Deformation behaviors of three-dimensional graphene honeycombs under out-of-plane compression: Atomistic simulations and predictive modeling

NASA Astrophysics Data System (ADS)

Meng, Fanchao; Chen, Cheng; Hu, Dianyin; Song, Jun

2017-12-01

Combining atomistic simulations and continuum modeling, a comprehensive study of the out-of-plane compressive deformation behaviors of equilateral three-dimensional (3D) graphene honeycombs was performed. It was demonstrated that under out-of-plane compression, the honeycomb exhibits two critical deformation events, i.e., elastic mechanical instability (including elastic buckling and structural transformation) and inelastic structural collapse. The above events were shown to be strongly dependent on the honeycomb cell size and affected by the local atomic bonding at the cell junction. By treating the 3D graphene honeycomb as a continuum cellular solid, and accounting for the structural heterogeneity and constraint at the junction, a set of analytical models were developed to accurately predict the threshold stresses corresponding to the onset of those deformation events. The present study elucidates key structure-property relationships of 3D graphene honeycombs under out-of-plane compression, and provides a comprehensive theoretical framework to predictively analyze their deformation responses, and more generally, offers critical new knowledge for the rational bottom-up design of 3D networks of two-dimensional nanomaterials.

Universal behavior of the osmotically compressed cell and its analogy to the colloidal glass transition

PubMed Central

Zhou, E. H.; Trepat, X.; Park, C. Y.; Lenormand, G.; Oliver, M. N.; Mijailovich, S. M.; Hardin, C.; Weitz, D. A.; Butler, J. P.; Fredberg, J. J.

2009-01-01

Mechanical robustness of the cell under different modes of stress and deformation is essential to its survival and function. Under tension, mechanical rigidity is provided by the cytoskeletal network; with increasing stress, this network stiffens, providing increased resistance to deformation. However, a cell must also resist compression, which will inevitably occur whenever cell volume is decreased during such biologically important processes as anhydrobiosis and apoptosis. Under compression, individual filaments can buckle, thereby reducing the stiffness and weakening the cytoskeletal network. However, the intracellular space is crowded with macromolecules and organelles that can resist compression. A simple picture describing their behavior is that of colloidal particles; colloids exhibit a sharp increase in viscosity with increasing volume fraction, ultimately undergoing a glass transition and becoming a solid. We investigate the consequences of these 2 competing effects and show that as a cell is compressed by hyperosmotic stress it becomes progressively more rigid. Although this stiffening behavior depends somewhat on cell type, starting conditions, molecular motors, and cytoskeletal contributions, its dependence on solid volume fraction is exponential in every instance. This universal behavior suggests that compression-induced weakening of the network is overwhelmed by crowding-induced stiffening of the cytoplasm. We also show that compression dramatically slows intracellular relaxation processes. The increase in stiffness, combined with the slowing of relaxation processes, is reminiscent of a glass transition of colloidal suspensions, but only when comprised of deformable particles. Our work provides a means to probe the physical nature of the cytoplasm under compression, and leads to results that are universal across cell type. PMID:19520830

Deformation behavior of welded steel sandwich panels under quasi-static loading

DOT National Transportation Integrated Search

2011-03-01

This report describes engineering studies that were conducted to examine the deformation behavior of flat, welded steel sandwich panels under two quasi-static loading conditions: (1) uniaxial compression; and (2) bending with an indenter. Testing and...

Dynamic Deformation Behavior of Soft Material Using Shpb Technique and Pulse Shaper

NASA Astrophysics Data System (ADS)

Lee, Ouk Sub; Cho, Kyu Sang; Kim, Sung Hyun; Han, Yong Hwan

This paper presents a modified Split Hopkinson Pressure Bar (SHPB) technique to obtain compressive stress strain data for NBR rubber materials. An experimental technique with a modified the conventional SHPB has been developed for measuring the compressive stress strain responses of materials with low mechanical impedance and low compressive strengths, such as the rubber and the polymeric material. This paper uses an aluminum pressure bar to achieve a closer impedance match between the pressure bar and the specimen materials. In addition, a pulse shaper is utilized to lengthen the rising time of the incident pulse to ensure dynamic stress equilibrium and homogeneous deformation of NBR rubber materials. It is found that the modified technique can determine the dynamic deformation behavior of rubbers more accurately.

Multiscale Modeling of Polycrystalline NiTi Shape Memory Alloy under Various Plastic Deformation Conditions by Coupling Microstructure Evolution and Macroscopic Mechanical Response

PubMed Central

Jiang, Shuyong; Zhou, Tao; Tu, Jian; Shi, Laixin; Chen, Qiang; Yang, Mingbo

2017-01-01

Numerical modeling of microstructure evolution in various regions during uniaxial compression and canning compression of NiTi shape memory alloy (SMA) are studied through combined macroscopic and microscopic finite element simulation in order to investigate plastic deformation of NiTi SMA at 400 °C. In this approach, the macroscale material behavior is modeled with a relatively coarse finite element mesh, and then the corresponding deformation history in some selected regions in this mesh is extracted by the sub-model technique of finite element code ABAQUS and subsequently used as boundary conditions for the microscale simulation by means of crystal plasticity finite element method (CPFEM). Simulation results show that NiTi SMA exhibits an inhomogeneous plastic deformation at the microscale. Moreover, regions that suffered canning compression sustain more homogeneous plastic deformation by comparison with the corresponding regions subjected to uniaxial compression. The mitigation of inhomogeneous plastic deformation contributes to reducing the statistically stored dislocation (SSD) density in polycrystalline aggregation and also to reducing the difference of stress level in various regions of deformed NiTi SMA sample, and therefore sustaining large plastic deformation in the canning compression process. PMID:29027925

Multiscale Modeling of Polycrystalline NiTi Shape Memory Alloy under Various Plastic Deformation Conditions by Coupling Microstructure Evolution and Macroscopic Mechanical Response.

PubMed

Hu, Li; Jiang, Shuyong; Zhou, Tao; Tu, Jian; Shi, Laixin; Chen, Qiang; Yang, Mingbo

2017-10-13

Numerical modeling of microstructure evolution in various regions during uniaxial compression and canning compression of NiTi shape memory alloy (SMA) are studied through combined macroscopic and microscopic finite element simulation in order to investigate plastic deformation of NiTi SMA at 400 °C. In this approach, the macroscale material behavior is modeled with a relatively coarse finite element mesh, and then the corresponding deformation history in some selected regions in this mesh is extracted by the sub-model technique of finite element code ABAQUS and subsequently used as boundary conditions for the microscale simulation by means of crystal plasticity finite element method (CPFEM). Simulation results show that NiTi SMA exhibits an inhomogeneous plastic deformation at the microscale. Moreover, regions that suffered canning compression sustain more homogeneous plastic deformation by comparison with the corresponding regions subjected to uniaxial compression. The mitigation of inhomogeneous plastic deformation contributes to reducing the statistically stored dislocation (SSD) density in polycrystalline aggregation and also to reducing the difference of stress level in various regions of deformed NiTi SMA sample, and therefore sustaining large plastic deformation in the canning compression process.

Deformation behavior of welded steel sandwich panels under quasi-static loading

DOT National Transportation Integrated Search

2011-03-16

This paper summarizes basic research (i.e., testing and analysis) : conducted to examine the deformation behavior of flat-welded : steel sandwich panels under two types of quasi-static loading: : (1) uniaxial compression; and (2) bending through an i...

Deformation Response of Unsymmetrically Laminated Plates Subjected to Inplane Loading

NASA Technical Reports Server (NTRS)

Ochinero, Tomoya T.; Hyer, Michael W.

2002-01-01

This paper discusses the out-of-plane deformation behavior of unsymmetric cross-ply composite plates compressed inplane by displacing one edge of the plate a known amount. The plates are assumed to be initially flat and several boundary conditions are considered. Geometrically nonlinear behavior is assumed. The primary objectives are to study the out-of-plane behavior as a function of increasing inplane compression and to determine if bifurcation behavior and secondary buckling can occur. It is shown that, depending on the boundary conditions, both can occur, though the characteristics are different than the pre and post-buckling behavior of a companion symmetric cross-ply plate. Furthermore, while a symmetric cross-ply plate can postbuckle with either a positive or negative out-of-plane displacement, the unsymmetric cross-ply plates studied deflect out-of-plane only in one direction throughout the range of inplane compression, the direction again depending on the boundary conditions

Molecular dynamics simulation of the plastic behavior anisotropy of shock-compressed monocrystal nickel

NASA Astrophysics Data System (ADS)

Chen, Ya-Zhou; Zhou, Liu-Cheng; He, Wei-Feng; Sun, Yu; Li, Ying-Hong; Jiao, Yang; Luo, Si-Hai

2017-01-01

Molecular dynamics simulations were used to study the plastic behavior of monocrystalline nickel under shock compression along the [100] and [110] orientations. The shock Hugoniot relation, local stress curve, and process of microstructure development were determined. Results showed the apparent anisotropic behavior of monocrystalline nickel under shock compression. The separation of elastic and plastic waves was also obvious. Plastic deformation was more severely altered along the [110] direction than the [100] direction. The main microstructure phase transformed from face-centered cubic to body-centered cubic and generated a large-scale and low-density stacking fault along the family of { 111 } crystal planes under shock compression along the [100] direction. By contrast, the main mechanism of plastic deformation in the [110] direction was the nucleation of the hexagonal, close-packed phase, which generated a high density of stacking faults along the [110] and [1̅10] directions.

Poromechanics of compressible charged porous media using the theory of mixtures.

PubMed

Huyghe, J M; Molenaar, M M; Baajens, F P T

2007-10-01

Osmotic, electrostatic, and/or hydrational swellings are essential mechanisms in the deformation behavior of porous media, such as biological tissues, synthetic hydrogels, and clay-rich rocks. Present theories are restricted to incompressible constituents. This assumption typically fails for bone, in which electrokinetic effects are closely coupled to deformation. An electrochemomechanical formulation of quasistatic finite deformation of compressible charged porous media is derived from the theory of mixtures. The model consists of a compressible charged porous solid saturated with a compressible ionic solution. Four constituents following different kinematic paths are identified: a charged solid and three streaming constituents carrying either a positive, negative, or no electrical charge, which are the cations, anions, and fluid, respectively. The finite deformation model is reduced to infinitesimal theory. In the limiting case without ionic effects, the presented model is consistent with Blot's theory. Viscous drag compression is computed under closed circuit and open circuit conditions. Viscous drag compression is shown to be independent of the storage modulus. A compressible version of the electrochemomechanical theory is formulated. Using material parameter values for bone, the theory predicts a substantial influence of density changes on a viscous drag compression simulation. In the context of quasistatic deformations, conflicts between poromechanics and mixture theory are only semantic in nature.

Understanding deformation mechanisms during powder compaction using principal component analysis of compression data.

PubMed

Roopwani, Rahul; Buckner, Ira S

2011-10-14

Principal component analysis (PCA) was applied to pharmaceutical powder compaction. A solid fraction parameter (SF(c/d)) and a mechanical work parameter (W(c/d)) representing irreversible compression behavior were determined as functions of applied load. Multivariate analysis of the compression data was carried out using PCA. The first principal component (PC1) showed loadings for the solid fraction and work values that agreed with changes in the relative significance of plastic deformation to consolidation at different pressures. The PC1 scores showed the same rank order as the relative plasticity ranking derived from the literature for common pharmaceutical materials. The utility of PC1 in understanding deformation was extended to binary mixtures using a subset of the original materials. Combinations of brittle and plastic materials were characterized using the PCA method. The relationships between PC1 scores and the weight fractions of the mixtures were typically linear showing ideal mixing in their deformation behaviors. The mixture consisting of two plastic materials was the only combination to show a consistent positive deviation from ideality. The application of PCA to solid fraction and mechanical work data appears to be an effective means of predicting deformation behavior during compaction of simple powder mixtures. Copyright © 2011 Elsevier B.V. All rights reserved.

Constitutive Behavior and Processing Map of T2 Pure Copper Deformed from 293 to 1073 K

NASA Astrophysics Data System (ADS)

Liu, Ying; Xiong, Wei; Yang, Qing; Zeng, Ji-Wei; Zhu, Wen; Sunkulp, Goel

2018-02-01

The deformation behavior of T2 pure copper compressed from 293 to 1073 K with strain rates from 0.01 to 10 s-1 was investigated. The constitutive equations were established by the Arrhenius constitutive model, which can be expressed as a piecewise function of temperature with two sections, in the ranges 293-723 K and 723-1073 K. The processing maps were established according to the dynamic material model for strains of 0.2, 0.4, 0.6, and 0.8, and the optimal processing parameters of T2 copper were determined accordingly. In order to obtain a better understanding of the deformation behavior, the microstructures of the compressed samples were studied by electron back-scattered diffraction. The grains tend to be more refined with decreases in temperature and increases in strain rate.

Investigation of primary static recrystallization in a NiTiFe shape memory alloy subjected to cold canning compression using the coupling crystal plasticity finite element method with cellular automaton

NASA Astrophysics Data System (ADS)

Zhang, Yanqiu; Jiang, Shuyong; Hu, Li; Zhao, Yanan; Sun, Dong

2017-10-01

The behavior of primary static recrystallization (SRX) in a NiTiFe shape memory alloy (SMA) subjected to cold canning compression was investigated using the coupling crystal plasticity finite element method (CPFEM) with the cellular automaton (CA) method, where the distribution of the dislocation density and the deformed grain topology quantified by CPFEM were used as the input for the subsequent SRX simulation performed using the CA method. The simulation results were confirmed by the experimental ones in terms of microstructures, average grain size and recrystallization fraction, which indicates that the proposed coupling method is well able to describe the SRX behavior of the NiTiFe SMA. The results show that the dislocation density exhibits an inhomogeneous distribution in the deformed sample and the recrystallization nuclei mainly concentrate on zones where the dislocation density is relatively higher. An increase in the compressive deformation degree leads to an increase in nucleation rate and a decrease in grain boundary spaces in the compression direction, which reduces the growth spaces for the SRX nuclei and impedes their further growth. In addition, both the mechanisms of local grain refinement in the incomplete SRX and the influence of compressive deformation degree on the grain size of SRX were vividly illustrated by the corresponding physical models.

Microstructure and hot compression deformation of the as-cast Mg-5.0Sn-1.5Y-0.1Zr alloy

NASA Astrophysics Data System (ADS)

Luo, Xiaoping; Kang, Li; Li, Qiushu; Chai, Yuesheng

2015-08-01

The hot compression deformation behavior and microstructure of as-cast Mg-5.0Sn-1.5Y-0.1Zr alloy were investigated by performing isothermal hot compression tests. The tests were conducted using a thermal mechanical simulator at 250-450 °C and strain rates ranging from 0.002 to 2 s-1, with a maximum deformation strain of 50 %. The effects of the deformation parameters on the microstructure evolution of the Mg-5.0Sn-1.5Y-0.1Zr alloy were discussed. The study revealed the flow behavior and the deformation mechanism of the Mg-5.0Sn-1.5Y-0.1Zr alloy. The dependence of flow stress on temperature and strain rate was described by a hyperbolic sine constitutive equation. Through regression analysis, the activation energy of 223.26 kJ mol-1 for plastic deformation was determined by considering flow stress at a strain rate of 0.2. Microstructure observation showed that dynamic recrystallization occurred extensively along grain boundaries at temperatures higher than 300 °C and strain rates lower than 0.02 s-1. This observation provides a theoretical basis for the manufacture and application of the Mg-5.0Sn-1.5Y-0.1Zr alloy.

Correlating Single Crystal Structure, Nanomechanical, and Bulk Compaction Behavior of Febuxostat Polymorphs.

PubMed

Yadav, Jayprakash A; Khomane, Kailas S; Modi, Sameer R; Ugale, Bharat; Yadav, Ram Naresh; Nagaraja, C M; Kumar, Navin; Bansal, Arvind K

2017-03-06

Febuxostat exhibits unprecedented solid forms with a total of 40 polymorphs and pseudopolymorphs reported. Polymorphs differ in molecular arrangement and conformation, intermolecular interactions, and various physicochemical properties, including mechanical properties. Febuxostat Form Q (FXT Q) and Form H1 (FXT H1) were investigated for crystal structure, nanomechanical parameters, and bulk deformation behavior. FXT Q showed greater compressibility, densification, and plastic deformation as compared to FXT H1 at a given compaction pressure. Lower mechanical hardness of FXT Q (0.214 GPa) as compared to FXT H1 (0.310 GPa) was found to be consistent with greater compressibility and lower mean yield pressure (38 MPa) of FXT Q. Superior compaction behavior of FXT Q was attributed to the presence of active slip systems in crystals which offered greater plastic deformation. By virtue of greater compressibility and densification, FXT Q showed higher tabletability over FXT H1. Significant correlation was found with anticipation that the preferred orientation of molecular planes into a crystal lattice translated nanomechanical parameters to a bulk compaction process. Moreover, prediction of compactibility of materials based on true density or molecular packing should be carefully evaluated, as slip-planes may cause deviation in the structure-property relationship. This study supported how molecular level crystal structure confers a bridge between particle level nanomechanical parameters and bulk level deformation behavior.

Effect of strain and deformation route on grain boundary characteristics and recrystallization behavior of aluminum

NASA Astrophysics Data System (ADS)

Sakai, Tetsuo; Utsunomiya, Hiroshi; Takahashi, Yasuo

2014-08-01

The effect of strain and deformation route on the recrystallization behavior of aluminum sheets has been investigated using well lubricated cold rolling and continuous equal channel angular extrusion. Three different deformation routes in plane strain corresponding to (1) simple shear, (2) compression, and (3) the combination of simple shear and compression were performed on 1100 aluminum sheet. Fixed amounts of the equivalent strain of 1.28 and 1.06 were accumulated in each route. In case of the combined deformation route, the ratio of shear strain to the total equivalent strain was varied. The recrystallized grain size was finer if the combined deformation route was employed instead of the monotonic route under the same amount of equivalent strain at either strain level. The density of high angle grain boundaries that act as nucleation sites for recrystallization was higher in materials deformed by the combined route. The orientation imaging micrographs revealed that the change in deformation route is effective for introducing a larger number of new high angle grain boundaries with relatively low misorientation angle.

Effect of Pre-Strain on the Fatigue Behavior of Extruded AZ31 Alloys

NASA Astrophysics Data System (ADS)

Wu, Yanjun

2017-09-01

An attempt is made to rationalize the effect of pre-strain history on fatigue behaviors of AZ31 magnesium alloy. Axial fatigue tests were conducted in the extruded and pre-compressioned AZ31 alloy under low cycle total strain control fatigue conditions. The pre-strain process influences the plastic deformation mechanism activated during fatigue deformation, especially during tensile loading, by enhancing the activity of detwinning mechanism. The low-cycle fatigue lifetime of extruded AZ31 alloy can be enhanced by the pre-compression process. And the hysteresis energy was successfully used to predict the low-cycle fatigue lifetime.

A Viscoplastic Constitutive Theory for Monolithic Ceramic Materials. Series 1

NASA Technical Reports Server (NTRS)

Janosik, Lesley A.; Duffy, Stephen F.

1997-01-01

With increasing use of ceramic materials in high temperature structural applications such as advanced heat engine components, the need arises to accurately predict thermomechanical behavior. This paper, which is the first of two in a series, will focus on inelastic deformation behavior associated with these service conditions by providing an overview of a viscoplastic constitutive model that accounts for time-dependent hereditary material deformation (e.g., creep, stress relaxation, etc.) in monolithic structural ceramics. Early work in the field of metal plasticity indicated that inelastic deformations are essentially unaffected by hydrostatic stress. This is not the case, however, for ceramic-based material systems, unless the ceramic is fully dense. The theory presented here allows for fully dense material behavior as a limiting case. In addition, ceramic materials exhibit different time-dependent behavior in tension and compression. Thus, inelastic deformation models for ceramics must be constructed in a fashion that admits both sensitivity to hydrostatic stress and differing behavior in tension and compression. A number of constitutive theories for materials that exhibit sensitivity to the hydrostatic component of stress have been proposed that characterize deformation using time-independent classical plasticity as a foundation. However, none of these theories allow different behavior in tension and compression. In addition, these theories are somewhat lacking in that they are unable to capture creep, relaxation, and rate-sensitive phenomena exhibited by ceramic materials at high temperature. When subjected to elevated service temperatures, ceramic materials exhibit complex thermomechanical behavior that is inherently time-dependent, and hereditary in the sense that current behavior depends not only on current conditions, but also on thermo-mechanical history. The objective of this work is to present the formulation of a macroscopic continuum theory that captures these time-dependent phenomena. Specifically, the overview contained in this paper focuses on the multiaxial derivation of the constitutive model, and examines the scalar threshold function and its attending geometrical implications.

A Finite Element Study of Micropipette Aspiration of Single Cells: Effect of Compressibility

PubMed Central

Jafari Bidhendi, Amirhossein; Korhonen, Rami K.

2012-01-01

Micropipette aspiration (MA) technique has been widely used to measure the viscoelastic properties of different cell types. Cells experience nonlinear large deformations during the aspiration procedure. Neo-Hookean viscohyperelastic (NHVH) incompressible and compressible models were used to simulate the creep behavior of cells in MA, particularly accounting for the effect of compressibility, bulk relaxation, and hardening phenomena under large strain. In order to find optimal material parameters, the models were fitted to the experimental data available for mesenchymal stem cells. Finally, through Neo-Hookean porohyperelastic (NHPH) material model for the cell, the influence of fluid flow on the aspiration length of the cell was studied. Based on the results, we suggest that the compressibility and bulk relaxation/fluid flow play a significant role in the deformation behavior of single cells and should be taken into account in the analysis of the mechanics of cells. PMID:22400045

Deformation behavior of human dentin in liquid nitrogen: a diametral compression test.

PubMed

Zaytsev, Dmitry; Panfilov, Peter

2014-09-01

Contribution of the collagen fibers into the plasticity of human dentin is considered. Mechanical testing of dentin at low temperature allows excluding the plastic response of its organic matrix. Therefore, deformation and fracture behavior of the dentin samples under diametral compression at room temperature and liquid nitrogen temperature are compared. At 77K dentin behaves like almost brittle material: it is deformed exclusively in the elastic regime and it fails due to growth of the sole crack. On the contrary, dentin demonstrates the ductile response at 300K. There are both elastic and plastic contributions in the deformation of dentin samples. Multiple cracking and crack tip blunting precede the failure of samples. Organic phase plays an important role in fracture of dentin: plasticity of the collagen fibers could inhibit the crack growth. Copyright © 2014 Elsevier B.V. All rights reserved.

Tension-compression asymmetry of a rolled Mg-Y-Nd alloy

NASA Astrophysics Data System (ADS)

Song, Bo; Pan, Hucheng; Ren, Weijie; Guo, Ning; Wu, Zehong; Xin, Renlong

2017-07-01

In this work, tension and compression deformation behaviors of rolled and aged Mg-Y-Nd alloys were investigated. The microstructure evolution and plastic deformation mechanism during tension and compression were analyzed by combined use of electron backscatter diffraction and a visco-plastic self-consistent crystal plasticity model. The results show that both rolled and aged Mg-Y-Nd sheets show an extremely low yield asymmetry. Elimination of yield asymmetry can be ascribed to the tilted basal texture and suppression of {10-12} twinning. The rolled sheet has almost no yield asymmetry, however exhibits a remarkable strain-hardening behavior asymmetry. Compressed sample shows lower initial strain hardening rate and keeps higher strain hardening rate at the later stage compared with tension. The strain-hardening asymmetry can be aggravated by aging at 280 C. It is considered the limited amount of twins in compression plays the critical role in the strain hardening asymmetry. Finally, the relevant mechanism was analyzed and discussed.

Anisotropy, size, and aspect ratio effects on micropillar compression of Al-SiC nanolaminate composites

DOE PAGES

Mayer, C. R.; Yang, L. W.; Singh, S. S.; ...

2016-05-20

Metal-ceramic nanolaminate composites show promise as high strength and toughness materials. Micropillar compression was used to characterize the mechanical behavior of AlSiC multilayers in different orientations including loading at 0°, 45° and 90° with respect to the direction of the layers. The 0° orientation showed the highest strength while the 45° orientation showed the lowest strength. Each orientation showed unique deformation behavior. Effects of pillar size and aspect ratio were also studied. Higher compressive strengths were observed in smaller pillars for all orientations. This effect was shown to be due to a lower probability of flaws using Weibull statistics. Additionally,more » changes in the aspect ratio was shown to have no significant effect on the behavior except an increase in the strain to failure in the 0° orientation. In conclusion, finite element analysis (FEA) was used to simulate and understand the effect of these parameters on the deformation behavior.« less

A material-sparing method for assessment of powder deformation characteristics using data collected during a single compression-decompression cycle.

PubMed

Katz, Jeffrey M; Roopwani, Rahul; Buckner, Ira S

2013-10-01

Compressibility profiles, or functions of solid fraction versus applied pressure, are used to provide insight into the fundamental mechanical behavior of powders during compaction. These functions, collected during compression (in-die) or post ejection (out-of-die), indicate the amount of pressure that a given powder formulation requires to be compressed to a given density or thickness. To take advantage of the benefits offered by both methods, the data collected in-die during a single compression-decompression cycle will be used to generate the equivalent of a complete out-of-die compressibility profile that has been corrected for both elastic and viscoelastic recovery of the powder. This method has been found to be both a precise and accurate means of evaluating out-of-die compressibility for four common tableting excipients. Using this method, a comprehensive characterization of powder compaction behavior, specifically in relation to plastic/brittle, elastic and viscoelastic deformation, can be obtained. Not only is the method computationally simple, but it is also material-sparing. The ability to characterize powder compressibility using this approach can improve productivity and streamline tablet development studies. © 2013 Wiley Periodicals, Inc. and the American Pharmacists Association.

The High Strain Rate Deformation Behavior of High Purity Magnesium and AZ31B Magnesium Alloy

NASA Astrophysics Data System (ADS)

Livescu, Veronica; Cady, Carl M.; Cerreta, Ellen K.; Henrie, Benjamin L.; Gray, George T.

The deformation in compression of pure magnesium and AZ31B magnesium alloy, both with a strong basal pole texture, has been investigated as a function of temperature, strain rate, and specimen orientation. The mechanical response of both metals is highly dependent upon the orientation of loading direction with respect to the basal pole. Specimens compressed along the basal pole direction have a high sensitivity to strain rate and temperature and display a concave down work hardening behavior. Specimens loaded perpendicularly to the basal pole have a yield stress that is relatively insensitive to strain rate and temperature and a work hardening behavior that is parabolic and then linearly upwards. Both specimen orientations display a mechanical response that is sensitive to temperature and strain rate. Post mortem characterization of the pure magnesium was conducted on a subset of specimens to determine the microstructural and textural evolution during deformation and these results are correlated with the observed work hardening behavior and strain rate sensitivities were calculated.

Effect of particle size on in-die and out-of-die compaction behavior of ranitidine hydrochloride polymorphs.

PubMed

Khomane, Kailas S; Bansal, Arvind K

2013-09-01

The present study investigates the effect of particle size on compaction behavior of forms I and II of ranitidine hydrochloride. Compaction studies were performed using three particle size ranges [450-600 (A), 300-400 (B), and 150-180 (C) μm] of both the forms, using a fully instrumented rotary tableting machine. Compaction data were analyzed for out-of-die compressibility, tabletability, and compactibility profiles and in-die Heckel and Kawakita analysis. Tabletability of the studied size fractions followed the order; IB > IA > > IIC > IIB > IIA at all the compaction pressures. In both the polymorphs, decrease in particle size improved the tabletability. Form I showed greater tabletability over form II at a given compaction pressure and sized fraction. Compressibility plot and Heckel and Kawakita analysis revealed greater compressibility and deformation behavior of form II over form I at a given compaction pressure and sized fraction. Decrease in particle size increased the compressibility and plastic deformation of both the forms. For a given polymorph, improved tabletability of smaller sized particles was attributed to their increased compressibility. However, IA and IB, despite poor compressibility and deformation, showed increased tabletability over IIA, IIB, and IIC by virtue of their greater compactibility. Microtensile testing also revealed higher nominal fracture strength of form I particles over form II, thus, supporting greater compactibility of form I. Taken as a whole, though particle size exhibited a trend on tabletability of individual forms, better compactibility of form I over form II has an overwhelming impact on tabletability.

The influence of cell morphology on the compressive fatigue behavior of Ti-6Al-4V meshes fabricated by electron beam melting.

PubMed

Zhao, S; Li, S J; Hou, W T; Hao, Y L; Yang, R; Misra, R D K

2016-06-01

Additive manufacturing technique is a promising approach for fabricating cellular bone substitutes such as trabecular and cortical bones because of the ability to adjust process parameters to fabricate different shapes and inner structures. Considering the long term safe application in human body, the metallic cellular implants are expected to exhibit superior fatigue property. The objective of the study was to study the influence of cell shape on the compressive fatigue behavior of Ti-6Al-4V mesh arrays fabricated by electron beam melting. The results indicated that the underlying fatigue mechanism for the three kinds of meshes (cubic, G7 and rhombic dodecahedron) is the interaction of cyclic ratcheting and fatigue crack growth on the struts, which is closely related to cumulative effect of buckling and bending deformation of the strut. By increasing the buckling deformation on the struts through cell shape design, the cyclic ratcheting rate of the meshes during cyclic deformation was decreased and accordingly, the compressive fatigue strength was increased. With increasing bending deformation of struts, fatigue crack growth in struts contributed more to the fatigue damage of meshes. Rough surface and pores contained in the struts significantly deteriorated the compressive fatigue strength of the struts. By optimizing the buckling and bending deformation through cell shape design, Ti-6Al-4V alloy cellular solids with high fatigue strength and low modulus can be fabricated by the EBM technique. Copyright © 2016 Elsevier Ltd. All rights reserved.

The deformation of gum metal under nanoindentation and sub-micron pillar compression

NASA Astrophysics Data System (ADS)

Withey, Elizabeth Ann

Reaching ideal strength has proven to be difficult in most materials. Dislocation slip, phase transformations, twinning, and fracture all tend to occur at stresses well below the ideal strength of a material. Only on very small scales has it been possible to approach ideal strength. Thus, it was of great interest when a set of beta-Ti alloys, Gum Metal, were found to have a bulk yield strength close to half of its ideal strength. However, some recent studies have questioned the reliability of this claim. Several studies have suggested Gum Metal deforms by dislocation slip. Others have suggested the possibility of transformation-induced plasticity. The present study was undertaken in order to help clarify if and how Gum Metal can reach ideal strength. Two different experiments, ex situ nanoindentation and quantitative in situ nanopillar compression in a transmission electron microscope to correlate real-time deformation behavior, were performed on a single composition of Gum Metal, Ti-23Nb-0.7Ta-2Zr-1.20 at. %, obtained from Toyota Central R&D Laboratories. Nanoindented specimens were thinned from the bottom surface until the pits of multiple indentations became electron-transparent allowing for qualitative analysis of the deformation microstructure in both fully cold-worked and solution-treated specimens. Real-time load-displacement behavior from the nanopillar compression tests was correlated with real-time video recorded during each compression to determine both the compressive strength of each pillar and the timing and strengths of different deformation behaviors observed. Combining the results from both experiments provided several important conclusions. First, Gum Metal approaches and can attain ideal strength in nanopillars regardless of processing condition. While dislocations exist in Gum Metal, they can be tightly pinned by obstacles with spacing less than ˜20 nm, which should inhibit their motion at strengths below the ideal shear strength. The plastic deformation of Gum Metal is not controlled by giant faults or by stress-induced phase transformations. Both of these phenomena, while active, are not the source of plasticity in Gum Metal.

On the use of a split Hopkinson pressure bar in structural geology: High strain rate deformation of Seeberger sandstone and Carrara marble under uniaxial compression

NASA Astrophysics Data System (ADS)

Zwiessler, Ruprecht; Kenkmann, Thomas; Poelchau, Michael H.; Nau, Siegfried; Hess, Sebastian

2017-04-01

There is increasing evidence that seismogenic fractures can propagate faster than the shear wave velocity of the surrounding rocks. Strain rates within the tip region of such super-shear earthquake ruptures can reach deformation conditions similar to impact processes, resulting in rock pulverization. The physical response of brittle rocks at high strain rates changes dramatically with respect to quasi-static conditions. Rocks become stiffer and their strength increases. A measure for the dynamic behavior of a rock and its strain dependency is the dynamic increase factor (DIF) which is the ratio of the dynamic compressive strength to the quasi-static uniaxial compressive strength. To investigate deformation in the high strain rate regime experimentally, we introduce the split Hopkinson pressure bar technology to the structural geology community, a method that is frequently used by rock and impact engineers. We measure the stress-strain response of homogeneous, fine-grained Seeberger sandstone and Carrara marble in uniaxial compression at strain rates ranging from 10+1 to 10+2 s-1 with respect to tangent modulus and dynamic uniaxial compressive strength. We present full stress-strain response curves of Seeberger sandstone and Carrara marble at high strain rates and an evaluation method to determine representative rates of deformation. Results indicate a rate-dependent elastic behavior of Carrara marble where an average increase of ∼18% could be observed at high strain rates of about 100 s-1. DIF reaches a factor of 2.2-2.4. Seeberger sandstone does not have a rate-dependent linear stress-strain response at high strain rates. Its DIF was found to be about 1.6-1.7 at rates of 100 s-1. The onset of dynamic behavior is accompanied with changes in the fracture pattern from single to multiple fractures to pervasive pulverization for increasing rates of deformation. Seismogenic shear zones and their associated fragment-size spectra should be carefully revisited in the light of dynamic deformation.

Compaction behavior and deformation mechanism of directly compressible textured mannitol in a rotary tablet press simulator.

PubMed

Tarlier, Nicolas; Soulairol, Ian; Bataille, Bernard; Baylac, Gilles; Ravel, Patrice; Nofrerias, Isaac; Lefèvre, Philippe; Sharkawi, Tahmer

2015-11-10

Textured mannitol powder is widely used as a pharmaceutical excipient for tablet compaction. In order to choose the right tableting parameters, it is necessary to understand its mechanical behavior during deformation under industrial tableting conditions. The aim of this study was to evaluate the mechanical behavior during deformation of a textured mannitol using a rotary tablet press simulator. Mean yield pressure (Py) obtained by Heckel modeling, Walker coefficients (W) and Stress Rate Sensitivity (SRS) were compared to reference excipients, known for either their plastic (microcrystalline cellulose) or fragmentary (lactose and dibasic calcium phosphate) deformation behavior. Py, W and SRS values showed that the studied textured mannitol has a fragmentary deformation mechanism. Furthermore, this mechanical behavior was not sensitive to lubrication, which is characteristic of fragmentary excipients. Copyright © 2015 Elsevier B.V. All rights reserved.

Finite element simulation of location- and time-dependent mechanical behavior of chondrocytes in unconfined compression tests.

PubMed

Wu, J Z; Herzog, W

2000-03-01

Experimental evidence suggests that cells are extremely sensitive to their mechanical environment and react directly to mechanical stimuli. At present, it is technically difficult to measure fluid pressure, stress, and strain in cells, and to determine the time-dependent deformation of chondrocytes. For this reason, there are no data in the published literature that show the dynamic behavior of chondrocytes in articular cartilage. Similarly, the dynamic chondrocyte mechanics have not been calculated using theoretical models that account for the influence of cell volumetric fraction on cartilage mechanical properties. In the present investigation, the location- and time-dependent stress-strain state and fluid pressure distribution in chondrocytes in unconfined compression tests were simulated numerically using a finite element method. The technique involved two basic steps: first, cartilage was approximated as a macroscopically homogenized material and the mechanical behavior of cartilage was obtained using the homogenized model; second, the solution of the time-dependent displacements and fluid pressure fields of the homogenized model was used as the time-dependent boundary conditions for a microscopic submodel to obtain average location- and time-dependent mechanical behavior of cells. Cells and extracellular matrix were assumed to be biphasic materials composed of a fluid phase and a hyperelastic solid phase. The hydraulic permeability was assumed to be deformation dependent and the analysis was performed using a finite deformation approach. Numerical tests were made using configurations similar to those of experiments described in the literature. Our simulations show that the mechanical response of chondrocytes to cartilage loading depends on time, fluid boundary conditions, and the locations of the cells within the specimen. The present results are the first to suggest that chondrocyte deformation in a stress-relaxation type test may exceed the imposed system deformation by a factor of 3-4, that chondrocyte deformations are highly dynamic and do not reach a steady state within about 20 min of steady compression (in an unconfined test), and that cell deformations are very much location dependent.

Deformation Behavior of Cementite in Deformed High Carbon Steel Observed by X-ray Diffraction with Synchrotron Radiation

NASA Astrophysics Data System (ADS)

Taniyama, Akira; Takayama, Toru; Arai, Masahiro; Hamada, Takanari

2017-10-01

The deformation behavior of cementite in drawn pearlitic steel and spheroidal cementite steel, which have hypereutectoid composition, was investigated by X-ray diffraction using synchrotron radiation. A detailed analysis of diffraction peak profiles reveals that the deformation behavior strongly depends on the shape of cementite in steel. The unit cell volume of the cementite in the drawn pearlitic steel compressively and elastically deforms by 1.5 to 2 pct of the initial volume at the early stage of drawing, whereas that in the drawn spheroidal cementite steel is compressed by 1 pct of the initial volume even at a large true strain. The cementite in the drawn pearlitic steel fragments into small pieces with increasing the true strain, and these pieces change to amorphous cementite. The dislocation densities of the cementite in the drawn pearlitic steel and in the drawn spheroidal cementite steel are estimated to be 1013/m2 before drawing and 1014/m2 after drawing. Although the large strain is induced in the cementite by drawing, the maximum strain energy in the cementite is too small to contribute to the dissolution of the cementite.

The Microstructural Evolution and Mechanical Properties of Zr-Based Metallic Glass under Different Strain Rate Compressions

PubMed Central

Chen, Tao-Hsing; Tsai, Chih-Kai

2015-01-01

In this study, the high strain rate deformation behavior and the microstructure evolution of Zr-Cu-Al-Ni metallic glasses under various strain rates were investigated. The influence of strain and strain rate on the mechanical properties and fracture behavior, as well as microstructural properties was also investigated. Before mechanical testing, the structure and thermal stability of the Zr-Cu-Al-Ni metallic glasses were studied with X-ray diffraction (XRD) and differential scanning calorimeter. The mechanical property experiments and microstructural observations of Zr-Cu-Al-Ni metallic glasses under different strain rates ranging from 10−3 to 5.1 × 103 s−1 and at temperatures of 25 °C were investigated using compressive split-Hopkinson bar (SHPB) and an MTS tester. An in situ transmission electron microscope (TEM) nanoindenter was used to carry out compression tests and investigate the deformation behavior arising at nanopillars of the Zr-based metallic glass. The formation and interaction of shear band during the plastic deformation were investigated. Moreover, it was clearly apparent that the mechanical strength and ductility could be enhanced by impeding the penetration of shear bands with reinforced particles. PMID:28788034

Experimental and Numerical Investigations on Strength and Deformation Behavior of Cataclastic Sandstone

NASA Astrophysics Data System (ADS)

Zhang, Y.; Shao, J. F.; Xu, W. Y.; Zhao, H. B.; Wang, W.

2015-05-01

This work is devoted to characterization of the deformation and strength properties of cataclastic sandstones. Before conducting mechanical tests, the physical properties were first examined. These sandstones are characterized by a loose damaged microstructure and poorly cemented contacts. Then, a series of mechanical tests including hydrostatic, uniaxial, and triaxial compression tests were performed to study the mechanical strength and deformation of the sandstones. The results obtained show nonlinear stress-strain responses. The initial microcracks are closed at hydrostatic stress of 2.6 MPa, and the uniaxial compressive strength is about 0.98 MPa. Under triaxial compression, there is a clear transition from volumetric compressibility to dilatancy and a strong dependency on confining pressure. Based on the experimental evidence, an elastoplastic model is proposed using a linear yield function and a nonassociated plastic potential. There is good agreement between numerical results and experimental data.

Experimental and theoretical investigation of deformation and fracture of subcutaneous fat under compression

NASA Astrophysics Data System (ADS)

Sapozhnikov, S. B.; Ignatova, A. V.

2013-01-01

The subcutaneous fat is considered as a structural material undergoing large inelastic deformations and failure under uniform compression. In calculation, the fat is replaced with a set of cells operating in parallel and suffering failure independently of one another. An elementary cell is considered as a closed thin-wall cylindrical shell filled with an incompressible liquid. All cells in the model are of the same size, and their material is hyperelastic, whose stiffness grows in tension. By comparing experimental data with the mathematical shell model, three parameters are determined to describe the hyperelastic behavior of the cells in transverse compression. A mathematical model with seven constants is presented for describing the deformation of subcutaneous fat under compression. The results obtained are used in a model of human thorax subjected to a local pulse action corresponding to the loading of human body under the impact of a bullet on an armor vest.

Size-dependent plastic deformation of twinned nanopillars in body-centered cubic tungsten

NASA Astrophysics Data System (ADS)

Xu, Shuozhi; Startt, Jacob K.; Payne, Thomas G.; Deo, Chaitanya S.; McDowell, David L.

2017-05-01

Compared with face-centered cubic metals, twinned nanopillars in body-centered cubic (BCC) systems are much less explored partly due to the more complicated plastic deformation behavior and a lack of reliable interatomic potentials for the latter. In this paper, the fault energies predicted by two semi-empirical interatomic potentials in BCC tungsten (W) are first benchmarked against density functional theory calculations. Then, the more accurate potential is employed in large scale molecular dynamics simulations of tensile and compressive loading of twinned nanopillars in BCC W with different cross sectional shapes and sizes. A single crystal, a twinned crystal, and single crystalline nanopillars are also studied as references. Analyses of the stress-strain response and defect nucleation reveal a strong tension-compression asymmetry and a weak pillar size dependence in the yield strength. Under both tensile and compressive loading, plastic deformation in the twinned nanopillars is dominated by dislocation slip on {110} planes that are nucleated from the intersections between the twin boundary and the pillar surface. It is also found that the cross sectional shape of nanopillars affects the strength and the initial site of defect nucleation but not the overall stress-strain response and plastic deformation behavior.

Anisotropic constitutive model incorporating multiple damage mechanisms for multiscale simulation of dental enamel.

PubMed

Ma, Songyun; Scheider, Ingo; Bargmann, Swantje

2016-09-01

An anisotropic constitutive model is proposed in the framework of finite deformation to capture several damage mechanisms occurring in the microstructure of dental enamel, a hierarchical bio-composite. It provides the basis for a homogenization approach for an efficient multiscale (in this case: multiple hierarchy levels) investigation of the deformation and damage behavior. The influence of tension-compression asymmetry and fiber-matrix interaction on the nonlinear deformation behavior of dental enamel is studied by 3D micromechanical simulations under different loading conditions and fiber lengths. The complex deformation behavior and the characteristics and interaction of three damage mechanisms in the damage process of enamel are well captured. The proposed constitutive model incorporating anisotropic damage is applied to the first hierarchical level of dental enamel and validated by experimental results. The effect of the fiber orientation on the damage behavior and compressive strength is studied by comparing micro-pillar experiments of dental enamel at the first hierarchical level in multiple directions of fiber orientation. A very good agreement between computational and experimental results is found for the damage evolution process of dental enamel. Copyright © 2016 The Authors. Published by Elsevier Ltd.. All rights reserved.

A size-dependent constitutive model of bulk metallic glasses in the supercooled liquid region

PubMed Central

Yao, Di; Deng, Lei; Zhang, Mao; Wang, Xinyun; Tang, Na; Li, Jianjun

2015-01-01

Size effect is of great importance in micro forming processes. In this paper, micro cylinder compression was conducted to investigate the deformation behavior of bulk metallic glasses (BMGs) in supercooled liquid region with different deformation variables including sample size, temperature and strain rate. It was found that the elastic and plastic behaviors of BMGs have a strong dependence on the sample size. The free volume and defect concentration were introduced to explain the size effect. In order to demonstrate the influence of deformation variables on steady stress, elastic modulus and overshoot phenomenon, four size-dependent factors were proposed to construct a size-dependent constitutive model based on the Maxwell-pulse type model previously presented by the authors according to viscosity theory and free volume model. The proposed constitutive model was then adopted in finite element method simulations, and validated by comparing the micro cylinder compression and micro double cup extrusion experimental data with the numerical results. Furthermore, the model provides a new approach to understanding the size-dependent plastic deformation behavior of BMGs. PMID:25626690

The cyclic stress-strain behavior of a nickel-base superalloy at 650 C

NASA Technical Reports Server (NTRS)

Gabb, T. P.; Welsch, G. E.

1986-01-01

It is pointed out that examinations of the monotonic tensile and fatigue behaviors of single crystal nickel-base superalloys have disclosed orientation-dependent tension-compression anisotropies and significant differences in the mechanical response of octahedral and cube slip at intermediate temperatures. An examination is conducted of the cyclic hardening response of the single crystal superalloy PWA 1480 at 650 C. In the considered case, tension-compression anisotropy is present, taking into account primarily conditions under which a single slip system is operative. Aspects of a deformation by single slip are considered along with cyclic hardening anisotropy in tension and compression. It is found that specimens deforming by octahedral slip on a single slip system have similar hardening responses in tensile and low cycle fatigue loading. Cyclic strain hardening is very low for specimens displaying single slip.

Investigating internal architecture effect in plastic deformation and failure for TPMS-based scaffolds using simulation methods and experimental procedure.

PubMed

Kadkhodapour, J; Montazerian, H; Raeisi, S

2014-10-01

Rapid prototyping (RP) has been a promising technique for producing tissue engineering scaffolds which mimic the behavior of host tissue as properly as possible. Biodegradability, agreeable feasibility of cell growth, and migration parallel to mechanical properties, such as strength and energy absorption, have to be considered in design procedure. In order to study the effect of internal architecture on the plastic deformation and failure pattern, the architecture of triply periodic minimal surfaces which have been observed in nature were used. P and D surfaces at 30% and 60% of volume fractions were modeled with 3∗3∗ 3 unit cells and imported to Objet EDEN 260 3-D printer. Models were printed by VeroBlue FullCure 840 photopolymer resin. Mechanical compression test was performed to investigate the compressive behavior of scaffolds. Deformation procedure and stress-strain curves were simulated by FEA and exhibited good agreement with the experimental observation. Current approaches for predicting dominant deformation mode under compression containing Maxwell's criteria and scaling laws were also investigated to achieve an understanding of the relationships between deformation pattern and mechanical properties of porous structures. It was observed that effect of stress concentration in TPMS-based scaffolds resultant by heterogeneous mass distribution, particularly at lower volume fractions, led to a different behavior from that of typical cellular materials. As a result, although more parameters are considered for determining dominant deformation in scaling laws, two mentioned approaches could not exclusively be used to compare the mechanical response of cellular materials at the same volume fraction. Copyright © 2014 Elsevier B.V. All rights reserved.

Mechanical and time-dependent behavior of wood-plastic composites subjected to tension and compression

Treesearch

Scott E. Hamel; John C. Hermanson; Steven M. Cramer

2012-01-01

The thermoplastics within wood—plastic composites (WPCs) are known to experience significant time-dependent deformation or creep. In some formulations, creep deformation can be twice as much as the initial quasi-static strain in as little as 4 days. While extensive work has been done on the creep behavior of pure polymers, little information is available on the...

Effect of Grain Scale Properties on Bulk Deformation of Granular Deposits Due to High Speed Projectile Impact

DTIC Science & Technology

2013-04-08

Details of 1D compression test Material: Florida coastal sand Mean diameter: 0.37(mm) Vessel: Stainless steel Vessel inner diameter 6.0(mm... turned out that the projectile deceleration behavior observed in the experiment is a consequence of the complicated compression behavior of sand...applicability of the proposed EOS into high-speed projectile impact experiment. It turned out that the projectile deceleration behavior observed in the

Twinning-detwinning behavior during cyclic deformation of magnesium alloy

DOE PAGES

Lee, Soo Yeol; Wang, Huamiao; Gharghouri, Michael A.

2015-05-26

In situ neutron diffraction has been used to examine the deformation mechanisms of a precipitation-hardened and extruded Mg-8.5wt.%Al alloy subjected to (i) compression followed by reverse tension (texture T1) and (ii) tension followed by reverse compression (texture T2). Two starting textures are used: (1) as-extruded texture, T1, in which the basal pole of most grains is normal to the extrusion axis and a small portion of grains are oriented with the basal pole parallel to the extrusion axis; (2) a reoriented texture, T2, in which the basal pole of most grains is parallel to the extrusion axis. For texture T1,more » the onset of extension twinning corresponds well with the macroscopic elastic-plastic transition during the initial compression stage. The non-linear macroscopic stress/strain behavior during unloading after compression is more significant than during unloading after tension. For texture T2, little detwinning occurs after the initial tension stage, but almost all of the twinned volumes are detwinned during loading in reverse compression.« less

Room temperature deformation mechanisms of alumina particles observed from in situ micro-compression and atomistic simulations.

DOE PAGES

Sarobol, Pylin; Chandross, Michael E.; Carroll, Jay D.; ...

2015-09-22

Aerosol deposition (AD) is a solid-state deposition technology that has been developed to fabricate ceramic coatings nominally at room temperature. Sub-micron ceramic particles accelerated by pressurized gas impact, deform, and consolidate on substrates under vacuum. Ceramic particle consolidation in AD coatings is highly dependent on particle deformation and bonding; these behaviors are not well understood. In this work, atomistic simulations and in situ micro-compressions in the scanning electron microscope, and the transmission electron microscope (TEM) were utilized to investigate fundamental mechanisms responsible for plastic deformation/fracture of particles under applied compression. Results showed that highly defective micron-sized alumina particles, initially containingmore » numerous dislocations or a grain boundary, exhibited no observable shape change before fracture/fragmentation. Simulations and experimental results indicated that particles containing a grain boundary only accommodate low strain energy per unit volume before crack nucleation and propagation. In contrast, nearly defect-free, sub-micron, single crystal alumina particles exhibited plastic deformation and fracture without fragmentation. Dislocation nucleation/motion, significant plastic deformation, and shape change were observed. Simulation and TEM in situ micro-compression results indicated that nearly defect-free particles accommodate high strain energy per unit volume associated with dislocation plasticity before fracture. As a result, the identified deformation mechanisms provide insight into feedstock design for AD.« less

Comparison of femoropopliteal artery stents under axial and radial compression, axial tension, bending, and torsion deformations.

PubMed

Maleckis, Kaspars; Deegan, Paul; Poulson, William; Sievers, Cole; Desyatova, Anastasia; MacTaggart, Jason; Kamenskiy, Alexey

2017-11-01

High failure rates of Peripheral Arterial Disease (PAD) stenting appear to be associated with the inability of certain stent designs to accommodate severe biomechanical environment of the femoropopliteal artery (FPA) that bends, twists, and axially compresses during limb flexion. Twelve Nitinol stents (Absolute Pro, Supera, Lifestent, Innova, Zilver, Smart Control, Smart Flex, EverFlex, Viabahn, Tigris, Misago, and Complete SE) were quasi-statically tested under bench-top axial and radial compression, axial tension, bending, and torsional deformations. Stents were compared in terms of force-strain behavior, stiffness, and geometrical shape under each deformation mode. Tigris was the least stiff stent under axial compression (6.6N/m axial stiffness) and bending (0.1N/m) deformations, while Smart Control was the stiffest (575.3N/m and 105.4N/m, respectively). Under radial compression Complete SE was the stiffest (892.8N/m), while Smart Control had the lowest radial stiffness (211.0N/m). Viabahn and Supera had the lowest and highest torsional stiffness (2.2μNm/° and 959.2μNm/°), respectively. None of the 12 PAD stents demonstrated superior characteristics under all deformation modes and many experienced global buckling and diameter pinching. Though it is yet to be determined which of these deformation modes might have greater clinical impact, results of the current analysis may help guide development of new stents with improved mechanical characteristics. Copyright © 2017 Elsevier Ltd. All rights reserved.

Nonlinear mechanics of a ring structure subjected to multi-pairs of evenly distributed equal radial forces

NASA Astrophysics Data System (ADS)

Chen, Q.; Sun, F.; Li, Z. Y.; Taxis, L.; Pugno, N.

2017-10-01

Combining the elastica theory, finite element (FE) analysis, and a geometrical topological experiment, we studied the mechanical behavior of a ring subjected to multi-pairs of evenly distributed equal radial forces by looking at its seven distinct states. The results showed that the theoretical predictions of the ring deformation and strain energy matched the FE results very well, and that the ring deformations were comparable to the topological experiment. Moreover, no matter whether the ring was compressed or tensioned by N-pairs of forces, the ring always tended to be regular polygons with 2 N sides as the force increased, and a proper compressive force deformed the ring into exquisite flower-like patterns. The present study solves a basic mechanical problem of a ring subjected to lateral forces, which can be useful for studying the relevant mechanical behavior of ring structures from the nano- to the macro-scale.

Deformation Behavior and Microstructure Evolution of As-Cast 42CrMo Alloy in Isothermal and Non-isothermal Compression

NASA Astrophysics Data System (ADS)

Qin, Fangcheng; Li, Yongtang; Qi, Huiping; Lv, Zhenhua

2016-11-01

The isothermal and non-isothermal multi-pass compression tests of centrifugal casting 42CrMo steel were conducted on a Gleeble-3500 thermal simulation machine. The effects of compression passes and finishing temperatures on deformation behavior and microstructure evolution were investigated. It is found that the microstructure is homogeneous with equiaxed grains, and the flow stress does not show significant change with the increase in passes, while the peak softening coefficient increases first and then decreases during inter-pass. Moreover, the dominant mechanisms of controlled temperature and accumulated static recrystallization for grain refinement and its homogeneous distribution are found after 5 passes deformation. As the finishing temperature increases, the flow stress decreases gradually, but the dynamic recrystallization accelerates and softening effect increases, resulting in the larger grain size and homogeneous microstructure. The microhardness decreases sharply because the sufficient softening occurs in microstructure. When the finishing temperature is 890 °C, the carbide particles are precipitated in the vicinity of the grain boundaries, thus inhibiting the dislocation motion. Thus, the higher finishing temperature (≥970 °C) for centrifugal casting 42CrMo alloy should be avoided in non-isothermal multi-pass deformation, which is beneficial to grain refinement and properties improvement.

Mechanical Behavior of AZ31B Mg Alloy Sheets under Monotonic and Cyclic Loadings at Room and Moderately Elevated Temperatures

PubMed Central

Nguyen, Ngoc-Trung; Seo, Oh Suk; Lee, Chung An; Lee, Myoung-Gyu; Kim, Ji-hoon; Kim, Heon Young

2014-01-01

Large-strain monotonic and cyclic loading tests of AZ31B magnesium alloy sheets were performed with a newly developed testing system, at different temperatures, ranging from room temperature to 250 °C. Behaviors showing significant twinning during initial in-plane compression and untwinning in subsequent tension at and slightly above room temperature were recorded. Strong yielding asymmetry and nonlinear hardening behavior were also revealed. Considerable Bauschinger effects, transient behavior, and variable permanent softening responses were observed near room temperature, but these were reduced and almost disappeared as the temperature increased. Different stress–strain responses were inherent to the activation of twinning at lower temperatures and non-basal slip systems at elevated temperatures. A critical temperature was identified to account for the transition between the twinning-dominant and slip-dominant deformation mechanisms. Accordingly, below the transition point, stress–strain curves of cyclic loading tests exhibited concave-up shapes for compression or compression following tension, and an unusual S-shape for tension following compression. This unusual shape disappeared when the temperature was above the transition point. Shrinkage of the elastic range and variation in Young’s modulus due to plastic strain deformation during stress reversals were also observed. The texture-induced anisotropy of both the elastic and plastic behaviors was characterized experimentally. PMID:28788514

Influence of cell shape on mechanical properties of Ti-6Al-4V meshes fabricated by electron beam melting method.

PubMed

Li, S J; Xu, Q S; Wang, Z; Hou, W T; Hao, Y L; Yang, R; Murr, L E

2014-10-01

Ti-6Al-4V reticulated meshes with different elements (cubic, G7 and rhombic dodecahedron) in Materialise software were fabricated by additive manufacturing using the electron beam melting (EBM) method, and the effects of cell shape on the mechanical properties of these samples were studied. The results showed that these cellular structures with porosities of 88-58% had compressive strength and elastic modulus in the range 10-300MPa and 0.5-15GPa, respectively. The compressive strength and deformation behavior of these meshes were determined by the coupling of the buckling and bending deformation of struts. Meshes that were dominated by buckling deformation showed relatively high collapse strength and were prone to exhibit brittle characteristics in their stress-strain curves. For meshes dominated by bending deformation, the elastic deformation corresponded well to the Gibson-Ashby model. By enhancing the effect of bending deformation, the stress-strain curve characteristics can change from brittle to ductile (the smooth plateau area). Therefore, Ti-6Al-4V cellular solids with high strength, low modulus and desirable deformation behavior could be fabricated through the cell shape design using the EBM technique. Copyright © 2014 Acta Materialia Inc. All rights reserved.

Investigation of the Behavior of Hardening Masonry Exposed to Variable Stresses

PubMed Central

Šlivinskas, Tomas; Jonaitis, Bronius; Marčiukaitis, Jonas Gediminas

2018-01-01

This paper analyzes the behavior of masonry under variable loads during execution (construction stage). It specifies the creep coefficient for calcium silicate brick masonry, presenting the research data of masonry deformation under variable and constant long-term loads. The interaction of separate layers of composite material in masonry is introduced and the formulae for determining long-term deformations are offered. The research results of masonry’s compressive strength and deformation properties under variable and constant long-term loads are presented. These are then compared to calculated ones. According to the presented comparison, the calculated long-term deformations coincide quite well with those determined experimentally. PMID:29710802

Investigation of the Behavior of Hardening Masonry Exposed to Variable Stresses.

PubMed

Šlivinskas, Tomas; Jonaitis, Bronius; Marčiukaitis, Jonas Gediminas; Zavalis, Robertas

2018-04-28

This paper analyzes the behavior of masonry under variable loads during execution (construction stage). It specifies the creep coefficient for calcium silicate brick masonry, presenting the research data of masonry deformation under variable and constant long-term loads. The interaction of separate layers of composite material in masonry is introduced and the formulae for determining long-term deformations are offered. The research results of masonry’s compressive strength and deformation properties under variable and constant long-term loads are presented. These are then compared to calculated ones. According to the presented comparison, the calculated long-term deformations coincide quite well with those determined experimentally.

Simultaneous observations of reaction kinetics, creep behavior, and AE activities during syndeformational antigorite dehydration at high pressures

NASA Astrophysics Data System (ADS)

Kubo, T.; Iwasato, T.; Higo, Y.; Kato, T.; Kaneshima, S.; Uehara, S.; Koizumi, S.; Imamura, M.; Tange, Y.

2015-12-01

Intermediate-depth earthquakes are seismic activities in Wadati-Benioff zone at depths from 60 km to 300 km, where subducting plates deform plastically rather than brittle failure. Although it has been reported that unstable faulting occurred during antigorite dehydration even at higher pressures than ~2 GPa (e.g., Jung et al., 2009), the recent study by Chernak and Hirth (2011) revealed that the syndefromational antigorite dehydration does not produces stick-slip instabilities but stable fault slip. In the present study, we newly developed an AE monitoring system for high-pressure reaction-deformation processes combined with D-DIA and synchrotron monochromatic X-ray to observe reaction kinetics, creep behaviors, and AE activities simultaneously. We applied this technique to investigate shear instability during syndeformational antigorite dehydration. High-pressure deformation experiments were conducted up to ~8 GPa, ~1050 K, and strain rates of 3.4-9.2 x 10-5 s-1 in compression using a D-DIA type apparatus installed at BL-04B1, SPring-8. 50 keV mono X-ray were used to measure reaction kinetics and stress-strain data. To monitor shear instabilities by detecting AEs, six piezoelectric devices were positioned between first and second stage anvils of MA 6-6 type system. We used three kinds of starting materials of polycrystalline antigorite, fine-grained forsterite polycrystal, and two-phase mixtures of antigorite and San Carlos olivine (10%, 30%, and 50%atg). Clear contrasts were observed in AE activities between forsterite and antigorite samples. AE activities detected within the forsterite polycrystal suggested (semi) brittle behaviors at low pressures during the cold compression stage.
Almost no AEs were detected within the antigorite samples during any stages of cold compression, ramping, deformation, and syndeformational dehydration although localized deformation textures were observed in recovered samples. Instead, we detected some AEs outside the sample, indicating the stick slipping at the boundaries of cylindrical parts. Our results suggest that localized deformation and dehydration of antigorite do not enhance shear instability at high pressures at least in compression under drained condition.

Microstructure evolution and dynamic recrystallization behavior of a powder metallurgy Ti-22Al-25Nb alloy during hot compression

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jia, Jianbo

The flow behavior of a powder metallurgy (P/M) Ti-22Al-25Nb alloy during hot compression tests has been investigated at a strain rate of 0.01 s{sup −1} and a temperature range of 980–1100 °C up to various true strains from 0.1 to 0.9. The effects of deformation temperature and strain on microstructure characterization and nucleation mechanisms of dynamic recrystallization (DRX) were assessed by means of Optical microscope (OM), electron backscatter diffraction (EBSD) and transmission electron microscope (TEM) techniques, respectively. The results indicated that the process of DRX was promoted by increasing deformation temperature and strain. By regression analysis, a power exponent relationshipmore » between peak stresses and sizes of stable DRX grains was developed. In addition, it is suggested that the discontinuous dynamic recrystallization (DDRX) and continuous dynamic recrystallization (CDRX) controlled nucleation mechanisms for DRX grains operated simultaneously during the whole hot process, and which played the leading role varied with hot process parameters of temperature and strain. It was further demonstrated that the CDRX featured by progressive subgrain rotation was weakened by elevating deformation temperatures. - Highlights: •Flow behavior of a P/M Ti-22Al-25Nb is studied by hot compression tests. •Microstructure evolution of alloy is affected by deformation temperature and strain. •The relationship between peak stress and stable DRX grain size was developed. •The process of DRX was promoted by increasing deformation temperature and strain. •Nucleation mechanisms of DRX were identified by EBSD analysis and TEM observation.« less

Compressive deformation of a single microcapsule

NASA Astrophysics Data System (ADS)

Liu, K. K.; Williams, D. R.; Briscoe, B. J.

1996-12-01

This paper reports an experimental and theoretical study of the compressive behavior of single microcapsules; that is, liquid-filled cellular entities (approximately 65 μm in diameter) with a thin polymeric membrane wall. An experimental technique which allows the simultaneous measurement of both the compressive displacement and the reaction forces of individual microcapsules deformed between two parallel plates up to a dimensionless approach [(compressive displacement)/(initial particle diameter)] of 60% is described. The corresponding major geometric parameters of the deformed microcapsule, such as central lateral extension as well as the failure phenomena, are reported and recorded through a microscopic visualization system. The elastic modulus, the bursting strength of the membrane, and the pressure difference across the membrane are computed by using a theoretical analysis which is also presented in this paper. This theoretical model, which was developed by Feng and Yang [

Constitutive Theory Developed for Monolithic Ceramic Materials

NASA Technical Reports Server (NTRS)

Janosik, Lesley A.

1998-01-01

With the increasing use of advanced ceramic materials in high-temperature structural applications such as advanced heat engine components, the need arises to accurately predict thermomechanical behavior that is inherently time-dependent and that is hereditary in the sense that the current behavior depends not only on current conditions but also on the material's thermomechanical history. Most current analytical life prediction methods for both subcritical crack growth and creep models use elastic stress fields to predict the time-dependent reliability response of components subjected to elevated service temperatures. Inelastic response at high temperatures has been well documented in the materials science literature for these material systems, but this issue has been ignored by the engineering design community. From a design engineer's perspective, it is imperative to emphasize that accurate predictions of time-dependent reliability demand accurate stress field information. Ceramic materials exhibit different time-dependent behavior in tension and compression. Thus, inelastic deformation models for ceramics must be constructed in a fashion that admits both sensitivity to hydrostatic stress and differing behavior in tension and compression. A number of constitutive theories for materials that exhibit sensitivity to the hydrostatic component of stress have been proposed that characterize deformation using time-independent classical plasticity as a foundation. However, none of these theories allow different behavior in tension and compression. In addition, these theories are somewhat lacking in that they are unable to capture the creep, relaxation, and rate-sensitive phenomena exhibited by ceramic materials at high temperatures. The objective of this effort at the NASA Lewis Research Center has been to formulate a macroscopic continuum theory that captures these time-dependent phenomena. Specifically, the effort has focused on inelastic deformation behavior associated with these service conditions by developing a multiaxial viscoplastic constitutive model that accounts for time-dependent hereditary material deformation (such as creep and stress relaxation) in monolithic structural ceramics. Using continuum principles of engineering mechanics, we derived the complete viscoplastic theory from a scalar dissipative potential function.

Strain Hardening of Hadfield Manganese Steel

NASA Astrophysics Data System (ADS)

Adler, P. H.; Olson, G. B.; Owen, W. S.

1986-10-01

The plastic flow behavior of Hadfield manganese steel in uniaxial tension and compression is shown to be greatly influenced by transformation plasticity phenomena. Changes in the stress-strain (σ-ɛ) curves with temperature correlate with the observed extent of deformation twinning, consistent with a softening effect of twinning as a deformation mechanism and a hardening effect of the twinned microstructure. The combined effects give upward curvature to the σ-ɛ curve over extensive ranges of plastic strain. A higher strain hardening in compression compared with tension appears to be consistent with the observed texture development. The composition dependence of stacking fault energy computed using a thermodynamic model suggests that the Hadfield composition is optimum for a maximum rate of deformation twinning. Comparisons of the Hadfield steel with a Co-33Ni alloy exhibiting similar twinning kinetics, and an Fe-21Ni-lC alloy deforming by slip indicate no unusual strain hardening at low strains where deformation is controlled by slip, but an unusual amount of structural hardening associated with the twin formation in the Hadfield steel. A possible mechanism of anomalous twin hardening is discussed in terms of modified twinning behavior (pseudotwinning) in nonrandom solid solutions.

Deformation behavior of HCP titanium alloy: Experiment and Crystal plasticity modeling

DOE PAGES

Wronski, M.; Arul Kumar, Mariyappan; Capolungo, Laurent; ...

2018-03-02

The deformation behavior of commercially pure titanium is studied using experiments and a crystal plasticity model. Compression tests along the rolling, transverse, and normal-directions, and tensile tests along the rolling and transverse directions are performed at room temperature to study the activation of slip and twinning in the hexagonal closed packed titanium. A detailed EBSD based statistical analysis of the microstructure is performed to develop statistics of both {10-12} tensile and {11-22} compression twins. A simple Monte Carlo (MC) twin variant selection criterion is proposed within the framework of the visco-plastic self-consistent (VPSC) model with a dislocation density (DD) basedmore » law used to describe dislocation hardening. In the model, plasticity is accommodated by prismatic, basal and pyramidal slip modes, and {10-12} tensile and {11-22} compression twinning modes. Thus, the VPSC-MC model successfully captures the experimentally observed activation of low Schmid factor twin variants for both tensile and compression twins modes. The model also predicts macroscopic stress-strain response, texture evolution and twin volume fraction that are in agreement with experimental observations.« less

Deformation behavior of HCP titanium alloy: Experiment and Crystal plasticity modeling

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wronski, M.; Arul Kumar, Mariyappan; Capolungo, Laurent

The deformation behavior of commercially pure titanium is studied using experiments and a crystal plasticity model. Compression tests along the rolling, transverse, and normal-directions, and tensile tests along the rolling and transverse directions are performed at room temperature to study the activation of slip and twinning in the hexagonal closed packed titanium. A detailed EBSD based statistical analysis of the microstructure is performed to develop statistics of both {10-12} tensile and {11-22} compression twins. A simple Monte Carlo (MC) twin variant selection criterion is proposed within the framework of the visco-plastic self-consistent (VPSC) model with a dislocation density (DD) basedmore » law used to describe dislocation hardening. In the model, plasticity is accommodated by prismatic, basal and pyramidal slip modes, and {10-12} tensile and {11-22} compression twinning modes. Thus, the VPSC-MC model successfully captures the experimentally observed activation of low Schmid factor twin variants for both tensile and compression twins modes. The model also predicts macroscopic stress-strain response, texture evolution and twin volume fraction that are in agreement with experimental observations.« less

Microstructural evolution and deformation behavior of Al-Cu alloys: A Transmission X-ray Microscopy (TXM) and micropillar compression study

DOE PAGES

Kaira, C. Shashank; Kantzos, Christopher; Williams, Jason J.; ...

2017-11-07

In this paper, a unique approach to correlating an evolving 3D microstructure in an Al-Cu alloy and its micro-scale mechanical properties has been introduced. Using these nanoscale three-dimensional microstructures derived from Transmission X-ray Microscopy (TXM), individual contributions from different strengthening mechanisms were quantified. The spatial distribution and morphology of the individual θ' and θ phases were seen to play an important role in influencing dislocation storage. Uniaxial micro-compression experiments were used to quantify the stress-strain response of the alloy at different aging times. Transmission electron microscopy (TEM) aided in discerning dislocation activity at these precipitates. A model is proposed tomore » accurately predict the variation in yield stress by using appropriate morphological parameters from the 3D microstructure and its validity has been corroborated using experimental measurements. Distributions of 2D and 3D inter-precipitate spacing were seen to provide crucial insights on influencing deformation in such precipitation-strengthened alloys. In conclusion, the transition in deformation behavior and origin of numerous strain bursts were investigated using in situ micropillar compression testing.« less

Microstructural evolution and deformation behavior of Al-Cu alloys: A Transmission X-ray Microscopy (TXM) and micropillar compression study

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kaira, C. Shashank; Kantzos, Christopher; Williams, Jason J.

In this paper, a unique approach to correlating an evolving 3D microstructure in an Al-Cu alloy and its micro-scale mechanical properties has been introduced. Using these nanoscale three-dimensional microstructures derived from Transmission X-ray Microscopy (TXM), individual contributions from different strengthening mechanisms were quantified. The spatial distribution and morphology of the individual θ' and θ phases were seen to play an important role in influencing dislocation storage. Uniaxial micro-compression experiments were used to quantify the stress-strain response of the alloy at different aging times. Transmission electron microscopy (TEM) aided in discerning dislocation activity at these precipitates. A model is proposed tomore » accurately predict the variation in yield stress by using appropriate morphological parameters from the 3D microstructure and its validity has been corroborated using experimental measurements. Distributions of 2D and 3D inter-precipitate spacing were seen to provide crucial insights on influencing deformation in such precipitation-strengthened alloys. In conclusion, the transition in deformation behavior and origin of numerous strain bursts were investigated using in situ micropillar compression testing.« less

Direct Shear Tests of Sandstone Under Constant Normal Tensile Stress Condition Using a Simple Auxiliary Device

NASA Astrophysics Data System (ADS)

Cen, Duofeng; Huang, Da

2017-06-01

Tension-shear failure is a typical failure mode in the rock masses in unloading zones induced by excavation or river incision, etc., such as in excavation-disturbed zone of deep underground caverns and superficial rocks of high steep slopes. However, almost all the current shear failure criteria for rock are usually derived on the basis of compression-shear failure. This paper proposes a simple device for use with a servo-controlled compression-shear testing machine to conduct the tension-shear tests of cuboid rock specimens, to test the direct shear behavior of sandstone under different constant normal tensile stress conditions ( σ = -1, -1.5, -2, -2.5 and -3 MPa) as well as the uniaxial tension behavior. Generally, the fracture surface roughness decreases and the proportion of comminution areas in fracture surface increases as the change of stress state from tension to tension-shear and to compression-shear. Stepped fracture is a primary fracture pattern in the tension-shear tests. The shear stiffness, shear deformation and normal deformation (except the normal deformation for σ = -1 MPa) decrease during shearing, while the total normal deformation containing the pre-shearing portion increases as the normal tensile stress level (| σ|) goes up. Shear strength is more sensitive to the normal tensile stress than to the normal compressive stress, and the power function failure criterion (or Mohr envelope form of Hoek-Brown criterion) is examined to be the optimal criterion for the tested sandstone in the full region of tested normal stress in this study.

High temperature deformation of Vitreloy bulk metallic glasses and their composite

NASA Astrophysics Data System (ADS)

Tao, Min

A complete understanding of the deformation mechanisms of BMGs and their composites requires investigation of the microstructural changes and their interplay with the mechanical behavior. In this dissertation, the deformation mechanisms of a series of Vitreloy glasses and their composites are experimentally investigated over a wide range of strain rates and temperatures, with focus on the supercooled liquid regime, by combining uniaxial mechanical testing with calorimetric and microscopic examinations. Various theories of deformation of metallic glasses and the composites are examined in light of the experimental data. A comparative structural relaxation study was performed on two closely related Vitreloy alloys, Zr41.2Ti13.8Cu12.5Ni 10Be22.5 (Vit 1) and Zr46.7Ti8.3Cu 7.5Ni10Be27.5 (Vit 4). Differential scanning calorimetric studies on the specimens deformed in compression at constant-strain-rate in supercooled liquid regime showed that mechanical loading accelerated the spinodal phase separation and nanocrystallization process in Vit 1, while the relaxation in Vit 4 featured local chemical composition fluctuation accompanied by annealing out of free volume. The effect of the structural relaxation on their mechanical behavior was further studied via single and multiple jump-in-strain-rate tests. The deformation and viscosity of a new Vitreloy alloy were characterized using uniaxial compression tests in its supercooled liquid regime. A new theoretical model named Cooperative Shear Model, which correlates the evolution of the macroscopic mechanical/thermal variables such as shear modulus and viscosity with the configurational energies of atom clusters in an amorphous alloy, was critically examined in this investigation. The model was successful in predicting the Newtonian and non-Newtonian viscosities of the material, as well as the shear moduli of the deformed specimens, in a self-consistent manner. The plastic flow of an in-situ metallic glass composite, beta-Vitreloy, was investigated under uniaxial compression in its supercooled liquid regime and at various strain rates (10-4 ˜ 10-1 s-1). The composite, with ˜ 25% volume fraction of crystalline beta-phase dendrites exhibited superplastic behavior similar to that of amorphous Vit 1. Significant strain hardening was observed when the material was deformed at high temperatures and low strain rates. A dual-phase composite model was employed in finite element simulations to understand the effect of the composite microstructure on its mechanical behavior.

Fabrication, pore structure and compressive behavior of anisotropic porous titanium for human trabecular bone implant applications.

