - Highlights: • Effects of two homogenization treatments on recrystallization in 7150 Al sheets • Quantitative study on the recrystallization evolution during post-rolling annealing • Al{sub 3}Zr dispersoids with higher densities and smaller sizes after two-step treatment • Higher recrystallization resistance of 7150 sheets with two-step homogenization.« less
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Efficient rolling texture predictions and texture-sensitive properties of α-uranium foils
Steiner, Matthew A.; Klein, Robert W.; Calhoun, Christopher A.; ...
2017-01-01
Here, finite element (FE) analysis was used to simulate the strain history of an α-uranium foil during cold-rolling, with the sheet modeled as an isotropic elastoplastic continuum. The resulting strain history was then used as input for a viscoplastic self-consistent (VPSC) polycrystal plasticity model to simulate crystallographic texture evolution. Mid-plane textures predicted via the combined FE→VPSC approach show alignment of the (010) poles along the rolling direction (RD), and the (001) poles along the normal direction (ND) with a symmetric splitting along RD. The surface texture is similar to that of the mid-plane, but with a shear-induced asymmetry that favorsmore » one of the RD split features of the (001) pole figure. Both the mid-plane and surface textures predicted by the FE→VPSC approach agree with published experimental results for cold-rolled α-uranium plates, as well as predictions made by a more computationally intensive full-field crystal plasticity based finite element model. α-uranium foils produced by cold-rolling must typically undergo a final recrystallization anneal to restore ductility prior to their final application, resulting in significant texture evolution from the cold-rolled plate deformation texture. Using the texture measured from a foil in the final recrystallized state, coefficients of the thermal expansion and elastic stiffness tensors were calculated using a thermo-elastic self-consistent model, and the anisotropic yield loci and flow curves along the RD, TD, and ND were predicted using the VPSC code.« less
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Efficient rolling texture predictions and texture-sensitive properties of α-uranium foils
DOE Office of Scientific and Technical Information (OSTI.GOV)
Steiner, Matthew A.; Klein, Robert W.; Calhoun, Christopher A.
Here, finite element (FE) analysis was used to simulate the strain history of an α-uranium foil during cold-rolling, with the sheet modeled as an isotropic elastoplastic continuum. The resulting strain history was then used as input for a viscoplastic self-consistent (VPSC) polycrystal plasticity model to simulate crystallographic texture evolution. Mid-plane textures predicted via the combined FE→VPSC approach show alignment of the (010) poles along the rolling direction (RD), and the (001) poles along the normal direction (ND) with a symmetric splitting along RD. The surface texture is similar to that of the mid-plane, but with a shear-induced asymmetry that favorsmore » one of the RD split features of the (001) pole figure. Both the mid-plane and surface textures predicted by the FE→VPSC approach agree with published experimental results for cold-rolled α-uranium plates, as well as predictions made by a more computationally intensive full-field crystal plasticity based finite element model. α-uranium foils produced by cold-rolling must typically undergo a final recrystallization anneal to restore ductility prior to their final application, resulting in significant texture evolution from the cold-rolled plate deformation texture. Using the texture measured from a foil in the final recrystallized state, coefficients of the thermal expansion and elastic stiffness tensors were calculated using a thermo-elastic self-consistent model, and the anisotropic yield loci and flow curves along the RD, TD, and ND were predicted using the VPSC code.« less
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NASA Astrophysics Data System (ADS)
Steiner, Matthew A.; Klein, Robert W.; Calhoun, Christopher A.; Knezevic, Marko; Garlea, Elena; Agnew, Sean R.
2017-11-01
Finite element (FE) analysis was used to simulate the strain history of an α-uranium foil during cold straight-rolling, with the sheet modeled as an isotropic elastoplastic continuum. The resulting strain history was then used as input for a viscoplastic self-consistent (VPSC) polycrystal plasticity model to simulate crystallographic texture evolution. Mid-plane textures predicted via the combined FE→VPSC approach show alignment of the (010) poles along the rolling direction (RD), and the (001) poles along the normal direction (ND) with a symmetric splitting along RD. The surface texture is similar to that of the mid-plane, but with a shear-induced asymmetry that favors one of the RD split features of the (001) pole figure. Both the mid-plane and surface textures predicted by the FE→VPSC approach agree with published experimental results for cold straight-rolled α-uranium plates, as well as predictions made by a more computationally intensive full-field crystal plasticity based finite element model. α-uranium foils produced by cold-rolling must typically undergo a recrystallization anneal to restore ductility prior to their final application, resulting in significant texture evolution from the cold-rolled plate deformation texture. Using the texture measured from a foil in the final recrystallized state, coefficients of thermal expansion and the elastic stiffness tensors were calculated using a thermo-elastic self-consistent model, and the anisotropic yield loci and flow curves along the RD, TD, and ND were predicted using the VPSC code.
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On the nature of low temperature internal friction peaks in metallic glasses
DOE Office of Scientific and Technical Information (OSTI.GOV)
Khonik, V.A.; Spivak, L.V.
Low temperature (30 < T < 300 K) internal friction in a metallic glass Ni{sub 60}Nb{sub 40} subjected to preliminary inhomogeneous deformation by cold rolling, homogeneous tensile deformation or electrolytic charging with hydrogen is investigated. Cold rolling or hydrogenation result in appearance of similar internal friction peaks and hysteresis damping. Homogeneous deformation has no influence on low temperature internal friction. The phenomenon of microplastic deformation during hydrogenation of weakly stressed samples is revealed. It is argued that microplastic deformation of metallic glasses during hydrogenation without external stress takes place too. Plastic flow both on cold rolling and hydrogenation occurs viamore » formation and motion of dislocation-like defects which are the reason of the observed anelastic anomalies. It is concluded that low temperature internal friction peaks described in the literature for as-cast, cold deformed and hydrogenated samples have common dislocation-like origin.« less
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Precipitation in cold-rolled Al–Sc–Zr and Al–Mn–Sc–Zr alloys prepared by powder metallurgy
DOE Office of Scientific and Technical Information (OSTI.GOV)
Vlach, M., E-mail: martin.vlach@mff.cuni.cz; Stulikova, I.; Smola, B.
2013-12-15
The effects of cold-rolling on thermal, mechanical and electrical properties, microstructure and recrystallization behaviour of the AlScZr and AlMnScZr alloys prepared by powder metallurgy were studied. The powder was produced by atomising in argon with 1% oxygen and then consolidated by hot extrusion at 350 °C. The electrical resistometry and microhardness together with differential scanning calorimetry measurements were compared with microstructure development observed by transmission and scanning electron microscopy, X-ray diffraction and electron backscatter diffraction. Fine (sub)grain structure developed and fine coherent Al{sub 3}Sc and/or Al{sub 3}(Sc,Zr) particles precipitated during extrusion at 350 °C in the alloys studied. Additional precipitationmore » of the Al{sub 3}Sc and/or Al{sub 3}(Sc,Zr) particles and/or their coarsening was slightly facilitated by the previous cold rolling. The presence of Sc,Zr-containing particles has a significant antirecrystallization effect that prevents recrystallization at temperatures minimally up to 420 °C. The precipitation of the Al{sub 6}Mn- and/or Al{sub 6}(Mn,Fe) particles of a size ∼ 1.0 μm at subgrain boundaries has also an essential antirecrystallization effect and totally suppresses recrystallization during 32 h long annealing at 550 °C. The texture development of the alloys seems to be affected by high solid solution strengthening by Mn. The precipitation of the Mn-containing alloy is highly enhanced by a cold rolling. The apparent activation energy of the Al{sub 3}Sc particles formation and/or coarsening and that of the Al{sub 6}Mn and/or Al{sub 6}(Mn,Fe) particle precipitation in the powder and in the compacted alloys were determined. The cold deformation has no effect on the apparent activation energy values of the Al{sub 3}Sc-phase and the Al{sub 6}Mn-phase precipitation. - Highlights: • The Mn, Sc and Zr additions to Al totally suppresses recrystallization at 550 °C. • The Sc,Zr-containing particle precipitation is slightly facilitated by cold rolling. • The Mn-containing particle precipitation is highly enhanced by cold rolling. • Cold rolling has no effect on activation energy of the Al{sub 3}Sc and Al{sub 6}Mn precipitation. • The texture development is affected by high solid solution strengthening by Mn.« less
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NASA Astrophysics Data System (ADS)
Hordych, Illia; Rodman, Dmytro; Nürnberger, Florian; Schmidt, Hans Christian; Orive, Alejandro Gonzalez; Homberg, Werner; Grundmeier, Guido; Maier, Hans Jürgen
2018-05-01
In the present study, heat-treatment assisted bonding of galfan-coated low-carbon steel sheets was investigated. Steel sheets were bonded by cold rolling subsequently to a heat treatment in the temperature range from 400 °C to 550°C. The reduction ratio during cold rolling was varied in the range from 50% to 80%. Such high reduction ratios were achieved by splitting the bonding process into three stages. By employing heat-treatments, the mechanical properties of the bonds were improved. The heat-pretreatment allowed the formation of brittle intermetallic phases that were easily fractured in the rolling gap during the bonding process. Thus, juvenile non-oxidized surfaces were formed, which facilitated the bonding between the steel layers, and thus increased the bond strength. The intermetallic phases were actively formed at temperatures of 450 °C and above; however increasing temperatures resulted in decreasing mechanical properties due to oxidation processes. The local microstructure was analyzed by scanning electron microscopy in order to characterize the contact zone on the micro level with a focus on the formation of intermetallic phases. The mechanical properties were determined in tensile shear tests. Interestingly, it was found that the galfan coating allowed for bonding at room temperature, and the aluminum fraction was primarily responsible for the enhanced oxide formation during the heat-pretreatment.
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NASA Astrophysics Data System (ADS)
Stockert, Sven; Wehr, Matthias; Lohmar, Johannes; Abel, Dirk; Hirt, Gerhard
2017-10-01
In the electrical and medical industries the trend towards further miniaturization of devices is accompanied by the demand for smaller manufacturing tolerances. Such industries use a plentitude of small and narrow cold rolled metal strips with high thickness accuracy. Conventional rolling mills can hardly achieve further improvement of these tolerances. However, a model-based controller in combination with an additional piezoelectric actuator for high dynamic roll adjustment is expected to enable the production of the required metal strips with a thickness tolerance of +/-1 µm. The model-based controller has to be based on a rolling theory which can describe the rolling process very accurately. Additionally, the required computing time has to be low in order to predict the rolling process in real-time. In this work, four rolling theories from literature with different levels of complexity are tested for their suitability for the predictive controller. Rolling theories of von Kármán, Siebel, Bland & Ford and Alexander are implemented in Matlab and afterwards transferred to the real-time computer used for the controller. The prediction accuracy of these theories is validated using rolling trials with different thickness reduction and a comparison to the calculated results. Furthermore, the required computing time on the real-time computer is measured. Adequate results according the prediction accuracy can be achieved with the rolling theories developed by Bland & Ford and Alexander. A comparison of the computing time of those two theories reveals that Alexander's theory exceeds the sample rate of 1 kHz of the real-time computer.
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LANL Experience Rolling Zr-Clad LEU-10Mo Foils for AFIP-7
DOE Office of Scientific and Technical Information (OSTI.GOV)
Hammon, Duncan L.; Clarke, Kester D.; Alexander, David J.
2015-05-29
The cleaning, canning, rolling and final trimming of Low Enriched Uranium-10 wt. pct. Molybdenum (LEU-10Mo) foils for ATR (Advanced Test Reactor) fuel plates to be used in the AFIP-7 (ATR Full Size Plate In Center Flux Trap Position) experiments are summarized. Six Zr-clad foils were produced from two LEU-10Mo castings supplied to Los Alamos National Laboratory (LANL) by Y-12 National Security Complex. Details of cleaning and canning procedures are provided. Hot- and cold-rolling results are presented, including rolling schedules, images of foils in-process, metallography and local compositions of regions of interest, and details of final foil dimensions and process yield.more » This report was compiled from the slides for the presentation of the same name given by Duncan Hammon on May 12, 2011 at the AFIP-7 Lessons Learned meeting in Salt Lake City, UT, with Los Alamos National Laboratory document number LA-UR 11-02898.« less
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NASA Astrophysics Data System (ADS)
Li, Jiheng; Liu, Yangyang; Li, Xiaojuan; Mu, Xing; Bao, Xiaoqian; Gao, Xuexu
2018-07-01
The effects of different rolling conditions on the microstructure and texture of primary and secondary recrystallization in magnetostrictive Fe82Ga9Al9+0.1at%NbC alloy sheets were investigated. After the primary recrystallization annealing at 850 °C for 5 min, the as-rolled sheets prepared by warm-cold rolling with an intermediate annealing, can be fully recrystallized, and obtain the homogeneous matrix in which the fine dispersed NbC precipitate particles are distributed. The primary recrystallization textures of sheets with different rolling conditions consist mostly of strong {1 0 0} textures, γ-fiber textures, {4 1 1}〈1 4 8〉 texture and weak Goss texture. In the primary recrystallized sheets prepared by warm-cold rolling with an intermediate annealing, the high energy grain boundaries and ∑9 boundaries have the highest proportion. After high temperature annealing, the secondary recrystallizations of Goss grains in these sheets are more complete, and the size of abnormal grown Goss grain is up to several centimeters, which results in the strongest Goss texture. Correspondingly, the largest magnetostriction of 183 ppm is observed. The sample prepared by warm-cold rolling with an intermediate annealing, has homogeneous primary matrix, special texture components and grain boundary distribution, all of which provide a better surrounding for the abnormal growth of Goss grains. This work indicates that the control of rolling conditions of Fe-Ga-Al alloy sheets is necessary to achieve the strong Goss texture and obtain a possible high magnetostriction if other appropriate conditions (stress, domain structure) are achieved.
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NASA Astrophysics Data System (ADS)
Garber, E. A.; Timofeeva, M. A.
2016-11-01
New propositions are introduced into the technique of energy-force calculation of pinch-pass mills in order to determine the energy-force and technological parameters of skin rolling of cold-rolled steel strips at the minimum errors. The application of these propositions decreases the errors of calculating the forces and torques in a working stand by a factor of 3-5 as compared to the calculation according to the well-known technique, saves the electric power in the existing mills, and demonstrates the possibility of decreasing the dimensions of working stands and the power of the rolling mill engine.
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Guan, Ben; Zang, Yong; Han, Xiaohui; Zheng, Kailun
2018-01-01
Driven by the demands for contactless stress detection, technologies are being used for shape control when producing cold-rolled strips. This paper presents a novel contactless stress detection technology based on a magnetoresistance sensor and the magnetoelastic effect, enabling the detection of internal stress in manufactured cold-rolled strips. An experimental device was designed and produced. Characteristics of this detection technology were investigated through experiments assisted by theoretical analysis. Theoretically, a linear correlation exists between the internal stress of strip steel and the voltage output of a magneto-resistive sensor. Therefore, for this stress detection system, the sensitivity of the stress detection was adjusted by adjusting the supply voltage of the magnetoresistance sensor, detection distance, and other relevant parameters. The stress detection experimental results showed that this detection system has good repeatability and linearity. The detection error was controlled within 1.5%. Moreover, the intrinsic factors of the detected strip steel, including thickness, carbon percentage, and crystal orientation, also affected the sensitivity of the detection system. The detection technology proposed in this research enables online contactless detection and meets the requirements for cold-rolled steel strips. PMID:29883387
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Guan, Ben; Zang, Yong; Han, Xiaohui; Zheng, Kailun
2018-05-21
Driven by the demands for contactless stress detection, technologies are being used for shape control when producing cold-rolled strips. This paper presents a novel contactless stress detection technology based on a magnetoresistance sensor and the magnetoelastic effect, enabling the detection of internal stress in manufactured cold-rolled strips. An experimental device was designed and produced. Characteristics of this detection technology were investigated through experiments assisted by theoretical analysis. Theoretically, a linear correlation exists between the internal stress of strip steel and the voltage output of a magneto-resistive sensor. Therefore, for this stress detection system, the sensitivity of the stress detection was adjusted by adjusting the supply voltage of the magnetoresistance sensor, detection distance, and other relevant parameters. The stress detection experimental results showed that this detection system has good repeatability and linearity. The detection error was controlled within 1.5%. Moreover, the intrinsic factors of the detected strip steel, including thickness, carbon percentage, and crystal orientation, also affected the sensitivity of the detection system. The detection technology proposed in this research enables online contactless detection and meets the requirements for cold-rolled steel strips.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Chang, E-E; Pan, Shu-Yuan; Yang, Liuhanzi
2015-09-15
Highlights: • Carbonation was performed using CO{sub 2}, wastewater and bottom ash in a slurry reactor. • A maximum capture capacity of 102 g CO{sub 2} per kg BA was achieved at mild conditions. • A maximum carbonation conversion of MSWI-BA was predicted to be 95% by RSM. • The CO{sub 2} emission from Bali incinerator could be expected to reduce by 6480 ton/y. • The process energy consumption per ton CO{sub 2} captured was estimated to be 180 kW h. - Abstract: Accelerated carbonation of alkaline wastes including municipal solid waste incinerator bottom ash (MSWI-BA) and the cold-rolling wastewatermore » (CRW) was investigated for carbon dioxide (CO{sub 2}) fixation under different operating conditions, i.e., reaction time, CO{sub 2} concentration, liquid-to-solid ratio, particle size, and CO{sub 2} flow rate. The MSWI-BA before and after carbonation process were analyzed by the thermogravimetry and differential scanning calorimetry, X-ray diffraction, and scanning electron microscopy equipped with energy dispersive X-ray spectroscopy. The MSWI-BA exhibits a high carbonation conversion of 90.7%, corresponding to a CO{sub 2} fixation capacity of 102 g per kg of ash. Meanwhile, the carbonation kinetics was evaluated by the shrinking core model. In addition, the effect of different operating parameters on carbonation conversion of MSWI-BA was statistically evaluated by response surface methodology (RSM) using experimental data to predict the maximum carbonation conversion. Furthermore, the amount of CO{sub 2} reduction and energy consumption for operating the proposed process in refuse incinerator were estimated. Capsule abstract: CO{sub 2} fixation process by alkaline wastes including bottom ash and cold-rolling wastewater was developed, which should be a viable method due to high conversion.« less
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An advanced dissymmetric rolling model for online regulation
NASA Astrophysics Data System (ADS)
Cao, Trong-Son
2017-10-01
Roll-bite model is employed to predict the rolling force, torque as well as to estimate the forward slip for preset or online regulation at industrial rolling mills. The rolling process is often dissymmetric in terms of work-rolls rotation speeds and diameters as well as the friction conditions at upper and lower contact surfaces between work-rolls and the strip. The roll-bite model thus must be able to account for these dissymmetries and in the same time has to be accurate and fast enough for online applications. In the present study, a new method, namely Adapted Discretization Slab Method (ADSM) is proposed to obtain a robust roll-bite model, which can take into account the aforementioned dissymmetries and has a very short response time, lower than one millisecond. This model is based on the slab method, with an adaptive discretization and a global Newton-Raphson procedure to improve the convergence speed. The model was validated by comparing with other dissymmetric models proposed in the literature, as well as Finite Element simulations and industrial pilot trials. Furthermore, back-calculation tool was also constructed for friction management for both offline and online applications. With very short CPU time, the ADSM-based model is thus attractive for all online applications, both for cold and hot rolling.
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NASA Astrophysics Data System (ADS)
Kasaei, M. M.; Naeini, H. Moslemi; Tehrani, M. Salmani; Tafti, R. Azizi
2011-01-01
Cage roll forming is one of the advanced methods of cold roll forming process which is used widely for producing ERW pipes. In addition to decreasing the production cost and time, using cage roll forming provides smooth deformation on the strip. Few studies can be found about cage roll forming because of its complexity, and the available knowledge is experience-based more than science-based. In this paper, deformation of pipes with low ratio of thickness/diameter is investigated by 3D finite element simulation in Marc-Mentat software. Edge buckling defect in cage roll forming of low ratio of thickness/diameter pipes is very important. Due to direct influence of longitudinal strain on the edge buckling phenomenon, longitudinal strains at the edge and center line of the strip are investigated and high risk stands are introduced. The deformed strip is predicted using the simulation results and effects of each cage forming stage on the deformed strip profile are specified. In order to verify the simulation results, strip width and opening distance of the two edges in different forming stages are obtained from the simulations and compared with the experimental data which were measured from the production line. A good agreement between the experimental and simulated results is observed.
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40 CFR 420.100 - Applicability; description of the cold forming subcategory.
Code of Federal Regulations, 2010 CFR
2010-07-01
... (CONTINUED) EFFLUENT GUIDELINES AND STANDARDS IRON AND STEEL MANUFACTURING POINT SOURCE CATEGORY Cold Forming... works from cold rolling and cold working pipe and tube operations in which unheated steel is passed... controlled mechanical properties in the steel. (b) The limitations and standards set out below for cold...
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Static Recovery Modeling of Dislocation Density in a Cold Rolled Clad Aluminum Alloy
NASA Astrophysics Data System (ADS)
Penlington, Alex
Clad alloys feature one or more different alloys bonded to the outside of a core alloy, with non-equilibrium, interalloy interfaces. There is limited understanding of the recovery and recrystallization behaviour of cold rolled clad aluminum alloys. In order to optimize the properties of such alloys, new heat treatment processes may be required that differ from what is used for the monolithic alloys. This study examines the recovery behaviour of a cold rolled Novelis Fusion(TM) alloy containing an AA6XXX core with an AA3003 cladding on one side. The bond between alloys appears microscopically discrete and continuous, but has a 30 microm wide chemical gradient. The as-deformed structure at the interalloy region consists of pancaked sub-grains with dislocations at the misorientation boundaries and a lower density organized within the more open interiors. X-ray line broadening was used to extract the dislocation density from the interalloy region and an equivalently deformed AA6XXX following static annealing using a modified Williamson-Hall analysis. This analysis assumed that Gaussian broadening contributions in a pseudo-Voigt function corresponded only to strain from dislocations. The kinetics of the dislocation density evolution to recrystallization were studied isothermally at 2 minute intervals, and isochronally at 175 and 205°C. The data fit the Nes model, in which the interalloy region recovered faster than AA6XXX at 175°C, but was slower at 205°C. This was most likely caused by change in texture and chemistry within this region such as over-aging of AA6XXX . Simulation of a continuous annealing and self homogenization process both with and without pre-recovery indicates a detectable, though small change in the texture and grain size in the interalloy region.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Mubarok, Naila; Manaf, Azwar, E-mail: azwar@ui.ac.id; Notonegoro, Hamdan Akbar
The 304 stainless steel (SS) type is widely used in oil and gas operations due to its excellent corrosion resistance. However, the presence of the fine sand particles and H{sub 2}S gas contained in crude oil could lead the erosion and abrasion in steel. In this study, cold rolled treatments were conducted to the 304 SS in order to increase the wear resistance of the steel. The cold work has resulted in thickness reduction to 20%, 40% and 60% of the original. Various microstructural characterizations were used to analyze the effect of deformation. The hardness characterization showed that the initialmore » hardness value increased from 145 HVC to 395 HVC as the level of deformation increase. Further, the wear resistance increased with the deformation rate from 0% to 40% and subsequently decreased from 40% to 60% deformation rate. Microstructural characterization shows that the boundary change to coincide by 56 µm, 49 µm, 45 µm, and 43 µm width and the grain go to flatten and being folded like needles. The effect of deformation on the grain morphology and structure was also studied by optical metallography and X-Ray Diffraction. It is shown that the deformation by means of a cold rolled process has transformed the austenite structure into martensitic structure.« less
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Progress in cold roll bonding of metals
Li, Long; Nagai, Kotobu; Yin, Fuxing
2008-01-01
Layered composite materials have become an increasingly interesting topic in industrial development. Cold roll bonding (CRB), as a solid phase method of bonding same or different metals by rolling at room temperature, has been widely used in manufacturing large layered composite sheets and foils. In this paper, we provide a brief overview of a technology using layered composite materials produced by CRB and discuss the suitability of this technology in the fabrication of layered composite materials. The effects of process parameters on bonding, mainly including process and surface preparation conditions, have been analyzed. Bonding between two sheets can be realized when deformation reduction reaches a threshold value. However, it is essential to remove surface contamination layers to produce a satisfactory bond in CRB. It has been suggested that the degreasing and then scratch brushing of surfaces create a strong bonding between the layers. Bonding mechanisms, in which the film theory is expressed as the major mechanism in CRB, as well as bonding theoretical models, have also been reviewed. It has also been showed that it is easy for bcc structure metals to bond compared with fcc and hcp structure metals. In addition, hardness on bonding same metals plays an important part in CRB. Applications of composites produced by CRB in industrial fields are briefly reviewed and possible developments of CRB in the future are also described. PMID:27877949
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NASA Astrophysics Data System (ADS)
Derevyagina, L. S.; Gordienko, A. I.; Pochivalov, Yu. I.; Smirnova, A. S.
2018-01-01
The paper reports the investigation results on the microstructure and mechanical properties of low-carbon pipe steel after helical rolling. The processing of the steel leads to the refinement of ferritic grains from 12 (for the coarse-grained state) to 5 μm, to the strengthening of ferrite by carbide particles, a decrease in the total fraction of perlite grains, a more uniform alternation of ferrite and perlite, and the formation of regions with bainitic structure. The mechanical properties of the steel have been determined in the conditions of static and dynamic loading in the range of test temperatures from +20 to-70°C. As a result of processing, the ultimate tensile strength increases (from 650 to 770 MPa at a rolling temperature from 920°C) and the viscoplastic properties at negative temperatures are improved significantly. The ductile-brittle transition temperature of the rolled steel decreases from-32 to-55°C and the impact toughness at the test temperature-40°C increases eight times compared to the initial state of the steel.
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NASA Astrophysics Data System (ADS)
Baranov, Vladimir; Sidelnikov, Sergey; Zenkin, Evgeny; Frolov, Viktor; Voroshilov, Denis; Yakivyuk, Olga; Konstantinov, Igor; Sokolov, Ruslan; Belokonova, Irina
2018-04-01
The results of a study on the strength of rolled products from aluminium alloys doped with scandium under various processing conditions of hot and cold rolling are presented. The regularities of metal flow and the level of strength of deformed semi-finished products from aluminum-scandium alloys are established, depending on the total degree of deformation and the various modes of single reduction during rolling. It is shown that when using one heating of a cast billet to obtain high-quality semi-finished products, the temperature during the rolling process should not be lower than 350-370°, and the total degree of deformation does not exceed 50-60%. It was found that the semi-finished products from alloys with a content of scandium in the range 0.11-0.12% in the deformed state had elevated values of ultimate tensile strength and yield strength of the metal, which allows them to be recommended for industrial production of sheet metal products.
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NASA Astrophysics Data System (ADS)
Roy, Rajat K.; Dutta, Siuli; Panda, Ashis K.; Rajinikanth, V.; Das, Swapan K.; Mitra, Amitava; Strangwood, M.; Davis, Claire L.
2018-07-01
The recovery and recrystallisation behaviours of cold rolled IF steel have been investigated by destructive (optical microscopy and hardness) and non-destructive electromagnetic sensor, (which allows direct measurement of strip samples with no surface preparation) techniques. The onset and completion of recrystallisation are clearly monitored through destructive techniques of optical microscopy and hardness measurements. The nucleation of new recrystallised grains is observed in the sample annealed at 600 °C/15 min, while completion of recrystallisation takes place at 700 °C/15 min. The destructive techniques are not very accurate in monitoring recovery, for example, changes in hardness of <20% are seen. In contrast, the magnetic properties of annealed steel show the onsets of both recovery and recrystallisation, with recovery accounting for ≈60% change in the coercivity value. Therefore, the measurement of magnetic softening through an electromagnetic sensor acts a crucial role for understanding recovery and recrystallisation behaviours of steels during industrial processing. The present investigation is aimed not only for controlling product quality but also saving characterisation time through off line monitoring during steel processing at industry.
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Method for improving the mechanical properties of uranium-1 to 3 wt % zirconium alloy
Anderson, R.C.
1983-11-22
A uranium-1 to 3 wt % zirconium alloy characterized by high strength, high ductility and stable microstructure is fabricated by an improved thermal mechanical process. A homogenous ingot of the alloy which has been reduced in thickness of at least 50% in the two-step forging operation, rolled into a plate with a 75% reduction and then heated in vacuum at a temperature of about 750 to 850/sup 0/C and then quenched in water, is subjected to further thermal-mechanical operation steps to increase the compressive yield strength approximately 30%, stabilize the microstructure, and decrease the variations in mechanical properties throughout the plate is provided. These thermal-mechanical steps are achieved by cold rolling the quenchd plate to reduce the thickness thereof about 8 to 12%, aging the cold rolled plate at a first temperature of about 325 to 375/sup 0/C for five to six hours and then aging the plate at a higher temperature ranging from 480 to 500/sup 0/C for five to six hours prior to cooling the billet to ambient conditions and sizing the billet or plate into articles provides the desired increase in mechanical properties and phase stability throughout the plate.
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NASA Astrophysics Data System (ADS)
Modak, Pranabananda; Patra, Sudipta; Mitra, Rahul; Chakrabarti, Debalay
2018-03-01
Effect of the initial as-cast structure on the microstructure-texture evolution during thermomechanical processing of 409L grade ferritic stainless steel was studied. Samples from the regions of cast slab having `columnar,' `equiaxed,' and a mixture of `columnar' and `equiaxed' grains were subjected to two different processing schedules: one with intermediate hot-band annealing before cold-rolling followed by final annealing, and another without any hot-band annealing. EBSD study reveals that large columnar crystals with cube orientation are very difficult to deform and recrystallize uniformly. Resultant variations in ferrite grain structure and retention of cube-textured band in cold-rolled and annealed sheet contribute to ridging behavior during stretch forming. Initial equiaxed grain structure is certainly beneficial to reduce or even eliminate ridging defect by producing uniform ferrite grain structure, free from any texture banding. Application of hot-band annealing treatment is also advantageous as it can maximize the evolution of beneficial gamma-fiber texture and eliminate the ridging defect in case of completely `equiaxed' starting structure. Such treatment reduces the severity of ridging even if the initial structure contains typically mixed `columnar-equiaxed' grains.
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NASA Astrophysics Data System (ADS)
Modak, Pranabananda; Patra, Sudipta; Mitra, Rahul; Chakrabarti, Debalay
2018-06-01
Effect of the initial as-cast structure on the microstructure-texture evolution during thermomechanical processing of 409L grade ferritic stainless steel was studied. Samples from the regions of cast slab having `columnar,' `equiaxed,' and a mixture of `columnar' and `equiaxed' grains were subjected to two different processing schedules: one with intermediate hot-band annealing before cold-rolling followed by final annealing, and another without any hot-band annealing. EBSD study reveals that large columnar crystals with cube orientation are very difficult to deform and recrystallize uniformly. Resultant variations in ferrite grain structure and retention of cube-textured band in cold-rolled and annealed sheet contribute to ridging behavior during stretch forming. Initial equiaxed grain structure is certainly beneficial to reduce or even eliminate ridging defect by producing uniform ferrite grain structure, free from any texture banding. Application of hot-band annealing treatment is also advantageous as it can maximize the evolution of beneficial gamma-fiber texture and eliminate the ridging defect in case of completely `equiaxed' starting structure. Such treatment reduces the severity of ridging even if the initial structure contains typically mixed `columnar-equiaxed' grains.
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Tribological investigation of oriented HDPE.
Hoseini, Mohammed; Lausmaa, Jukka; Boldizar, Antal
2002-09-15
The possibility to control the wear properties of high-density polyethylene (HDPE) material at an early processing stage is explored. Wear measurements of cold roll-drawn HDPE with two different draw ratios were carried out for three sliding planes, each in two directions. The dependence of the wear properties on the degree and direction of orientation was investigated. The experiments were performed in a pin-on-disc machine in a dry environment. The tribo-couple consisted of HDPE plates versus a standardised diamond coated steel disc. The results show that the wear resistance of cold roll-drawn HDPE differ widely, by a factor up to 6, depending on the sliding direction relative to the drawing direction. The material has a significantly better wear resistance when the sliding direction was perpendicular to the processing direction. The best wear resistance was in the end plane and it was improved by a factor up to 3.6 when the draw ratio was increased from 2 to 4. These results indicate that molecular orientation by polymer processing is a promising method to improve the wear properties and decrease the wear debris production of HDPE. Copyright 2002 Wiley Periodicals, Inc.
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Strengthening of Aluminum Wires Treated with A206/Alumina Nanocomposites.
Florián-Algarín, David; Marrero, Raúl; Li, Xiaochun; Choi, Hongseok; Suárez, Oscar Marcelo
2018-03-10
This study sought to characterize aluminum nanocomposite wires that were fabricated through a cold-rolling process, having potential applications in TIG (tungsten inert gas) welding of aluminum. A206 (Al-4.5Cu-0.25Mg) master nanocomposites with 5 wt % γAl₂O₃ nanoparticles were first manufactured through a hybrid process combining semi-solid mixing and ultrasonic processing. A206/1 wt % γAl₂O₃ nanocomposites were fabricated by diluting the prepared master nanocomposites with a monolithic A206 alloy, which was then added to a pure aluminum melt. The fabricated Al-γAl₂O₃ nanocomposite billet was cold-rolled to produce an Al nanocomposite wire with a 1 mm diameter and a transverse area reduction of 96%. Containing different levels of nanocomposites, the fabricated samples were mechanically and electrically characterized. The results demonstrate a significantly higher strength of the aluminum wires with the nanocomposite addition. Further, the addition of alumina nanoparticles affected the wires' electrical conductivity compared with that of pure aluminum and aluminum-copper alloys. The overall properties of the new material demonstrate that these wires could be an appealing alternative for fillers intended for aluminum welding.
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Strengthening of Aluminum Wires Treated with A206/Alumina Nanocomposites
Marrero, Raúl; Li, Xiaochun; Choi, Hongseok
2018-01-01
This study sought to characterize aluminum nanocomposite wires that were fabricated through a cold-rolling process, having potential applications in TIG (tungsten inert gas) welding of aluminum. A206 (Al-4.5Cu-0.25Mg) master nanocomposites with 5 wt % γAl2O3 nanoparticles were first manufactured through a hybrid process combining semi-solid mixing and ultrasonic processing. A206/1 wt % γAl2O3 nanocomposites were fabricated by diluting the prepared master nanocomposites with a monolithic A206 alloy, which was then added to a pure aluminum melt. The fabricated Al–γAl2O3 nanocomposite billet was cold-rolled to produce an Al nanocomposite wire with a 1 mm diameter and a transverse area reduction of 96%. Containing different levels of nanocomposites, the fabricated samples were mechanically and electrically characterized. The results demonstrate a significantly higher strength of the aluminum wires with the nanocomposite addition. Further, the addition of alumina nanoparticles affected the wires’ electrical conductivity compared with that of pure aluminum and aluminum–copper alloys. The overall properties of the new material demonstrate that these wires could be an appealing alternative for fillers intended for aluminum welding. PMID:29534441
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Federal Register 2010, 2011, 2012, 2013, 2014
2013-11-19
... Memorandum 1. Background 2. Scope of the Investigation 3. Respondent Selection 4. Discussion of Methodology a...: Scope of the Investigation The diffusion-annealed, nickel-plated flat-rolled steel products included in this investigation are flat-rolled, cold-reduced steel products, regardless of chemistry; whether or...
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Microplastic Deformation of Submicrocrystalline Copper at Room and Elevated Temperatures
NASA Astrophysics Data System (ADS)
Dudarev, E. F.; Pochivalova, G. P.; Tabachenko, A. N.; Maletkina, T. Yu.; Skosyrskii, A. B.; Osipov, D. A.
2017-02-01
of investigations of submicrocrystalline copper subjected to cold rolling after abc pressing by methods of backscatter electron diffraction and x-ray diffraction analysis are presented. It is demonstrated that after such combined intensive plastic deformation, the submicrocrystalline structure with average grain-subgrain structure elements having sizes of 0.63 μm is formed with relative fraction of high-angle grain boundaries of 70% with texture typical for rolled copper. Results of investigation of microplastic deformation of copper with such structure at temperatures in the interval 295-473 K and with submicrocrystalline structure formed by cold rolling of coarse-grained copper are presented.
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Recycle of valuable products from oily cold rolling mill sludge
NASA Astrophysics Data System (ADS)
Liu, Bo; Zhang, Shen-gen; Tian, Jian-jun; Pan, De-an; Liu, Yang; Volinsky, Alex A.
2013-10-01
Oily cold rolling mill (CRM) sludge contains lots of iron and alloying elements along with plenty of hazardous organic components, which makes it as an attractive secondary source and an environmental contaminant at the same time. The compound methods of "vacuum distillation + oxidizing roasting" and "vacuum distillation + hydrogen reduction" were employed for the recycle of oily cold rolling mill sludge. First, the sludge was dynamically vacuum distilled in a rotating furnace at 50 r/min and 600°C for 3 h, which removed almost hazardous organic components, obtaining 89.2wt% ferrous resultant. Then, high purity ferric oxide powders (99.2wt%) and reduced iron powders (98.9wt%) were obtained when the distillation residues were oxidized and reduced, respectively. The distillation oil can be used for fuel or chemical feedstock, and the distillation gases can be collected and reused as a fuel.
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NASA Astrophysics Data System (ADS)
Wang, Xianglong; Li, Haoze; Zhang, Weina; Liu, Zhenyu; Wang, Guodong; Luo, Zhonghan; Zhang, Fengquan
2016-09-01
As-cast strip of 6.5 wt pct Si steel was fabricated by twin-roll strip casting. After hot rolling at 1323 K (1050 °C), thin sheets with the thickness of 0.35 mm were produced by warm rolling at 373 K (100 °C) with rolling reductions of 15, 25, 35, 45, 55, and 65 pct. Influence of warm rolling reduction on ductility was investigated by room temperature bending test. The measurement of macro-hardness showed that "work softening" could begin when the warm rolling reduction exceeded 35 pct. The room temperature ductility of the thin sheets gradually increased with the increase of warm rolling reductions, and the plastic deformation during bending began to form when the warm rolling reduction was greater than 45 pct, the 65 pct rolled thin sheet exhibited the maximum plastic deformation of about 0.6 pct during bending at room temperature, with a few small dimples having been observed on the fracture surfaces. B2-ordered domains were formed in the 15, 25, 35, 45, and 55 pct rolled specimens, and their average size decreased with the increase of warm rolling reductions. By contrast, no B2-ordered domain could be found in the 65 pct rolled specimen. It had been observed that large-ordered domains could be split into several small parts by the slip of partial super-dislocations during warm rolling, which led to significant decrease of the order degree to cause the phenomenon of deformation-induced disordering. On the basis of these results, cold rolling schedule was developed to successfully fabricate 0.25-mm-thick sheets with good surface qualities and magnetic properties from warm rolled sheets.
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2011-08-01
the Texture Evolution During Cold Rolling of Al –Mg Alloys . s.l.: Journal of Alloys and Compounds 2011, 508, 922–928. 11. Suhuddin, U.F.H.R.; Mironov...graphene onto a substrate with insulator properties . The current transfer process is still preliminary and presents a number of challenges. Since the...dimensions. The fabrication process flow for the stators uses chemical solution deposited PZT, metal sputtering and evaporation, reactive ion etching
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Klimova, Margarita; Stepanov, Nikita; Shaysultanov, Dmitry; Chernichenko, Ruslan; Yurchenko, Nikita; Sanin, Vladimir; Zherebtsov, Sergey
2017-12-29
The effect of cold rolling on the microstructure and mechanical properties of an Al- and C-containing CoCrFeNiMn-type high-entropy alloy was reported. The alloy with a chemical composition (at %) of (20-23) Co, Cr, Fe, and Ni; 8.82 Mn; 3.37 Al; and 0.69 C was produced by self-propagating high-temperature synthesis with subsequent induction. In the initial as-cast condition the alloy had an face centered cubic single-phase coarse-grained structure. Microstructure evolution was mostly associated with either planar dislocation glide at relatively low deformation during rolling (up to 20%) or deformation twinning and shear banding at higher strain. After 80% reduction, a heavily deformed twinned/subgrained structure was observed. A comparison with the equiatomic CoCrFeNiMn alloy revealed higher dislocation density at all stages of cold rolling and later onset of deformation twinning that was attributed to a stacking fault energy increase in the program alloy; this assumption was confirmed by calculations. In the initial as-cast condition the alloy had low yield strength of 210 MPa with yet very high uniform elongation of 74%. After 80% rolling, yield strength approached 1310 MPa while uniform elongation decreased to 1.3%. Substructure strengthening was found to be dominated at low rolling reductions (<40%), while grain (twin) boundary strengthening prevailed at higher strains.
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Rolling-element fatigue life of AMS 5900 balls
NASA Technical Reports Server (NTRS)
Parker, R. J.
1983-01-01
The rolling-element fatigue life of AMS 5900 12.7-mm (1/2-in.) dia was determined in five-ball fatigue testers. The 10% life with the warm headed AMS 5900 balls was equivalent to that of AMS 5749 and over eight times that of AISI M-50. The AMS balls fabricated by cold heading had small surface cracks which initiated fatigue spalls where these cracks were crossed by running tracks. The cold-headed AMS 5900 balls had a 10% fatigue life an order of magnitude less than that of the warm headed balls even when failures on the cold headed balls at visible surface cracks were omitted.
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Fiber vs Rolling Texture: Stress State Dependence for Cold-Drawn Wire
NASA Astrophysics Data System (ADS)
Zorina, M. A.; Karabanalov, M. S.; Stepanov, S. I.; Demakov, S. L.; Loginov, Yu. N.; Lobanov, M. L.
2018-02-01
The texture of the cold-drawn copper wire was investigated along the radius using electron backscatter diffraction. The complex fiber texture of the central region of the wire was considered as the rolling texture consisting of a set of preferred orientations. The texture of the periphery region was revealed to be similar to the shear texture. The orientation-dependent properties of the wire were proven to be determined by the texture of the near-surface layers.
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Microscopic Observations of Adiabatic Shear Bands in Three Different Steels
1988-09-01
low thermal conductivity, and a high thermal softening rate. Examples include alloys of titanium. aluminum, copper , as well as steels [5-221... steels : 1 (1) an AISI 1018 cold rolled steel , (2) a high strength low alloy structural steel , and deformation in shear was impo.ed to produce shear bands...stecls: (1) an AISI 1018 cold rolled steel , (2) a high strength low alloy structural steel , and (3) an AISI 4340 VAR steel tempered
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Numerical simulation on chain-die forming of an AHSS top-hat section
NASA Astrophysics Data System (ADS)
Majji, Raju; Xiang, Yang; Ding, Scott; Yang, Chunhui
2018-05-01
The applications of Advanced High-Strength Steels (AHSS) in the automotive industry are rapidly increasing due to a demand for a lightweight material that significantly reduces fuel consumption without compromising passenger safety. Automotive industries and material suppliers are expected by consumers to deliver reliable and affordable products, thus stimulating these manufacturers to research solutions to meet these customer requirements. The primary advantage of AHSS is its extremely high strength to weight ratio, an ideal material for the automotive industry. However, its low ductility is a major disadvantage, in particular, when using traditional cold forming processes such as roll forming and deep drawing process to form profiles. Consequently, AHSS parts frequently fail to form. Thereby, in order to improve quality and reliability on manufacturing AHSS products, a recently-developed incremental cold sheet metal forming technology called Chain-die Forming (CDF) is recognised as a potential solution to the forming process of AHSS. The typical CDF process is a combination of bending and roll forming processes which is equivalent to a roll with a large deforming radius, and incrementally forms the desired shape with split die and segments. This study focuses on manufacturing an AHSS top-hat section with minimum passes without geometrical or surface defects by using finite element modelling and simulations. The developed numerical simulation is employed to investigate the influences on the main control parameter of the CDF process while forming AHSS products and further develop new die-punch sets of compensation design via a numerical optimal process. In addition, the study focuses on the tool design to compensate spring-back and reduce friction between tooling and sheet-metal. This reduces the number of passes, thereby improving productivity and reducing energy consumption and material waste. This numerical study reveals that CDF forms AHSS products of complex profiles with much less residual stress, low spring back, low strain and of higher geometrical accuracy compared to other traditional manufacturing processes.
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NASA Astrophysics Data System (ADS)
Park, Keecheol; Oh, Kyungsuk
2017-09-01
In order to investigate the effect of leveling conditions on residual stress evolution during the leveling process of hot rolled high strength steels, the in-plane residual stresses of sheet processed under controlled conditions at skin-pass mill and levelers were measured by cutting method. The residual stress was localized near the edge of sheet. As the thickness of sheet was increased, the residual stress occurred region was expanded. The magnitude of residual stress within the sheet was reduced as increasing the deformation occurred during the leveling process. But the residual stress itself was not removed completely. The magnitude of camber occurred at cut plate was able to be predicted by the residual stress distribution. A numerical algorithm was developed for analysing the effect of leveling conditions on residual stress. It was able to implement the effect of plastic deformation in leveling, tension, work roll bending, and initial state of sheet (residual stress and curl distribution). The validity of simulated results was verified from comparison with the experimentally measured residual stress and curl in a sheet.
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40 CFR 468.14 - Pretreatment standards for existing sources (PSES).
Code of Federal Regulations, 2010 CFR
2010-07-01
... for monthly average Metric units—mg/off-kg of copper or copper alloy hot rolled English units—pounds... rolled English units—pounds per 1,000,000 off-pounds of copper or copper alloy cold rolled Chromium 0.166... copper or copper alloy drawn English units—pounds per 1,000,000 off-pounds of copper or copper alloy...
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NASA Astrophysics Data System (ADS)
Sai Srinadh, K. V.; Singh, Vakil
2007-08-01
Cold rolling of the titanium alloy Timetal 834 was found to cause marked enhancement in low-cycle fatigue (LCF) life at low strain amplitude and to eliminate bilinear behavior from the Coffin Manson (C-M) relationship. It was due to work hardening of surface grains of soft orientation and consequent increase in resistance of the material against crack initiation. The observed effect was not associated with texture.
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Federal Register 2010, 2011, 2012, 2013, 2014
2012-09-04
... Southwest Cold Weather Event Follow-up Technical Conference; Notice of Technical Conference Take notice that... August 16, 2011 Report on Outages and Curtailments During the Southwest Cold Weather Event of February 1... severe cold weather issues that led to rolling blackouts affecting over 4 million customers and natural...
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Anderson, Robert C.
1986-01-01
A uranium-1 to 3 wt. % zirconium alloy characterized by high strength, high ductility and stable microstructure is fabricated by an improved thermal mechanical process. A homogenous ingot of the alloy which has been reduced in thickness of at least 50% in the two-step forging operation, rolled into a plate with a 75% reduction and then heated in vacuum at a temperature of about 750.degree. to 850.degree. C. and then quenched in water is subjected to further thermal-mechanical operation steps to increase the compressive yield strength approximately 30%, stabilize the microstructure, and decrease the variations in mechanical properties throughout the plate is provided. These thermal-mechanical steps are achieved by cold rolling the quenched plate to reduce the thickness thereof about 8 to 12%, aging the cold rolled plate at a first temperature of about 325.degree. to 375.degree. C. for five to six hours and then aging the plate at a higher temperature ranging from 480.degree. to 500.degree. C. for five to six hours prior to cooling the billet to ambient conditions and sizing the billet or plate into articles provides the desired increase in mechanical properties and phase stability throughout the plate.
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Finite element modelling of chain-die forming for ultra-high strength steel
NASA Astrophysics Data System (ADS)
Majji, Raju; Xiang, Yang; Ding, Scott; Yang, Chunhui
2017-10-01
There has been a high demand for weight reduction in automotive vehicles while maintaining passenger safety. A potential steel material to achieve this is Ultra High Strength Steel (UHSS). As a high strength material, it is difficult to be formed with desired profiles using traditional sheet metal forming processes such as Cold Roll Forming. To overcome this problem, a potentially alternative solution is Chain-die Forming (CDF), recently developed. The basic principal of the CDF is to fully combine roll forming and bending processes. The main advantage of this process is the elongated deformation length that significantly increases effective roll radius. This study focuses on identifying issues with the CDF by using CAD modelling, Motion Analysis and Finite Element Analysis (FEA) to devise solutions and construct a more reliable process in an optimal design sense. Some attempts on finite element modelling and simulation of the CDF were conducted using relatively simple models in literature and the research was still not sufficient enough for optimal design of a typical CDF for UHSS. Therefore two numerical models of Chain-die Forming process are developed in this study, including a) one having a set of rolls similar to roll forming but with a large radius, i.e., 20 meters; and b) the other one with dies and punch segments similar to a typical CDF machine. As a case study, to form a 60° channel with single pass was conducted using these two devised models for a comparison. The obtained numerical results clearly show the CDF could generate less residual stress, low strain and small springback of a single pass for the 60° UHSS channel. The design analysis procedure proposed in this study could greatly help the mechanical designers to devise a cost-effective and reliable CDF process for forming UHSS.