PubMed

Li, Fuping; Li, Jinshan; Xu, Guangsheng; Liu, Gejun; Kou, Hongchao; Zhou, Lian

2015-06-01

Porous titanium with average pore size of 100-650 μm and porosity of 30-70% was fabricated by diffusion bonding of titanium meshes. Pore structure was characterized by Micro-CT scan and SEM. Compressive behavior of porous titanium in the out-of-plane direction was studied. The effect of porosity and pore size on the compressive properties was also discussed based on the deformation mode. The results reveal that the fabrication process can control the porosity precisely. The average pore size of porous titanium can be tailored by adjusting the pore size of titanium meshes. The fabricated porous titanium possesses an anisotropic structure with square pores in the in-plane direction and elongated pores in the out-of-plane direction. The compressive Young's modulus and yield stress are in the range of 1-7.5 GPa and 10-110 MPa, respectively. The dominant compressive deformation mode is buckling of mesh wires, but some uncoordinated buckling is present in porous titanium with lower porosity. Relationship between compressive properties and porosity conforms well to the Gibson-Ashby model. The effect of pore size on compressive properties is fundamentally ascribed to the aspect ratio of titanium meshes. Porous titanium with 60-70% porosity has potential for trabecular bone implant applications. Copyright © 2015 Elsevier Ltd. All rights reserved.

Temperature-dependent phase-specific deformation mechanisms in a directionally solidified NiAl-Cr(Mo) lamellar composite

DOE PAGES

Yu, Dunji; An, Ke; Chen, Xu; ...

2015-10-09

Phase-specific thermal expansion and mechanical deformation behaviors of a directionally solidified NiAl–Cr(Mo) lamellar in situ composite were investigated by using real-time in situ neutron diffraction during compression at elevated temperatures up to 800 °C. Tensile and compressive thermal residual stresses were found to exist in the NiAl phase and Crss (solid solution) phase, respectively. Then, based on the evolution of lattice spacings and phase stresses, the phase-specific deformation behavior was analyzed qualitatively and quantitatively. Moreover, estimates of phase stresses were derived by Hooke's law on the basis of a simple method for the determination of stress-free lattice spacing in inmore » situ composites. During compressive loading, the NiAl phase yields earlier than the Crss phase. The Crss phase carries much higher stress than the NiAl phase, and displays consistent strain hardening at all temperatures. The NiAl phase exhibits strain hardening at relatively low temperatures and softening at high temperatures. During unloading, the NiAl phase yields in tension whereas the Crss phase unloads elastically. Additionally, post-test microstructural observations show phase-through cracks at room temperature, micro cracks along phase interfaces at 600 °C and intact lamellae kinks at 800 °C, which is due to the increasing deformability of both phases as temperature rises.« less

A study on the crushing behavior of basalt fiber reinforced composite structures

NASA Astrophysics Data System (ADS)

Pandian, A.; Veerasimman, A. P.; Vairavan, M.; Francisco, C.; Sultan, M. T. H.

2016-10-01

The crushing behavior and energy absorption capacity of basalt fiber reinforced hollow square structure composites are studied under axial compression. Using the hand layup technique, basalt fiber reinforced composites were fabricated using general purpose (GP) polyester resin with the help of wooden square shaped mould of varying height (100 mm, 150 mm and 200 mm). For comparison, similar specimens of glass fiber reinforced polymer composites were also fabricated and tested. Axial compression load is applied over the top end of the specimen with cross head speed as 2 mm/min using Universal Testing Machine (UTM). From the experimental results, the load-deformation characteristics of both glass fiber and basalt fiber composites were investigated. Crashworthiness and mode of collapse for the composites were determined from load-deformation curve, and they were then compared to each other in terms of their crushing behaviors.

Study on Thermal Deformation Behavior of TC4 – ELI Titanium Alloy

NASA Astrophysics Data System (ADS)

Song, Y.; Zhang, F. S.; Huang, T.; Song, K. X.

2018-05-01

The TC4-ELI titanium alloy was subjected to hot compression deformation test by the Gleeble-1500D thermal simulation test machine. The thermal deformation behavior of the TC4-ELI titanium alloy was studied under the condition of 850°C-1050°C, 0.001s-1-10s-1 strain rate and 50% deformation. The constitutive equation of TC4-ELI titanium alloy was established based on the hyperbolic sine model of Arrhenius equation. The results show that the flow stress of TC4-ELI titanium alloy decreases with the increase of temperature at high temperature. The calculated heat activation energy of TC4-ELI titanium alloy is 300367.5807J / mol.

Compression deformation of WC: atomistic description of hard ceramic material

NASA Astrophysics Data System (ADS)

Feng, Qing; Song, Xiaoyan; Liu, Xuemei; Liang, Shuhua; Wang, Haibin; Nie, Zuoren

2017-11-01

The deformation characteristics of WC, as a typical hard ceramic material, were studied on the nanoscale using atomistic simulations for both the single-crystal and polycrystalline forms under uniaxial compression. In particular, the effects of crystallographic orientation, grain boundary coordination and grain size on the origin of deformation were investigated. The deformation behavior of the single-crystal and polycrystalline WC both depend strongly on the orientation towards the loading direction. The grain boundaries play a significant role in the deformation coordination and the potential high fracture toughness of the nanocrystalline WC. In contrast to conventional knowledge of ceramics, maximum strength was obtained at a critical grain size corresponding to the turning point from a Hall-Petch to an inverse Hall-Petch relationship. For this the mechanism of the combined effect of dislocation motion within grains and the coordination of stress concentration at the grain boundaries were proposed. The present work has moved forward our understanding of plastic deformability and the possibility of achieving a high strength of nanocrystalline ceramic materials.

Compression deformation of WC: atomistic description of hard ceramic material.

PubMed

Feng, Qing; Song, Xiaoyan; Liu, Xuemei; Liang, Shuhua; Wang, Haibin; Nie, Zuoren

2017-11-24

The deformation characteristics of WC, as a typical hard ceramic material, were studied on the nanoscale using atomistic simulations for both the single-crystal and polycrystalline forms under uniaxial compression. In particular, the effects of crystallographic orientation, grain boundary coordination and grain size on the origin of deformation were investigated. The deformation behavior of the single-crystal and polycrystalline WC both depend strongly on the orientation towards the loading direction. The grain boundaries play a significant role in the deformation coordination and the potential high fracture toughness of the nanocrystalline WC. In contrast to conventional knowledge of ceramics, maximum strength was obtained at a critical grain size corresponding to the turning point from a Hall-Petch to an inverse Hall-Petch relationship. For this the mechanism of the combined effect of dislocation motion within grains and the coordination of stress concentration at the grain boundaries were proposed. The present work has moved forward our understanding of plastic deformability and the possibility of achieving a high strength of nanocrystalline ceramic materials.

Quantifying the influence of twin boundaries on the deformation of nanocrystalline copper using atomistic simulations

DOE PAGES

Tucker, Garritt J.; Foiles, Stephen Martin

2014-09-22

Over the past decade, numerous efforts have sought to understand the influence of twin boundaries on the behavior of polycrystalline materials. Early results suggested that twin boundaries within nanocrystalline face-centered cubic metals have a considerable effect on material behavior by altering the activated deformation mechanisms. In this work, we employ molecular dynamics simulations to elucidate the role of twin boundaries on the deformation of <100> columnar nanocrystalline copper at room temperature under uniaxial strain. We leverage non-local kinematic metrics, formulated from continuum mechanics theory, to compute atomically-resolved rotational and strain fields during plastic deformation. These results are then utilized tomore » compute the distribution of various nanoscale mechanisms during straining, and quantitatively resolve their contribution to the total strain accommodation within the microstructure, highlighting the fundamental role of twin boundaries. Our results show that nanoscale twins influence nanocrystalline copper by altering the cooperation of fundamental deformation mechanisms and their contributed role in strain accommodation, and we present new methods for extracting useful information from atomistic simulations. The simulation results suggest a tension–compression asymmetry in the distribution of deformation mechanisms and strain accommodation by either dislocations or twin boundary mechanisms. In highly twinned microstructures, twin boundary migration can become a significant deformation mode, in comparison to lattice dislocation plasticity in non-twinned columnar microstructures, especially during compression.« less

Nanomechanical behavior of MoS2 and WS2 multi-walled nanotubes and Carbon nanohorns

PubMed Central

Maharaj, Dave; Bhushan, Bharat

2015-01-01

Nano-objects have been investigated for drug delivery, oil detection, contaminant removal, and tribology applications. In some applications, they are subjected to friction and deformation during contact with each other and their surfaces on which they slide. Experimental studies directly comparing local and global deformation are lacking. This research performs nanoindentation (local deformation) and compression tests (global deformation) with a nanoindenter (sharp tip and flat punch, respectively) on molybdenum disulfide (MoS2) multi-walled nanotubes (MWNTs), ~500 nm in diameter. Hardness of the MoS2 nanotube was similar to bulk and does not follow the “smaller is stronger” phenomenon as previously reported for other nano-objects. Tungsten disulfide (WS2) MWNTs, ~300 nm in diameter and carbon nanohorns (CNHs) 80–100 nm in diameter were of interest and also selected for compression studies. These studies aid in understanding the mechanisms involved during global deformation when nano-objects are introduced to reduce friction and wear. For compression, highest loads were required for WS2 nanotubes, then MoS2 nanotubes and CNHs to achieve the same displacement. This was due to the greater number of defects with the MoS2 nanotubes and the flexibility of the CNHs. Repeat compression tests of nano-objects were performed showing a hardening effect for all three nano-objects. PMID:25702922

Transition of temporal scaling behavior in percolation assisted shear-branching structure during plastic deformation

DOE PAGES

Ren, Jingli; Chen, Cun; Wang, Gang; ...

2017-03-22

This study explores the temporal scaling behavior induced shear-branching structure in response to variant temperatures and strain rates during plastic deformation of Zr-based bulk metallic glass (BMG). The data analysis based on the compression tests suggests that there are two states of shear-branching structures: the fractal structure with a long-range order at an intermediate temperature of 223 K and a larger strain rate of 2.5 × 10 –2 s –1; the disordered structure dominated at other temperature and strain rate. It can be deduced from the percolation theory that the compressive ductility, ec, can reach the maximum value at themore » intermediate temperature. Furthermore, a dynamical model involving temperature is given for depicting the shear-sliding process, reflecting the plastic deformation has fractal structure at the temperature of 223 K and strain rate of 2.5 × 10 –2 s –1.« less

High-temperature deformation of stoichiometric /sup 239/PuO/sub 2/

DOE Office of Scientific and Technical Information (OSTI.GOV)

Petrovic, J.J.; Land, C.C.

1980-03-01

The deformation behavior of stoichiometric /sup 239/PuO/sub 2/ was examined at 800/sup 0/ to 1500/sup 0/C, using direct and diametral compression. Maximum ductility was observed at 1000/sup 0/C, but above this temperature both strength and ductility decreased and the fracture mode changed from transgranular to intergranular. The deformation activation energy measured at 1000/sup 0/C was 598 kJ/mol. Comparison to the deformation behavior of hypostoichiometric /sup 239/PuO/sub 2-x/ suggests that high-temperature dislocation motion becomes more difficult with increasing O/Pu ratio due to effects of stoichiometry on diffusion rates. Deformation mechanisms in /sup 239/PuO/sub 2/ appear to be a combination of dislocationmore » motion and grain-boundary sliding.« less

Deformation behavior of TC6 alloy in isothermal forging

NASA Astrophysics Data System (ADS)

Li, Xiaoli; Li, Miaoquan; Zhu, Dasong; Xiong, Aiming

2005-10-01

Isothermal compression of the TC6 alloy was carried out in a Thermecmaster-Z (Wuhan Iron and Steel Corporation, P.R. China) simulator at deformation temperatures of 800˜1040 °C, strain rates of 0.001˜50.0 s-1, and maximum height reduction of 50%. The deformation behavior of the TC6 alloy in isothermal forging was characterized based on stress-strain behavior and kinetic analysis. The activation energy of deformation obtained in the isothermal forging of the TC6 alloy was 267.49 kJ/mol in the β phase region and 472.76 kJ/mol in the α+β phase region. The processing map was constructed based on the dynamic materials model, and the optimal deformation parameters were obtained. Constitutive equations describing the flow stress as a function of strain rate, strain, and deformation temperature were proposed for the isothermal forging of the TC6 alloy, and a good agreement between the predicted and experimental stress-strain curves was achieved.

Dynamic recrystallization behavior of an as-cast TiAl alloy during hot compression

DOE Office of Scientific and Technical Information (OSTI.GOV)

Li, Jianbo, E-mail: lijianbo1205@163.com; Liu, Yong, E-mail: yonliu@csu.edu.cn; Wang, Yan, E-mail: wangyan@csu.edu.cn

2014-11-15

High temperature compressive deformation behaviors of as-cast Ti–43Al–4Nb–1.4W–0.6B alloy were investigated at temperatures ranging from 1050 °C to 1200 °C, and strain rates from 0.001 s{sup −1} to 1 s{sup −1}. Electron back scattered diffraction technique, scanning electron microscopy and transmission electron microscopy were employed to investigate the microstructural evolutions and nucleation mechanisms of the dynamic recrystallization. The results indicated that the true stress–true strain curves show a dynamic flow softening behavior. The dependence of the peak stress on the deformation temperature and the strain rate can well be expressed by a hyperbolic-sine type equation. The activation energy decreases withmore » increasing the strain. The size of the dynamically recrystallized β grains decreases with increasing the value of the Zener–Hollomon parameter (Z). When the flow stress reaches a steady state, the size of β grains almost remains constant with increasing the deformation strain. The continuous dynamic recrystallization plays a dominant role in the deformation. In order to characterize the evolution of dynamic recrystallization volume fraction, the dynamic recrystallization kinetics was studied by Avrami-type equation. Besides, the role of β phase and the softening mechanism during the hot deformation was also discussed in details. - Highlights: • The size of DRXed β grains decreases with increasing the value of the Z. • The CDRX plays a dominant role in the deformation. • The broken TiB{sub 2} particles can promote the nucleation of DRX.« less

Hot Deformation Behavior and a Two-Stage Constitutive Model of 20Mn5 Solid Steel Ingot during Hot Compression

PubMed Central

Liu, Min; Ma, Qing-Xian; Luo, Jian-Bin

2018-01-01

20Mn5 steel is widely used in the manufacture of heavy hydro-generator shaft forging due to its strength, toughness, and wear resistance. However, the hot deformation and recrystallization behaviors of 20Mn5 steel compressed under a high temperature were not studied. For this article, hot compression experiments under temperatures of 850–1200 °C and strain rates of 0.01 s−1–1 s−1 were conducted using a Gleeble-1500D thermo-mechanical simulator. Flow stress-strain curves and microstructure after hot compression were obtained. Effects of temperature and strain rate on microstructure are analyzed. Based on the classical stress-dislocation relationship and the kinetics of dynamic recrystallization, a two-stage constitutive model is developed to predict the flow stress of 20Mn5 steel. Comparisons between experimental flow stress and predicted flow stress show that the predicted flow stress values are in good agreement with the experimental flow stress values, which indicates that the proposed constitutive model is reliable and can be used for numerical simulation of hot forging of 20Mn5 solid steel ingot. PMID:29547570

In situ spectroscopic study of the plastic deformation of amorphous silicon under nonhydrostatic conditions induced by indentation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gerbig, Yvonne B.; Michaels, C. A.; Bradby, Jodie E.

Indentation-induced plastic deformation of amorphous silicon (a-Si) thin films was studied by in situ Raman imaging of the deformed contact region of an indented sample, employing a Raman spectroscopy-enhanced instrumented indentation technique (IIT). The occurrence and evolving spatial distribution of changes in the a-Si structure caused by processes, such as polyamorphization and crystallization, induced by indentation loading were observed. Furthermore, the obtained experimental results are linked with previously published work on the plastic deformation of a-Si under hydrostatic compression and shear deformation to establish a model for the deformation behavior of a-Si under indentation loading.

In situ spectroscopic study of the plastic deformation of amorphous silicon under nonhydrostatic conditions induced by indentation

DOE PAGES

Gerbig, Yvonne B.; Michaels, C. A.; Bradby, Jodie E.; ...

2015-12-17

Indentation-induced plastic deformation of amorphous silicon (a-Si) thin films was studied by in situ Raman imaging of the deformed contact region of an indented sample, employing a Raman spectroscopy-enhanced instrumented indentation technique (IIT). The occurrence and evolving spatial distribution of changes in the a-Si structure caused by processes, such as polyamorphization and crystallization, induced by indentation loading were observed. Furthermore, the obtained experimental results are linked with previously published work on the plastic deformation of a-Si under hydrostatic compression and shear deformation to establish a model for the deformation behavior of a-Si under indentation loading.

Local deformation behavior of surface porous polyether-ether-ketone.

PubMed

Evans, Nathan T; Torstrick, F Brennan; Safranski, David L; Guldberg, Robert E; Gall, Ken

2017-01-01

Surface porous polyether-ether-ketone has the ability to maintain the tensile monotonic and cyclic strength necessary for many load bearing orthopedic applications while providing a surface that facilitates bone ingrowth; however, the relevant deformation behavior of the pore architecture in response to various loading conditions is not yet fully characterized or understood. The focus of this study was to examine the compressive and wear behavior of the surface porous architecture using micro Computed Tomography (micro CT). Pore architectures of various depths (~0.5-2.5mm) and pore sizes (212-508µm) were manufactured using a melt extrusion and porogen leaching process. Compression testing revealed that the pore architecture deforms in the typical three staged linear elastic, plastic, and densification stages characteristic of porous materials. The experimental moduli and yield strengths decreased as the porosity increased but there was no difference in properties between pore sizes. The porous architecture maintained a high degree of porosity available for bone-ingrowth at all strains. Surface porous samples showed no increase in wear rate compared to injection molded samples, with slight pore densification accompanying wear. Copyright © 2016 Elsevier Ltd. All rights reserved.

Microstructural Evolution and Dynamic Softening Mechanisms of Al-Zn-Mg-Cu Alloy during Hot Compressive Deformation

PubMed Central

Shi, Cangji; Lai, Jing; Chen, X.-Grant

2014-01-01

The hot deformation behavior and microstructural evolution of an Al-Zn-Mg-Cu (7150) alloy was studied during hot compression at various temperatures (300 to 450 °C) and strain rates (0.001 to 10 s−1). A decline ratio map of flow stresses was proposed and divided into five deformation domains, in which the flow stress behavior was correlated with different microstructures and dynamic softening mechanisms. The results reveal that the dynamic recovery is the sole softening mechanism at temperatures of 300 to 400 °C with various strain rates and at temperatures of 400 to 450 °C with strain rates between 1 and 10 s−1. The level of dynamic recovery increases with increasing temperature and with decreasing strain rate. At the high deformation temperature of 450 °C with strain rates of 0.001 to 0.1 s−1, a partially recrystallized microstructure was observed, and the dynamic recrystallization (DRX) provided an alternative softening mechanism. Two kinds of DRX might operate at the high temperature, in which discontinuous dynamic recrystallization was involved at higher strain rates and continuous dynamic recrystallization was implied at lower strain rates. PMID:28788454

Constitutive Equation and Hot Compression Deformation Behavior of Homogenized Al–7.5Zn–1.5Mg–0.2Cu–0.2Zr Alloy

PubMed Central

He, Jianliang; Zhang, Datong; Zhang, Weiweng; Qiu, Cheng; Zhang, Wen

2017-01-01

The deformation behavior of homogenized Al–7.5Zn–1.5Mg–0.2Cu–0.2Zr alloy has been studied by a set of isothermal hot compression tests, which were carried out over the temperature ranging from 350 °C to 450 °C and the strain rate ranging from 0.001 s−1 to 10 s−1 on Gleeble-3500 thermal simulation machine. The associated microstructure was studied using electron back scattered diffraction (EBSD) and transmission electron microscopy (TEM). The results showed that the flow stress is sensitive to strain rate and deformation temperature. The shape of true stress-strain curves obtained at a low strain rate (≤0.1 s−1) conditions shows the characteristic of dynamic recrystallization (DRX). Two Arrhenius-typed constitutive equation without and with strain compensation were established based on the true stress-strain curves. Constitutive equation with strain compensation has more precise predictability. The main softening mechanism of the studied alloy is dynamic recovery (DRV) accompanied with DRX, particularly at deformation conditions, with low Zener-Holloman parameters. PMID:29057825

Dual-phase steel sheets under cyclic tension-compression to large strains: Experiments and crystal plasticity modeling

NASA Astrophysics Data System (ADS)

Zecevic, Milovan; Korkolis, Yannis P.; Kuwabara, Toshihiko; Knezevic, Marko

2016-11-01

In this work, we develop a physically-based crystal plasticity model for the prediction of cyclic tension-compression deformation of multi-phase materials, specifically dual-phase (DP) steels. The model is elasto-plastic in nature and integrates a hardening law based on statistically stored dislocation density, localized hardening due to geometrically necessary dislocations (GNDs), slip-system-level kinematic backstresses, and annihilation of dislocations. The model further features a two level homogenization scheme where the first level is the overall response of a two-phase polycrystalline aggregate and the second level is the homogenized response of the martensite polycrystalline regions. The model is applied to simulate a cyclic tension-compression-tension deformation behavior of DP590 steel sheets. From experiments, we observe that the material exhibits a typical decreasing hardening rate during forward loading, followed by a linear and then a non-linear unloading upon the load reversal, the Bauschinger effect, and changes in hardening rate during strain reversals. To predict these effects, we identify the model parameters using a portion of the measured data and validate and verify them using the remaining data. The developed model is capable of predicting all the particular features of the cyclic deformation of DP590 steel, with great accuracy. From the predictions, we infer and discuss the effects of GNDs, the backstresses, dislocation annihilation, and the two-level homogenization scheme on capturing the cyclic deformation behavior of the material.

Fabrication and Deformation of 3D Multilayered Kirigami Microstructures.

PubMed

Humood, Mohammad; Shi, Yan; Han, Mengdi; Lefebvre, Joseph; Yan, Zheng; Pharr, Matt; Zhang, Yihui; Huang, Yonggang; Rogers, John A; Polycarpou, Andreas A

2018-03-01

Mechanically guided 3D microassembly with controlled compressive buckling represents a promising emerging route to 3D mesostructures in a broad range of advanced materials, including single-crystalline silicon (Si), of direct relevance to microelectronic devices. During practical applications, the assembled 3D mesostructures and microdevices usually undergo external mechanical loading such as out-of-plane compression, which can induce damage in or failure of the structures/devices. Here, the mechanical responses of a few mechanically assembled 3D kirigami mesostructures under flat-punch compression are studied through combined experiment and finite element analyses. These 3D kirigami mesostructures consisting of a bilayer of Si and SU-8 epoxy are formed through integration of patterned 2D precursors with a prestretched elastomeric substrate at predefined bonding sites to allow controlled buckling that transforms them into desired 3D configurations. In situ scanning electron microscopy measurement enables detailed studies of the mechanical behavior of these structures. Analysis of the load-displacement curves allows the measurement of the effective stiffness and elastic recovery of various 3D structures. The compression experiments indicate distinct regimes in the compressive force/displacement curves and reveals different geometry-dependent deformation for the structures. Complementary computational modeling supports the experimental findings and further explains the geometry-dependent deformation. © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Tuned critical avalanche scaling in bulk metallic glasses

DOE PAGES

Antonaglia, James; Xie, Xie; Schwarz, Gregory; ...

2014-03-17

In this study, ingots of the bulk metallic glass (BMG), Zr 64.13Cu 15.75Ni 10.12Al 10 in atomic percent (at. %), are compressed at slow strain rates. The deformation behavior is characterized by discrete, jerky stress-drop bursts (serrations). Here we present a quantitative theory for the serration behavior of BMGs, which is a critical issue for the understanding of the deformation characteristics of BMGs. The mean-field interaction model predicts the scaling behavior of the distribution, D(S), of avalanche sizes, S, in the experiments. D(S) follows a power law multiplied by an exponentially-decaying scaling function. The size of the largest observed avalanchemore » depends on experimental tuning-parameters, such as either imposed strain rate or stress. Similar to crystalline materials, the plasticity of BMGs reflects tuned criticality showing remarkable quantitative agreement with the slip statistics of slowly-compressed nanocrystals. The results imply that material-evaluation methods based on slip statistics apply to both crystalline and BMG materials.« less

Flow Curve Analysis of 17-4 PH Stainless Steel under Hot Compression Test

NASA Astrophysics Data System (ADS)

Mirzadeh, Hamed; Najafizadeh, Abbas; Moazeny, Mohammad

2009-12-01

The hot compression behavior of a 17-4 PH stainless steel (AISI 630) has been investigated at temperatures of 950 °C to 1150 °C and strain rates of 10-3 to 10 s-1. Glass powder in the Rastegaev reservoirs of the specimen was used as a lubricant material. A step-by-step procedure for data analysis in the hot compression test was given. The work hardening rate analysis was performed to reveal if dynamic recrystallization (DRX) occurred. Many samples exhibited typical DRX stress-strain curves with a single peak stress followed by a gradual fall toward the steady-state stress. At low Zener-Hollomon ( Z) parameter, this material showed a new DRX flow behavior, which was called multiple transient steady state (MTSS). At high Z, as a result of adiabatic deformation heating, a drop in flow stress was observed. The general constitutive equations were used to determine the hot working constants of this material. Moreover, after a critical discussion, the deformation activation energy of 17-4 PH stainless steel was determined as 337 kJ/mol.

Mechanical properties and deformation mechanism of Al2O3 determined from in situ transmission electron microscopy compression

NASA Astrophysics Data System (ADS)

Lin, Kai-Peng; Stachiv, Ivo; Fang, Te-Hua

2017-07-01

The mechanical properties and deformation mechanism of alumina (Al2O3) ceramic nanopillars and microstructures have been studied using in situ transmission electron microscopy (TEM) compression and nanoindentation experiments. It has been found that the Young’s modulus of Al2O3 nanopillars significantly increases with a decrease of its thickness; it ranges from 54.8 GPa for the nanopillar of radius 175 nm to 347.5 GPa for the one of radius of 75 nm. The hardness of Al2O3 microstructures estimated by the nanoindentation is between 3.19 to 20.60 GPa. The Raman spectra of Al2O3 substrate has a production peak (577.3 cm-1) between 418.3 and 645.2 (cm-1) peaks. The strain hardening behavior of Al2O3 microstructures has been observed and the impact of size on the compressive and bending behavior of Al2O3 micro-pillared structures is also examined and explained.

Effect of swaging on the 1000 C compressive slow plastic flow characteristics of the directionally solidified eutectic alloy gamma/gamma prime-alpha

NASA Technical Reports Server (NTRS)

Whittenberger, J. D.; Wirth, G.

1983-01-01

Swaging between 750 and 1050 C has been investigated as a means to introduce work into the directionally solidified eutectic alloy gamma/gamma prime-alpha (Ni-32.3 wt percent Mo-6.3 wt percent Al) and increase the elevated temperature creep strength. The 1000 C slow plastic compressive flow stress-strain rate properties in air of as-grown, annealed, and worked nominally 10 and 25 percent materials have been determined. Swaging did not improve the slow plastic behavior. In fact large reductions tended to degrade the strength and produced a change in the deformation mechanism from uniform flow to one involving intense slip band formation. Comparison of 1000 C tensile and compressive strength-strain rate data reveals that deformation is independent of the stress state.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhang, Junsong; Hao, Shijie; Yu, Cun

The deformation behavior and load transfer of a dual-phase composite composed of martensite NiTi embedded in brittle Ti{sub 2}Ni matrices were investigated by using in situ synchrotron x-ray diffraction during compression. The composite exhibits a stage-wise deformation feature and a double-yielding phenomenon, which were caused by the interaction between Ti{sub 2}Ni and NiTi with alternative microscopic deformation mechanism. No load transfer occurs from the soft NiTi dendrites to the hard Ti{sub 2}Ni matrices during the pseudoplastic deformation (detwinning) of NiTi, which is significantly different from that previously reported in bulk metallic glasses matrices composites.

Formation of the structure and properties of an Mg-Al-Zn-Mn alloy during plastic deformation by rolling

NASA Astrophysics Data System (ADS)

Bozhko, S. A.; Betsofen, S. Ya.; Kolobov, Yu. R.; Vershinina, T. N.

2015-03-01

The laws of formation of an ultrafine structure in an Mg-Al-Zn-Mn alloy (MA5 alloy) under severe plastic deformation have been studied during lengthwise section rolling at a strain e = 1.59. The deformation behavior and the physical factors of anisotropy of yield strength during compression tests in various directions with respect to axis of rolling are analyzed. The role of crystallographic texture and twinning processes in the generation of strength processes and the development of plastic deformation of the alloy is analyzed.

The hot deformation behavior and microstructure evolution of HA/Mg-3Zn-0.8Zr composites for biomedical application.

PubMed

Liu, Debao; Liu, Yichi; Zhao, Yue; Huang, Y; Chen, Minfang

2017-08-01

The hot deformation behavior of nano-sized hydroxylapatite (HA) reinforced Mg-3Zn-0.8Zr composites were performed by means of Gleeble-1500D thermal simulation machine in a temperature range of 523-673K and a strain rate range of 0.001-1s -1 , and the microstructure evolution during hot compression deformation were also investigated. The results show that the flow stress increases increasing strain rates at a constant temperature, and decreases with increasing deforming temperatures at a constant strain rate. Under the same processing conditions, the flow stresses of the 1HA/Mg-3Zn-0.8Zr specimens are higher than those of the Mg-3Zn-0.8Zr alloy specimens, and the difference is getting closer with increasing deformation temperature. The hot deformation behaviors of Mg-3Zn-0.8Zr and 1HA/Mg-3Zn-0.8Zr can be described by constitutive equation of hyperbolic sine function with the hot deformation activation energy being 124.6kJ/mol and 125.3kJ/mol, respectively. Comparing with Mg-3Zn-0.8Zr alloy, the instability region in the process map of 1HA/Mg-3Zn-0.8Zr expanded to a bigger extent at the same conditions. The optimum process conditions of 1HA/Mg-3Zn-0.8Zr composite is concluded as between the temperature window of 573-623K with a strain rate range of 0.001-0.1s -1 . A higher volume fraction and smaller grain size of dynamic recrystallization (DRX) grains was observed in 1HA/Mg-3Zn-0.8Zr specimens after the hot compression deformation compared with Mg-3Zn-0.8Zr alloy, which was ascribed to the presence of the HA particles that play an important role in particle-stimulated nucleation (PSN) mechanism and can effectively hinder the migration of interfaces. Copyright © 2017 Elsevier B.V. All rights reserved.

Radiologic study of disc behavior following compression fracture of the thoracolumbar hinge managed by kyphoplasty: A 52-case series.

PubMed

Teyssédou, S; Saget, M; Gayet, L E; Pries, P; Brèque, C; Vendeuvre, T

2016-02-01

Kyphoplasty has proved effective for durable correction of traumatic vertebral deformity following Magerl A fracture, but subsequent behavior of the adjacent discs is unclear. The objective of the present study was to analyze evolution according to severity of initial kyphosis and quality of fracture reduction. A single-center prospective study included cases of single compression fracture of the thoracolumbar hinge managed by Kyphon Balloon Kyphoplasty with polymethylmethacrylate bone cement. Radiology focused on traumatic vertebral kyphosis (VK), disc angulation (DA) and disc height index (DHI) in the adjacent discs. Linear regression assessed the correlation between superior disc height index (SupDHI) and postoperative VK on the one hand and correction gain on the other, using the Student t test for matched pairs and Pearson correlation coefficient. Fifty-two young patients were included, with mean follow-up of 18.6 months. VK fell from 13.9° preoperatively to 8.2° at last follow-up. DHI found significant superior disc subsidence (P=0.0001) and non-significant inferior disc subsidence (P=0.116). DA showed significantly reduced superior disc lordosis (P=4*10(-5)). SupDHI correlated with VK correction (r=0.32). Preoperative VK did not correlate with radiologic degeneration of the adjacent discs. Correction of traumatic vertebral deformity avoids subsidence and loss of mechanical function in the superior adjacent disc. The underlying disc compensates for residual deformity. Balloon kyphoplasty is useful in compression fracture, providing significant reduction of traumatic vertebral deformity while conserving free and healthy adjacent discs. IV. Copyright © 2015 Elsevier Masson SAS. All rights reserved.

Microstructure and Deformation Response of TRIP-Steel Syntactic Foams to Quasi-Static and Dynamic Compressive Loads

PubMed Central

Ehinger, David; Weise, Jörg; Baumeister, Joachim; Funk, Alexander; Krüger, Lutz; Martin, Ulrich

2018-01-01

The implementation of hollow S60HS glass microspheres and Fillite 106 cenospheres in a martensitically transformable AISI 304L stainless steel matrix was realized by means of metal injection molding of feedstock with varying fractions of the filler material. The so-called TRIP-steel syntactic foams were studied with respect to their behavior under quasi-static compression and dynamic impact loading. The interplay between matrix material behavior and foam structure was discussed in relation to the findings of micro-structural investigations, electron back scatter diffraction EBSD phase analyses and magnetic measurements. During processing, the cenospheres remained relatively stable retaining their shape while the glass microspheres underwent disintegration associated with the formation of pre-cracked irregular inclusions. Consequently, the AISI 304L/Fillite 106 syntactic foams exhibited a higher compression stress level and energy absorption capability as compared to the S60HS-containing variants. The α′ -martensite kinetic of the steel matrix was significantly influenced by material composition, strain rate and arising deformation temperature. The highest ferromagnetic α′-martensite phase fraction was detected for the AISI 304L/S60HS batches and the lowest for the TRIP-steel bulk material. Quasi-adiabatic sample heating, a gradual decrease in strain rate and an enhanced degree of damage controlled the mechanical deformation response of the studied syntactic foams under dynamic impact loading. PMID:29695107

Microstructure and Deformation Response of TRIP-Steel Syntactic Foams to Quasi-Static and Dynamic Compressive Loads.

PubMed

Ehinger, David; Weise, Jörg; Baumeister, Joachim; Funk, Alexander; Waske, Anja; Krüger, Lutz; Martin, Ulrich

2018-04-24

The implementation of hollow S60HS glass microspheres and Fillite 106 cenospheres in a martensitically transformable AISI 304L stainless steel matrix was realized by means of metal injection molding of feedstock with varying fractions of the filler material. The so-called TRIP-steel syntactic foams were studied with respect to their behavior under quasi-static compression and dynamic impact loading. The interplay between matrix material behavior and foam structure was discussed in relation to the findings of micro-structural investigations, electron back scatter diffraction EBSD phase analyses and magnetic measurements. During processing, the cenospheres remained relatively stable retaining their shape while the glass microspheres underwent disintegration associated with the formation of pre-cracked irregular inclusions. Consequently, the AISI 304L/Fillite 106 syntactic foams exhibited a higher compression stress level and energy absorption capability as compared to the S60HS-containing variants. The α ′ -martensite kinetic of the steel matrix was significantly influenced by material composition, strain rate and arising deformation temperature. The highest ferromagnetic α ′ -martensite phase fraction was detected for the AISI 304L/S60HS batches and the lowest for the TRIP-steel bulk material. Quasi-adiabatic sample heating, a gradual decrease in strain rate and an enhanced degree of damage controlled the mechanical deformation response of the studied syntactic foams under dynamic impact loading.

Deformation of high performance concrete plate under humid tropical weather

NASA Astrophysics Data System (ADS)

Niken, C.; Elly, T.; Supartono, FX; Laksmi, I.

2018-03-01

This paper presents the relationship between surrounding relative humidity and temperature on deformation behavior of one sample concrete plate with compressive strength of 60MPa. This research was done in Indonesia that is in humid tropical weather. A specimens measuring 3000 mm × 1600 mm × 150 mm were used. The behavior was obtained by using four embedded vibrating wire strain gauges (VWESG). As a result there is a very strong relationship between humidity and deformation at the age range of 7 until 21 days. The largest deformation occurs in the corner and the fluctuation of deformation in side position is larger than in the corner and in the middle. The peaks of surrounding relative humidity were fully followed by the deepest valley of deformation on time in the corner, while in another position the range delay time was 8 - 11 hours. There is a strong relationship between surrounding temperature and deformation at the range of 7 until 14 days. The influenced of surrounding relative humidity to concrete behavior is faster and longer than surrounding temperature. The influence of surrounding temperature in humid tropical weather was shorter than in non-humid tropical weather.

Compressive Strength and Indentation Damage in Ceramic Materials.

DTIC Science & Technology

1978-05-31

The extent of the plastically deformed region associated with indentation in silicon carbide is determined by means of selected area electron...microfracture mechanisms responsible for the temperature-sensitive compressive strength behavior of polycrystalline Al2O3 and alpha-SiC. It is determined ...that the early stages of damage can be related to the presence or absence of microplasticity , depending upon the ceramic. Further, local plastic flow in

Analysis of Shock Compression of Strong Single Crystals With Logarithmic Thermoelastic-Plastic Theory

DTIC Science & Technology

2014-05-01

Royal Society of London Series A, 465, 307–334. Clayton, J. (2010a). Modeling nonlinear electromechanical behavior of shocked silicon carbide . Journal...and fourth-order longitudinal elastic constants by shock compression techniques–application to sapphire and fused quartz. Journal of the Acoustical...Vogler, T., & Clayton, J. (2008). Heterogeneous deformation and spall of an extruded tungsten alloy: Plate impact experiments and crystal plasticity

Dynamic Recrystallization Kinetics of 690 Alloy During Hot Compression of Double-Cone Samples

NASA Astrophysics Data System (ADS)

Wang, Jue; Zhai, Shun-Chao

2017-03-01

Hot compression tests of double-cone samples were conducted for 690 alloy to study the kinetic behavior of the complete dynamic recrystallization (DRX) process under low deformation temperatures from 960 to 1080 °C. The microstructure of 82 points in the vertical section of every deformed sample was quantitatively analyzed to determine the DRX fraction. Corresponding strain of these points was calculated by finite element simulations. Kinetic curves of the specimens with different preheating temperatures were then constructed. The features of various boundaries with different misorientation angles were investigated by electron backscatter diffraction technology and transmission electron microscope. The results showed that the strain is continuously and symmetrically distributed along the centerline of the vertical section. Large strain of 1.84 was obtained when the compression amount is 12 mm for double-cone samples. All the fitted kinetic curves display an "S" type, which possess a low growth rate of DRX at the beginning and the end of compression. The critical strain of recrystallization decreases with the increase in preheating temperature, while the completion strain remains around 1.5 for all the samples. The initial and maximum growth rates of DRX fraction have the opposite trend with the change in temperature, which is considered to be attributed to the behaviors of different misorientation boundaries.

Modeling the Nonlinear, Strain Rate Dependent Deformation of Shuttle Leading Edge Materials with Hydrostatic Stress Effects Included

NASA Technical Reports Server (NTRS)

Goldberg, Robert K.; Carney, Kelly S.

2004-01-01

An analysis method based on a deformation (as opposed to damage) approach has been developed to model the strain rate dependent, nonlinear deformation of woven ceramic matrix composites, such as the Reinforced Carbon Carbon (RCC) material used on the leading edges of the Space Shuttle. In the developed model, the differences in the tension and compression deformation behaviors have also been accounted for. State variable viscoplastic equations originally developed for metals have been modified to analyze the ceramic matrix composites. To account for the tension/compression asymmetry in the material, the effective stress and effective inelastic strain definitions have been modified. The equations have also been modified to account for the fact that in an orthotropic composite the in-plane shear response is independent of the stiffness in the normal directions. The developed equations have been implemented into LS-DYNA through the use of user defined subroutines (UMATs). Several sample qualitative calculations have been conducted, which demonstrate the ability of the model to qualitatively capture the features of the deformation response present in woven ceramic matrix composites.

The deformation and failure response of closed-cell PMDI foams subjected to dynamic impact loading

DOE PAGES

Koohbor, Behrad; Mallon, Silas; Kidane, Addis; ...

2015-04-07

The present work aims to investigate the bulk deformation and failure response of closed-cell Polymeric Methylene Diphenyl Diisocyanate (PMDI) foams subjected to dynamic impact loading. First, foam specimens of different initial densities are examined and characterized in quasi-static loading conditions, where the deformation behavior of the samples is quantified in terms of the compressive elastic modulus and effective plastic Poisson's ratio. Then, the deformation response of the foam specimens subjected to direct impact loading is examined by taking into account the effects of material compressibility and inertia stresses developed during deformation, using high speed imaging in conjunction with 3D digitalmore » image correlation. The stress-strain response and the energy absorption as a function of strain rate and initial density are presented and the bulk failure mechanisms are discussed. As a result, it is observed that the initial density of the foam and the applied strain rates have a substantial influence on the strength, bulk failure mechanism and the energy dissipation characteristics of the foam specimens.« less

Mass-related traumatic tissue displacement and behavior: a screen for treatments that reduce [corrected] harm to bystander cells and recovery of function.

PubMed

Yang, Hongyan; Preston, Marnie; Chopp, Michael; Jiang, Feng; Zhang, Xuepeng; Schallert, Timothy

2006-05-01

In this study, we focused on a preclinical model of brain compression injury that has relevance to pathological conditions such as tumor, hematoma, blood clot, and intracerebral bony fragment. We investigated behavioral impairment as a result of rapid-onset small mass, and the factors involved in lesion formation and neuroplasticity. An epidural bead implantation method was adopted. Two sizes (1.5 mm and 2.0 mm thick) of hemisphere-shaped beads were used. The beads were implanted into various locations over the sensorimotor cortex (SMC--anterior, middle and posterior). The effects of early versus delayed bead removal were examined to model clinical neurosurgical or other treatment procedures. Forelimb and hind-limb behavioral deficits and recovery were observed, and histological changes were quantified to determine brain reaction to focal compression. Our results showed that the behavioral deficits of compression were influenced by the location, timing of compression release, and magnitude of compression. Even persistent compression by the thicker bead (2.0 mm) caused only minor behavioral deficits, followed by fast recovery within a week in most animals, suggesting a mild lesion pattern for this model. Brain tissue was compressed into a deformed shape under pressure with slight tissue damage, evidenced by pathological evaluation on hematoxylin and eosin (H&E)- and TUNEL-stained sections. Detectable but not severe behavioral dysfunction exhibited by this model makes it particularly suitable for direct assessment of adverse effects of interventions on neuroplasticity after brain compression injury. This model may permit development of treatment strategies to alleviate brain mass effects, without disrupting neuroplasticity.

Shock-Wave Pulse Compression and Stretching of Dodecane and Mineral Oils

NASA Astrophysics Data System (ADS)

Bannikova, I. A.; Zubareva, A. N.; Utkin, A. V.

2018-04-01

The behavior of dodecane, vacuum, and transformer oils under shock-wave pulse compression and stretching are studied experimentally. The wave profiles are registered using a VISAR laser interferometer. The shock adiabats, the dependence of the sound velocity on the pressure, and the maximum negative pressures developed in the studied liquids are determined. It is shown that the negative pressure value does not depend on the deformation rate in the case of oils and is a strong function of the compression pulse amplitude in the case of dodecane.

Compression Behavior and Energy Absorption of Aluminum Alloy AA6061 Tubes with Multiple Holes

NASA Astrophysics Data System (ADS)

Simhachalam, Bade; Lakshmana Rao, C.; Srinivas, Krishna

2014-05-01

In this article, compression behavior and energy absorption of aluminum alloy AA6061 tubes are investigated both experimentally and numerically. Static and dynamic simulations are done using LS-Dyna Software for AA6061 tubes. True stress-plastic strain curves from the tensile test are used in the static and dynamic simulations of AA6061 tubes. The energy absorption values between experimental compression results and numeral simulation are found to be in good agreement. Dynamic simulations are done with drop velocity of up to 10 m/s to understand the inertia effects on energy absorption. The deformed modes from the numerical simulation are compared between tubes with and without holes in static and dynamic conditions.

Texture Studies and Compression Behaviour of Apple Flesh

NASA Astrophysics Data System (ADS)

James, Bryony; Fonseca, Celia

Compressive behavior of fruit flesh has been studied using mechanical tests and microstructural analysis. Apple flesh from two cultivars (Braeburn and Cox's Orange Pippin) was investigated to represent the extremes in a spectrum of fruit flesh types, hard and juicy (Braeburn) and soft and mealy (Cox's). Force-deformation curves produced during compression of unconstrained discs of apple flesh followed trends predicted from the literature for each of the "juicy" and "mealy" types. The curves display the rupture point and, in some cases, a point of inflection that may be related to the point of incipient juice release. During compression these discs of flesh generally failed along the centre line, perpendicular to the direction of loading, through a barrelling mechanism. Cryo-Scanning Electron Microscopy (cryo-SEM) was used to examine the behavior of the parenchyma cells during fracture and compression using a purpose designed sample holder and compression tester. Fracture behavior reinforced the difference in mechanical properties between crisp and mealy fruit flesh. During compression testing prior to cryo-SEM imaging the apple flesh was constrained perpendicular to the direction of loading. Microstructural analysis suggests that, in this arrangement, the material fails along a compression front ahead of the compressing plate. Failure progresses by whole lines of parenchyma cells collapsing, or rupturing, with juice filling intercellular spaces, before the compression force is transferred to the next row of cells.

Instability of fiber-reinforced viscoelastic composite plates to in-plane compressive loads

NASA Technical Reports Server (NTRS)

Chandiramani, N. K.; Librescu, L.

1990-01-01

This study analyzes the stability behavior of unidirectional fiber-reinforced composite plates with viscoelastic material behavior subject to in-plane biaxial compressive edge loads. To predict the effective time-dependent material properties, elastic fibers embedded in a linearly viscoelastic matrix are examined. The micromechanical relations developed for a transversely isotropic medium are discussed along with the correspondence principle of linear viscoelasticity. It is concluded that the stability boundary obtained for a viscoelastic plate is lower (more critical) than its elastic counterpart, and the transverse shear deformation effects are more pronounced in viscoelastic plates than in their elastic counterparts.

Analysis of behavior of simply supported flat plates compressed beyond the buckling load into the plastic range

NASA Technical Reports Server (NTRS)

Mayers, J; Budiansky, Bernard

1955-01-01

An analysis is presented of the postbuckling behavior of a simply supported square flat plate with straight edges compressed beyond the buckling load into the plastic range. The method of analysis involves the application of a variational principle of the deformation theory of plasticity in conjunction with computations carried out on a high-speed calculating machine. Numerical results are obtained for several plate proportions and for one material. The results indicate plate strengths greater than those that have been found experimentally on plates that do not satisfy straight-edge conditions. (author)

Three-Dimensional Numerical Simulation on Triaxial Failure Mechanical Behavior of Rock-Like Specimen Containing Two Unparallel Fissures

NASA Astrophysics Data System (ADS)

Huang, Yan-Hua; Yang, Sheng-Qi; Zhao, Jian

2016-12-01

A three-dimensional particle flow code (PFC3D) was used for a systematic numerical simulation of the strength failure and cracking behavior of rock-like material specimens containing two unparallel fissures under conventional triaxial compression. The micro-parameters of the parallel bond model were first calibrated using the laboratory results of intact specimens and then validated from the experimental results of pre-fissured specimens under triaxial compression. Numerically simulated stress-strain curves, strength and deformation parameters and macro-failure modes of pre-fissured specimens were all in good agreement with the experimental results. The relationship between stress and the micro-crack numbers was summarized. Crack initiation, propagation and coalescence process of pre-fissured specimens were analyzed in detail. Finally, horizontal and vertical cross sections of numerical specimens were derived from PFC3D. A detailed analysis to reveal the internal damage behavior of rock under triaxial compression was carried out. The experimental and simulated results are expected to improve the understanding of the strength failure and cracking behavior of fractured rock under triaxial compression.

Flow behavior of Ti-24Al-11Nb at high strain rates

DOE Office of Scientific and Technical Information (OSTI.GOV)

Harbison, L.S.; Koss, D.A.; Bourcier, R.J.

The deformation and crack initiation behavior of Ti-24Al-11Nb has been examined over a temperature range of 298 to 923 K and for strain rates from 10{sup {minus}4}/s to 10{sup 2}/s. Tests performed in compression indicate much lower strain hardening at 10{sup 2}/s than at either 10{sup {minus}1}/s or 10{sup {minus}4}/s at all temperatures. Associated with this behavior is the occurrence of non-uniform, localized deformation bands at 10{sup 2}/s. An analysis indicates that adiabatic deformation conditions predominate at 10{sup 2}/s and that these result in adiabatic softening. Furthermore, as a result of non-uniform deformation and adiabatic heating, this Ti{sub 3}-Al-based alloymore » is actually more resistant to strain-induced microcrack initiation at 10{sup 2}/s than at 10{sup {minus}4}/s during room temperature testing. 16 refs., 7 figs.« less

Influence of High-Current-Density Impulses on the Compression Behavior: Experiments with Iron and a Nickel-Based Alloy

NASA Astrophysics Data System (ADS)

Demler, E.; Gerstein, G.; Dalinger, A.; Epishin, A.; Rodman, D.; Nürnberger, F.

2017-01-01

Difficulties of processing of high strength and/or brittle materials by plastic deformation, e.g., by forging, require to develop new industrial technologies. In particular, the feasible deformation rates are limited for low-ductile metallic materials. For this reason, processes were investigated to improve the deformability in which electrical impulses are to be applied to lower the yield strength. However, owing to the impulse duration and low current densities, concomitant effects always occur, e.g., as a result of Joule heating. Current developments in power electronics allow now to transmit high currents as short pulses. By reducing the impulse duration and increasing the current density, the plasticity of metallic materials can be correspondingly increased. Using the examples of polycrystalline iron and a single-crystal, nickel-based alloy (PWA 1480), current advances in the development of methods for forming materials by means of high-current-density impulses are demonstrated. For this purpose, appropriate specimens were loaded in compression and, using novel testing equipment, subjected to a current strength of 10 kA with an impulse duration of 2 ms. For a pre-defined strain, the test results show a significant decrease in the compressive stress during the compression test and a significant change in the dislocation distribution following the current impulse treatment.

Elastic Behavior of a Rubber Layer Bonded between Two Rigid Spheres.

DTIC Science & Technology

1988-05-01

Cracking, Composites, Compressibility, Def ormition, Dilatancy, Elasticity, Elastomers , Failure, Fracture, Particle ’,-1tr1f6rcement, Rubber, Stress...Analysis. 2.AITRACT (Ca~mmi ON VOW...lds It 񔨾Y MtE fIdnt & bp04 bo ambwe - Finite element methods ( FEM ) have been employed to calculate the stresses...deformations set up by compression or extension of the layer, using finite element methods ( FEM ) and not invoking the condition of incompressibility

Hot deformation behaviors and processing maps of B{sub 4}C/Al6061 neutron absorber composites

DOE Office of Scientific and Technical Information (OSTI.GOV)

Li, Yu-Li

In this study, the hot deformation behaviors of 30 wt.% B{sub 4}C/Al6061 neutron absorber composites (NACs) have been investigated by conducting isothermal compression tests at temperatures ranging from 653 K to 803 K and strain rates from 0.01 to 10 s{sup −1}. It was found that, during hot compression, the B{sub 4}C/Al6061 NACs exhibited a steady flow characteristic which can be expressed by the Zener-Hollomon parameter as a hyperbolic-sine function of flow stress. High average activation energy (185.62 kJ/mol) of B{sub 4}C/Al6061 NACs is noted in current study owing to the high content of B{sub 4}C particle. The optimum hotmore » working conditions for B{sub 4}C/Al6061 NACs are found to be 760–803 K/0.01–0.05 s{sup −1} based on processing map and microstructure evolution. Typical material instabilities are thought to be attributed to void formation, adiabatic shear bands (ASB), particle debonding, and matrix cracking. Finally, the effect of the plastic deformation zones (PDZs) on the microstructure evolution in this 30 wt.% B{sub 4}C/Al6061 composite is found to be very important. - Highlights: •The hot deformation behavior of the 30 wt.% B{sub 4}C/Al6061 NACs was first analyzed. •The 3D efficiency map and the instability map are developed. •The optimum hot working conditions were identified and validated by SEM and TEM. •The hot deformation schematic diagram of 30 wt.% B{sub 4}C/Al6061 NACs is developed.« less

Effect of cooling rates on the structure, density and micro-indentation behavior of the Fe, Co-based bulk metallic glass

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lesz, Sabina, E-mail: sabina.lesz@polsl.pl

The experiments demonstrate that ductility of the samples of bulk metallic glass (BMG) with the same chemical composition increased with decreasing sample size. It is shown that microhardness and density increases with decreasing the cooling rate. The fracture morphology of rods after compressive fracture were different on the cross section. Two characteristic features of the compressive fracture morphologies of metallic glasses (MGs) were observed in samples: smooth region and the vein pattern. Many parallel shear bands were observed on the deformed specimen with ϕ = 2 mm in diameter. The results provide more understanding on the relationship among the coolingmore » rate, structure and micro-indentation behavior of the Fe-Co-based BMGs. - Highlights: •Fracture morphology and micro-indentation behavior is studied. •The smaller BMG sample exhibits the larger plasticity. •Microhardness and density increase with decreasing the cooling rate. •Formation of shear bands has been reported in deformed specimens. •Structure and mechanical properties of BMGs can be controlled by the cooling rate.« less

The Temperature Effect on the Compressive Behavior of Closed-Cell Aluminum-Alloy Foams

NASA Astrophysics Data System (ADS)

Movahedi, Nima; Linul, Emanoil; Marsavina, Liviu

2018-01-01

In this research, the mechanical behavior of closed-cell aluminum (Al)-alloy foams was investigated at different temperatures in the range of 25-450 °C. The main mechanical properties of porous Al-alloy foams are affected by the testing temperature, and they decrease with the increase in the temperature during uniaxial compression. From both the constant/serrated character of stress-strain curves and macro/microstructural morphology of deformed cellular structure, it was found that Al foams present a transition temperature from brittle to ductile behavior around 192 °C. Due to the softening of the cellular structure at higher temperatures, linear correlations of the stress amplitude and that of the absorbed energy with the temperature were proposed. Also, it was observed that the presence of inherent defects like micropores in the foam cell walls induced further local stress concentration which weakens the cellular structure's strength and crack propagation and cell-wall plastic deformation are the dominant collapse mechanisms. Finally, an energy absorption study was performed and an optimum temperature was proposed.

Modeling the Flow Behavior, Recrystallization, and Crystallographic Texture in Hot-Deformed Fe-30 Wt Pct Ni Austenite

NASA Astrophysics Data System (ADS)

Abbod, M. F.; Sellars, C. M.; Cizek, P.; Linkens, D. A.; Mahfouf, M.

2007-10-01

The present work describes a hybrid modeling approach developed for predicting the flow behavior, recrystallization characteristics, and crystallographic texture evolution in a Fe-30 wt pct Ni austenitic model alloy subjected to hot plane strain compression. A series of compression tests were performed at temperatures between 850 °C and 1050 °C and strain rates between 0.1 and 10 s-1. The evolution of grain structure, crystallographic texture, and dislocation substructure was characterized in detail for a deformation temperature of 950 °C and strain rates of 0.1 and 10 s-1, using electron backscatter diffraction and transmission electron microscopy. The hybrid modeling method utilizes a combination of empirical, physically-based, and neuro-fuzzy models. The flow stress is described as a function of the applied variables of strain rate and temperature using an empirical model. The recrystallization behavior is predicted from the measured microstructural state variables of internal dislocation density, subgrain size, and misorientation between subgrains using a physically-based model. The texture evolution is modeled using artificial neural networks.

Properties of a Ni(sub 19.5)Pd(sub 30)Ti(sub 50.5) high-temperature shape memory alloy in tension and compression

NASA Technical Reports Server (NTRS)

Noebe, Ronald; Padula, Santo, II; Bigelow, Glen; Rios, Orlando; Garg, Anita; Lerch, Brad

2006-01-01

Potential applications involving high-temperature shape memory alloys have been growing in recent years. Even in those cases where promising new alloys have been identified, the knowledge base for such materials contains gaps crucial to their maturation and implementation in actuator and other applications. We begin to address this issue by characterizing the mechanical behavior of a Ni19.5Pd30Ti50.5 high-temperature shape memory alloy in both uniaxial tension and compression at various temperatures. Differences in the isothermal uniaxial deformation behavior were most notable at test temperatures below the martensite finish temperature. The elastic modulus of the material was very dependent on strain level; therefore, dynamic Young#s Modulus was determined as a function of temperature by an impulse excitation technique. More importantly, the performance of a thermally activated actuator material is dependent on the work output of the alloy. Consequently, the strain-temperature response of the Ni19.5Pd30Ti50.5 alloy under various loads was determined in both tension and compression and the specific work output calculated and compared in both loading conditions. It was found that the transformation strain and thus, the specific work output were similar regardless of the loading condition. Also, in both tension and compression, the strain-temperature loops determined under constant load conditions did not close due to the fact that the transformation strain during cooling was always larger than the transformation strain during heating. This was apparently the result of permanent plastic deformation of the martensite phase with each cycle. Consequently, before this alloy can be used under cyclic actuation conditions, modification of the microstructure or composition would be required to increase the resistance of the alloy to plastic deformation by slip.

Characterization of the Hot Deformation Behavior of a Newly Developed Nickel-Based Superalloy

NASA Astrophysics Data System (ADS)

Shi, Zhaoxia; Yan, Xiaofeng; Duan, Chunhua; Tang, Cunjiang; Pu, Enxiang

2018-03-01

To clarify the microstructural evolution and hot workability of GH4282 during hot forming processes, the hot deformation behavior of this superalloy was investigated by isothermal compression tests in the temperature interval of 950-1210 °C and the strain rate range of 0.01-10 s-1 with a true strain of 0.7. The results show that the flow stresses decrease with an increase in the deformation temperature and a decrease in the strain rate. The characteristic of dynamic recrystallization is revealed by the flow curves. The variation rule of the flow stress can be well described by the hyperbolic sine type equation, and the thermal deformation activation energy is determined to be 498.118 kJ/mol. The optimum hot working parameters are 1100-1180 °C and 0.01-0.1 s-1, under which the fine and uniform microstructure can be obtained.

Temperature effects on deformation and serration behavior of high-entropy alloys (HEAs)

DOE PAGES

Antonaglia, J.; Xie, X.; Tang, Z.; ...

2014-09-16

Many materials are known to deform under shear in an intermittent way with slip avalanches detected as acoustic emission and serrations in the stress–strain curves. Similar serrations have recently been observed in a new class of materials, called high-entropy alloys (HEAs). Here, we discuss the serration behaviors of several HEAs from cryogenic to elevated temperatures. The experimental results of slow compression and tension tests are compared with the predictions of a slip-avalanche model for the deformation of a broad range of solids. The results shed light on the deformation processes in HEAs. Temperature effects on the distributions of stress dropsmore » and the decrease of the cutoff (i.e., of the largest observed slip size) for increasing temperature qualitatively agree with the model predictions. As a result, the model is used to quantify the serration characteristics of HEAs, and pertinent implications are discussed.« less

Investigation on Static Softening Behaviors of a Low Carbon Steel Under Ferritic Rolling Condition

NASA Astrophysics Data System (ADS)

Dong, Haifeng; Cai, Dayong; Zhao, Zhengzheng; Wang, Zhiyong; Wang, Yuhui; Yang, Qingxiang; Liao, Bo

2010-03-01

The study aims to postulate a theoretical hypothesis for the finishing period of ferritic rolling technique of the low carbon steel. The static softening behavior during multistage hot deformation of a low carbon steel has been studied by double hot compression tests at 700-800 °C and strain rate of 1 s-1 using a Gleeble-3500 simulator. Interrupted deformation is conducted with interpass times varying from 1 to 100 s after achieving a true strain of 0.5 in the first stage. The results indicate that the flow stress value at the second deformation is lower than that at the first one, and the flow stress drops substantially. The static softening effects increase with the increase of deformation temperature, holding temperature, and interpass time. The value of the ferritic static softening activation energy is obtained, and the static softening kinetics is modeled by the Avrami equation.

Study on the Aging Behaviors of Rubber Materials in Tension and Compression Loads

NASA Astrophysics Data System (ADS)

Jiang, Can; Wang, Hongyu; Ma, Xiaobing

Rubber materials are widely used in aviation, aerospace, shipbuilding, automobile and other military field. However, rubber materials are easy to aging, which largely restricts its using life. In working environment, due to the combined effect of heat and oxygen, vulcanized rubber will undergo degradation and crosslinking reaction which will cause elasticity decease and permanent deformation, so mostly rubber products are used under stress state. Due to the asymmetric structure and asymmetric stress distribution, mechanical stress may cause serious damage to molecular structure; therefore, this paper is aimed to analyze the aging behavior of rubber materials under tensile and compressive loadings, through analyzing experiment data, and adopting Gauss function to describe stress relaxation coefficient, to build an aging equation containing compression ratio parameter and aging time.

Determination of elastomeric foam parameters for simulations of complex loading.

PubMed

Petre, M T; Erdemir, A; Cavanagh, P R

2006-08-01

Finite element (FE) analysis has shown promise for the evaluation of elastomeric foam personal protection devices. Although appropriate representation of foam materials is necessary in order to obtain realistic simulation results, material definitions used in the literature vary widely and often fail to account for the multi-mode loading experienced by these devices. This study aims to provide a library of elastomeric foam material parameters that can be used in FE simulations of complex loading scenarios. Twelve foam materials used in footwear were tested in uni-axial compression, simple shear and volumetric compression. For each material, parameters for a common compressible hyperelastic material model used in FE analysis were determined using: (a) compression; (b) compression and shear data; and (c) data from all three tests. Material parameters and Drucker stability limits for the best fits are provided with their associated errors. The material model was able to reproduce deformation modes for which data was provided during parameter determination but was unable to predict behavior in other deformation modes. Simulation results were found to be highly dependent on the extent of the test data used to determine the parameters in the material definition. This finding calls into question the many published results of simulations of complex loading that use foam material parameters obtained from a single mode of testing. The library of foam parameters developed here presents associated errors in three deformation modes that should provide for a more informed selection of material parameters.

A numerical and experimental study of temperature effects on deformation behavior of carbon steels at high strain rates

NASA Astrophysics Data System (ADS)

Pouya, M.; Winter, S.; Fritsch, S.; F-X Wagner, M.

2017-03-01

Both in research and in the light of industrial applications, there is a growing interest in methods to characterize the mechanical behavior of materials at high strain rates. This is particularly true for steels (the most important structural materials), where often the strain rate-dependent material behavior also needs to be characterized in a wide temperature range. In this study, we use the Finite Element Method (FEM), first, to model the compressive deformation behavior of carbon steels under quasi-static loading conditions. The results are then compared to experimental data (for a simple C75 steel) at room temperature, and up to testing temperatures of 1000 °C. Second, an explicit FEM model that captures wave propagation phenomena during dynamic loading is developed to closely reflect the complex loading conditions in a Split-Hopkinson Pressure Bar (SHPB) - an experimental setup that allows loading of compression samples with strain rates up to 104 s-1 The dynamic simulations provide a useful basis for an accurate analysis of dynamically measured experimental data, which considers reflected elastic waves. By combining numerical and experimental investigations, we derive material parameters that capture the strain rate- and temperature-dependent behavior of the C75 steel from room temperature to 1000 °C, and from quasi-static to dynamic loading.

Anomalous compression behavior of ˜12 nm nanocrystalline TiO2

NASA Astrophysics Data System (ADS)

Wang, Qiming; Li, Shourui; Peng, Fang; Lei, Li; Hu, Qiwei; Wang, Pei; Nan, Xiaolong; Liu, Jing; Zhu, Wenjun; He, Duanwei

2017-06-01

When the grain size decreases, there inevitably exists a critical size (dc) where the contribution of surface atoms to the physical properties is competitive with that of the interior atoms, giving rise to a wide variety of new phenomena. The behavior of granular materials near dc is particularly interesting because of the crossover, a continuous transition from one type of mechanism to another. In situ high-pressure x-ray diffraction experiments showed that the compression curve of nanocrystalline anatase TiO2 with grain size near dc reached a platform after about 5%-6% of deformation under hydrostatic compression. Eventually, the unit cell volume of anatase expanded at ˜14-16 GPa. We propose that the anomalous compression behavior is attributed to the formation and thickening of the stiff high density amorphous shell under high pressure, giving rise to a great arching effect at the grain boundary at the nanolevel. This process results in a remarkable difference in stress between inside and outside of the shell, generating the illusions of the hardening and the negative compressibility. This study offers a new insight into the mechanical properties of nanomaterials under extreme conditions.

High speed X-ray phase contrast imaging of energetic composites under dynamic compression

NASA Astrophysics Data System (ADS)

Parab, Niranjan D.; Roberts, Zane A.; Harr, Michael H.; Mares, Jesus O.; Casey, Alex D.; Gunduz, I. Emre; Hudspeth, Matthew; Claus, Benjamin; Sun, Tao; Fezzaa, Kamel; Son, Steven F.; Chen, Weinong W.

2016-09-01

Fracture of crystals and frictional heating are associated with the formation of "hot spots" (localized heating) in energetic composites such as polymer bonded explosives (PBXs). Traditional high speed optical imaging methods cannot be used to study the dynamic sub-surface deformation and the fracture behavior of such materials due to their opaque nature. In this study, high speed synchrotron X-ray experiments are conducted to visualize the in situ deformation and the fracture mechanisms in PBXs composed of octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) crystals and hydroxyl-terminated polybutadiene binder doped with iron (III) oxide. A modified Kolsky bar apparatus was used to apply controlled dynamic compression on the PBX specimens, and a high speed synchrotron X-ray phase contrast imaging (PCI) setup was used to record the in situ deformation and failure in the specimens. The experiments show that synchrotron X-ray PCI provides a sufficient contrast between the HMX crystals and the doped binder, even at ultrafast recording rates. Under dynamic compression, most of the cracking in the crystals was observed to be due to the tensile stress generated by the diametral compression applied from the contacts between the crystals. Tensile stress driven cracking was also observed for some of the crystals due to the transverse deformation of the binder and superior bonding between the crystal and the binder. The obtained results are vital to develop improved understanding and to validate the macroscopic and mesoscopic numerical models for energetic composites so that eventually hot spot formation can be predicted.

High speed X-ray phase contrast imaging of energetic composites under dynamic compression

DOE PAGES

Parab, Niranjan D.; Roberts, Zane A.; Harr, Michael H.; ...

2016-09-26

Fracture of crystals and subsequent frictional heating are associated with formation of hot spots in energetic composites such as polymer bonded explosives (PBXs). Traditional high speed optical imaging methods cannot be used to study the dynamic sub-surface deformation and fracture behavior of such materials due to their opaque nature. In this study, high speed synchrotron X-ray experiments are conducted to visualize the in situ deformation and fracture mechanisms in PBXs manufactured using octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) crystals and hydroxyl-terminated polybutadiene (HTPB) binder. A modified Kolsky bar apparatus was used to apply controlled dynamic compression on the PBX specimens, and a high speedmore » synchrotron X-ray phase contrast imaging (PCI) setup was used to record the in situ deformation and failure in the specimens. The experiments show that synchrotron X-ray PCI provides a sufficient contrast between the HMX crystals and the doped binder, even at ultrafast recording rates. Under dynamic compression, most of the cracking in the crystals was observed to be due to the tensile stress generated by the diametral compression applied from the contacts between the crystals. Tensile stress driven cracking was also observed for some of the crystals due to the transverse deformation of the binder and superior bonding between the crystal and the binder. In conclusion, the obtained results are vital to develop improved understanding and to validate the macroscopic and mesoscopic numerical models for energetic composites so that eventually hot spot formation can be predicted.« less

Compression induced phase transition of nematic brush: A mean-field theory study

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tang, Jiuzhou; Zhang, Xinghua, E-mail: zhangxh@bjtu.edu.cn; Yan, Dadong, E-mail: yandd@bnu.edu.cn

2015-11-28

Responsive behavior of polymer brush to the external compression is one of the most important characters for its application. For the flexible polymer brush, in the case of low grafting density, which is widely studied by the Gaussian chain model based theory, the compression leads to a uniform deformation of the chain. However, in the case of high grafting density, the brush becomes anisotropic and the nematic phase will be formed. The normal compression tends to destroy the nematic order, which leads to a complex responsive behaviors. Under weak compression, chains in the nematic brush are buckled, and the bendingmore » energy and Onsager interaction give rise to the elasticity. Under deep compression, the responsive behaviors of the nematic polymer brush depend on the chain rigidity. For the compressed rigid polymer brush, the chains incline to re-orientate randomly to maximize the orientational entropy and its nematic order is destroyed. For the compressed flexible polymer brush, the chains incline to fold back to keep the nematic order. A buckling-folding transition takes place during the compressing process. For the compressed semiflexible brush, the chains are collectively tilted to a certain direction, which leads to the breaking of the rotational symmetry in the lateral plane. These responsive behaviors of nematic brush relate to the properties of highly frustrated worm-like chain, which is hard to be studied by the traditional self-consistent field theory due to the difficulty to solve the modified diffusion equation. To overcome this difficulty, a single chain in mean-field theory incorporating Monte Carlo simulation and mean-field theory for the worm-like chain model is developed in present work. This method shows high performance for entire region of chain rigidity in the confined condition.« less

Orientation-dependent deformation mechanisms of bcc niobium nanoparticles

NASA Astrophysics Data System (ADS)

Bian, J. J.; Yang, L.; Niu, X. R.; Wang, G. F.

2018-07-01

Nanoparticles usually exhibit pronounced anisotropic properties, and a close insight into the atomic-scale deformation mechanisms is of great interest. In present study, atomic simulations are conducted to analyse the compression of bcc nanoparticles, and orientation-dependent features are addressed. It is revealed that surface morphology under indenter predominantly governs the initial elastic response. The loading curve follows the flat punch contact model in [1 1 0] compression, while it obeys the Hertzian contact model in [1 1 1] and [0 0 1] compressions. In plastic deformation regime, full dislocation gliding is dominated in [1 1 0] compression, while deformation twinning is prominent in [1 1 1] compression, and these two mechanisms coexist in [0 0 1] compression. Such deformation mechanisms are distinct from those in bulk crystals under nanoindentation and nanopillars under compression, and the major differences are also illuminated. Our results provide an atomic perspective on the mechanical behaviours of bcc nanoparticles and are helpful for the design of nanoparticle-based components and systems.

Microstructural Evolution and Constitutive Relationship of M350 Grade Maraging Steel During Hot Deformation

NASA Astrophysics Data System (ADS)

Chakravarthi, K. V. A.; Koundinya, N. T. B. N.; Narayana Murty, S. V. S.; Nageswara Rao, B.

2017-03-01

Maraging steels exhibit extraordinary strength coupled with toughness and are therefore materials of choice for critical structural applications in defense, aerospace and nuclear engineering. Thermo-mechanical processing is an important step in the manufacture of these structural components. This process assumes significance as these materials are expensive and the mechanical properties obtained depend on the microstructure evolved during thermo-mechanical processing. In the present study, M350 grade maraging steel specimens were hot isothermally compressed in the temperature range of 900-1200 °C and in the strain rate range of 0.001-100 s-1, and true stress-true strain curves were generated. The microstructural evolution as a function of strain rate and temperature in the deformed compression specimens was studied. The effect of friction between sample and compression dies was evaluated, and the same was found to be low. The measured flow stress data was used for the development of a constitutive model to represent the hot deformation behavior of this alloy. The proposed equation can be used as an input in the finite element analysis to obtain the flow stress at any given strain, strain rate, and temperature useful for predicting the flow localization or fracture during thermo-mechanical simulation. The activation energy for hot deformation was calculated and is found to be 370.88 kJ/mol, which is similar to that of M250 grade maraging steel.

Holographic study of non-affine deformation in copper foam with a negative Poisson's ratio of -0.8

NASA Technical Reports Server (NTRS)

Chen, C. P.; Lakes, R. S.

1993-01-01

While conventional foams have positive Poisson's ratios (become smaller in cross-section when stretched and larger when compressed), foam materials have recently been defined which possess 'reentrant' cellular architectures; in these, inwardly-protruding cell ribs are responsible for negative Poisson's ratio behavior, yielding greater resilience than conventional foams. Double-exposure holographic interferometry is presently used to examine the microdeformation of a reentrant copper foam. Attention is given to the nonaffine (inhomogeneous) deformation of this foam.

Anomalous behavior of curves of pseudo-elastic deformation of Ni-Fe-Ga-Co alloy crystals as a result of interphase stresses

NASA Astrophysics Data System (ADS)

Malygin, G. A.; Nikolaev, V. I.; Averkin, A. I.; Zograf, A. P.

2016-12-01

The compression diagram of Ni49Fe18Ga27Co6 alloy crystals in the [011] direction was studied until full shape memory strain at various temperatures in the range of 259-340 K. It is found that all load curves are anomalously shaped and contain portions of sharp and gradual decreases in deformation stresses. Simulation of pseudo-elastic stress-strain curves within the theory of diffuse martensitic transitions, describing not only equilibrium of phases, but also the kinetics of the transition between them, shows that elastic interphase stresses during martensitic reactions Ll 2 → 14 M and 14 M → Ll 0 characteristic of this alloy can be responsible for the extraordinary shape of compression diagrams.

Dissipative processes under the shock compression of glass

NASA Astrophysics Data System (ADS)

Savinykh, A. S.; Kanel, G. I.; Cherepanov, I. A.; Razorenov, S. V.

2016-03-01

New experimental data on the behavior of the K8 and TF1 glasses under shock-wave loading conditions are obtained. It is found that the propagation of shock waves is close to the self-similar one in the maximum compression stress range 4-12 GPa. Deviations from a general deformation diagram, which are related to viscous dissipation, take place when the final state of compression is approached. The parameter region in which failure waves form in glass is found not to be limited to the elastic compression stress range, as was thought earlier. The failure front velocity increases with the shock compression stress. Outside the region covered by a failure wave, the glasses demonstrate a high tensile dynamic strength (6-7 GPa) in the case of elastic compression, and this strength is still very high after transition through the elastic limit in a compression wave.

Fabrication, microstructure, properties and deformation mechanisms of a nanocrystalline aluminum-iron-chromium-titanium alloy by mechanical alloying

NASA Astrophysics Data System (ADS)

Luo, Hong

A multi-phase nanocrystalline Al93Fe3Cr2Ti 2 alloy containing 30 vol.% intermetallic particles was prepared via mechanical alloying starting from elemental powders, followed by hot extrusion. The grain size of 6-45 nm can be achieved after 30-hours of milling. Thermal stability of nanostructured Al93Fe3Ti2Cr 2 alloys was investigated using a variety of analytical techniques including modulated differential scanning calorimetry, X-ray diffraction, scanning electron microscopy, transmission electron microscopy. The MA-processed Al93Fe 3Ti2Cr2 alloy in the as-milled condition was composed of an Al-based supersaturated solid solution with high internal strains. Release of internal strains, intermetallic precipitation and grain growth occurred upon heating of the MA-processed Al alloy. Nevertheless, grain growth in the MA-processed Al alloy was very limited and fcc-Al grains with sizes in the range of 20 nm were still present in the alloys after exposure to 450°C (0.77 Tm). Systematic compressive tests and modulus measurements were performed as a function of temperature and strain rate to investigate the deformation behavior and mechanisms of the nc Al-Fe-Cr-Ti alloys. High strengths and moduli at both ambient and elevated temperatures have been demonstrated. The ductility of the nc Al93Fe3Cr2Ti2 alloy depends strongly on whether the oxide film at the prior powder particle boundary has been broken down or not. The MA-processed Al93Fe3Cr 2Ti2 alloy is brittle when the oxide film is continuous at PPB, and is ductile when the oxide film is broken down into discontinuous particles during extrusion. It is argued that the compressive strength at ambient temperature is controlled by propagation of dislocations into nc fcc-Al grains, whereas the compressive strength at elevated temperature is determined by dislocation propagation as well as dynamic recovery. Since the stress for dislocation propagation into nc fcc-Al grains increases with decreasing the grain size, the smaller the grain size, the higher the compressive strength. This new microstructural design approach could present opportunities for exploiting nc materials in structural applications at both ambient and elevated temperatures. The nanocrystalline Al-Fe-Cr-Ti alloy exhibited significant difference in deformation behavior between tension and compression at 25, 200 and 300°C. However, the strengths obtained in tension and compression were similar at 400°C. Systematic microstructure examinations and deformation mechanism analyses indicate that the asymmetry of this nc Al93Fe3Cr 2Ti2 alloy is related to its dislocation mediated plastic deformation mechanism, its nanoscale grain microstructure, and premature brittle failure in tension tests.