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Method of manufacturing iron aluminide by thermomechanical processing of elemental powders
Deevi, Seetharama C.; Lilly, Jr., A. Clifton; Sikka, Vinod K.; Hajaligol, Mohammed R.
2000-01-01
A powder metallurgical process of preparing iron aluminide useful as electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 20 to 32% Al, and optional additions such as .ltoreq.1% Cr, .gtoreq.05% Zr or ZrO.sub.2 stringers extending perpendicular to an exposed surface of the heating element, .ltoreq.2% Ti, .ltoreq.2% Mo, .ltoreq.1% Zr, .ltoreq.1% C, .ltoreq.0.1% B, .ltoreq.30% oxide dispersoid and/or electrically insulating or electrically conductive covalent ceramic particles, .ltoreq.1 % rare earth metal, .ltoreq.1% oxygen, and/or .ltoreq.3% Cu. The process includes forming a mixture of aluminum powder and iron powder, shaping the mixture into an article such as by cold rolling the mixture into a sheet, and sintering the article at a temperature sufficient to react the iron and aluminum powders and form iron aluminide. The sintering can be followed by hot or cold rolling to reduce porosity created during the sintering step and optional annealing steps in a vacuum or inert atmosphere.
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NASA Technical Reports Server (NTRS)
Titran, Robert H.; Uz, Mehmet
1994-01-01
Effects of thermomechanical processing on the mechanical properties of Nb-1 wt. percent Zr-0.1 wt. percent C, a candidate alloy for use in advanced space power systems, were investigated. Sheet bars were cold rolled into 1-mm thick sheets following single, double, or triple extrusion operations at 1900 K. All the creep and tensile specimens were given a two-step heat treatment 1 hr at 1755 K + 2 hr 1475 K prior to testing. Tensile properties were determined at 300 as well as at 1350 K. Microhardness measurements were made on cold rolled, heat treated, and crept samples. Creep tests were carried out at 1350 K and 34.5 MPa for times of about 10,000 to 19,000 hr. The results show that the number of extrusions had some effects on both the microhardness and tensile properties. However, the long-time creep behavior of the samples were comparable, and all were found to have adequate properties to meet the design requirements of advanced power systems regardless of thermomechanical history. The results are discussed in correlation with processing and microstructure, and further compared to the results obtained from the testing of Nb-1 wt. percent Zr and Nb-1 wt. percent Zr-0.06 wt. percent C alloys.
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Effects of microalloying on hot-rolled and cold-rolled Q&P steels
NASA Astrophysics Data System (ADS)
Azevedo de Araujo, Ana Luiza
Third generation advanced high strength steels (AHSS) have been a major focus in steel development over the last decade. The premise of these types of steel is based on the potential to obtain excellent combinations of strength and ductility with low-alloy compositions by forming mixed microstructures containing retained austenite (RA). The development of heat treatments able to achieve the desired structures and properties, such as quenching and partitioning (Q&P) steels, is driven by new requirements to increase vehicle fuel economy by reducing overall weight while maintaining safety and crashworthiness. Microalloying additions of niobium (Nb) and vanadium (V) in sheet products are known to provide strengthening via grain refinement and precipitation hardening and may influence RA volume fraction and transformation behavior. Additions of microalloying elements in Q&P steels have not been extensively studied to date, however. The objective of the present study was to begin to understand the potential roles of Nb and V in hot-rolled and cold-rolled Q&P steel. For that, a common Q&P steel composition was selected as a Base alloy with 0.2C-1.5Si-2.0Mn (wt. %). Two alloys with an addition of Nb (0.02 and 0.04 wt. %) and one with an addition of V (0.06 wt. %) to the Base alloy were investigated. Both hot-rolled and cold-rolled/annealed Q&P simulations were conducted. In the hot-rolled Q&P study, thermomechanical processing was simulated via hot torsion testing in a GleebleRTM 3500, and four coiling temperatures (CT) were chosen. Microstructural evaluation (including RA measurements via electron backscattered diffraction - EBSD) and hardness measurements were performed for all alloys and coiling conditions. The analysis showed that Nb additions led to overall refinement of the prior microstructure. Maximum RA fractions were measured at the 375 °C CT, and microalloying was associated with increased RA in this condition when compared to the Base alloy. A change in austenite morphology from lath-like to blocky with increasing CT was observed. Hardness generally increased with decreasing CT, consistent with the increased fraction of harder phases in the microstructure. For the cold-rolled Q&P study, several combinations of quenching temperature (QT), partitioning temperature (PT), and partitioning time (t p) were examined using heat treatments in salt baths. Uniaxial tensile tests and RA measurements via x-ray diffraction (XRD) were performed for all alloys and heat treatment conditions. Scanning electron microscope (SEM) imaging and EBSD were conducted for a few select conditions. In terms of microstructure, Nb promoted an extensive refinement of the prior austenite grain size. Additions of V and Nb also seemed to affect the morphology of the microstructural constituents. It was observed that V generally increased austenite fractions at lower t p's, and the Nb-containing alloys had greater austenite fractions in most instances when compared to the Base alloy. Carbon content in austenite was usually increased or maintained with additions of Nb and V. In terms of mechanical properties, V slightly improved strength and elongation when compared to the Base alloy for most conditions. Niobium additions were somewhat more effective in improving ductility.
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Orientation Dependence of the Deformation Microstructure of Ta-4%W after Cold-Rolling
NASA Astrophysics Data System (ADS)
Zhang, J.; Ma, G. Q.; Godfrey, A.; Shu, D. Y.; Chen, Q.; Wu, G. L.
2017-07-01
One of the common features of deformed face-centered cubic metals with medium to high stacking fault energy is the formation of geometrically necessary dislocation boundaries. The dislocation boundary arrangements in refractory metals with body-centered cubic crystal structure are, however, less well known. To address this issue a Ta-4%W alloy was cold rolled up to 70% in thickness in the present work. The resulting deformation microstructures were characterized by electron back-scattering diffraction and the dislocation boundary arrangements in each grain were revealed using sample-frame misorientation axis maps calculated using an in-house code. The maps were used to analyze the slip pattern of individual grains after rolling, revealing an orientation dependence of the slip pattern.
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Code of Federal Regulations, 2011 CFR
2011-07-01
... beading, straightening, corrugating, flanging, or bending rolls; and hot or cold rolling mills. (ii) All... area between the dies; power presses; and plate punches. (iii) All bending machines, such as apron...
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EBSD characterization of twinning in cold-rolled CP-Ti
DOE Office of Scientific and Technical Information (OSTI.GOV)
Li, X., E-mail: csulixu@hotmail.com; Duan, Y.L., E-mail: 876270744@qq.com; Xu, G.F., E-mail: csuxgf66@csu.edu.cn
2013-10-15
This work presents the use of a mechanical testing system and the electron backscatter diffraction technique to study the mechanical properties and twinning systems of cold-rolled commercial purity titanium, respectively. The dependence of twinning on the matrix orientation is analyzed by the distribution map of Schmid factor. The results showed that the commercial purity titanium experienced strong strain hardening and had excellent formability during rolling. Both the (112{sup ¯}2)<112{sup ¯}3{sup ¯}> compressive twins and (101{sup ¯}2)<101{sup ¯}1{sup ¯}> tensile twins were dependent on the matrix orientation. The Schmid factor of a grain influenced the activation of a particular twinning system.more » The specific rolling deformation of commercial purity titanium controlled the number and species of twinning systems and further changed the mechanical properties. - Highlights: • CP-Ti experienced strain hardening and had excellent formability. • Twins were dependent on the matrix orientation. • Schmid factor of a grain influenced the activation of a twinning system. • Rolling deformation controlled twinning systems and mechanical properties.« less
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NASA Technical Reports Server (NTRS)
Butt, Adam; Popp, Christopher G.; Holt, Kimberly A.; Pitts, Hank M.
2010-01-01
The Ares I launch vehicle is the selected design, chosen to return humans to the moon, Mars, and beyond. It is configured in two inline stages: the First Stage is a Space Shuttle derived five-segment Solid Rocket Booster and the Upper Stage is powered by a Saturn V derived J-2X engine. During launch, roll control for the First Stage (FS) is handled by a dedicated Roll Control System (RoCS) located on the connecting Interstage. That system will provide the Ares I with the ability to counteract induced roll torque while any induced yaw or pitch moments are handled by vectoring of the booster nozzle. This paper provides an overview of NASA s Ares I FS RoCS cold flow development test program including detailed test objectives, types of tests run to meet those objectives, an overview of the results, and applicable lessons learned. The test article was built and tested at the NASA Marshall Space Flight Center in Huntsville, AL. The FS RoCS System Development Test Article (SDTA) is a full scale, flight representative water flow test article whose primary objective was to obtain fluid system performance data to evaluate integrated system level performance characteristics and verify analytical models. Development testing and model correlation was deemed necessary as there is little historical precedent for similar large flow, pulsing systems such as the FS RoCS. The cold flow development test program consisted of flight-similar tanks, pressure regulators, and thruster valves, as well as plumbing simulating flight geometries, combined with other facility grade components and structure. Orifices downstream of the thruster valves were used to simulate the pressure drop through the thrusters. Additional primary objectives of this test program were to: evaluate system surge pressure (waterhammer) characteristics due to thruster valve operation over a range of mission duty cycles at various feed system pressures, evaluate temperature transients and heat transfer in the pressurization system, including regulator blowdown and propellant ullage performance, measure system pressure drops for comparison to analysis of tubing and components, and validate system activation and re-activation procedures for the helium pressurant system. Secondary objectives included: validating system processes for loading, unloading, and purging, validating procedures and system response for multiple failure scenarios, including relief valve operation, and evaluating system performance for contingency scenarios. The test results of the cold flow development test program are essential in validating the performance and interaction of the Roll Control System and anchoring analysis tools and results to a Critical Design Review level of fidelity.
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Shock compression response of cold-rolled Ni/Al multilayer composites
Specht, Paul E.; Weihs, Timothy P.; Thadhani, Naresh N.
2017-01-06
Uniaxial strain, plate-on-plate impact experiments were performed on cold-rolled Ni/Al multilayer composites and the resulting Hugoniot was determined through time-resolved measurements combined with impedance matching. The experimental Hugoniot agreed with that previously predicted by two dimensional (2D) meso-scale calculations. Additional 2D meso-scale simulations were performed using the same computational method as the prior study to reproduce the experimentally measured free surface velocities and stress profiles. Finally, these simulations accurately replicated the experimental profiles, providing additional validation for the previous computational work.
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Code of Federal Regulations, 2010 CFR
2010-07-01
..., or bending rolls; and hot or cold rolling mills. (ii) All pressing or punching machines, such as... presses; and plate punches. (iii) All bending machines, such as apron brakes and press brakes. (iv) All...
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NASA Astrophysics Data System (ADS)
Pimentel, G.; Aranda, M. M.; Chao, J.; González-Carrasco, J. L.; Capdevila, C.
2015-09-01
The first part of this two-part study reported the possibility of simultaneously generating a dense, self-healing α-alumina layer by thermal oxidation and a coarse-grained microstructure with a potential goodness for high-temperature creep resistance in a FeCrAl oxide dispersion-strengthened ferritic alloy that was cold deformed after hot rolling and extrusion. In this second part, the factors affecting the formation of the coarse-grained microstructure such as strain gradients induced during the rolling process are analyzed. It is concluded that larger strain gradients lead to more refined and more isotropic grain structures.
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40 CFR 468.13 - New source performance standards (NSPS).
Code of Federal Regulations, 2012 CFR
2012-07-01
... copper alloy hot rolled Chromium 0.038 0.015 Copper 0.131 0.062 Lead 0.010 0.0092 Nickel 0.056 0.038 Zinc... rolled English units—pounds per 1,000,000 off-pounds of copper or copper alloy cold rolled Chromium 0.140... copper or copper alloy drawn Chromium 0.031 0.012 Copper 0.108 0.051 Lead 0.0085 0.0076 Nickel 0.046 0...
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40 CFR 468.13 - New source performance standards (NSPS).
Code of Federal Regulations, 2013 CFR
2013-07-01
... copper alloy hot rolled Chromium 0.038 0.015 Copper 0.131 0.062 Lead 0.010 0.0092 Nickel 0.056 0.038 Zinc... rolled English units—pounds per 1,000,000 off-pounds of copper or copper alloy cold rolled Chromium 0.140... copper or copper alloy drawn Chromium 0.031 0.012 Copper 0.108 0.051 Lead 0.0085 0.0076 Nickel 0.046 0...
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40 CFR 468.13 - New source performance standards (NSPS).
Code of Federal Regulations, 2014 CFR
2014-07-01
... copper alloy hot rolled Chromium 0.038 0.015 Copper 0.131 0.062 Lead 0.010 0.0092 Nickel 0.056 0.038 Zinc... rolled English units—pounds per 1,000,000 off-pounds of copper or copper alloy cold rolled Chromium 0.140... copper or copper alloy drawn Chromium 0.031 0.012 Copper 0.108 0.051 Lead 0.0085 0.0076 Nickel 0.046 0...
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NASA Astrophysics Data System (ADS)
Puff, Werner; Rabitsch, Herbert; Wilde, Gerhard; Dinda, Guru P.; Würschum, Roland
2007-06-01
With the aim to contribute to a microscopical understanding of the processes of solid-state amorphization, the chemically sensitive technique of background—reduced Doppler broadening of positron-electron annihilation radiation in combination with positron lifetime spectroscopy and microstructural characterization is applied to a free volume study of the amorphization of Cu60Zr40 induced by consecutive folding and rolling. Starting from the constituent pure metal foils, a nanosale multilayer structure of elemental layers and amorphous interlayers develops in an intermediate state of folding and rolling, where free volumes with a Zr-rich environment occur presumably located in the hetero-interfaces between the various layers or in grain boundaries of the Cu layers. After complete intermixing and amorphization, the local chemical environment of the free volumes reflects the average chemical alloy composition. In contrast to other processes of amorphization, free volumes of the size of few missing atoms occur in the rolling-induced amorphous state. Self-consistent results from three different methods for analyzing the Doppler broadening spectra, i.e., S-W-parameter correlation, multicomponent fit, and the shape of ratio curves, demonstrate the potential of the background-reduced Doppler technique for chemically sensitive characterization of structurally complex materials on an atomic scale.
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Deformability of Oxide Inclusions in Tire Cord Steels
NASA Astrophysics Data System (ADS)
Zhang, Lifeng; Guo, Changbo; Yang, Wen; Ren, Ying; Ling, Haitao
2018-04-01
The deformation of oxide inclusions in tire cord steels during hot rolling was analyzed, and the factors influencing their deformability at high and low temperatures were evaluated and discussed. The aspect ratio of oxide inclusions decreased with the increasing reduction ratio of the steel during hot rolling owing to the fracture of the inclusions. The aspect ratio obtained after the first hot-rolling process was used to characterize the high-temperature deformability of the inclusions. The deformation first increased and then decreased with the increasing (MgO + Al2O3)/(SiO2 + MnO) ratio of the inclusions. It also increased with the decreasing melting temperatures of the inclusions. Young's modulus was used to evaluate the low-temperature deformability of the inclusions. An empirical formula was fitted to calculate the Young's moduli of the oxides using the mean atomic volume. The moduli values of the inclusions causing wire fracture were significantly greater than the average. To reduce fracture in tire cord steel wires during cold drawing, it is proposed that inclusions be controlled to those with high SiO2 content and extremely low Al2O3 content. This proposal is based on the hypothesis that the deformabilities of oxides during cold drawing are inversely proportional to their Young's moduli. The future study thus proposed includes an experimental confirmation for the abovementioned predictions.
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Possibilities for specific utilization of material properties for an optimal part design
NASA Astrophysics Data System (ADS)
Beier, T.; Gerlach, J.; Roettger, R.; Kuhn, P.
2017-09-01
High-strength, cold-formable steels offer great potential for meeting cost and safety requirements in the automotive industry. In view of strengths of up to 1200 MPa now attainable, certain aspects need to be analysed and evaluated in advance in the development process using these materials. In addition to early assessment of crash properties, it is also highly important to adapt the forming process to match the material potential. The steel making companies have widened their portfolios of cold-rolled dual-phase steels well beyond the conventional high-strength steels. There are added new grades which offer a customized selection of high energy absorption, deformation resistance or enhanced cold-forming properties. In this article the necessary components for material modelling for finite element simulation are discussed. Additionally the required tests for material model calibration are presented and the potentials of the thyssenkrupp Steel material data base are introduced. Besides classical tensile tests at different angles to rolling direction and the forming limit curve, the hydraulic bulge test is now available for a wide range of modern steel grades. Using the conventional DP-K®60/98 and the DP-K®700Y980T with higher yield strength the method for calibrating yield locus, hardening and formability is given. With reference to the examples of an A-pillar reinforcement and different crash tests the procedure is shown how the customer can evaluate an optimal steel grade for specific requirements. Although the investigated materials have different yield strengths, no large differences in the forming process between the two steel grades can be found. However some advantages of the high-yield grade can be detected in crash performance depending on the specific boundary and loading conditions.
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Code of Federal Regulations, 2013 CFR
2013-07-01
... GUIDELINES AND STANDARDS IRON AND STEEL MANUFACTURING POINT SOURCE CATEGORY Cold Forming Subcategory § 420...) Cold rolling mills—(1) Recirculation—single stand. Subpart J Pollutant or pollutant property BCT...) (1) 1 Within the range of 6.0 to 9.0. (b) Cold worked pipe and tube—(1) Using water. Subpart J...
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Code of Federal Regulations, 2014 CFR
2014-07-01
... GUIDELINES AND STANDARDS IRON AND STEEL MANUFACTURING POINT SOURCE CATEGORY Cold Forming Subcategory § 420...) Cold rolling mills—(1) Recirculation—single stand. Subpart J Pollutant or pollutant property BCT...) (1) 1 Within the range of 6.0 to 9.0. (b) Cold worked pipe and tube—(1) Using water. Subpart J...
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Code of Federal Regulations, 2011 CFR
2011-07-01
... GUIDELINES AND STANDARDS IRON AND STEEL MANUFACTURING POINT SOURCE CATEGORY Cold Forming Subcategory § 420...) Cold rolling mills—(1) Recirculation—single stand. Subpart J Pollutant or pollutant property BCT...) (1) 1 Within the range of 6.0 to 9.0. (b) Cold worked pipe and tube—(1) Using water. Subpart J...
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Code of Federal Regulations, 2010 CFR
2010-07-01
... GUIDELINES AND STANDARDS IRON AND STEEL MANUFACTURING POINT SOURCE CATEGORY Cold Forming Subcategory § 420...) Cold rolling mills—(1) Recirculation—single stand. Subpart J Pollutant or pollutant property BCT...) (1) 1 Within the range of 6.0 to 9.0. (b) Cold worked pipe and tube—(1) Using water. Subpart J...
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Code of Federal Regulations, 2012 CFR
2012-07-01
... GUIDELINES AND STANDARDS IRON AND STEEL MANUFACTURING POINT SOURCE CATEGORY Cold Forming Subcategory § 420...) Cold rolling mills—(1) Recirculation—single stand. Subpart J Pollutant or pollutant property BCT...) (1) 1 Within the range of 6.0 to 9.0. (b) Cold worked pipe and tube—(1) Using water. Subpart J...
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NASA Astrophysics Data System (ADS)
Suh, Dong-Woo; Park, Seong-Jun; Lee, Tae-Ho; Oh, Chang-Seok; Kim, Sung-Joon
2010-02-01
Microstructural design with an Al addition is suggested for low-carbon, manganese transformation-induced-plasticity (Mn TRIP) steel for application in the continuous-annealing process. With an Al content of 1 mass pct, the competition between the recrystallization of the cold-rolled microstructure and the austenite formation cannot be avoided during intercritical annealing, and the recrystallization of the deformed matrix does not proceed effectively. The addition of 3 mass pct Al, however, allows nearly complete recrystallization of the deformed microstructure by providing a dual-phase cold-rolled structure consisting of ferrite and martensite and by suppressing excessive austenite formation at a higher annealing temperature. An optimized annealing condition results in the room-temperature stability of the intercritical austenite in Mn TRIP steel containing 3 mass pct Al, permitting persistent transformation to martensite during tensile deformation. The alloy presents an excellent strength-ductility balance combining a tensile strength of approximately 1 GPa with a total elongation over 25 pct, which is comparable to that of Mn TRIP steel subjected to batch-type annealing.
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NASA Astrophysics Data System (ADS)
Adam, Khaled; Zöllner, Dana; Field, David P.
2018-04-01
Modeling the microstructural evolution during recrystallization is a powerful tool for the profound understanding of alloy behavior and for use in optimizing engineering properties through annealing. In particular, the mechanical properties of metallic alloys are highly dependent upon evolved microstructure and texture from the softening process. In the present work, a Monte Carlo (MC) Potts model was used to model the primary recrystallization and grain growth in cold rolled single-phase Al alloy. The microstructural representation of two kinds of dislocation densities, statistically stored dislocations and geometrically necessary dislocations were quantified based on the ViscoPlastic Fast Fourier transform method. This representation was then introduced into the MC Potts model to identify the favorable sites for nucleation where orientation gradients and entanglements of dislocations are high. Additionally, in situ observations of non-isothermal microstructure evolution for single-phase aluminum alloy 1100 were made to validate the simulation. The influence of the texture inhomogeneity is analyzed from a theoretical point of view using an orientation distribution function for deformed and evolved texture.
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Optimized Gen-II FeCrAl cladding production in large quantity for campaign testing
DOE Office of Scientific and Technical Information (OSTI.GOV)
Yamamoto, Yukinori; Sun, Zhiqian; Pint, Bruce A.
2016-06-03
There are two major objectives in this report; (1) to optimize microstructure control of ATF FeCrAl alloys during tube drawing processes, and (2) to provide an update on the progress of ATF FeCrAl tube production via commercial manufacturers. Experimental efforts have been made to optimize the process parameters balancing the tube fabricability, especially for tube drawing processes, and microstructure control of the final tube products. Lab-scale sheet materials of Gen II FeCrAl alloys (Mo-containing and Nb-containing FeCrAl alloys) were used in the study, combined with a stepwise warm-rolling process and intermediate annealing, aiming to simulate the tube drawing process inmore » a commercial tube manufacturer. The intermediate annealing at 650ºC for 1h was suggested for the tube-drawing process of Mo-containing FeCrAl alloys because it successfully softened the material by recovering the work hardening introduced through the rolling step, without inducing grain coarsening due to recrystallization. The final tube product is expected to have stabilized deformed microstructure providing the improved tensile properties with sufficient ductility. Optimization efforts on Nb-containing FeCrAl alloys focused on the effect of alloying additions and annealing conditions on the stability of deformed microstructure. Relationships between the second-phase precipitates (Fe 2Nb-Laves phase) and microstructure stability are discussed. FeCrAl tube production through commercial tube manufacturers is currently in progress. Three different manufacturers, Century Tubes, Inc. (CTI), Rhenium Alloys, Inc. (RAI), and Superior Tube Company, Inc. (STC), are providing capabilities for cold-drawing, warm-drawing, and HPTR cold-pilgering, respectively. The first two companies are currently working on large quantity tube production (expected 250 ft length) of Gen I model FeCrAl alloy (B136Y3, at CTI) and Gen II (C35M4, at RAI), with the process parameters obtained from the experimental efforts. The expected delivery dates are at the end of July, 2016, and the middle of June, 2016, respectively. Tube production at STC would be the first attempt to apply cold-pilgering to the FeCrAl alloys. Communication has been initiated, and the materials have been machined for the cold-pilgering process.« less
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Shock compression response of cold-rolled Ni/Al multilayer composites
NASA Astrophysics Data System (ADS)
Specht, Paul E.; Weihs, Timothy P.; Thadhani, Naresh N.
2017-01-01
Uniaxial strain, plate-on-plate impact experiments were performed on cold-rolled Ni/Al multilayer composites and the resulting Hugoniot was determined through time-resolved measurements combined with impedance matching. The experimental Hugoniot agreed with that previously predicted by two dimensional (2D) meso-scale calculations [Specht et al., J. Appl. Phys. 111, 073527 (2012)]. Additional 2D meso-scale simulations were performed using the same computational method as the prior study to reproduce the experimentally measured free surface velocities and stress profiles. These simulations accurately replicated the experimental profiles, providing additional validation for the previous computational work.
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40 CFR 468.14 - Pretreatment standards for existing sources (PSES).
Code of Federal Regulations, 2011 CFR
2011-07-01
... per 1,000,000 off-pounds of copper or copper alloy hot rolled Chromium 0.045 0.018 Copper 0.195 0.103... rolled English units—pounds per 1,000,000 off-pounds of copper or copper alloy cold rolled Chromium 0.166... drawn Chromium 0.037 0.015 Copper 0.161 0.085 Lead 0.012 0.011 Nickel 0.163 0.107 Zinc 0.124 0.051 TTO 0...
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40 CFR 468.14 - Pretreatment standards for existing sources (PSES).
Code of Federal Regulations, 2013 CFR
2013-07-01
... rolled English units—pounds per 1,000,000 off-pounds of copper or copper alloy hot rolled Chromium 0.045... alloy cold rolled Chromium 0.166 0.068 Copper 0.720 0.379 Lead 0.056 0.049 Nickel 0.727 0.481 Zinc 0.553... copper or copper alloy drawn Chromium 0.037 0.015 Copper 0.161 0.085 Lead 0.012 0.011 Nickel 0.163 0.107...
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40 CFR 468.14 - Pretreatment standards for existing sources (PSES).
Code of Federal Regulations, 2014 CFR
2014-07-01
... rolled English units—pounds per 1,000,000 off-pounds of copper or copper alloy hot rolled Chromium 0.045... alloy cold rolled Chromium 0.166 0.068 Copper 0.720 0.379 Lead 0.056 0.049 Nickel 0.727 0.481 Zinc 0.553... copper or copper alloy drawn Chromium 0.037 0.015 Copper 0.161 0.085 Lead 0.012 0.011 Nickel 0.163 0.107...
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40 CFR 468.14 - Pretreatment standards for existing sources (PSES).
Code of Federal Regulations, 2012 CFR
2012-07-01
... rolled English units—pounds per 1,000,000 off-pounds of copper or copper alloy hot rolled Chromium 0.045... alloy cold rolled Chromium 0.166 0.068 Copper 0.720 0.379 Lead 0.056 0.049 Nickel 0.727 0.481 Zinc 0.553... copper or copper alloy drawn Chromium 0.037 0.015 Copper 0.161 0.085 Lead 0.012 0.011 Nickel 0.163 0.107...
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Federal Register 2010, 2011, 2012, 2013, 2014
2010-10-29
...., Steubenville, OH By applications dated May 15 and May 21, 2010, United Steel, Paper and Forestry, Rubber... back plate coils (TA-W-71,572A), hot rolled coils (TA- W-71,572B), and cold rolled coils (TA-W-71,572C...
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Federal Register 2010, 2011, 2012, 2013, 2014
2011-11-03
... determined that Philippines, Indonesia, Ukraine, Thailand, Colombia, and South Africa are countries... Flat-Rolled Carbon-Quality Steel Products from the Russian Federation, 65 FR 5510, 5518 (February 4...\\ See Final Determination of Sales at Less Than Fair Value: Certain Cold-Rolled Carbon Quality Steel...
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Evolution of Oxide Inclusions in Si-Mn Killed Steels During Hot-Rolling Process
NASA Astrophysics Data System (ADS)
Yang, Wen; Guo, Changbo; Zhang, Lifeng; Ling, Haitao; Li, Chao
2017-10-01
The evolution of oxide inclusions in Si-Mn killed steels refined by slags of different basicity during a four-pass industrial hot-rolling process was investigated using an automated microscopy system. High-basicity refining slag induced the formation of CaO- and Al2O3-containing inclusions, while refining slag with 0.8 basicity induced dominant inclusions of SiO2 and MnO-SiO2. CaO-SiO2-Al2O3 inclusions mainly formed endogenously during solidification and cooling of Ca-containing steels, where Ca originated from slag-steel reactions. However, the larger-sized higher-CaO inclusions originated from slag entrainment. Different inclusions presented different hot-rolling behaviors. The inclusion composition changed by deformation and new phase formation. The dominant oxide types were unchanged under refinement by low-basicity slag; however, they changed under refinement with high-basicity slag. The deformation index of inclusions decreased with increasing accumulated reduction (AR) of the steel. The difference in deformation index between different inclusion types was the largest in the first rolling stage and decreased in subsequent stages. SiO2-CaO and SiO2-MnO-CaO inclusions had larger deformation indices during hot rolling but smaller indices in the last two stages. High-basicity slag increased inclusion complexity; from the perspective of cold-drawing performance, low-basicity refining slag is better for the industrial production of tire-cord steels.
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NASA Astrophysics Data System (ADS)
Dubinskiy, S.; Brailovski, Vladimir; Prokoshkin, S.; Pushin, V.; Inaekyan, K.; Sheremetyev, V.; Petrzhik, M.; Filonov, M.
2013-09-01
In this work, the ternary Ti-19.7Nb-5.8Ta (at.%) alloy for biomedical applications was studied. The ingot was manufactured by vacuum arc melting with a consumable electrode and then subjected to hot forging. Specimens were cut from the ingot and processed by cold rolling with e = 0.37 of logarithmic thickness reduction and post-deformation annealing (PDA) between 400 and 750 °C (1 h). Selected samples were subjected to aging at 300 °C (10 min to 3 h). The influence of the thermomechanical processing on the alloy's structure, phase composition, and mechanical and functional properties was studied. It was shown that thermomechanical processing leads to the formation of a nanosubgrained structure (polygonized with subgrains below 100 nm) in the 500-600 °C PDA range, which transforms to a recrystallized structure of β-phase when PDA temperature increases. Simultaneously, the phase composition and the β → α″ transformation kinetics vary. It was found that after conventional cold rolling and PDA, Ti-Nb-Ta alloy manifests superelastic and shape memory behaviors. During aging at 300 °C (1 h), an important quantity of randomly scattered equiaxed ω-precipitates forms, which results in improved superelastic cyclic properties. On the other hand, aging at 300 °C (3 h) changes the ω-precipitates' particle morphology from equiaxed to elongated and leads to their coarsening, which negatively affects the superelastic and shape memory functional properties of Ti-Nb-Ta alloy.
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A Systematic Study of Kelvin-Helmholtz Instability in Galaxy Clusters
NASA Astrophysics Data System (ADS)
Su, Yuanyuan
2017-09-01
Kelvin-Helmholtz instabilities (KHI) were observed at cold fronts in a handful of clusters. KHI are predicted at all cold fronts in hydro simulation of intracluster medium (ICM). Their presence and absence provides a unique probe of transport processes in the hot plasma, which are essential to the dissipation and redistribution of the energy in the ICM. We propose the first systematic study of the prevalence of KHI in galaxy clusters by analyzing the archived Chandra observations of a sample of 50 nearby galaxy clusters. We will associate the occurrence and properties of KHI rolls with various cluster parameters such as their gas temperature and density, and put constraints on effective transport coefficients in the ICM
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Characterization of particle exposure in ferrochromium and stainless steel production.
Järvelä, Merja; Huvinen, Markku; Viitanen, Anna-Kaisa; Kanerva, Tomi; Vanhala, Esa; Uitti, Jukka; Koivisto, Antti J; Junttila, Sakari; Luukkonen, Ritva; Tuomi, Timo
2016-07-01
This study describes workers' exposure to fine and ultrafine particles in the production chain of ferrochromium and stainless steel during sintering, ferrochromium smelting, stainless steel melting, and hot and cold rolling operations. Workers' personal exposure to inhalable dust was assessed using IOM sampler with a cellulose acetate filter (AAWP, diameter 25 mm; Millipore, Bedford, MA). Filter sampling methods were used to measure particle mass concentrations in fixed locations. Particle number concentrations and size distributions were examined using an SMPS+C sequential mobile particle sizer and counter (series 5.400, Grimm Aerosol Technik, Ainring, Germany), and a hand-held condensation particle counter (CPC, model 3007, TSI Incorporated, MN). The structure and elemental composition of particles were analyzed using TEM-EDXA (TEM: JEM-1220, JEOL, Tokyo, Japan; EDXA: Noran System Six, Thermo Fisher Scientific Inc., Madison,WI). Workers' personal exposure to inhalable dust averaged 1.87, 1.40, 2.34, 0.30, and 0.17 mg m(-3) in sintering plant, ferrochromium smelter, stainless steel melting shop, hot rolling mill, and the cold rolling mill, respectively. Particle number concentrations measured using SMPS+C varied from 58 × 10(3) to 662 × 10(3) cm(-3) in the production areas, whereas concentrations measured using SMPS+C and CPC3007 in control rooms ranged from 24 × 10(3) to 243 × 10(3) cm(-3) and 5.1 × 10(3) to 97 × 10(3) cm(-3), respectively. The elemental composition and the structure of particles in different production phases varied. In the cold-rolling mill non-process particles were abundant. In other sites, chromium and iron originating from ore and recycled steel scrap were the most common elements in the particles studied. Particle mass concentrations were at the same level as that reported earlier. However, particle number measurements showed a high amount of ultrafine particles, especially in sintering, alloy smelting and melting, and tapping operations. Particle number concentration and size distribution measurements provide important information regarding exposure to ultrafine particles, which cannot be seen in particle mass measurements.
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NASA Astrophysics Data System (ADS)
Togano, Kazumasa; Gao, Zhaoshun; Matsumoto, Akiyoshi; Kumakura, Hiroaki
2013-11-01
We report that the transport critical current density Jc of ex situ powder-in-tube (PIT) processed (Ba, K)Fe2As2 (Ba-122) tapes can be significantly enhanced by applying uniaxial cold pressing at the final stage of deformation. The tapes were prepared by packing high quality precursor powder into a Ag tube, cycles of rolling and intermediate annealing, and pressing followed by the final heat treatment for sintering. The Jc values in applied magnetic fields were increased by almost one order of magnitude compared to the tapes processed without pressing, exceeding 104 A cm-2 at 4.2 K. We achieved the highest Jc (at 4.2 K and 10 T) of 2.1×104 A cm-2 among PIT-processed Fe-based wires and tapes reported so far. The Jc-H curves measured at higher temperatures maintain small field dependence up to around 20 K, suggesting that these tapes are promising for applications at higher temperatures as well as at liquid helium temperature. The microstructure investigations reveal that there are two possible causes of the large Jc enhancement by pressing: one is densification and the other is the change of crack structure. Optimization of processing parameters such as the reduction ratio of rolling and pressing is expected to yield further Jc enhancement.
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NASA Astrophysics Data System (ADS)
Tutar, Mumin; Aydin, Hakan; Bayram, Ali
2017-08-01
Formability and energy absorption capability of a steel sheet are highly desirable properties in manufacturing components for automotive applications. TWinning Induced Plastisity (TWIP) steels are, new generation high Mn alloyed steels, attractive for the automotive industry due to its outstanding elongation (%40-45) and tensile strength (~1000MPa). So, TWIP steels provide excellent formability and energy absorption capability. Another required property from the steel sheets is suitability for manufacturing methods such as welding. The use of the steel sheets in the automotive applications inevitably involves welding. Considering that there are 3000-5000 welded spots on a vehicle, it can be interpreted that one of the most important manufacturing method is Resistance Spot Welding (RSW) for the automotive industry. In this study; firstly, TWIP steel sheet were cold rolled to 15% reduction in thickness. Then, the cold rolled TWIP steel sheets were welded with RSW method. The welding parameters (welding current, welding time and electrode force) were optimized for maximizing the peak tensile shear load and minimizing the indentation of the joints using a Taguchi L9 orthogonal array. The effect of welding parameters was also evaluated by examining the signal-to-noise ratio and analysis of variance (ANOVA) results.
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Arctic PBL Cloud Height and Motion Retrievals from MISR and MINX
NASA Technical Reports Server (NTRS)
Wu, Dong L.
2012-01-01
How Arctic clouds respond and feedback to sea ice loss is key to understanding of the rapid climate change seen in the polar region. As more open water becomes available in the Arctic Ocean, cold air outbreaks (aka. off-ice flow from polar lows) produce a vast sheet of roll clouds in the planetary boundary layer (PBl). The cold air temperature and wind velocity are the critical parameters to determine and understand the PBl structure formed under these roll clouds. It has been challenging for nadir visible/IR sensors to detect Arctic clouds due to lack of contrast between clouds and snowy/icy surfaces. In addition) PBl temperature inversion creates a further problem for IR sensors to relate cloud top temperature to cloud top height. Here we explore a new method with the Multiangle Imaging Spectro-Radiometer (MISR) instrument to measure cloud height and motion over the Arctic Ocean. Employing a stereoscopic-technique, MISR is able to measure cloud top height accurately and distinguish between clouds and snowy/icy surfaces with the measured height. We will use the MISR INteractive eXplorer (MINX) to quantify roll cloud dynamics during cold-air outbreak events and characterize PBl structures over water and over sea ice.
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Grain Orientation Dependence of the Residual Lattice Strain in a Cold Rolled Interstitial-Free Steel
Xie, Qingge; Gorti, Sarma B.; Sidor, Jurij; ...
2018-01-10
The experimentally measured grain-orientation-dependent residual lattice strains, evolved in an interstitia-free steel after 70% cold rolling reduction, are studied by means of crystal elastic visco-plastic finite element simulations, which provides a very satisfactory prediction of deformation texture. The calculated residual lattice strain pole figure matches well with the experimentally measured counterpart within the highest density regions of major texture components observed. Both experimental evidence and results of modeling clearly indicate that the residual lattice strain is orientation dependent, based on comprehensive information on the evolution of residual lattice strain in various crystallographic orientations during plastic deformation. It appears that inmore » a cold rolled material, there is a general correlation between the stresses developed just prior to unloading and the residual lattice strains in particular directions. Here, it is also shown that the cumulative plastic shear does not reveal a clear correlation with the components of residual lattice strain while presented in the normal correlation plot, however, this relationship can be better understood by means of the orientation distribution function of residual lattice strain, which can be derived from the neutron or X-ray diffraction experiments.« less
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Grain Orientation Dependence of the Residual Lattice Strain in a Cold Rolled Interstitial-Free Steel
DOE Office of Scientific and Technical Information (OSTI.GOV)
Xie, Qingge; Gorti, Sarma B.; Sidor, Jurij
The experimentally measured grain-orientation-dependent residual lattice strains, evolved in an interstitia-free steel after 70% cold rolling reduction, are studied by means of crystal elastic visco-plastic finite element simulations, which provides a very satisfactory prediction of deformation texture. The calculated residual lattice strain pole figure matches well with the experimentally measured counterpart within the highest density regions of major texture components observed. Both experimental evidence and results of modeling clearly indicate that the residual lattice strain is orientation dependent, based on comprehensive information on the evolution of residual lattice strain in various crystallographic orientations during plastic deformation. It appears that inmore » a cold rolled material, there is a general correlation between the stresses developed just prior to unloading and the residual lattice strains in particular directions. Here, it is also shown that the cumulative plastic shear does not reveal a clear correlation with the components of residual lattice strain while presented in the normal correlation plot, however, this relationship can be better understood by means of the orientation distribution function of residual lattice strain, which can be derived from the neutron or X-ray diffraction experiments.« less
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Advances in Integrated Computational Materials Engineering "ICME"
NASA Astrophysics Data System (ADS)
Hirsch, Jürgen
The methods of Integrated Computational Materials Engineering that were developed and successfully applied for Aluminium have been constantly improved. The main aspects and recent advances of integrated material and process modeling are simulations of material properties like strength and forming properties and for the specific microstructure evolution during processing (rolling, extrusion, annealing) under the influence of material constitution and process variations through the production process down to the final application. Examples are discussed for the through-process simulation of microstructures and related properties of Aluminium sheet, including DC ingot casting, pre-heating and homogenization, hot and cold rolling, final annealing. New results are included of simulation solution annealing and age hardening of 6xxx alloys for automotive applications. Physically based quantitative descriptions and computer assisted evaluation methods are new ICME methods of integrating new simulation tools also for customer applications, like heat affected zones in welding of age hardening alloys. The aspects of estimating the effect of specific elements due to growing recycling volumes requested also for high end Aluminium products are also discussed, being of special interest in the Aluminium producing industries.
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INTERIOR OF WESTERN SECTION, SHOWING WALL OF COLD STORAGE ROOM ...
INTERIOR OF WESTERN SECTION, SHOWING WALL OF COLD STORAGE ROOM (IN BAYS 32 TO 34) AND ROLLING DOORS AT WEST END, VIEW FACING SOUTH-SOUTHWEST. - Naval Air Station Barbers Point, Aircraft Storehouse, Between Midway & Card Streets at Enterprise Avenue intersection, Ewa, Honolulu County, HI
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A Study of the Cold Resistance of Pipe Coiled Stock Produced at Foundry-Rolling Works. Part 2
NASA Astrophysics Data System (ADS)
Bagmet, O. A.; Naumenko, V. V.; Smetanin, K. S.
2018-03-01
Results of a study of coiled stock from low-carbon steels alloyed with manganese and silicon and different additives of niobium and titanium are presented. The coiled stock is produced at foundry-rolling works by the method of direct rolling of thin slabs right after their continuous casting. The microdeformation of the crystal lattice and the crystallographic texture are determined. The conditions of formation of the most favorable structure and texture in the steels are specified.
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NASA Astrophysics Data System (ADS)
Hendrik; Sebleku, P.; Siswayanti, B.; Pramono, A. W.
2017-05-01
The manufacture of high critical temperature (Tc) Bi, Pb-Sr-Ca-Cu-O (HTS BPSCCO) superconductor wire fabricated by power-in-tube (PIT) is a multi-step process. The main difficulty is that the value of Tc superconductor wire determined by various factors for each step. The objective of this research is to investigate the effect of sintering parameters on the properties of final rolled material. The fabrication process of 1 m rolled-silver sheath monofilament superconductor BPSCCO wire using mechanical deformation process including rolling and drawing has been carried out. The pure silver powders were melted and formed into pure silver (Ag) tube. The tube was 10 mm in diameter with a sheath material: superconductor powders ratio of about 6 : 1. Starting powders, containing the nominal composition of Bi2-Sr2-Cam-1-Cum-Oy, were inserted into the pure silver tube and rolled until it reached a diameter of 4 mm. A typical area reduction ratio of about 5% per step has been proposed to prevent microcracking during the cold-drawing process. The process of rolling of the silver tube was subsequently repeated to obtain three samples and then followed by heat-treated at 820 °C, 840 °C, and 860 °C, respectively. The surface morphology was analyzed by using SEM; the crystal structure was studied by using X-RD, whereas the superconductivity was investigated by using temperature dependence resistivity measurement by using four-point probe technique. SEM images showed the porosity of the cross-sectional surface of the samples. The sample with low heating temperature showed porosity more than the one with high temperature. The value of critical temperature (Tc) of the sample with a dwelling time of heating of 8 hours is 70 K. At above 70 K, it shows the behavior of conductor properties. However, the porosity increased as the heating time increased up to 24 hours. The critical temperature was difficult to be identified due to its porosity. According to XRD results, the Bi-2212 phase is prominent in all samples.
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Micromechanical Characterization and Texture Analysis of Direct Cast Titanium Alloys Strips
NASA Technical Reports Server (NTRS)
2000-01-01
This research was conducted to determine a post-processing technique to optimize mechanical and material properties of a number of Titanium based alloys and aluminides processed via Melt Overflow Solidification Technique (MORST). This technique was developed by NASA for the development of thin sheet titanium and titanium aluminides used in high temperature applications. The materials investigated in this study included conventional titanium alloy strips and foils, Ti-1100, Ti-24Al-11Nb (Alpha-2), and Ti-48Al-2Ta (Gamma). The methodology used included micro-characterization, heat-treatment, mechanical processing and mechanical testing. Characterization techniques included optical, electron microscopy, and x-ray texture analysis. The processing included heat-treatment and mechanical deformation through cold rolling. The initial as-cast materials were evaluated for their microstructure and mechanical properties. Different heat-treatment and rolling steps were chosen to process these materials. The properties were evaluated further and a processing relationship was established in order to obtain an optimum processing condition. The results showed that the as-cast material exhibited a Widmanstatten (fine grain) microstructure that developed into a microstructure with larger grains through processing steps. The texture intensity showed little change for all processing performed in this investigation.
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40 CFR 468.13 - New source performance standards (NSPS).
Code of Federal Regulations, 2010 CFR
2010-07-01
... copper alloy hot rolled English units—pounds per 1,000,000 off-pounds of copper or copper alloy hot... for monthly average Metric units—mg/off-kg of copper or copper alloy cold rolled English units—pounds... copper or copper alloy drawn English units—pounds per 1,000,000 off-pounds of copper or copper alloy...
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NASA Astrophysics Data System (ADS)
Chen, Zhiguo; Ren, Jieke; Zhang, Jishuai; Chen, Jiqiang; Fang, Liang
2016-02-01
Scanning electron microscopy, transmission electron microscopy, tensile test, exfoliation corrosion test, and slow strain rate tensile test were applied to investigate the properties and microstructure of Al-Zn-Mg-Cu alloy processed by final thermomechanical treatment, retrogression reaging, and novel thermomechanical treatment (a combination of retrogression reaging with cold or warm rolling). The results indicate that in comparison with conventional heat treatment, the novel thermomechanical treatment reduces the stress corrosion susceptibility. A good combination of mechanical properties, stress corrosion resistance, and exfoliation corrosion resistance can be obtained by combining retrogression reaging with warm rolling. The mechanism of the novel thermomechanical treatment is the synergistic effect of composite microstructure such as grain morphology, dislocation substructures, as well as the morphology and distribution of primary phases and precipitations.
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NASA Astrophysics Data System (ADS)
Galdos, L.; Saenz de Argandoña, E.; Mendiguren, J.; Silvestre, E.
2017-09-01
The roll levelling is a flattening process used to remove the residual stresses and imperfections of metal strips by means of plastic deformations. During the process, the metal sheet is subjected to cyclic tension-compression deformations leading to a flat product. The process is especially important to avoid final geometrical errors when coils are cold formed or when thick plates are cut by laser. In the last years, and due to the appearance of high strength materials such as Ultra High Strength Steels, machine design engineers are demanding reliable tools for the dimensioning of the levelling facilities. Like in other metal forming fields, finite element analysis seems to be the most widely used solution to understand the occurring phenomena and to calculate the processing loads. In this paper, the roll levelling process of the third generation Fortiform 1050 steel is numerically analysed. The process has been studied using the MSC MARC software and two different material laws. A pure isotropic hardening law has been used and set as the baseline study. In the second part, tension-compression tests have been carried out to analyse the cyclic behaviour of the steel. With the obtained data, a new material model using a combined isotropic-kinematic hardening formulation has been fitted. Finally, the influence of the material model in the numerical results has been analysed by comparing a pure isotropic model and the later combined mixed hardening model.
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Atzmon, M.; Johnson, W.L.; Verhoeven, J.D.
1987-02-03
Bulk metastable, amorphous or fine crystalline alloy materials are produced by reacting cold-worked, mechanically deformed filamentary precursors such as metal powder mixtures or intercalated metal foils. Cold-working consolidates the metals, increases the interfacial area, lowers the free energy for reaction, and reduces at least one characteristic dimension of the metals. For example, the grains of powder or the sheets of foil are clad in a container to form a disc. The disc is cold-rolled between the nip of rollers to form a flattened disc. The grains are further elongated by further rolling to form a very thin sheet of a lamellar filamentary structure containing filaments having a thickness of less than 0.01 microns. Thus, diffusion distance and time for reaction are substantially reduced when the flattened foil is thermally treated in oven to form a composite sheet containing metastable material dispersed in unreacted polycrystalline material. 4 figs.