1000 to 1300 K slow plastic compression properties of Al-deficient NiAl

NASA Technical Reports Server (NTRS)

Whittenberger, J. D.; Kumar, K. S.; Mannan, S. K.

1991-01-01

Nickel aluminides containing 37, 38.5 and 40 at. pct Al have been fabricated by XD synthesis and hot pressing. Such materials were compression tested in air under constant velocity conditions between 1000 and 1300 K. Examination of the microstructures of hot pressed and compression tested aluminides indicated that the structure consisted of two phases, gamma-prime and NiAl, for essentially all conditions, where gamma-prime was usually found on the NiAl grain boundaries. The stress-strain behavior of all three intermetallics was similar where flow at a nominally constant stress occurred after about two-percent plastic deformation. Furthermore, the 1000 to 1300 K flow stress-strain rate properties are nearly identical for these materials, and they are much lower than those for XD processed Ni-50Al. The overall deformation of the two phase nickel aluminides appears to be controlled by dislocation climb in NiAl rather than processes in gamma-prime.

Deformation modeling and constitutive modeling for anisotropic superalloys

NASA Technical Reports Server (NTRS)

Milligan, Walter W.; Antolovich, Stephen D.

1989-01-01

A study of deformation mechanisms in the single crystal superalloy PWA 1480 was conducted. Monotonic and cyclic tests were conducted from 20 to 1093 C. Both (001) and near-(123) crystals were tested, at strain rates of 0.5 and 50 percent/minute. The deformation behavior could be grouped into two temperature regimes: low temperatures, below 760 C; and high temperatures, above 820 to 950 C depending on the strain rate. At low temperatures, the mechanical behavior was very anisotropic. An orientation dependent CRSS, a tension-compression asymmetry, and anisotropic strain hardening were all observed. The material was deformed by planar octahedral slip. The anisotropic properties were correlated with the ease of cube cross-slip, as well as the number of active slip systems. At high temperatures, the material was isotropic, and deformed by homogeneous gamma by-pass. It was found that the temperature dependence of the formation of superlattice-intrinsic stacking faults was responsible for the local minimum in the CRSS of this alloy at 400 C. It was proposed that the cube cross-slip process must be reversible. This was used to explain the reversible tension-compression asymmetry, and was used to study models of cross-slip. As a result, the cross-slip model proposed by Paidar, Pope and Vitek was found to be consistent with the proposed slip reversibility. The results were related to anisotropic viscoplastic constitutive models. The model proposed by Walter and Jordan was found to be capable of modeling all aspects of the material anisotropy. Temperature and strain rate boundaries for the model were proposed, and guidelines for numerical experiments were proposed.

Modeling Deformation Flow Curves and Dynamic Recrystallization of BA-160 Steel During Hot Compression

NASA Astrophysics Data System (ADS)

Shahriari, Babak; Vafaei, Reza; Mohammad Sharifi, Ehsan; Farmanesh, Khosro

2018-03-01

The hot deformation behavior of a high strength low carbon steel was investigated using hot compression test at the temperature range of 850-1100 °C and under strain rates varying from 0.001 to 1 s-1. It was found that the flow curves of the steel were typical of dynamic recrystallization at the temperature of 950 °C and above; at tested strain rates lower than 1 s-1. A very good correlation between the flow stress and Zener-Hollomon parameter was obtained using a hyperbolic sine function. The activation energy of deformation was found to be around 390 kJ mol-1. The kinetics of dynamic recrystallization of the steel was studied by comparing it with a hypothetical dynamic recovery curve, and the dynamically fraction recrystallized was modeled by the Kolmogorov-Johnson-Mehl-Avrami relation. The Avrami exponent was approximately constant around 1.8, which suggested that the type of nucleation was one of site saturation on grain boundaries and edges.

Ported jacket for use in deformation measurement apparatus

DOEpatents

Wagner, L.A.; Senseny, P.E.; Mellegard, K.D.; Olsberg, S.B.

1990-03-06

A device for allowing deformation measurement of a jacketed specimen when the specimen is loaded includes an elastomeric specimen container or jacket surrounding a specimen while the specimen is being loaded by a test apparatus. The specimen jacket wall is compressible, and the wall follows and allows deformation of the specimen. The jacket wall of compressible material is provided with at least one opening and a thin layer or shim of substantially non-compressible (metal) material which covers and seals this opening. An extensometer is then positioned with its specimen engaging contact members engaging the substantially non-compressible material to measure the deformation of the specimen when the specimen is loaded, without compressibility effects of the jacket. 9 figs.

N-Cadherin Maintains the Healthy Biology of Nucleus Pulposus Cells under High-Magnitude Compression.

PubMed

Wang, Zhenyu; Leng, Jiali; Zhao, Yuguang; Yu, Dehai; Xu, Feng; Song, Qingxu; Qu, Zhigang; Zhuang, Xinming; Liu, Yi

2017-01-01

Mechanical load can regulate disc nucleus pulposus (NP) biology in terms of cell viability, matrix homeostasis and cell phenotype. N-cadherin (N-CDH) is a molecular marker of NP cells. This study investigated the role of N-CDH in maintaining NP cell phenotype, NP matrix synthesis and NP cell viability under high-magnitude compression. Rat NP cells seeded on scaffolds were perfusion-cultured using a self-developed perfusion bioreactor for 5 days. NP cell biology in terms of cell apoptosis, matrix biosynthesis and cell phenotype was studied after the cells were subjected to different compressive magnitudes (low- and high-magnitudes: 2% and 20% compressive deformation, respectively). Non-loaded NP cells were used as controls. Lentivirus-mediated N-CDH overexpression was used to further investigate the role of N-CDH under high-magnitude compression. The 20% deformation compression condition significantly decreased N-CDH expression compared with the 2% deformation compression and control conditions. Meanwhile, 20% deformation compression increased the number of apoptotic NP cells, up-regulated the expression of Bax and cleaved-caspase-3 and down-regulated the expression of Bcl-2, matrix macromolecules (aggrecan and collagen II) and NP cell markers (glypican-3, CAXII and keratin-19) compared with 2% deformation compression. Additionally, N-CDH overexpression attenuated the effects of 20% deformation compression on NP cell biology in relation to the designated parameters. N-CDH helps to restore the cell viability, matrix biosynthesis and cellular phenotype of NP cells under high-magnitude compression. © 2017 The Author(s). Published by S. Karger AG, Basel.

Flow and fracture behavior of NiAl in relation to the brittle-to-ductile transition temperature

NASA Technical Reports Server (NTRS)

Noebe, R. D.; Bowman, R. R.; Cullers, C. L.; Raj, S. V.

1991-01-01

NiAl has only three independent slip systems operating at low and intermediate temperatures whereas five independent deformation mechanisms are required to satisfy the von Mises criterion for general plasticity in polycrystalline materials. Yet, it is generally recognized that polycrystalline NiAl can be deformed extensively in compression at room temperature and that limited tensile ductility can be obtained in extruded materials. In order to determine whether these results are in conflict with the von Mises criterion, tension and compression tests were conducted on powder-extruded, binary NiAl between 300 and 1300 K. The results indicate that below the brittle-to-ductile transition temperature (BDTT) the failure mechanism in NiAl involves the initiation and propagation of cracks at the grain boundaries which is consistent with the von Mises analysis. Furthermore, evaluation of the flow behavior of NiAl indicates that the transition from brittle to ductile behavior with increasing temperature coincides with the onset of recovery mechanisms such as dislocation climb. The increase in ductility above the BDTT is therefore attributed to the climb of the 001 line type dislocations which in combination with dislocation glide enable grain boundary compatibility to be maintained at the higher temperatures.

Microstructure and mechanical behavior of metallic glass fiber-reinforced Al alloy matrix composites

PubMed Central

Wang, Z.; Georgarakis, K.; Nakayama, K. S.; Li, Y.; Tsarkov, A. A.; Xie, G.; Dudina, D.; Louzguine-Luzgin, D. V.; Yavari, A. R.

2016-01-01

Metallic glass-reinforced metal matrix composites are an emerging class of composite materials. The metallic nature and the high mechanical strength of the reinforcing phase offers unique possibilities for improving the engineering performance of composites. Understanding the structure at the amorphous/crystalline interfaces and the deformation behavior of these composites is of vital importance for their further development and potential application. In the present work, Zr-based metallic glass fibers have been introduced in Al7075 alloy (Al-Zn-Mg-Cu) matrices using spark plasma sintering (SPS) producing composites with low porosity. The addition of metallic glass reinforcements in the Al-based matrix significantly improves the mechanical behavior of the composites in compression. High-resolution TEM observations at the interface reveal the formation of a thin interdiffusion layer able to provide good bonding between the reinforcing phase and the Al-based matrix. The deformation behavior of the composites was studied, indicating that local plastic deformation occurred in the matrix near the glassy reinforcements followed by the initiation and propagation of cracks mainly through the matrix. The reinforcing phase is seen to inhibit the plastic deformation and retard the crack propagation. The findings offer new insights into the mechanical behavior of metal matrix composites reinforced with metallic glasses. PMID:27067824

Investigation of Hot Deformation Behavior of Duplex Stainless Steel Grade 2507

NASA Astrophysics Data System (ADS)

Kingklang, Saranya; Uthaisangsuk, Vitoon

2017-01-01

Recently, duplex stainless steels (DSSs) are being increasingly employed in chemical, petro-chemical, nuclear, and energy industries due to the excellent combination of high strength and corrosion resistance. Better understanding of deformation behavior and microstructure evolution of the material under hot working process is significant for achieving desired mechanical properties. In this work, plastic flow curves and microstructure development of the DSS grade 2507 were investigated. Cylindrical specimens were subjected to hot compression tests for different elevated temperatures and strain rates by a deformation dilatometer. It was found that stress-strain responses of the examined steel strongly depended on the forming rate and temperature. The flow stresses increased with higher strain rates and lower temperatures. Subsequently, predictions of the obtained stress-strain curves were done according to the Zener-Hollomon equation. Determination of material parameters for the constitutive model was presented. It was shown that the calculated flow curves agreed well with the experimental results. Additionally, metallographic examinations of hot compressed samples were performed by optical microscope using color tint etching. Area based phase fractions of the existing phases were determined for each forming condition. Hardness of the specimens was measured and discussed with the resulted microstructures. The proposed flow stress model can be used to design and optimize manufacturing process at elevated temperatures for the DSS.

Simulation of Texture Evolution during Uniaxial Deformation of Commercially Pure Titanium

NASA Astrophysics Data System (ADS)

Bishoyi, B.; Debta, M. K.; Yadav, S. K.; Sabat, R. K.; Sahoo, S. K.

2018-03-01

The evolution of texture in commercially pure (CP) titanium during uniaxial tension and compression through VPSC (Visco-plastic self-consistent) simulation is reported in the present study. CP-titanium was subjected to both uniaxial tension and compression upto 35% deformation. During uniaxial tension, tensile twin of \\{10\\bar{1}2\\}\\unicode{x003C;}\\bar{1}011\\unicode{x003E;} type and compressive twin of \\{11\\bar{2}2\\}\\unicode{x003C;}11\\bar{2}\\bar{3}\\unicode{x003E;} type were observed in the samples. However, only tensile twin of \\{10\\bar{1}2\\}\\unicode{x003C;}\\bar{1}011\\unicode{x003E;} type and compressive twin of type was observed in the samples during uniaxial compression. Volume fractions of the twins were increased linearly as a function of percentage deformation during uniaxial tension. Whereas, during uniaxial compression the twinning volume fraction was increased up to 20% deformation and then decreased rapidly on further increasing the percentage deformation. During uniaxial tension, the general t-type textures were observed in the samples irrespective of the percentage deformation. The initial non-basal texture was oriented to split basal texture during uniaxial compression of the sample. VPSC formulation was used for simulating the texture development in the material. Different hardening parameters were estimated through correlating the simulated stress-strain curve with the experimental stress-strain data. It was observed that, prismatic slip \\{10\\bar{1}0\\}\\unicode{x003C;}11\\bar{2}0\\unicode{x003E;} operated as the primary deformation mode during uniaxial tension whereas basal slip \\{0001\\}\\unicode{x003C;}11\\bar{2}0\\unicode{x003E;} acquired the leading role during deformation through uniaxial compression. It was also revealed that active deformation modes were fully depending on percentage deformation, loading direction, and orientation of grains.

Elasticity of excised dog lung parenchyma

NASA Technical Reports Server (NTRS)

Vawter, D. L.; Fung, Y. C.; West, J. B.

1978-01-01

An optical-electromechanical system is used to measure the force-deformation behavior of biaxially loaded rectangular slabs of excised dog lung parenchyma. In the course of the study, the effects of time, the consistency of reference lengths and areas, the presence of hysteresis, the necessity of preconditioning, the repeatability of results, the effects of lateral load, the effect of strain rate, the effect of pH, the influence of temperature, and the variations among specimens are considered. A new finding is that there is a change in elastic behavior when the tissue undergoes a compressive strain. When the tissue is in tension, increasing the lateral load decreases the compliance, whereas the opposite is true when compressive strain is present.

A finite element-based machine learning approach for modeling the mechanical behavior of the breast tissues under compression in real-time.

PubMed

Martínez-Martínez, F; Rupérez-Moreno, M J; Martínez-Sober, M; Solves-Llorens, J A; Lorente, D; Serrano-López, A J; Martínez-Sanchis, S; Monserrat, C; Martín-Guerrero, J D

2017-11-01

This work presents a data-driven method to simulate, in real-time, the biomechanical behavior of the breast tissues in some image-guided interventions such as biopsies or radiotherapy dose delivery as well as to speed up multimodal registration algorithms. Ten real breasts were used for this work. Their deformation due to the displacement of two compression plates was simulated off-line using the finite element (FE) method. Three machine learning models were trained with the data from those simulations. Then, they were used to predict in real-time the deformation of the breast tissues during the compression. The models were a decision tree and two tree-based ensemble methods (extremely randomized trees and random forest). Two different experimental setups were designed to validate and study the performance of these models under different conditions. The mean 3D Euclidean distance between nodes predicted by the models and those extracted from the FE simulations was calculated to assess the performance of the models in the validation set. The experiments proved that extremely randomized trees performed better than the other two models. The mean error committed by the three models in the prediction of the nodal displacements was under 2 mm, a threshold usually set for clinical applications. The time needed for breast compression prediction is sufficiently short to allow its use in real-time (<0.2 s). Copyright © 2017 Elsevier Ltd. All rights reserved.

Influence of tools geometry and processing conditions on behavior of a difficult-to-work Al-Mg alloy during equal channel angular pressing

NASA Astrophysics Data System (ADS)

Comǎneci, Radu Ioachim; Nedelcu, Dumitru; Bujoreanu, Leandru Gheorghe

2017-10-01

Equal channel angular pressing (ECAP) is a well-established method for grain refinement in metallic materials by large shear plastic deformation, being the most promising and effective severe plastic deformation (SPD) technique. ECAP is a discontinuous process, so the billet removal implies a new development of the procedure: the new sample pushes out the previous sample. In resuming the process the head and the tail ends of the work piece which becomes strongly distorted and receiving different amount of strain have to be removed. Due to the path difference in material flow between upper and lower region of the outlet channel, a non-uniform strain and stress distribution across the width of the workpiece leaving the plastic deformation zone (PDZ) is achieved. A successful ECAP requires surpassing two obstacles: the necessary load level which directly affects tools and a favorable stress distribution so the material withstanding the accumulated strain of repeated deformation. Under back pressure (BP), materials have shown to be able to withstand more passes. As soon as the billet passes the PDZ along the bisector plane of the two channels, the compressive mean stress changes to tensile (leading to crack initiation), while in the presence of BP, a negative (compressive) stress is applied during the process. In this paper a comparative tridimensional finite element analysis (FEA) is performed to evaluate the behavior of a difficult-to-work Al-Mg alloy depending on tools geometry and process parameters. The results in terms of load level and strain distribution show the influence of the punch geometry and BP on the material behavior.

Tensile and compressive creep behavior of extruded Mg–10Gd–3Y–0.5Zr (wt.%) alloy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, H.; The State Key Laboratory of Metal Matrix Composites, Shanghai Jiao Tong University, 800 Dongchuan Road, Shanghai 200240; Wang, Q.D., E-mail: wangqudong@sjtu.edu.cn

2015-01-15

The tensile and compressive creep behavior of an extruded Mg–10Gd–3Y–0.5Zr (wt.%) alloy was investigated at temperatures ranging from 200 °C to 300 °C and under stresses ranging from 30 MPa to 120 MPa. There existed an asymmetry in the tensile and compressive creep properties. The minimum creep rate of the alloy was slightly greater in tension than in compression. The measured values of the transient strain and initial creep rate in compression were greater than those in tension. The creep stress exponent was approximately 2.5 at low temperatures (T < 250 °C) and 3.4 at higher temperatures both in tensionmore » and in compression. The compression creep activation energy at low temperatures and high temperatures was 83.4 and 184.3 kJ/mol respectively, while one activation energy (184 kJ/mol) represented the tensile–creep behavior over the temperature range examined. Dislocation creep was suggested to be the main mechanism in tensile creep and in the high-temperature regime in compressive creep, while grain boundary sliding was suggested to dominate in the low-temperature regime in compressive creep. Precipitate free zones were observed near grain boundaries perpendicular to the loading direction in tension and parallel to the loading direction in compression. Electron backscattered diffraction analysis revealed that the texture changed slightly during creep. Non-basal slip was suggested to contribute to the deformation after basal slip was introduced. In the tensile–creep ruptured specimens, intergranular cracks were mainly observed at general high-angle boundaries. - Highlights: • Creep behavior of an extruded Mg–RE alloy was characterized by EBSD. • T5 aging treatment enhanced the tension–compression creep asymmetry. • The grains grew slightly during tensile creep, but not for compressive creep. • Precipitate free zones (PFZs) were observed at specific grain boundaries. • Intergranular fracture was dominant and cracks mainly originated at GHABs.« less

Viscoelastic behavior of basaltic ash from Stromboli volcano inferred from intermittent compression experiments

NASA Astrophysics Data System (ADS)

Kurokawa, A. K.; Miwa, T.; Okumura, S.; Uesugi, K.

2017-12-01

After ash-dominated Strombolian eruption, considerable amount of ash falls back to the volcanic conduit forming a dense near-surface region compacted by weights of its own and other fallback clasts (Patrick et al., 2007). Gas accumulation below this dense cap causes a substantial increase in pressure within the conduit, causing the volcanic activity to shift to the preliminary stages of a forthcoming eruption (Del Bello et al., 2015). Under such conditions, rheology of the fallback ash plays an important role because it controls whether the fallback ash can be the cap. However, little attention has been given to the point. We examined the rheology of ash collected at Stromboli volcano via intermittent compression experiments changing temperature and compression time/rate. The ash deformed at a constant rate during compression process, and then it was compressed without any deformation during rest process. The compression and rest processes repeated during each experiment to see rheological variations with progression of compaction. Viscoelastic changes during the experiment were estimated by Maxwell model. The results show that both elasticity and viscosity increases with decreasing porosity. On the other hand, the elasticity shows strong rate-dependence in the both compression and rest processes while the viscosity dominantly depends on the temperature, although the compression rate also affects the viscosity in the case of the compression process. Thus, the ash behaves either elastically or viscously depending on experimental process, temperature, and compression rate/time. The viscoelastic characteristics can be explained by magnitude relationships between the characteristic relaxation times and times for compression and rest processes. This indicates that the balance of the time scales is key to determining the rheological characteristics and whether the ash behaves elastically or viscously may control cyclic Strombolian eruptions.

Elastic and Plastic Behavior of an Ultrafine-Grained Mg Reinforced with BN Nanoparticles

NASA Astrophysics Data System (ADS)

Trojanová, Zuzanka; Dash, Khushbu; Máthis, Kristián; Lukáč, Pavel; Kasakewitsch, Alla

2018-04-01

Pure microcrystalline magnesium (µMg) was reinforced with hexagonal boron nitride (hBN) nanoparticles and was fabricated by powder metallurgy process followed by hot extrusion. For comparison pure magnesium powder was consolidated by hot extrusion too. Both materials exhibited a significant fiber texture. Mg-hBN nanocomposites (nc) and pure Mg specimens were deformed between room temperature and 300 °C under tension and compression mode. The yield strength and ultimate tensile and compression strength as well as characteristic stresses were evaluated and reported. The tensile and compressive strengths of Mg-hBN nc are quiet superior in values compared to monolithic counterpart as well as Mg alloys. The compressive yield strength of µMg was recorded as 90 MPa, whereas the Mg-hBN nancomposite shows 125 MPa at 200 °C. The tensile yield strength of µMg was computed as 67 MPa which is quite lower as compared to Mg-hBN nanocomposite's value which was recorded as 157 MPa at 200 °C. Under tensile stress the true stress-strain curves are flat in nature, whereas the stress-strain curves observed in compression at temperatures up to 100 °C exhibited small local maxima at the onset of deformation followed by a significant work hardening.

Research on the hot deformation behavior of a Fe-Ni-Cr alloy (800H) at temperatures above 1000 °C

NASA Astrophysics Data System (ADS)

Cao, Yu; Di, Hongshuang

2015-10-01

Considering the pinning effect of fine carbides on grain boundaries, hot compression tests were performed above the dissolution temperature of Cr23C6 to investigate the hot deformation behavior of a Fe-Ni-Cr alloy (800H). The results show that the single peak stress associated with dynamic recrystalization (DRX) became more distinct at higher temperature and lower strain rate. The process of DRX was thoroughly stimulated when deformed above 1000 °C. Constitutive equations for hot deformation were established by regression analysis of conventional hyperbolic sine equation. The relationships between Zener-Hollomon parameter (Z) and the characteristic points of flow curves were established using the power law relation. Furthermore, kernel average misorientation (KAM) and grain orientation spread (GOS) were used to map the distribution of local misorientation and estimate the fraction of DRX, respectively. The critical strain and peak strain were used to predict the kinetics of DRX with the Avrami-type equation.

Equilibrium stability of a cylindrical body subject to the internal structure of the material and inelastic behaviour of the completely compressed matrix

NASA Astrophysics Data System (ADS)

Gotsev, D. V.; Perunov, N. S.; Sviridova, E. N.

2018-03-01

The mathematical model describing the stress-strain state of a cylindrical body under the uniform radial compression effect is constructed. The model of the material is the porous medium model. The compressed skeleton of the porous medium possesses hardening elastic-plastic properties. Deforming of the porous medium under the specified compressive loads is divided into two stages: elastic deforming of the porous medium and further elastic-plastic deforming of the material with completely compressed matrix. The analytical relations that define the fields of stress and displacement at each stage of the deforming are obtained. The influence of the porosity and other physical, mechanical and geometric parameters of the construction on the size of the plastic zone is evaluated. The question of the ground state equilibrium instability is investigated within the framework of the three-dimensional linearized relationships of the stability theory of deformed bodies.

High- and Low-Temperature Deformation Behavior of Different Orientation Hot-Rolled Annealed Zircaloy-4

NASA Astrophysics Data System (ADS)

Zong, Yingying; Gen, Qingfeng; Jiang, Hongwei; Shan, Debin; Guo, Bin

2018-03-01

In this paper, the hot-rolled annealed Zircaloy-4 samples with different orientation were subjected to uniaxial compression with a strain rate of 0.001 s-1 to obtain the stress-strain curves of different initial orientation samples at different temperatures. Electron backscatter diffraction (EBSD) technique and transmission electron microscope (TEM) technique were used to analyze the microstructures and textures of compressed samples. The mechanical properties and microstructural evolution of rolling directions (RD), transverse directions (TD) and normal directions (ND) were investigated under the conditions of - 150 °C low temperature, room temperature and 200 °C high temperature (simulated lunar temperature environment). The results show that the strength of Zircaloy-4 decreases with the increase in deformation temperature, and the strength in three orientations is ND > TD > RD. The deformation mechanism of hot-rolled annealed Zircaloy-4 with different orientation is different. In RD, { 10\\bar{1}0} < {a} > prismatic slip has the highest Schmid factor (SF), so it is most easy to activate the slip, followed by TD orientation, and ND orientation is the most difficult to activate. The deformed grains abide slip→twinning→slip rule, and the different orientation Zircaloy-4 deformation mechanisms mainly are the twinning coordinated with the slip.

Micropillar Compression Technique Applied to Micron-Scale Mudstone Elasto-Plastic Deformation

NASA Astrophysics Data System (ADS)

Dewers, T. A.; Boyce, B.; Buchheit, T.; Heath, J. E.; Chidsey, T.; Michael, J.

2010-12-01

Mudstone mechanical testing is often limited by poor core recovery and sample size, preservation and preparation issues, which can lead to sampling bias, damage, and time-dependent effects. A micropillar compression technique, originally developed by Uchic et al. 2004, here is applied to elasto-plastic deformation of small volumes of mudstone, in the range of cubic microns. This study examines behavior of the Gothic shale, the basal unit of the Ismay zone of the Pennsylvanian Paradox Formation and potential shale gas play in southeastern Utah, USA. Precision manufacture of micropillars 5 microns in diameter and 10 microns in length are prepared using an ion-milling method. Characterization of samples is carried out using: dual focused ion - scanning electron beam imaging of nano-scaled pores and distribution of matrix clay and quartz, as well as pore-filling organics; laser scanning confocal (LSCM) 3D imaging of natural fractures; and gas permeability, among other techniques. Compression testing of micropillars under load control is performed using two different nanoindenter techniques. Deformation of 0.5 cm in diameter by 1 cm in length cores is carried out and visualized by a microscope loading stage and laser scanning confocal microscopy. Axisymmetric multistage compression testing and multi-stress path testing is carried out using 2.54 cm plugs. Discussion of results addresses size of representative elementary volumes applicable to continuum-scale mudstone deformation, anisotropy, and size-scale plasticity effects. Other issues include fabrication-induced damage, alignment, and influence of substrate. This work is funded by the US Department of Energy, Office of Basic Energy Sciences. Sandia is a multiprogram laboratory operated by Sandia Corporation, a Lockheed Martin Company, for the United States Department of Energy’s National Nuclear Security Administration under contract DE-AC04-94AL85000.

Mechanism for amorphization of boron carbide under complex stress conditions

NASA Astrophysics Data System (ADS)

Li, Jun; Xu, Shuang; Liu, Lisheng; Wang, Zhen; Zhang, Jinyong; Liu, Qiwen

2018-05-01

As an excellent material, the application of boron carbide (B4C) is limited by pressure-induced amorphization. To understand the mechanism for amorphization in B4C, first-principles methods based on density functional theory were employed to investigate the mechanical behaviors and the deformation process in B4C under complex stress conditions with six different biaxial perpendicular compression directions. The angle (θ) between one of the loading directions and the [0 0 0 1] c-axis ranged from 0° to 75° with every 15° interval. We found that the maximum stress at θ = 30° is 124.5 GPa, which is the lowest among six biaxial compressions. Simulation results show that the mechanism for amorphization in B4C under complex stress conditions is complicated. We take the θ = 30° biaxial compression as an example to explain the complicated deformation process. In the elastic deformation region, sudden bending of three-atom chains occurs and results in a stress fluctuation. Then the formation of new B–B bonds between the three-atom chains and the icosahedra leads to the first stress drop. After that, the B–C bonds in the chains are broken, resulting in the second stress drop. In this process, the icosahedra are partially destroyed. The stress increases continuously and then drops at the critical failure strain. Finally, the fully destruction of icosahedra leads to amorphization in B4C. However, under other five biaxial compressions, the B–C bonds in three-atom chains are not fractured before structural failure. Understanding the deformation mechanism for amorphization of B4C in real applications is prime important for proposing how to resist amorphization and enhance the toughness of B4C.

High strain rate behavior of a SiC particulate reinforced Al{sub 2}O{sub 3} ceramic matrix composite

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hall, I.W.; Guden, M.

The high strain rate deformation behavior of composite materials is important for several reasons. First, knowledge of the mechanical properties of composites at high strain rates is needed for designing with these materials in applications where sudden changes in loading rates are likely to occur. Second, knowledge of both the dynamic and quasi-static mechanical responses can be used to establish the constitutive equations which are necessary to increase the confidence limits of these materials, particularly if they are to be used in critical structural applications. Moreover, dynamic studies and the knowledge gained form them are essential for the further developmentmore » of new material systems for impact applications. In this study, the high strain rate compressive deformation behavior of a ceramic matrix composite (CMC) consisting of SiC particles and an Al{sub 2}O{sub 3} matrix was studied and compared with its quasi-static behavior. Microscopic observations were conducted to investigate the deformation and fracture mechanism of the composite.« less

Modeling High Temperature Deformation Behavior of Large-Scaled Mg-Al-Zn Magnesium Alloy Fabricated by Semi-continuous Casting

NASA Astrophysics Data System (ADS)

Li, Jianping; Xia, Xiangsheng

2015-09-01

In order to improve the understanding of the hot deformation and dynamic recrystallization (DRX) behaviors of large-scaled AZ80 magnesium alloy fabricated by semi-continuous casting, compression tests were carried out in the temperature range from 250 to 400 °C and strain rate range from 0.001 to 0.1 s-1 on a Gleeble 1500 thermo-mechanical machine. The effects of the temperature and strain rate on the hot deformation behavior have been expressed by means of the conventional hyperbolic sine equation, and the influence of the strain has been incorporated in the equation by considering its effect on different material constants for large-scaled AZ80 magnesium alloy. In addition, the DRX behavior has been discussed. The result shows that the deformation temperature and strain rate exerted remarkable influences on the flow stress. The constitutive equation of large-scaled AZ80 magnesium alloy for hot deformation at steady-state stage (ɛ = 0.5) was The true stress-true strain curves predicted by the extracted model were in good agreement with the experimental results, thereby confirming the validity of the developed constitutive relation. The DRX kinetic model of large-scaled AZ80 magnesium alloy was established as X d = 1 - exp[-0.95((ɛ - ɛc)/ɛ*)2.4904]. The rate of DRX increases with increasing deformation temperature, and high temperature is beneficial for achieving complete DRX in the large-scaled AZ80 magnesium alloy.

Buckling Behavior of Compression-Loaded Composite Cylindrical Shells With Reinforced Cutouts

NASA Technical Reports Server (NTRS)

Hilburger, Mark W.; Sarnes, James H., Jr.

2004-01-01

Results from a numerical study of the response of thin-walled compression-loaded quasi-isotropic laminated composite cylindrical shells with unreinforced and reinforced square cutouts are presented. The effects of cutout reinforcement orthotropy, size, and thickness on the nonlinear response of the shells are described. A nonlinear analysis procedure has been used to predict the nonlinear response of the shells. The results indicate that a local buckling response occurs in the shell near the cutout when subjected to load and is caused by a nonlinear coupling between local shell-wall deformations and in-plane destabilizing compression stresses near the cutout. In general, reinforcement around a cutout in a compression-loaded shell is shown to retard or eliminate the local buckling response near the cutout and increase the buckling load of the shell. However, some results show that certain reinforcement configurations can cause an unexpected increase in the magnitude of local deformations and stresses in the shell and cause a reduction in the buckling load. Specific cases are presented that suggest that the orthotropy, thickness, and size of a cutout reinforcement in a shell can be tailored to achieve improved buckling response characteristics.

Anisotropic crystal deformation measurements determined using powder X-ray diffraction and a new in situ compression stage.

PubMed

Haware, Rahul V; Kim, Paul; Ruffino, Lauren; Nimi, Brian; Fadrowsky, Catherine; Doyle, Michael; Boerrigter, Stephan X M; Cuitino, Alberto; Morris, Ken

2011-10-14

This report addresses the development of experimental and computational estimations of the anisotropic elastic moduli (EM) of single crystals to aid in the a priori (i.e., starting with the crystal structure) prediction of the trend as a function of the direction of applied stress. Experimentally EM values in the normal direction to the X-, Y- and Z-planes of block shaped aspirin and acetaminophen crystals were determined using data generated by the newly designed compression stage housed in our powder X-ray diffractometer. Computational estimations of EM were made using the applicable modules in Material Studio 5.5. The measured EM values normal to the (100), (020) and (002) planes of aspirin, and (20-1), (020) and (001) planes of acetaminophen crystals by both methods succeeded in detected the anisotropic behavior. However, disparity in the relative values between measured EM values by different techniques was observed. This may be attributed to deformation sources other than lattice compression including inelastic processes such as local failure and plasticity as well as deformation at the crystal-probe interfaces due to crystal surface roughness (asperities). The trend of the ratio of the values from the respective methods showed reasonable agreement and promise for the technique. The present approach demonstrated the suitability of the compression stage to determine and predict anisotropic EM of subjected small molecular organic crystals. Copyright © 2011 Elsevier B.V. All rights reserved.

The Microstructural Evolution and Special Flow Behavior of Ti-5Al-2Sn-2Zr-4Mo-4Cr During Isothermal Compression at a Low Strain Rate

NASA Astrophysics Data System (ADS)

Sun, J. Z.; Li, M. Q.; Li, H.

2017-09-01

The microstructural evolution and special flow behavior of Ti-5Al-2Sn-2Zr-4Mo-4Cr during isothermal compression at a strain rate of 0.0001 s-1 were investigated. The dislocation climbs in elongated α grains resulted in the formation of low-angle boundaries that transform into high-angle boundaries with greater deformation, and the elongated α grains subsequently separated into homogenous globular α grains with the penetration of the β phase. The simultaneous occurrence of discontinuous dynamic recrystallization and continuous dynamic recrystallization in the primary β grains resulted in a trimode grain distribution. The β grains surrounded by dislocations presented an equilateral-hexagonal morphology, which suggests that grain boundary sliding through dislocation climbs was the main deformation mechanism. The true stress-strain curves for 1073 and 1113 K abnormally intersect at a strain of 0.35, related to the α → β phase transformation and distinct growth of the β grain size.

Effect of SiC Nanoparticles on Hot Deformation Behavior and Processing Maps of Magnesium Alloy AZ91

PubMed Central

Nie, Kaibo; Kang, Xinkai; Deng, Kunkun; Wang, Ting; Guo, Yachao; Wang, Hongxia

2018-01-01

The hot deformation behavior and processing characteristics of AZ91 alloy and nano-SiCp/AZ91 composite were compared at temperature ranges of 523 K–673 K and strain rates of 0.001–1 s−1. Positive impact of SiC nanoparticles on pinning grain boundaries and inhibiting grain growth was not obvious when deformation temperature was below 623 K, but was remarkable when the temperature was above 623 K. By comparing compressive stress-strain curves of AZ91 alloy and nano-SiCp/AZ91 composites, the addition of nanoparticles could improve the deformation ability of a matrix alloy under high-temperature conditions. There was no essential difference of deformation mechanism between AZ91 alloy and the composite, but hot deformation activation energy of the composite was significantly lower than that of the AZ91 alloy. The AZ91 alloy and the composite had the same workability region of 600 K–673 K and 0.001–1 s−1, while instability region for the composite was reduced compared with that of AZ91 alloy at high temperature. PMID:29389888

Comparison studies on the percolation thresholds of binary mixture tablets containing excipients of plastic/brittle and plastic/plastic deformation properties.

PubMed

Amin, Mohd C I; Fell, John T

2004-01-01

Percolation theory has been used with great interest in understanding the design and characterization of dosage forms. In this study, work has been carried out to investigate the behavior of binary mixture tablets containing excipients of similar and different deformation properties. The binary mixture tablets were prepared by direct compression using lactose, polyvinyl chloride (PVC), Eudragit RS 100, and microcrystalline cellulose (MCC). The application of percolation theory on the relationships between compactibility, Pmax, or compression susceptibility (compressibility), gamma, and mixture compositions reveals the presence of percolation thresholds even for mixtures of similar deformation properties. The results showed that all mixture compositions exhibited at least one discreet change in the slope, which was referred to as the percolation threshold. The PVC/Eudragit RS100 mixture compositions showed significant percolation threshold at 80% (w/w) PVC loading. Two percolation thresholds were observed from a series of binary mixtures containing similar plastic deformation materials (PVC/MCC). The percolation thresholds were determined at 20% (w/w) and 80% (w/w) PVC loading. These are areas where one of the components percolates throughout the system and the properties of the tablets are expected to experience a sudden change. Experimental results, however, showed that total disruption of the tablet physical properties at the specified percolation thresholds can be observed for PVC/lactose mixtures at 20-30% (w/w) loading while only minor changes in the tablets' strength for PVC/MCC or PVC/Eudragit RS 100 mixtures were observed.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Parab, Niranjan D.; Roberts, Zane A.; Harr, Michael H.

Fracture of crystals and subsequent frictional heating are associated with formation of hot spots in energetic composites such as polymer bonded explosives (PBXs). Traditional high speed optical imaging methods cannot be used to study the dynamic sub-surface deformation and fracture behavior of such materials due to their opaque nature. In this study, high speed synchrotron X-ray experiments are conducted to visualize the in situ deformation and fracture mechanisms in PBXs manufactured using octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) crystals and hydroxyl-terminated polybutadiene (HTPB) binder. A modified Kolsky bar apparatus was used to apply controlled dynamic compression on the PBX specimens, and a high speedmore » synchrotron X-ray phase contrast imaging (PCI) setup was used to record the in situ deformation and failure in the specimens. The experiments show that synchrotron X-ray PCI provides a sufficient contrast between the HMX crystals and the doped binder, even at ultrafast recording rates. Under dynamic compression, most of the cracking in the crystals was observed to be due to the tensile stress generated by the diametral compression applied from the contacts between the crystals. Tensile stress driven cracking was also observed for some of the crystals due to the transverse deformation of the binder and superior bonding between the crystal and the binder. In conclusion, the obtained results are vital to develop improved understanding and to validate the macroscopic and mesoscopic numerical models for energetic composites so that eventually hot spot formation can be predicted.« less

Pituitary stalk compression by the dorsum sellae: possible cause for late childhood onset growth disorders.

PubMed

Taoka, Toshiaki; Iwasaki, Satoru; Okamoto, Shingo; Sakamoto, Masahiko; Nakagawa, Hiroyuki; Otake, Shoichiro; Fujioka, Masayuki; Hirohashi, Shinji; Kichikawa, Kimihiko

2006-06-01

The purpose of this study was to evaluate the relationship between pituitary stalk compression by the dorsum sellae and clinical or laboratory findings in short stature children. We retrospectively reviewed magnetic resonance images of the pituitary gland and pituitary stalk for 34 short stature children with growth hormone (GH) deficiency and 24 age-matched control cases. We evaluated the degree of pituitary stalk compression caused by the dorsum sellae. Body height, GH level, pituitary height and onset age of the short stature were statistically compared between cases of pituitary stalk compression with associated stalk deformity and cases without compression. Compression of the pituitary stalk with associated stalk deformity was seen in nine cases within the short stature group. There were no cases observed in the control group. There were no significant differences found for body height, GH level and pituitary height between the cases of pituitary stalk compression with associated stalk deformity and cases without compression. However, a significant difference was seen in the onset age between cases with and without stalk compression. Pituitary stalk compression with stalk deformity caused by the dorsum sellae was significantly correlated with late childhood onset of short stature.

Effect of texture on rheological properties: the case of ɛ-Fe (Invited)

NASA Astrophysics Data System (ADS)

Merkel, S.; Gruson, M.; Tomé, C. N.; Nishiyama, N.; Wang, Y.

2009-12-01

Lattice preferred orientations (LPO) are known to affect the physical properties of materials. However, in most high pressure deformation experiments, LPO are ignored when interpreting the measured stress-strain curves. In addition, stress measurements in those experiments are complicated by the effect of plastic deformation on the measured lattice strains(1). Here, we present a new interpretation of the results obtained on hcp-iron at up to 19 GPa and 600 K in the deformation-DIA(2). In those experiments, five independent stress-strain curves were obtained on axial shortening with a ductile behavior of the sample for all. Stress were studied using results of monochromatic X-ray diffraction and the elastic theory of lattice strains(3). However, measured stresses were inconsistent with a change of behavior after 4% axial strain, particularly for strains measured on the 0002 line. We use elasto-plastic self consistent modeling(1) to show that this change of behavior is due to the evolution of LPO in the sample. With compression, 10-10 planes in hcp-iron align parallel to the compression direction and this affects the rheological behavior of the sample, which can not be summarized in a simple average law. We will also discuss the implication of those results for the extraction of polycrystalline rheological properties for materials with non-random lattice preferred orientations and how this could affect our understanding of the Earth deep interior. 1- S. Merkel, C.N. Tomé, H.-R Wenk, A modeling analysis of the influence of plasticity on high pressure deformation of hcp-Co, Phys. Rev. B, 79, 064110 (2009) 2- N. Nishiyama, Y. Wang, M. L. Rivers, S. R. Sutton, D. Cookson, Rheology of e-iron up to 19 GPa and 600 K in the D-DIA, Geophys. Res. Lett., 34, L23304 (2007) 3- A. K. Singh, C. Balasingh, H. K. Mao, R. J. Hemley, J. Shu, Analysis of lattice strains measured under non-hydrostatic pressure, J. Appl. Phys., 83, 7567-7575 (1998)

Modelling the viscoplastic behavior and the heterogeneous intracrystalline deformation of columnar ice polycrystals

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lebensohn, Ricardo A; Montagnat, Maurine; Mansuy, Philippe

2008-01-01

A full-field formulation based on Fast Fourier Transforms (FFT) has been adapted and used to predict the micromechanical fields that develop in columnar Ih ice polycrystals deforming in compression by dislocation creep. The predicted intragranular mechanical fields are in qualitative good agreement with experimental observations, in particular those involving the formation of shear and kink bands. These localization bands are associated with the large internal stresses that develop during creep in such anisotropic material, and their location, intensity, morphology and extension are found to depend strongly on the crystallographic orientation of the grains and on their interaction with neighbor crystals.more » The predictions of the model are also discussed in relation with the deformation of columnar sea and lake ice, and with the mechanical behavior of granular ice of glaciers and polar ice sheets, as well.« less

Strength Differential Measured in Inconel 718: Effects of Hydrostatic Pressure Studied

NASA Technical Reports Server (NTRS)

Lewandowski, John J.; Wesseling, Paul; Prabhu, Nishad S.; Larose, Joel; Lissenden, Cliff J.; Lerch, Bradley A.

2003-01-01

Aeropropulsion components, such as disks, blades, and shafts, are commonly subjected to multiaxial stress states at elevated temperatures. Experimental results from loadings as complex as those experienced in service are needed to help guide the development of accurate viscoplastic, multiaxial deformation models that can be used to improve the design of these components. During a recent study on multiaxial deformation (ref. 1) on a common aerospace material, Inconel 718, it was shown that the material in the aged state exhibits a strength differential effect (SDE), whereby the uniaxial compressive yield and subsequent flow behavior are significantly higher than those in uniaxial tension. Thus, this material cannot be described by a standard von Mises yield formulation. There have been other formulations postulated (ref. 2) that involve other combinations of the stress invariants, including the effect of hydrostatic stress. The question remained as to which invariants are necessary in the flow model. To capture the physical mechanisms occurring during deformation and reflect them in the plasticity formulation, researchers examined the flow of Inconel 718 under various amounts of hydrostatic stress to determine whether or not hydrostatic stress is needed in the formulation. Under NASA Grant NCC3-464, monitored by the NASA Glenn Research Center, a series of tensile tests were conducted at Case Western Reserve University on aged (precipitation hardened) Inconel 718 at 650 C and with superimposed hydrostatic pressure. Dogbone shaped tensile specimens (3-mm-diameter gauge by 16-mm gauge length) and cylindrical compression specimens (3-mm-diameter gauge by 6-mm gauge length) were strain gauged and loaded in a high-pressure testing apparatus. Hydrostatic pressures were obtained with argon and ranged from 210 to 630 MPa. The aged Inconel 718 showed a pronounced difference in the tension and compression yield strength (i.e., an SDE), as previously observed. Also, there were no significant effects of hydrostatic pressure on either the tensile and compressive yield strength (see the graph) or on the magnitude of the SDE. This behavior is not consistent with the pressure-dependent theory of the SDE, which postulates that the SDE is associated with pressure-dependent and/or internal friction dependent deformation associated with non-Schmid effects at the crystal level (refs. 3 and 4). Flow in Inconel 718 appears to be independent of hydrostatic pressure, suggesting that this invariant may be removed from the phenomenological constitutive model. As part of an ongoing effort to develop advanced constitutive models, Glenn s Life Prediction Branch coordinated this work with that of research on the multiaxial deformation behavior of Inconel 718 being conducted at Pennsylvania State University under NASA Grant NCC597.

Influence of the Starting Microstructure on the Hot Deformation Behavior of a Low Stacking Fault Energy Ni-based Superalloy

NASA Astrophysics Data System (ADS)

McCarley, Joshua; Alabbad, B.; Tin, S.

2018-03-01

The influence of varying fractions of primary gamma prime precipitates on the hot deformation and annealing behavior of an experimental Nickel-based superalloy containing 24 wt pct. Co was investigated. Billets heat treated at 1110 °C or 1135 °C were subjected to hot compression tests at temperatures ranging from 1020 °C to 1060 °C and strain rates ranging from 0.001 to 0.1/s. The microstructures were characterized using electron back scatter diffraction in the as-deformed condition as well as following a super-solvus anneal heat treatment at 1140 °C for 1 hour. This investigation sought to quantify and understand what effect the volume fraction of primary gamma prime precipitates has on the dynamic recrystallization behavior and resulting length fraction ∑3 twin boundaries in the low stacking fault superalloy following annealing. Although deformation at the lower temperatures and higher strain rates led to dynamic recrystallization for both starting microstructures, comparatively lower recrystallized fractions were observed in the 1135 °C billet microstructures deformed at strain rates of 0.1/s and 0.05/s. Subsequent annealing of the 1135 °C billet microstructures led to a higher proportion of annealing twins when compared to the annealed 1110 °C billet microstructures.

Modeling the Effects of Cu Content and Deformation Variables on the High-Temperature Flow Behavior of Dilute Al-Fe-Si Alloys Using an Artificial Neural Network.

PubMed

Shakiba, Mohammad; Parson, Nick; Chen, X-Grant

2016-06-30

The hot deformation behavior of Al-0.12Fe-0.1Si alloys with varied amounts of Cu (0.002-0.31 wt %) was investigated by uniaxial compression tests conducted at different temperatures (400 °C-550 °C) and strain rates (0.01-10 s -1 ). The results demonstrated that flow stress decreased with increasing deformation temperature and decreasing strain rate, while flow stress increased with increasing Cu content for all deformation conditions studied due to the solute drag effect. Based on the experimental data, an artificial neural network (ANN) model was developed to study the relationship between chemical composition, deformation variables and high-temperature flow behavior. A three-layer feed-forward back-propagation artificial neural network with 20 neurons in a hidden layer was established in this study. The input parameters were Cu content, temperature, strain rate and strain, while the flow stress was the output. The performance of the proposed model was evaluated using the K-fold cross-validation method. The results showed excellent generalization capability of the developed model. Sensitivity analysis indicated that the strain rate is the most important parameter, while the Cu content exhibited a modest but significant influence on the flow stress.

Modeling the Effects of Cu Content and Deformation Variables on the High-Temperature Flow Behavior of Dilute Al-Fe-Si Alloys Using an Artificial Neural Network

PubMed Central

Shakiba, Mohammad; Parson, Nick; Chen, X.-Grant

2016-01-01

The hot deformation behavior of Al-0.12Fe-0.1Si alloys with varied amounts of Cu (0.002–0.31 wt %) was investigated by uniaxial compression tests conducted at different temperatures (400 °C–550 °C) and strain rates (0.01–10 s−1). The results demonstrated that flow stress decreased with increasing deformation temperature and decreasing strain rate, while flow stress increased with increasing Cu content for all deformation conditions studied due to the solute drag effect. Based on the experimental data, an artificial neural network (ANN) model was developed to study the relationship between chemical composition, deformation variables and high-temperature flow behavior. A three-layer feed-forward back-propagation artificial neural network with 20 neurons in a hidden layer was established in this study. The input parameters were Cu content, temperature, strain rate and strain, while the flow stress was the output. The performance of the proposed model was evaluated using the K-fold cross-validation method. The results showed excellent generalization capability of the developed model. Sensitivity analysis indicated that the strain rate is the most important parameter, while the Cu content exhibited a modest but significant influence on the flow stress. PMID:28773658

FEM simulation of the die compaction of pharmaceutical products: influence of visco-elastic phenomena and comparison with experiments.

PubMed

Diarra, Harona; Mazel, Vincent; Busignies, Virginie; Tchoreloff, Pierre

2013-09-10

This work studies the influence of visco-elastic behavior in the finite element method (FEM) modeling of die compaction of pharmaceutical products and how such a visco-elastic behavior may improve the agreement between experimental and simulated compression curves. The modeling of the process was conducted on a pharmaceutical excipient, microcrystalline cellulose (MCC), by using Drucker-Prager cap model coupled with creep behavior in Abaqus(®) software. The experimental data were obtained on a compaction simulator (STYLCAM 200R). The elastic deformation of the press was determined by performing experimental tests on a calibration disk and was introduced in the simulation. Numerical optimization was performed to characterize creep parameters. The use of creep behavior in the simulations clearly improved the agreement between the numerical and experimental compression curves (stresses, thickness), mainly during the unloading part of the compaction cycle. For the first time, it was possible to reproduce numerically the fact that the minimum tablet thickness is not obtained at the maximum compression stress. This study proves that creep behavior must be taken into account when modeling the compaction of pharmaceutical products using FEM methods. Copyright © 2013 Elsevier B.V. All rights reserved.

In situ synchrotron high-energy X-ray diffraction study of microscopic deformation behavior of a hard-soft dual phase composite containing phase transforming matrix

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhang, Junsong; Hao, Shijie; Jiang, Daqiang

This study explored a novel intermetallic composite design concept based on the principle of lattice strain matching enabled by the collective atomic load transfer. It investigated the hard-soft microscopic deformation behavior of a Ti3Sn/TiNi eutectic hard-soft dual phase composite by means of in situ synchrotron high-energy X-ray diffraction (HE-XRD) during compression. The composite provides a unique micromechanical system with distinctive deformation behaviors and mechanisms from the two components, with the soft TiNi matrix deforming in full compliance via martensite variant reorientation and the hard Ti3Sn lamellae deforming predominantly by rigid body rotation, producing a crystallographic texture for the TiNi matrixmore » and a preferred alignment for the Ti3Sn lamellae. HE-XRD reveals continued martensite variant reorientation during plastic deformation well beyond the stress plateau of TiNi. The hard and brittle Ti3Sn is also found to produce an exceptionally large elastic strain of 1.95% in the composite. This is attributed to the effect of lattice strain matching between the transformation lattice distortion of the TiNi matrix and the elastic strain of Ti3Sn lamellae. With such unique micromechanic characteristics, the composite exhibits high strength and large ductility.« less

Hot Ductility and Compression Deformation Behavior of TRIP980 at Elevated Temperatures

NASA Astrophysics Data System (ADS)

Zhang, Mei; Li, Haiyang; Gan, Bin; Zhao, Xue; Yao, Yi; Wang, Li

2018-02-01

The hot ductility tests of a kind of 980 MPa class Fe-0.31C (wt pct) TRIP steel (TRIP980) with the addition of Ti/V/Nb were conducted on a Gleeble-3500 thermomechanical simulator in the temperatures ranging from 873 K to 1573 K (600 °C to 1300 °C) at a constant strain rate of 0.001 s-1. It is found that the hot ductility trough ranges from 873 K to 1123 K (600 °C to 850 °C). The recommended straightening temperatures are from 1173 K to 1523 K (900 °C to 1250 °C). The isothermal hot compression deformation behavior was also studied by means of Gleeble-3500 in the temperatures ranging from 1173 K to 1373 K (900 °C to 1100 °C) at strain rates ranging from 0.01 s-1 to 10 s-1. The results show that the peak stress decreases with the increasing temperature and the decreasing strain rate. The deformation activation energy of the test steel is 436.7 kJ/mol. The hot deformation equation of the steel has been established, and the processing maps have been developed on the basis of experimental data and the principle of dynamic materials model (DMM). By analyzing the processing maps of strains of 0.5, 0.7, and 0.9, it is found that dynamic recrystallization occurs in the peak power dissipation efficiency domain, which is the optimal area of hot working. Finally, the factors influencing hot ductility and thermal activation energy of the test steel were investigated by means of microscopic analysis. It indicates that the additional microalloying elements play important roles both in the loss of hot ductility and in the enormous increase of deformation activation energy for the TRIP980 steel.

Volume and tissue composition preserving deformation of breast CT images to simulate breast compression in mammographic imaging

NASA Astrophysics Data System (ADS)

Han, Tao; Chen, Lingyun; Lai, Chao-Jen; Liu, Xinming; Shen, Youtao; Zhong, Yuncheng; Ge, Shuaiping; Yi, Ying; Wang, Tianpeng; Shaw, Chris C.

2009-02-01

Images of mastectomy breast specimens have been acquired with a bench top experimental Cone beam CT (CBCT) system. The resulting images have been segmented to model an uncompressed breast for simulation of various CBCT techniques. To further simulate conventional or tomosynthesis mammographic imaging for comparison with the CBCT technique, a deformation technique was developed to convert the CT data for an uncompressed breast to a compressed breast without altering the breast volume or regional breast density. With this technique, 3D breast deformation is separated into two 2D deformations in coronal and axial views. To preserve the total breast volume and regional tissue composition, each 2D deformation step was achieved by altering the square pixels into rectangular ones with the pixel areas unchanged and resampling with the original square pixels using bilinear interpolation. The compression was modeled by first stretching the breast in the superior-inferior direction in the coronal view. The image data were first deformed by distorting the voxels with a uniform distortion ratio. These deformed data were then deformed again using distortion ratios varying with the breast thickness and re-sampled. The deformation procedures were applied in the axial view to stretch the breast in the chest wall to nipple direction while shrinking it in the mediolateral to lateral direction re-sampled and converted into data for uniform cubic voxels. Threshold segmentation was applied to the final deformed image data to obtain the 3D compressed breast model. Our results show that the original segmented CBCT image data were successfully converted into those for a compressed breast with the same volume and regional density preserved. Using this compressed breast model, conventional and tomosynthesis mammograms were simulated for comparison with CBCT.

Dynamic Fracture Behavior of Plastic-Bonded Explosives

NASA Astrophysics Data System (ADS)

Fu, Hua; Li, Jun-Ling; Tan, Duo-Wang; Ifp, Caep Team

2011-06-01

Plastic-Bonded Explosives (PBX) are used as important energetic materials in nuclear or conventional weapons. Arms Warhead in the service process and the ballistic phase, may experience complex process such as long pulse and higher loading, compresson, tension and reciprocating compression - tension, friction with the projectile shell, which would lead to explosive deformation and fracture.And the dynamic deformation and fracture behavior of PBX subsequently affect reaction characteristics and initiation mechanism in explosives, then having influence on explosives safety. The dynamic fracure behavior of PBX are generally complex and not well studied or understood. In this paper, the dynamic fracture of explosives are conducted using a Kolsky bar. The Brazilian test, also known as a indirect tensile test or splitting test, is chosen as the test method. Tensile strength under different strain rates are obtained using quartz crystal embedded in rod end. The dynamic deformation and fracture process are captured in real-time by high-speed digital camera, and the displacement and strain fields distribution before specimen fracture are obtained by digital correlation method. Considering the non-uniform microstructure of explosives,the dynamic fracture behavior of explosive are simulated by discrete element method, the simulation results can reproduce the deformation and fracture process in Brazilian test using a maximum tensile strain criterion.

Nondestructive evaluation of loading and fatigue effects in Haynes(R) 230(R) alloy

NASA Astrophysics Data System (ADS)

Saleh, Tarik Adel

Nondestructive evaluation is a useful method for studying the effects of deformation and fatigue. In this dissertation I employed neutron and X-ray diffraction, nonlinear resonant ultrasound spectroscopy (NRUS), and infrared thermography to study the effects of deformation and fatigue on two different nickel based superalloys. The alloys studied were HAYNES 230, a solid solution strengthened alloy with 4% M6C carbides, and secondarily HASTELLOY C-2000 a similar single phase alloy. Using neutron and X-ray diffraction, the deformation behavior of HAYNES 230 was revealed to be composite-like during compression, but unusual in tension, where the carbides provide strengthening until just after the macroscopic yield strength and then they begin to debond and crack, creating a tension-compression asymmetry that is revealed clearly by in situ diffraction. In fatigue of HAYNES 230, the hkl elastic strains changed very little in tension-tension fatigue. However, in situ tension-compression studies showed large changes over the initial stages of fatigue. The HAYNES 230 samples studies had two distinct starting textures, measured by neutron diffraction. Some samples were texture free initially and deformed in tension and compression to fiber textures. Other samples started with a bimodal texture due to cross-rolling and incomplete annealing. The final texture of these bimodal samples is shown through modeling to be a superposition of the initial texture and typical FCC deformation mechanisms. The texture-free samples deformed significantly more macroscopically and in internal elastic strains than the samples with the cross-rolled texture. In contrast to the relative insensitivity of neutron diffraction to the effects of tension-tension fatigue, NRUS revealed large differences between as-received and progressively fatigued samples. This showed that microcracking and void formation are the primary mechanisms responsible for fatigue damage in tension-tension fatigue. NRUS is shown to be a useful complimentary technique to neutron diffraction to evaluate fatigue damage. Finally, infrared thermography is used to show temperature changes over the course of fatigue in HASTELLOY C-2000. Four stages of temperature are shown over the course of a single fatigue test. Both empirical and theoretical relationships between steady state temperature and fatigue life are developed and presented.

In Situ Neutron Diffraction Analyzing Stress-Induced Phase Transformation and Martensite Elasticity in [001]-Oriented Co49Ni21Ga30 Shape Memory Alloy Single Crystals

NASA Astrophysics Data System (ADS)

Reul, A.; Lauhoff, C.; Krooß, P.; Gutmann, M. J.; Kadletz, P. M.; Chumlyakov, Y. I.; Niendorf, T.; Schmahl, W. W.

2018-02-01

Recent studies demonstrated excellent pseudoelastic behavior and cyclic stability under compressive loads in [001]-oriented Co-Ni-Ga high-temperature shape memory alloys (HT-SMAs). A narrow stress hysteresis was related to suppression of detwinning at RT and low defect formation during phase transformation due to the absence of a favorable slip system. Eventually, this behavior makes Co-Ni-Ga HT-SMAs promising candidates for several industrial applications. However, deformation behavior of Co-Ni-Ga has only been studied in the range of theoretical transformation strain in depth so far. Thus, the current study focuses not only on the activity of elementary deformation mechanisms in the pseudoelastic regime up to maximum theoretical transformation strains but far beyond. It is shown that the martensite phase is able to withstand about 5% elastic strain, which significantly increases the overall deformation capability of this alloy system. In situ neutron diffraction experiments were carried out using a newly installed testing setup on Co-Ni-Ga single crystals in order to reveal the nature of the stress-strain response seen in the deformation curves up to 10% macroscopic strain.

Mechanical Properties of Mg-Gd and Mg-Y Solid Solutions

NASA Astrophysics Data System (ADS)

Kula, Anna; Jia, Xiaohui; Mishra, Raj K.; Niewczas, Marek

2016-12-01

The mechanical properties of Mg-Gd and Mg-Y solid solutions have been studied under uniaxial tension and compression between 4 K and 298 K (-269 °C and 25 °C). The results reveal that Mg-Gd alloys exhibit higher strength and ductility under tension and compression attributed to the more effective solid solution strengthening and grain-boundary strengthening effects. Profuse twinning has been observed under compression, resulting in a material texture with strong dominance of basal component parallel to compression axis. Under tension, twining is less active and the texture evolution is controlled mostly by slip. The alloys exhibit pronounced yield stress asymmetry and significantly different work-hardening behavior under tension and compression. Increasing of Gd and/or Y concentration leads to the reduction of the tension-compression asymmetry due to the weakening of the recrystallization texture and more balanced twinning and slip activity during plastic deformation. The results suggest that under compression of Mg-Y alloys slip is more active than twinning in comparison to Mg-Gd alloys.

Fracture and fatigue behavior of shot-blasted titanium dental implants.

PubMed

Gil, F J; Planell, J A; Padrós, A

2002-01-01

This investigation studies the effect of the shot-blasting treatment on the cyclic deformation behavior of a commercially pure titanium, with two microstructures: equiaxed and acicular. The fatigue tests were carried out in artificial saliva medium at 37 degrees C. Cyclic deformation tests have been carried out up to fracture, and the fatigue crack nucleation and propagation have been analyzed. The results show that the shot-blasting treatment improves the fatigue life in the microstructures studied, and that the equiaxed was better in mechanical properties than the acicular. The cause of this improvement in the mechanical properties is due to the compressive stress on the material surface for the shot-blasted specimens. Hardness tests were carried out to determine the value of these internal stresses.

Prediction of the Stress-Strain Behavior of Open-Cell Aluminum Foam under Compressive Loading and the Effects of Various RVE Boundary Conditions

NASA Astrophysics Data System (ADS)

Hamidi Ghaleh Jigh, Behrang; Farsi, Mohammad Ali; Hosseini Toudeshky, Hossein

2018-05-01

The prediction of the mechanical behavior of metallic foams with realistic microstructure and the effects of various boundary conditions on the mechanical behavior is an important and challenging issue in modeling representative volume elements (RVEs). A numerical investigation is conducted to determine the effects of various boundary conditions and cell wall cross sections on the compressive mechanical properties of aluminum foam, including the stiffness, plateau stress and onset strain of densification. The open-cell AA6101-T6 aluminum foam Duocel is used in the analyses in this study. Geometrical characteristics including the cell size, foam relative density, and cross-sectional shape and thickness of the cell walls are extracted from images of the foam. Then, the obtained foam microstructure is analyzed as a 2D model. The ligaments are modeled as shear deformable beams with elastic-plastic material behavior. To prevent interpenetration of the nodes and walls inside the cells with large deformations, self-contact-type frictionless interaction is stipulated between the internal surfaces. Sensitivity analyses are performed using several boundary conditions and cells wall cross-sectional shapes. The predicted results from the finite element analyses are compared with the experimental results. Finally, the most appropriate boundary conditions, leading to more consistent results with the experimental data, are introduced.

Prediction of the Stress-Strain Behavior of Open-Cell Aluminum Foam under Compressive Loading and the Effects of Various RVE Boundary Conditions

NASA Astrophysics Data System (ADS)

Hamidi Ghaleh Jigh, Behrang; Farsi, Mohammad Ali; Hosseini Toudeshky, Hossein

2018-04-01

The prediction of the mechanical behavior of metallic foams with realistic microstructure and the effects of various boundary conditions on the mechanical behavior is an important and challenging issue in modeling representative volume elements (RVEs). A numerical investigation is conducted to determine the effects of various boundary conditions and cell wall cross sections on the compressive mechanical properties of aluminum foam, including the stiffness, plateau stress and onset strain of densification. The open-cell AA6101-T6 aluminum foam Duocel is used in the analyses in this study. Geometrical characteristics including the cell size, foam relative density, and cross-sectional shape and thickness of the cell walls are extracted from images of the foam. Then, the obtained foam microstructure is analyzed as a 2D model. The ligaments are modeled as shear deformable beams with elastic-plastic material behavior. To prevent interpenetration of the nodes and walls inside the cells with large deformations, self-contact-type frictionless interaction is stipulated between the internal surfaces. Sensitivity analyses are performed using several boundary conditions and cells wall cross-sectional shapes. The predicted results from the finite element analyses are compared with the experimental results. Finally, the most appropriate boundary conditions, leading to more consistent results with the experimental data, are introduced.

Experimental and theoretical study of the buckling of narrow thin plates on an elastic foundation under compression

NASA Astrophysics Data System (ADS)

Kurguzov, V. D.; Demeshkin, A. G.

2016-05-01

The paper describes the processes of elastic deformation of thin films under mechanical loading. The film is modeled longitudinally by a compressed plate arranged on an elastic foundation. A computer model of the buckling of the narrow thin plate with a delamination portion located on an elastic foundation is constructed. This paper also touches upon the supercritical behavior of the plate-substrate system. The experiments on the axial compression of a metal strip adhered to a rubber plate are performed, and 2 to 7 buckling modes are obtained therein. The critical loads and buckling modes obtained in the numerical calculations are compared with the experimental data. It is shown that there is the possibility of progressive delamination of the metal plate from the foundation if the critical load is exceeded. It is found that the use of the proposed approach, which, in contrast to other approaches, accounts for the elastic deformation of the substrate, causes the dependence between the critical bending stress and the stiffness of the foundation.

The Effect of Grain Size on the Strain Hardening Behavior for Extruded ZK61 Magnesium Alloy

NASA Astrophysics Data System (ADS)

Zhang, Lixin; Zhang, Wencong; Chen, Wenzhen; Duan, Junpeng; Wang, Wenke; Wang, Erde

2017-12-01

The effects of grain size on the tensile and compressive strain hardening behaviors for extruded ZK61 alloys have been investigated by uniaxial tensile and compressive tests along the extrusion directions. Cylindrical tension and compression specimens of extruded ZK61 alloys with various sized grain were fabricated by annealing treatments. Tensile and compressive tests at ambient temperature were conducted at a strain rate of 0.5 × 10-3 s-1. The results indicate that both tensile strain hardening and compressive strain hardening of ZK61 alloys with different grain sizes have an athermal regime of dislocation accumulation in early deformation. The threshold stress value caused dynamic recovery is predominantly related to grain size in tensile strain hardening, but the threshold stress values for different grain sizes are almost identical in compressive strain hardening. There are obvious transition points on the tensile strain hardening curves which indicate the occurrence of dynamic recrystallization (DRX). The tensile strain hardening rate of the coarse-grained alloy obviously decreases faster than that of fine-grained alloys before DRX and the tensile strain hardening curves of different grain sizes basically tend to parallel after DRX. The compressive strain hardening rate of the fine-grained alloy obviously increases faster than that of coarse-grained alloy for twin-induced strain hardening, but compressive strain hardening curves also tend to parallel after twinning is exhausted.

Three-dimensional Sponges with Super Mechanical Stability: Harnessing True Elasticity of Individual Carbon Nanotubes in Macroscopic Architectures

PubMed Central

Dai, Zhaohe; Liu, Luqi; Qi, Xiaoying; Kuang, Jun; Wei, Yueguang; Zhu, Hongwei; Zhang, Zhong

2016-01-01

Efficient assembly of carbon nanotube (CNT) based cellular solids with appropriate structure is the key to fully realize the potential of individual nanotubes in macroscopic architecture. In this work, the macroscopic CNT sponge consisting of randomly interconnected individual carbon nanotubes was grown by CVD, exhibiting a combination of super-elasticity, high strength to weight ratio, fatigue resistance, thermo-mechanical stability and electro-mechanical stability. To deeply understand such extraordinary mechanical performance compared to that of conventional cellular materials and other nanostructured cellular architectures, a thorough study on the response of this CNT-based spongy structure to compression is conducted based on classic elastic theory. The strong inter-tube bonding between neighboring nanotubes is examined, believed to play a critical role in the reversible deformation such as bending and buckling without structural collapse under compression. Based on in-situ scanning electron microscopy observation and nanotube deformation analysis, structural evolution (completely elastic bending-buckling transition) of the carbon nanotubes sponges to deformation is proposed to clarify their mechanical properties and nonlinear electromechanical coupling behavior. PMID:26732143

Predicting the flexure response of wood-plastic composites from uni-axial and shear data using a finite-element model

Treesearch

Scott E. Hamel; John C. Hermanson; Steven M. Cramer

2014-01-01

Wood-plastic composites (WPCs), commonly used in residential decks and railings, exhibit mechanical behavior that is bimodal, anisotropic, and nonlinear viscoelastic. They exhibit different stress-strain responses to tension and compression, both of which are nonlinear. Their mechanical properties vary with respect to extrusion direction, their deformation under...

Effect of borides on hot deformation behavior and microstructure evolution of powder metallurgy high borated stainless steel

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhou, Xuan

To investigate borides effect on the hot deformation behavior and microstructure evolution of powder metallurgy high borated stainless steel, hot compression tests at the temperatures of 950– 1150 °C and the strain rates of 0.01– 10 s{sup −1} were performed. Flow stress curves indicated that borides increased the material's stress level at low temperature but the strength was sacrificed at temperatures above 1100 °C. A hyperbolic-sine equation was used to characterize the dependence of the flow stress on the deformation temperature and strain rate. The hot deformation activation energy and stress exponent were determined to be 355 kJ/mol and 3.2,more » respectively. The main factors leading to activation energy and stress exponent of studied steel lower than those of commercial 304 stainless steel were discussed. Processing maps at the strains of 0.1, 0.3, 0.5, and 0.7 showed that flow instability mainly concentrated at 950– 1150 °C and strain rate higher than 0.6 s{sup −1}. Results of microstructure illustrated that dynamic recrystallization was fully completed at both high temperature-low strain rate and low temperature-high strain rate. In the instability region cracks were generated in addition to cavities. Interestingly, borides maintained a preferential orientation resulting from particle rotation during compression. - Highlights: •The decrement of activation energy was affected by boride and boron solution. •The decrease of stress exponent was influenced by composition and Cottrell atmosphere. •Boride represented a preferential orientation caused by particle rotation.« less

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ren, Jingli; Chen, Cun; Wang, Gang

This study explores the temporal scaling behavior induced shear-branching structure in response to variant temperatures and strain rates during plastic deformation of Zr-based bulk metallic glass (BMG). The data analysis based on the compression tests suggests that there are two states of shear-branching structures: the fractal structure with a long-range order at an intermediate temperature of 223 K and a larger strain rate of 2.5 × 10 –2 s –1; the disordered structure dominated at other temperature and strain rate. It can be deduced from the percolation theory that the compressive ductility, ec, can reach the maximum value at themore » intermediate temperature. Furthermore, a dynamical model involving temperature is given for depicting the shear-sliding process, reflecting the plastic deformation has fractal structure at the temperature of 223 K and strain rate of 2.5 × 10 –2 s –1.« less

AFM study of the plastic deformation behavior of poly-synthetically-twinned (PST) titanium aluminide crystals

NASA Astrophysics Data System (ADS)

Chen, Yali

The plastic deformation behavior of PST TiAl crystals was investigated using AFM techniques to reveal the effects of lamellar structure on the deform mechanisms of two-phase TiAl materials. PST crystals with a nominal composition of Ti52Al48 (atomic percent) were grown by the floating zone method and at various orientations deformed in compression at room temperature. Atomic Force Microscopy (AFM) was employed to investigate the deformation structure on the free surfaces. The deformation of the PST crystals is highly anisotropic and the deformation mechanism changes dramatically with sample orientation. When the angle between the loading axis and the lamellar interfaces is below 20°, the gamma lamellae deform by dislocation slip and twinning on planes oblique to the lamellar interfaces, but the Burgers vectors or the resultant shear vectors are parallel to the lamellar interfaces inside each lamella. When the angle is between 20° and 80° the gamma phase deforms by shear on planes parallel to the lamellar interfaces. Some domains deform by a combination of ordinary dislocation slip and twinning. In the domains where twinning cannot be activated, slip occurs by ordinary dislocations or superdislocations. When the loading axis is nearly perpendicular to the lamellar interfaces ordinary dislocation slip and twinning on slip planes inclined with the lamellar interfaces are dominant and the shear is trans-lamellar. The three deformation modes are termed as A, B and N type deformation modes respectively. In the A type mode the alpha2 lamellae concomitantly deform by prismatic slip. In the other two modes, the alpha2 phase does not deform and acts as strong obstacles to the transfer of deformation. Abundant misfit dislocations are emitted from the lamellar interfaces which is beneficial for the plastic deformation. On the other hand, the lamellar interfaces strongly impede trans-lamellar deformation and channel the deformation inside each lamella. The inhomogeneous coherency stresses at the lamellar interfaces also lead to heterogeneous deformation of PST crystals. The deformation behavior of the lamellar grains produces remarkable strain incompatibility in lamellar polycrystals and deteriorates the deformability.

Formulation and in vitro evaluation of theophylline matrix tablets prepared by direct compression: Effect of polymer blends

PubMed Central

El-Bagory, Ibrahim; Barakat, Nahla; Ibrahim, Mohamed A.; El-Enazi, Fouza

2011-01-01

The deformation mechanism of pharmaceutical powders, used in formulating directly compressed matrix tablets, affects the characteristics of the formed tablets. Three polymers of different deformation mechanisms were tested for their impact on theophylline directly compressed tablets namely Kollidon SR (KL SR, plastic deformation), Ethylcellulose (EC, elastic deformation) and Carnauba wax (CW, brittle deformation) at different compression forces. However, tablets based mainly on KL SR, the plastically deformed polymer (TN1) exhibited the highest hardness values compared to the other formulae which are based on either blends of KL SR with CW, the very brittle deformed polymer. The upper detected force for TN formulae and the lower punch force were found to dependent mainly on the powder deformation. This difference is attributed to the work done during the compression phase as well as the work lost during the decompression phase. Furthermore, the release profiles of TN from formulae TN2 and TN4 that are based on the composition (2KL SR:1EC) and (1KL SR:2EC), respectively, were consistent with different deformation mechanisms of KL SR and EC and on the physicochemical properties like the water absorptive capacity of EC. Upon increasing the weight ratio of KL SR (TN2), the release rate was greatly retarded (39.4%, 37.1%, 35.0% and 33.6% released after 8 h at 5, 10, 15 and 20 kN. PMID:24115902

Strength and deformability of compressed concrete elements with various types of non-metallic fiber and rods reinforcement under static loading

NASA Astrophysics Data System (ADS)

Nevskii, A. V.; Baldin, I. V.; Kudyakov, K. L.

2015-01-01

Adoption of modern building materials based on non-metallic fibers and their application in concrete structures represent one of the important issues in construction industry. This paper presents results of investigation of several types of raw materials selected: basalt fiber, carbon fiber and composite fiber rods based on glass and carbon. Preliminary testing has shown the possibility of raw materials to be effectively used in compressed concrete elements. Experimental program to define strength and deformability of compressed concrete elements with non-metallic fiber reinforcement and rod composite reinforcement included design, manufacture and testing of several types of concrete samples with different types of fiber and longitudinal rod reinforcement. The samples were tested under compressive static load. The results demonstrated that fiber reinforcement of concrete allows increasing carrying capacity of compressed concrete elements and reducing their deformability. Using composite longitudinal reinforcement instead of steel longitudinal reinforcement in compressed concrete elements insignificantly influences bearing capacity. Combined use of composite rod reinforcement and fiber reinforcement in compressed concrete elements enables to achieve maximum strength and minimum deformability.

Regional variations in growth plate chondrocyte deformation as predicted by three-dimensional multi-scale simulations.

PubMed

Gao, Jie; Roan, Esra; Williams, John L

2015-01-01

The physis, or growth plate, is a complex disc-shaped cartilage structure that is responsible for longitudinal bone growth. In this study, a multi-scale computational approach was undertaken to better understand how physiological loads are experienced by chondrocytes embedded inside chondrons when subjected to moderate strain under instantaneous compressive loading of the growth plate. Models of representative samples of compressed bone/growth-plate/bone from a 0.67 mm thick 4-month old bovine proximal tibial physis were subjected to a prescribed displacement equal to 20% of the growth plate thickness. At the macroscale level, the applied compressive deformation resulted in an overall compressive strain across the proliferative-hypertrophic zone of 17%. The microscale model predicted that chondrocytes sustained compressive height strains of 12% and 6% in the proliferative and hypertrophic zones, respectively, in the interior regions of the plate. This pattern was reversed within the outer 300 μm region at the free surface where cells were compressed by 10% in the proliferative and 26% in the hypertrophic zones, in agreement with experimental observations. This work provides a new approach to study growth plate behavior under compression and illustrates the need for combining computational and experimental methods to better understand the chondrocyte mechanics in the growth plate cartilage. While the current model is relevant to fast dynamic events, such as heel strike in walking, we believe this approach provides new insight into the mechanical factors that regulate bone growth at the cell level and provides a basis for developing models to help interpret experimental results at varying time scales.

Regional Variations in Growth Plate Chondrocyte Deformation as Predicted By Three-Dimensional Multi-Scale Simulations

PubMed Central

Gao, Jie; Roan, Esra; Williams, John L.

2015-01-01

The physis, or growth plate, is a complex disc-shaped cartilage structure that is responsible for longitudinal bone growth. In this study, a multi-scale computational approach was undertaken to better understand how physiological loads are experienced by chondrocytes embedded inside chondrons when subjected to moderate strain under instantaneous compressive loading of the growth plate. Models of representative samples of compressed bone/growth-plate/bone from a 0.67 mm thick 4-month old bovine proximal tibial physis were subjected to a prescribed displacement equal to 20% of the growth plate thickness. At the macroscale level, the applied compressive deformation resulted in an overall compressive strain across the proliferative-hypertrophic zone of 17%. The microscale model predicted that chondrocytes sustained compressive height strains of 12% and 6% in the proliferative and hypertrophic zones, respectively, in the interior regions of the plate. This pattern was reversed within the outer 300 μm region at the free surface where cells were compressed by 10% in the proliferative and 26% in the hypertrophic zones, in agreement with experimental observations. This work provides a new approach to study growth plate behavior under compression and illustrates the need for combining computational and experimental methods to better understand the chondrocyte mechanics in the growth plate cartilage. While the current model is relevant to fast dynamic events, such as heel strike in walking, we believe this approach provides new insight into the mechanical factors that regulate bone growth at the cell level and provides a basis for developing models to help interpret experimental results at varying time scales. PMID:25885547

Numerical estimation of deformation energy of selected bulk oilseeds in compression loading

NASA Astrophysics Data System (ADS)

Demirel, C.; Kabutey, A.; Herak, D.; Gurdil, G. A. K.

2017-09-01

This paper aimed at the determination of the deformation energy of some bulk oilseeds or kernels namely oil palm, sunflower, rape and flax in linear pressing applying the trapezoidal rule which is characterized by the area under the force and deformation curve.The bulk samples were measured at the initial pressing height of 60 mm with the vessel diameter of 60 mm where they were compressed under the universal compression machine at a maximum force of 200 kN and speed of 5 mm/min.Based on the compression test, the optimal deformation energy for recovering the oil was observed at a force of 163 kN where there was no seed/kernel cake ejection in comparison to the initial maximum force used particularly for rape and flax bulk oilseeds.This information is needed for analyzing the energy efficiency of the non-linear compression process involving a mechanical screw press or expeller.

Mapping local deformation behavior in single cell metal lattice structures

DOE Office of Scientific and Technical Information (OSTI.GOV)

Carlton, Holly D.; Lind, Jonathan; Messner, Mark C.

The deformation behavior of metal lattice structures is extremely complex and challenging to predict, especially since strain is not uniformly distributed throughout the structure. Understanding and predicting the failure behavior for these types of light-weighting structures is of great interest due to the excellent scaling of stiffness- and strength-to weight ratios they display. Therefore, there is a need to perform simplified experiments that probe unit cell mechanisms. This study reports on high resolution mapping of the heterogeneous structural response of single unit cells to the macro-scale loading condition. Two types of structures, known to show different stress-strain responses, were evaluatedmore » using synchrotron radiation micro-tomography while performing in-situ uniaxial compression tests to capture the local micro-strain deformation. These structures included the octet-truss, a stretch-dominated lattice, and the rhombic-dodecahedron, a bend-dominated lattice. The tomographic analysis showed that the stretch- and bend-dominated lattices exhibit different failure mechanisms and that the defects built into the structure cause a heterogeneous localized deformation response. Also shown here is a change in failure mode for stretch-dominated lattices, where there appears to be a transition from buckling to plastic yielding for samples with a relative density between 10 and 20%. In conclusion, the experimental results were also used to inform computational studies designed to predict the mesoscale deformation behavior of lattice structures. Here an equivalent continuum model and a finite element model were used to predict both local strain fields and mechanical behavior of lattices with different topologies.« less

Mapping local deformation behavior in single cell metal lattice structures

DOE PAGES

Carlton, Holly D.; Lind, Jonathan; Messner, Mark C.; ...

2017-02-08

The deformation behavior of metal lattice structures is extremely complex and challenging to predict, especially since strain is not uniformly distributed throughout the structure. Understanding and predicting the failure behavior for these types of light-weighting structures is of great interest due to the excellent scaling of stiffness- and strength-to weight ratios they display. Therefore, there is a need to perform simplified experiments that probe unit cell mechanisms. This study reports on high resolution mapping of the heterogeneous structural response of single unit cells to the macro-scale loading condition. Two types of structures, known to show different stress-strain responses, were evaluatedmore » using synchrotron radiation micro-tomography while performing in-situ uniaxial compression tests to capture the local micro-strain deformation. These structures included the octet-truss, a stretch-dominated lattice, and the rhombic-dodecahedron, a bend-dominated lattice. The tomographic analysis showed that the stretch- and bend-dominated lattices exhibit different failure mechanisms and that the defects built into the structure cause a heterogeneous localized deformation response. Also shown here is a change in failure mode for stretch-dominated lattices, where there appears to be a transition from buckling to plastic yielding for samples with a relative density between 10 and 20%. In conclusion, the experimental results were also used to inform computational studies designed to predict the mesoscale deformation behavior of lattice structures. Here an equivalent continuum model and a finite element model were used to predict both local strain fields and mechanical behavior of lattices with different topologies.« less

The influence of the compression interface on the failure behavior and size effect of concrete

NASA Astrophysics Data System (ADS)

Kampmann, Raphael

The failure behavior of concrete materials is not completely understood because conventional test methods fail to assess the material response independent of the sample size and shape. To study the influence of strength and strain affecting test conditions, four typical concrete sample types were experimentally evaluated in uniaxial compression and analyzed for strength, deformational behavior, crack initiation/propagation, and fracture patterns under varying boundary conditions. Both low friction and conventional compression interfaces were assessed. High-speed video technology was used to monitor macrocracking. Inferential data analysis proved reliably lower strength results for reduced surface friction at the compression interfaces, regardless of sample shape. Reciprocal comparisons revealed statistically significant strength differences between most sample shapes. Crack initiation and propagation was found to differ for dissimilar compression interfaces. The principal stress and strain distributions were analyzed, and the strain domain was found to resemble the experimental results, whereas the stress analysis failed to explain failure for reduced end confinement. Neither stresses nor strains indicated strength reductions due to reduced friction, and therefore, buckling effects were considered. The high-speed video analysis revealed localize buckling phenomena, regardless of end confinement. Slender elements were the result of low friction, and stocky fragments developed under conventional confinement. The critical buckling load increased accordingly. The research showed that current test methods do not reflect the "true'' compressive strength and that concrete failure is strain driven. Ultimate collapse results from buckling preceded by unstable cracking.

Characterization of particle deformation during compression measured by confocal laser scanning microscopy.

PubMed

Guo, H X; Heinämäki, J; Yliruusi, J

1999-09-20

Direct compression of riboflavin sodium phosphate tablets was studied by confocal laser scanning microscopy (CLSM). The technique is non-invasive and generates three-dimensional (3D) images. Tablets of 1% riboflavin sodium phosphate with two grades of microcrystalline cellulose (MCC) were individually compressed at compression forces of 1.0 and 26.8 kN. The behaviour and deformation of drug particles on the upper and lower surfaces of the tablets were studied under compression forces. Even at the lower compression force, distinct recrystallized areas in the riboflavin sodium phosphate particles were observed in both Avicel PH-101 and Avicel PH-102 tablets. At the higher compression force, the recrystallization of riboflavin sodium phosphate was more extensive on the upper surface of the Avicel PH-102 tablet than the Avicel PH-101 tablet. The plastic deformation properties of both MCC grades reduced the fragmentation of riboflavin sodium phosphate particles. When compressed with MCC, riboflavin sodium phosphate behaved as a plastic material. The riboflavin sodium phosphate particles were more tightly bound on the upper surface of the tablet than on the lower surface, and this could also be clearly distinguished by CLSM. Drug deformation could not be visualized by other techniques. Confocal laser scanning microscopy provides valuable information on the internal mechanisms of direct compression of tablets.

Strain induced grain boundary migration effects on grain growth of an austenitic stainless steel during static and metadynamic recrystallization

DOE Office of Scientific and Technical Information (OSTI.GOV)

Paggi, A., E-mail: alpaggi@tenaris.com; Angella, G.; Donnini, R.

Static and metadynamic recrystallization of an AISI 304L austenitic stainless steel was investigated at 1100 °C and 10{sup −} {sup 2} s{sup −} {sup 1} strain rate. The kinetics of recrystallization was determined through double hit compression tests. Two strain levels were selected for the first compression hit: ε{sub f} = 0.15 for static recrystallization (SRX) and 0.25 for metadynamic recrystallization (MDRX). Both the as-deformed and the recrystallized microstructures were investigated through optical microscopy and electron back-scattered diffraction (EBSD) technique. During deformation, strain induced grain boundary migration appeared to be significant, producing a square-like grain boundary structure aligned along themore » directions of the maximum shear stresses in compression. EBSD analysis revealed to be as a fundamental technique that the dislocation density was distributed heterogeneously in the deformed grains. Grain growth driven by surface energy reduction was also investigated, finding that it was too slow to explain the experimental data. Based on microstructural results, it was concluded that saturation of the nucleation sites occurred in the first stages of recrystallization, while grain growth driven by strain induced grain boundary migration (SIGBM) dominated the subsequent stages. - Highlights: • Recrystallization behavior of a stainless steel was investigated at 1100 °C. • EBSD revealed that the dislocation density distribution was heterogeneous during deformation. • Saturation of nucleation sites occurred in the first stages of recrystallization. • Strain induced grain boundary migration (SIGBM) effects were significant. • Grain growth driven by SIGBM dominated the subsequent stages.« less

Two-Dimensional Imaging Velocimetry of Heterogeneous Flow and Brittle Failure in Diamond

NASA Astrophysics Data System (ADS)

Ali, S. J.; Smith, R.; Erskine, D.; Eggert, J.; Celliers, P. M.; Collins, G. W.; Jeanloz, R.

2014-12-01

Understanding the nature and dynamics of heterogeneous flow in diamond subjected to shock compression is important for many fields of research, from inertial confinement fusion to the study of carbon rich planets. Waves propagating through a shocked material can be significantly altered by the various deformation mechanisms present in shocked materials, including anisotropic sound speeds, phase transformations, plastic/inelastic flow and brittle failure. Quantifying the spatial and temporal effects of these deformation mechanisms has been limited by a lack of diagnostics capable of obtaining simultaneous micron resolution spatial measurements and nanosecond resolution time measurements. We have utilized the 2D Janus High Resolution Velocimeter at LLNL to study the time and space dependence of fracture in shock-compressed diamond above the Hugoniot elastic limit. Previous work on the OMEGA laser facility (Rochester) has shown that the free-surface reflectivity of μm-grained diamond samples drops linearly with increasing sample pressure, whereas under the same conditions the reflectivity of nm-grained samples remains unaffected. These disparate observations can be understood by way of better documenting fracture in high-strain compression of diamond. To this end, we have imaged the development and evolution of elastic-wave propagation, plastic-wave propagation and fracture networks in the three primary orientations of single-crystal diamond, as well as in microcrystalline and nanocrystalline diamond, and find that the deformation behavior depends sensitively on the orientation and crystallinity of the diamonds.

Flexible Foam Model.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Neilsen, Michael K.; Lu, Wei-Yang; Werner, Brian T.

Experiments were performed to characterize the mechanical response of a 15 pcf flexible polyurethane foam to large deformation at different strain rates and temperatures. Results from these experiments indicated that at room temperature, flexible polyurethane foams exhibit significant nonlinear elastic deformation and nearly return to their original undeformed shape when unloaded. However, when these foams are cooled to temperatures below their glass transition temperature of approximately -35 o C, they behave like rigid polyurethane foams and exhibit significant permanent deformation when compressed. Thus, a new model which captures this dramatic change in behavior with temperature was developed and implemented intomore » SIERRA with the name Flex_Foam to describe the mechanical response of both flexible and rigid foams to large deformation at a variety of temperatures and strain rates. This report includes a description of recent experiments. Next, development of the Flex Foam model for flexible polyurethane and other flexible foams is described. Selection of material parameters are discussed and finite element simulations with the new Flex Foam model are compared with experimental results to show behavior that can be captured with this new model.« less

Static Recrystallization Behavior of Z12CN13 Martensite Stainless Steel

NASA Astrophysics Data System (ADS)

Luo, Min; Zhou, Bing; Li, Rong-bin; Xu, Chun; Guo, Yan-hui

2017-09-01

In order to increase the hot workability and provide proper hot forming parameters of forging Z12CN13 martensite stainless steel for the simulation and production, the static recrystallization behavior has been studied by double-pass hot compression tests. The effects of deformation temperature, strain rate and inter-pass time on the static recrystallization fraction by the 2% offset method are extensively studied. The results indicate that increasing the inter-pass time and the deformation temperature as well as strain rate appropriately can increase the fraction of static recrystallization. At the temperature of 1050-1150 °C, inter-pass time of 30-100 s and strain rate of 0.1-5 s-1, the static recrystallization behavior is obvious. In addition, the kinetics of static recrystallization behavior of Z12CN13 steel has been established and the activation energy of static recrystallization is 173.030 kJ/mol. The substructure and precipitates have been studied by TEM. The results reveal that the nucleation mode is bulging at grain boundary. Undissolved precipitates such as MoNi3 and Fe3C have a retarding effect on the recrystallization kinetics. The effect is weaker than the accelerating effect of deformation temperature.

Effect of pre-straining on the evolution of material anisotropy in rolled magnesium alloy AZ31 sheet

NASA Astrophysics Data System (ADS)

Qiao, H.; Guo, X. Q.; Wu, P. D.

2013-12-01

The large strain Elastic Visco-Plastic Self-Consistent (EVPSC) model and the recently developed Twinning and De-Twinning (TDT) model are applied to study the mechanical behavior of rolled magnesium alloy AZ31 sheet. Three different specimen orientations with tilt angles of 0°, 45° and 90° between the rolling direction and longitudinal specimen axis are used to study the mechanical anisotropy under both uniaxial tension and compression. The effect of pre-strain in uniaxial compression along the rolling direction on subsequent uniaxial tension/compression along the three directions is also investigated. It is demonstrated that the twinning during pre-strain in compression and the detwinning in the subsequent deformation have a significant influence on the mechanical anisotropy. Numerical results are in good agreement with the experimental observations found in the literature.

Stress path dependent hydromechanical behaviour of heterogeneous carbonate rock

NASA Astrophysics Data System (ADS)

Gland, N.; Dautriat, J.; Dimanov, A.; Raphanel, J.

2010-06-01

The influence of stress paths, representative of reservoir conditions, on the hydromechanical behavior of a moderately heterogeneous carbonate has been investigated. Multiscale structural heterogeneities, common for instance in carbonate rocks, can strongly alter the mechanical response and significantly influence the evolution of flow properties with stress. Using a triaxial cell, the permeability evolutions during compression and the effects of brittle (fracture) and plastic (pore collapse) deformations at yield, were measured. A strong scattering was observed on the mechanical response both in term of compressibility and failure threshold. Using the porosity scaling predicted by an adapted effective medium theory (based on crack growth under Hertzian contact), we have rescaled the critical pressures by the normalized porosity deviation. This procedure reduces efficiently the scattering, revealing in the framework of proportional stress path loading, a linear relation between the critical pressures and the stress path parameter through all the deformation regimes. It leads to a new formulation for the critical state envelope in the 'mean stress, deviatoric stress' diagram. The attractive feature of this new yield envelope formulation relies on the fact that only the two most common different mechanical tests 'Uniaxial Compression' and 'Hydrostatic Compression', are needed to define entirely the yield envelope. Volumic strains and normalized permeabilities are finally mapped in the stresses diagram and correlated.

Experimental Study on the Seismic Performance of Recycled Concrete Brick Walls Embedded with Vertical Reinforcement.

PubMed

Cao, Wanlin; Zhang, Yongbo; Dong, Hongying; Zhou, Zhongyi; Qiao, Qiyun

2014-08-19

Recycled concrete brick (RCB) is manufactured by recycled aggregate processed from discarded concrete blocks arising from the demolishing of existing buildings. This paper presents research on the seismic performance of RCB masonry walls to assess the applicability of RCB for use in rural low-rise constructions. The seismic performance of a masonry wall is closely related to the vertical load applied to the wall. Thus, the compressive performance of RCB masonry was investigated firstly by constructing and testing eighteen RCB masonry compressive specimens with different mortar strengths. The load-bearing capacity, deformation and failure characteristic were analyzed, as well. Then, a quasi-static test was carried out to study the seismic behavior of RCB walls by eight RCB masonry walls subjected to an axial compressive load and a reversed cyclic lateral load. Based on the test results, equations for predicting the compressive strength of RCB masonry and the lateral ultimate strength of an RCB masonry wall were proposed. Experimental values were found to be in good agreement with the predicted values. Meanwhile, finite element analysis (FEA) and parametric analysis of the RCB walls were carried out using ABAQUS software. The elastic-plastic deformation characteristics and the lateral load-displacement relations were studied.

Experimental Study on the Seismic Performance of Recycled Concrete Brick Walls Embedded with Vertical Reinforcement

PubMed Central

Cao, Wanlin; Zhang, Yongbo; Dong, Hongying; Zhou, Zhongyi; Qiao, Qiyun

2014-01-01

Recycled concrete brick (RCB) is manufactured by recycled aggregate processed from discarded concrete blocks arising from the demolishing of existing buildings. This paper presents research on the seismic performance of RCB masonry walls to assess the applicability of RCB for use in rural low-rise constructions. The seismic performance of a masonry wall is closely related to the vertical load applied to the wall. Thus, the compressive performance of RCB masonry was investigated firstly by constructing and testing eighteen RCB masonry compressive specimens with different mortar strengths. The load-bearing capacity, deformation and failure characteristic were analyzed, as well. Then, a quasi-static test was carried out to study the seismic behavior of RCB walls by eight RCB masonry walls subjected to an axial compressive load and a reversed cyclic lateral load. Based on the test results, equations for predicting the compressive strength of RCB masonry and the lateral ultimate strength of an RCB masonry wall were proposed. Experimental values were found to be in good agreement with the predicted values. Meanwhile, finite element analysis (FEA) and parametric analysis of the RCB walls were carried out using ABAQUS software. The elastic-plastic deformation characteristics and the lateral load-displacement relations were studied. PMID:28788170

Measurement of compressed breast thickness by optical stereoscopic photogrammetry.

PubMed

Tyson, Albert H; Mawdsley, Gordon E; Yaffe, Martin J

2009-02-01

The determination of volumetric breast density (VBD) from mammograms requires accurate knowledge of the thickness of the compressed breast. In attempting to accurately determine VBD from images obtained on conventional mammography systems, the authors found that the thickness reported by a number of mammography systems in the field varied by as much as 15 mm when compressing the same breast or phantom. In order to evaluate the behavior of mammographic compression systems and to be able to predict the thickness at different locations in the breast on patients, they have developed a method for measuring the local thickness of the breast at all points of contact with the compression paddle using optical stereoscopic photogrammetry. On both flat (solid) and compressible phantoms, the measurements were accurate to better than 1 mm with a precision of 0.2 mm. In a pilot study, this method was used to measure thickness on 108 volunteers who were undergoing mammography examination. This measurement tool will allow us to characterize paddle surface deformations, deflections and calibration offsets for mammographic units.

Loads and Deformations of Buckled Rectangular Plates. Degree awarded by Virginia Polytechnic Inst., Jun. 1958

NASA Technical Reports Server (NTRS)

Stein, Manuel

1959-01-01

The nonlinear large-deflection equations of von Karman for plates are converted into a set of linear equations by expanding the displacements Into a power series in terms of an arbitrary parameter. The postbuckling behavior of simply supported rectangular plates subjected to longitudinal compression and subject to a uniform temperature rise is investigated in detail by solving the first few of the equations. Experimental data are presented for the compression problem. Comparisons are made for total shortening and local strains and deflections which indicate good agreement between experimental and theoretical results.

Unraveling cyclic deformation mechanisms of a rolled magnesium alloy using in situ neutron diffraction

DOE PAGES

Wu, Wei; An, Ke; Liaw, Peter K.

2014-12-23

In the current study, the deformation mechanisms of a rolled magnesium alloy were investigated under cyclic loading using real-time in situ neutron diffraction under a continuous-loading condition. The relationship between the macroscopic cyclic deformation behavior and the microscopic response at the grain level was established. The neutron diffraction results indicate that more and more grains are involved in the twinning and detwinning deformation process with the increase of fatigue cycles. The residual twins appear in the early fatigue life, which is responsible for the cyclic hardening behavior. The asymmetric shape of the hysteresis loop is attributed to the early exhaustionmore » of the detwinning process during compression, which leads to the activation of dislocation slips and rapid strain-hardening. The critical resolved shear stress for the activation of tensile twinning closely depends on the residual strain developed during cyclic loading. In the cycle before the sample fractured, the dislocation slips became active in tension, although the sample was not fully twinned. The increased dislocation density leads to the rise of the stress concentration at weak spots, which is believed to be the main reason for the fatigue failure. Furthermore, the deformation history greatly influences the deformation mechanisms of hexagonal-close-packed-structured magnesium alloy during cyclic loading.« less

Hot deformation constitutive equation and processing map of Alloy 690

NASA Astrophysics Data System (ADS)

Feng, Han; Zhang, Songchuang; Ma, Mingjuan; Song, Zhigang

The hot deformation behavior of alloy 690 was studied in the temperature range of 800-1300 C and strain rate range of 0.1-10 s-1 by hot compression tests in a Gleeble 1500+ thermal mechanical simulator. The results indicated that flow stress of alloy 690 is sensitive to deformation temperature and strain rate and peak stress increases with decreasing of temperature and increasing of strain rate. In addition, the hot deformation parameters of deformation activation were calculated and the apparent activation energy of this alloy is about 300 kJ/mol. The constitutive equation which can be used to relate peak stress to the absolute temperature and strain rate was obtained. It's further found that the processing maps exhibited two domains which are considered as the optimum windows for hot working. The microstructure observations of the specimens deformed in this domain showed the full dynamic recrystallization (DRX) structure. There was a flow instability domain in the processing map where hot working should be avoided.

Deformation behavior of a Ni-30Al-20Fe-0.05Zr intermetallic alloy in the temperature range 300 to 1300 K

NASA Technical Reports Server (NTRS)

Raj, S. V.; Locci, I. E.; Noebe, R. D.

1992-01-01

The deformation properties of an extruded Ni-30Al-20Fe-0.05Zr (at. pct) alloy in the temperature range 300-1300 K were investigated under initial tensile strain rates that varied between 10 exp -6 and 10 exp -3/sec and in constant load compression creep between 1073 and 1300 K. Three deformation regimes were observed: region I, occurring between 400 and 673 K, which consisted of an athermal regime of less than 0.3 percent tensile ductility; region II, between 673 and 1073, where exponential creep was dominant; and region III, between 1073 and 1300 K, where a significant improvement in tensile ductility was observed.

Modeling Micro-cracking Behavior of Bukit Timah Granite Using Grain-Based Model

NASA Astrophysics Data System (ADS)

Peng, Jun; Wong, Louis Ngai Yuen; Teh, Cee Ing; Li, Zhihuan

2018-01-01

Rock strength and deformation behavior has long been recognized to be closely related to the microstructure and the associated micro-cracking process. A good understanding of crack initiation and coalescence mechanisms will thus allow us to account for the variation of rock strength and deformation properties from a microscopic view. This paper numerically investigates the micro-cracking behavior of Bukit Timah granite by using a grain-based modeling approach. First, the principles of grain-based model adopted in the two-dimensional Particle Flow Code and the numerical model generation procedure are reviewed. The micro-parameters of the numerical model are then calibrated to match the macro-properties of the rock obtained from tension and compression tests in the laboratory. The simulated rock properties are in good agreement with the laboratory test results with the errors less than ±6%. Finally, the calibrated model is used to study the micro-cracking behavior and the failure modes of the rock under direct tension and under compression with different confining pressures. The results reveal that when the numerical model is loaded in direct tension, only grain boundary tensile cracks are generated, and the simulated macroscopic fracture agrees well with the results obtained in laboratory tests. When the model is loaded in compression, the ratio of grain boundary tensile cracks to grain boundary shear cracks decreases with the increase in confining pressure. In other words, the results show that as the confining pressure increases, the failure mechanism changes from tension to shear. The simulated failure mode of the model changes from splitting to shear as the applied confining pressure gradually increases, which is comparable with that observed in laboratory tests. The grain-based model used in this study thus appears promising for further investigation of microscopic and macroscopic behavior of crystalline rocks under different loading conditions.

Prediction of Flow Stress in Cadmium Using Constitutive Equation and Artificial Neural Network Approach

NASA Astrophysics Data System (ADS)

Sarkar, A.; Chakravartty, J. K.

2013-10-01

A model is developed to predict the constitutive flow behavior of cadmium during compression test using artificial neural network (ANN). The inputs of the neural network are strain, strain rate, and temperature, whereas flow stress is the output. Experimental data obtained from compression tests in the temperature range -30 to 70 °C, strain range 0.1 to 0.6, and strain rate range 10-3 to 1 s-1 are employed to develop the model. A three-layer feed-forward ANN is trained with Levenberg-Marquardt training algorithm. It has been shown that the developed ANN model can efficiently and accurately predict the deformation behavior of cadmium. This trained network could predict the flow stress better than a constitutive equation of the type.

High Cycle Fatigue (HCF) Science and Technology Program 2000 Annual Report

DTIC Science & Technology

2000-01-01

in an area of deep compressive stress. • Results of industry and government testing have indicated the ability to stop crack initiation and...fatigue crack nucleation process with the cyclic deformation behavior of the alloy for different microstructures and crystallographic texture ... texture combinations investigated, bimodal fine uni-rolled and lamellar cross-rolled displayed superior fatigue properties to the remaining four

Modeling the Effect of Glass Microballoon (GMB) Volume Fraction on Behavior of Sylgard/GMB Composites.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Brown, Judith Alice; Long, Kevin Nicholas

2017-05-01

This work was done to support customer questions about whether a Sylgard/Glass Microballoon (GMB) potting material in current use could be replaced with pure Sylgard and if this would significantly change stresses imparted to internal components under thermal cycling conditions. To address these questions, we provide micromechanics analysis of Sylgard/GMB materials using both analytic composite theory and finite element simulations to better understand the role of the GMB volume fraction in determining thermal expansion coefficient, elastic constants, and behavior in both confined and unconfined compression boundary value problems. A key finding is that damage accumulation in the material from breakagemore » of GMBs significantly limits the global stress magnitude and results in a plateau stress behavior over large ranges of compressive strain. The magnitude of this plateau stress is reduced with higher volume fractions of GMBs. This effect is particularly pronounced in confined compression, which we estimate bears the most similarity to the application of interest. This stress-limiting damage mechanism is not present in pure Sylgard, however, and the result is much higher stresses under confined compression. Thus, we recommend that some volume fraction greater than 10% GMBs be used for confined deformation applications.« less

Hot deformation behavior of uniform fine-grained GH4720Li alloy based on its processing map

NASA Astrophysics Data System (ADS)

Yu, Qiu-ying; Yao, Zhi-hao; Dong, Jian-xin

2016-01-01

The hot deformation behavior of uniform fine-grained GH4720Li alloy was studied in the temperature range from 1040 to 1130°C and the strain-rate range from 0.005 to 0.5 s-1 using hot compression testing. Processing maps were constructed on the basis of compression data and a dynamic materials model. Considerable flow softening associated with superplasticity was observed at strain rates of 0.01 s-1 or lower. According to the processing map and observations of the microstructure, the uniform fine-grained microstructure remains intact at 1100°C or lower because of easily activated dynamic recrystallization (DRX), whereas obvious grain growth is observed at 1130°C. Metallurgical instabilities in the form of non-uniform microstructures under higher and lower Zener-Hollomon parameters are induced by local plastic flow and primary γ' local faster dissolution, respectively. The optimum processing conditions at all of the investigated strains are proposed as 1090-1130°C with 0.08-0.5 s-1 and 0.005-0.008 s-1 and 1040-1085°C with 0.005-0.06 s-1.

Transmission Electron Microscope In Situ Straining Technique to Directly Observe Defects and Interfaces During Deformation in Magnesium

DOE PAGES

Morrow, Benjamin M.; Cerreta, E. K.; McCabe, R. J.; ...

2015-05-14

In-situ straining was used to study deformation behavior of hexagonal close-packed (hcp) metals.Twinning and dislocation motion, both essential to plasticity in hcp materials, were observed.Typically, these processes are characterized post-mortem by examining remnant microstructural features after straining has occurred. By imposing deformation during imaging, direct observation of active deformation mechanisms is possible. This work focuses on straining of structural metals in a transmission electron microscope (TEM), and a recently developed technique that utilizes familiar procedures and equipment to increase ease of experiments. In-situ straining in a TEM presents several advantages over conventional post-mortem characterization, most notably time-resolution of deformation andmore » streamlined identification of active deformation mechanisms. Drawbacks to the technique and applicability to other studies are also addressed. In-situ straining is used to study twin boundary motion in hcp magnesium. A {101¯2} twin was observed during tensile and compressive loading. Twin-dislocation interactions are directly observed. Notably, dislocations are observed to remain mobile, even after multiple interactions with twin boundaries, a result which suggests that Basinki’s dislocation transformation mechanism by twinning is not present in hcp metals. The coupling of in-situ straining with traditional post-mortem characterization yields more detailed information about material behavior during deformation than either technique alone.« less

Drop Weight Impact Behavior of Al-Si-Cu Alloy Foam-Filled Thin-Walled Steel Pipe Fabricated by Friction Stir Back Extrusion

NASA Astrophysics Data System (ADS)

Hangai, Yoshihiko; Nakano, Yukiko; Utsunomiya, Takao; Kuwazuru, Osamu; Yoshikawa, Nobuhiro

2017-02-01

In this study, Al-Si-Cu alloy ADC12 foam-filled thin-walled stainless steel pipes, which exhibit metal bonding between the ADC12 foam and steel pipe, were fabricated by friction stir back extrusion. Drop weight impact tests were conducted to investigate the deformation behavior and mechanical properties of the foam-filled pipes during dynamic compression tests, which were compared with the results of static compression tests. From x-ray computed tomography observation, it was confirmed that the fabricated foam-filled pipes had almost uniform porosity and pore size distributions. It was found that no scattering of the fragments of collapsed ADC12 foam occurred for the foam-filled pipes owing to the existence of the pipe surrounding the ADC12 foam. Preventing the scattering of the ADC12 foam decreases the drop in stress during dynamic compression tests and therefore improves the energy absorption properties of the foam.

Effects of transverse shear deformation on buckling of laminated cylinders as a function of thickness and ply orientation

NASA Technical Reports Server (NTRS)

Jegley, Dawn C.

1987-01-01

Buckling loads of thick-walled, orthotropic, simply-supported right circular cylinders are predicted using a new higher-order transverse shear deformation theory. The higher-order theory shows that, by more accurately accounting for transverse shear deformation effects, the predicted buckling load may be reduced by as much as 80 percent compared to predictions based on conventional transverse shear deformation theory. A parametric study of the effect of ply orientation on the buckling load of axially compressed cylinders indicates that laminates containing 0 deg plies are the most sensitive to transverse shear deformation effects. Interaction curves for buckling of cylinders with axial compressive and external pressure loadings indicate that buckling loads due to external pressure loadings are much less sensitive to transverse shear deformation effects than those due to axial compressive loadings.

Bifurcation and response analysis of a nonlinear flexible rotating disc immersed in bounded compressible fluid

NASA Astrophysics Data System (ADS)

Remigius, W. Dheelibun; Sarkar, Sunetra; Gupta, Sayan

2017-03-01

Use of heavy gases in centrifugal compressors for enhanced oil extraction have made the impellers susceptible to failures through acousto-elastic instabilities. This study focusses on understanding the dynamical behavior of such systems by considering the effects of the bounded fluid housed in a casing on a rotating disc. First, a mathematical model is developed that incorporates the interaction between the rotating impeller - modelled as a flexible disc - and the bounded compressible fluid medium in which it is immersed. The nonlinear effects arising due to large deformations of the disc have been included in the formulation so as to capture the post flutter behavior. A bifurcation analysis is carried out with the disc rotational speed as the bifurcation parameter to investigate the dynamical behavior of the coupled system and estimate the stability boundaries. Parametric studies reveal that the relative strengths of the various dissipation mechanisms in the coupled system play a significant role that affect the bifurcation route and the post flutter behavior in the acousto-elastic system.

The effect of various deformation processes on the corrosion behavior of casing and tubing carbon steels in sweet environment

NASA Astrophysics Data System (ADS)

Elramady, Alyaa Gamal

The aim of this research project is to correlate the plastic deformation and mechanical instability of casing steel materials with corrosion behavior and surface change, in order to identify a tolerable degree of deformation for casing steel materials. While the corrosion of pipeline and casing steels has been investigated extensively, corrosion of these steels in sweet environments with respect to plastic deformation due to bending, rolling, autofrettage, or handling needs more investigation. Downhole tubular expansion of pipes (casings) is becoming standard practice in the petroleum industry to repair damaged casings, shutdown perforations, and ultimately achieve mono-diameter wells. Tubular expansion is a cold-drawing metal forming process, which consists of running conical mandrels through casings either mechanically using a piston or hydraulically by applying a back pressure. This mechanism subjects the pipes to large radial plastic deformations of up to 30 pct. of the inner diameter. It is known that cold-working is a way of strengthening materials such as low carbon steel, but given that this material will be subjected to corrosive environments, susceptibility to stress corrosion cracking (SCC) should be investigated. This research studies the effect of cold-work, in the form of cold-rolling and cold-expansion, on the surface behavior of API 5CT steels when it is exposed to a CO2-containing environment. Cold-work has a pronounced influence on the corrosion behavior of both API 5CT K55 and P110 grade steels. The lowest strength grade steel, API 5CT K55, performed poorly in a corrosive environment in the slow strain rate test. The ductile material exhibited the highest loss in strength and highest susceptibility to stress corrosion cracking in a CO 2-containing environment. The loss in strength declined with cold-rolling, which can be ascribed to the surface compressive stresses induced by cold-work. On the other hand, API 5CT P110 grade steels showed higher susceptibility to SCC when they were cold-rolled and cold-expanded. The research found that surface compressive stresses have an effect on the SCC behavior of casing and tubing steels. The CO2 corrosion behavior and atomic processes at the corroding interface were investigated at laboratory temperature using electrochemical techniques. Cold-work was found to have an influence on the corrosion behavior of both API 5CT K55 and P110 grade steels. These behaviors were found to be material and process dependent. Surface evaluation techniques such as field emission scanning electron microscope (FE-SEM) and X-ray diffraction (XRD) analysis did not detect formation of a protective scale. X-ray diffraction and X-ray photoelectron spectroscopy (XPS) analysis both detected the appearance of a scale that was traced back to magnetite.

The Compressive Behavior of Isocyanate-crosslinked Silica Aerogel at High Strain Rates

NASA Technical Reports Server (NTRS)

Luo, H.; Lu, H.; Leventis, N.

2006-01-01

Aerogels are low-density, highly nano-porous materials. Their engineering applications are limited due to their brittleness and hydrophilicity. Recently, a strong lightweight crosslinked silica aerogel has been developed by encapsulating the skeletal framework of amine-modified silica aerogels with polyureas derived by isocyanate. The mesoporous structure of the underlying silica framework is preserved through conformal polymer coating, and the thermal conductivity remains low. Characterization has been conducted on the thermal, physical properties and the mechanical properties under quasi-static loading conditions. In this paper, we present results on the dynamic compressive behavior of the crosslinked silica aerogel (CSA) using a split Hopkinson pressure bar (SHPB). A new tubing pulse shaper was employed to help reach the dynamic stress equilibrium and constant strain rate. The stress-strain relationship was determined at high strain rates within 114-4386/s. The effects of strain rate, density, specimen thickness and water absorption on the dynamic behavior of the CSA were investigated through a series of dynamic experiments. The Young's moduli (or 0.2% offset compressive yield strengths) at a strain rate approx.350/s were determined as 10.96/2.08, 159.5/6.75, 192.2/7.68, 304.6/11.46, 407.0/20.91 and 640.5/30.47 MPa for CSA with densities 0.205, 0.454, 0.492, 0.551,0.628 and 0.731 g/cu cm, respectively. The deformation and failure behaviors of a native silica aerogel with density (0.472 g/cu cm ), approximately the same as a typical CSA sample were observed with a high speed digital camera. Digital image correlation technique was used to determine the surface strains through a series of images acquired using high speed photography. The relative uniform axial deformation indicated that localized compaction did not occur at a compressive strain level of approx.17%, suggesting most likely failure mechanism at high strain rate to be different from that under quasi-static loading condition. The Poisson s ratio was determined to be 0.162 in nonlinear regime under high strain rates. CSA samples failed generally by splitting, but were much more ductile than native silica aerogels.

An experimental study on fracture mechanical behavior of rock-like materials containing two unparallel fissures under uniaxial compression

NASA Astrophysics Data System (ADS)

Huang, Yan-Hua; Yang, Sheng-Qi; Tian, Wen-Ling; Zeng, Wei; Yu, Li-Yuan

2016-06-01

Strength and deformability characteristics of rock with pre-existing fissures are governed by cracking behavior. To further research the effects of pre-existing fissures on the mechanical properties and crack coalescence process, a series of uniaxial compression tests were carried out for rock-like material with two unparallel fissures. In the present study, cement, quartz sand, and water were used to fabricate a kind of brittle rock-like material cylindrical model specimen. The mechanical properties of rock-like material specimen used in this research were all in good agreement with the brittle rock materials. Two unparallel fissures (a horizontal fissure and an inclined fissure) were created by inserting steel during molding the model specimen. Then all the pre-fissured rock-like specimens were tested under uniaxial compression by a rock mechanics servo-controlled testing system. The peak strength and Young's modulus of pre-fissured specimen all first decreased and then increased when the fissure angle increased from 0° to 75°. In order to investigate the crack initiation, propagation and coalescence process, photographic monitoring was adopted to capture images during the entire deformation process. Moreover, acoustic emission (AE) monitoring technique was also used to obtain the AE evolution characteristic of pre-fissured specimen. The relationship between axial stress, AE events, and the crack coalescence process was set up: when a new crack was initiated or a crack coalescence occurred, the corresponding axial stress dropped in the axial stress-time curve and a big AE event could be observed simultaneously. Finally, the mechanism of crack propagation under microscopic observation was discussed. These experimental results are expected to increase the understanding of the strength failure behavior and the cracking mechanism of rock containing unparallel fissures.

Effect of Aging Treatment on the Compressibility and Recovery of NiTi Shape Memory Alloys as Static Seals

NASA Astrophysics Data System (ADS)

Lu, Xiaofeng; Li, Gang; Liu, Luwei; Zhu, Xiaolei; Tu, Shan-Tung

2017-07-01

The improvement of the compressibility and recovery of the gaskets can decrease the leakage occurrence in bolted flange connections. In this study, the effect of aging treatment on the compressibility and recovery of NiTi shape memory alloys is investigated as static seals together with thermal analysis. The experimental results indicate that different phase transformations of NiTi alloys are exhibited in the DSC curves during aging treatment. The recovery coefficient of NiTi alloys aged at 500 °C for 2 h is quite low accompanied with a large residual strain. With increasing aging time at the aging temperature of 400 °C, the residual strain and area of hysteresis loop of NiTi alloys are both increased, whereas the recovery coefficient is decreased. Since the deformation associates the phase transformation behavior, aging treatment could improve the compressibility and recovery of NiTi alloys as static seals.

Buckling Behavior of Compression-Loaded Composite Cylindrical Shells with Reinforced Cutouts

NASA Technical Reports Server (NTRS)

Hilburger, Mark W.; Starnes, James H., Jr.

2002-01-01

Results from a numerical study of the response of thin-wall compression-loaded quasi-isotropic laminated composite cylindrical shells with reinforced and unreinforced square cutouts are presented. The effects of cutout reinforcement orthotropy, size, and thickness on the nonlinear response of the shells are described. A high-fidelity nonlinear analysis procedure has been used to predict the nonlinear response of the shells. The analysis procedure includes a nonlinear static analysis that predicts stable response characteristics of the shells and a nonlinear transient analysis that predicts unstable dynamic buckling response characteristics. The results illustrate how a compression-loaded shell with an unreinforced cutout can exhibit a complex nonlinear response. In particular, a local buckling response occurs in the shell near the cutout and is caused by a complex nonlinear coupling between local shell-wall deformations and in-plane destabilizing compression stresses near the cutout. In general, the addition of reinforcement around a cutout in a compression-loaded shell can retard or eliminate the local buckling response near the cutout and increase the buckling load of the shell, as expected. However, results are presented that show how certain reinforcement configurations can actually cause an unexpected increase in the magnitude of local deformations and stresses in the shell and cause a reduction in the buckling load. Specific cases are presented that suggest that the orthotropy, thickness, and size of a cutout reinforcement in a shell can be tailored to achieve improved response characteristics.

High Strain Rate Deformation Modeling of a Polymer Matrix Composite. Part 1; Matrix Constitutive Equations

NASA Technical Reports Server (NTRS)

Goldberg, Robert K.; Stouffer, Donald C.

1998-01-01

Recently applications have exposed polymer matrix composite materials to very high strain rate loading conditions, requiring an ability to understand and predict the material behavior under these extreme conditions. In this first paper of a two part report, background information is presented, along with the constitutive equations which will be used to model the rate dependent nonlinear deformation response of the polymer matrix. Strain rate dependent inelastic constitutive models which were originally developed to model the viscoplastic deformation of metals have been adapted to model the nonlinear viscoelastic deformation of polymers. The modified equations were correlated by analyzing the tensile/ compressive response of both 977-2 toughened epoxy matrix and PEEK thermoplastic matrix over a variety of strain rates. For the cases examined, the modified constitutive equations appear to do an adequate job of modeling the polymer deformation response. A second follow-up paper will describe the implementation of the polymer deformation model into a composite micromechanical model, to allow for the modeling of the nonlinear, rate dependent deformation response of polymer matrix composites.

Liquid Between Macromolecules in Protein Crystals: Static Versus Dynamics

NASA Technical Reports Server (NTRS)

Chernov, A. A.

2005-01-01

Protein crystals are so fragile that they often can not be handled by tweezers. Indeed, measurements of the Young modulus, E, of lysozyme crystals resulted in E approx. equals 0.1 - 1 GPa, the lower figures, 0.1 - 0.5 GPa, being obtained from triple point bending of as-grown and not cross-linked crystals sitting in solution. The bending strength was found to be approx.10(exp -2) E. On the other hand, ultrasound speed and Mandelstam-Raman-Brilloin light scattering experiments led to much higher figures, E approx. equals 2.7 GPa. The lower figures for E were found from static or low frequency crystal deformations measurements, while the higher moduli are based on high frequency lattice vibrations, 10(exp 7) - 10(exp 10) 1/s. The physical reason for the about an order of magnitude discrepancy is in different behavior of water filling space between protein molecules. At slow lattice deformation, the not-bound intermolecular water has enough time to flow from the compressed to expanded regions of the deformed crystal. At high deformation frequencies in the ultra- and hypersound waves, the water is confined in the intermolecular space and, on that scale, behaves like a solid, thus contributing to the elastic crystal moduli. In this case, the reciprocal crystal modulus is expected to be an average of the water protein and water compressibilities (reciprocal compressibilities): the bulk modulus for lysozyme is 26 GPa, for water it is 7 GPa. Anisotropy of the crystal moduli comes from intermolecular contacts within the lattice while the high frequency hardness comes from the bulk of protein molecules and water bulk moduli. These conclusions are based on the analysis of liquid flow in porous medium to be presented.

3D printed hierarchical honeycombs with shape integrity under large compressive deformations

DOE PAGES

Chen, Yanyu; Li, Tiantian; Jia, Zian; ...

2017-10-12

Here, we describe the in-plane compressive performance of a new type of hierarchical cellular structure created by replacing cell walls in regular honeycombs with triangular lattice configurations. The fabrication of this relatively complex material architecture with size features spanning from micrometer to centimeter is facilitated by the availability of commercial 3D printers. We apply to these hierarchical honeycombs a thermal treatment that facilitates the shape preservation and structural integrity of the structures under large compressive loading. The proposed hierarchical honeycombs exhibit a progressive failure mode, along with improved stiffness and energy absorption under uniaxial compression. High energy dissipation and shapemore » integrity at large imposed strains (up to 60%) have also been observed in these hierarchical honeycombs under cyclic loading. Experimental and numerical studies suggest that these anomalous mechanical behaviors are attributed to the introduction of a structural hierarchy, intrinsically controlled by the cell wall slenderness of the triangular lattice and by the shape memory effect induced by the thermal and mechanical compressive treatment.« less

3D printed hierarchical honeycombs with shape integrity under large compressive deformations

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chen, Yanyu; Li, Tiantian; Jia, Zian

Here, we describe the in-plane compressive performance of a new type of hierarchical cellular structure created by replacing cell walls in regular honeycombs with triangular lattice configurations. The fabrication of this relatively complex material architecture with size features spanning from micrometer to centimeter is facilitated by the availability of commercial 3D printers. We apply to these hierarchical honeycombs a thermal treatment that facilitates the shape preservation and structural integrity of the structures under large compressive loading. The proposed hierarchical honeycombs exhibit a progressive failure mode, along with improved stiffness and energy absorption under uniaxial compression. High energy dissipation and shapemore » integrity at large imposed strains (up to 60%) have also been observed in these hierarchical honeycombs under cyclic loading. Experimental and numerical studies suggest that these anomalous mechanical behaviors are attributed to the introduction of a structural hierarchy, intrinsically controlled by the cell wall slenderness of the triangular lattice and by the shape memory effect induced by the thermal and mechanical compressive treatment.« less

A knitted glove sensing system with compression strain for finger movements

NASA Astrophysics Data System (ADS)

Ryu, Hochung; Park, Sangki; Park, Jong-Jin; Bae, Jihyun

2018-05-01

Development of a fabric structure strain sensor has received considerable attention due to its broad application in healthcare monitoring and human–machine interfaces. In the knitted textile structure, it is critical to understand the surface structural deformation from a different body motion, inducing the electrical signal characteristics. Here, we report the electromechanical properties of the knitted glove sensing system focusing on the compressive strain behavior. Compared with the electrical response of the tensile strain, the compressive strain shows much higher sensitivity, stability, and linearity via different finger motions. Additionally, the sensor exhibits constant electrical properties after repeated cyclic tests and washing processes. The proposed knitted glove sensing system can be readily extended to a scalable and cost-effective production due to the use of a commercialized manufacturing system.

Mechanical properties of fullerite of various composition

NASA Astrophysics Data System (ADS)

Rysaeva, L. Kh.

2017-12-01

Molecular dynamics simulation is used to study the structures of fullerite of various composition as well as their mechanical properties. Fullerites based on fullerene C60 with simple cubic and face-centered packing, fullerene-like molecule C48 and fullerene C240 with simple cubic packing are studied. Compliance and stiffness coefficients are calculated for fullerites C60 and C48. For fullerite C240, C60, and C48, deformation behavior under the effect of hydrostatic compression is also investigated. It is shown that the fullerenes in the fullerite remain almost spherical up to high values of compressive strain, as a result of which the fullerite is an elastic medium up to densities of 2.5 g/cm3. The increasing stiffness and strength under an applied compression is found for all the considered fullerites.

Microstructure, strengthening mechanisms and hot deformation behavior of an oxide-dispersion strengthened UFG Al6063 alloy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Asgharzadeh, H.; Kim, H.S.; Simchi, A., E-mail: simchi@sharif.edu

2013-01-15

An ultrafine-grained Al6063/Al{sub 2}O{sub 3} (0.8 vol.%, 25 nm) nanocomposite was prepared via powder metallurgy route through reactive mechanical alloying and hot powder extrusion. Scanning electron microcopy, transmission electron microscopy, and back scattered electron diffraction analysis showed that the grain structure of the nanocomposite is trimodal and composed of nano-size grains (< 0.1 {mu}m), ultrafine grains (0.1-1 {mu}m), and micron-size grains (> 1 {mu}m) with random orientations. Evaluation of the mechanical properties of the nanocomposite based on the strengthening-mechanism models revealed that the yield strength of the ultrafine-grained nanocomposite is mainly controlled by the high-angle grain boundaries rather than nanometricmore » alumina particles. Hot deformation behavior of the material at different temperatures and strain rates was studied by compression test and compared to coarse-grained Al6063 alloy. The activation energy of the hot deformation process for the nanocomposite was determined to be 291 kJ mol{sup -1}, which is about 64% higher than that of the coarse-grained alloy. Detailed microstructural analysis revealed that dynamic recrystallization is responsible for the observed deformation softening in the ultrafine-grained nanocomposite. - Highlights: Black-Right-Pointing-Pointer The strengthening mechanisms of Al6063/Al{sub 2}O{sub 3} nanocomposite were evaluated. Black-Right-Pointing-Pointer Hot deformation behavior of the nanocomposite was studied. Black-Right-Pointing-Pointer The hot deformation activation energy was determined using consecutive models. Black-Right-Pointing-Pointer The restoration mechanisms and microstructural changes are presented.« less

Comment on 'volume of magma accumulation or withdrawal estimated from surface uplift or subsidence, with application to the 1960 collapse of Kilauea volcano' by P.T. Delaney and D.F. McTigue

USGS Publications Warehouse

Johnson, Daniel J.; Sigmundsson, F.; Delaney, P.T.

2000-01-01

In volcanoes that store a significant quantity of magma within a subsurface summit reservoir, such as Kilauea, bulk compression of stored magma is an important mode of deformation. Accumulation of magma is also accompanied by crustal deformation, usually manifested at the surface as uplift. These two modes of deformation - bulk compression of resident magma and deformation of the volcanic edifice - act in concert to accommodate the volume of newly added magma. During deflation, the processes reverse and reservoir magma undergoes bulk decompression, the chamber contracts, and the ground surface subsides. Because magma compression plays a role in creating subsurface volume of accommodate magma, magma budget estimates that are derived from surface uplift observations without consideration of magma compression will underestimate actual magma volume changes.

Ion transport restriction in mechanically strained separator membranes

NASA Astrophysics Data System (ADS)

Cannarella, John; Arnold, Craig B.

2013-03-01

We use AC impedance methods to investigate the effect of mechanical deformation on ion transport in commercial separator membranes and lithium-ion cells as a whole. A Bruggeman type power law relationship is found to provide an accurate correlation between porosity and tortuosity of deformed separators, which allows the impedance of a separator membrane to be predicted as a function of deformation. By using mechanical compression to vary the porosity of the separator membranes during impedance measurements it is possible to determine both the α and γ parameters from the modified Bruggeman relation for individual separator membranes. From impedance testing of compressed pouch cells it is found that separator deformation accounts for the majority of the transport restrictions arising from compressive stress in a lithium-ion cell. Finally, a charge state dependent increase in the impedance associated with charge transfer is observed with increasing cell compression.

Analysis of Deformation and Equivalent Stress during Biomass Material Compression Molding

NASA Astrophysics Data System (ADS)

Xu, Guiying; Wei, Hetao; Zhang, Zhien; Yu, Shaohui; Wang, Congzhe; Huang, Guowen

2018-02-01

Ansys is adopted to analyze mold deformation and stress field distribution rule during the process of compressing biomass under pressure of 20Mpa. By means of unit selection, material property setting, mesh partition, contact pair establishment, load and constraint applying, and solver setting, the stress and strain of overall mold are analyzed. Deformation and equivalent Stress of compression structure, base, mold, and compression bar were analyzed. We can have conclusions: The distribution of stress forced on compressor is not completely uniform, where the stress at base is slightly decreased; the stress and strain of compression bar is the largest, and stress concentration my occur at top of compression bar, which goes against compression bar service life; the overall deformation of main mold is smaller; although there is slight difference between upper and lower part, the overall variation is not obvious, but the stress difference between upper and lower part of main mold is extremely large so that reaches to 10 times; the stress and strain in base decrease in circular shape, but there is still stress concentration in ledge, which goes against service life; contact stress does not distribute uniformly, there is increasing or decreasing trend in adjacent parts, which is very large in some parts. in constructing both.

The Effect of Simulated Thermomechanical Processing on the Transformation Behavior and Microstructure of a Low-Carbon Mo-Nb Linepipe Steel

NASA Astrophysics Data System (ADS)

Cizek, P.; Wynne, B. P.; Davies, C. H. J.; Hodgson, P. D.

2015-01-01

The present work investigates the transformation behavior of a low-carbon Mo-Nb linepipe steel and the corresponding transformation product microstructures using deformation dilatometry. The continuous cooling transformation (CCT) diagrams have been constructed for both the fully recrystallized austenite and that deformed in uniaxial compression at 1148 K (875 °C) to a strain of 0.5 for cooling rates ranging from 0.1 to about 100 K/s. The obtained microstructures have been studied in detail using electron backscattered diffraction complemented by transmission electron microscopy. Heavy deformation of the parent austenite has caused a significant expansion of the polygonal ferrite transformation field in the CCT diagram, as well as a shift in the non-equilibrium ferrite transformation fields toward higher cooling rates. Furthermore, the austenite deformation has resulted in a pronounced refinement in both the effective grain (sheaf/packet) size and substructure unit size of the non-equilibrium ferrite microstructures. The optimum microstructure expected to display an excellent balance between strength and toughness is a mix of quasi-polygonal ferrite and granular bainite (often termed "acicular ferrite") produced from the heavily deformed austenite within a processing window covering the cooling rates from about 10 to about 100 K/s.

Fracture behaviors under pure shear loading in bulk metallic glasses

NASA Astrophysics Data System (ADS)

Chen, Cen; Gao, Meng; Wang, Chao; Wang, Wei-Hua; Wang, Tzu-Chiang

2016-12-01

Pure shear fracture test, as a special mechanical means, had been carried out extensively to obtain the critical information for traditional metallic crystalline materials and rocks, such as the intrinsic deformation behavior and fracture mechanism. However, for bulk metallic glasses (BMGs), the pure shear fracture behaviors have not been investigated systematically due to the lack of a suitable test method. Here, we specially introduce a unique antisymmetrical four-point bend shear test method to realize a uniform pure shear stress field and study the pure shear fracture behaviors of two kinds of BMGs, Zr-based and La-based BMGs. All kinds of fracture behaviors, the pure shear fracture strength, fracture angle and fracture surface morphology, are systematically analyzed and compared with those of the conventional compressive and tensile fracture. Our results indicate that both the Zr-based and La-based BMGs follow the same fracture mechanism under pure shear loading, which is significantly different from the situation of some previous research results. Our results might offer new enlightenment on the intrinsic deformation and fracture mechanism of BMGs and other amorphous materials.

Fracture behaviors under pure shear loading in bulk metallic glasses.

PubMed

Chen, Cen; Gao, Meng; Wang, Chao; Wang, Wei-Hua; Wang, Tzu-Chiang

2016-12-23

Pure shear fracture test, as a special mechanical means, had been carried out extensively to obtain the critical information for traditional metallic crystalline materials and rocks, such as the intrinsic deformation behavior and fracture mechanism. However, for bulk metallic glasses (BMGs), the pure shear fracture behaviors have not been investigated systematically due to the lack of a suitable test method. Here, we specially introduce a unique antisymmetrical four-point bend shear test method to realize a uniform pure shear stress field and study the pure shear fracture behaviors of two kinds of BMGs, Zr-based and La-based BMGs. All kinds of fracture behaviors, the pure shear fracture strength, fracture angle and fracture surface morphology, are systematically analyzed and compared with those of the conventional compressive and tensile fracture. Our results indicate that both the Zr-based and La-based BMGs follow the same fracture mechanism under pure shear loading, which is significantly different from the situation of some previous research results. Our results might offer new enlightenment on the intrinsic deformation and fracture mechanism of BMGs and other amorphous materials.

Research on the deformation and failure evolution of sandstone under triaxial compression based on PFC2D

NASA Astrophysics Data System (ADS)

Yang, X. B.; Han, X. X.; Zhou, T. B.; Liu, E. L.

2017-04-01

Through the comparative analysis of the results of the triaxial compression experiments of sandstone and the numerical simulation results of particle flow code PFC2D under the same conditions, the typical simulation curve and the corresponding simulation process were selected to analyze the evolution characteristics of the surface deformation field, the evolution characteristics of the velocity field and displacement field of the deformation localization bands of sandstone under triaxial compression. Research results show that the changes of the velocities and displacements of deformation localization bands corresponds to the change of stress during compression; In the same deformation localization band, the dislocation velocities are always in the same direction, but in the direction vertical to the localization band, the localization band sometimes squeezes and sometimes stretches; At different positions of the same deformation localization band, the dislocation velocities and extrusion velocities are both different at the same time; In the post-peak stage of loading, along the same deformation localization band, the dislocation displacements close to both loaded ends are generally greater than the ones near to the middle position of the specimen, the stretching displacements close to both loaded ends are generally smaller than the ones near to the middle position of the specimen.

Mechanochromic behavior of a luminescent silicone rubber under tensile deformation

NASA Astrophysics Data System (ADS)

Kim, Yeon Ju; Lee, Sang Hwan; Jeong, Kwang-Un; Nah, Changwoon

2016-09-01

A novel mechanochromic elastomer based on silicone rubber and coumarin 6 dye have been prepared with various concentrations of the dye ranges from 2wt.% to a maximum of 5wt.% by solution mixing technique. After evaporating the solvent, cured samples were prepared as thin films using compression molding at 170° C. The optimum composition of the dye in rubber composites was determined based on the mechanochromic performance characterized with ultraviolet/visible (UV/Vis) spectrometer, x-ray diffraction (XRD) and spectrofluorometer (FL). The UV/Vis spectrometer monitors the dye aggregation in polymer film during the tensile deformation. The XRD monitors the change in size of dye aggregates. The FL monitors the optical response during tensile deformation due to the re-arrangement of dyes. As increasing a mechanical deformation to the polymeric composite film, UV/Vis absorption intensity was decreased and the FL emission wavelength was moved to decrease wavelength because of breaking dye aggregations. Also, XRD intensity peak was decreased, which dye aggregations were broken after mechanical deformation.

Triaxial testing system for pressure core analysis using image processing technique

NASA Astrophysics Data System (ADS)

Yoneda, J.; Masui, A.; Tenma, N.; Nagao, J.

2013-11-01

In this study, a newly developed innovative triaxial testing system to investigate strength, deformation behavior, and/or permeability of gas hydrate bearing-sediments in deep sea is described. Transport of the pressure core from the storage chamber to the interior of the sealing sleeve of a triaxial cell without depressurization was achieved. An image processing technique was used to capture the motion and local deformation of a specimen in a transparent acrylic triaxial pressure cell and digital photographs were obtained at each strain level during the compression test. The material strength was successfully measured and the failure mode was evaluated under high confining and pore water pressures.

Fluid-Driven Deformation of a Soft Granular Material

NASA Astrophysics Data System (ADS)

MacMinn, Christopher W.; Dufresne, Eric R.; Wettlaufer, John S.

2015-01-01

Compressing a porous, fluid-filled material drives the interstitial fluid out of the pore space, as when squeezing water out of a kitchen sponge. Inversely, injecting fluid into a porous material can deform the solid structure, as when fracturing a shale for natural gas recovery. These poromechanical interactions play an important role in geological and biological systems across a wide range of scales, from the propagation of magma through Earth's mantle to the transport of fluid through living cells and tissues. The theory of poroelasticity has been largely successful in modeling poromechanical behavior in relatively simple systems, but this continuum theory is fundamentally limited by our understanding of the pore-scale interactions between the fluid and the solid, and these problems are notoriously difficult to study in a laboratory setting. Here, we present a high-resolution measurement of injection-driven poromechanical deformation in a system with granular microsctructure: We inject fluid into a dense, confined monolayer of soft particles and use particle tracking to reveal the dynamics of the multiscale deformation field. We find that a continuum model based on poroelasticity theory captures certain macroscopic features of the deformation, but the particle-scale deformation field exhibits dramatic departures from smooth, continuum behavior. We observe particle-scale rearrangement and hysteresis, as well as petal-like mesoscale structures that are connected to material failure through spiral shear banding.

Acoustic Behavior of Subfloor Lightweight Mortars Containing Micronized Poly (Ethylene Vinyl Acetate) (EVA).

PubMed

Brancher, Luiza R; Nunes, Maria Fernanda de O; Grisa, Ana Maria C; Pagnussat, Daniel T; Zeni, Mára

2016-01-15

This paper aims to contribute to acoustical comfort in buildings by presenting a study about the polymer waste micronized poly (ethylene vinyl acetate) (EVA) to be used in mortars for impact sound insulation in subfloor systems. The evaluation method included physical, mechanical and morphological properties of the mortar developed with three distinct thicknesses designs (3, 5, and 7 cm) with replacement percentage of the natural aggregate by 10%, 25%, and 50% EVA. Microscopy analysis showed the surface deposition of cement on EVA, with preservation of polymer porosity. The compressive creep test estimated long-term deformation, where the 10% EVA sample with a 7 cm thick mortar showed the lowest percentage deformation of its height. The impact noise test was performed with 50% EVA samples, reaching an impact sound insulation of 23 dB when the uncovered slab was compared with the 7 cm thick subfloor mortar. Polymer waste addition decreased the mortar compressive strength, and EVA displayed characteristics of an influential material to intensify other features of the composite.

Deformation and failure mechanism of secondary cell wall in Spruce late wood

NASA Astrophysics Data System (ADS)

Adusumalli, Ramesh-Babu; Raghavan, Rejin; Ghisleni, Rudy; Zimmermann, Tanja; Michler, Johann

2010-08-01

The deformation and failure of the secondary cell wall of Spruce wood was studied by in-situ SEM compression of micropillars machined by the focused ion beam technique. The cell wall exhibited yield strength values of approximately 160 MPa and large scale plasticity. High resolution SEM imaging post compression revealed bulging of the pillars followed by shear failure. With additional aid of cross-sectional analysis of the micropillars post compression, a model for deformation and failure mechanism of the cell wall has been proposed. The cell wall consists of oriented cellulose microfibrils with high aspect ratio embedded in a hemicellulose-lignin matrix. The deformation of the secondary wall occurs by asymmetric out of plane bulging because of buckling of the microfibrils. Failure of the cell wall following the deformation occurs by the formation of a shear or kink band.

Compression behavior of delaminated composite plates

NASA Technical Reports Server (NTRS)

Peck, Scott O.; Springer, George S.

1989-01-01

The response of delaminated composite plates to compressive in-plane loads was investigated. The delaminated region may be either circular or elliptical, and may be located between any two plies of the laminate. For elliptical delaminations, the axes of the ellipse may be arbitrarily oriented with respect to the applied loads. A model was developed that describes the stresses, strains, and deformation of the sublaminate created by the delamination. The mathematical model is based on a two dimensional nonlinear plate theory that includes the effects of transverse shear deformation. The model takes into account thermal and moisture induced strains, transverse pressures acting on the sublaminate, and contact between the sublaminate and plate. The solution technique used is the Ritz method. A computationally efficient computer implementation of the model was developed. The code can be used to predict the nonlinear-load-strain behavior of the sublaminate including the buckling load, postbuckling behavior, and the onset of delamination growth. The accuracy of the code was evaluated by comparing the model results to benchmark analytical solutions. A series of experiments was conducted on Fiberite T300/976 graphite/epoxy laminates bonded to an aluminum honeycomb core forming a sandwich panel. Either circles or ellipses made from Teflon film were embedded in the laminates, simulating the presence of a delamination. Each specimen was loaded in compression and the strain history of the sublaminate was recorded far into the postbuckling regime. The extent of delamination growth was evaluated by C-scan examination of each specimen. The experimental data were compared to code predictions. The code was found to describe the data with reasonable accuracy. A sensitivity study examined the relative importance of various material properties, the delamination dimensions, the contact model, the transverse pressure differential, the critical strain energy release rate, and the relative growth direction on the buckling load, the postbuckling behavior, and the growth load of the sublaminate.

Prediction of hot deformation behavior of high phosphorus steel using artificial neural network

NASA Astrophysics Data System (ADS)

Singh, Kanchan; Rajput, S. K.; Soota, T.; Verma, Vijay; Singh, Dharmendra

2018-03-01

To predict the hot deformation behavior of high phosphorus steel, the hot compression experiments were performed with the help of thermo-mechanical simulator Gleeble® 3800 in the temperatures ranging from 750 °C to 1050 °C and strain rates of 0.001 s-1, 0.01 s-1, 0.1 s-1, 0.5 s-1, 1.0 s-1 and 10 s-1. The experimental stress-strain data are employed to develop artificial neural network (ANN) model and their predictability. Using different combination of temperature, strain and strain rate as a input parameter and obtained experimental stress as a target, a multi-layer ANN model based on feed-forward back-propagation algorithm is trained, to predict the flow stress for a given processing condition. The relative error between predicted and experimental stress are in the range of ±3.5%, whereas the correlation coefficient (R2) of training and testing data are 0.99986 and 0.99999 respectively. This shows that a well-trained ANN model has excellent capability to predict the hot deformation behavior of materials. Comparative study shows quite good agreement of predicted and experimental values.

Study of high strain rate plastic deformation of low carbon microalloyed steels using experimental observation and computational modeling

NASA Astrophysics Data System (ADS)

Majta, J.; Zurek, A. K.; Trujillo, C. P.; Bator, A.

2003-09-01

This work presents validation of the integrated computer model to predict the impact of the microstructure evolution on the mechanical behavior of niobium-microalloyed steels under dynamic loading conditions. The microstructurally based constitutive equations describing the mechanical behavior of the mixed α and γ phases are proposed. It is shown that for a given finishing temperature and strain, the Nb steel exhibits strong influence of strain rate on the flow stress and final structure. This tendency is also observed in calculated results obtained using proposed modeling procedures. High strain rates influence the deformation mechanism and reduce the extent of recovery occurring during and after deformation and, in turn, increase the driving force for transformation. On the other hand, the ratio of nucleation rate to growth rate increases for lower strain rates (due to the higher number of nuclei that can be produced during an extended loading time) leading to the refined ferrite structure. However, as it was expected such behavior produces higher inhomogeneity in the final product. Multistage quasistatic compression tests and test using the Hopkinson Pressure Bar under different temperature, strain, and strain rate conditions, are used for verification of the proposed models.

Effect of acoustic softening on the thermal-mechanical process of ultrasonic welding.

PubMed

Chen, Kunkun; Zhang, Yansong; Wang, Hongze

2017-03-01

Application of ultrasonic energy can reduce the static stress necessary for plastic deformation of metallic materials to reduce forming load and energy, namely acoustic softening effect (ASE). Ultrasonic welding (USW) is a rapid joining process utilizing ultrasonic energy to form a solid state joint between two or more pieces of metals. Quantitative characterization of ASE and its influence on specimen deformation and heat generation is essential to clarify the thermal-mechanical process of ultrasonic welding. In the present work, experiments were set up to found out mechanical behavior of copper and aluminum under combined effect of compression force and ultrasonic energy. Constitutive model was proposed and numerical implemented in finite element model of ultrasonic welding. Thermal-mechanical analysis was put forward to explore the effect of ultrasonic energy on the welding process quantitatively. Conclusions can be drawn that ASE increases structural deformation significantly, which is beneficial for joint formation. Meanwhile, heat generation from both frictional work and plastic deformation is slightly influenced by ASE. Based on the proposed model, relationship between ultrasonic energy and thermal-mechanical behavior of structure during ultrasonic welding was constructed. Copyright © 2016 Elsevier B.V. All rights reserved.

Osteoporosis affects both post-yield microdamage accumulation and plasticity degradation in vertebra of ovariectomized rats

NASA Astrophysics Data System (ADS)

Li, Siwei; Niu, Guodong; Dong, Neil X.; Wang, Xiaodu; Liu, Zhongjun; Song, Chunli; Leng, Huijie

2017-04-01

Estrogen withdrawal in postmenopausal women increases bone loss and bone fragility in the vertebra. Bone loss with osteoporosis not only reduces bone mineral density (BMD), but actually alters bone quality, which can be comprehensively represented by bone post-yield behaviors. This study aimed to provide some information as to how osteoporosis induced by estrogen depletion could influence the evolution of post-yield microdamage accumulation and plastic deformation in vertebral bodies. This study also tried to reveal the part of the mechanisms of how estrogen deficiency-induced osteoporosis would increase the bone fracture risk. A rat bilateral ovariectomy (OVX) model was used to induce osteoporosis. Progressive cyclic compression loading was developed for vertebra testing to elucidate the post-yield behaviors. BMD, bone volume fraction, stiffness degradation, and plastic deformation evolution were compared among rats raised for 5 weeks (ovx5w and sham5w groups) and 35 weeks (ovx35w and sham35w groups) after sham surgery and OVX. The results showed that a higher bone loss in vertebral bodies corresponded to lower stiffness and higher plastic deformation. Thus, osteoporosis could increase the vertebral fracture risk probably through microdamage accumulation and plastic deforming degradation.

Hot Deformation Behavior of 1Cr12Ni3Mo2VN Martensitic Stainless Steel

NASA Astrophysics Data System (ADS)

He, Xiaomao; Jiang, Peng; Zhou, Leyu; Chen, Chao; Deng, Xiaochun

2017-08-01

1Cr12Ni3Mo2VN is a new type of martensitic stainless steel for the last-stage blades of large-capacity nuclear and thermal power turbines. The deformation behavior of this steel was studied by thermal compression experiments that performed on a Gleeble-3500 thermal simulator at a temperature range of 850°C to 1200°C and a strain rate of 0.01s-1 to 20s-1. When the deformation was performed at high temperature and low strain rate, a necklace type of microstructures was observed, the plastic deformation mechanism is grain boundary slip and migration, when at low temperature and lower strain rate, the slip bands were observed, the mechanism is intracrystalline slips, and when at strain rate of 20s-1, twins were observed, the mechanism are slips and twins. The Arrhenius equation was applied to describe the constitutive equation of the flow stress. The accuracy of the equation was verified by using the experimental data and the correlation coefficient R2 = 0.9786, and the equation can provide reasonable data for the design and numerical simulation of the forging process.

Methodology based on genetic heuristics for in-vivo characterizing the patient-specific biomechanical behavior of the breast tissues

PubMed Central

Lago, M. A.; Rúperez, M. J.; Martínez-Martínez, F.; Martínez-Sanchis, S.; Bakic, P. R.; Monserrat, C.

2015-01-01

This paper presents a novel methodology to in-vivo estimate the elastic constants of a constitutive model proposed to characterize the mechanical behavior of the breast tissues. An iterative search algorithm based on genetic heuristics was constructed to in-vivo estimate these parameters using only medical images, thus avoiding invasive measurements of the mechanical response of the breast tissues. For the first time, a combination of overlap and distance coefficients were used for the evaluation of the similarity between a deformed MRI of the breast and a simulation of that deformation. The methodology was validated using breast software phantoms for virtual clinical trials, compressed to mimic MRI-guided biopsies. The biomechanical model chosen to characterize the breast tissues was an anisotropic neo-Hookean hyperelastic model. Results from this analysis showed that the algorithm is able to find the elastic constants of the constitutive equations of the proposed model with a mean relative error of about 10%. Furthermore, the overlap between the reference deformation and the simulated deformation was of around 95% showing the good performance of the proposed methodology. This methodology can be easily extended to characterize the real biomechanical behavior of the breast tissues, which means a great novelty in the field of the simulation of the breast behavior for applications such as surgical planing, surgical guidance or cancer diagnosis. This reveals the impact and relevance of the presented work. PMID:27103760

Methodology based on genetic heuristics for in-vivo characterizing the patient-specific biomechanical behavior of the breast tissues.

PubMed

Lago, M A; Rúperez, M J; Martínez-Martínez, F; Martínez-Sanchis, S; Bakic, P R; Monserrat, C

2015-11-30

This paper presents a novel methodology to in-vivo estimate the elastic constants of a constitutive model proposed to characterize the mechanical behavior of the breast tissues. An iterative search algorithm based on genetic heuristics was constructed to in-vivo estimate these parameters using only medical images, thus avoiding invasive measurements of the mechanical response of the breast tissues. For the first time, a combination of overlap and distance coefficients were used for the evaluation of the similarity between a deformed MRI of the breast and a simulation of that deformation. The methodology was validated using breast software phantoms for virtual clinical trials, compressed to mimic MRI-guided biopsies. The biomechanical model chosen to characterize the breast tissues was an anisotropic neo-Hookean hyperelastic model. Results from this analysis showed that the algorithm is able to find the elastic constants of the constitutive equations of the proposed model with a mean relative error of about 10%. Furthermore, the overlap between the reference deformation and the simulated deformation was of around 95% showing the good performance of the proposed methodology. This methodology can be easily extended to characterize the real biomechanical behavior of the breast tissues, which means a great novelty in the field of the simulation of the breast behavior for applications such as surgical planing, surgical guidance or cancer diagnosis. This reveals the impact and relevance of the presented work.