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Microstructure and Precipitate's Characterization of the Cu-Ni-Si-P Alloy
NASA Astrophysics Data System (ADS)
Zhang, Yi; Tian, Baohong; Volinsky, Alex A.; Sun, Huili; Chai, Zhe; Liu, Ping; Chen, Xiaohong; Liu, Yong
2016-04-01
Microstructure of the Cu-Ni-Si-P alloy was investigated by transmission electron microscopy (TEM). The alloy had 551 MPa tensile strength, 226 HV hardness, and 36% IACS electrical conductivity after 80% cold rolling and aging at 450 °C for 2 h. Under the same aging conditions, but without the cold rolling, the strength, hardness, and electrical conductivity were 379 MPa, 216 HV, and 32% IACS, respectively. The precipitates identified by TEM characterization were δ-Ni2Si. Some semi-coherent spherical precipitates with a typical coffee bean contrast were found after aging for 48 h at 450 °C. The average diameter of the observed semi-coherent precipitates is about 5 nm. The morphology of the fracture surface was observed by scanning electron microscopy. All samples showed typical ductile fracture. The addition of P refined the grain size and increased the nucleation rate of the precipitates. The precipitated phase coarsening was inhibited by the small additions of P. After aging, the Cu-Ni-Si-P alloy can gain excellent mechanical properties with 804 MPa strength and 49% IACS conductivity. This study aimed to optimize processing conditions of the Cu-Ni-Si-P alloys.
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The Role of Second Phase Intermetallic Particles on the Spall Failure of 5083 Aluminum
2016-12-01
of mechanically processed 5083 aluminum (i.e., cold and hot rolled, extruded , etc.) has been previously studied by several researchers [1–4]. Results...Velocity Interferometry System for Any Reflector (VISAR) [6]. In addition, four end-state (ex situ spall recovery) experiments were conducted to augment all... extruded AMX602 Mg alloy (unpublished) J. dynamic behavior mater. (2016) 2:476–483 483 123 9 1 DEFENSE TECHNICAL (PDF) INFORMATION CTR DTIC OCA
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Finding an Optimal Thermo-Mechanical Processing Scheme for a Gum-Type Ti-Nb-Zr-Fe-O Alloy
NASA Astrophysics Data System (ADS)
Nocivin, Anna; Cojocaru, Vasile Danut; Raducanu, Doina; Cinca, Ion; Angelescu, Maria Lucia; Dan, Ioan; Serban, Nicolae; Cojocaru, Mirela
2017-09-01
A gum-type alloy was subjected to a thermo-mechanical processing scheme to establish a suitable process for obtaining superior structural and behavioural characteristics. Three processes were proposed: a homogenization treatment, a cold-rolling process and a solution treatment with three heating temperatures: 1073 K (800 °C), 1173 K (900 °C) and 1273 K (1000 °C). Results of all three proposed processes were analyzed using x-ray diffraction and scanning electron microscopy imaging, to establish and compare the structural modifications. The behavioural status was completed with micro-hardness and tensile strength tests. The optimal results were obtained for solution treatment at 1073 K.
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Inamura, T; Shimizu, R; Kim, H Y; Miyazaki, S; Hosoda, H
2016-04-01
The rolling rate (r) dependence of textures was investigated in the Ti-26Nb-3Al (mol%) alloy to reveal the conditions required to form the {001}<110> recrystallization texture, which is a desirable orientation for the β-titanium shape memory alloy. {001}<110> was the dominant cold-rolling texture when r=90% and it was transferred to the recrystallization texture without forming {112}<110>, which is detrimental for the isotropic mechanical properties of the rolled sheet. A further increase in r resulted in the formation of {112}<110> in both rolling and recrystallization textures. Therefore, r should be controlled to form only the {001}<110> rolling texture, because the {112}<110> texture can overwhelm the {001}<110> texture during recrystallization. Copyright © 2016 Elsevier B.V. All rights reserved.
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Analytical solution for shear bands in cold-rolled 1018 steel
NASA Astrophysics Data System (ADS)
Voyiadjis, George Z.; Almasri, Amin H.; Faghihi, Danial; Palazotto, Anthony N.
2012-06-01
Cold-rolled 1018 (CR-1018) carbon steel has been well known for its susceptibility to adiabatic shear banding under dynamic loadings. Analysis of these localizations highly depends on the selection of the constitutive model. To deal with this issue, a constitutive model that takes temperature and strain rate effect into account is proposed. The model is motivated by two physical-based models: the Zerilli and Armstrong and the Voyiadjis and Abed models. This material model, however, incorporates a simple softening term that is capable of simulating the softening behavior of CR-1018 steel. Instability, localization, and evolution of adiabatic shear bands are discussed and presented graphically. In addition, the effect of hydrostatic pressure is illustrated.
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Review on cold-formed steel connections.
Lee, Yeong Huei; Tan, Cher Siang; Mohammad, Shahrin; Tahir, Mahmood Md; Shek, Poi Ngian
2014-01-01
The concept of cold-formed light steel framing construction has been widespread after understanding its structural characteristics with massive research works over the years. Connection serves as one of the important elements for light steel framing in order to achieve its structural stability. Compared to hot-rolled steel sections, cold-formed steel connections perform dissimilarity due to the thin-walled behaviour. This paper aims to review current researches on cold-formed steel connections, particularly for screw connections, storage rack connections, welded connections, and bolted connections. The performance of these connections in the design of cold-formed steel structures is discussed.
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Review on Cold-Formed Steel Connections
Tan, Cher Siang; Mohammad, Shahrin; Md Tahir, Mahmood; Shek, Poi Ngian
2014-01-01
The concept of cold-formed light steel framing construction has been widespread after understanding its structural characteristics with massive research works over the years. Connection serves as one of the important elements for light steel framing in order to achieve its structural stability. Compared to hot-rolled steel sections, cold-formed steel connections perform dissimilarity due to the thin-walled behaviour. This paper aims to review current researches on cold-formed steel connections, particularly for screw connections, storage rack connections, welded connections, and bolted connections. The performance of these connections in the design of cold-formed steel structures is discussed. PMID:24688448
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40 CFR 468.15 - Pretreatment standards for new sources (PSNS).
Code of Federal Regulations, 2010 CFR
2010-07-01
... average Metric units—mg/off-kg of copper or copper alloy hot rolled English units—pounds per 1,000,000 off... English units—pounds per 1,000,000 off-pounds of copper or copper alloy cold rolled Chromium 0.140 0.056... copper alloy drawn English units—pounds per 1,000,000 off-pounds of copper or copper alloy drawn Chromium...
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Effect of Rolling on High-Cycle Fatigue and Fracture of an Al - Mg - Sc Alloy
NASA Astrophysics Data System (ADS)
Zhemchuzhnikova, D. A.; Petrov, A. P.; Eremeev, N. V.; Eremeev, V. V.; Kaibyshev, R. O.
2016-07-01
The tensile strength and fatigue properties of alloy 1575 of the Al - Mg - Sc system are studied after hot deformation (at 360°C) and subsequent cold rolling with different reduction ratios. The effect of the deformed structure on the properties and mechanisms of fracture of the alloy under cyclic tests is determined.
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New technology for recyclingmaterials from oily cold rollingmill sludge
NASA Astrophysics Data System (ADS)
Liu, Bo; Zhang, Shen-gen; Tian, Jian-jun; Pan, De-an; Meng, Ling; Liu, Yang
2013-12-01
Oily cold rolling mill (CRM) sludge is one of metallurgical industry solid wastes. The recycle of these wastes can not only protect the environment but also permit their reutilization. In this research, a new process of "hydrometallurgical treatment + hydrothermal synthesis" was investigated for the combined recovery of iron and organic materials from oily CRM sludge. Hydrometallurgical treatment, mainly including acid leaching, centrifugal separation, neutralization reaction, oxidizing, and preparation of hydrothermal reaction precursor, was first utilized for processing the sludge. Then, micaceous iron oxide (MIO) pigment powders were prepared through hydrothermal reaction of the obtained precursor in alkaline media. The separated organic materials can be used for fuel or chemical feedstock. The quality of the prepared MIO pigments is in accordance with the standards of MIO pigments for paints (ISO 10601-2007). This clean, effective, and economical technology offers a new way to recycle oily CRM sludge.
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Magnetostrictive clad steel plates for high-performance vibration energy harvesting
NASA Astrophysics Data System (ADS)
Yang, Zhenjun; Nakajima, Kenya; Onodera, Ryuichi; Tayama, Tsuyoki; Chiba, Daiki; Narita, Fumio
2018-02-01
Energy harvesting technology is becoming increasingly important with the appearance of the Internet of things. In this study, a magnetostrictive clad steel plate for harvesting vibration energy was proposed. It comprises a cold-rolled FeCo alloy and cold-rolled steel joined together by thermal diffusion bonding. The performances of the magnetostrictive FeCo clad steel plate and conventional FeCo plate cantilevers were compared under bending vibration; the results indicated that the clad steel plate construct exhibits high voltage and power output compared to a single-plate construct. Finite element analysis of the cantilevers under bending provided insights into the magnetic features of a clad steel plate, which is crucial for its high performance. For comparison, the experimental results of a commercial piezoelectric bimorph cantilever were also reported. In addition, the cold-rolled FeCo and Ni alloys were joined by thermal diffusion bonding, which exhibited outstanding energy harvesting performance. The larger the plate volume, the more the energy generated. The results of this study indicated not only a promising application for the magnetostrictive FeCo clad steel plate as an efficient energy harvester, related to small vibrations, but also the notable feasibility for the formation of integrated units to support high-power trains, automobiles, and electric vehicles.
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NASA Astrophysics Data System (ADS)
Bakare, F.; Alsubhi, Y.; Ragkousis, A.; Ebomwonyi, O.; Damisa, J.; Okunzuwa, S.
2017-07-01
The novel thermomechanical treatment employed by Wang Z et al (2014 Mater. Sci. Eng. A 607 313-7) in enhancing the mechanical and microstructure properties of 6000 series aluminium alloys has been replicated for AA2139 aerospace aluminium alloys. The novel route which involves under-ageing, cold-rolling reductions and re-ageing at a fixed temperature has been carried out focusing on the effect of pre-straining and pre-ageing on the alloy properties. The influence of varying cold-rolling reductions and pre-ageing has been examined by tensile testing, hardness testing, differential scanning calorimetry, thermoelectric power measurements and scanning electron microscope (SEM). Further analyses were conducted with DSC and TEP measurements to check for precipitation sequence and solute retention respectively. On comparing the hardness and strength of the non pre-aged to the pre-aged samples, there is a remarkable increase in the hardness and strength of the aerospace alloy showing the huge influence of both pre-ageing and pre-straining stage of the novel thermomechanical treatment as observed in the 6000 series alloy, albeit at a higher rate. The treatments that exhibited the most promising mechanical properties (hardness, yield and ultimate tensile strength, elongation to failure) were found to be at a pre-ageing temperature of 175 °C for 1.5 h, 40% cold-rolling and re-ageing at 150 °C. The material was found to have yield strength of 590 MPa and 8.1% uniform elongation, which is well above the 5% acceptable value for structural applications and with strength levels adaptable for aerospace industries. The presence of higher volume fraction of well dispersed precipitates observed in the SEM further shows that intermediate cold-rolling reductions combines well with pre-ageing to give the best mechanical properties in this alloy.
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Rapidly solidified titanium alloys by melt overflow
NASA Technical Reports Server (NTRS)
Gaspar, Thomas A.; Bruce, Thomas J., Jr.; Hackman, Lloyd E.; Brasmer, Susan E.; Dantzig, Jonathan A.; Baeslack, William A., III
1989-01-01
A pilot plant scale furnace was designed and constructed for casting titanium alloy strips. The furnace combines plasma arc skull melting techniques with melt overflow rapid solidification technology. A mathematical model of the melting and casting process was developed. The furnace cast strip of a suitable length and width for use with honeycomb structures. Titanium alloys Ti-6Al-4V and Ti-14Al-21 Nb were successfully cast into strips. The strips were evaluated by optical metallography, microhardness measurements, chemical analysis, and cold rolling.
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Effect of oxide particles on the stabilization and final microstructure in aluminium
Bachmaier, Andrea; Pippan, Reinhard
2011-01-01
Bulk aluminium samples containing alumina particles have been produced by different severe plastic deformation methods. Aluminium foils with different initial foil thicknesses were cold rolled to different amounts of strain and aluminium powders were consolidated and deformed by high pressure torsion (HPT). During processing, alumina particles from the foil or particle surface are easily incorporated and dispersed in the bulk material. The influence of these alumina particles on the developing microstructures and the mechanical properties has been studied. PMID:21976787
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DOE Office of Scientific and Technical Information (OSTI.GOV)
De Moor, Emmanuel
The present project investigated Quenching and Partitioning (Q&P) to process cold rolled steels to develop high strength sheet steels that exhibit superior ductility compared to available grades with the intent to allow forming of high strength parts at room temperature to provide an alternative to hot stamping of parts. Hot stamping of boron alloyed steel is the current technology to manufacture thinner gauge sections in automotive structures to guarantee anti-intrusion during collisions whilst improving fuel efficiency by decreasing vehicle weight. Hot stamping involves reheating steel to 900 °C or higher followed by deformation and quenching in the die to producemore » ultra-high strength materials. Hot stamping requires significant energy to reheat the steel and is less productive than traditional room temperature stamping operations. Stamping at elevated temperature was developed due to the lack of available steels with strength levels of interest possessing sufficient ductility enabling traditional room temperature forming. This process is seeing growing demand within the automotive industry and, given the reheating step in this operation, increased energy consumption during part manufacturing results. The present research program focused on the development of steel grades via Q&P processing that exhibit high strength and formability enabling room temperature forming to replace hot stamping. The main project objective consisted of developing sheet steels exhibiting minimum ultimate tensile strength levels of 1200 MPa in combination with minimum tensile elongation levels of 15 pct using Q&P processing through judicious alloy design and heat treating parameter definition. In addition, detailed microstructural characterization and study of properties, processing and microstructure interrelationships were pursued to develop strategies to further enhance tensile properties. In order to accomplish these objectives, alloy design was conducted towards achieving the target properties. Twelve alloys were designed and laboratory produced involving melting, alloying, casting, hot rolling, and cold rolling to obtain sheet steels of approximately 1 mm thickness. Q&P processing of the samples was then conducted. Target properties were achieved and substantially exceeded demonstrating success in the developed and employed alloy design approaches. The best combinations of tensile properties were found at approximately 1550 MPa with a total elongation in excess of 20 pct clearly showing the potential for replacement of hot stamping to produce advanced high strength steels.« less
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40 CFR 468.15 - Pretreatment standards for new sources (PSNS).
Code of Federal Regulations, 2011 CFR
2011-07-01
...-pounds of copper or copper alloy hot rolled Chromium 0.038 0.015 Copper 0.131 0.062 Lead 0.010 0.0092... English units—pounds per 1,000,000 off-pounds of copper or copper alloy cold rolled Chromium 0.140 0.056... copper alloy drawn English units—pounds per 1,000,000 off-pounds of copper or copper alloy drawn Chromium...
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Crystallographic and magnetic structure of HAVAR under high-pressure using diamond anvil cell (DAC)
NASA Astrophysics Data System (ADS)
Halevy, Itzhak; Haroush, Shlomo; Eisen, Yosef; Silberman, Ido; Moreno, Dany; Hen, Amir; Winterrose, Mike L.; Ghose, Sanjit; Chen, Zhiqiang
2010-04-01
Annealed (H1) and cold-rolled (H2) HAVAR has been studied using high-pressure synchrotron X-ray diffraction. A structural phase transformation was discovered at ˜13 GPa at ambient temperature, transforming from m - 3 m (S.G. 225) to P 63/m m c (S.G. 194) symmetry. The transition was not reversible on pressure release. The low-pressure cubic phase was found to be more compressible than the high-pressure hexagonal phase. Conventional Mössbauer and NFS shows that the HAVAR is not magnetic at room temperature and no splitting is observed. The SQUID indicates a huge difference in the temperature dependence of the magnetic susceptibility between the cold Rolled HAVAR compared to the annealed HAVAR.
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The Measurement of Elastic Constants for the Determination of Stresses by X-Rays
1983-07-01
both cases the hhh reflection is at the s.me or hlqher iN 29 value as the hkl reflection; thus any oscillations should be equally clear since the...reduct.oa 70-30 .2471" cold rolled to .02V (A-bras a 90" reduction 304 tainlaess .059’ cold re,’ .055" steel as rUI-. 1075 steel .03s " "ld rolled .03...6.85 4.83 5.54 6.14 4.36 .53 304 C 331 4.48 .20 4.01 3.82 3.92 3.13 stainless Te 222 3.75 .35 4.01 3.09 3.55 3.63 steil 3.51 .38 1075 Fe 220 4.17 .17
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Non-destructive Magnetic Evaluation of Laser Weld Quality in Hot Rolled Coils
NASA Astrophysics Data System (ADS)
Mohapatra, J. N.; Chakradhar, I.; Rao, K. R. C.; Rao, V. V. L.; Kaza, Marutiram
2015-06-01
Weld quality evaluation was conducted on laser welded thin sectsions (2 mm) of hot-rolled (HR) low-carbon steel coils during cold rolling process. The analysis revealed that the poor welds consisting of the weld defects like incomplete fusion, cluster of porosity, and large difference in hardness between the weld zone and base metal were responsible for the weld failures. Experiments were conducted by varying the welding parameters; laser power and welding speed to optimize the parameters for minimizing the weld defects. The optimized weld process parameters have helped elimination of weld defects and the results are verified with microscopy and microhardness measurements. As destructive evaluation techniques are time consuming and not always permitted in industrial applications, attempts have been made in the present investigation for the utilization of suitable non-destructive techniques for the evaluation of weld quality. Non-destructive magnetic techniques of magnetic hysteresis loop and magnetic Barkhausen emissions were used in the present investigation to establish possible correlations of magnetic properties across the weld seam with the mechanical property (microhardness) for evaluation of weld quality. It is inferred that the magnetic properties of coercivity and inverse of root mean square voltage can be effectively utilized to determine weld quality in HR steel coils.
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Bhattacharjee, T; Wani, I S; Sheikh, S; Clark, I T; Okawa, T; Guo, S; Bhattacharjee, P P; Tsuji, N
2018-02-19
Nano-lamellar (L1 2 + B2) AlCoCrFeNi 2.1 eutectic high entropy alloy (EHEA) was processed by cryo-rolling and annealing. The EHEA developed a novel hierarchical microstructure featured by fine lamellar regions consisting of FCC lamellae filled with ultrafine FCC grains (average size ~200-250 nm) and B2 lamellae, and coarse non-lamellar regions consisting of ultrafine FCC (average size ~200-250 nm), few coarse recrystallized FCC grains and rather coarse unrecrystallized B2 phase (~2.5 µm). This complex and hierarchical microstructure originated from differences in strain-partitioning amongst the constituent phases, affecting the driving force for recrystallization. The hierarchical microstructure of the cryo-rolled and annealed material resulted in simultaneous enhancement in strength (Yield Strength/YS: 1437 ± 26 MPa, Ultimate Tensile Strength/UTS: 1562 ± 33 MPa) and ductility (elongation to failure/e f ~ 14 ± 1%) as compared to the as-cast as well as cold-rolled and annealed materials. The present study for the first time demonstrated that cryo-deformation and annealing could be a novel microstructural design strategy for overcoming strength-ductility trade off in multiphase high entropy alloys.
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Atzmon, Michael; Johnson, William L.; Verhoeven, John D.
1987-01-01
Bulk metastable, amorphous or fine crystalline alloy materials are produced by reacting cold-worked, mechanically deformed filamentary precursors such as metal powder mixtures or intercalated metal foils. Cold-working consolidates the metals, increases the interfacial area, lowers the free energy for reaction, and reduces at least one characteristic dimension of the metals. For example, the grains (13) of powder or the sheets of foil are clad in a container (14) to form a disc (10). The disc (10) is cold-rolled between the nip (16) of rollers (18,20) to form a flattened disc (22). The grains (13) are further elongated by further rolling to form a very thin sheet (26) of a lamellar filamentary structure (FIG. 4) containing filaments having a thickness of less than 0.01 microns. Thus, diffusion distance and time for reaction are substantially reduced when the flattened foil (28) is thermally treated in oven (32) to form a composite sheet (33) containing metastable material (34) dispersed in unreacted polycrystalline material (36).
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NASA Technical Reports Server (NTRS)
Titran, Robert H.; Uz, Mehmet
1996-01-01
A systematic study to evaluate the effects of thermomechanical processing on the microstructure and mechanical properties of Nb-1Zr alloy sheet containing 0.06 and 0.1 wt.%C (PWC-11) was conducted and compared to the results of Nb-1Zr. Coarse orthorhombic Nb2C precipitates were present in all the cast, extruded and cold rolled Nb-Zr samples containing C. After high temperature (greater than 0.5 T(sub m)) exposure (with or without applied stress), the Nb2C transforms to very fine and extremely stable FCC (Zr, Nb)C dispersoid, resulting in a highly creep resistant material. Only ZrO2 precipitates were found in Nb-1Zr. The creep strength of the 0.06C and the 0.1C carbide strengthened alloys were much superior to Nb-1Zr. At 1350 K the strength of the 0.06C alloy was about three times that of Nb-1Zr, while the 0.1C alloy had about five times the creep stress capability of Nb-1Zr. The tensile strength, long term creep strength, and stability of the microstructure of the PWC-11 sheet appear to be independent of the number of 1900 K extrusions performed prior to cold rolling. The microhardness of these single, double and triple extnided PWC-11 sheets also were comparable. The tensile strength of PWC-11 and Nb-1Zr at room temperature and 1350 K were comparable.
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Code of Federal Regulations, 2010 CFR
2010-07-01
... Metric units—mg/off-kg of copper or copper alloy hot rolled English units—pounds per 1,000,000 off-pounds... copper or copper alloy cold rolled English units—pounds per 1,000,000 off-pounds of copper or copper... drawn English units—pounds per 1,000,000 off-pounds of copper or copper alloy drawn Chromium 0.037 0.015...
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Code of Federal Regulations, 2010 CFR
2010-07-01
... English Units—pounds per 1,000,000 off-pounds of copper or copper alloy hot rolled Chromium 0.045 0.018... monthly average Metric units—mg/off-kg of copper or copper alloy cold rolled English units—pounds per 1.../off-kg of copper or copper alloy drawn English units—pounds per 1,000,000 off-pounds of copper or...
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Fabrication of seamless calandria tubes by cold pilgering route using 3-pass and 2-pass schedules
NASA Astrophysics Data System (ADS)
Saibaba, N.
2008-12-01
Calandria tube is a large diameter, extremely thin walled zirconium alloy tube which has diameter to wall thickness ratio as high as 90-95. Such tubes are conventionally produced by the 'welded route', which involves extrusion of slabs followed by a series of hot and cold rolling passes, intermediate anneals, press forming of sheets into circular shape and closing the gap by TIG welding. Though pilgering is a well established process for the fabrication of seamless tubes, production of extremely thin walled tubes offers several challenges during pilgering. Nuclear fuel complex (NFC), Hyderabad, has successfully developed a process for the production of Zircaloy-4 calandria tubes by adopting the 'seamless route' which involves hot extrusion of mother blanks followed by three-pass pilgering or two-pass pilgering schedules. This paper deals with standardization of the seamless route processes for fabrication of calandria tubes, comparison between the tubes produced by 2-pass and 3-pass pilgering schedules, role of ultrasonic test charts for control of process parameters, development of new testing methods for burst testing and other properties.
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NASA Astrophysics Data System (ADS)
Li, Xiaopei; Li, Xiaohui; Kure-Chu, Song-Zhu; Tang, Guoyi
2017-12-01
Cold-rolled AZ31 Mg alloy strips, with a reduction of 33 pct, were subjected to electropulse treatment (EPT) and conventional heat treatment (HT) to evaluate the respective influences of electropulses and temperature on the recrystallization behavior of AZ31. The highest measured temperature during the EPT (543 K) was used in HT. The electron backscattered diffraction results demonstrated that the EPT-stimulated recrystallization was completed within 8 seconds, whereas for HT, recrystallization was still far from completion even after 240 seconds. It was found that both the nucleation and grain growth of these two processes were totally different. In the EPT samples, nucleation tended to occur preferentially near extension twin boundaries and grain boundaries by continuous recrystallization, whereas in the HT samples, nucleation occurred mainly by grain boundaries bulging via discontinuous recrystallization. As grain growth proceeded, the texture intensities of the EPT samples decreased gradually and finally evolved into an obvious transverse-direction-split texture. This is likely attributable to the impact of electropulses on the boundary energy and the contribution of nonbasal dislocations; however, the basal-type textures of the HT samples were notably strengthened, which is associated with a 30 deg〈0001〉 orientation with respect to the deformed texture.
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NASA Astrophysics Data System (ADS)
Li, Xiaopei; Li, Xiaohui; Kure-Chu, Song-Zhu; Tang, Guoyi
2018-02-01
Cold-rolled AZ31 Mg alloy strips, with a reduction of 33 pct, were subjected to electropulse treatment (EPT) and conventional heat treatment (HT) to evaluate the respective influences of electropulses and temperature on the recrystallization behavior of AZ31. The highest measured temperature during the EPT (543 K) was used in HT. The electron backscattered diffraction results demonstrated that the EPT-stimulated recrystallization was completed within 8 seconds, whereas for HT, recrystallization was still far from completion even after 240 seconds. It was found that both the nucleation and grain growth of these two processes were totally different. In the EPT samples, nucleation tended to occur preferentially near extension twin boundaries and grain boundaries by continuous recrystallization, whereas in the HT samples, nucleation occurred mainly by grain boundaries bulging via discontinuous recrystallization. As grain growth proceeded, the texture intensities of the EPT samples decreased gradually and finally evolved into an obvious transverse-direction-split texture. This is likely attributable to the impact of electropulses on the boundary energy and the contribution of nonbasal dislocations; however, the basal-type textures of the HT samples were notably strengthened, which is associated with a 30 deg〈0001〉 orientation with respect to the deformed texture.
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NASA Astrophysics Data System (ADS)
Papa Rao, M.; Subramanya Sarma, V.; Sankaran, S.
2017-03-01
Ultrafine-grained (UFG) dual-phase (DP) steel was produced by severe cold rolling (true strain of 2.4) and intercritical annealing of a low carbon V-Nb microalloyed steel in a temperature range of 1003 K to 1033 K (730 °C to 760 °C) for 2 minutes, and water quenching. The microstructure of UFG DP steels consisted of polygonal ferrite matrix with homogeneously distributed martensite islands (both of size <1 µm) and a small fraction of the inter lath films of retained austenite. The UFG DP steel produced through intercritical annealing at 1013 K (740 °C) has good combination of strength (1295 MPa) and ductility (uniform elongation, 13 pct). The nanoscale V- and Nb-based carbides/carbonitrides and spheroidized cementite particles have played a crucial role in achieving UFG DP microstructure and in improving the strength and work hardening. Analysis of work hardening behavior of the UFG DP steels through modified Crussard-Jaoul analysis showed a continuously varying work hardening rate response which could be approximated by 2 or 3 linear regimes. The transmission electron microscopy analysis on post tensile-tested samples indicated that these regimes are possibly related to the work hardening of ferrite, lath, and twin martensite, respectively.
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NASA Astrophysics Data System (ADS)
Yan, Ru; He, Wei; Zhai, Tianhua; Ma, Houyi
2018-06-01
Seeing that amino trimethylene phosphonic acid (ATMP) possesses very strong complexation ability to metal ions and the phosphonic acid group has good affinity for the oxidized iron surface, herein a simple and rapid film-forming method (one-step assembly method) was developed to construct the ATMP-Zn complex conversion layers (ATMP-Zn layers for short) on the cold-rolled steel (CRS) substrate. Zinc ions were found to participate in the formation process of ATMP-based composite film, which made the Zn-containing ATMP film significantly different in appearance, thickness, microstructure and film-forming mechanisms from the Zn-free ATMP film. There was mainly iron (ш) phosphonate in the Zn-free ATMP film, whereas there were Zn2+-ATMP complex and a certain amount of ZnO in the ATMP-Zn composite film. In addition, electrochemical test results clearly indicate that corrosion resistance of ATMP-Zn composite film was greatly enhanced due to the presence of Zn component. Moreover, the corrosion resistance performance could be controlled by adjusting film-forming time, pH and ATMP concentration in the film-forming solutions. The present study provides a new method for the design and fabrication of high-quality environmentally-friendly conversion layers.
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NASA Astrophysics Data System (ADS)
Nakano, Hayato; Hakoyama, Tomoyuki; Kuwabara, Toshihiko
2017-10-01
Hole expansion forming of a cold rolled steel sheet is investigated both experimentally and analytically to clarify the effects of material models on the predictive accuracy of finite element analyses (FEA). The multiaxial plastic deformation behavior of a cold rolled steel sheet with a thickness of 1.2 mm was measured using a servo-controlled multiaxial tube expansion testing machine for the range of strain from initial yield to fracture. Tubular specimens were fabricated from the sheet sample by roller bending and laser welding. Many linear stress paths in the first quadrant of stress space were applied to the tubular specimens to measure the contours of plastic work in stress space up to a reference plastic strain of 0.24 along with the directions of plastic strain rates. The anisotropic parameters and exponent of the Yld2000-2d yield function (Barlat et al., 2003) were optimized to approximate the contours of plastic work and the directions of plastic strain rates. The hole expansion forming simulations were performed using the different model identifications based on the Yld2000-2d yield function. It is concluded that the yield function best capturing both the plastic work contours and the directions of plastic strain rates leads to the most accurate predicted FEA.
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Corrosion Inhibition of Cold-rolled Low Carbon Steel with Pulse Fiber Laser Ablation in Water
NASA Astrophysics Data System (ADS)
Chan, Sze Ney; Wong, Wai Yin; Walvekar, Rashmi; Kadhum, Abdul Amir H.; Khalid, Mohammad; Lim, Kean Long
2018-04-01
This study aims at the use of a fiber laser for modifying the surface properties of cold-rolled low carbon steel via a pulse laser ablation technique in water. The effect on the corrosion behavior of the fiber laser-treated metal surface was investigated in NaCl and HCl environments. Electrochemical tests showed significant improvement in the corrosion resistance of the laser-treated sample in NaCl, with an increase in open-circuit potential (OCP) from - 0.65 to - 0.60 V and an inhibition efficiency of 89.22% as obtained from the impedance study. Such improvement was less significant in an acidic environment. Lower corrosion rates of 20.9 mpy and 5.819 × 103 mpy were obtained for the laser-treated samples in neutral and acidic electrolytes, respectively, than the corrosion rates obtained for the as-received samples (33.2 mpy and 11.98 × 103 mpy). Morphological analysis indicated a passive film built by spherical grains of regular size on the metal surface after laser treatment. The corrosion inhibition effects in NaCl were evident by the nonexistence of the common corrosion products of lepidocrocite and crystalline structures that were seen on as-received samples; only polyhedral crystals with micrograins grown on them were seen covering the laser-treated surface. Therefore, the laser treatment using a fiber laser source improved the corrosion resistance of cold-rolled low carbon steel.
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NASA Astrophysics Data System (ADS)
Dutton, Kenneth
Shape (or flatness) control for rolled steel strip is becoming increasingly important as customer requirements become more stringent. Automatic shape control is now more or less mandatory on all new four-high cold mills, but no comprehensive scheme yet exists on a Sendzimir mill. This is due to the complexity of the control system design on such a mill, where many more degrees of freedom for control exist than is the case with the four-high mills.The objective of the current work is to develop, from first principles, such a system; including automatic control of the As-U-Roll and first intermediate roll actuators in response to the measured strip shape. This thesis concerns itself primarily with the As-U-Roll control system. The material presented is extremely wide-ranging. Areas covered include the development of original static and dynamic mathematical models of the mill systems, and testing of the plant by data-logging to tune these models. A basic control system philosophy proposed by other workers is modified and developed to suit the practical system requirements and the data provided by the models. The control strategy is tested by comprehensive multivariable simulation studies. Finally, details are given of the practical problems faced when installing the system on the plant. These include problems of manual control inter-action bumpless transfer and integral desaturation.At the time of presentation of the thesis, system commissioning is still in progress and production results are therefore not yet available. Nevertheless, the simulation studies predict a successful outcome, although performance is expected to be limited until the first intermediate roll actuators are eventually included in the scheme also.
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NASA Astrophysics Data System (ADS)
Deng, Yonggang; Di, Hongshuang; Hu, Meiyuan; Zhang, Jiecen; Misra, R. D. K.
2017-07-01
Ultrafine-grained dual-phase (UFG-DP) steel consisting of ferrite (1.2 μm) and martensite (1 μm) was uniquely processed via combination of hot rolling, cold rolling and continuous annealing of a low-carbon Nb-microalloyed steel. Room temperature tensile properties were evaluated and fracture mechanisms studied and compared to the coarse-grained (CG) counterpart. In contrast to the CG-DP steel, UFG-DP had 12.7% higher ultimate tensile strength and 10.7% greater uniform elongation. This is partly attributed to the increase in the initial strain-hardening rate, decrease in nanohardness ratio of martensite and ferrite. Moreover, a decreasing number of ferrite grains with {001} orientation increased the cleavage fracture stress and increased the crack initiation threshold stress with consequent improvement in ductility UFG-DP steel.
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NASA Astrophysics Data System (ADS)
Han, Yun; Kuang, Shuang; Qi, Xiumei; Xie, Chunqian; Liu, Guanghui
Effects of galvanizing simulation parameters on microstructures and mechanical properties of Ti-microalloyed cold rolled hot-dip galvanizing DP980 steel were investigated in this study by optical microscopy (OM), transmission electron microscopy (TEM), energy dispersive spectroscopy (EDS) and tensile test. Moreover, the precipitation behavior of Ti in the experimental steel was also studied. The results show that, as the heating temperature increases, the tensile strength of experimental galvanizing DP980 steel decreases while the yield ratio and elongation of the steel are enhanced. The microstructures of experimental steels exhibit typical dual phase steel character and the volume fractions of MA islands are almost 30%. In addition, lots of nano-sized TiC precipitates can be found in the ferrite grains.
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Manufacturing of calcium, lithium and molybdenum targets for use in nuclear physics experiments
NASA Astrophysics Data System (ADS)
Kheswa, N. Y.; Papka, P.; Buthelezi, E. Z.; Lieder, R. M.; Neveling, R.; Newman, R. T.
2010-02-01
This paper describes methods used in the manufacturing of chemically reactive targets such as calcium ( natCa), lithium-6 ( 6Li) and molybdenum-97 ( 97Mo) for nuclear physics experiments at the iThemba LABS cyclotron facility (Faure, South Africa). Due to the chemical properties of these materials a suitable and controlled environment was established in order to minimize oxygen contamination of targets. Calcium was prepared by means of vacuum evaporation while lithium was cold rolled to a desired thickness. In the case of molybdenum, the metallic powder was melted under vacuum using an e-gun followed by cold rolling of the metal bead to a desired thickness. In addition, latest developments toward the establishment of a dedicated nuclear physics target laboratory are discussed.
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NASA Astrophysics Data System (ADS)
Ogawa, Toshio; Dannoshita, Hiroyuki; Maruoka, Kuniaki; Ushioda, Kohsaku
2017-08-01
Microstructural evolution during cold rolling and subsequent annealing of low-carbon steel with different initial microstructures was investigated from the perspective of the competitive phenomenon between recrystallization of ferrite and reverse phase transformation from ferrite to austenite. Three kinds of hot-rolled sheet specimens were prepared. Specimen P consisted of ferrite and pearlite, specimen B consisted of bainite, and specimen M consisted of martensite. The progress of recovery and recrystallization of ferrite during annealing was more rapid in specimen M than that in specimens P and B. In particular, the recrystallized ferrite grains in specimen M were fine and equiaxed. The progress of ferrite-to-austenite phase transformation during intercritical annealing was more rapid in specimen M than in specimens P and B. In all specimens, the austenite nucleation sites were mainly at high-angle grain boundaries, such as those between recrystallized ferrite grains. The austenite distribution was the most uniform in specimen M. Thus, we concluded that fine equiaxed recrystallized ferrite grains were formed in specimen M, leading to a uniform distribution of austenite.
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NASA Astrophysics Data System (ADS)
Rokhlin, L. L.; Dobatkina, T. V.; Luk'yanova, E. A.; Korol'kova, I. G.; Choporov, V. F.
2016-07-01
The microstructure and strength properties of hot-pressed alloy IMV7-1 of the Mg - Y - Gd - Zr system are studied after additional cold and hot rolling deformation. It is shown that the strength properties of the pressed alloy can be elevated by cold deformation at an admissible level of ductility.
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Texture evolution in Oxide Dispersion Strengthened (ODS) steel tubes during pilgering process
NASA Astrophysics Data System (ADS)
Vakhitova, E.; Sornin, D.; Barcelo, F.; François, M.
2017-10-01
Oxide Dispersion Strengthened (ODS) steels are foreseen as fuel cladding material in the coming generation of Sodium Fast Reactors (SFR). Cladding tubes are manufactured by hot extrusion and subsequent cold forming steps. In this study, a 9 wt% Cr ODS steel exhibiting α-γ phase transformation at high temperature is cold formed under industrial conditions with a large section reduction in two pilgering steps. The influence of pilgering process parameters and intermediate heat treatment on the microstructure evolution is studied experimentally using Electron Backscattering Diffraction (EBSD) and X-ray Diffraction (XRD) methods. Pilgered samples show elongated grains and a high texture formation with a preferential orientation along the rolling direction. During the heat treatment, grain morphology is recovered from elongated grains to almost equiaxed ones, while the well-known α-fiber texture presents an unexpected increase in intensity. The remarkable temperature stability of this fiber is attributed to a crystallographic structure memory effect during phase transformations.
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NASA Astrophysics Data System (ADS)
Leuning, Nora; Steentjes, Simon; Stöcker, Anett; Kawalla, Rudolf; Wei, Xuefei; Dierdorf, Jens; Hirt, Gerhard; Roggenbuck, Stefan; Korte-Kerzel, Sandra; Weiss, Hannes A.; Volk, Wolfram; Hameyer, Kay
2018-04-01
Thin laminations of non-grain oriented (NO) electrical steels form the magnetic core of rotating electrical machines. The magnetic properties of these laminations are therefore key elements for the efficiency of electric drives and need to be fully utilized. Ideally, high magnetization and low losses are realized over the entire polarization and frequency spectrum at reasonable production and processing costs. However, such an ideal material does not exist and thus, achievable magnetic properties need to be deduced from the respective application requirements. Parameters of the electrical steel such as lamination thickness, microstructure and texture affect the magnetic properties as well as their polarization and frequency dependence. These structural features represent possibilities to actively alter the magnetic properties, e.g., magnetization curve, magnetic loss or frequency dependence. This paper studies the influence of production and processing on the resulting magnetic properties of a 2.4 wt% Si electrical steel. Aim is to close the gap between production influence on the material properties and its resulting effect on the magnetization curves and losses at different frequencies with a strong focus on occurring interdependencies between production and mechanical processing. The material production is realized on an experimental processing route that comprises the steps of hot rolling, cold rolling, annealing and punching.
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NASA Astrophysics Data System (ADS)
Gong, Yu
For galvanized or galvannealed steels to be commercially successful, they must exhibit several attributes: (i) easy and inexpensive processing in the hot mill, cold mill and on the coating line, (ii) high strength with good formability and spot weldability, and (iii) good corrosion resistance. At the beginning of this thesis, compositions with a common base but containing various additions of V or Nb with or without high N were designed and subjected to Gleeble simulations of different galvanizing(GI), galvannealing(GA) and supercooling processing. The results revealed the phase balance was strongly influenced by the different microalloying additions, while the strengths of each phase were somewhat less affected. Our research revealed that the amount of austenite formed during intercritical annealing can be strongly influenced by the annealing temperature and the pre-annealing conditions of the hot band (coiling temperature) and cold band (% cold reduction). In the late part of this thesis, the base composition was a low carbon steel which would exhibit good spot weldability. To this steel were added two levels of Cr and Mo for strengthening the ferrite and increasing the hardenability of intercritically formed austenite. Also, these steels were produced with and without the addition of vanadium in an effort to further increase the strength. Since earlier studies revealed a relationship between the nature of the starting cold rolled microstructure and the response to CGL processing, the variables of hot band coiling temperature and level of cold reduction prior to annealing were also studied. Finally, in an effort to increase strength and ductility of both the final sheet (general formability) and the sheared edges of cold punched holes (local formability), a new thermal path was developed that replaced the conventional GI ferrite-martensite microstructure with a new ferrite-martensite-tempered martensite and retained austenite microstructure. The new microstructure exhibited a somewhat lower strength but much high general and local formabilities. In this thesis, both the physical and mechanical metallurgy of these steels and processes will be discussed. This research has shown that simple compositions and processes can result in DP steels with so-called Generation III properties.
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CRN5EXP: Expert system for statistical quality control
NASA Technical Reports Server (NTRS)
Hentea, Mariana
1991-01-01
The purpose of the Expert System CRN5EXP is to assist in checking the quality of the coils at two very important mills: Hot Rolling and Cold Rolling in a steel plant. The system interprets the statistical quality control charts, diagnoses and predicts the quality of the steel. Measurements of process control variables are recorded in a database and sample statistics such as the mean and the range are computed and plotted on a control chart. The chart is analyzed through patterns using the C Language Integrated Production System (CLIPS) and a forward chaining technique to reach a conclusion about the causes of defects and to take management measures for the improvement of the quality control techniques. The Expert System combines the certainty factors associated with the process control variables to predict the quality of the steel. The paper presents the approach to extract data from the database, the reason to combine certainty factors, the architecture and the use of the Expert System. However, the interpretation of control charts patterns requires the human expert's knowledge and lends to Expert Systems rules.
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Code of Federal Regulations, 2013 CFR
2013-07-01
... of copper or copper alloy hot rolled Chromium 0.045 0.018 Copper 0.195 0.103 Lead 0.015 0.013 Nickel... alloy cold rolled Chromium 0.166 0.068 Copper 0.720 0.379 Lead 0.056 0.049 Nickel 0.727 0.481 Zinc 0.553... drawn English units—pounds per 1,000,000 off-pounds of copper or copper alloy drawn Chromium 0.037 0.015...
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Code of Federal Regulations, 2014 CFR
2014-07-01
... English Units—pounds per 1,000,000 off-pounds of copper or copper alloy hot rolled Chromium 0.045 0.018...,000,000 off-pounds of copper or copper alloy cold rolled Chromium 0.166 0.068 Copper 0.720 0.379 Lead... copper alloy drawn Chromium 0.037 0.015 Copper 0.161 0.085 Lead 0.012 0.011 Nickel 0.163 0.107 Zinc 0.124...
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40 CFR 468.13 - New source performance standards (NSPS).
Code of Federal Regulations, 2011 CFR
2011-07-01
... rolled Chromium 0.038 0.015 Copper 0.131 0.062 Lead 0.010 0.0092 Nickel 0.056 0.038 Zinc 0.105 0.043 Oil... per 1,000,000 off-pounds of copper or copper alloy cold rolled Chromium 0.140 0.056 Copper 0.485 0.231... drawn Chromium 0.031 0.012 Copper 0.108 0.051 Lead 0.0085 0.0076 Nickel 0.046 0.031 Zinc 0.086 0.035 Oil...
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Code of Federal Regulations, 2013 CFR
2013-07-01
... English Units—pounds per 1,000,000 off-pounds of copper or copper alloy hot rolled Chromium 0.045 0.018...,000,000 off-pounds of copper or copper alloy cold rolled Chromium 0.166 0.068 Copper 0.720 0.379 Lead... copper alloy drawn Chromium 0.037 0.015 Copper 0.161 0.085 Lead 0.012 0.011 Nickel 0.163 0.107 Zinc 0.124...
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Code of Federal Regulations, 2012 CFR
2012-07-01
... of copper or copper alloy hot rolled Chromium 0.045 0.018 Copper 0.195 0.103 Lead 0.015 0.013 Nickel... alloy cold rolled Chromium 0.166 0.068 Copper 0.720 0.379 Lead 0.056 0.049 Nickel 0.727 0.481 Zinc 0.553... drawn English units—pounds per 1,000,000 off-pounds of copper or copper alloy drawn Chromium 0.037 0.015...
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Code of Federal Regulations, 2012 CFR
2012-07-01
... English Units—pounds per 1,000,000 off-pounds of copper or copper alloy hot rolled Chromium 0.045 0.018...,000,000 off-pounds of copper or copper alloy cold rolled Chromium 0.166 0.068 Copper 0.720 0.379 Lead... copper alloy drawn Chromium 0.037 0.015 Copper 0.161 0.085 Lead 0.012 0.011 Nickel 0.163 0.107 Zinc 0.124...
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Code of Federal Regulations, 2011 CFR
2011-07-01
... of copper or copper alloy hot rolled Chromium 0.045 0.018 Copper 0.195 0.103 Lead 0.015 0.013 Nickel... alloy cold rolled Chromium 0.166 0.068 Copper 0.720 0.379 Lead 0.056 0.049 Nickel 0.727 0.481 Zinc 0.553... drawn English units—pounds per 1,000,000 off-pounds of copper or copper alloy drawn Chromium 0.037 0.015...
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Code of Federal Regulations, 2011 CFR
2011-07-01
... English Units—pounds per 1,000,000 off-pounds of copper or copper alloy hot rolled Chromium 0.045 0.018...,000,000 off-pounds of copper or copper alloy cold rolled Chromium 0.166 0.068 Copper 0.720 0.379 Lead... copper alloy drawn Chromium 0.037 0.015 Copper 0.161 0.085 Lead 0.012 0.011 Nickel 0.163 0.107 Zinc 0.124...
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Code of Federal Regulations, 2014 CFR
2014-07-01
... of copper or copper alloy hot rolled Chromium 0.045 0.018 Copper 0.195 0.103 Lead 0.015 0.013 Nickel... alloy cold rolled Chromium 0.166 0.068 Copper 0.720 0.379 Lead 0.056 0.049 Nickel 0.727 0.481 Zinc 0.553... drawn English units—pounds per 1,000,000 off-pounds of copper or copper alloy drawn Chromium 0.037 0.015...
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NASA Astrophysics Data System (ADS)
De Giorgi, Chiara; Furlan, Valentina; Demir, Ali Gökhan; Tallarita, Elena; Candiani, Gabriele; Previtali, Barbara
2017-06-01
In this work, laser micropolishing (LμP) was employed to reduce the surface roughness and waviness of cold-rolled AISI 304 stainless steel sheets. A pulsed fibre laser operating in the ns regime was used and the influence of laser parameters in a N2-controlled atmospheres was evaluated. In the optimal conditions, the surface remelting induced by the process allowed to reduce the surface roughness by closing cracks and defects formed during the rolling process. Other conditions that did not improve the surface quality were analysed for defect typology. Moreover, laser treatments allowed the production of more hydrophobic surfaces, and no surface chemistry modification was identified. Surface cleanability was investigated with Escherichia coli (E. coli), evaluating the number of residual bacteria adhering to the substrate after a washing procedure. These results showed that LμP is a suitable way to lower the average surface roughness by about 58% and average surface waviness by approximately 38%. The LμP process proved to be effective on the bacteria cleanability as approximately five times fewer bacteria remained on the surfaces treated with the optimized LμP parameters compared to the untreated surfaces.
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SCC of Alloy 690 and its Weld Metals
NASA Astrophysics Data System (ADS)
Andresen, Peter L.; Morra, Martin M.; Ahluwalia, Kawaljit
Alloy 690 base metal, HAZ and weld metal were tested in representative PWR primary water at 290 to 360°C. Intergranular cracking was observed in all materials. Growth rates as high as 1.2 × 10-6 mm/s were observed in the S-L orientation with micro structural banded material after cold rolling or forging to align the planes of banding, rolling and cracking. However, not all banded material has exhibited such high growth rates. Growth rates on homogeneous Alloy 690, including extruded CRDM tubing, often showed growth rates in the range of 2 - 8 × 10-8 mm/s in cold worked condition and an S-L orientation. Crack growth rates in some Alloy 690 tests were in the range of 1 to 10 × 10-9 mm/s, primarily in orientations other than S-L. For cracks aligned along the HAZ, growth rates as high as 1.2 × 10-8 mm/s were observed. Alloy 152/52/52i weld metals always exhibited low growth rates, apart from a weld that was further cold worked by 20%, which grew at 7 × 10-9 mm/s.