Measurement of compressed breast thickness by optical stereoscopic photogrammetry

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tyson, Albert H.; Mawdsley, Gordon E.; Yaffe, Martin J.

2009-02-15

The determination of volumetric breast density (VBD) from mammograms requires accurate knowledge of the thickness of the compressed breast. In attempting to accurately determine VBD from images obtained on conventional mammography systems, the authors found that the thickness reported by a number of mammography systems in the field varied by as much as 15 mm when compressing the same breast or phantom. In order to evaluate the behavior of mammographic compression systems and to be able to predict the thickness at different locations in the breast on patients, they have developed a method for measuring the local thickness of themore » breast at all points of contact with the compression paddle using optical stereoscopic photogrammetry. On both flat (solid) and compressible phantoms, the measurements were accurate to better than 1 mm with a precision of 0.2 mm. In a pilot study, this method was used to measure thickness on 108 volunteers who were undergoing mammography examination. This measurement tool will allow us to characterize paddle surface deformations, deflections and calibration offsets for mammographic units.« less

Elastic-Plastic Behaviour of Ultrasonic Assisted Compression of Polyvinyl Chloride (PVC) Foam

NASA Astrophysics Data System (ADS)

Muhalim, N. A. D.; Hassan, M. Z.; Daud, Y.

2018-04-01

The present study aims to investigate the elastic-plastic behaviour of ultrasonic assisted compression of PVC closed-cell foam. A series of static and ultrasonic compression test of PVC closed-cell foam were conducted at a constant cross head speed of 30 mm/min on dry surface condition. For quasi-static test, specimen was compressed between two rigid platens using universal testing machine. In order to evaluate the specimen behavior under ultrasonic condition, specimen was placed between a specifically design double-slotted block horn and rigid platen. The horn was designed and fabricated prior to the test as a medium to transmit the ultrasonic vibration from the ultrasonic transducer to the working specimen. It was tuned to a frequency of 19.89 kHz in longitudinal mode and provided an average oscillation amplitude at 6 µm on the uppermost surface. Following, the characteristics of stress-strain curves for quasi-static and ultrasonic compression tests were analyzed. It was found that the compressive stress was significantly reduced at the onset of superimposed ultrasonic vibration during plastic deformation.

Constitutive modeling and dynamic softening mechanism during hot deformation of an ultra-pure 17%Cr ferritic stainless steel stabilized with Nb

NASA Astrophysics Data System (ADS)

Gao, Fei; Liu, Zhenyu; Misra, R. D. K.; Liu, Haitao; Yu, Fuxiao

2014-09-01

The hot deformation behavior of an ultra-pure 17%Cr ferritic stainless steel was studied in the temperature range of 750-1000 °C and strain rates of 0.5 to 10 s-1 using isothermal hot compression tests in a thermomechanical simulator. The microstructural evolution was investigated using electron backscattered diffraction and transmission electron microscopy. A modified constitutive equation considering the effect of strain on material constant was developed, which predicted the flow stress for the deformation conditions studied, except at 950 °C in 1 s-1 and 900 °C in 10 s-1. Decreasing deformation temperature and increasing strain was beneficial in refining the microstructure. Decreasing deformation temperature, the in-grain shear bands appeared in the microstructure. It is suggested that the dynamic softening mechanism is closely related to deformation temperature. At low deformation temperature, dynamic recovery was major softening mechanism and no dynamic recrystallization occurred. At high deformation temperature, dynamic softening was explained in terms of efficient dynamic recovery and limited continuous dynamic recrystallization. A drop in the flow stress was not found due to very small fraction of new grains nucleated during dynamic recrystallization.

Global deformation on the surface of Venus

NASA Technical Reports Server (NTRS)

Bilotti, Frank; Connors, Chris; Suppe, John

1992-01-01

Large-scale mapping of tectonic structures on Venus shows that there is an organized global distribution to deformation. The structures we emphasize are linear compressive mountain belts, extensional rafted zones, and the small-scale but widely distributed wrinkle ridges. Ninety percent of the area of the planet's compressive mountain belts are concentrated in the northern hemisphere whereas the southern hemisphere is dominated by extension and small-scale compression. We propose that this striking concentration of fold belts in the northern hemisphere, along with the globe-encircling equatorial rift system, represents a global organization to deformation on Venus.

Effect of Nb Content on Mechanical Behavior and Structural Properties of W/(Zr55Cu30Al10Ni5)100- x Nb x Composite

NASA Astrophysics Data System (ADS)

Mahmoodan, Morteza; Gholamipour, Reza; Mirdamadi, Shamseddin; Nategh, Said

2017-05-01

In the present study, (Zr55Cu30Al10Ni5)100- x Nb( x=0,1,2,3) bulk metallic glass matrix/tungsten wire composites were fabricated by infiltration process. Structural studies were investigated by scanning electron microscopy and X-ray diffraction method. Also, mechanical behaviors of the materials were analyzed using quasi-static compressive tests. Results indicated that the best mechanical properties i.e., 2105 MPa compressive ultimate strength and 28 pct plastic strain before failure, were achieved in the composite sample with X = 2. It was also found that adding Nb to the matrix modified interface structure in W fiber/(Zr55Cu30Al10Ni5)98Nb2 since the stable diffusion band formation acts as a functionally graded layer. Finally, the observation of multiple shear bands formation in the matrix could confirm the excellent plastic deformation behavior of the composite.

Target Soil Impact Verification: Experimental Testing and Kayenta Constitutive Modeling.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Broome, Scott Thomas; Flint, Gregory Mark; Dewers, Thomas

2015-11-01

This report details experimental testing and constitutive modeling of sandy soil deformation under quasi - static conditions. This is driven by the need to understand constitutive response of soil to target/component behavior upon impact . An experimental and constitutive modeling program was followed to determine elastic - plastic properties and a compressional failure envelope of dry soil . One hydrostatic, one unconfined compressive stress (UCS), nine axisymmetric compression (ACS) , and one uniaxial strain (US) test were conducted at room temperature . Elastic moduli, assuming isotropy, are determined from unload/reload loops and final unloading for all tests pre - failuremore » and increase monotonically with mean stress. Very little modulus degradation was discernable from elastic results even when exposed to mean stresses above 200 MPa . The failure envelope and initial yield surface were determined from peak stresses and observed onset of plastic yielding from all test results. Soil elasto - plastic behavior is described using the Brannon et al. (2009) Kayenta constitutive model. As a validation exercise, the ACS - parameterized Kayenta model is used to predict response of the soil material under uniaxial strain loading. The resulting parameterized and validated Kayenta model is of high quality and suitable for modeling sandy soil deformation under a range of conditions, including that for impact prediction.« less

Review: mechanical behavior of metal/ceramic interfaces in nanolayered composites—experiments and modeling

DOE Office of Scientific and Technical Information (OSTI.GOV)

Li, Nan; Liu, Xiang-Yang

In this study, recent experimental and modeling studies in nanolayered metal/ceramic composites are reviewed, with focus on the mechanical behaviors of metal/nitrides interfaces. The experimental and modeling studies of the slip systems in bulk TiN are reviewed first. Then, the experimental studies of interfaces, including co-deformation mechanism by micropillar compression tests, in situ TEM straining tests for the dynamic process of the co-deformation, thickness-dependent fracture behavior, and interrelationship among the interfacial bonding, microstructure, and mechanical response, are reviewed for the specific material systems of Al/TiN and Cu/TiN multilayers at nanoscale. The modeling studies reviewed cover first-principles density functional theory-based modeling,more » atomistic molecular dynamics simulations, and mesoscale modeling of nanolayered composites using discrete dislocation dynamics. The phase transformation between zinc-blende and wurtzite AlN phases in Al/AlN multilayers at nanoscale is also reviewed. Finally, a summary and perspective of possible research directions and challenges are given.« less

Review: mechanical behavior of metal/ceramic interfaces in nanolayered composites—experiments and modeling

DOE PAGES

Li, Nan; Liu, Xiang-Yang

2017-11-03

In this study, recent experimental and modeling studies in nanolayered metal/ceramic composites are reviewed, with focus on the mechanical behaviors of metal/nitrides interfaces. The experimental and modeling studies of the slip systems in bulk TiN are reviewed first. Then, the experimental studies of interfaces, including co-deformation mechanism by micropillar compression tests, in situ TEM straining tests for the dynamic process of the co-deformation, thickness-dependent fracture behavior, and interrelationship among the interfacial bonding, microstructure, and mechanical response, are reviewed for the specific material systems of Al/TiN and Cu/TiN multilayers at nanoscale. The modeling studies reviewed cover first-principles density functional theory-based modeling,more » atomistic molecular dynamics simulations, and mesoscale modeling of nanolayered composites using discrete dislocation dynamics. The phase transformation between zinc-blende and wurtzite AlN phases in Al/AlN multilayers at nanoscale is also reviewed. Finally, a summary and perspective of possible research directions and challenges are given.« less

Enhancement of orientation gradients during simple shear deformation by application of simple compression

NASA Astrophysics Data System (ADS)

Jahedi, Mohammad; Ardeljan, Milan; Beyerlein, Irene J.; Paydar, Mohammad Hossein; Knezevic, Marko

2015-06-01

We use a multi-scale, polycrystal plasticity micromechanics model to study the development of orientation gradients within crystals deforming by slip. At the largest scale, the model is a full-field crystal plasticity finite element model with explicit 3D grain structures created by DREAM.3D, and at the finest scale, at each integration point, slip is governed by a dislocation density based hardening law. For deformed polycrystals, the model predicts intra-granular misorientation distributions that follow well the scaling law seen experimentally by Hughes et al., Acta Mater. 45(1), 105-112 (1997), independent of strain level and deformation mode. We reveal that the application of a simple compression step prior to simple shearing significantly enhances the development of intra-granular misorientations compared to simple shearing alone for the same amount of total strain. We rationalize that the changes in crystallographic orientation and shape evolution when going from simple compression to simple shearing increase the local heterogeneity in slip, leading to the boost in intra-granular misorientation development. In addition, the analysis finds that simple compression introduces additional crystal orientations that are prone to developing intra-granular misorientations, which also help to increase intra-granular misorientations. Many metal working techniques for refining grain sizes involve a preliminary or concurrent application of compression with severe simple shearing. Our finding reveals that a pre-compression deformation step can, in fact, serve as another processing variable for improving the rate of grain refinement during the simple shearing of polycrystalline metals.

Effect of water on nanomechanics of bone is different between tension and compression

DOE Office of Scientific and Technical Information (OSTI.GOV)

Samuel, Jitin; Park, Jun-Sang; Almer, Jonathan

Water, an important constituent in bone, resides in different compartments in bone matrix and may impose significant effects on its bulk mechanical properties. However, a clear understanding of the mechanistic role of water in toughening bone is yet to emerge. To address this issue, this study used a progressive loading protocol, coupled with measurements of in situ mineral and collagen fibril deformations using synchrotron X-ray diffraction techniques. Using this unique approach, the contribution of water to the ultrastructural behavior of bone was examined by testing bone specimens in different loading modes (tension and compression) and hydration states (wet and dehydrated).more » The results indicated that the effect of water on the mechanical behavior of mineral and collagen phases at the ultrastructural level was loading mode dependent and correlated with the bulk behavior of bone. Tensile loading elicited a transitional drop followed by an increase in load bearing by the mineral phase at the ultrastructural level, which was correlated with a strain hardening behavior of bone at the bulk level. Compression loading caused a continuous loss of load bearing by the mineral phase, which was reflected at the bulk level as a strain softening behavior. In addition, viscous strain relaxation and pre-strain reduction were observed in the mineral phase in the presence of water. Taken together, the results of this study suggest that water dictates the bulk behavior of bone by altering the interaction between mineral crystals and their surrounding matrix.« less

Cervical Disc Deformation During Flexion–Extension in Asymptomatic Controls and Single-Level Arthrodesis Patients

PubMed Central

Anderst, William; Donaldson, William; Lee, Joon; Kang, James

2016-01-01

The aim of this study was to characterize cervical disc deformation in asymptomatic subjects and single-level arthrodesis patients during in vivo functional motion. A validated model-based tracking technique determined vertebral motion from biplane radiographs collected during dynamic flexion–extension. Level-dependent differences in disc compression–distraction and shear deformation were identified within the anterior and posterior annulus (PA) and the nucleus of 20 asymptomatic subjects and 15 arthrodesis patients using a mixed-model statistical analysis. In asymptomatic subjects, disc compression and shear deformation per degree of flexion–extension progressively decreased from C23 to C67. The anterior and PA experienced compression–distraction deformation of up to 20%, while the nucleus region was compressed between 0% (C67) and 12% (C23). Peak shear deformation ranged from 16% (at C67) to 33% (at C45). In the C5–C6 arthrodesis group, C45 discs were significantly less compressed than in the control group in all disc regions (all p ≤ 0.026). In the C6–C7 arthrodesis group, C56 discs were significantly less compressed than the control group in the nucleus (p = 0.023) and PA (p = 0.014), but not the anterior annulus (AA; p = 0.137). These results indicate in vivo disc deformation is level-dependent, and single-level anterior arthrodesis alters the compression–distraction deformation in the disc immediately superior to the arthrodesis. PMID:23861160

Universal Viscous-Brittle Transition in Magmatic Liquids

NASA Astrophysics Data System (ADS)

Witcher, T.; Wadsworth, F. B.; Hess, K. U.; Vossen, C.; Unwin, H.; Dingwell, D. B.

2017-12-01

Physical processes occurring in a volcanic conduit are thought to dictate the eruptivebehavior of volcanoes. One of these processes is the rheological response of the liquidmagma to the enormous stresses applied to it during ascent. In this study we investigatedthe behavior of both synthetic and natural silicate glass at high temperature. We chosetemperatures at which the glass viscosity was high in the range of 109 - 1012 Pa s. Afterthermal equilibration, we deformed the samples by uniaxial compression. We measured theforce and displacement applied to 20 x 40 mm glass cylinders at controlled strain rates. Toparameterize the deformation behavior we defined a dimensionless quantity, the Deborahnumber (De), which is a ratio between viscoelastic relaxation time of the liquid (λr) and thedeformation time (λ) both in units of seconds. Each deformed sample had a De assignedto it and was plotted on a 'Deformation Map.' After performing over 60 experiments,three deformational regimes were defined: viscous, transitional, and brittle. We found thatall samples with De < 0.01 behaved purely viscously with no stress drops. Between De =0.01 and De = 0.04 the behavior was unrelaxed, in which small stress drops were observedbetween otherwise viscous flow, indicating the onset of elastic behavior. Furthermore,samples with De > 0.04 were categorized as brittle and behaved purely elastically withlittle to no fracturing before one large stress drop. The implications of this study showthat when a silicate melt is not given enough time to dissipate the stress applied to itthrough viscous flow, it will behave like an elastic solid and support fracture propagation.It is through this capability of brittle failure that magma can rapidly ascend through theshallow crust-the fractures would provide pathways for fluid along the conduit margin.These fluids would lubricate the magma body as it ascends.

Cubical Mass-Spring Model design based on a tensile deformation test and nonlinear material model.

PubMed

San-Vicente, Gaizka; Aguinaga, Iker; Tomás Celigüeta, Juan

2012-02-01

Mass-Spring Models (MSMs) are used to simulate the mechanical behavior of deformable bodies such as soft tissues in medical applications. Although they are fast to compute, they lack accuracy and their design remains still a great challenge. The major difficulties in building realistic MSMs lie on the spring stiffness estimation and the topology identification. In this work, the mechanical behavior of MSMs under tensile loads is analyzed before studying the spring stiffness estimation. In particular, the performed qualitative and quantitative analysis of the behavior of cubical MSMs shows that they have a nonlinear response similar to hyperelastic material models. According to this behavior, a new method for spring stiffness estimation valid for linear and nonlinear material models is proposed. This method adjusts the stress-strain and compressibility curves to a given reference behavior. The accuracy of the MSMs designed with this method is tested taking as reference some soft-tissue simulations based on nonlinear Finite Element Method (FEM). The obtained results show that MSMs can be designed to realistically model the behavior of hyperelastic materials such as soft tissues and can become an interesting alternative to other approaches such as nonlinear FEM.

Compressive Behaviour and Energy Absorption of Aluminium Foam Sandwich

NASA Astrophysics Data System (ADS)

Endut, N. A.; Hazza, M. H. F. Al; Sidek, A. A.; Adesta, E. T. Y.; Ibrahim, N. A.

2018-01-01

Development of materials in automotive industries plays an important role in order to retain the safety, performance and cost. Metal foams are one of the idea to evolve new material in automotive industries since it can absorb energy when it deformed and good for crash management. Recently, new technology had been introduced to replace metallic foam by using aluminium foam sandwich (AFS) due to lightweight and high energy absorption behaviour. Therefore, this paper provides reliable data that can be used to analyze the energy absorption behaviour of aluminium foam sandwich by conducting experimental work which is compression test. Six experiments of the compression test were carried out to analyze the stress-strain relationship in terms of energy absorption behavior. The effects of input variables include varying the thickness of aluminium foam core and aluminium sheets on energy absorption behavior were evaluated comprehensively. Stress-strain relationship curves was used for energy absorption of aluminium foam sandwich calculation. The result highlights that the energy absorption of aluminium foam sandwich increases from 12.74 J to 64.42 J respectively with increasing the foam and skin thickness.

Experimental investigation of the strength and failure behavior of layered sandstone under uniaxial compression and Brazilian testing

NASA Astrophysics Data System (ADS)

Yin, Peng-Fei; Yang, Sheng-Qi

2018-05-01

As a typical inherently anisotropic rock, layered sandstones can differ from each other in several aspects, including grain size, type of material, type of cementation, and degree of compaction. An experimental study is essential to obtain and convictive evidence to characterize the mechanical behavior of such rock. In this paper, the mechanical behavior of a layered sandstone from Xuzhou, China, is investigated under uniaxial compression and Brazilian test conditions. The loading tests are conducted on 7 sets of bedding inclinations, which are defined as the angle between the bedding plane and horizontal direction. The uniaxial compression strength (UCS) and elastic modulus values show an undulatory variation when the bedding inclination increases. The overall trend of the UCS and elastic modulus values with bedding inclination is decreasing. The BTS value decreases with respect to the bedding inclination and the overall trend of it is approximating a linear variation. The 3D digital high-speed camera images reveal that the failure and fracture of a specimen are related to the surface deformation. Layered sandstone tested under uniaxial compression does not show a typical failure mode, although shear slip along the bedding plane occurs at high bedding inclinations. Strain gauge readings during the Brazilian tests indicate that the normal stress on the bedding plane transforms from compression to tension as the bedding inclination increases. The stress parallel to the bedding plane in a rock material transforms from tension to compression and agrees well with the fracture patterns; "central fractures" occur at bedding inclinations of 0°-75°, "layer activation" occurs at high bedding inclinations of 75°-90°, and a combination of the two occurs at 75°.

Influence of granulating method on physical and mechanical properties, compression behavior, and compactibility of lactose and microcrystalline cellulose granules.

PubMed

Horisawa, E; Danjo, K; Sunada, H

2000-06-01

The physical and mechanical properties of lactose (LC) and microcrystalline cellulose (MCC) granules prepared by various granulating methods were determined, and their effects on the compression and strength of the tablets were examined. From the force-displacement curve obtained in a crushing test on a single granule, all LC granules appeared brittle, and MCC granules were somewhat plastically deformable. Inter-granular porosity epsilon inter clearly decreased with greater spherical granule shape for both materials. Decrease in intragranular porosity epsilon intra enhanced the crushing force of a single granule Fg. Agitating granulation brought about the most compactness and hardness of granules. In granule compression tests, the initial slope of Heckel plots K1 appeared closely related to ease of filling voids in a granule bed by the slippage or rolling of granules. The reciprocal of the slope in the succeeding step 1/K2 in compression of MCC granules indicated positive correlation to Fg, while in LC granules, no such obvious relation was evident. 1/K2 differed only slightly among granulating methods. Tensile strength of tablets Tt obtained by compression of various LC granules was low as a whole and was little influenced by granulating method. For MCC granules, which are plastically deformable, tablet strength greatly depended on granulation. Granules prepared by extruding or dry granulation gave strong tablets. Tablets prepared from granules made by the agitating method showed particularly low Tt. From stereomicroscopic observation, the contact area between granule particles in a tablet appeared smaller; this would explain the decrease in inter-granular bond formation.

Modeling of the flow behavior of SAE 8620H combing microstructure evolution in hot forming

NASA Astrophysics Data System (ADS)

Fu, Xiaobin; Wang, Baoyu; Tang, Xuefeng

2017-10-01

With the development of net-shape forming technology, hot forming process is widely applied to manufacturing gear parts, during which, materials suffer severe plastic distortion and microstructure changes continually. In this paper, to understand and model the flow behavior and microstructure evolution, SAE 8620H, a widely used gear steel, is selected as the object and the flow behavior and microstructure evolution are observed by an isothermal hot compression tests at 1273-1373 K with a strain rate of 0.1-10 s-1. Depending on the results of the compression test, a set of internal-state-variable based unified constitutive equations is put forward to describe the flow behavior and microstructure evaluation of SAE 8620H. Moreover, the evaluation of the dislocation density and the fraction of dynamic recrystallization based on the theory of thermal activation is modeled and reincorporated into the constitutive law. The material parameters in the constitutive model are calculated based on the measured flow stress and dynamic recrystallization fraction. The predicted flow stress under different deformation conditions has a good agreement with the measured results.

Post-deformation shape-recovery behavior of vitamin E-diffused, radiation crosslinked polyethylene acetabular components.

PubMed

Takahashi, Yasuhito; Tateiwa, Toshiyuki; Shishido, Takaaki; Masaoka, Toshinori; Kubo, Kosuke; Yamamoto, Kengo

2016-10-01

The in-vivo progression of creep and wear in ultra-high molecular weight polyethylene (UHMWPE) acetabular liners has been clinically evaluated by measuring radiographic penetration of femoral heads. In such clinical assessments, however, viscoelastic strain relaxation has been rarely considered after a removal of hip joint loading, potentially leading to an underestimation of the penetrated thickness. The objective of this study was to investigate shape-recovery behavior of pre-compressed, radiation crosslinked and antioxidant vitamin E-diffused UHMWPE acetabular liners, and also to characterize the effects of varying their internal diameter (ID) and wall thickness (WT). We applied uniaxial compression to the UHMWPE specimens of various ID (28, 32, 36mm) and WT (4.8, 6.8, 8.9mm) for 4320min under the constant load of 3000N, and subsequently monitored the strain-relaxation behavior as a function of time after unloading. It was observed that there was a considerable shape recovery of the components after removal of the external static load. Reducing ID and WT significantly accelerated the rate of creep strain recovery, and varying WT was more sensitive to the recovery behavior than ID. Creep deformation of the tested liners recovered mostly within the first 300min after unloading. Note that approximately half of the total recovery amount proceeded just within 5min after unloading. These results suggest a remarkably high capability of shape recovery of vitamin E-diffused highly crosslinked UHMWPE. In conclusion, the time-dependent shape recovering and the diameter-thickness effect on its behavior should be carefully considered when the postoperative penetration is quantified in highly crosslinked UHMWPE acetabular liners (especially on the non-weight bearing radiographs). Copyright © 2016 Elsevier Ltd. All rights reserved.

Grain-size-induced weakening of H2O ices I and II and associated anisotropic recrystallization

USGS Publications Warehouse

Stern, L.A.; Durham, W.B.; Kirby, S.H.

1997-01-01

Grain-size-dependent flow mechanisms tend to be favored over dislocation creep at low differential stresses and can potentially influence the rheology of low-stress, low-strain rate environments such as those of planetary interiors. We experimentally investigated the effect of reduced grain size on the solid-state flow of water ice I, a principal component of the asthenospheres of many icy moons of the outer solar system, using techniques new to studies of this deformation regime. We fabricated fully dense ice samples of approximate grain size 2 ?? 1 ??m by transforming "standard" ice I samples of 250 ?? 50 ??m grain size to the higher-pressure phase ice II, deforming them in the ice II field, and then rapidly releasing the pressure deep into the ice I stability field. At T ??? 200 K, slow growth and rapid nucleation of ice I combine to produce a fine grain size. Constant-strain rate deformation tests conducted on these samples show that deformation rates are less stress sensitive than for standard ice and that the fine-grained material is markedly weaker than standard ice, particularly during the transient approach to steady state deformation. Scanning electron microscope examination of the deformed fine-grained ice samples revealed an unusual microstructure dominated by platelike grains that grew normal to the compression direction, with c axes preferentially oriented parallel to compression. In samples tested at T ??? 220 K the elongation of the grains is so pronounced that the samples appear finely banded, with aspect ratios of grains approaching 50:1. The anisotropic growth of these crystallographically oriented neoblasts likely contributes to progressive work hardening observed during the transient stage of deformation. We have also documented remarkably similar microstructural development and weak mechanical behavior in fine-grained ice samples partially transformed and deformed in the ice II field.

Characterization of Hot Deformation Behavior of a Fe-Cr-Ni-Mo-N Superaustenitic Stainless Steel Using Dynamic Materials Modeling

NASA Astrophysics Data System (ADS)

Pu, Enxiang; Zheng, Wenjie; Song, Zhigang; Feng, Han; Zhu, Yuliang

2017-03-01

Hot deformation behavior of a Fe-24Cr-22Ni-7Mo-0.5N superaustenitic stainless steel was investigated by hot compression tests in a wide temperature range of 950-1250 °C and strain rate range of 0.001-10 s-1. The flow curves show that the flow stress decreases as the deformation temperature increases or the strain rate decreases. The processing maps developed on the basis of the dynamic materials model and flow stress data were adopted to optimize the parameters of hot working. It was found that the strain higher than 0.2 has no significant effect on the processing maps. The optimum processing conditions were in the temperature range of 1125-1220 °C and strain rate range of 0.1-3 s-1. Comparing to other stable domains, microstructural observations in this domain revealed the complete dynamic recrystallization (DRX) with finer and more uniform grain size. Flow instability occurred in the domain of temperature lower than 1100 °C and strain rate higher than 0.1 s-1.

Hot Roll Bonding of Aluminum to Twin-Roll Cast (TRC) Magnesium and Its Subsequent Deformation Behavior

NASA Astrophysics Data System (ADS)

Saleh, H.; Schmidtchen, M.; Kawalla, R.

2018-02-01

In an experiment in which twin-roll cast AZ31 magnesium alloy and commercial purity aluminum (AA 1050) sheets were bonded by hot rolling as Al/Mg/Al laminate composites, it was found that increasing the preheating temperatures up to 400 °C enhances the bonding strength of composites. Further increases in the preheating temperatures accelerate the magnesium oxide growth and thus reduce the bonding strength. The influence of the reduction ratio on the bonding properties was also studied, whereby it was observed that increasing the rolling reduction led to an increase in the bonding strength. The experimental results show that the optimum bonding strength can be obtained at rolling temperatures of 375-400 °C with a 50-60% reduction in thickness. On the other hand, the subsequent deformation behavior of composite was assessed using plane strain compression and deep drawing tests. We demonstrate that the composites produced using the optimum roll bonding conditions exhibited sufficient bonding during subsequent deformation and did not reveal any debonding at the bonding interface.

Analytical Solutions to Coupled HM Problems to Highlight the Nonlocal Nature of Aquifer Storage

NASA Astrophysics Data System (ADS)

De Simone, Silvia; Carrera, Jesús

2017-11-01

Specific storage reflects the volumetric deformation capacity of permeable media. Classical groundwater hydrology equates elastic storage to medium compressibility (plus fluid compressibility times porosity). However, it is unclear if storage behavior can be represented by a single parameter. Hydraulic gradients act as body forces that push the medium in the direction of flow causing it to deform instantaneously everywhere, i.e., even in regions where pressure would not have changed according to conventional fluid flow. Therefore, actual deformation depends not only on the mechanical properties of the medium but also on aquifer geometry and on surrounding strata, which act like constraints to displacements. Here we discuss the question and highlight the nonlocal nature of storage (i.e., the volume of water released at a point depends on the poroelastic response over the whole aquifer). Proper evaluation of transient pressure and water release from storage requires acknowledging the hydromechanical coupling, which generally involves the use of numerical methods. We propose analytical solutions to the HM problem of fluid injection (extraction) into finite aquifers with one-dimensional or cylindrical geometries. We find that pressure response is much faster (virtually instantaneous) and larger than expected from traditional purely hydraulic solutions when aquifer deformation is restrained, whereas the pressure response is reversed (i.e., pressure drop in response to injection) when the permeable medium is free to deform. These findings suggest that accounting for hydromechanical coupling may be required when hydraulic testing is performed in low permeability media, which is becoming increasingly demanded for energy-related applications.

Effect of grain orientation on aluminum relocation at incipient melt conditions

DOE PAGES

Yilmaz, Nadir; Vigil, Francisco M.; Vigil, Miquela S.; ...

2015-09-01

Aluminum is commonly used for structural applications in the aerospace industry because of its high strength in relation to its weight. It is necessary to understand the mechanical response of aluminum structures at elevated temperatures such as those experienced in a fire. Additionally, aluminum alloys exhibit many complicated behaviors that require further research and understanding, such as aluminum combustion, oxide skin formation and creep behavior. This paper discusses the effect of grain orientation on aluminum deformation subjected to heating at incipient melt conditions. Experiments were conducted by applying a vertical compressive force to aluminum alloy 7075 block test specimens. Furthermore,more » compression testing was done on test specimens with the applied load on the long transverse and short transverse orientations. Our results showed that the grain orientation significantly influences aluminum’s strength and mode of failure.« less

Universal Quake Statistics: From Compressed Nanocrystals to Earthquakes.

PubMed

Uhl, Jonathan T; Pathak, Shivesh; Schorlemmer, Danijel; Liu, Xin; Swindeman, Ryan; Brinkman, Braden A W; LeBlanc, Michael; Tsekenis, Georgios; Friedman, Nir; Behringer, Robert; Denisov, Dmitry; Schall, Peter; Gu, Xiaojun; Wright, Wendelin J; Hufnagel, Todd; Jennings, Andrew; Greer, Julia R; Liaw, P K; Becker, Thorsten; Dresen, Georg; Dahmen, Karin A

2015-11-17

Slowly-compressed single crystals, bulk metallic glasses (BMGs), rocks, granular materials, and the earth all deform via intermittent slips or "quakes". We find that although these systems span 12 decades in length scale, they all show the same scaling behavior for their slip size distributions and other statistical properties. Remarkably, the size distributions follow the same power law multiplied with the same exponential cutoff. The cutoff grows with applied force for materials spanning length scales from nanometers to kilometers. The tuneability of the cutoff with stress reflects "tuned critical" behavior, rather than self-organized criticality (SOC), which would imply stress-independence. A simple mean field model for avalanches of slipping weak spots explains the agreement across scales. It predicts the observed slip-size distributions and the observed stress-dependent cutoff function. The results enable extrapolations from one scale to another, and from one force to another, across different materials and structures, from nanocrystals to earthquakes.

Universal Quake Statistics: From Compressed Nanocrystals to Earthquakes

PubMed Central

Uhl, Jonathan T.; Pathak, Shivesh; Schorlemmer, Danijel; Liu, Xin; Swindeman, Ryan; Brinkman, Braden A. W.; LeBlanc, Michael; Tsekenis, Georgios; Friedman, Nir; Behringer, Robert; Denisov, Dmitry; Schall, Peter; Gu, Xiaojun; Wright, Wendelin J.; Hufnagel, Todd; Jennings, Andrew; Greer, Julia R.; Liaw, P. K.; Becker, Thorsten; Dresen, Georg; Dahmen, Karin A.

2015-01-01

Slowly-compressed single crystals, bulk metallic glasses (BMGs), rocks, granular materials, and the earth all deform via intermittent slips or “quakes”. We find that although these systems span 12 decades in length scale, they all show the same scaling behavior for their slip size distributions and other statistical properties. Remarkably, the size distributions follow the same power law multiplied with the same exponential cutoff. The cutoff grows with applied force for materials spanning length scales from nanometers to kilometers. The tuneability of the cutoff with stress reflects “tuned critical” behavior, rather than self-organized criticality (SOC), which would imply stress-independence. A simple mean field model for avalanches of slipping weak spots explains the agreement across scales. It predicts the observed slip-size distributions and the observed stress-dependent cutoff function. The results enable extrapolations from one scale to another, and from one force to another, across different materials and structures, from nanocrystals to earthquakes. PMID:26572103

High-pressure behavior of intermediate scapolite: compressibility, structure deformation and phase transition

NASA Astrophysics Data System (ADS)

Lotti, Paolo; Comboni, Davide; Merlini, Marco; Hanfland, Michael

2018-05-01

Scapolites are common volatile-bearing minerals in metamorphic rocks. In this study, the high-pressure behavior of an intermediate member of the scapolite solid solution series (Me47), chemical formula (Na1.86Ca1.86K0.23Fe0.01)(Al4.36Si7.64)O24[Cl0.48(CO3)0.48(SO4)0.01], has been investigated up to 17.79 GPa, by means of in situ single-crystal synchrotron X-ray diffraction. The isothermal elastic behavior of the studied scapolite has been described by a III-order Birch-Murnaghan equation of state, which provided the following refined parameters: V 0 = 1110.6(7) Å3, {K_{{V_0}}} = 70(2) GPa ({β _{{V_0}}} = 0.0143(4) GPa-1) and {K_{{V}}^' = 4.8(7). The refined bulk modulus is intermediate between those previously reported for Me17 and Me68 scapolite samples, confirming that the bulk compressibility among the solid solution increases with the Na content. A discussion on the P-induced structure deformation mechanisms of tetragonal scapolite at the atomic scale is provided, along with the implications of the reported results for the modeling of scapolite stability. In addition, a single-crystal to single-crystal phase transition, which is displacive in character, has been observed toward a triclinic polymorph at 9.87 GPa. The high-pressure triclinic polymorph was found to be stable up to the highest pressure investigated.

Stress relaxation of swine growth plate in semi-confined compression: depth dependent tissue deformational behavior versus extracellular matrix composition and collagen fiber organization.

PubMed

Amini, Samira; Mortazavi, Farhad; Sun, Jun; Levesque, Martin; Hoemann, Caroline D; Villemure, Isabelle

2013-01-01

Mechanical environment is one of the regulating factors involved in the process of longitudinal bone growth. Non-physiological compressive loading can lead to infantile and juvenile musculoskeletal deformities particularly during growth spurt. We hypothesized that tissue mechanical behavior in sub-regions (reserve, proliferative and hypertrophic zones) of the growth plate is related to its collagen and proteoglycan content as well as its collagen fiber orientation. To characterize the strain distribution through growth plate thickness and to evaluate biochemical content and collagen fiber organization of the three histological zones of growth plate tissue. Distal ulnar growth plate samples (N = 29) from 4-week old pigs were analyzed histologically for collagen fiber organization (N = 7) or average zonal thickness (N = 8), or trimmed into the three average zones, based on the estimated thickness of each histological zone, for biochemical analysis of water, collagen and glycosaminoglycan content (N = 7). Other samples (N = 7) were tested in semi-confined compression under 10% compressive strain. Digital images of the fluorescently labeled nuclei were concomitantly acquired by confocal microscopy before loading and after tissue relaxation. Strain fields were subsequently calculated using a custom-designed 2D digital image correlation algorithm. Depth-dependent compressive strain patterns and collagen content were observed. The proliferative and hypertrophic zone developed the highest axial and transverse strains, respectively, under compression compared to the reserve zone, in which the lowest axial and transverse strains arose. The collagen content per wet mass was significantly lower in the proliferative and hypertrophic zones compared to the reserve zone, and all three zones had similar glycosaminoglycan and water content.Polarized light microscopy showed that collagen fibers were mainly organized horizontally in the reserve zone and vertically aligned with the growth direction in the proliferative and hypertrophic zones. Higher strains were developed in growth plate areas (proliferative and hypertrophic) composed of lower collagen content and of vertical collagen fiber organization. The stiffer reserve zone, with its higher collagen content and collagen fibers oriented to restrain lateral expansion under compression, could play a greater role of mechanical support compared to the proliferative and hypertrophic zones, which could be more susceptible to be involved in an abnormal growth process.

Improving Tensile and Compressive Properties of an Extruded AZ91 Rod by the Combined Use of Torsion Deformation and Aging Treatment

PubMed Central

Song, Bo; Wang, Chunpeng; Guo, Ning; Pan, Hucheng; Xin, Renlong

2017-01-01

In this study, AZ91 magnesium alloy rods were used to investigate the effects of torsion deformation on microstructure and subsequent aging behavior. Extruded AZ91 rod has a uniform microstructure and typical fiber texture. Torsion deformation can generate a gradient microstructure on the cross-section of the rod. After torsion, from the center to the edge in the cross-section of the rod, both stored dislocations and area fraction of {10-12} twins gradually increase, and the basal pole of the texture tends to rotate in the ED direction. Direct aging usually generates coarse discontinuous precipitates and fine continuous precipitates simultaneously. Both twin structures and dislocations via torsion deformation can be effective microstructures for the nucleation of continuous precipitates during subsequent aging. Thus, aging after torsion can promote continuous precipitation and generate gradient precipitation characteristics. Both aging treatment and torsion deformation can reduce yield asymmetry, and torsion deformation enhances the aging hardening effect by promoting continuous precipitation. Therefore, combined use of torsion deformation and aging treatment can effectively enhance the yield strength and almost eliminate the yield asymmetry of the present extruded AZ91 rod. Finally, the relevant mechanisms are discussed. PMID:28772638

Transverse compression of PPTA fibers

NASA Astrophysics Data System (ADS)

Singletary, James

2000-07-01

Results of single transverse compression testing of PPTA and PIPD fibers, using a novel test device, are presented and discussed. In the tests, short lengths of single fibers are compressed between two parallel, stiff platens. The fiber elastic deformation is analyzed as a Hertzian contact problem. The inelastic deformation is analyzed by elastic-plastic FE simulation and by laser-scanning confocal microscopy of the compressed fibers ex post facto. The results obtained are compared to those in the literature and to the theoretical predictions of PPTA fiber transverse elasticity based on PPTA crystal elasticity.

An internal variable constitutive model for the large deformation of metals at high temperatures

NASA Technical Reports Server (NTRS)

Brown, Stuart; Anand, Lallit

1988-01-01

The advent of large deformation finite element methodologies is beginning to permit the numerical simulation of hot working processes whose design until recently has been based on prior industrial experience. Proper application of such finite element techniques requires realistic constitutive equations which more accurately model material behavior during hot working. A simple constitutive model for hot working is the single scalar internal variable model for isotropic thermal elastoplasticity proposed by Anand. The model is recalled and the specific scalar functions, for the equivalent plastic strain rate and the evolution equation for the internal variable, presented are slight modifications of those proposed by Anand. The modified functions are better able to represent high temperature material behavior. The monotonic constant true strain rate and strain rate jump compression experiments on a 2 percent silicon iron is briefly described. The model is implemented in the general purpose finite element program ABAQUS.

Effects of applied stress ratio on the fatigue behavior of additively manufactured porous biomaterials under compressive loading.

PubMed

de Krijger, Joep; Rans, Calvin; Van Hooreweder, Brecht; Lietaert, Karel; Pouran, Behdad; Zadpoor, Amir A

2017-06-01

Additively manufactured (AM) porous metallic biomaterials are considered promising candidates for bone substitution. In particular, AM porous titanium can be designed to exhibit mechanical properties similar to bone. There is some experimental data available in the literature regarding the fatigue behavior of AM porous titanium, but the effect of stress ratio on the fatigue behavior of those materials has not been studied before. In this paper, we study the effect of applied stress ratio on the compression-compression fatigue behavior of selective laser melted porous titanium (Ti-6Al-4V) based on the diamond unit cell. The porous titanium biomaterial is treated as a meta-material in the context of this work, meaning that R-ratios are calculated based on the applied stresses acting on a homogenized volume. After morphological characterization using micro computed tomography and quasi-static mechanical testing, the porous structures were tested under cyclic loading using five different stress ratios, i.e. R = 0.1, 0.3, 0.5, 0.7 and 0.8, to determine their S-N curves. Feature tracking algorithms were used for full-field deformation measurements during the fatigue tests. It was observed that the S-N curves of the porous structures shift upwards as the stress ratio increases. The stress amplitude was the most important factor determining the fatigue life. Constant fatigue life diagrams were constructed and compared with similar diagrams for bulk Ti-6Al-4V. Contrary to the bulk material, there was limited dependency of the constant life diagrams to mean stress. The notches present in the AM biomaterials were the sites of crack initiation. This observation and other evidence suggest that the notches created by the AM process cause the insensitivity of the fatigue life diagrams to mean stress. Feature tracking algorithms visualized the deformation during fatigue tests and demonstrated the root cause of inclined (45°) planes of specimen failure. In conclusion, the R-ratio behavior of AM porous biomaterials is both quantitatively and qualitatively different from that of bulk materials. Copyright © 2016 Elsevier Ltd. All rights reserved.

Hydro-mechanical behavior of Municipal Solid Waste subject to leachate recirculation in a large-scale compression reactor cell

DOE Office of Scientific and Technical Information (OSTI.GOV)

Olivier, Franck; Gourc, Jean-Pierre

2007-07-01

The paper presents the results of a laboratory experiment on Municipal Solid Waste (MSW) subjected to one-dimensional compression in a 1 m{sup 3} instrumented cell. The focus was on the hydro-mechanical behavior of the material under conditions of confinement and leachate percolation that replicate those found in real-scale landfills. The operation of the apparatus is detailed together with the testing methodology and the monitoring program. Two samples of waste were tested: the first extended over a period of 10 months ('Control Test') and the second for 22 months ('Enhanced Test' with leachate recirculation). Consolidation data is reported with regard tomore » both short-term (stress-dependent) and long-term (time-dependent) settlements. A discussion follows based on the derived values of primary and secondary compression ratios. Correlations between compression parameters and the biodegradation process are presented. In particular, results clearly highlight the effect of leachate recirculation on waste settlement: 24% secondary deformation reached after slightly less than 2 years (equivalent to a 5-fold increase in compressibility) and 17.9% loss of dry matter. Comparisons are proposed considering the results derived from the few monitoring programs conducted on experimental bioreactors worldwide. Finally, the hydraulic characterization of waste is discussed with regard to the evaluation of effective porosity and permeability.« less

Deformation Mechanism Map of Cu/Nb Nanoscale Metallic Multilayers as a Function of Temperature and Layer Thickness

DOE Office of Scientific and Technical Information (OSTI.GOV)

Snel, J.; Monclús, M. A.; Castillo-Rodríguez, M.

The mechanical properties and deformation mechanisms of Cu/Nb nanoscale metallic multilayers (NMMs) manufactured by accumulative roll bonding are studied at 25°C and 400°C. Cu/Nb NMMs with individual layer thicknesses between 7 nm and 63 nm were tested by in situ micropillar compression inside a scanning electron microscope. Yield strength, strain-rate sensitivities and activation volumes were obtained from the pillar compression tests. The deformed micropillars were examined under scanning and transmission electron microscopy in order to examine the deformation mechanisms active for different layer thicknesses and temperatures. The paper suggests that room temperature deformation was determined by dislocation glide at largermore » layer thicknesses and interface-related mechanisms at the thinner layer thicknesses. The high-temperature compression tests, in contrast, revealed superior thermo-mechanical stability and strength retention for the NMMs with larger layer thicknesses with deformation controlled by dislocation glide. A remarkable transition in deformation mechanism occurred as the layer thickness decreased, to a deformation response controlled by diffusion processes along the interfaces, which resulted in temperature-induced softening. Finally, a deformation mechanism map, in terms of layer thickness and temperature, is proposed from the results obtained in this investigation.« less

Deformation Mechanism Map of Cu/Nb Nanoscale Metallic Multilayers as a Function of Temperature and Layer Thickness

DOE PAGES

Snel, J.; Monclús, M. A.; Castillo-Rodríguez, M.; ...

2017-08-29

The mechanical properties and deformation mechanisms of Cu/Nb nanoscale metallic multilayers (NMMs) manufactured by accumulative roll bonding are studied at 25°C and 400°C. Cu/Nb NMMs with individual layer thicknesses between 7 nm and 63 nm were tested by in situ micropillar compression inside a scanning electron microscope. Yield strength, strain-rate sensitivities and activation volumes were obtained from the pillar compression tests. The deformed micropillars were examined under scanning and transmission electron microscopy in order to examine the deformation mechanisms active for different layer thicknesses and temperatures. The paper suggests that room temperature deformation was determined by dislocation glide at largermore » layer thicknesses and interface-related mechanisms at the thinner layer thicknesses. The high-temperature compression tests, in contrast, revealed superior thermo-mechanical stability and strength retention for the NMMs with larger layer thicknesses with deformation controlled by dislocation glide. A remarkable transition in deformation mechanism occurred as the layer thickness decreased, to a deformation response controlled by diffusion processes along the interfaces, which resulted in temperature-induced softening. Finally, a deformation mechanism map, in terms of layer thickness and temperature, is proposed from the results obtained in this investigation.« less

Buckling of Carbon Nanotubes: A State of the Art Review

PubMed Central

Shima, Hiroyuki

2011-01-01

The nonlinear mechanical response of carbon nanotubes, referred to as their “buckling" behavior, is a major topic in the nanotube research community. Buckling means a deformation process in which a large strain beyond a threshold causes an abrupt change in the strain energy vs. deformation profile. Thus far, much effort has been devoted to analysis of the buckling of nanotubes under various loading conditions: compression, bending, torsion, and their certain combinations. Such extensive studies have been motivated by (i) the structural resilience of nanotubes against buckling and (ii) the substantial influence of buckling on their physical properties. In this contribution, I review the dramatic progress in nanotube buckling research during the past few years. PMID:28817032

Ultrasonic characterization of plastic deformation in metals

NASA Technical Reports Server (NTRS)

Allison, S. G.; Heyman, J. S.; Salama, K.

1986-01-01

Acoustic tone burst spectroscopy is used to examine the effect of plastic deformation on higher order elastic properties of specimens of AISI 1016, 1045, 1095 and 8620 steel rods by measuring the stress acoustic constants (SACs). The SAC is found to be influenced by prestraining, and prestrain SAC measurements on 8620 steel demonstrate similar behavior to previously measured steels even though the composition of 8620 steel is significantly different. It is suggested from bias stress measurements that the stress acoustic response of prestrained 8620 steel is sensitive to the sign of the applied stress due to the different directions is which dislocations move under tension as opposed to compression, providing an approach to nondestructive testing of residual stress in steels.

Yield Asymmetry Design of Magnesium Alloys by Integrated Computational Materials Engineering

DOE Office of Scientific and Technical Information (OSTI.GOV)

Li, Dongsheng; Joshi, Vineet V.; Lavender, Curt A.

2013-11-01

Deformation asymmetry of magnesium alloys is an important factor on machine design in automobile industry. Represented by the ratio of compressive yield stress (CYS) against tensile yield stress (TYS), deformation asymmetry is strongly related to microstructure, characterized by texture and grain size. Modified intermediate phi-model, a polycrystalline viscoplasticity model, is used to predict the deformation behavior of magnesium alloys with different grain sizes. Validated with experimental results, integrated computational materials engineering is applied to find out the route in achieving desired asymmetry by thermomechanical processing. In some texture, for example, rolled texture, CYS/TYS is smaller than 1 under different loadingmore » directions. In some texture, for example, extruded texture, asymmetry is large along normal direction. Starting from rolled texture, the asymmetry will increased to close to 1 along rolling direction after compressed to a strain of 0.2. Our model shows that grain refinement increases CYS/TYS. Besides texture control, grain refinement can also optimize the yield asymmetry. After the grain size decreased to a critical value, CYS/TYS reaches to 1 since CYS increases much faster than TYS. By tailoring the microstructure using texture control and grain refinement, it is achievable to optimize yield asymmetry in wrought magnesium alloys.« less

Yield asymmetry design of magnesium alloys by integrated computational materials engineering

DOE Office of Scientific and Technical Information (OSTI.GOV)

Li, Dongsheng; Joshi, Vineet; Lavender, Curt

2013-11-01

Deformation asymmetry of magnesium alloys is an important factor on machine design in the automobile industry. Represented by the ratio of compressive yield stress (CYS) against tensile yield stress (TYS), deformation asymmetry is strongly related to texture and grain size. A polycrystalline viscoplasticity model, modified intermediate Φ-model, is used to predict the deformation behavior of magnesium alloys with different grain sizes. Validated with experimental results, integrated computational materials engineering is applied to find out the route in achieving desired asymmetry via thermomechanical processing. For example, CYS/TYS in rolled texture is smaller than 1 under different loading directions. In other textures,more » such as extruded texture, CYS/TYS is large along the normal direction. Starting from rolled texture, asymmetry will increase to close to 1 along the rolling direction after being compressed to a strain of 0.2. Our modified Φ-model also shows that grain refinement increases CYS/TYS. Along with texture control, grain refinement also can optimize the yield asymmetry. After the grain size decreases to a critical value, CYS/TYS reaches to 1 because CYS increases much faster than TYS. By tailoring the microstructure using texture control and grain refinement, it is achievable to optimize yield asymmetry in wrought magnesium alloys.« less

Estimating zero strain states of very soft tissue under gravity loading using digital image correlation⋆,⋆⋆,★

PubMed Central

Gao, Zhan; Desai, Jaydev P.

2009-01-01

This paper presents several experimental techniques and concepts in the process of measuring mechanical properties of very soft tissue in an ex vivo tensile test. Gravitational body force on very soft tissue causes pre-compression and results in a non-uniform initial deformation. The global Digital Image Correlation technique is used to measure the full field deformation behavior of liver tissue in uniaxial tension testing. A maximum stretching band is observed in the incremental strain field when a region of tissue passes from compression and enters a state of tension. A new method for estimating the zero strain state is proposed: the zero strain position is close to, but ahead of the position of the maximum stretching band, or in other words, the tangent of a nominal stress-stretch curve reaches minimum at λ ≳ 1. The approach, to identify zero strain by using maximum incremental strain, can be implemented in other types of image-based soft tissue analysis. The experimental results of ten samples from seven porcine livers are presented and material parameters for the Ogden model fit are obtained. The finite element simulation based on the fitted model confirms the effect of gravity on the deformation of very soft tissue and validates our approach. PMID:20015676

Buckling Behavior of Compression-Loaded Quasi-Isotropic Curved Panels with a Circular Cutout

NASA Technical Reports Server (NTRS)

Hilburger, Mark W.; Britt, Vicki O.; Nemeth, Michael P.

1999-01-01

Results from a numerical and experimental study of the response of compression-loaded quasi-isotropic curved panels with a centrally located circular cutout are presented. The numerical results were obtained by using a geometrically nonlinear finite element analysis code. The effects of cutout size, panel curvature and initial geo- metric imperfections on the overall response of compression-loaded panels are described. In addition, results are presented from a numerical parametric study that indicate the effects of elastic circumferential edge restraints on the prebuckling and buckling response of a selected panel and these numerical results are compared to experimentally measured results. These restraints are used to identify the effects of circumferential edge restraints that are introduced by the test fixture that was used in the present study. It is shown that circumferential edge restraints can introduce substantial nonlinear prebuckling deformations into shallow compression-loaded curved panels that can results in a significant increase in buckling load.

Jamming by compressing a system of granular crosses

NASA Astrophysics Data System (ADS)

Zheng, Hu; Wang, Dong; Barés, Jonathan; Behringer, Robert

2017-06-01

A disordered stress-free granular packing can be jammed, transformed into a mechanically rigid structure, by increasing the density of particles or by applying shear deformation. The jamming behavior of systems made of 2D circular discs has been investigated in detail, but very little is known about jamming for non-spherical particles, and particularly, non-convex particles. Here, we perform an experimental study on jamming by compression of a system of quasi-2D granular crosses made of photo-elastic crosses. We measure the pressure evolution during cyclic compression and decompression. The Jamming packing fraction of these quasi-2D granular crosses is ϕJ ≃ 0.475, which is much smaller than the value ϕJ ≃ 0.84 for-2D granular disks. The packing fraction shifts systematically to higher values under compressive cycling, corresponding to systematic shifts in the stress-strain response curves. Associated with these shifts are rotations of the crosses, with minimal changes in their centers of mass.

Wrinkles, folds, and plasticity in granular rafts

NASA Astrophysics Data System (ADS)

Jambon-Puillet, Etienne; Josserand, Christophe; Protière, Suzie

2017-09-01

We investigate the mechanical response of a compressed monolayer of large and dense particles at a liquid-fluid interface: a granular raft. Upon compression, rafts first wrinkle; then, as the confinement increases, the deformation localizes in a unique fold. This characteristic buckling pattern is usually associated with floating elastic sheets, and as a result, particle laden interfaces are often modeled as such. Here, we push this analogy to its limits by comparing quantitative measurements of the raft morphology to a theoretical continuous elastic model of the interface. We show that, although powerful to describe the wrinkle wavelength, the wrinkle-to-fold transition, and the fold shape, this elastic description does not capture the finer details of the experiment. We describe an unpredicted secondary wavelength, a compression discrepancy with the model, and a hysteretic behavior during compression cycles, all of which are a signature of the intrinsic discrete and frictional nature of granular rafts. It suggests also that these composite materials exhibit both plastic transition and jamming dynamics.

Numerical and Experimental Studies on Crash Characteristics of Closed Form Thin—Walled Steel Sections

NASA Astrophysics Data System (ADS)

Veerasamy, M.; Srinivasan, K.; Prakash, Raghu V.

2010-10-01

The crash behavior of Cold Rolled Mild Steel (CRMS) closed form thin section was studied by conducting compressive tests at loading velocities of 5 mm/min and 1000 mm/min. The numerical simulations were conducted for the same experimental conditions to understand the deformation shape, peak forces and energy absorption capacity of sections at different impact velocities. The simulation results correlated well with the experimental results.

Residual Stress Reversal in Highly Strained Shot Peened Structural Elements. Degree awarded by Florida Univ.

NASA Technical Reports Server (NTRS)

Mitchell, William S.; Throckmorton, David (Technical Monitor)

2002-01-01

The purpose of this research was to further the understanding of a crack initiation problem in a highly strained pressure containment housing. Finite Element Analysis methods were used to model the behavior of shot peened materials undergoing plastic deformation. Analytical results are in agreement with laboratory tensile tests that simulated the actual housing load conditions. These results further validate the original investigation finding that the shot peened residual stress had reversed, changing from compressive to tensile, and demonstrate that analytical finite element methods can be used to predict this behavior.

Superelastic carbon spheres under high pressure

NASA Astrophysics Data System (ADS)

Li, Meifen; Guo, Junjie; Xu, Bingshe

2013-03-01

We report a superelastic deformation behavior of carbon spheres by the in situ Raman spectroscopy in a high-pressure diamond anvil cell. The carbon spheres produced by arc discharging in toluene have a mean diameter of 200 nm and an onion-like multilayer graphitic structure. We find that the elastic coefficients, during both the compression and decompression processes, remain a constant up to 10 GPa, indicating a superior high-pressure structural stability. Such superelastic behavior is related to the isotropic and concentric configuration of carbon spheres and provides additional insight into improving the microscopic mechanical properties of small-scale particles.

Flexural and compressive mechanical behaviors of the porous titanium materials with entangled wire structure at different sintering conditions for load-bearing biomedical applications.

PubMed

He, Guo; Liu, Ping; Tan, Qingbiao; Jiang, Guofeng

2013-12-01

The entangled titanium materials with various porosities have been investigated in terms of the flexural and compressive mechanical properties and the deformation and failure modes. The effect of the sintering parameters on the mechanical properties and the porosity reduction has been comprehensively studied. The results indicate that both the flexural and compressive mechanical properties increase significantly as the porosity decreases. In the porosity range investigated the flexural elastic modulus is in the range of 0.05-6.33GPa, the flexural strength is in the range of 9.8-324.9MPa, the compressive elastic modulus is in the range of 0.03-2.25GPa, and the compressive plateau stress is in the range of 2.3-147.8MPa. The mechanical properties of the entangled titanium materials can be significantly improved by sintering, which increase remarkably as the sintering temperature and/or the sintering time increases. But on other hand, the sintering process can induce the porosity reduction due to the oxidation on the titanium wire surface. © 2013 Elsevier Ltd. All rights reserved.

The application of continuum damage mechanics to solve problems in geodynamics

NASA Astrophysics Data System (ADS)

Manaker, David Martin

Deformation within the Earth's lithosphere is largely controlled by the rheology of the rock. Ductile behavior in rocks is often associated with plasticity due to dislocation motion or diffusion under high pressures and temperatures. However, ductile behavior can also occur in brittle materials. An example would be cataclastic flow associated with folding at shallow crustal levels, steep subduction zones, and large-scale deformation at plate boundaries. Engineers utilize damage mechanics to model the continuum deformation of brittle materials. We utilize a modified form of damage mechanics where damage represents a reduction in frictional strength and includes a yield stress. We use this empirical approach to simulate the bending of the lithosphere. We use numerical simulations to obtain elastostatic solutions for plate bending and where the stress exceeds a yield stress, we apply damage to reduce the elastic moduli. Damage is calculated at each time step by a power-law relationship of the ratio of the yield stress to stress and the yield strain to the strain. To test our method, we apply our damage rheology to a plate deforming under applied shear, a constant bending moment, and a constant load. We simulate a wide range of behaviors from slow relaxation to instantaneous failure, over timescales that span six orders of magnitude. Stress relaxation produces elastic-perfectly plastic behavior in cases where failure does not occur. For cases of failure, we observe a rapid increase in damage leading to failure. The changes in the rate of damage accumulation in failure cases are similar to the changes in b-values of acoustic emissions observed in triaxial compression tests of fractured rock and b-value changes prior to some large earthquakes. Thus continuum damage mechanics can simulate ductile behavior due to brittle mechanisms as well as observations of laboratory experiments and seismicity.

Study on elevated-temperature flow behavior of Ni-Cr-Mo-B ultra-heavy-plate steel via experiment and modelling

NASA Astrophysics Data System (ADS)

Gao, Zhi-yu; Kang, Yu; Li, Yan-shuai; Meng, Chao; Pan, Tao

2018-04-01

Elevated-temperature flow behavior of a novel Ni-Cr-Mo-B ultra-heavy-plate steel was investigated by conducting hot compressive deformation tests on a Gleeble-3800 thermo-mechanical simulator at a temperature range of 1123 K–1423 K with a strain rate range from 0.01 s‑1 to10 s‑1 and a height reduction of 70%. Based on the experimental results, classic strain-compensated Arrhenius-type, a new revised strain-compensated Arrhenius-type and classic modified Johnson-Cook constitutive models were developed for predicting the high-temperature deformation behavior of the steel. The predictability of these models were comparatively evaluated in terms of statistical parameters including correlation coefficient (R), average absolute relative error (AARE), average root mean square error (RMSE), normalized mean bias error (NMBE) and relative error. The statistical results indicate that the new revised strain-compensated Arrhenius-type model could give prediction of elevated-temperature flow stress for the steel accurately under the entire process conditions. However, the predicted values by the classic modified Johnson-Cook model could not agree well with the experimental values, and the classic strain-compensated Arrhenius-type model could track the deformation behavior more accurately compared with the modified Johnson-Cook model, but less accurately with the new revised strain-compensated Arrhenius-type model. In addition, reasons of differences in predictability of these models were discussed in detail.

Deformation Characteristics and Recrystallization Response of a 9310 Steel Alloy

NASA Astrophysics Data System (ADS)

Snyder, David; Chen, Edward Y.; Chen, Charlie C.; Tin, Sammy

2013-01-01

The flow behavior and recrystallization response of a 9310 steel alloy deformed in the ferrite temperature range were studied in this work. Samples were compressed under various conditions of strain (0.6, 0.8 and multi-axial), strain rate (10-4 seconds-1 to 10-1 seconds-1) and temperature [811 K to 1033 K (538 °C to 760 °C)] using a Gleeble thermo-mechanical simulator. Deformation was characterized by both qualitative and quantitative means, using standard microscopy, electron backscatter diffraction (EBSD) analysis and flow stress modeling. The results indicate that deformation is primarily accommodated through dynamic recovery in sub-grain formation. EBSD analysis shows a continuous increase in sub-grain boundary misorientation with increasing strain, ultimately producing recrystallized grains from the sub-grains at high strains. This suggests that a sub-grain rotation recrystallization mechanism predominates in this temperature range. Analyses of the results reveal a decreasing mean dynamically recrystallized grain size with increasing Zener-Hollomon parameter, and an increasing recrystallized fraction with increasing strain.

Elevated temperature deformation of thoria dispersed nickel-chromium

NASA Technical Reports Server (NTRS)

Kane, R. D.; Ebert, L. J.

1974-01-01

The deformation behavior of thoria nickel-chromium (TD-NiCr) was examined over the temperature range 593 C (1100 F) to 1260 C (2300 F) in tension and compression and at 1093 C (2000 F) in creep. Major emphasis was placed on: (1) the effects of the material and test related variables (grain size, temperature, stress and strain rate) on the deformation process; and (2) the evaluation of single crystal TD-NiCr material produced by a directional recrystallization process. Elevated temperature yield strength levels and creep activation enthalpies were found to increase with increasing grain size reaching maximum values for the single crystal TD-NiCr. Stress exponent of the steady state creep rate was also significantly higher for the single crystal TD-NiCr as compared to that determined for the polycrystalline materials. The elevated temperature deformation of TD-NiCr was analyzed in terms of two concurrent, parallel processes: diffusion controlled grain boundary sliding, and dislocation motion.

Time-dependent deformation of polymer network in polymer-stabilized cholesteric liquid crystals (Conference Presentation)

NASA Astrophysics Data System (ADS)

Lee, Kyung Min; Tondiglia, Vincent P.; Bunning, Timothy J.; White, Timothy J.

2017-02-01

Recently, we reported direct current (DC) field controllable electro-optic (EO) responses of negative dielectric anisotropy polymer stabilized cholesteric liquid crystals (PSCLCs). A potential mechanism is: Ions in the liquid crystal mixtures are trapped in/on the polymer network during the fast photopolymerization process, and the movement of ions by the application of the DC field distorts polymer network toward the negative electrode, inducing pitch variation through the cell thickness, i.e., pitch compression on the negative electrode side and pitch expansion on positive electrode side. As the DC voltage is directly applied to a target voltage, charged polymer network is deformed and the reflection band is tuned. Interestingly, the polymer network deforms further (red shift of reflection band) with time when constantly applied DC voltage, illustrating DC field induced time dependent deformation of polymer network (creep-like behavior). This time dependent reflection band changes in PSCLCs are investigated by varying the several factors, such as type and concentration of photoinitiators, liquid crystal monomer content, and curing condition (UV intensity and curing time). In addition, simple linear viscoelastic spring-dashpot models, such as 2-parameter Kelvin and 3-parameter linear models, are used to investigate the time-dependent viscoelastic behaviors of polymer networks in PSCLC.

Finite element simulation of the T-shaped ECAP processing of round samples

NASA Astrophysics Data System (ADS)

Shaban Ghazani, Mehdi; Fardi-Ilkhchy, Ali; Binesh, Behzad

2018-05-01

Grain refinement is the only mechanism that increases the yield strength and toughness of the materials simultaneously. Severe plastic deformation is one of the promising methods to refine the microstructure of materials. Among different severe plastic deformation processes, the T-shaped equal channel angular pressing (T-ECAP) is a relatively new technique. In the present study, finite element analysis was conducted to evaluate the deformation behavior of metals during T-ECAP process. The study was focused mainly on flow characteristics, plastic strain distribution and its homogeneity, damage development, and pressing force which are among the most important factors governing the sound and successful processing of nanostructured materials by severe plastic deformation techniques. The results showed that plastic strain is localized in the bottom side of sample and uniform deformation cannot be possible using T-ECAP processing. Friction coefficient between sample and die channel wall has a little effect on strain distributions in mirror plane and transverse plane of deformed sample. Also, damage analysis showed that superficial cracks may be initiated from bottom side of sample and their propagation will be limited due to the compressive state of stress. It was demonstrated that the V shaped deformation zone are existed in T-ECAP process and the pressing load needed for execution of deformation process is increased with friction.

Experimental Evaluation of the Taylor-Type Polycrystal Model for the Finite Deformation of an FCC Metal (OFHC Copper)

DTIC Science & Technology

1991-05-01

was received as bar stocks in the work hardened condition. Before machining, the copper rods were annealed at 400 °C in argon for one hour. This...ABSTRACT Large deformation uniaxial compression and fixed-end torsion (simple shear) experiments were conducted on annealed OFHC Copper to obtain its... annealing treatment produced an average grain diameter of 45 jim. Experimental Procedure Compression Tests All the compression tests were conducted with

Large-deformation and high-strength amorphous porous carbon nanospheres

NASA Astrophysics Data System (ADS)

Yang, Weizhu; Mao, Shimin; Yang, Jia; Shang, Tao; Song, Hongguang; Mabon, James; Swiech, Wacek; Vance, John R.; Yue, Zhufeng; Dillon, Shen J.; Xu, Hangxun; Xu, Baoxing

2016-04-01

Carbon is one of the most important materials extensively used in industry and our daily life. Crystalline carbon materials such as carbon nanotubes and graphene possess ultrahigh strength and toughness. In contrast, amorphous carbon is known to be very brittle and can sustain little compressive deformation. Inspired by biological shells and honeycomb-like cellular structures in nature, we introduce a class of hybrid structural designs and demonstrate that amorphous porous carbon nanospheres with a thin outer shell can simultaneously achieve high strength and sustain large deformation. The amorphous carbon nanospheres were synthesized via a low-cost, scalable and structure-controllable ultrasonic spray pyrolysis approach using energetic carbon precursors. In situ compression experiments on individual nanospheres show that the amorphous carbon nanospheres with an optimized structure can sustain beyond 50% compressive strain. Both experiments and finite element analyses reveal that the buckling deformation of the outer spherical shell dominates the improvement of strength while the collapse of inner nanoscale pores driven by twisting, rotation, buckling and bending of pore walls contributes to the large deformation.

Measurement of the through thickness compression of a battery separator

NASA Astrophysics Data System (ADS)

Yan, Shutian; Huang, Xiaosong; Xiao, Xinran

2018-04-01

The mechanical integrity of the separator is critical to the reliable operation of a battery. Due to its minimal thickness, compression experiments with a single/a few layers of separator are difficult to perform. In this work, a capacitance based displacement set-up has been developed for the measurement of the through thickness direction (TTD) compression stress-strain behavior of the separator and the investigation of its interaction with the electrode. The experiments were performed for a stack of two layers of Celgard 2400 separator, NMC cathode, and separator/NMC cathode/separator stack in both dry and wet (i.e. submersed in dimethyl carbonate DMC) conditions. The experimental results reveal that the separator compression modulus can be significantly affected by the presence of DMC. The iso-stress based rule of mixtures was used to compute the compressive stress-strain curve for the stack from that of the separator and NMC layer. The computed curve agreed with the experimental curve reasonably well up to about 0.16 strain but deviated significantly to a softer response at higher strains. The results suggest that, in the stack, the TTD compressive deformation of the separator is influenced by the NMC cathode.

An analytical study of the effects of transverse shear deformation and anisotropy on buckling loads of laminated cylinders. M.S. Thesis - George Washington Univ.

NASA Technical Reports Server (NTRS)

Jegley, Dawn C.

1987-01-01

Buckling loads of thick-walled orthotropic and anisotropic simply supported circular cylinders are predicted using a higher-order transverse-shear deformation theory. A comparison of buckling loads predicted by the conventional first-order transverse-shear deformation theory and the higher-order theory show that the additional allowance for transverse shear deformation has a negligible effect on the predicted buckling loads of medium-thick metallic isotropic cylinders. However, the higher-order theory predicts buckling loads which are significantly lower than those predicted by the first-order transverse-shear deformation theory for certain short, thick-walled cylinders which have low through-the-thickness shear moduli. A parametric study of the effects of ply orientation on the buckling load of axially compressed cylinders indicates that laminates containing 45 degree plies are most sensitive to transverse-shear deformation effects. Interaction curves for buckling loads of cylinders subjected to axial compressive and external pressure loadings indicate that buckling loads due to external pressure loadings are as sensitive to transverse-shear deformation effects as buckling loads due to axial compressive loadings. The effects of anisotropy are important over a much wider range of cylinder geometries than the effects of transverse shear deformation.

1200 to 1400 K slow strain rate compressive properties of NiAl/Ni2AlTi-base materials

NASA Technical Reports Server (NTRS)

Whittenberger, J. Daniel; Viswanadham, R. K.; Mannan, S. K.; Kumar, K. S.

1989-01-01

An attempt to apply the Martin Marietta Corporation's XD technology to the fabrication of NiAl-Ni2AlTi materials with improved creep properties is presented. Composite materials, containing from 0 to 30 vol pct of nominally 1-micron-diameter TiB2 particles in the intermetallic matrix have been produced by the XD process and compacted by hot pressing. Such composites demonstrated significant strength increases, approaching 3-fold for the 20 vol pct materials, in comparison to the unreinforced aluminide. This behavior was accomplished without deleterious side effects as the grain boundaries and particle-matrix interfaces were intact after compressive deformation to 10 percent or more strain. Typical true compressive stress-strain diagrams for materials tested in air between 1200 and 1400 K at approximate strain rates of 1.7 x 10 to the -6th/sec are presented.

A kinematic hardening constitutive model for the uniaxial cyclic stress-strain response of magnesium sheet alloys at room temperature

NASA Astrophysics Data System (ADS)

He, Zhitao; Chen, Wufan; Wang, Fenghua; Feng, Miaolin

2017-11-01

A kinematic hardening constitutive model is presented, in which a modified form of von Mises yield function is adopted, and the initial asymmetric tension and compression yield stresses of magnesium (Mg) alloys at room temperature (RT) are considered. The hardening behavior was classified into slip, twinning, and untwinning deformation modes, and these were described by two forms of back stress to capture the mechanical response of Mg sheet alloys under cyclic loading tests at RT. Experimental values were obtained for AZ31B-O and AZ31B sheet alloys under both tension-compression-tension (T-C-T) and compression-tension (C-T) loadings to calibrate the parameters of back stresses in the proposed model. The predicted parameters of back stresses in the twinning and untwinning modes were expressed as a cubic polynomial. The predicted curves based on these parameters showed good agreement with the tests.

Improvement of the Assignment Methodology of the Approach Embankment Design to Highway Structures in Difficult Conditions

NASA Astrophysics Data System (ADS)

Chistyy, Y.; Kuzakhmetova, E.; Fazilova, Z.; Tsukanova, O.

2018-03-01

Design issues of junction of bridges and overhead road with approach embankment are studied. The reasons for the formation of deformations in the road structure are indicated. Activities to ensure sustainability and acceleration of the shrinkage of a weak subgrade approach embankment are listed. The necessity of taking into account the man-made impact of the approach embankment on the subgrade behavior is proved. Modern stabilizing agents to improve the properties of used soils in the embankment and the subgrade are suggested. Clarified methodology for determining an active zone of compression in the subgrade under load from the weight of the embankment is described. As an additional condition to the existing methodology for establishing the lower bound of the active zone of compression it is offered to accept the accuracy of evaluation of soil compressibility and determine shrinkage.

Acoustic Behavior of Subfloor Lightweight Mortars Containing Micronized Poly (Ethylene Vinyl Acetate) (EVA)

PubMed Central

Brancher, Luiza R.; Nunes, Maria Fernanda de O.; Grisa, Ana Maria C.; Pagnussat, Daniel T.; Zeni, Mára

2016-01-01

This paper aims to contribute to acoustical comfort in buildings by presenting a study about the polymer waste micronized poly (ethylene vinyl acetate) (EVA) to be used in mortars for impact sound insulation in subfloor systems. The evaluation method included physical, mechanical and morphological properties of the mortar developed with three distinct thicknesses designs (3, 5, and 7 cm) with replacement percentage of the natural aggregate by 10%, 25%, and 50% EVA. Microscopy analysis showed the surface deposition of cement on EVA, with preservation of polymer porosity. The compressive creep test estimated long-term deformation, where the 10% EVA sample with a 7 cm thick mortar showed the lowest percentage deformation of its height. The impact noise test was performed with 50% EVA samples, reaching an impact sound insulation of 23 dB when the uncovered slab was compared with the 7 cm thick subfloor mortar. Polymer waste addition decreased the mortar compressive strength, and EVA displayed characteristics of an influential material to intensify other features of the composite. PMID:28787851

Large Strain Behaviour of ZEK100 Magnesium Alloy at Various Strain Rates

NASA Astrophysics Data System (ADS)

Lévesque, Julie; Kurukuri, Srihari; Mishra, Raja; Worswick, Michael; Inal, Kaan

A constitutive framework based on a rate-dependent crystal plasticity theory is employed to simulate large strain deformation in hexagonal closed-packed metals that deform by slip and twinning. The model allows the twinned zones and the parent matrix to rotate independently. ZEK100 magnesium alloy sheets which significant texture weakening compared to AZ31 sheets are investigated using the model. There is considerable in-plane anisotropy and tension compression asymmetry in the flow behavior of ZEK100. Simulations of uniaxial tension in different directions at various strain rates and the accompanying texture evolution are performed and they are in very good agreement with experimental measurements. The effect of strain rate on the activation of the various slip systems and twinning show that differences in the strain rate dependence of yield stress and Rvalues in ZEK100 have their origin in the activation of different deformation mechanisms.

Modeling multiscale evolution of numerous voids in shocked brittle material.

PubMed

Yu, Yin; Wang, Wenqiang; He, Hongliang; Lu, Tiecheng

2014-04-01

The influence of the evolution of numerous voids on macroscopic properties of materials is a multiscale problem that challenges computational research. A shock-wave compression model for brittle material, which can obtain both microscopic evolution and macroscopic shock properties, was developed using discrete element methods (lattice model). Using a model interaction-parameter-mapping procedure, qualitative features, as well as trends in the calculated shock-wave profiles, are shown to agree with experimental results. The shock wave splits into an elastic wave and a deformation wave in porous brittle materials, indicating significant shock plasticity. Void collapses in the deformation wave were the natural reason for volume shrinkage and deformation. However, media slippage and rotation deformations indicated by complex vortex patterns composed of relative velocity vectors were also confirmed as an important source of shock plasticity. With increasing pressure, the contribution from slippage deformation to the final plastic strain increased. Porosity was found to determine the amplitude of the elastic wave; porosity and shock stress together determine propagation speed of the deformation wave, as well as stress and strain on the final equilibrium state. Thus, shock behaviors of porous brittle material can be systematically designed for specific applications.

Evolution of Mechanical Properties and Microstructures in the Inner Accretionary Prism of the Nankai Subduction Zone

NASA Astrophysics Data System (ADS)

Kuo, S. T.; Kitamura, M.; Kitajima, H.

2016-12-01

Mechanical properties and microstructural characteristics of accretionary prism sediments can provide detailed deformation history and processes in subduction zones. The IODP Nankai Trough Seismogenic Zone Experiment (NanTroSEIZE) Expedition 348 has extended the deep riser hole down to 3058.5 meters below sea floor (mbsf) to the inner accretionary wedge at Site C0002 located 35 km landward from the trench. Here, we conducted deformation experiments on the core samples recovered from 2185 msbf at Site C0002 to understand mechanical behaviors and deformation of inner prism sediments. We deformed the siltstone samples with a porosity of 20% at 25°C or 60°C under isotropic loading path (S1=S2=S3) and triaxial compression (S1>S2=S3). In the isotropic loading test, we step-wisely increased confining pressure (Pc) from 11.5 to 194 MPa and kept pore pressure (Pp) at 10 MPa. In a series of triaxial compression loading tests, we first increased Pc to the targeting 42-78 MPa and Pp to 20 MPa, and then applied the differential load at a constant displacement rate of 0.005 μm/s while keeping Pc and Pp constant. We will analyze the microstructures of the experimentally deformed samples to understand deformation mechanism. We define yield points based on slope changes in relationships between volumetric strain and effective mean stress (p') for isotropic loading and those between differential stress (q) and axial strain for triaxial loading. The sample yields at p' of 100 MPa (q = 0 MPa) in isotropic loading test. In triaxial loading, the samples at effective pressure (Pe) of 22, 28, and 58 MPa yield at q = 30 MPa (p' = 32 MPa), q = 30 MPa (p' = 38 MPa) and q = 45 MPa (p' = 73 MPa), respectively. Upon yield, the samples deformed at Pe of 22 MPa and 28 MPa show brittle behavior with a peak q of 50 MPa and 55 MPa followed by strain weakening to reach q of 36 and 46 MPa at steady state. Both samples show single fracture planes with angles of 30° to S1. On the other hand, the sample at Pe of 58 MPa shows strain hardening after the yield and exhibits barreling. In triaxial loading experiments, all samples show an increase in volumetric strain with increasing Pe. Our experiment results at different Pe are consistent with a critical state soil mechanics theory. We will further correlate the microstructural features of the deformed samples with the mechanical data.

Grain size dependence of dynamic mechanical behavior of AZ31B magnesium alloy sheet under compressive shock loading

DOE Office of Scientific and Technical Information (OSTI.GOV)

Asgari, H., E-mail: hamed.asgari@usask.ca; Odeshi, A.G.; Szpunar, J.A.

2015-08-15

The effects of grain size on the dynamic deformation behavior of rolled AZ31B alloy at high strain rates were investigated. Rolled AZ31B alloy samples with grain sizes of 6, 18 and 37 μm, were subjected to shock loading tests using Split Hopkinson Pressure Bar at room temperature and at a strain rate of 1100 s{sup −} {sup 1}. It was found that a double-peak basal texture formed in the shock loaded samples. The strength and ductility of the alloy under the high strain-rate compressive loading increased with decreasing grain size. However, twinning fraction and strain hardening rate were found tomore » decrease with decreasing grain size. In addition, orientation imaging microscopy showed a higher contribution of double and contraction twins in the deformation process of the coarse-grained samples. Using transmission electron microscopy, pyramidal dislocations were detected in the shock loaded sample, proving the activation of pyramidal slip system under dynamic impact loading. - Highlights: • A double-peak basal texture developed in all shock loaded samples. • Both strength and ductility increased with decreasing grain size. • Twinning fraction and strain hardening rate decreased with decreasing grain size. • ‘g.b’ analysis confirmed the presence of dislocations in shock loaded alloy.« less

Dynamic Recrystallization Behavior and Corrosion Resistance of a Dual-Phase Mg-Li Alloy

PubMed Central

Liu, Gang; Xie, Wen; Wei, Guobing; Yang, Yan; Liu, Junwei; Xu, Tiancai; Xie, Weidong; Peng, Xiaodong

2018-01-01

The hot deformation and dynamic recrystallization behavior of the dual-phase Mg-9Li-3Al-2Sr-2Y alloy had been investigated using a compression test. The typical dual-phase structure was observed, and average of grain size of as-homogenized alloy is about 110 µm. It mainly contains β-Li, α-Mg, Al4Sr and Al2Y phases. The dynamic recrystallization (DRX) kinetic was established based on an Avrami type equation. The onset of the DRX process occurred before the peak of the stress–strain flow curves. It shows that the DRX volume fraction increases with increasing deformation temperature or decreasing strain rate. The microstructure evolution during the hot compression at various temperatures and strain rates had been investigated. The DRX grain size became larger with the increasing testing temperature or decreasing strain rate because the higher temperature or lower strain rate can improve the migration of DRX grain boundaries. The fully recrystallized microstructure can be achieved in a small strain due to the dispersed island-shape α-Mg phases, continuous the Al4Sr phases and spheroidal Al2Y particles, which can accelerate the nucleation. The continuous Al4Sr phases along the grain boundaries are very helpful for enhancing the corrosion resistance of the duplex structured Mg-Li alloy, which can prevent the pitting corrosion and filiform corrosion. PMID:29522473

Dynamic Recrystallization Behavior and Corrosion Resistance of a Dual-Phase Mg-Li Alloy.

PubMed

Liu, Gang; Xie, Wen; Wei, Guobing; Yang, Yan; Liu, Junwei; Xu, Tiancai; Xie, Weidong; Peng, Xiaodong

2018-03-09

The hot deformation and dynamic recrystallization behavior of the dual-phase Mg-9Li-3Al-2Sr-2Y alloy had been investigated using a compression test. The typical dual-phase structure was observed, and average of grain size of as-homogenized alloy is about 110 µm. It mainly contains β-Li, α-Mg, Al₄Sr and Al₂Y phases. The dynamic recrystallization (DRX) kinetic was established based on an Avrami type equation. The onset of the DRX process occurred before the peak of the stress-strain flow curves. It shows that the DRX volume fraction increases with increasing deformation temperature or decreasing strain rate. The microstructure evolution during the hot compression at various temperatures and strain rates had been investigated. The DRX grain size became larger with the increasing testing temperature or decreasing strain rate because the higher temperature or lower strain rate can improve the migration of DRX grain boundaries. The fully recrystallized microstructure can be achieved in a small strain due to the dispersed island-shape α-Mg phases, continuous the Al₄Sr phases and spheroidal Al₂Y particles, which can accelerate the nucleation. The continuous Al₄Sr phases along the grain boundaries are very helpful for enhancing the corrosion resistance of the duplex structured Mg-Li alloy, which can prevent the pitting corrosion and filiform corrosion.

Modelling deformation and fracture in confectionery wafers

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mohammed, Idris K.; Charalambides, Maria N.; Williams, J. Gordon

2015-01-22

The aim of this research is to model the deformation and fracture behaviour of brittle wafers often used in chocolate confectionary products. Three point bending and compression experiments were performed on beam and circular disc samples respectively to determine the 'apparent' stress-strain curves in bending and compression. The deformation of the wafer for both these testing types was observed in-situ within an SEM. The wafer is modeled analytically and numerically as a composite material with a core which is more porous than the skins. X-ray tomography was used to generate a three dimensional volume of the wafer microstructure which wasmore » then meshed and used for quantitative analysis. A linear elastic material model, with a damage function and element deletion, was used and the XMT generated architecture was loaded in compression. The output from the FE simulations correlates closely to the load-deflection deformation observed experimentally.« less

Highly deformation-tolerant carbon nanotube sponges as supercapacitor electrodes.

PubMed

Li, Peixu; Kong, Chuiyan; Shang, Yuanyuan; Shi, Enzheng; Yu, Yuntao; Qian, Weizhong; Wei, Fei; Wei, Jinquan; Wang, Kunlin; Zhu, Hongwei; Cao, Anyuan; Wu, Dehai

2013-09-21

Developing flexible and deformable supercapacitor electrodes based on porous materials is of high interest in energy related fields. Here, we show that carbon nanotube sponges, consisting of highly porous conductive networks, can serve as compressible and deformation-tolerant supercapacitor electrodes in aqueous or organic electrolytes. In aqueous electrolytes, the sponges maintain a similar specific capacitance (>90% of the original value) under a predefined compressive strain of 50% (corresponding to a volume reduction of 50%), and retain more than 70% of the original capacitance under 80% strain while the volume normalized capacitance increases by 3-fold. The sponge electrode maintains a stable performance after 1000 large strain compression cycles. A coin-shaped cell assembled with these sponges shows excellent stability over 15,000 charging cycles with negligible degradation after 500 cycles. Our results indicate that carbon nanotube sponges have the potential to fabricate deformable supercapacitor electrodes with stable performance.

Modelling deformation and fracture in confectionery wafers

NASA Astrophysics Data System (ADS)

Mohammed, Idris K.; Charalambides, Maria N.; Williams, J. Gordon; Rasburn, John

2015-01-01

The aim of this research is to model the deformation and fracture behaviour of brittle wafers often used in chocolate confectionary products. Three point bending and compression experiments were performed on beam and circular disc samples respectively to determine the 'apparent' stress-strain curves in bending and compression. The deformation of the wafer for both these testing types was observed in-situ within an SEM. The wafer is modeled analytically and numerically as a composite material with a core which is more porous than the skins. X-ray tomography was used to generate a three dimensional volume of the wafer microstructure which was then meshed and used for quantitative analysis. A linear elastic material model, with a damage function and element deletion, was used and the XMT generated architecture was loaded in compression. The output from the FE simulations correlates closely to the load-deflection deformation observed experimentally.

The Deformation Behavior and Microstructure Evolution of a Mn- and Cr-Containing Al-Mg-Si-Cu Alloy During Hot Compression and Subsequent Heat Treatment

NASA Astrophysics Data System (ADS)

Xu, Yi; Nagaumi, Hiromi; Han, Yi; Zhang, Gongwang; Zhai, Tongguang

2017-03-01

Hot compression tests on a newly developed Mn- and Cr-containing Al-Mg-Si-Cu alloy were carried out at temperatures ranging from 623 K (350 °C) to 823 K (550 °C) and strain rates between 0.001 and 1 s-1 after casting and subsequent homogenization heat treatment. The true stress-true strain curves of the alloy exhibited a peak stress at a small plastic strain followed by dynamic flow softening. Using the constitutive equation containing the strain rate, peak stress, and temperature, the activation energy for hot deformation in the alloy was determined to be 249.67 kJ/mol, much higher than that (143.4 kJ/mol) for self-diffusion in pure Al. Scanning transmission electron microscopy experiments revealed that Mn- and Cr-containing α-dispersoids formed during homogenization showed a strong pinning effect on dislocations and grain boundaries, which was responsible for the increase in activation energy for hot deformation in the alloy. A threshold stress was consequently introduced and determined in the constitutive equation to count for the dispersoid hardening effect on hot deformation in the alloy. Electron back-scatter diffraction measurements revealed that the softening occurred in the alloy was mainly due to dynamic recovery taking place at relatively large Z values, and that it was dominated by continuous dynamic recrystallization at relatively low Z. In subsequent annealing after hot deformation at large Z, abnormal grain growth could occur, as a result of the critical strain-annealing effect. After upsetting at higher temperatures, the alloy showed superior tensile properties due to a high non-recrystallized area fraction.

Effects of varying material properties on the load deformation characteristics of heel cushions.

PubMed

Sun, Pi-Chang; Wei, Hung-Wen; Chen, Chien-Hua; Wu, Chun-Hao; Kao, Hung-Chan; Cheng, Cheng-Kung

2008-07-01

Various insole materials were used in attenuation of heel-strike impact. This study presented a compression test to investigate the deformation characteristics of common heel cushions. There were two materials (thermoplastic elastomer "TPE" and silicone) with three hardness and six thickness being analyzed. They underwent consecutive loading-unloading cycles with a load control mode. The displacement of material thickness was recorded during cyclic compression being applied and released from 0 to 1050 N. The energy input, return and dissipation were evaluated based on the load deformation curves when new and after repeated compression. The TPE recovered more deformed energy and thickness than the silicone after the first loading cycle. The silicone would preserve more strain energy with increasing its hardness for the elastic recovery in the unloading process. The deformed energy was decreased as the original thickness did not completely recover under cyclic tests. The reduction in hysteresis area was gradually converged within 20 cycles. The silicone attenuated more impact energy in the initial cycles, but its energy dissipation was reduced after repeated loading. To increase hardness or thickness should be considered to improve resilience or accommodate persistent compression without flattening. The careful selection of cushion materials is imperative to meet individual functional demands.

Bacterial Polymertropism, the Response to Strain-Induced Alignment of Polymers

NASA Astrophysics Data System (ADS)

Lemon, David J.

In nature, bacteria often live in surface-associated communities known as biofilms. Biofilm-forming bacteria deposit a layer of polysaccharide on the surfaces they inhabit; hence, polysaccharide is their immediate environment on any surface. In this study, we examined how the physical characteristics of polysaccharide substrates influence the behavior of the biofilm-forming bacterium Myxococcus xanthus. M. xanthus colonies, and indeed those of the majority of biofilm-forming species tested, respond to the compression-induced deformation of polysaccharide substrates by preferentially spreading across the surface perpendicular to the axis of compression. This response is conserved across multiple distantly related phyla and is found in species with an array of distinct motility apparatuses.The birefringence and small angle X-ray scattering patterns of compressed polysaccharide substrates indicate that the directed surface movements of these bacteria consistently match the orientation of the long axes of aligned and tightly packed polysaccharide fibers in compressed substrates. Therefore, we refer to this behavior as polymertropism to denote that the directed movements are a response to the physical arrangement of the change in packing and alignment of the polymers in the substrate. In addition to altering the colony morphology we find the behavior of groups of cells, called flares, is also affected in several species resulting in increased flare speed, duration, and displacement on compressed gel substrates.We suggest that polymertropism, which requires a downward-facing motility apparatus in M. xanthus, may be responsible for the observed tendency of bacterial cells to follow trails of extruded and presumably aligned polysaccharides, which their neighbors secrete and deposit on the substrate as they move across it. Polymertropism may also play a role in the organization of bacteria in a biofilm, as the iterative process of polysaccharide trail deposition and following is proposed to yield aggregates of cells.

Finite Element Modeling of Multilayer Orthogonal Auxetic Composites under Low-Velocity Impact

PubMed Central

Jiang, Lili; Hu, Hong

2017-01-01

The multilayer orthogonal auxetic composites have been previously developed and tested to prove that they own excellent energy absorption and impact protection characteristics in a specific strain range under low-velocity impact. In this study, a three dimensional finite element (FE) model in ANSYS LS-DYNA was established to simulate the mechanical behavior of auxetic composites under low-velocity drop-weight impact. The simulation results including the Poisson’s ratio versus compressive strain curves and the contact stress versus compressive strain curves were compared with those in the experiments. The clear deformation pictures of the FE models have provided a simple and effective way for investigating the damage mechanism and optimizing the material, as well as structure design. PMID:28783054

Effects of Cooling Rate on Precipitate Evolution and Residual Stresses in Al-Si-Mn-Mg Casting Alloy

NASA Astrophysics Data System (ADS)

Lee, Eunkyung; Walde, Caitlin; Mishra, Brajendra

2018-07-01

The residual stresses with different heat treatment conditions have been measured and correlated with the microstructural behavior of AA365. 30 and 100 K/min cooling of AA365 inhibited the transformation of precipitates under 773 K, respectively. The alloy cooled at 30 and 100 K/min exhibited tensile residual stresses of 6.2 and 5.4 MPa, respectively, while the alloy cooled at 1 and 10 K/min showed compressive stresses of - 12.8 and - 10.3 MPa, respectively. The formation β', β″, and other intermetallic compounds affected the compressive residual stresses, and that the fracture of the brittle intermetallic phases could reduce the extent of residual stresses in the lattice through plastic deformation.

Effects of Cooling Rate on Precipitate Evolution and Residual Stresses in Al-Si-Mn-Mg Casting Alloy

NASA Astrophysics Data System (ADS)

Lee, Eunkyung; Walde, Caitlin; Mishra, Brajendra

2018-03-01

The residual stresses with different heat treatment conditions have been measured and correlated with the microstructural behavior of AA365. 30 and 100 K/min cooling of AA365 inhibited the transformation of precipitates under 773 K, respectively. The alloy cooled at 30 and 100 K/min exhibited tensile residual stresses of 6.2 and 5.4 MPa, respectively, while the alloy cooled at 1 and 10 K/min showed compressive stresses of - 12.8 and - 10.3 MPa, respectively. The formation β', β″, and other intermetallic compounds affected the compressive residual stresses, and that the fracture of the brittle intermetallic phases could reduce the extent of residual stresses in the lattice through plastic deformation.

Experimental study on dynamic mechanical behaviors of polycarbonate

NASA Astrophysics Data System (ADS)

Zhang, Wei; Gao, Yubo; Ye, Nan; Huang, Wei; Li, Dacheng

2017-01-01

Polycarbonate (PC) is a widely used engineering material in aerospace field, since it has excellent mechanical and optical property. In present study, both compressive and tensile tests of PC were conducted at high strain rates by using a split Hopkinson pressure bar. The high-speed camera and 2D Digital Image Correlation method (DIC) were used to analyze the dynamic deformation behavior of PC. Meanwhile, the plate impact experiment was carried out to measure the equation of state of PC in a single-stage gas gun, which consists of asymmetric impact technology, manganin gauges, PVDF, electromagnetic particle velocity gauges. The results indicate that the yield stress of PC increased with the strain rates in both dynamic compression and tension tests. The same phenomenon was similar to elasticity modulus at different strain rate. A constitutive model was used to describe the mechanical behaviors of PC accurately in different strain rates by contrast with the results of 2D-DIC. At last, The D-u Hugoniot curve of polycarbonate in high pressure was fitted by the least square method.

Deformation of a geo-medium with considering for internal self-balancing stresses

NASA Astrophysics Data System (ADS)

Lavrikov, S. V.; Revuzhenko, A. F.

2016-11-01

Based on the general concept of rock as a medium with inner sources and sinks of energy, the authors consider an approach to mathematical modeling of a geo-medium with account for internal self-balancing stresses. The description of stresses and strains at the level of microstructural elements and macrovolume of the medium uses methods of non-Archimedean analysis. The model allows describing the accumulation of elastic energy in the form of internal self-balancing stresses. A finite element algorithm and a software program for solving plane boundary-value problems have been developed. The calculated data on rock specimen compression are given. It is shown that the behavior of plastic deformation zones depends on the pre-assigned initial microstresses.

Mechanical Properties of 17-4PH Stainless Steel Foam Panels

NASA Technical Reports Server (NTRS)

Raj, S. V.; Ghosn, L. J.; Lerch, B. a.; Hebsur, M.; Cosgriff, L. M.; Fedor, J.

2007-01-01

Rectangular 17-4PH stainless steel sandwiched foam panels were fabricated using a commercial manufacturing technique by brazing two sheets to a foam core. Microstructural observations and ultrasonic nondestructive evaluation of the panels revealed large variations in the quality of the brazed areas from one panel to the next as well as within the same panel. Shear tests conducted on specimens machined from the panels exhibited failures either in the brazed region or in the foam core for the poorly brazed and well-brazed samples, respectively. Compression tests were conducted on the foam cores to evaluate their elastic and plastic deformation behavior. These data were compared with published data on polymeric and metallic foams, and with theoretical deformation models proposed for open cell foams.

The mechanics of pressed-pellet separators in molten salt batteries

DOE Office of Scientific and Technical Information (OSTI.GOV)

Long, Kevin Nicholas; Roberts, Christine Cardinal; Roberts, Scott Alan

2014-06-01

We present a phenomenological constitutive model that describes the macroscopic behavior of pressed-pellet materials used in molten salt batteries. Such materials include separators, cathodes, and anodes. The purpose of this model is to describe the inelastic deformation associated with the melting of a key constituent, the electrolyte. At room temperature, all constituents of these materials are solid and do not transport cations so that the battery is inert. As the battery is heated, the electrolyte, a constituent typically present in the separator and cathode, melts and conducts charge by flowing through the solid skeletons of the anode, cathode, and separator.more » The electrochemical circuit is closed in this hot state of the battery. The focus of this report is on the thermal-mechanical behavior of the separator, which typically exhibits the most deformation of the three pellets during the process of activating a molten salt battery. Separator materials are composed of a compressed mixture of a powdered electrolyte, an inert binder phase, and void space. When the electrolyte melts, macroscopically one observes both a change in volume and shape of the separator that depends on the applied boundary conditions during the melt transition. Although porous flow plays a critical role in the battery mechanics and electrochemistry, the focus of this report is on separator behavior under flow-free conditions in which the total mass of electrolyte is static within the pellet. Specific poromechanics effects such as capillary pressure, pressure-saturation, and electrolyte transport between layers are not considered. Instead, a phenomenological model is presented to describe all such behaviors including the melting transition of the electrolyte, loss of void space, and isochoric plasticity associated with the binder phase rearrangement. The model is appropriate for use finite element analysis under finite deformation and finite temperature change conditions. The model reasonably describes the stress dependent volume and shape change associated with dead load compression and spring-type boundary conditions; the latter is relevant in molten salt batteries. Future work will transition the model towards describing the solid skeleton of the separator in the traditional poromechanics context.« less

Effects of Texture and Grain Size on the Yield Strength of ZK61 Alloy Rods Processed by Cyclic Extrusion and Compression

PubMed Central

Zhang, Lixin; Zhang, Wencong; Cao, Biao; Chen, Wenzhen; Duan, Junpeng; Cui, Guorong

2017-01-01

The ZK61 alloy rods with different grain sizes and crystallographic texture were successfully fabricated by cyclic extrusion and compression (CEC). Their room-temperature tension & compression yield strength displayed a significant dependence on grain size and texture, essentially attributed to {10-12} twinning. The texture variations were characterized by the angle θ between the c-axis of the grain and the extrusion direction (ED) during the process. The contour map of room-temperature yield strength as a function of grain size and the angle θ was obtained. It showed that both the tension yield strength and the compression yield strength of ZK61 alloy were fully consistent with the Hall-Patch relationship at a certain texture, but the change trends of the tension yield strength and the compression yield strength were completely opposite at the same grain size while texture altered. The friction stresses of different deformation modes calculated based on the texture confirmed the tension yield strength of the CECed ZK61 alloy rods, which was determined by both the basal slip and the tension twinning slip during the tension deformation at room temperature, while the compression yield strength was mainly determined by the basal slip during the compression deformation. PMID:29072616

Multi-axis dose accumulation of noninvasive image-guided breast brachytherapy through biomechanical modeling of tissue deformation using the finite element method

PubMed Central

Ghadyani, Hamid R.; Bastien, Adam D.; Lutz, Nicholas N.; Hepel, Jaroslaw T.

2015-01-01

Purpose Noninvasive image-guided breast brachytherapy delivers conformal HDR 192Ir brachytherapy treatments with the breast compressed, and treated in the cranial-caudal and medial-lateral directions. This technique subjects breast tissue to extreme deformations not observed for other disease sites. Given that, commercially-available software for deformable image registration cannot accurately co-register image sets obtained in these two states, a finite element analysis based on a biomechanical model was developed to deform dose distributions for each compression circumstance for dose summation. Material and methods The model assumed the breast was under planar stress with values of 30 kPa for Young's modulus and 0.3 for Poisson's ratio. Dose distributions from round and skin-dose optimized applicators in cranial-caudal and medial-lateral compressions were deformed using 0.1 cm planar resolution. Dose distributions, skin doses, and dose-volume histograms were generated. Results were examined as a function of breast thickness, applicator size, target size, and offset distance from the center. Results Over the range of examined thicknesses, target size increased several millimeters as compression thickness decreased. This trend increased with increasing offset distances. Applicator size minimally affected target coverage, until applicator size was less than the compressed target size. In all cases, with an applicator larger or equal to the compressed target size, > 90% of the target covered by > 90% of the prescription dose. In all cases, dose coverage became less uniform as offset distance increased and average dose increased. This effect was more pronounced for smaller target–applicator combinations. Conclusions The model exhibited skin dose trends that matched MC-generated benchmarking results within 2% and clinical observations over a similar range of breast thicknesses and target sizes. The model provided quantitative insight on dosimetric treatment variables over a range of clinical circumstances. These findings highlight the need for careful target localization and accurate identification of compression thickness and target offset. PMID:25829938

FE Analysis of Buckling Behavior Caused by Welding in Thin Plates of High Tensile Strength Steel

NASA Astrophysics Data System (ADS)

Wang, Jiangchao; Rashed, Sherif; Murakawa, Hidekazu

2014-12-01

The target of this study was to investigate buckling behavior during the entire welding process which consists of the heating and the cooling processes. For thin plate structures made of high tensile strength steel, not only residual buckling during or after cooling down but also transient buckling during heating may occur. The thermal elastic plastic FE analysis to investigate welding-induced buckling during the entire welding process is presented. Because of the high yield stress of high tensile strength steel, larger longitudinal compressive thermal stress is produced near the welding line compared with that in the case of carbon steel. Therefore, the plate may buckle due to thermal expansion, before the material nears yielding. During cooling down, the longitudinal compressive thermal stress close to the welding line disappears, and longitudinal tensile residual stress is produced due to contraction. Meanwhile, longitudinal compressive residual stress occurs far from the welding line to balance the tensile stress close to the welding line. This distribution of longitudinal residual stress would change the deformed dish shape of transient buckling into a saddle buckling type when the stress exceeds the critical buckling condition.

SU-F-BRF-13: Investigating the Feasibility of Accurate Dose Measurement in a Deforming Radiochromic Dosimeter

DOE Office of Scientific and Technical Information (OSTI.GOV)

Juang, T; Adamovics, J; Oldham, M

Purpose: Presage-Def, a deformable radiochromic 3D dosimeter, has been previously shown to have potential for validating deformable image registration algorithms. This work extends this effort to investigate the feasibility of using Presage-Def to validate dose-accumulation algorithms in deforming structures. Methods: Two cylindrical Presage-Def dosimeters (8cm diameter, 4.5cm length) were irradiated in a water-bath with a simple 4-field box treatment. Isocentric dose was 20Gy. One dosimeter served as control (no deformation) while the other was laterally compressed during irradiation by 21%. Both dosimeters were imaged before and after irradiation with a fast (∼10 minutes for 1mm isotropic resolution), broad beam, highmore » resolution optical-CT scanner. Measured dose distributions were compared to corresponding distributions calculated by a commissioned Eclipse planning system. Accuracy in the control was evaluated with 3D gamma (3%/3mm). The dose distribution calculated for the compressed dosimeter in the irradiation geometry cannot be directly compared via profiles or 3D gamma to the measured distribution, which deforms with release from compression. Thus, accuracy under deformation was determined by comparing integral dose within the high dose region of the deformed dosimeter distribution versus calculated dose. Dose profiles were used to study temporal stability of measured dose distributions. Results: Good dose agreement was demonstrated in the control with a 3D gamma passing rate of 96.6%. For the dosimeter irradiated under compression, the measured integral dose in the high dose region (518.0Gy*cm3) was within 6% of the Eclipse-calculated integral dose (549.4Gy*cm3). Elevated signal was noted on the dosimeter edge in the direction of compression. Change in dosimeter signal over 1.5 hours was ≤2.7%, and the relative dose distribution remained stable over this period of time. Conclusion: Presage-Def is promising as a 3D dosimeter capable of accurately measuring dose in a deforming structure, and warrants further study to quantify comprehensive accuracy at different levels of deformation. This work was supported by NIH R01CA100835. John Adamovics is the president of Heuris Inc., which commercializes PRESAGE.« less

Nonlocal postbuckling analysis of graphene sheets with initial imperfection based on first order shear deformation theory

NASA Astrophysics Data System (ADS)

Soleimani, Ahmad; Naei, Mohammad Hasan; Mashhadi, Mahmoud Mosavi

In this paper, the first order shear deformation theory (FSDT) is used to investigate the postbuckling behavior of orthotropic single-layered graphene sheet (SLGS) under in-plane loadings. Nonlocal elasticity theory and von-Karman nonlinear model in combination with the isogeometric analysis (IGA) have been applied to study the postbuckling characteristics of SLGSs. In contrast to the classical model, the nonlocal continuum model developed in this work considers the size-effects on the postbuckling characteristics of SLGSs. FSDT takes into account effects of shear deformations through-the-thickness of plate. Geometric imperfection which is defined as a very small transverse displacement of the mid-plane is applied on undeformed nanoplate to create initial deviation in graphene sheet from being perfectly flat. Nonlinear governing equations of motion for SLGS are derived from the principle of virtual work and a variational formulation. At the end, the results are presented as the postbuckling equilibrium paths of SLGS. The influence of various parameters such as edge length, nonlocal parameter, compression ratio, boundary conditions and aspect ratio on the postbuckling path is investigated. The results of this work show the high accuracy of nonlocal FSDT-based analysis for postbuckling behavior of graphene sheets.

Dynamic recrystallization behavior of a biomedical Ti-13Nb-13Zr alloy.

PubMed

Bobbili, Ravindranadh; Madhu, V

2016-06-01

The dynamic recrystallization (DRX) behavior of a biomedical titanium Ti-13Nb-13Zr alloy has been investigated using the high temperature compression tests under wide range of strain rates (0.001-1/s) and temperatures 900-1050°C. A constitutive equation represented as a function of temperature, strain rate and true strain is developed and the hot deformation apparent activation energy is calculated about 534kJ/mol. By considering the exponential relationship between work-hardening rate (θ) and stress, a new mathematical model was proposed for predicting flow stress up to the critical strain during hot deformation. The mathematical model for predicting flow stress up to the critical strain exhibits better consistency and accuracy. The DRX kinetic equation of Ti-13Nb-13Zr alloy is described as XDRX=1-exp[-0.32(Ɛ-ƐcƐ(*))(2.3)] . The DRX kinetic model was validated by microstructure observation. It was also found that the process of DRX was promoted by decreasing strain rate and increasing deformation temperature. Eventually, the continuous dynamic recrystallization (CDRX) was identified to be the DRX mechanism using transmission electron microscope (TEM). Copyright © 2015 Elsevier Ltd. All rights reserved.

Detection of plasticity mechanisms in an energetic molecular crystal through shock-like 3D unidirectional compressions: A Molecular Dynamics study

NASA Astrophysics Data System (ADS)

Lafourcade, Paul; Denoual, Christophe; Maillet, Jean-Bernard

2017-06-01

TATB crystal structure consists in graphitic-like sheets arranged in the a-b plane where a, b and c define the edge vectors of the unit cell. This type of stacking provides the TATB monocrystal very anisotropic physical, chemical and mechanical properties. In order to explore which mechanisms are involved in TATB plasticity, we use a Molecular Dynamics code in which the overall deformation is prescribed as a function of time, for any deformation path. Furthermore, a computation of the Green-Lagrange strain tensor is proposed, which helps reveal various defects and plasticity mechanisms. Through prescribed large strain of shock-like deformations, a three-dimensional characterization of TATB monocrystal yield stress has been obtained, confirming the very anisotropic behavior of this energetic material. Various plasticity mechanisms are triggered during these simulations, including counter intuitive defects onset such as gliding along transveral planes containing perfect dislocations and twinning. Gliding in the a-b plane occurs systematically and does not lead to significant plastic behavior, in accordance with a previous study on dislocation core structures for this plane, based on a coupling between the Peierls-Nabarro-Galerkin method and Molecular Dynamics simulations.

Prediction of water loss and viscoelastic deformation of apple tissue using a multiscale model.

PubMed

Aregawi, Wondwosen A; Abera, Metadel K; Fanta, Solomon W; Verboven, Pieter; Nicolai, Bart

2014-11-19

A two-dimensional multiscale water transport and mechanical model was developed to predict the water loss and deformation of apple tissue (Malus × domestica Borkh. cv. 'Jonagold') during dehydration. At the macroscopic level, a continuum approach was used to construct a coupled water transport and mechanical model. Water transport in the tissue was simulated using a phenomenological approach using Fick's second law of diffusion. Mechanical deformation due to shrinkage was based on a structural mechanics model consisting of two parts: Yeoh strain energy functions to account for non-linearity and Maxwell's rheological model of visco-elasticity. Apparent parameters of the macroscale model were computed from a microscale model. The latter accounted for water exchange between different microscopic structures of the tissue (intercellular space, the cell wall network and cytoplasm) using transport laws with the water potential as the driving force for water exchange between different compartments of tissue. The microscale deformation mechanics were computed using a model where the cells were represented as a closed thin walled structure. The predicted apparent water transport properties of apple cortex tissue from the microscale model showed good agreement with the experimentally measured values. Deviations between calculated and measured mechanical properties of apple tissue were observed at strains larger than 3%, and were attributed to differences in water transport behavior between the experimental compression tests and the simulated dehydration-deformation behavior. Tissue dehydration and deformation in the high relative humidity range ( > 97% RH) could, however, be accurately predicted by the multiscale model. The multiscale model helped to understand the dynamics of the dehydration process and the importance of the different microstructural compartments (intercellular space, cell wall, membrane and cytoplasm) for water transport and mechanical deformation.

Cyclic deformation of NI/sub 3/(Al,Nb) single crystals at ambient and elevated temperatures

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bonda, N.R.

Cyclic tests were performed on Ni/sub 3/(Al,Nb) (..gamma..' phase) single crystals by using a servo-hydraulic machine under fully reversed plastic strain control at a frequency of 0.1-0.2 Hz at room temperature, 400/sup 0/C and 700/sup 0/C. Since the monotonic behavior is orientation dependent, three orientations were studied. Asymmetry in tensile and compressive stresses was observed in the cyclic hardening curves of specimens tested at these temperatures and they were discussed with regard to the model suggested by Paider et al for monotonic behavior. The stress levels in the cyclic stress-strain curves (CSSC) at room temperature depended on orientation and cyclicmore » history. No CSSCs were established at 400/sup 0/C and 700/sup 0/C. The deformation in cyclic tests at small plastic strain amplitudes was found to be different from that in monotonic tests in the microplastic regions in which the deformation is believed to be carried by a small density of edge dislocations. But in cyclic deformation, to and from motion of dislocations trap the edge dislocations into dipoles and therefore screw dislocations will be forced to participate in the deformation. Cracks on the surfaces of specimens tested at room temperature and 400/sup 0/C were found to be of stage I type, whereas at 700/sup 0/C, they were of stage II type.« less

Effects of grain size on the quasi-static mechanical properties of ultrafine-grained and nanocrystalline tantalum

NASA Astrophysics Data System (ADS)

Ligda, Jonathan Paul

The increase in strength due to the Hall-Petch effect, reduced strain hardening capacity, a reduced ductility, and changes in deformation mechanisms are all effects of reducing grain size (d) into the ultrafine-grained (UFG, 100 < d < 1000 nm) and nanocrystalline (NC, d<100 nm) state. However, most of the studies on the mechanical behavior of UFG/NC metals have been on face-centered cubic (FCC) metals. Of the few reports on UFG/NC body-centered cubic (BCC) metals, the interest is related to their increase in strength and reduced strain rate sensitivity. This combination increases their propensity to deform via adiabatic shear bands (ASBs) at high strain rates, which is a desired response for materials being considered as a possible replacement for depleted uranium in kinetic energy penetrators. However, an ideal replacement material must also plastically deform in tension under quasi-static rates to survive initial launch conditions. This raises the question: if the material forms ASBs at dynamic rates, will it also form shear bands at quasi-static isothermal rates? As well as, is there a specific grain size for a material that will plastically deform in tension at quasi-static rates but form adiabatic shear bands at dynamic rates? Using high pressure torsion, a polycrystalline bulk tantalum disk was refined into the UFG/NC regime. Using microscale mechanical testing techniques, such as nanoindentation, microcompression, and microtension, it is possible to isolate locations with a homogeneous grain size within the disk. Pillars are compressed using a nanoindenter with a flat punch tip, while "dog-bone" specimens were pulled in tension using a custom built in-situ tension stage within a scanning electron microscope (SEM). The observed mechanical behavior is related to the microstructure by using transmission electron microscopy (TEM) on the as-processed material and tested specimens. Synchrotron X-ray based texture analysis was also conducted on the disk to determine if any changes in the deformation texture occur during HPT processing. Nanoindentation data shows a trend of increasing hardness with radial position that saturates at 4.5 GPa near the edge, and decreasing strain rate sensitivity. The micromechanical tests show two distinct regions on a processed circular disk, a non-shearing region and a shearing region. Microcompression/tension tests in the region of 1.0< X < 5.3 mm (X is the radial distance from the disk center) show limited strain hardening, homogeneous plastic deformation, and tensile elongation that varies from 0.3--4.0%. Tests performed at X > 5.3 mm show a drastic switch to localized plastic deformation in the form of shear bands, with evidence of grain rotation as the active deformation mechanism, and a measureable tension-compression asymmetry. Grains are elongated at all locations, and while the minimum diameters are consistent between regions, the elongated diameter in the shearing region is reduced. The transition to localized deformation is attributed to this reduced dimension. A larger percentage of grains in the shearing region have an elongated diameter below the critical grain size necessary to activate the grain rotation mechanism. The tension-compression asymmetry is due to an increased dependence on the normal stress for yielding, meaning NC Ta would follow a Mohr-Coulomb criterion over the traditional Tresca or von Mises.

Influence of Tension-Compression Asymmetry on the Mechanical Behavior of AZ31B Magnesium Alloy Sheets in Bending

NASA Astrophysics Data System (ADS)

Zhou, Ping; Beeh, Elmar; Friedrich, Horst E.

2016-03-01

Magnesium alloys are promising materials for lightweight design in the automotive industry due to their high strength-to-mass ratio. This study aims to study the influence of tension-compression asymmetry on the radius of curvature and energy absorption capacity of AZ31B-O magnesium alloy sheets in bending. The mechanical properties were characterized using tension, compression, and three-point bending tests. The material exhibits significant tension-compression asymmetry in terms of strength and strain hardening rate due to extension twinning in compression. The compressive yield strength is much lower than the tensile yield strength, while the strain hardening rate is much higher in compression. Furthermore, the tension-compression asymmetry in terms of r value (Lankford value) was also observed. The r value in tension is much higher than that in compression. The bending results indicate that the AZ31B-O sheet can outperform steel and aluminum sheets in terms of specific energy absorption in bending mainly due to its low density. In addition, the AZ31B-O sheet was deformed with a larger radius of curvature than the steel and aluminum sheets, which brings a benefit to energy absorption capacity. Finally, finite element simulation for three-point bending was performed using LS-DYNA and the results confirmed that the larger radius of curvature of a magnesium specimen is mainly attributed to the high strain hardening rate in compression.

Oil point and mechanical behaviour of oil palm kernels in linear compression

NASA Astrophysics Data System (ADS)

Kabutey, Abraham; Herak, David; Choteborsky, Rostislav; Mizera, Čestmír; Sigalingging, Riswanti; Akangbe, Olaosebikan Layi

2017-07-01

The study described the oil point and mechanical properties of roasted and unroasted bulk oil palm kernels under compression loading. The literature information available is very limited. A universal compression testing machine and vessel diameter of 60 mm with a plunger were used by applying maximum force of 100 kN and speed ranging from 5 to 25 mm min-1. The initial pressing height of the bulk kernels was measured at 40 mm. The oil point was determined by a litmus test for each deformation level of 5, 10, 15, 20, and 25 mm at a minimum speed of 5 mmmin-1. The measured parameters were the deformation, deformation energy, oil yield, oil point strain and oil point pressure. Clearly, the roasted bulk kernels required less deformation energy compared to the unroasted kernels for recovering the kernel oil. However, both kernels were not permanently deformed. The average oil point strain was determined at 0.57. The study is an essential contribution to pursuing innovative methods for processing palm kernel oil in rural areas of developing countries.

Effects of Cyclic Loading on the Deformation and Elastic-Plastic Fracture Behavior of a Cast Stainless Steel

DTIC Science & Technology

1991-10-01

23 8. High Cycle Fatigue Crack Growth Data for Cast Stainless Steel Showing Comparison with Rolfe and Barsom Fit .......... 24 9. Cyclic Load...compared to the Rolfe /Barsom4 fatigue crack propagation equation for austenitic stainless steels in Fig. 8. ELASTIC-PLASTIC Cyclic J-testing was...place during both the compression and tensile loadings. The J-integral was calculated on each cycle using the Merkle -Corten 9 J equation as modified by

The comparison of numerical models of a sandwich panel in the context of the core deformations at the supports

NASA Astrophysics Data System (ADS)

Pozorska, Jolanta; Pozorski, Zbigniew

2018-01-01

The paper presents the problem of static structural behavior of sandwich panels at the supports. The panels have a soft core and correspond to typical structures applied in civil engineering. To analyze the problem, five different 3-D numerical models were created. The results were compared in the context of core compression and stress redistribution. The numerical solutions verify methods of evaluating the capacity of the sandwich panel that are known from the literature.

Creep of Bridgmanite Analog, Neighborite (NaMgF3), and Implications for Viscous Flow in the Lower Mantle

NASA Astrophysics Data System (ADS)

Kaercher, P. M.; Mecklenburgh, J.; Mariani, E.; Wheeler, J.

2016-12-01

The rheology of the lower mantle directly influences mantle viscosity and strength and therefore affects a number of geophysical processes including mantle mixing, formation of mantle plumes and hotspots, slab subduction and stagnation, and plate motion. Experimental flow laws of lower mantle minerals, which quantify rheology of the lower mantle, are needed to help resolve discrepancies in estimates of lower mantle viscosity, better constrain geophysical models, and answer a number of outstanding questions such as, why slabs descend to different depths, and why the lower mantle is mostly isotropic despite large strains predicted by convection models. However, we lack natural lower mantle samples from which to infer deformation history. Furthermore, deformation experiments at lower mantle pressures and temperatures are challenging, and strain rates and stress cannot always be precisely controlled or measured. As a valuable alternative we have synthesized and deformed neighborite (NaMgF3), a low pressure analog of bridgmanite (MgSiO3), the most abundant mineral in the lower mantle and the Earth. Neighborite was deformed at 200 MPa confining pressure and between 500-700°C in compression using a fluid-medium deformation apparatus, and in torsion using a Patterson rig. In these experiments strain rate and stress can be accurately controlled and measured, and flow laws reliably determined. In addition we have recovered samples and examined deformation microstructures in a scanning electron microscope using electron backscatter diffraction. Preliminary mechanical results show a switch from linear-viscous deformation at lower stress (<50 MPa) to power law creep accommodated by grain boundary sliding at higher stress (>50 MPa). We also see strain weakening. Microstructures of samples deformed at a range of stress steps show grain boundary migration recrystallization (likely from lower stress) and crystallographic preferred orientation with poles to (100) planes parallel to compression (likely from higher stress). Further work is in progress to obtain microstructures that can be univocally associated with the observed mechanical behavior. We compare our results to those of other bridgmanite analogs and bridgmanite itself and extrapolate to geologic strain rates.

Designing a Uniaxial Tension/Compression Test for Springback Analysis in High-Strength Steel Sheets

PubMed Central

Stoudt, M. R.; Levine, L. E.; Ma, L.

2016-01-01

We describe an innovative design for an in-plane measurement technique that subjects thin sheet metal specimens to bidirectional loading. The goal of this measurement is to provide the critical performance data necessary to validate complex predictions of the work hardening behavior during reversed uniaxial deformation. In this approach, all of the principal forces applied to the specimen are continually measured in real-time throughout the test. This includes the lateral forces that are required to prevent out of plane displacements in the specimen that promote buckling. This additional information will, in turn, improve the accuracy of the compensation for the friction generated between the anti-bucking guides and the specimen during compression. The results from an initial series of experiments not only demonstrate that our approach is feasible, but that it generates data with the accuracy necessary to quantify the directionally-dependent changes in the yield behavior that occur when the strain path is reversed (i.e., the Bauschinger Effect). PMID:28133391

Universal Quake Statistics: From Compressed Nanocrystals to Earthquakes

DOE PAGES

Uhl, Jonathan T.; Pathak, Shivesh; Schorlemmer, Danijel; ...

2015-11-17

Slowly-compressed single crystals, bulk metallic glasses (BMGs), rocks, granular materials, and the earth all deform via intermittent slips or “quakes”. We find that although these systems span 12 decades in length scale, they all show the same scaling behavior for their slip size distributions and other statistical properties. Remarkably, the size distributions follow the same power law multiplied with the same exponential cutoff. The cutoff grows with applied force for materials spanning length scales from nanometers to kilometers. The tuneability of the cutoff with stress reflects “tuned critical” behavior, rather than self-organized criticality (SOC), which would imply stress-independence. A simplemore » mean field model for avalanches of slipping weak spots explains the agreement across scales. It predicts the observed slip-size distributions and the observed stressdependent cutoff function. In conclusion, the results enable extrapolations from one scale to another, and from one force to another, across different materials and structures, from nanocrystals to earthquakes.« less

Mechanical behavior of Kenaf/Epoxy corrugated sandwich structures

NASA Astrophysics Data System (ADS)

Bakhori, S.; Hassan, M. Z.; Daud, Y.; Sarip, S.; Rahman, N.; Ismail, Z.; Aziz, S. A.

2015-12-01

This study presents the response of kenaf/epoxy corrugated sandwich structure during quasi-static test. Force-displacements curves have been deducted to determine the deformation pattern and collapse behavior of the structure. Kenaf/epoxy sandwich structures skins fabricated by using hand layup technique and the corrugated core were moulded by using steel mould. Different thicknesses of corrugated core web with two sizes of kenaf fibers were used. The corrugated core is then bonded with the skins by using poly-epoxy resin and has been cut into different number of cells. The specimens then tested under tensile and compression at different constant speeds until the specimens fully crushed. Tensile tests data showed the structure can be considered brittle when it breaking point strain, ε less than 0.025. In compression test, the specimens fail due to dominated by stress concentration that initiated by prior cracks. Also, the specimens with more number of cells and thicker core web have higher strength and the ability to absorb higher energy.

Dynamic Behavior of Engineered Lattice Materials

PubMed Central

Hawreliak, J. A.; Lind, J.; Maddox, B.; Barham, M.; Messner, M.; Barton, N.; Jensen, B. J.; Kumar, M.

2016-01-01

Additive manufacturing (AM) is enabling the fabrication of materials with engineered lattice structures at the micron scale. These mesoscopic structures fall between the length scale associated with the organization of atoms and the scale at which macroscopic structures are constructed. Dynamic compression experiments were performed to study the emergence of behavior owing to the lattice periodicity in AM materials on length scales that approach a single unit cell. For the lattice structures, both bend and stretch dominated, elastic deflection of the structure was observed ahead of the compaction of the lattice, while no elastic deformation was observed to precede the compaction in a stochastic, random structure. The material showed lattice characteristics in the elastic response of the material, while the compaction was consistent with a model for compression of porous media. The experimental observations made on arrays of 4 × 4 × 6 lattice unit cells show excellent agreement with elastic wave velocity calculations for an infinite periodic lattice, as determined by Bloch wave analysis, and finite element simulations. PMID:27321697

Influence of Rare-Earth Additions on Properties of Titanium Alloys - Effects of Yttrium and Erbium Additions on Ti-8Al and Ti-10Al Alloy.

DTIC Science & Technology

1980-08-31

loop generated during the alternate tension-compression fatigue testing of Ti-8A1 alloy at 6000C at a plastic strain amplitude of * 0.5Z...Dependence of peak stress on the number of cycles in the longitudinal orientation of Ti-lOAl-RE alloys deformed in alternate tension-compression at...of cycles in the transverse orientation of Ti-OAl-RE alloys deformed in alternate tension- A compression fatigue at 500 0C at a plastic strain

Strain-Rate Dependence of Deformation-Twinning in Tantalum

NASA Astrophysics Data System (ADS)

Abeywardhana, Jayalath; Germann, Tim; Ravelo, Ramon

2017-06-01

Large-Scale molecular dynamics (MD) simulations are used to model quasi-isentropic compression and expansion (QIC) in tantalum crystals varying the rate of deformation between the range 108 -1012s-1 and compressive pressures up to 100 GPa. The atomic interactions were modeled employing an embedded-atom method (EAM) potential of Ta. Isentropic expansion was done employing samples initially compressed to pressures of 60 and 100 GPa followed by uniaxial and quasi-isentropically expansion to zero pressure. The effect of initial dislocation density on twinning was also examined by varying the initial defect density of the Ta samples (1010 -1012cm-2). At these high-strain rates, a threshold in strain-rate on deformation twining is observed. Under expansion or compression, deformation twinning increases with strain rate for strain-rates >109s-1 . Below this value, small fraction of twins nucleates but anneal out with time. Samples with lower fraction of twins equilibrate to defect states containing higher screw dislocation densities from those with initially higher twinning fractions. This work was supported by the Department of Energy under contract DE-AC52-06NA25396 and by the Air Force Office of Scientific Research under AFOSR Award No. FA9550-12-1-0476.

Hydrodynamically Lubricated Rotary Shaft Having Twist Resistant Geometry

DOEpatents

Dietle, Lannie; Gobeli, Jeffrey D.

1993-07-27

A hydrodynamically lubricated squeeze packing type rotary shaft with a cross-sectional geometry suitable for pressurized lubricant retention is provided which, in the preferred embodiment, incorporates a protuberant static sealing interface that, compared to prior art, dramatically improves the exclusionary action of the dynamic sealing interface in low pressure and unpressurized applications by achieving symmetrical deformation of the seal at the static and dynamic sealing interfaces. In abrasive environments, the improved exclusionary action results in a dramatic reduction of seal and shaft wear, compared to prior art, and provides a significant increase in seal life. The invention also increases seal life by making higher levels of initial compression possible, compared to prior art, without compromising hydrodynamic lubrication; this added compression makes the seal more tolerant of compression set, abrasive wear, mechanical misalignment, dynamic runout, and manufacturing tolerances, and also makes hydrodynamic seals with smaller cross-sections more practical. In alternate embodiments, the benefits enumerated above are achieved by cooperative configurations of the seal and the gland which achieve symmetrical deformation of the seal at the static and dynamic sealing interfaces. The seal may also be configured such that predetermined radial compression deforms it to a desired operative configuration, even through symmetrical deformation is lacking.

An Experimental and Numerical Study on Cracking Behavior of Brittle Sandstone Containing Two Non-coplanar Fissures Under Uniaxial Compression

NASA Astrophysics Data System (ADS)

Yang, Sheng-Qi; Tian, Wen-Ling; Huang, Yan-Hua; Ranjith, P. G.; Ju, Yang

2016-04-01

To understand the fracture mechanism in all kinds of rock engineering, it is important to investigate the fracture evolution behavior of pre-fissured rock. In this research, we conducted uniaxial compression experiments to evaluate the influence of ligament angle on the strength, deformability, and fracture coalescence behavior of rectangular prismatic specimens (80 × 160 × 30 mm) of brittle sandstone containing two non-coplanar fissures. The experimental results show that the peak strength of sandstone containing two non-coplanar fissures depends on the ligament angle, but the elastic modulus is not closely related to the ligament angle. With the increase of ligament angle, the peak strength decreased at a ligament angle of 60°, before increasing up to our maximum ligament angle of 120°. Crack initiation, propagation, and coalescence were all observed and characterized from the inner and outer tips of pre-existing non-coplanar fissures using photographic monitoring. Based on the results, the sequence of crack evolution in sandstone containing two non-coplanar fissures was analyzed in detail. In order to fully understand the crack evolution mechanism of brittle sandstone, numerical simulations using PFC2D were performed for specimens containing two non-coplanar fissures under uniaxial compression. The results are in good agreement with the experimental results. By analyzing the stress field, the crack evolution mechanism in brittle sandstone containing two non-coplanar fissures under uniaxial compression is revealed. These experimental and numerical results are expected to improve the understanding of the unstable fracture mechanism of fissured rock engineering structures.

The anelastic Ericksen problem: universal eigenstrains and deformations in compressible isotropic elastic solids.

PubMed

Yavari, Arash; Goriely, Alain

2016-12-01

The elastic Ericksen problem consists of finding deformations in isotropic hyperelastic solids that can be maintained for arbitrary strain-energy density functions. In the compressible case, Ericksen showed that only homogeneous deformations are possible. Here, we solve the anelastic version of the same problem, that is, we determine both the deformations and the eigenstrains such that a solution to the anelastic problem exists for arbitrary strain-energy density functions. Anelasticity is described by finite eigenstrains. In a nonlinear solid, these eigenstrains can be modelled by a Riemannian material manifold whose metric depends on their distribution. In this framework, we show that the natural generalization of the concept of homogeneous deformations is the notion of covariantly homogeneous deformations -deformations with covariantly constant deformation gradients. We prove that these deformations are the only universal deformations and that they put severe restrictions on possible universal eigenstrains . We show that, in a simply-connected body, for any distribution of universal eigenstrains the material manifold is a symmetric Riemannian manifold and that in dimensions 2 and 3 the universal eigenstrains are zero-stress.

Characterization and investigation of the deformation behavior of porous magnesium scaffolds with entangled architectured pore channels.

PubMed

Jiang, Guofeng; Li, Qiuyan; Wang, Cunlong; Dong, Jie; He, Guo

2016-12-01

We report a kind of porous magnesium with entangled architectured pore structure for potential applications in biomedical implant. The pore size, spatial structure and Young׳s modulus of the as-prepared porous Mg are suitable for bone tissue engineering applications. Particularly, with regard to the load-bearing conditions, a new analytical model is employed to investigate its structure and mechanical response under compressive stress based on Gibson-Ashby model. It is found that there are three types of stress-strain behaviors in the large range of porosity from 20% to 80%. When the porosity is larger than an upper critical value, the porous magnesium exhibits densifying behavior with buckling deformation mechanism. When the porosity is smaller than a lower critical value, the porous magnesium exhibits shearing behavior with cracking along the maximum shear stress. Between the two critical porosities, both the buckling deformation and shearing behavior coexist. The upper critical porosity is experimentally determined to be 60% for 270μm pore size and 62% for 400μm pore size, while the lower critical porosity is 40% for 270μm pore size and 42% for 400μm pore size. A new analytical model could be used to accurately predict the mechanical response of the porous magnesium. No matter the calculated critical porosity or yielding stress in a large range of porosity by using the new model are well consistent with the experimental values. All these results could help to provide valuable data for developing the present porous magnesium for potential bio applications. Copyright © 2016 Elsevier Ltd. All rights reserved.

Comparison of mechanical compressive properties of commercial and autologous fibrin glues for tissue engineering applications.

PubMed

Cravens, Matthew G; Behn, Anthony W; Dragoo, Jason L

2017-11-01

Fibrin glues are widely used in orthopedic surgery as adhesives and hemostatic agents. We evaluated the compressive properties of selected fibrin glues in order to identify which are appropriate for tissue regeneration applications subject to compression. Uniaxial unconfined compression tests were performed on fibrin gels prepared from commercial and autologous products: (1) Evicel (Ethicon), (2) Tisseel (Baxter), (3) Angel (Arthrex), and (4) ProPlaz (Biorich). Cyclic loads were applied from 0 to 30% strain for 100cycles at 0.5Hz. Following cyclic testing, specimens were subjected to ramp displacement of 1% strain per second to 80% strain. Throughout cyclic loading, Evicel and Tisseel deformed (shortened) less than Angel at all but one time point, and deformed less than ProPlaz at cycles 10 and 20. The dynamic moduli, peak stress, and strain energy were significantly greater in Tisseel than all other groups. Evicel displayed significantly greater dynamic moduli, peak stress, and strain energy than Angel and ProPlaz. Following cyclic testing, Tisseel and Evicel were significantly less deformed than Angel. No specimens exhibited gross failure during ramp loading to 80% strain. Ramp loading trends mirrored those of cyclic loading. The tested commercial glues were significantly more resistant to compression than the autologous products. The compressive properties of Tisseel were approximately twice those of Evicel. All preparations displayed moduli multiple orders of magnitude less than that of native articular cartilage. We conclude that in knee surgeries requiring fibrin glue to undergo compression of daily activity, commercial products are preferable to autologous preparations from platelet-poor plasma, though both will deform significantly. Copyright © 2017 Elsevier Ltd. All rights reserved.

Closure of fatigue cracks at high strains

NASA Technical Reports Server (NTRS)

Iyyer, N. S.; Dowling, N. E.

1985-01-01

Experiments were conducted on smooth specimens to study the closure behavior of short cracks at high cyclic strains under completely reversed cycling. Testing procedures and methodology, and closure measurement techniques, are described in detail. The strain levels chosen for the study cover from predominantly elastic to grossly plastic strains. Crack closure measurements are made at different crack lengths. The study reveals that, at high strains, cracks close only as the lowest stress level in the cycle is approached. The crack opening is observed to occur in the compressive part of the loading cycle. The applied stress needed to open a short crack under high strain is found to be less than for cracks under small scale yielding. For increased plastic deformations, the value of sigma sub op/sigma sub max is observed to decrease and approaches the value of R. Comparison of the experimental results with existing analysis is made and indicates the limitations of the small scale yielding approach where gross plastic deformation behavior occurs.

Inelastic properties of ice Ih at low temperatures and high pressures

USGS Publications Warehouse

Kirby, S.H.; Durham, W.B.; Beeman, M.L.; Heard, H.C.; Daley, M.A.

1987-01-01

The aim of our research programme is to explore the rheological behavior of H2O ices under conditions appropriate to the interiors of the icy satellites of the outer planets in order to give insight into their deformation. To this end, we have performed over 100 constant-strain-rate compression tests at pressures to 500 MPa and temperatures as low as 77 K. At P > 30 MPa, ice Ih fails by a shear instability producing faults in the maximum shear stress orientation and failure strength typically is independent of pressure. This unusual faulting behavior is thought to be connected with phase transformations localized in the shear zones. The steady-state strength follows rheological laws of the thermally-activated power-law type, with different flow law parameters depending on the range of test temperatures. The flow laws will be discussed with reference to the operating deformation mechanisms as deduced from optical-scale microstructures and comparison with other work.

Microstructure Evolution and Flow Stress Model of a 20Mn5 Hollow Steel Ingot during Hot Compression.

PubMed

Liu, Min; Ma, Qing-Xian; Luo, Jian-Bin

2018-03-21

20Mn5 steel is widely used in the manufacture of heavy hydro-generator shaft due to its good performance of strength, toughness and wear resistance. However, the hot deformation and recrystallization behaviors of 20Mn5 steel compressed under high temperature were not studied. In this study, the hot compression experiments under temperatures of 850-1200 °C and strain rates of 0.01/s-1/s are conducted using Gleeble thermal and mechanical simulation machine. And the flow stress curves and microstructure after hot compression are obtained. Effects of temperature and strain rate on microstructure are analyzed. Based on the classical stress-dislocation relation and the kinetics of dynamic recrystallization, a two-stage constitutive model is developed to predict the flow stress of 20Mn5 steel. Comparisons between experimental flow stress and predicted flow stress show that the predicted flow stress values are in good agreement with the experimental flow stress values, which indicates that the proposed constitutive model is reliable and can be used for numerical simulation of hot forging of 20Mn5 hollow steel ingot.

Plastic Flow and Microstructure Evolution during Thermomechanical Processing of a PM Nickel-Base Superalloy

NASA Astrophysics Data System (ADS)

Semiatin, S. L.; McClary, K. E.; Rollett, A. D.; Roberts, C. G.; Payton, E. J.; Zhang, F.; Gabb, T. P.

2013-06-01

Plastic flow and microstructure evolution during sub- and supersolvus forging and subsequent supersolvus heat treatment of the powder-metallurgy superalloy LSHR (low-solvus, high-refractory) were investigated to develop an understanding of methods that can be used to obtain a moderately coarse gamma grain size under well-controlled conditions. To this end, isothermal, hot compression tests were conducted over broad ranges of temperature [(1144 K to 1450 K) 871 °C to 1177 °C] and constant true strain rate (0.0005 to 10 s-1). At low temperatures, deformation was generally characterized by flow softening and dynamic recrystallization that led to a decrease in grain size. At high subsolvus temperatures and low strain rates, steady-state flow or flow hardening was observed. These latter behaviors were ascribed to superplastic deformation and microstructure evolution characterized by a constant grain size or concomitant dynamic grain growth, respectively. During supersolvus heat treatment following subsolvus deformation, increases in grain size whose magnitude was a function of the prior deformation conditions were noted. A transition in flow behavior from superplastic to nonsuperplastic and the development during forging at a high subsolvus temperature of a wide (possibly bi- or multimodal) gamma-grain-size distribution having some large grains led to a substantially coarser grain size during supersolvus annealing in comparison to that produced under all other forging conditions.

Structure and mechanical behaviors of protective armored pangolin scales and effects of hydration and orientation.

PubMed

Liu, Z Q; Jiao, D; Weng, Z Y; Zhang, Z F

2016-03-01

As natural flexible dermal armor, pangolin scales provide effective protection against predatory threats and possess other notable properties such as anti-adhesion and wear-resistance. In this study, the structure, mechanical properties, deformation and damage behaviors of pangolin scales were systematically investigated with the effects of hydration and orientation evaluated. The scales are divided into three macro-layers constituted by overlapping keratin tiles with distinct lamellar arrangements which are further composed of lower-ordered lamellae. Both hardness and strength are significantly decreased by hydration; while the plasticity is markedly improved concomitantly, and as such, the mechanical damages are mitigated. The tensile strength invariably approximates to one third of hardness in value. The tensile deformation is dominated by lamellae stretching and pulling out under wet condition, which is distinct from the trans-lamellar fracture in dry samples. The compressive behaviors are featured by pronounced plasticity in both dry and wet scales; and notable strain-hardening capacity is introduced by hydration, especially along the thickness direction wherein kinking occurs. Inter-lamellar cracking is effectively alleviated in wet samples compared with the dry ones and both of them deform by macroscopic buckling. This study may help stimulate possible inspiration for the design of high-performance synthetic armor materials by mimicking pangolin scales. Copyright © 2015 Elsevier Ltd. All rights reserved.

Shape memory behavior of single and polycrystalline nickel rich nickel titanium alloys

NASA Astrophysics Data System (ADS)

Kaya, Irfan

NiTi is the most commonly used shape memory alloy (SMA) and has been widely used for bio-medical, electrical and mechanical applications. Nickel rich NiTi shape memory alloys are coming into prominence due to their distinct superelasticity and shape memory properties as compared to near equi-atomic NiTi shape memory alloys. Besides, their lower density and higher work output than steels makes these alloys an excellent candidate for aerospace and automotive industry. Shape memory properties and phase transformation behavior of high Ni-rich Ni54Ti46 (at.%) polycrystals and Ni-rich Ni 51Ti49 (at.%) single-crystals are determined. Their properties are sensitive to heat treatments that affect the phase transformation behavior of these alloys. Phase transformation properties and microstructure were investigated in aged Ni54Ti46 alloys with differential scanning calorimetry (DSC) and transmission electron microscopy (TEM) to reveal the precipitation characteristics and R-phase formation. It was found that Ni54Ti46 has the ability to exhibit perfect superelasticity under high stress levels (~2 GPa) with 4% total strain after 550°C-3h aging. Stress independent R-phase transformation was found to be responsible for the change in shape memory behavior with stress. The shape memory responses of [001], [011] and [111] oriented Ni 51Ti49 single-crystals alloy were reported under compression to reveal the orientation dependence of their shape memory behavior. It has been found that transformation strain, temperatures and hysteresis, Classius-Clapeyron slopes, critical stress for plastic deformation are highly orientation dependent. The effects of precipitation formation and compressive loading at selected temperatures on the two-way shape memory effect (TWSME) properties of a [111]- oriented Ni51Ti49 shape memory alloy were revealed. Additionally, aligned Ni4Ti3 precipitates were formed in a single crystal of Ni51Ti49 alloy by aging under applied compression stress along the [111] direction. Formation of a single family of Ni4Ti3 precipitates were exhibited significant TWSME without any training or deformation. When the homogenized and aged specimens were loaded in martensite, positive TWSME was observed. After loading at high temperature in austenite, the homogenized specimen did not show TWSME while the aged specimen revealed negative TWSME.

Comparative study on twinning characteristics during two post-weld compression paths and their effects on joint enhancement.

PubMed

Liu, Zhe; Xin, Renlong; Li, Dongrong; Sun, Liyun; Liu, Qing

2016-12-23

Friction stir welding (FSW) has promising application potential in Mg alloys. However, the texture distribution in stir zone (SZ) is usually complicated for Mg alloys, which deterioriates the joint performance. In this study, the texture distribution in SZ was tailored by applying two kinds of post-weld compression deformation along normal direction (ND) or welding direction (WD) of the FSWed AZ31 Mg alloy plates. The twinning behavior and texture change in the various regions of SZ were then evaluated by electron back scatter diffraction (EBSD) characterization. The effect of texture change on the joint performance was discussed in terms of Schmid factors (SFs) for basal slip and extension twinning. The results showed that profuse extension twins were formed through the whole SZ for the sample subjected to compression along ND, whereas they were observed mainly in SZ-side for the sample compressed along WD. Most of the twins were present in the forms of twin bands or chains. The directions of the twin bands or chains were related to the habit plane traces of selected twin variants. The ND post-weld compression had better strengthening effects on the joints compared to the WD compression, and the underline mechanism was discussed.

Comparative study on twinning characteristics during two post-weld compression paths and their effects on joint enhancement

PubMed Central

Liu, Zhe; Xin, Renlong; Li, Dongrong; Sun, Liyun; Liu, Qing

2016-01-01

Friction stir welding (FSW) has promising application potential in Mg alloys. However, the texture distribution in stir zone (SZ) is usually complicated for Mg alloys, which deterioriates the joint performance. In this study, the texture distribution in SZ was tailored by applying two kinds of post-weld compression deformation along normal direction (ND) or welding direction (WD) of the FSWed AZ31 Mg alloy plates. The twinning behavior and texture change in the various regions of SZ were then evaluated by electron back scatter diffraction (EBSD) characterization. The effect of texture change on the joint performance was discussed in terms of Schmid factors (SFs) for basal slip and extension twinning. The results showed that profuse extension twins were formed through the whole SZ for the sample subjected to compression along ND, whereas they were observed mainly in SZ-side for the sample compressed along WD. Most of the twins were present in the forms of twin bands or chains. The directions of the twin bands or chains were related to the habit plane traces of selected twin variants. The ND post-weld compression had better strengthening effects on the joints compared to the WD compression, and the underline mechanism was discussed. PMID:28008982

Transition-metal alloying of γ'-Ni3Al : Effects on the ideal uniaxial compressive strength from first-principles calculations

NASA Astrophysics Data System (ADS)

Wen, Minru; Wang, Chong-Yu

2018-01-01

The addition of transition-metal (TM) elements into the γ' precipitate phase of a Ni-based single-crystal superalloy can significantly affect its mechanical properties, including the intrinsic mechanical property of compressive strength. Using first-principles density functional calculations, the effects of 3 d (Sc-Zn), 4 d (Y-Cd), and 5 d (Hf-Au) TM alloying elements on the ideal uniaxial compressive strength of γ'-Ni3Al were investigated. The stress-strain relationships of pure Ni3Al under [100], [110], and [111] compressive loads and the site occupancy behavior of TM elements in Ni3Al were previously studied using a total-energy method based on density functional theory. Our results showed that the capacity of TM elements for strengthening the ideal compressive strength was associated with the d -electron number. The alloying elements with half-filled d bands (i.e., Cr, Mo, W, Tc, and Re) manifested the greatest efficacy for improving the ideal strength of Ni3Al under a deformation along the weakest compressive direction. Furthermore, the charge redistribution of Ni3Al doped with 5 d elements were also analyzed to understand the strengthening mechanisms of TM elements in the γ'-Ni3Al phase.

Diffusive, Displacive Deformations and Local Phase Transformation Govern the Mechanics of Layered Crystals: The Case Study of Tobermorite.

PubMed

Tao, Lei; Shahsavari, Rouzbeh

2017-07-19

Understanding the deformation mechanisms underlying the mechanical behavior of materials is the key to fundamental and engineering advances in materials' performance. Herein, we focus on crystalline calcium-silicate-hydrates (C-S-H) as a model system with applications in cementitious materials, bone-tissue engineering, drug delivery and refractory materials, and use molecular dynamics simulation to investigate its loading geometry dependent mechanical properties. By comparing various conventional (e.g. shear, compression and tension) and nano-indentation loading geometries, our findings demonstrate that the former loading leads to size-independent mechanical properties while the latter results in size-dependent mechanical properties at the nanometer scales. We found three key mechanisms govern the deformation and thus mechanics of the layered C-S-H: diffusive-controlled and displacive-controlled deformation mechanisms, and strain gradient with local phase transformations. Together, these elaborately classified mechanisms provide deep fundamental understanding and new insights on the relationship between the macro-scale mechanical properties and underlying molecular deformations, providing new opportunities to control and tune the mechanics of layered crystals and other complex materials such as glassy C-S-H, natural composite structures, and manmade laminated structures.

A rare cause of late onset neurological deficit in post tuberculous kyphotic deformity-case report.

PubMed

Subramani, Suresh; Shetty, Ajoy Prasad; Kanna, Rishi M; Rajasekaran, Shanmuganathan

2017-12-01

Late onset neurological deficit is a rare complication of spinal tuberculosis. Reactivation of the disease and compression by internal gibbus are the common causes for late onset neurological deficit. We report a rare cause of late onset paraplegia in a patient with post tubercular kyphotic deformity. The late onset neurological deficit was due to the adjacent segment degeneration proximal to the kyphotic deformity. Posterior hypertrophied ligamentum flavum and anterior disc osteophyte complex caused the cord compression. The increased stress for prolonged period at the end of the deformity was the reason for the accelerated degeneration. Patient underwent posterior decompression, posterolateral and interbody fusion. Deformity correction was not done. To our best knowledge, this is only the second report of this unusual cause of late onset paraplegia.

Deformation mechanisms to ameliorate the mechanical properties of novel TRIP/TWIP Co-Cr-Mo-(Cu) ultrafine eutectic alloys

PubMed Central

Kim, J. T.; Hong, S. H.; Park, H. J.; Kim, Y. S.; Suh, J. Y.; Lee, J. K.; Park, J. M.; Maity, T.; Eckert, J.; Kim, K. B.

2017-01-01

In the present study, the microstructural evolution and the modulation of the mechanical properties have been investigated for a Co-Cr-Mo (CCM) ternary eutectic alloy by addition of a small amount of copper (0.5 and 1 at.%). The microstructural observations reveal a distinct dissimilarity in the eutectic structure such as a broken lamellar structure and a well-aligned lamellar structure and an increasing volume fraction of Co lamellae as increasing amount of copper addition. This microstructural evolution leads to improved plasticity from 1% to 10% without the typical tradeoff between the overall strength and compressive plasticity. Moreover, investigation of the fractured samples indicates that the CCMCu alloy exhibits higher plastic deformability and combinatorial mechanisms for improved plastic behavior. The improved plasticity of CCMCu alloys originates from several deformation mechanisms; i) slip, ii) deformation twinning, iii) strain-induced transformation and iv) shear banding. These results reveal that the mechanical properties of eutectic alloys in the Co-Cr-Mo system can be ameliorated by micro-alloying such as Cu addition. PMID:28067248

Seismotectonics and rates of active crustal deformation in the Burmese arc and adjacent regions

NASA Astrophysics Data System (ADS)

Radha Krishna, M.; Sanu, T. D.

2000-11-01

The close vicinity of the Burmese subduction zone to the Himalayan collision zone across northeast India produces complex tectonics giving rise to a high level of seismicity. Using the hypocentral data of shallow earthquakes ( h≤70 km) for the period 1897-1995, a large number of focal mechanism solutions and other geophysical data in correlation with major morphotectonic features in the Burmese arc and the adjoining areas, we identified 12 broad seismogenic zones of relatively homogeneous deformation. Crustal deformation rates have been determined for each one of these sources based on summation of moment tensors. The results indicate that along the Kopili-Bomdila fault zone in eastern Himalaya, the deformation is taken up as a compression of 0.12±0.01 mm/yr along N16° and an extension of 0.05±0.004 mm/yr along N104° direction. The deformation velocities show a NS compression of 18.9±2.5 mm/yr and an EW extension of 17.1±2.2 mm/yr in the Shillong Plateau region, while a compression of 5.4±2.8 mm/yr along N33° is observed in the Tripura fold belt and the Bengal basin region. The vertical component in the Shillong Plateau shows crustal thickening of 2.4±0.3 mm/yr. The deformation velocities in Indo-Burman ranges show a compression of 0.19±0.02 mm/yr along N11° and an extension of 0.17±0.01 mm/yr along N101° in the Naga hills region, a compression of 3.3±0.4 mm/yr along N20° and an extension of 3.1±0.36 mm/yr along N110° in the Chin hills region and a compression of 0.21±0.3 mm/yr in N20° and an extension of 0.18±0.03 mm/yr along N110° in the Arakan-Yoma region. The dominance of strike-slip motions with the P axis oriented on an average along N17° indicate that the Burma platelet may be getting dragged along with the Indian plate and the motion of these two together is accommodated along the Sagaing fault. The velocities estimated along Sagaing transform fault in the back-arc region suggest that the deformation is taken up as an extension of 29.5±4.7 mm/yr along N344° and a compression of 12.4±1.9 mm/yr along N74° in the northern part of the fault zone, and a compression of 17.4±2.3 mm/yr along N71° and an extension of 59.8±8.0 mm/yr along N341° in the southern part of the fault zone. The average shear motion of about 13.7 mm/yr is observed along the Sagaing fault. The deformation observed in the southern part of the syntaxis zone along the Mishmi thrust indicate a compression of 0.63±0.08 mm/yr in N58° and an extension of 0.6±0.07 mm/yr in N328° direction. The region of Shan Plateau, west of Red River fault, shows a compression of 17.7±2.6 mm/yr along N36° and an extension of 16.1±2.4 mm/yr along N126°.

Recent development in the design, testing and impact-damage tolerance of stiffened composite panels

NASA Technical Reports Server (NTRS)

Williams, J. G.; Anderson, M. S.; Rhodes, M. D.; Starnes, J. H., Jr.; Stroud, W. J.

1979-01-01

Structural technology of laminated filamentary-composite stiffened-panel structures under combined inplane and lateral loadings is discussed. Attention is focused on: (1) methods for analyzing the behavior of these structures under load and for determining appropriate structural proportions for weight-efficient configurations; and (2) effects of impact damage and geometric imperfections on structural performance. Recent improvements in buckling analysis involving combined inplane compression and shear loadings and transverse shear deformations are presented. A computer code is described for proportioning or sizing laminate layers and cross-sectional dimensions, and the code is used to develop structural efficiency data for a variety of configurations, loading conditions, and constraint conditions. Experimental data on buckling of panels under inplane compression is presented. Mechanisms of impact damage initiation and propagation are described.

High-temperature slow-strain-rate compression studies on CoAl-TiB2 composites

NASA Technical Reports Server (NTRS)

Mannan, S. K.; Kumar, K. S.; Whittenberger, J. D.

1990-01-01

Results are presented of compressive deformation tests performed on particulate-reinforced CoAl-TiB2 composites in the temperature range 1100-1300 K. Hot-pressed and postdeformation microstructures were characterized by TEM and by optical microscopy. It was found that the addition of TiB2 particles improves the deformation resistance of the matrix, due to dislocation-particle interactions.