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Reverse-transformation austenite structure control with micro/nanometer size
NASA Astrophysics Data System (ADS)
Wu, Hui-bin; Niu, Gang; Wu, Feng-juan; Tang, Di
2017-05-01
To control the reverse-transformation austenite structure through manipulation of the micro/nanometer grain structure, the influences of cold deformation and annealing parameters on the microstructure evolution and mechanical properties of 316L austenitic stainless steel were investigated. The samples were first cold-rolled, and then samples deformed to different extents were annealed at different temperatures. The microstructure evolutions were analyzed by optical microscopy, scanning electron microscopy (SEM), magnetic measurements, and X-ray diffraction (XRD); the mechanical properties are also determined by tensile tests. The results showed that the fraction of stain-induced martensite was approximately 72% in the 90% cold-rolled steel. The micro/nanometric microstructure was obtained after reversion annealing at 820-870°C for 60 s. Nearly 100% reversed austenite was obtained in samples annealed at 850°C, where grains with a diameter ≤ 500 nm accounted for 30% and those with a diameter > 0.5 μm accounted for 70%. The micro/nanometer-grain steel exhibited not only a high strength level (approximately 959 MPa) but also a desirable elongation of approximately 45%.
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The Mechanical Property of Batch Annealed High Strength Low Alloy Steel HC260LA
NASA Astrophysics Data System (ADS)
Yang, Xiaojiang; Xia, Mingsheng; Zhang, Hongbo; Han, Bin; Li, Guilan
Cold rolled high strength low alloy steel is widely applied in the automotive parts due to its excellent formability and weldability. In this paper, the steel grade HC260LA according to European Norm was developed with batch annealing process. With commercial C-Mn mild steel as a benchmark, three different groups of chemistry namely C-Mn-Si, C-Mn-Nb-Ti and C-Mn-Nb were compared in terms of yield-tensile strength (Y/T) ratio. Microstructure and mechanical properties were characterized as well. Based on industrial production results, chemistry and detailed process parameters for batch annealing were identified. In the end the optimal Y/T ratio was proposed for this steel grade under batch annealing process.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Kim, J.S.; Kim, S.I.; Choi, S.-H., E-mail: shihoon@sunchon.ac.kr
2014-06-01
The electron backscatter diffraction technique has been used to characterize the microstructure of deformed grains in cold-rolled, Cu-added, bake-hardenable steel. A new scheme based on the kind and number of average orientations, as determined from a unique grain map of the deformed grains, was developed in order to classify deformed grains by type. The α-fiber components, γ-fiber components and random orientations, those which could not be assigned to either γ-fiber or α-fiber components, were used to define the average orientation of unique grains within individual deformed grains. The microstructures of deformed grains in as-rolled specimens were analyzed based on themore » Taylor factor, stored energy, and misorientation. The relative levels and distributions of the Taylor factor, the stored energy and the misorientation were examined in terms of the types of deformed grains. - Highlights: • We characterized the microstructure of Cu-added BH steel using EBSD. • A new scheme was developed in order to classify deformed grains by type. • Stored energy and misorientation are strongly dependent on the type of deformed grains. • Microstructure was examined in terms of the types of deformed grains.« less
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Roll type conducting polymer legs for rigid-flexible thermoelectric generator
NASA Astrophysics Data System (ADS)
Park, Teahoon; Lim, Hanwhuy; Hwang, Jong Un; Na, Jongbeom; Lee, Hyunki; Kim, Eunkyoung
2017-07-01
A roll-type conducting polymer film was explored as a flexible organic p-type thermoelectric leg using poly(3,4-ethylenedioxythiophene) (PEDOT) doped with tosylate. The PEDOT films were prepared through solution casting polymerization and rolled up for a roll-type leg. Due to the high flexibility, the roll-type PEDOT leg enabled easy contact to both top and bottom electrodes. Simulation on the dynamic heat transfer and convective cooling for a vertically roosted rod- and roll-type PEDOT leg showed that the temperature difference (ΔT) between the hot and cold sides of the leg was much higher in the roll than that of the rod. The PEDOT legs were integrated with n-type Bi2Te3 blocks, to give a 36-couple rigid-flexible thermoelectric generator (RF-TEG). The maximum output voltage from the 36-couple RF-TEG under a ΔT of 7.9 K was determined as 36.7 mV along with a high output power of 115 nW. A wearable RF-TEG was prepared upon the combination of the 36-couple RF-TEG with an arm warmer, to afford an output voltage of 10.6 mV, which was generated constantly and steadily from human wrist heat.
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NASA Astrophysics Data System (ADS)
Bannykh, O. A.; Betsofen, S. Ya.; Lukin, E. I.; Blinov, V. M.; Voznesenskaya, N. M.; Tonysheva, O. A.; Blinov, E. V.
2016-04-01
The effect of the rolling temperature and strain on the structure and the properties of corrosionresistant austenitic-martensitic 14Kh15AN4M steel is studied. The steel is shown to exhibit high ductility: upon rolling in the temperature range 700-1100°C at a reduction per pass up to 80%, wedge steel specimens are uniformly deformed along and across the rolling direction without cracking and other surface defects. Subsequent cold treatment and low-temperature tempering ensure a high hardness of the steel (50-56 HRC). Austenite mainly contributes to the hardening upon rolling in the temperature range 700-800°C at a reduction of 50-70%, and martensite makes the main contribution at higher temperatures and lower strains. Texture does not form under the chosen deformation conditions, which indicates dynamic recrystallization with the nucleation and growth of grains having no preferential orientation.
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NASA Astrophysics Data System (ADS)
Bellavoine, Marion; Dumont, Myriam; Drillet, Josée; Hébert, Véronique; Maugis, Philippe
2018-05-01
Adjusting ferrite recrystallization kinetics during annealing is a way to control the final microstructure and thus the mechanical properties of advanced cold-rolled high-strength steels. Two strategies are commonly used for this purpose: adjusting heating rates and/or adding microalloying elements. The present work investigates the effect of heating rate and microalloying elements Ti, Nb, and Mo on recrystallization kinetics during annealing in various cold-rolled Dual-Phase steel grades. The use of combined experimental and modeling approaches allows a deeper understanding of the separate influence of heating rate and the addition of microalloying elements. The comparative effect of Ti, Nb, and Mo as solute elements and as precipitates on ferrite recrystallization is also clarified. It is shown that solute drag has the largest delaying effect on recrystallization in the present case and that the order of solute drag effectiveness of microalloying elements is Nb > Mo > Ti.
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NASA Astrophysics Data System (ADS)
Bellavoine, Marion; Dumont, Myriam; Drillet, Josée; Hébert, Véronique; Maugis, Philippe
2018-07-01
Adjusting ferrite recrystallization kinetics during annealing is a way to control the final microstructure and thus the mechanical properties of advanced cold-rolled high-strength steels. Two strategies are commonly used for this purpose: adjusting heating rates and/or adding microalloying elements. The present work investigates the effect of heating rate and microalloying elements Ti, Nb, and Mo on recrystallization kinetics during annealing in various cold-rolled Dual-Phase steel grades. The use of combined experimental and modeling approaches allows a deeper understanding of the separate influence of heating rate and the addition of microalloying elements. The comparative effect of Ti, Nb, and Mo as solute elements and as precipitates on ferrite recrystallization is also clarified. It is shown that solute drag has the largest delaying effect on recrystallization in the present case and that the order of solute drag effectiveness of microalloying elements is Nb > Mo > Ti.
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The response of the Seasat and Magsat infrared horizon scanners to cold clouds
NASA Technical Reports Server (NTRS)
Bilanow, S.; Phenneger, M.
1980-01-01
Cold clouds over the Earth are shown to be the principal cause of pitch and roll measurement noise in flight data from the infrared horizon scanners onboard Seasat and Magsat. The observed effects of clouds on the fixed threshold horizon detection logic of the Magsat scanner and on the variable threshold detection logic of the Seasat scanner are discussed. National Oceanic and Atmospheric Administration (NOAA) Earth photographs marked with the scanner ground trace clearly confirm the relationship between measurement errors and Earth clouds. A one to one correspondence can be seen between excursion in the pitch and roll data and cloud crossings. The characteristics of the cloud-induced noise are discussed, and the response of the satellite control systems to the cloud errors is described. Changes to the horizon scanner designs that would reduce the effects of clouds are noted.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Li, Li; Ungár, Tamás; Toth, Laszlo S.
The evolution of texture, grain size, grain shape, dislocation and twin density has been determined by synchrotron X-ray diffraction and line profile analysis in a nanocrystalline Ni- Fe alloy after cold rolling along different directions related to the initial fiber and the long axis of grains. The texture evolution has been simulated by the Taylor-type relaxed constraints viscoplastic polycrystal model. The simulations were based on the activity of partial dislocations in correlation with the experimental results of dislocation density determination. The concept of stress-induced shear-coupling is supported and strengthened by both the texture simulations and the experimentally determined evolution ofmore » the microstructure parameters. Grain-growth and texture evolution are shown to proceed by the shear-coupling mechanism supported by dislocation activity as long as the grain size is not smaller than about 20 nm.« less
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NASA Astrophysics Data System (ADS)
Zaba, K.; Dul, I.; Puchlerska, S.
2017-02-01
Superalloys based on nickel and selected steels are widely used in the aerospace industry, because of their excellent mechanical properties, heat resistance and creep resistance. Metal sheets of these materials are plastically deformed and applied, inter alia, to critical components of aircraft engines. Due to their chemical composition these materials are hardly deformable. There are various methods to improve the formability of these materials, including plastic deformation at an elevated or high temperature, or a suitable heat treatment before forming process. The paper presents results of the metal sheets testing after heat treatment. For the research, sheets of two types of nickel superalloys type Inconel and of three types of steel were chosen. The materials were subjected to multivariate heat treatment at different temperature range and time. After this step, mechanical properties were examined according to the metal sheet rolling direction. The results were compared and the optimal type of pre-trial softening heat treatment for each of the materials was determined.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Dai, Qiang; Kelly, Jarod C.; Burnham, Andrew
This report serves as an update for the life-cycle analysis (LCA) of aluminum production based on the most recent data representing the state-of-the-art of the industry in North America. The 2013 Aluminum Association (AA) LCA report on the environmental footprint of semifinished aluminum products in North America provides the basis for the update (The Aluminum Association, 2013). The scope of this study covers primary aluminum production, secondary aluminum production, as well as aluminum semi-fabrication processes including hot rolling, cold rolling, extrusion and shape casting. This report focuses on energy consumptions, material inputs and criteria air pollutant emissions for each processmore » from the cradle-to-gate of aluminum, which starts from bauxite extraction, and ends with manufacturing of semi-fabricated aluminum products. The life-cycle inventory (LCI) tables compiled are to be incorporated into the vehicle cycle model of Argonne National Laboratory’s Greenhouse Gases, Regulated Emissions, and Energy Use in Transportation (GREET) Model for the release of its 2015 version.« less
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NASA Astrophysics Data System (ADS)
Motoshima, Hiroaki; Hirosawa, Shoichi; Lee, Seungwon; Horita, Zenji; Matsuda, Kenji; Terada, Daisuke
The age-hardening behavior and precipitation microstructures with high dislocation density and ultrafine grains have been studied for cold-rolled and severely deformed 2091 Al-Li-Cu alloy. The age-hardenability at 463K was reduced by high-pressure torsion (HPT) due to the accelerated formation of larger 8-AlLi precipitates at grain boundaries, in place of transgranular precipitation of refined δ'-Al3Li particles that are predominantly observable in the no-deformed and 10%-rolled specimens. When aged at 373K, however, it was successfully achieved for the HPT specimen to increase the hardness up to 290HV, the highest level of hardness among conventional wrought aluminum alloys. The corresponding TEM microstructures confirmed that refined δ' particles precipitate within ultrafine grains while keeping the grain size at 206nm. This result suggests that the combined processing of severe plastic deformation with age-hardening technique enables the fabrication of novel aluminum alloys concurrently strengthened by ultrafine-grained and precipitation hardenings.
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Study of soft magnetic iron cobalt based alloys processed by powder injection molding
NASA Astrophysics Data System (ADS)
Silva, Aline; Lozano, Jaime A.; Machado, Ricardo; Escobar, Jairo A.; Wendhausen, Paulo A. P.
As a near net shape process, powder injection molding (PIM) opens new possibilities to process Fe-Co alloys for magnetic applications. Due to the fact that PIM does not involve plastic deformation of the material during processing, we envisioned the possibility of eliminating vanadium (V), which is generally added to Fe-Co alloys to improve the ductility in order to enable its further shaping by conventional processes such as forging and cold rolling. In our investigation we have found out two main futures related to the elimination of V, which lead to a cost-benefit gain in manufacturing small magnetic components where high-saturation induction is needed at low frequencies. Firstly, the elimination of V enables the achievement of much better magnetic properties when alloys are processed by PIM. Secondly, a lower sintering temperature can be used when the alloy is processed starting with elemental Fe and Co powders without the addition of V.
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NASA Astrophysics Data System (ADS)
Ragkousis, A.; Bakare, F.; Babalola, M. I.
2017-11-01
This study presents the effects of a novel thermomechanical treatment on the mechanical properties of the AA2139 aerospace aluminium alloys. The novel treatment, which is comprised of a combination of under-aging, cold-rolling, and re-aging, was successfully employed by Wang et al (2014 Mater. Sci. Eng. A 607 313-7) to enhance the mechanical and microstructure properties of 6000 series aluminium alloys. The influence of under-ageing and re-aging parameters of the treatment on the AA2139 properties has been examined by tensile and hardness testing, differential scanning calorimetry, and thermoelectric power measurements. It was determined that a higher temperature under-ageing, combined with lower temperature and long duration re-ageing resulted in the most attractive mechanical properties, which significantly exceeded those of other traditional treatments. More specifically, a 175 °C/1.5 h under-ageing treatment, followed by a cold rolling reduction of 75% and a 110 °C/96 h re-ageing resulted in a yield strength of 554 MPa, an ultimate tensile strength of 618 MPa, and an elongation of 7.5%, far exceeding the strength requirements and 5% acceptable elongation for applications in the aerospace industry. These results, in conjunction with the results of the parallel study focusing on the effects of the cold-rolling component of the treatment (Bakare et al 2017 Mater. Res. Express 4) further reinforce the position that the treatment employed is superior to conventional ones for the 2139 alloy.
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Improving cold chain systems: Challenges and solutions.
Ashok, Ashvin; Brison, Michael; LeTallec, Yann
2017-04-19
While a number of new vaccines have been rolled out across the developing world (with more vaccines in the pipeline), cold chain systems are struggling to efficiently support national immunization programs in ensuring the availability of safe and potent vaccines. This article reflects on the Clinton Health Access Initiative, Inc. (CHAI) experience working since 2010 with national immunization programs and partners to improve vaccines cold chains in 10 countries-Ethiopia, Nigeria, Kenya, Malawi, Tanzania, Uganda, Cameroon, Mozambique, Lesotho and India - to identify the root causes and solutions for three common issues limiting cold chain performance. Key recommendations include: Collectively, the solutions detailed in this article chart a path to substantially improving the performance of the cold chain. Combined with an enabling global and in-country environment, it is possible to eliminate cold chain issues as a substantial barrier to effective and full immunization coverage over the next few years. Copyright © 2017. Published by Elsevier Ltd.
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NASA Technical Reports Server (NTRS)
Uz, Mehmet; Titran, R. H.
1993-01-01
High temperature stability of the microstructure of Nb-1Zr sheet containing 0.1 and 0.06 wt. percent C was studied as affected by processing and prolonged 1350 K exposure with and without applied stress. Sheets were fabricated by cold rolling bars that were single-, double-, or triple-extruded at 1900 K. Creep samples were double-annealed (1 h at 1755 K + 2 h at 1475 K) prior to testing at 1350 K and 10,000 - 34,500 h. The microstructures of the as-cast, extruded, rolled, DA, and crept samples were characterized using various metallographic and analytical methods. The precipitates were rather coarse Nb2C initially, but transformed to finer (less than or equal to 1 micron) carbides of (Zr, Nb)C with each subsequent high temperature process. The grain size, and the relative amount and morphology of (Zr, Nb)C were found to be affected by the number of extrusions and to some extent by C-content. However, the microstructures of all the crept samples were similar with (Zr, Nb)C distributed throughout the matrix indicating that prolonged exposure to 1350 K gave rise to complete transformation of Nb2C to (Zr, Nb)C regardless of the processing history. These and other observations are presented with the emphasis on the correlation between processing, microstructure, and creep properties.
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NASA Astrophysics Data System (ADS)
Sagapuram, Dinakar
Application of lightweight Mg sheet is limited by its low workability, both in production of sheet (typically by multistep hot and cold-rolling) and forming of sheet into components. Large strain extrusion machining (LSEM), a constrained chip formation process, is used to create Mg alloy AZ31B sheet in a single deformation step. The deformation in LSEM is shown to be intense simple shear that is confined to a narrow zone, which results in significant deformation-induced heating up to ~ 200°C and reduces the need for pre-heating to realize continuous sheet forms. This study focuses on the texture and microstructure development in the sheet processed by LSEM. Interestingly, deep, highly twinned steady-state layer develops in the workpiece subsurface due to the compressive field ahead of the shear zone. The shear deformation, in conjunction with this pre-deformed twinned layer, results in tilted-basal textures in the sheet with basal planes tilted well away from the surface. These textures are significantly different from those in rolled sheet, where basal planes are nearly parallel to the surface. By controlling the strain path, the basal plane inclination from the surface could be varied in the range of 32-53°. B-fiber (basal plane parallel to LSEM shear plane), associated with basal slip, is the major texture component in the sheet. An additional minor C2-fiber component appears above 250°C due to the thermal activation of pyramidal slip. Together with these textures, microstructure ranges from severely cold-worked to (dynamically) recrystallized type, with the corresponding grain sizes varying from ultrafine- (~ 200 nm) to fine- (2 mum) grained. Small-scale limiting dome height (LDH) confirmed enhanced formability (~ 50% increase in LDH) of LSEM sheet over the conventional rolled sheet. Premature, twinning-driven shear fractures are observed in the rolled sheet with the basal texture. In contrast, LSEM sheet with a tilted-basal texture favorably oriented for basal slip exhibits ductile tensile-type fracture. A two-fold increase in ductility is also observed for the LSEM sheet under uniaxial tensile testing without significant changes in the strength. Among texture and microstructure (grain size), texture is shown to be more critical for Mg sheet formability. However, in conjunction with a favorable texture, fine recrystallized microstructure provides for additional enhancement of strain-hardening capacity and formability. In-situ imaging of material flow during uniaxial tensile testing revealed new, interesting flow localization phenomena and fracture behavior. It is shown that the deformation behavior of Mg sheet is highly texture dependent, and also radically different from that of conventional ductile metals both in terms of necking and fracture. The implications of these observations for the LDH test results and formability of Mg sheet, in general, are briefly discussed.
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High dislocation density-induced large ductility in deformed and partitioned steels
NASA Astrophysics Data System (ADS)
He, B. B.; Hu, B.; Yen, H. W.; Cheng, G. J.; Wang, Z. K.; Luo, H. W.; Huang, M. X.
2017-09-01
A wide variety of industrial applications require materials with high strength and ductility. Unfortunately, the strategies for increasing material strength, such as processing to create line defects (dislocations), tend to decrease ductility. We developed a strategy to circumvent this in inexpensive, medium manganese steel. Cold rolling followed by low-temperature tempering developed steel with metastable austenite grains embedded in a highly dislocated martensite matrix. This deformed and partitioned (D and P) process produced dislocation hardening but retained high ductility, both through the glide of intensive mobile dislocations and by allowing us to control martensitic transformation. The D and P strategy should apply to any other alloy with deformation-induced martensitic transformation and provides a pathway for the development of high-strength, high-ductility materials.
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NASA Astrophysics Data System (ADS)
Wang, Xiao-feng; Guo, Ming-xing; Cao, Ling-yong; Wang, Fei; Zhang, Ji-shan; Zhuang, Lin-zhong
2015-07-01
The effect of rolling geometry on mechanical properties, microstructure, and recrystallization texture of Al-Mg-Si alloys was studied by means of tensile tests, microstructural observations, and electron backscatter diffraction measurements. The results reveal that the elongation and the average plasticity strain ratio ( r) values of the T4P (pre-aging plus natural aging)-treated alloy sheet with a rolling geometry value between 1 and 3 are somewhat higher than those of the T4P-treated sheet with a rolling geometry value between 3 and 6. The deformation and recrystallization microstructures of the sheet with a rolling geometry value between 1 and 3 are more uniform than those of the sheet with a rolling geometry value between 3 and 6. The former also possesses somewhat higher surface quality. H {001}<110> and Goss {110}<001> orientations are the main recrystallization texture components for the former case, whereas the latter case only includes H{001}<110> orientation. Texture gradients are present in the two alloy sheets. Shear texture component F on the surface of the sheet with a rolling geometry value between 3 and 6 and its higher texture gradients have revealed that non-uniform deformation occurred during cold rolling. The effects of texture on the yield strength and r value were also discussed.
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Self-rolling up micro 3D structures using temperature-responsive hydrogel sheet
NASA Astrophysics Data System (ADS)
Iwata, Y.; Miyashita, S.; Iwase, E.
2017-12-01
This paper proposes a micro self-folding using a self-rolling up deformation. In the fabrication method at micro scale, self-folding is an especially useful method of easily fabricating complex three-dimensional (3D) structures from engineered two-dimensional (2D) sheets. However, most self-folded structures are limited to 3D structures with a hollow region. Therefore, we made 3D structures with a small hollow region by self-rolling up a 2D sheet consisting of SU-8 and a temperature-responsive hybrid hydrogel of poly(N-isopropylacrylamide-co-acrylic acid) (pNIPAM-AAc). The temperature-responsive hydrogel can provide repetitive deformation, which is a good feature for micro soft robots or actuators, using hydrogel shrinking and swelling. Our micro self-rolling up method is a self-folding method for a 3D structure performed by rolling up a 2D flat sheet, like making a croissant, through continuous self-folding. We used our method to fabricate 3D structures with a small hollow region, such as cylindrical, conical, and croissant-like ellipsoidal structures, and 3D structures with a hollow region, such as spiral shapes. All the structures showed repetitive deformation, forward rolling up in 20 °C cold water and backward rolling up in 40 °C hot water. The results demonstrate that self-rolling up deformation can be useful in the field of micro soft devices.
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Crack growth testing on Cold Worked Alloy 690 in Primary Water Environment
NASA Astrophysics Data System (ADS)
Tice, David R.; Medway, Stuart L.; Platts, Norman; Stairmand, John W.
While plant experience so far has shown excellent resistance of Alloy 690 to stress corrosion cracking in PWR primary water environments, laboratory tests have reported that susceptibility may be enhanced substantially by non-uniform cold working, particularly when the plane of crack growth is in the plane of rolling or forging. The Alloy 690 program aims to further the understanding of the mechanisms behind this susceptibility and the heat-to-heat variability reported for different materials.
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NASA Astrophysics Data System (ADS)
Melnikov, Eugene; Astafurova, Elena; Maier, Galina; Moskvina, Valentina
2017-12-01
The influence of multi-pass cold rolling on the phase composition and microhardness of austenitic Fe-18Cr-9Ni-0.21C, Fe-18Cr-9Ni-0.5Ti-0.08C, Fe-17Cr-13Ni-3Mo-0.01C (in wt %) steels with different stacking fault energies was studied. The metastable Fe-18Cr-9Ni-0.5Ti-0.08C steel undergoes γ → α' phase transformations during rolling, the volume fraction of strain-induced α'-martensite in steel structure is increased with increasing strain. Metastable austenite Fe-18Cr-9Ni-0.21C steel does not undergo the formation of an appreciable amount of strain-induced α'-martensite under rolling, but the magnetophase analysis reveals a small amount of ferrite phase in the structure of steel after rolling. The structure of stable Fe-17Cr-13Ni-3Mo-0.01C steel remains austenitic independently under strain. Investigations of microhardness of the steels show that their values are increased with strain and are dependent on propensity of steels to strain-induced martensitic transformation.
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NASA Astrophysics Data System (ADS)
Kumar, Amit; Khatirkar, Rajesh Kisni; Gupta, Aman; Shekhawat, Satish K.; Suwas, Satyam
2018-06-01
In the present work, the influence of strain path on the evolution of microstructure, crystallographic texture, and magnetic properties of a two-phase Fe-Cr-Ni alloy was investigated. The Fe-Cr-Ni alloy had nearly equal proportion of austenite and ferrite and was cold rolled up to a true strain of 1.6 (thickness reduction) using two different strain paths—unidirectional rolling and multi-step cross rolling. The microstructures were characterized by scanning electron microscopy (SEM) and electron backscattered diffraction (EBSD), while crystallographic textures were determined using X-ray diffraction. For magnetic characterization, B-H loops and M-H curves were measured and magnetic force microscopy was performed. After unidirectional rolling, ferrite showed the presence of strong α-fiber (rolling direction, RD//<110>) and austenite showed strong brass type texture (consisting of Brass (Bs) ({110}<112>), Goss ({110}<001>), and S ({123}<634>)). After multi-step cross rolling, strong rotated cube ({100}<110>) was developed in ferrite, while austenite showed ND (normal direction) rotated brass ( 10 deg) texture. The strain-induced martensite (SIM) was found to be higher in unidirectionally rolled samples than multi-step cross-rolled samples. The coherently diffracting domain size, micro-strain, coercivity, and core loss also showed a strong correlation with strain and strain path. More strain was partitioned into austenite than ferrite during deformation (unidirectional as well as cross rolling). Further, the strain partitioning (in both austenite and ferrite) was found to be higher in unidirectionally rolled samples.
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Application of RNAMlet to surface defect identification of steels
NASA Astrophysics Data System (ADS)
Xu, Ke; Xu, Yang; Zhou, Peng; Wang, Lei
2018-06-01
As three main production lines of steels, continuous casting slabs, hot rolled steel plates and cold rolled steel strips have different surface appearances and are produced at different speeds of their production lines. Therefore, the algorithms for the surface defect identifications of the three steel products have different requirements for real-time and anti-interference. The existing algorithms cannot be adaptively applied to surface defect identification of the three steel products. A new method of adaptive multi-scale geometric analysis named RNAMlet was proposed. The idea of RNAMlet came from the non-symmetry anti-packing pattern representation model (NAM). The image is decomposed into a set of rectangular blocks asymmetrically according to gray value changes of image pixels. Then two-dimensional Haar wavelet transform is applied to all blocks. If the image background is complex, the number of blocks is large, and more details of the image are utilized. If the image background is simple, the number of blocks is small, and less computation time is needed. RNAMlet was tested with image samples of the three steel products, and compared with three classical methods of multi-scale geometric analysis, including Contourlet, Shearlet and Tetrolet. For the image samples with complicated backgrounds, such as continuous casting slabs and hot rolled steel plates, the defect identification rate obtained by RNAMlet was 1% higher than other three methods. For the image samples with simple backgrounds, such as cold rolled steel strips, the computation time of RNAMlet was one-tenth of the other three MGA methods, while the defect identification rates obtained by RNAMlet were higher than the other three methods.
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Experiment Research on Hot-Rolling Processing of Nonsmooth Pit Surface.
Gu, Yun-Qing; Fan, Tian-Xing; Mou, Jie-Gang; Yu, Wei-Bo; Zhao, Gang; Wang, Evan
2016-01-01
In order to achieve the nonsmooth surface drag reduction structure on the inner polymer coating of oil and gas pipelines and improve the efficiency of pipeline transport, a structural model of the machining robot on the pipe inner coating is established. Based on machining robot, an experimental technique is applied to research embossing and coating problems of rolling-head, and then the molding process rules under different conditions of rolling temperatures speeds and depth are analyzed. Also, an orthogonal experiment analysis method is employed to analyze the different effects of hot-rolling process apparatus on the embossed pits morphology and quality of rolling. The results also reveal that elevating the rolling temperature or decreasing the rolling speed can also improve the pit structure replication rates of the polymer coating surface, and the rolling feed has little effect on replication rates. After the rolling-head separates from the polymer coating, phenomenon of rebounding and refluxing of the polymer coating occurs, which is the reason of inability of the process. A continuous hot-rolling method for processing is used in the robot and the hot-rolling process of the processing apparatus is put in a dynamics analysis.
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Experiment Research on Hot-Rolling Processing of Nonsmooth Pit Surface
Gu, Yun-qing; Fan, Tian-xing; Mou, Jie-gang; Yu, Wei-bo; Zhao, Gang; Wang, Evan
2016-01-01
In order to achieve the nonsmooth surface drag reduction structure on the inner polymer coating of oil and gas pipelines and improve the efficiency of pipeline transport, a structural model of the machining robot on the pipe inner coating is established. Based on machining robot, an experimental technique is applied to research embossing and coating problems of rolling-head, and then the molding process rules under different conditions of rolling temperatures speeds and depth are analyzed. Also, an orthogonal experiment analysis method is employed to analyze the different effects of hot-rolling process apparatus on the embossed pits morphology and quality of rolling. The results also reveal that elevating the rolling temperature or decreasing the rolling speed can also improve the pit structure replication rates of the polymer coating surface, and the rolling feed has little effect on replication rates. After the rolling-head separates from the polymer coating, phenomenon of rebounding and refluxing of the polymer coating occurs, which is the reason of inability of the process. A continuous hot-rolling method for processing is used in the robot and the hot-rolling process of the processing apparatus is put in a dynamics analysis. PMID:27022235
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Intermixing in Cu/Ni multilayers induced by cold rolling
DOE Office of Scientific and Technical Information (OSTI.GOV)
Wang, Z.; Perepezko, J. H., E-mail: perepezk@engr.wisc.edu; Larson, D.
2015-04-28
Repeated cold rolling was performed on multilayers of Cu60/Ni40 and Cu40/Ni60 foil arrays to study the details of driven atomic scale interfacial mixing. With increasing deformation, there is a significant layer refinement down to the nm level that leads to the formation of a solid solution phase from the elemental end members. Intriguingly, the composition of the solid solution is revealed by an oscillation in the composition profile across the multilayers, which is different from the smoothly varying profile due to thermally activated diffusion. During the reaction, Cu mixed into Ni preferentially compared to Ni mixing into Cu, which ismore » also in contrast to the thermal diffusion behavior. This is confirmed by observations from X-ray diffraction, electron energy loss spectrum and atom probe tomography. The diffusion coefficient induced by cold rolling is estimated as 1.7 × 10{sup −17} m{sup 2}/s, which cannot be attributed to any thermal effect. The effective temperature due to the deformation induced mixing is estimated as 1093 K and an intrinsic diffusivity d{sub b}, which quantifies the tendency towards equilibrium in the absence of thermal diffusion, is estimated as 6.38 × 10{sup −18} m{sup 2}/s. The fraction of the solid solution phase formed is illustrated by examining the layer thickness distribution and is described by using an error function representation. The evolution of mixing in the solid solution phase is described by a simplified sinusoid model, in which the amplitude decays with increased deformation level. The promoted diffusion coefficient could be related to the effective temperature concept, but the establishment of an oscillation in the composition profile is a characteristic behavior that develops due to deformation.« less
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Jiang, Daqiang, E-mail: dq80jiang@126.com; Cui, Lishan; Jiang, Jiang
Graphical abstract: - Highlights: • In situ NiTi/Nb(Ti) composites were fabricated. • The transformation temperature was affected by the mixing Ti:Ni atomic ratios. • The NiTi component became micron-scale lamella after forging and rolling. • The composite exhibited high strength and high damping capacity. - Abstract: This paper reports on the creation of a series of in situ NiTi/Nb(Ti) composites with controllable transformation temperatures based on the pseudo-binary hypereutectic transformation of NiTi–Nb system. The composite constituent morphology was controlled by forging and rolling. It is found that the thickness of the NiTi lamella in the composite reached micron level aftermore » the hot-forging and cold-rolling. The NiTi/Nb(Ti) composite exhibited high damping capacity as well as high yield strength.« less
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Material engineering to fabricate rare earth erbium thin films for exploring nuclear energy sources
NASA Astrophysics Data System (ADS)
Banerjee, A.; Abhilash, S. R.; Umapathy, G. R.; Kabiraj, D.; Ojha, S.; Mandal, S.
2018-04-01
High vacuum evaporation and cold-rolling techniques to fabricate thin films of the rare earth lanthanide-erbium have been discussed in this communication. Cold rolling has been used for the first time to successfully fabricate films of enriched and highly expensive erbium metal with areal density in the range of 0.5-1.0 mg/cm2. The fabricated films were used as target materials in an advanced nuclear physics experiment. The experiment was designed to investigate isomeric states in the heavy nuclei mass region for exploring physics related to nuclear energy sources. The films fabricated using different techniques varied in thickness as well as purity. Methods to fabricate films with thickness of the order of 0.9 mg/cm2 were different than those of 0.4 mg/cm2 areal density. All the thin films were characterized using multiple advanced techniques to accurately ascertain levels of contamination as well as to determine their exact surface density. Detailed fabrication methods as well as characterization techniques have been discussed.
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NASA Astrophysics Data System (ADS)
Khalique, Abdul; Khan, Mohammad Riaz
1997-07-01
The present scientific and technological advancement in space travel has given an added impetus to the development and production of light metal high strength alloys, capable of enduring rapid changes in temperature and other environmental conditions. Al-3.3 Mg-1.22 Mn (weight %) cold rolled alloy sheet of 2 mm thickness was selected for the study. This alloy falls in the category of non-heat treatable, corrosive resistant alloys. The change in mechanical behaviour when age-softened in N2 gas atomsphere was studied. In addition, mechanical properties of samples when artificially aged in the temperature range of 150°C-250°C for 3 hours each, after solution treatment at 450°C for 12 h followed by quenching to room temperature were investigated. It is revealed that improvement, though limited, in tensile strength, surface hardness and ductility during aging is a function of cooling rate during quenching.
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Characterization of a cold-rolled 2101 lean duplex stainless steel.
Bassani, Paola; Breda, Marco; Brunelli, Katya; Mészáros, Istvan; Passaretti, Francesca; Zanellato, Michela; Calliari, Irene
2013-08-01
Duplex stainless steels (DSS) may be defined as a category of steels with a two-phase ferritic-austenitic microstructure, which combines good mechanical and corrosion properties. However, these steels can undergo significant microstructural modification as a consequence of either thermo-mechanical treatments (ferrite decomposition, which causes σ- and χ-phase formation and nitride precipitation) or plastic deformation at room temperature [austenite transformation into strain-induced martensite (SIM)]. These secondary phases noticeably affect the properties of DSS, and therefore are of huge industrial interest. In the present work, SIM formation was investigated in a 2101 lean DSS. The material was subjected to cold rolling at various degrees of deformation (from 10 to 80% thickness reduction) and the microstructure developed after plastic deformation was investigated by electron backscattered diffraction, X-ray diffraction measurements, and hardness and magnetic tests. It was observed that SIM formed as a consequence of deformations higher than ~20% and residual austenite was still observed at 80% of thickness reduction. Furthermore, a direct relationship was found between microstructure and magnetic properties.
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Multiphysical FE-analysis of a front-end bending phenomenon in a hot strip mill
NASA Astrophysics Data System (ADS)
Ilmola, Joonas; Seppälä, Oskari; Leinonen, Olli; Pohjonen, Aarne; Larkiola, Jari; Jokisaari, Juha; Putaansuu, Eero
2018-05-01
In hot steel rolling processes, a slab is generally rolled to a transfer bar in a roughing process and to a strip in a hot strip rolling process. Over several rolling passes the front-end may bend upward or downward due to asymmetrical rolling conditions causing entry problems in the next rolling pass. Many different factors may affect the front-end bending phenomenon and are very challenging to measure. Thus, a customized finite element model is designed and built to simulate the front-end bending phenomenon in a hot strip rolling process. To simulate the functioning of the hot strip mill precisely, automated controlling logic of the mill must be considered. In this paper we studied the effect of roll bite friction conditions and amount of reduction on the front-end bending phenomenon in a hot strip rolling process.
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NASA Astrophysics Data System (ADS)
Moore, Kent; Renfrew, Ian; Bromwich, David; Wilson, Aaron; Vage, Kjetil; Bai, Lesheng
2017-04-01
Open ocean convection, where a loss of surface buoyancy leads to an overturning of the water column, occurs in four distinct regions of the North Atlantic and is an integral component of the Atlantic Meridional Overturning Circulation (AMOC). The overturning typically occurs during cold air outbreaks characterized by large surface turbulent heat fluxes and convective roll cloud development. Here we compare the statistics of the air-sea interaction over these convection sites as represented in three reanalyses with horizontal grid sizes ranging from 80km to 15km. We show that increasing the resolution increases the magnitude and frequency of the most extreme total turbulent heat fluxes, as well as displacing the maxima downstream away from the ice edges. We argue that these changes are a result of the higher resolution reanalysis being better able to represent mesoscale processes that occur within the atmospheric boundary layer during cold air outbreaks.
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AISI/DOE Technology Roadmap Program: Cold Work Embrittlement of Interstitial Free Steel
DOE Office of Scientific and Technical Information (OSTI.GOV)
John T Bowker; Pierre Martin
2002-10-31
This work addresses the issues of measurement of secondary cold work embrittlement (SCWE) of an IF steel in deep-drawn parts using laboratory tests, and its correlation with real part fracture. It aimed at evaluating the influence of the steel chemistry and processing condition, microstructure, and test conditions, on SCWE as well as the effect of SCWE on fatigue properties. Size 6-in. cups produced with various draw ratios or trimmed at different heights were tested to determine the ductile-to-brittle-transition temperature (DBTT) as a function of strain. The 2-in. cup/expansion test, bend test and fracture of notched specimens were also used tomore » generate information complementary to that provided by the 6-inch cup/expansion test. The relationship between laboratory tests and fracture in real parts was established by testing large-scale parts. The fatigue behavior was investigated in the as-rolled and deep drawn (high stain) conditions, using prestrained specimens taken from the wall of a formed part.« less
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Reasonable Temperature Schedules for Cold or Hot Charging of Continuously Cast Steel Slabs
NASA Astrophysics Data System (ADS)
Li, Yang; Chen, Xin; Liu, Ke; Wang, Jing; Wen, Jin; Zhang, Jiaquan
2013-12-01
Some continuously cast steel slabs are sensitive to transverse fracture problems during transportation or handling away from their storage state, while some steel slabs are sensitive to surface transverse cracks during the following rolling process in a certain hot charging temperature range. It is revealed that the investigated steel slabs with high fracture tendency under room cooling condition always contain pearlite transformation delayed elements, which lead to the internal brittle bainitic structure formation, while some microalloyed steels exhibit high surface crack susceptibility to hot charging temperatures due to carbonitride precipitation. According to the calculated internal cooling rates and CCT diagrams, the slabs with high fracture tendency during cold charging should be slowly cooled after cutting to length from hot strand or charged to the reheating furnace directly above their bainite formation temperatures. Based on a thermodynamic calculation for carbonitride precipitation in austenite, the sensitive hot charging temperature range of related steels was revealed for the determination of reasonable temperature schedules.
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NASA Astrophysics Data System (ADS)
Liang, Y. L.; Wang, Z. B.; Zhang, J.; Zhang, J. B.; Lu, K.
2016-11-01
By means of surface mechanical attrition treatment (SMAT), a gradient nanostructured surface layer was fabricated on a hot-rolled interstitial-free steel plate. A Zn-Al coating was subsequently deposited on the SMAT sample by using cold spray process. The bonding property of the coating on the SMAT substrate was compared with that on the coarse-grained (CG) sample. Stud-pull tests showed that the bonding strength in the as-sprayed SMAT sample is ∼30% higher than that in the as-sprayed CG sample. No further improvement in bonding strength was achieved in the coated SMAT sample after annealing at 400 °C, mostly due to the formation of cracks and intermetallic compounds at the coating/substrate interface in an earlier stage (<30 min) and in a final stage (>90 min), respectively. The enhanced bonding property of the Zn-Al coating on the SMAT sample might be related with the promoted atomic diffusion and hardness in the nanostructured surface layer.
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NASA Astrophysics Data System (ADS)
Muojekwu, Cornelius Anaedu
The present research was directed at adequate prediction of the temperature, deformation behavior (roll force, flow stress, strain and strain rate) and microstructural evolution (recovery, recrystallization, grain growth, austenite and ferrite grain sizes) during rolling in the Compact Strip Production (CSP) process, as well as the final mechanical properties of the hot rolled strips. This was accomplished with the aid of integrated process modeling, involving mathematical simulation, laboratory experiments and industrial campaigns. The study covered two conventional plain carbon steel grades, the A36 (AISI 1018, 0.17C-0.74Mn) and DQSK (AISI 1005, 0.038C-0.3Mn), and a range of plain carbon steel grades (0.06-0.09 C, 0.16-0.9 Mn) produced at HYLSA's CSP mill at Monterrey, Mexico. In the laboratory, compression tests (both single and double-hits) were carried out on the Gleeble 1500 thermomechanical simulator in order to elucidate the effect of coarse austenite grain size on the flow stress and recrystallization behavior of the plain carbon steels. It was found that coarse grain size not only decreased the flow stress at a given strain but also substantially reduced the tendency toward dynamic recrystallization. An increase in grain size from 244 to 1110 mum which is typical of the first stands of a conventional finishing mill and CSP hot-strip mill respectively, resulted in up to a 30 MPa decrease in the flow stress of both A36 and DQSK steel grades at similar operating conditions of temperature, strain and strain rate. In order to validate the model and laboratory results with mill measurements from an operating CSP plant, an industrial trial was carried out at HYLSA's CSP mill in Monterrey, Mexico. During the industrial campaign, intermediate temperature measurements were made, CSP slab and coil samples were acquired, and all measured and recorded mill data and practices were obtained. Comprehensive mathematical modeling of the rolling process was carried out employing finite difference and finite element analysis. The CSP mill measurements were utilized to validate model predictions of temperature, roll force, grain size and mechanical properties. Good agreement was obtained between prediction and measurement in most of the cases. An estimate of the heat extraction from the various mill sub-units was conducted from the validated calculations. It was found that heat loss by radiation accounted for 48-51 percent of the total heat loss, the work rolls accounted for 41-44 percent, the descaling unit accounted for 4-6 percent and the interstand sprays accounted for the remaining 3-4 percent. It was found that the uniform strain model consistently predicts lower temperatures than the target exit temperature for thin gauges due to a low estimate of deformation heat. Model results captured the details of heat transfer, deformation, recrystallization and austenite decomposition in the CSP mill. The effect of various mill parameters were elucidated, and the similarities and differences between conventional cold-charge rolling and CSP rolling were highlighted. (Abstract shortened by UMI.)
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Sheremetyev, V; Brailovski, V; Prokoshkin, S; Inaekyan, K; Dubinskiy, S
2016-01-01
Ti-22Nb-6Zr (at.%) alloy with different processing-induced microstructures (highly-dislocated partially recovered substructure, polygonized nanosubgrained (NSS) dislocation substructure, and recrystallized structure) was subjected to strain-controlled tension-tension fatigue testing in the 0.2...1.5% strain range (run-out at 10^6 cycles). The NSS alloy obtained after cold-rolling with 0.3 true strain and post-deformation annealing at 600 °C showed the lowest Young's modulus and globally superior fatigue performance due to the involvement of reversible stress-induced martensitic transformation in the deformation process. This NSS structure appears to be suitable for biomedical applications with an extended variation range of loading conditions (orthopedic implants). Copyright © 2015 Elsevier B.V. All rights reserved.
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Hu, J.; Du, L.-X.; Sun, G.-S.; Xie, H.; Misra, R.D.K.
2015-01-01
We describe here for the first time the low temperature superplasticity of nanostructured low carbon steel (microalloyed with V, N, Mn, Al, Si, and Ni). Low carbon nanograined/ultrafine-grained (NG/UFG) bulk steel was processed using a combination of cold-rolling and annealing of martensite. The complex microstructure of NG/UFG ferrite and 50–80 nm cementite exhibited high thermal stability at 500 °C with low temperature elongation exceeding 100% (at less than 0.5 of the absolute melting point) as compared to the conventional fine-grained (FG) counterpart. The low temperature superplasticity is adequate to form complex components. Moreover, the low strength during hot processing is favorable for decreasing the spring back and minimize die loss. PMID:26687012
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Federal Register 2010, 2011, 2012, 2013, 2014
2013-07-18
... rubber articles, cartons, bags, corrugated boxes with fillers, instruction sheets, range hood filters, bathroom mirrors, filters for whole house ventilation systems, cold- rolled steel for manufacturing, flat..., damper or filter springs for grille, stainless steel kitchen backsplashes, brackets, aluminum stainless...
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Development of nano/sub-micron grain structures in metastable austenitic stainless steels
NASA Astrophysics Data System (ADS)
Rajasekhara, Shreyas
2007-12-01
This dissertation is a part of a collaborative work between the University of Texas, Austin-Texas, the University of Oulu, Oulu-Finland, and Outokumpu Stainless Oy, Tornio-Finland, to develop commercial austenitic stainless steels with high strength and ductility. The idea behind this work involves cold-rolling a commercial metastable austenitic stainless steel - AISI 301LN stainless steel to produce strain-induced martensite, followed by an annealing treatment to generate nano/sub-micron grained austenite. AISI 301LN stainless steel sheets are cold-rolled to 63% reduction and subsequently annealed at 600°C, 700°C, 800°C, 900°C and 1000°C for 1, 10 and 100 seconds. The samples are analyzed by X-Ray diffraction, SQUID, transmission electron microscopy, and tensile testing to fundamentally understand the microstructural evolution, the mechanism for the martensite → austenite reversion, the formation of nano/sub-micron austenite grains, and the relationship between the microstructure and the strength obtained in this stainless steel. The results show that cold-rolled AISI 301LN stainless steel consist of dislocation-cell martensite, heavily deformed lath-martensite and austenite shear bands. Subsequent annealing at 600°C for short durations of 1 and 10 seconds leads to negligible martensite to austenite reversion. These 600°C samples exhibit a similar microstructure to the cold-rolled sample. However, for samples annealed at 600°C for 100 seconds and those annealed at higher temperatures (700°C, 800°C, 900°C and 1000°C) exhibit equiaxed austenitic grains of sizes 0.2mum-10mum and secondary phase precipitates. The microstructural analysis also reveals that the martensite → austenite reversion occurs via a diffusion-type reversion mechanism. In this regard, a generalized form of Avrami's equation is used to model the kinetics of martensite → austenite phase reversion. The results from the model agree reasonably well with the experiments. Furthermore, the activation energy for grain growth in nano/sub-micron grained AISI 301LN stainless steel is found to be ˜ 205kJ/mol, which is comparable to values observed in coarse grained commercial stainless steels (AISI 304, 316). However, the driving force for grain growth in nano/sub-micron grained AISI 301LN stainless steel is considerably higher when compared to other stainless steels. Finally, the average grain sizes in AISI 301LN stainless steels are related to the mechanical properties obtained, through the Hall-Petch relationship.
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New Forming Technologies for Autobody at POSCO
NASA Astrophysics Data System (ADS)
Lee, Hong-Woo; Cha, Myung-Hwan; Choi, Byung-Keun; Kim, Gyo-Sung; Park, Sung-Ho
2011-08-01
As development of car body with light weight and enhanced safety became one of the hottest issues in the auto industry, the advanced high strength steels have been broadly applied to various automotive parts over the last few years. Corresponding to this trend, POSCO has developed various types of cold and hot rolled AHSSs such as DP, TRIP, CP and FB, and continues to develop new types of steel in order to satisfy the requirement of OEMs more extensively. To provide optimal technical supports to customers, POSCO has developed more advanced EVI concept, which includes the concept of CE/SE, VA/VE, VI and PP as well as the conventional EVI strategy. To realize this concept, POSCO not only supports customers with material data, process guideline, and evaluation of formability, weld-ability, paint-ability and performance but also provides parts or sub-assemblies which demand highly advanced technologies. Especially, to accelerate adoption of AHSS in autobody, POSCO has tried to come up with optimal solutions to AHSS forming. Application of conventional forming technologies has been restricted more and more by relatively low formability of AHSS with high tensile-strength. To overcome the limitation in the forming, POSCO has recently developed new forming technologies such as hydro-forming, hot press forming, roll forming and form forming. In this paper, tailored strength HPF, hydroformed torsion beam axle and multi-directional roll forming are introduced as examples of new forming technologies.