The anelastic Ericksen problem: universal eigenstrains and deformations in compressible isotropic elastic solids

PubMed Central

2016-01-01

The elastic Ericksen problem consists of finding deformations in isotropic hyperelastic solids that can be maintained for arbitrary strain-energy density functions. In the compressible case, Ericksen showed that only homogeneous deformations are possible. Here, we solve the anelastic version of the same problem, that is, we determine both the deformations and the eigenstrains such that a solution to the anelastic problem exists for arbitrary strain-energy density functions. Anelasticity is described by finite eigenstrains. In a nonlinear solid, these eigenstrains can be modelled by a Riemannian material manifold whose metric depends on their distribution. In this framework, we show that the natural generalization of the concept of homogeneous deformations is the notion of covariantly homogeneous deformations—deformations with covariantly constant deformation gradients. We prove that these deformations are the only universal deformations and that they put severe restrictions on possible universal eigenstrains. We show that, in a simply-connected body, for any distribution of universal eigenstrains the material manifold is a symmetric Riemannian manifold and that in dimensions 2 and 3 the universal eigenstrains are zero-stress. PMID:28119554

An in situ neutron diffraction study of plastic deformation in a Cu 46.5Zr 46.5Al 7 bulk metallic glass composite

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, D. M.; Chen, Yan; Mu, Juan

Micro-mechanical behaviors of a Cu 46.5Zr 46.5Al 7 bulk metallic glass composite in the plastic regime were investigated by continuous in situ neutron diffraction during compression. Three stages of the plastic deformation were observed according to the work-hardening rate. Here, the underlying natures of the work hardening, correlating with the lattice/microscopic strain evolution, are revealed for the three stages: (1) the initiation of shear bands, (2) the phase load transferring from the amorphous phase to the B2 phase and (3) the accelerated martensitic transformation and the work hardening of the polycrystalline phases promoted by the rapid propagation of the shearmore » bands.« less

An in situ neutron diffraction study of plastic deformation in a Cu 46.5Zr 46.5Al 7 bulk metallic glass composite

DOE PAGES

Wang, D. M.; Chen, Yan; Mu, Juan; ...

2018-05-21

Micro-mechanical behaviors of a Cu 46.5Zr 46.5Al 7 bulk metallic glass composite in the plastic regime were investigated by continuous in situ neutron diffraction during compression. Three stages of the plastic deformation were observed according to the work-hardening rate. Here, the underlying natures of the work hardening, correlating with the lattice/microscopic strain evolution, are revealed for the three stages: (1) the initiation of shear bands, (2) the phase load transferring from the amorphous phase to the B2 phase and (3) the accelerated martensitic transformation and the work hardening of the polycrystalline phases promoted by the rapid propagation of the shearmore » bands.« less

Computational Simulation of Breast Compression Based on Segmented Breast and Fibroglandular Tissues on Magnetic Resonance Images

PubMed Central

Shih, Tzu-Ching; Chen, Jeon-Hor; Liu, Dongxu; Nie, Ke; Sun, Lizhi; Lin, Muqing; Chang, Daniel; Nalcioglu, Orhan; Su, Min-Ying

2010-01-01

This study presents a finite element based computational model to simulate the three-dimensional deformation of the breast and the fibroglandular tissues under compression. The simulation was based on 3D MR images of the breast, and the craniocaudal and mediolateral oblique compression as used in mammography was applied. The geometry of whole breast and the segmented fibroglandular tissues within the breast were reconstructed using triangular meshes by using the Avizo® 6.0 software package. Due to the large deformation in breast compression, a finite element model was used to simulate the non-linear elastic tissue deformation under compression, using the MSC.Marc® software package. The model was tested in 4 cases. The results showed a higher displacement along the compression direction compared to the other two directions. The compressed breast thickness in these 4 cases at 60% compression ratio was in the range of 5-7 cm, which is the typical range of thickness in mammography. The projection of the fibroglandular tissue mesh at 60% compression ratio was compared to the corresponding mammograms of two women, and they demonstrated spatially matched distributions. However, since the compression was based on MRI, which has much coarser spatial resolution than the in-plane resolution of mammography, this method is unlikely to generate a synthetic mammogram close to the clinical quality. Whether this model may be used to understand the technical factors that may impact the variations in breast density measurements needs further investigation. Since this method can be applied to simulate compression of the breast at different views and different compression levels, another possible application is to provide a tool for comparing breast images acquired using different imaging modalities – such as MRI, mammography, whole breast ultrasound, and molecular imaging – that are performed using different body positions and different compression conditions. PMID:20601773

Computational simulation of breast compression based on segmented breast and fibroglandular tissues on magnetic resonance images.

PubMed

Shih, Tzu-Ching; Chen, Jeon-Hor; Liu, Dongxu; Nie, Ke; Sun, Lizhi; Lin, Muqing; Chang, Daniel; Nalcioglu, Orhan; Su, Min-Ying

2010-07-21

This study presents a finite element-based computational model to simulate the three-dimensional deformation of a breast and fibroglandular tissues under compression. The simulation was based on 3D MR images of the breast, and craniocaudal and mediolateral oblique compression, as used in mammography, was applied. The geometry of the whole breast and the segmented fibroglandular tissues within the breast were reconstructed using triangular meshes by using the Avizo 6.0 software package. Due to the large deformation in breast compression, a finite element model was used to simulate the nonlinear elastic tissue deformation under compression, using the MSC.Marc software package. The model was tested in four cases. The results showed a higher displacement along the compression direction compared to the other two directions. The compressed breast thickness in these four cases at a compression ratio of 60% was in the range of 5-7 cm, which is a typical range of thickness in mammography. The projection of the fibroglandular tissue mesh at a compression ratio of 60% was compared to the corresponding mammograms of two women, and they demonstrated spatially matched distributions. However, since the compression was based on magnetic resonance imaging (MRI), which has much coarser spatial resolution than the in-plane resolution of mammography, this method is unlikely to generate a synthetic mammogram close to the clinical quality. Whether this model may be used to understand the technical factors that may impact the variations in breast density needs further investigation. Since this method can be applied to simulate compression of the breast at different views and different compression levels, another possible application is to provide a tool for comparing breast images acquired using different imaging modalities--such as MRI, mammography, whole breast ultrasound and molecular imaging--that are performed using different body positions and under different compression conditions.

1200 and 1300 K slow plastic compression properties of Ni-50Al composites

NASA Technical Reports Server (NTRS)

Whittenberger, J. D.; Kumar, K. S.; Mannan, S. K.

1991-01-01

XD synthesis, powder blending, and hot pressing techniques have been utilized to produce NiAl composites containing 4, 7.5, 15, and 25 vol pct alumina whiskers and hybrid composite materials with 15 vol pct Al2O3 + 10 or 20 vol pct, nominally 1 micron TiB2 particles. The resistance to slow plastic flow was determined at 1200 and 1300 K via compression testing in air under constant velocity conditions. The stress-strain behavior of the intermetallic composites depended on the fraction of second phases where the 4 and 7.5 percent Al2O3 materials flowed at a nominally constant stress after about 2 percent deformation, while all the other composites exhibited diffuse yielding followed by strain softening. The flow stress-strain rate properties increased with volume fraction of Al2O3 whiskers except for the 4 and 7.5 percent materials, which had similar strengths. The hybrid composite NiAl + 15Al2O3 + 10TiB2 was substantially stronger than the materials simply containing alumina. Deformation in these composites can be described by the Kelly and Street model of creep in perfectly bonded, rigid, discontinuous fiber materials.

The role of thermal shock in cyclic oxidation

NASA Technical Reports Server (NTRS)

Lowell, C. E.; Deadmore, D. L.

1978-01-01

The effect of thermal shock on the spalling of oxides from the surfaces of several commercial alloys was determined. The average cooling rate was varied from approximately 240 C per second to less than 1.0 C per second during cyclic oxidation tests in air. The tests consisted of one hundred cycles of one hour at the maximum temperature (1100 or 1200 C). The alloys were HOS-875, TD-Ni, TD-NiCrAl, IN-601, IN-702, and B-1900 plus Hf. All of these alloys exhibited partial spalling within the oxide rather than total oxide loss down to bare metal. Thermal shock resulted in deformation of the metal which in turn resulted, in most cases, in changing the oxide failure mode from compressive to tensile. Tensile failures were characterized by cracking of the oxide and little loss, while compressive failures were characterized by explosive loss of platelets of oxide. This behavior was confirmed by examination of mechanically stressed oxide scales. The thermally shocked oxides spalled less than the slow cooled samples with the exception of TD-NiCrAl. This material failed in a brittle manner rather than by plastic deformation.

Compressive Deformation Behavior of Open-Cell Cu-Zn-Al Alloy Foam Made Through P/M Route Using Mechanically Alloyed Powder

NASA Astrophysics Data System (ADS)

Barnwal, Ajay Kumar; Mondal, D. P.; Kumar, Rajeev; Prasanth, N.; Dasgupta, R.

2018-03-01

Cu-Zn-Al foams of varying porosity fractions using mechanical alloyed powder have been made through powder metallurgy route. Here, NH4 (HCO3) was used as a space holder. Mechanically alloyed Cu-Zn-Al is made using a planetary ball mill taking the ratio of Cu/Zn/Al = 70:25:5 (by weight ratio). The ball/powder ratios were varied in the four ranges 10:1, 15:1, 20:1, and 25:1. Green compacts of milled powder and space holder samples were sintered at three stages at three different temperatures 350, 550, and 850 °C for 1 h at each stage. The crystalline size and particle size as a function of ball/powder ratios were examined. The compressive deformation responses of foams are varied with relative density and the ball/powder ratio. The plateau stress and energy absorption of these foams increase with an increase in relative density but decreases with increase in ball/powder ratio, even though crystalline size decreases. This has further been explained on the basis of particle morphology as a function of ball/powder ratio.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Neilsen, Michael K.; Lu, Wei-Yang; Scherzinger, William M.

Numerous experiments were performed to characterize the mechanical response of several different rigid polyurethane foams (FR3712, PMDI10, PMDI20, and TufFoam35) to large deformation. In these experiments, the effects of load path, loading rate, and temperature were investigated. Results from these experiments indicated that rigid polyurethane foams exhibit significant volumetric and deviatoric plasticity when they are compressed. Rigid polyurethane foams were also found to be very strain-rate and temperature dependent. These foams are also rather brittle and crack when loaded to small strains in tension or to larger strains in compression. Thus, a new Unified Creep Plasticity Damage (UCPD) model wasmore » developed and implemented into SIERRA with the name Foam Damage to describe the mechanical response of these foams to large deformation at a variety of temperatures and strain rates. This report includes a description of recent experiments and experimental findings. Next, development of a UCPD model for rigid, polyurethane foams is described. Selection of material parameters for a variety of rigid polyurethane foams is then discussed and finite element simulations with the new UCPD model are compared with experimental results to show behavior that can be captured with this model.« less

A theoretical framework for the study of compression sensing in ionic polymer metal composites

NASA Astrophysics Data System (ADS)

Volpini, Valentina; Bardella, Lorenzo; Rodella, Andrea; Cha, Youngsu; Porfiri, Maurizio

2017-04-01

Ionic Polymer Metal Composites (IPMCs) are electro-responsive materials for sensing and actuation, consisting of an ion-exchange polymeric membrane with ionized units, plated within noble metal electrodes. In this work, we investigate the sensing response of IPMCs that are subject to a through-the-thickness compression, by specializing the continuum model introduced by Cha and Porfiri,1 to this one-dimensional problem. This model modifies the classical Poisson-Nernst-Plank system governing the electrochemistry in the absence of mechanical effects, by accounting for finite deformations underlying the actuation and sensing processes. With the aim of accurately describing the IPMC dynamic compressive behavior, we introduce a spatial asymmetry in the properties of the membrane, which must be accounted for to trigger a sensing response. Then, we determine an analytical solution by applying the singular perturbation theory, and in particular the method of matched asymptotic expansions. This solution shows a good agreement with experimental findings reported in literature.

Objective evaluation of insert material for diabetic and athletic footwear.

PubMed

Brodsky, J W; Kourosh, S; Stills, M; Mooney, V

1988-12-01

Five of the most commonly used materials for shoe inserts (soft Plastazote, medium Pelite, PPT, Spenco, and Sorbothane) were objectively evaluated in the laboratory to characterize their behavior in the following three specific functions that correspond to clinical use: (1) the effect on the materials of repeated compression. (2) the effect of a combination of repetitive shear and compression. (3) the force-distribution (force-attenuation) properties of these materials, both when new and after repeated compression. The last function represents a model for relief of pressure beneath plantar bony prominences, a topic of special concern for the insensitive foot. All materials were effective in reducing transmitted force over the simulated bony prominence with a rank order of effectiveness. Other factors considered were: amount and rate of permanent deformation offset by considerations of enhanced moldability when comparing the neoprene and urethane materials with the polyethylene foams. The ideal insert represents a combination of material to achieve both durability and moldability.

Characterization of cell mechanical properties by computational modeling of parallel plate compression.

PubMed

McGarry, J P

2009-11-01

A substantial body of work has been reported in which the mechanical properties of adherent cells were characterized using compression testing in tandem with computational modeling. However, a number of important issues remain to be addressed. In the current study, using computational analyses, the effect of cell compressibility on the force required to deform spread cells is investigated and the possibility that stiffening of the cell cytoplasm occurs during spreading is examined based on published experimental compression test data. The effect of viscoelasticity on cell compression is considered and difficulties in performing a complete characterization of the viscoelastic properties of a cell nucleus and cytoplasm by this method are highlighted. Finally, a non-linear force-deformation response is simulated using differing linear viscoelastic properties for the cell nucleus and the cell cytoplasm.

Chondron curvature mapping in growth plate cartilage under compressive loading.

PubMed

Vendra, Bhavya B; Roan, Esra; Williams, John L

2018-05-18

The physis, or growth plate, is a layer of cartilage responsible for long bone growth. It is organized into reserve, proliferative and hypertrophic zones. Unlike the reserve zone where chondrocytes are randomly arranged, either singly or in pairs, the proliferative and hypertrophic chondrocytes are arranged within tubular structures called chondrons. In previous studies, the strain patterns within the compressed growth plate have been reported to be nonuniform and inhomogeneous, with an apparent random pattern in compressive strains and a localized appearance of tensile strains. In this study we measured structural deformations along the entire lengths of chondrons when the physis was subjected to physiological (20%) and hyper-physiological (30% and 40%) levels of compression. This provided a means to interpret the apparent random strain patterns seen in texture correlation maps in terms of bending deformations of chondron structures and provided a physical explanation for the inhomogeneous and nonuniform strain patterns reported in previous studies. We observed relatively large bending deformations (kinking) of the chondron structures at the interface of the reserve and proliferative zones during compression. Bending in this region may induce dividing cells to align longitudinally to maintain column formation and drive longitudinal growth. Copyright © 2018 Elsevier Ltd. All rights reserved.

Buckling analysis of planar compression micro-springs

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhang, Jing; Sui, Li; Shi, Gengchen

2015-04-15

Large compression deformation causes micro-springs buckling and loss of load capacity. We analyzed the impact of structural parameters and boundary conditions for planar micro-springs, and obtained the change rules for the two factors that affect buckling. A formula for critical buckling deformation of micro-springs under compressive load was derived based on elastic thin plate theory. Results from this formula were compared with finite element analysis results but these did not always correlate. Therefore, finite element analysis is necessary for micro-spring buckling analysis. We studied the variation of micro-spring critical buckling deformation caused by four structural parameters using ANSYS software undermore » two constraint conditions. The simulation results show that when an x-direction constraint is added, the critical buckling deformation increases by 32.3-297.9%. The critical buckling deformation decreases with increase in micro-spring arc radius or section width and increases with increase in micro-spring thickness or straight beam width. We conducted experiments to confirm the simulation results, and the experimental and simulation trends were found to agree. Buckling analysis of the micro-spring establishes a theoretical foundation for optimizing micro-spring structural parameters and constraint conditions to maximize the critical buckling load.« less

Modeling the Nonlinear, Strain Rate Dependent Deformation of Woven Ceramic Matrix Composites With Hydrostatic Stress Effects Included

NASA Technical Reports Server (NTRS)

Goldberg, Robert K.; Carney, Kelly S.

2004-01-01

An analysis method based on a deformation (as opposed to damage) approach has been developed to model the strain rate dependent, nonlinear deformation of woven ceramic matrix composites with a plain weave fiber architecture. In the developed model, the differences in the tension and compression response have also been considered. State variable based viscoplastic equations originally developed for metals have been modified to analyze the ceramic matrix composites. To account for the tension/compression asymmetry in the material, the effective stress and effective inelastic strain definitions have been modified. The equations have also been modified to account for the fact that in an orthotropic composite the in-plane shear stiffness is independent of the stiffness in the normal directions. The developed equations have been implemented into a commercially available transient dynamic finite element code, LS-DYNA, through the use of user defined subroutines (UMATs). The tensile, compressive, and shear deformation of a representative plain weave woven ceramic matrix composite are computed and compared to experimental results. The computed values correlate well to the experimental data, demonstrating the ability of the model to accurately compute the deformation response of woven ceramic matrix composites.

Nanoindentation study of the mechanical behavior of TiO2 nanotube arrays

NASA Astrophysics Data System (ADS)

Xu, Y. N.; Liu, M. N.; Wang, M. C.; Oloyede, A.; Bell, J. M.; Yan, C.

2015-10-01

Titanium dioxide (TiO2) nanotube arrays are attracting increasing attention for use in solar cells, lithium-ion batteries, and biomedical implants. To take full advantage of their unique physical properties, such arrays need to maintain adequate mechanical integrity in applications. However, the mechanical performance of TiO2 nanotube arrays is not well understood. In this work, we investigate the deformation and failure of TiO2 nanotube arrays using the nanoindentation technique. We found that the load-displacement response of the arrays strongly depends on the indentation depth and indenter shape. Substrate-independent elastic modulus and hardness can be obtained when the indentation depth is less than 2.5% of the array height. The deformation mechanisms of TiO2 nanotube arrays by Berkovich and conical indenters are closely associated with the densification of TiO2 nanotubes under compression. A theoretical model for deformation of the arrays under a large-radius conical indenter is also proposed.

Myths and Truths of Nitinol Mechanics: Elasticity and Tension-Compression Asymmetry

NASA Astrophysics Data System (ADS)

Bucsek, Ashley N.; Paranjape, Harshad M.; Stebner, Aaron P.

2016-09-01

Two prevalent myths of Nitinol mechanics are examined: (1) Martensite is more compliant than austenite; (2) Texture-free Nitinol polycrystals do not exhibit tension-compression asymmetry. By reviewing existing literature, the following truths are revealed: (1) Martensite crystals may be more compliant, equally stiff, or stiffer than austenite crystals, depending on the orientation of the applied load. The Young's Modulus of polycrystalline Nitinol is not a fixed number—it changes with both processing and in operando deformations. Nitinol martensite prefers to behave stiffer under compressive loads and more compliant under tensile loads. (2) Inelastic Nitinol martensite deformation in and of itself is asymmetric, even for texture-free polycrystals. Texture-free Nitinol polycrystals also exhibit tension-compression transformation asymmetry.

A simple laminate theory using the orthotropic viscoplasticity theory based on overstress. I - In-plane stress-strain relationships for metal matrix composites

NASA Technical Reports Server (NTRS)

Krempl, Erhard; Hong, Bor Zen

1989-01-01

A macromechanics analysis is presented for the in-plane, anisotropic time-dependent behavior of metal matrix laminates. The small deformation, orthotropic viscoplasticity theory based on overstress represents lamina behavior in a modified simple laminate theory. Material functions and constants can be identified in principle from experiments with laminae. Orthotropic invariants can be repositories for tension-compression asymmetry and for linear elasticity in one direction while the other directions behave in a viscoplastic manner. Computer programs are generated and tested for either unidirectional or symmetric laminates under in-plane loading. Correlations with the experimental results on metal matrix composites are presented.

Dynamic behaviors of various volume rate steel-fiber reinforced reactive powder concrete after high temperature burnt

NASA Astrophysics Data System (ADS)

Pang, Baojun; Wang, Liwen; Yang, Zhenqi; Chi, Runqiang

2009-06-01

Dynamic strain-stress curves of reactive powder concrete under high strain rate (10/s-100/s) were determined by improved split Hopkinson pressure bar (SHPB) system. A plumbum pulse shaper was used to ensure the symmetrical stress in the specimens before fracture and avoid the fluctuation of test data due to input shaky stress pulse. A time modified method was induced for data processing in order to get accurate SHPB results. The results of experiment showed after high temperature burnt, different volume rate (0.0%, 0.5%, 1.0%, 1.5%) steel-fiber reinforced reactive power concrete had the same changing tendency of residual mechanics behaviors, e.g. after 400 centigrade burnt, the residual compression strength was about 70% of material strength without burnt under 100/s. After 800 centigrade burnt, the compression strength is about 30% under 100/s while the deformation ability increased. At meanwhile, steel fiber had improved the mechanism of reinforcing effect and toughening effect of concrete material after burnt. With increasing of steel fiber volume rate, dynamic residual behavior of samples was improved. Microcosmic characteristics and energy absorption were induced for explaining the experiment results.

Modeling constitutive behavior of a 15Cr-15Ni-2.2Mo-Ti modified austenitic stainless steel under hot compression using artificial neural network

NASA Astrophysics Data System (ADS)

Mandal, Sumantra

2006-11-01

ABSTRACT In this paper, an artificial neural network (ANN) model has been suggested to predict the constitutive flow behavior of a 15Cr-15Ni-2.2Mo-Ti modified austenitic stainless steel under hot deformation. Hot compression tests in the temperature range 850°C- 1250°C and strain rate range 10-3-102 s-1 were carried out. These tests provided the required data for training the neural network and for subsequent testing. The inputs of the neural network are strain, log strain rate and temperature while flow stress is obtained as output. A three layer feed-forward network with ten neurons in a single hidden layer and back-propagation learning algorithm has been employed. A very good correlation between experimental and predicted result has been obtained. The effect of temperature and strain rate on flow behavior has been simulated employing the ANN model. The results have been found to be consistent with the metallurgical trend. Finally, a monte carlo analiysis has been carried out to find out the noise sensitivity of the developed model.

Deformation Behavior of Al/a-Si Core-shell Nanostructures

NASA Astrophysics Data System (ADS)

Fleming, Robert

Al/a-Si core-shell nanostructures (CSNs), consisting of a hemispherical Al core surrounded by a hard shell of a-Si, have been shown to display unusual mechanical behavior in response to compression loading. Most notably, these nanostructures exhibit substantial deformation recovery, even when loaded much beyond the elastic limit. Nanoindentation measurements revealed a unique mechanical response characterized by discontinuous signatures in the load-displacement data. In conjunction with the indentation signatures, nearly complete deformation recovery is observed. This behavior is attributed to dislocation nucleation and annihilation events enabled by the 3-dimensional confinement of the Al core. As the core confinement is reduced, either through an increase in confined core volume or a change in the geometrical confinement, the indentation signatures and deformation resistance are significantly reduced. Complimentary molecular dynamics simulations show that a substantial amount of dislocation egression occurs in the core of CSNs during unloading as dislocations annihilate at the core/shell interface. Smaller core diameters correlate with the development of a larger back-stress within the core during unloading, which further correlates with improved dislocation annihilation after unloading. Furthermore, dislocations nucleated in the core of core-shell nanorods are not as effectively removed as compared to CSNs. Nanostructure-textured surfaces (NSTSs) composed of Al/a-Si CSNs have improved tribological properties compared surfaces patterned with Al nanodots and a flat (100) Si surface. NSTSs have a coefficient of friction (COF) as low as 0.015, exhibit low adhesion with adhesion forces on the order of less than 1 microN, and are highly deformation resistant, with no apparent surface deformation after nanoscratch testing, even at contact forces up to 8000 microN. In comparison, (100) Si has substantially higher adhesion and COF ( 10 microN and 0.062, respectively), while the Al nanodots have both higher friction (COF 0.044) and are deformed when subjected to contact loads as low as 250 microN. This integrated experimental and computational study elucidates the mechanisms that contribute to the novel properties of Al/a-Si CSNs and characterizes the tribological properties of surface composed of these nanostructures, which provides a foundation for the rational design of novel technologies based on CSNs.

Strength, Fracture Toughness, Fatigue, and Standardization Issues of Free-standing Thermal Barrier Coatings

NASA Technical Reports Server (NTRS)

Choi, Sung R.; Zhu, Dong-Ming; Miller, Robert A.

2003-01-01

Strength, fracture toughness and fatigue behavior of free-standing thick thermal barrier coatings of plasma-sprayed ZrO2-8wt % Y2O3 were determined at ambient and elevated temperatures in an attempt to establish a database for design. Strength, in conjunction with deformation (stress-strain behavior), was evaluated in tension (uniaxial and trans-thickness), compression, and uniaxial and biaxial flexure; fracture toughness was determined in various load conditions including mode I, mode II, and mixed modes I and II; fatigue or slow crack growth behavior was estimated in cyclic tension and dynamic flexure loading. Effect of sintering was quantified through approaches using strength, fracture toughness, and modulus (constitutive relations) measurements. Standardization issues on test methodology also was presented with a special regard to material's unique constitutive relations.

Influence of Composition and Deformation Conditions on the Strength and Brittleness of Shale Rock

NASA Astrophysics Data System (ADS)

Rybacki, E.; Reinicke, A.; Meier, T.; Makasi, M.; Dresen, G. H.

2015-12-01

Stimulation of shale gas reservoirs by hydraulic fracturing operations aims to increase the production rate by increasing the rock surface connected to the borehole. Prospective shales are often believed to display high strength and brittleness to decrease the breakdown pressure required to (re-) initiate a fracture as well as slow healing of natural and hydraulically induced fractures to increase the lifetime of the fracture network. Laboratory deformation tests were performed on several, mainly European black shales with different mineralogical composition, porosity and maturity at ambient and elevated pressures and temperatures. Mechanical properties such as compressive strength and elastic moduli strongly depend on shale composition, porosity, water content, structural anisotropy, and on pressure (P) and temperature (T) conditions, but less on strain rate. We observed a transition from brittle to semibrittle deformation at high P-T conditions, in particular for high porosity shales. At given P-T conditions, the variation of compressive strength and Young's modulus with composition can be roughly estimated from the volumetric proportion of all components including organic matter and pores. We determined also brittleness index values based on pre-failure deformation behavior, Young's modulus and bulk composition. At low P-T conditions, where samples showed pronounced post-failure weakening, brittleness may be empirically estimated from bulk composition or Young's modulus. Similar to strength, at given P-T conditions, brittleness depends on the fraction of all components and not the amount of a specific component, e.g. clays, alone. Beside strength and brittleness, knowledge of the long term creep properties of shales is required to estimate in-situ stress anisotropy and the healing of (propped) hydraulic fractures.

Experimental Investigation on the Fatigue Mechanical Properties of Intermittently Jointed Rock Models Under Cyclic Uniaxial Compression with Different Loading Parameters

NASA Astrophysics Data System (ADS)

Liu, Yi; Dai, Feng; Dong, Lu; Xu, Nuwen; Feng, Peng

2018-01-01

Intermittently jointed rocks, widely existing in many mining and civil engineering structures, are quite susceptible to cyclic loading. Understanding the fatigue mechanism of jointed rocks is vital to the rational design and the long-term stability analysis of rock structures. In this study, the fatigue mechanical properties of synthetic jointed rock models under different cyclic conditions are systematically investigated in the laboratory, including four loading frequencies, four maximum stresses, and four amplitudes. Our experimental results reveal the influence of the three cyclic loading parameters on the mechanical properties of jointed rock models, regarding the fatigue deformation characteristics, the fatigue energy and damage evolution, and the fatigue failure and progressive failure behavior. Under lower loading frequency or higher maximum stress and amplitude, the jointed specimen is characterized by higher fatigue deformation moduli and higher dissipated hysteresis energy, resulting in higher cumulative damage and lower fatigue life. However, the fatigue failure modes of jointed specimens are independent of cyclic loading parameters; all tested jointed specimens exhibit a prominent tensile splitting failure mode. Three different crack coalescence patterns are classified between two adjacent joints. Furthermore, different from the progressive failure under static monotonic loading, the jointed rock specimens under cyclic compression fail more abruptly without evident preceding signs. The tensile cracks on the front surface of jointed specimens always initiate from the joint tips and then propagate at a certain angle with the joints toward the direction of maximum compression.

A study on the dynamic behavior of the Meuse/Haute-Marne argillite

NASA Astrophysics Data System (ADS)

Cai, M.; Kaiser, P. K.; Suorineni, F.; Su, K.

Excavation of underground tunnels can be conducted by tunnel boring machines (TBM) or drill-and-blast. TBMs cause minimum damage to excavation walls. Blasting effects on excavation walls depend on the care with which the blasting is executed. For blast-induced damage in excavation walls, two issues have to be addressed: rate of loss of confinement (rate of excavation) and dynamic loading from wave propagation that causes both intended and unintended damage. To address these two aspects, laboratory dynamic tests were conducted for the determination of the dynamic properties of the Meuse/Haute-Marne argillite. In the present study, 17 tensile (Brazilian) and 15 compression split Hopkinson pressure bar (SHPB) tests were conducted. The test revealed that the dynamic strengths of the argillite are strain rate dependent. The average dynamic increase factors (ratio of dynamic strength to static strength) for tensile and compressive strength are about 3.3 and 2.4, respectively. A high-speed video camera was used to visualize the initiation of failure and subsequent deformation of the specimens. The direct compression specimens were found to deform and fail uniformly around the circumference of the specimen, by a spalling process. The SHPB Brazilian tests indicated that failure occurred in tension along the line of load application. Radial fractures were also observed. The test results can be used for the development of a dynamic constitutive model for the argillite for the prediction of damage in underground excavation utilizing the drill-and blast method.

A sheet metal forming simulation of automotive outer panels considering the behavior of air in die cavity

NASA Astrophysics Data System (ADS)

Choi, Kwang Yong; Kim, Yun Chang; Choi, Hee Kwan; Kang, Chul Ho; Kim, Heon Young

2013-12-01

During a sheet metal forming process of automotive outer panels, the air trapped between a blank sheet and a die tool can become highly compressed, ultimately influencing the blank deformation and the press force. To prevent this problem, vent holes are drilled into die tools and needs several tens to hundreds according to the model size. The design and the drilling of vent holes are based on expert's experience and try-out result and thus the process can be one of reasons increasing development cycle. Therefore the study on the size, the number, and the position of vent holes is demanded for reducing development cycle, but there is no simulation technology for analyzing forming defects, making numerical sheet metal forming process simulations that incorporate the fluid dynamics of air. This study presents a sheet metal forming simulation of automotive outer panels (a roof and a body side outer) that simultaneously simulates the behavior of air in a die cavity. Through CAE results, the effect of air behavior and vent holes to blank deformation was analyzed. For this study, the commercial software PAM-STAMP{trade mark, serif} and PAM-SAFE{trade mark, serif} was used.

Nonlinear characterization of elasticity using quantitative optical coherence elastography.

PubMed

Qiu, Yi; Zaki, Farzana R; Chandra, Namas; Chester, Shawn A; Liu, Xuan

2016-11-01

Optical coherence elastography (OCE) has been used to perform mechanical characterization on biological tissue at the microscopic scale. In this work, we used quantitative optical coherence elastography (qOCE), a novel technology we recently developed, to study the nonlinear elastic behavior of biological tissue. The qOCE system had a fiber-optic probe to exert a compressive force to deform tissue under the tip of the probe. Using the space-division multiplexed optical coherence tomography (OCT) signal detected by a spectral domain OCT engine, we were able to simultaneously quantify the probe deformation that was proportional to the force applied, and to quantify the tissue deformation. In other words, our qOCE system allowed us to establish the relationship between mechanical stimulus and tissue response to characterize the stiffness of biological tissue. Most biological tissues have nonlinear elastic behavior, and the apparent stress-strain relationship characterized by our qOCE system was nonlinear an extended range of strain, for a tissue-mimicking phantom as well as biological tissues. Our experimental results suggested that the quantification of force in OCE was critical for accurate characterization of tissue mechanical properties and the qOCE technique was capable of differentiating biological tissues based on the elasticity of tissue that is generally nonlinear.

Effects of Loading Frequency on Fatigue Behavior, Residual Stress, and Microstructure of Deep-Rolled Stainless Steel AISI 304 at Elevated Temperatures

NASA Astrophysics Data System (ADS)

Nikitin, I.; Juijerm, P.

2018-02-01

The effects of loading frequency on the fatigue behavior of non-deep-rolled (NDR) and deep-rolled (DR) austenitic stainless steel AISI 304 were systematically clarified at elevated temperatures, especially at temperatures exhibiting the dynamic strain aging (DSA) phenomena. Tension-compression fatigue tests were performed isothermally at temperatures of 573 K and 773 K (300 °C and 500 °C) with different loading frequencies of 5, 0.5, 0.05, and 0.005 Hz. For the DR condition, the residual stresses and work-hardening states will be presented. It was found that DSA would be detected at appropriate temperatures and deformation rates. The cyclic deformation curves and the fatigue lives of the investigated austenitic stainless steel AISI 304 are considerably affected by the DSA, especially on the DR condition having high dislocation densities at the surface and in near-surface regions. In the temperature range of the DSA, residual stresses and work-hardening states of the DR condition seem to be stabilized. The microstructural alterations were investigated by transmission electron microscopy (TEM). At an appropriate temperature with low loading frequency, the plastic deformation mechanism shifted from a wavy slip manner to a planar slip manner in the DSA regimes, whereas the dislocation movements were obstructed.

Constitutive Model for Hot Deformation of the Cu-Zr-Ce Alloy

NASA Astrophysics Data System (ADS)

Zhang, Yi; Sun, Huili; Volinsky, Alex A.; Wang, Bingjie; Tian, Baohong; Liu, Yong; Song, Kexing

2018-02-01

Hot compressive deformation behavior of the Cu-Zr-Ce alloy has been investigated according to the hot deformation tests in the 550-900 °C temperature range and 0.001-10 s-1 strain rate range. Based on the true stress-true strain curves, the flow stress behavior of the Cu-Zr-Ce alloy was investigated. Microstructure evolution was observed by optical microscopy. Based on the experimental results, a constitutive equation, which reflects the relationships between the stress, strain, strain rate and temperature, has been established. Material constants n, α, Q and ln A were calculated as functions of strain. The equation predicting the flow stress combined with these materials constants has been proposed. The predicted stress is consistent with experimental stress, indicating that developed constitutive equation can adequately predict the flow stress of the Cu-Zr-Ce alloy. Dynamic recrystallization critical strain was determined using the work hardening rate method. According to the dynamic material model, the processing maps for the Cu-Zr and Cu-Zr-Ce alloy were obtained at 0.4 and 0.5 strain. Based on the processing maps and microstructure observations, the optimal processing parameters for the two alloys were determined, and it was found that the addition of Ce can promote the hot workability of the Cu-Zr alloy.

Modeling deformation behavior of Cu-Zr-Al bulk metallic glass matrix composites

NASA Astrophysics Data System (ADS)

Pauly, S.; Liu, G.; Wang, G.; Das, J.; Kim, K. B.; Kühn, U.; Kim, D. H.; Eckert, J.

2009-09-01

In the present work we prepared an in situ Cu47.5Zr47.5Al5 bulk metallic glass matrix composite derived from the shape memory alloy CuZr. We use a strength model, which considers percolation and a three-microstructural-element body approach, to understand the effect of the crystalline phase on the yield stress and the fracture strain under compressive loading, respectively. The intrinsic work-hardenability due to the martensitic transformation of the crystalline phase causes significant work hardening also of the composite material.

Compression fatigue behavior and failure mechanism of porous titanium for biomedical applications.

PubMed

Li, Fuping; Li, Jinshan; Huang, Tingting; Kou, Hongchao; Zhou, Lian

2017-01-01

Porous titanium and its alloys are believed to be one of the most attractive biomaterials for orthopedic implant applications. In the present work, porous pure titanium with 50-70% porosity and different pore size was fabricated by diffusion bonding. Compression fatigue behavior was systematically studied along the out-of-plane direction. It resulted that porous pure titanium has anisotropic pore structure and the microstructure is fine-grained equiaxed α phase with a few twins in some α grains. Porosity and pore size have some effect on the S-N curve but this effect is negligible when the fatigue strength is normalized by the yield stress. The relationship between normalized fatigue strength and fatigue life conforms to a power law. The compression fatigue behavior is characteristic of strain accumulation. Porous titanium experiences uniform deformation throughout the entire sample when fatigue cycle is lower than a critical value (N T ). When fatigue cycles exceed N T , strain accumulates rapidly and a single collapse band forms with a certain angle to the loading direction, leading to the sudden failure of testing sample. Both cyclic ratcheting and fatigue crack growth contribute to the fatigue failure mechanism, while the cyclic ratcheting is the dominant one. Porous titanium possesses higher normalized fatigue strength which is in the range of 0.5-0.55 at 10 6 cycles. The reasons for the higher normalized fatigue strength were analyzed based on the microstructure and fatigue failure mechanism. Copyright © 2016 Elsevier Ltd. All rights reserved.

Orientation dependence of the dislocation microstructure in compressed body-centered cubic molybdenum

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, S.; Wang, M.P.; Chen, C., E-mail: chench011-33@163.com

2014-05-01

The orientation dependence of the deformation microstructure has been investigated in commercial pure molybdenum. After deformation, the dislocation boundaries of compressed molybdenum can be classified, similar to that in face-centered cubic metals, into three types: dislocation cells (Type 2), and extended planar boundaries parallel to (Type 1) or not parallel to (Type 3) a (110) trace. However, it shows a reciprocal relationship between face-centered cubic metals and body-centered cubic metals on the orientation dependence of the deformation microstructure. The higher the strain, the finer the microstructure is and the smaller the inclination angle between extended planar boundaries and the compressionmore » axis is. - Highlights: • A reciprocal relationship between FCC metals and BCC metals is confirmed. • The dislocation boundaries can be classified into three types in compressed Mo. • The dislocation characteristic of different dislocation boundaries is different.« less

Study on Plastic Deformation Characteristics of Shot Peening of Ni-Based Superalloy GH4079

NASA Astrophysics Data System (ADS)

Zhong, L. Q.; Liang, Y. L.; Hu, H.

2017-09-01

In this paper, the X-ray stress diffractometer, surface roughness tester, field emission scanning electron microscope(SEM), dynamic ultra-small microhardness tester were used to measure the surface residual stress and roughness, topography and surface hardness changes of GH4079 superalloy, which was processed by metallographic grinding, turning, metallographic grinding +shot peening and turning + shot peening. Analysized the effects of shot peening parameters on shot peening plastic deformation features; and the effects of the surface state before shot peening on shot peening plastic deformation characteristics. Results show that: the surface residual compressive stress, surface roughness and surface hardness of GH4079 superalloy were increased by shot peening, in addition, the increment of the surface residual compressive stress, surface roughness and surface hardness induced by shot peening increased with increasing shot peening intensity, shot peening time, shot peening pressure and shot hardness, but harden layer depth was not affected considerably. The more plastic deformation degree of before shot peening surface state, the less increment of the surface residual compressive stress, surface roughness and surface hardness induced by shot peening.

Mechanical Properties Experimental Study of Engineering Vehicle Refurbished Tire

NASA Astrophysics Data System (ADS)

Qiang, Wang; Xiaojie, Qi; Zhao, Yang; Yunlong, Wang; Guotian, Wang; Degang, Lv

2018-05-01

The vehicle refurbished tire test system was constructed, got load-deformation, load-stiffness, and load-compression ratio property laws of engineering vehicle refurbished tire under the working condition of static state and ground contact, and built radial direction loading deformation mathematics model of 26.5R25 engineering vehicle refurbished tire. The test results show that radial-direction and side-direction deformation value is a little less than that of the new tire. The radial-direction stiffness and compression ratio of engineering vehicle refurbished tire were greatly influenced by radial-direction load and air inflation pressure. When load was certain, radial-direction stiffness would increase with air inflation pressure increasing. When air inflation pressure was certain, compression ratio of engineering vehicle refurbished tire would enlarge with radial-direction load increasing, which was a little less than that of the new and the same type tire. Aging degree of old car-case would exert a great influence on deformation property of engineering vehicle refurbished tire, thus engineering vehicle refurbished tires are suitable to the working condition of low tire pressure and less load.

Anisotropic deformation of extruded magnesium alloy AZ31 under uniaxial compression: A study with simultaneous in situ synchrotron x-ray imaging and diffraction

DOE PAGES

Lu, L.; Huang, J. W.; Fan, D.; ...

2016-08-29

In situ synchrotron x-ray imaging and diffraction are used to investigate anisotropic deformation of an extruded magnesium alloy AZ31 under uniaxial compression along two different directions, with the loading axis (LA) either parallel or perpendicular to the extrusion direction (ED), referred to as LA∥ED and LAED, respectively. Multiscale measurements including stress–strain curves (macroscale), x-ray digital image correlation (mesoscale), and diffraction (microscale) are obtained simultaneously. Electron backscatter diffraction is performed on samples collected at various strains to characterize deformation twins. The rapid increase in strain hardening rate for the LA∥ED loading is attributed to marked {101¯2} extension twinning and subsequent homogenizationmore » of deformation, while dislocation motion leads to inhomogeneous deformation and a decrease in strain hardening rate.« less

Constitutive modeling of polycarbonate over a wide range of strain rates and temperatures

NASA Astrophysics Data System (ADS)

Wang, Haitao; Zhou, Huamin; Huang, Zhigao; Zhang, Yun; Zhao, Xiaoxuan

2017-02-01

The mechanical behavior of polycarbonate was experimentally investigated over a wide range of strain rates (10^{-4} to 5× 103 s^{-1}) and temperatures (293 to 353 K). Compression tests under these conditions were performed using a SHIMADZU universal testing machine and a split Hopkinson pressure bar. Falling weight impact testing was carried out on an Instron Dynatup 9200 drop tower system. The rate- and temperature-dependent deformation behavior of polycarbonate was discussed in detail. Dynamic mechanical analysis (DMA) tests were utilized to observe the glass (α ) transition and the secondary (β ) transition of polycarbonate. The DMA results indicate that the α and β transitions have a dramatic influence on the mechanical behavior of polycarbonate. The decompose/shift/reconstruct (DSR) method was utilized to decompose the storage modulus into the α and β components and extrapolate the entire modulus, the α-component modulus and the β-component modulus. Based on three previous models, namely, Mulliken-Boyce, G'Sell-Jonas and DSGZ, an adiabatic model is proposed to predict the mechanical behavior of polycarbonate. The model considers the contributions of both the α and β transitions to the mechanical behavior, and it has been implemented in ABAQUS/Explicit through a user material subroutine VUMAT. The model predictions are proven to essentially coincide with the experimental results during compression testing and falling weight impact testing.

A critical Examination of the Phenomenon of Bonding Area - Bonding Strength Interplay in Powder Tableting.

PubMed

Osei-Yeboah, Frederick; Chang, Shao-Yu; Sun, Changquan Calvin

2016-05-01

Although the bonding area (BA) and bonding strength (BS) interplay is used to explain complex tableting behaviors, it has never been experimentally proven. The purpose of this study is to unambiguously establish the distinct contributions of each by decoupling the contributions from BA and BS. To modulate BA, a Soluplus® powder was compressed into tablets at different temperatures and then broken following equilibration at 25°C. To modulate BS, tablets were equilibrated at different temperatures. To simultaneously modulate BA and BS, both powder compression and tablet breaking test were carried out at different temperatures. Lower tablet tensile strength is observed when the powder is compressed at a lower temperature but broken at 25°C. This is consistent with the increased resistance to polymer deformation at lower temperatures. When equilibrated at different temperatures, the tensile strength of tablets prepared under identical conditions increases with decreasing storage temperature, indicating that BS is higher at a lower temperature. When powder compression and tablet breaking are carried out at the same temperature, the profile with a maximum tensile strength at 4°C is observed due to the BA-BS interplay. By systematically varying temperature during tablet compression and breaking, we have experimentally demonstrated the phenomenon of BA-BS interplay in tableting.

Random three-dimensional jammed packings of elastic shells acting as force sensors

NASA Astrophysics Data System (ADS)

Jose, Jissy; van Blaaderen, Alfons; Imhof, Arnout

2016-06-01

In a jammed solid of granular particles, the applied stress is in-homogeneously distributed within the packing. A full experimental characterization requires measurement of all the interparticle forces, but so far such measurements are limited to a few systems in two and even fewer in three dimensions. Particles with the topology of (elastic) shells are good local force sensors as relatively large deformations of the shells result from relatively small forces. We recently introduced such fluorescent shells as a model granular system in which force distributions can be determined in three dimensions using confocal microscopy and quantitative image analysis. An interesting aspect about these shells that differentiates them from other soft deformable particles is their buckling behavior at higher compression. This leads to deformations that do not conserve the inner volume of the particle. Here we use this system to accurately measure the contact forces in a three-dimensional packing of shells subjected to a static anisotropic compression and to shear. At small deformations forces are linear, however, for a buckled contact, the restoring force is related to the amount of deformation by a square root law, as follows from the theory of elasticity of shells. Near the unjamming-jamming transition (point J ), we found the probability distribution of the interparticle forces P (f ) to decay nearly exponentially at large forces, with little evidence of long-range force chains in the packings. As the packing density is increased, the tail of the distribution was found to crossover to a Gaussian, in line with other experimental and simulation studies. Under a small shear strain, up to 0.216, applied at an extremely low shear rate, we observed a shear-induced anisotropy in both the pair correlation function and contact force network; however, no appreciable change was seen in the number of contacts per particle.

Neogene ongoing tectonics in the Southern Ecuadorian Andes: analysis of the evolution of the stress field

NASA Astrophysics Data System (ADS)

Lavenu, A.; Noblet, C.; Winter, T. H.

1995-01-01

Microtectonic analysis of infilling deposits in South Ecuadorian Neogene basins brings to light a compressive stress field with σ1 along a NNE-SSW to NE-SW direction in the early Miocene, changing to an E-W direction in the Middle and Late Miocene. The syn-sedimentary deformations which affect the deposits of the basins suggest similar stress regimes due to a compressive ongoing tectonic system in the Miocene, for at least 15 Ma. There is a good correlation between rapid convergence in the Neogene and the time period during which the continental South Ecuadorian basins were deformed by compression (Quechua period).

Optimization of the dynamic behavior of strongly nonlinear heterogeneous materials

NASA Astrophysics Data System (ADS)

Herbold, Eric B.

New aspects of strongly nonlinear wave and structural phenomena in granular media are developed numerically, theoretically and experimentally. One-dimensional chains of particles and compressed powder composites are the two main types of materials considered here. Typical granular assemblies consist of linearly elastic spheres or layers of masses and effective nonlinear springs in one-dimensional columns for dynamic testing. These materials are highly sensitive to initial and boundary conditions, making them useful for acoustic and shock-mitigating applications. One-dimensional assemblies of spherical particles are examples of strongly nonlinear systems with unique properties. For example, if initially uncompressed, these materials have a sound speed equal to zero (sonic vacuum), supporting strongly nonlinear compression solitary waves with a finite width. Different types of assembled metamaterials will be presented with a discussion of the material's response to static compression. The acoustic diode effect will be presented, which may be useful in shock mitigation applications. Systems with controlled dissipation will also be discussed from an experimental and theoretical standpoint emphasizing the critical viscosity that defines the transition from an oscillatory to monotonous shock profile. The dynamic compression of compressed powder composites may lead to self-organizing mesoscale structures in two and three dimensions. A reactive granular material composed of a compressed mixture of polytetrafluoroethylene (PTFE), tungsten (W) and aluminum (Al) fine-grain powders exhibit this behavior. Quasistatic, Hopkinson bar, and drop-weight experiments show that composite materials with a high porosity and fine metallic particles exhibit a higher strength than less porous mixtures with larger particles, given the same mass fraction of constituents. A two-dimensional Eulerian hydrocode is implemented to investigate the mechanical deformation and failure of the compressed powder samples in simulated drop-weight tests. The calculations indicate that the dynamic formation of mesoscale force chains increase the strength of the sample. This is also apparent in three-dimensional finite element calculations of drop-weight test simulations using LS-Dyna despite a higher granular bulk coordination number, and an increased mobility of individual grains.

Experimental and Numerical Evaluation of the Mechanical Behavior of Strongly Anisotropic Light-Weight Metallic Fiber Structures under Static and Dynamic Compressive Loading

PubMed Central

Andersen, Olaf; Vesenjak, Matej; Fiedler, Thomas; Jehring, Ulrike; Krstulović-Opara, Lovre

2016-01-01

Rigid metallic fiber structures made from a variety of different metals and alloys have been investigated mainly with regard to their functional properties such as heat transfer, pressure drop, or filtration characteristics. With the recent advent of aluminum and magnesium-based fiber structures, the application of such structures in light-weight crash absorbers has become conceivable. The present paper therefore elucidates the mechanical behavior of rigid sintered fiber structures under quasi-static and dynamic loading. Special attention is paid to the strongly anisotropic properties observed for different directions of loading in relation to the main fiber orientation. Basically, the structures show an orthotropic behavior; however, a finite thickness of the fiber slabs results in moderate deviations from a purely orthotropic behavior. The morphology of the tested specimens is examined by computed tomography, and experimental results for different directions of loading as well as different relative densities are presented. Numerical calculations were carried out using real structural data derived from the computed tomography data. Depending on the direction of loading, the fiber structures show a distinctively different deformation behavior both experimentally and numerically. Based on these results, the prevalent modes of deformation are discussed and a first comparison with an established polymer foam and an assessment of the applicability of aluminum fiber structures in crash protection devices is attempted. PMID:28773522

Experimental and Numerical Evaluation of the Mechanical Behavior of Strongly Anisotropic Light-Weight Metallic Fiber Structures under Static and Dynamic Compressive Loading.

PubMed

Andersen, Olaf; Vesenjak, Matej; Fiedler, Thomas; Jehring, Ulrike; Krstulović-Opara, Lovre

2016-05-21

Rigid metallic fiber structures made from a variety of different metals and alloys have been investigated mainly with regard to their functional properties such as heat transfer, pressure drop, or filtration characteristics. With the recent advent of aluminum and magnesium-based fiber structures, the application of such structures in light-weight crash absorbers has become conceivable. The present paper therefore elucidates the mechanical behavior of rigid sintered fiber structures under quasi-static and dynamic loading. Special attention is paid to the strongly anisotropic properties observed for different directions of loading in relation to the main fiber orientation. Basically, the structures show an orthotropic behavior; however, a finite thickness of the fiber slabs results in moderate deviations from a purely orthotropic behavior. The morphology of the tested specimens is examined by computed tomography, and experimental results for different directions of loading as well as different relative densities are presented. Numerical calculations were carried out using real structural data derived from the computed tomography data. Depending on the direction of loading, the fiber structures show a distinctively different deformation behavior both experimentally and numerically. Based on these results, the prevalent modes of deformation are discussed and a first comparison with an established polymer foam and an assessment of the applicability of aluminum fiber structures in crash protection devices is attempted.

A Comparative Study on Johnson Cook, Modified Zerilli-Armstrong and Arrhenius-Type Constitutive Models to Predict High-Temperature Flow Behavior of Ti-6Al-4V Alloy in α + β Phase

NASA Astrophysics Data System (ADS)

Cai, Jun; Wang, Kuaishe; Han, Yingying

2016-03-01

True stress and true strain values obtained from isothermal compression tests over a wide temperature range from 1,073 to 1,323 K and a strain rate range from 0.001 to 1 s-1 were employed to establish the constitutive equations based on Johnson Cook, modified Zerilli-Armstrong (ZA) and strain-compensated Arrhenius-type models, respectively, to predict the high-temperature flow behavior of Ti-6Al-4V alloy in α + β phase. Furthermore, a comparative study has been made on the capability of the three models to represent the elevated temperature flow behavior of Ti-6Al-4V alloy. Suitability of the three models was evaluated by comparing both the correlation coefficient R and the average absolute relative error (AARE). The results showed that the Johnson Cook model is inadequate to provide good description of flow behavior of Ti-6Al-4V alloy in α + β phase domain, while the predicted values of modified ZA model and the strain-compensated Arrhenius-type model could agree well with the experimental values except under some deformation conditions. Meanwhile, the modified ZA model could track the deformation behavior more accurately than other model throughout the entire temperature and strain rate range.

Extracting material response from simple mechanical tests on hardening-softening-hardening viscoplastic solids

NASA Astrophysics Data System (ADS)

Mohan, Nisha

Compliant foams are usually characterized by a wide range of desirable mechanical properties. These properties include viscoelasticity at different temperatures, energy absorption, recoverability under cyclic loading, impact resistance, and thermal, electrical, acoustic and radiation-resistance. Some foams contain nano-sized features and are used in small-scale devices. This implies that the characteristic dimensions of foams span multiple length scales, rendering modeling their mechanical properties difficult. Continuum mechanics-based models capture some salient experimental features like the linear elastic regime, followed by non-linear plateau stress regime. However, they lack mesostructural physical details. This makes them incapable of accurately predicting local peaks in stress and strain distributions, which significantly affect the deformation paths. Atomistic methods are capable of capturing the physical origins of deformation at smaller scales, but suffer from impractical computational intensity. Capturing deformation at the so-called meso-scale, which is capable of describing the phenomenon at a continuum level, but with some physical insights, requires developing new theoretical approaches. A fundamental question that motivates the modeling of foams is `how to extract the intrinsic material response from simple mechanical test data, such as stress vs. strain response?' A 3D model was developed to simulate the mechanical response of foam-type materials. The novelty of this model includes unique features such as the hardening-softening-hardening material response, strain rate-dependence, and plastically compressible solids with plastic non-normality. Suggestive links from atomistic simulations of foams were borrowed to formulate a physically informed hardening material input function. Motivated by a model that qualitatively captured the response of foam-type vertically aligned carbon nanotube (VACNT) pillars under uniaxial compression [2011,"Analysis of Uniaxial Compression of Vertically Aligned Carbon Nanotubes," J. Mech.Phys. Solids, 59, pp. 2227--2237, Erratum 60, 1753-1756 (2012)], the property space exploration was advanced to three types of simple mechanical tests: 1) uniaxial compression, 2) uniaxial tension, and 3) nanoindentation with a conical and a flat-punch tip. The simulations attempt to explain some of the salient features in experimental data, like 1) The initial linear elastic response. 2) One or more nonlinear instabilities, yielding, and hardening. The model-inherent relationships between the material properties and the overall stress-strain behavior were validated against the available experimental data. The material properties include the gradient in stiffness along the height, plastic and elastic compressibility, and hardening. Each of these tests was evaluated in terms of their efficiency in extracting material properties. The uniaxial simulation results proved to be a combination of structural and material influences. Out of all deformation paths, flat-punch indentation proved to be superior since it is the most sensitive in capturing the material properties.

Numerical Simulation of Shock/Detonation-Deformable-Particle Interaction with Constrained Interface Reinitialization

NASA Astrophysics Data System (ADS)

Zhang, Ju; Jackson, Thomas; Balachandar, Sivaramakrishnan

2015-06-01

We will develop a computational model built upon our verified and validated in-house SDT code to provide improved description of the multiphase blast wave dynamics where solid particles are considered deformable and can even undergo phase transitions. Our SDT computational framework includes a reactive compressible flow solver with sophisticated material interface tracking capability and realistic equation of state (EOS) such as Mie-Gruneisen EOS for multiphase flow modeling. The behavior of diffuse interface models by Shukla et al. (2010) and Tiwari et al. (2013) at different shock impedance ratio will be first examined and characterized. The recent constrained interface reinitialization by Shukla (2014) will then be developed to examine if conservation property can be improved. This work was supported in part by the U.S. Department of Energy and by the Defense Threat Reduction Agency.

A rare cause of late onset neurological deficit in post tuberculous kyphotic deformity—case report

PubMed Central

Shetty, Ajoy Prasad; Kanna, Rishi M.; Rajasekaran, Shanmuganathan

2017-01-01

Late onset neurological deficit is a rare complication of spinal tuberculosis. Reactivation of the disease and compression by internal gibbus are the common causes for late onset neurological deficit. We report a rare cause of late onset paraplegia in a patient with post tubercular kyphotic deformity. The late onset neurological deficit was due to the adjacent segment degeneration proximal to the kyphotic deformity. Posterior hypertrophied ligamentum flavum and anterior disc osteophyte complex caused the cord compression. The increased stress for prolonged period at the end of the deformity was the reason for the accelerated degeneration. Patient underwent posterior decompression, posterolateral and interbody fusion. Deformity correction was not done. To our best knowledge, this is only the second report of this unusual cause of late onset paraplegia. PMID:29354759

In Situ Time-Resolved Measurements of Extension Twinning During Dynamic Compression of Polycrystalline Magnesium

NASA Astrophysics Data System (ADS)

Hustedt, C. J.; Lambert, P. K.; Kannan, V.; Huskins-Retzlaff, E. L.; Casem, D. T.; Tate, M. W.; Philipp, H. T.; Woll, A. R.; Purohit, P.; Weiss, J. T.; Gruner, S. M.; Ramesh, K. T.; Hufnagel, T. C.

2018-04-01

We report in situ time-resolved measurements of the dynamic evolution of the volume fraction of extension twins in polycrystalline pure magnesium and in the AZ31B magnesium alloy, using synchrotron x-ray diffraction during compressive loading at high strain rates. The dynamic evolution of the twinning volume fraction leads to a dynamic evolution of the texture. Although both the pure metal and the alloy had similar initial textures, we observe that the evolution of texture is slower in the alloy. We also measured the evolution of the lattice strains in each material during deformation which, together with the twin volume fractions, allows us to place some constraints on the relative contributions of dislocation-based slip and deformation twinning to the overall plastic deformation during the dynamic deformations.

Coupled Fracture and Flow in Shale in Hydraulic Fracturing

NASA Astrophysics Data System (ADS)

Carey, J. W.; Mori, H.; Viswanathan, H.

2014-12-01

Production of hydrocarbon from shale requires creation and maintenance of fracture permeability in an otherwise impermeable shale matrix. In this study, we use a combination of triaxial coreflood experiments and x-ray tomography characterization to investigate the fracture-permeability behavior of Utica shale at in situ reservoir conditions (25-50 oC and 35-120 bars). Initially impermeable shale core was placed between flat anvils (compression) or between split anvils (pure shear) and loaded until failure in the triaxial device. Permeability was monitored continuously during this process. Significant deformation (>1%) was required to generate a transmissive fracture system. Permeability generally peaked at the point of a distinct failure event and then dropped by a factor of 2-6 when the system returned to hydrostatic failure. Permeability was very small in compression experiments (< 1 mD), possibly because of limited fracture connectivity through the anvils. In pure share experiments, shale with bedding planes perpendicular to shear loading developed complex fracture networks with narrow apertures and peak permeability of 30 mD. Shale with bedding planes parallel to shear loading developed simple fractures with large apertures and a peak permeability as high as 1 D. Fracture systems held at static conditions for periods of several hours showed little change in effective permeability at hydrostatic conditions as high as 140 bars. However, permeability of fractured systems was a function of hydrostatic pressure, declining in a pseudo-linear, exponential fashion as pressure increased. We also observed that permeability decreased with increasing fluid flow rate indicating that flow did not follow Darcy's Law, possibly due to non-laminar flow conditions, and conformed to Forscheimer's law. The coupled deformation and flow behavior of Utica shale, particularly the large deformation required to initiate flow, indicates the probable importance of activation of existing fractures in hydraulic fracturing and that these fractures can have adequate permeability for the production of hydrocarbon.

Compression member response of double steel angles on truss structure with member length variation

NASA Astrophysics Data System (ADS)

Hasibuan, Purwandy; Panjaitan, Arief; Haiqal, Muhammad

2018-05-01

One type of structures that implements steel angles as its members is truss system of telecommunication tower. For this structure, reinforcements on tower legs are also needed when antennas and microwaves installation placed on the peak of tower increases in quantity. One type of reinforcement methods commonly used is by increasing areas section capacity, where tower leg consisted of single angle section will be reinforced to be double angle sections. Regarding this case, this research discussed behavior two types of double angle steel section 2L 30.30.3 that were designed identically in area section but vary in length: 103 cm and 83 cm. At the first step, compression member together with tension member was formed to be a truss system, where compression and tension member were met at the joint plate. Schematic loading was implemented by giving tension loading on the joint plate, and this loading was terminated when each specimen reached its failure. Research findings showed that implementing shorter double angle (83 cm) sections, increased compression strength of steel angle section up to 13 %. Significant deformation occurring only on the flange for both of specimens indicated that implementing double angle is effective to prevent lateral-torsional buckling.

Microstructure Evolution and Flow Stress Model of a 20Mn5 Hollow Steel Ingot during Hot Compression

PubMed Central

Liu, Min; Ma, Qing-Xian; Luo, Jian-Bin

2018-01-01

20Mn5 steel is widely used in the manufacture of heavy hydro-generator shaft due to its good performance of strength, toughness and wear resistance. However, the hot deformation and recrystallization behaviors of 20Mn5 steel compressed under high temperature were not studied. In this study, the hot compression experiments under temperatures of 850–1200 °C and strain rates of 0.01/s–1/s are conducted using Gleeble thermal and mechanical simulation machine. And the flow stress curves and microstructure after hot compression are obtained. Effects of temperature and strain rate on microstructure are analyzed. Based on the classical stress-dislocation relation and the kinetics of dynamic recrystallization, a two-stage constitutive model is developed to predict the flow stress of 20Mn5 steel. Comparisons between experimental flow stress and predicted flow stress show that the predicted flow stress values are in good agreement with the experimental flow stress values, which indicates that the proposed constitutive model is reliable and can be used for numerical simulation of hot forging of 20Mn5 hollow steel ingot. PMID:29561826

Minimally invasive repair of pectus carinatum and how to deal with complications

PubMed Central

Aragone, Xavier; Blanco, Javier Borbore; Ciano, Alejandro; Abramson, Leonardo

2016-01-01

While less common than pectus excavatum, pectus carinatum is also a chest wall deformity affecting males in higher proportion than women. Patient requests for a solution of this disease occur especially during the growth spurt of puberty when this malformation becomes more obvious and difficult to conceal. Those people suffering from pectus carinatum are very likely subject to behavioral changes and negative personality impacts. By compressing the protruding anterior region of the chest wall we achieve correction of the chest contour and simultaneous lateral expansion of the depressed costochondral arches. This original technique and the procedure to apply it fit within the category of minimally invasive surgery. The compression system acts in a way similar to that of orthodontic braces. Two rectangular fixation plates are fixed to the compression strut with screws. The plates have threaded holes along a groove in the central portion, and two holes at both ends used to attach them to the ribs by means of steel wire suture. The compression strut has to be modified into a convex shape to adapt it to the particular characteristics of the patient’s malformation. This molding is done using benders designed as part of the procedure. PMID:29078492

Minimally invasive repair of pectus carinatum and how to deal with complications.

PubMed

Abramson, Horacio; Aragone, Xavier; Blanco, Javier Borbore; Ciano, Alejandro; Abramson, Leonardo

2016-01-01

While less common than pectus excavatum, pectus carinatum is also a chest wall deformity affecting males in higher proportion than women. Patient requests for a solution of this disease occur especially during the growth spurt of puberty when this malformation becomes more obvious and difficult to conceal. Those people suffering from pectus carinatum are very likely subject to behavioral changes and negative personality impacts. By compressing the protruding anterior region of the chest wall we achieve correction of the chest contour and simultaneous lateral expansion of the depressed costochondral arches. This original technique and the procedure to apply it fit within the category of minimally invasive surgery. The compression system acts in a way similar to that of orthodontic braces. Two rectangular fixation plates are fixed to the compression strut with screws. The plates have threaded holes along a groove in the central portion, and two holes at both ends used to attach them to the ribs by means of steel wire suture. The compression strut has to be modified into a convex shape to adapt it to the particular characteristics of the patient's malformation. This molding is done using benders designed as part of the procedure.

Development of a multi-cycle shear-compression testing for the modeling of severe plastic deformation

NASA Astrophysics Data System (ADS)

Pesin, A.; Pustovoytov, D.; Lokotunina, N.

2017-12-01

The mechanism of severe plastic deformation comes from very significant shear strain. Shear-compression testing of materials is complicated by the fact that a state of large equivalent strain with dominant shear strain is not easily achievable. This paper presents the novel technique of laboratory simulation of severe plastic deformation by multi-cycle shear-compression testing at room temperature with equivalent strain e=1…5. The specimen consisted of a parallelepiped having an inclined gauge section created by two diametrically opposed semi-circular slots which were machined at 45°. Height of the specimen was 50 mm, section dimensions were 25×25 mm, gauge thickness was 5.0 mm and gauge width was 6.0 mm. The specimen provided dominant shear strain in an inclined gauge-section. The level of shear strain and equivalent strain was controlled through adjustment of the height reduction of the specimen, load application direction and number of cycles of shear-compression. Aluminium alloy Al-6.2Mg-0.7Mn was used as a material for specimen. FE simulation and analysis of the stress-strain state were performed. The microstructure of the specimen after multi-cycle shear-compression testing with equivalent strain e=1…5 was examined by optical and scanning electron microscope.

The influence of void and porosity on deformation behaviour of nanocrystalline Ni under tensile followed by compressive loading

NASA Astrophysics Data System (ADS)

Meraj, Md.; Nayak, Shradha; Krishanjeet, Kumar; Pal, Snehanshu

2018-03-01

In this paper, we present a lucid understanding about the deformation behaviour of nanocrystalline (NC) Ni with and without defects subjected to tensile followed by compressive loading using molecular dynamic (MD) simulations. The embedded atom method (EAM) potential have been incorporated in the simulation for three kinds of samples-i.e. for NC Ni (without any defect), porous NC Ni and NC Ni containing a centrally located void. All the three samples, which have been prepared by implementing the Voronoi method and using Atom Eye software, consist of 16 uniform grains. The total number of atoms present in NC Ni, porous NC Ni and NC Ni containing a void are 107021, 105968 and 107012 respectively. The stress-strain response of NC Ni under tensile followed by compressive loading are simulated at a high strain rate of 107 s-1 and at a constant temperature of 300K. The stress-strain curves for the NC Ni with and without defects have been plotted for three different types of loading: (a) tensile loading (b) compressive loading (c) forward tensile loading followed by reverse compressive loading. Prominent change in yield strength of the NC Ni is observed due to the introduction of defects. For tensile followed by compressive loading (during forward loading), the yield point for NC Ni with void is lesser than the yield point of NC Ni and porous NC Ni. The saw tooth shape or serration portion of the stress-strain curve is mainly due to three characteristic phenomena, dislocation generation and its movement, dislocation pile-up at the junctions, and dislocation annihilation. Both twins and stacking faults are observed due to plastic deformation as the deformation mechanism progresses. The dislocation density, number of clusters and number of vacancy of the NC sample with and without defects are plotted against the strain developed in the sample. It is seen that introduction of defects brings about change in mechanical properties of the NC Ni. The crystalline nature of NC Ni is found to decrease with introduction of defects. The findings of this work can thus be extended in bringing a whole new insight related to the deformation behaviour and properties of Nano- materials during cyclic deformation at various temperatures.

Deformation behavior and mechanical analysis of vertically aligned carbon nanotube (VACNT) bundles

NASA Astrophysics Data System (ADS)

Hutchens, Shelby B.

Vertically aligned carbon nanotubes (VACNTs) serve as integral components in a variety of applications including MEMS devices, energy absorbing materials, dry adhesives, light absorbing coatings, and electron emitters, all of which require structural robustness. It is only through an understanding of VACNT's structural mechanical response and local constitutive stress-strain relationship that future advancements through rational design may take place. Even for applications in which the structural response is not central to device performance, VACNTs must be sufficiently robust and therefore knowledge of their microstructure-property relationship is essential. This thesis first describes the results of in situ uniaxial compression experiments of 50 micron diameter cylindrical bundles of these complex, hierarchical materials as they undergo unusual deformation behavior. Most notably they deform via a series of localized folding events, originating near the bundle base, which propagate laterally and collapse sequentially from bottom to top. This deformation mechanism accompanies an overall foam-like stress-strain response having elastic, plateau, and densification regimes with the addition of undulations in the stress throughout the plateau regime that correspond to the sequential folding events. Microstructural observations indicate the presence of a strength gradient, due to a gradient in both tube density and alignment along the bundle height, which is found to play a key role in both the sequential deformation process and the overall stress-strain response. Using the complicated structural response as both motivation and confirmation, a finite element model based on a viscoplastic solid is proposed. This model is characterized by a flow stress relation that contains an initial peak followed by strong softening and successive hardening. Analysis of this constitutive relation results in capture of the sequential buckling phenomenon and a strength gradient effect. This combination of experimental and modeling approaches motivates discussion of the particular microstructural mechanisms and local material behavior that govern the non-trivial energy absorption via sequential, localized buckle formation in the VACNT bundles.

Structure and rheological behavior of casein micelle suspensions during ultrafiltration process

NASA Astrophysics Data System (ADS)

Pignon, F.; Belina, G.; Narayanan, T.; Paubel, X.; Magnin, A.; Gésan-Guiziou, G.

2004-10-01

The stability and mechanism underlying the formation of deposits of casein micelles during ultrafiltration process were investigated by small-angle and ultra small-angle x-ray scattering (SAXS and USAXS). The casein micelle dispersions consisted of phospho-caseinate model powders and the measurements probed length scales ranging from 1 to 2000 nm. Rheometric and frontal filtration measurements were combined with SAXS to establish the relationship between the rheological behavior of deposits (shear and/or compression) and the corresponding microstructure. The results revealed two characteristic length scales for the equilibrium structure with radius of gyrations Rg, about 100 and 5.6 nm pertaining to the globular micelles and their non-globular internal structure, respectively. The SAXS measurements further indicated that the increase of temperature from 20 to 70 °C or the decrease of pH from 6.6 to 6 lead to agglomeration of the globular micelles. In situ scattering measurements showed that the decrease of permeation flows is directly related to the deformation and compression of the micelles in the immediate vicinity of the membrane.

Wrinkling and folding of nanotube-polymer bilayers

NASA Astrophysics Data System (ADS)

Semler, Matthew R.; Harris, John M.; Hobbie, Erik K.

2014-07-01

The influence of a polymer capping layer on the deformation of purified single-wall carbon nanotube (SWCNT) networks is analyzed through the wrinkling of compressed SWCNT-polymer bilayers on polydimethylsiloxane. The films exhibit both wrinkling and folding under compression and we extract the elastoplastic response using conventional two-plate buckling schemes. The formation of a diffuse interpenetrating nanotube-polymer interface has a dramatic effect on the nanotube layer modulus for both metallic and semiconducting species. In contrast to the usual percolation exhibited by the pure SWCNT films, the capped films show a crossover from "composite" behavior (the modulus of the SWCNT film is enhanced by the polymer) to "plasticized" behavior (the modulus of the SWCNT film is reduced by the polymer) as the SWCNT film thickness increases. For almost all thicknesses, however, the polymer enhances the yield strain of the nanotube network. Conductivity measurements on identical films suggest that the polymer has a modest effect on charge transport, which we interpret as a strain-induced polymer penetration of interfacial nanotube contacts. We use scaling, Flory-Huggins theory, and independently determined nanotube-nanotube and nanotube-polymer Hamaker constants to model the response.

Molecular dynamics simulation of shock induced ejection on fused silica surface

DOE Office of Scientific and Technical Information (OSTI.GOV)

Su, Rui; Xiang, Meizhen; Jiang, Shengli

2014-05-21

Shock response and surface ejection behaviors of fused silica are studied by using non-equilibrium molecular dynamics combining with the Tersoff potential. First, bulk structure and Hugoniot curves of fused silica are calculated and compared with experimental results. Then, the dynamical process of surface ejection behavior is simulated under different loading velocities ranging from 3.5 to 5.0 km∕s, corresponding to shock wave velocities from 7.1 to 8.8 km∕s. The local atomistic shear strain parameter is used to describe the local plastic deformation under conditions of shock compression or releasing. Our result shows that the shear strain is localized in the bottom area ofmore » groove under the shock compression. Surface ejection is observed when the loading velocity exceeds 4.0 km∕s. Meanwhile, the temperature of the micro-jet is ∼5574.7 K, which is close to experiment measurement. Several kinds of structural defects including non-bridging oxygen are found in the bulk area of the sample after ejection.« less

Hot Deformation Behavior of As-Cast 2101 Grade Lean Duplex Stainless Steel and the Associated Changes in Microstructure and Crystallographic Texture

NASA Astrophysics Data System (ADS)

Patra, Sudipta; Ghosh, Abhijit; Singhal, Lokesh Kumar; Podder, Arijit Saha; Sood, Jagmohan; Kumar, Vinod; Chakrabarti, Debalay

2017-01-01

The hot deformation behavior of 2101 grade lean duplex stainless steel (DSS, containing 5 wt pct Mn, 0.2 wt pct N, and 1.4 wt pct Ni) and associated microstructural changes within δ-ferrite and austenite ( γ) phases were investigated by hot-compression testing in a GLEEBLE 3500 simulator over a range of deformation temperatures, T def [1073 K to 1373 K (800 °C to 1100 °C)], and applied strains, ɛ (0.25 to 0.80), at a constant true strain rate of 1/s. The microstructural softening inside γ was dictated by discontinuous dynamic recrystallization (DDRX) at a higher T def [1273 K to 1373 K (1000 °C to 1100 °C)], while the same was dictated by continuous dynamic recrystallization (CDRX) at a lower T def (1173 K (900 °C)]. Dynamic recovery (DRV) and CDRX dominated the softening inside δ-ferrite at T def ≥ 1173 K (900 °C). The dynamic recrystallization (DRX) inside δ and γ could not take place upon deformation at 1073 K (800 °C). The average flow stress level increased 2 to 3 times as the T def dropped from 1273 to 1173 K (1000 °C to 900 °C) and finally to 1073 K (800 °C). The average microhardness values taken from δ-ferrite and γ regions of the deformed samples showed a different trend. At T def of 1373 K (1100 °C), microhardness decreased with the increase in strain, while at T def of 1173 K (900 °C), microhardness increased with the increase in strain. The microstructural changes and hardness variation within individual phases of hot-deformed samples are explained in view of the chemical composition of the steel and deformation parameters ( T def and ɛ).

Microstructure based hygromechanical modelling of deformation of fruit tissue

NASA Astrophysics Data System (ADS)

Abera, M. K.; Wang, Z.; Verboven, P.; Nicolai, B.

2017-10-01

Quality parameters such as firmness and susceptibility to mechanical damage are affected by the mechanical properties of fruit tissue. Fruit tissue is composed of turgid cells that keep cell walls under tension, and intercellular gas spaces where cell walls of neighboring cells have separated. How the structure and properties of these complex microstructures are affecting tissue mechanics is difficult to unravel experimentally. In this contribution, a modelling methodology is presented to calculate the deformation of apple fruit tissue affected by differences in structure and properties of cells and cell walls. The model can be used to perform compression experiments in silico using a hygromechanical model that computes the stress development and water loss during tissue deformation, much like in an actual compression test. The advantage of the model is that properties and structure can be changed to test the influence on the mechanical deformation process. The effect of microstructure, turgor pressure, cell membrane permeability, wall thickness and damping) on the compressibility of the tissue was simulated. Increasing the turgor pressure and thickness of the cell walls results in increased compression resistance of apple tissue increases, as do decreasing cell size and porosity. Geometric variability of the microstructure of tissues plays a major role, affecting results more than other model parameters. Different fruit cultivars were compared, and it was demonstrated, that microstructure variations within a cultivar are so large that interpretation of cultivar-specific effects is difficult.