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Hubble Space Telescope solar cell module thermal cycle test
NASA Technical Reports Server (NTRS)
Douglas, Alexander; Edge, Ted; Willowby, Douglas; Gerlach, Lothar
1992-01-01
The Hubble Space Telescope (HST) solar array consists of two identical double roll-out wings designed after the Hughes flexible roll-up solar array (FRUSA) and was developed by the European Space Agency (ESA) to meet specified HST power output requirements at the end of 2 years, with a functional lifetime of 5 years. The requirement that the HST solar array remain functional both mechanically and electrically during its 5-year lifetime meant that the array must withstand 30,000 low Earth orbit (LEO) thermal cycles between approximately +100 and -100 C. In order to evaluate the ability of the array to meet this requirement, an accelerated thermal cycle test in vacuum was conducted at NASA's Marshall Space Flight Center (MSFC), using two 128-cell solar array modules which duplicated the flight HST solar array. Several other tests were performed on the modules. The thermal cycle test was interrupted after 2,577 cycles, and a 'cold-roll' test was performed on one of the modules in order to evaluate the ability of the flight array to survive an emergency deployment during the dark (cold) portion of an orbit. A posttest static shadow test was performed on one of the modules in order to analyze temperature gradients across the module. Finally, current in-flight electrical performance data from the actual HST flight solar array will be tested.
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An approach to develop an algorithm to detect the climbing height in radial-axial ring rolling
NASA Astrophysics Data System (ADS)
Husmann, Simon; Hohmann, Magnus; Kuhlenkötter, Bernd
2017-10-01
Radial-axial ring rolling is the mainly used forming process to produce seamless rings, which are applied in miscellaneous industries like the energy sector, the aerospace technology or in the automotive industry. Due to the simultaneously forming in two opposite rolling gaps and the fact that ring rolling is a mass forming process, different errors could occur during the rolling process. Ring climbing is one of the most occurring process errors leading to a distortion of the ring's cross section and a deformation of the rings geometry. The conventional sensors of a radial-axial rolling machine could not detect this error. Therefore, it is a common strategy to roll a slightly bigger ring, so that random occurring process errors could be reduce afterwards by removing the additional material. The LPS installed an image processing system to the radial rolling gap of their ring rolling machine to enable the recognition and measurement of climbing rings and by this, to reduce the additional material. This paper presents the algorithm which enables the image processing system to detect the error of a climbing ring and ensures comparable reliable results for the measurement of the climbing height of the rings.
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Electrochemically induced annealing of stainless-steel surfaces.
Burstein, G T; Hutchings, I M; Sasaki, K
2000-10-19
Modification of the surface properties of metals without affecting their bulk properties is of technological interest in demanding applications where surface stability and hardness are important. When austenitic stainless steel is heavily plastically deformed by grinding or rolling, a martensitic phase transformation occurs that causes significant changes in the bulk and surface mechanical properties of the alloy. This martensitic phase can also be generated in stainless-steel surfaces by cathodic charging, as a consequence of lattice strain generated by absorbed hydrogen. Heat treatment of the steel to temperatures of several hundred degrees can result in loss of the martensitic structure, but this alters the bulk properties of the alloy. Here we show that martensitic structures in stainless steel can be removed by appropriate electrochemical treatment in aqueous solutions at much lower temperature than conventional annealing treatments. This electrochemically induced annealing process allows the hardness of cold-worked stainless steels to be maintained, while eliminating the brittle martensitic phase from the surface. Using this approach, we are able to anneal the surface and near-surface regions of specimens that contain rolling-induced martensite throughout their bulk, as well as those containing surface martensite induced by grinding. Although the origin of the electrochemical annealing process still needs further clarification, we expect that this treatment will lead to further development in enhancing the surface properties of metals.
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XRD and EBSD analysis of anisotropic microstructure development in cold rolled F138 stainless steel
DOE Office of Scientific and Technical Information (OSTI.GOV)
De Vincentis, N.S., E-mail: devincentis@ifir-conic
The microstructural characteristics of deformation-processed materials highly influence their mechanical properties. For a complete characterization of a microstructure both local and global information must be gathered, which requires the combination of different analysis techniques. X-ray and Electron Backscatter Diffraction were used in the present paper to characterize the deformation induced in a cold rolled F138 austenitic stainless steel sample. The results obtained using laboratory and synchrotron X-ray sources were compared and combined with EBSD quantitative results, allowing the global and local characterization and orientation dependence of the deformation microstructure. A particular behavior was observed in the XRD data corresponding tomore » the planes with < 220 >∥ ND, likely due to a smaller amount of defects accumulated in the crystals with that particular orientation. EBSD was used to separate the scans data into partitions and to calculate misorientation variables and parameters, showing that this behavior can be attributed to a combination of larger grain sizes, lower local boundary misorientations and dislocation densities for crystals having < 220 >∥ ND. Several conclusions, of general validity for the evaluation of microstructure anisotropy, can be extracted from the results. - Highlights: •Combined XRD and EBSD for studying microstructure gave a superb insight on anisotropic accumulation of defects. •W-H and CMWP methods were applied for checking consistency of results. •XRD showed that a smaller accumulation of defects occurred in crystals with < 220 >∥ ND. •High brilliance X-ray beam allowed to study the anisotropy of defect accumulation.« less
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Local laser-strengthening: Customizing the forming behavior of car body steel sheets
NASA Astrophysics Data System (ADS)
Wagner, M.; Jahn, A.; Beyer, E.; Balzani, D.
2018-05-01
Future trends in designing lightweight components especially for automotive applications increasingly require complex and delicate structures with highest possible level of capacity [1]. The manufacturing of metallic car body components is primarily realized by deep or stretch drawing. The forming process of especially cold rolled and large-sized components is typically characterized by inhomogeneous stress and strain distributions. As a result, the avoidance of undesirable deep drawing effects like earing and local necking is among the greatest challenges in forming complex car body structures [2]. Hence, a novel local laser-treatment approach with the objective of customizing the forming behavior of car body steel sheets is currently explored.
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Evaluation of the Susceptibility to SCC Initiation of Alloy 690 in Simulated PWR Primary Water
NASA Astrophysics Data System (ADS)
Tsutsumi, Kazuya; Couvant, Thierry
Alloy 690 has been widely used in fabricating components of LWR plants as an alternative material to Alloy 600 which has exhibited a significant susceptibility to PWSCC. However, some authors have reported that Alloy 690 can suffer a significant susceptibility to SCC crack growth when highly cold worked. While most of the recent studies emphasize SCC propagation phase, EDF and its partners are focusing on the material's resistance to SCC initiation. This paper summarizes the current work carried out at EDF MAI on the SCC initiation. By means of constant elongation rate tests (CERTs) and constant displacement tests, experimental investigation of the susceptibility to PWSCC were performed. No SCC was observed on either an extruded bar or on two plates, even after 24%-1D cold rolling, confirming the superior PWSCC resistance of Alloy 690 independent of a amount of intergranular precipitation of carbides, and also revealing that such cold rolling does not necessarily decrease the resistance to SCC. On the other hand, a experimental steam generator tube that has a degraded microstructure due to specific heat-treatment revealed its susceptibility to SCC, probably because of the interactive effect of microstructure with heavy intragranular carbide precipitations and the cold worked superficial layer. This phenomenon is in good agreement with results previously published. In this study, the maximal crack depth slightly increased when DH increased from 5 to 60 cc.kg-1H2O. No significant prior ageing effect on the crack depth was observed, even when ageing was combined with high DH.
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Effect of Grain Misorientation Angle on Twinning Propagation in Ti-15Mo Alloy
NASA Astrophysics Data System (ADS)
Im, Y.-D.; Lee, Y.-K.; Song, K. H.
2018-07-01
This study was carried out to evaluate the effect of grain misorientation angle distribution on the deformation behavior and twinning of Ti-15Mo alloy. Cold rolling exhibited a significant texture with grains oriented along the {111}//normal direction, which correlate with a higher fraction of low-angle boundaries. This material showed a lower yield strength and higher elongation than those of the hot rolled material. The twinning propagation mainly occurred between neighboring grains with a low-angle relation. Consequently, the texture development was correlated with low-angle boundaries and affected by the increase in the twinning density, which increased the strain hardening rate.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Zieger, H.
1961-10-01
The as-cast structure of d.c.-cast aluminum ingots sometimes shows feather-like crystals. The influence of this type of crystals on the earing behavior and on the surface markings after anodizing was investigated on Al 99.5- sheets of 2 mm thickness. Feather-like crystals gave rise to more irregular and higher earings in all cases. Hot and afterwards cold rolled sheets showed markings on the anodized surface, which were intensified by feather-like crystals in the ingot. Extruding prior to hot rolling suppressed these markings completely, but did not affect the earing behavior. (auth)
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Closure behavior of spherical void in slab during hot rolling process
NASA Astrophysics Data System (ADS)
Cheng, Rong; Zhang, Jiongming; Wang, Bo
2018-04-01
The mechanical properties of steels are heavily deteriorated by voids. The influence of voids on the product quality should be eliminated through rolling processes. The study on the void closure during hot rolling processes is necessary. In present work, the closure behavior of voids at the center of a slab at 800 °C during hot rolling processes has been simulated with a 3D finite element model. The shape of the void and the plastic strain distribution of the slab are obtained by this model. The void decreases along the slab thickness direction and spreads along the rolling direction but hardly changes along the strip width direction. The relationship between closure behavior of voids and the plastic strain at the center of the slab is analyzed. The effects of rolling reduction, slab thickness and roller diameter on the closure behavior of voids are discussed. The larger reduction, thinner slab and larger roller diameter all improve the closure of voids during hot rolling processes. Experimental results of the closure behavior of a void in the slab during hot rolling process mostly agree with the simulation results..
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NASA Astrophysics Data System (ADS)
Ji, Liang-Bo; Chen, Fang
2017-07-01
Numerical simulation and intelligent optimization technology were adopted for rolling and extrusion of zincked sheet. By response surface methodology (RSM), genetic algorithm (GA) and data processing technology, an efficient optimization of process parameters for rolling of zincked sheet was investigated. The influence trend of roller gap, rolling speed and friction factor effects on reduction rate and plate shortening rate were analyzed firstly. Then a predictive response surface model for comprehensive quality index of part was created using RSM. Simulated and predicted values were compared. Through genetic algorithm method, the optimal process parameters for the forming of rolling were solved. They were verified and the optimum process parameters of rolling were obtained. It is feasible and effective.
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Boron-copper neutron absorbing material and method of preparation
Wiencek, Thomas C.; Domagala, Robert F.; Thresh, Henry
1991-01-01
A composite, copper clad neutron absorbing material is comprised of copper powder and boron powder enriched with boron 10. The boron 10 content can reach over 30 percent by volume, permitting a very high level of neutron absorption. The copper clad product is also capable of being reduced to a thickness of 0.05 to 0.06 inches and curved to a radius of 2 to 3 inches, and can resist temperatures of 900.degree. C. A method of preparing the material includes the steps of compacting a boron-copper powder mixture and placing it in a copper cladding, restraining the clad assembly in a steel frame while it is hot rolled at 900.degree. C. with cross rolling, and removing the steel frame and further rolling the clad assembly at 650.degree. C. An additional sheet of copper can be soldered onto the clad assembly so that the finished sheet can be cold formed into curved shapes.
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Combustion Engineering, Inc. [LMFBR
DOE Office of Scientific and Technical Information (OSTI.GOV)
Not Available
1980-01-01
Four (4) 3 '' O.D. x 0.470'' nominal wall thickness (NWT) hot rotary pierced/roll reduced modified AOD/ESR tube hollows were cold pilger reduced through one pass to 2'' O.D. x 0.250'' NWT tubing. Two (2) additional hollows of same size and process history were cold pilger reduced through one pass to 2 1/8'' O.D. x 0.200'' NWT. Six (6) 3 3/4'' O.D. x 0.600'' NWT hot extruded tube hollows were cold pilger reduced through two passes to 2'' O.D. x 0.250'' NWT tubing. Four of the extrusions represented duplex AOD/ESR melting practice and two extrusions represented AOD melting practice. Twelvemore » (12) pieces of 2 1/8'' O.D. x 0.200'' NWT x approx. 9' long tubing were final heat treated, straightened, and ultrasonically tested. Twelve (12) more pieces of 2 1/8'' O.D. tubing have been solution austenitized (1177/sup 0/C) and are to be reaustenitized (1066/sup 0/C), tempered (760/sup 0/C), straightened, and ultrasonically inspected. All 2'' O.D. x 0.250'' NWT tubing is in the solution austenitized condition. Creep and stress rupture testing has continued on aged material from CarTech heat 91887 and on unaged material from CarTech heat 30182A.« less
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Finite-element model to predict roll-separation force and defects during rolling of U-10Mo alloys
NASA Astrophysics Data System (ADS)
Soulami, Ayoub; Burkes, Douglas E.; Joshi, Vineet V.; Lavender, Curt A.; Paxton, Dean
2017-10-01
A major goal of the Convert Program of the U.S. Department of Energy's National Nuclear Security Administration (DOE/NNSA) is to enable high-performance research reactors to operate with low-enriched uranium rather than the high-enriched uranium currently used. To this end, uranium alloyed with 10 wt% molybdenum (U-10Mo) represents an ideal candidate because of its stable gamma phase, low neutron caption cross section, acceptable swelling response, and predictable irradiation behavior. However, because of the complexities of the fuel design and the need for rolled monolithic U-10Mo foils, new developments in processing and fabrication are necessary. This study used a finite-element code, LS-DYNA, as a predictive tool to optimize the rolling process. Simulations of the hot rolling of U-10Mo coupons encapsulated in low-carbon steel were conducted following two different schedules. Model predictions of the roll-separation force and roll pack thicknesses at different stages of the rolling process were compared with experimental measurements. The study reported here discussed various attributes of the rolled coupons revealed by the model (e.g., waviness and thickness non-uniformity like dog-boning). To investigate the influence of the cladding material on these rolling defects, other cases were simulated: hot rolling with alternative can materials, namely, 304 stainless steel and Zircaloy-2, and bare-rolling. Simulation results demonstrated that reducing the mismatch in strength between the coupon and can material improves the quality of the rolled sheet. Bare-rolling simulation results showed a defect-free rolled coupon. The finite-element model developed and presented in this study can be used to conduct parametric studies of several process parameters (e.g., rolling speed, roll diameter, can material, and reduction).
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Preparation of isotopic molybdenum foils utilizing small quantities of material
NASA Astrophysics Data System (ADS)
Lipski, A. R.; Lee, L. L.; Liang, J. F.; Mahon, J. C.
1993-09-01
A simple method utilizing a small amount of isotopic material for production of molybdenum foils is discussed. An e-gun is used in the procedure. The Mo powder undergoes reduction-sintering and melting-solidifying steps leading to the creation of a metallic droplet suitable for further cold rolling or vacuum deposition.
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Cold Rolled Steel and Knowledge: What Can Higher Education Learn about Productivity?
ERIC Educational Resources Information Center
Thille, Candace; Smith, Joel
2011-01-01
Higher education is simply not making substantial progress in addressing its most significant challenges: educating an increasingly diverse body of students while containing the cost that is putting postsecondary education beyond the reach of a growing percentage of the world's population. Tweaking long-standing strategies to achieve incremental…
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Federal Register 2010, 2011, 2012, 2013, 2014
2010-05-12
... On-Site Leased Workers From Adecco, ESW, Inc., Guardsmark, Hudson Global Resources and Multi Serv... and cold rolled steel. The company reports that workers leased from Multi Serv were employed on-site at the Hennepin, Illinois location of Arcelor Mittal. The Department has determined that these...
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Sohn, Seok Su; Song, Hyejin; Jo, Min Chul; Song, Taejin; Kim, Hyoung Seop; Lee, Sunghak
2017-04-28
Needs for steel designs of ultra-high strength and excellent ductility have been an important issue in worldwide automotive industries to achieve energy conservation, improvement of safety, and crashworthiness qualities. Because of various drawbacks in existing 1.5-GPa-grade steels, new development of formable cold-rolled ultra-high-strength steels is essentially needed. Here we show a plausible method to achieve ultra-high strengths of 1.0~1.5 GPa together with excellent ductility above 50% by actively utilizing non-recrystallization region and TRansformation-Induced Plasticity (TRIP) mechanism in a cold-rolled and annealed Fe-Mn-Al-C-based steel. We adopt a duplex microstructure composed of austenite and ultra-fine ferrite in order to overcome low-yield-strength characteristics of austenite. Persistent elongation up to 50% as well as ultra-high yield strength over 1.4 GPa are attributed to well-balanced mechanical stability of non-crystallized austenite with critical strain for TRIP. Our results demonstrate how the non-recrystallized austenite can be a metamorphosis in 1.5-GPa-grade steel sheet design.
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Cheng, Hai-Hsuan; Whang, Liang-Ming; Yi, Tse-Fu; Liu, Cheng-Pin; Lin, Tsair-Fuh; Yeh, Mao-Song
2018-05-09
A pilot-scale single-stage anaerobic fluidized membrane bioreactor (AFMBR) was firstly used in this study to treat cold-rolling emulsion wastewater from steel industry. It was continuously operated for 302 days with influent COD concentration of 860-1120 mg/L. Under a hydraulic retention time of 1.5 d, the average effluent COD concentration of 72 mg/L achieved corresponding 90% of COD removal. The permeate flux was varied between 1.7 and 2.9 L/m 2 /h during operation which decreased with increased biomass concentration inside AFMBR. The trans-membrane pressure (TMP) was generally around 35-40 kPa, however, it increased up to 60 kPa when volatile suspended solid increased to above 2.5 g/L. Both flux and TMP data reveal the importance of biomass control for AFMBR operation. Results from terminal restriction fragment length polymorphism (T-RFLP) show the genus Methanosaeta was dominant on GAC and it shared dominance with the genera Methanomethylovorans and Methanosarcina in suspended sludge. Copyright © 2018 Elsevier Ltd. All rights reserved.
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GRCop-84 Rolling Parameter Study
NASA Technical Reports Server (NTRS)
Loewenthal, William S.; Ellis, David L.
2008-01-01
This report is a section of the final report on the GRCop-84 task of the Constellation Program and incorporates the results obtained between October 2000 and September 2005, when the program ended. NASA Glenn Research Center (GRC) has developed a new copper alloy, GRCop-84 (Cu-8 at.% Cr-4 at.% Nb), for rocket engine main combustion chamber components that will improve rocket engine life and performance. This work examines the sensitivity of GRCop-84 mechanical properties to rolling parameters as a means to better define rolling parameters for commercial warm rolling. Experiment variables studied were total reduction, rolling temperature, rolling speed, and post rolling annealing heat treatment. The responses were tensile properties measured at 23 and 500 C, hardness, and creep at three stress-temperature combinations. Understanding these relationships will better define boundaries for a robust commercial warm rolling process. The four processing parameters were varied within limits consistent with typical commercial production processes. Testing revealed that the rolling-related variables selected have a minimal influence on tensile, hardness, and creep properties over the range of values tested. Annealing had the expected result of lowering room temperature hardness and strength while increasing room temperature elongations with 600 C (1112 F) having the most effect. These results indicate that the process conditions to warm roll plate and sheet for these variables can range over wide levels without negatively impacting mechanical properties. Incorporating broader process ranges in future rolling campaigns should lower commercial rolling costs through increased productivity.
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Heterogeneous multi-layered IF steel with simultaneous high strength and good ductility
NASA Astrophysics Data System (ADS)
Zhang, Ling; Jiang, Xiaojuan; Wang, Yuhui; Chen, Qiang; Chen, Zhen; Zhang, Yonghong; Huang, Tianlin; Wu, Guilin
2017-07-01
Multi-layered IF steel samples were designed and fabricated by hot compression followed by cold forging of an alternating stack of cold-rolled and annealed IF steel sheets, with an aim to improve the strength of the material without losing much ductility. A very good combination of strength and ductility was achieved by proper annealing after deformation. Microstructural analysis by electron back-scatter diffraction revealed that the good combination of strength and ductility is related to a characteristic hierarchical structure that is characterized by layered and lamella structures with different length scales.
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Roll forming of eco-friendly stud
NASA Astrophysics Data System (ADS)
Keum, Y. T.; Lee, S. Y.; Lee, T. H.; Sim, J. K.
2013-12-01
In order to manufacture an eco-friendly stud, the sheared pattern is designed by the Taguchi method and expanded by the side rolls. The seven geometrical shape of sheared pattern are considered in the structural and thermal analyses to select the best functional one in terms of the durability and fire resistance of dry wall. For optimizing the size of the sheared pattern chosen, the L9 orthogonal array and smaller-the-better characteristics of the Taguchi method are used. As the roll gap causes forming defects when the upper-and-lower roll type is adopted for expanding the sheared pattern, the side roll type is introduced. The stress and strain distributions obtained by the FEM simulation of roll-forming processes are utilized for the design of expanding process. The expanding process by side rolls shortens the length of expanding process and minimizes the cost of dies. Furthermore, the stud manufactured by expanding the sheared pattern of the web is an eco-friend because of the scrapless roll-forming process. In addition, compared to the conventionally roll-formed stud, the material cost is lessened about 13.6% and the weight is lightened about 15.5%.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Soulami, Ayoub; Lavender, Curt A.; Paxton, Dean M.
2014-04-23
Pacific Northwest National Laboratory (PNNL) has been investigating manufacturing processes for the uranium-10% molybdenum (U-10Mo) alloy plate-type fuel for the U.S. high-performance research reactors. This work supports the Convert Program of the U.S. Department of Energy’s National Nuclear Security Administration (DOE/NNSA) Global Threat Reduction Initiative. This report documents modeling results of PNNL’s efforts to perform finite-element simulations to predict roll separating forces and rolling defects. Simulations were performed using a finite-element model developed using the commercial code LS-Dyna. Simulations of the hot rolling of U-10Mo coupons encapsulated in low-carbon steel have been conducted following two different schedules. Model predictions ofmore » the roll-separation force and roll-pack thicknesses at different stages of the rolling process were compared with experimental measurements. This report discusses various attributes of the rolled coupons revealed by the model (e.g., dog-boning and thickness non-uniformity).« less
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Corrosion-Prevention Capabilities of a Water-Borne, Silicone-Based, Primerless Coating
NASA Technical Reports Server (NTRS)
Calle, Luz Marina; MacDowell, Louis G.; Vinje, Rubie D.
2005-01-01
Comparative tests have been performed to evaluate the corrosion-prevention capabilities of an experimental paint of the type described in Water-Borne, Silicone-Based, Primerless Paints, NASA Tech Briefs, Vol. 26, No. 11 (November 2002), page 30. To recapitulate: these paints contain relatively small amounts of volatile organic solvents and were developed as substitutes for traditional anticorrosion paints that contain large amounts of such solvents. An additional desirable feature of these paints is that they can be applied without need for prior application of primers to ensure adhesion. The test specimens included panels of cold-rolled steel, stainless steel 316, and aluminum 2024-T3. Some panels of each of these alloys were left bare and some were coated with the experimental water-borne, silicone-based, primerless paint. In addition, some panels of aluminum 2024-T3 and some panels of a fourth alloy (stainless steel 304) were coated with a commercial solvent-borne paint containing aluminum and zinc flakes in a nitrile rubber matrix. In the tests, the specimens were immersed in an aerated 3.5-weight-percent aqueous solution of NaCl for 168 hours. At intervals of 24 hours, the specimens were characterized by electrochemical impedance spectroscopy (EIS) and measurements of corrosion potentials. The specimens were also observed visually. As indicated by photographs of specimens taken after the 168-hour immersion (see figure), the experimental primerless silicone paint was effective in preventing corrosion of stainless steel 316, but failed to protect aluminum 2024-T3 and cold-rolled steel. The degree of failure was greater in the case of the cold-rolled steel. On the basis of visual observations, EIS, and corrosion- potential measurements, it was concluded that the commercial aluminum and zinc-filled nitrile rubber coating affords superior corrosion protection to aluminum 2024-T3 and is somewhat less effective in protecting stainless steel 304.
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Digitalization in roll forming manufacturing
NASA Astrophysics Data System (ADS)
Sedlmaier, A.; Dietl, T.; Ferreira, P.
2017-09-01
Roll formed profiles are used in automotive chassis production as building blocks for the body-in-white. The ability to produce profiles with discontinuous cross sections, both in width and in depth, allows weight savings in the final automotive chassis through the use of load optimized cross sections. This has been the target of the 3D Roll Forming process. A machine concept is presented where a new forming concept for roll formed parts in combination with advanced robotics allowing freely positioned roll forming tooling in 3D space enables the production of complex shapes by roll forming. This is a step forward into the digitalization of roll forming manufacturing by making the process flexible and capable of rapid prototyping and production of small series of parts. Moreover, data collection in a large scale through the control system and integrated sensors lead to an increased understanding of the process and provide the basis to develop self-optimizing roll forming machines, increasing the productivity, quality and predictability of the roll-forming process. The first parts successfully manufactured with this new forming concept are presented.
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NASA Astrophysics Data System (ADS)
Huang, Xiao-Jie; Zhang, Li; Hu, Yu-Peng; Li, You-Rong
2018-06-01
In order to understand the effect of the Rayleigh number, the density inversion phenomenon and the aspect ratio on the flow patterns and the heat transfer characteristics of Rayleigh–Bénard convection of cold water in the neighborhood of the maximum density, a series of large eddy simulations are conducted by using the finite volume method. The Rayleigh number ranges between 106 and 109, the density inversion parameter and the aspect ratio are varied from 0 to 0.9 and from 0.4 to 2.5, respectively. The results indicate that the reversal of the large scale circulation (LSC) occurs with the increase of the Rayleigh number. When there exists a density inversion phenomenon, the key driver for the LSC is hot plumes. When the density inversion parameter is large enough, a stagnant region is found near the top of the container as the hot plumes cannot move to the top wall. The flow pattern structures depend mainly on the aspect ratio. When the aspect ratio is small, the rolls are vertically stacked and the flow keeps on switching among different flow states. For a moderate aspect ratio, different long-lived roll states coexist at a fixed aspect ratio. For a larger aspect ratio, the flow state is everlasting. The number of rolls increases with the increase of the aspect ratio. Furthermore, the aspect ratio has only slight influence on the time averaged Nusselt number for all density inversion parameters.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Rabin, S.A.; Martin, M.M.; Lotts, A.L.
The fabricability of dispersion fuels using UO/sub 2/ or UC as the dispersoid and uranium combined with 10 to 15 wt% Mo as the matrix was investigated. Cores containing l7.8 wt% UO/sub 2/ dispersed in U-- 15 wt.% Mo were successfully fabricated to about 80% of theoretical density by cold pressing at 50 tsi, sintering at 1100 deg C, and cold coining at 50 tsi. Comparable results were obtained with UC as the dispersoid. Core fabrication results varied greatly with the type of matrix powder used. Occluded gases, pour density, and surface cleanliness bore important relations to the fabrication behaviormore » of powders. Suitable pressing and sintering results were obtained with prealloyed, calcium-reduced U--Mo powder and with molybdenum and calcium-reduced uranium as elemental powders. Shotted prealloyed powders were difficult to press and sinter, as were elemental and prealloyed powders prepared by hydriding. The cores containing UO/sub 2/ were picture-frame, hot-roll-clad as miniature plates. Molybdenum, Fansteel 82, and Zr--3 wt% Al were investigated as cladding materials. While each bonded well to itself, only the molybdenum-clad core, rolled at 1150 deg C to 10/1 reduction, resulted in dispersions free of ruptures and UO/sub 2/ fragmentation and in strong bonding to the core, evaluated by metallography, mechanical peel, and thermal shock tests. The matrix phase was homogeneous, but the UO/sub 2/ dispersoid showed stringering characteristic of cores worked by hot rolling. Core densities as high as 99% of theoretical were obtained. (auth)« less
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NASA Astrophysics Data System (ADS)
Liu, Yangyang; Li, Jiheng; Gao, Xuexu
2017-08-01
Magnetostrictive Fe82Ga4.5Al13.5 sheets with 0.1 at% NbC were prepared from directional solidified alloys with <0 0 1> preferred orientation. The slabs were hot rolled at 650 °C and warm rolled at 500 °C. Then some warm-rolled sheets were annealed intermediately at 850 °C for 5 min but the others not. After that, all the sheets were cold rolled to a final thickness of ∼0.3 mm. The microstructures, the textures and the distributions of second phase particles in the primary recrystallized samples were investigated. With intermediate annealing, the inhomogeneous microstructure was improved remarkably and strong Goss ({1 1 0}<0 0 1>) and γ-fiber (<1 1 1>//normal direction [ND]) textures were produced in the primary recrystallized samples. But, an evident disadvantage in size and quantity was observed for Goss grains in the primary recrystallized sample without intermediate annealing. After a final annealing, the final textures and magnetostrictions of samples with and without intermediate annealing were characterized. For samples without intermediate annealing, abnormal growth of {1 1 3} grains occurred and deteriorated the magnetostriction. In contrast, abnormal Goss grain growth occurred completely in samples with intermediate annealing and led to saturation magnetostriction as high as 156 ppm.
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Development of a Rolling Process Design Tool for Use in Improving Hot Roll Slab Recovery
DOE Office of Scientific and Technical Information (OSTI.GOV)
Couch, R; Becker, R; Rhee, M
2004-09-24
Lawrence Livermore National Laboratory participated in a U. S. Department of Energy/Office of Industrial Technology sponsored research project 'Development of a Rolling Process Design Tool for Use in Improving Hot Roll Slab Recovery', as a Cooperative Agreement TC-02028 with the Alcoa Technical Center (ATC). The objective of the joint project with Alcoa is to develop a numerical modeling capability to optimize the hot rolling process used to produce aluminum plate. Product lost in the rolling process and subsequent recycling, wastes resources consumed in the energy-intensive steps of remelting and reprocessing the ingot. The modeling capability developed by project partners willmore » be used to produce plate more efficiently and with reduced product loss.« less
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Celada-Casero, C., E-mail: c.celada@cenim.csic.es
The primary objective of this work is to obtain fundamental insights on phase transformations, with focus on the reaustenitization process (α′→γ transformation), of a cold-rolled (CR) semi-austenitic metastable stainless steel upon different isochronal conditions (0.1, 1, 10 and 100 °C/s). For this purpose, an exhaustive microstructural characterization has been performed by using complementary experimental such as scanning and transmission electron microscopy (SEM and TEM), electron backscattered diffraction (EBSD), electron probe microanalysis (EPMA), micro-hardness Vickers and magnetization measurements. It has been detected that all microstructural changes shift to higher temperatures as the heating rate increases. The reaustenitization occurs in two-steps formore » all heating rates, which is attributed to the chemical banding present in the CR state. The α′→γ transformation is controlled by the migration of substitutional alloying elements across the austenite/martensite (γ/α′) interface, which finally leads to ultrafine-grained reaustenitized microstructures (440–280 nm). The morphology of the martensite phase in the CR state has been found to be the responsible for such a grain refinement, along with the presence of χ-phase and nanometric Ni{sub 3}(Ti,Al) precipitates that pin the austenite grain growth, especially upon slowly heating at 0.1 °C/s. - Highlights: •Ultrafine-grained austenite structures are obtained isochronally at 0.1–100 °C/s •The α′→γ transformation occurs in two steps due to the initial chemical banding •A diffusional mechanism governs the α′→γ transformation for all heating rates •The dislocation-cell-type of martensite promotes a diffusional mechanism •Precipitates located at α′/γ interfaces hinder the austenite growth.« less
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Metallurgical characterization of brass objects from the Akko 1 shipwreck, Israel
DOE Office of Scientific and Technical Information (OSTI.GOV)
Ashkenazi, D., E-mail: dana@eng.tau.ac.il; Cvikel, D.; Stern, A.
2014-06-01
The Akko 1 shipwreck was a small Egyptian armed vessel or auxiliary naval brig built in the eastern Mediterranean at the beginning of the 19th century. During the underwater excavations, about 230 brass hook-and-eye closures were found, mainly in the bow area. In addition, 158 brass cases were found, mainly between midships and the aft extremity of the shipwreck. Metallurgical non-destructive and destructive characterizations of selected items were performed, including radiographic testing, XRF, lead isotope analysis, optical microscopy, SEM–EDS and microhardness tests. The hook-and-eye closures and the cases were both found to be made of binary copper–zinc alloy (about 30more » wt.% zinc). While the brass cases were made from rolled sheets, hand-made using simple tools, and joined by tin–lead soldering material, the brass hook-and-eye closures were hand-made from drawn brass wire, and manufactured from commercial drawn brass bars by a cold-working process. The lead isotope analyses suggest different provenances of the raw materials used for making the brass objects, thus the different origins of the ores may hint that the brass wire and sheet were imported to the workshops in which the objects were manufactured. - Highlights: • Brass cases and hook-and-eye closures were retrieved from the Akko 1 shipwreck. • Both types of objects were made of binary copper–zinc alloy (about 30 wt.% zinc). • The cases were hand-made from rolled sheets and joined by tin–lead soldering. • Hook-and-eye closures were made from drawn brass wire manufactured by cold-working. • Lead isotope analyses suggest that the origins of the raw material were diverse.« less
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Numerical analysis of the flexible roll forming of an automotive component from high strength steel
NASA Astrophysics Data System (ADS)
Abeyrathna, B.; Abvabi, A.; Rolfe, B.; Taube, R.; Weiss, M.
2016-11-01
Conventional roll forming is limited to components with uniform cross-section; the recently developed flexible roll forming (FRF) process can be used to form components which vary in both width and depth. It has been suggested that this process can be used to manufacture automotive components from Ultra High Strength Steel (UHSS) which has limited tensile elongation. In the flexible roll forming process, the pre-cut blank is fed through a set of rolls; some rolls are computer-numerically controlled (CNC) to follow the 3D contours of the part and hence parts with a variable cross-section can be produced. This paper introduces a new flexible roll forming technique which can be used to form a complex shape with the minimum tooling requirements. In this method, the pre-cut blank is held between two dies and the whole system moves back and forth past CNC forming rolls. The forming roll changes its angle and position in each pass to incrementally form the part. In this work, the process is simulated using the commercial software package Copra FEA. The distribution of total strain and final part quality are investigated as well as related shape defects observed in the process. Different tooling concepts are used to improve the strain distribution and hence the part quality.
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Analysis of roll-stamped light guide plate fabricated with laser-ablated stamper
NASA Astrophysics Data System (ADS)
Na, Hyunjun; Hong, Seokkwan; Kim, Jongsun; Hwang, Jeongho; Joo, Byungyun; Yoon, Kyunghwan; Kang, Jeongjin
2017-12-01
LGP (light guide plate) is one of the major components of LCD (liquid crystal display), and it makes surface illumination for LCD backlit. LGP is a transparent plastic plate usually produced by injection molding process. On the back of LGP there are micron size patterns for extraction of light. Recently a roll-stamping process has achieved the high mass productivity of thinner LGPs. In order to fabricate optical patterns on LGPs, a fabricating tool called as a stamper is used. Micro patterns on metallic stampers are made by several micro machining processes such as chemical etching, LIGA-reflow, and laser ablation. In this study, a roll-stamping process by using a laser ablated metallic stamper was dealt with in consideration of the compatibility with the roll-stamping process. LGP fabricating tests were performed using a roll-stamping process with four different roll pressures. Pattern shapes on the stamper fabricated by laser ablation and transcription ratios of the roll-stamping process were analyzed, and LGP luminance was evaluated. Based on the evaluation, optical simulation model for LGP was made and simulation accuracy was evaluated. Simulation results showed good agreements with optical performance of LGPs in the brightness and uniformity. It was also shown that the roll-stamped LGP has the possibility of better optical performance than the conventional injection molded LGP. It was also shown that the roll-stamped LGP with the laser ablated stamper is potential to have better optical performance than the conventional injection molded LGP.
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Modeling the Hot Ductility of AA6061 Aluminum Alloy After Severe Plastic Deformation
NASA Astrophysics Data System (ADS)
Khamei, A. A.; Dehghani, K.; Mahmudi, R.
2015-05-01
Solutionized AA6061 aluminum alloy was processed by equal-channel angular pressing followed by cold rolling. The hot ductility of the material was studied after severe plastic deformation. The hot tensile tests were carried out in the temperature range of 300-500°C and at the strain rates of 0.0005-0.01 s-1. Depending on the temperature and strain rate, the applied strain level exhibited significant effects on the hot ductility, strain-rate sensitivity, and activation energy. It can be suggested that the possible mechanism dominated the hot deformation during tensile testing is dynamic recovery and dislocation creep. Constitutive equations were developed to model the hot ductility of the severe plastic deformed AA6061 alloy.
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Investigation into the Origin of Magnetic Properties of Amorphous Metallic Alloys.
1981-10-01
Luborsky, F.E., J.L. Walter, and D. LeGrand. "Cold Rolling and Annealing of Amor- phous Ribbons," IEEE Trans. Magn. Mag-12, 1976, p. 930. Reprint 8011 ...curve. Iiii) For Fe-B-Al they lie significantly below. The differences between the T, for the three different aluminium containing alloys is not
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Environmentally Friendly Zirconium Oxide Pretreatment
2013-05-01
during the conversion of the highly soluble hexavalent chromate ions to an inert and relatively insoluble trivalent chromium oxide layer. Depletion of...are being used commercially in automotive and other industrial operations as replacements to hexavalent chromium -based and zinc phosphate...Society for Testing and Materials AVCRAD Aviation Classification Repair Activity Depot Chrome (VI) Hexavalent Chromium CRS Cold Rolled Steel
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The Effects of Forming Parameters on Conical Ring Rolling Process
Meng, Wen; Zhao, Guoqun; Guan, Yanjin
2014-01-01
The plastic penetration condition and biting-in condition of a radial conical ring rolling process with a closed die structure on the top and bottom of driven roll, simplified as RCRRCDS, were established. The reasonable value range of mandrel feed rate in rolling process was deduced. A coupled thermomechanical 3D FE model of RCRRCDS process was established. The changing laws of equivalent plastic strain (PEEQ) and temperature distributions with rolling time were investigated. The effects of ring's outer radius growth rate and rolls sizes on the uniformities of PEEQ and temperature distributions, average rolling force, and average rolling moment were studied. The results indicate that the PEEQ at the inner layer and outer layer of rolled ring are larger than that at the middle layer of ring; the temperatures at the “obtuse angle zone” of ring's cross-section are higher than those at “acute angle zone”; the temperature at the central part of ring is higher than that at the middle part of ring's outer surfaces. As the ring's outer radius growth rate increases at its reasonable value ranges, the uniformities of PEEQ and temperature distributions increase. Finally, the optimal values of the ring's outer radius growth rate and rolls sizes were obtained. PMID:25202716
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NASA Astrophysics Data System (ADS)
Girina, O.; Fonstein, N.; Yakubovsky, O.; Panahi, D.; Bhattacharya, D.; Jansto, S.
The influence of Nb, Mo, Cr and B on phase transformations and mechanical properties are studied in a 0.15C-2.0Mn-0.3Si-0.020Ti dual phase steel separately and in combination. The formation and decomposition of austenite together with recrystallization of ferrite are evaluated by dilatometry and constructed CCT-diagrams in laboratory processed cold rolled material cooled after full austenitization and from intercritical temperature range. The effect of alloying elements on formation of austenite through their effect on initial hot rolled structure is taken into account. The interpretation of phase transformations during heating and cooling is supported by metallography. The effect of alloying elements on mechanical properties and structure are evaluated by annealing simulations. It has been shown that mechanical properties are strongly influenced by alloying additions such as Nb, Mo, Cr and B through their effect on ferrite formation during continuous cooling and corresponding enrichment of remaining austenite by carbon. Depending on combined effect of these alloying elements, different phase transformations can be promoted during cooling. This allows controlling of final microstructural constituents and mechanical properties.
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NASA Astrophysics Data System (ADS)
Morozov, O.; Mats, O.; Mats, V.; Zhurba, V.; Khaimovich, P.
2018-01-01
The present article introduces the data of analysis of ranges of ion-implanted deuterium desorption from Zr-1% Nb alloy. The samples studied underwent plastic deformation, low temperature extrusion and electron irradiation. Plastic rolling of the samples at temperature ∼300 K resulted in plastic deformation with the degree of ε = 3.9 and the formation of nanostructural state with the average grain size of d = 61 nm. The high degree of defectiveness is shown in thermodesorption spectrum as an additional area of the deuterium desorption in the temperature ranges 650-850 K. The further processing of the sample (that had undergone plastic deformation by plastic rolling) with electron irradiation resulted in the reduction of the average grain size (58 nm) and an increase in borders concentration. As a result the amount of deuterium desorpted increased in the temperature ranges 650-900 K. In case of Zr-1% Nb samples deformed by extrusion the extension of desorption area is observed towards the temperature reduction down to 420 K. The formation of the phase state of deuterium solid solution in zirconium was not observed. The structural state behavior is a control factor in the process of deuterium thermodesorption spectrum structure formation with a fixed implanted deuterium dose (hydrogen diagnostics). It appears as additional temperature ranges of deuterium desorption depending on the type, character and defect content.
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High-rate, roll-to-roll nanomanufacturing of flexible systems
NASA Astrophysics Data System (ADS)
Cooper, Khershed P.; Wachter, Ralph F.
2012-10-01
Since the National Nanotechnology Initiative was first announced in 2000, nanotechnology has developed an impressive catalog of nano-scale structures with building-blocks such as nanoparticles, nanotubes, nanorods, nanopillars, and quantum dots. Similarly, there are accompanying materials processes such as, atomic layer deposition, pulsed layer deposition, nanoprinting, nanoimprinting, transfer printing, nanolithography and nanopatterning. One of the challenges of nanomanufacturing is scaling up these processes reliably and affordably. Roll-to-roll manufacturing is a means for scaling up, for increasing throughput. It is high-speed production using a continuous, moving platform such as a web or a flexible substrate. The adoption of roll-to-roll to nanomanufacturing is novel. The goal is to build structures and devices with nano-scale features and specific functionality. The substrate could be a polymer, metal foil, silk, cloth or paper. The materials to build the structures and multi-level devices could be organic, inorganic or biological. Processing could be solution-based, e.g., ink-jet printing, or vacuum-based, e.g., chemical vapor deposition. Products could be electronics, optoelectronics, membranes, catalysts, microfluidics, lab-on-film, filters, etc. By this means, processing of large and conformal areas is achievable. High-throughput translates into low cost, which is the attraction of roll-to-roll nanomanufacturing. There are technical challenges requiring fundamental scientific advances in materials and process development and in manufacturing and system-integration where achieving nano-scale feature size, resolution and accuracy at high speeds can be major hurdles. We will give an overview of roll-to-roll nanomanufacturing with emphasis on the need to understand the material, process and system complexities, the need for instrumentation, measurement, and process control and describe the concept of cyber-enabled nanomanufacturing for reliable and predictable production.
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Thermodynamic Behavior Research Analysis of Twin-roll Casting Lead Alloy Strip Process
NASA Astrophysics Data System (ADS)
Jiang, Chengcan; Rui, Yannian
2017-03-01
The thermodynamic behavior of twin-roll casting (TRC) lead alloy strip process directly affects the forming of the lead strip, the quality of the lead strip and the production efficiency. However, there is little research on the thermodynamics of lead alloy strip at home and abroad. The TRC lead process is studied in four parameters: the pouring temperature of molten lead, the depth of molten pool, the roll casting speed, and the rolling thickness of continuous casting. Firstly, the thermodynamic model for TRC lead process is built. Secondly, the thermodynamic behavior of the TRC process is simulated with the use of Fluent. Through the thermodynamics research and analysis, the process parameters of cast rolling lead strip can be obtained: the pouring temperature of molten lead: 360-400 °C, the depth of molten pool: 250-300 mm, the roll casting speed: 2.5-3 m/min, the rolling thickness: 8-9 mm. Based on the above process parameters, the optimal parameters(the pouring temperature of molten lead: 375-390 °C, the depth of molten pool: 285-300 mm, the roll casting speed: 2.75-3 m/min, the rolling thickness: 8.5-9 mm) can be gained with the use of the orthogonal experiment. Finally, the engineering test of TRC lead alloy strip is carried out and the test proves the thermodynamic model is scientific, necessary and correct. In this paper, a detailed study on the thermodynamic behavior of lead alloy strip is carried out and the process parameters of lead strip forming are obtained through the research, which provide an effective theoretical guide for TRC lead alloy strip process.
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Circular RNAs: diversity of form and function.
Lasda, Erika; Parker, Roy
2014-12-01
It is now clear that there is a diversity of circular RNAs in biological systems. Circular RNAs can be produced by the direct ligation of 5' and 3' ends of linear RNAs, as intermediates in RNA processing reactions, or by "backsplicing," wherein a downstream 5' splice site (splice donor) is joined to an upstream 3' splice site (splice acceptor). Circular RNAs have unique properties including the potential for rolling circle amplification of RNA, the ability to rearrange the order of genomic information, protection from exonucleases, and constraints on RNA folding. Circular RNAs can function as templates for viroid and viral replication, as intermediates in RNA processing reactions, as regulators of transcription in cis, as snoRNAs, and as miRNA sponges. Herein, we review the breadth of circular RNAs, their biogenesis and metabolism, and their known and anticipated functions. © 2014 Lasda and Parker; Published by Cold Spring Harbor Laboratory Press for the RNA Society.
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Controlling the mechanical properties of carbon steel by thermomechanical treatment
NASA Astrophysics Data System (ADS)
Balavar, Mohsen; Mirzadeh, Hamed
2018-01-01
The effect of thermomechanical processing and heat treatment on the microstructure and mechanical properties of low carbon steel was studied. It was revealed that the dual phase ferritic-martensitic microstructure shows a good combination of tensile strength and ductility along with superior work hardening response. On the other hand, the bimodal-sized structure containing ultrafine grained (UFG) and micron-sized ferrite phase can be easily produced by cold rolling and annealing of the dual phase starting microstructure. This steel showed high yield stress, tensile strength, and ductility, but poor work hardening ability. The full annealed ferritic-pearlitic sheet with banded morphology exhibited low strength and high total elongation with the appearance of the yield point phenomenon. The martensitic steels, however, had high tensile strength and low ductility. By comparing the tensile properties of these steels, it was shown that it is possible to control the mechanical properties of low carbon steel by simple processing routes.
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Integrated process for the removal of emulsified oils from effluents in the steel industry
DOE Office of Scientific and Technical Information (OSTI.GOV)
Benito, J.M.; Rios, G.; Gutierrez, B.
1999-11-01
Emulsified oils contained in aqueous effluents from cold-rolling mills of the steel industry can be effectively removed via an integrated process consisting of a coagulation/flocculation stage followed by ultrafiltration of the resulting aqueous phase. The effects of CaCl{sub 2}, NaOH, and lime on the stability of different industrial effluents were studied in the coagulation experiments. The flocculants tested were inorganic prehydrolyzed aluminum salts and quaternary polyamines. Ultrafiltration of the aqueous phase from the coagulation/flocculation stage was carried out in a stirred cell using Amicon PM30 and XM300 organic membranes. Permeate fluxes were measured for industrial effluents to which the indicatedmore » coagulants and flocculants had been added. Oil concentrations in the permeate were 75% lower than the limits established by all European Union countries. Complete regeneration of the membrane was accomplished with an aqueous solution of a commercial detergent.« less
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Producing thin strips by twin-roll casting—part I: Process aspects and quality issues
NASA Astrophysics Data System (ADS)
Li, Ben Q.
1995-05-01
This two-part paper discusses recent advances in research and development for the direct production of coilable thin strips by twin-roll casting in both the aluminum and steel industries. While the former is empowering the casters to approach the theoretical productivity limit, the latter is striving to put pilot casters into commercial operation. These intensive R&D efforts are derived from the advantages, both economic and metallurgical, offered by the process. As twin-roll casting combines solidification and hot rolling into a single operation, the process requires low capital investment and low operational cost. Also, because of the high solidification rate attained in the process, the thin strips produced have a refined metallurgical structure, characterized by columnar and equiaxed zones with fine intermetallic particles. The enthusiasm about twin-roll casting is now being spread worldwide. This paper focuses on the process aspects and quality control of twin-roll casting. Part II, which will appear in the August issue, will review process modeling and pilot-plant development activities.
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Numerical simulation study on rolling-chemical milling process of aluminum-lithium alloy skin panel
NASA Astrophysics Data System (ADS)
Huang, Z. B.; Sun, Z. G.; Sun, X. F.; Li, X. Q.
2017-09-01
Single curvature parts such as aircraft fuselage skin panels are usually manufactured by rolling-chemical milling process, which is usually faced with the problem of geometric accuracy caused by springback. In most cases, the methods of manual adjustment and multiple roll bending are used to control or eliminate the springback. However, these methods can cause the increase of product cost and cycle, and lead to material performance degradation. Therefore, it is of significance to precisely control the springback of rolling-chemical milling process. In this paper, using the method of experiment and numerical simulation on rolling-chemical milling process, the simulation model for rolling-chemical milling process of 2060-T8 aluminum-lithium alloy skin was established and testified by the comparison between numerical simulation and experiment results for the validity. Then, based on the numerical simulation model, the relative technological parameters which influence on the curvature of the skin panel were analyzed. Finally, the prediction of springback and the compensation can be realized by controlling the process parameters.
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Toward large-area roll-to-roll printed nanophotonic sensors
NASA Astrophysics Data System (ADS)
Karioja, Pentti; Hiltunen, Jussi; Aikio, Sanna M.; Alajoki, Teemu; Tuominen, Jarkko; Hiltunen, Marianne; Siitonen, Samuli; Kontturi, Ville; Böhlen, Karl; Hauser, Rene; Charlton, Martin; Boersma, Arjen; Lieberzeit, Peter; Felder, Thorsten; Eustace, David; Haskal, Eliav
2014-05-01
Polymers have become an important material group in fabricating discrete photonic components and integrated optical devices. This is due to their good properties: high optical transmittance, versatile processability at relative low temperatures and potential for low-cost production. Recently, nanoimprinting or nanoimprint lithography (NIL) has obtained a plenty of research interest. In NIL, a mould is pressed against a substrate coated with a moldable material. After deformation of the material, the mold is separated and a replica of the mold is formed. Compared with conventional lithographic methods, imprinting is simple to carry out, requires less-complicated equipment and can provide high-resolution with high throughput. Nanoimprint lithography has shown potential to become a method for low-cost and high-throughput fabrication of nanostructures. We show the development process of nano-structured, large-area multi-parameter sensors using Photonic Crystal (PC) and Surface Enhanced Raman Scattering (SERS) methodologies for environmental and pharmaceutical applications. We address these challenges by developing roll-to-roll (R2R) UV-nanoimprint fabrication methods. Our development steps are the following: Firstly, the proof of concept structures are fabricated by the use of wafer-level processes in Si-based materials. Secondly, the master molds of successful designs are fabricated, and they are used to transfer the nanophotonic structures into polymer materials using sheet-level UV-nanoimprinting. Thirdly, the sheet-level nanoimprinting processes are transferred to roll-to-roll fabrication. In order to enhance roll-to-roll manufacturing capabilities, silicone-based polymer material development was carried out. In the different development phases, Photonic Crystal and SERS sensor structures with increasing complexities were fabricated using polymer materials in order to enhance sheet-level and roll-to-roll manufacturing processes. In addition, chemical and molecular imprint (MIP) functionalization methods were applied in the sensor demonstrators. In this paper, the process flow in fabricating large-area nanophotonic structures by the use of sheet-level and roll-to-roll UV- nanoimprinting is reported.
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Continuous roll-to-roll growth of graphene films by chemical vapor deposition
NASA Astrophysics Data System (ADS)
Hesjedal, Thorsten
2011-03-01
Few-layer graphene is obtained in atmospheric chemical vapor deposition on polycrystalline copper in a roll-to-roll process. Raman and x-ray photoelectron spectroscopy were employed to confirm the few-layer nature of the graphene film, to map the inhomogeneities, and to study and optimize the growth process. This continuous growth process can be easily scaled up and enables the low-cost fabrication of graphene films for industrial applications.
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A Simplified Finite Element Simulation for Straightening Process of Thin-Walled Tube
NASA Astrophysics Data System (ADS)
Zhang, Ziqian; Yang, Huilin
2017-12-01
The finite element simulation is an effective way for the study of thin-walled tube in the two cross rolls straightening process. To determine the accurate radius of curvature of the roll profile more efficiently, a simplified finite element model based on the technical parameters of an actual two cross roll straightening machine, was developed to simulate the complex straightening process. Then a dynamic simulation was carried out using ANSYS LS-DYNA program. The result implied that the simplified finite element model was reasonable for simulate the two cross rolls straightening process, and can be obtained the radius of curvature of the roll profile with the tube’s straightness 2 mm/m.
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Consolidation Process in Near Net Shape Manufacturing of Armstrong CP-Ti/Ti-6Al-4V Powders
DOE Office of Scientific and Technical Information (OSTI.GOV)
Yamamoto, Yukinori; Kiggans, Jim; Clark, Michael B
2010-01-01
This paper summarizes our recent efforts to develop the manufacturing technologies of consolidated net-shape components by using new low-cost commercially pure titanium (CP-Ti) and Ti-6Al-4V alloy powders made by the Armstrong process. Fabrication processes of net shape/ near net shape components, such as uniaxial die-pressing, cold isostatic pressing (CIP), sintering, roll compaction and stamping, have been evaluated. The press-and-sinter processing of the powders were systematically investigated in terms of theoretical density and microstructure as a function of time, pressure, and temperature. Up to 96.4% theoretical density has been achieved with the press-and-sinter technology. Tensile properties of the consolidated samples exhibitmore » good ductility as well as equivalent yield/ultimate tensile strengths to those of fully consolidate materials, even with the presence of a certain amount of porosity. A consolidation model is also under development to interpret the powder deformation during processing. Net shape components made of the Armstrong powder can successfully be fabricated with clearer surface details by using press-and-sinter processing.« less
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Effect of roll-compaction and milling conditions on granules and tablet properties.
Perez-Gandarillas, Lucia; Perez-Gago, Ana; Mazor, Alon; Kleinebudde, Peter; Lecoq, Olivier; Michrafy, Abderrahim
2016-09-01
Dry granulation is an agglomeration process used to produce size-enlarged particles (granules), improving the handling properties of powders such as flowability. In this process, powders are compacted using a roll press to produce ribbons, which are milled in granules used further in the tableting process. The granule and tablet properties are influenced by the existence of different designs of the roll compactors, milling systems and the interaction between process parameters and raw material properties. The main objective of this work was to investigate how different roll-compaction conditions and milling process parameters impact on ribbons, granules and tablet properties, highlighting the role of the sealing system (cheek plates and rimmed roll). In this context, two common excipients differing in their mechanical behaviour (MCC and mannitol) are used. The study is based on the analysis of granule size distribution together with the characterization of loss of compactability during die compaction. Results show that the tensile strength of tablets is lower when using granules than when the raw materials are compressed. Moreover, the plastic material (MCC) is more sensitive than the brittle one (mannitol). Regarding the roll-force, it is observed that the higher the roll force, the lower the tensile strength of tablets from granulated material is. These findings are in agreement with the literature. The comparison of sealing systems shows that the rimmed-roll system leads to slightly stronger tablets than the use of cheek plates. In addition, the use of the rimmed-roll system reduces the amount of fines, in particular when high roll force is applied. Overall, it can be concluded that roll-compaction effect is predominant over the milling effect on the production of fines but less significant on the tablet properties. This study points out that the balance between a good flowability by reducing the amount of fines and appropriate tablet strength is achieved with rimmed-roll and the highest roll-force used. Copyright © 2016 Elsevier B.V. All rights reserved.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Chen, Hongmei, E-mail: hmchen@just.edu.cn; Zang, Qianhao; Yu, Hui
2015-08-15
Twin roll cast (designated as TRC in short) ZK60 magnesium alloy strip with 3.5 mm thickness was used in this paper. The TRC ZK60 strip was multi-pass rolled at different temperatures, intermediate annealing heat treatment was performed when the thickness of the strip changed from 3.5 mm to 1 mm, and then continued to be rolled until the thickness reached to 0.5 mm. The effect of intermediate annealing during rolling process on microstructure, texture and room temperature mechanical properties of TRC ZK60 strip was studied by using OM, TEM, XRD and electronic universal testing machine. The introduction of intermediate annealingmore » can contribute to recrystallization in the ZK60 sheet which was greatly deformed, and help to reduce the stress concentration generated in the rolling process. Microstructure uniformity and mechanical properties of the ZK60 alloy sheet were also improved; in particular, the room temperature elongation was greatly improved. When the TRC ZK60 strip was rolled at 300 °C and 350 °C, the room temperature elongation of the rolled sheet with 0.5 mm thickness which was intermediate annealed during the rolling process was increased by 95% and 72% than that of no intermediate annealing, respectively. - Highlights: • Intermediate annealing was introduced during hot rolling process of twin roll cast ZK60 alloy. • Intermediate annealing can contribute to recrystallization and reduce the stress concentration in the deformed ZK60 sheet. • Microstructure uniformity and mechanical properties of the ZK60 sheet were improved, in particular, the room temperature elongation. • The elongation of the rolled ZK60 sheet after intermediate annealed was increased by 95% and 72% than that of no intermediate annealing.« less
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Effect of differential speed rolling on the texture evolution of Mg-4Zn-1Gd alloy
NASA Astrophysics Data System (ADS)
Shim, Myeong-Shik; Suh, Byeong-Chan; Kim, Jae H.; Kim, Nack J.
2015-05-01
The microstructural and texture evolution during differential speed rolling process of Mg 4Zn-1Gd (wt%) alloy have been investigated by means of electron backscatter diffraction observation and texture analysis. The angular distribution of basal poles are inclined about 10° from the normal direction towards the rolling direction and the maximum intensities of basal poles are decreased, compared to the conventional rolling process. Such an inclination of angular distribution of basal poles can be induced by the operation of shear stress along the rolling direction, as much as one quarter of tensile stress along the RD and one quarter of compressive stress along the ND. When the reduction ratios in differential speed rolling increase, there is no difference in texture evolution although there is a significant change in activated twinning systems. In addition, the engineering stresses after differential speed rolling are also similar to that after conventional rolling process, while ductility and stretch formability in the former are worse than those in the latter.
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Non-Heat Treatable Alloy Sheet Products
DOE Office of Scientific and Technical Information (OSTI.GOV)
Hayden, H.W.; Barthold, G.W.; Das, S.K.
ALCAR is an innovative approach for conducting multi-company, pre-competitive research and development programs. ALCAR has been formed to crate a partnership of aluminum producers, the American Society of Mechanical Engineers Center for Research and Technology Development (ASME/CRTD), the United States Department of Energy (USDOE), three USDOE National Laboratories, and a Technical Advisory Committee for conducting cooperative, pre-competitive research on the development of flower-cost, non-heat treated (NHT) aluminum alloys for automotive sheet applications with strength, formability and surface appearance similar to current heat treated (HT) aluminum alloys under consideration. The effort has been supported by the USDOE, Office of Transportation Technologymore » (OTT) through a three-year program with 50/50 cost share at a total program cost of $3 million. The program has led to the development of new and modified 5000 series aluminum ally compositions. Pilot production-size ingots have bee n melted, cast, hot rolled and cold rolled. Stamping trials on samples of rolled product for demonstrating production of typical automotive components have been successful.« less
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NASA Astrophysics Data System (ADS)
Chang, Chih-Yuan; Tsai, Meng-Hsun
2015-12-01
This paper reports a highly effective method for the mass production of large-area plastic optical films with a microlens array pattern based on a continuous roll-to-roll film extrusion and roller embossing process. In this study, a thin steel mold with a micro-circular hole array pattern is fabricated by photolithography and a wet chemical etching process. The thin steel mold was then wrapped onto a metal cylinder to form an embossing roller mold. During the roll-to-roll process operation, a thermoplastic raw material (polycarbonate grains) was put into the barrel of the plastic extruder with a flat T-die. Then, the molten polymer film was extruded and immediately pressed against the surface of the embossing roller mold. Under the proper processing conditions, the molten polymer will just partially fill the micro-circular holes of the mold and due to surface tension form a convex lens surface. A continuous plastic optical film with a microlens array pattern was obtained. Experiments are carried out to investigate the effect of plastic microlens formation on the roll-to-roll process. Finally, the geometrical and optical properties of the fabricated plastic optical film were measured and proved satisfactory. This technique shows great potential for the mass production of large-area plastic optical films with a microlens array pattern.
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Vanadium Microalloyed High Strength Martensitic Steel Sheet for Hot-Dip Coating
NASA Astrophysics Data System (ADS)
Hutchinson, Bevis; Komenda, Jacek; Martin, David
Cold rolled steels with various vanadium and nitrogen levels have been treated to simulate the application of galvanizing and galvannealing to hardened martensitic microstructures. Strength levels were raised 100-150MPa by alloying with vanadium, which mitigates the effect of tempering. This opens the way for new ultra-high strength steels with corrosion resistant coatings produced by hot dip galvanising.
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Lubricating Coolant for Cold Rolling of Aluminum and Its Alloys,
The title fluid consists of a mixtures of alkyl esters of high molecular weight acids, an ester of xylitol and a C(subscript 6) or higher fatty acid...molecular weight acids 3-6, an ester of xylitol and a C(subscript 6) or higher fatty acid 1-3, an Al soap 0.3-1, a mineral oil 10-60, a polyoxyethylene
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Code of Federal Regulations, 2012 CFR
2012-07-01
... wastewaters. 2 Within the range of 6.0 to 9.0. (5) Fume scrubbers. Subpart I Pollutant or pollutant property... fume scrubber associated with a sulfuric acid pickling operation. (b) Hydrochloric acid pickling (spent... pickling wastewaters are treated with cold rolling wastewaters. 2 Within the range of 6.0 to 9.0. (4) Fume...
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Code of Federal Regulations, 2010 CFR
2010-07-01
... wastewaters. 2 Within the range of 6.0 to 9.0. (5) Fume scrubbers. Subpart I Pollutant or pollutant property... fume scrubber associated with a sulfuric acid pickling operation. (b) Hydrochloric acid pickling (spent... pickling wastewaters are treated with cold rolling wastewaters. 2 Within the range of 6.0 to 9.0. (4) Fume...
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Code of Federal Regulations, 2014 CFR
2014-07-01
... wastewaters. 2 Within the range of 6.0 to 9.0. (5) Fume scrubbers. Subpart I Pollutant or pollutant property... fume scrubber associated with a sulfuric acid pickling operation. (b) Hydrochloric acid pickling (spent... pickling wastewaters are treated with cold rolling wastewaters. 2 Within the range of 6.0 to 9.0. (4) Fume...
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Code of Federal Regulations, 2011 CFR
2011-07-01
... wastewaters. 2 Within the range of 6.0 to 9.0. (5) Fume scrubbers. Subpart I Pollutant or pollutant property... fume scrubber associated with a sulfuric acid pickling operation. (b) Hydrochloric acid pickling (spent... pickling wastewaters are treated with cold rolling wastewaters. 2 Within the range of 6.0 to 9.0. (4) Fume...
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Code of Federal Regulations, 2013 CFR
2013-07-01
... wastewaters. 2 Within the range of 6.0 to 9.0. (5) Fume scrubbers. Subpart I Pollutant or pollutant property... fume scrubber associated with a sulfuric acid pickling operation. (b) Hydrochloric acid pickling (spent... pickling wastewaters are treated with cold rolling wastewaters. 2 Within the range of 6.0 to 9.0. (4) Fume...
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40 CFR 420.106 - Pretreatment standards for new sources (PSNS).
Code of Federal Regulations, 2014 CFR
2014-07-01
... (pounds per 1,000 lb) of product Chromium 1 0.0000209 0.0000084 Lead 0.0000094 0.0000031 Nickel 1 0... limitations for chromium and nickel shall be applicable in lieu of those for lead and zinc when cold rolling... Chromium 1 0.0000418 0.0000167 Lead 0.0000188 0.0000063 Nickel 1 0.0000376 0.0000125 Zinc 0.0000125 0...
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40 CFR 420.106 - Pretreatment standards for new sources (PSNS).
Code of Federal Regulations, 2013 CFR
2013-07-01
... (pounds per 1,000 lb) of product Chromium 1 0.0000209 0.0000084 Lead 0.0000094 0.0000031 Nickel 1 0... limitations for chromium and nickel shall be applicable in lieu of those for lead and zinc when cold rolling... Chromium 1 0.0000418 0.0000167 Lead 0.0000188 0.0000063 Nickel 1 0.0000376 0.0000125 Zinc 0.0000125 0...
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40 CFR 420.106 - Pretreatment standards for new sources (PSNS).
Code of Federal Regulations, 2012 CFR
2012-07-01
... (pounds per 1,000 lb) of product Chromium 1 0.0000209 0.0000084 Lead 0.0000094 0.0000031 Nickel 1 0... limitations for chromium and nickel shall be applicable in lieu of those for lead and zinc when cold rolling... Chromium 1 0.0000418 0.0000167 Lead 0.0000188 0.0000063 Nickel 1 0.0000376 0.0000125 Zinc 0.0000125 0...
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DIMENSIONALLY STABLE, CORROSION RESISTANT NUCLEAR FUEL
Kittel, J.H.
1963-10-31
A method of making a uranium alloy of improved corrosion resistance and dimensional stability is described. The alloy contains from 0-9 weight per cent of an additive of zirconium and niobium in the proportions by weight of 5 to 1 1/ 2. The alloy is cold rolled, heated to two different temperatures, air-cooled, heated to a third temperature, and quenched in water. (AEC)
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40 CFR 420.106 - Pretreatment standards for new sources (PSNS).
Code of Federal Regulations, 2011 CFR
2011-07-01
... (pounds per 1,000 lb) of product Chromium 1 0.0000209 0.0000084 Lead 0.0000094 0.0000031 Nickel 1 0... limitations for chromium and nickel shall be applicable in lieu of those for lead and zinc when cold rolling... Chromium 1 0.0000418 0.0000167 Lead 0.0000188 0.0000063 Nickel 1 0.0000376 0.0000125 Zinc 0.0000125 0...
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40 CFR 420.106 - Pretreatment standards for new sources (PSNS).
Code of Federal Regulations, 2010 CFR
2010-07-01
... (pounds per 1,000 lb) of product Chromium 1 0.0000209 0.0000084 Lead 0.0000094 0.0000031 Nickel 1 0... limitations for chromium and nickel shall be applicable in lieu of those for lead and zinc when cold rolling... Chromium 1 0.0000418 0.0000167 Lead 0.0000188 0.0000063 Nickel 1 0.0000376 0.0000125 Zinc 0.0000125 0...
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Microstructure and Property Modifications of Cold Rolled IF Steel by Local Laser Annealing
NASA Astrophysics Data System (ADS)
Hallberg, Håkan; Adamski, Frédéric; Baïz, Sarah; Castelnau, Olivier
2017-10-01
Laser annealing experiments are performed on cold rolled IF steel whereby highly localized microstructure and property modification are achieved. The microstructure is seen to develop by strongly heterogeneous recrystallization to provide steep gradients, across the submillimeter scale, of grain size and crystallographic texture. Hardness mapping by microindentation is used to reveal the corresponding gradients in macroscopic properties. A 2D level set model of the microstructure development is established as a tool to further optimize the method and to investigate, for example, the development of grain size variations due to the strong and transient thermal gradient. Particular focus is given to the evolution of the beneficial γ-fiber texture during laser annealing. The simulations indicate that the influence of selective growth based on anisotropic grain boundary properties only has a minor effect on texture evolution compared to heterogeneous stored energy, temperature variations, and nucleation conditions. It is also shown that although the α-fiber has an initial frequency advantage, the higher probability of γ-nucleation, in combination with a higher stored energy driving force in this fiber, promotes a stronger presence of the γ-fiber as also observed in experiments.
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NASA Astrophysics Data System (ADS)
Suslova, A.; El-Atwani, O.; Sagapuram, D.; Harilal, S. S.; Hassanein, A.
2014-11-01
Tungsten has been chosen as the main candidate for plasma facing components (PFCs) due to its superior properties under extreme operating conditions in future nuclear fusion reactors such as ITER. One of the serious issues for PFCs is the high heat load during transient events such as ELMs and disruption in the reactor. Recrystallization and grain size growth in PFC materials caused by transients are undesirable changes in the material, since the isotropic microstructure developed after recrystallization exhibits a higher ductile-to-brittle transition temperature which increases with the grain size, a lower thermal shock fatigue resistance, a lower mechanical strength, and an increased surface roughening. The current work was focused on careful determination of the threshold parameters for surface recrystallization, grain growth rate, and thermal shock fatigue resistance under ELM-like transient heat events. Transient heat loads were simulated using long pulse laser beams for two different grades of ultrafine-grained tungsten. It was observed that cold rolled tungsten demonstrated better power handling capabilities and higher thermal stress fatigue resistance compared to severely deformed tungsten. Higher recrystallization threshold, slower grain growth, and lower degree of surface roughening were observed in the cold rolled tungsten.
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Microstructures and mechanical properties of duplex low carbon steel
NASA Astrophysics Data System (ADS)
Alfirano; Eben, U. S.; Hidayat, M.
2018-04-01
The microstructures behavior of duplex cold-rolled low carbon steel for automotive applications has been investigated. Intercritical annealing treatment is commonly used to develop a duplex low carbon steel containing ferrite and martensite. To get a duplex phase ferrite and martensite, the specimens were heated at inter-critical annealing temperature of 775°C - 825°C, for heating time up to 20 minutes, followed by water-quenched. The hardness of specimens was studied. The optical microscopy was used to analyze the microstructures. The optimal annealing conditions (martensite volume fraction approaching 20%) at 775°C with a heating time of 10 minutes was achieved. The highest hardness value was obtained in cold-rolled specimens of 41% in size reduction for intercritical annealing temperature of 825°C. In this condition, the hardness value was 373 HVN. The correlation between intercritical annealing temperature and time can be expressed in the transformation kinetics as fγ/fe = 1-exp(-Ktn) wherein K and n are grain growth rate constant and Avrami’s exponent, respectively. From experiment, the value of K = 0.15 and n = 0.461. Using the relationship between temperatures and heating time, activation energy (Q) can be calculated that is 267 kJ/mol.
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NASA Astrophysics Data System (ADS)
Huang, Hongfeng; Jiang, Feng; Zhou, Jiang; Wei, Lili; Qu, Jiping; Liu, Lele
2015-11-01
The mechanical properties and microstructures of Al-6Mg-0.25Sc-0.1Zr alloy (wt.%) during annealing were investigated by means of uniaxial tensile testing, optical microscope, scanning electron microscope, transmission electron microscope, and high-resolution transmission electron microscope. The results show that a large number of micro and grain-scale shear bands form in this alloy after cold rolling. As the tensile-loading force rises, strain softening would generate in shear bands, resulting in the occurrence of shear banding fracture in cold-rolled Al-Mg-Sc-Zr alloys. Recrystallization takes place preferentially in shear bands during annealing. Due to the formation of coarse-grain bands constructed by new subgrains, recrystallization softening tends to occur in these regions. During low-temperature annealing, recrystallization is inhibited by nano-scale Al3(Sc,Zr) precipitates which exert significant coherency strengthening and modulus hardening. However, the strengthening effect of Al3(Sc,Zr) decreases with the increasing of particle diameter at elevated annealing temperature. The mechanical properties of the recrystallized Al-Mg-Sc-Zr alloy decrease to a minimum level, and the fracture plane exhibits pure ductile fracture characteristics.
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Singhbabu, Y N; Sivakumar, B; Singh, J K; Bapari, H; Pramanick, A K; Sahu, Ranjan K
2015-05-07
We report the production of an efficient anti-corrosive coating of cold-rolled (CR) steel in a seawater environment (∼3.5 wt% NaCl aqueous solution) using an oil-based graphene oxide ink. The graphene oxide was produced by heating Aeschynomene aspera plant as a carbon source at 1600 °C in an argon atmosphere. The ink was prepared by cup-milling the mixture of graphene oxide and sunflower oil for 10 min. The coating of ink on the CR steel was made using the dip-coating method, followed by curing at 350 °C for 10 min in air atmosphere. The results of the potentiodynamic polarization show that the corrosion rate of bare CR steel decreases nearly 10,000-fold by the ink coating. Furthermore, the salt spray test results show that the red rusting in the ink-coated CR steel is initiated after 100 h, in contrast to 24 h and 6 h in the case of oil-coated and bare CR steel, respectively. The significant decrease in the corrosion rate by the ink-coating is discussed based on the impermeability of graphene oxide to the corrosive ions.
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Suslova, A.; El-Atwani, O.; Sagapuram, D.; Harilal, S. S.; Hassanein, A.
2014-01-01
Tungsten has been chosen as the main candidate for plasma facing components (PFCs) due to its superior properties under extreme operating conditions in future nuclear fusion reactors such as ITER. One of the serious issues for PFCs is the high heat load during transient events such as ELMs and disruption in the reactor. Recrystallization and grain size growth in PFC materials caused by transients are undesirable changes in the material, since the isotropic microstructure developed after recrystallization exhibits a higher ductile-to-brittle transition temperature which increases with the grain size, a lower thermal shock fatigue resistance, a lower mechanical strength, and an increased surface roughening. The current work was focused on careful determination of the threshold parameters for surface recrystallization, grain growth rate, and thermal shock fatigue resistance under ELM-like transient heat events. Transient heat loads were simulated using long pulse laser beams for two different grades of ultrafine-grained tungsten. It was observed that cold rolled tungsten demonstrated better power handling capabilities and higher thermal stress fatigue resistance compared to severely deformed tungsten. Higher recrystallization threshold, slower grain growth, and lower degree of surface roughening were observed in the cold rolled tungsten. PMID:25366885
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Suslova, A; El-Atwani, O; Sagapuram, D; Harilal, S S; Hassanein, A
2014-11-04
Tungsten has been chosen as the main candidate for plasma facing components (PFCs) due to its superior properties under extreme operating conditions in future nuclear fusion reactors such as ITER. One of the serious issues for PFCs is the high heat load during transient events such as ELMs and disruption in the reactor. Recrystallization and grain size growth in PFC materials caused by transients are undesirable changes in the material, since the isotropic microstructure developed after recrystallization exhibits a higher ductile-to-brittle transition temperature which increases with the grain size, a lower thermal shock fatigue resistance, a lower mechanical strength, and an increased surface roughening. The current work was focused on careful determination of the threshold parameters for surface recrystallization, grain growth rate, and thermal shock fatigue resistance under ELM-like transient heat events. Transient heat loads were simulated using long pulse laser beams for two different grades of ultrafine-grained tungsten. It was observed that cold rolled tungsten demonstrated better power handling capabilities and higher thermal stress fatigue resistance compared to severely deformed tungsten. Higher recrystallization threshold, slower grain growth, and lower degree of surface roughening were observed in the cold rolled tungsten.
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Advances in roll to roll processing of optics
NASA Astrophysics Data System (ADS)
Watts, Michael P. C.
2008-02-01
Today, there are a number of successful commercial applications that utilize roll to roll processing and almost all involve optics; unpatterned film, patterned film, and devices on film. The largest applications today are in holograms, and brightness enhancement film (BEF) for LCD. Solar cells are rapidly growing. These are mostly made in large captive facilities with their own proprietary equipment, materials and pattern generation capability. World wide roll to roll volume is > 100M meters2 year -1, and generates sales of > $5B. The vast majority of the sales are in BEF film by 3M.
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NASA Astrophysics Data System (ADS)
Isaenkova, M.; Perlovich, Yu.; Fesenko, V.; Babich, Y.; Zaripova, M.; Krapivka, N.
2018-05-01
The paper presents the results of investigation of the regularities of the structure and texture formation during rolling of single crystals of Zr-25%Nb alloy differing in their initial orientations relative to the external principal directions in the rolled plate: normal (ND) and rolling directions (RD). The features of rolled single crystals with initial orientations of planes {001}, {011} or {111} parallel to the rolling plane and different crystallographic directions along RD are considered. A comparison of the peculiarities of plastic deformation in a polycrystalline alloy of the same composition is made. For the samples studied, a decrease in the lattice parameter of the β-phase has been recorded, the minimum of the parameter being observed for different degrees of deformation, varying from 20 to 50%. Observed decrease in the unit cell parameter can be connected with the precipitation of the α(α')-Zr phase from the deformed nonequilibrium β-phase of the Zr-25%Nb alloy, i.e. change in the composition of the solid solution. Distributions of the increase in the dimensions of the deformed single crystal along RD and the transverse direction (TD) with its deformation up to 30% in thickness, which indicate the anisotropy of the plasticity of single crystals during their rolling, are constructed on stereographic projection. It is shown, that the deformation of single crystals occurs practically without increasing of their dimensions in the <110> direction with a total thickness deformation of up to 30%. Direction <110> is characterized by maximum hardening (microhardness) with indentation along it, which causes low plasticity of deformed and annealed foils from Zr-25%Nb alloy at the stretching along and across RD, that is connected with the features of their crystallographic texture.
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Evolution of microstructure and residual stress during annealing of austenitic and ferritic steels
DOE Office of Scientific and Technical Information (OSTI.GOV)
Wawszczak, R.; Baczmański, A., E-mail: Andrzej.Baczmanski@fis.agh.edu.pl; Marciszko, M.
2016-02-15
In this work the recovery and recrystallization processes occurring in ferritic and austenitic steels were studied. To determine the evolution of residual stresses during material annealing the nonlinear sin{sup 2}ψ diffraction method was used and an important relaxation of the macrostresses as well as the microstresses was found in the cold rolled samples subjected to heat treatment. Such relaxation occurs at the beginning of recovery, when any changes of microstructure cannot be detected using other experimental techniques. Stress evolution in the annealed steel samples was correlated with the progress of recovery process, which significantly depends on the value of stackingmore » fault energy. - Highlights: • X-ray diffraction was used to determine the first order and second order stresses. • Diffraction data were analyzed using scale transition elastoplastic models model. • Stress relaxation in annealed ferritic and austenitic steels was correlated with evolution of microstructure. • Influence of stacking fault energy on thermally induced processes was discussed.« less
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Rolling contact fatigue of low hardness steel for slewing ring application
NASA Astrophysics Data System (ADS)
Knuth, Jason A.
This thesis discusses the rolling contact fatigue of steel utilized in anti-friction bearings, also referred to as slewing bearings. These slewing bearings are utilized in cranes, excavators, wind turbines and other similar applications. Five materials composed of two different material types were tested. The two material types were high carbon steel and medium carbon alloy steel. The test specimens were processed from forged rolled rings. Two machines were evaluated a ZF-RCF and 3-Ball test machine. The evaluation was to determine which machine can best simulate the application in which the slewing bearing is utilized. Initially, each specimen will be pretested to determine the appropriate testing direction from within the forged rolled rings. Pretesting is needed in order to establish consistent failure modes between samples. The primary goal of the test is to understand the life differences and failure modes between high carbon steel and medium carbon alloy steel. The high carbon steel ring was cut into two sections, one of which was stress relieved and the other was quenched and tempered. The medium carbon alloy steel was cut into three sections, all of which were quenched and tempered to different hardness levels. The test program was dynamically adjusted based upon the previous sample's life and load. An S-N curve was then established from the 5 materials tested at two target loads. The samples were run until the first sign of a crack was detected by an eddy current. At the completion of the rolling contact test, select sample's microstructure was evaluated for crack initiation location. The selected samples were divided into four groups which represent different maximum shear stress levels. These samples displayed indications of material deformation in which the high carbon steel experienced an increased amount of cold work when compared to medium carbon alloy steel. The life of the high carbon steel was nearly equivalent to the expected life of the medium carbon alloy. The work hardening of the high carbon steel increased the surface hardness that exceeded the medium carbon alloy steel surface hardness.
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Analytical study on web deformation by tension in roll-to-roll printing process
NASA Astrophysics Data System (ADS)
Kang, Y. S.; Hong, M. S.; Lee, S. H.; Jeon, Y. H.; Kang, D.; Lee, N. K.; Lee, M. G.
2017-08-01
Recently, flexible devices have gained high intentions for flexible display, Radio Frequency Identification (RFID), bio-sensor and so on. For manufacturing of the flexible devices, roll-to-roll process is a good candidate because of its low production cost and high productivity. Flexible substrate has a non-uniform deformation distribution by tension. Because the roll-to-roll process carries out a number of overlay printing processes, the deformation affect overlay printing precision and printable areas. In this study, the deformation of flexible substrate was analyzed by using finite element analysis and it was verified through experiments. More deformation occurred in the middle region in the direction parallel to rolling of the flexible substrate. It is confirmed through experiments and analysis that deformation occurs less at the both ends than in the middle region. Based on these results, a hourglass roll is proposed as a mechanical design of the roll to compensate the non-uniform deformation of the flexible substrate. In the hourglass roll, high stiffness material is used in the core and low stiffness material such as an elastic material is wrapped. The diameter of the core roll was designed to be the minimum at the middle and the maximum at both ends. We tried to compensate the non-uniform deformation distribution of the flexible substrate by using the variation of the contact stiffness between the roll and the flexible substrate. Deformation distribution of flexible substrates was confirmed by finite element analysis by applying hourglass roll shape. In the analysis when using the hourglass roll, it is confirmed that the stress distribution is compensated by about 70% and the strain distribution is compensated by about 67% compared to the case using the hourglass roll. To verify the compensation of the non-uniform deformation distribution due to the tension, deformation measurement experiment when using the proposed hourglass roll was carried out. Experiments have shown that the distribution of deformation is compensated by about 34%. From the results, we verified the performance of the proposed.
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Multi-stage FE simulation of hot ring rolling
NASA Astrophysics Data System (ADS)
Wang, C.; Geijselaers, H. J. M.; van den Boogaard, A. H.
2013-05-01
As a unique and important member of the metal forming family, ring rolling provides a cost effective process route to manufacture seamless rings. Applications of ring rolling cover a wide range of products in aerospace, automotive and civil engineering industries [1]. Above the recrystallization temperature of the material, hot ring rolling begins with the upsetting of the billet cut from raw stock. Next a punch pierces the hot upset billet to form a hole through the billet. This billet, referred to as preform, is then rolled by the ring rolling mill. For an accurate simulation of hot ring rolling, it is crucial to include the deformations, stresses and strains from the upsetting and piercing process as initial conditions for the rolling stage. In this work, multi-stage FE simulations of hot ring rolling process were performed by mapping the local deformation state of the workpiece from one step to the next one. The simulations of upsetting and piercing stages were carried out by 2D axisymmetric models using adaptive remeshing and element erosion. The workpiece for the ring rolling stage was subsequently obtained after performing a 2D to 3D mapping. The commercial FE package LS-DYNA was used for the study and user defined subroutines were implemented to complete the control algorithm. The simulation results were analyzed and also compared with those from the single-stage FE model of hot ring rolling.
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NASA Astrophysics Data System (ADS)
Hadadzadeh, Amir; Wells, Mary
Although the Twin Roll Casting (TRC) process has been used in the aluminum sheet production industry for more than 60 years, the usage of this process to fabricate magnesium sheets is still at its early stages. Similar to other manufacturing processes, the development of the TRC process for magnesium alloys has followed a typical route of preliminary studies using a laboratory-scale facility, followed by pilot-scale testing and most recently attempting to use an industrial-scale twin roll caster. A powerful tool to understand and quantify the trends of the processing conditions and effects of scaling up from a laboratory size TRC machine to an industrial scale one is develop a mathematical model of the process. This can elucidate the coupled fluid-thermo-mechanical behavior of the cast strip during the solidification and then deformation stages of the process. In the present study a Thermal-Fluid-Stress model has been developed for TRC of AZ31 magnesium alloy for three roll diameters by employing the FEM commercial package ALSIM. The roll diameters were chosen as 355mm, 600mm and 1150mm. The effect of casting speed for each diameter was studied in terms of fluid flow, thermal history and stress-strain evolution in the cast strip in the roll bite region.
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Manufacturing Demonstration Facility: Roll-to-Roll Processing
DOE Office of Scientific and Technical Information (OSTI.GOV)
Datskos, Panos G; Joshi, Pooran C; List III, Frederick Alyious
This Manufacturing Demonstration Facility (MDF)e roll-to-roll processing effort described in this report provided an excellent opportunity to investigate a number of advanced manufacturing approaches to achieve a path for low cost devices and sensors. Critical to this effort is the ability to deposit thin films at low temperatures using nanomaterials derived from nanofermentation. The overarching goal of this project was to develop roll-to-roll manufacturing processes of thin film deposition on low-cost flexible substrates for electronics and sensor applications. This project utilized ORNL s unique Pulse Thermal Processing (PTP) technologies coupled with non-vacuum low temperature deposition techniques, ORNL s clean roommore » facility, slot dye coating, drop casting, spin coating, screen printing and several other equipment including a Dimatix ink jet printer and a large-scale Kyocera ink jet printer. The roll-to-roll processing project had three main tasks: 1) develop and demonstrate zinc-Zn based opto-electronic sensors using low cost nanoparticulate structures manufactured in a related MDF Project using nanofermentation techniques, 2) evaluate the use of silver based conductive inks developed by project partner NovaCentrix for electronic device fabrication, and 3) demonstrate a suite of low cost printed sensors developed using non-vacuum deposition techniques which involved the integration of metal and semiconductor layers to establish a diverse sensor platform technology.« less
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NASA Astrophysics Data System (ADS)
Pesin, A.; Pustovoytov, D.; Shveyova, T.; Vafin, R.
2017-12-01
The level of a shear strain and equivalent strain plays a key role in terms of the possibility of using the asymmetric rolling process as a method of severe plastic deformation. Strain mode (pure shear or simple shear) can affect very strongly on the equivalent strain and the grain refinement of the material. This paper presents the results of FEM simulations and comparison of the equivalent strain in the aluminium alloy 5083 processed by a single-pass equal channel angular pressing (simple shear), symmetric rolling (pure shear) and asymmetric rolling (simultaneous pure and simple shear). The nonlinear effect of rolls speed ratio on the deformation characteristics during asymmetric rolling was found. Extremely high equivalent strain up to e=4.2 was reached during a single-pass asymmetric rolling. The influence of the shear strain on the level of equivalent strain is discussed. Finite element analysis of the deformation characteristics, presented in this study, can be used for optimization of the asymmetric rolling process as a method of severe plastic deformation.
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NASA Technical Reports Server (NTRS)
Hamrock, B. J.; Anderson, W. J.
1983-01-01
Rolling element bearings are a precision, yet simple, machine element of great utility. A brief history of rolling element bearings is reviewed and the type of rolling element bearings, their geometry and kinematics, as well as the materials they are made from and the manufacturing processes they involve are described. Unloaded and unlubricated rolling element bearings, loaded but unlubricated rolling element bearings and loaded and lubricated rolling element bearings are considered. The recognition and understanding of elastohydrodynamic lubrication covered, represents one of the major development in rolling element bearings.
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Defect Analysis of Roll-to-Roll SAIL Manufactured Flexible Display Backplanes
2011-01-01
tenting defect through the SAIL process Figure 5: Flexible backplane electrical tester Figure 6: R2R optical inspection system Figure 7: TEM of TFT ...Analysis of Roll-to-Roll SAIL Manufactured Flexible Display...Marcia Almanza-Workman, Robert A. Garcia, HanJun Kim, Ohseung Kwon, Frank Jeffrey HP Laboratories HPL-2011-35 SAIL, flexible displays, roll-to-roll HP
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Grain-Structure Development in Heavily Cold-Rolled Alpha-Titanium (Postprint)
2014-04-01
H.P. Lee, C. Esling , H.J. Bunge, Textures Microstruct. 7 (1988) 317–337. [10] S. Nourbakhsh, T.D. O’Brien, Mater. Sci. Eng. 100 (1988) 109–114. [11...2010) 4536–4548. [20] Y. Zhong, F. Yin, K. Nagai, J. Mater. Res. 23 (2008) 2954–2966. [21] M.J. Philippe, M. Serghat, P. Van Houtte, C. Esling , Acta
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1974-12-01
Breakfast Cereals 11 Griddle Cakes 12 Eggs 13 Breakfast Meats Arm®d Forces High Preference and Low Preference Foods HIGH Tom. Veg. Noodle Soup...Tomato Soup Chicken Noodle Soup Orange Juice Grape Juice Lemonade Iced Tea Milk Ice Cream Cola Doughnuts Sweet Rolls Cold Cereal Griddle...Grape Lemonade Lime-Flavored Drink Cherry-Flavored Drink Instant Coffee Freeze-Dried Coffee Skimmed Milk Buttermilk Frutt-Flvd. Yogurt Lo-cal
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High-Throughput Printing Process for Flexible Electronics
NASA Astrophysics Data System (ADS)
Hyun, Woo Jin
Printed electronics is an emerging field for manufacturing electronic devices with low cost and minimal material waste for a variety of applications including displays, distributed sensing, smart packaging, and energy management. Moreover, its compatibility with roll-to-roll production formats and flexible substrates is desirable for continuous, high-throughput production of flexible electronics. Despite the promise, however, the roll-to-roll production of printed electronics is quite challenging due to web movement hindering accurate ink registration and high-fidelity printing. In this talk, I will present a promising strategy for roll-to-roll production using a novel printing process that we term SCALE (Self-aligned Capillarity-Assisted Lithography for Electronics). By utilizing capillarity of liquid inks on nano/micro-structured substrates, the SCALE process facilitates high-resolution and self-aligned patterning of electrically functional inks with greatly improved printing tolerance. I will show the fabrication of key building blocks (e.g. transistor, resistor, capacitor) for electronic circuits using the SCALE process on plastics.
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NASA Astrophysics Data System (ADS)
Gatti, J. R.; Bhattacharjee, P. P.
2014-12-01
Evolution of microstructure and texture during severe deformation and annealing was studied in Al-2.5%Mg alloy processed by two different routes, namely, monotonic Accumulative Roll Bonding (ARB) and a hybrid route combining ARB and conventional rolling (CR). For this purpose Al-2.5%Mg sheets were subjected to 5 cycles of monotonic ARB (equivalent strain (ɛeq) = 4.0) processing while in the hybrid route (ARB + CR) 3 cycle ARB-processed sheets were further deformed by conventional rolling to 75% reduction in thickness (ɛeq = 4.0). Although formation of ultrafine structure was observed in the two processing routes, the monotonic ARB—processed material showed finer microstructure but weak texture as compared to the ARB + CR—processed material. After complete recrystallization, the ARB + CR-processed material showed weak cube texture ({001}<100>) but the cube component was almost negligible in the monotonic ARB-processed material-processed material. However, the ND-rotated cube components were stronger in the monotonic ARB-processed material-processed material. The observed differences in the microstructure and texture evolution during deformation and annealing could be explained by the characteristic differences of the two processing routes.
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Computer-aided roll pass design in rolling of airfoil shapes
NASA Technical Reports Server (NTRS)
Akgerman, N.; Lahoti, G. D.; Altan, T.
1980-01-01
This paper describes two computer-aided design (CAD) programs developed for modeling the shape rolling process for airfoil sections. The first program, SHPROL, uses a modular upper-bound method of analysis and predicts the lateral spread, elongation, and roll torque. The second program, ROLPAS, predicts the stresses, roll separating force, the roll torque and the details of metal flow by simulating the rolling process, using the slab method of analysis. ROLPAS is an interactive program; it offers graphic display capabilities and allows the user to interact with the computer via a keyboard, CRT, and a light pen. The accuracy of the computerized models was evaluated by (a) rolling a selected airfoil shape at room temperature from 1018 steel and isothermally at high temperature from Ti-6Al-4V, and (b) comparing the experimental results with computer predictions. The comparisons indicated that the CAD systems, described here, are useful for practical engineering purposes and can be utilized in roll pass design and analysis for airfoil and similar shapes.
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Microstructure Evolution During Creep of Cold Worked Austenitic Stainless Steel
NASA Astrophysics Data System (ADS)
Krishan Yadav, Hari; Ballal, A. R.; Thawre, M. M.; Vijayanand, V. D.
2018-04-01
The 14Cr–15Ni austenitic stainless steel (SS) with additions of Ti, Si, and P has been developed for their superior creep strength and better resistance to void swelling during service as nuclear fuel clad and wrapper material. Cold working induces defects such as dislocations that interact with point defects generated by neutron irradiation and facilitates recombination to make the material more resistant to void swelling. In present investigation, creep properties of the SS in mill annealed condition (CW0) and 40 % cold worked (CW4) condition were studied. D9I stainless steel was solution treated at 1333 K for 30 minutes followed by cold rolling. Uniaxial creep tests were performed at 973 K for various stress levels ranging from 175-225 MPa. CW4 samples exhibited better creep resistance as compared to CW0 samples. During creep exposure, cold worked material exhibited phenomena of recovery and recrystallization wherein new strain free grains were observed with lesser dislocation network. In contrast CW0 samples showed no signs of recovery and recrystallization after creep exposure. Partial recrystallization on creep exposure led to higher drop in hardness in cold worked sample as compared to that in mill annealed sample. Accelerated precipitation of carbides at the grain boundaries was observed during creep exposure and this phenomenon was more pronounced in cold worked sample.
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Yi, Hoon; Hwang, Insol; Lee, Jeong Hyeon; Lee, Dael; Lim, Haneol; Tahk, Dongha; Sung, Minho; Bae, Won-Gyu; Choi, Se-Jin; Kwak, Moon Kyu; Jeong, Hoon Eui
2014-08-27
A simple yet scalable strategy for fabricating dry adhesives with mushroom-shaped micropillars is achieved by a combination of the roll-to-roll process and modulated UV-curable elastic poly(urethane acrylate) (e-PUA) resin. The e-PUA combines the major benefits of commercial PUA and poly(dimethylsiloxane) (PDMS). It not only can be cured within a few seconds like commercial PUA but also possesses good mechanical properties comparable to those of PDMS. A roll-type fabrication system equipped with a rollable mold and a UV exposure unit is also developed for the continuous process. By integrating the roll-to-roll process with the e-PUA, dry adhesives with spatulate tips in the form of a thin flexible film can be generated in a highly continuous and scalable manner. The fabricated dry adhesives with mushroom-shaped microstructures exhibit a strong pull-off strength of up to ∼38.7 N cm(-2) on the glass surface as well as high durability without any noticeable degradation. Furthermore, an automated substrate transportation system equipped with the dry adhesives can transport a 300 mm Si wafer over 10,000 repeating cycles with high accuracy.
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NASA Astrophysics Data System (ADS)
Si, Lina; Guo, Dan; Luo, Jianbin; Lu, Xinchun; Xie, Guoxin
2011-04-01
In an abrasive chemical mechanical polishing (CMP) process, materials were considered to be removed by abrasive sliding and rolling. Abrasive sliding has been investigated by many molecular dynamics (MD) studies; while abrasive rolling was usually considered to be negligible and therefore was rarely investigated. In this paper, an MD simulation was used to study the effects of abrasive rolling on material removal and surface finish in the CMP process. As the silica particle rolled across the silicon substrate, some atoms of the substrate were dragged out from their original positions and adhered to the silica particle, leaving some atomic vacancies on the substrate surface. Meanwhile, a high quality surface could be obtained. During the abrasive rolling process, the influencing factors of material removal, e.g., external down force and driving force, were also discussed. Finally, MD simulations were carried out to examine the effects of abrasive sliding on material removal under the same external down force as abrasive rolling. The results showed that the ability of abrasive rolling to remove material on the atomic scale was not notably inferior to that of abrasive sliding. Therefore, it can be proposed that both abrasive sliding and rolling play important roles in material removal in the abrasive CMP of the silicon substrate.
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NASA Astrophysics Data System (ADS)
Boehlert, C. J.; Dickmann, D. S.; Eisinger, Ny. N. C.
2006-01-01
The grain size, grain boundary character distribution (GBCD), creep, and tensile behavior of INCONEL alloy 718 (IN 718) were characterized to identify processing-microstructure-property relationships. The alloy was sequentially cold rolled (CR) to 0, 10, 20, 30, 40, 60, and 80 pct followed by annealing at temperatures between 954 °C and 1050 °C and the traditional aging schedule used for this alloy. In addition, this alloy can be superplastically formed (IN 718SPF) to a significantly finer grain size and the corresponding microstructure and mechanical behavior were evaluated. The creep behavior was evaluated in the applied stress (σ a ) range of 300 to 758 MPa and the temperature range of 638 °C to 670 °C. Constant-load tensile creep experiments were used to measure the values of the steady-state creep rate and the consecutive load reduction method was used to determine the values of backstress (σ0). The values for the effective stress exponent and activation energy suggested that the transition between the rate-controlling creep mechanisms was dependent on effective stresses (σ e =σ a σ0) and the transition occurred at σ e ≅ 135 MPa. The 10 to 40 pct CR samples exhibited the greatest 650 °C strength, while IN 718SPF exhibited the greatest room-temperature (RT) tensile strength (>1550 MPa) and ductility (ɛ f >16 pct). After the 954 °C annealing treatment, the 20 pct CR and 30 pct CR microstructures exhibited the most attractive combination of elevated-temperature tensile and creep strength, while the most severely cold-rolled materials exhibited the poorest elevated-temperature properties. After the 1050 °C annealing treatment, the IN 718SPF material exhibited the greatest backstress and best creep resistance. Electron backscattered diffraction was performed to identify the GBCD as a function of CR and annealing. The data indicated that annealing above 1010 °C increased the grain size and resulted in a greater fraction of twin boundaries, which in turn increased the fraction of coincident site lattice boundaries. This result is discussed in light of the potential to grain boundary engineer this alloy.