Deformation Behavior of a Coarse-Grained Mg-8Al-1.5Ca-0.2Sr Magnesium Alloy at Elevated Temperatures

NASA Astrophysics Data System (ADS)

Lou, Yan; Liu, Xiao

2018-02-01

The compression tests were carried out on a coarse-grained Mg-8Al-1.5Ca-0.2Sr magnesium alloy samples at temperatures from 300 to 450 °C and strain rates from 0.001 to 10 s-1. The flow stress curves were analyzed using the double-differentiation method, and double minima were detected on the flow curves. The first set of minima is shown to identify the critical strain for twinning, while the second set indicates the critical strain for the initiation of dynamic recrystallization (DRX). Twin variant selection was numerically identified by comprehensive analysis of the Schmid factors for different deformation modes and the accommodation strains imposed on neighboring grains. It was found that twinning is initiated before DRX. Dynamic recrystallization volume increases with strain rate at a given deformation temperature. At high strain rate, various twin variants are activated to accommodate deformation, leading to the formation of twin intersections and high DRX volume. Fully dynamic recrystallized structure can be obtained at both high and low strain rates due to the high mobility of the grain and twin boundaries at the temperature of 400 °C.

Phase Transformation Study in Nb-Mo Microalloyed Steels Using Dilatometry and EBSD Quantification

NASA Astrophysics Data System (ADS)

Isasti, Nerea; Jorge-Badiola, Denis; Taheri, Mitra L.; Uranga, Pello

2013-08-01

A complete microstructural characterization and phase transformation analysis has been performed for several Nb and Nb-Mo microalloyed low-carbon steels using electron backscattered diffraction (EBSD) and dilatometry tests. Compression thermomechanical schedules were designed resulting in the undeformed and deformed austenite structures before final transformation. The effects of microalloying additions and accumulated deformation were analyzed after CCT diagram development and microstructural quantification. The resulting microstructures ranged from polygonal ferrite and pearlite at slow cooling ranges, to a combination of quasipolygonal ferrite and granular ferrite for intermediate cooling rates, and finally, to bainitic ferrite with martensite for fast cooling rates. The addition of Mo promotes a shift in the CCT diagrams to lower transformation start temperatures. When the amount of Nb is increased, CCT diagrams show little variations for transformations from the undeformed austenite and higher initial transformation temperatures in the transformations from the deformed austenite. This different behavior is due to the effect of niobium on strain accumulation in austenite and its subsequent acceleration of transformation kinetics. This article shows the complex interactions between chemical composition, deformation, and the phases formed, as well as their effect on microstructural unit sizes and homogeneity.

Strain distribution and failure mode of polymer separators for Li-ion batteries under biaxial loading

NASA Astrophysics Data System (ADS)

Kalnaus, Sergiy; Kumar, Abhishek; Wang, Yanli; Li, Jianlin; Simunovic, Srdjan; Turner, John A.; Gorney, Phillip

2018-02-01

Deformation of polymer separators for Li-ion batteries has been studied under biaxial tension by using a dome test setup. This deformation mode provides characterization of separator strength under more complex loading conditions, closer representing deformation of an electric vehicle battery during crash event, compared to uniaxial tension or compression. Two polymer separators, Celgard 2325 and Celgard 2075 were investigated by deformation with spheres of three different diameters. Strains in separators were measured in situ by using Digital Image Correlation (DIC) technique. The results show consistent rupture of separators along the machine direction coinciding with areas of high strain accumulation. The critical first principal strain for failure was independent of the sphere diameter and was determined to be approximately 34% and 43% for Celgard 2325 and Celgard 2075 respectively. These values can be taken as a criterion for internal short circuit in a battery following an out-of-plane impact. A Finite Element (FE) model was built with the anisotropic description of separator behavior, derived from tensile tests in orthogonal directions. The results of simulations predicted the response of separator rather well when compared to experimental results for various sizes of rigid sphere.

Strain distribution and failure mode of polymer separators for Li-ion batteries under biaxial loading

DOE PAGES

Kalnaus, Sergiy; Kumar, Abhishek; Wang, Yanli; ...

2017-12-16

Deformation of polymer separators for Li-ion batteries has been studied under biaxial tension by using a dome test setup. This deformation mode provides characterization of separator strength under more complex loading conditions, closer representing deformation of an electric vehicle battery during crash event, compared to uniaxial tension or compression. Two polymer separators, Celgard 2325 and Celgard 2075 were investigated by deformation with spheres of three different diameters. Strains in separators were measured in situ by using Digital Image Correlation (DIC) technique. The results show consistent rupture of separators along the machine direction coinciding with areas of high strain accumulation. Themore » critical first principal strain for failure was independent of the sphere diameter and was determined to be approximately 34% and 43% for Celgard 2325 and Celgard 2075 respectively. These values can be taken as a criterion for internal short circuit in a battery following an out-of-plane impact. A Finite Element (FE) model was built with the anisotropic description of separator behavior, derived from tensile tests in orthogonal directions. In conclusion, the results of simulations predicted the response of separator rather well when compared to experimental results for various sizes of rigid sphere.« less

A Computational Study of Plastic Deformation in AISI 304 Induced by Surface Mechanical Attrition Treatment

NASA Astrophysics Data System (ADS)

Zhang, X. C.; Lu, J.; Shi, S. Q.

2010-05-01

As a technique of grain refinement process by plastic deformation, surface mechanical attrition treatment (SMAT) has been developed to be one of the most effective ways to optimize the mechanical properties of various materials including pure metals and alloys. SMAT can significantly reduce grain size into nanometer regime in the surface layer of bulk materials, providing tremendous opportunities for improving physical, chemical and mechanical properties of the materials. In this work, a computational modeling of the surface mechanical attrition treatment (SMAT) process is presented, in which Johnson-Cook plasticity model and the finite element method were employed to study the high strain rate, elastic-plastic dynamic process of ball impact on a metallic target. AISI 304 steel with low stacking fault energy was chosen as the target material. First, a random impact model was used to analyze the statistic characteristics of ball impact, and then the plastic deformation behavior and residual stress distribution in AISI 304 stainless steel during SMAT were studied. The simulation results show that the compressive residual stress and vertical deformation of the surface structures were directly affected by ball impact frequency, incident impact angle and ball diameter used in SMAT process.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kalnaus, Sergiy; Kumar, Abhishek; Wang, Yanli

Deformation of polymer separators for Li-ion batteries has been studied under biaxial tension by using a dome test setup. This deformation mode provides characterization of separator strength under more complex loading conditions, closer representing deformation of an electric vehicle battery during crash event, compared to uniaxial tension or compression. Two polymer separators, Celgard 2325 and Celgard 2075 were investigated by deformation with spheres of three different diameters. Strains in separators were measured in situ by using Digital Image Correlation (DIC) technique. The results show consistent rupture of separators along the machine direction coinciding with areas of high strain accumulation. Themore » critical first principal strain for failure was independent of the sphere diameter and was determined to be approximately 34% and 43% for Celgard 2325 and Celgard 2075 respectively. These values can be taken as a criterion for internal short circuit in a battery following an out-of-plane impact. A Finite Element (FE) model was built with the anisotropic description of separator behavior, derived from tensile tests in orthogonal directions. In conclusion, the results of simulations predicted the response of separator rather well when compared to experimental results for various sizes of rigid sphere.« less

New intrinsic mechanism on gum-like superelasticity of multifunctional alloys

PubMed Central

Liu, Jia-Peng; Wang, Yan-Dong; Hao, Yu-Lin; Wang, Yunzhi; Nie, Zhi-Hua; Wang, Dong; Ren, Yang; Lu, Zhao-Ping; Wang, Jinguo; Wang, Haoliang; Hui, Xidong; Lu, Ning; Kim, Moon J.; Yang, Rui

2013-01-01

Ti-Nb-based Gum Metals exhibit extraordinary superelasticity with ultralow elastic modulus, superior strength and ductility, and a peculiar dislocation-free deformation behavior, most of which challenge existing theories of crystal strength. Additionally, this kind of alloys actually displays even more anomalous mechanical properties, such as the non-linear superelastic behavior, accompanied by a pronounced tension-to-compression asymmetry, and large ductility with a low Poisson's ratio. Two main contradictory arguments exist concerning the deformation mechanisms of those alloys, i.e., formation of reversible nanodisturbance and reversible martensitic transformation. Herein we used the in-situ synchrotron high-energy X-ray scattering technique to reveal the novel intrinsic physical origin of all anomalous mechanical properties of the Ti-24Nb-4Zr-8Sn-0.10O alloy, a typical gum-like metal. Our experiments provide direct evidence on two different kinds of interesting, stress-induced, reversible nanoscale martensitic transitions, i.e., the austenitic regions with B2 structure transform to α″ martensite and those with BCC structure transform to δ martensite. PMID:23831664

Characterization and modeling of mechanical behavior of single crystal titanium deformed by split-Hopkinson pressure bar

DOE PAGES

Morrow, B. M.; Lebensohn, R. A.; Trujillo, C. P.; ...

2016-03-28

Single crystal titanium samples were dynamically loaded using split-Hopkinson pressure bar (SHPB) and the resulting microstructures were examined. Characterization of the twins and dislocations present in the microstructure was conducted to understand the pathway for observed mechanical behavior. Electron backscatter diffraction (EBSD) was used to measure textures and quantify twinning. Microstructures were profusely twinned after loading, and twin variants and corresponding textures were different as a function of initial orientation. Focused ion beam (FIB) foils were created to analyze dislocation content using transmission electron microscopy (TEM). Large amounts of dislocations were present, indicating that plasticity was achieved through slip andmore » twinning together. Viscoplastic self-consistent (VPSC) modeling was used to confirm the complex order of operations during deformation. The activation of different mechanisms was highly dependent upon crystal orientation. For [0001] and View the MathML source[101¯1]-oriented crystals, compressive twinning was observed, followed by secondary tensile twinning. Furthermore, dislocations though prevalent in the microstructure, contributed to final texture far less than twinning.« less

The dependence of granular plasticity on particle shape

NASA Astrophysics Data System (ADS)

Murphy, Kieran; Jaeger, Heinrich

Granular materials plastically deform through reworking an intricate network of particle-particle contacts. Some particle rearrangements have only a fleeting effect before being forgotten while others set in motion global restructuring. How particle shape affects local interactions and how those, in turn, influence the nature of the aggregate's plasticity is far from clear, especially in three dimensions. Here we investigate the remarkably wide range of behaviors in the yielding regime, from quiescent flow to violent jerks, depending on particle shape. We study this complex dependence via uniaxial compression experiments on aggregates of 3D-printed particles, and complement stress-strain data with simultaneous x-ray videos and volumetric strain measurements. We find power law distributions of the slip magnitudes, and discuss their universality. Our data show that the multitude of small slips serves to gradually dilate the packing whereas the fewer large ones accompany significant compaction events. Our findings provide new insights into general features of granular materials during plastic deformation and highlight how small changes in particle shape can give rise to drastic differences in yielding behavior.

A 3D dislocation dynamics analysis of the size effect on the strength of [1 1 1] LiF micropillars at 300K and 600K

NASA Astrophysics Data System (ADS)

Chang, Hyung-Jun; Segurado, Javier; Molina-Aldareguía, Jon M.; Soler, Rafael; LLorca, Javier

2016-03-01

The mechanical behavior in compression of [1 1 1] LiF micropillars with diameters in the range 0.5 μm to 2.0 μm was analyzed by means of discrete dislocation dynamics at ambient and elevated temperature. The dislocation velocity was obtained from the Peach-Koehler force acting on the dislocation segments from a thermally-activated model that accounted for the influence of temperature on the lattice resistance. A size effect of the type ‘smaller is stronger’ was predicted by the simulations, which was in quantitative agreement with previous experimental results by the authors [1]. The contribution of the different physical deformation mechanisms to the size effect (namely, nucleation of dislocations, dislocation exhaustion and forest hardening) could be ascertained from the simulations and the dominant deformation mode could be assessed as a function of the specimen size and temperature. These results shed light into the complex interaction among size, lattice resistance and dislocation mobility in the mechanical behavior of μm-sized single crystals.

An Investigation of a Vertical Test Method for Large Deformation Bending of High Strain Composite Laminates

NASA Astrophysics Data System (ADS)

Herrmann, Kelsey M.

Research to date indicates that traditional composite material failure analysis methods are not appropriate for thin laminates in flexure. Thin composite structures subjected to large bending deformations often attain significantly higher strain-to-failure than previously anticipated tensile and compression coupon test data and linear material model assumption predict. At NASA Langley Research Center, a new bend test method is being developed for High Strain Composite (HSC) structures. This method provides an adequate approximation of a pure moment, large deformation bend test for thin-ply, high strain composites to analyze the large strain flexure response of the laminates. The objective of this research was to further develop this new test method to measure the true bending stiffness and strain-to-failure of high strain composite materials. Of primary importance is the ability to characterize composite laminates that are of interest for current NASA deployable structures in both materials and layups. Two separate testing campaigns were performed for the development of the testing procedure. Initially six laminates were bend tested in three different fiber orientations. These laminates were some combination of unidirectional intermediate modulus (IM) carbon, high tenacity (HT) carbon plain weave, and astroquartz plain weave composite materials. The second test campaign was performed as a more detailed look into the simplest composite laminates at thicknesses that better represented deployable boom structures. The second campaign tested three basic, thinner laminates, again in three different fiber orientations. All testing was monotonic loading to failure. The thickness of the laminates tested ranged from 0.166mm (campaign 2) to 0.45mm (campaign 1). The measured strains at failure for the unidirectional material were approximately 2.1% and 1.4% at the compression and tension sides, respectively, failing as fiber tensile fracture. Both of these values differ from what would be expected from considering much thicker coupons tested under pure compression and tension, that show a strain-to-failure of 1.0-1.1% and 1.6-1.7%, respectively. The significant differences in strain values obtained at the outer surfaces of the coupon is thought to be related to the shift in neutral axis that the specimen experiences during the large deformation bending test as a result of fiber material nonlinearities at higher strains. The vertical test nature of the CBT when compared to other test methods proves to be helpful for visually capturing with Digital Image Correlation the distinct behavior of the flexure on both the compressive and tensile sides. It was found that the thinner the laminate tested, the more confirmation of a nonlinear response of this classification of composites. The moment versus curvature curves were predominantly nonlinear resulting in a near linear bending stiffness versus curvature response. At these large strains, carbon fibers are highly nonlinear resulting in the laminate flexure modulus increasing by up to 5x. The theoretical bending stiffness values calculated using Classical Lamination Theory analysis are within small differences with respect to the experimentally measured values: errors of approximately 5-10% for both D11 and D22. The error between the finite element model computed strain response and the experimental values was on average around 22%, with 35% of the laminates and orientation having errors less than 7%. Comparison between CLT, FEA, and experimentation show that the Column Bend Test appears to be a promising candidate for characterization of large deformation bending behavior of thin-ply high strain composite laminates.

Evolution of interphase and intergranular strain in zirconium-niobium alloys during deformation at room temperature

NASA Astrophysics Data System (ADS)

Cai, Song

Zr-2.5Nb is currently used for pressure tubes in the CANDU (CANada Deuterium Uranium) reactor. A complete understanding of the deformation mechanism of Zr-2.5Nb is important if we are to accurately predict the in-reactor performance of pressure tubes and guarantee normal operation of the reactors. This thesis is a first step in gaining such an understanding; the deformation mechanism of ZrNb alloys at room temperature has been evaluated through studying the effect of texture and microstructure on deformation. In-situ neutron diffraction was used to monitor the evolution of the lattice strain of individual grain families along both the loading and Poisson's directions and to track the development of interphase and intergranular strains during deformation. The following experiments were carried out with data interpreted using elasto-plastic modeling techniques: (1) Compression tests of a 100%betaZr material at room temperature. (2) Tension and compression tests of hot rolled Zr-2.5Nb plate material. (3) Compression of annealed Zr-2.5Nb. (4) Cyclic loading of the hot rolled Zr-2.5Nb. (5) Compression tests of ZrNb alloys with different Nb and oxygen contents. The experimental results were interpreted using a combination of finite element (FE) and elasto-plastic self-consistent (EPSC) models. The phase properties and phase interactions well represented by the FE model, the EPSC model successfully captured the evolution of intergranular constraint during deformation and provided reasonable estimates of the critical resolved shear stress and hardening parameters of different slip systems under different conditions. The consistency of the material parameters obtained by the EPSC model allows the deformation mechanism at room temperature and the effect of textures and microstructures of ZrNb alloys to be understood. This work provides useful information towards manufacturing of Zr-2.5Nb components and helps in producing ideal microstructures and material properties for pressure tubes. Also it is helpful in guiding the development of new materials for the next generation of nuclear reactors. Furthermore, the large data set obtained from this study can be used in evaluation and improving current and future polycrystalline deformation models.

Influence of deformation on dolomite rim growth kinetics

NASA Astrophysics Data System (ADS)

Helpa, Vanessa; Rybacki, Erik; Grafulha Morales, Luiz Fernando; Dresen, Georg

2015-04-01

Using a gas-deformation apparatus stacks of oriented calcite (CaCO3) and magnesite (MgCO3) single crystals were deformed at T = 750° C and P = 400 MPa to examine the influence of stress and strain on magnesio-calcite and dolomite (CaMg[CO3]2) growth kinetics. Triaxial compression and torsion tests performed at constant stresses between 7 and 38 MPa and test durations between 4 and 171 hours resulted in bulk strains of 0.03-0.2 and maximum shear strains of 0.8-5.6, respectively. The reaction rims consist of fine-grained (2-7 μm) dolomite with palisade-shaped grains growing into magnesite reactants and equiaxed granular dolomite grains next to calcite. In between dolomite and pure calcite, magnesio-calcite grains evolved with an average grain size of 20-40 μm. Grain boundaries tend to be straighter at high bulk strains and equilibrium angles at grain triple junctions are common within the magnesio-calcite layer. Transmission electron microscopy shows almost dislocation free palisades and increasing dislocation density within granular dolomite towards the magnesio-calcite boundary. Within magnesio-calcite grains, dislocations are concentrated at grain boundaries. Variation of time at fixed stress (˜17 MPa) yields a parabolic time dependence of dolomite rim width, indicating diffusion-controlled growth, similar to isostatic rim growth behavior. In contrast, the magnesio-calcite layer growth is enhanced compared to isostatic conditions. Triaxial compression at given time shows no significant change of dolomite rim thickness (11±2 μm) and width of magnesio-calcite layers (33±5 μm) with increasing stress. In torsion experiments, reaction layer thickness and grain size decrease from the center (low stress/strain) to the edge (high strain/stress) of samples. Chemical analysis shows nearly stoichiometric composition of dolomite palisades, but enhanced Ca content within granular grains, indicating local disequilibrium with magnesio-calcite, in particular for twisted samples. The shift from local equilibrium is ˜3 mol% in triaxial compression and ˜7 mol% in torsion. Electron backscatter diffraction analysis reveals a crystallographic preferred orientation (CPO) within the reaction layers with [0001] axes parallel to the compression/rotation axis and poles of {2-1-10} and {10-10} prismatic planes parallel to the reaction interface. Compared to isostatic annealing, the CPO is more pronounced and the amount of low-angle grain boundaries is increased. At the imposed experimental conditions, most of the bulk deformation is accommodated by calcite single, which is stronger than magnesite. Application of flow laws for magnesio-calcite and dolomite suggest that the fine-grained reaction products should deform by grain boundary diffusion creep, resulting in lower flow strength than the single crystal reactants. However, microstructural observations indicate that deformation of granular dolomite and magnesio-calcite is at least partially assisted by dislocation creep, which would result in an almost similar strength to calcite. Therefore, flattening of the reaction layers during triaxial compression may be counterbalanced by enhanced reaction rates, resulting in almost constant layer thickness, independent of the applied stress. For simple shear, the reduced reaction kinetics in the high stress/strain region of twisted samples may be related to increased nucleation rates, resulting in a lower grain size and rim thickness.

Interfraction Liver Shape Variability and Impact on GTV Position During Liver Stereotactic Radiotherapy Using Abdominal Compression

DOE Office of Scientific and Technical Information (OSTI.GOV)

Eccles, Cynthia L., E-mail: cynthia.eccles@rob.ox.ac.uk; Dawson, Laura A.; Moseley, Joanne L.

2011-07-01

Purpose: For patients receiving liver stereotactic body radiotherapy (SBRT), abdominal compression can reduce organ motion, and daily image guidance can reduce setup error. The reproducibility of liver shape under compression may impact treatment delivery accuracy. The purpose of this study was to measure the interfractional variability in liver shape under compression, after best-fit rigid liver-to-liver registration from kilovoltage (kV) cone beam computed tomography (CBCT) scans to planning computed tomography (CT) scans and its impact on gross tumor volume (GTV) position. Methods and Materials: Evaluable patients were treated in a Research Ethics Board-approved SBRT six-fraction study with abdominal compression. Kilovoltage CBCTmore » scans were acquired before treatment and reconstructed as respiratory sorted CBCT scans offline. Manual rigid liver-to-liver registrations were performed from exhale-phase CBCT scans to exhale planning CT scans. Each CBCT liver was contoured, exported, and compared with the planning CT scan for spatial differences, by use of in house-developed finite-element model-based deformable registration (MORFEUS). Results: We evaluated 83 CBCT scans from 16 patients with 30 GTVs. The mean volume of liver that deformed by greater than 3 mm was 21.7%. Excluding 1 outlier, the maximum volume that deformed by greater than 3 mm was 36.3% in a single patient. Over all patients, the absolute maximum deformations in the left-right (LR), anterior-posterior (AP), and superior-inferior directions were 10.5 mm (SD, 2.2), 12.9 mm (SD, 3.6), and 5.6 mm (SD, 2.7), respectively. The absolute mean predicted impact of liver volume displacements on GTV by use of center of mass displacements was 0.09 mm (SD, 0.13), 0.13 mm (SD, 0.18), and 0.08 mm (SD, 0.07) in the left-right, anterior-posterior, and superior-inferior directions, respectively. Conclusions: Interfraction liver deformations in patients undergoing SBRT under abdominal compression after rigid liver-to-liver registrations on respiratory sorted CBCT scans were small in most patients (<5 mm).« less

Deformation modes in an Icelandic basalt: From brittle failure to localized deformation bands

NASA Astrophysics Data System (ADS)

Adelinet, M.; Fortin, J.; Schubnel, A.; Guéguen, Y.

2013-04-01

According to the stress state, deformation mode observed in rocks may be very different. Even in the brittle part of the crust a differential stress can induce shear failure but also localized compacting deformation, such as compaction bands in porous sedimentary rocks. The mode of deformation controls many hydrodynamic factors, such as permeability and porosity. We investigate in this paper two different modes of deformation in an Icelandic basalt by using laboratory seismological tools (elastic waves and acoustic emissions) and microstructural observations. First of all, we show that at low effective confining pressure (Peff = 5 MPa) an axial loading induces a shear failure in the basalt with an angle of about 30° with respect to the main stress direction. On the contrary, at high effective confining pressure (Peff ≥ 75 MPa and more) an increase of the axial stress induces a localization of the deformation in the form of subhorizontal bands again with respect to the main stress direction. In this second regime, focal mechanisms of the acoustic emissions reveal an important number of compression events suggesting pore collapse mechanisms. Microstructural observations confirm this assumption. Similar compaction structures are usually obtained for porous sedimentary rocks (20-25%). However, the investigated basalt has an initial total porosity of only about 10% so that compaction structures were not expected. The pore size and the ratio of pore to grain size are likely to be key factors for the particular observed mechanical behavior.

The failure of brittle materials under overall compression: Effects of loading rate and defect distribution

NASA Astrophysics Data System (ADS)

Paliwal, Bhasker

The constitutive behaviors and failure processes of brittle materials under far-field compressive loading are studied in this work. Several approaches are used: experiments to study the compressive failure behavior of ceramics, design of experimental techniques by means of finite element simulations, and the development of micro-mechanical damage models to analyze and predict mechanical response of brittle materials under far-field compression. Experiments have been conducted on various ceramics, (primarily on a transparent polycrystalline ceramic, aluminum oxynitride or AlON) under loading rates ranging from quasi-static (˜ 5X10-6) to dynamic (˜ 200 MPa/mus), using a servo-controlled hydraulic test machine and a modified compression Kolsky bar (MKB) technique respectively. High-speed photography has also been used with exposure times as low as 20 ns to observe the dynamic activation, growth and coalescence of cracks and resulting damage zones in the specimen. The photographs were correlated in time with measurements of the stresses in the specimen. Further, by means of 3D finite element simulations, an experimental technique has been developed to impose a controlled, homogeneous, planar confinement in the specimen. The technique can be used in conjunction with a high-speed camera to study the in situ dynamic failure behavior of materials under confinement. AlON specimens are used for the study. The statically pre-compressed specimen is subjected to axial dynamic compressive loading using the MKB. Results suggest that confinement not only increases the load carrying capacity, it also results in a non-linear stress evolution in the material. High-speed photographs also suggest an inelastic deformation mechanism in AlON under confinement which evolves more slowly than the typical brittle-cracking type of damage in the unconfined case. Next, an interacting micro-crack damage model is developed that explicitly accounts for the interaction among the micro-cracks in brittle materials. The model incorporates pre-existing defect distributions and a crack growth law. The damage is defined as a scalar parameter which is a function of the micro-crack density, the evolution of which is a function of the existing defect distribution and the crack growth dynamics. A specific case of a uniaxial compressive loading under constant strain-rate has been studied to predict the effects of the strain-rate, defect distribution and the crack growth dynamics on the constitutive response and failure behavior of brittle materials. Finally, the effects of crack growth dynamics on the strain-rate sensitivity of brittle materials are studied with the help of the micro-mechanical damage model. The results are compared with the experimentally observed damage evolution and the rate-sensitive behavior of the compressive strength of several engineering ceramics. The dynamic failure of armor-grade hot-pressed boron carbide (B 4C) under loading rates of ˜ 5X10-6 to 200 MPa/mus is also discussed.

Testing a thermo-chemo-hydro-geomechanical model for gas hydrate-bearing sediments using triaxial compression laboratory experiments

NASA Astrophysics Data System (ADS)

Gupta, S.; Deusner, C.; Haeckel, M.; Helmig, R.; Wohlmuth, B.

2017-09-01

Natural gas hydrates are considered a potential resource for gas production on industrial scales. Gas hydrates contribute to the strength and stiffness of the hydrate-bearing sediments. During gas production, the geomechanical stability of the sediment is compromised. Due to the potential geotechnical risks and process management issues, the mechanical behavior of the gas hydrate-bearing sediments needs to be carefully considered. In this study, we describe a coupling concept that simplifies the mathematical description of the complex interactions occurring during gas production by isolating the effects of sediment deformation and hydrate phase changes. Central to this coupling concept is the assumption that the soil grains form the load-bearing solid skeleton, while the gas hydrate enhances the mechanical properties of this skeleton. We focus on testing this coupling concept in capturing the overall impact of geomechanics on gas production behavior though numerical simulation of a high-pressure isotropic compression experiment combined with methane hydrate formation and dissociation. We consider a linear-elastic stress-strain relationship because it is uniquely defined and easy to calibrate. Since, in reality, the geomechanical response of the hydrate-bearing sediment is typically inelastic and is characterized by a significant shear-volumetric coupling, we control the experiment very carefully in order to keep the sample deformations small and well within the assumptions of poroelasticity. The closely coordinated experimental and numerical procedures enable us to validate the proposed simplified geomechanics-to-flow coupling, and set an important precursor toward enhancing our coupled hydro-geomechanical hydrate reservoir simulator with more suitable elastoplastic constitutive models.

Behavior of an MBT waste in monotonic triaxial shear tests

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bhandari, Athma Ram, E-mail: athma.bhandari@beg.utexas.edu; Powrie, William, E-mail: w.powrie@soton.ac.uk

2013-04-15

Highlights: ► We studied the stress–strain–strength characteristics of an MBT waste. ► Rate of mobilization of strength with strain depends on initial density. ► Image analysis technique was used to determine whole-specimen displacement fields. ► Initial mode of deformation of a loose specimen is one-dimensional compression. ► Reinforcing elements enhance the resistance to lateral and volumetric deformation. - Abstract: Legislation in some parts of the world now requires municipal solid waste (MSW) to be processed prior to landfilling to reduce its biodegradability and hence its polluting potential through leachate and fugitive emission of greenhouse gases. This pre-processing may be achievedmore » through what is generically termed mechanical–biological-treatment (MBT). One of the major concerns relating to MBT wastes is that the strength of the material may be less than for raw MSW, owing to the removal of sheet, stick and string-like reinforcing elements during processing. Also, the gradual increase in mobilized strength over strains of 30% or so commonly associated with unprocessed municipal solid waste may not occur with treated wastes. This paper describes a series of triaxial tests carried out to investigate the stress–strain–strength characteristics of an MBT waste, using a novel digital image analysis technique for the determination of detailed displacement fields over the whole specimen. New insights gained into the mechanical behavior of MBT waste include the effect of density on the stress–strain response, the initial 1-D compression of lightly consolidated specimens, and the likely reinforcing effect of small sheet like particles remaining in the waste.« less

Effect of material inhomogeneity on the cyclic plastic deformation behavior at the microstructural level: micromechanics-based modeling of dual-phase steel

NASA Astrophysics Data System (ADS)

Paul, Surajit Kumar

2013-07-01

The microstructure of dual-phase (DP) steels typically consists of a soft ferrite matrix with dispersed islands of hard martensite phase. Due to the composite effect of ferrite and martensite, DP steels exhibit a unique combination of strain hardening, strength and ductility. A microstructure-based micromechanical modeling approach is adopted in this work to capture the tensile and cyclic plastic deformation behavior of DP steel. During tensile straining, strain incompatibility between the softer ferrite matrix and the harder martensite phase arises due to a difference in the flow characteristics of these two phases. Microstructural-level inhomogeneity serves as the initial imperfection, triggering strain incompatibility, strain partitioning and finally shear band localization during tensile straining. The local deformation in the ferrite phase is constrained by adjacent martensite islands, which locally results in stress triaxiality development in the ferrite phase. As the martensite distribution varies within the microstructure, the stress triaxiality also varies in a band within the microstructure. Inhomogeneous stress and strain distribution within the softer ferrite phase arises even during small tensile straining because of material inhomogeneity. The magnitude of cyclic plastic deformation within the softer ferrite phase also varies according to the stress distribution in the first-quarter cycle tensile loading. Accumulation of tensile/compressive plastic strain with number of cycles is noted in different locations within the ferrite phase during both symmetric stress and strain controlled cycling. The basic mode of cyclic plastic deformation in an inhomogeneous material is cyclic strain accumulation, i.e. ratcheting. Microstructural inhomogeneity results in cyclic strain accumulation in the aggregate DP material even in symmetric stress cycling.

Variable percolation threshold of composites with fiber fillers under compression

NASA Astrophysics Data System (ADS)

Lin, Chuan; Wang, Hongtao; Yang, Wei

2010-07-01

The piezoresistant effect in conducting fiber-filled composites has been studied by a continuum percolation model. Simulation was performed by a Monte Carlo method that took into account both the deformation-induced fiber bending and rotation. The percolation threshold was found to rise with the compression strain, which explains the observed positive piezoresistive coefficients in such composites. The simulations unveiled the effect of the microstructure evolution during deformation. The fibers are found to align perpendicularly to the compression direction. As the fiber is bended, the effective length in making a conductive network is shortened. Both effects contribute to a larger percolation threshold and imply a positive piezoresistive coefficient according the universal power law.

Preferred orientation in experimentally deformed stishovite: implications for deformation mechanisms

DOE PAGES

Kaercher, Pamela M.; Zepeda-Alarcon, Eloisa; Prakapenka, Vitali B.; ...

2014-11-07

Although the crystal structure of the high pressure SiO 2 polymorph stishovite has been studied in detail, little is known about the development of crystallographic preferred orientation (CPO) during deformation in stishovite. Insight into CPO and associated deformation mechanics of stishovite would provide important information for understanding subduction of quartz-bearing crustal rocks into the mantle. To study CPO development, we converted a natural sample of flint to stishovite in a laser heated diamond anvil cell and compressed the stishovite aggregate up to 38 GPa. We collected diffraction patterns in radial geometry to examine in situ development of crystallographic preferred orientationmore » and find that (001) poles preferentially align with the compression direction. Viscoplastic self-consistent modeling suggests the most likely slip systems at high pressure and ambient temperature are pyramidal and basal slip.« less

Representation of deformable motion for compression of dynamic cardiac image data

NASA Astrophysics Data System (ADS)

Weinlich, Andreas; Amon, Peter; Hutter, Andreas; Kaup, André

2012-02-01

We present a new approach for efficient estimation and storage of tissue deformation in dynamic medical image data like 3-D+t computed tomography reconstructions of human heart acquisitions. Tissue deformation between two points in time can be described by means of a displacement vector field indicating for each voxel of a slice, from which position in the previous slice at a fixed position in the third dimension it has moved to this position. Our deformation model represents the motion in a compact manner using a down-sampled potential function of the displacement vector field. This function is obtained by a Gauss-Newton minimization of the estimation error image, i. e., the difference between the current and the deformed previous slice. For lossless or lossy compression of volume slices, the potential function and the error image can afterwards be coded separately. By assuming deformations instead of translational motion, a subsequent coding algorithm using this method will achieve better compression ratios for medical volume data than with conventional block-based motion compensation known from video coding. Due to the smooth prediction without block artifacts, particularly whole-image transforms like wavelet decomposition as well as intra-slice prediction methods can benefit from this approach. We show that with discrete cosine as well as with Karhunen-Lo`eve transform the method can achieve a better energy compaction of the error image than block-based motion compensation while reaching approximately the same prediction error energy.

Localisation of deformations of the midfacial complex in subjects with class III malocclusions employing thin-plate spline analysis

PubMed Central

SINGH, G. D.; McNAMARA JR, J. A.; LOZANOFF, S.

1997-01-01

This study determines deformations of the midface that contribute to a class III appearance, employing thin-plate spline analysis. A total of 135 lateral cephalographs of prepubertal children of European-American descent with either class III malocclusions or a class I molar occlusion were compared. The cephalographs were traced and checked, and 7 homologous landmarks of the midface were identified and digitised. The data sets were scaled to an equivalent size and subjected to Procrustes analysis. These statistical tests indicated significant differences (P<0.05) between the averaged class I and class III morphologies. Thin-plate spline analysis indicated that both affine and nonaffine transformations contribute towards the total spline for the averaged midfacial configuration. For nonaffine transformations, partial warp 3 had the highest magnitude, indicating the large scale deformations of the midfacial configuration. These deformations affected the palatal landmarks, and were associated with compression of the midfacial complex in the anteroposterior plane predominantly. Partial warp 4 produced some vertical compression of the posterior aspect of the midfacial complex whereas partial warps 1 and 2 indicated localised shape changes of the maxillary alveolus region. Large spatial-scale deformations therefore affect the midfacial complex in an anteroposterior axis, in combination with vertical compression and localised distortions. These deformations may represent a developmental diminution of the palatal complex anteroposteriorly that, allied with vertical shortening of midfacial height posteriorly, results in class III malocclusions with a retrusive midfacial profile. PMID:9449078

Localisation of deformations of the midfacial complex in subjects with class III malocclusions employing thin-plate spline analysis.

PubMed

Singh, G D; McNamara, J A; Lozanoff, S

1997-11-01

This study determines deformations of the midface that contribute to a class III appearance, employing thinplate spline analysis. A total of 135 lateral cephalographs of prepubertal children of European-American descent with either class III malocclusions or a class I molar occlusion were compared. The cephalographs were traced and checked, and 7 homologous landmarks of the midface were identified and digitised. The data sets were scaled to an equivalent size and subjected to Procrustes analysis. These statistical tests indicated significant differences (P < 0.05) between the averaged class I and class III morphologies. Thinplate spline analysis indicated that both affine and nonaffine transformations contribute towards the total spline for the averaged midfacial configuration. For nonaffine transformations, partial warp 3 had the highest magnitude, indicating the large scale deformations of the midfacial configuration. These deformations affected the palatal landmarks, and were associated with compression of the midfacial complex in the anteroposterior plane predominantly. Partial warp 4 produced some vertical compression of the posterior aspect of the midfacial complex whereas partial warps 1 and 2 indicated localised shape changes of the maxillary alveolus region. large spatial-scale deformations therefore affect the midfacial complex in an anteroposterior axis, in combination with vertical compression and localised distortions. These deformations may represent a developmental diminution of the palatal complex anteroposteriorly that, allied with vertical shortening of midfacial height posteriorly, results in class III malocclusions with a retrusive midfacial profile.

Effect of Stress and Strain Path on Cavity Closure During Hot Working of an Alpha/Beta Titanium Alloy (Preprint)

DTIC Science & Technology

2007-07-01

damage totally. 15. SUBJECT TERMS Ti- 6Al - 4V , strain, stress, cavity closure, hot working, titanium alloy 16. SECURITY CLASSIFICATION OF: 17...stress state on deformation and cavitation during hot working of Ti- 6Al - 4V was established via torsion-compression and reversed-torsion tests...strain path and stress state on deformation and cavitation during hot working of Ti- 6Al - 4V was established via torsion-compression and reversed

Temperature Evolution During Plane Strain Compression Of Tertiary Oxide Scale On Steel

NASA Astrophysics Data System (ADS)

Suarez, L.; Vanden Eynde, X.; Lamberigts, M.; Houbaert, Y.

2007-04-01

An oxide scale layer always forms at the steel surface during hot rolling. This scale layer separates the work roll from the metal substrate. Understanding the deformation behaviour and mechanical properties of the scale is of great interest because it affects the frictional conditions during hot rolling and the heat-transfer behaviour at the strip-roll interface. A thin wustite scale layer (<20 μm) was created under controlled conditions in an original laboratory device adequately positioned in a compression testing machine to investigate plane strain compression. Oxidation tests were performed on an ULC steel grade. After the oxide growth at 1050°C, plane strain compression (PSC) was performed immediately to simulate the hot rolling process. PSC experiments were performed at a deformation temperature of 1050°C, with reduction ratios from 5 to 70%, and strain rates of 10s-1 under controlled gas atmospheres. Results show that for wustite, ductility is obvious at 1050°C. Even after deformation oxide layers exhibit good adhesion to the substrate and homogeneity over the thickness. The tool/sample temperature difference seems to be the reason for the unexpected ductile behaviour of the scale layer.

Poisson's Ratio of a Hyperelastic Foam Under Quasi-static and Dynamic Loading

DOE PAGES

Sanborn, Brett; Song, Bo

2018-06-03

Poisson's ratio is a material constant representing compressibility of material volume. However, when soft, hyperelastic materials such as silicone foam are subjected to large deformation into densification, the Poisson's ratio may rather significantly change, which warrants careful consideration in modeling and simulation of impact/shock mitigation scenarios where foams are used as isolators. The evolution of Poisson's ratio of silicone foam materials has not yet been characterized, particularly under dynamic loading. In this study, radial and axial measurements of specimen strain are conducted simultaneously during quasi-static and dynamic compression tests to determine the Poisson's ratio of silicone foam. The Poisson's ratiomore » of silicone foam exhibited a transition from compressible to nearly incompressible at a threshold strain that coincided with the onset of densification in the material. Poisson's ratio as a function of engineering strain was different at quasi-static and dynamic rates. Here, the Poisson's ratio behavior is presented and can be used to improve constitutive modeling of silicone foams subjected to a broad range of mechanical loading.« less

Poisson's Ratio of a Hyperelastic Foam Under Quasi-static and Dynamic Loading

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sanborn, Brett; Song, Bo

Poisson's ratio is a material constant representing compressibility of material volume. However, when soft, hyperelastic materials such as silicone foam are subjected to large deformation into densification, the Poisson's ratio may rather significantly change, which warrants careful consideration in modeling and simulation of impact/shock mitigation scenarios where foams are used as isolators. The evolution of Poisson's ratio of silicone foam materials has not yet been characterized, particularly under dynamic loading. In this study, radial and axial measurements of specimen strain are conducted simultaneously during quasi-static and dynamic compression tests to determine the Poisson's ratio of silicone foam. The Poisson's ratiomore » of silicone foam exhibited a transition from compressible to nearly incompressible at a threshold strain that coincided with the onset of densification in the material. Poisson's ratio as a function of engineering strain was different at quasi-static and dynamic rates. Here, the Poisson's ratio behavior is presented and can be used to improve constitutive modeling of silicone foams subjected to a broad range of mechanical loading.« less

Finite Element Analysis of Aluminum Honeycombs Subjected to Dynamic Indentation and Compression Loads

PubMed Central

Ashab, A.S.M. Ayman; Ruan, Dong; Lu, Guoxing; Bhuiyan, Arafat A.

2016-01-01

The mechanical behavior of aluminum hexagonal honeycombs subjected to out-of-plane dynamic indentation and compression loads has been investigated numerically using ANSYS/LS-DYNA in this paper. The finite element (FE) models have been verified by previous experimental results in terms of deformation pattern, stress-strain curve, and energy dissipation. The verified FE models have then been used in comprehensive numerical analysis of different aluminum honeycombs. Plateau stress, σpl, and dissipated energy (EI for indentation and EC for compression) have been calculated at different strain rates ranging from 102 to 104 s−1. The effects of strain rate and t/l ratio on the plateau stress, dissipated energy, and tearing energy have been discussed. An empirical formula is proposed to describe the relationship between the tearing energy per unit fracture area, relative density, and strain rate for honeycombs. Moreover, it has been found that a generic formula can be used to describe the relationship between tearing energy per unit fracture area and relative density for both aluminum honeycombs and foams. PMID:28773288

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hayashi, T; Morokuma, Keiji; Meunier, Vincent

We have used in-situ current-voltage measurements of cup-stacked carbon nanotubes (CSCNTs) to establish a reversible strain induced (compressive bending) semiconducting to metallic behavior. The corresponding electrical resistance decreases by two orders of magnitude during the process, and reaches values comparable to those of highly crystalline multi-walled carbon nanotube (MWCNT) and graphite. Joule heating experiments on the same CSCNTs showed that the edges of individual cups merge to form loops induced by the heating process. The resistance of these looped CSCNTs was close to that of highly deformed CSCNTs (and crystalline MWCNTs), thus suggesting that a similar conduction mechanism took placemore » in both cases. Using a combination of molecular dynamics and first-principles calculations based on density functional theory, we conclude that an edge-to-edge interlayer transport mechanism results in conduction channels at the compressed side of the CSCNTs due to electronic density overlap between individual cups, thus making CSCNT more conducting. This strain-induced CSCNT semiconductor to metal transition could potentially be applied to enabling functional composite materials (e.g. mechanical sensors) with enhanced and tunable conducting properties upon compression.« less

Power capacity from earcanal dynamic motion

NASA Astrophysics Data System (ADS)

Carioli, Johan; Delnavaz, Aidin; Zednik, Ricardo J.; Voix, Jérémie

2016-12-01

In-ear devices, such as a hearing aids, electronic earplugs, and wearables, need electrical power to operate. Batteries are the current solution, but unfortunately they also create other problems. For example, several hundred million users, mostly elderly, must change their hearing aid batteries on a weekly basis, which represents not only significant financial costs but a negative environmental impact. A promising alternative involves harvesting energy by converting the dynamic jaw movements into electrical energy via the earcanal. The extent that jaw movements distort the earcanal is still unknown, making it difficult to design the appropriate energy harvesting system for the earplug. Moreover, the finite element methods are barely capable to model the behavior of the earcanal distortion because of the complexity of mechanisms that deform the earcanal. However, this paper presents an alternative method, based on analytical considerations, to understand in-ear mechanical quasi-static deformations using earcanal point clouds. This model quantifies the bending and compressive movements of the earcanal. It can therefore be used to select an appropriate deformation mode for harvesting energy from the earcanal's dynamic motion. The value of this approach was illustrated by calculating the obtainable mechanical energy from 12 human subjects. On average, the bending energy in a human earcanal was found to be three times greater than the radial compression energy. This key finding will need to be considered in the design of future in-ear energy harvesting devices. Such an energy harvesting device has the potential to revolutionize the market for in-ear wearable devices and hearing aids by complementing or replacing battery technology.

Mechanisms of High-Temperature Fatigue Failure in Alloy 800H

NASA Technical Reports Server (NTRS)

BhanuSankaraRao, K.; Schuster, H.; Halford, G. R.

1996-01-01

The damage mechanisms influencing the axial strain-controlled Low-Cycle Fatigue (LCF) behavior of alloy 800H at 850 C have been evaluated under conditions of equal tension/compression ramp rates (Fast-Fast (F-F): 4 X 10(sup -3)/s and Slow-Slow (S-S): 4 X 10(sup -5)/s) and asymmetrical ramp rates (Fast-Slow (F-S): 4 x 10(sup -3)/s / 4 X 10(sup -5/s and Slow-Fast (S-F): 4 X 10(sup -5) / 4 X 10(sup -3)/s) in tension and compression. The fatigue life, cyclic stress response, and fracture modes were significantly influenced by the waveform shape. The fatigue lives displayed by different loading conditions were in the following order: F-F greater than S-S greater than F-S greater than S-F. The fracture mode was dictated by the ramp rate adopted in the tensile direction. The fast ramp rate in the tensile direction led to the occurrence of transgranular crack initiation and propagation, whereas the slow ramp rate caused intergranular initiation and propagation. The time-dependent processes and their synergistic interactions, which were at the basis of observed changes in cyclic stress response and fatigue life, were identified. Oxidation, creep damage, dynamic strain aging, massive carbide precipitation, time-dependent creep deformation, and deformation ratcheting were among the several factors influencing cyclic life. Irrespective of the loading condition, the largest effect on life was exerted by oxidation processes. Deformation ratcheting had its greatest influence on life under asymmetrical loading conditions. Creep damage accumulated the greatest amount during the slow tensile ramp under S-F conditions.

Preparation and Dynamic Mechanical Properties at Elevated Temperatures of a Tungsten/Glass Composite

NASA Astrophysics Data System (ADS)

Gao, Chong; Wang, Yingchun; Ma, Xueya; Liu, Keyi; Wang, Yubing; Li, Shukui; Cheng, Xingwang

2018-03-01

Experiments were conducted to prepare a borosilicate glass matrix composite containing 50 vol.% tungsten and examine its dynamic compressive behavior at elevated temperatures in the range of 450-775 °C. The results show that the homogenous microstructure of the tungsten/glass composite with relative density of 97% can be obtained by hot-pressing sintering at 800 °C for 1 h under pressure of 30 MPa. Dynamic compressive testing was carried out by a separate Hopkinson pressure bar system with a synchronous device. The results show that the peak stress decreases and the composite transforms from brittle to ductile in nature with testing temperature increasing from 450 to 750 °C. The brittle-ductile transition temperature is about 500 °C. Over 775 °C, the composite loses load-bearing capacity totally because of the excessive softening of the glass phase. In addition, the deformation and failure mechanism were analyzed.

Deformation Failure Characteristics of Coal Body and Mining Induced Stress Evolution Law

PubMed Central

Wen, Zhijie; Wen, Jinhao; Shi, Yongkui; Jia, Chuanyang

2014-01-01

The results of the interaction between coal failure and mining pressure field evolution during mining are presented. Not only the mechanical model of stope and its relative structure division, but also the failure and behavior characteristic of coal body under different mining stages are built and demonstrated. Namely, the breaking arch and stress arch which influence the mining area are quantified calculated. A systematic method of stress field distribution is worked out. All this indicates that the pore distribution of coal body with different compressed volume has fractal character; it appears to be the linear relationship between propagation range of internal stress field and compressed volume of coal body and nonlinear relationship between the range of outburst coal mass and the number of pores which is influenced by mining pressure. The results provide theory reference for the research on the range of mining-induced stress and broken coal wall. PMID:24967438

Molecular dynamics study of strengthening mechanism of nanolaminated graphene/Cu composites under compression.

PubMed

Weng, Shayuan; Ning, Huiming; Fu, Tao; Hu, Ning; Zhao, Yinbo; Huang, Cheng; Peng, Xianghe

2018-02-15

Molecular dynamics simulations of nanolaminated graphene/Cu (NGCu) and pure Cu under compression are conducted to investigate the underlying strengthening mechanism of graphene and the effect of lamella thickness. It is found that the stress-strain curves of NGCu undergo 3 regimes i.e. the elastic regime I, plastic strengthening regime II and plastic flow regime III. Incorporating graphene monolayer is proved to simultaneously contribute to the strength and ductility of the composites and the lamella thickness has a great effect on the mechanical properties of NGCu composites. Different strengthening mechanisms play main role in different regimes, the transition of mechanisms is found to be related to the deformation behavior. Graphene affected zone is developed and integrated with rule of mixtures and confined layer slip model to describe the elastic properties of NGCu and the strengthening effect of the incorporated graphene.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hou, Huilong; Simsek, Emrah; Stasak, Drew

The stress-induced martensitic phase transformation of shape memory alloys (SMAs) is the basis for elastocaloric cooling. In this paper, we employ additive manufacturing to fabricate TiNi SMAs, and demonstrate compressive elastocaloric cooling in the TiNi rods with transformation latent heat as large as 20 J g -1. Adiabatic compression on as-fabricated TiNi displays cooling ΔT as high as -7.5 °C with recoverable superelastic strain up to 5%. Unlike conventional SMAs, additive manufactured TiNi SMAs exhibit linear superelasticity with narrow hysteresis in stress–strain curves under both adiabatic and isothermal conditions. Microstructurally, we find that there are Ti 2Ni precipitates typically onemore » micron in size with a large aspect ratio enclosing the TiNi matrix. Finally, a stress transfer mechanism between reversible phase transformation in the TiNi matrix and mechanical deformation in Ti 2Ni precipitates is believed to be the origin of the unique superelasticity behavior.« less

Recent results concerning the stability of viscoelastic shear deformable plates under compressive edge loading

NASA Technical Reports Server (NTRS)

Librescu, L.; Chandiramani, N. K.

1989-01-01

Some recent results obtained by the authors are summarized concerning the stability of transversely isotropic flat panels whose materials exhibit a viscoelastic behavior and whose edges are subjected to in-plane biaxial compressive loads. Two transversely isotropic type materials, largely used in advanced technology, are considered: (1) the pyrolytic-graphite type, used in the thermal protection of aerospace vehicles, and (2) the type corresponding to unidirectional fiber-reinforced composites. In the former case, the planes of isotropy are parallel at each point to the midplane of the plate. In the latter case, they are normal to the fiber directions. The micromechanical relations developed by Aboudi (1984, 1986, 1987) are considered in conjunction with the correspondence principle of linear viscoelastic theory in order to predict the macroscopic viscoelastic properties of a material composed of uniaxial elastic fibers embedded in a linear viscoelastic matrix.

Elastocaloric cooling of additive manufactured shape memory alloys with large latent heat

NASA Astrophysics Data System (ADS)

Hou, Huilong; Simsek, Emrah; Stasak, Drew; Hasan, Naila Al; Qian, Suxin; Ott, Ryan; Cui, Jun; Takeuchi, Ichiro

2017-10-01

The stress-induced martensitic phase transformation of shape memory alloys (SMAs) is the basis for elastocaloric cooling. Here we employ additive manufacturing to fabricate TiNi SMAs, and demonstrate compressive elastocaloric cooling in the TiNi rods with transformation latent heat as large as 20 J g-1. Adiabatic compression on as-fabricated TiNi displays cooling ΔT as high as  -7.5 °C with recoverable superelastic strain up to 5%. Unlike conventional SMAs, additive manufactured TiNi SMAs exhibit linear superelasticity with narrow hysteresis in stress-strain curves under both adiabatic and isothermal conditions. Microstructurally, we find that there are Ti2Ni precipitates typically one micron in size with a large aspect ratio enclosing the TiNi matrix. A stress transfer mechanism between reversible phase transformation in the TiNi matrix and mechanical deformation in Ti2Ni precipitates is believed to be the origin of the unique superelasticity behavior.

Mechanical responses, texture evolution, and yield loci of extruded AZ31 magnesium alloy under various loading conditions: Experiment and modeling

NASA Astrophysics Data System (ADS)

Kabirian, Farhoud

Mechanical responses and texture evolution of extruded AZ31 Mg are measured under uniaxial (tension-compression) and multiaxial (free-end torsion) loadings. Compression loading is carried out in three different directions at temperature and strain rate ranges of 77-423 K and 10-4 -3000 s -1, respectively. Texture evolution at different intermediate strains reveals that crystal reorientation is exhausted at smaller strains with increase in strain rate while increase in temperature retards twinning. In addition to the well-known tension-compression yield asymmetry, a strong anisotropy in strain hardening response is observed. Strain hardening during the compression experiment is intensified with decreasing and increasing temperature and strain rate, respectively. This complex behavior is explained through understanding the roles of deformation mechanisms using the Visco-Plastic Self Consistent (VPSC) model. In order to calibrate the VPSC model's constants as accurate as possible, a vast number of mechanical responses including stress-strain curves in tension, compression in three directions, and free-end torsion, texture evolution at different strains, lateral strains of compression samples, twin volume fraction, and axial strain during the torsion experiment. Modeling results show that depending on the number of measurements used for calibration, roles of different mechanisms in plastic deformation change significantly. In addition, a precise definition of yield is established for the extruded AZ31magnesium alloy after it is subjected to different loading conditions (uniaxial to multiaxial) at four different plastic strains. The yield response is measured in ?-? space. Several yield criteria are studied to predict yield response of extruded AZ31. This study proposes an asymmetrical fourth-order polynomial yield function. Material constants in this model can be directly calculated using mechanical measurements. Convexity of the proposed model is discussed, and domains of constants where convexity holds are determined. Effects of grain refinement induced by Equal Channel Angular Pressing, ECAP, on mechanical responses and texture evolution are investigated. Yield strength in compression increases after ECAP, however, strain-hardening rate drops with number of ECAP passes while failure strain increases. Texture measurements reveal the higher propensity to twinning in the extruded material compared with ECAPed magnesium. Calculated Schmid factor maps are utilized to connect the observed mechanical responses to the texture.

Study of non-linear deformation of vocal folds in simulations of human phonation

NASA Astrophysics Data System (ADS)

Saurabh, Shakti; Bodony, Daniel

2014-11-01

Direct numerical simulation is performed on a two-dimensional compressible, viscous fluid interacting with a non-linear, viscoelastic solid as a model for the generation of the human voice. The vocal fold (VF) tissues are modeled as multi-layered with varying stiffness in each layer and using a finite-strain Standard Linear Solid (SLS) constitutive model implemented in a quadratic finite element code and coupled to a high-order compressible Navier-Stokes solver through a boundary-fitted fluid-solid interface. The large non-linear mesh deformation is handled using an elliptic/poisson smoothening technique. Supra-glottal flow shows asymmetry in the flow, which in turn has a coupling effect on the motion of the VF. The fully compressible simulations gives direct insight into the sound produced as pressure distributions and the vocal fold deformation helps study the unsteady vortical flow resulting from the fluid-structure interaction along the full phonation cycle. Supported by the National Science Foundation (CAREER Award Number 1150439).

Semi-regular remeshing based trust region spherical geometry image for 3D deformed mesh used MLWNN

NASA Astrophysics Data System (ADS)

Dhibi, Naziha; Elkefi, Akram; Bellil, Wajdi; Ben Amar, Chokri

2017-03-01

Triangular surface are now widely used for modeling three-dimensional object, since these models are very high resolution and the geometry of the mesh is often very dense, it is then necessary to remesh this object to reduce their complexity, the mesh quality (connectivity regularity) must be ameliorated. In this paper, we review the main methods of semi-regular remeshing of the state of the art, given the semi-regular remeshing is mainly relevant for wavelet-based compression, then we present our method for re-meshing based trust region spherical geometry image to have good scheme of 3d mesh compression used to deform 3D meh based on Multi library Wavelet Neural Network structure (MLWNN). Experimental results show that the progressive re-meshing algorithm capable of obtaining more compact representations and semi-regular objects and yield an efficient compression capabilities with minimal set of features used to have good 3D deformation scheme.

CONSTITUTIVE BEHAVIOR OF AS-QUENCHED Al-Cu-Mn ALLOY

NASA Astrophysics Data System (ADS)

Yang, Xia-Wei; Zhu, Jing-Chuan; Nong, Zhi-Sheng; Ye, Mao; Lai, Zhong-Hong; Liu, Yong

2013-07-01

The hot flow stress of as-quenched Al-Cu-Mn alloy was modeled using the constitutive equations. The as-quenched Al-Cu-Mn alloy were treated with isothermal hot compression tests in the temperature range of 350-500°C, the strain rate range of 0.001-1 s-1. The hyperbolic sine equation was found to be appropriate for flow stress modeling and prediction. Based on the hyperbolic sine equation, a constitutive equation is a relation between 0.2 pct yield stress and deformation conditions (strain rate and deformation temperature) was established. The corresponding hot deformation activation energy (Q) for as-quenched Al-Cu-Mn alloy was determined to be 251.314 kJ/mol. Parameters of constitutive equation of as-quenched Al-Cu-Mn alloy were calculated at different small strains (≤ 0.01). The calculated flow stresses from the constitutive equation are in good agreement with the experimental results. Therefore, this constitutive equation can be used as an accurate temperature-stress model to solve the problems of quench distortion of Al-Cu-Mn alloy parts.

A Comparative Study of Hot Deformation Behaviors for Sand Casting and Centrifugal Casting Q235B Flange Blanks

NASA Astrophysics Data System (ADS)

Qin, Fangcheng; Li, Yongtang; Ju, Li

2017-03-01

Hot compression tests of sand casting and centrifugal casting Q235B flange blanks were performed at strain rate range of 0.01-5 s-1 and temperature range of 850-1,150 °C. The evolutions of microstructure and texture were revealed. The constitutive models based on Arrhenius constitutive modeling were proposed by considering the effects of strain on material constants. The results show that recrystallization in centrifugal casting Q235B is more apparent than that in sand casting, resulting in the finer grains and lower flow stress for centrifugal casting Q235B. The intensities of textures slightly weaken with the increase of temperature. At 1,050 °C and 5 s-1, the textures of sand casting are characterized by strong {001}<100> and {001}<110>, which are related with severe deformation, while the textures of centrifugal casting are composed of {110}<110> and {111}<112>, which are related with dynamic recovery and shear deformation. A good agreement between the predicted and experimental flow stress is achieved and demonstrates that the proposed constitutive models are reliable.

High-Temperature Flow Stress and Recrystallization Characteristics of Al-Bearing Microalloyed TWIP Steels

NASA Astrophysics Data System (ADS)

Somani, Mahesh Chandra; Porter, David A.; Hamada, Atef S.; Karjalainen, L. Pentti

2015-11-01

In this study, the effects of microalloying (Nb,V) and aluminum on the constitutive flow behavior and static recrystallization (SRX) characteristics of microalloyed TWIP steels (Fe-20Mn-0.6C-Al-(Nb,V)) have been investigated under hot deformation conditions. Compression tests in a Gleeble simulator, including the double-hit technique, enabled the acquisition of flow stress and recrystallization data. These were analyzed to determine the powers of strain and strain rate as well as the activation energies of deformation and recrystallization ( Q def and Q rex). Aluminum increased the flow stress and activation energy of deformation and delayed the onset of dynamic recrystallization of microalloyed TWIP steels. While microalloying with V up to 0.3 pct seems to have little or no effect on the SRX kinetics, microalloying with 0.026 pct Nb significantly slowed down the SRX rate, similarly as in the case of low C-Mn steels. Addition of high aluminum (4.9 pct) marginally retarded the SRX kinetics in comparison with the steels with low aluminum (1.5 pct), with or without microalloying with V.

Quasi-static Tensile and Compressive Behavior of Nanocrystalline Tantalum based on Miniature Specimen Testing—Part I: Materials Processing and Microstructure

NASA Astrophysics Data System (ADS)

Ligda, J.; Scotto D'Antuono, D.; Taheri, M. L.; Schuster, B. E.; Wei, Q.

2016-11-01

Grain size reduction of metals into ultrafine-grained (UFG, grain size 100 nm < d < 1000 nm) and nanocrystalline (NC, d < 100 nm) regimes results in considerable increase in strength along with other changes in mechanical behavior such as vanishing strain hardening and limited ductility. Severe plastic deformation (SPD) has been among the favored technologies for the fabrication of UFG/NC metals. Primary past research efforts on SPD UFG/NC metals have been focused on easy-to-work metals, especially face-centered cubic metals such as copper, nickel, etc., and the limited efforts on body-centered cubic metals have mainly focused on high strain rate behavior where these metals are shown to deform via adiabatic shear bands. Except for the work on Fe, only a few papers can be found associated with UFG/NC refractory metals. In the first part of the present work (Part I), high-pressure torsion (HPT) is used to process UFG/NC tantalum, a typical refractory metal. The microstructure of the HPT disk as a function of radial location as well as orientation will be examined. In the subsequent part (Part II), the location-specific mechanical behavior will be presented and discussed. It is suggested that refractory metals such as Ta are ideal to employ SPD technology for microstructure refinement because of the extremely high melting point and relatively good workability.

Investigation on Hot Workability of Homogenized Al-Zn-Mg-Cu Alloy Based on Activation Energy and Processing Map

NASA Astrophysics Data System (ADS)

Peng, Xiaoyan; Su, Wusen; Xiao, Dan; Xu, Guofu

2018-06-01

Hot deformation behaviors of the homogenized Al-Zn-Mg-Cu alloy were studied by uniaxial compression tests carried out at 623-743 K and strain rates of 0.01-10 s-1. The constitutive equation was developed for the activation energy, and thus the activation energy map was constructed. During the hot deformation, the dominated softening mechanisms were the dynamic recovery and dynamic recrystallization, which were most likely to be driven with increasing temperature and decreasing activation energy. Based on the superposition of the activation energy map and the processing map, together with the microstructure characteristics, the optimized hot workability of the alloy was proposed at the domain (670-743 K and 0.01-0.16 s-1), where the peak efficiency was 0.39 and the activation energy range was 196-260 kJ mol-1.

Viscoelasticity and plasticity mechanisms of human dentin

NASA Astrophysics Data System (ADS)

Borodin, E. N.; Seyedkavoosi, S.; Zaitsev, D.; Drach, B.; Mikaelyan, K. N.; Panfilov, P. E.; Gutkin, M. Yu.; Sevostianov, I.

2018-01-01

Theoretical models of viscoelastic behavior and plastic deformation mechanisms of human dentin are considered. Using the linear viscoelasticity theory in which creep and relaxation kernels have the form of fraction-exponential functions, numerical values of instantaneous and long-time Young's moduli and other characteristics of dentin viscoelasticity under uniaxial compression are found. As dentin plastic deformation mechanisms, mutual collagen fiber sliding in the region of contact of their side surfaces, separation of these fibers from each other, and irreversible tension of some collagen fibers, are proposed. It is shown that the second mechanism activation requires a smaller stress than that for activating others. The models of plastic zones at the mode I crack tip, which correspond to these mechanisms, are studied. It is shown that the plastic zone size can increase from a few hundreds of nanometers to hundreds of micrometers with increasing applied stress.

Mammogram registration using the Cauchy-Navier spline

NASA Astrophysics Data System (ADS)

Wirth, Michael A.; Choi, Christopher

2001-07-01

The process of comparative analysis involves inspecting mammograms for characteristic signs of potential cancer by comparing various analogous mammograms. Factors such as the deformable behavior of the breast, changes in breast positioning, and the amount/geometry of compression may contribute to spatial differences between corresponding structures in corresponding mammograms, thereby significantly complicating comparative analysis. Mammogram registration is a process whereby spatial differences between mammograms can be reduced. Presented in this paper is a nonrigid approach to matching corresponding mammograms based on a physical registration model. Many of the earliest approaches to mammogram registration used spatial transformations which were innately rigid or affine in nature. More recently algorithms have incorporated radial basis functions such as the Thin-Plate Spline to match mammograms. The approach presented here focuses on the use of the Cauchy-Navier Spline, a deformable registration model which offers approximate nonrigid registration. The utility of the Cauchy-Navier Spline is illustrated by matching both temporal and bilateral mammograms.

Influence of creep damage on the low cycle thermal-mechanical fatigue behavior of two tantalum base alloys

NASA Technical Reports Server (NTRS)

Sheffler, K. D.; Doble, G. S.

1972-01-01

Low cycle fatigue tests have been performed on the tantalum base alloys T-111 and ASTAR 811C with synchronized, independently programmed temperature and strain cycling. The thermal-mechanical cycles applied fell into three basic categories: these were isothermal cycling, in-phase thermal cycling, and out-of-phase thermal cycling. In-phase cycling was defined as tensile deformation associated with high temperature and compressive deformation with low temperature, while out-of-phase thermal cycling was defined as the reverse case. The in-phase thermal cycling had a pronounced detrimental influence on the fatigue life of both alloys, with the life reduction being greater in the solid solution strengthened T-111 alloy than in the carbide strengthened ASTAR 811C alloy. The out-of-phase tests also showed pronounced effects on the fatigue life of both alloys, although not as dramatic.

Verification of the FBR fuel bundle-duct interaction analysis code BAMBOO by the out-of-pile bundle compression test with large diameter pins

NASA Astrophysics Data System (ADS)

Uwaba, Tomoyuki; Ito, Masahiro; Nemoto, Junichi; Ichikawa, Shoichi; Katsuyama, Kozo

2014-09-01

The BAMBOO computer code was verified by results for the out-of-pile bundle compression test with large diameter pin bundle deformation under the bundle-duct interaction (BDI) condition. The pin diameters of the examined test bundles were 8.5 mm and 10.4 mm, which are targeted as preliminary fuel pin diameters for the upgraded core of the prototype fast breeder reactor (FBR) and for demonstration and commercial FBRs studied in the FaCT project. In the bundle compression test, bundle cross-sectional views were obtained from X-ray computer tomography (CT) images and local parameters of bundle deformation such as pin-to-duct and pin-to-pin clearances were measured by CT image analyses. In the verification, calculation results of bundle deformation obtained by the BAMBOO code analyses were compared with the experimental results from the CT image analyses. The comparison showed that the BAMBOO code reasonably predicts deformation of large diameter pin bundles under the BDI condition by assuming that pin bowing and cladding oval distortion are the major deformation mechanisms, the same as in the case of small diameter pin bundles. In addition, the BAMBOO analysis results confirmed that cladding oval distortion effectively suppresses BDI in large diameter pin bundles as well as in small diameter pin bundles.

Hot Deformation Behavior and Processing Maps of Diamond/Cu Composites

NASA Astrophysics Data System (ADS)

Zhang, Hongdi; Liu, Yue; Zhang, Fan; Zhang, Di; Zhu, Hanxing; Fan, Tongxiang

2018-03-01

The hot deformation behaviors of 50 vol pct uncoated and Cr-coated diamond/Cu composites were investigated using hot isothermal compression tests under the temperature and strain rate ranging from 1073 K to 1273 K (800 °C to 1000 °C) and from 0.001 to 5 s-1, respectively. Dynamic recrystallization was determined to be the primary restoration mechanism during deformation. The Cr3C2 coating enhanced the interfacial bonding and resulted in a larger flow stress for the Cr-coated diamond/Cu composites. Moreover, the enhanced interfacial affinity led to a higher activation energy for the Cr-coated diamond/Cu composites (238 kJ/mol) than for their uncoated counterparts (205 kJ/mol). The strain-rate-dependent constitutive equations of the diamond/Cu composites were derived based on the Arrhenius model, and a high correlation (R = 0.99) was observed between the calculated flow stresses and experimental data. With the help of processing maps, hot extrusions were realized at 1123 K/0.01 s-1 and 1153 K/0.01 s-1 (850 °C/0.01 s-1 and 880 °C/0.01 s-1) for the uncoated and coated diamond/Cu composites, respectively. The combination of interface optimization and hot extrusion led to increases of the density and thermal conductivity, thereby providing a promising route for the fabrication of diamond/Cu composites.

Hot Deformation and Processing Window Optimization of a 70MnSiCrMo Carbide-Free Bainitic Steel.

PubMed

Han, Ying; Sun, Yu; Zhang, Wei; Chen, Hua

2017-03-21

The hot deformation behavior of a high carbon carbide-free bainitic steel was studied through isothermal compression tests that were performed on a Gleeble-1500D thermal mechanical simulator at temperatures of 1223-1423 K and strain rates of 0.01-5 s -1 . The flow behavior, constitutive equations, dynamic recrystallization (DRX) characteristics, and processing map were respectively analyzed in detail. It is found that the flow stress increases with increasing the strain rate and decreases with increasing the temperature, and the single-peak DRX can be easily observed at high temperatures and/or low strain rates. The internal relationship between the flow stress and processing parameters was built by the constitutive equations embracing a parameter of Z/A, where the activation energy for hot deformation is 351.539 kJ/mol and the stress exponent is 4.233. In addition, the DRX evolution and the critical conditions for starting DRX were discussed. Then the model of the DRX volume fraction was developed with satisfied predictability. Finally, the processing maps at different strains were constructed according to the dynamic material model. The safety domains and flow instability regions were identified. The best processing parameters of this steel are within the temperature range of 1323-1423 K and strain rate range of 0.06-1 s -1 .

Hot Deformation Behavior and Processing Maps of Diamond/Cu Composites

NASA Astrophysics Data System (ADS)

Zhang, Hongdi; Liu, Yue; Zhang, Fan; Zhang, Di; Zhu, Hanxing; Fan, Tongxiang

2018-06-01

The hot deformation behaviors of 50 vol pct uncoated and Cr-coated diamond/Cu composites were investigated using hot isothermal compression tests under the temperature and strain rate ranging from 1073 K to 1273 K (800 °C to 1000 °C) and from 0.001 to 5 s-1, respectively. Dynamic recrystallization was determined to be the primary restoration mechanism during deformation. The Cr3C2 coating enhanced the interfacial bonding and resulted in a larger flow stress for the Cr-coated diamond/Cu composites. Moreover, the enhanced interfacial affinity led to a higher activation energy for the Cr-coated diamond/Cu composites (238 kJ/mol) than for their uncoated counterparts (205 kJ/mol). The strain-rate-dependent constitutive equations of the diamond/Cu composites were derived based on the Arrhenius model, and a high correlation ( R = 0.99) was observed between the calculated flow stresses and experimental data. With the help of processing maps, hot extrusions were realized at 1123 K/0.01 s-1 and 1153 K/0.01 s-1 (850 °C/0.01 s-1 and 880 °C/0.01 s-1) for the uncoated and coated diamond/Cu composites, respectively. The combination of interface optimization and hot extrusion led to increases of the density and thermal conductivity, thereby providing a promising route for the fabrication of diamond/Cu composites.

Unusual plastic deformation and damage features in titanium: Experimental tests and constitutive modeling

NASA Astrophysics Data System (ADS)

Revil-Baudard, Benoit; Cazacu, Oana; Flater, Philip; Chandola, Nitin; Alves, J. L.

2016-03-01

In this paper, we present an experimental study on plastic deformation and damage of polycrystalline pure HCP Ti, as well as modeling of the observed behavior. Mechanical characterization data were conducted, which indicate that the material is orthotropic and displays tension-compression asymmetry. The ex-situ and in-situ X-ray tomography measurements conducted reveal that damage distribution and evolution in this HCP Ti material is markedly different than in a typical FCC material such as copper. Stewart and Cazacu (2011) anisotropic elastic/plastic damage model is used to describe the behavior. All the parameters involved in this model have a clear physical significance, being related to plastic properties, and are determined from very few simple mechanical tests. It is shown that this model predicts correctly the anisotropy in plastic deformation, and its strong influence on damage distribution and damage accumulation. Specifically, for a smooth axisymmetric specimen subject to uniaxial tension, damage initiates at the center of the specimen, and is diffuse; the level of damage close to failure being very low. On the other hand, for a notched specimen subject to the same loading the model predicts that damage initiates at the outer surface of the specimen, and further grows from the outer surface to the center of the specimen, which corroborates with the in-situ tomography data.

Hot Deformation and Processing Window Optimization of a 70MnSiCrMo Carbide-Free Bainitic Steel

PubMed Central

Han, Ying; Sun, Yu; Zhang, Wei; Chen, Hua

2017-01-01

The hot deformation behavior of a high carbon carbide-free bainitic steel was studied through isothermal compression tests that were performed on a Gleeble-1500D thermal mechanical simulator at temperatures of 1223–1423 K and strain rates of 0.01–5 s−1. The flow behavior, constitutive equations, dynamic recrystallization (DRX) characteristics, and processing map were respectively analyzed in detail. It is found that the flow stress increases with increasing the strain rate and decreases with increasing the temperature, and the single-peak DRX can be easily observed at high temperatures and/or low strain rates. The internal relationship between the flow stress and processing parameters was built by the constitutive equations embracing a parameter of Z/A, where the activation energy for hot deformation is 351.539 kJ/mol and the stress exponent is 4.233. In addition, the DRX evolution and the critical conditions for starting DRX were discussed. Then the model of the DRX volume fraction was developed with satisfied predictability. Finally, the processing maps at different strains were constructed according to the dynamic material model. The safety domains and flow instability regions were identified. The best processing parameters of this steel are within the temperature range of 1323–1423 K and strain rate range of 0.06–1 s−1. PMID:28772678

Micromechanics of plastic deformation and phase transformation in a three-phase TRIP-assisted advanced high strength steel: Experiments and modeling

NASA Astrophysics Data System (ADS)

Srivastava, Ankit; Ghassemi-Armaki, Hassan; Sung, Hyokyung; Chen, Peng; Kumar, Sharvan; Bower, Allan F.

2015-05-01

The micromechanics of plastic deformation and phase transformation in a three-phase advanced high strength steel are analyzed both experimentally and by microstructure-based simulations. The steel examined is a three-phase (ferrite, martensite and retained austenite) quenched and partitioned sheet steel with a tensile strength of 980 MPa. The macroscopic flow behavior and the volume fraction of martensite resulting from the austenite-martensite transformation during deformation were measured. In addition, micropillar compression specimens were extracted from the individual ferrite grains and the martensite particles, and using a flat-punch nanoindenter, stress-strain curves were obtained. Finite element simulations idealize the microstructure as a composite that contains ferrite, martensite and retained austenite. All three phases are discretely modeled using appropriate crystal plasticity based constitutive relations. Material parameters for ferrite and martensite are determined by fitting numerical predictions to the micropillar data. The constitutive relation for retained austenite takes into account contributions to the strain rate from the austenite-martensite transformation, as well as slip in both the untransformed austenite and product martensite. Parameters for the retained austenite are then determined by fitting the predicted flow stress and transformed austenite volume fraction in a 3D microstructure to experimental measurements. Simulations are used to probe the role of the retained austenite in controlling the strain hardening behavior as well as internal stress and strain distributions in the microstructure.