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5. VIEW OF BERYLLIUM PROCESSING AREA, ROLLING MILL. BERYLLIUM FORMING ...
5. VIEW OF BERYLLIUM PROCESSING AREA, ROLLING MILL. BERYLLIUM FORMING BEGAN IN SIDE A OF THE BUILDING IN 1962. (11/5/73) - Rocky Flats Plant, Uranium Rolling & Forming Operations, Southeast section of plant, southeast quadrant of intersection of Central Avenue & Eighth Street, Golden, Jefferson County, CO
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Promising Sparingly Alloyed Boron-Bearing Steels for the Production of High-Strength Fasteners
NASA Astrophysics Data System (ADS)
Bobylev, M. V.; Koroleva, E. G.; Shtannikov, P. A.
2005-05-01
The main advantages of boron-bearing steels used for production of rolled sections at cold upset shops of Russian automotive plants are considered. A thermodynamic model for the majority of boron-bearing steels for high-strength fasteners is used to plot nomograms characterizing the effect of titanium, aluminum, nitrogen, and boron on the amount of nitrides and oxides segregated in crystallization and on the content of effective boron. The effect of effective boron on the characteristics of hardenability is estimated. The studies conducted are used for determining the range of permissible contents of titanium and aluminum ensuring through hardenability of rolled bars from steels 12G1R, 20G2R, and 30G1R up to 25 mm in diameter.
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NASA Astrophysics Data System (ADS)
Naizabekov, Abdrakhman; Lezhnev, Sergey; Arbuz, Alexandr; Panin, Evgeniy
2018-02-01
Ultrafine-grained materials are one of the most promising structural and functional materials. However, the known methods of obtaining them are not enough powerful and technologically advanced for profitable industrial applications. Development of the combined process "helical rolling-pressing" is an attempt to bring technology to produce ultrafine-grained materials to the industry. The combination of intense processing of the surface by helical rolling and the entire cross section of workpiece in equal channel angular matrix, with intense deformation by torsion between rolls and matrix will increase the degree of deformation per pass and allows to mutually compensate disadvantages of these methods in the case of their separate use. This paper describes the development of a laboratory stand and study of influence of combined process "helical rolling-pressing"on the microstructure of tool steel, technical copper and high alloy stainless high-temperature steel.
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Behavior of sheets from Ti-alloys by rolling and heat treatment
NASA Astrophysics Data System (ADS)
Isaenkova, M.; Perlovich, Yu.; Fesenko, V.; Gritskevich, M.; Stolbov, S.; Zaripova, M.
2017-10-01
Sheets from single- and two-phase Ti-alloys (VT1-0, Ti-22Nb-9%Zr and VT-16) were rolled at the room temperature up to various deformation degrees and annealed at temperatures 500-900 °C. The regularities of texture formation in both phases were established. In the technically pure Ti (VT1-0) with the single α-Ti phase the final stable texture component is (0001)±30-40°ND-TD<101 ¯0>. In the two-phase alloy the reorientation of basal axes of α-Ti occurs by the same trajectories as in the single phase alloy. However, in the case of two-phase alloy texture development in α-Ti stops at the intermediate stage, when this texture consists of components with rolling planes (0001)±15-20°ND-RD and (0001)±30-40°ND-TD. The stability of the first components can be provided both by the mutually balanced operation of pyramidal and basal slip systems, activity of which remains at the high deformation degree of two-phase alloy, and by the dynamic α↔β phase transformations, taking place in the distorted structures of α- and β-phases in the course of its cold rolling. At recrystallization of technically pure Ti the basal component disappears in its texture. At the same time, prismatic axes turn by angles 20÷30° depending on the heating rate of the rolled sheet and annealing temperature. At recrystallization of the two-phase Ti-alloy prismatic axes of its α-grains doesn't turn relative to their positions in the rolling texture, as it occurs in the single-phase alloy. This fact indicates to some alternative mode of arising new recrystallized grains in two-phase alloys.
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2009-10-01
cryostat and cooled at a temperature under 77K by a Stirling cryocooler , as represented on the following Figure 5 : Cryostat...Figure 5. Detector cryostat and cryocooler The read-out frequency of the detectors is adapted to the ground speed of the plane above...Cold shield Detector plane Cryocoole r Cryocoole r compresso r Fixed frame Roll frame Pitch frame Yaw frame SIELETERS: a Static Fourier
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Crack Growth in Mercury Embrittled Aluminum Alloys under Cyclic and Static Loading Conditions
1983-03-01
STATEMENT (ol the abalract entered In Block 20, It dlHerent from Report) 18. SUPPLEMENTARY NOTES This was a thesis in partial fulfillment of...argued that the strengthening that occurs from cold rolling suppresses crack nucleation at the surface under monotonlc loading. Under cyclic loading...precracking. Copper was chosen because It can be easily electrodeposited on aluminum, easily wet with mercury, and remains wet almost indefinitely
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The Effects of Carbon Nanotube Reinforcement on Adhesive Joints for Naval Applications
2009-12-01
ACRONYMS AND ABBREVIATIONS CNT Carbon Nanotube CoNap Cobalt Naphthenate DMA Dimethylaniline IR Infared MEKP Methyl Ethyl Ketone Peroxide... removed prior to use. The selection of cold rolled steel significantly reduced the surface preparation required for each sample. The steel was one...6% Cobalt Naphthenate (CoNap), as well as an accelerator, dimethylaniline (DMA), can be varied to control gel time of the resign based on ambient
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Unsupported palladium alloy membranes and methods of making same
Way, J. Douglas; Thoen, Paul; Gade, Sabina K.
2015-06-02
The invention provides support-free palladium membranes and methods of making these membranes. Single-gas testing of the unsupported foils produced hydrogen permeabilities equivalent to thicker membranes produced by cold-rolling. Defect-free films as thin as 7.2 microns can be fabricated, with ideal H.sub.2/N.sub.2 selectivities as high as 40,000. Homogeneous membrane compositions may also be produced using these methods.
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Development of Highly Ductile Spheroidized Steel from High C (0.61 wt.% C) Low-Alloy Steel
NASA Astrophysics Data System (ADS)
Monia, S.; Varshney, A.; Gouthama; Sangal, S.; Kundu, S.; Samanta, S.; Mondal, K.
2015-11-01
This research aims to develop a multiphase steel combining spheroidal cementite and bainite in ductile ferrite matrix possessing an optimal balance of reasonably high strength and excellent ductility. A high carbon (0.61 wt.%) high silicon (1.71 wt.%) EN45 spring steel was annealed to obtain ferrite pearlite microstructure. The samples were given 5 and 10% cold rolling followed by holding at temperature below Ac1 for about 3 h. The samples were then held in intercritical range at 770 °C temperature for different durations ranging from 5 to 20 min for partial re-austenitization followed by quenching in a salt bath maintained at 350 °C and holding for 10 min to get bainite. The samples were finally water quenched. Characterizations of the samples with the help of optical microscopy, x-ray diffraction, scanning electron microscopy, and atomic force microscopy were carried out. Optimal heat-treatment conditions were found out after correlating with tensile properties. The best combination of high tensile strength (~800 MPa) with very high elongation (~29%) was obtained. Effects of cold-rolled strain and holding time in the intercritical region on the mechanical properties and microstructural changes were studied. Finally, structural property correlation is established.
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Elastic-Plastic Behavior of U6Nb Under Ramp Wave Loading
NASA Astrophysics Data System (ADS)
Hayes, D. B.; Hall, C.; Hixson, R. S.
2005-07-01
Prior shock experiments on the alloy uranium-niobium-6 wt.% (U6Nb) were absent an elastic precursor when one was expected (A. K. Zurek, et. al., Journal de Physique IV, 10 (#9) p677-682). This was later explained as a consequence of shear stress relaxation from time-dependent twinning that prevented sufficient shear stress for plastic yielding. (D. B. Hayes, et. al., Shock Compression of Condensed Matter-2003, p1177, American Institute of Physics 2004) Pressure was ramped to 13 GPa in 150-ns on eight U6Nb specimens with thicknesses from 0.5 -- 1.1-mm and the back surface velocities were measured with laser interferometry. This pressure load produces a stress wave with sufficiently fast rise time so that, according to the prior work, twins do not have time to form. Four of the U6Nb specimens had been cold-rolled which increased the yield stress. Each velocity history was analyzed with a backward integration analysis to give the stress-strain response of the U6Nb. Comparison of these results with prior Hugoniot measurements shows that the U6Nb in the present experiments responds as an elastic-plastic material and the deduced yield strength of the baseline and of the cold-rolled material agree with static results.
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Retaining {1 0 0} texture from initial columnar grains in 6.5 wt% Si electrical steels
NASA Astrophysics Data System (ADS)
Liang, Ruiyang; Yang, Ping; Mao, Weimin
2017-11-01
6.5 wt% Si electrical steel is a superior soft magnetic material with excellent magnetic properties which highly depends on texture. In this study, based on the heredity of 〈0 0 1〉 orientation in columnar grains, columnar grains are used as the initial material to prepare non-oriented 6.5 wt% Si electrical steel with excellent magnetic properties. EBSD and XRD techniques are adopted to explore the structure and texture evolution during hot rolling, warm rolling, cold rolling and annealing. The results show that, due to the heredity of "structure and texture" from the initial strong {1 0 0} columnar grains, annealed sheet with {1 0 0}〈0 0 1〉 texture had better magnetic properties, which can be used as non-oriented high-silicon electrical steel. Both preferred cube grain nucleation in deformed {1 1 3}〈3 6 1〉 grains in subsurface and coarse {1 0 0}〈0 0 1〉 deformed grains in center layer show the effect of initial columnar grains with {1 0 0} texture.
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NASA Astrophysics Data System (ADS)
Fan, Zhijian; Jóni, Bertalan; Xie, Lei; Ribárik, Gábor; Ungár, Tamás
2018-04-01
Specimens of cold-rolled zirconium were tensile-deformed along the rolling (RD) and the transverse (TD) directions. The stress-strain curves revealed a strong texture dependence. High resolution X-ray line profile analysis was used to determine the prevailing active slip-systems in the specimens with different textures. The reflections in the X-ray diffraction patterns were separated into two groups. One group corresponds to the major and the other group to the random texture component, respectively. The dislocation densities, the subgrain size and the prevailing active slip-systems were evaluated by using the convolutional multiple whole profile (CMWP) procedure. These microstructure parameters were evaluated separately in the two groups of reflections corresponding to the two different texture components. Significant differences were found in both, the evolution of dislocation densities and the development of the fractions of and
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High-intensity fibre laser design for micro-machining applications
NASA Astrophysics Data System (ADS)
Ortiz-Neria, D. I.; Martinez-Piñón, F.; Hernandez-Escamilla, H.; Alvarez-Chavez, J. A.
2010-11-01
This work is focused on the design of a 250W high-intensity continuous-wave fibre optic laser with a 15μm spot size beam and a beam parameter product (BPP) of 1.8 for its use on Laser-assisted Cold Spray process (LCS) in the micro-machining areas. The metal-powder deposition process LCS, is a novel method based on Cold Spray technique (CS) assisted by laser technology. The LCS accelerates metal powders by the use of a high-pressure gas in order to achieve flash welding of particles over substrate. In LCS, the critical velocity of impact is lower with respect with CS while the powder particle is heated before the deposition by a laser beam. Furthermore, LCS does not heat the powder to achieve high temperatures as it happens in plasma processes. This property puts aside cooling problems which normally happen in sintered processes with high oxygen/nitrogen concentration levels. LCS will be used not only in deposition of thin layers. After careful design, proof of concept, experimental data, and prototype development, it should be feasible to perform micro-machining precise work with the use of the highintensity fibre laser presented in this work, and selective deposition of particles, in a similar way to the well-known Direct Metal Laser Sintering process (DMLS). The fibre laser consists on a large-mode area, Yb3+-doped, semi-diffraction limited, 25-m fibre laser cavity, operating in continuous wave regime. The fibre shows an arguably high slope-efficiency with no signs of roll-over. The measured M2 value is 1.8 and doping concentration of 15000ppm. It was made with a slight modification of the traditional MCVD technique. A full optical characterization will be presented.
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NASA Astrophysics Data System (ADS)
Li, Shaopo; Li, Jiading; Ding, Wenhua; Zhang, Hai
This paper reports on the experience with the production of 27/33 mm X80 heavy wall thicknesses, large OD (48") in Shouqin Steel Co., Ltd. (SQS). Considering the technology capability of the plate mill in SQS, a optimized rolling and cooling process was developed to achieve stable heavy gauge X80 mechanical properties. The importance of the slab reheating process and rolling schedule will be discussed in the paper. In addition, the per pass reductions logic used during recrystallized rough rolling, and special emphasis on the reduction of the final roughing pass prior to the intermediate holding resulting in a fine uniform prior austenite microstructure will be discussed. The optimized cooling process application after finish rolling guarantees the steady control of the final bainitic microstructure with optimum M/A phase for heavy gauge X80 plates. The plates produced by this process achieved good flatness and excellent mechanical properties. SQS has produced 10000 tons 27mm X80 for the Middle Asia C Line Project and 1000 tons 33mm X80 for the 3rd West-to-East Natural Gas Transmission Pipeline Project in 2013-2014. The products utilizing optimized rolling and cooling process showed extremely excellent low temperature toughness.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Joshi, Pooran C.; Compton, Brett G.; Li, Jianlin
2015-04-01
The purpose of this Cooperative Research and Development Agreement (CRADA) was to develop and evaluate ZrO 2/acrylic nanocomposite coatings for integrated optoelectronic applications. The formulations engineered to be compatible with roll-to-roll process were evaluated in terms of optical and dielectric properties. The uniform distribution of the ZrO 2 nanocrystals in the polymer matrix resulted in highly tunable refractive index and dielectric response suitable for advanced photonic and electronic device applications.
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NASA Technical Reports Server (NTRS)
Hosman, R. J. A. W.; Vandervaart, J. C.
1984-01-01
An experiment to investigate visual roll attitude and roll rate perception is described. The experiment was also designed to assess the improvements of perception due to cockpit motion. After the onset of the motion, subjects were to make accurate and quick estimates of the final magnitude of the roll angle step response by pressing the appropriate button of a keyboard device. The differing time-histories of roll angle, roll rate and roll acceleration caused by a step response stimulate the different perception processes related the central visual field, peripheral visual field and vestibular organs in different, yet exactly known ways. Experiments with either of the visual displays or cockpit motion and some combinations of these were run to asses the roles of the different perception processes. Results show that the differences in response time are much more pronounced than the differences in perception accuracy.
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Mechanical Properties of TRIP Steel Microalloyed with Ti
NASA Astrophysics Data System (ADS)
Krizan, Daniel; De Cooman, Bruno C.
2014-07-01
The precipitation state, microstructure, retained austenite stability, and mechanical properties of cold-rolled Ti-microalloyed CMnAlSiP TRIP steel were investigated. The precipitation state was analyzed in each processing step by means of transmission electron microscopy, chemical analysis using the anodic dissolution method, and by model calculations. Ti additions refined the microstructure mainly by the pinning of austenite and ferrite grain boundaries by various Ti-containing precipitates. Ti additions also resulted in a refinement of the size of the retained austenite islands and caused a slight decrease of the volume fraction and carbon content of the retained austenite. The morphology of the retained austenite was also changed and the stability of the retained austenite decreased, but Ti addition still resulted in an adequate strength-ductility balance and a tensile strength close to 1 GPa.
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Seasat. Volume 4: Attitude determination
NASA Technical Reports Server (NTRS)
Treder, A. J.
1980-01-01
The Seasat project was a feasibility demonstration of the use of orbital remote sensing for global ocean observation. The satellite was launched in June 1978 and was operated successfully until October 1978. A massive electrical failure occurred in the power system, terminating the mission prematurely. The actual implementation of the Seasat Attitude Determination system and the contents of the attitude data files generated by that system are documented. The deviations from plan caused by the anomalous Sun interference with horizon sensors, inflight calibration of Sun sensor head 2 alignment and horizon sensor biomass, estimation of yaw interpolation parameters, Sun and horizon sensor error sources, and yaw interpolation accuracy are included. Examples are given of flight attitude data from all modes of the Orbital Attitude Control System, of the ground processing effects on attitude data, and of cold cloud effects on pitch, and roll data.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Zaid, Md; Bhattacharjee, P.P., E-mail: pinakib@iith.ac.in
2014-10-15
The evolution of microstructure and texture during cross-rolling and annealing was investigated by electron backscatter diffraction in a ferritic–austenitic duplex stainless steel. For this purpose an alloy with nearly equal volume fraction of the two phases was deformed by multi-pass cross-rolling process up to 90% reduction in thickness. The rolling and transverse directions were mutually interchanged in each pass by rotating the sample by 90° around the normal direction. In order to avoid deformation induced phase transformation and dynamic strain aging, the rolling was carried out at an optimized temperature of 898 K (625 °C) at the warm-deformation range. Themore » microstructure after cross warm-rolling revealed a lamellar structure with alternate arrangement of the bands of two phases. Strong brass and rotated brass components were observed in austenite in the steel after processing by cross warm-rolling. The ferrite in the cross warm-rolling processed steel showed remarkably strong RD-fiber (RD//< 011 >) component (001)< 011 >. The development of texture in the two phases after processing by cross warm-rolling could be explained by the stability of the texture components. During isothermal annealing of the 90% cross warm-rolling processed material the lamellar morphology was retained before collapse of the lamellar structure to the mutual interpenetration of the phase bands. Ferrite showed recovery resulting in annealing texture similar to the deformation texture. In contrast, the austenite showed primary recrystallization without preferential orientation selection leading to the retention of deformation texture. The evolution of deformation and annealing texture in the two phases of the steel was independent of one another. - Highlights: • Effect of cross warm-rolling on texture formation is studied in duplex steel. • Brass texture in austenite and (001)<110 > in ferrite are developed. • Ferrite shows recovery during annealing retaining the (001)<110 > component. • Austenite shows recrystallization during annealing retaining the deformation texture. • The deformation of recrystallization of two phases is independent of one other.« less
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Development in high-grade dual phase steels with low C and Si design
NASA Astrophysics Data System (ADS)
Zhu, Guo-hui; Zhang, Xue-hui; Mao, Wei-min
2009-12-01
Cold rolled dual phase steels with low C and Si addition were investigated in terms of combination of composition and processing in order to improve mechanical properties and workability including welding and galvanizing. Mo and Cr could be used as alloying elements to partially replace C and Si to assure enough hardening ability of the steels and also give solute-hardening. Mo addition is more effective than Cr addition in terms of obtaining the required volume fraction of martensite and mechanical strength. The ferrite grain was effectively refined by addition of Nb microalloying, which gives optimized mechanical properties. The experimental results show that it is possible to obtain the required mechanical properties of high grade 800 MPa dual phase steel, i.e., tensile strength > 780 MPa, elongation > 15%, and yield/tensile strength ratio < 0.6 in the condition of low carbon (C < 0.11 wt.%) and low silicon design (Si < 0.05 wt.%) through adequate combination of composition and processing.
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NASA Astrophysics Data System (ADS)
Naghizadeh, Meysam; Mirzadeh, Hamed
2018-03-01
Microstructural evolutions during reversion annealing of a plastically deformed AISI 316 stainless steel were investigated and three distinct stages were identified: the reversion of strain-induced martensite to austenite, the primary recrystallization of the retained austenite, and the grain growth process. It was found that the slow kinetics of recrystallization at lower annealing temperatures inhibit the formation of an equiaxed microstructure and might effectively impair the usefulness of this thermomechanical treatment for the objective of grain refinement. By comparing the behavior of AISI 316 and 304 alloys, it was found that the mentioned slow kinetics is related to the retardation effect of solute Mo in the former alloy. At high reversion annealing temperature, however, an equiaxed austenitic microstructure was achieved quickly in AISI 316 stainless steel due to the temperature dependency of retardation effect of molybdenum, which allowed the process of recrystallization to happen easily. Conclusively, this work can shed some light on the issues of this efficient grain refining approach for microstructural control of austenitic stainless steels.
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Orzi, Daniel J O; Bilmes, Gabriel M
2004-12-01
Laser-induced breakdown spectroscopy (LIBS) was used for the characterization of the main components of the surface residual dirt produced in cold-rolled steel plates as a consequence of the manufacturing stages. At laser fluences between 0.05 J/cm(2) < F < 0.30 J/cm(2), dirt ablation takes place without any contribution from the substrate. Results show that the main components of the dirt are fine particles of Fe mostly homogeneously distributed in a thin layer of grease and soaps. In the primary stages of the manufacturing process carbon residuals can also be found. By measuring light emission from the lambda = 495.9 nm line of Fe(I) after laser ablation, we developed a real-time on-line method for the determination of the concentration of iron particles present in the surface dirt. The obtained results open new possibilities in the design of real-time instruments for industrial applications as a quality control of products and processes.
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NASA Astrophysics Data System (ADS)
Naghizadeh, Meysam; Mirzadeh, Hamed
2018-06-01
Microstructural evolutions during reversion annealing of a plastically deformed AISI 316 stainless steel were investigated and three distinct stages were identified: the reversion of strain-induced martensite to austenite, the primary recrystallization of the retained austenite, and the grain growth process. It was found that the slow kinetics of recrystallization at lower annealing temperatures inhibit the formation of an equiaxed microstructure and might effectively impair the usefulness of this thermomechanical treatment for the objective of grain refinement. By comparing the behavior of AISI 316 and 304 alloys, it was found that the mentioned slow kinetics is related to the retardation effect of solute Mo in the former alloy. At high reversion annealing temperature, however, an equiaxed austenitic microstructure was achieved quickly in AISI 316 stainless steel due to the temperature dependency of retardation effect of molybdenum, which allowed the process of recrystallization to happen easily. Conclusively, this work can shed some light on the issues of this efficient grain refining approach for microstructural control of austenitic stainless steels.
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NASA Technical Reports Server (NTRS)
Alexander, D. W.
1992-01-01
The Hubble space telescope (HST) solar array was designed to meet specific output power requirements after 2 years in low-Earth orbit, and to remain operational for 5 years. The array, therefore, had to withstand 30,000 thermal cycles between approximately +100 and -100 C. The ability of the array to meet this requirement was evaluated by thermal cycle testing, in vacuum, two 128-cell solar cell modules that exactly duplicated the flight HST solar array design. Also, the ability of the flight array to survive an emergency deployment during the dark (cold) portion of an orbit was evaluated by performing a cold-roll test using one module.
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The effect of thermomechanical processing on second phase particle redistribution in U-10 wt%Mo
DOE Office of Scientific and Technical Information (OSTI.GOV)
Hu, Xiaohua; Wang, Xiaowo; Joshi, Vineet V.
2018-03-01
The multi-pass hot-rolling process of an annealed uranium-10 wt% molybdenum coupon was studied by plane-strain compression finite element modeling. Two point correlation function (2PCF) was used to analyze the carbide particle distribution after each rolling reduction. The hot rolling simulation results show that the alignment of UC particles along grain boundaries will rotate during rolling until it is parallel to the rolling direction, to form stringer-like distributions which are typically observed in rolled products that contain inclusions. 2PCF analysis of simulation shows that the interparticle spacing shrinks along the normal direction. The number of major peaks of 2PCF along NDmore » decreases after large reduction. The locations of major peaks indicate the inter-stringer distances.« less
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NASA Astrophysics Data System (ADS)
Liu, Yang; Li, Feng; Li, Xue Wen; Shi, Wen Yong
2018-03-01
Rolling is currently a widely used method for manufacturing and processing high-performance magnesium alloy sheets and has received widespread attention in recent years. Here, we combined continuous variable cross-section direct extrusion (CVCDE) and rolling processes. The microstructure and mechanical properties of the resulting sheets rolled at different temperatures from CVCDE extrudate were investigated by optical microscopy, scanning electron microscope, transmission electron microscopy and electron backscatter diffraction. The results showed that a fine-grained microstructure was present with an average grain size of 3.62 μm in sheets rolled from CVCDE extrudate at 623 K. Dynamic recrystallization and a large strain were induced by the multi-pass rolling, which resulted in grain refinement. In the 573-673 K range, the yield strength, tensile strength and elongation initially increased and then declined as the CVCDE temperature increased. The above results provide an important scientific basis of processing, manufacturing and the active control on microstructure and property for high-performance magnesium alloy sheet.
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Anisotropy of mechanical and thermal properties of AZ31 sheets prepared using the ARB technique
NASA Astrophysics Data System (ADS)
Halmešová, K.; Trojanová, Z.; Džugan, J.; Drozd, Z.; Minárik, P.; Knapek, M.
2017-07-01
In the accumulative roll bonding (ARB) technique, repeated stacking of material followed by conventional roll-bonding is carried out. For this process the surfaces are cleaned with ethanol and then joined together by rolling. The rolled material is then cut into two halves, again surface treated and roll-bonded. This process may be repeated several times. For the magnesium alloy AZ31 (Mg-3Al-1Zn) rolling at an elevated temperature of 400 °C is necessary for ARB because of the low plasticity of hexagonal magnesium alloys at lower temperatures. Samples for this study were prepared using 1 to 3 ARB passes through the rolling mill. It was found that the ARB substantially refined the grain size of sheets to the micrometer scale. The microstructure and texture of the deformed samples were studied by light and electron microscopy. The mechanical properties of the ARB samples were explored using tensile test-pieces cut from the sheets with the tensile axis taken either parallel or perpendicular to the rolling direction, where a significant anisotropy in both mechanical properties and Young’s modulus was found. Anisotropy is explained on the basis of the specific microstructure and texture formed during the ARB process.
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Roll splitting for field processing of biomass
Dennis T. Curtin; Donald L. Sirois; John A. Sturos
1987-01-01
The concept of roll splitting wood originated in 1967 when the Tennessee Valley Authority (TVA) forest products specialists developed a wood fibrator. The objective of that work was to produce raw materials for reconstituted board products. More recently, TVA focused on roll splitting as a field process to accelerate drying of small trees (3-15 cm diameter), much...
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Tribology and Tool Wear of Hot Dip Galvanized Zinc Magnesium Alloys on Cold Rolled Steel Sheets
NASA Astrophysics Data System (ADS)
Raab, A. E.; Berger, E.; Freudenthaler, J.; Leomann, F.; Walch, C.
2011-05-01
Recently zinc based coatings on cold rolled steel with improved functionality in terms of forming and/or corrosion behaviour have been intensively investigated in the steel industry1,2,3. One of the most promising products are zinc magnesium alloys produced in hot dip galvanizing process. These coatings were already introduced in construction industry a few years ago1. With some modifications the improved properties of the coating are also interesting for automotive industry. In the present work the tribological potential of hot dip galvanized zinc magnesium coatings (HDG/ZM) produced at an industrial line under regular production, was studied in terms of sliding properties, adhesive and abrasive tool wear. First a short introduction into surface morphology of HDG/ZM will be given. For the tribological characterization of the material, which is the main topic of the contribution, different tests were performed on hot dip galvanised zinc magnesium material and results were compared with classic hot dip galvanized zinc coating (HDG/Z). The investigations are mainly based on the strip draw test which allows the determination of the friction coefficient directly by using a constant contact pressure. Deep drawing property was tested by forming model cups. The abrasive tool wear was tested using a standard test for material used in automotive industry. The adhesive tool wear was investigated by characterizing the coating material transferred to the tool in the strip draw test. All performed tests show an improved drawability of HDG/ZM compared to classical HDG/Z reference material. However the most promising difference between HDG/ZM and HDG/Z is that galling was found to be less for HDG/ZM than for HDG/Z. Therefore HDG/ZM is an interesting system not only with respect to corrosion protection but also in terms of tribology and provides clear advantages in formability.
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Tribology and Tool Wear of Hot Dip Galvanized Zinc Magnesium Alloys on Cold Rolled Steel Sheets
DOE Office of Scientific and Technical Information (OSTI.GOV)
Raab, A. E.; Berger, E.; Freudenthaler, J.
Recently zinc based coatings on cold rolled steel with improved functionality in terms of forming and/or corrosion behaviour have been intensively investigated in the steel industry. One of the most promising products are zinc magnesium alloys produced in hot dip galvanizing process. These coatings were already introduced in construction industry a few years ago. With some modifications the improved properties of the coating are also interesting for automotive industry. In the present work the tribological potential of hot dip galvanized zinc magnesium coatings (HDG/ZM) produced at an industrial line under regular production, was studied in terms of sliding properties, adhesivemore » and abrasive tool wear.First a short introduction into surface morphology of HDG/ZM will be given. For the tribological characterization of the material, which is the main topic of the contribution, different tests were performed on hot dip galvanised zinc magnesium material and results were compared with classic hot dip galvanized zinc coating (HDG/Z). The investigations are mainly based on the strip draw test which allows the determination of the friction coefficient directly by using a constant contact pressure. Deep drawing property was tested by forming model cups. The abrasive tool wear was tested using a standard test for material used in automotive industry. The adhesive tool wear was investigated by characterizing the coating material transferred to the tool in the strip draw test.All performed tests show an improved drawability of HDG/ZM compared to classical HDG/Z reference material. However the most promising difference between HDG/ZM and HDG/Z is that galling was found to be less for HDG/ZM than for HDG/Z. Therefore HDG/ZM is an interesting system not only with respect to corrosion protection but also in terms of tribology and provides clear advantages in formability.« less
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15. VIEW OF ROLLING OPERATION. INGOTS AND BAR STOCK WERE ...
15. VIEW OF ROLLING OPERATION. INGOTS AND BAR STOCK WERE ROLLED TO A SPECIFIED THICKNESS IN PREPARATION FOR FURTHER PROCESSING. (11/82) - Rocky Flats Plant, Uranium Rolling & Forming Operations, Southeast section of plant, southeast quadrant of intersection of Central Avenue & Eighth Street, Golden, Jefferson County, CO
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Texture evolution and mechanical anisotropy of biomedical hot-rolled Co-Cr-Mo alloy.
Mori, Manami; Yamanaka, Kenta; Sato, Shigeo; Chiba, Akihiko
2015-11-01
Crystallographic textures and their effect on the mechanical anisotropy of a hot-rolled biomedical Co-Cr-Mo alloy were investigated. The hot-rolled Co-28Cr-6Mo-0.13N (mass%) alloy examined here exhibited a monotonic strength increment following hot-rolling reduction, eventually reaching a 0.2% proof stress of 1400 MPa while maintaining acceptable ductility (>10%). The dominant hot-rolling texture was a brass-type component, which is characterized by the alloy's peculiarly low stacking fault energy (SFE) even at hot rolling temperatures, although the minor peaks of the near copper component were also identified. However, because of the onset of dynamic recrystallization (DRX) during the hot rolling process, the texture intensity was relatively weak even after 90% hot rolling, although the grain refinement originating from the DRX was not significant (the "less active DRX" condition increased the strain accumulation during the process, resulting in high-strength samples). The weakened texture development resulted in negligible in-plane anisotropy for the hot-rolled specimen strength, when the specimens were tensile strained in the rolling direction (RD) and transverse direction (TD). The elongation-to-failure, however, exhibited a difference with respect to the tensile loading axis. It is suggested that the ductility anisotropy is closely related to a strain-induced γ (fcc) → ε (hcp) martensitic transformation during tensile loading, resulting in a difference in the proportion of quasi-cleavage fracture surfaces. The obtained results will be helpful in the development of high-strength Co-Cr-Mo alloy plates and sheets, and have implications regarding plastic deformation and texture evolution during the hot rolling of non-conventional metallic materials with low SFE at elevated temperatures, where planar dislocation slips of Shockley partial dislocations and thermally activated process interplay. Copyright © 2015 Elsevier Ltd. All rights reserved.
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NASA Technical Reports Server (NTRS)
Bird, R. Keith; Hibberd, Joshua
2009-01-01
Electron beam freeform fabrication (EBF3) direct metal deposition processing was used to fabricate two Inconel 718 single-bead-width wall builds and one multiple-bead-width block build. Specimens were machined to evaluate microstructure and room temperature tensile properties. The tensile strength and yield strength of the as-deposited material from the wall and block builds were greater than those for conventional Inconel 718 castings but were less than those for conventional cold-rolled sheet. Ductility levels for the EBF3 material were similar to those for conventionally-processed sheet and castings. An unexpected result was that the modulus of the EBF3-deposited Inconel 718 was significantly lower than that of the conventional material. This low modulus may be associated with a preferred crystallographic orientation resultant from the deposition and rapid solidification process. A heat treatment with a high solution treatment temperature resulted in a recrystallized microstructure and an increased modulus. However, the modulus was not increased to the level that is expected for Inconel 718.
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NASA Astrophysics Data System (ADS)
Gali, Olufisayo A.
Near-surface deformed layers developed on aluminum alloys significantly influence the corrosion and tribological behavior as well as reduce the surface quality of the rolled aluminum. The evolution of the near-surface microstructures induced on magnesium containing aluminum alloys during thermomechanical processing has been investigated with the aim generating an understanding of the influence of individual forming parameters on its evolution and examine the microstructure of the roll coating induced on the mating steel roll through material transfer during rolling. The micro-mechanisms related to the various features of near-surface microstructure developed during tribological conditions of the simulated hot rolling process were identified. Thermomechanical processing experiments were performed with the aid of hot rolling (operating temperature: 550 to 460 °C, 4, 10 and 20 rolling pass schedules) and hot forming (operating temperature: 350 to 545 °C, strain rate: 4 x 10-2 s-1) tribo-simulators. The surface, near-surface features and material transfer induced during the elevated temperature plastic deformation were examined and characterized employing optical interferometry, SEM/EDS, FIB and TEM. Near-surface features characterized on the rolled aluminum alloys included; cracks, fractured intermetallic particles, aluminum nano-particles, oxide decorated grain boundaries, rolled-in oxides, shingles and blisters. These features were related to various individual rolling parameters which included, the work roll roughness, which induced the formation of shingles, rolling marks and were responsible for the redistribution of surface oxide and the enhancements of the depth of the near-surface damage. The enhanced stresses and strains experienced during rolling were related to the formation and propagation of cracks, the nanocrystalline structure of the near-surface layers and aluminum nano-particles. The mechanism of the evolution of the near-surface microstructure were determined to include grain boundary sliding which induced the cracks at the surface and subsurface of the alloy, magnesium diffusion to free surfaces, crack propagation from shear stresses and the shear strains inducing the nanocrystalline grain structure, the formation of shingles by the shear deformation of micro-wedges induced by the work roll grooves, and the deformation of this oxide covered micro-wedges inducing the rolled-in oxides. Magnesium diffusion to free surfaces was identified as inducing crack healing due to the formation of MgO within cracks and was responsible for the oxide decorated grain boundaries. An examination of the roll coating revealed a complex layered microstructure that was induced through tribo-chemical and mechanical entrapment mechanisms. The microstructure of the roll coating suggested that the work roll material and the rolled aluminum alloy were essential in determining its composition and structure. Subsequent hot forming processes revealed the rich oxide-layer of the near-surface microstructure was beneficial for reducing the coefficient of friction during tribological contact with the steel die. Damage to the microstructure include cracks induced from grain boundary sliding of near-surface grains and the formation of oxide fibres within cracks of the near-surface deformed layers.
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Du, Hang; Song, Ci; Li, Shengyi; Xu, Mingjin; Peng, Xiaoqiang
2017-05-20
In the process of computer controlled optical surfacing (CCOS), the uncontrollable rolled edge restricts further improvements of the machining accuracy and efficiency. Two reasons are responsible for the rolled edge problem during small tool polishing. One is that the edge areas cannot be processed because of the orbit movement. The other is that changing the tool influence function (TIF) is difficult to compensate for in algorithms, since pressure step appears in the local pressure distribution at the surface edge. In this paper, an acentric tool influence function (A-TIF) is designed to remove the rolled edge after CCOS polishing. The model of A-TIF is analyzed theoretically, and a control point translation dwell time algorithm is used to verify that the full aperture of the workpiece can be covered by the peak removal point of the tool influence functions. Thus, surface residual error in the full aperture can be effectively corrected. Finally, the experiments are carried out. Two fused silica glass samples of 100 mm×100 mm are polished by traditional CCOS and the A-TIF method, respectively. The rolled edge was clearly produced in the sample polished by the traditional CCOS, while residual errors do not show this problem the sample polished by the A-TIF method. Therefore, the rolled edge caused by the traditional CCOS process is successfully suppressed during the A-TIF process. The ability to suppress the rolled edge of the designed A-TIF has been confirmed.
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1987-06-01
cold-rolled zinc-copper-aluminum eutectic alloy exhibited this superplastic response. Superplasticity was initially viewed as a curious observation...limited to eutectic alloys when tested under the correct laboratory conditions. However, in 1962 Underwood [Ref. 23 reviewed Soviet work; this review...formation of a very fine dispersoid, ZrAI3. This dispersoid results in grain refinement, raises the recrystallization temperature (Ref. 7:p. 414] and gives
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Food Service Alternatives for Meals Away from the Dining Facility
1984-06-01
Chicken Salad Ham Salad Italian Cold Cuts Roast Beef Ham Turkey Hot Meatball with Cheese Hot Sausage Egg Roll Fried Rice Beef and Vegetables Desserts...Salami Provolone American Cheese Swiss Cheese Tuna Salad Egg Salad Chicken Salad Ham Salad *Hot Sausage *Hot Meatball with Cheese Chili Beef...Cake Ham Brownies Hot Sausage Puddings Hot Meatball with Cheese Jello Shaved Steak with Pie Eggs Cookies Cheese Cole Slaw Onions Macaroni Salad Peppers
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NASA Astrophysics Data System (ADS)
Veerasamy, M.; Srinivasan, K.; Prakash, Raghu V.
2010-10-01
The crash behavior of Cold Rolled Mild Steel (CRMS) closed form thin section was studied by conducting compressive tests at loading velocities of 5 mm/min and 1000 mm/min. The numerical simulations were conducted for the same experimental conditions to understand the deformation shape, peak forces and energy absorption capacity of sections at different impact velocities. The simulation results correlated well with the experimental results.
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Code of Federal Regulations, 2014 CFR
2014-07-01
....000626 O&G 0.000522 0.000209 Chromium 1 0.0000209 0.0000084 Lead 0.0000094 0.0000031 Nickel 1 0.0000188 0... limitations for chromium and nickel shall be applicable in lieu of those for lead and zinc when cold rolling...) of product TSS 0.00626 0.00313 O&G 0.00261 0.00104 Chromium 1 0.000104 0.0000418 Lead 0.0000469 0...
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Code of Federal Regulations, 2013 CFR
2013-07-01
....000626 O&G 0.000522 0.000209 Chromium 1 0.0000209 0.0000084 Lead 0.0000094 0.0000031 Nickel 1 0.0000188 0... limitations for chromium and nickel shall be applicable in lieu of those for lead and zinc when cold rolling...) of product TSS 0.00626 0.00313 O&G 0.00261 0.00104 Chromium 1 0.000104 0.0000418 Lead 0.0000469 0...
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Code of Federal Regulations, 2012 CFR
2012-07-01
....000626 O&G 0.000522 0.000209 Chromium 1 0.0000209 0.0000084 Lead 0.0000094 0.0000031 Nickel 1 0.0000188 0... limitations for chromium and nickel shall be applicable in lieu of those for lead and zinc when cold rolling...) of product TSS 0.00626 0.00313 O&G 0.00261 0.00104 Chromium 1 0.000104 0.0000418 Lead 0.0000469 0...
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NASA Technical Reports Server (NTRS)
Viswanathan, Tito (Inventor)
2007-01-01
The invention provides coatings useful for preventing corrosion of metals. The coatings comprise a film-forming resin and conductive polymers comprising linearly conjugated .pi.-systems and residues of sulfonated lignin or a sulfonated polyflavonoid or derivatives of solfonated lignin or a sulfonated polyflavonoid. The invention also provides a latex formulation of the coatings, and articles of manufacture comprising a metal substrate and a coating in contact with the metal substrate.
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NASA Technical Reports Server (NTRS)
Viswanathan, Tito (Inventor)
2007-01-01
The invention provides coatings useful for preventing corrosion of metals. The coatings comprise a film-forming resin and conductive polymers comprising linearly conjugated x-systems and residues of sulfonated lignin or a sulfonated polyflavonoid or derivatives of solfonated lignin or a sulfonated polyflavonoid. The invention also provides a latex formulation of the coatings, and articles of manufacture comprising a metal substrate and a coating in contact with the metal substrate.
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NASA Technical Reports Server (NTRS)
Viswanathan, Tito (Inventor)
2005-01-01
The invention provides coatings useful for preventing corrosion of metals. The coatings comprise a film-forming resin and conductive polymers comprising linearly conjugated pi-systems and residues of sulfonated lignin or a sulfonated polyflavonoid or derivatives of sulfonated lignin or a sulfonated polyflavonoid. The invention also provides a latex formulation of the coatings, and articles of manufacture comprising a metal substrate and a coating in contact with the metal substrate.
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Code of Federal Regulations, 2010 CFR
2010-07-01
....000626 O&G 0.000522 0.000209 Chromium 1 0.0000209 0.0000084 Lead 0.0000094 0.0000031 Nickel 1 0.0000188 0... limitations for chromium and nickel shall be applicable in lieu of those for lead and zinc when cold rolling...) of product TSS 0.00626 0.00313 O&G 0.00261 0.00104 Chromium 1 0.000104 0.0000418 Lead 0.0000469 0...
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Code of Federal Regulations, 2011 CFR
2011-07-01
....000626 O&G 0.000522 0.000209 Chromium 1 0.0000209 0.0000084 Lead 0.0000094 0.0000031 Nickel 1 0.0000188 0... limitations for chromium and nickel shall be applicable in lieu of those for lead and zinc when cold rolling...) of product TSS 0.00626 0.00313 O&G 0.00261 0.00104 Chromium 1 0.000104 0.0000418 Lead 0.0000469 0...
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Effect of tempering treatment upon the residual stress of bimetallic roll
NASA Astrophysics Data System (ADS)
Sano, Y.; Noda, N.-A.; Takase, Y.; Torigoe, R.; Tsuboi, K.; Aridi, M. R.; Sanada, Y.; Lan, L. Y.
2018-06-01
Bimetallic rolls are widely used in steel rolling industries because of the excellent hardness, wear resistance, and high temperature properties. However, thermal stress is produced by heating-cooling thermal cycles, which is a great challenge for their practical application. Indeed, if severe thermal tensile stress is introduced into these rolls, it can assist the thermal cracks to propagate, even lead to the overall failure of rolls. In this paper, we investigated the effect of tempering treatment on the residual stress after the bimetallic rolls were subjected to quenching. Compared with the non-uniform heating-quenching process, the tempering process makes the maximum stress at the core decreased by 15% (from 275 MPa to 234 MPa) with considering martensite transformation but decreased by 26% (from 275 MPa to 201 MPa) without considering martensite transformation. For tempering process after uniform heating quenching, the maximum stress at the core decreases by 24% from 357 MPa to 273 MPa with considering martensite transformation but decreases by 30% from 357 MPa to 246 MPa without considering martensite transformation. And compared with the non-uniform heating-quenching process, the double tempering process makes the maximum stress at the core decreased by 8% (from 275 MPa to 253 MPa) with considering martensite transformation but decreased by 27% (from 275 MPa to 200 MPa) without considering martensite transformation.
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Tube manufacturing and characterization of oxide dispersion strengthened ferritic steels
NASA Astrophysics Data System (ADS)
Ukai, Shigeharu; Mizuta, Shunji; Yoshitake, Tunemitsu; Okuda, Takanari; Fujiwara, Masayuki; Hagi, Shigeki; Kobayashi, Toshimi
2000-12-01
Oxide dispersion strengthened (ODS) ferritic steels have an advantage in radiation resistance and superior creep rupture strength at elevated temperature due to finely distributed Y2O3 particles in the ferritic matrix. Using a basic composition of low activation ferritic steel (Fe-12Cr-2W-0.05C), cladding tube manufacturing by means of pilger mill rolling and subsequent recrystallization heat-treatment was conducted while varying titanium and yttria contents. The recrystallization heat-treatment, to soften the tubes hardened due to cold-rolling and to subsequently improve the degraded mechanical properties, was demonstrated to be effective in the course of tube manufacturing. For a titanium content of 0.3 wt% and yttria of 0.25 wt%, improvement of the creep rupture strength can be attained for the manufactured cladding tubes. The ductility is also adequately maintained.
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Geometrical accuracy improvement in flexible roll forming lines
NASA Astrophysics Data System (ADS)
Larrañaga, J.; Berner, S.; Galdos, L.; Groche, P.
2011-01-01
The general interest to produce profiles with variable cross section in a cost-effective way has increased in the last few years. The flexible roll forming process allows producing profiles with variable cross section lengthwise in a continuous way. Until now, only a few flexible roll forming lines were developed and built up. Apart from the flange wrinkling along the transition zone of u-profiles with variable cross section, the process limits have not been investigated and solutions for shape deviations are unknown. During the PROFOM project a flexible roll forming machine has been developed with the objective of producing high technological components for automotive body structures. In order to investigate the limits of the process, different profile geometries and steel grades including high strength steels have been applied. During the first experimental tests, several errors have been identified, as a result of the complex stress states generated during the forming process. In order to improve the accuracy of the target profiles and to meet the tolerance demands of the automotive industry, a thermo-mechanical solution has been proposed. Additional mechanical devices, supporting flexible the roll forming process, have been implemented in the roll forming line together with local heating techniques. The combination of both methods shows a significant increase of the accuracy. In the present investigation, the experimental results of the validation process are presented.
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Mechanical Behaviour of 304 Austenitic Stainless Steel Processed by Room Temperature Rolling
NASA Astrophysics Data System (ADS)
Singh, Rahul; Goel, Sunkulp; Verma, Raviraj; Jayaganthan, R.; Kumar, Abhishek
2018-03-01
To study the effect of room temperature rolling on mechanical properties of 304 Austenitic Stainless Steel, the as received 304 ASS was rolled at room temperature for different percentage of plastic deformation (i.e. 30, 50, 70 and 90 %). Microstructural study, tensile and hardness tests were performed in accordance with ASTM standards to study the effect of rolling. The ultimate tensile strength (UTS) and hardness of a rolled specimen have enhanced with rolling. The UTS has increased from 693 MPa (as received) to 1700 MPa (after 90% deformation). The improvement in UTS of processed samples is due to combined effect of grain refinement and stress induced martensitic phase transformation. The hardness values also increases from 206 VHN (as received) to 499 VHN (after 90% deformation). Magnetic measurements were also conducted to confirm the formation of martensitic phase.
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NASA Astrophysics Data System (ADS)
Li, Yu; Milbourn, David
Vanadium microalloying is highly effective in high strength strip steels produced by thin slab casting and direct rolled process. Because of the high solubility of V(C,N) in austenite, vanadium is likely to remain in solution during casting, equalisation and rolling. Vanadium microalloyed steels have better hot ductility and are less prone to transverse cracking than niobium containing steels. Despite a coarse as-cast austenite grain size before rolling, significant grain refinement can be achieved in vanadium microalloyed steels by repeated recrystallization during rolling, resulting in a fine uniform ferrite microstructure in final strip. Almost all vanadium present in microalloyed steels is available to precipitate in ferrite as very fine particles, contributing to precipitation strengthening. Vanadium microalloyed steels show less sensitivity to rolling process variables and exhibit excellent combination of strength and toughness.
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Calendering and Rolling of Viscoplastic Materials: Theory and Experiments
NASA Astrophysics Data System (ADS)
Mitsoulis, E.; Sofou, S.; Muliawan, E. B.; Hatzikiriakos, S. G.
2007-04-01
The calendering and rolling processes are used in a wide variety of industries for the production of rolled sheets or films of specific thickness and final appearance. The acquired final sheet thickness depends mainly on the rheological properties of the material. Materials which have been used in the present study are foodstuff (such as mozzarella cheese and flour-water dough) used in food processing. These materials are rheologically viscoplastic, obeying the Herschel-Bulkley model. The results give the final sheet thickness and the torque as a function of the roll speed. Theoretical analysis based on the Lubrication Approximation Theory (LAT) shows that LAT is a good predictive tool for calendering, where the sheet thickness is very small compared with the roll size. However, in rolling where this is not true, LAT does not hold, and a 2-D analysis is necessary.
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Finite-element model to predict roll-separation force and defects during rolling of U-10Mo alloys
DOE Office of Scientific and Technical Information (OSTI.GOV)
Soulami, Ayoub; Burkes, Douglas E.; Joshi, Vineet V.
This study used a finite element code, LSDYNA, as a predictive tool to optimize the rolling process. Simulations of the hot rolling of U-10Mo coupons encapsulated in low-carbon steel were conducted following two different schedules. Model predictions of the roll-separation force and roll pack thicknesses at different stages of the rolling process were compared with experimental measurements. The study reported here discussed various attributes of the rolled coupons revealed by the model (e.g., waviness and thickness non-uniformity like dog boning). To investigate the influence of the cladding material on these rolling defects, other cases were simulated: hot rolling with alternative can materials, namely, 304 stainless steel and Zircaloy-2, and bare-rolling.
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Spatial orientation of caloric nystagmus in semicircular canal-plugged monkeys.
Arai, Yasuko; Yakushin, Sergei B; Cohen, Bernard; Suzuki, Jun-Ichi; Raphan, Theodore
2002-08-01
We studied caloric nystagmus before and after plugging all six semicircular canals to determine whether velocity storage contributed to the spatial orientation of caloric nystagmus. Monkeys were stimulated unilaterally with cold ( approximately 20 degrees C) water while upright, supine, prone, right-side down, and left-side down. The decline in the slow phase velocity vector was determined over the last 37% of the nystagmus, at a time when the response was largely due to activation of velocity storage. Before plugging, yaw components varied with the convective flow of endolymph in the lateral canals in all head orientations. Plugging blocked endolymph flow, eliminating convection currents. Despite this, caloric nystagmus was readily elicited, but the horizontal component was always toward the stimulated (ipsilateral) side, regardless of head position relative to gravity. When upright, the slow phase velocity vector was close to the yaw and spatial vertical axes. Roll components became stronger in supine and prone positions, and vertical components were enhanced in side down positions. In each case, this brought the velocity vectors toward alignment with the spatial vertical. Consistent with principles governing the orientation of velocity storage, when the yaw component of the velocity vector was positive, the cross-coupled pitch or roll components brought the vector upward in space. Conversely, when yaw eye velocity vector was downward in the head coordinate frame, i.e., negative, pitch and roll were downward in space. The data could not be modeled simply by a reduction in activity in the ipsilateral vestibular nerve, which would direct the velocity vector along the roll direction. Since there is no cross coupling from roll to yaw, velocity storage alone could not rotate the vector to fit the data. We postulated, therefore, that cooling had caused contraction of the endolymph in the plugged canals. This contraction would deflect the cupula toward the plug, simulating ampullofugal flow of endolymph. Inhibition and excitation induced by such cupula deflection fit the data well in the upright position but not in lateral or prone/supine conditions. Data fits in these positions required the addition of a spatially orientated, velocity storage component. We conclude, therefore, that three factors produce cold caloric nystagmus after canal plugging: inhibition of activity in ampullary nerves, contraction of endolymph in the stimulated canals, and orientation of eye velocity to gravity through velocity storage. Although the response to convection currents dominates the normal response to caloric stimulation, velocity storage probably also contributes to the orientation of eye velocity.
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NASA Astrophysics Data System (ADS)
Hördemann, C.; Hirschfelder, K.; Schaefer, M.; Gillner, A.
2015-09-01
The breakthrough of flexible organic electronics and especially organic photovoltaics is highly dependent on cost-efficient production technologies. Roll-2-Roll processes show potential for a promising solution in terms of high throughput and low-cost production of thin film organic components. Solution based material deposition and integrated laser patterning processes offer new possibilities for versatile production lines. The use of flexible polymeric substrates brings along challenges in laser patterning which have to be overcome. One main challenge when patterning transparent conductive layers on polymeric substrates are material bulges at the edges of the ablated area. Bulges can lead to short circuits in the layer system leading to device failure. Therefore following layers have to have a sufficient thickness to cover and smooth the ridge. In order to minimize the bulging height, a study has been carried out on transparent conductive ITO layers on flexible PET substrates. Ablation results using different beam shapes, such as Gaussian beam, Top-Hat beam and Donut-shaped beam, as well as multi-pass scribing and double-pulsed ablation are compared. Furthermore, lab scale methods for cleaning the patterned layer and eliminating bulges are contrasted to the use of additional water based sacrificial layers in order to obtain an alternative procedure suitable for large scale Roll-2-Roll manufacturing. Besides progress in research, ongoing transfer of laser processes into a Roll-2-Roll demonstrator is illustrated. By using fixed optical elements in combination with a galvanometric scanner, scribing, variable patterning and edge deletion can be performed individually.
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The effect of thermomechanical processing on second phase particle redistribution in U-10 wt%Mo
NASA Astrophysics Data System (ADS)
Hu, Xiaohua; Wang, Xiaowo; Joshi, Vineet V.; Lavender, Curt A.
2018-03-01
The multi-pass hot-rolling process of an annealed uranium-10 wt% molybdenum (U10Mo) coupon was studied by plane-strain compression finite element modeling. As-cast U10Mo typically contains second phase particles such as uranium carbides (UC) and silicides along the grain boundaries. The volume fraction of UC is typically large, while the other phases can be redissolved in the matrix by certain heat treatments. The UC particle distribution is important due to its influence on the recrystallization processes (particle stimulated nucleation) that occur during annealing between rolling passes. Unfavorable particle distribution and fracture after rolling can affect the grain size and also influence the fuel performance in the reactor. A statistical method, i.e., the two-point correlation function (2PCF), was used to analyze the carbide particle distribution after each rolling reduction. The hot rolling simulation results show that the alignment of UC particles along grain boundaries will rotate during rolling until it is parallel to the rolling direction, to form stringer-like distributions which are typically observed in rolled products that contain inclusions. 2PCF analysis shows that the interparticle spacing shrinks along the normal direction (ND) and increases along the rolling direction (RD). The simulated particle distribution is very similar to that measured experimentally for similar rolling reductions. The magnitudes of major peaks of 2PCF along the ND decrease after large reduction. The locations of major peaks indicate the inter-stringer distances. Many more small peaks appear for the 2PCF along the RD, and this is related to the neighboring particles within stringers, which are along the RD.
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Fabrication of GRCop-84 Rocket Thrust Chambers
NASA Technical Reports Server (NTRS)
Loewenthal, William; Ellis, David
2006-01-01
GRCop-84, a copper alloy, Cu-8 at% Cr-4 at% Nb developed at NASA Glenn Research Center for regenerative1y cooled rocket engine liners has excellent combinations of elevated temperature strength, creep resistance, thermal conductivity and low cycle fatigue. GRCop-84 is produced from pre-alloyed atomized powder and has been fabricated into plate, sheet and tube forms as well as near net shapes. Fabrication processes to produce demonstration rocket combustion chambers will be presented and includes powder production, extruding, rolling, forming, friction stir welding, and metal spinning. GRCop-84 has excellent workability and can be readily fabricated into complex components using conventional powder and wrought metallurgy processes. Rolling was examined in detail for process sensitivity at various levels of total reduction, rolling speed and rolling temperature representing extremes of commercial processing conditions. Results indicate that process conditions can range over reasonable levels without any negative impact to properties.
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Fabrication of GRCop-84 Rocket Thrust Chambers
NASA Technical Reports Server (NTRS)
Loewenthal, William S.; Ellis, David L.
2005-01-01
GRCop-84, a copper alloy, Cu-8 at% Cr-4 at% Nb developed at NASA Glenn Research Center for regeneratively cooled rocket engine liners has excellent combinations of elevated temperature strength, creep resistance, thermal conductivity and low cycle fatigue. GRCop-84 is produced from prealloyed atomized powder and has been fabricated into plate, sheet and tube forms as well as near net shapes. Fabrication processes to produce demonstration rocket combustion chambers will be presented and includes powder production, extruding, rolling, forming, friction stir welding, and metal spinning. GRCop-84 has excellent workability and can be readily fabricated into complex components using conventional powder and wrought metallurgy processes. Rolling was examined in detail for process sensitivity at various levels of total reduction, rolling speed and rolling temperature representing extremes of commercial processing conditions. Results indicate that process conditions can range over reasonable levels without any negative impact to properties.
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NASA Astrophysics Data System (ADS)
Blom, Paul; van Mol, Ton
2011-11-01
Light-emitting diodes are more efficient than conventional lighting, but high production costs limit their uptake. Organic versions that can be produced using a cheap newspaper-style "roll-to-roll" printing process are likely to revolutionize our lighting and signage.
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Rapid Prototyping of Slot Die Devices for Roll to Roll Production of EL Fibers
Bellingham, Alyssa; Bromhead, Nicholas; Fontecchio, Adam
2017-01-01
There is a growing interest in fibers supporting optoelectrical properties for textile and wearable display applications. Solution-processed electroluminescent (EL) material systems can be continuously deposited onto fiber or yarn substrates in a roll-to-roll process, making it easy to scale manufacturing. It is important to have precise control over layer deposition to achieve uniform and reliable light emission from these EL fibers. Slot-die coating offers this control and increases the rate of EL fiber production. Here, we report a highly adaptable, cost-effective 3D printing model for developing slot dies used in automatic coating systems. The resulting slot-die coating system enables rapid, reliable production of alternating current powder-based EL (ACPEL) fibers and can be adapted for many material systems. The benefits of this system over dip-coating for roll-to-roll production of EL fibers are demonstrated in this work. PMID:28772954
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Rapid Prototyping of Slot Die Devices for Roll to Roll Production of EL Fibers.
Bellingham, Alyssa; Bromhead, Nicholas; Fontecchio, Adam
2017-05-29
There is a growing interest in fibers supporting optoelectrical properties for textile and wearable display applications. Solution-processed electroluminescent (EL) material systems can be continuously deposited onto fiber or yarn substrates in a roll-to-roll process, making it easy to scale manufacturing. It is important to have precise control over layer deposition to achieve uniform and reliable light emission from these EL fibers. Slot-die coating offers this control and increases the rate of EL fiber production. Here, we report a highly adaptable, cost-effective 3D printing model for developing slot dies used in automatic coating systems. The resulting slot-die coating system enables rapid, reliable production of alternating current powder-based EL (ACPEL) fibers and can be adapted for many material systems. The benefits of this system over dip-coating for roll-to-roll production of EL fibers are demonstrated in this work.
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Kazemi, Pezhman; Khalid, Mohammad Hassan; Pérez Gago, Ana; Kleinebudde, Peter; Jachowicz, Renata; Szlęk, Jakub; Mendyk, Aleksander
2017-01-01
Dry granulation using roll compaction is a typical unit operation for producing solid dosage forms in the pharmaceutical industry. Dry granulation is commonly used if the powder mixture is sensitive to heat and moisture and has poor flow properties. The output of roll compaction is compacted ribbons that exhibit different properties based on the adjusted process parameters. These ribbons are then milled into granules and finally compressed into tablets. The properties of the ribbons directly affect the granule size distribution (GSD) and the quality of final products; thus, it is imperative to study the effect of roll compaction process parameters on GSD. The understanding of how the roll compactor process parameters and material properties interact with each other will allow accurate control of the process, leading to the implementation of quality by design practices. Computational intelligence (CI) methods have a great potential for being used within the scope of quality by design approach. The main objective of this study was to show how the computational intelligence techniques can be useful to predict the GSD by using different process conditions of roll compaction and material properties. Different techniques such as multiple linear regression, artificial neural networks, random forest, Cubist and k-nearest neighbors algorithm assisted by sevenfold cross-validation were used to present generalized models for the prediction of GSD based on roll compaction process setting and material properties. The normalized root-mean-squared error and the coefficient of determination (R2) were used for model assessment. The best fit was obtained by Cubist model (normalized root-mean-squared error =3.22%, R2=0.95). Based on the results, it was confirmed that the material properties (true density) followed by compaction force have the most significant effect on GSD. PMID:28176905
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Kazemi, Pezhman; Khalid, Mohammad Hassan; Pérez Gago, Ana; Kleinebudde, Peter; Jachowicz, Renata; Szlęk, Jakub; Mendyk, Aleksander
2017-01-01
Dry granulation using roll compaction is a typical unit operation for producing solid dosage forms in the pharmaceutical industry. Dry granulation is commonly used if the powder mixture is sensitive to heat and moisture and has poor flow properties. The output of roll compaction is compacted ribbons that exhibit different properties based on the adjusted process parameters. These ribbons are then milled into granules and finally compressed into tablets. The properties of the ribbons directly affect the granule size distribution (GSD) and the quality of final products; thus, it is imperative to study the effect of roll compaction process parameters on GSD. The understanding of how the roll compactor process parameters and material properties interact with each other will allow accurate control of the process, leading to the implementation of quality by design practices. Computational intelligence (CI) methods have a great potential for being used within the scope of quality by design approach. The main objective of this study was to show how the computational intelligence techniques can be useful to predict the GSD by using different process conditions of roll compaction and material properties. Different techniques such as multiple linear regression, artificial neural networks, random forest, Cubist and k-nearest neighbors algorithm assisted by sevenfold cross-validation were used to present generalized models for the prediction of GSD based on roll compaction process setting and material properties. The normalized root-mean-squared error and the coefficient of determination ( R 2 ) were used for model assessment. The best fit was obtained by Cubist model (normalized root-mean-squared error =3.22%, R 2 =0.95). Based on the results, it was confirmed that the material properties (true density) followed by compaction force have the most significant effect on GSD.
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Deformation and annealing response of TD-nickel chromium sheet
NASA Technical Reports Server (NTRS)
Kane, R. D.; Ebert, L. J.
1973-01-01
The deformation and annealing response of TD-nickel chromium (TD-NiCr) 0.1 inch thick sheet was examined using various cold-rolling and annealing treatments. Upon annealing (above 816 C (1500 F), the as-received material was converted from an initially ultra-fine grain size (average grain dimension 0.51 micron) to a large grain structure. Increases in grain size by a factor of 100 to 200 were observed for this transformation. However, in those material states where the large grain transformation was absent, a fine grain recrystallized structure formed upon annealing (above 732 C (1350 F)). The deformation and annealing response of TD-NiCr sheet was evaluated with respect to the processing related variables as mode and severity of deformation and annealing temperature. Results indicate that the large grain transformation, classical primary recrystallization occurs. Using selected materials produced during the deformation and annealing study, the elevated temperature tensile properties of TD-NiCr sheet were examined in the temperature range 593 C (1100 F) to 1093 C (2000 F). It was observed that the elevated temperature tensile properties of TD-NiCr sheet could be optimized by the stabilization of a large grain size in this material using the cold working and/or annealing treatments developed during the present investigation.
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NASA Astrophysics Data System (ADS)
Cha, Joon-Hyeon; Kim, Su-Hyeon; Lee, Yun-Soo; Kim, Hyoung-Wook; Choi, Yoon Suk
2016-09-01
Multi-layered Al alloy sheets can exhibit unique properties by the combination of properties of component materials. A poor corrosion resistance of high strength Al alloys can be complemented by having a protective surface with corrosion resistant Al alloys. Here, a special care should be taken regarding the heat treatment of multi-layered Al alloy sheets because dissimilar Al alloys may exhibit unexpected interfacial reactions upon heat treatment. In the present study, A6022/A7075/A6022 sheets were fabricated by a cold roll-bonding process, and the effect of the heat treatment on the microstructure and mechanical properties was examined. The solution treatment gave rise to the diffusion of Zn, Mg, Cu and Si elements across the core/clad interface. In particular, the pronounced diffusion of Zn, which is a major alloying element (for solid-solution strengthening) of the A7075 core, resulted in a gradual hardness change across the core/clad interface. Mg2Si precipitates and the precipitate free zone were also formed near the interface after the heat treatment. The heat-treated sheet showed high strengths and reasonable elongation without apparent deformation misfit or interfacial delamination during the tensile deformation. The high strength of the sheet was mainly due to the T4 and T6 heat treatment of the A7075 core.
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Cryogenic Testing of Different Seam Concepts for Multilayer Insulation Systems
NASA Technical Reports Server (NTRS)
Johnson, Wesley L.; Fesmire, J. E.
2009-01-01
Recent testing in a cylindrical, comparative cryostat at the Cryogenics Test Laboratory has focused on various seam concepts for multilayer insulation systems. Three main types of seams were investigated: straight overlap, fold-over, and roll wrapped. Each blanket was comprised of 40 layer pairs of reflector and spacer materials. The total thickness was approximately 12.5-mm, giving an average layer density of 32 layers per centimeter. The blankets were tested at high vacuum, soft vacuum, and no vacuum using liquid nitrogen to maintain the cold boundary temperature at 77 K. Test results show that all three seam concepts are all close in thermal performance; however the fold-over method provides the lowest heat flux. For the first series of tests, seams were located 120 degrees around the circumference of the cryostat from the previous seam. This technique appears to have lessened the degradation of the blanket due to the seams. In a follow-on test, a 20 layer blanket was tested in a roll wrapped configuration and then cut down the side of the cylinder, taped together, and re-tested. This test result shows the thermal performance impact of having the seams all in one location versus having the seams clocked around the vessel. This experimental investigation indicates that the method of joining the seams in multilayer insulation systems is not as critical as the quality of the installation process.
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Determination of the Emissivity of Materials
1962-12-31
testing. The window is protected by a magnetically-ope-ated rolling disc shutter. Bakeout heaters are provided to outgas the chamber before testing...nitrogen cold trap over a period of two hours. During this period the chamber was baked out at 350 °F. The ion-gettering pump was then started and the...If the chamber had been contaminated by previous testing, it was baked out at 350 °F during pump-down. During testing, the chamber walls were cooled to
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Polyfibroblast: A Self-Healing and Galvanic Protection Additive
2013-03-22
polyurethane-urea (MCPU). When scratched, the foaming action of a propellant ejects the resin from the broken tubes and completely fills the crack . No...Resistivities of Control NCP and Enhanced NCP primers are 5xl06 and UxlO6 Ohm/sq respectively indicating we may be able to use simple enamel rater...instrumentation to evaluate self-healing. 1. Enamel rater evaluation underway. 2. 1 |im films of OTS prepared on Cold Rolled Steel and Blasted Steel panels
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USSR and Eastern Europe Scientific Abstracts, Materials Science and Metallurgy. Number 40.
1976-11-01
means of increasing the deformability of two- phase martensite - ferrite steels during subsequent cold rolling, as well as austenite- ferrite steels ...carbon steel , VT-4 titanium alloy and M-l copper . The specimens were placed in July 1972 and removed in April 1974. Tables are given summarizing...between the degree of development of the a -*• y conversion at the deformation focus in steels of the martensite - ferrite class and the position of
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NASA Astrophysics Data System (ADS)
Sohn, Seok Su; Song, Hyejin; Kim, Jung Gi; Kwak, Jai-Hyun; Kim, Hyoung Seop; Lee, Sunghak
2016-02-01
Tensile properties of recently developed automotive high-strength steels containing about 10 wt pct of Mn and Al are superior to other conventional steels, but the active commercialization has been postponed because they are often subjected to cracking during formation or to the delayed fracture after formation. Here, the delayed fracture behavior of a ferrite-austenite duplex lightweight steel whose microstructure was modified by a batch annealing treatment at 1023 K (750 °C) prior to cold rolling was examined by HCl immersion tests of cup specimens, and was compared with that of an unmodified steel. After the batch annealing, band structures were almost decomposed as strong textures of {100}<011> α-fibers and {111}<112> γ-fibers were considerably dissolved, while ferrite grains were refined. The steel cup specimen having this modified microstructure was not cracked when immersed in an HCl solution for 18 days, whereas the specimen having unmodified microstructure underwent the delayed fracture within 1 day. This time delayed fracture was more critically affected by difference in deformation characteristics such as martensitic transformation and deformation inhomogeneity induced from concentration of residual stress or plastic strain, rather than the difference in initial microstructures. The present work gives a promise for automotive applications requiring excellent mechanical and delayed fracture properties as well as reduced specific weight.
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Chang, E-E; Chen, Tse-Lun; Pan, Shu-Yuan; Chen, Yi-Hung; Chiang, Pen-Chi
2013-09-15
In this study, direct and indirect carbonation of basic oxygen furnace slag (BOFS) coupled with cold-rolling wastewater (CRW) was carried out via a rotating packed bed (RPB). The solid products were qualitatively characterized by scanning electron microscopy (SEM) and X-ray diffraction (XRD) and quantitatively analyzed with thermogravimetric analysis (TGA). The leachate was analyzed with inductively coupled plasma-optical emission spectroscopy (ICP-OES). The results indicate that the maximum achievable carbonation conversion (MACC) of BOFS was 90.7%, corresponding to a capture capacity of 0.277 g CO₂/g of BOFS, by direct carbonation with CRW under a rotation speed of 750 rpm at 30 °C for 20 min. In addition, CO₂ mass balance among the gas, liquid, and solid phases within an RPB was well-developed, with an error less than 10%, to confirm the actual CO₂ capture capacity of BOFS with precision and accuracy. Furthermore, a reaction kinetic model based on mass balance was established to determine the reaction rate constant for various liquid agents (CRW and pure water). It was concluded that co-utilization of alkaline wastes including BOFS and CRW via the RPB is a novel approach for both enhancing CO₂ capture capacity and reducing the environmental impacts of alkaline wastes. Copyright © 2013 Elsevier B.V. All rights reserved.
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The interface character distribution of cold-rolled and annealed duplex stainless steel
DOE Office of Scientific and Technical Information (OSTI.GOV)
Fang, Xiaoying, E-mail: fxy@sdut.edu.cn
The interface character distributions (ICDs) of cold-rolled and annealed duplex stainless steel specimens, previously solid-solution-heated (SHT) at 1573 K and 1323 K, are investigated using electron backscatter diffraction (EBSD) and five-parameter analysis (FPA). For the δ-ferrite phase, high concentrations of low angle grain boundaries (LAGBs) are developed, and the boundary planes are predominantly oriented on (111). High angle grain boundaries (HAGBs) with misorientations ranging from 50{sup o} to 60° are mostly pure tilt boundaries, and the boundary planes are primarily located on (112). For the austenite phase, very high density of coherent twin boundaries are introduced, implying that the boundarymore » planes are exactly oriented on (111). The phase boundary character distribution (PBPD) appears to be connected with the K-S and N-W orientation relationships (ORs) terminating on (110) {sub F}‖(111) {sub A} and (110){sub F}‖(hkl){sub A}, respectively. - Highlights: •Five-parameter analysis was used to determine interface character distribution. •ICD results of statistical meaning were achieved. •Initial microstructure has a significant effect on ICD. •Low and high angle GBs in δ phase prefer in (111) and (112) planes, respectively. •K-S phase boundaries terminate on (110){sub F}‖(111){sub A} while N-W ones on (110){sub F}‖(hkl){sub A}.« less
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Characterization of the α phase nucleation in a two-phase metastable β titanium alloy
NASA Astrophysics Data System (ADS)
Lenain, A.; Clément, N.; Jacques, P. J.; Véron, M.
2005-12-01
Beta titanium alloys are increasingly the best choice for automotive and aerospace applications due to their high performance-to-density ratio. Among these alloys, the TIMETAL Ti-LCB is already used in the automotive industry because it presents excellent mechanical properties and a lower cost compared with other Ti alloys. The current study deals with the characterization of the nucleation and growth of the α phase in several thermomechanical processes, because the distribution and size of the α phase strongly influence the mechanical properties of the resulting microstructures. Several heat treatments were conducted after either cold rolling or annealing. The resulting microstructures were characterized by scanning electron microscopy, transmission electron microscopy, x-ray diffraction, or electron backscatter diffraction. It was observed that the morphology and the volume fraction of the α phase are strongly dependent on the holding temperature, on the heating or cooling rate, and on the β grain size.
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Influence of carbon conductive additives on electrochemical double-layer supercapacitor parameters
NASA Astrophysics Data System (ADS)
Kiseleva, E. A.; Zhurilova, M. A.; Kochanova, S. A.; Shkolnikov, E. J.; Tarasenko, A. B.; Zaitseva, O. V.; Uryupina, O. V.; Valyano, G. V.
2018-01-01
Electrochemical double-layer capacitors (EDLC) offer energy storage technology, highly demanded for rapid transition processes in transport and stationary applications, concerned with fast power fluctuations. Rough structure of activated carbon, widely used as electrode material because of its high specific area, leads to poor electrode conductivity. Therefore there is the need for conductive additive to decrease internal resistance and to achieve high specific power and high specific energy. Usually carbon blacks are widely used as conductive additive. In this paper electrodes with different conductive additives—two types of carbon blacks and single-walled carbon nanotubes—were prepared and characterized in organic electrolyte-based EDLC cells. Electrodes are based on original wood derived activated carbon produced by potassium hydroxide high-temperature activation at Joint Institute for High Temperatures RAS. Electrodes were prepared from slurry by cold-rolling. For electrode characterization cyclic voltammetry, impedance spectra analysis, equivalent series resistance measurements and galvanostatic charge-discharge were used.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Chang, L. L.; Wang, Y. D.; Ren, Y.
Microstructure evolution, mechanical behaviors of cold rolled Ti-Nb alloys with different Nb contents subjected to different heat treatments were investigated. Here, optical microstructure and phase compositions of Ti-Nb alloys were characterized using optical microscopy and X-ray diffractometre, while mechanical behaviors of Ti-Nb alloys were examined by using tension tests. Stress-induced martensitic transformation in a Ti-30. at%Nb binary alloy was in-situ explored by synchrotron-based high-energy X-ray diffraction (HE-XRD). The results obtained suggested that mechanical behavior of Ti-Nb alloys, especially Young's modulus was directly dependent on chemical compositions and heat treatment process. According to the results of HE-XRD, α"-V1 martensite generated priormore » to the formation of α"-V2 during loading and a partial reversible transformation from α"-V1 to β phase was detected while α"-V2 tranformed to β completely during unloading.« less
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Adaptive attenuation of aliased ground roll using the shearlet transform
NASA Astrophysics Data System (ADS)
Hosseini, Seyed Abolfazl; Javaherian, Abdolrahim; Hassani, Hossien; Torabi, Siyavash; Sadri, Maryam
2015-01-01
Attenuation of ground roll is an essential step in seismic data processing. Spatial aliasing of the ground roll may cause the overlap of the ground roll with reflections in the f-k domain. The shearlet transform is a directional and multidimensional transform that separates the events with different dips and generates subimages in different scales and directions. In this study, the shearlet transform was used adaptively to attenuate aliased and non-aliased ground roll. After defining a filtering zone, an input shot record is divided into segments. Each segment overlaps adjacent segments. To apply the shearlet transform on each segment, the subimages containing aliased and non-aliased ground roll, the locations of these events on each subimage are selected adaptively. Based on these locations, mute is applied on the selected subimages. The filtered segments are merged together, using the Hanning function, after applying the inverse shearlet transform. This adaptive process of ground roll attenuation was tested on synthetic data, and field shot records from west of Iran. Analysis of the results using the f-k spectra revealed that the non-aliased and most of the aliased ground roll were attenuated using the proposed adaptive attenuation procedure. Also, we applied this method on shot records of a 2D land survey, and the data sets before and after ground roll attenuation were stacked and compared. The stacked section after ground roll attenuation contained less linear ground roll noise and more continuous reflections in comparison with the stacked section before the ground roll attenuation. The proposed method has some drawbacks such as more run time in comparison with traditional methods such as f-k filtering and reduced performance when the dip and frequency content of aliased ground roll are the same as those of the reflections.
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NASA Astrophysics Data System (ADS)
Silva, J. M.; Baêta Júnior, E. S.; Moraes, N. R. D. C.; Botelho, R. A.; Felix, R. A. C.; Brandao, L.
2017-01-01
The purpose of this work was to study the influence of different kinds of rolling on the magnetic properties of NOG steel, an electric steel widely used in electrical motors. These properties are highly correlated with the crystallographic texture of the material, which can be changed by rolling. Three kinds of rolling were examined: conventional rolling, cross-rolling and asymmetrical rolling. The crystallographic texture was determined by X-ray diffraction and the magnetic properties were calculated from a theoretical model that related the magnetic induction to crystallographic texture through the anisotropy energy. The results show that cross-rolling yields higher values of magnetic induction than the other processes.
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Microstructure based procedure for process parameter control in rolling of aluminum thin foils
NASA Astrophysics Data System (ADS)
Johannes, Kronsteiner; Kabliman, Evgeniya; Klimek, Philipp-Christoph
2018-05-01
In present work, a microstructure based procedure is used for a numerical prediction of strength properties for Al-Mg-Sc thin foils during a hot rolling process. For this purpose, the following techniques were developed and implemented. At first, a toolkit for a numerical analysis of experimental stress-strain curves obtained during a hot compression testing by a deformation dilatometer was developed. The implemented techniques allow for the correction of a temperature increase in samples due to adiabatic heating and for the determination of a yield strength needed for the separation of the elastic and plastic deformation regimes during numerical simulation of multi-pass hot rolling. At the next step, an asymmetric Hot Rolling Simulator (adjustable table inlet/outlet height as well as separate roll infeed) was developed in order to match the exact processing conditions of a semi-industrial rolling procedure. At each element of a finite element mesh the total strength is calculated by in-house Flow Stress Model based on evolution of mean dislocation density. The strength values obtained by numerical modelling were found in a reasonable agreement with results of tensile tests for thin Al-Mg-Sc foils. Thus, the proposed simulation procedure might allow to optimize the processing parameters with respect to the microstructure development.
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In-situ Roll-to-Roll Printing of Highly Efficient Organic Solar Cells
DOE Office of Scientific and Technical Information (OSTI.GOV)
Bao, Zhenan; Toney, Michael; Clancy, Paulette
2016-05-30
This project focuses on developing a roll-to-roll printing setup for organic solar cells with the capability to follow the film formation in situ with small and wide angle X-ray scattering, and to improve the performance of printed organic solar cells. We demonstrated the use of the printing setup to capture important aspects of existing industrial printing methods, which ensures that the solar cell performance achieved in our printing experiments would be largely retained in an industrial fabrication process. We employed both known and newly synthesized polymers as the donor and acceptor materials, and we studied the morphological changes in realmore » time during the printing process by X-ray scattering. Our experimental efforts are also accompanied by theoretical modeling of both the fluid dynamic aspects of the printing process and the nucleation and crystallization kinetics during the film formation. The combined insight into the printing process gained from the research provides a detailed understanding of the factors governing the printed solar cell’s performance. Finally using the knowledge we gained, we demonstrated large area ( > 10 cm2) printed organic solar cells with more than 5 percent power conversion efficiency, which is best achieved performance for roll-to-roll printed organic solar cells.« less
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Mariner Mars 1971 attitude control subsystem
NASA Technical Reports Server (NTRS)
Edmunds, R. S.
1974-01-01
The Mariner Mars 1971 attitude control subsystem (ACS) is discussed. It is comprised of a sun sensor set, a Canopus tracker, an inertial reference unit, two cold gas reaction control assemblies, two rocket engine gimbal actuators, and an attitude control electronics unit. The subsystem has the following eight operating modes: (1) launch, (2) sun acquisition, (3) roll search, (4) celestial cruise, (5) all-axes inertial, (6) roll inertial, (7) commanded turn, and (8) thrust vector control. In the celestial cruise mode, the position control is held to plus or minus 0.25 deg. Commanded turn rates are plus or minus 0.18 deg/s. The attitude control logic in conjunction with command inputs from other spacecraft subsystems establishes the ACS operating mode. The logic utilizes Sun and Canopus acquisition signals generated within the ACS to perform automatic mode switching so that dependence of ground control is minimized when operating in the sun acquisition, roll search, and celestial cruise modes. The total ACS weight is 65.7 lb, and includes 5.4 lb of nitrogen gas. Total power requirements vary from 9 W for the celestial cruise mode to 54 W for the commanded turn mode.
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Temperature corrections in routine spirometry.
Cramer, D; Peacock, A; Denison, D
1984-01-01
Forced expiratory volume (FEV1) and forced vital capacity (FVC) were measured in nine normal subjects with three Vitalograph and three rolling seal spirometers at three different ambient temperatures (4 degrees C, 22 degrees C, 32 degrees C). When the results obtained with the rolling seal spirometer were converted to BTPS the agreement between measurements in the three environments improved, but when the Vitalograph measurements obtained in the hot and cold rooms were converted an error of up to 13% was introduced. The error was similar whether ambient or spirometer temperatures were used to make the conversion. In an attempt to explain the behaviour of the Vitalograph spirometers the compliance of their bellows was measured at the three temperatures. It was higher at the higher temperature (32 degrees C) and lower at the lower temperature (4 degrees C) than at the normal room temperature. These changes in instrument compliance could account for the differences in measured values between the two types of spirometer. It is concluded that the ATPS-BTPS conversion is valid and necessary for measurements made with rolling seal spirometers, but can cause substantial error if it is used for Vitalograph measurements made under conditions other than normal room temperature. PMID:6495245
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Chen, Ming-biao; Li, Yong-wei; Tan, Yuan-biao; Ma, Min; Wang, Xue-min; Liu, Wen-chang
2015-03-01
At present the study of relation between microstructure, texture and performance of CC 5083 aluminium alloy after cold tolling and recrystallization processes is still finitude. So that the use of the CC 5083 aluminium alloy be influenced. Be cased into electrical furnace, hot up with unlimited speed followed the furnace hot up to different temperature and annealed 2h respectively, and be cased into salt-beth furnace, hot up quickly to different temperature and annealed 30 min respectively for CC 5083 and CC 5182 aluminum alloy after cold roling with 91.5% reduction. The microstructure be watched use metallographic microscope, the texture be inspected by XRD. The start temperature of recrystallization and grain grow up temperature within annealing in the electric furnace of CC 5083 aluminum alloy board is 343 degrees C, and the shap of grain after grow up with long strip (the innovation point ); The start temperature of recrystallization within annealling in the salt bath furnace of CC 5083 is 343 degrees C. The start temperature and end temperature of recrystallization within annealling of CC 5083 and CC 5182 aluminum alloy is 371 degrees C. The grain grow up outstanding of cold rooled CC 5152 aluminum alloy after annealed with 454 degrees C in the electric furnace and salt bath furnace. The start temperature of grain grow up of CC 5083 alluminurn alloy annealed in the electric furnace and salt bath furnace respectively is higher than the start temperature of grain grow up of CC 5182 alluminum alloy annealed in the electric furnace and salt bath furnace respectively. The strat temperature of recrystallization grain grow up is higher than which annealled with other three manner annealing process. The recrystallization temperature of CC 5182 annealed in the salt bath furnace is higher than which annealed in the electric furnace. The recrystallization temperature of the surface layer of CC 5083 and CC 5182 aluminum alloy is higher than the inner layer (the innovation point). There is a difference each other of the structure and the texture of the four manner annealing aluminum alloy (the innovation point). There is a little difference at the recrystallization processes course reflectived by the observe results of structure transform and by the examination results of texture transmission.
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Material-Process-Performance Relationships for Roll-to-Roll Coated PEM Electrodes
DOE Office of Scientific and Technical Information (OSTI.GOV)
Mauger, Scott; Neyerlin, K.C.; Stickel, Jonathan
2017-04-26
Roll-to-roll (R2R) coating is the most economical and highest throughput method for producing fuel cell electrodes. R2R coating encompasses many different methodologies to create uniform films on a moving web substrate. Here we explore two coating methods, gravure and slot die, to understand the impacts of each on film uniformity and performance.
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Deformation and recrystallization behavior of super high-purity niobium for SRF cavity
NASA Astrophysics Data System (ADS)
Yamaguchi, Y.; Doryo, H.; Yuasa, M.; Miyamoto, H.; Yamanaka, M.
2017-05-01
Deformation and recyrstallization behavior of pure niobium was investigated in order to clarify the origin of its low hydro-formability despite of its high ductility comparable with pure iron. It was found that pure niobium exhibits lower strain hardening in cold rolling compared with pure iron. Furthermore, in post-deformation annealing, the hardness of niobium decreased monotonously with an increase of temperature, and the typical sharp drop by recrystallization was not evident. This softening behavior was contrasted with the high-purity iron. It is suggested that niobium exhibit the so-called in-situ recrystallization possibly because of low elastic modulus and low accumulative plastic strain energy in spite of high melting temperature. The low hydro-formability of pure niobium sheets or tubes is caused by its low strain hardening and its unique plastic anisotropy which is associated with this recovered residual rolled texture.
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New high-strength, high-conductivity Cu-Ag alloy sheets
DOE Office of Scientific and Technical Information (OSTI.GOV)
Sakai, Y.; Inoue, K.; Maeda, H.
1995-04-01
A sheet-conductor fabrication method has been developed for Cu-Ag alloys containing 6--24 wt% Ag in which high-strength and high-conductivity are obtained by coldworking combined with intermediate heat treatments. The intermediate heat treatments were repeated three times at 400--450 C for 1--2 h at appropriate stages of cold-rolling. The optimized Cu-24 wt% Ag alloy sheet with a 96% reduction ratio shows an ultimate tensile strength of 1,050 MPa and an electrical conductivity of 75% IACS at room temperature. Anisotropy in the strength with respect to the rolling direction is less than 10%, and no anisotropy in the electrical conductivity occurs. Themore » authors demonstrated the ability to manufacture the Cu-Ag sheets for Bitter magnet on a commercial basis. The sheets fabricated by this method are promising as conductors for high-field Bitter magnet coils.« less
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Controlled cooling technology for bar and rod mills -- Computer simulation and operational results
DOE Office of Scientific and Technical Information (OSTI.GOV)
Mauk, P.J.; Kruse, M.; Plociennik, U.
The Controlled Cooling Technology (CCT) developed by SMS to simulate the rolling process and automatic control of the water cooling sections is presented. The Controlled Rolling and Cooling Technology (CRCT) model is a key part of the CCT system. It is used to simulate temperature management for the rolling stock on the computer before the actual rolling process takes place. This makes it possible to dispense with extensive rolling tests in the early stages of project planning and to greatly reduce the extent of such tests prior to the start of commercial production in a rolling mill. The CRCT modelmore » has been in use at Von Moos Stahl Ag for three years. It demonstrates that, by targeted improvement of the set-up values in both the technology and the plant, it is possible to improve microstructure quality and achieve better geometrical parameters in the rolled products. Also, the results gained with the CCT system in practical operation at the Kia Steel Bar Mill, Kunsan, Korea, are presented.« less
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Coupled thermal-fluid-mechanics analysis of twin roll casting of A7075 aluminum alloy
NASA Astrophysics Data System (ADS)
Lee, Yun-Soo; Kim, Hyoung-Wook; Cho, Jae-Hyung; Chun, Se-Hwan
2017-09-01
Better understanding of temperature distribution and roll separation force during twin roll casting of aluminum alloys is critical to successfully fabricate good quality of aluminum strips. Therefore, the simulation techniques are widely applied to understand the twin roll casting process in a comprehensive way and to reduce the experimental time and cost of trial and error. However, most of the conventional approaches are considered thermally coupled flow, or thermally coupled mechanical behaviors. In this study, a fully coupled thermal-fluid-mechanical analysis of twin roll casting of A7075 aluminum strips was carried out using the finite element method. Temperature profile, liquid fraction and metal flow of aluminum strips with different thickness were predicted. Roll separation force and roll temperatures were experimentally obtained from a pilot-scale twin roll caster, and those results were compared with model predictions. Coupling the fluid of the liquid melt to the thermal and mechanical modeling reasonably predicted roll temperature distribution and roll separation force during twin roll casting.
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Multiscale structural changes of atomic order in severely deformed industrial aluminum
NASA Astrophysics Data System (ADS)
Samoilenko, Z. A.; Ivakhnenko, N. N.; Pushenko, E. I.; Pashinskaya, E. G.; Varyukhin, V. N.
2016-02-01
The regularities of multiscale structural changes in the atomic order of the aluminum alloy AD-1 after a severe cold plastic deformation by conventional rolling in smooth rolls or in rolls with relief recesses favorable for shear deformation have been investigated. It has been found that there are four types of structural fractions that differ in scale and perfection of atomic order: crystallographic planes with a long-range order; nanoscale fragments of the planes ( D = 100-300 Å) with an incipient long-range order; smaller groups of atoms ( D = 20-30 Å) of amorphized structure; and the least ordered structural fraction of intercluster medium, keeping only a short-range atomic order (2-3 interatomic distances, 10 Å). The presence of diffuse halo bands in the region of intense Debye lines indicates phase transitions of the order → disorder type with the formation of one to three groups of amorphous clusters with the dominance, in the nanometer scale, of the atomic order characteristic of the family of planes (111), (220), and (311) of crystalline aluminum. We have found a dynamic phase transition with the changing crystallographic order of aluminum, with the matrix structure of a face-centered cubic (FCC) lattice, in the form of nanosized local groups of atoms, that is, the deformation clusters of aluminum with a simple cubic K6 lattice. In the case of conventional rolling, the development of large clusters 50-500 Å in size is observed; however, in the use of rolls with relief recesses, the difference in the sizes of the clusters is one half as much: 50-250 Å. Based on the analysis of the integrated intensity of incoherent X-ray scattering by the samples, we have elucidated the nature of the lowest measured density for the sample subjected to conventional rolling, which consists in the volume concentration of disorderly arranged atoms, the highest of the compared structures, which indicates the formation therein of the greatest amount of fluctuation "voids."
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Spectral characteristics of wake vortex sound during roll-up
DOT National Transportation Integrated Search
2003-12-01
This report presents an analysis of the sound spectra generated by a trailing aircraft vortex during its rolling-up process. The : study demonstrates that a rolling-up vortex could produce low frequency (less than 100 Hz) sound with very high intensi...
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Ring rolling process simulation for geometry optimization
NASA Astrophysics Data System (ADS)
Franchi, Rodolfo; Del Prete, Antonio; Donatiello, Iolanda; Calabrese, Maurizio
2017-10-01
Ring Rolling is a complex hot forming process where different rolls are involved in the production of seamless rings. Since each roll must be independently controlled, different speed laws must be set; usually, in the industrial environment, a milling curve is introduced to monitor the shape of the workpiece during the deformation in order to ensure the correct ring production. In the present paper a ring rolling process has been studied and optimized in order to obtain anular components to be used in aerospace applications. In particular, the influence of process input parameters (feed rate of the mandrel and angular speed of main roll) on geometrical features of the final ring has been evaluated. For this purpose, a three-dimensional finite element model for HRR (Hot Ring Rolling) has been implemented in SFTC DEFORM V11. The FEM model has been used to formulate a proper optimization problem. The optimization procedure has been implemented in the commercial software DS ISight in order to find the combination of process parameters which allows to minimize the percentage error of each obtained dimension with respect to its nominal value. The software allows to find the relationship between input and output parameters applying Response Surface Methodology (RSM), by using the exact values of output parameters in the control points of the design space explored through FEM simulation. Once this relationship is known, the values of the output parameters can be calculated for each combination of the input parameters. After the calculation of the response surfaces for the selected output parameters, an optimization procedure based on Genetic Algorithms has been applied. At the end, the error between each obtained dimension and its nominal value has been minimized. The constraints imposed were the maximum values of standard deviations of the dimensions obtained for the final ring.
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How rolling forecasting facilitates dynamic, agile planning.
Miller, Debra; Allen, Michael; Schnittger, Stephanie; Hackman, Theresa
2013-11-01
Rolling forecasting may be used to replace or supplement the annual budget process. The rolling forecast typically builds on the organization's strategic financial plan, focusing on the first three years of plan projections and comparing the strategic financial plan assumptions with the organization's expected trajectory. Leaders can then identify and respond to gaps between the rolling forecast and the strategic financial plan on an ongoing basis.
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Rupich, Martin W.; Sathyamurthy, Srivatsan; Fleshler, Steven
We demonstrate a twofold increase in the in-field critical current of AMSC's standard 2G coil wire by irradiation with 18-MeV Au ions. The optimum pinning enhancement is achieved with a dose of 6 × 10 11 Au ions/cm 2. Although the 77 K, self-field critical current is reduced by about 35%, the in-field critical current (H//c) shows a significant enhancement between 4 and 50 K in fields > 1 T. The process was used for the roll-to-roll irradiation of AMSC's standard 46-mm-wide production coated conductor strips, which were further processed into standard copper laminated coil wire. The long-length wires showmore » the same enhancement as attained with short static irradiated samples. The roll-to-roll irradiation process can be incorporated in the standard 2G wire manufacturing, with no modifications to the current process. In conclusion, the enhanced performance of the wire will benefit rotating machine and magnet applications.« less
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Rupich, Martin W.; Sathyamurthy, Srivatsan; Fleshler, Steven
We demonstrate a twofold increase in the in-field critical current of AMSC's standard 2G coil wire by irradiation with 18-MeV Au ions. The optimum pinning enhancement is achieved with a dose of 6 x 10(11) Au ions/cm(2). Although the 77 K, self-field critical current is reduced by about 35%, the in-field critical current (H//c) shows a significant enhancement between 4 and 50 K in fields > 1 T. The process was used for the roll-to-roll irradiation of AMSC's standard 46-mm-wide production coated conductor strips, which were further processed into standard copper laminated coil wire. The long-length wires show the samemore » enhancement as attained with short static irradiated samples. The roll-to-roll irradiation process can be incorporated in the standard 2G wire manufacturing, with no modifications to the current process. The enhanced performance of the wire will benefit rotating machine and magnet applications.« less
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DOE Office of Scientific and Technical Information (OSTI.GOV)
Hamad, Kotiba; Chung, Bong Kwon; Ko, Young Gun, E-mail: younggun@ynu.ac.kr
2014-08-15
This paper reports the effect of the deformation path on the microstructure, microhardness, and texture evolution of interstitial free (IF) steel processed by differential speed rolling (DSR) method. For this purpose, total height reductions of 50% and 75% were imposed on the samples by a series of differential speed rolling operations with various height reductions per pass (deformation levels) ranging from 10 to 50% under a fixed roll speed ratio of 1:4 for the upper and lower rolls, respectively. Microstructural observations using transmission electron microscopy and electron backscattered diffraction measurements showed that the samples rolled at deformation level of 50%more » had the finest mean grain size (∼ 0.5 μm) compared to the other counterparts; also the samples rolled at deformation level of 50% showed a more uniform microstructure. Based on the microhardness measurements along the thickness direction of the deformed samples, gradual evolution of the microhardness value and its homogeneity was observed with the increase of the deformation level per pass. Texture analysis showed that, as the deformation level per pass increased, the fraction of alpha fiber and gamma fiber in the deformed samples increased. The textures obtained by the differential speed rolling process under the lubricated condition would be equivalent to those obtained by the conventional rolling. - Highlights: • Effect of DSR deformation path on microstructure of IF steel is significant. • IF steel rolled at deformation level of 50% has the ultrafine grains of ∼ 0.5 μm. • Rolling texture components are pronounced with increasing deformation level.« less
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NASA Astrophysics Data System (ADS)
Moya Riffo, A.; Vicente Alvarez, M. A.; Santisteban, J. R.; Vizcaino, P.; Limandri, S.; Daymond, M. R.; Kerr, D.; Okasinski, J.; Almer, J.; Vogel, S. C.
2017-05-01
This work presents a detailed characterization of the microstructural and crystallographic texture changes observed in the transition region in a weld between two Zircaloy-4 cold rolled and recrystallized plates. The microstructural study was performed by optical microscopy under polarized light and scanning electron microscopy (SEM). Texture changes were characterized at different lengthscales: in the micrometric size, orientation imaging maps (OIM) were constructed by electron backscatter diffraction (EBSD), in the millimetre scale, high energy XRD experiments were done at the Advanced Photon Source (USA) and compared to neutron diffraction texture determinations performed in the HIPPO instrument at Los Alamos National Laboratory. In the heat affected zone (HAZ) we observed the development of Widmanstätten microstructures, typical of the α(hcp) to β(bcc) phase transformation. Associated with these changes a rotation of the c-poles is found in the HAZ and fusion zone. While the base material shows the typical texture of a cold rolled plate, with their c-poles pointing 35° apart from the normal direction of the plate in the normal-transversal line, in the HAZ, c-poles align along the transversal direction of the plate and then re-orient along different directions, all of these changes occurring within a lengthscale in the order of mm. The evolution of texture in this narrow region was captured by both OIM and XRD, and is consistent with previous measurements done by Neutron Diffraction in the HIPPO diffractometer at Los Alamos National Laboratory, USA. The microstructural and texture changes along the HAZ were interpreted as arising due to the effect of differences in the cooling rate and β grain size on the progress of the different α variants during transformation. Fast cooling rates and large β grains are associated to weak variant selection during the β->α transformation, while slow cooling rates and fine β grains result in strong variant selection.